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HomeMy WebLinkAboutWQ0016376_Monitoring - 12-2023_20240312Monitoring Report Submittal Permit Number#* WQ0016376 Name of Facility:* S&J VILLARI LIVESTOCK PROCESSING FACILITY - WARSAW Month: * December Year: * 2023 Report Information Type* Upload Document* NDMR, NDAR-1, NDAR-2, NDMLR wwt Dec. 2023.pdf 7.62MB PDF Only Please upload one PDF containing all applicable monitoring reports (i.e., NDMR, NDAR-1, NDAR-2, NDMLR, GW-59). Confirmation Email Address: * gerald.m@vfgmail.com Name of Submitter: * Gerald Matthews Signature: Date of submittal: 3/12/2024 This will be filled in automatically Initial Review Reviewer: Wanda.Gerald Is the project number correct?* W00016376 Is the monitoring report accepted?* Yes NO Regional Office* Wilmington Reviewer: _anonymous Review Date: 3/15/2024 FORMNUMP, 03-12 NON -DISCHARGE IbiONITORING REPORT (NDMR) Faye _L of Permit No.: WQ0016376 Facility Name: S&J Villari Livestock Processing Facility-Warsa County: Duplin Month: December t Year: 2023 PPI: 001 Flow Measuring Point: � Influent C Effluent ' No flofi generated Parameter MonitoringPoint: Influent Lf Effluent _ Groundrara- Lowering Cl Surface Water Parameter Code - 11- c 50050 00310 00940 50060 31616 00610 00625 00620 00600 - 00400 00665 70300 00530 O> m .` ¢ E O m E - n O O m U @ U °°.m ° N I = U m mc Q t (0 c ° .M z 1°- ° ` c y a� o La FZ a vom in �CC! 0t.- O -v7aam, c°U m0 y° rn 1 2 3 4 24-hr 07:00 07:00 08:00 07:00 hrs 10 4 2 10 GPD 67,644 19,670 14,310 79,371 mg/L mg/L mg/L 1 *100 mL mg/L mg/L mg/L mg/L su mg/L mg/L mg/L 5 6 7 8 9 07:00 07:00 07:00 0700 07:00 10 10 10 10 10 82,039 79,048 82.357 88,528 65,199 63 <0.1 7.45 10 11 12 14:00 07:00 07:00 2 10 10 36,900 88,069 84,162 13 07.00 1 D 81,590 114 7 77 14 07:00 10 77,239 <0,1 7.2 15 16 17 07:00 07:00 07:00 10 10 10 77,986 18,251 82,716 309 43 112000 139 404 1.28 4.5 7.28 18.8 276 4200 18 19 07:00 07:00 10 10 88,280 81,230 48 7.4 20 0700 10 10 10 $3,256 80,230 76,810 <0.10 7.3 LOT 0 1 5,200 5,410 0 10 9,530 79,505 28 07:00 10 10 84,423 82.831 72 <0.10 7.51 29 30 07:00 0700 10 10442663 81,281 2 31 00:00 00 Average:34 Daily Maximum:8 Daily Minimum:0 Sampling Type: Monthly Avg. Limit: Recorder 100.260 309.00 309.00 309.00 Grab 68.00 114.00 43.00 Grab 0.00 0.10 0.10 Grab #### Grab 139.00 139.00 139.00 1 Grab 404.00 404.00 404.00 1 Grab 1.28 1.28 1.28 Grab 4.50 4.50 4.50 Grab 7.77 720 Grab 18.80 18.80 18.80 Grab 276.00 4.200.00 276.00 4,200.00 276.00 Grab 4,200.00 Grab Daily Limit: Sample Frequency: Recorder Month;y Monthly I nncnth;y Monthly Moithly Monthly �Aontr,;y Monthly rdio-rriy h,1onthiy FORM: NDMR 03-12 NON -DISCHARGE MONITORING REPORT (NDMR) Page '?i _ of q Permit No.: WQ0016376 Facility Name: S&J Villari Livestock Processing Facility-WarsaT county: Duplin Month: December Year: 2023 PPI: 002 Flow Measuring Point: Influent _. Effluent ` No flow generated Parameter Monitoring Point: Influent LEffluent ,_ Groundwater Lowering Surface Water Parameter Code — 0 50050 00625 00610 00620 00665 31616 00600 > ra m < E U 0 c 0 i- to U O 0- m Y N 0 2 F.. c E E < 2 N o O N ~ p s a E d 0 t+- O U w O O` F 1' 2 24-hr hrs GPO mg/L mg/L mg/L mg/L #/100 mL mg/L 1 07:00 10 67,644 2 07:00 4 19,670 3 08:00 2 14,310 4 07:00 10 79,371 5 07:00 10 82,039 6 07:00 10 79,048 7 07:00 10 82,357 8 07:00 10 88,528 9 07:00 10 65,199 10 14:00 2 36,900 11 07:00 10 88,069 — 12 07:00 10 84,162 13 07:00 10 81,590 14 07:00 10 77,239 15 07:00 10 77,986 0.7 <0.2 <0.02 0,92 59 0.7 16 07:00 10 18,251 17 07:00 10 82,716 18 07:00 10 88,280 19 07:00 10 81,230 20 07:00 10 83.256 21 07:00 10 80.230 22 07:00 10 76,810 23 00:00 0 5,200 24jO 2:00 1 5,410 2500:00 0 9,530 267:00 10 79$05 277:00 10 84,423 28 07:00 10 82,831 29 07:00 10 81,281 30 07:00 10 63.632 31 00:00 0 4,260 Average: 62,934 0.70 0.00 0.00 0.92 59.00 0.70 Daily Maximum: 88,528 0.70 0.20 0.02 0.92 59.00 0.70 Daily Minimum: 4.260 0.70 0.20 0.02 0.92 59.00 0.70 Sampling Type: Recorder Grab Grab Grab Grab Grab Monthly Avg. Limit: Daily Limit: Sample Frequency: Recorder Mortriy Monthly Mon, •-Ay Monthly Monthly __ FORM. NDMR 03-12 NON -DISCHARGE MONITORING REPORT (NDMR) Page 1 of Permit No.: WQ0016376 Facility Name: S&J Villari Livestock Processing Facility-Warsa county: Duplin Month: December Year: 2023 PPI: 003 Flow Measuring Point: Influent L Effluent _ No flow generated Parameter Monitoring Point: Influent Effluent ( Groundwater Lowering _Surface Water Parameter Code 0 50050 00625 00610 00620 00665 31616 00600 N O m 2 , Y Z . ~p� e a So� �� 0 ~pO Z 24-hr I hrs GPD mg/L mg/L mg/L mg/L #/100 mL mg/L 1 07:00 10 67,644 2 07:00 4 19,670 3 08:00 2 14,310 4 07:00 10 79.371 5 07:00 10 82,039 6M07:OO1 79,048 782,357 888,528 965,199 10 14:00 2 36,900 11 07:00 10 88,069 12 07:00 10 84,162 13 07:00 10 81,590 14 07:00 10 77,239 15 07:00 10 77,986 1.4 1.1 0.18 0.65 410 1.58 16 07:00 10 18,251 17 07:00 10 82,716 18 07:00 10 88,280 19 07:00 10 81,230 20 07:00 10 83,256 21 07:00 10 80,230 22 07:00 10 76.810 23 00:00 0 5.200 24 12:00 1 5.410 25 00:00 0 9,530 26 07:00 10 79,505 27 07:00 10 $4,423 28 07:00 10 82.831 — 29 07:00 10 81,281 30 07:00 10 63,632 31 00:00 0 4,260 Average: 62,934 1.40 1.10 0.18 0.65 410.00 1.58 Daily Maximum: 88,528 1.40 1.10 0.18 0.65 410.00 1.58 Daily Minimum: 4,260 1 40 1.10 0.18 0.65 410.00 1.58 Sampling Type: Recorder Grab Grab Grab Grab Grab Monthly Avg. Limit: Daily Limit: Sample Frequency: Recorder f_lccth'; Monthly Monthly Monthly Monthly — — FORM: NDMR 03-12 NON -DISCHARGE MONITORING REPORT (NDMR) Page of Sampling Person(s) Name: GERALD LAMAR MATTHEWS Name: Certified Laboratories Name: Environmentat Chemists INC. Name: Water Agricultural Laboratories uoes all monitoring data and sampling frequencies meet the requirements in Attachment A of your permit? ❑ Compliant ❑ Non -Compliant If the facility is non -compliant, please explain in the space below the reason(s) the facility was not in compliance. Provide in your explanation the date(s) of the non-compliance and describe the corrective action(s) taken. Attach additional sheets if necessary. Operator in Responsible Charge (ORC) Certification ORC: GERALD LAMAR MATTHEWS Certification No.: 993131 I Grade: SI Phone Number: 910-289-7500 Has the ORC changed since the previous NDMR? PI yes ❑ No x'2 Y- Signature Date By this signature, I certify that this report is accurrate and complete to the best of my knowledge. Permittee Certification Permittee: SAM VILLARI Signing Official: Signing Official's Title: OWNER Phone Number: 910-293-2157 Permit Expiration: 11/30/2025 Signature Date I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that all qualified personnel properly gathered and evaluated the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete- I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations. Mail Original and Two Copies to: Division of Water Quality Information Processing Unit 1617 Mail Service Center Raleigh, North Carolina 27699-1617 FORM: NDAR-1 08-11 NON -DISCHARGE APPLICATION REPORT (NDAR-1) Page 4- of to Permit No.: W00016376 Facility Name: S&J Villari Livestock Processing Facility -Warsaw County: Duplin Month: December Year: 2023 Did irrigation occur Field Name: 1 Field Name: 2 Field Name: 3 Field Name: 4 at this facility? Area (acres): 0.65 -- Area (acres): 1.16 Area (acres): 1.12 Area (acres): 1.07 over Crop: Coastal Bermuda Cover Crop: Coastal Bermuda Cover Crop: Coastal Bermuda over Crop: Coastal Bermuda YES NO Hourly Rate (in): 0.6 Hourly Rate (in): 0.6 Hourly Rate (in): 0.6 Hourly Rate (in): 0.6 Annual Rate (in): 41.96 Annual Rate (in): 41.96 Annual Rate (in): 41.96 Annual Rate (in): 41.96 Weather Freeboard Field Irrigated? [j YES ❑ No Field Irrigated? - YES NO Field Irrigated? Yes C NO Field Irrigated. - - YES _ NO ❑ U o % Q- a E ` ~ a o rn o rn` rn m o _ "� ~ a 0 o y Q m E m rn i= .`� > rn ,� V ❑ m .,J = �, r E v x o m = J m m a � Q m E m a� ~ rn a ❑ J E T £ a co = J y v Q � Q ti E m rn ~ _`. rn m a ❑ J E o� � E 3 0 t6 2 .J g m E 2� a 0 CLi Q a _E m ~ rn ❑ O _ E rn E v m = � 1 C 2 CL °F in in 78 in 60 gal 8,146 min 23 in 0.46 in 0.46 gal 14,538 min 42 in 0.46 in 0.46 gal 14,037 min 40 in 0.46 in 0.46 gal 13.410 min 39 in 0.46 m 0.46 3 R 0.04 4 5 6 7 8 9 CL C C C C R 1 7,377 4,324 4,637 6,948 3,849 23 0.42 12 0.25 12 0.26 21 0.39 12 0.22 0.42 0.25 0.26 0.39 0.22 13,166 7,716 8,275 12,400 6.868 42 21 21 38 21 0.42 0.24 0.26 0.39 0.22 0.42 0.24 0.26 0.39 0.22 12,712 7,450 7,990 11,973 6,631 40 20 20 36 20 0.42 0.24 0.26 0.39 0.22 0.42 0.24 0.26 0.39 0,22 12.144 7.118 7,633 11.438 6.335 39 0.42 0.42 19 0.25 0.25 19 0.26 0.26 35 0.39 0.39 19 0.22 0.22 10 C 11 12 13 C C C 3.815 8,110 12 23 0.22 0.46 0.22 0.46 6.808 14.474 21 42 0.22 OA6 0.22 0.46 6,574 13,975 20 40 022 0.46 0.22 0.46 6,280 13,351 19 0.22 0.22 39 0.46 0.46 14 C 15 C 16 CL 17 R 5.5 18 CL 19 C 20 C 21 C 22 C 23 C 24 C 25 CL 26 CL 27 R 0.07 28 C 29 CL 30 C - 31 C 48 72 Monthly Loading: 47,206 2.67 84 245 2.67 g1,342 267 267 12 Month Floating Total (in): 24 45 24.a5 V _ FORM: NDAR-1 08-11 NON -DISCHARGE APPLICATION REPORT (NDAR-1) Page Z of Permit No.: WQ0016376 Facility Name: S&J Villari Livestock Processing Facility -Warsaw county: Duplin Month: December Year: 2023 Did irrigation occur Field Name: 5 Field Name: 6 Field Name: 7 Field Name:WalBe at this facility? Area (acres): 1.19 Area (acres): 1.17 Area (acres): Area (acres): Cover Crop: Coastal Bermuda Cover Crop: Coastal Bermuda Cover Crop:�CoEastalrmuda Cover Crop: ! YES No Hourly Rate (in): 0.6 Hourly Rate (in): 0.6 Hourly Rate (in): 0.6 Hourly Rate (in): Annual Rate (in): 41.96 Annual Rate (in): 41.96 Annual Rate (in): 41.96 Annual Rate (in): Weather Freeboard Field Irrigated? YES ❑ No Field Irrigated? Q✓ YES l No Field Irrigated? J YES J No Field Irrigated? ,� U CD m m ° c o M Qrn� c m °oa cc ° m o x H EL o 0- m E@ F •� rn � i3 ° �' E w a x o Ea aim � Q E� o a Q1 c 3Lc ,� o E� ''D >< o M Ed � a yd E go Tom' v M m _ Env m =• Q. m@ E '@ o J E c � J 1 C 2 CL °F in in 78 in 60 gal 14,914 min 43 in 0.46 in 1 0.46 gal 14.663 min 42 in 0.46 in 0.46 gal 13,159 min 38 in 0,46 in 0.46 gal 15,666 min 45 in 0.46 in 0.46 3 R 0.04 4 5 6 7 8 9 CL C C C C R 1 13,506 7,916 8,489 12,721 7,046 43 21 21 39 21 0.42 0.24 0.26 0,39 0.22 0.42 0.24 0.26 0.39 0.22 13,279 7,783 8,347 12.507 6,927 42 21 21 38 21 0.42 0.24 0.26 0.39 0.22 0.42 0.2485 0.26 0,39 0.22 17 b7,490 11,224 6,217 38 19 19 34 19 0.42 0.25 0.26 0.39 0.22 0.42 0.25 0.26 0.39 0.22 14.187 8.315 8.917 13.362 7.401 45 22 22 40 22 0.42 0.42 0.24 0.24 0.26 0.26 0.39 0.39 0.22 0.22 10 C 11 12 13 C C C 6,984 14,848 21 43 0.22 0.46 0.22 0.46 6,867 14,599 21 42 0.22 0.46 0.22 0.46 6.163 13,101 19 38 0.22 0.46 0.22 0.46 7.337 15,597 22 0.22 0.22 45 0.46 0.46 14 C 15 C 16 CL 17 R 5.5 18 CL 19 C 20 C 21 C 22 C 23 C 24 C 25 CL 26 CL 27 R 0.07 28 C 29 CL 1301 C 1311 C 48 72 Monthly Loading:11 86,424 2.67 24,45 84 972 1 2.67 76,256 2,67 ?_4.451 9^ '?2 2.67 12 Month Floating Total (in): 24 45 'A' 24.45 FORM: NDAR-1 08-11 NON -DISCHARGE APPLICATION REPORT (NDAR-1) Page I of Permit No.: WQ0016376 Facility Name: S&J Villari Livestock Processing Facility -Warsaw County: Duplin Month: December Year: 2023 Did irrigation occur Field Name: 9 Field Name: 10 Field Name: 11 Field Name: 12 at this facility? Area (acres): ---- 1 - Area (acres): 1.46 Area (acres): 1.43 Area (acres): 1.23 Cover Crop: Coastal Bermuda Cover Crop: Coastal Bermuda Cover Crop: Coastal Bermuda Cover Crop: Coastal Bermuda v] YES ^ No Hourly Rate (in): 0.6 Hourly Rate (in): 0.6 Hourly Rate (in): 0.6 Hourly Rate (in): 0.6 Annual Rate (in): 41.96 Annual Rate (in): 41.96 Annual Rate (in): 41.96 Annual Rate (in): 41.96 Weather Freeboard Field Irrigated?' YES ❑ No Field Irrigated? J YES ( I NO Field Irrigated? YES ❑ No Field Irrigated? J YES -, No v 9 m c o m o E m F a o rn O o J rn m `�° o n ,� °' m E ._ a o Co Q d rn 1- •,- �. rn ro m p 0 J a ?� rn E o m= o +� J v m E ._ a o n• Q m aoi Ern .` i °' > c '� o o J= E °' - c E o x o o J m -a E m a O Q Q 'o y� E rn rn T c o J E c E X O N S J E 2D '�' � Q 6 CL a °' @ _Ern ~ rn > c '� m O J FE 2 1JR °F in in 78 in 60 gal 12,533 min 36 in 0.46 in 0.46 gal 18.298 min 53 in 0.46 in 0.46 gal 17,922 min 51 in 0.46 in 0.46 gal 15.415 min 44 in 0.46 in 0.46 3 0.04 4 5 6 C 7 C 8 C 9 R i 11;350 61652 7,134 10,690 5,921 36 18 18 32 18 0.42 0.24 0.26 0.39 0.22 0.42 0.24 0.26 0.39 0.22 16,571 9.712 10,415 15.607 8.644 53 26 26 47 26 0.42 0.24 0.26 0.39 0.22 0.42 0.24 0.26 0.39 0.22 16,230 9,512 10,201 15,287 8 ,467 51 26 26 46 26 0.42 0.24 0.26 0.39 0.22 0.42 0.24 0.26 0.39 0.22 13.960 44 0.42 0.42 8.182 22 0.24 0.24 8.775 22 0.26 0.26 13,149 40 0.39 0.39 7.283 22 0.22 0.22 10 C 11 C 12 C 13 C 5,869 12,478 18 36 0.22 0,46 0.22 0.46 8.569 18,217 26 53 0.22 0.46 0.22 0.46 8,393 17,843 26 51 022 0.46 0.22 0.46 7.219 15.347 22 44 0.22 0.46 0.22 0.46 14 C 15 C 16 CL 17 R 5.5 18 CL 19 C 20 C 21 C 22 C 23 C 24 C 25 CL 26 CL 27 R 0.07 28 C CL Ef48 C E C 72 Monthly Loading. -I 12 Month Floating 72,627 2.67 1 106,033 267 103,855 2 67 95 30 Total (in):1 24.45 4 -" FORM: NDAR-1 08-11 NON -DISCHARGE APPLICATION REPORT (NDAR-1) Page _'-* o` Permit No.: WQ0016376 Facility Name: S&J Villari Livestock Processing Facility -Warsaw County: Duplin Month: December Year: 2023 Did irrigation occur Field Name: 13 Field Name: 14E Field Name: 14W Field Name: 15 at this facility? Area (acres): 2.16 Area (acres): 13.73 Area (acres): 7.7 Area (acres): 0.73 Cover Crop: Coastal Bermuda Cover Crop: Coastal Bermuda Cover Crop: Coastal Bermuda Cover Crop: Coastal Bermuda i YES _ NO Hourly Rate (in): 0.6 Hourly Rate (in): 0.6 Hourly Rate (in): 0.6 Hourly Rate (in): 0.6 Annual Rate (in): 41.96 Annual Rate (in): 31.6 Annual Rate (in): 24.21 Annual Rate (in): 30.44 Weather Freeboard Field Irrigated? YES ❑ No Field Irrigated? YES J NO Field Irrigated? YES No Field Irrigated? YES �_: No y 0 U d L° c o :° m rn c w 0 o �o ern 472,g- a m m ? c om ° E o, E X'o'°° x� m o E2D oa >a v am:: Ern ~ rn aE "� �� E rn c Xoc°a mx� m a E m �a >°a v ya; Ec, rn �,E M �� E rnm ` c E_ x 0 �a >° m E� �'O7 Tom' @'a o -j_°F > �'`0. E3'�, x o 1 2 C CL in in 78 inn 60 27,071 78 in 0.46 in 0.36 gal 127.319 min 384 in 0.34 in 0.05 gal 71,402 rnin 216 in 0.34 in 0.09 gal 9,149 min 26 in 0.46 in 0.46 3 R 0.04 4 5 7 6JR 8 9 CL C 1 24,515 14,368 15,409 23,090 12,789 78 39 39 70 39 0.42 0.24 0.26 0.39 0.22 0.32 0.24 0.26 0.34 0.22 8.285 4,856 5.208 7.804 4,322 26 13 13 24 13 0.42 0.42 0.24 0.24 0.26 0.26 0.39 0.39 0.22 0.22 10 C 11 12 13 C C C K12.678 39 78 0.22 0.46 0.22 0.35 4,285 9.109 13 26 0.22 0.22 0.46 0.46 14 C 15 C 16 CL 17 R 5.5 18 CL 19 C 20 C 21 C 22 C 23 C 24 C 25 CL 26 CL 27 R 0.07 - 28 C 29 CL 30 C 31 C 48 72 Monthly Loading:1 156,871 2-67 24.45 , 127,319 0.34 71.402 y 0.34 1635 l2 Month Floating Total (in): '6.35 LELLEM:�A FORM NDAR-1 08-11 NON -DISCHARGE APPLICATION REPORT (NDAR-1) Page of Permit No.: WQ0016376 Facility Name: S&J Villari Livestock Processing Facility -Warsaw County: Duplin Month: December Year: 2023 Did irrigation occur Field Name: 16 Field Name: 17 Field Name:YYESNO, Field Name: at this facility? Area (acres): 1.25 Area (acres): 0.82 _ Area (acres):Area (acres): Cover Crop: Coastal Bermuda Cover Crop: Coastal Bermuda Cover Crop:Cover Crop: J YES [ NO Hourly Rate (in): 0.6 Hourly Rate (in): 0.5 Hourly Rate (in):Hourly Rate (in): Annual Rate (in): 13.83 Annual Rate (in): 16.95 Annual Rate (in):Annual Rate (in): Weather Freeboard Field trrigated7 YES n No ed? (] YES = No Field Irrigated? Field Irrigated? ( YES NO > m ° U ro M o as = a p m ° cv rn� a° m m `�° ° Cn Y I-- m E_ �a ars d„ E� i=°t rn A c ,�v p� E rn 4 c E�ii ><°`° Ed °@ orn T �' o �m ° m E3o ><°m °' aai �'� R E� rn m o E2D �a CL D E E� rn m'v _I — E rnp E E°0 J 1 C °F in in 78 in 11 60 gal 14,426 min 181 in 0.43 in 0.14 gal 9,464 min 119 in 0.43 in 0.21 gal min in in gal min in in 2 CL 3 R 0.04 4 CL 5 C 6 C 7 C 8 C 12,742 181 0.38 0,12 8,358 119 0.38 0.19 9 R 1 10 C 11 C 12 C 13 C 14 C 15 C 16 CL 17 R 5.5 18 CL 19 C 20 C 21 C 22 C 23 C 24 C 25 CI_ 26 CL 27 R 0.07 28 C 29 CL 30 C 31 C 48 72 Monthly Loading: 27 168 0.80 17 822 0.80 �� 12 Month Floating Total 8-38 -- ' FORM: NDAR-1 08-11 NON -DISCHARGE APPLICATION REPORT (NDAR-1) Page _�L of Did the application rates exceed the limits in Attachment B of your permit? El Compliant Ll Non -Compliant Were adequate measures taken to prevent effluent ponding in or runoff from the sites? El Compliant ❑ Non -Compliant Was a suitable vegetative cover maintained on all sites as specified in your permit? Q Compliant ❑ Non -Compliant Were all setbacks listed in your permit maintained for every application to each permitted site? 0 Compliant ❑ Non -Compliant Were all freeboards maintained in accordance with the specified freeboard heights in your permit? ❑� Compliant ❑ Non -Compliant If the facility is non -compliant, please explain in the space below the reason(s) the facility was not in compliance. Provide in your explanation the date(s) of the non-compliance and describe the corrective action(s) taken. Attach additional sheets if necessary. Operator in Responsible Charge (ORC) Certification Permittee Certification ORC: Gerald Lamar Matthews Permittee: Sam Villari Certification No.: 993131 Signing Official: Grade: SI Phone Number: 910-289-7500 Signing Officials Title: Owner Has the ORC changed since the previous NDAR-1? [ I Yes j No Phone Number: 910-293-2157 Permit Exp,: 11/302025 Signature Date Signature Date By this signature, I certify that this report is accurrate and complete to the best of my knowledge I certify, under penally of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that all qualified personnel properly gathered and evaluated the information submitted Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations. Mail Original and Two Copies to: Division of Water Quality Information Processing Unit 1617 Mail Service Center Raleigh, North Carolina 27699-1617 FORM: NDMLR 10-13 NON -DISCHARGE MASS LOADING REPORT (NDMLR) Page __/ of SI Permit No.: WQ0016376 Facility Name: S&J Villari Livestock Processing Facility -Warsaw County: Duplin Month: December Year: 2023 Field Name: Zone 1 Field Name: Zone 2 Field Name: Zone 3 Field Name: Zone 4 Field Name: Zone 5 Area (acres):qaBe Area (acres): 1.16 Area (acres): 1.12 Area {acres): 1.07 Area (acres): 1.19 Cover Crop: ud Cover Crop: Coastal Bermud Cover Crop: Coastal Bermud Cover Crop: Coastal Bermud Cover Crop: Coastal Bermud Load Type: Load Type: PAN Load Type: PAN Load Type: PAN Load Type: PAN Field Loaded?NO Field loaded? L YES 7 NO Field Loaded? L! YES - NO Field Loaded? L YES U NO Field Loaded? L YESa U NO a° v 4°z °' o > Q a° z a °� v T z o m °-� z p z° Q a m J ¢ ` a, ° ,� io ° ° a y n a > o a ° a ;� a a a. « � a R io a � �Z N N L° d r O J z C. m J z Q ° A s om `>, m e N J¢ °> C° 0_ E u ; c =_j O E 7 a E CD C � C ° 7 a E m a� N VC JE Q E m U r 0 C J E zO > Q UO > Q O U > O a� U a > O a� O U 0. > > C O 7 a Month gal mg/L Ibs/ac Ibs/ac gal mg/L lbs/ac Ibs/ac >° gal mg/L Ibs/ac Ibs/ac > gal mg/L Ibs/ac Ibs/ac >° gal a0 mg/L Ibs/ac Ibs/ac January 33.163 36.2 15.4 15.4 59,182 36.2 15.4 15.4 57.142 36.2 15.4 15.4 54,590 36.2 15.4 15.4 54.590 36.2 13.8 13.8 February 0 31.8 0.0 15.4 0 31.8 0.0 15A 0 31.8 0.0 15.4 0 31.8 0.0 154 0 31.8 0.0 13.8 March 60.397 41 31.8 47.2 107,787 41 31.8 47.2 104,071 41 31.8 47.2 99,425 41 31.8 47.2 99.425 41 28.6 42A April 36.868 28.6 13.5 60.7 65,797 28.6 13.5 60.7 63.527 28.6 13.5 60.7 60.692 28.6 13.5 60.7 60.692 28.6 12.2 54.6 May 75,027 24.4 23.5 84.2 133,893 24.4 23.5 84.2 129,275 24.4 23.5 84.2 123,505 24.4 23.5 84.2 123.505 24.4 21.1 75.7 June 19.824 37 9.4 93.6 35,380 37 9A 93.6 34,160 37 9.4 93.6 32,638 37 94 93.6 32.638 37 8.5 84.2 July 23.085 55.8 16.5 110.1 41,198 55.8 16.5 110.1 39,777 55.8 16.5 110.1 38,002 55.8 16.5 110.1 38.002 55.8 14.9 99.0 August 21.276 36.6 10.0 120.1 37,970 36.6 10.0 120.1 36.661 36.6 10.0 120.1 35,024 36.6 10.0 120.1 38.952 36.6 10.0 109.0 September 53.310 42.8 29.3 149.4 95,138 42,8 293 149.4 91,858 42.8 29.3 149.4 87,758 42.8 29.3 149.4 97.598 42.8 29.3 138.3 October 41'191 51.1 27.0 176.4 73,513 51.1 27.0 176.4 70,977 51.1 27.0 176.4 67,809 51.1 27.0 176.4 75,415 51.1 27.0 165.3 November 20.377 123 32.2 208.6 36,364 123 32.2 208.6 35.110 123 32.2 208.6 33,543 123 32.2 208.6 37.304 123 32.2 197.5 December 47,206 150 90.9 299.4 84,245 150 909 299A 81.342 150 90.9 299.4 77,709 150 90.9 299.4 86A24 150 1 90.9 288.3 12 Month Floating PAN Load (Ibs/ac/yr): 299.4 299.4 299.4 299.4 288.3 Annual PAN Load Limit 350.00 (Ibs/ac/yr): 350 350.00 350.00 350.00 FORM NDMLR'0.13 NON -DISCHARGE MASS LOADING REPORT (NDMLR) Page ', or .S Permit No.: WQ0016376 Facility Name: SU Villari Livestock Processing Facility -Warsaw County: Duplin Month: December Year: 2023 Field Name: Zone 6 Field Name: Zone 7 Field Name: Zone 8 Field Name: Zone 9 Field Name: Zone 10 Area (acres): 1.17 Area (acres): 1.05 Area (acres): 1.25 Area (acres): 1 Area (acres): 1.46 Cover Crop: Coastal Bermud Cover Crop: Coastal Bermud Cover Crop: Coastal Bermud Cover Crop: Coastal Bermud Cover Crop: Coastal Bermud Load Type: PAN Load Type: PAN Load Type: PAN Load Type: PAN Load Type: PAN Field Loaded? YES rl rvo Field Loaded? YES (� rvo Field Loaded? YES i No Field Loaded? YES _ No Field Loaded? '' YES NO a a a '- N ° Q 'O Q a O Q > O Q.2 Q d z 0 z a m °� v M o Q ° a ``° a o o a ° a '- m a a u a N > m Q N L O zQ d ,`�° C J Q o Q m C ?. tB0 J Q ate+ >, N N J E " c J o E E Lau d o c E z = Q °' E `° c°'i m � J E z Q m E '° °' v s O � J E z °' m e U o J E z o > ac°� Ua o a' ° L)°' > o o �a ' ' o o sa U ' Q) > o o �Qa U Month gal mg/L Ibs/ac Ibs/ac gal mgiL Ibs/ac Ibs/ac gal mg/L Ibs/ac Ibs/ac gal mg/L Ibs/ac Ibs/ac gal mg/L Ibs/ac Ibs/ac January 59,691 36.2 15.4 15.4 53,571 36.2 15A 15.4 63,773 36.2 15.4 15.4 51,019 36.2 15 4 15.4 74,489 36.2 15.4 15.4 February 0 31.8 0.0 15.4 0 31.8 0.0 15.4 1 0 31.8 0.0 15.4 0 31.8 0.0 15.4 0 31.8 0.0 15.4 March 108.717 41 31.8 47.2 97,567 41 31.8 47.2 116.151 41 31.8 47.2 92,920 41 31.8 47.2 135.664 41 31.8 47.2 April 66.364 28.6 13.5 60.7 59,556 28.6 13.5 60.7 70,901 28.6 13.5 60.7 56,722 28.6 13.5 60.7 82.813 28.6 13.5 60.7 May 135.047 24.4 23.5 84.2 121,196 24.4 23.5 84.2 144.281 24.4 23.5 84.2 115,424 24.4 23.5 84.2 168.518 24.4 23.5 84.2 June 35.685 37 9.4 93.6 32,025 37 9.4 93.6 38,125 37 9.4 93.6 30,500 37 9.4 93.6 44.531 3W62 July 41.553 55.8 16.5 110.1 37,291 55.8 16.5 110.1 44.395 55.8 16.5 110.1 35,516 55.8 16.5 110.1 51.853 550.1 .6 August 38,298 36.6 10.0 120.1 34,370 36.6 10.0 120.1 40.917 36.6 10.0 120.1 32,732 36.6 10.0 120.1 47.791 360.1 September 95,958 42.8 29.3 149.4 86,117 42.8 29.3 149.4 102.521 42.8 29.3 149.4 82,016 42.8 29.3 149.4 119,734 42.9.4 October 74,147 51.1 27.0 176.4 66.541 51.1 27.0 176.4 79.216 51.1 27.0 176.4 63,373 51.1 27.0 176.4 92.524 51.6.4 November 36,677 123 32.2 208.E 32,915 123 32.2 208.6 39.189 123 32.2 208.E 31,349 123 32.2 208.E 45.769 123 32.2 208.E December 84,972 150 90.9 299.4 76,256 150 90.9 299.4 90,782 150 90.9 299.4 72,627 150 90.9 299.4 106.033 150 90.9 299.4 12 Month Floating PAN Load (Ibs/ac/yr): 299.4 299.4 299.4 2994 299.4 Annual PAN Load Limit (Ibs/ac/yr): 350 350.00 350 00 350.00 17T350.00 FORM: rvordlLR 10-13 NON -DISCHARGE MASS LOADING REPORT (NDMLR) Page -3 of Permit No.: W00016376 Facility Name: SU Villari Livestock Processing Facility -Warsaw County: Dupiin Month: December Year: 2023 Field Name: Zone 11 Field Name: Zone 12 Field Name: Zone 13 Field Name: Zone 14E Field Name: Zone 14W Area (acres): 1.43 Area (acres): 1.23 Area (acres): 2.16 Area (acres): 13.73 Area (acres): 7.7 Cover Crop: Coastal Bermud Cover Crop: Coastal Bermud Cover Crop: Coastal Bermud Cover Crop: Coastal Bermud Cover Crop: Coastal Bermud Load Type: PAN Load Type: PAN Load Type: PAN Load Type: PAN Load Type: PAN Field Loaded? OYES (� NO Field Loaded? ❑ YES ❑ NO Field Loaded? YES NO Field loaded? 0 YES NO Field Loaded? J YES ❑ NO 0dz z . a za z - zoz yz° z z° aaa D a a ° s Q0 '0a teJ a.m ° =°� z J ro O o J Ta- ro( oroCU ° U CL Ca ja = Z] EE> a ' a � o o ° �ao > >a U Month gal mg/L Ibs/ac Ibs/ac gal mg/L Ibs/ac Ibs/ac gal mg/L I Ibs/ac I Ibs/ac gal mglL Ibslac ibs/ac gal mg/L lbslac Ibs/ac January 72.957 36.2 15.4 15.4 62,753 36.2 15.4 15.4 110,202 36.2 15.4 15.4 546,990 36.2 12.0 12.0 306,760 36.2 12.0 12.0 February 0 31.8 0.0 15.4 0 31.8 0.0 15.4 0 31.8 0.0 15.4 246,807 31.8 4.8 16.8 138,414 31.8 4.8 16.8 March 132.877 41 31.8 47.2 114,293 41 31.8 47.2 200,711 41 31.8 47.2 689,966 41 17.2 34.0 386.943 41 17.2 34.0 April 81,111 28.6 13.5 60.7 69,768 28.6 13.5 60.7 122,517 28.6 13.5 60.7 631,610 28.61 11.0 45.0 354.216 28.6 11.0 45.0 May 165,057 24.4 23.5 84.2 141,972 24.4 23.5 84.2 249.316 24.4 23.5 84.2 558,451 24.4 8.3 53.2 313.186 24.4 8.3 53.2 June 43.617 37 9.4 93.6 37,515 37 9.4 93.6 65,881 37 9.4 93.6 286,429 37 6.4 59.7 160.633 37 6.4 59.7 July 50.787 55.8 16.5 110.1 43,684 55.8 16.5 110.1 76,713 55.8 16.5 110.1 413,380 55.8 14.0 73.7 231,830 55.8 14.0 73.7 August 46.808 36.6 10.0 120.1 40,262 36.6 10.0 120.1 70.703 36.6 10.0 120.1 387,717 36.6 J 8.6 82.3 217.438 36.6 8.6 82.3 September 117.284 42.8 29.3 149A 100,881 42.8 29.3 149.4 177.154 42.5 29.1 149.2 282.056 42.8 7.3 89.6 158.183 42.8 7.3 89.6 October 90,623 51.1 27.0 176.4 77,948 51.1 27,0 176.4 136.884 51.1 27.0 176.2 282,056 51.1 8.8 588.398 51.1 32.6 122.2 November 44,828 123 32.2 208.6 38,559 123 32.2 2066 67.712 123 32.2 208.4 875,365 123 65.4490,920 123 65.4 187.6 December 103.855 150 90.9 299.4 89,330 150 90.9 299.4 156,871 150 90.9 299.2 127,319 150 11.6 71.402 150 11.6 199.2 12 Month Floating PAN Load (Ibs/ac/yr): 299 4 299.4 299.2 175.4 i 199.2 Annual PAN Load Limit (Ibslac/yr): 350 350.00 350.00 . 350.00 350 00 FORM: NDMLR 10-13 NON -DISCHARGE MASS LOADING REPORT (NDMLR) Page 5P of-S� Permit No.: WQ0016376 Facility Name: S&J Villari Livestock Processing Facility -Warsaw County: Duplin Month: December Year: 2023 Field Name: Zone 15 Field Name: Zone 16 Field Name: Zone 17 Field Name: Field Name: Area (acres): 0.73 Area (acres): 1.25 Area (acres):ECoastal 82 Area (acres): Area (acres): Cover Crop: Norfolk Cover Crop: Coastal Bermud Cover Crop: Bermud Cover Crop: Cover Crop: Month Load Type: Field Loaded? z d ¢ o ° o � N V <L) gal mg/L 37,243 36.2 PAN � YES No Q m a s '' o `°� C J E z o �a U Ibslac Ibs/ac 15.4 15.4 Load Type: Field Loaded? z o n n m ¢ d.. d C E U m e o < gal mg/L 11,612 36.2 PAN 11 YES E NO z > a 0- >ia m o _¢ J E Z o �¢ �° Ibs/ac Ibs/ac 2.8 2.8 Load Type: Field Loaded? z o ¢ a a m: C i m E �, c o aU gal mg/L 7,618 36.2 PAN L YES I- J NotFieldded?, z ¢ aa� a m¢ D oa >. f9 = J>. +� J Z �¢ g° �a lbs/ac Ibs/acIbs/ac 2.8 2.8 Load Type: PAN L YES ] No z > m m o i0 @ J y o Z �r E¢ o Ibs/ac Load Type: Field Loaded? z o° a ¢ +� a a ca ¢ N ai±>, co E L ' > o 0¢ U gal mg/L PAN U YES z¢ ¢ 0 y� L>> Ibs/ac Q✓ NO >¢ JE Ez j°¢> Ibs/ac January February 0 31.8 0.0 15.4 11,783 31.8 2.5 5.3 7,730 31.8 2.5 5.3 March 67,833 41 31.8 47.2 24,159 41 6.6 11.9 15.849 41 6.6 11.9 April 41,407 28.6 13.5 60.7 23,725 28.6 4.5 16A 15.563 28.6 4.5 16.4 May 84,259 24.4 23.5 84.2 24,162 24.4 3.9 20.4 15.851 24.4 3.9 20.4 June 22,2G4 37 9.4 93.6 24,801 37 6.1 26.5 16.269 37 6.1 26.5 July 25.927 55.8 16.5 110.1 26,666 55.8 9.9 36.4 17,494 55.8 9.9 36.4 August 23.895 36.6 10.0 120.1 20,489 36.6 5.0 41A 13.440 36.6 5.0 41.4 September 59,872 42.8 29.31 149.4 36.603 42.8 10.5 51.9 24.011 42.8 10.5 51.9 October 46,262 51.1 27.0 I 176.4 27,706 51.1 9.4 61.3 18.175 51.1 9.4 61.3 November 22.884 123 32.2 208.6 24,526 123 20.1 81.5 16,089 123 20.1 81.5 December 53.018 1 150 90.9 299.4 27,168 150 27.2 108.6 17.822 150 27.2 108.E 12 Month Floating PAN Load (Ibs/ac/yr): 299.4 108.6 108.6 0.0 0.00 0.0 Annual PAN Load Limit (Ibs/ac/yr): 350 350.00 350.00 0.00 FORM: NDMLR 10-13 NON -DISCHARGE MASS LOADING REPORT (NDMLR) Page J of S� Did the mass loading rates exceed the limits in Attachment B of your permit? ❑ Compliant ❑ Non -Compliant If the facility is non -compliant, please explain in the space below the reason(s) the facility was not in compliance. Provide in your explanation the date(s) of the non-compliance and describe the corrective artinn/c1 taken Attach nd liti—I if n...o­. Operator in Responsible Charge (ORC) Certification Permittee Certification ORC: Gerald Lamar Matthews Permittee: SAM VILLARI Certification Number: 993131 Signing Official: Grade: SI Phone Number: 910-289-7500 Signing Official's Title: OWNER Has the ORC changed since the revious NDMLR? ❑ yes E/j No Phone No.: 910-293-2157 Permit Exp.: 11/30/25 2- t —,�— -Zs= Z V, Signature Date Signature Date By this signature, I certify that this report is accurrate and complete to the best of my knowledge. I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that all qualified personnel properly gathered and evaluated the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true. accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations. Mail Original and Two Copies to: Division of Water Resources Information Processing Unit 1617 Mail Service Center Raleigh, North Carolina 27699-1617 Environmental Chemists, Inc. envirochem 6602 Windmill Way, Wilmington, NC 28405 0 910.392.0223 Lab ' 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 4 252.473.5702 Lab.'Fax 255-A Wilmington Highway, Jacksonville, NC 28540 ° 910.347.9843 Lab/Fax ANALYTICAL 8 CONSULTING CHEMISTS infoa environmentalchemisis.conl The Pork Company Date of Report: Jan 10, 2024 892 Penny Branch Road Customer P® #: Warsaw NC 28398 Customer ID: 08100099 Attention: Report #: 2023-29459 Project ID: WWTF Eff - Mthly Lab ID Sample ID: Collect Date/Time Matrix Sampled by 23-71323 Site: Effluent 12/1512023 8:15 AM Water Gerald Matthews Test Method Results Date Analyzed PAN Used 30°k Mineralization Rate Calcuation 150mg/L 01/10/2024 Fecal Coliform ldem Colilert-te 112000 MPN/100ml 12/15/2023 Total Dissolved Solids (TDS) SM 2540 C-2015 276 mg/L 12118/2023 Residue Suspended (TSS) SM 2540 D-2015 4200 mg/L 12/18/2023 Ammonia Nitrogen SM 4500 NH3 C-2011 139 mg/L 01/09/2024 Total Kjeldahl Nitrogen (TKN) SM 4500 Norg B-2011 404 mg/L 01/09/2024 Total Phosphorus SM 4500 P (F•H)-2011 18.8 mg/L 12/21/2023 BOD SM 5210 6-2016 309 mg/L 12/15/2023 Chloride SM4500 CI E-2011 43 mg/L 12/19/2023 Nitrate Nitrogen (Cale) Nitrite Nitrogen Analyzed outside of hold time. EPA 353 2, Rev. 2 0,1993 0.21 m /L g 12/18/2023 Nitrate+Nitrite-Nitrogen EPA 3532. Rev. 20, 1993 1.49 mg/L 12/18/2023 Nitrate Nitrogen Subtraction Method 1.28 mg/L 12/29/2023 Total Nitrogen (Cale) Total Nitrogen `total Nitrogen 405 mg/L 01/09/2024 port C 2023-29459 - Page 1 of 2 Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 ` 910.392,0223 Lab m 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 s 252.473.5702 Lab i Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab., Fax ANALYTICAL & CONSULTING CHEMISTS info iz.environmentalchemists.com The Pork Company Date of Report: Jan 10, 2024 892 Penny Branch Road Customer PO #: Warsaw NC 28398 Customer ID: 08100099 Attention-. Report #: 2023-29459 Project ID: WWTF Eff - Mthly Lab ID Sample ID: Collect Datefiime Matrix Sampled by 23-71324 Site: PPI-002 Upstream 12/15/2023 8:30 AM Water Gerald Matthews Test Method Results Date Analyzed Ammonia Nitrogen EPA 350.1. Rev 2 0. 1993 < 0.2 mg/L 12/20/2023 Total Phosphorus SM 4500 P (F-N-2011 0.92 mg/L 12121 /2023 Fecal Coliform SM 9222 D-2015 MF 59 Colon ies/100ml- 12/15/2023 Nitrate Nitrogen (Cale) Nitrite Nitrogen EPA 353.2, Rev 2 0, 1993 < 0.02 mg/L 12/1512023 Nitrate Nitrogen Subtraction McU`wd <0.02 mg/L 12/29/2023 Total Nitrogen (Cale) Total Kjeldahl Nitrogen (TKN) EPA351.2, Rev.2.0, 1993 0.7mg/L 12/21/2023 Nitrate+Nitrite-Nitrogen EPA 353.2, Rev. 2.0, 1993 < 0.02 mg/L 12/18/2023 Total Nitrogen Total Nitrogen 0.70 mg/L 12/21/2023 Lab ID Sample ID: Collect DatelTime Matrix Sampled by 23-71326 Site: PPI-003 Downstream 12/15/2023 8:00 AM Water Gerald Matthews Test Method Results Date Analyzed Ammonia Nitrogen Total Phosphorus Fecal Coliform Nitrate Nitrogen (Cale) Nitrite Nitrogen Nitrate+Nitrite-Nitrogen Nitrate Nitrogen Total Nitrogen (Cale) EPA 350.1, Rev. 2.0. 1993 SRO 4500 P (F-H)-2011 SM 9222 D-2015 MF EPA 353.2, Rev. 2.0, 1993 EPA 353.2, Rev. 2.0, 1993 Subtraction Method 1.1 mg/L 12/20/2023 0.65 mg/L 12/2112023 410 Colonies/100ml- 12/15/2023 < 0.02 mg/L 0.18 mg/L 0.18 mg/L 12/15/2023 12/18/2023 12/2912023 Total Kjeldahl Nitrogen (TKN) EPA 351.2, Rev. 2.0. 1993 1.4 mg/L 12/21/2023 Total Nitrogen Total Nitrogen 1.58 mg/L 12/21/2023 Comment: Reviewed by: Report #: 2023-29459 Page 2 72 Environmental Chemist, Inc., Wilmington, NC Lab #94 6602 Windmill Way Wilmington, NC 28405 Sample Receipt Checklist 910392 0223 Client: C)C� Date:AW51 Report Number: sample: ❑ NO ECHEM Pickup Client Delivery ❑ UPS ❑ FedEx ❑ CI N A Other ❑ / RReceipt ❑ NO 1. Were custody seals present on the cooler? N/A mperature upon 2Ifeals were present, were they intact/unbroken? receipt °C Corrected temperature upon receipt oC How temperature taken: ❑ Temperature Blank O IR Gun ID: Against Bottles Thomas Traceable S/N 210886869 YES 13 NO IR Gun Correction Factor'C: 0.0 3. If temperature of cooler exceeded 6°C, O YES YES ❑ NO was Project Mgr./QA notified? 4. Were proper custody procedures (relinquished/received) followed? ❑ NO S. Were sample ID's listed on the COC? 19 YES O YES ❑ ❑ NO 6. Were samples ID's listed on sample containers? 0 YES ❑ NO 7. Were collection date and time listed on the COC? Ox YES ❑ NO 8. Were tests to be performed listed on the COC? 0 YES ❑ NO 9. Did samples arrive in proper containers for each test? !] YES ❑ NO 10. Did samples arrive in good condition for each test? YES ❑ NO 11. Was adequate sample volume available?' YES ❑ NO NO 12. Were samples received within proper holding time for requested tests? V❑O YES ❑ NO 13. Were acid preserved samples received at a pH of <2? ❑ YES ❑ 14. Were cyanide samples received at a pH >12? YES ❑ NO 15. Were sulfide samples received at a pH >9? YES ❑ NO NO 16. Were NH3JTKN/Phenol received at a chlorine residual of <0.5 m/L? ** ❑ YES ❑ NO 17. Were Sulfide/Cyanide received at a chlorine residual of <0.5 m/L? 18. Were orthophosphate samples filtered in the field within 15 minutes? * TOC/volatiles are pH checked at time of analysis and recorded on the benchsheet. ** Bacteria .samples are checked for Chlorine at time of analysis and recorded on the benchsheet. Sample Preservation: (Must be completed for any sample(s) incorrectly y preserved or with headspace) were received incorrectly preserved and were adjusted accordingly by adding (circle one): H SO HNO � a a HCi NaOH Time of preservation: If more than one preservative is needed, notate in comments below Note: Notify customer service immediately for incorrectly preserved samples. Obtain a new sample or notify the state lab if directed to analyzed by the customer. who was notified, date and time: Voiatiles sample(s) were received with headspace COMMENTS: DOC. QA.002 Rev 1 dmill mington ENVIRONMENTAL CHEMISTS, INC OFFICE: n910392-02 3'IFAX910-392-44245 Analytical & Consu@ing Chemists NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 info@environmentalchemists.com Client: The Pork Company -Warsaw s-V ..WIT P%v Vr Vl.1a 1 VL%► PROJECT NAME: WWTF Effluent REPORT N0: ADDRESS: CONTACT NAME: PO NO: REPORT TO: Gerald Matthews, ORC PHONEIFAX: Permit Number: W00016376 email: , ` SAMPLE TYPE: I = Influent_ E = Pfflimnt W = Wall AT = cfr� an - im .a ev - Collection m ` PRESERVATION Sample Identification a w a ° 0e° " g m 0 @' CDz E v a o p o w ANALYSIS REQUESTED Date Time Tempv � zz z° PPI-001 Effluent-1/month / �3 G G X BOD, TSS, NO2 H field): �.� G G X NO3, NH3, TKN, Total P, PAN, Total N C P G G X Fecal Coliform C P -001 ue t e G C G P -- Mar r G G X LTDS, Chloride (triannuais C P GG ----_'_--.-- Z- � 7 C PG PPI-002 U stream G X NO2 C P G G X JTKN, NH3, NO3, TP, TN C P G G X Fecal j U h PPl-003 Downstream) C G P G X NO2 C P ,- G G X GJ FKN, NH3, NO3, TP, TN C P G G 1 [X17Fe C a l Transfer Rell uished By: Date/Time Rec DatelTime 2. Temperature when Received "C: 77 Accepted: Rejected: esample Requested: �-� Delivered By: Received By: Date: M < Time: Comments: TURNAROUND: