NCG060409_DMR_20210513

NCr Department of
Environmental Qualit
NCDEQ Division of Energy, Mineral and Land Resources Received Y
Stormwater Discharge Monitoring Report (DMR) Form for NCG060000 MAY 1 3 2021
Food and Kindred Winston-Salem
Click here for instructions Regional n{f7Ce
Complete,sign,scan and submit the DMR via the Stormwater NPDES Permit Data Monitoring Report(DMR) Upload form within
30 days of receiving sampling results. Mail the original, signed hard copy of the DMR to the appropriate DEMLR Regional Office.
Certificate of Coverage No. NCGO6 0409 Person Collecting Samples: Parker Cliatt
Facility Name:Amazon.com Services LLC-GSO1 Laboratory Name: Eurofins Test America
Facility County: Guilford Laboratory Cert. No.: 269
Discharge during this period: ✓❑ Yes ❑ No (if no,skip to signature and date)
Has your facility implemented mandatory Tier response actions this sample period for any benchmark exceedances?❑Yes ✓❑ No
If so,which Tier(I,II,or III)?
A copy of this DMR has been uploaded electronically via https://edocs.deq.nc.gov/Forms/SW-DMR ✓❑ Yes ❑ No
Date Uploaded:
Analytical Monitoring Requirements for Outfalls with Industrial Activities—Benchmarks in(Red)
Parameter Parameter Outfall 001 Outfall Outfall Outfall Outfall
Code
N/A Receiving Stream Class WS
N/A Date Sample Collected MM/DD/YYYY 4/24/2021
46529 24-Hour Rainfall in inches 0.3
C0530 TSS in mg/L(100 or 50*) 5.4
00400 pH in standard units(6.0-9.0) 7.44
00556 Oil&Grease in mg/L(30) 1.9
31616 Fecal Coliform per 100 ml of N/A
freshwater(if required)(1000)
61211 Enterococci per 100 ml of saltwater N/A
(if required)(500)
00340 Chemical Oxygen Demand in mg/L 17
(120)
Additional parameters for outfalls in drainage areas that use>55 gallons per month of new hydraulic oil on average
NCOIL Estimated New Motor/Hydraulic Oil N/A
Usage in gal/month
00552 Non-Polar Oil&Grease in mg/L(15) N/A
Outfalls to Outstanding Resource Waters(ORW),High Quality Waters(HQW),Trout Waters(Tr)and Primary Nursery Areas(PNA)
have a benchmark TSS limit of 50 mg/L.All other water classifications have a benchmark of 100 111 /L
Notes(optional):
"I certify by my signature below,under penalty of law,that this document and all attachments were prepared under my direction or supervision in
accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted.Based on my
inquiry of the person or persons who manage the system,or those persons directly responsible for gathering the information,the information
submitted is,to the best of my knowledge and belief,true,accurate,and complete.I am aware that there are significant penalties for submitting
false informa o ,i•cluding the possibility of fines and imprisonment for knowing violations."
• I,
ijo-4 •
Signatur 'erm ttee or Delegated Authorized Individual Date
Email Address [e-mail] Phone Number [phone]

n
I/ ti eurofins
Environment Testing
America
ANALYTICAL REPORT
Eurofins TestAmerica, Savannah
>s — 5102 LaRoche Avenue
c ,, Savannah, GA 31404
41111110 Tel: [phone]
: ► AbigaiQgoiiLaboratory Job ID: 680-198096-1
, OF ___________- Client Project/Site: Storm Water - Amazon Warehouses (GSO1)
_ For:
ERM-West
,*41, 1920 Main Street
Suite 300
Irvine, California 92614
Attn: Doug J Wade
•
X ,
` Authorized for release by:
5/4/2021 8:33:52 AM
` Lauren Evans, Project Manager I
[phone]
[e-mail]
1
LINKS
Review your project
results through
Total Access
I
Have a Question?
As k—i
/i e The test results in this report meet all 2003 NELAC,2009 TNI,and 2016 TNI requirements for
accredited parameters.exceptions are noted in this report. This report may not be reproduced
Li Ex art except in full,and with written approval from the laboratory.For questions please contact the
Project Manager at the e-mail address or telephone number listed on this page.
. This report has been electronically signed and authorized by the signatory.Electronic signature is
intended to be the legally binding equivalent of a traditionally handwritten signature.
Visit us at:
www eurofinsus com/Env Results relate only to the items tested and the sample(s)as received by the laboratory.
I

Definitions/Glossary
Client: ERM-West Job ID: 680-198096-1 w
Project/Site: Storm Water-Amazon Warehouses (GSO1) LI
Qualifiers
General Chemistry
Qualifier Qualifier Description
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
Glossary
Abbreviation These commonly used abbreviations may or may not be present in this report.
o Listed under the"D"column to designate that the result is reported on a dry weight basis
%R Percent Recovery
CFL Contains Free Liquid
CFU Colony Forming Unit
CNF Contains No Free Liquid
DER Duplicate Error Ratio(normalized absolute difference)
Dil Fac Dilution Factor
DL Detection Limit(DoD/DOE)
DL,RA,RE,IN Indicates a Dilution,Re-analysis,Re-extraction,or additional Initial metals/anion analysis of the sample
DLC Decision Level Concentration(Radiochemistry)
EDL Estimated Detection Limit(Dioxin)
LOD Limit of Detection(DoD/DOE)
LOQ Limit of Quantitation(DoD/DOE)
MCL EPA recommended"Maximum Contaminant Level"
MDA Minimum Detectable Activity(Radiochemistry)
MDC Minimum Detectable Concentration(Radiochemistry)
MDL Method Detection Limit
ML Minimum Level(Dioxin)
MPN Most Probable Number
MQL Method Quantitation Limit
NC Not Calculated
ND Not Detected at the reporting limit(or MDL or EDL if shown)
NEG Negative/Absent
POS Positive/Present
PQL Practical Quantitation Limit
PRES Presumptive
QC Quality Control
RER Relative Error Ratio(Radiochemistry)
RL Reporting Limit or Requested Limit(Radiochemistry)
RPD Relative Percent Difference,a measure of the relative difference between two points
TEF Toxicity Equivalent Factor(Dioxin)
TEQ Toxicity Equivalent Quotient(Dioxin)
TNTC Too Numerous To Count
Eurofins TestAmerica, Savannah
Page 2 of 13 5/4/2021

•
Sample Summary •
Client: ERM-West Job ID: 680-198096-1
Project/Site: Storm Water-Amazon Warehouses(GSO1)
Lab Sample ID Client Sample ID Matrix Collected Received Asset ID
680-198096-1 GS01_Sample_Point_01_20210424 Water 04/24/21 16:42 04/27/21 09:55
Eurofins TestAmerica, Savannah
Page 3 of 13 5/4/2021

Case Narrative
Client: ERM-West Job ID: 680-198096-1
Project/Site: Storm Water-Amazon Warehouses (GSO1)
Job ID: 680-198096-1
Laboratory: Eurofins TestAmerica, Savannah
Narrative
Job Narrative
680-198096-1
Comments
No additional comments.
Receipt
The sample was received on 4/27/2021 9:55 AM. Unless otherwise noted below,the sample arrived in good condition,and where
required, properly preserved and on ice. The temperature of the cooler at receipt was 2.4°C.
General Chemistry
Methods SM 2540D:The sample duplicate precision for the following sample associated with analytical batch 680-666128 was outside
control limits:(680-198102-C-1 DU). The associated Laboratory Control Sample/Laboratory Control Sample Duplicate(LCS/LCSD)
precision met acceptance criteria.
Methods 410.4:The matrix spike/matrix spike duplicate(MSIMSD)recoveries for batch 666299 were outside control limits. Sample matrix
interference is suspected because the associated laboratory control sample(LCS)recovery was within acceptance limits.
Methods 1664A: Insufficient sample volume was available to perform a matrix spike/matrix spike duplicate/sample duplicate
(MS/MSD/DUP)associated with preparation batch 680-666593.
No additional analytical or quality issues were noted,other than those described above or in the Definitions/Glossary page.
Eurofins TestAmerica, Savannah
Page 4 of 13 5/4/2021

Client Sample Results
Client: ERM-West Job ID: 680-198096-1
Project/Site: Storm Water-Amazon Warehouses (GSO1)
Client Sample ID: GS01_Sample_Point_01_20210424 Lab Sample ID: 680-198096-1
Date Collected: 04/24/21 16:42 Matrix: Water
Date Received: 04/27/21 09:55
General Chemistry
Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac 0
HEM(Oil&Grease) 1.9 J 4.8 1.3 mglL 04/30/21 08:23 04/30/21 10:34 1
Total Suspended Solids 5.4 2.5 2.5 mg/L 04/27/21 14:14 1
Chemical Oxygen Demand 17 10 5.0 mg/L 04/28/21 13:10 1
Eurofins TestAmerica, Savannah
Page 5 of 13 5/4/2021

QC Sample Results
Client: ERM-West Job ID: 680-198096-1
Project/Site: Storm Water- Amazon Warehouses (GSO1)
Method: 1664A- HEM and SGT-HEM
Lab Sample ID: MB 680-666593/1-A Client Sample ID: Method Blank
Matrix: Water Prep Type: Total/NA
Analysis Batch: 666656 Prep Batch: 666593
MB MB
Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac
HEM(Oil&Grease) <1.4 5.0 1.4 mg/L 04/30/21 08:23 04/30/21 10:34 1 U
Lab Sample ID: LCS 680-666593/2-A Client Sample ID: Lab Control Sample
Matrix: Water Prep Type:Total/NA
Analysis Batch: 666656 Prep Batch: 666593
Spike LCS LCS %Rec.
Analyte Added Result Qualifier Unit D %Rec Limits
HEM(Oil&Grease) 40.0 34.80 mg/L 87 78-114
Lab Sample ID: LCSD 680-666593/3-A Client Sample ID: Lab Control Sample Dup
Matrix: Water Prep Type: Total/NA
Analysis Batch: 666656 Prep Batch: 666593
Spike LCSD LCSD %Rec. RPD
Analyte Added Result Qualifier Unit D %Rec Limits RPD Limit
HEM(Oil&Grease) 40.0 34.00 mg/L 85 78-114 2 18
Method: 2540 D-2011 - Total Suspended Solids (Dried at 103-105°C)Lab Sample ID: MB 680-666128/1 Client Sample ID: Method Blank
Matrix: Water Prep Type: Total/NA
Analysis Batch: 666128
MB MB
Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac
Total Suspended Solids <2.5 2.5 2.5 mg/L 04/27/21 14:14 1
' Lab Sample ID: LCS 680-666128/2 Client Sample ID: Lab Control Sample
Matrix: Water Prep Type: Total/NA
Analysis Batch: 666128
Spike LCS LCS %Rec.
Analyte Added Result Qualifier Unit D %Rec Limits
LTotal Suspended Solids 951 906 mg/L 95 80-120
Lab Sample ID: LCSD 6R0-666128/3 Client Sample ID: Lab Control Sample Dup
Matrix: Water Prep Type: Total/NA
Analysis Batch: 666128
Spike LCSD LCSD %Rec. RPD
Analyte Added Result Qualifier Unit D %Rec Limits RPD Limit
Total Suspended Solids 951 932 mg/L 98 80-120 3 25
Method: 410.4-1993 R2.0 - COD
Lab Sample ID: MB 680-666299/3 Client Sample ID: Method Blank
Matrix: Water Prep Type: Total/NA
Analysis Batch: 666299
MB MB
Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac
Chemical Oxygen Demand <5.0 10 5.0 mg/L 04/28/21 13:10
Eurofins TestAmerica, Savannah
Page 6 of 13 5/4/2021

QC Sample Results
Client: ERM-West Job ID: 680-198096-1
Project/Site: Storm Water-Amazon Warehouses (GSO1)
Method: 410.4-1993 R2.0 - COD (Continued)
Lab Sample ID: LCS 680-666299/4 Client Sample ID: Lab Control Sample
Matrix: Water Prep Type: Total/NA
Analysis Batch: 666299
Spike LCS LCS %Rec.
Analyte Added Result Qualifier Unit D %Rec Limits
Chemical Oxygen Demand 50.0 50.7 mg/L 101 90-110
Eurofins TestAmerica, Savannah
Page 7 of 13 5/4/2021

QC Association Summary
Client: ERM-West Job ID: 680-198096-1
Project/Site: Storm Water-Amazon Warehouses (GSO1)
General Chemistry
Analysis Batch: 666128
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
680-198096-1 GS01_Sample_Point_01_20210424 Total/NA Water 2540 D-2011
MB 680-666128/1 Method Blank Total/NA Water 2540 D-2011
LCS 680-666128/2 Lab Control Sample Total/NA Water 2540 D-2011
LCSD 680-666128/3 Lab Control Sample Dup Total/NA Water 2540 D-2011
Analysis Batch: 666299
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
680-198096-1 GS01_Sample_Point_01_20210424 Total/NA Water 410.4-1993 R2.0
MB 680-666299/3 Method Blank Total/NA Water 410.4-1993 R2.0
1 LCS 680-666299/4 Lab Control Sample Total/NA Water 410.4-1993 R2.0
Prep Batch: 666593
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
680-198096-1 GS01_Sample_Point_01_20210424 Total/NA Water 1664A
MB 680-666593/1-A Method Blank Total/NA Water 1664A
LCS 680-666593/2-A Lab Control Sample Total/NA Water 1664A
LCSD 680-666593/3-A Lab Control Sample Dup Total/NA Water 1664A
Analysis Batch: 666656
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
680-198096-1 GS01_Sample_Polnt_01_20210424 Total/NA Water 1664A 666593
MB 680-666593/1-A Method Blank Total/NA Water 1664A 666593
LCS 680-666593/2-A Lab Control Sample Total/NA Water 1664A 666593
LCSD 680-666593/3-A Lab Control Sample Dup Total/NA Water 1664A 666593
Eurofins TestAmerica, Savannah
Page 8 of 13 5/4/2021

Lab Chronicle
Client: ERM-West Job ID: 680-198096-1
Project/Site: Storm Water-Amazon Warehouses (GSO1)
Client Sample ID: GS01_Sample_Point_01_20210424 Lab Sample ID: 680-198096-1
Date Collected: 04/24/21 16:42 Matrix: Water
Date Received: 04/27/21 09:55
Batch Batch Dil Initial Final Batch Prepared
Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab
Total/NA Prep 1664A 525 mL 500 mL 666593 04/30/21 08:23 JAS TAL SAV
Total/NA Analysis 1664A 1 666656 04/30/21 10:34 JAS TAL SAV
Instrument ID: NoEquip
Total/NA Analysis 2540 D-2011 1 1000 mL 1000 mL 666128 04/27/21 14:14 PG TAL SAV
Instrument ID: NOEQUIP
Total/NA Analysis 410.4-1993 R2.0 1 2 mL 2 mL 666299 04/28/21 13:10 MCL TAL SAV 8
Instrument ID: SPC7
Laboratory References:
TAL SAV=Eurofins TestAmerica,Savannah,5102 LaRoche Avenue,Savannah,GA 31404,TEL[phone]
Eurofins TestAmerica, Savannah
Page 9 of 13 5/4/2021

Accreditation/Certification Summary
Client: ERM-West Job ID: 680-198096-1
Project/Site: Storm Water-Amazon Warehouses (GSO1)
Laboratory: Eurofins TestAmerica, Savannah
The accreditations/certifications listed below are applicable to this report.
Authority Program Identification Number Expiration Date
North Carolina(WW/SW) State 269 12-31-21
Eurofins TestAmerica, Savannah
Page 10 of 13 5/4/2021

Method Summary
Client: ERM-West Job ID: 680-198096-1
Project/Site:Storm Water-Amazon Warehouses(GSO1)
Method Method Description Protocol Laboratory
1664A HEM and SGT-HEM 1664A TAL SAV
2540 D-2011 Total Suspended Solids(Dried at 103-105°C) SM TAL SAV
410.4-1993 R2.0 COD MCAWW TAL SAV
1664A HEM and SGT-HEM (Aqueous) 1664A TAL SAV
Protocol References:
1664A=EPA-821-98-002
MCAWW="Methods For Chemical Analysis Of Water And Wastes",EPA-600/4-79-020,March 1983 And Subsequent Revisions.
SM="Standard Methods For The Examination Of Water And Wastewater"
Laboratory References:
TAL SAV=Eurofins TestAmerica,Savannah,5102 LaRoche Avenue,Savannah,GA 31404,TEL[phone]
Eurofins TestAmerica, Savannah
Page 11 of 13 5/4/2021

Eurofins TestAmerica,Savannah
5102 LaRoche Avenue C?eurofins
Chain of Custody Record
Savannah GA 31404 An+•:•c.
Phone[phone] Fax[phone]
Sv"cje / /' Lao'M Cw:..r Tracarq Nat, COC No
Client Information _ f't..ra4at_I CI'-" Evans Lauren R 240.78217-31058
CI•enr Ccteact Phone E-Ma+ Slate or Qog n Page
Doug Waoe 7c,i, 5-7 i -5-3i`7 Lauren Evans@Eurofmset corn Page of
for p.,nr P::[.,[1 Joh if
ERM-West Analysis Requested
Aporess Due Dale Requested I Preservation Codes:
1920 Main Street Suite 300
City TAT Requested(days) A-MCI M-Me•ane
B 1440, N Noee
Irvine C Zn Acetate 0 AsNa02
Stare.LP 0 Nanc AM P Na204S
CA 92614 Compliance Project A Yes .1 No E NaMS04 0•Na2S03
'Phone — PO a
r Me-OH R•Na2S203
443.312.0046(Tel) Purchase Order Requested G As orth S.TSPH2SO4
Email — - WO e = H•As[orbc An0 T TSP OdYTcanydraN
ce V Acetone
doug wade@erm corn o 2 t' J DI Water V MCAA
Protect Name Project e a C C K•EDTA W of 4 5
Storm Waler Amazon Warehouses( j 24024260 • = A L EOA Z othe lspecrfyl
S-re STOWS E
el S Other
jytw�D•l �.)U 1 Of h �• so.
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Sample Matrix e is N w ci E
(N� r ? Z
Type s-.we '� -C C
Sample (C=comp, o- 2 i o m o D
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Sample Identification Sample Date Time G drab)ier-r........)Ir. e : r°- Special Instructions/Note:
Preservation Code N S S
mN r?
6rc. t_)r-„pr, r.�T,.,,i_ O1 —?'.,-l`42 / `I Lit . i(.,-�LT G � (-J Al i\i e z ' - - 1 I - -------- --
N f y
W I
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-
- 1 111
rars— — 0r Cus(ody — —
t 1 I I f l l
Possible Hazard Identification Sample Disposal I A fee may be assessed if samples are retained longer than I month)
El Hon.Ha:.aril Fla ,3hle+ C, [ R!Dyson 8 Unknown alotr3rcT' LJReturn IT.()Chem 71
Disposal©y Lab air,h+:F Fr.•_ __ _ Months
Deliverable Requested I II,Ill IV.Other(specify) Special Instructions/OC Requirements
Empty Kit Re,nquished by !Date lime 1M.,^o1 o',•c-+•-•
Heirisie, br � Oarer•,�..e Company 11 )Rece'rea/t) I I [Darem a 'r,r+Dany
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'RcL. cl.„tf 1 _ L•(_ l.�
+,.nu•.. r r `� pate.rne I Company Recewedr by ' ..I ID,•e� ��1`' ICo,••ranr
l'1J►ll.I<Ill Liriu)-1 I(5tG - i 'Z7 ) ( lT��
Ret.no u.shed by Dare/T,ee Company Rec eared Or Da•e T.,,,e cn rCc ro r
1
CustodySeals Intact CustodySeal No % y
N Coder Temjxrature!t)Y,and Other Remar+rs
Ti
O A Yes A No ,�
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Login Sample Receipt Checklist
Client: ERM-West Job Number:680-198096-1
Login Number: 198096 List Source:Eurofins TestAmerica,Savannah
List Number:1
Creator:Sims,Robert D
Question Answer Comment
Radioactivity wasn't checked or is</=background as measured by a survey N/A
meter.
The cooler's custody seal,if present,is intact. True
Sample custody seals,if present,are intact. True
The cooler or samples do not appear to have been compromised or True
tampered with.
Samples were received on ice. True
Cooler Temperature is acceptable. True
Cooler Temperature is recorded. True
COC is present. True
COC is filled out in ink and legible. True
COC is filled out with all pertinent information. True
Is the Field Sampler's name present on COC? True
There are no discrepancies between the containers received and the COC. True
Samples are received within Holding Time(excluding tests with immediate True
HTs)
Sample containers have legible labels. True
Containers are not broken or leaking. True
Sample collection date/times are provided. True
Appropriate sample containers are used. True
Sample bottles are completely filled. True
Sample Preservation Verified. N/A
There is sufficient vol.for all requested analyses,incl.any requested True
MS/MSDs
Containers requiring zero headspace have no headspace or bubble is True
<6mm(1/4").
Multiphasic samples are not present. True
Samples do not require splitting or compositing. True
Residual Chlorine Checked. NIA
Eurofins TestAmerica,Savannah
Page 13 of 13 5/4/2021