WQ0018525_2023 Residual Annual Report_20240223 (2)

Initial Review
Reviewer
nathaniel.thorn burg
Is this submittal an application? (Excluding additional information.) *
Yes No
If not an application what is the submittal type?* Annual Report
Residual Annual Report
Additional Information
Other
Annual Report Year* 2023
Permit Number (IR) * WQ0018525
Applicant/Permittee Barnes Environmental Waste and Hauling, Inc.
Email Notifications
Does this need review by the hydrogeologist? * Yes OO No
Regional Office Wilmington
CO Reviewer
Admin Reviewer Wanda Gerald

Submittal Form
Project Contact Information
Please provide information on the person to be contacted by NDB Staff regarding electronic submittal, confirmation of receipt, and other correspondence.
Name* Martin Mabe
Email Address*
[e-mail]
Project Information
.........................
Application/Document Type*
New (Fee Required)
Modification - Major (Fee Required)
Renewal with Major Modification (Fee
Required)
Annual Report
Additional Information
Other
Phone Number*
3363121396
Modification - Minor
Renewal
GW-59, NDMR, NDMLR, NDAR-1,
N DAR-2
Residual Annual Report
Change of Ownership
We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form.
https://edoes.deq.nc.gov/Forms/NonDischarge_Monitoring_Report
Permit Type:*
Wastewater Irrigation
High -Rate Infiltration
Other Wastewater
Reclaimed Water
Closed -Loop Recycle
Residuals
Single -Family Residence Wastewater
Other
Irrigation
Permit Number:*
WQ0018525
Has Current Existing permit number
Applicant/Permittee Address*
PO Box 654, Newport, NC 28570
Facility Name*
Barnes Environmental Class B Residuals Program
Please provide comments/notes on your current submittal below.
At this time, paper copies are no longer required. If you have any questions about what is required, please contact Nathaniel Thornburg
at [e-mail].
Please attach all information required or requested for this submittal to be reviewed here.
(Application Form, Engineering Plans, Specifications, Calculations, Etc.)
Barnes Environmental 2023 Annual Report WQ0018525.pdf 27MB
Upload only 1 PDF document (less than 250 MB). Multiple documents must be combined into one PDF file unless file is larger
than upload limit.
* By checking this box, I acknowledge that I understand the application will not be accepted for pre -review until the fee (if required) has
been received by the Non -Discharge Branch. Application fees must be submitted by check or money order and made payable to the
North Carolina Department of Environmental Quality (NCDEQ). I also confirm that the uploaded document is a single PDF with all parts
of the application in correct order (as specified by the application).
Mail payment to:
NCDEQ — Division of Water Resources
Attn: Non -Discharge Branch
1617 Mail Service Center
Raleigh, NC 27699-1617
Signature
Submission Date 2/23/2024

2023 ANNUAL REPORT
LAND APPLICATION PROGRAM
BARNES ENVIRONMENTAL WASTE AND HAULING, INC.
PERMIT #WQ0018525
WMSS Project No. 15-02 Ph: 01
Prepared for:
Barnes Environmental Waste and Hauling, Inc.
Post Office Box 654
Newport, North Carolina 28570
Compiled by:
Willcox & Mabe Soil Solutions, PLLC
7231B Summerfield Road
Summerfield, North Carolina 27358
February 2024

�1
willcox&mabe
SOIL SOLUTIONS
February 23, 2024
NCDEQ-DWR Non -Discharge Compliance Unit
512 North Salisbury Street
9th Floor, Office# 942X
Raleigh, North Carolina 27604
Attention: Non -Discharge Compliance Unit
Reference: 2023 ANNUAL REPORT FOR WQ0018525
Barnes Environmental Waste and Hauling, Inc.
WMSS, Inc. Project No. 15-02 Ph: 01
Non -Discharge Compliance Unit:
Willcox & Mabe Soil Solutions, PLLC (WMSS) is submitting all monitoring and reporting
requirements as specified in the above referenced permit on behalf of Barnes Environmental
Waste and Hauling, Inc. (Barnes Environmental Waste). WMSS compiled this report using
data gathered during the compliance year by Barnes Environmental Waste.
If there is any further information required or questions regarding this land application
program please do not hesitate to contact Mr. Steve Barnes, with Barnes Environmental
Waste 252-241-5014 for further assistance.
Sincerely,
Willcox & Mabe Soil Solutions, PLLC
i
i,
Martin Mabe
NC Land Application/Residuals Operator
#22753
EncIosure(s)
cc Barnes Environmental Waste
SharedlWMSS Proiects12015115-02 Barnes EnvironmentaI 2023 Annual Report12023 ANNUAL REPORT.doc
Willcox & Mabe Soil Solutions, PLLC 17231 B Summerfield Road I Summerfield, NC 273581 Rob 336,339,9128 or
Martin 336.312.13961 www.willeoxmabesoil.com

TABLE OF CONTENTS
SECTION NO. TITLE
Certification Form
II Residuals Analyses & Pathogen and Vector Attraction
III Application Summary and Field Loading Rate Reports
IV Soil Analysis

CERTIFICATION FORM

ANNUAL LAND APPLICATION CERTIFICATION FORM
WQ Permit#: WQ0018525 County: Carteret Year: 2023
Facility Name (as shown on permit): Barnes Environmental Waste and Hauling, Inc.
Land Application Operator: Steven M. Barnes Phone: [phone]
Land application of residuals as allowed by the permit occurred during the past calendar year?
0 Yes ❑ No - If No, skip Part A, and Part B and proceed to Part C. Also, If residuals were
generated but not land applied, please attach an explanation on how the residuals were handled.
Total number ofapplication fields in the f
Total number of fields utilized for land application during the
Total amount of dry tons applied during the year for all application sites: 22.61
Total number of acres utilized for land application during the year: 24.7
Part B - Annual Complianee Statement:
Facility was compliant during calendar year 2023 with all conditions of the land application permit
(including but not limited to items 1-13 below) issued by the Division of Water Quality. [�] Yes ❑ No
If no please, provide a written description why the facility was not compliant, the dates, and explain corrective
action taken.
1) Only residuals approved for this permit were applied to the permitted sites.
2) Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or
the limit specified in the permit.
3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies
of laboratory results are attached.
4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5) All other monitoring was performed in accordance with the permit and reported during the year as required and three
(3) copies of certified laboratory results are attached.
6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .1105(a) or the Pollutant
Loading Rates in 15A NCAC 02T .1105(b) (applicable to 40 CFR Part 503 regulated facilities).
7) All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part
503 re ;elated facilities).
8) All monitoring and reporting requirements in 15A NCAC 02T .1111 were complied with (applicable to 40 CFR Part
503 regulated facilities).
9) Al I operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Quality.
10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
11) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as
specified in the permit.
12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13) All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C - Certification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate,
and complete. I am aware that there are significant penalties for submitting false information, including the
possibility of fines and imprisonment for knowing violations."
Steven M. Barnes, President Stea &aLa
Permittee Name and Title (type or print) Signature of Permittee Date
Signature of Preparer* Date Signature of Land Applier Date
(if different from Pennittee) (if different from Permittee and Preparer)
* Preparer is defined in 40 CFR Part 503.9 (r) and 15A NCAC 02T .1102 (26)
DENR FORM ACF (12/2006)

RESIDUAL ANALYSES REPORTS AND
PATHOGEN AND VECTOR ATTRACTION REDUCTION

Permit Number W00016525
Facility Name Bames Environmental
NPDES # See Below
❑WPfP Name See Below
R@SIDIfAL ANALYSIS I1ATA
ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Attach ails form to the corresponding laboratory analysis.
Pleaso note that your permil may contain additional poramelom to be analyzed than those requited to be summarized an This farm.
Laboratory 1 1 Environment 1, Inc.
2 Environmental Chemists, Inc.
3
HPDES0
WOOD04059
WOOO13676
WOOOD5173
V1-15.17
V[-16.13
I V1.14.13
I W00003044
I W00000986
IVI-02-18
VI.13.17
VVYV'fP Name
Allanlic Station
Beacons Reach
Cape Royal
CC Sass
Cedar Point
Colony by Sea
Dunest:ape
Maud Beach
Hampton Suites
Mariner's Point
CampasitedlGrah
01119/23
01117l23
03/10/23
03/10123
03/10/23
B8122/23
02107123
08/17123
0021123
08/17123
..e Percent Solids _ `�
0.44
0.99
0,43
2.46
0.61
1.92
1.06
1.37
0,77'
0.58
Arsenic
1 2.50
2.50
45,80
19.90
3280
2.50
2.50
1 2.50
2.50
2.50
Cadmium
0.7D
IIA0
45.80
19,90
32.80
1-30
0.80
0.70
0.50
0.80
Copper
470.00
1.295.00
251.00
533.00
313.00
103.00
614.00
$72.00
1.159.00
657.00
Lead
12.00
14.00
45,80
19.90
32.80
6.90
14.00
7.80
5.40
7.60
Mercury
0.18
0.28
4,28
0.69
2.74
0.22
0.22
0.14
0.11
OA5
Molybdenum
5.00
6.50
45.80
19.90
32.80
5.00
5.00
5.90
5.00
5.00
Nickel
12.00
23.00
45.80
19,90
32.80
10.00
26.00
8.00
16.00
8.60
Selenium
5.00
5.00
45.80
19.90
32.80
5.00
5.00
5.00
5,00
5.00
Zinc
1.242.00
1.413.00
2,740 00
776.00
877.00
2,339.00
1,496.00
1,228.00
560.00
1.173.00
TKN
62.370.00
60.360-00
53,600.00
60,000.00
48.800.00
84.280.00
61,750.00
67,960.00
59.600.00
61,620.00
Ammonia -Nitrogen
32.72
105.10
4.620.00
1.310,00
4.560.00
525.00
391.30
414.70
130.90
49.94
Nltrele-Nilr en
7.93
4.96
12.300.00
1,090.00
1.130,00
7.98
8.98
4.99
29,99
3.99
Total Phosphorus
9,309 00
12,640.00
15.500,00
19,600,00
19,400,00
f7,470.00
19.532.00
30,590.00
15,590.00
23,540.00
RESIDUAL ANALYSIS DATA
NPDES#
V1-12-18
W00019321
W00003067 W00018420
VI-08•16
WOODD212B W00011313 WOOD00224
WQOD03437
WQ0000165
V4VvrP Name
1
McGinnis Paint
NC Aquarium
Ocean Bay Villas Ocean Club
Ocean Condos
Pebble Beach Peppertree Rosorl Point Emerald
queens Court
Sands Villa
CvmpvsitedlGrab
01117/23
01126/23
01126123 01/19123
02121/23
02121123 D1128l23 01112/23
03/10123
02/21123
Percent Solids
DAD AIe107COC r.....1L..­.....e..
2.14
1.09
0,74 0.43
1.41
0.96 0,68 0.66
1 1.09
0,61
Arsenic
2.50
2.50
2.50
2.50
12.00
2.50
2.50
2.50
18.20
2.50
Cadmium
0.90
6.20
0190
0.90
0.90
1.10
1.00
0.90
18.20
0.68
Cap er
1,728.00
23q,00
305.00
381,00
507.00
260.00
404.00
386.00
173.00
164.00
Lead
22.00
23.00
29.00
8,80
14.00
15.00
11.DO
37.00
18.20
5.70
Mercury
0.40
0.06
0,38
0.14
0.10
0.16
0,26
0.27
1.62
0.12
Mal bdenum
5.00
5.40
5,00
5.00
5.00
5.00
500
5.00
18.20
5,00
Nickel
17.00
20.00
11.00
11.00
12.00
12.00
13.00
13.00
18.20
8,70
Selenium
5.00
5.00
5.00
5.00
5.00
5,00
5.00
5.60
18.20
5.00
Zinc
1.533,00
750.00
1A63,00
2.575.00
1,108.00
2.692.00
2,183.00
2369.00
1.300.00
968.00
TKN
59,960.00
40.370.00
50.840.00
53.250.00
93.990.00
69,610.01)
43.470.00
38,650.00
44,000.00
66.730.00
Ammonia -Nitrogen
349.90
115.70
59.92
50.91
3.019-00
835.40
11.98
207.40
4,650,00
124.80
Nitrate -Nitrogen
2.98
9.97
72.91
5.99
5.00
24,98
4.99
5.58
84.50
19,97
TotaE Phosphorus
10,250.00
21.540.00
11,000.00
15.420.00
13,790,00
14.710.00
16,170.00
8,527.00
17.400.00
14,920.00
dea Eames
(SIGNATURE OF PREPARER) DATE
I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant
penalties for submitting false information, including the passibility or fines and Imprisonment for knowing violations.
Page 1

Permit Number W00018525
Facility Name Sames Environmental
NPDES# seeBelaw
WWTP Name See Below
RESIDUAL ANALYSIS DATA
ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Attach this form to the correspandinq laboratory analysis.
Pleare note that your pemvt may contain additional parameters to be analyzed than erase required to be summarized on this form.
Laboratory 1 Environment 1. Inc.
2 Environmental Chemists. Inc.
3�
NPOES 9 WQD013027
VI.03-17
WQ0007103
1 WCIGD16992
VI-12-17
WOD024756 Vr-20-15
VNMfP Name Sea We Plantation
Sea Spray
I Sound o1 the Soa
Soulhv4nds Condos
Summer Winds
The Grave Whaler Inn
Cam sited l Grab 01/19123
02121/23
I 021IW23
1 02121/23
02/21123
02141l23 08129123
Percent Solids 0,97
oaohasnre0e /,. -l- ��.._�,_­
0.97
1 0.64
1 0.99
0.76
0,69 1.58
Arsenic
2.50
2.50
2.50
2.50
2.5D
2.50
2.50
Cadmium
0.60
0.66
1.20
0.78
0161
0.59
0.80
Copper
364.00
710.00
1.352.00
665.00
421.00
106,00
693.00
Lead
31,00
8.20
34.00
12.00
6.90
5.00
8.70
Mercury
0.18
0,19
0.22
0,24
0.16
0.05
0.15
Molybdenum
5.00
5.00
5.00
S.OD
5.00
5.00
5.00
Nickel
13.00
12.00
12.00
9.80
10.00
1 11.00
12.00
Selenium
5.00
5.00
5.00
5.00
5.00
5.00
5.OD
Zinc
823.00
1,232.00
2.640.00
1.561.00
1.393,00
893.00
1.267,00
TKN
69.010.00
62.750.00
24,660A0
69,670.00
21,330.00
69.710.00
64,720, 00
Ammonia -Nitrogen
1,824.00
523.70
727.70
200.00
827.30
2.250.00
1,969.00
Nitrate -Nitrogen
6.98
9.00
4.98
9.00
35,120.00
16.00
4.00
Total Phosphorus
9.892.00
14,540.00
5,915.00
16,950.00
23,670.00
25,900,00
22,930.00
SO Ile Eames
x 1
(SIGNATURE OF PREPARER) DATE
I certify, under penally of law, that this document was prepared under my direction or supervision in accordance wllh a system designed
to assure that qualified personnel property gathered and evaluated the Information submitted, I am aware that there are significant
penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations.
Page 2

BARNES ENVIRONMENTAL WASTE
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled. January 19, 2023
Atlantic Station
Parameter
s
AN (injected)'
AN (surface)*
,mmonia Nitro
'alcium Carbonate
lagnesium _
odium
ulfur
litrate N 1 Nitrite N
arium
'hloride
Ic
ium
iium
Selenium
Zinc
Permit No. WQ0018525
0.44 % Solids
12.33 pH (taken from lime stabilization event)
%
Mg/Kg Dry Weight
(% x 10,000)
Pounds/Dry Ton
(Mg/Kg(Mg/Kg x 0.002)
0.723
62,3 70.000
t 24.740
0.263
9,309,000
18.618
0.449
5,955.000
11.910
0.255
2,545.830
5.092
0.228
2,282.330
4.565
0.053
32.720
0.065
3.558
29,890.000
59.780
---
5,233.000
10.466
- -
38,956.000
77.912
---
7.930
0.016
---
2,444.00
4.888
---
2.50
0.005
---
0.70
0.001
---
12.000
---
---
470.00
0.940
---
12.00
0.024
---
0.18
0.000
---
5.00
0,010
---
12.00
0.024
---
5.00
0.0I0
---
1,242.00
2.484
Environment I, Incorporated 108A
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N +Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits
for calculation purposes.
SA R
3.62
Ceiling Concen.
(mg/Kg)
75
85
4,300
840
57
75
420
100
7,500

E040nME(W % howpumUd
114 OAKMONT DRIVE
GREENVILLE, N.C. 27858
ATLANTIC STATION (FORTIN)
MR. DAN FORTIN
FORTIN CONTRACT SERVICES
P.O. BOX 4188
EMERALD ISLE, NC 28594
PARAMETERS
Aluminum, (dry wt. basis), mg/kg
Arsenic (dry wt, basis), mg/kg
Calcium (dry wt. basis), mg/kg
Cadmium (dry wt. basis), mg/kg
Copper (dry wt. basis), mg/kg
Chromium, T.(dry wt. basis),mglkg
Lead (dry weight basis), mg/kg
Magnesium (dry wt. basis), mglkg
Mercury (dry wvt. basis), mg/kg
Nickel (dry tut. basis), mgllcg
Potassium (dry wt. basis), mgllcg
Selenium (dry wt. basis), mg/kg
Sodium (dry wt. basis), mg/kg
Zinc (dry wt. basis), mg/kg
Total Solids, %
TKN (dry wt.), mgllcg
Ammonia Nitrogen (dry wt.),mg/lcg
Phosphorus, T. (dry wt.), mg/kg
Nitrate+Nitrite (dry wt.), mg/kg
Plant Available Nitrogen, mg/kg
Molybdenum (dry wt. basis), mg/kg
Sludge Analysis Method
Sample Date Analyst Code
2444
02/10/23
MTM
EPA200.7
<2.S
02/01/23
DRC
3113E-04
29890
02/10/23
MTM
EPA200.7
0.7
02/02/23
DRC
3113B-04
470
02/10/23
MTM
EPA200.7
12
02/10/23
MTM
EPA200.7
12
02/02/23
DRC
3113B-04
5233
02/10/23
MTM
EPA200.7
0.18
01/30/23
DRC
EPA7471B
12
02/10/23
MTM
EPA200.7
5955
02/10/23
MTM
EPA200.7
<5.0
02/02/23
DRC
3113E-04
38956
02/10/23
MTM
EPA200.7
1242
02/10/23
MTM
EPA200.7
0.44
01/24/23
HMV
254OG-15
c 62370
01/24/23
B1V1D
351.2 R2-93
c 32.72
01/26/23
KES
350.1 R2-93
c 9309
01/24/23
TRJ
365.4-74
c 7.93
01/26/23
BMD
353.2 R2-93
18726
02/03/23
BMD
<5.0
02/10/23
MTM
EPA200.7
Drinking Water ;Mt 37715
Wastewater ID: 10
PHONE [phone]
FAX [phone]
ID#: 108 A
DATE COLLECTED: 01/19/23
DATE REPORTED : 02/13/23
REVIEWED BY:
c Uncertified data. OWR dose not offer non -aqueous certification for this analytical procedure.

A
FO
P
E
Environment 1, Inc. CHAIN OF CUSTODY RECORD
P.O. Box 7095, 114 Oakmont Dr. Page 1 of x
Greenville. NC 27858
ei_--v i ran o lion t l i ne.com
Phone [phone] • Fax [phone]
CLIENT: 108 A Weep: 8
TLANTIC STATION (FORTIN)
R. DAN FORTIN
RTTN CONTRACT SERVICES
O. BOX 4188
MERALD ISLE NC 28594
52) 393-8720
COLLECTION
DISINFECTION
cHl.olzlNr:
UV
NONE
CHLORINE NEUTRALIZED AT COLLECTION
pH CHECK (LAB)
P
P
P
P
P
P
CONTAINER TYPE, PIG
A
A
A
A
A
A
CHEMICAL PRESERVATION
A - NONE D - NAOH
w
C B- HNO_ E- HCL
C- H,SO, F - ZINC ACETATEiNAOH
G NATHIQSULFATE
o
E
C7
z
o0
¢
o
U
LLi z
�-
u�
Uj -j
v
%" a
co
w
z
LL
o
o
F,
E^
z
.F
O
a;
+
Z
SAMPLE LOCATION
DATE
TIME
Sludge Sample
j 2
4•"
CLASSIFICATION:
WASTEWATER (NPOES)
DRINKING WATER
DWRIGW
SOLID WASTE SECTION
CHAIN OF CUSTODY (SEAL) MAINTAINED
DURIN6IMENTIDELIVERY
Y N
SAMPLES COLLECTED BY:
(Please Print} s�
AV-�� i
SAMPLES RECEIVED fN LAB AT - °C
INO�!lSHED BY (51G.} {SAMPLER)
U1.
DATErn
11 73 :0D
RECEIVED BY (SIG.)
~
DATE) IME
tlt�jz3 =i
COMMENTS:
R LINQUISHED Y (SIG.)
DATEMME
RECEIVED BY (SIG,)
DATEMME
REUNQUISHED BY (SIG.)
DATEMME
RECEIVED BY (SIG.)
DATEITIME
PLFASE READ Instructions for completing this form on the reverse side. Sampler must place a "C" for composite sample or a "G for FORM Its Grab sample in the blocks above for each parameter requested. NQ 412688

BARNES ENVIRONMENTAL WASTE
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: January 17, 2023
Permit No. WQ0018525
Beacons Reach 0.99 % SoIids
6.2 p H
Parameter
%
7gfKg Dry Weight
(% x 10,000)
Pounds/Dry Ton
(M /K x 0.002)
Nitrogen (TKN)
6.036
60,360.000
120.720
Phosphorus
I.264
12,640,000
25.280
Potassium
0.503
5,034.000
10.068
PAN (injected)*
1.819
18,186.530
36.373
PAN (surface)*
1.813
18,133,980
36.268
Ammonia Nitrogen
0.011
105.100
0.210
Calcium
3.224
32,238.000
64.476
Calcium Carbonate L .
---
--..
---
Magnesium
---
3,814.000
7.628
Sodium
---
14,975.000
29.950
Sulfur
---
---
Nitrate N / Nitrite N
---
4.960
0.010
Barium
---
---
---
Chloride
---
---
---
Iron
---
---
---
Aluminum
---
2,401.00
4.802
Arsenic
---
2.50
0.005
Cadmium
---
1.400
0.003
Chromium
---
15.000
---
Co er
---
1,295.00
2.590
Lead
---
14.00
0.028
Mercury
---
0.28
0.001
Molybdenum
---
6.50
0.013
Nickel
---
23.00
0.046
Selenium
--- 1
5.00
0.010
Zinc
--- 1
1,413.00
2.826
Environment 14 554A
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits
for calculation purposes.
SAR
172.09
Ceiling Concen.
(M /K )
75
85
4,300
840
57
75
420
100
7,500

&W,nfln(W % hmpufflUd
114 OAKMONT DRIVE
GREENVILLE, N.C. 27858
BEACON'S REACH I/POND (HYDROTECH)
EMAIL DATA & COC
NO MAILED COPY
PARAMETERS
PH (not to be used for reporting)
Aluminum, (dry wt. basis), mg/kg
Arsenic (dry wt. basis), mg/kg
Calcium (dry wt. basis), mg/kg
Cadmium (dry wt. basis), mg/lig
Copper (dry wt. basis), mg/kg
Chromium, T.(dry wt. basis),mglkg
Lead (dry weight basis), mg/kg
Magnesium (dry wt. basis), mg/kg
Mercury (dry wt. basis), mg/kg
Nickel (dry wt. basis), mg/lig
Potassium (dry wt. basis), mg/kg
Selenium (dry wt. basis), mg/kg
Sodium (dry wt. basis), mg/kg
Zinc (dry wt. basis), mg/lig
Total Solids,
TIN (dry wt.), mg/lig
Ammonia Nitrogen (dry wt.),mglkg
Phosphorus, T. (dry wt.), mg/kg
Nitrate+Nitrite (dry wt.), mg/lig
Molybdenum (dry wt. basis), mg/kg
Sludge Analysis Method
Sample Date Analyst Code
6.2
01/17/23
JMS
450ORB-11
2401
02/10/23
MTM
EPA200.7
c 2.5
02/01/23
DRC
3113B-04
32238
02/10/23
MTM
EPA200.7
1.4
02/02/23
DRC
3113B-04
1295
02/10/23
MTM
EPA200.7
15
02/10/23
MTM
EPA200.7
14
02/02/23
DRC
3I13B-04
3814
02/10/23
MTM
EPA200.7
0.28
01/30/23
DRC
EPA7471B
23
02/10/23
MTM
EPA200.7
5034
02/10/23
MTM
EPA200.7
5.0
02/02/23
DRC
3113B-04
14975
02/10/23
MTM
EPA200.7
1413
02/10/23
MTM
EPA200.7
0.99
01/17/23
JDJ
2540G-15
c 60360
01/24/23
BMD
351.2 R2-93
c 105.1
01/26/23
KES
350.1 R2-93
c 12640
01/24/23
TRJ
365.4-74
c 4.96
01/26/23
BMD
353.2 R2-93
6.5
02/10/23
MTM
EPA200.7
Drinking Water ID: 37715
Wastewater ID: 10
PHONE [phone]
FAX [phone]
ID#: 554 A
DATE COLLECTED: 01/17/23
DATE REPORTED : 02/13/23
REVIEWED BY:
c Uncertified data. ➢WR does not offer non-aqueaue certification ear this analytical procedure.

Environment 1, Inc. CHAIN OF CUSTODY RECORD
P.O. Box 7085. 114 Oakmont Dr. Page 1 of 1
Greenville. INC 27855
environincr.tl inc.ccnn
DISINFECTION
CHLORINENEUTRALIZEDATCOLLECTION
Phone f.25'?1 75ti-f�248 • Fax (2.5?) 756-0633
CHLORINE
CLIENT: 554 A Week: 8
UV
pH CHECK (LAB)
EACON'S REACH IIPOND (HYDROTECH)
_NONE
P
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CONTAINERTYPE, NG
TTN: DON O'MARA
IYDROTECH
CHEMICAL PRESERVATION
.O. SOX 4602
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1VIERALD ISLE NC 28594
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SAMPLE LOCATION
DATE
TIME
Sludge Sample
l
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CLASSIFICATION:
WASTEWATER(NPDES)
DRINKINGWATER
DWRIGW
SOLID WASTE SECTION
CHAIN OF CUSTODY (SEAL) MAINTAINED
DURING SHIPMENT/DELIVERY
�Y N
SAMPLES COLLECTED BY:
(Please 'nt}
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SAMPLES RECEIVED IN LAB AT—A7-. 0 °C
RELI DISHED BY (SIG.) (SAMPLER)
DATEMME
RECEIVED BY (SIG.)
ATEMME
COMMENTS:
RELINQUISHED BY (SIG.)
DATEMME
RE IVED BY (SIG.)
DATEMME
RELINQUISHED BY (SIG.)
DATEMME
RECEIVED BY (SIG.)
DATE HME
PLEASE READ Instructions for completing this form on the reverse side. Sampler must place a "C" for composite sample or a "G" for o
FORM N5 Grab sample in the blocks above for each parameter requested. 41 3048

BARNES ENVIRONMENTAL WASTE
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: March 10, 2023
Permit No. WQ0018525
Cane Royal Dolphin 0.43 % Solids
6.88 pH
Parameter
%
Mg/Kg Dry Weight
(% x 10,000)
Pounds/Dry Ton
(Mg/Kg(Mg/Kg x 0.002)
Nitrogen (TKN)
5.360
53,600.000
107.200
Phosphorus
1.550
15,500.000
31.000
Potassium
0.500
5,000.000
10.000
PAN (injected)*
3.161
31,614.000
63.228
PAN (surface)*
2.930
29,304.000
58.608
Ammonia Nitrogen
0.462
4,620.000
9.240
Calcium
1.710
17,100.000
34.200
Calcium Carbonate E .
---
---
Magnesium
- -
3,230,000
6.460
(Sodium
---
42,600.000
85.200
Sulfur
___
___
Nitrate N / Nitrite N
---
12,300.000
24.600
Barium
---
Chloride
---
___
.,.-
Iron
---
---
_--
Aluminum
---
3,810.00
7.620
Arsenic
---
45.80
0.092
Cadmium
---
45.80
0.092
Chromium
---
45,800
Copper
---
251.00
0.502
Lead
---
45.80
0.092
Mercury
---
4.280
0.009
Molybdenum
---
45.80
0.092
Nickel
---
45.80
0.092
Selenium
---
45.80
0.092
Zinc
---
2,740.00
5.480
Envirochem # 2023-04005
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) +Nitrate N + Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or < detection limits are Iisted as detection limits
for calculation purposes.
SAR
5.12
Ceiling Concen.
(MIK)
75
85
4,300
840
57
75
420
100
7,500

t Environmental Chemists, .Inc.
® 6602 Windmill Way, Wilmington, NC 2W5 '.: 910.392.0223 Lab o 910.392.4424 Fax
710 Bowsertown road, Manteo, NC 27954 •-252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 '1 910.347.5843 Lab/Fax
ANALYTICAL. CONSULTING CHEMISTS infotd3environmentalchemists.com
Fortin Contract Services Date of Report: Mar 10, 2023
Post Office Box 4188 Customer PO M
Emerald We NC 28594 Customer ID: 08100061
Attention: Dan Fortin Report #• 2023-04005
Project ID, Cape Royal Sludge
Lab ID Sample ID: Collect DatelTime Matrix Sampled by
23-09925 Site: Sludge 2/28/2023 8:45 AM Solid/Sludge Kevin Stanley
Test Method Results Date Analyzed
Sludge Reslduats
Aluminum
Arsenic
Cadmium
Calcium
Chromium
Copper
Lead
Magnesium
Molybdenum
Nickel
Potassium
Selenium
Sodium
Zinc
Nitrate+Nitrite-Nitrogen
Total Solids (%)
Ammonia Nitrogen
EPA 200.7. Rev,-4.4. 1994
EPA 2001. Rev. 4.4. 1994
EPA 2002. Rev: 4.4, 1994
EPA,240.7; Rev._4A; 1994
EPA 200,7, Rev, 4-4,1994
EPA 200.7, Rev, 4.4,1 D04
EPA 200.7, Rev. 4.4, 1994
EPA 200.7. Rev, 4.4, 1094
EPA 200.7. Rev, 4A, 1994
EPA 200.7. Rev, 4.4, 1994
EPA 200.7, Rev. 4.4. 1904
EPA 200.7, Rev,AA 1094
EPA 200.7, Rev. 4.4;1994
EPA 200.7,. Rev, 4.4,1094
EPA 353,2
SM 2640 0
SM 4500 NH3 C-2011
Total Kjeldahl Nitrogen (TKN) SM 4500 Norg B-2011
Total Phosphorus SM 4500 P (F•H)-2011
PM SW e46 Melhod 0046D
Result estimated. Analyzed out of 15 minutes hold time.
3810 mglkg
<45.8 mglkg
<45.8 mg/kg
17100 mglkg
<46.8 mglkg
251. rnglkg
<45.8 mglkg
$230 mglkg
<45.8 mg/kg
<45.8 mglkg
5000 mglkg
<45.8 mglkg
42600 mglkg
2740 mglkg
12300 mglkg
0,43 %
4620 mg/kg
53600 mg/kg
15500 mglkg
6.88 units
03/01/2023
03/01/2023
03/01/2023
03101/2023
03/01/2023
03/01/2023
03/01/2023
03/0112023
0310112023
03/01/2023
03/01/2023
03/01/2023
03/01/2023
03/01/2023
03/01/2023
03/01/2023
03/01/2023
03/01/2023
03/08/2023
03101 /2023
Mercury SW-1146 74718 <4.28 mglkg 03/03/2023
ReportV.; 2023-0400ti -- - - Pape 1 oT2

BARNES ENVIRONMENTAL WASTE
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: March 10, 2023
Permit No. WQ0018525
CC Sass 2.46 % Solids
6.97 n14
Parameter
%
Mg/Kg Dry Weight
(% x 10,000)
Pounds/Dry Ton
(Mg/Kg x 0.002)
Nitrogen (TKN)
6.000
60,000.000
120.000
Phosphorus
1.960
19,600.000
39.200
Potassium
0.732
7,320.000
14.640
PAN (injected)*
2.001
20,007.000
40.014
PAN (surface)*
1.935
19,352.000
38.704
Ammonia Nitrogen
0.131
1,310.000
2.620
Calcium
1.470
14,700.000
29.400
Calcium Carbonate E .
---
---
---
Magnesium
---
4,430.000
8.860
Sodium
---
9,110.000
18.220
Sulfur
---
---
Nitrate N / Nitrite N
---
1,090.000
2.180
Barium
---
---
---
Chloride
---
---
---
Iron
---
---
---
Aluminum
---
1,130.00
2.260
Arsenic
---
19.90
0.040
Cadmium
---
1990
0.040
Chromium
---
19.900
0.040
Copper
---
533.00
1.066
Lead
---
19.90
0.040
Mercury
---
0.687
0.001
Molybdenum
---
19.90
0.040
Nickel
--- 1
19.90
0.040
Selenium
---
19.90
0.040
Zinc
---
776.00
1.552
f
I
Envirochem # 2023-04008
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N - % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0,5)(Ammonia N) + Nitrate N + Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits
for calculation purposes.
SAR
2.64
Ceiling Concen.
75
85
840
57
75
420
100
7.501

Environmental Chemists, Inc.
0 6602 Windmill Way, Wilmington, NC 28403 - 910.392.0223 Lab `f, 910,392.4424 Fax
710 Bowsectown Road, Manteo, NC 27954 4 252,473,5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910,347.5943 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS info@en%rironmentalchemists,com
Fortin Contract Service& Date of Report: Mar 10, 2023
Post Office Box 416E Customer PO #:
Emerald isle NC 28594 Customer ID: 08100061
Attention: Dan Fortin Report 2020
Proje #CSA5udge6
Lab ID Sample ID:
Collect DatefTime
Matrix Sampled by
23-09928 Site: Sludge
2/28/2023 9:15 AM
Solid/Sludge Kevin Stanley
Test
Method
Results Date Analyzed
Sludge Residuals
Aluminum
EPA 200.7,Ray, 4.4,1994
1130mg/kg
03/01/2023
Arsenic
EPA2001,Rav,.4.4,1994
<19.9mglkg
03/01/2023
Cadmium
EPA 200.7. Ray. 4A,1994
<19,9mg/kg
03/01/2023
Calcium
EPA200.7, Rev.4.4,1994
14700mglkg
03/01/2023
Chromium
EPA 200.7, Rev, 4.4,1994
<19.9 rriglkg
03/01/2023
Copper
EPA 200,7. Rev. 4.4,1904
533 mglkg
03/01/2023
Lead
EPA 200.7, Rev. 4.4.1004
<19.9 mglkg
03/01/2023
Magnesium
EPA 200.7, Rev. 4.4.1904
4430 mglkg
03/01/2023
Molybdenum
EPA 200.7. Rev. 4.4,1994
<19,9 mglkg
03/01/2023
Nickel
EPA200.7, Rev.4.4,1094
<19.9 mglkg
03/01/2023
Potassium
EPA 200.7. Rev, 4.4, 1994
7320 mg/kg
03/01/2023
Selenium
EPA 200.7, Rev. 4A,19e4
<19.9 mg/kg,
03/01/2023
Sodium
EPA 200.7, Rev. 4.4,1994
9110 mg/kg
03/01/2023
zinc
EPA 200.7. Rev. 4.40994
776 mglkg
03/01/2023.
Nitrate*Nitrite=Nitrogen
EPA353.2
1090mglkg
03/02/2023
Total Solids (%)
SM 2540 B
2,46 %
03/0112023
Ammonia Nitrogen
SM4500NH3 C.2011
1310mglkg
03/01/2023
Total Kjeldahl Nitrogen (TKN)
SM4500 Norg B-2011
60000 mglkg
03/01/2023
Total Phosphorus
SM 4500 P (F.fi).2011
19600 mglkg
03/0812023
PH
Resultes*nated,. Analyzed out of
SW e46 Method 9045D
15 minutes hold time,
6.97 units
03/01/2023
Mercury sW-8407471a <0.687mg/kg 03/03/2023
Raport Bi;' 2o2a at4oa -, Page 1 of 2

BARNES ENVIRONMENTAL WASTE
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: March 10, 2023
Permit No. WQ0018525
Cedar Point 0.61 % Solids
7.37 pH
Parameter
%
Mg/Kg Dry Weight
(% x 10,000)
PoundslDry Ton
(Mg/Kg(Mg/Kg x 0.002)
Nitrogen (TKN)
4.880
48,800.000
97.600
Phosphorus
1.940
19,400.000
38.800
Potassium
0.687
6,870.000
13.740
PAN (injected)*
1.896
18,962.000
37.924
PAN (surface)*
1.668
16,682,000
33.364
Ammonia Nitrogen
0.456
4,560.000
9.120
Calcium
I.930
19,300.000
38.600
Calcium Carbonate E .
---
---
---
Magnesium
---
4,110.000
8.220
Sodium
---
23,000.000
46.000
Sulfur
___
---
---
Nitrate N / Nitrite N
---
1,130.000
2.260
Barium
---
---
---
SAR
3.05
Chloride
---
---
Iron
---
---
C iling Concen.
(Mg/Kg)
Aluminum
---
3,340.00
6.680
Arsenic
---
32.80
0.066
75
Cadmium
---
32.80
0.066
85
Chromium
---
36.400
---
---
Copper
---
313.00
0.626
4,300
Lead
---
32.80
0.066
840
Mercury
---
2.74
0.005
57
Molybdenum
---
32.80
0.066
75
Nickel
---
32.80
0.066
420
Selenium
---
32.80
0.066
100
Zinc
---
877.00
1.754
7,500
> nvirodicra # 2023-04006
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
Surface Application;
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits
for calculation purposes.

Environmental Chemists, Inc.
" 6 6602 Windmill Way, Wilmington, NC 2M5. x: 910,392.0223 Lab 0 910.392.4424 Fax
® 710 Bowsertown Road, Manteo, NC 27954 ... 252.473.57b2 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 .. 910.347,580 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS info@environmentalchemismeom
Fortin Contract Services Date of Report: Mar 10, 2023
Post Office Box 4188 Customer PO #:
Emerald Isle NC 28594 Customer ID: 08100061
Attention: Dan Fortin Report#: 2023-04006
Project ID: Cedar Point Sludge
Lab ID sample ID:
Collect DateiTime
Matrix Sampled by
23-09926 Site: sludge
2/28/2023 6:30 AM
Solid/Sludge Kevin Stanley
Test
Method
Results hate Analyzed
Sludge Residuals
Aluminum
EPA 20q.7, Rev. 4,4,11984
3340 mglkg
03/0112023
Arsenic
EPA 200.7, Rev. 4,411904
<32.8 mglkg
0310112023
Cadmium
EPA 200.7. Rev.4,4; 1994
<32.8mglkg
03/01/2023
Calcium
EPA 200.7, Rev A.4,109a
19300 mglkg
0310112023
Chromium
EPA 200.7. Rev, 4,4,1994
36.4 mglkg
03101 /2023
Copper
EPA 200,7, Rev, 4.4, 104
313 mg/kg'
03/01/2023
lrt3ad
.. erPA 200.7, Rev. 4.4, 1994
<32,8 mglkg
03/01/2023
Magnesium
EPA 200.7, Rev, 4.4,1994
4110 mglkg
03/01/2023
Molybdenum
EPA 200.7, Rev. 4.4. 104
<32.8 mg/kg
03/01/2023
Nickel
EPA 240,7, Rev. 4-4,1994
<32.8 mglkg
03/01/2023
Potassium
EPA 200.7. Ray. 4A. 1994
6870 mglkg
03/01/2023
Selenium
EPA 200.7, Rev._ 4.4. 1894
<32.8 mglkg
03/01/2023
Sodium
t:t;A 200.7, Rev. 4.4, 1904
23000 mglkg
03/01/2023
Zinc
EPA 200.7, Rev. 4.4,1094
877 mglkg
03/01/2023
Nitrate+N61te-Nitrogen
EPA 353,2
1130 mglkg
03101 /2023
Total Solids (a/o)
SM2540 a
0161 %
03/01/2023
Ammonia Nitrogen
SM 460a NH3 0-2011
4560 mg/kg
03/01/2023
Total Kjeldahi Nitrogen (TKN)
SM 4600 Norg @-2011
48800 mglkg
03/01/2023
Total Phosphorus
5M 4600 P (F•H)-2011
19400 mglkg
03/08/2023
PH
Result estimated. Analyzed out of
5W 846 Method 00450
15 minutes hold time.
7.37 units
03/01/2023
Mercury SW-84e 7471 B- <2.74 mglkg 03/03/2023
PABe 1.612

BARNES ENVIRONMENTAL WASTE
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: August 22, 2023
Colony By The Sea
Parameter
otassium
AN (inje
AN (surf
t,alcium
Calcium Carbonate:
Magnesium
Sodium
Sulfur
Nitrate N / Nitrite N
Barium
Iron
Aluminum
Arsenic
Lead
Permit No. WQ0018525
1.92 % Solids
12.38 pH (taken from lime stabilization event)
/o
Mg/Kg Dry Weight
(% x 10,000)
Pounds/Dry Ton
(Mg/Kg x 0.002)
8.428
84,280.000
168.560
1.747
17,470.000
34.940
0.398
3,979.000
7.958
2.566
25,659.480
51.319
2.540
25,396.980
50.794
0.053
525.000
1.050
2.361
23,610.000
47.220
---
3,640.000
7,280
---
5,805.000
11.610
---
7,980
0.016
---
2,367.00
4.734
---
2.50
0,005
---
1.30
0.003
---
12.000
---
---
183.00
0.366
---
6.90
0.014
---
0.22
0.000
---
5.00
0.010
---
10.00
0.020
---
5.00
0.010
---
2,339.00
4.678
Environment 1 # 616A
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits
for calculation purposes.
SAR
1.28
Ceiling Concen.
(Mg/Kg)
75
85
4,300
840
57
75
420
100
7,500

Waypoint,"'w';'
ANALYTICAL
114 OAKMONT DRIVE
GREENVILLE, NC 27858
COLONY BY THE SEA (HYDROTECH)
EMAIL DATA & COC
NO MAILED COPY
PARAMETERS
Aiuminurn, (dry wt. basis), mg/kg
Arsenic (dry wt. basis), mg/kg
Calcium (thy wt. basis), mgllcg
Cadmium (dry wt. basis), rug/kg
Copper (dry wt. basis), mgll(g
Chromium, T*lry wt. basis),niglkg
Lead (dry weight basis), ing/hg
Magnesium (dry wt. basis), mgllcg
Mercury (dry wt. basis), mgllcg
Nickel (dry wt. basis). mg/kg
Potassium (dry wt. basis), mgllcg
Selenium (dry wt. basis), mg/kg
Sodium (dry wt. basis), mgllcg
Zinc (dry wt. basis), mg/lcg
Total Solids, %
TKN (dry wt.), mg/kg
Ammonia Nitrogen (dry wt.),mglkg
Phosphorus, T. (dry wt.), mgllcg
Nitrate+Nitrite (dry wt.), mg/kg
Plant Available Nitrogen, mgllcg
Molybdenum (dry wt. basis), mg/kg
Sledge Analysis Method
Sample Date Analyst Code
2367
09/06/23
MTM
EPA200.7
<2.5
09/07/23
DRC
3113B-04
23610
09/06/23
NITNI
EPA200.7
1.3
09/07/23
DRC
3113B-04
183
09/06/23
MTNI
EPA200.7
12
09/06/23
MTM
EPA200.7
6,9
09/07/23
DRC
3113B-04
3640
09106/23
NITM
EPA200.7
0.22
08/30/23
DRC
EPA7471B
10
09/06/23
MTM
EPA200.7
3979
09/06/23
NITNI
EPA200.7
<5.0
09/06/23
DRC
3113B-04
5805
09/06/23
N[TM
EPA200.7
2339
09/06/23
MTM
EPA200.7
1.92
08/24/23
HMV
2540GI5
c 84280
08/29/23
AMC
351.2 R2-93
c 525.0
08/30/23
AMC
350.1 R2-93
c 17470
08/29/23
AMC
365.4-74
c 7.98
08/28/23
AMC
353.2 R2-93
17022
09/01/23
BMD
<5,0
09/06/23
MTM
EPA200.7
Drinking Water ID: 37715
Waotawa ter ID: 10
PHONE [phone]
FAX [phone]
ID#: 616 A
DATE COLLECTED: 08/22/23
DATE REPORTED : 09/08/23
REVIEWED BY:
c Uncertified data, DWR does not offer non -aqueous certification for this analytical procedure.

Wayp int® CHAIN OF CUSTODY RECORD
Waypoint Analytical - Greenville Page I of
Greenville, NC 27858
DISINFECTION
CHLORINE NEUTRALIZEDg/L-Ye)
www.Wa ointAnal tical.com
YP Y
or No (ECTION
To �0.5 rnglL -Yes (Y} or No (N)
Phone [phone] • Fax [phone]
CHLORINE
ID
CLIENT: 616 A Week: S
pH CHECK (S.U.) (LAB)
Ijuv
CONTAINER TYPE, PIG
COLONY BY THE SEA (HYDROTECH)
41NONE
EMAIL DATA & COC
NO MAILED COPY
A
CHEMICALPRESERVATION
NC 25594
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(252)725'2319
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SAMPLELOCATION
DATE
TIME
Sludge Sample �� '
lZ�
, ��
4
t;:'k
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CLASSIFICATION:
FA WASTEWATER(NPDES)
DRINKING WATER
DWRIGW
SOLI D WASTE SECTION
CHAIN OF CUSTODY (SEAL) MAINTAINED
DURING SHIPMENT/DELIVERY
�1(1 N
SAMPLES COLLECTED BY:
(Please Print)
SAMPLES RECEIVED 1N LABAT� °C
R I DISHED BY (SIG.) (SAMPLER)
DATEITIME
RECEIVED BY SIG
QATEMM
COMMENTS:
SAMPLES RECEIVED ON ICE: - NO
-LLNjvj
_
'D
RELINQUISHED BY (SIG.)
DATEMME
RFCENtF.P BY (SIG.)
DATEITIME
RELINQUISHED BY (SIG.)
DATEInME
RECEIVED BY (SIG.)
DATE TME
PLEASE READ Instructions for completing this form on the reverse side. Sampler must place a "C" for composite sample or a "G" for
FORM 95 Grab sample in the blocks above for each parameter requested.

BARNES ENVIRONMENTAL WASTE
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: February 7, 2023
Permit No. WQ0018525
Dun^ escape 1.06 % Solids
7.3 pR
Parameter
%
Mg/Kg Dry Weight
(% x 10,000)
Pounds/Dry Ton
(Mg/Kg(Mg/Kg x 0.002)
Nitrogen (TKN)
6.175
61,750.000
123.500
Phosphorus
1.953
19,532.000
39.064
Potassium
0.444
4,443.000
8.886
PAN (injected)*
1.881
18,807.890
37.616
PAN (surface)*
1.861
18,612.240
37.224
Ammonia Nitrogen
0.039
391.300
0.783
Calcium
3.786
37,857.000
75.714
Calcium Carbonate E .
---
---
---
Magnesium
---
3,091.000
6.182
Sodium
---
13,435.000
26.870
Sulfur
---
Nitrate N / Nitrite N
---
8.980
0.018
Barium
---
---
---
SAR
1.83
Chloride
---
---
---
Iron
---
....
---
Ceiling Concen.
(Mg/Kg)
Aluminum
---
2,860.00
5.720
Arsenic
---
2.50
0.005
75
Cadmium
---
0.80 1
0.002
85
Chromium
---
13.000
---
---
Copper
---
614.00
1.228
4,300
Lead
---
14.00
0.028
840
Mercury
---
0.22
0.000
57
Molybdenum
---
5.00
0,010
75
Nickel
---
26.00
0.052
420
Selenium
---
5.00
0.010
100
Zinc
---
1,496.00
2,992
7,500
Environment 14 556 A
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits
for calculation purposes.

Emko ffo l % 4wPuMd
114 OAKMONT DRIVE
GREENVILLE, N.C. 27858
DUNESCAPE (HYDROTECH)
EMAIL DATA & COC
NO MAILED COPY
PARAMETERS
PH (not to be used for reporting)
Aluminum, (dry wt. basis), mg/kg
Arsenic (dry wt. basis), mg/kg
Calcium (dry wt. basis), mg/kg
Cadmium (dry wt. basis), mg/kg
Copper (dry wt. basis), mg/kg
Chromium, T.(dry wt. basis),mglkg
Lead (dry weight basis), mg/kg
Magnesium (dry wt. basis), mg/kg
Mercury (dry wt. basis), mg/kg
Nickel (dry wt. basis), mglkg
Potassium (dry wt. basis), mg/kg
Selenium (dry wt. basis), mg/kg
Sodium (dry wt. basis), mg/kg
Zinc (dry wt. basis), mg/kg
Total Solids, %
TKN (dry wt.), mg/kg
Ammonia Nitrogen (dry wt.),mglkg
Phosphorus, T. (dry wt.), mg/kg
Nitrate+Nitrite (dry wt.), mg/kg
Molybdenum (dry wt. basis), mg/kg
Sludge Analysis Method
Sample Date Analyst Code
7.3
02/07/23
BLV
4500HB-11
2860
02/15/23
MTM
EPA200.7
2.5
02/16/23
DRC
3113E-04
37857
02/15/23
MTM
EPA200.7
0.8
02/16/23
DRC
3113B-04
614
02/15/23
MTM
EPA200.7
13
02/15/23
MTM
EPA200.7
14
02/16/23
DRC
3113E-04
3091
02/15/23
MTM
EPA200.7
0.22
02/23/23
DRC
EPA7471B
26
02/15/23
MTM
EPA200.7
4443
02/15/23
MTM
EPA200.7
C 5.0
02/17/23
DRC
31138-04
13435
02/15/23
MTM
EPA200.7
1496
02/15/23
MTM
EPA200.7
1.06
02/07/23
JMS
254OG-15
c 61750
02/14/23
BMD
351.2 112-93
c 39L3
02/15/23
TRJ
350.1 R2-93
c 19532
02/14/23
TRJ
365.4-74
c 8.98
02/14/23
BMD
353.2 R2-93
c 5.0
02/15/23
MTM
EPA200.7
Drinking Water ID: 3771s
Wastewater ID: 10
PHONE [phone]
FAX [phone]
ID#: 556 A
DATE COLLECTED: 02/07/23
DATE REPORTED : 02/24/23
REVIEWED BY:
c Uncertified data. DWR does not offer non -aqueous certification for this analytical procedure.

Environment 1, Ilnc. CHAIN OF CUSTODY RECORD
P.O. Box 7085, 1 14 Oakmunr Dr, Page 1 nl-
Greenville. NC 27858
environmer d inc-cwn
DISINFECTION
CHLORINE NEUTRALIZED AT COLLECTION
t'liane [phone] • Fax t252) 756-0E33
Ij CFII.ORINL
CLIENT: 556 A Week: 8
pH CHECK (LAS)
Ij uv
P
P
P
P
P
P
P
CONTAINERTYPE,P/G
UNESCAPE(HYDROTECH)
Nt'-
TTN: DON O'MARA
YDROTECH
CHEMICAL PRESERVATION
.O. BOX 4602
A
A
AlA
A
A
A
MERALD ISLE NC 28594
A NONE D NAOM
z
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725-2319
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Slu a Sam le
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5
A` 112
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CLASSIFICATION:
WASTEWATER(NPDES)
DRINKING WATER
DWRlGW
SOLID WASTE SECTION
CHAIN OF CUSTODY (SEAL) MAINTAINED
DURING�k"ENT/DELIVERY
N
SAMPLES COLLECTED BY:
(Please Prinl)
SAMPLES RECEIVED IN LAB AT .S• Z� cC
REUNQ (SHED BY (SIG.) (SAMPLER)
DATErrIME
RECEIVED BY (SIG.)
DATEfiIME
COMMENTS:
2--�-z ZS
RELINQUISHED BY (SIG.)
DATETIME
RECEIVED BY (SIG.)
D TFJTIME
RELINQUISHED BY (SIG.)
DATEIiME
RECEIVED BY (SIG.)
DATEfRME
Sampler must place a T" for composite sample or a "G" for
PLEASE READ Instructions for completing this form on the reverse side.
FORM #5 Grab sample in the blocks above for each parameter requested. N-o
413047

114 OAKMONT DRIVE
GREENVILLE, N.C. 27858
DUNESCAPE (HYDROTECH)
EMAIL DATA & COC
NO MAILED COPY
PARAMETERS
BOD, mg/I
Fecal Coliform (MF'), I100 Mls
Total Suspended Residue, mg/I
Ammonia Nitrogen as N, mg/I
Total IGjeldahl Nitrogen as N,mg/I
Nitrate+Nitrite as N, mg/l (calc)
Nitrate Nitrogen as N, mg/I
Nitrite Nitrogen as N, mg/1
Total Phosphorus as P, mg/l
Total Nitrogen, mg/I (calc)
Effluent
Analysis
Method
Date Analyst
Code
<2.0
02/14/23
ADR
5210B-16
< 1
02/14/23
BNC
9222D-15
L <2.5
02/15/23
BLV
254OD-15
<0.04
02/22/23
BMD
350.1 R2-93
2.32
02/21/23
BMD
351.2 R2-93
0.20
353.2 R2-93
0.20
02/15/23
BMD
353.2 R2-93
<0.02
02/15/23
TRJ
353.2 112-93
0.69
02/21/23
TRJ
365.4-74
2.52
Drinking Water IDt 37715 _
wastewater ID: 10
PHONE [phone]
FAX [phone]
ID#: 556 B
DATE COLLECTED: 02/14/23
DATE REPORTED ; 02/24/23
REVIEWED BY: ✓�V
All QC requirements were not met: L Laboratory Control Sample exceeded control limits.

Environment 1. Inc. CHAIN OF CUSTODY RECORD
P.O. Box 7085, 114 Oakmont Dr. gage I of
(;rrnnvillr� tV(' �7RSR
em;�ronmeiyt I inc.com
DISINFECTION
CHLORINE NEUTRALIZED AT COLLECTION
Phone [phone] • Fax [phone]
Ij CHLORINE
(L
pH CHECK (LAB)
CLIENT: 556 B Week: 13
)UAIESCAPE(HYDROTECH)
NONE
P
P
P
P
P
P
P
P
P
CONTAINER TYPE,P/G
CHEMICALPRESERVATtON
;MAIL DATA & COC
10 MAILED COPY
A
C
C
C
A
A
C
NC 28594
co A -NONE D-NAOH
�
252) 725-2319
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SAMPLELOCATION
DATE
TIME-NATHIOSULFATE
Effluent
5
::
--.4.
-::.
CLASSIFICATION:
WASTEWATER(NPDES)
IF
DRINKING WATER
DWRIGW
SOLID WASTE SECTION
CHAIN OF CUSTODY (SEAL) MAINTAINED
DURING ,11PPMENTIDELIVERY
i N
SAMPLES COLLECTED BY:
(Please Pnpt)
SAMPLES RECEIVED IN LAB AT °C
RELINQjIISHED BY (SIG.) (SAMPLER)
DATEITIME
RECEIVED BY (SIG.)
COMMENTS:
j
/
e�D?ATTEITIIME
+W
�r L! -5 rD
RELINQUI HED BY (SIG.)
DATErr
RECEIVED BY (SIG.)
DATEITIME
RELINQUISHED BY (SIG.)
DATEITIME
RECEIVED BY (SIG)
DATEITIME
Sampler must place a "C" for composite sample or a "G" for
PLEASE READ Instructions for completing this form on the reverse side. 411117
FORM 95 Grab sample in the blocks above for each parameter requested.

BARNES ENVIRONMENTAL WASTE
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: August 17, 2023
Permit No. WQ0018525
Island Beach 1.37 % Solids
7.4 pH
Parameter
%
Mg/Kg Dry Weight
(% x 10,000)
Pounds/Dry Ton
(M /KZ x 0.002)
Nitrogen (TKN)
6.796
67,960.000
135.920
Phosphorus
3.059
30,590.000
61.180
Potassium
0.418
4,183.000
$.366
PAN (injected)*
2.068
20,683.280
41.367
PAN (surface)*
2.048
20,475.930
40.952
Ammonia Nitrogen
0.041
414.700
0.829
Calcium
4.510
45,095.000
90.190
Calcium Carbonate E .
---
---
Magnesium
---
4,312.000
8.624
Sodium
---
5,829.000
11.658
Sulfur
---
___
_-_
Nitrate N / Nitrite N
---
4.990
0.010
Barium
---
---
---
SAR
L 0.82
Chloride
---
---
---
Iron
---
---
---
Ceiling Concen.
(Mg/Kg)
Aluminum
---
9,952.00
19.904
Arsenic
---
2.50
0.005
75
Cadmium
---
0.70
0.001
85
Chromium
---
10.000
---
---
Copper
---
672.00
1.344
4,300
Lead
---
7.80
0.016
840
Mercury
---
0.14
0.000
57
Molybdenum
---
5.90
0.012
75
Nickel
---
8.60
0.017
420
Selenium
---
5.00
0.010
100
Zinc
---
1,228.00
2.456
7,500
Environment I # 564 A
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N +Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or a detection limits are listed as detection limits
for calculation purposes.

r ,
Waypoi t
ANALYTICAL
114 OAKMONT DREVE
GREENViLLE, NC 27858
drinking Water ZVi 37715
West 'water ZD: 10
*** THIS IS A CORRECTED COPY OF PREVIOUSLY REPORTED DATA ***
ID#: 564 A
ENVIRACON UTILITIES
C/O MR. STANLEY BUCK
1745 BELLGRADE-SWANSBORO ROAD
MAYSVILLE, NC 26555
Sludge
Analysis
Method
PARAMETERS
Sample
Date
Analyst
Code
PFI (not to he used For reporting)
7.4
08/18/23
ADR
4500FIB-1I
Aluminum, (dry wt. basis), mg/leg
9952
09/06/23
MTM
EPA200.7
Arsenic (dry wt. basis), mglkg
<2.5
09/07/23
DRC
311313-04
Calcium (dry wt. basis), mg/kg
45095
09/0023
MTM
EPA200.7
Cadmium (dry wt. basis), nlglkg
0.7
09/07/23
DRC
3 L 13B-04
Copper (dry wt, basis), mg/kg
672
09/06/23
IITIN
EPA200.7
Chromium, T,(dry wt. basis),mg/kg
LO
09/06/23
IIThi
EPAZ00.7
Lead (dry weight basis), mg/kg
7.8
09/07/23
DRC
3113B-04
Magnesium (dry wt. basis), mg/kg
4312
09/06/23
INTIN
EPA200.7
Mercury (dry wt. basis), mg/kg
0.14
08/30/23
DRC
EPA7471B
Nickel (drti• wt. basis), mglkg
8.6
09/06/23
MTM
EPA200.7
Potassium (dry wt. basis), mgllcg
4183
09/06/23
MTIN
EPA200.7
Selenium (dry wt. basis), mg/leg
<5.0
09/06/23
DRC
311313-04
Sodium (dry wt. basis), nig/leg
5829
09106123
INTM
EPA200.7
Zinc (dry wt. basis), mgllcg
1228
09/06/23
INTII
EPA200.7
Total Solids, %
1.37
08/22123
BLV
254OG-15
TKN (dry yet.), ing/leg
a 67960
08/22/23
BIND
351.2 112-93
Ammonia Nitrogen ((try wt.),ulglkg
c 414.7
08/30123
AMC
350.1 112-93
Phosphorus, T. (dry wt.), mgllcg
c 30590
08/22/23
Bit\10
365.4-74
Nitrate+Nitrite ((try set.), mg/kg
a 4.99
08/25/23
Ail[C
353.2 R2-93
Molybdenum (dry wt. basis), nrglkg
5.9
09/06123
MTIN
EPA200.7
PHONE [phone]
FAX [phone]
DATE COLLECTED: 08/17/23
DATE REPORTED : 09/08/23
_1� REVIEWED BY:
c•Uneertified data. DWR does not offer non -aqueous certification for this analytical procedure.

BARNES ENVIRONMENTAL WASTE
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: February 21, 2023
Permit No. WQ0018525
Hampton Suites 0.77 % Solids
7.30 pH
Parameter
%
Mg/Kg Dry Weight
x 10,000)
Pounds/Dry Ton
(Mg/Kg(Mg/Kg x 0.002)
Nitrogen (TKN)
5.960
59,600,000
119.200
Phosphorus
1.559
15,590.000
31.180
Potassium
0.314
3,144.000
6.28$
PAN (injected)*
1.800
18,001.620
36.003
PAN (surface)'
1.794
17,936,170
35.872
Ammonia Nitrogen
0.013
130,900
0.262
Calcium
4.730
47,300.000
94.600
Calcium Carbonate E .
---
---
Magnesium
---
2,731.000
5.462
Sodium
---
19,871.000
39.742
Sulfur
---
---
---
Nitrate N / Nitrite N
---
29.990
0.060
Barium
---
---
---
SAR
2.11
Chloride
---
---
---
Iron
---
---
---
Ceiling Concert.
(Mg/Kg)
Aluminum
---
2624.000
5.248
Arsenic
Cadmium
---
---
2.50
0.50
0.005
0.001
75
85
Chromium
---
8.600
---
---
Copper
---
1,159.00
2.318
4,300
Lead
---
5.40
0,011
840
Mercury
---
0.11
0.000
57
Molybdenum
---
5.00
0.010
75
Nickel
---
16.00
0.032
420
Selenium
---
5.00
0.010
100
Zinc
---
560.00
1.120
71500
Environment 1, Incorporated 551 A
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits
for calculation purposes.

oW'u@MHoo2 % hCoQpumUd
114 OAKMONT DRIVE
GREENVILLE, N.C. 27858
HAMPTON INN (HYDROTECH)
EMAIL DATA & COC
NO MAILED COPY
PARAMETERS
PH (not to be used For reporting)
Aluminum, (dry wt. basis), mglkg
Arsenic (dry wt. basis), mg/lcg
Calcium (dry wt. basis), mglkg
Cadmium (dry wt. basis), mglkg
Copper (dry wt. basis), mg/kg
Chromium, T.(dry wt, basis),nig/kg
Lead (dry weight basis), mg/kg
Magnesium (dry wt. basis), mg/kg
Mercury (dry wt. basis), mg/kg
Nickel (dry wt. basis), mg/kg
Potassium (dry wt. basis), mg/kg
Selenium (dry wt. basis), mg/kg
Sodium (dry wt. basis), mg/kg
Zinc (dry wt. basis), mg/kg
Total Solids,
TKN (dry wt.), mg/kg
Ammonia Nitrogen (dry wt.),mglltg
Phosphorus, T. (dry wt.), mg/kg
Nitrate+Nitrite (dry wt.), mg/kg
Molybdenum (dry wt. basis), mg/kg
Sludge Analysis Method
Sample Date Analyst Code
7.3
02/21/23
ADR 4500HB-1I
2624
03/01/23
MTM EPA200.7
<2.5
03/06/23
DRC 3113E-04
47300
03/01/23
MTM EPA200.7
<0.5
03/07/23
DRC 3113B-04
1159
03/01/23
MTM EPA200.7
8.6
03/01/23
MTM EPA200.7
5.4
03/08/23
DRC 3113E-04
2731
03/01/23
MTM EPA200.7
0.11
03/14/23
DRC EPA7471B
16
03/01/23
MTM EPA200.7
3144
03/01/23
MTM EPA200.7
<5.0
03/02/23
DRC 31I3B-04
19871
03/01/23
MTM EPA200.7
560
03/01/23
MTM EPA200.7
0.77
02/21/23
HMV 254OG-15
c 59600
03/01/23
BMD 351.2 R2-93
c 130.9
03/03/23
BMD 350.1 R2-93
c 15590
02/28/23
TRJ 365.4-74
c 29.99
03/01/23
TRJ 353.2 R2-93
<5.0
03/01/23
MTM EPA200.7
Drinking water ID: 37715
Wastewater ID; 30
PHONE [phone]
FAX [phone]
ID#: 551 A
DATE COLLECTED: 02/21/23
DATE REPORTED : 03/15/23
REVIEWED BY: v
c Uncertified data. DWR does not offer non -aqueous certification for this analytical procedure.

Environment 1, Inc. CHAIN QT CUSTODY RECORD
P.O. Rox 7085. 114 Oakmont Dr. Page 1 of 1
Greenville, NC 278�,8
cnvirrntment I inc.com
DISINFECTION
CHLORINE NEUTRALIZED AT COLLECTION
Phone [phone] • Fax [phone]
CHLORINE
pH CHECK (LAB)
CLIENT: 551 A week: 9
lioCi V
P
P
P
P
P
P
P
CONTAINER TYPE, PiG
AMPTONINN (HYDROTECH)
NONE
TTN: DON O'MARA
CHEMICAL PRESERVATION
YDROTECH
J
.0. BOX 4602
A
A
A
A
A
A
A
MERALD ISLE NC 28594
A -NONE D NAOH
z5
d}ow
Rr
�
52) 725 2319
z �
z
;�
;;
C B - HNO E - HCL
¢Q
o
�vu
CZ
U
z
p
d
p
�
r
M
� a
ti C- H2SO, F- ZINC ACETATP/NAOH
COLLECTION
J¢
F -
o
O
LL
1
=
S
I'
Q
�'
z
G NATHIOSULFATE
SAMPLE LOCATION
DATE
TIME
a o
E
o
E.
Q—t
z
Sludge Sample
'J.
5
€
,.
ti; `
3e»fi
<""
_>
w
CLASSIFICATION:
WASTEWATER (NPDES)
DRINKING WATER
DWR/GW
SOLID WASTE SECTION
CHAIN OF CUSTODY {SEAL) MAINTAINED
DURING SHIPMENTIDELIVERY
Y N
SAMPLES COLLECTED BY:
(Please m)
`P�r
I' 1fC�.1
SAMPLES RECEIVED IN LAB AT Ov°C
RELIN�HED BY (SIG.) (SAMPLER)
DATEfnME
REC VED BY (SIG.
ATE/TIME
COMMENTS:
RELINQUISHED BY (SIG)
DATEMME
RE ED BY (S1G.)
DAT EMME
RELINQUISHED BY (SIG.)
DATEIITME
RECEIVED BY (SIG.)
DATE MME
on the reverse side. PLEASE READ Instructions for completing this formSampler must place a "C" for composite sample or a "G" for
FORM its Grab sample in the blocks above for each parameter requested. 412927

BARNES ENVIRONMENTAL WASTE
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: August 17, 2023
Permit No. WQ0018525
Mariners Point 0.58 % Solids
7.1 nH
Parameter
IF—
%
Mg/Kg Dry Weight
(% x 10,000)
Pounds/Dry Ton
(Mg/Kg(Mg/Kg x 0.002)
Nitrogen (TKN)
6.162
61,620.000
123.240
Phosphorus
2.354
23,540.000
47.080
Potassium
0.381
3,809.000
7.618
PAN (infected)*
1.852
18,524.948
37.050
PAN (surface)*
1.850
18,499.978
37.000
Ammonia Nitrogen
0.005
49.940
0.100
Calcium
4923
49,232.000
98.464
Calcium Carbonate E .
---
_._
---
Magnesium
---
3,862,000
7.724
Sodium
---
7,666.000
15.332
Sulfur
_--
Nitrate N / Nitrite N
---
3.990
0.008
Barium
---
---
---
SAR
0.68
Chloride
---
---
---
Iron
---
---
---
Ceiling Concen.
(Mg/Kg)
Aluminum
---
9,066.00
18.132
Arsenic
---
2.50
0.005
75
Cadmium
---
0.80
0.002
85
Chromium
---
9.000
---
---
Copper
---
657.00
1.3I4
4,300
Lead
---
7.60
0.015
$40
Mercury
---
0.15
0.000
57
Molybdenum
---
5.00
0.010
75
Nickel
---
8.60
0.017
420
Selenium
---
5.00
0.010
100
Zinc
---
1,173.00
2.346
7,500
Environment 14 307
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits
for calculation purposes.

waypol t,c`-��
ANALYTICAL
114 OAKMONT DRIVE
GREENVILLE, NC 27858
MARINERS POINT (BUCK)
C/O MR. STANLEY BUCK
1745 BELGRADE-SWANSBORO RD.
MAYSVILLE, NC 28555
PARAMETERS
PH (not to be used for reporting)
Aluminum, (dry wt. basis), mg/kg
Arsenic (dry wt. basis), mg/kg
Calcium (dry wt. basis), mgllcg
Cadmium (dry wt. basis), mg/kg
Copper (dry wt. basis), mgllcg
Chromium, T.(dry wt. basis),mg/leg
Lead (dry weight basis), mglkg
Magnesium (dry wt. basis), mg/lcg
Mercury (dry wt. basis), mglkg
Nickel (dry wt. basis), mg/kg
Potassium (dry wt. basis), mg/kg
Selenium ((try wt. basis), mg/kg
Sodium (dry wt. basis), mgllcg
Zinc (dry wt. basis), mg/kg
Sodium Adsorption Ratio (talc)
Total Solids, %
TKN (dry wt.), n1g/kg
Ammonia Nitrogen (dry wt.),mgllcg
Phosphorus, T. (dry wt.), mgllcg
Nitrate+Nitrite (dry wt.), mg/kg
Molybdenum (dry wt. basis), mg/lig
Sludge Analysis Method
Sample Date Analyst Code
7.1
08/18/23
ADR
4300HB-11
9066
09/06/23
MTlb1
EPA200.7
<2.5
09/07/23
DRC
3113B-04
49232
09/06/23
MTM
EPA200.7
0.8
09/07/23
DRC
3113E-04
657
09/06/23
MTM
EPA200.7
9.0
09/06/23
MTM
EPA200.7
7.6
09/07/23
ARC
3113E-04
3862
09/06/23
MTM
EPA200.7
0.15
08/23/23
MTM
EPA7471B
8.6
09/06/23
MTM
EPA200.7
3809
09/06/23
MTM
EPA200.7
<5.0
09/06/23
DRC
3113B-04
7666
09/06/23
MTM
EPA200.7
1173
09/06/23
MTM
EPA200.7
9.0
0.58
08/22/23
BLV
254OG-I5
c 61620
08/22/23
BMD
351.2 112-93
c 49.94
08/30/23
AMC
350.1 112-93
c 23540
08/22/23
B141D
365.4-74
c 3.99
08/25/23
AMC
353.2 112-93
<5.0
09/06/23
141TM
EPA200.7
Drinking Water I13: 37715
Wantewater ID; 10
PHONE [phone]
FAX [phone]
ID#: 307
DATE COLLECTED: 08/17/23
DATE REPORTED : 09/08/23
REVIEWED BY:�
c Uncertified data. DWR does not offer non -aqueous certification for this analytical procedure,

Waypoint® CHAIN OF CUSTODY RECORD
'"M1L+ilp
Waypoint Analytical - Greenville Page or
Greenville, NC 27858
www.Wa ointAnal tical-com
YP Y
DISINFECTION
CHLORINE NEUTRALIZED AT COLLECTION
Phone[phone] •Fax [phone]
❑CHLORINE
To a0.5 mg1L - Yes (Y) or No (N)
CLIENT: lJ/., u, Cr 2��t- 10
❑ uv
pH CHECK (S.U.) (LAB)
CONTAINER TYPE, PIG
NONE
A
/j
CHEMICAL PRESERVATION
❑
A NONE D - NAOH
o
y
z_j
Fr 0
Ld z
w
T
Jl
� B-HNO3 E-HCL
0
_
CZ
w
z
ar
°c
C-HzSO4 F -ZINC ACEfATEINAOH
�
COLLECTION
¢
F m
ro m
J
oc�
w ¢
W
S
C ­
'�`
y
O
fr
G-NATHIOSULFATE
SAMPLE LOCATION
DATE
TIME
S tJmt'_ jg-w f if ,
1111d
G
C2
G
6&
CLASSIFICATION:
WASTEWATER(NPDES)
❑ DRINKINGWATER
❑ DWRIGW
❑ SOLID WASTE SECTION
CHAIN OF CUSTODY (SEAL) MAINTAINED
DURING SHIPMENTID E LIVERY
N
SAMPLES COLLECTED BY:
(Please Font)
('te LIC
SAMPLES RECEIVED IN LAB AT 5 °C
RELINQUISHED BY (SIG.) (SAMPLER)
t ATE1TIME
RECEIV �(S;G,
D TEfTIME
COMMENTS:
SAMPLES RECEIVED ON IC ' YES NO
RELINQUISHED BY (SIG.)
DATEMME
REC IVED BY (SI .)
DATEMME
RELINQUISHED BY (SIG.)
DATEMME
RECEIVED BY (SIG.)
DATEfnME
Sampler must place a "C" for composite sample or a "G" for
PLEASE READ Instructions for completing this form an the reverse side.
FORM #5 Grab sample in the blocks above for each parameter requested.

BARNES ENVIRONMENTAL WASTE
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: January 17, 2023
Permit No. WQ0018525
McGinnis Point 2.14 % Solids
7.3 pH
Parameter
%
Mg/Kg Dry Weight
(% x 10,001
Pounds/Dry Ton
(Mg/Kg(Mg/Kg x 0.002)
Nitrogen (TKN)
5.996
59,960.000
119,920
Phosphorus
1.025
10,250,000
20.500
Potassium
0.193
1,932,000
3.864
PAN (injected)*
1.824
18,235.910
36.472
PAN (surface)*
L806
18,060.960
36.122
Ammonia Nitrogen
0.035
349.900
0.700
Calcium
4.569
45,694.000
91.388
Calcium Carbonate Eq.
---
I ---
Ma nesium
---
3,149.000
6.298
Sodium
---
12,461.000
24.922
Sulfur
---
---
---
Nitrate N / Nitrite N
---
2.980
0.006
Barium
---
---
---
SA R
2.22
Chloride
---
---
---
Iron
---
---
---
Ceiling Concen.
(Mg/Kg)
Aluminum
---
5,206.00
10.4I2
Arsenic
---
2.50
0.005
75
Cadmium
---
0.90
0.002
85
Chromium
---
26.000
---
---
Copper
---
1,728.00
3.456
4,300
Lead
---
22.00
0.044
840
Mercut
---
0.40
0.001
57
Molybdenum
---
5.00
0.010
75
Nickel
---
17.00
0.034
420
Selenium
---
5.00
0.010
100
Zinc
---
1,533,00
3.066
7,500
Environment 1 9 555 A
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N +Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits
for calculation purposes.

ERW'nEH@V % howpoa od
114 OAKMONT DRIVE
GREENVILLE, N.C. 27858
MCGINNIS POINT (HYDROTECH)
EMAIL DATA & COC
NO MAILED COPY
PARAMETERS
PH (not to be used for reporting)
Aluminum, (dry wt. basis), mg/kg
Arsenic (dry wt. basis), mg/kg
Calcium (dry wt. basis), mg/kg
Cadmium (dry wt. basis), mglkg
Copper (dry wt. basis), mg/kg
Chromium, T.(dry wt. basis),mg/kg
Lead (dry weight basis), mg/kg
Magnesium (dry wt. basis), mg/kg
Mercury (dry wt. basis), mg/kg
Nickel (dry wt. basis), mg/kg
Potassium (dry wt. basis), mgllcg
Selenium (dry wt. basis), mg/kg
Sodium (dry wt. basis), mgllcg
Zinc (dry wt. basis), mg/kg
Total Solids,
TICN (dry wt.), mg/kg
Ammonia Nitrogen (dry wt.),mg/lcg
Phosphorus, T. (dry wt.), mg/kg
Nitrate+Nitrite (dry wt.), mg/kg
Molybdenum (dry wt. basis), mg/kg
Sludge Analysis Method
Sample Date Analyst Code
7.3
01/17/23
JMS 4500HB-11
5206
02/10/23
MTM EPA200.7
C 2.5
02/01/23
DRC 3113B-04
45694
02/10/23
MTM EPA200.7
0.9
02/02/23
DRC 3113E-04
1728
02/10/23
MTM EPA200.7
26
02/10/23
MTM EPA200.7
22
02/02/23
DRC 3113B-04
3149
02/10/23
MTM EPA200.7
0.40
01/30/23
ARC EPA7471B
17
02/10/23
MTM EPA200.7
1932
02/10/23
MTM EPA200.7
C 5.0
02/02/23
DRC 3113E-04
12461
02/10/23
MTM EPA200.7
I533
02/10/23
MTM EPA200.7
2.14
01/17/23
JDJ 2540G15
c 59960
01/24/23
BMD 351.2 R2-93
c 349.9
01/26/23
ICES 350.1 R2-93
c 10250
01/24/23
TRJ 365.4-74
c 2.98
01/26/23
BMD 353.2 R2-93
C 5.0
02/10/23
MTM EPA200.7
Drinking water ID, 37715
Wastewater ID; 10
PHONE [phone]
FAX [phone]
ID#: 555 A
DATE COLLECTED: 01/17/23
DATE REPORTED : 02/13/23
i)
REVIEWED 8Y:.-
c Vneertified data. DWR does not offer non -aqueous cextification for this analytical procedure.

1'snvironment 1, Inc. CHAIN OF CUSTODY RECORD
P.O. Box 7085. 114 Oakmont Dr. Page 1 of
C]reeiiville. NC 27858
eiivironinent I ine.com
DISINFECTION
CHLORINI=NEUTRALIZEDATCOLLECTION
Phone (252) 75(i-G2O8j• Fax [phone]
Ij CHLORINE
CLIENT: 555 A Week- 9
uv
l
pH CHECK (LAB)
P
P
P
P
P
P
P
CONTAINER TYPE. PIG
[CGINNIS POINT (HYDROT)ECH)
iNF
'ITN: DON O'MARA
CHI CHEMICAL RESERVATION
YDROTRCH
.0. SOX 4602
A
A
A
A
A
A
A
[YIERALD ISLE NC 28594
r A NONE D NAOH
— z
o
52) 725-2319
L V
(�}
�
N
o
y;
w
B-HNO, E-HCL
0 0
Ld o
z
z
Otl
o
�'
-`0—�
+
C - H2SO, F - ZINC ACETATE/NAOH
COLLECTION
ifs T
o o
�
M d
w tR
�°
G
g;
0O
,C°L,
w
G- NATHIOSULFATE
SAMPLE LOCATION
DATE
TIME
Sludge Sample
�� Z
(��
5
+' �.Y
?eyv
-
' .'4.r
QYY
A¢i�'}:
}y 2x:
S. `
J��.
Ci v'� i
f
}}..e...
'`
CLASSIFICATION:
WASTEWATER (NPDES)
DRINKING WATER
C� DWR/GW
SOLID WASTE SECTION
CHAIN OF CUSTODY (SEAL) MAINTAINED
DURING HIPMENT/DELIVERY
N
SAMPLES COLLECTED BY:
(Please P
SAMPLES RECEIVED IN LABAT_1 (a °C
RELINQ (SHED BY (SIG.) (SAMPLER)
DATEITIME
RECEIVED BY (SIG.) _
DATEMME
COMMENTS:
JZ3 `�w
f ", -
(61 'S'4
RELINQUISHED BY (SIG.)
DATErfIME
RECEIVED BY (SIG.)
DATEMME
RELINQUISHED BY (SIG.)
DATE/TIME
RECEIVED BY (SIG.)
DATEMME
PLEASE READ InStFLletiO11S for completing this form on the reverse side. Sampler must place a "C" for composite sample or a "G" for FGRM #s Grab sample in the blocks above for each parameter requested. Np 412924

BARNES ENVIRONMENTAL WASTE
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: January 26, 2023
Permit No. WQ0018525
NC Aquarium at Pine 1.09 % Solids
Knoll Shores ! 12.18 pH (taken from lime stabilization event)
Parameter
%
Mg/Kg Dry Weight
(% x 10,000)
Pounds/Dry Ton
(M /K x 0,002)
Nitrogen (TKN)
4.037
40,370.000
80.740
Phosphorus
2.154
21,540.000
43,080
Potassium
0.525
5,249.000
10.498
PAN (injected)*
1.220
12,201.960
24.404
PAN (surface)*
1.214
12,144.110
24.288
Ammonia Nitrogen
0.012
115.700
0.231
Calcium
4.529
45,287.000
90.574
Calcium Carbonate E .
---
---
Magnesium
---
9,834.000
19.668
Sodium
---
83,936.000
167.872
Sulfur
---
---
Nitrate N / Nitrite N
---
9.970
0.020
Barium
---
---
---
Chloride
---
___
---
Iron
---
---
..._
Aluminum
---
1,272.00
2.544
Arsenic
---
2.50
0.005
Cadmium
---
6.20
0.012
Chromium
---
18.000
---
Copper
---
234.00
0.468
Lead
---
23.00
0.046
Mercury
---
0.06
0.000
Molybdenum
---
5.00
0.010
Nickel
---
20.00
0.040
Selenium
---
5.00
0.010
Zinc
---
750.00
1.500
Environment l # 444 A
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits
for calculation purposes.
SAR
9.70
!(MgfKg)
ling Concen.
75
85
4,300
840
57
75
420
100
7,500

Enwo @@EOM % hmp(PTINd
114 OAKMONT DRIVE
GREENVILLE, N.G. 27858
NC AQUARIUM AT PINE KNOLL SHORES
MR. DAN FORTIN
FORTIN CONTRACT SERVICES
P.O. BOX 4188
EMERALD ISLE, NC 28594
PARAMETERS
Aluminum, (dry wt, basis), mg/kg
Arsenic (dry wt. basis), mg/kg
Calcium (dry wt, basis), mg/kg
Cadmium (dry wt. basis), mg/kg
Copper (dry wt. basis), mg/kg
Chromium, T.(dry wt. basis),mg/kg
Lead (dry weight basis), mg/kg
Magnesium (dry wt. basis), mglkg
Mercury (dry wt. basis), mg/kg
Nickel (dry wt. basis), mg/kg
Potassium (dry wt. basis), mglkg
Selenium (dry wt. basis), mg/kg
Sodium (dry wt. basis), mg/kg
Zinc (dry wt. basis), mg/kg
Total Solids, %
TICN (dry wt.), mglkg
Ammonia Nitrogen (dry wt.),mg/kg
Phosphorus, T. (dry wt.), mg/kg
Nitrate+Nitrite (dry wt,), mg/kg
Plant Available Nitrogen, mglkg
Molybdenum (dry wt, basis), mg/kg
Sludge Analysis Method
Sample Date Analyst Code
1272
02/15/23
MTM
EPA200.7
<2.5
02/16/23
DRC
3113E-04
45287
02/15/23
MTM
EPA200.7
6.2
02/16/23
DRC
3113B-04
234
02/15/23
MTM
EPA200.7
18
02/15/23
MTM
EPA200.7
23
02/16/23
DRC
3113B-04
9834
02/15/23
MTM
EPA200.7
0.06
02/14/23
DRC
EPA7471B
20
02/15/23
MTM
EPA200.7
5249
02/15/23
MTM
EPA200.7
<5.0
02/17/23
DRC
3113E-04
83936
02/15/23
MTM
EPA200.7
750
02/15/23
MTM
EPA200.7
1.09
01/26/23
,IMS
2540G-15
c 40370
01/31/23
BMD
351.2 R2-93
c 115.7
02/01/23
ICES
350.1 R2-93
c 21540
01/31/23
TRJ
365.4-74
c 9.97
02/02/23
KES
353.2 R2-93
12144
02/03/23
BMD
<5.0
02/15/23
MTM
EPA200.7
Drinking Water ID: 37715
Wastewater ID: 10
PHONE [phone]D8
FAX [phone]
ID#: 444 A
DATE COLLECTED: 01/26/23
DATE REPORTED : 02/20/23
REVIEWED BY:
c Uncertified data. DWR does not offer non -aqueous certification for thin analytical procedure,

(Environment 1, Inc. CHAIN OF CUSTODY RECORD
P.U. Box 7085, 114 Oakmont Dr. Page 1 of 1
Greenville NC 27858
environment I inc.com
DISINFECTION
CHLORINE: NEUTRALIZED AT COLLECTION
Phone [phone] • Fax (252) 750_0633
CHLORINE
pH CHECK (tAS)
CLIENT: 444 A Week: 9
UV
P
P
P
P
P
P
CONTAINER TYPE, P/G
C AQUARIUM AT PINE KNOLL SHORES
NONE
OR. DAN FORTIN
CHEMICALPRESERVATION
DRTIN CONTRACT SERVICES
❑
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HERALD ISLE NC 28594
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CLASSIFICATION:
JWASTEWATER (NPDES)
DRINKING WATER
DWRIGW
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CHAIN OF CUSTODY (SEAL) MAINTAINED
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N
SAMPLES COLLECTED BY:
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SAMPLES RECEIVED IN LAB AT cC
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PLEASE READ Instructions for completing this form on the reverse side. Sampler must place a "C" for composite sample or a "G" for FORM #5 Grab sample in the blocks above for each parameter requested. Nq 412961

BARNES ENVIRONMENTAL WASTE
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: January 26, 2023
Permit No. WQ0003067
Ocean Bay Villas 0.74 % Solids
12.41 pH (taken from lime stab.)
Parameter
%
Mg/Kg Dry Weight
(% x 10,000}
Pounds/Dry Ton
(Mg/Kg(Mg/Kg x 0.002)
Nitrogen (TKN)
5.084
50,840.000
101.680
Phosphorus
1.100
11,000.000
22.000
Potassium
0i46
3,455.000
6.910
PAN (injected)*
1.537
15,366.854
30.734
PAN (surface)*
L534
15,336.894
30.674
Ammonia Nitrogen
0.006
59.920
0. l20
Calcium
3.545
35,454.000
70.908
Calcium Carbonate E .
---
---
Magnesium
---
3,232.000
6.464
Sodium
---
18,075.000
36.150
Sulfur
---
___
__-
Nitrate N / Nitrite N
---
72.910
0.146
Barium
---
---
---
SAR
2.12
Chloride
---
---
-_-
Iron
---
---
---
Ceiling Concen.
(Mg/Kg)
Aluminum
---
4,974.00
9.948
Arsenic
---
2.50
0.005
75
Cadmium
---
0.90
0,002
85
Chromium
---
17.000
---
---
Copper
---
305.00
0.610
4,300
Lead
---
29.00
0.058
840
Mercury
---
0.38
0.001
57
Molybdenum
---
5.00
0.010
75
Nickel
---
11.00
0.022
420
Selenium
---
5.00
0.010
100
Zinc
---
1,463.00
2.926
7,500
Environment 1 # 442 A
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N +Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits
for calculation purposes.

114 OAKMONT DRIVE
GREENVILLE, N.C. 27858
C&P ENTERPRISES (FORTIN)
MR. D,AN FORTIN
FORTIN CONTRACT SERVICES
P.O. BOX 4188
EMERALD ISLE, NC 28594
PARAMETERS
Aluminum, (dry wt. basis), mg/kg
Arsenic (dry wt. basis), mg/kg
Calcium (dry wt. basis), mg/kg
Cadmium (dry wt. basis), mg/kg
Copper (dry wt. basis), mg/kg
Chromium, T.(dry wt. basis),mg/kg
Lead (dry weight basis), mg/lcg
Magnesium (dry wt. basis), mg/kg
Mercury (dry wt. basis), mg/kg
Nickel (dry ►yt. basis), mgllcg
Potassium (dry wt. basis), mg/kg
Selenium (dry wt. basis), mg/kg
Sodium (dry wt. basis), mg/lig
Zinc (dry wt. basis), mg/kg
Sodium Adsorption Ratio (talc)
Total Solids, %
TIN (dry wt.), mg/lig
Ammonia Nitrogen (dry wt.),mg/kg
Phosphorus, T. (dry wt.), mg/kg
Nitrate+Nitrite (dry wt.), mg/kg
Molybdenum (dry wt. basis), mg/kg
Sludge Analysis Method
Sample Date Analyst Code
4974
02/15/23
NITM EPA200.7
<2.5
02/16/23
DRC 311313-04
35454
02/15/23
MTM EPA200.7
0.9
02/16/23
DRC 3113B-04
305
02/15/23
MTM EPA200.7
17
02/15/23
MTM EPA200.7
29
02/16/23
DRC 3113B-04
3232
02/15/23
MTM EPA200.7
0.38
02/14/23
DRC EPA7471B
11
02/15/23
MTM EPA200.7
3455
02/15/23
MTM EPA200.7
<5.0
02/17/23
DRC 3113E-04
18075
02/15/23
MTM EPA200.7
1463
02/15/23
MTM EPA200.7
8.3
0.74
01/26/23
JMS 2540G-15
c 50840
01/31/23
BMD 351.2 R2-93
c 59.92
02/01/23
KES 350.1 112-93
c 11000
01/31/23
TRJ 365.4-74
c 72.91
02/02/23
KES 353.2 R2-93
<5.0
02/15/23
MTM EPA200.7
Drinking Water ID: 37715
Wastewater ID: 16
PHONE [phone]
FAX [phone]
ID#: 442 A
DATE COLLECTED: 01/26/23
DATE REPORTED : 02/20/23
REVIEWED BY: ✓ �i
e Uncertified data. DWR does not Offer non -aqueous certification for this analytical procedure.

I:jivironnient k, Inc. CHAIN OF CUSTODY RECORD
P.O_ Box 7085, J 14 Oakmont Dr. Page 1 of 1
Greenville. NC 27858
errvirunment I inc.corrl
DISINFECTION
CHLORINE NEUTRALIZED AT COLLECTION
Phone [phone] " 1-ax (252) 756-063
CFII,ORINI;
CLIENT: 442 A Week: 10
pH CHECK (LAB)
UV
P
P
P
P
P
P
CONTAINER TYPE, PiG
&P ENTERPRISES (FORTIN)
NONE
IR. DAN FORTIN
CHEMICAL PRESERVATION
ORTIN CONTRACT SERVICES
.O. SOX 4188
A
A
A
A
A
A
A
,MERALD ISLE NC 28594
A -NONE D-NAOH
E
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DATE
TIME
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CLASSIFICATION:
WASTEWATER(NPDES)
DRINKING WATER
DWRIGW
SOLID WASTE SECTION
CHAIN OF CUSTODY (SEAL) MAINTAINED
DURING II MENT/DELIVERY
SY
N
SAMPLES COLLECTED BY;
(Please Pant)
YgaJ SiTANa
SAMPLES RECEIVED IN LAB AT eC
R LINQUISHED B (SIG.} ( AMPLER)
DATErI1ME
RECEIVED BY IG.)
DATEMME
COMMENTS:
R LINQUISHED Y (SIG.)
UATETIME
RECEIVE Y (SIG.)
DATEJTIME
RELINQUISHED BY (SIG.)
DATENIME
RECEIVED BY (SIG.)
DATUnME
PLEASE READ instructions for completing this form an the reverse side. Sampler must place a "C" for composite sample or a "G' for 412138
FORM 45 Grab sample in the blocks above for each parameter requested. Ng

BARNES ENVIRONMENTAL WASTE
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: January 19, 2023
Permit No. WQ0018525
Ocean Club 0.43 % Solids
12.12 DH (taken from lime stabilization event)
Parameter
%
Mg/Kg Dry Weight
(% x 10,000)
Pounds/Dry Ton
(Mg/Kg(Mg/Kg x 0.002)
Nitrogen (TKN)
5.325
53.250.000
106.500
Phosphorus
1.542
15,420.000
30.840
Potassium
0.677
6,772.000
13.544
PAN (injected)*
1.602
16,016.627
32.033
PAN (surface)*
1.599
t5,991.172
31.982
Ammonia Nitrogen
0.005
50.910
0.102
Calcium
3.409
34,092.000
68.184
Calcium Carbonate E .
---
---
Magnesium
---
4,754.000
9.508
Sodium
---
29,18 I.000
58.362
Sulfur
---
---
Nitrate N / Nitrite N
---
5.990
0.0I2
Barium
---
---
---
SA R
2.57
Chloride
---
---
---
Iron
---
---
---
Ceiling Concen.
(M /K )
Aluminum
---
2,287.00
4,574
Arsenic
---
2.50
0.005
75
Cadmium
---
0.90
0.002
85
Chromium
---
11.000
---
---
Copper
---
361.00
0.722
4,300
Lead
---
8.80
0.018
840
Mercury
---
0.14
0,000
57
Molybdenum
---
5.00
0.010
75
Nickel
---
11,00
0.022
420
Selenium
--- 1
5.00
0.010
100
Zinc
---
2,575.00
5.150
7,500
Environment 1 # 404 A
Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N � % PAN
Note: Constituents N.D. (Not Detected) or a detection limits are listed as detection limits
for calculation purposes.

Eww'OnflumM Ala WupTOW
114 OAKMONT DRIVE
GREENVILLE, N.C. 27858
OCEAN CLUB (FORTIN)
MR. DAN FORTIN
F'ORTIN CONTRACT SERVICES
P.O. BOX 4188
EMERALD ISLE, NC 28594
PARAMETERS
Aluminum, (dry wt. basis), mg/Icg
Arsenic (dry wt. basis), mg/kg
Calcium (dry wt. basis), mg/lcg
Cadmium (dry wt. basis), mg/kg
Copper (dry wt. basis), mg/kg
Chromium, T.(dry wt. basis),mg/kg
Lead (dry weight basis), mg/kg
Magnesium (dry wt. basis), mg/kg
Mercury (dry wt. basis), mglkg
Nickel (dry wt. basis), mg/kg
Potassium (dry wt. basis), mg/kg
Selenium (dry wt. basis), mg/Icg
Sodium (dry wt. basis), mg/lcg
Zinc (dry wt. basis), ing/kg
Total Solids, %
TKN (dry wt.), mglkg
Ammonia Nitrogen (dry wt.),mgtkg
Phosphorus, T. (dry wt.), mg/kg
Nitrate+Nitrite (dry wt.), mgllcg
Plant Available Nitrogen, mg/kg
Molybdenum (dry wt. basis), mg/kg
Sludge Analysis Method
Sample Date Analyst Code
2287
02/10/23
MTM EPA200.7
¢2.5
02/01/23
ARC 3113E-04
34092
02/10/23
IV1TM EPA200.7
0.9
02/02/23
DRC 3113E-04
361
02/10/23
MTM EPA200.7
11
02/10/23
MTM EPA200.7
8.8
02/02/23
DRC 3113E-04
4754
02/10/23
MTM EPA200.7
0.14
02/14/23
DRC EPA7471B
11
02/10/23
MTM EPA200.7
6772
02/10/23
MTM EPA200.7
C5.0
02/02/23
DRC 3113B-04
29181
02/10/23
MTM EPA200.7
2575
02/10/23
MTM EPA200.7
0.43
01/24/23
HMV 2540G15
c 53250
01/24/23
BMD 351.2 R2-93
c 50.91
01/26/23
KES 350.1 R2-93
c 16420
01/24/23
TRJ 365.4-74
c 5.99
01/26/23
BMD 353.2 R2-93
15991
02/03/23
BMA
5.0
02/10/23
MTM EPA200.7
Drinking Water ID: 37715
Wastewater ID: 10
PHONE [phone]
FAX [phone]
ID#I:: 404 A
DATE COLLECTED: 01/19/23
DATE REPORTED : 02/15/23
REVIEWED BY:
c Uncertified data. DWR does not offer non-agueoua certification for this analytical procedure.

O
M
F4
P.
Ei
Environment 1, [nc. CHAIN OF CUSTODY RECORD
I'.O. Box 7085. 114 Oakmow Dr. Pa-e 1 of 1
(;reenville NC ')WiR
env i rori me l d l inexor n
DISINFECTION
CHLORINE NEUTRALIZED AT COLLECTION
Phone [phone] - Fax [phone]
CHLORINE
CLIENT: 404 A Week: 9
uv
pH CHECK (LAB)
P
P
P
P
P
P
CONTAINER TYPE,P/G
CEAN CLUB (FORTIN)
❑ NONE
R. DAN FORTIN
3RTIN CONTRACT SERVICES
CHEMICAL PRESERVATION
O. BOX 4188
A
A
A
A
A
A
HERALD ISLE NC 28594
v' A -NONE D-NAOH
o
E
52) 393-8720
z�
w z
w
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COLLECTION
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SAMPLE LOCATION
DATE
TIME
Sludge Sample
4
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{Ur s
� .z
CLA551FICATION:
WASTEWATER (NPDES)
DRINKING WATER
DWRIGW
SOLID WASTE SECTION
CHAIN OF CUSTODY (SEAL) MAINTAINED
DURING IPNiENT/DELIVERY
Y N
SAMPLES COLLECTED BY:
(Please Print)
NMI
SAMPLES RECEIVED IN LAB AT r °C
QUSHED BY G.) (5 PIER)
ATEITME
RECEIVED BY (SI .)
DATEIIME
COMMENTS:
)RINOU'ISHED
i -00
ram-
�1� 1 ? LG
a
B {SIG.)
AT _TTIME
RECEIVED BY (SIG.)
DATEITIME
RELINQUISHED BY (SIG.)
DATISTIME
RECEIVED BY (SIG.)
DATEITIME
PLEASE READ instructions for completing this form on the reverse side. Sampler must place a "C for composite sample or a "G" for FORM #5 Grab sample in the blocks above for each parameter requested. No 41 2975

BARNES ENVIRONMENTAL WASTE
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: February 21, 2023
Permit No. WQOO18525
Oceans Condominiums 1.41 % Solids
F_R nH
Parameter
%
Mg/Kg Dry Weight
(% x 10,000)
Pounds/Dry on
(Mg/Kg(Mg/Kg x 0.002)
Nitrogen (TKN)
0.330
93,900.000
187.800
Phosphorus
0.266
13,790,000
27.590
Potassium
0.504
7,009.000
14.018
PAN (infected)*
O.118
1,182.400
2.365
PAN (surface)*
0.105
1,047.900
2.096
Ammonia Nitrogen
0.027
3,019.000
6.038
Calcium
5.876
25,139.000
50.278
Calcium Carbonate E .
---
---
Magnesium
0.418
4,085.000
8.170
Sodium
---
4,903.000
9.806
Sulfur
Nitrate N / Nitrite N
---
5.000
0.010
Barium
---
-__
-- f
Chloride
---
Iron
Aluminum
---
1,382.00
2.764
Arsenic
---
12.00
0.024
Cadmium
---
0.90
0.002
Chromium
---
25.000
---
Co er
---
507.00
1.014
Lead
---
14.00
0.028
Mercury
---
0.10
0.000
Molybdenum
---
5.00
0,010
Nickel
---
12.00
0.024
Selenium
---
5.00
0.010
Zinc
---
1,108.00
2.216
r
f
Environment 14 566 A
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits
for calculation purposes.
SAR
0.90
Ceiling Coneen.
75
85
840
57
75
420
100
7,501

Waypo�nt,-
ANALYTICAL
114 OAKMONT DRIVE
GREENVILLE, N.C. 27858
OCEANS CONDOMINIUMS (HYDROTECH)
EMAIL DATA & COC
NO MAILED COPY
PARAMETERS
PH (not to be used for reporting)
Aluminum, (dry wt. basis), mg/kg
Arsenic (dry wt. basis), mg/kg
Calcium (dry wt. basis), mg/kg
Cadmium (dry wt. basis), mg/kg
Copper (dry wt. basis), mg/kg
Chromium, T.(dry wt. basis),mg/Icg
Lead (dry weight basis), mg/kg
Magnesium (dry wt. basis), mg/kg
Mercury (dry wt. basis), mg/kg
Nickel (dry wt. basis), mgllcg
Potassium (dry wt. basis), mg/kg
Selenium (dry wt. basis), mg/kg
Sodium (dry wt. basis), mg/kg
Zinc (dry wt. basis), mg/kg
Total Solids, %
TKN (dry wt.), mg/kg
Ammonia Nitrogen (dry wt.),mg/kg
Phosphorus, T. (dry wt.), mg/kg
Nitrate+Nitrite (dry wt.), mg/kg
Molybdenum (dry wt. basis), mg/kg
Sludge Analysis Method
Sample Date Analyst Code
6.8
02/21/23
ADR 4500HB-11
1382
03/16/23
MTM EPA200.7
12
03/21/23
DRC 3113E-04
25139
03/16/23
MTM EPA200.7
0.9
03/23/23
DRC 3113B-04
507
03/16/23
MTM EPA200.7
25
03/16/23
MTM EPA200.7
14
03/22/23
DRC 3113E-04
4085
03/16/23
MTM EPA200.7
0.10
03/14/23
DRC EPA7471B
12
03/I6/23
MTM EPA200.7
7009
03/16/23
MTM EPA200.7
<5.0
03/20/23
DRC 3113B-04
4903
03/16/23
MTM EPA200.7
1108
03/16/23
MTM EPA200.7
1.41
02/21/23
HMV 2540G-15
c 93900
03/09/23
TRJ 351.2 R2-93
c 3019
03/03/23
BMD 350.1 R2-93
c 13790
02/28/23
TRJ 365.4-74
c 5.00
03/01/23
TRJ 353.2 R2-93
<5.0
03/16/23
MTM EPA200.7
Drinking Water ID: 37715
ID#: 566 A
DATE COLLECTED: 02/21/23
DATE REPORTS : 03/24/23
v �
REVIEWED BY:
c VncertiEied data. DWR does not offer non -aqueous certification for this analytical procedure.

BARNES ENVIRONMENTAL WASTE
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: February 21, 2023
Permit No. WQ0018525
Pebble Beach 0.96 % Solids
6.7 pH
Parameter
%
Mg/Kg Dry Weight
(% x 10,000)
Pounds/Dry Ton
(Mg/Kg(Mg/Kg x 0.002)
Nitrogen (TKN)
6.961
69,610.000
139.220
Phosphorus
1.471
14,710,000
29.420
Potassium
0.3 09
3,092,000
6_ l 84
PAN (infected)*
2.149
2,464.097
4.928
PAN (surface)*
2.108
2,435.542
4.871
Ammonia Nitrogen
0.084
835.400
1.671
Calcium
2.201
22,013.000
44.026
Calcium Carbonate E .
---
---
---
Magnesium
---
3,191.000
6.382
Sodium
---
12,256,000
24.512
Sulfur
---
___
Nitrate N / Nitrite N
---
24.980
0.050
Barium
---
---
---
SAR
2.00
Chloride
---
-
Iron
---
---
---
Ceiling Concert.
(Mg/Kg)
Aluminum
---
3,406.000
6.812
Arsenic
---
2.50
0.005
75
Cadmium
---
1,10
0.002
85
Chromium
---
9.600
---
Copper
---
260.00
0.520
4,300
Lead
---
15.00
0.030
840
Mercu
---
0.16
0.000
57
Molybdenum
---
5.00
0,0I0
75
Nickel
---
12.00
0.024
420
Selenium
---
5.00
0.010
100
Zinc
---
2,692.00
5.384
7,500
Environment 14 287A
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N +Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) +Nitrate N + Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits
for calculation purposes.

114 OAKMONT DRIVE
GREENVILLE, N.C, 27858
PEBBLE BEACH (HYDROTECH)
wwwwwwwwwwww*wwwwwwwwwwwwwwwww
EMAIL DATA & COC
NO MAILED COPY
PARAMETERS
PH (not to be used for reporting)
Aluminum, (dry wt. basis), mg/lcg
Arsenic (dry wt. basis), mg/kg
Calcium (dry wt. basis), mg/kg
Cadmium (dry wt. basis), mg/lig
Copper (dry wt. basis), mg/lig
Chromium, T.(dry wt. basis),mg/kg
Lead (dry weight basis), mg/leg
Magnesium (dry wt. basis), mg/kg
Mercury (dry wt. basis), mg/kg
Nickel (dry wt. basis), mg/kg
Potassium (dry wt. basis), mg/kg
Selenium (dry wt. basis), mg/kg
Sodium (dry wt. basis), mg/kg
Zinc (dry wt. basis), mg/kg
Total Solids, %
TKN (dry wt.), mg/leg
Ammonia Nitrogen (dry wt.),mg/kg
Phosphorus, T. (dry wt.), mg/lcg
Nitrate+Nitrite (dry wt.), mg/kg
Plant Available Nitrogen, mg/kg
Molybdenum (dry wt. basis), mg/lcg
Sludge Analysis Method
Sample Date Analyst Code
6.7
02/21/23
ADR
450OBB-11
3406
03/01/23
MTM
EPA200.7
<2.5
03/06/23
DRC
3113E-04
22013
03/01/23
MTM
EPA200.7
1.1
03/07/23
DRC
3113E-04
260
03/01/23
MTM
EPA200.7
9.6
03/01/23
MTM
EPA200.7
15
03/08/23
DRC
3113B-04
3191
03/01/23
MTM
EPA200.7
0.16
03/14/23
DRC
EPA7471B
12
03/01/23
MTM
EPA200.7
3092
03/01/23
MTM
EPA200.7
<5.0
03/02/23
DRC
3113B-04
I2256
03/01/23
MTM
EPA200.7
2692
03/01/23
MTM
EPA200.7
0.96
02/21/23
HMV
2540G-15
c 69610
03/01/23
BMD
351.2 112-93
c 835.4
03/03/23
BMD
350.1 112-93
c 14710
02/28/23
TRJ
365.4-74
c 24.98
03/02/23
BMD
353.2 R2-93
14198
03/13/23
BMD
<5.0
03/01/23
MTM
EPA200.7
Drinking Water ID: 37715
Wastewater ID1 10
PHONE [phone]
FAX [phone]
ID#: 287 A
DATE COLLECTED: 02/21/23
DATE REPORTED : 03/15/23
J 1
REVIEWED BY: f� v
o Uncertified data. DWR does not offer non -aqueous certification for this analytical procedure.

PI
A
H
P.
E:
Envii-mirnent 1, InC. CHAIN OF CUSTODY RECORD
P.O. Box 7085. 114 Oakmont Or.
Greenville. INC 27858 PagenI
er; v i mn nien l I i nc.com
DISINFECTION
CHLORINE NEUTRALIZED AT COLLECTION
Phone (25-') 756-6208 a Fax [phone]
Ij CHLORINE
CLIENT- 287 A week: 8
uv
LI
pH CHECK (LAB)
P
P
P
P
P
P
P
CONTAINER TYPE, PIG
1BBLE BEACH (HYDROTECH)
A NONE
TTN: DON O'? ARA
CHEMICAL PRESERVATION
YDROTECH
O. BOX 4602
A
A
A
A
A
A
A
WERALD ISLE NC 28594
A -NONE D-NAOH
—
0
52) 725-2319
La.i U
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G NATHIOSULFATE
SAMPLE LOCATION
DATE
TIME
iry
S
Sludge Sample
5
¢•!
^
YJ.ti
CLASSIFICATION:
WASTEWATER(NPDES)
DRINKING WATER
DWR/GW
SOLID WASTE SECTION
CHAIN OF CUSTODY (SEAL) MAINTAINED
IPMENT/DELIVERY
DURIZ__
N
SAMPLES COLLECTED BY;
{Please Print}
�'
SAMPLES RECE ED IN LAB ATj,!�_ °C
RE 12U]EDB IG.)(SAMPLER)
DATEITIME
RECEIVED BY (SIG.)
D TERIME
COMMENTS:
RELINQUIS (SIG.)
DATEITIME
RECkWED BY Or)
OATEINE
RELINQUISHED BY (SIG.)
DATErnME
RECEIVED BY (SIG.)
DATEfnME
PLEASE READ Instructions for completing this form on the reverse side. Sampler must place a "C" for composite sample or a "G" for FORM #s Grab sample in the blocks above for each parameter requested. o412650

BARNES ENVIRONMENTAL WASTE
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: January 26, 2023
Permit No. WQ0018525
Pennertree 0.68 % Solids
12.14 pH (taken from lime stabilization event)
Parameter
%
Mg/Kg Dry Weight
(% x 10,000)
Pounds[Dry Ton
(Mg/Kg(Mg/Kg x 0.002) :1
Nitrogen (TKN)
4.347
43,470,000
86.940
Phosphorus
1.617
16,170.000
32.340
Potassium
0.351
3,506.000
7.012
PAN (injected)*
L305
13,054.376
26.109
PAN (surface)*
1.305
13,048.386
26.097
Ammonia Nitrogen
0.001
11.980
0.024
Calcium
3,955
39,550.000
79.100
Calcium Carbonate E ,
-__
___
---
Magnesium
---
2,380.000
4.760
Sodium
---
20,026.000
40.052
Sulfur
---
___
Nitrate N / Nitrite N
---
4.990
0.010
Barium
---
---
---
SAR
2.18
Chloride
---
---
_-.
Iron
---
---
---
Ceiling Concen.
(Mg/Kg)
Aluminum
---
3,063.000
6.126
Arsenic
---
2.50
0.005
75
Cadmium
---
1.00
0.002
85
Chromium
---
17.000
---
---
Copper
---
404.00
0.808
4,300
Lead
---
11.00
0.022
840
Mercury
---
0.26
0.001
57
Molybdenum
---
5.00
0.010
75
Nickel
---
13.00
0.026
420
Selenium
---
5.00
0.0I0
100
Zinc
---
2,I83.00
4.366
7,500
Environment 1 # 129 C
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits
for calculation purposes.

��ddQo����� Ala ��c�oQpoQa��d
Wastewater -IDS 10
114 OAKMONT DRIVE
GREENVILLE, N.C. 27858
PEPPERTREE RESORTS (FORTIN)
ATTN: MR. DAN FORTIN
P.O. BOX 1068
ATLANTIC BEACHr NC 28512
PARAMETERS
Aluminum, (dry wt. basis), mgllcg
Arsenic (dry wt. basis), mg/kg
Calcium (dry wt. basis), mg/kg
Cadmium (dry wt. basis), mg/kg
Copper (dry wt. basis), mg/kg
Chromium, T.(dry wt. basis),mglkg
Lead (dry weight basis), mg/kg
Magnesium (dry wt. basis), mg/kg
Mercury (dry wt. basis), mg/kg
Nickel (dry wt. basis), mg/lig
Potassium (dry wt. basis), mg/kg
Selenium (dry wt, basis), mg/kg
Sodium (dry wt. basis), mg/kg
Zinc (dry wt. basis), mg/lig
Total Solids, %
TKN (dry wt.), mg/kg
Ammonia Nitrogen (dry wt.),mg/kg
Phosphorus, T. (dry wt.), mg/kg
Nitrate+Nitrite (dry wt.), mglkg
Plant Available Nitrogen, mg/kg
Molybdenum (dry wt. basis), mg/kg
Sludge Analysis Method
Sample Date Analyst Code
3063
02/10/23
MTM EPA200.7
<2.5
02/01/23
DRC
3113B-04
39550
02/10/23
MTM
EPA200.7
1.0
02/02/23
DRC
3113E-04
404
02/10/23
1VITM
EPA200,7
17
02/10/23
MTM
EPA200.7
11
02/02/23
ARC
3113E-04
2380
02/10/23
MTM
EPA200.7
0.26
02/14/23
DRC
EPA7471B
13
02/10/23
MTM
EPA200.7
3506
02/10/23
MTM
EPA200.7
<5.0
02/02/23
DRC
3113E-04
20026
02/10/23
MTM
EPA200.7
2183
02/10/23
MTM
EPA200.7
0.68
01/26/23
JMS
254OG-15
c 43470
01/31/23
BMD
351.2 R2-93
c 11.98
02/01/23
KES
350.1 R2-93
c 16170
01/31/23
TRJ
365.4-74
c 4.99
02/02/23
ICES
353.2 R2-93
13048
02/03/23
BMD
<5.0
02/10/23
MTM
EPA200.7
PHONE [phone]
FAX [phone]
ID#: 129 C
DATE COLLECTED: 01/26/23
DATE REPORTED : 02/15/23
REVIEWED BY: 1 �\
c Uncertified data. DWR does not offer non -aqueous certification for this analytical procedure.

Envirnninen4 1, [tic. CHAIN OF CUSTODY RECORD
P.O. Box 7085. 114 Oakmont [fir. Page 1 of 1
Greenvilic NC'785ti
environment I ine.com
r7I5INFLCTION
CHLORINE NEUTRALIZED AT COLLECTION
]']1[�Ite (252) 75fi-(>"_'O8 • Rix ('�5'?) 756-06?_�
Ij CIILO121NC
CLIENT: 129 C Week: 10
UV
pH CHECK (LAB)
EPPERTREE RESORTS (FORTIN)
NONE
P
P
P
P
P
P
CONTAINER TYPE.P1G
TTN: MR. DAN FORTIN
.O. BOX 1068
CHEMICAL PRESERVATION
TLANTIC BEACH NC 28512
❑
A
A
A
A
A
A
A - NONE D - NAOH
E p
,52) 247-5841
r
z�
L z
L
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B- HNO, E- HCL
Mo
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COLLECTION
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G-NATHIOSULFATE
SAMPLE LOCATION
DATE
TIME
`` .
'
Sludge Sample
��
4
€ '
a
11.. --
%'
CLASSIFICATION;
WASTEWATER(NPDES)
LlDRINKING WATER
DWRlGW
SOLID WASTE SECTION
CHAIN OF CUSTODY (SEAL) MAINTAINED
DURING IPMENT/DELIVERY
Y N
SAMPLES COLLECTED BY:
(Please Print) c L
Who J wt
FtlSAMPLES
RECEIVED IN LAB AT IC
RELINQUISHED B SIG.) ( PLER)
RECEIVED BY {SIG.)
DATEMME
COMMENTS:
l 7�rJ..ATEMME :p$
112,6I23 3 = 3
LINQUISHED IG.)
DATEMME
RECEIVED BY (SIG.)
DATEMME
RELINQUISHED BY (SIG.)
DATEMME
RECEIVED BY (SIG.)
DATEMME
PLEASE READ Instructions for completing this form on the reverse side. Sampler must place a "C for composite sample or a "G" for Ng 41 ZZQ9
FORM h5 Grab sample in the blocks above for each parameter requested.

BARNES ENVIRONMENTAL WASTE
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type. Wastewater Treatment Plant
Date Sampled: January 12, 2023
Permit No. WQ0018525
Point Emerald Villas 0.66 % Solids
8.3 pH
Parameter
%
Mg/Kg Dry Weight
(% x I0,000)
Pounds/Dry Ton
(Mg/Kg(MglKg x 0.002)
Nitrogen (TKN)
5.254
38,650.000
77.300
Phos horus
1.482
8,527.000
17.054
Potassium
0.273
3,540.000
7.080
PAN (injected)*
1.601
16,005.380
32.011
PAN (surface)*
1.583
15,834,880
31.670
Ammonia Nitrogen
0.034
207.400
0.415
Calcium
4.028
15,207.000
30.414
Calcium Carbonate E .
---
---
Magnesium
---
2,633.000
5.266
Sodium
---
23,779.000
47.558
Sulfur
---
_--
Nitrate N / Nitrite N
---
5.580
0.011
Curium
__-
_--
_--
Chloride
---
Iron
---
_--
---
Aluminum
---
5,042.00
10.084
Arsenic
---
2.50
0.005
Cadmium
---
0.90
0.002
Chromium
---
14.000
---
Co er
---
396.00
0.772
Lead
---
37.00
0.074
Mercury
---
0.27
0.001
Molybdenum
---
5.00
0.010
Nickel
---
13.00
0.026
Selenium
---
5.60
0.011
Zinc
---
2,369.00
4.738
Environment 1 # 348 A
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN
Note. Constituents N.D. (Not Detected) or < detection limits arc listed as detection limits
for calculation purposes.
SAR
3.79
Ceiling Concen.
(Mg/Kg)
75
85
4,300
840
57
75
420
100
7,500

ERW'n1@ @W % hmpumud
114 OAKMONT DRIVE
GREENVILLE, N.C. 27858
POINT EMERALD VILLAS (FORTIN)
MR. DAN FORTIN
FORTIN CONTRACT SERVICES
P.O. BOX 4188
EMERALD ISLE, NC 28594
PARAMETERS
PH, Units (Non -Aqueous)
Aluminum, (dry wt. basis), mglkg
Arsenic (dry wt. basis), mg/kg
Calcium (dry wt. basis), mg/kg
Cadmium (dry wt. basis), mgllcg
Copper (dry wt. basis), mg/kg
Chromium, T.(dry wt. basis),mg/kg
Lead (dry weight basis), mg/Icg
Magnesium (dry wt. basis), mgllcg
Mercury (dry wt. basis), mg/kg
NiCkel (dry wt. basis), mglkg
Potassium (dry wt, basis), mgllcg
Selenium (dry wt. basis), mglkg
Sodium (dry wt. basis), mglkg
Zinc (dry wt. basis), mg/kg
Total Solids, %
TKN (dry wt.), mg/kg
Ammonia Nitrogen (dry wt.),mg/icg
Phosphorus, T. (dry wt.), mgllcg
Nitrate+Nitrite (dry wt.), mg/kg
Molybdenum (dry wt. basis), mg/kg
Sludge Analysis Method
Sample Date Analyst Code
c 8.3
01/17/23
JMS 4500HB-11
5042
01/20/23
NITM EPA200.7
C 2.5
01/20/23
DRC 3113B-04
15207
01/20/23
MTM EPA200.7
0.9
01/24/23
DRC 3113E-04
386
01/27/23
MTM EPA200.7
14
01/20/23
MTM EPA200.7
37
01/23/23
DRC 3113E-04
2633
01/20/23
MTM EPA200.7
0.27
01/30/23
DRC EPA7471B
13
01/20/23
MTM EPA200.7
3540
01120/2.3
MTM EPA200.7
5.6
01/23/23
DRC 3113B-04
23779
01/20/23
MTM EPA200.7
2369
01/20/23
MTM EPA200.7
0,66
01/12/23
JMS 254OG-15
c 38650
01/18/23
BMD 351.2 R2-93
c 207.4
01/24/23
KES 350.1 R2-93
c 8527
01/24/23
TRJ 365.4-74
c 5.58
01/25/23
BMD 353.2 R2-93
5.0
01/20/23
MTM EPA200.7
Drinking Water ID: 37715
Waatewa ter ID: 10
PHONE [phone]
FAX [phone]
ID#: 348 A
DATE COLLECTED: 01/12/23
DATE REPORTED : 01/31/23
REVIEWi3D BY:
c Uncertified data. DWR does not offer non -aqueous certification for this analytical procedure.

P(
M
F(
P.
EI
Envirozimcat 1. Iiie. CHAIN OF CUSTODY RECORD
P-U. Box 7085, 114 Oakmont Dr. Pane 1 OF 1
C,reenviDe. N(. 27858
ens ironmei41 inc.com
DISINFECTION
CHLORINE NEUTRALIZED AT COLLECTION
Ph6ne (25_) 755-6208 • Fax [phone]
CI-iLORiNF,
CLIENT: 348 A Week: 8
UV
pH CHECK (LAB)
P
P
P
P
P
P
P
CONTAINER TYPE, PIG
)INT EMERALD VILLAS (FORTTN)
NONE
R. DAN FORTIN
}RTIN CONTRACT SERVICES
CHEMICAL PRESERVATION
O. BOX 4188
A
A
A
A
A
A
A
VI)ERALD ISLE NC 28594
A - NONE D - NAOH
z
o
52) 393-8720
L6z
,�,,
^o
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%
w
B HNO3 E HCL
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c}
LUC HP, F -ZINC ACETATE/NROH
COLLECTION
n
W J
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N
7
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< G- NATHIOSULFATE
Cr
SAMPLELOCATION
DATE
TIME
Sludge Sample
q:�tD
5
<• ' .
�w :..
_ ...
«,....;
CLASSIFICATION:
WASTEWATER(NPDES)
DRINKING WATER
DWRIGW
SOLID WASTE SECTION
CHAIN OF CUSTODY (SEAL) MAINTAINED
DURING SHIPMENT/DELIVERY
Y N
SAMPLES COLLECTED BY.
(Please Pdnt)
No
SAMPLES RECEIVED IN LAB AT 20 -,C
R
QUISHED UY (SIG. (SAMPLER)
DATE(TIME
REC ED BY 51G.]
DATFJi1ME
COMMENTS:
!
11-00
S
R INQUISHED BY (SIG..)
DATEITIME
RECEIVED BY (SIG.J
DATEITIME
RELINQUISHED BY (SIG.)
DATE/TIME
RECEIVED BY (SIG.)
DATEMME
PLEASE READ Instructions for completing this form on the reverse side. Sampler must place a "C" for composite sample or a "G" For ° 4� 2636
FORM #5 Grab sample in the blocks above for each parameter requested.

BARNES ENVIRONMENTAL WASTE
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled. March 10, 2023
Permit No. WQ0018525
Queens Court 1.09 % Solids
7.22 pH
Parameter
%
Mg/Kg Dry Weight
(% x 10,000)
Pounds/Dry Ton
(Mg/Kg(Mg/Kg x 0.002)
Nitrogen (TKN)
4.400
44,000.000
88.000
Phosphorus
1.740
17,400.000
34.800
Potassium
0.904
9,040.000
18.080
PAN (injected)*
1.610
16,099.500
32.199
PAN (surface)*
1.407
14,074.500
28.149
Ammonia Nitrogen
0.405
4,050.000
8.100
Calcium
0.914
9,140.000
18.280
Calcium Carbonate E .
---
---
Magnesium
---
3,120,000
6.240
Sodium
---
16.000,000
32.000
Sulfur
---
__-
Nitrate N / Nitrite N
---
64500
0.129
Barium
---
---
---
SAR
3.84
Chloride
---
---
Iron
---
---
---
Ceiling Concen.
(MQIK )
Aluminum
---
1,360.00
2.720
Arsenic
_..
18.20
0.036
75
Cadmium
---
18.20
0,036
85
Chromium
---
18.200
---
---
Copper
---
173.00
0.346
4,300
Lead
---
18.20
0.036
840
Mercury
---
1.62
0.003
57
Molybdenum
---
18.20
0.036
75
Nickel
---
18.20
0.036
420
Selenium
---
18.20
0.036
100
Zinc
---
1,300.00
2.600
7,500
Envirochem # 2023-04007
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N w % PAN
Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits
for calculation purposes.

ANALYTICAL CONSULTING CHEMISTS ini'o(c,environmentalchemists.com
Fortin Contract Services
Date of Report: Mar 10, 2023
Post Office Box 4188
Customer PO M
Emerald Isle NC
28594
Customer ID: 08100061
Attention-, Dan Fortin
Report M 2023-04007
Project ID: Queens Court
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
23-09927 $Ite: Sludge
2/28/2023
9:00 AM Solid/Sludge Kevin Stanley
Test
Method
Results mate Analyzed
Sludge Residuals
Aluminum
EPA 200.7. Rev, 4,4,1994
1360 mg/kg
03/01/2023
Arsenio
EPA 200.7. Rev, 4.4,1994
<18.2'mg/kg
03/01/2023
Cadmlum
EPA 200.7, Rev, 44,1094
<18,2 mg/kg
03/01/2023
Calcium
EPA 200.7, Rev, 4.4,1994
9140 mg/kg
03/01/2.023
Chromium
EPA 200.1,Rev_.4,4,1904
<18.2mglkg
03/01/2023
Copper
EPA so0,7, Rev. 4.4,1094
173 mg/kg
03/01/2023
Lead
EPA 200.7, Rev, 4A, 1994
<18.2 mg/kg
03/01/2023
Magnesium
EPA 200.7, Rev, 4.4, 104
3120mglkg
03/01/2023
Molybdenum
EPA 200,7, Rev, 4.4, 19a4
<18.2 mglkg
03101 /2023
Nickel
OPA 200;7; Rev. 4.4. W4
<18.2 mg/kg
03/0112023
Potassium
EPA 200.7, Ran, 4,4,1994
9040 mglkg
03/01/2023
Selenium
EPA 200.7, Rev: 4A,1994
<18.2 mglkg
03/01/2023
Sodium
EPA 200,7, Rev. 4A,1994
16000 mglkg
03101 /2023
Zinc
EPA 200,7, Rev, 3.4, 1994
1300 mglkg
03/61 /2023
Nitrate+Nitrite-Nitrogen
EPA 353,2 .
64.5 mg/kg
03/0112023
Total Solids (%)
SM 2 40 0
1.09 %
03/01/2023
Ammonia Nitrogen
SM 4600 NH3 C•2011
4050 mg/kg
03/01/2023
Total Kleldahl Nitrogen (TKN)
SM4600 Norg 8.2011
44000 mglkg
03/01/2023
Total Phosphorus
SM 4500 P (P•H)-2011
17400 mglkg
03/0812023
pH
Result estimated. Analyzed out
SW SO Melhod.9046D
of 15 minutes hold 1lme.
7.22 units
03/0112023
Mercury
SW-046 74716
<1.62 mglkg .
03/03/2023
Report i! . ZOZ3.0Abo7 Pape 1 of 2

BARNES ENVIRONMENTAL WASTE
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: February 21, 2023
Permit No. WQ0018525
Sands Villas 0.61 %Solids
7.5 pH
Parameter
%
Mg/Kg Dry Weight
(% x 10,000)
Pounds/Dry Ton
x 0.0021
Nitrogen (TKN)
6.673
66,730.000
133.460
Phosphorus
1.492
14,920.000
29.840
Potassium
0.698
6,983.000
13.966
PAN (injected)*
2.013
20,126.330
40.253
PAN (surface)*
2.006
20,063.930
40.128
Ammonia Nitrogen
0.012
124.800
0.250
Calcium
2.778
27,778.000
55.556
Calcium Carbonate E .
---
---
---
Magnesium
---
3,755,000
7.510
Sodium
---
21,004.000
42.008
Sulfur
---
-_-
---
Nitrate N / Nitrite N
---
t9.970
0.040
Barium
--_
---
---
SA R
2.45
Chloride
---
---
---
Iron
---
---
---
Ceiling Concen.
(Mg/Kg)
Aluminum
---
1,708.00
3.416
Arsenic
---
2.50
0.005
75
Cadmium
---
0.68
0.001
85
Chromium
---
6.200
---
---
Copper
---
164.00
0.328
4,300
Lead
---
5.70
0.011
840
Mercury
---
0.12
0.000
57
Molybdenum
---
5.00
0.010
75
Nickel
---
8.70
0.017
420
Selenium
--- 1
5.00
0.010
100
Zinc
---
968.00
1.936
7,500
Environment 1 # 559
*Determination of Plant Available Nitrogen (PAN):
Injected Application_
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection Iimits
for calculation purposes.

E1flWoz®1M1ffi&U alp WuPOTMUd
114 OAKMONT DRIVE
GREENVILLE, N.C. 27858
SANDS VILLA (HYDROTECH)
EMAIL DATA & COC
NO MAILED COPY
PARAMETERS
PH (not to be used for reporting)
Aluminum, (dry wt. basis), mg/kg
Arsenic (dry wt. basis), mg/kg
Calcium (dry wt, basis), mg/kg
Cadmium (dry wt. basis), mg/kg
Copper (dry wt. basis), mg/kg
Chromium, T.(dry wt. basis),mg/kg
Lead (dry weight basis), mg/kg
Magnesium (dry wt. basis), mg/kg
Mercury (dry wt. basis), mg/kg
Nickel (dry wt. basis), mg/kg
Potassium (dry wt. basis), mg/kg
Selenium (dry wt. basis), mg/kg
Sodium (dry %vt. basis), mgllcg
Zinc (dry wt, basis), mgllcg
Total Solids, %
TKN (dry wt.), mg/kg
Ammonia Nitrogen (dry wt.),mg/kg
Phosphorus, T. (dry wt.), mg/kg
Nitrate+Nitrite (dry wt.), mg/kg
Molybdenum (dry wt. basis), mg/kg
Sludge
Analysis
Method
Sample
Date
Analyst
Code
7.5
02/21/23
ADR
4500HB-11
1708
03/01/23
MTM
EPA200.7
<2.5
03/06/23
DRC
311313-04
27778
03/01/23
MTM
EPA200.7
0.68
03/07/23
DRC
3113E-04
164
03/01/23
MTM
EPA200.7
6.2
03/01/23
MTM
EPA200.7
5.7
03/08/23
DRC
31138-04
3755
03/01/23
MTM
EPA200.7
0.12
03/I4123
DRC
EPA7471B
8.7
03/01/23
MTM
EPA200.7
6983
03/01/23
MTM
EPA200.7
<5.0
03/02/23
DRC
3113E-04
21004
03/01/23
MTM
EPA200.7
968
03/01/23
MTM
EPA200.7
0.6I
02/21/23
HMV
2540G15
c 66730
03/01/23
BMD
351.2 112-93
c 124.8
03/03/23
BMD
350.1 R2-93
c 14920
02/28/23
TRJ
365.4-74
c 19.97
03/01/23
TRJ
353.2 R2-93
<5.0
03/01/23
MTM
EPA200.7
Drinking Water ID; 37715
Wastewater ID: 10
PHONE [phone]
FAX [phone]
ID#: 559
DATE COLLECTED: 02/21/23
DATE REPORTED : 03/15/23
REVIEWED BY: �% v
c Uncertified data. DWR does not offer non-aqueoua certification for this analytical. procedure.

EE'snvironrnent-1, Inc. CHAIN OF CUSTODY RECORD
P.O. Box 7085. 114 Oakmont Dr.
Page I of 1
Greenville, NC 27858
eirvirnnment I inc.com
DISINFECTION
CHLORINE NEUTRALIZED AT COLLECTION
Phone. E252) 756-6'-08 e Fax [phone]
CHLORINE
CLIENT.- -S ]Week: 13
�
pH CHECK (LAB)
rT V'��:
i fpI l�(HYDROTECH)
NONE
P
P
P
P
P
P
P
P
P
CONTAINER TYPE,PrG
CHEMICALPRESERVATION
EMAIL DATA & COC
'4O MAILED COPY
A
G
C
C
C
A I
A
C
NC 28594
A -NONE D-NAOH
;252) 725-2319
E ti-
z
ca z
ca
M
=
�
C B - HNO E - HCL
o0
_
�n
t3
zCn
¢
Y
Z
o
C- H,SO, F -ZINC ACETATE/NAOH
COLLECTION
CD
o o¢
w
mi C)L
O
E
z
4
_�
7
k
E�
G NAiHIOSULFATE
cc
SAMPLE LOCATION
DATE
TIME
EMuent
( 7f
1
iISZ
5
CLASSIFICATION:
C WASTEWATERJNPDES)
DRINKINGWATER
DWR/GW
SOLID WASTE SECTION
CHAIN OF CUSTODY (SEAL) MAINTAINED
DURING SHIPMENT/DELIVERY
Y N
SAMPLES COLLECTED BY,
(Please Print)
SAMPLES RECEIVED IN LAB AT Z °C
RELINQ ISHED BYE (SIG.i (S^AMPLER)
DATE TIME
RECEIVED BY (Sir.)
COMMENT
S:
�JjDATEMME
//7 1
RELIN LiESHED BY (SIG.)
DATEIPME
RECEIVED BY (SIG.)
DATErnME
RELINQUISHED BY (S(G.)
DATEI3IME
RECEIVED BY (SIG.)
DATEITIME
PLEASE READ instructians for completing this form on the reverse side. Sampler must place a "C for composite sample or a "C" for FORM its Grab sample in the blocks above for each parameter requested. N- a
411218

BARNES ENVIRONMENTAL WASTE
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: January 19, 2023
Sea Isle Plantation
Parameter
Phosphorus
Potassium
PAN (injected)*
PAN (surface)*
Ammonia Nitrogen
Calcium
Calcium Carbonate
Magnesium
Sodium
Sulfur
Nitrate N I Nitrite N
Barium
Iron
Aluminum
Arsenic
Cadmium
Chromium
'ickel
elenium
Permit No. WQ0018525
0.97 % Solids
12.15 pH (taken from lime stabilization event)
%
Mg/Kg Dry Weight
(% x 11
Pounds/Dry Ton
1 (Mg/Kg(Mg/Kg x 0.002)
1.917
69,010.000
138.020
0,675
9,892.000
19.784
0.452
6,575,000
13.150
0.581
5,811.128
11.622
0.577
5,772.308
11.545
0.008
1,824.000
3.648
4.831
25,025.000
50.050
---
2,853.000
5.706
---
18,175.000
36.350
---
6.980
0.014
---
1,644.00
3.288
---
2.50
0.005
---
0.60
0.001
---
13.000
---
---
364.00
0.728
---
3 L00
0.062
---
0.18
0.000
---
5.00
0.010
---
13.00
0.026
---
5.00
0.010
---
823.00
1.646
Environment I # 96A
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits
for calculation purposes.
SAR
2.85
Ceiling Concen.
(Mg/Kg)
75
85
4,300
840
57
75
420
100
7,500

Euwu timid % hC0TP0T&@d
114 OAKMONT DRIVE
GREENVILLE, N.C. 27858
SEA ISLE PLANTATION (FORTIN)
MR. DAN FORTIN
FORTIN CONTRACT SERVICES
P.O. BOX 4188
EMERALD ISLE, NC 28594
PARAMETERS
Aluminum, (dry wt. basis), mgllcg
Arsenic (dry wt. basis), mg/kg
Calcium (dry wt. basis), mg/kg
Cadmium (dry wt. basis), mg/kg
Copper (dry wt. basis), mglkg
Chromium, T.(dry wt. basis),mg/kg
Lead (dry weight basis), mg/kg
Magnesium (dry wt. basis), mgllcg
Mercury (dry wt. basis), mglkg
Nickel (dry wt. basis), mgllcg
Potassium (dry wt. basis), mglkg
Selenium (dry wt. basis), mg/kg
Sodium (dry wt. basis), mg/kg
Zinc (dry wt. basis), mg/kg
Total Solids, %
TICN (dry wt.), mg/kg
Anunonia Nitrogen (dry wt.),mg/kg
Phosphorus, T. (dry wt.), mgHcg
Nitrate+Nitrite (dry wt.), mgllcg
Plant Available Nitrogen, mg/kg
Molybdenum (dry wt. basis), mg/kg
Sludge Analysis Method
Sample Date Analyst Code
1644
02/10/73
MTM EPA200.7
<2.5
02/01/23
ARC 3113B-04
25025
02/10/23
MTM EPA200.7
0.6
02/02/23
DRC 311313-04
364
02/10/23
MTM EPA200.7
13
02/10/23
MTM EPA200.7
31
02/02/23
DRC 3113B-04
2853
02/10/23
MTM EPA200.7
0.18
01/30/23
DRC EPA7471B
13
02/10/23
MTM EPA200.7
6575
02/10/23
MTM EPA200.7
<5.0
02/02/23
DRC 3113E-04
18175
02/10/23
MTM EPA200.7
823
02/10/23
MTM EPA200.7
0.97
01/24/23
HMV 254OG-15
c 69010
01/24/23
BMD 351.2 R2-93
c 1824
01/26/23
ICES 350.1 R2-93
c 9892
01/24/23
TRJ 365.4-74
c 6.98
01/26/23
BMD 353.2 112-93
21075
02/03/23
BMD
<5.0
02/10/23
MTM EPA200.7
DrinkingWaterXDc 37715
Wastewater ID: 10
PHONE [phone]
FAX [phone]
ID#: 96 A
DATE COLLECTED: 01/19/23
DATE REPORTED : 02/13/23
REVIEWED BY: ZJM3
�\
c Uncertified data. DWR does not offer non -aqueous certification for this analytical procedure.

SI
M
FI
P.
V
Environment 1, Inc. CHAIN OF CUSTODY RECORD
P.O. Box 7085. 114 Oakmont Dr. Page I _cif _ �
�r.'PPI1111111. �� 77u l.e
environ'llent I in'.Com
DISINFECTION
CHLORINE NEUTRALIZED AT COLLECTION
Phone [phone] • Fax [phone]
CHLORINE
CLIENT: 96 A Week: 8ea
UV
pH CHECK (LAB)
P
P
P
P
P
P
CONTAINER TYPE, PIG
''A ISLE PLANTATION (FORTIN)
NONE
R. DAN FORTIN
)RTIN CONTRACT SERVICES
CHEMICAL PRESERVATION
O. SOX 4188
A
A
A
A
A
A
uERALD ISLE NC 28594
A - NONE D - NAOH
o
52) 393-8720
z-
w Z
w
�o
u
LU
B- HNO, E- HCL
Cc:
_
'r �
U
w
z
z
+
oG
C H,SOA F -ZINC ACETATE/NAQH
COLLECTION
¢
F
o o
U
r ¢
o
u
oft
a
Eo
0
z
4
¢ G NATHIOSULFATE
0�
SAMPLE LOCATION
DATE
TIME
Sludge Sample
1 Into
4:551
1 4
:r " }
l '
CLASSIFICATION:
WASTEWATER (NPDES)
LjDRINKING WATER
DWR/GW
SOLID WASTE SECTION
CHAIN OF CUSTODY (SEAL) MAINTAINED
DURING HIPMENT/DELIVERY
Y N
SAMPLES COLLECTED BY:
(Please Pant)
w
SAMPLES RECEIVED IN LAB AT 1,77 °C
RE NQUISHED
IG.) AMPLER)
DATE/TIME
RECEIVED BY (SIG.)
COMMENTS:
11 �3 �1•�i�
gDATE/T1ME
E11 Llz� ����
-LINQUISHE (SIG.)
ATEIT1ME
RECEIVED BY (SIG.)
DATEinmE
RELINQUISHED BY (SIG.)
DATEMME
RECEIVED BY (SIG.)
DATNIME
Sampler must place a "CI for composite sample or a °G" for
PLEASE READ Instructions for completing this farm on the reverse side. o 4� 2��0
FORM us Grab sample in the blocks above for each parameter requested. N-

BARNES ENVIRONMENTAL WASTE
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: February 21, 2023
Sea Sprav
Parameter
PAN (injected)*
PAN (surface)*
Ammonia Nitrogen
Calcium
Calcium Carbonate
Magnesium
Sodium
Sulfur
Nitrate N / Nitrite N
Curium
Chloride
Iron
Aluminum
um
,ienium
nc
0.97 % Solids
7.2 nH
%
Mg/Kg Dry Weight
(% x 10,000)
2.885
62,750.000
0.416
14,540.000
0A 00
4,206.000
0.889
8,887.200
0.873
8,728,200
0.032
523.700
3.890
36.448.000
--- 2,653.000
--- 12,557.000
--- 9.000
--- 2,533.00
--- 2.50
--- 0.68
--- 9.600
--- 710.00
--- 8.20
--- 0.19
--- 5.00
--- 12.00
--- 5.00
--- 1,232.00
Permit No. WQ0018525
Pounds/Dry Ton
(Mg/Kg x 0.002)
I25.500
29.080
8.412
17.774
17.456
1.047
72.896
Environment 14 560
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or < detection limits are Iisted as detection limits
for calculation purposes.
5.306
25.114
0.018
5.070
0.005
0.001
1.420
0.016
0.000
0.010
0.024
0.010
2.464
SAR
1.68
Ceiling Concen.
(Mg/Kg)
75
85
4,300
840
57
75
420
100
7,500

• �
Way ��nt o
ANALYTICAL
114 OAKMONT DRIVE
GREENVILLE, NC 27858
A PLACE AT THE BEACH II(HYDROTECH)
EMAIL DATA & COC
NO MAILED COPY
PARAMETERS
PH (not to be used for reporting)
Aluminum, (dry wt. basis), mg/Icg
Arsenic (dry wt. basis), mgllcg
Calcium (dry wt. basis), mg/kg
Cadmium (dry wt. basis), mg/kg
Copper (dry wt. basis), mg/kg
Chromium, T.(dry wt. basis),mg/kg
Lead (dry weight basis), mg/kg
Magnesium (dry wt. basis), mg/kg
Mercury (dry wt. basis), mg/kg
Nickel (dry wt. basis), mgllcg
Potassiuln (dry wt. basis), mg/kg
Selenium (dry wt. basis), mg/kg
Sodium (dry wt. basis), mgllcg
Zinc (dry wt. basis), mg/kg
Total Solids,
TICN (dry wt.), mg/kg
Ammonia Nitrogen (dry wt-),mg/kg
Phosphorus, T. (dry wt.), mg/kg
Nitrate+Nitrite (dry wt.), mg/Icg
Molybdenum (dry wt. basis), mgllcg
Sludge Analysis Method
Sample bate Analyst Code
7.2
02/21/23
ADR
450ORB-11
2535
03/01/23
MTM
EPA200.7
<2.5
03/06/23
DRC
3113B-04
36448
03/01/23
MTM
EPA200.7
0.68
03/07/23
DRC
3113E-04
710
03/01/23
MTM
EPA200.7
9.6
03/01/23
MTM
EPA200.7
8.2
03/08/23
DRC
3113E-04
2653
03/01/23
MTM
EPA200.7
0.19
03/14/23
DRC
EPA7471B
12
03/01/23
MTM
EPA200.7
4206
03/01/23
MTM
EPA200.7
<5.0
03/02/23
DRC
3113B-04
12557
03/01/23
MTM
EPA200.7
1232
03/01/23
MTM
EPA200.7
0.97
02/21/23
HMV
2540C-15
c 62750
03101/23
BMD
351.2 112-93
c 523.7
03/03/23
BMD
350.1 R2-93
c 14540
02/28/23
TR.I
365.4-74
c 9.00
03/01/23
TR.I
353.2 R2-93
<5.0
03/01/23
MTM
EPA200.7
Drinking Water ID: 37715
Wastewater ID. 20
PHONE [phone]
FAX [phone]
ID#: 560
DATE COLLECTED: 02/21/23
DATE REPORTED : 03/15/23
1
REVIEWED B dv- "I,
c Unoertified data. DWR does not offer non -aqueous certification for this analytical procedure.

BARNES ENVIRONMENTAL WASTE
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: February 16, 2023
Permit No. WQ0018525
Sound Of The Sea 0.64 % Solids
5.9 pH
Parameter
%
Mg/Kg Dry Weight
(% x 10,000)
Pounds/Dry Too
(Mg/Kg(Mg/Kg x 0.002)
Nitrogen (TKN)
2.885
24,660.000
49.320
Phosphorus
0.416
5,915.000
11.830
Potassium
0.100
5,479.000
10.958
PAN (injected)*
0.888
8,883.I80
17.766
PAN (surface)*
0.872
8,724.180
17.448
Ammonia Nitrogen
0.032
727.700
1.455
Calcium
3.890
30,363,000
60.726
Calcium Carbonate E .
---
---
Magnesium
---
3,477.000
6.954
Sodium
---
12,343.000
24.686
Sulfur
---
---
N i trate N / Nitrite N
---
4.980
0.010
Barium
---
---
---
SAR
1.43
Chloride
---
---
---
Iron
---
---
---
Ceiling Concen.
{M /K )
Aluminum
---
3,335.00
6.670
Arsenic
_--
2.50
0.005
75
Cadmium
---
1.20
0.002
85
Chromium
---
13.000
---
---
Copper
---
1,352.00
2.704
4,300
Lead
---
34.00
0.068
840
Mercury
---
0.22
0.000
57
Molybdenum
---
5.00
0.010
75
Nickel
---
12.00
0.024
420
Selenium
---
5.00
0.010
100
Zinc
2,640.00
5.280
1 7,500
i—----
Environment 19 561
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or < detection limits are Iisted as detection limits
for calculation purposes.

EIMAT01ME&MR % hCupddbd
114 OAKMONT DRIVE
GREENVILLE, N.G. 27858
SOUND OF THE SEA MASTER ASSO.
ATTN: DON O'MARA
HYDROTECH
P.O. BOX 4602
EMERALD ISLE, NC 28594
PARAMETERS
PH (not to be used for reporting)
Aluminum, (dry wt. basis), mg/lig
Arsenic (dry wt. basis), mg/lig
Calcium (dry wt. basis), mg/kg
Cadmium (dry wt. basis), mg/kg
Copper (dry wt. basis), mg/kg
Chromium, T.(dry wt. basis),mglkg
Lead (dry weight basis), mg/lig
Magnesium (dry wt. basis), mg/kg
Mercury (dry wt. basis), mg/kg
Nickel (dry wt. basis), mg/kg
Potassium (dry wt. basis), mglkg
Selenium (dry wt. basis), mg/kg
Sodium (dry wt. basis), mg/kg
Zinc (dry wt. basis), mg/lig
Total Solids, %
TKN (dry wt.), mg/kg
Ammonia Nitrogen (dry wt.),mglkg
Phosphorus, T. (dry wt.), mglkg
Nitrate+Nitrite (dry wt.), mgllig
Molybdenum (dry wt. basis), mg/kg
Sludge Analysis Method
Sample Date Analyst Code
5.9
02/16/23
ADR 4500HB-11
3335
03/01/23
MTlvl EPA200.7
<2.5
03/06/23
DRC 311313-04
30363
03/01/23
MTM EPA200.7
1.2
03/07/23
DRC 3113E-04
1352
03/01/23
MTM EPA200.7
13
03/01/23
MTM EPA200.7
34
03/08/23
DRC 311311-04
3477
03/01/23
MTM EPA200.7
0.22
02/23/23
DRC EPA7471B
12
03/01/23
MTM EPA200.7
5479
03/01/23
MTM EPA200.7
<5.0
03/02/23
DRC 3113B-04
12343
03/01/23
MTM EPA200.7
2640
03/01/23
MTM EPA200.7
0.64
02/16/23
BLV 254OG-15
c 24660
02/23/23
TRJ 351.2 R2-93
c 727.7
02/27/23
BMD 350.1 R2-93
c 5915
02/23/23
BMD 365.4-74
c 4.98
02/27/23
TRJ 353.2 R2-93
< 5.0
03/01/23
MTM EPA200.7
Drinking Water ID: 37715
Wastewater ID: 10
PHONE [phone]
FAX [phone]
ID#: 561
DATE COLLECTED: 02/16/23
DATE REPORTED ; 03/09/23
REVIEWED BY:
c Uncertified data. DWR does not offer non -aqueous certification for this analytical procedure.

Envii-onnacnt 1. Inc. CHAIN OF CUSTODY RECORD
P.O. Box 7085. 114 Oakmont Dr. Page 1 of 1
(ircenvillc. NC 1785.i
environment! i nc.com,
DISINFECTION
CHLORINE NEUTRALIZETIAT COLLECTION
Phone [phone] " Fax (25Z) 756-0633
CHl..OItINT3
CLIENT: 561 Week: 8
Lf V
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pH CHECK (LAB)
p
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DONE
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YDROTECH
J
CHEMICAL PRESERVATION
.O. SOX 4602
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HERALD ISLE NC 28594
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SAMPLE LOCATION
DATE
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CLASSIFICATION:
WASTEWATER(NPDES)
DRINKINGWATER
FA DWRIGW
SOLID WASTE SECTION
CHAIN OF CUSTODY (SEAL) MAINTAINED
DURING SHIPMENT/DELIVERY
Y N
SAMPLES COLLECTED BY:
(Please Print)
SAMPLES REC9kD IN LAB AT
RED HE Y IG. (SAMPLER}
ATErRME
RECEIVED BY (SIG.)
DATEMME
COMMENTS:
i r
zs
ELINQUISHED BY (SIG.)
DATEMME
RECEIVED BY (SIG.)
DATEMME
RELINQUISHED BY (SIG.)
DATEMME
RECEIVED BY (SIG.)
DATEMME
Sampler must place a "C" for composite sample or a "T for
PLEASE READ Instructions for completing this form on the reverse side. �� 4 3045
FORM 85 Grab sample in the blocks above for each parameter requested.

r K^ 0
Waypon
ANALYTICAL
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 Fax [phone]
www.waypointanalytical.com
Waypoint Analytical LLC, a national leader in environmental and agricultural testing, announces the
successful transaction to acquire Environment 1, Inc., a Greenville, NC based environmental testing
company.
Environment 1, Inc., an environmental testing and field services provider has been a business concern
since 1974. The company employs very experienced, educated, and talented scientists, laboratory
technicians, and support personnel in Greenville, NC. Their expertise is supported by environmental
certifications held in the markets served including comprehensive environmental laboratory certifications
granted by the State of North Carolina.
Environment 1, Inc. provides a wide array of laboratory and field services to industries, municipalities, local
and state agencies, and residential customers. The wastewater and drinking water regulatory compliance
testing offered by the company is unparalleled in quality and service consistency. This has allowed for
steady growth for decades through client recommendations and word of mouth.
The acquisition of Environment 1, Inc. allows Waypoint Analytical LLC, now with three laboratory locations
and numerous field services and support locations in North Carolina to provide more support and analytical
depth with greater expediency than any other laboratory in the state. This acquisition reflects the ongoing
efforts of Waypoint Analytical LLC to make available the best laboratory services and field support services
to its clients wherever they are located.
Comment from Nathan A. Pera IV, Waypoint Analytical LLC's Environmental Division President: "The
addition of Environment 1 to the Waypoint Analytical Family is just one more step toward our goal of
improving the lives of the people in the communities in which we operate. We do this by offering higher
quality, client -focused and ever-expanding laboratory services to the businesses and agencies therein. We
are extremely pleased to welcome the talented Environment 1 Team to our family. Their dedication to
service, their reputation for outstanding quality, and the E-1 geographic footprint further strengthen
Waypoint's reputation and helps cement our ranking as the best in lab service. Expanding our footprint to
include the addition of the laboratory in eastern North Carolina demonstrates our commitment to the
industries and to the communities that Waypoint Analytical calls home. Waypoint is embracing those clients
and communities who are responsible for our success."
Comment from Mr. Mark Oliveira, President of Environment 1, Inc.: "Elizabeth and our team at
Environment 1 have dedicated many years to offering, the best quality and service to our customers. The
Waypoint Analytical vision of bringing lab testing and lab support services closer to the people needing
those services, especially in those communities that other lab companies have no interest in investing in,
made our choice for the future an easy one. Waypoint allows the Environment 1 lab team to expand upon
our 49 years of dedication to our customers and our community. They bring all of the resources that smaller
labs cannot access. We look forward to tapping into the diverse talent and experience of Waypoint's
personnel, redundant North Carolina certifications, equipment, and wide-ranging capabilities_ Waypoint
offers all the advantages of a large laboratory while focusing on the personalized service that our clients
deserve. Our team is excited to be joining forces with Waypoint. We look forward to providing more
resources to our customers, employees, and community."
For more information, please visit www.waypointanalytical.com or contact:
Ann Baynor — aba nor environment) inc.com or Mark Oliveira — moliveira6Denvironment1 inc.com

BARNES ENVIRONMENTAL WASTE
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: February 21, 2023
Permit No. WQ0018525
Southrvinds Condominiums 0.99 % Solids
7.4 pH
Parameter
%
Mg/Kg Dry Weight
(% x 10,000)
Pounds/Dry ion
(Mg/Kg(Mg/Kg x 0.002)
Nitrogen (TKN)
6.967
69,670.000
139.340
Phosphorus
1.695
16,950.000
33.900
Potassium
0.338
3,383.000
6.766
PAN (injected)*
2.105
21,050.000
42.100
PAN (surface)*
2.095
20,950.000
41.900
Ammonia Nitrogen
0.020
200.000
0.400
Calcium
6.400
64,003.000
128.006
Calcium Carbonate E .
---
---
Magnesium
---
2.943.000
5.886
Sodium
---
10,094,000
20.188
Sulfur
---
---
---
Nitrate N / Nitrite N
---
9.000
0.018
Barium
---
---
---
SA R
1.05
Chloride
---
---
---
Iron
---
---
---
Ceiling Concen.
(M /K�
Aluminum
---
4199.000
8.398
Arsenic
---
2.50
OA05
75
Cadmium
---
0.78
0.002
85
Chromium
---
12.500
---
---
Copper
---
665.00
1.330
4,300
Lead
---
12.00
0.024
840
Mercury
---
0.24
0.000
57
Molybdenum
---
5.00
0.010
75
Nickel
---
9.80
0.020
420
Selenium
---
5.00
0.010
100
Zinc
---
I,561.00 1
3.122
7,500
Environment 1 # 562 B
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N +Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits
for calculation purposes.

Waypoint.
ANALYTICAL
114 OAKMONT DRIVE
GREENVILLE, NC 27858
SOUTHWINDS (HYDROTECH)
EMAIL DATA & COC
NO MAILED COPY
PARAMETERS
PH (not to be used for reporting)
Aluminum, (dry wt. basis), mgllcg
Arsenic (dry wt. basis), mglkg
Calcium (dry wt. basis), mglkg
Cadmium (dry wt. basis), mgllcg
Copper (dry wt. basis), mg/kg
Chromium, T.(dn, wt. basis),mg/kg
Lead (dry weight basis), mglkg
Magnesium (dry wt. basis), mgllcg
Mercury (dry wt. basis), mg/Itg
Nickel (dry wt. basis), mgllcg
Potassium (dry wt. basis), mg/kg
Selenium (dry wt. basis), niglkg
Sodium (dry wt. basis), mg/kg
Zinc (dry wt. basis), mgllcg
Total Solids, %
TKN (dry wt.), mg/kg
Ammonia Nitrogen (dry wt.),mglicg
Phosphorus, T. (dry wt.), mgllcg
Nitrate+Nitrite (dry wt.), mgllcg
Molybdenum (dry wt. basis), mgllcg
Sludge
Analysis
Method
Sample
Date
Analyst
Code
7,4
02/21/23
ADR
4500HB-11
4199
03/01/23
MT11-[
EPA200.7
<2.5
03/06/23
DRC
31I3B-04
64003
03/01/23
14ITM
CPA200.7
0.78
03/07/23
DRC
3113B-04
665
03/01/23
1blTitil
EPA200.7
12.5
03/01/23
A-ITNI
EPA200.7
12
03/08/23
DRC
3113B-04
2943
03101/23
MTNI
EPA200.7
0.24
03/14/23
DRC
EPA747IB
9.8
03101/23
NlTlikl
EPA200.7
3383
03/01/23
MTM
EPA200.7
<5.0
03/02/23
DRC
3113B-04
10094
03/01/23
MTM
EPA200.7
1561
03/01/23
11ITM
EPA200.7
0.99
02/21/23
HMV
254OC-15
c 69670
03/01/23
BMD
351.2 R2-93
c 200.0
03/03/23
BibID
350.1 R2-93
c 16950
02/28/23
TRJ
365.4-74
c 9.00
03/01/23
TRJ
353.2 R2-93
< 5.0
03/01/23
MTM
EPA200.7
Drinking Water ID: 37715
Wastewater ID: 10
PHONE [phone]
FAX [phone]
ID#: 562 B
DATE COLLECTED: 02/21/23
DATE REPORTED : 03/15/23
REVIEWED BY:
c uncertified data. DWR does not offer non -aqueous certification for this analytical procedure.

BARNES ENVIRONMENTAL WASTE
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: February 21, 2023
Permit No. WQ0018525
Summer Winds 0.76 % Solids
4.5 pH
Parameter
%
Mg/Kg Dry Weight
(% x 10,OOo}
Pounds/Dry Ton
(Mg/Kg x 0.002)
Nitrogen (TKN)
2.133
21,330.000
42.660
--Phosphorus
2.367
23,670.000
47340
Potassium
1.069
10,694.000
21.388
PAN (injected)*
4.210
42,098.110
84.196
PAN (surface)*
4.168
41,684.460
83.369
Ammonia Nitrogen
0.083
827.300
1.655
Calcium
6.139
61,388.000
122.776
Calcium Carbonate E .
---
---
Magnesium
---
7,890,000
15.780
Sodium
---
45,900,000
91.800
Sulfur
---
---
Nitrate N / Nitrite N
---
35,120.000
70.240
Barium
---
---
---
Chloride
---
---
---
Iron
---
---
Aluminum
---
1,530.00
3.060
Arsenic
---
2.50
0.005
Cadmium
---
0.61
0.001
Chromium
---
7.100
Copper
---
421.00
0.842
Lead
---
6.90
0,014
Mercury
---
0.16
0.000
Molybdenum
---
5.00
0.010
Nickel
---
10.00
0.020
Selenium
---
5.00
0.010
Zinc
--- 1
1,393.00
2.786
Environment I tl 119A
*Determination of Plant Available Nitrogen (PAN):
Injected Application_
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits
for calculation purposes.
SAR
F-4.03
Ceiling Coneen.
(M /K }
75
85
4,300
840
57
75
420
too
7,500

114 OAKMONT DRIVE
GREENVILLE, N.C. 27858
SWNC MASTER OWNERS ASSOC, INC
ATTN: DON O'MARA
HYDROTECH; SUMMER WINDS
P.O. SOX 4602
EMERALD ISLE, NC 28594
PARAMETERS
PH (not to be used for reporting)
Aluminum, (dry wt. basis), mg/kg
Arsenic (dry wt. basis), mg/kg
Calcium (dry wt. basis), mg/kg
Cadmium (dry wt. basis), mg/kg
Copper (dry wt. basis), mglkg
Chromium, T.(dry wt. basis),mgllcg
Lead (dry weight basis), mgllcg
Magnesium (dry wt, basis), mg/kg
Mercury (dry wt. basis), mg/kg
Nickel (dry wt. basis), mgllcg
Potassium (dry wt. basis), mgllcg
Selenium (dry wt. basis), mg/kg
Sodium (dry wt. basis), mgllcg
Zuie (dry wt, basis), mg/lcg
Total Solids,
TKN (dry wt.), mg/Icg
Ammonia Nitrogen (dry wt.),mglkg
Phosphorus, T. (dry wt.), mg/Icg
Nitrate+Nitrite (dry wt.), mg/kg
Molybdenum (dry wt. basis), mg/kg
Sludge Analysis Method
Sample Date Analyst Code
4.5
02/21/23
ADR 4500HB-11
1530
03/01/23
MTM EPA200.7
G2.5
03/06/23
DRC 311313-04
61388
03/01/23
MTM EPA200.7
0.61
03/07/23
DRC 3113E-04
421
03/01/23
MTM EPA200.7
7.1
03/01/23
MTM EPA200.7
6.9
03/08/23
DRC 3113E-04
7890
03/01/23
MTM EPA200.7
0.16
03/14/23
DRC EPA7471B
10
03/01/23
MTM EPA200.7
10694
03/01/23
MTM EPA200.7
C 5.0
03/02/23
DRC 311313-04
45900
03/01/23
MTM EPA200.7
1393
03/01/23
MTM EPA200.7
0.76
02/21/23
HMV 2540G-15
c 21330
03/01/23
BMD 351.2 R2-93
c 827.3
03/03/23
BMD 350.1 R2-93
c 23670
02/28/23
TRJ 365.4-74
c 35120
03/02/23
BMD 353.2 R2-93
C 5.0
03/01/23
MTM EPA200.7
Drinking Water ID: 37715
Wastewater ID: 10
PHONE [phone]
FAX [phone]
ID#: 119 A
DATE COLLECTED: 02/21/23
DATE REPORTED : 03/15/23
REVIEWED BY: 4
c Uncertified data. DWR does not offer non -aqueous certification for this analytical procedure.

Environment l,Ine. CHAIN OF CUSTODY RECORD
P.O. Box 7035, 114 Oakmont Dr, Page 1 of 1
Cireenville_ NC 27,S5R
environment I nc.com
DISINFECTION
CHLORINE NEUTRALIZED AT COLLECTION
Phone [phone] • Fax [phone]
CHLORINE:
CLIENT: 119 A Week- 10
pH CHECK (LAB)
Ij UV
p
p
p
p
p
p
P
CONTAINER TYPE. PIG
WNC MASTER OWNERS ASSOC, INC
NONE
TTN: DON O'MARA
CHEMICAL PRESERVATION
NDROTECH; SUMMER WINDS
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DRINKINGWATER
DWRIGW
SOLID WASTE SECTION
CHAIN OF CUSTODY (SEAL) MAINTAINED
DURING SHIPMENT/DELIVERY
t,Y 1 N
SAMPLES COLLECTED BY:
(Please Port}
SAMPLES RECEIVED IN LAB AT _ "C
RELINQUt HED BY (SIG.) (SAMPLER)
DATEMME
RECE VED BY (S1 . r
DATFIR E
COMMENTS:
RELINQ (SHED BY (SIG.)
MruflME
FlEtEIVED BY (510.)
DATEMME
RELINQUISHED BY (SIG.)
DATEIIIME
RECEIVED BY (SIG.)
TDATOTIME
PLEASE READ Instructions for completing this form on the reverse Side. Sampler must place a "C" for composite sample or a "G" for o 41 ��1
FORM S5 Grab sample in the blocks above for each parameter requested.

BARNES ENVIRONMENTAL WASTE
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment PIant
Date Sampled: February 21, 2023
Permit No. WQ0024756
The Grove WWTP 0.69 % Solids
6.9 p H
Parameter
%
Mg/Kg Dry Weight
(% x 10,000)
Pounds/Dry Ton
(Mg/Kg(Mg/Kg x 0.002)
Nitrogen (TKN)
6.971
69,710.000
139.420
Phosphorus
2.590
25,900.000
51.800
Potassium
0.827
8,272.000
16.544
PAN (injected)*
2.251
22,506.000
45.012
PAN (surface)*
2.I38
21,381.000
42.762
Ammonia Nitrogen
0.225
2,250.000
4.500
Calcium
2.311
23,108.000
46.216
Calcium Carbonate E .
---
-_-
___
Ma nesium
---
5,538.000
11.076
Sodium
---
14,358,000
28.716
Sulfur
---
---
Nitrate N / Nitrite N
---
18.000
0.036
Barium
---
---
---
SAR
1.82
Chloride
---
---
---
Iron
---
---
---
Ceiling Concen.
(Mg/Kg)
Aluminum
---
1194.000
2.388
Arsenic
---
2.50
0.005
75
Cadmium
---
0.59
0.001
85
Chromium
---
9.100
---
---
Copper
---
106.00
0.212
4,300
Lead
---
5.00
0.010
840
Mercury
---
0.05
0.000
57
Molybdenum
---
5.00
0.010
75
Nickel
---
11.00
0.022
420
Selenium
---
5.00
0.010
100
Zinc
---
893.00
1.786
7,500
Environment I # 549 A
Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits
for calculation purposes.

ANIL
ILTAM
Waypoel t-W
ANALYTICAL
114 OAKMONT DRIVE
GREENVILLE, NC 27858
THE GROVE WWTP (HYDROTECH)
EMAIL DATA & COC
NO MAILED COPY
PARAMETERS
PH (not to be used for reporting)
Aluminum, (dry wt. basis), mglkg
Arsenic (dry wt. basis), mglkg
Calcium (dry wt. basis), mglkg
Cadmium (dry wt. basis), mg/kg
Copper (dry wt. basis), mglkg
Chromium, T.(dry wt. basis),mg/kg
Lead (dry weight basis), mg/kg
Magnesium (dry wt. basis), mglkg
ivlercury (dry wt. basis), mg/1%
Nickel (dry wt. basis), mglkg
Potassium (dry wt. basis), mglkg
Selenium (dry wt. basis), mglkg
Sodium (dry wt. basis), mglkg
Zinc (dry wt. basis), mg/hg
Total Solids, %
TNN (dry wt.), mg/kg
Ammonia Nitrogen (dry wt.),mg/kg
Phosphorus, T. (dry wt.), mglkg
Nitrate+Nitrite (dry wt.), mgllcg
MoIybdenum (dry wt. basis), mgllcg
Sludge
Analysis
Method
Sample
Date
Analyst
Code
6.9
02/21/23
ADR
4500HB-11
1194
03/01/23
liT1l
EPA200.7
<2.5
03/06/23
DRC
311313-04
23108
03/01/23
NUNI
EPA200.7
0.59
03/07/23
DRC
311313-04
106
03/01/23
NUM
EPA200.7
9.I
03/01/23
NITi1J
EPA200.7
<5.0
03108/23
DRC
31138-04
5538
03/01/23
NITNI
EPA200.7
0.05
03/14/23
DRC
EPA747111
11
03/01/23
NIThl
EPA200.7
8272
03/01/23
MTM
EPA200.7
<5.0
03/02/23
DRC
311313-04
14358
03/01/23
i4IT'M
EPA200.7
893
03/01/23
MTM
EPA200.7
0.69
02/21/23
Hi4IV
254OG-15
c 69710
03101/23
MUD
351.2 112-93
c 2250
02127/23
BID
350.1 R2-93
c 25900
02128/23
TRJ
365.4-74
c 18.00
02127/23
TRJ
353.2 R2-93
<5.0
03/01/23
NITM
EPA200.7
Drinking Water ID: 37715
Wastewater ID; 10
PHONE [phone]
FAX [phone]
ID##: 549 A
DATE COLLECTED: 02/21/23
DATE REPORTED : 03/15/23
REVIEWED BY:
c Uncertified data. DWR does not offer non -aqueous certification for this analytical procedure.

BARNES ENVIRONMENTAL WASTE
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: August 29, 2023
Whaler Inn 1.58 % Solids
7.1 pH
Parameter
%
Mg/Kg Dry Weight
(% x 10,000)
Nitrogen (TKN)
1.60I
64,720.000
Phosphorus
0.397
22,930.000
Potassium
0.399
4,254.000
PAN (injected)*
0.501
5,011.200
PAN (surface)*
0.487
4,866.200
Ammonia Nitrogen
0.029
1,969.000
Calcium
5.591
46,636.000
Calcium Carbonate E .
---
---
Magnesium
---
4,198.000
Sodium
---
6,646.000
Sulfur
---
---
Nitrate N 1 Nitrite N
---
4.000
Barium
---
---
Chloride
---
Iron
---
...-
Aluminum
---
9,668.00
Arsenic
---
2.50
Cadmium
---
0.80
Chromium
---
7.500
Copper
---
693.00
Lead
---
8.70
Mercury
---
0.15
Molybdenum
---
5.00
Nickel
---
12.00
Selenium
---
5.00
Zinc
---
1,267.00
Environment I # 70A
Permit No. WQ0018525
Pounds/Dry Ton
(Mg/Kg(Mg/Kg x 0.002)
129.440
45.860
8.508
10.022
9.732
3.938
93.272
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits
for calculation purposes.
8.396
13.292
0.008
19.336
0.005
0.002
1.3 86
0.017
0.000
0.010
0.024
0.010
2.534
SA R
0.99
ngl<g)
g Concen.
75
85
4,300
840
57
75
420
100
7,500

0
Waypoi t,..
ANALYTICAL
114 OAKMONT DRIVE
GREENVILLE, NC 2785B
THE WHALER INN (BUCK)
C/O MR. STANLEY BUCK
1745 BELGRADE-SWANSBORO RD.
MAYSVILLE, NC 28555
PARAMETERS
P11 (not to he used For reporting)
Aluminum, (dry wt. basis), mgllig
Arsenic (dry wt. basis), mgllig
Calcbirm (dry wt. basis), mg/kg
Cadmium (dry wt. basis), mg/kg
Copper (dry wt. basis), mg/kg
Chromium, T.(dry wt. basis),mg/lig
Lead (dry weight basis), mg/kg
Magnesium (dry wt, basis), mg/kg
Mercury (dry wt, basis), mg/kg
Nickel (dry wt. basis), mg/kg
Potassium (dry wt. basis), mglkg
Selenium (dry wt. basis), mg/kg
Sodium (dry wt. basis), mgllig
Zinc (dry wi. basis), utg/kg
Total Solids, %
TKN (dry wt.), mg/kg
Ammonia Nitrogen (dry wt.),nig/lig
Pbosphorus, T. (dry wt.), mg/kg
Nitrate+Nitrite (dry wt.), mg/kg
Plant Available Nitrogen, mglkg
Molybdenum (dry wt. basis), mg/kg
Sludge Analysis Method
Sample Date Analyst Code
7.1
08/29/23
JMS
4500HB-11
9668
09/06/23
MTM
EPA200.7
C2.5
09/07/23
DRC
311313-04
40636
09/06/23
MTM
EPA200.7
0.8
09/07/23
DRC
311313-04
693
09/06/23
MTM
EPA200.7
7.5
09/06/23
MTM
EPA200.7
8.7
09/07/23
DRC
3113B-04
4198
09/06/23
MTM
EPA200.7
0.15
09/18/23
DRC
EPA7471B
10
09/06/23
MTM
EPA200.7
4254
09/06/23
MTM
EPA200.7
C 5.0
09/06/23
DRC
31138-04
6646
09/06/23
MTM
EPA200.7
1267
09/06/23
MTM
EPA200.7
1.58
08/29/23
ADR
254OG-15
c 64720
09/07/23
AMC
351.2 R2-93
c I969
09/11/23
AMC
350.1 R2-93
c 22930
09/07/23
AMC
365.4-74
c 4.00
09/08/23
BMD
353.2 R2-93
26090
09/15/23
TRJ
C 5.0
09/06/23
MTM
EPA200.7
Drinking Water 1D; 17715
Wantowater ID! 10
PHONE [phone]
FAX [phone]
1D#: 70 A
DATE COLLECTED: 08/29/23
DATE REPORTED : 09/19/23
REVIEWED BY:
c Uncertified data. DWR done not offer non -aqueous certification for thin analytical procedure.

_'Naypciint Va CHAIN OF CUSTODY RECORD
Waypoint Analytical - Greenville Page 1 of I
I l4 UaKmom Ur.
3reenville. NC 27858
DISINFECTION
CHLORINE NEUTRALIZEDAT COLLECTION
wW W.WaypoinLAnaly[ical.coni
To c0.5 mg/L- Yes M or No (NJ
Phone [phone] • Fax [phone]
CHLORIDE
CLIENT: 70 A Week: S
pH CHECK (S.U.) (LAB)
uv
CITE WHALER INN (BUCK)
NONE
p
p
CONTAINER TYPE, PIG
'/0 MR. STANLEY BUCK
CHEMICALPAESERVATION
:745 BELGRADE-SWANSBORO RD.
vdAYSVILLE NC 28555
A -NONE D-NAOH
252) 503-3307
E
z
¢
w
t` B-HNO� E-HCL
O
ur z
o
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F?
w C HMSO, F- ZINC ACETATE/NAOH
COLLECTION
F j
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cc
a n
LU d
o
a
SAMPLELOCATION
DATE
TIME
Sludge Sample/
�'
S
':-s.>:.3
..
,�
L
J
CLASSIFICATION:
WASTEWATER(NPDES)
DRINKINGWATER
DWWC3W
SOLID WASTE SECTION
CHAIN OF CUSTODY (SEAL) MAINTAINED
DURING _ MENT/DELIVERY
Y N
'GO] I ECTED BY'.
(Please Pant) l
SAMPLES RECE ED IN LA13ATQ's °C
RELI UISH DBY SAMPLER)
ATE/TIME
RECEIVED BY (SIG.)
DTElTIME
COMMENTS:
SAMPLES RECEIVED ON ICE: YE - NO
14
jlffL1NCUISH S[G.)
DATEITI
RECEIVE [3Y (SIG.)
❑ATETIME
RELINQUISHED BY (SIG.)
DATErnME
RECEIVED BY (SIG.)
DATEITIME
Sampler must place a "C" for composite sample or a "G" for
PLEASE READ Instructions for completing this farm on the reverse side.
Foam as Grab sample in the blocks above for each parameter requested.

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Barnes Environmental Waste and Hauling, Inc. WQ Permit Number: WQ0018525
WWTP Name: SEE ATTACHED LIST NPDES Number: SEE ATTACHED
Monitoring Period: From 1/l/2023 To 12/3112023
Pathogen Reduction (15A NCAC 02T .1 M61- Please inrlliratP IP.,at gri,ipvQa onrl
Class A:
Alt. A time/tens ❑
{ P)
Alt B Alk Treatment ❑
{ )
Alt. C (Prior Testing)❑
=
Alt.D (No Prior Test) ❑I Process to Further Reduce Patho eggs ❑
If applicable to alternative
performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost ❑
Heat Drying ❑ Heat Treatment ❑ Thenno philic ❑
Beta Ray ❑ 0,unina Ray ❑
Pasteurization ❑
Class B: Alt. (1) Fecal Density ❑
Alt. (2) Process to Significantly Reduce Pathogens El
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization El Air Drying ❑ CornpostiuE ❑ lAerobic Digestion ❑
o '
Anaerobic Digestion 0_
If a licable to alternative erformed Class A or Class B complete the following
pp p { ) p
monitoringin.... at
data:
Allowable Level Pathogen Density Number ot
Parameter
Frequency Sample na tca
P
in Sludge Excee-
g Minima Geo. Mean Maxima Units
Tech-
of Analysis
ysis Type ninilp
2 x 10 to the
MPN
6th power
Fecal Coliform
per gram of
total solids
CFU
1000 mpn per gram
of total solid (dry
weight
Salmonella bacterial
3 MPN per 4 grams
(in lieu of fecal
total solid (dry
coliform)
�,__ l
weight
..v.. A\4M[3{ %yal ki—t3, i�%- %— urrl .11V f) - 1 icase muica[e anernarlve. perrormea:
Aft.1 (VS reduction) ❑ Alt. 2 (40-day bench) ❑ Alt. 3 (30-day bench) ❑ I Alt. 4 (Spec. 0, uptake) ❑
Alt. 5 (I4-Day Aerobic) ❑ Alt. 6 (Alk. Stabilization 1] Alt 7 (Drying - Stable) ❑ lAlt. 8 (Drying - Unstable) ❑
Alt. 9 (Injection) ❑ Alt. 10 (Incorporation) ❑ No vector attraction reduction alternatives were performed ❑
CERTIFICATION STATEMENT (please check the appropriate statement)
El "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note
if you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Steven M. Barnes, President
Preparer Name and Title (type or print)
SM ye, 6
Signature of Preparer* Date
Land Applier Name and Title (if applicable)(type or print)
Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DEAR FORM PVRF 02T (12/2006)

BARNES ENVIRONMENTAL WASTE AND HAULING, INC.
WQ 0018525 ALKALINE STABILIZATION OF WASTEWATER BIOSOLIDS
Facility Name: Hampton Suites 1 aka Alice Hotel P.O.#
Batch Size (gallons): 7,000
Lbs. or Gallons Used: 350
Material Used For Stabilization: Llme
Eno
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BARNES ENVIRONMENTAL WASTE AND HAULING, INC.
WQ 0018525 ALKALINE STABILIZATION OF WASTEWATER BIOSOLIDS
Facility Name: Atlantic Station
Batch Size (gallons): 59,500
P.O.#
Lbs. or Gallons Used: 3,000
Material Used For Stabilization: Lime
Initial pH
>12 pH
2 Hour pH
24 Hour pH
Operator
Date
pH
Temp C
Corr.
Factor +
Corrected
pH
Time
pH
Temp C
Corr,
Factor +
Corrected
pH
Time
pH
Temp C
Corrected
pH
Time
pH
Temp C
Corr.
Factor +
Corrected
pH
Time
Initials
3/8/2023
7.09
26
-0.03
7.12
12:30p
12.21
26
0.03
12.24
2:35p
12.23
26.0
jFac
12.26
2:35pm
12.3
26.0
-0.03
12.33
12:45p
SMB
3/27/2023
7.11
25
0
7.11
8:00am
12.15
24
-0.03
12.12
:05a
12.15
25.012.1510:15a
12.19
25.0
0.00
12.19
8:30am
SMB
4/26/2023
7.45
25
0
7.45
9:00am
12.46
26
0.03
12.491:35an.
:05a
12.45
26.0
0.03
12.4811:05a
12.43
27.0
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12.49
9:15am
SMB
5/10/2023
7.22
27
0.06
7.28
8:30am
12.50
26
0.03
12.53:35a
12.46
27.0
0.06
12.5210:35a
12.36
26.0
0.03
12.39
9:00am
SMB
6/20/2023
6.78
30
0.15
6.93
8:00am
12.10
30
0.15
12.25:05a
12.03
30.0
0.15
12.1810:15a
12.09
31.0
0.18
12.27
8:30am
SMB
7/412023
6.8
31
0.18
6.98
9:00am
12.24
32
0.21
12.45:05a
12.1
32.0
0.21
12.31
10:10a
12.15
32.0
0.21
12.36
9:30am
SMB
7/17/2023
7.41
34
0.27
7.68
8:30am
12.19
33
0.24
12.4312,14
34.0
0.27
12.41
10:35a
12.16
35.0
0.30
12.46
9:00am
SMB
8/10/2023
7.23
37
0.36
7.59
9:00aml
12.10
36
0.33
12.43
9:05arr
12.05
37.0
0.36
12.41
11:30arr
12.1
38.0
0.39
12.49
9:30am
SMB
8/15/2023
7.28
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0.27
1 7.55
10:00a
12.291
34
0.27
12.56
0:05ar
12.21
35.0
0.3
12.51
12:15prT
12.23
35.0
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10:10a
SMB
9/12/2023
7.31
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0.24
7.55
11 Marr
12.35
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12.53
1:05a
12.18
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12.42
1:35pm
12.19
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12.46
12:30p
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BARNES ENVIRONMENTAL WASTE AND HAULING, INC.
WQ 0018525 ALKALINE STABILIZATION OF WASTEWATER BIOSOLIDS
Facility Name: Beacons Reach P.O.#
Batch Size (gallons): 49,000
Lbs. or Gallons Used: 2,450
Material Used For Stabilization: Lime
Initial pH
>12 pH
2 Hour pH
24 Hour pH
Operator
Date
p H
TernC
p
Corr.
Factor+
Corrected
pH
Time
p H
Temp C
p
Corr.
Factor +
Corrected
pH
Time
P H
Temp C
p
Corr.
Factor+
corrected
pH
Time
pH
Temp C
Corr.
Factor+
Corrected
pH
Time
Initials
3/6/2023
6.88
23
0.06
6.82
7:00am
12.21
23
-0.06
12.15
,05an
12.22
23
0.06
12.16
9:05AM
12.2
23
0.06
12.14
7:15am
SMB
4/12/2023
7.1
26
0.03
7.13
11 : 00ary
12.1
26
0.03
12.13
1:05ar
12.08
26
0.03
12.11
1:05PM
12.16
26
0.03
12.19
11:30arr
SMB
4/24/2023
7.21
27
0.06
7.27
8:00am
12.05
27
0.06
12.11
3:05arr
12.02
27
0.06
12.08
10:05AN
12.1
27
0.06
12.16
8:30am
SMB
6/9/2023
7.42
1 31
0.18
7.6
1 1:00arr
12.11
30
0.15
12.26
1:05ar
12.1
31
0.18
12.28
1:05pm
12.2
31
0.18
12.38
11:15a
SMB
7/12/2023
7.52
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0.24
7.76
1 0:00arT
12.11
33
0.24
12.35
0:05ar
12.06
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0.24
12.3
12:05prt
12.22
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12.46
10:15arr
SMB
8/1/2023
7.61
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0.21
7.82
8:00am
12.2
31
0.18
12.38
3:05arr
12.08
32
0.21
12.2910:052
12.16
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0.21
12.37
8:05am
SMB
12/18/2023
7.51
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7.63
9:00am
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BARNES ENVIRONMENTAL WASTE AND HAULING, INC.
WQ 0018525 ALKALINE STABILIZATION OF WASTEWATER BIOSOLIDS
Facility Name: Cape Royal Dolphin P.O.#
Batch Size (gallons): 3,500
Lbs. or Gallons Used: 150
Material Used For Stabilization: Lime
maw
®=-
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BARNES ENVIRONMENTAL WASTE AND HAULING, INC.
WQ 0018525 ALKALINE STABILIZATION OF WASTEWATER BIOSOLIDS
Facility Name: CC Sass
Batch Size (gallons): 45,500
P.O.#
Lbs. or Gallons Used: 1.750
Material Used For Stabilization: Lime
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Operator
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pH
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2/8/2023
6.8
22
-0.09
6.71
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12.19
22
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12.2
22
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12.11
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12.22
22
12.13
11:30a
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3/13/2023
7.11
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7.08
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12.17
24
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12.14
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12.18
24
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12.15
9:05am
12.18
24
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12.15
7:30am
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3/22/2023
7.18
23
-0.06
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12.2
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12.17
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12.12
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12.2
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4/24/2023
7.25
28
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7.34
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12.21
28
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12.3
:35a
12.1
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12.19
9:35am
12.15
28
0.09
12.24
7:45am
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5/1/2023
7.41
31
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7.59
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12.11
30
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12.26
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12.02
30
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5/24/2023
7.35
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12.13
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6/9/2023
7.51
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12.02
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12.21
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7/20/2023
7.62
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12.22
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12/11/2023
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BARNES ENVIRONMENTAL WASTE AND HAULING, INC.
WQ 0018525 ALKALINE STABILIZATION OF WASTEWATER BIOSOLIDS
Facility Name: Cedar Point Villas
Batch Size (gallons): 7,000
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Lbs. or Gallons Used: 300
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BARNES ENVIRONMENTAL WASTE AND HAULING, INC.
WQ 0018525 ALKALINE STABILIZATION OF WASTEWATER BIOSOLIDS
Facility Name: Colony By The Sea P.O.#
Batch Size (gallons): 7,000
Lbs. or Gallons Used: 350
Material Used For Stabilization: Lime
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BARNES ENVIRONMENTAL WASTE AND HAULING, INC.
WQ 0018525 ALKALINE STABILIZATION OF WASTEWATER BIOSOLIDS
Facility Name: Dunescape villas P.O.#
Batch Size (gallons): 21,000 Lbs. or Gallons Used: 350 Material Used For Stabilization: Lime
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BARNES ENVIRONMENTAL WASTE AND HAULING, INC.
WQ 0018525 ALKALINE STABILIZATION OF WASTEWATER BIOSOLIDS
Facility Name: Island Beach & Racquet Club
Batch Size (gallons): 10,500
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200
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BARNES ENVIRONMENTAL WASTE AND HAULING, INC.
WQ 0018525 ALKALINE STABILIZATION OF WASTEWATER BIOSOL1DS
Facility Name: Mariners Pt
Batch Size (gallons): 3,500
Lbs. or Gallons Used: 150
Material Used For Stabilization: Lime
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BARNES ENVIRONMENTAL WASTE AND HAULING, INC.
WQ 0018525 ALKALINE STABILIZATION OF WASTEWATER BIOSOL1DS
Facility Name: McGinnis Pt
Batch Size (gallons): 7,000
P.O.#
!_bs. or Gallons Used: 300
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BARNES ENVIRONMENTAL WASTE AND HAULING, INC.
WQ 0018525 ALKALINE STABILIZATION OF WASTEWATER BIOSOLIDS
Facility Name: NC Aquarium
Batch Size (gallons): 17,500
Lbs. or Gallons Used:
P.O.#
Material Used For Stabilization: Lime
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BARNES ENVIRONMENTAL WASTE AND HAULING, INC.
WQ 0018525 ALKALINE STABILIZATION OF WASTEWATER BIOSOLIDS
Facility Name: Ocean Bay Villas P.O.#
Batch Size (gallons): 3,500
f_bs. or Gallons Used: 150
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BARNES ENVIRONMENTAL WASTE AND HAULING, INC.
WQ 0018525 ALKALINE STABILIZATION OF WASTEWATER BIOSOLIDS
Facility Name: Ocean Club P.O.#
Batch Size (gallons): 38,500 Lbs. or Gallons Used: 1,950 Material Used For Stabilization: Lime
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Operator
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p H
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2/20/2023
7.01
23
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6.95
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12.25
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12.19
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12.2
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0.24
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12.18
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0.21
12.12
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4/3/2023
7.11
26
0.03
7.14
9:00am
12.21
26
0.03
12.241:35an
:05a
12.2
26
0.03
12.2311:05a
12.2
26
0.03
12.23
9:05am
SMB
5/29/2023
7.22
30
0.15
7.37
9:00am
12.15
30
0.15
12.30:05a
12.1
30
0.15
12.2511:05a
12.18
29
0.12
12.30
9:05am
SMB
7/12/2023
7.56
31
0.18
7.74
8:00am
12.26
31
0.18
12.44:05a
12.1
31
0.18
12.2810:05a
12.2
31
0.18
12.38
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SMB
7/27/2023
7.61
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7.76
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12.35
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12.5012.37
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12.15
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12.33
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9/6/2023
7.33
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12.13
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12.34
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12.02
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12.23
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12.18
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11/1/2023
7.6
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12.22
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WQ 0018525 ALKALINE STABILIZATION OF WASTEWATER BIOSOLIDS
Facility Name: Ocean's Condominiums P.O.#
Batch Size (gallons): 3,500
Lbs- or Gallons Used: 150
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BARNES ENVIRONMENTAL WASTE AND HAULING, INC.
WQ 0018525 ALKALINE STABILIZATION OF WASTEWATER BIOSOLIDS
Facility Name: Pebble Beach P.O.##
Batch Size (gallons): 42,000 Lbs. or Gallons Used: 2,100 Material Used For Stabilization: Lime
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BARNES ENVIRONMENTAL WASTE AND HAULING, INC.
WQ 0018525 ALKALINE STABILIZATION OF WASTEWATER BIOSOLIDS
Facility Name: Pepper Tree P.O.#
Batch Size (gallons): 14,000 Lbs. or Gallons Used: 700
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BARNES ENVIRONMENTAL WASTE AND HAULING, INC.
WQ 0018525 ALKALINE STABILIZATION OF WASTEWATER BIOSOL1DS
Facility Name: PT Emerald Villas
Batch Size (gallons): 3,500
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BARNES ENVIRONMENTAL WASTE AND HAULING, INC.
WQ 0018525 ALKALINE STABILIZATION OF WASTEWATER BIOSOLIDS
Facility Name: Queens Court
Batch Size (gallons): 24,500
P.O.#
!_bs. or Gallons Used: 1,250
Material Used For Stabilization: Lime
Initial pH
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Operator
Date
pH
Temp C
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Time
pH
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Time
pH
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Time
pH
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2/6/2023
6.88
24
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6.85
8:30am
12.25
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-0.06
12.19
3:35an
12.2
23.0
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12.14
10:40arT
12.2
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12.17
8:45am
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3127/2023
7.41
30
0.15
7.56
9:00am
12.19
31
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12.37
):05an.
12.1
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12.28
11:05arr.
12.3
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12.48
9:30am
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4/26/2023
7.21
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7.36
8:00am
12.20
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12.35
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12.05
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12.20
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12.15
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12.30
8:15am
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5/22/2023
7.3
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12.25
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9/6/2023
7.5
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9/19/2023
7.61
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7:30am
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11/1/2023
7.48
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BARNES ENVIRONMENTAL WASTE AND HAULING, INC.
WQ 0018525 ALKALINE STABILIZATION OF WASTEWATER BIOSOLIDS
Facility Name: Sands Villa P.O.#
Batch Size (gallons): 28,000
Lbs. or Gallons Used: 1.400
Material Used For Stabilization: Lime
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BARNES ENVIRONMENTAL WASTE AND HAULING, INC.
WQ 0018525 ALKALINE STABILIZATION OF WASTEWATER BIOSOLIDS
Facility Name: Sea Isle P.O.#
Batch Size (gallons): 28,000 Lbs. or Gallons Used: 1,400 Material Used For Stabilization: Lime
Initial pH 1
12 pH
2 Hour
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Operato
Date
pH
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pH
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2/8/2023
7.1
23
-0.06
7.04
8:00am
12.20
22
-0.09
12.11
8:05arT
12.1
22.0
-0.09
12.01
10:05an
12.21
23.0
12.15
8:10am
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3/22/2023
7.05
26
0.03
7.08
8:30am
12.15
26
0.03
12.18
B:35ar
12.08
26.0
0.03
12.11
10:35art
12.1
26.0
0.03
12.13
8:40am
SMB
6/22/2023
7.68
29
0.12
7.80
7:00am
12.16
29
0.12
12.28
17.05arr
12.08
30.0
0.15
12.23
9:05am
12.2
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0.12
12.32
7:30am
SMB
6/7/2023
7.5
31
0.18
7.68
7:30am
12.19
31
0.18
12.37
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12.18
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6/26/2023
7.52
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12.20
30
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12.18
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8/3/2023
7.45
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12.10
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12.01
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12.15
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8/15/2023
7.5
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10/17/2023
7.61
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BARNES ENVIRONMENTAL WASTE AND HAULING, INC.
WQ 0018525 ALKALINE STABILIZATION OF WASTEWATER BIOSOLIDS
Facility Name: Sea Spray P.O.#
Batch Size (gallons): 17,500 Lbs. or Gallons Used: 1,400 Material Used For Stabilization: Lime
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BARNES ENVIRONMENTAL WASTE AND HAULING, INC.
WQ 0018525 ALKALINE STABILIZATION OF WASTEWATER BIOSOLIDS
Facility Name: Sound of the Sea P.O.*
Batch Size (gallons): 3,500
Lbs. or Gallons Used: 150
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BARNES ENVIRONMENTAL WASTE AND HAULING, INC.
WQ 0018525 ALKALINE STABILIZATION OF WASTEWATER BIOSOLIDS
Facility Name: Southwinds
Batch Size (gallons): 14,000
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BARNES ENVIRONMENTAL WASTE AND HAULING, INC.
WQ 0018525 ALKALINE STABILIZATION OF WASTEWATER BIOSOLIDS
Facility Name: Summerwinds P.O.#
Batch Size (gallons): 73,500 Lbs, or Gallons Used: 3,500 Material Used For Stabilization: Lime
Initial pH
>12 pH
2 Hour pH
24 Hour pH
Operator
Date
pH
Temp C
Corr.
Factor +
Corrected
pH
Time
pH
Temp C
Corr.
Factor +
Corrected
pH
Time
pH
Temp C
Corr.
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corrected
pH
Time
pH
Tempt;
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Time
Initials
4/5/2023
6.78
25
0
6.78
7:30am
12.25
27
0.06
12.31
7:35an
12.25
27.0
-0.06
12.31
9:35am
12.39
27.0
-0.06
12.45
8:30am
SMB
4/17/2023
7.09
24
-0.03
7.06
9:30am
12.20
25
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12.20
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12.20
11:35ary.
12.25
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0.00
12.25
10:00a
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5/11/2023
7.16
28
0.09
7.25
8:00am
12.26
29
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12.38
.05arT
12.26
29.0
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12.38
10: 1 5arr
12.18
28.0
0.09
12.27
8:05am
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6/5/2023
7.17
31
0.18
7.35
7:00am
12.30
33
0.24
12.54
:05arr
12.31
31.0
0.18
12.49
9:35am
12.2
31.0
0.18
12.38
7:30am
SMB
6/29/2023
7.31
33
0.24
7.55
9:00am
12.29
33
0.24
12.53
:05aiT
12.34
33.0
0.24
12.58
11:15ary
12.2
33.0
0.24
12.44
9:30am
SMB
7/17/2023
7.02
34
0.27
7.29
8:00am
12.15
35
0.3
12.45
:05ary.
12.1
35.0
0.3
12.40
10:35ary
12.25
34.0
0.27
12.52
8:30am
SMB
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BARNES ENVIRONMENTAL WASTE AND HAULING, INC.
WQ 0018525 ALKALINE STABILIZATION OF WASTEWATER BIOSOLIDS
Facility Name: The Grove P.O.#
Batch Size (gallons): 24,500 Lbs. or Gallons Used: 1,250
Material Used For Stabilization: Lime
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BARNES ENVIRONMENTAL WASTE AND HAULING, INC.
WQ 0018525 ALKALINE STABILIZATION OF WASTEWATER BIOSOLIDS
Facility Name: Whaler Inn
Batch Size (gallons): 3,500
Lbs. or Gallons Used:
P.O.#
150
Material Used For Stabilization. Lime
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2023 APPLICATION SUMMARY

BARNES ENVIRONMENTAL WASTE
Permit # WQ 0018525
RESIDUALS APPLICATION
2023 APPLICATION
SUMMARY
ii!*!P4 -'A
Will Turner
Site WT
2023
1
6.20
63,000
2.69
8.31
5.66
2023
2
5.00
140,000
6.42
24.45
16.00
2023
3
8.00
150,500
5.24
27.71
0.81
2023
5
2.60
108,500
4.53
.59.01
14.72
2023
6
2.90
98,000
1 3.73
126.47
3.09
Totals
Total Gallons 560,000
WWTP - Metric Tons 20.51

FIELD APPLICATION SUMMARIES

JAN
FEB
MAR
APR
MAY
JUN
JUL
AUG
SEP
OCT
NOV
DEC
TOTALS
Corn
Rye
JAN
FEB
MAR
APR
MAY
JUN
JUL
AUG
SEP
OCT
NOV
DEC
TOTALS
Corn
Rye
BARNES ENVIRONMENTAL WASTE
2023 FIELD APPLICATION SUMMARY FORM
Permit WQ0018525
FIELD WT-01 6.2 ACRES TOTAL GALLONS 63,000
NMI
--
---------------
--
--------------
-
----------------
-
---
--------------
---
--------------
----
-------------
----
-------------
-----
------------
-----
------------
------
--
--
-
-
-----
��
IF
0
11
II
�
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0000�00�©
00
1 1
0
1 1
00
1 1
0000000
00
---------------
--
0 0000
1 1
0
I I I
000
00000
0
--
----
-------------
-----------
------
------
--
------
---
-------
----------
---------------
--
----------------
-
--------
-
----------------
0
0
00
00
®®®®00®0
0
0
0 3,560
0 0
10,500
0
0
3,500
3,500
3,500
3,500
0
0
7,000
0
0
0
0 0
0 0
0
0
0
0
0
3,500
0
0
0
0
0
1 0

JAN
FEB
MAR
APR
MAY
JUN
JUL
AUG
SEP
OCT
NOV
DEC
TOTALS
Coastal
Rye
JAN
FEB
MAR
APR
MAY
JUN
JUL
AUG
SEP
OCT
NOV
DEC
TOTALS
Coastal
Rye
BARNES ENVIRONMENTAL WASTE
2023 FIELD APPLICATION SUMMARY FORM
Permit W00018525
FIELD WT-02 5.0 ACRES TOTAL GALLONS 140,000
Alantic
Station
Beacons
Reach
CC Sass
Cape Royal
Dolphin n
Cedar
Point
Colon B
The Seat
Hampton
Suites
Dunesca a
Eight 112
Marina
Emerald
Planlalion
Genesis
Condos
Harkcrs
Point
Island
Beach
Kingsbn a
1[ 6
Mariner's
Paint
McGinnis
Point
NC
A unrium
3,500
7,000
10,500
7,000
7,000
3,500
3,500
3,500
3,500
7,000
7,000
3,500
3,500
7,000
7,000
7,000
1
21,000
21,000
21,000
3,500
0
0
3,500
7,000
0
0
D 1---O--T
0
0
3,500
7,000
3,500
------------
----
-----------------
-----------------
-----------------
0
0
3,500
14.000
0
0
10,500
3,500
0
0
3,500
0
0
0
0
0
3,500
3,500
0
0
0
0
0
0
0
0
0
0
0
0
7,000
0
0
0
0

JAN
FEB
MAR
APR
MAY
JUN
JUL
AUG
SEP
OCT
NOV
DEC
TOTALS
Coastal
Ryc
JAN
FEB
APR
MAY
JUN
JUL
AUG
SEP
OCT
NOV
DEC
TOTALS
Coastal
Rye
BARNES ENVIRONMENTAL WASTE
2023 FIELD APPLICATION SUMMARY FORM
Permit WQ0018525
FIELD WT-03 8.0 ACRES TOTAL GALLONS 154,000
P..
W�
Eight1/2jFF.;,,,1dj
Marina
Ptantation
E-cte c
FHakm,
P.,nl
-----------------
-----------------
-----------------
-----------------
11----------
-----------------
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!1
111
I!1
000
M1
00�©000000
111
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111
000 11 0000000000
-----------------
000000000000©00©©
The
Grave
Ocean Bay
Villas
an
Club
Ocean
Condos
Ocean
Terrace
Pebble
Beach
Peppertree
Resort
Pine
Knoll
Point
Emerald
Queens
Court
Sands I
Villa
Sea Island
Plantation
Sea
S ra
SOURd OF
The Sea
Sauthtvinds
Condos
Summer
Winds
ff�!j
3,500
7,000
7,000
I o,500
10,500
7,000
10,500
7,000
10,500
24,500
10,500
3,500
3,500
3,500
24,500
0
10,500
0
0
10,500
0
0
0
7,000
21,000
3,500
0
0
7,000
35,000
0
24,500 0
7,000
0
0
10,500
0
D
0
3,500 1 21,000 3,500
0
0
1 7,000
1 35,000
0
0 0
3,500
0
0
0
1 0
L 0
0
3,500 0 0
0
0
0
0
0

JAN
FEB
MAR
APR
MAY
JUN
JUL
AUG
S EP
OCT
NOV
DEC
TOTALS
Coastal
Rye
JAN
FEB
MAR
APR
MAY
JUN
JUL
AUG
SEP
OCT
NOV
DEC
TOTALS
Coastal
Rye
BARNES ENVIRONMENTAL WASTE
2023 FIELD APPLICATION SUMMARY FORM
Permit WQ0018525
FIELD NVT-05 2.6 ACRES TOTAL GALLONS I08,500
Alanfic
Station
-----------------
-----------------
-----------------
-----------------
-----------------
-----------------
-----------------
-----------------
-----------------
111
11 !
1 1!
00�000000
1 1 1
0000
0
111
1 ! 1
000©000000000�
-----------------
-----------------
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-------------
-----------------
-----------------
00
11
1!
00
II!
0©00
1 11
1 11
11
�
!11
0

JAN
FEB
MAR
APR
MAY
JUN
JUL
AUG
SEP
OCT
NOV
DEC
TOTALS
Coastal
Rye
JAN
FEB
MAR
APR
MAY
JUN
JUL
AUG
SEP
OCT
NOV
DEC
TOTALS
Coastal
Rye
BARNES ENVIRONMENTAL WASTE
2023 FIELD APPLICATION SUMMARY FORM
Permit WQ0018525
FIELD WT-06 2.9 ACRES TOTAL GALLONS 98,000
-------------
--
--
-
----------------
----
-
--
----------
-----------------
-----------------
-----------------
II
1!!
111
�
II
00000000�00
111
21,000
7,000
7,000
0
3,500
0
0
0
0 0
0 0 0
0
0
0
14,000
3,500
0
0
0
0
0
0
0
0 0
0 0 0
0
0
0
0
'��IM-Et:]L_Condos
JI
T�,w�_Jmlw.
-----------------
-----------------
-------------
-
---
-
--------
--------
-
----------------
00
11 1
00
1 1 1
F I
00
1 1!
0
! 11
00000
0
0
7,000
0
0 10,500 0
0
0
7,000
0
7,000
0
0
0
0
0
0
0
0
0
0 0 3,500
0
0
3,500
0
3,500
0
0
0
0
0

FIELD LOADING RATE REPORTS

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
Facility Name: narnas Environmental Wasta & Hauling Permit #: W00018525 Annual Dry Tons Applied: 2.69
Owner: Will Turner Operator: Steve Barnes Cation Exchange Capacity( non 503): 2.2
Site #: WT Field #: 1 Acres Utilized: 6.20 Acres Permitted: 6.20
Application Method*- S Vollitilizntion Rntc**: 0.5 Mineralization Rate: 30 % Predominant Snil Seriec: r.nA
.....
....
. 0 ili§:i
E:Fi+14
. s�:..
Ni: ....€.L�'s€
'•a:7 'i:::
�... ..:::�1'a€€:�€�iXl
;_��:::2gn;#NI_I'Pc�i�k�€'i�•x�'-.1�
2023
3,500
565
2.46
0.06
CC Sus
G/D
0.002
0.002
0.062
0,002
0.000
0.002
0.002
0.002
0.090
2.24
2.27
Com
6.95
0.15
0.13
2023
3,500
565
0.61
0.01
Cedar Point
G/1)
0.001
0.001
0.009
0.001
0.000
0,001
0.001
0.001
0.025
0.48
0.56
Corn
1.40
0.13
0.03
2023
3,500
565
1.92
0.05
Colony By The
qya
GID
0.000
0.000
0.017
0,001
0.000
0.000
0.001
0.000
0.211
2.30
1.58
Rye
7.62
0.05
0.00
2023
14,000
2,258
1.06
O.IO
Dunescapc
GID
O.ODq
1 0,000
10.1231
0.003
0.000
0-001
1 0.005
0.001
0.299
0.93
2.79
3.90
Corn
Rye
1233
0.08
0.00
2023
3,500
565
0.43
0.01
OccanClub
GID
0.000
0.000
0.007
0.000
0.000
0.000
0.000
0.000
0.052
0.32
0.31
Com
1.08
0.00
0,00
2023
10,500
1,694
0.96
0.07
Pehble Beach
G/D
0.000
0.000
0.035
0.002
0.000
0.001
0,002
0.001
0.365
0.33
1.99
Corn
9.44
0.11
0.00
2023
2023
2023
2023
2023
3,500
3,500
7.000
3,500
7,000
565
565
1,129
565
1,129
0.66
1.09
0.61
0.97
0.99
0.02
0.03
0.03
0.02
0,05
Point Emerald
c
Qucens Coun
Sands Villas
Sca lslc Plaata"on
Soulhwinds
a
GID
GID
GID
GID
G/D
0,000
0.001
0.000
0.0001
0.000
0.000
0.001
1 0.000
0.000
0.000
0.012
0.009
0.0091
0-017
0.062
0.001
0.001
0.000
0.001
0.001
0.000
0.000
0.000
0.000
0,000
0.000
O.001
0.000
0.000
0.000
0.000
0.001
10.000
0.001
0.001
0.000
0.001
0.0001
0,000
0.000
0.074
0.067
0.056
0,039
0,146
0.49
0.72
0.58
0.26
1.95
0.58
0.26
0.89
0.86
0.45
1.58
Com
Cam
1 Cam
Co.
Com
Rye
1.20
226
3.83
3.15
6.49
0.01
0.21
0.01
0.08
0.02
0.00
0.00
0.00
0.00
0.00
Total 63,000
Annual lbs/acre 0.006 0.005 0.361 0.014 0.000 0.008 0.015 0.008 1 1,421 9.31 5.66 14,66
Current Cumulative Ibs/acre 0.10 0.07 23.35 0.42 0.01 0116 1 0.26 0.15 33.82 147 50 Permit PAN Unit lstl2nd Crop
Prior Years Cumulative lbs/acre 0.10 0.06 22.98 0.41 0.01 0.15 0.25 O.14 32.40
Perm ittC.P.L.R.*** 36 34 1338 267 15 NIA 374 89 2498
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance wilh a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
Lime A
Date
Lbs/A
_Steve games
x Steve Barnes Feb 23 2024 1.4:10 EST) *Application Method: S - Surface, IN - Injection, INC - Incorporation
(Signature of Land AppIicr) Date **Volalilization Rate: Surface -0.5, InjeetionAneorporation - LO
***C.P.L.R-: Cumulative Pollutant Loading Rate
WMSS, PLLC DENR FORM FSF (7/2002) Mod.

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
Facility Name: Barnes enviroamentat wss,e &, nataittr Permit to: W00018525 Annual Dry Tans Applied: 6.42
Owner: Will Turner Operator: Steve Barnes Cation Exchange Capacity ( non 503): 6.8
Site 8: 3VT Field #: 2 Acres Utilized: 5.00 Acres Permitted: 5.00
Application i4lethod": S Volatilization Rate": 0.5 Mineralization Role: 30 % Predom inant Sail Series: t:nA
-.-R:►K�::-:-G�1s:=:.:��alr:::::7�:::k�ra
::::::cult .
rc+;:::::Gottt4
iWl­
- ..
::::11s:::.:::t41::::::�tz:::::::pp�::::::�f
':::.:��ru::::=:iVir�i
€S�€€
€€�4��:P>��'.=E:
=1'��2s
►:>:-�€!�rb�ik'.:4'��
€�i�Is
4NFI3
.
fy'2�•I�13
2023
21,000
4,200
4.44
0.08
Atlamicstation
GID
0,000
0.000
0.072
0.002
0,000
0.001
0.002
0.001
0.191
0.29
0.06
1,43
Coastal
Rye
9.61
0.01
0.00
2023
21,000
4,200
0.99
0.17
BeaeonsReach
GID
0,001
0.000
0A49
0.005
0.000
0.002
0.008
0.002
0,490
4.19
2.10
4.38
Coastal
Rye
20.93
0,04
0.00
2023
21,000
4,200
2.46
0.43
CC sass
GID
0.017
0.017
0.459
0.017
0.001
0,017
0,017
0.017
0.669
8.34
8.34
16.89
Coastal
Rye
51.70
1.13
0,94
2023
3,500
1 700
0.43
0.01
Canc Royal
1 nol.hi,
GID
0.001
0.001
0,006
0.001
0.000
0.001
1 0,001
0.001
0.069
0.74
0.39
Cwstal
1.35
0.12
0.31
2023
3,500
700
0.77
0.02
tl"P"Suttes
GID
0.W0
1 0.000
0.052
0,000
0.00p
0.00D
0.001
0,000
0.025
0,81
0.70
Coastal
2.68
0.01
0.00
2023
7,000
1,400
1,06
0,06
D,s 1-Pe
GID
0.000
0.000
0.076
0.002
0.000
0.001
0,DO3
0,001
0.185
2.30
2.42
Cuasta[
7.64
10.05
0.00
2023
3,500
700
0.58
0.02
Mariners Point
GID
0.000
0.000
0.022
0.000
0.000
0.000
0.000
0.000
0,040
0.63
0.80
Coastal
2.09
0.00
0,00
2023
1 7,000
1,400
1 2.14
0.12
McGinnis Point
GID
0,001
0,000
0.432
0.005
0,000
0.001
0,004
0.001
0.333
4,51
2.56
R e
14.98
0.09
0.00
2023
3,500
700
1.09
0.03
NC Aquarium at
plot ynQllghnmg
GID
0.000
0.000
0.015
0,00)
0.000
0.000
0.001
0,000
0.048
0.77
1.37
Coastal
1
2.57
0.01
0.00
2023
2023
2023
2023
3,500
14,000
10,500
3,500
700
200
2.100
700
0.74
0.43
0.96
0.68
0,o2
0.05
0.08 1
0.02
Ocwn Bay Villas
Ocean Club
Pebble Beach
PePPenxe
GID
G/D
G/D
GID
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.013
0.036
0.044
0.016
0 001
0.001
0.003
0.000
0.000
0.000
0.000
0.000
0,000
0.001
0.001
0.000
0.000
0.001
0.002
0.001
0.000
0,001
0.001
0,000
0.063
0.259
0A53
0.087
0,66
1.61
0.41
0.52
1
0.48
1.55
2.47
1 0,64
Coasml
Coastal
Coastal
Coasts[
2.20
5.35
11.70
1.73
0,00
0.01
0.14
1 0.00
13.00
0.00
0.00
0,00
2023
2023
3,500
7,000
700
1.400
1.09
0,97
0.03
0.06
Quecm Court
sea spray
G/D
GID
0.001
0.000
0,001
0.000
0,011
0.080
0.001
0.001
0.000
0.000
0.001
0.001
0.001
0.001
0.001
0.001
0,093
0,140
0.90
0.99
].II
1.65
coastal
R
2,80
7.11
0.26
0.06
0,00
0.00
2023
3.500
700
0.76
0.02
Sum,ne""Ml
GID
0.000
0.000
0,019
0.000
0.000
0,000
0.000
0.000
0.062
1.85
1.05
Coastal
0.95
0.04
1.56
2023
3,500
700
1.58
0.051
Whaler Inn
G/D
0.000
0.000
0.064 1
0,001
0.000
0.000
0A01
0.000
0,117
0.45
1
2,12
Coastal 1
5.97
0.18
0.00
Total
140,000
Annual lbslacre 0.024 0.021 1.867 0.042 0.001 0.028 0.046 0.028 3,362 24.45 16.00 42.00
Current Cumulative Ibslacre 1.91 0.13 83.13 25.20 0.46 0.37 1,11 0.70 1 102-80 299 50 1 Permit PAN Limt lst/2nd Crop
Prior Venn Cumulative Ibslncro 1.89 0.1I 1 81.26 1 2.5.16 0.46 0.34 1 1.07 0.68 99.44
Permilt C.P.1-R.-"" 3G 1 34 1 1336 1 267 15 NIA 1 374 89 1 2499
"I certify, under penalty of lacy, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, Including the possibility of fines and imprisonment for knowing violations."
Lime A
Date
LbslAc
_Steve Rmet
X _ eta,,,. na., opal,1a_znza ta-m FsTi _ 'Application Melhod: S - Surface, IN - Injection, MC - incorporation
(Signature of Land Applier) Date "Volatilization Rate: Surface - 0.5, injection/Incorporation - 1,0
***C.P.L.R,: Cumulative Pollutant Loading Rate
WMSS, PLLC DENR FORM FSF (7/2002) Mod.

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
Facility Name: Domes Environmental Waste & Mauling Permit 8: W00418525 Annual Dry Tons Applied: 5.24
Owner: Will Turner Operator: Steve Barnes Cation Exchange Capacity ( non 503): 8.2
Site #: WT Field if: 3 Acres Utilized: 8.00 Acres Permitted: 8.00
Application Method": S Valatiliztition Rate**: 0.5_ Mineralization Raw 30 % Predominant Soil Series: GoA
8?i
_
:' ••'1•S:ifi
:r..
Eii.''8�.7..
i° ''•tit4iiE
.:.f .:.:
'`t •i
•.13.'fi
'k•'i
: r•:.:...
E 1. 1. tlal`•fli•'
` iiS • 1 .
.y 4111 �FEii
1:.
�Da(u=
:;0'
..>_ let s::'.tti•'j;i':•:
•i
j
li�..
'.�.� .
'i:ii
....:�:
a .
...EEI`I
� i'c=�
............,4
iii�Fii:i:•:i:%•i:i:
....�
iF. k�.ls
...
: il'ff2
��....
.�iEc�iESiiE
G"-T'.� •E3E
E�r4 •��
i�;�fiK0l�€
2023
7,000
875
0.44
0.02
Atlantic Station
G/D
0.000
0.000
0.015
0,000
0,000
0.000
0.000
0.000
0.040
0,07
0.30
Coastal
2.00
0.00
0.00
2023
14,000
1,750
0.99
0.07
Beacons Rcacls
G/D
0.000
0.000
0.187
0.002
0.000
0.001
0.003
0.001
0.204
2.62
1.83
Coastal
3.72
0.02
0.00
2023
7,000
875
2.46
0.09
CC Sass
GAD
0,004
0.004
0_096
0.004
0.000
0.004
0,004
0.004
0.139
3.47
3.52
Coastal
10.77
0.24
0.20
2023
3,500
438
0.77
0.01
1lamPlon Suites
G/D
0.000
0.000
0,033
0,000
0.000
0.000
0.000
0.0001.
0,016
0,50
0.44
Coastal
L67
0.00
0.00
2023
24,500
3,063
0.64
0.09
ThM=Pe Grove
GID
4.004
0.000
0.019
0.001
0.0001
0.001
0.002
0,001
1 0.157
3.77
4.56
Coastal
12.29
0.40
0,00
2023
10,500
1,313
0.43
0.02
Ocenn Club
G/D
0-000
1 0.000
0.017
4.000
0.0001
0.000
0.001
0.0001
0.121
0.50
0.25
0.73
Coastal
Rye
2.51
0.00
0.00
2023
10,500
1,313 1
0.96
0.05
Pebble Beach
G/D
().0001
0.000
0.027
0.002
0-0001
0.001
0.001
0.001
0.293
0.26
1.55
Caattai
7.31
0.09
0.00
2023
7,000
875
1.09
0.04
1 QuecnsCoure
G/D
0.001
0.001
0.014
0,001
0.000
0.001
0.001
0-001
0.103
0.56
0.56
1.38
Coastal
Rye
3.50
0.32
0.01
2023
21,000
2,625
0.61
0.07
Sands Villas
G/D
0.000
0.000
0.022
0.001
0.000
0.001
0.001
0.001
0.129
2.68
1.99
Coastal
8.91
0.02
0.00
2023
3,500
438
0.97
0.02
Sea isle pinntsuon
G/D
0.000
0.000
0.013
0.001
0.000
0.000
0.000
0,000
0.029
0.20
0.35
Coastal
2.44
0.06
0,00
2023
7,000
875
0,99
0.04
Soul win s
GID
0.000
0,000
0-M
0.001
0.000
0.000
0.001
0.000
0.113
1.51
1.22
Coastal
5.03
0.01
0.00
2023
35,000
4.375
..76
0.14
SummcrWinds
GID
0.001
0-000
0,117
0,0021
0.000
0.001
0.003
0.001
0.386
11.56
6.56
Coastal
5-91
0.23
9.74
LT,tal
150,500
Annual lb-dwe 0.009 0,00E 1 0.607 0.015 0.000 0.010 0.018 0.010 1 1.721 27.71 1 0.81 24.43 1
Current Cumulative tbsfacre 0.22 0.42 65.32 1.04 0.01 0.28 0.71 0.75 73.01 299 50 Permit PAN Unit lstl2nd Crop
Prior Yenrs Cumulative Ibslacre 0.22 0.41 64.71 1.03 0.01 1 0.27 1 0.69 0.24 71.29
Permilt C.P.L.1L*''* 36 34 1338 267 15 1 NIA 1 374 89 2498
"1 certify, under penaltyof law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submilted. I am aevarc that there are
significant penalties for submitting Use information, Including the possibility of fines and imprisonment for knowing violations."
Li mc A
Date
Lbs/A
a s SteyeFen Vries a esn *Application Melliod: S - Surface, IN - Injection, INC - Incorporation
(Signature of Land Applier) Date **Volatilization Rate: Surface - 0.5. Injection/Incorporation - 1.0
***C.P.L.R.: Cumulative Pollutant Loading Rate
WMSS, PLI.G DENR FORM FSF (7/2002) Mod.

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
Facility Name: Barnes Envirenmenlal Wave & llnuline Permit it• W00018525
Owner: Will Turner
Site H: WT
Operator: Steve Barnes
Field M 5 Acres Utilized: 2.60
Application Method*: S Volatilization Rate**: 0.5
Annual Dry Tons Applied: 4.53
Cnlion Exchange Capacity ( non 503): 5.9
Acres Permitted: 2.60
Mineralization Rate: 30 % Predominant Soil Series: GoA
...�S.i? ......:.:..�....t
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ul�c+`:::::::�uh�,
..
...............•.•.•.......-......�4i'et1qlk-.
lls�!>rG
:.:-:.:-:.:...........:.....:.:.::.:.:.:.:.:.:.-.::...:.:-•-:...-.-...-.-.•.-..............i'�
t .
.: r�s=:::.:�t1:::::,.�st:::::::1'I7.:::.::ill
:=:::-hlv::::::�f:•:.:.:$>a:::::::�u::::�r1il[I::J'-iktsl:�:::::::-1r:::::C1�p
.�#�
c�r� :;:
?::`�::::t�.l���:
:1`i3
2023
7,000
2,692
0,44
0.05
Atlantic Station
GID
0.000
0.000
0.046
0.001
0.000
0.000
0.001
0.000
0.123
0.23
0.92
Consml
6.16
0,00
0,00
2023
7,000
2,692
0.99
0.11
Beacons Reach
GID
0.001
0.000
0.288
0.003
0.000
0.001
0.005
0.001
0.314
4.03
2.81
Rye
13.42
0,02
0.00
2023
7,000
2,692
2.46
0.28
CC Sass
G/D
0.011
0.011
0.294
0.011
0.000
0.011
0.011
0.011
0.429
10.69
10,83
Rye
33.14
0.72
0.60
2023
3,500
1,346
1.92
0.11
Cotony By The
Sen
GID
0.001
1 0.000
0.039
0.001
0.000
0,001
0.002
0.001
0,504
5.47
3.77
Coastal
18.17 ,
0.11
0.00
2023
10,500
4,038
1.37
0.23
island Beach
GID
0A01
0.000
0.310
0.004
0,000
0.003
0.004
0.002
0.567
9.45
14.12
Coastal
31.36
0.19
0.00
2023
3,500
1,346
0.43
0.02
Ocean Club
GID
0.000
0.000
0.017
0.000
0.000
0.000
0.001
0.000
0.124
0.77
0.74
Coastal
2.57
0.00
0.00
2023
2023
3.500
7,000
1.346
2,692
1.41
0.68
0,08
0.08
Oceans
Condominiums
Peppearee
GID
GID
0,002
0.000
0.000
0-000
0.080
0.062
0.002
0.002
0.000
0.000
0.001
0.001
0.002
0.002
0.001
0.001
0-175
1 0.333
0.17
1.99
2.18
2.47
Coastal
Coastal
14.86
6,64
0.48
0.00
0.00
0.00
2023
10,500
4.038
0.97
0.16
Sen isle plantation
GID
0,001
0.000
0.119
0.010
0.000
0.002
0.004
0.002
0.269
1.89
3.23
Coastal
22.55
0.60
0,00
2023
2023
2023 1
10.500
3,500
35,000
4.038
1,346
13,462
0.97
0.64
0.76
0.16
0.04
0.43
sea Sp-y
Sound OfThe Sea
Summer winds
GID
GID
GID 1
0.001
0.000
0.002
0.000
0.000
0-001
0.232
0.097
0,3591
0.003
1 0.002
0,006
0.000
0.000
0.000
0,002
0.000
0.004
0.004
0.001
0.009
0.002
0.000
0,004
0.402
0.190
1.189
2.85
0,63
35.57
4.75
0A3
20.20
Coastal
Coastal
Coastal
20.50
1.77
18.20
0.17
0.05
0.71
0.00
0.00
29.97
Total 108,500
Annual Ibslacre 0.020 0.013 1.949 10.046 0.001 0.026 0.045 0.026 4.619
Current Cumulative Ibslacre 0.149 0.102 24.528 0.614 0.012 0.231 0.416 0.210 41.111
Prior Years Cumulative Ibslacre 0.129 1 0.088 22.583 0.568 0.011 0.205 0.371 0,184 36A92
Permitt C.P.L,R,*** 36 1 34 1338 267 15 NIA 374 $9 2498
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated (lie information submitted. I am aivare that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
59.01
299
14.72 66.44
50 Permit PAN Unit lst/2nd Crop
Lim c App,
Date
LbslAc
Steve &&-iler
%t '1ZR= 'rc �a �n� t snFsn �i *Application Method: 5 -Surface IN Injection, INC - Enwrporation
(Signature of Land Applier) Date **Volatilization Rate: Surface - 0.5, Injectionlincorporation - 1.0
***C.P.L.R.: Cumulative Pollutant Loading Rate
WMSS, PLLC DENR FORM FSF (712002) Mad.

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
Facility Name: Barnes F.nviranmrnral Wasic & llauline permit d: W00018525 Annual Dry Tans Applied: 3.73
Owner: Will Turner Operator: Steve Barnes Cation Cscltange Capacity ( non 503): 6.7
Site #: WT field 4: 6 Acres Utilized: 2.90 Acres Permitted: 2.90
Application Melhad*: S - VoNtiliza lion Rnte k; 0.5 Min ern lizalion Rate: 30 %
Prednminanf Rnil Rrriwc• (:nd
�.
s . [: tg . ilu li•'
...ii�{js'i
ii:rtl::::..
:jj'E ...
2023
24,500
8,448
0.44
0.16
AdaraieStation
G/D
0,001
0.000
0.146
0.004
0,000
0,002
0.004
0.002
0.385
0.61
0.10
2.89
Coastal
Rye
19,34
0.01
0.00
2023
7,000
2,414
0,99
0.10
beacons Reach
G/D
0.000
0.000
0.258
0.003
0.000
0.001
0,005
0.001
0.282
3.61
2.52
Coastal
12,03
0.02
0.00
2023
2023
7.000
3,500
2,414
1207
2.46
0.61
0.25
0.03
CcSm
CedarPoim
-RUTquanum
GID
G/D
0.010
0.0021
0.010
0.002
0.264
1 0,019
0.0I0
1 0.002
0.000
0.000
0.010
0.002
0.010
0,002
0.010
0,002
0.384
0.054
9.58
1.02
9.71
1.19
Coastal
Coastal
29.71
3.00
0.65
0.28
0,54
0.07
2023
2023
2023
14,000
7,000
10,500
4,828
2,414
3,621
1.09
0.43
0.96
0.22
0.04
0.14
at
Pin. Knoll Shores
CcemClub
Pebble Beach
G/D
G/D
GID
0.001
0.000
0.001
1 0.003
0.000
0.000
0,103
0.031
0.075
0.010
0.00i
0.004
0.000
0,000
0,000
0.002
0,000
0,001
0,009
0.001
0.003
0-002
0.000
0.001
0.329
0.223
0.780
5.33
1.38
0.71
9.45
1.33
4.26
Coastal
Coastal
Coastal
1
17.72
4.61
20-18
0.05
HO
0.24
0.00
0.00
0,01
2023
3,500
1,207
0.68
0.03
Peppertrce
GID
0,000
0,000
0.029
0,001
0,000
0.000
0.001
0.000
0.149
0.89
I,I ]
R e
2.98
0.00
0.00
2023 10,500 3,621 1,09 0.16 Queens Conn G/D 0,006 0.006 0.057 0.006 0.001 0.006 0.006 0.006 0.429
2023 10,500 3,621 0.97 0.15 Sn We Plaotmim G/D 0.001 0.000 0.107 0.009 0,000 0.001 0.004 0,001 0,241
Total 98,00o
Annual lbs/acre 0.022 0.022 1.087 0,049 0.001 0.027 10.044 0.026 3.256
Current Cumulative Ibs/acre 0.131 0.082 28.234 O.G70 0.012 0.210 0.453 0.219 47.134
Prior Years Cumulnlivc Ibs/acre 0.109 0.060 27.14G 0.G24 0.011 0.183 0.409 0.193 143.878
Permits C.P.L.R *** 36 34 ]338 2G7 15 NIA 374 89 1 2498
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false inrormation, including the possibility of fines and imprisonment for knowing violations."
3.09
1.13
26,47
299
1.54
0.56
3.09
50
5.73 Coastal Ryc 14.48
2.90 Coastal Rye 20.21
41.09
Permit PAN Lim( Ist/2nd Crop
1.33
0.53
Lime
0.02
0,00
A .
Date JLWA,
Steve E-am
x *Application Method: S - Surface, IN - Injection, INC - Incorporation
(Signature of Land Applier) slate "Volatilization Rate: Surface - 0.5, Injection/Incorporation- 1.0
***C.P.L.R.: Cumulative Pollutant Loading Rate
WMSS, PLLC DENR FORM FSF (7/2002) Mod.

Barnes - 2023 Ann Rpt Signature Pages
Final Audit Report 2024-02-23
Created: 2024-02-23
By: Martin Mabe ([e-mail])
Status: Signed
Transaction ID: CBJCHBCAABAAe911xtE9yKBiF1P97erV4DktlgW0ex02
"Barnes - 2023 Ann Rpt Signature Pages" History
5 Document created by Martin Mabe ([e-mail])
2024-02-23 - 7:04:49 PM GMT- IP address: 173.94.169.164
c'- Document emailed to Steve Barnes ([e-mail]) for signature
2024-02-23 - 7:04:54 PM GMT
m5 Email viewed by Steve Barnes ([e-mail])
2024-02-23 - 7:08:13 PM GMT- IP address: 69.147.95.10
�Q Document e-signed by Steve Barnes ([e-mail])
Signature Date: 2024-02-23 - 7:10:41 PM GMT - Time Source: server- IP address: 174.106.211.237
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SOIL ANALYSIS REPORTS

Page 1 of 1
Report No: 23-340-0593
Account No: 07837
Advisor: Willcox & Mabe Soil Solutions, PLLC
7231 B. Summerfield Rd
Summerfield NC 27358
Waypoint
ANALYTICAL
Client: BARNES ENVIR.WMSS JOB NO. 15-02
2850 Daisy Lane, Wilson, NC 27896
Main 252-206-1721 ° Fax [phone]
www.waypointanalytical.com
Farm:
Date Received: 12/06/2023
Date of Report: 12/07/2023
Lab No Field 1D
Sample 1D
Soil Class HM% W/V pH
Ac
P-1
K-1
S-1
Mn-1
Mn-All Mn-Al2 Zn-1
Zn-Al
Cu-1
CEC BS%
Ca%
Mg%
ESP
Na
00761
WT-01
MIN
0.8
1.2 6.3
1.0
89
37
19
88
65
65
88
88
75
4.0
76
54
17
1.0
0
Crop Recommendations:
Rec Uom
Lime (t/acre)
N
P2 05
K2
5
Mn
Zn
Cu
8
Mg
Last Crop
i- Corn
lb/acre
0.0
160
0
64
20
0
0
0
0
0
2- Rye
lb/acre
0.0
62
0
50
20
4
0
0
1.5
0
00762
WT-02
MIN
1.0
1.1 6.4
0.8
137
18
23
56
44
44
210
210
380
5.0
83
69
11
1.0
0.1
Crop Recommendations:
Rec Uom
Lime (t/acre)
N
P205
Kz0
S
Mn
Zn
Cu
8
Mg
Last Crop
1- Coastal Bermuda
lb/acre
0.0
220
0
195
20
0
0
0
0
0
2- Rye
lb/acre
0.0
62
0
85
20
4
0
0
1.4
0
00764
WT-03
MIN
1.2
1.1 6-6
0.6
154
12
23
38
31
31
235
235
625
5.9
89
79
8
1.0
0.1
Crop Recommendations:
Rec Uom
Lime (flacre)
N
P205
K20
S
Mn
Zn
Cu
B
Mg
Last Crop
1- Coastal Bermuda
lb/acre
0.0
220
0
212
20
0
0
0
0
0
2- Rye
lb/acre
0.0
62
0
93
20
4
0
0
1.2
0
00765
WT-05
MIN
0.9
1.1 6.8
0.8
382
9
42
31
23
23
1203
1203
1165
9.8
91
84
6
0.8
0.1
Crop Recommendations:
Rec Uom
Lime (t/acre)
N
PZ 05
K20
S
Mn
Zn
Cu
B
Mg
Last Crop
1- Coastal Bermuda
lb/acre
0.0
220
0
222
0
10
0
0
0
0
2- Rye
lb/acre
0.0
62
0
99
0
4
0
0
1-0
0
00766
WT-06
MIN
0.8
0.8 7.0
0.0
422
9
46
31
20
20
1713
1713
1190
10.2
100
93
6
0.8
0.1
Crop Recommendations:
Rec Uom
Lime (Vacre)
N
P205
K2
S
Mn
Zn
Cu
B
Mg
Last Crop
1- Coastal Bermuda
lb/acre
0-0
220
0
222
0
10
0
0
0
0
2- Rye
lb/acre
0.0
62
0
112
0
4
0
0
0.8
0
Comment:
Test result units = CEC and Na in megl100cm3; NO N in mgldm3: WN in glcm3
North Carolina Division of Water Quality Cerlificaflon #257, Analysis and fertility recommendations shown on this report are performed in accordance within NCDA guidelines, Analysis prepared by: Waypolni Analytical Carolina, Inc.