WQ0028653_2023 Residual Annual Report_20240223 (2)

Initial Review
Reviewer
nathaniel.thorn burg
Is this submittal an application? (Excluding additional information.) *
Yes No
If not an application what is the submittal type?* Annual Report
Residual Annual Report
Additional Information
Other
Annual Report Year* 2023
Permit Number (IR) * WQ0028653
Applicant/Permittee Pilgrim's Pride Corporation
Email Notifications
Does this need review by the hydrogeologist? * Yes No
Regional Office Raleigh
CO Reviewer
Admin Reviewer Wanda Gerald

Submittal Form
Project Contact Information
Please provide information on the person to be contacted by NDB Staff regarding electronic submittal, confirmation of receipt, and other correspondence.
Name* Robert T. Branch
Email Address*
[e-mail]
Project Information
.........................
Application/Document Type*
New (Fee Required)
Modification - Major (Fee Required)
Renewal with Major Modification (Fee
Required)
Annual Report
Additional Information
Other
Phone Number*
3363129007
Modification - Minor
Renewal
GW-59, NDMR, NDMLR, NDAR-1,
N DAR-2
Residual Annual Report
Change of Ownership
We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form.
https://edoes.deq.nc.gov/Forms/NonDischarge_Monitoring_Report
Permit Type:*
Wastewater Irrigation
High -Rate Infiltration
Other Wastewater
Reclaimed Water
Closed -Loop Recycle
Residuals
Single -Family Residence Wastewater
Other
Irrigation
Permit Number:*
WQ0028653
Has Current Existing permit number
Applicant/Permittee Address*
484 Zimmerman Road Sanford, NC 27331
Facility Name*
Pilgrim's Pride - Sanford Class A Residuals Program
Please provide comments/notes on your current submittal below.
At this time, paper copies are no longer required. If you have any questions about what is required, please contact Nathaniel Thornburg
at [e-mail].
Please attach all information required or requested for this submittal to be reviewed here.
(Application Form, Engineering Plans, Specifications, Calculations, Etc.)
2023_M_D_Annual_Report_PP_Sanford_Complete.pdf 1.16MB
Upload only 1 PDF document (less than 250 MB). Multiple documents must be combined into one PDF file unless file is larger
than upload limit.
* By checking this box, I acknowledge that I understand the application will not be accepted for pre -review until the fee (if required) has
been received by the Non -Discharge Branch. Application fees must be submitted by check or money order and made payable to the
North Carolina Department of Environmental Quality (NCDEQ). I also confirm that the uploaded document is a single PDF with all parts
of the application in correct order (as specified by the application).
Mail payment to:
NCDEQ — Division of Water Resources
Attn: Non -Discharge Branch
1617 Mail Service Center
Raleigh, NC 27699-1617
Signature
Submission Date 2/23/2024

2023 ANNUAL REPORT
PILGRIM'S PRIDE CORPORATION
WATER TREATMENT PLANT
SANFORD, NORTH CAROLINA
PERMIT #WQ0028653
Prepared For:
Pilgrim's Pride Corporation
484 Zimmerman Road
Sanford, N.C. 27331-3668
Prepared By:
Branch Residuals & Soils, LLC
1735 Heckle Blvd. Suite 103-291
Rock Hill SC. 29732
February 2024

BRANCH RESIDUALS & SOILS, LLC
173-555 Heckle Blvd, Suite 103-291, Rock Hill, SC 29732
PHONE [phone]
February 23, 2024
North Carolina Department of Environmental Quality
Division of Water Resources
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
Reference: 2023 LAND APPLICATION ANNUAL REPORT
Pilgrim's Pride Corporation.
Sanford, North Carolina
Permit No. WQ0028653
BR&S Project No. 2007-66
Information Processing Unit:
Branch Residuals & Soils is submitting all monitoring and reporting information as required in
the referenced permit on behalf of Pilgrim's Pride Corporation for their facility in Sanford, North
Carolina. This report includes: 1) Distribution and Marketing Certification and Summary Forms,
2) Annual Residual Sampling Summary Form, 3) Annual Metals Field Loading Summary Forms,
4) Annual land application Field Summary Forms, 5) Residual Analysis Lab Sheets, 6) TCLP
Lab Sheets, 7) Pathogen & Vector Attraction Form, 8) Pathogen and Vector Attraction
Reduction Documentation, 9) Soils Lab Data 10) 2023 Application Summary Table, and 11)
2023 Application Condition Summaries.
A total of 643,800 gallons (42.42 dry tons) of alum residuals were distributed to sites on the
Pilgrim's Pride Facility at Sanford, NC in September of 2023.
If any further information is required regarding this land application program, please do not
hesitate to contact me at [phone].
Sinc y,
Robert T. Branch, L.S.S.
Land Application/Residuals Operator
#15676
RTB
Enclosures

SECTION NO.
TABLE OF CONTENTS
TITLE
I Distribution and Marketing Certification and Summary
Forms
II Annual Residual Sampling Summary Form
III Annual Metals Field Loading Summary Forms
IV Annual Land Application Field Summary Forms
V Residual Analysis Lab Sheets
VI Toxicity Characteristics Leaching Procedure
(TCLP) Analysis Report
VII Pathogen and Vector Attraction Reduction
Form
VIII Pathogen and Vector Attraction Reduction Documentation
IX Soil Analysis Report
X 2023 Application Summary Table
XI 2023 Application Condition Summaries

DISTRIBUTION AND MARKETING CERTIFICATION AND SUMMARY FORM

CLASS A ANNUAL DISTRIBUTION AND MARKETING/ SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM
WQ PERMIT #: Wg0028653 FACILITY NAME: Pilgrim's Pride Corporation
PHONE: [phone] COUNTY: Lee OPERATOR: Denali Water
FACILITY TYPE (please check one): ❑ Surface Disposal (complete Part A (Source(s) and "Residual In" Volume only) and Part C)
El Distribution and Marketing (complete Parts A, B, and C)
Was the facility in operation during the past calendar year? Yes 0 No ❑ —► If No skip parts A, B, C and certify form below
Part A*:
Part B*:
Month
Sources(s) (include NPDES # if
applicable)
pp � )
Volumed tons}
Recipient Information
Amen men
Bulkin Agent
Residual In
Product Out
Nam s
�)
Volumed
(dry tons)
Intended use s
( )
January
February
March
April
May
June
Jul
August
September
October
November
PWS 03-53-130
0
NA
42.42
Pilgrim's Pride Corporation
42.42
Soil Amendment
December
Total from FORM DMSDF (sup)l
0
0
0
0
Totals:
Annual (dry tons):1
0
0
42A2
42.42
Amendment(s) used: 1 Bulking A ent(s) used:
* If more space is required, attach additional information sheets (FORM DMSDF (supp)): Total Number of Form DMSDF (Supp)
Part C:
Facility was compliant during the past calendar year with all conditions of the land application permit p Yes
(including but not limited to items I-3 below) issued by the Division of Water Quality: ❑ No -- - ► If No, Explain in Narritive
1. All monitoring was done in accordance with the permit and reported for the year as required and three (3) copies of certified laboratory results are attached.
2. All operation and maintenance requirements were compiled with or, in the case of a deviation, prior authorization was received from the Division of Water Quality.
3. No contravention of Ground Water Quality Standards occurred at a monitoring well.
,I ")
Signature of Permittee Date Signature of Preparer**
(if different from Pennittee)
**Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .l 102 (26)
a-.z9,-91Lr
Date
DBNR FORM DMSDF (12/2006)

ANNUAL RESIDUAL SAMPLING SUMMARY FORM

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ANNUAL METALS FIELD LOADING SUMMARY FORMS

ANNUAL METALS FIELD LOADING SUMMARY FORM
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
Pilgrim's Pride Corporation Total Dry Tons Applied (Annual):
WQ0028653 Cation Exchange Capacity (non 503 only):
Pilgrim's Pride Corporation Owner: Pilgrim's Pride Corporation Predominant Soil Series
7.14 Acres Permitted: 7.14 Site #: 1 Field #:
n/a
StA
17.20
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent ft
23-222-0072
WHO
Elm MMEM
00
Total
Phos-
phorusMENEENEENEEN
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
a W M
0 1 1 t
Total
Phos-
1
1
..
"I certify, under penalty of law, that this document was prepared under my direction or supervision in
accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information,
includ' a ossi i y of fines and imprisonment for knowing violations"
z1'Z3/z1/
Signature of Land Applier Date
Author Daryl D. Merritt DENR FORM MFLSF (7/2002)

ANNUAL METALS FIELD LOADING SUMMARY FORM
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
Pilgrim's Pride Corporation Total Dry Tons Applied (Annual):
WQ0028653 Cation Exchange Capacity (non 503 only):
Pilgrim's Pride Corporation Owner: Pilgrim's Pride Corporation Predominant Soil Series
16.01 Acres Permitted:
16.01 Site #:
Field #:
25.22
n/a
StA
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
23-222-0072
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
Phos-
..
..
phorus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in
accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
i
ma ' n sub ' ed. I am aware that there are significant penalties for submitting false information,
i e si of fines and imprisonment for knowing violations"
ZIZ3l2 L/
Signature of Land Applier Date
Author Daryl D. Merritt DENR FORM MFLSF (7/2002)

ANNUAL LAND APPLICATION FIELD SUMMARY FORMS

ANNUAL LAND APPLICATION FIELD SUMMARY FORMS LEGEND
All nutrients and metals concentrations listed on the following annual land application field
summary forms are on a pound per acre basis.
The following is a list of symbols and abbreviations used on the field loading rate report:
%TS — Percent Solids
DT/ACRE — Dry Tons Applied per Acre
lb/ac — Pounds per Acre
Metals (lbs/ac)
As —
Arsenic
Cd — Cadmium
Cr —
Chromium
Cu
— Copper
Pb —
Lead
Hg
— Mercury
Mo
— Molybdenum
Ni —
Nickel
Se —
Selenium
Zn —
Zinc
Nutrients (lbs/ac)
PAN — Plant Available Nitrogen
P — Phosphorus
K — Potassium
Annual Totals — lbs/ac applied during the calendar year.
Cumulative Totals — lbs/ac applied during the lifetime of field use.

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RESIDUAL ANALYSIS LAB SHEETS

Facility:
Source:
Location:
Contractor:
Type of Analysis:
Report No:
Date Sampled:
Date Reported:
Pilgrim's Pride WTP
Water Treatment Plant
Sanford, North Carolina
Denali Water Solutions
Water Treatment Plant
23-222-0072
8/9/2023
8/18/2023
Reporting Period: Annual 2023
Parameter
%
PPM
Dry Weight
EPA
Monthly Limits
Solids*
1.58
Nitrogen (TKN)
1.210
12,100.000
Phosphorus
0.084
844.000
Potassium
0.063
625.000
Sulfur
0.000
Calcium
0.313
3,130.000
Magnesium
0.061
614.000
Sodium
0.189
1,890.000
Iron
---
Aluminum
---
90,000.000
Manganese
---
Copper
---
85.000
1,500
Zinc
---
78.100
2,800
Ammonia Nitrogen
0.625
6,250.000
Nitrate N / Nitrite N
---
625.000
Cadmium
---
6.250
39
Chromium
---
1,200
Nickel
---
15.600
420
Lead
---
18.800
300
Arsenic
---
31.300
41
Mercury
---
11.600
17
Selenium
---
31.300
100
pH
8.000
Calcium Carbonate Eq.
0.000
Organic Nitrogen
0.585
Molybdenum
---
15.600
75
Chloride
---
Boron
Available P2O5
Specific Gravity

Pilgrim's Pride WTP
Water Treatment Plant
Sanford, North Carolina
Denali Water Solutions
Annual 2023
Date Reported: 8/18/2023 Report No: 23-222-0072
Note All Units in Pounds Per Dry Ton
Macro Nutrients Physical Characteristics
PAN Surf.
12.180
PAN Inj.
18.430
P
1.688
K
1.250
Lime
0.000
Secondary Nutrients
Calcium
6.260
Magnesium
1.228
Sodium
3.780
SAR
1.014
Chloride
0.000
Iron
0.000
Alumium
180.000
Manganese
0.000
Boron
0.000
Sulfur
0.000
Residual Nitrogen Calculation
Year Min Rate PAN #/Acre
% Solids
1.58
pH
8.000
Min Rate
0.400
Metals
Arsenic
0.063
Cadmium
0.013
Chromium
0.000
Copper
0.170
Lead
0.038
Mercury
0.023
Molybdenum
0.031
Nickel
0.031
Seleniun
0.063
Zinc
0.156
2021
2022
2023
0.40
4.68
2024
0.20
1.40
2025
0.10
0.56
2026
0.05
0.25
2027
2028
2029
2030
2031

Waypointo
ANALYTICAL
8/18/2023
Branch Residuals and Soils LLC
Mr. Bob Branch
1735 Heckle Blvd
Suite 103-291
Rock Hill, SC, 29732
Ref: Analytical Testing
Lab Report Number: 23-222-0072
Client Project Description: Sanford, NC
Project #2007-66
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 ° fax [phone]
www.waypointanalytical.com
Dear Mr. Bob Branch:
Waypoint Analytical, LLC. received sample(s) on 8/10/2023 for the analyses presented in the following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Where the laboratory was not responsible for the sampling
stage (refer to the chain of custody) results apply to the sample as received.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2021) and NELAC unless otherwise indicated. Any parameter
for which the laboratory is not officially NELAP accredited is indicated by a symbol. These are not included in
the scope because NELAP accreditation is either not available or has not been applied for. Additional
certifications may be held/are available for parameters, where NELAP accreditation is not required or applicable.
A full list of certifications is available upon request.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Connie Cook
Project Manager
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
4

Waypointo
ANALYTICAL
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 Fax [phone]
www,waypointa nalytical.com
Certification Summary
Laboratory ID: WP MTN: Waypoint Analytical, LLC., Memphis, TN
State
Program
Lab ID
Expiration Date
Alabama
State Program
40750
02/29/2024
Arkansas
State Program
88-0650
02/07/2024
California
State Program
2904
06/30/2024
Florida
State Program - NELAP
E871157
06/30/2024
Georgia
State Program
C044
11/14/2025
Georgia
State Program
04015
06/30/2024
Illinois
State Program - NELAP
200078
10/31/2024
Kentucky
State Program
80215
06/30/2024
Kentucky
State Program
KY90047
12/31/2023
Louisiana
State Program - NELAP
LA037
12/31/2023
Louisiana
State Program - NELAP
04015
06/30/2024
Mississippi
State Program
MS
11/14/2025
North Carolina
State Program
47701
07/31/2024
North Carolina
State Program
415
12/31/2023
Pennsylvania
State Program - NELAP
68-03195
05/31/2024
South Carolina
State Program
84002
06/30/2023
Tennessee
State Program
02027
11/14/2025
Texas
State Program - NELAP
T104704180
09/30/2023
Virginia
State Program
00106
06/30/2024
Virginia
State Program - NELAP
460181
09/14/2023
Page 1 of 1 00001 /23-222-0072

(2)
Waypoint 2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 ° Fax [phone]
ANALYTICAL www.waypointanalytical.com
Sample Summary Table
Report Number: 23-222-0072
Client Project Description: Sanford, NC
Project #2007-66
Lab No Client Sample ID Matrix Date Collected Date Received
92508 PS Solids 08/09/2023 10:35 08/10/2023

Waypointo
ANALYTICAL
Client: Branch Residuals and Soils LLC
Project: Sanford, NC
Lab Report Number: 23-222-0072
Date: 8/17/2023
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 1 Fax [phone]
www.waypointanalytical.com
CASE NARRATIVE
Block Digestion and FIA Method 4600NORGD-2011
Analyte: Total Kjeldahl Nitrogen
QC Batch No: 1-698416/1-698358
Matrix spike recovery is outside of control limits. Acceptable LCS recovery indicates the system was in control,
but the reported result could be affected by matrix interference.
Metals Analysis Method 6010D
Sample 63033 (Chesterfield)
Analyte: Aluminum
QC Batch No: 1-698628/1-698102
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 63033 (Chesterfield)
Analyte: Potassium
QC Batch No: 1-698628/1-698102
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Solids Total Mercury Analysis - CVAA Method 7471A
Sample 92740 (23-3182-0809-1)
Analyte: Mercury
QC Batch No: 1-698441/1-698222
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Anions by Ion Chromatography Method 9056A
Sample 92446 (Sludge)
QC Batch No: 1-698919/1-698345
The sample was diluted due to the nature of the sample matrix. Reporting limits have been adjusted accordingly.
Sample 92508 (PS)
QC Batch No: 1-698919/1-698345
The sample was diluted due to the nature of the sample matrix. Reporting limits have been adjusted accordingly.

Waypointo
ANALYTICAL
22972
Branch Residuals and Soils LLC Project Sanford, NC
Mr. Bob Branch
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 1 Fax [phone]
www.waypointanalytical.com
1735 Heckle Blvd Information : Project #2007-66
Suite 103-291
Rock Hill , SC 29732
Report Number : 23-222-0072
REPORT OFANAL YSIS
Report Date : 08/18/2023
Received : 08/10/2023
Lab No : 92508
Sample ID : PS
Matrix: Solids
Sampled: 8/9/2023 10:35
Test
Results
Units
MQL
DF
Date / Time
By
Analytical
Analyzed
Method
Moisture
98.4
0/0
0.010
1
08/14/23 16:57
CJR
2540G-2011
Ammonia Nitrogen
<6250
mg/Kg - dry
6250
1
08/17/23 14:30
JPJ
4500NH3C-2011
Nitrate (NO3-N)
<625
mg/Kg - dry
625
10
08/15/23 20:32
SDS
9056A
Nitrite (NO2-N)
<625
mg/Kg - dry
625
10
08/15/23 20:32
SDS
9056A
Nitrate+Nitrite-N
<625
mg/Kg - dry
625
10
08/15/23 20:32
9056A
pH
8.0
s.u.
1
08/14/2316:00
CNB
9045D
Total Solids
1.58
%
0.010
1
08/14/23 16:57
CJR
254OG-2011
Total Volatile Solids
30.8
%
0.010
1
08/14/23 16:57
CJR
2540G-2011
Total Kjeldahl Nitrogen
<12100
mg/Kg - dry
12100
1
08/14/23 13:40
ANH 4500NORGD-2011
Phosphorus
844
mg/Kg - dry
313
1
08/14/23 23:21
TJS
6010D
Aluminum
90000
mg/Kg - dry
313
1
08/14/23 23:21
TJS
6010D
Arsenic
<31.3
mg/Kg - dry
31.3
1
08/14/23 23:21
TJS
6010D
Cadmium
<6.25
mg/Kg - dry
6.25
1
08/14/23 23:21
TJS
6010D
Calcium
<3130
mg/Kg - dry
3130
1
08/14/23 23:21
TJS
6010D
Copper
85.0
mg/Kg - dry
31.3
1
08/14/23 23:21
TJS
6010D
Lead
<18.8
mg/Kg - dry
18.8
1
08/14/23 23:21
TJS
6010D
Magnesium
614
mg/Kg - dry
313
1
08/14/23 23:21
TJS
6010D
Mercury
<11.6
mg/Kg - dry
11.6
1
08/14/23 11:07
FDS
7471A
Molybdenum
<15.6
mg/Kg - dry
15.6
1
08/14/23 23:21
TJS
6010D
Nickel
<15.6
mg/Kg - dry
15.6
1
08/14/23 23:21
TJS
6010D
Potassium
<625
mg/Kg - dry
625
1
08/14/23 23:21
TJS
6010D
Selenium
<31.3
mg/Kg - dry
31.3
1
08/14/23 23:21
TJS
6010D
Sodium
1890
mg/Kg - dry
1560
1
08/14/23 23:21
TJS
6010D
Qualifiers/ DF Dilution Factor MQL Method Quantitation Limit
Definitions

Waypointo.
ANALYTICAL
22972
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 1 Fax [phone]
www.waypointanalytical.com
Branch Residuals and Soils LLC Project Sanford, NC
Mr. Bob Branch
1735 Heckle Blvd Information : Project #2007-66
Suite 103-291
Rock Hill , SC 29732
Report Date : 08/18/2023
Received : 08/10/2023
Report Number : 23-222-0072 REPORT OPANALYSIS
Lab No : 92508 Matrix: Solids
Sample ID : PS Sampled: 8/9/2023 10:35
Test Results Units MQL DF Date / Time By Analytical
Analyzed Method
Zinc
<78.1 mg/Kg - dry 78.1 1 08/14/23 23:21 TJS 6010D
Qualifiers/ DF Dilution Factor MQL Method Quantitation Limit
Definitions

(D
WayPAoi nt
NALYTICAL
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 ° Fax [phone]
www.waypointa nalytical.com
Shipment Receipt Form
Customer Number: 22972
Customer Name: Branch Residuals and Soils LLC
Report Number: 23-222-0072
Shipping Method
0 Fed Ex 0 US Postal 0 Lab 0 Other:
UPS 0 Client 0 Courier Thermometer ID: 135
Shipping container/cooler uncompromised?
* Yes
0 No
Number of coolers/boxes received
1
Custody seals intact on shipping container/cooler?
0 Yes
0 No
Not Present
Custody seals intact on sample bottles?
0 Yes
0 No
0 Not Present
Chain of Custody (COC) present?
* Yes
0 No
COC agrees with sample label(s)?
# Yes
0 No
COC properly completed
Yes
0 No
Samples in proper containers?
0 Yes
0 No
Sample containers intact?
* Yes
0 No
Sufficient sample volume for indicated test(s)?
0 Yes
0 No
All samples received within holding time?
# Yes
0 No
Cooler temperature in compliance?
Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
Yes
0 No
Water - Sample containers properly preserved
0 Yes
0 No
N/A
Water - VOA vials free of headspace
0 Yes
0 No
# N/A
Trip Blanks received with VOAs
0 Yes
0 No
# N/A
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
# N/A
High concentration container (48 hr) I Low concentration Encore samplers (48 hr)
High concentration pre -weighed (methanol -14 d) Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included?
0 Yes
0 No
Comments:
Signature: Makayla Weaver Date & Time: 08/10/2023 12:31:40

TOXICITY CHARACTERISTICS LEACHING PROCEDURE
(TCLP) ANALYSIS REPORT

Environmental Chemists,
Inc.
envirochem
6602 Windmill Way, Wilmington, NC 28405 i 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL 8 CONSULTING CHEMISTS
[e-mail]
Branch Residuals/Bob Branch
Date of Report: Oct 16, 2023
1735 Heckle Blvd Suite 103-291
Customer PO M
Rock Hill SC 29732
Customer ID: 15060009
Attention:
Report M 2023-21866
Project ID: Pilgrim's - Sanford
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
23-53326 Site: Pilgrim's-Sanford (Sludge) 9/20/2023
12:20 PM Solid/Sludge Bob Branch
Test
Method
Results Date Analyzed
Chlordane (TCLP)
SW-846 8081 B
<0.02 mg/L
09/26/2023
Endrin (TCLP)
$W-8466081 B
<0.0005 mg/L
09/26/2023
Heptachlor (TCLP)
SW-846 8081 B
<0.0005 mg/L
09/26/2023
Heptachlor epoxide (TCLP)
SW-846 8081 B
<0.0005 mg/L
09/26/2023
Lindane (TCLP)
SW-846 8081 B
<0.0005 mg/L
09/26/2023
Methoxychlor (TCLP)
SW-846 8081 B
<0.0005 mg/L
09/26/2023
Toxaphene (TCLP)
SW-846 8081 B
<0.05 mg/L
09/26/2023
2,4,5-TP (TCLP)
SW-846 8151 A
<0.003 mg/L
09/27/2023
2,4-D (TCLP)
SW-846 8151 A
<0.003 mg/L
09/27/2023
1,4-Dichlorobenzene (TCLP)
SW-846 8270 E
<0.050 mg/L
09/27/2023
2,4,5-Trichlorophenol (TCLP)
SW-846 8270 E
<0.050 mg/L
09/27/2023
2,4,6-Trichlorophenol (TCLP)
SW-846 8270 E
<0.050 mg/L
09/27/2023
2.4-Dinitrotoluene (TCLP)
SW-846 8270 E
<0.050 mg/L
09/27/2023
Cresol (TCLP)
SW-846 8270 E
<0.050 mg/L
09/27/2023
Hexachloro-1,3-butadiene (TCLP)
SW-846 82r0 E
<0.050 mg/L
09/27/2023
Hexachlorobenzene (TCLP)
SW-846 8270 E
<0.050 mg/L
09/27/2023
Hexachloroethane (TCLP)
SW-846 8270 E
<0.050 mg/L
09/27/2023
m + p-Cresol (TCLP)
SW -MO 8270 E
<0.050 mg/L
09/27/2023
Nitrobenzene (TCLP)
SW-846 8270 E
<0.050 mg/L
09/27/2023
o-Cresol (TCLP)
SW-846 8270 E
<0.050 mg/L
09/27/2023
Pentachlorophenol (TCLP)
SW-846 8270 E
<0.250 mg/L
09/27/2023
Pyridine (TCLP)
SW-846 82?0 E
<0.050 mg/L
09/27/2023
1,1-Dichloroethylene (TCLP)
SW-846 Method 8260D
<0.01 mg/L
09/27/2023
1,2-Dichloroethane (TCLP)
SW-846 Method 8260D
<0.01 mg/L
09/27/2023
Benzene (TCLP)
SW-846 Method 8260D
<0.01 mg/L
09/27/2023
Carbon Tetrachloride (TCLP)
SW-846 Method 82600
<0.01 mg/L
09/27/2023
Report it 2023.21868
Page 1 of 2

F7 007
6 Lnviroche]m
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab 1 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
[e-mail]
Branch Residuals/Bob Branch
Date of Report: Oct 16, 2023
1735 Heckle Blvd Suite 103-291
Customer PO #:
Rock Hill SC 29732
Customer ID: 15060009
Attention:
Report M 2023-21866
Project ID: Pilgrim's - Sanford
Chlorobenzene (TCLP)
SW-846 Method 8260D
<0.01 mg/L
09/27/2023
Chloroform (TCLP)
SW-846 Method 8260D
<0.01 mg/L
09/27/2023
Methyl ethyl ketone (TCLP)
SW-646 Method 8260D
<0.05 mg/L
09/27/2023
Tetrachloroethylene (TCLP)
SW-846 Method 8260D
<0.01 mg/L
09/27/2023
Tnchloroethylene (TCLP)
SW-846 Method 8260D
<0.01 mg/L
09/27/2023
Vinyl Chloride (TCLP)
SW-846 Method 8260D
<0.01 mg/L
09/27/2023
RCI
Cyanide
SM 4500 CN D-2016
2.55 mg/kg
09/27/2023
Sulfide
SM 4500 S D-2011
4.84 mg/kg
10/06/2023
Ignitability
SW 646 method 1010
>158 OF
09/29/2023
pH
SW 846 Method 9045D
7.80 units
10/09/2023
Resu.t estimated Analyzed out of 15 minutes hold time
TCLP Metals
Arsenic (TCLP)
EPA 200 7, Rev 4 4 1994
<1 0 mg/L
09/28/2023
Barium (TCLP)
EPA 200 7, Rev 4 4 1994
<1.0 mg/L
09/28/2023
Cadmium (TCLP)
EPA 200.7, Rev 4 4 1994
<1 0 mg/L
09/28/2023
Chromium (TCLP)
EPA 200 7, Rev 44 1994
<1.0 mg/L
09/28/2023
Lead (TCLP)
EPA 200 7, Rev 4 4 1994
<1.0 mg/L
09/28/2023
Selenium (TCLP)
EPA 200 7. Rev 4 4. 1994
<1.0 mg/L
09/28/2023
Silver (TCLP)
EPA 200 7. Rev 4 4. 1904
<1.0 mg/L
10/03/2023
Mercury (TCLP)
EPA 245 1
<0.0002 mg/L
10/04/2023
Comment:
Reviewed by:
T.
Report # 2023-21866 Page 2 of 2

Environmental Chemist, Inc., Wilmington, NC lab #94
Sample Receipt Checklist
6602 Windmill Way
Wilmington, NC 28405
910.392.0223
Client: POWDate: 100109 Report Number: _ 2023-
Receipt of sample: ECHEM Pickup Client Delivery ❑ UPS ❑ FedEx D Other ❑
❑ YES ❑ NO IN N/A II. Were custody seals present on the cooler?
❑ YES ❑ NO ❑O N/A 2. If custody seals were present, were they intact/unbroken?
Original temperature upon receipt °C Corrected temperature upon receipt °C
How temperature taken: ❑ Temperature Blank X❑ Against Bottles
IR Gun ID: Thomas Traceable S/N 210886869 IR Gun Correction Factor °C: 0.0
N YES ❑ NO 3. If temperature of cooler exceeded 6°C, was Project Mgr./QA notified?
0 YES ❑ NO 4. Were proper custody procedures (relinquished/received) followed?
N
YES
❑
NO
5. Were sample ID's listed on the COC?
N
YES
❑
NO
6. Were samples ID's listed on sample containers?
O
YES
❑
NO
7. Were collection date and time listed on the COC?
O
YES
17
NO
8. Were tests to be performed listed on the COC?
O
YES
❑
NO
9. Did samples arrive in proper containers for each test?
YES
❑
NO
10. Did samples arrive in good condition for each test?
N
YES
❑
NO
11. Was adequate sample volume available?'
YES
❑
NO
12. Were samples received within proper holding time for requested tests?
❑
YES
❑
NO
13. Were acid preserved samples received at a pH of <27
❑
YES
❑
NO
14. Were cyanide samples received at a pH >12?
❑
YES
❑
NO
15. Were sulfide samples received at a pH >9?
❑
YES
❑
NO
16. Were NH3/TKN/Phenol received at a chlorine residual of <0.5 m/L? **
❑
YES 10
NO
17. Were Sulfide/Cyanide received at a chlorine residual of <0.5 m/L?
❑
YES I
❑
NO 118.
Were orthophosphate samples filtered in the field within 15 minutes?
* TOC/Volatiles are pH checked at time of analysis and recorded on the benchsheet.
** Bacteria samples are checked for Chlorine at time of analysis and recorded on the benchsheet.
Preservation:
Sample(s)
by adding (circle one)
me of preservation:
(Must be completed for any sample(s) incorrectly preserved or with headspace)
were received incorrectly preserved and were adjusted accordingly
H2SO4 HNO3 HCl NaOH
If more than one preservative is needed, notate in comments below
Note Notify customer service immediately for incorrectly preserved samples Obta'n a new sample or
notify the state lab if directed to analyzed by the customer Who was notified date and time
olatiles Sample(s)
were received with headspace
COMMENTS:
DOC. QA.002 Rev 1

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PATHOGEN AND VECTOR
ATTRACTION REDUCTION FORM

PATHOGEN REDUCTION AND VECTOR ATTRACTION REDUCTION
The current permit, WQ0028653, does not have vector attraction requirements but does have Class
A requirements for pathogens. The form is marked to reflect these requirements.

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Pilgrinfs Pride Corporation
WWTP Name: Pilgrim's Pride Corporation Sanford NC WTP
Monitoring Period: From 1/1/2023 TO.
WQ Permit Number: WQ0028653
NPDES Number: PWS 03-53-130
12/31/2023
Pathoeen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A: Alt. A (time/temp) ❑ I
Alt B (Alk Treatment) ❑
Alt. C (Prior Testin ) Ed
A1t.D (No Prior Test) ❑
Process to Further Reduce Patho engs ❑
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost ❑ I Heat Drying ❑
Heat Treatment ❑ Thermophilic Ll
Beta Ray ❑ Gamma Ray ❑ I
Pasteurization ❑
Class B: Alt. (1) Fecal Density ❑
1 Alt. (2) Process to Significantly Reduce Pathogens Li
If applicable to alternative performed (Class
B only indicate "Process to Signlficaatly Reduce Pathogens":
Lime Stabilization ❑ AirDrying ❑
Compostin ❑
jAerobic Digestion ❑
Anaerobic Digestion ❑
If applicable to alternative performed
(Class A or Class B) complete the following monitoring data:
Parameter
Allowable Level
in Sludge
8
Pathogen Density
Flumner, or
Excee-
Frequency
of Analysis
Sample
Type
yP
a ica
Tech-
Minimum
Geo. Mean
aximu
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
CFU
1000 mpn per gram
of total solid (dry
weight)Gram
87
96
103
MPN/
0
Annually
Grab
SM I
9221 C,E
Salmonella bacteria
(in lieu of fecal
coliform
3 MPN per 4 grams
total solid (dry
weight)
Vector Attraction Reduction (15A I 02T .1107) - Please indicate alternative performed:
Alt.I (VS reduction) ❑
Alt. 2 (40-day bench) ❑
Alt. 3 (30-day bench) ❑
Alt. 4 (Spec. Oz uptake) ❑
Alt. 5 (14-Day Aerobic) ❑
Alt. 6 (Alk. Stabilization ❑
Alt 7 (Drying - Stable) ❑
Alt. 8 (Drying - Unstable) ❑
Alt. 9 (Injection) ❑
Alt. 10 (Incorporation) ❑
No vector attraction reduction alternatives
were performed El
CERTIFICATION STATEMENT (please check the appropriate statement)
El "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
❑ "1 certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note
if you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This deteriMation has been made un er my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Ms. Tina Pedley, WTP Lagoons ORC
Preparer Name and Title (type or print)
Signature of Prepare Date
Land Applier Name and Title (if applicable)(type or print)
Signature of Land Applier (if applicable)
Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM DMSDF (12/2006)

PATHOGEN AND VECTOR
ATTRACTION REDUCTION DOCUMENTATION

PATHOGEN REDUCTION AND VECTOR
ATTRACTION REDUCTION DOCUMENTATION
The current permit, WQ0028653, does not have vector attraction requirements but does have Class
A requirements for pathogens. Documentation is attached to reflect these requirements.

Pilgrim's Pride WTP
Sanford, North Carolina
WQ0028653
8/1/2023
Data Analyzed
8/10/2023
kl #::::::::::::::.:::::.
Fecal Colifotm
o `€€
L .........................
g.......................
... .... .... ........
Mph �r gram
23-43771
98
1.991
23-43772
103
2.013
23-43773
92
1.964
23-43774
97
1.987
23-43775
87
1.940
23-43776
99
1.996
23-43777
94
1.973
Total 13,863
Average 1;�$#1
Mean Colonies 1 Gram 96 : Fecal Coliformlgram
Fecal Coliform values are less than 1,000 and meets the Class A pathogen
reduction requirement

envirochem
ANALYTICAL & CONSULTING CHEMISTS
Branch Residuals/Bob Branch
1735 Heckle Blvd Suite 103-291
Rock Hill SC 29732
Attention:
Lab ID Sample ID:
2343771 Site: psi
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 ' 910.392.0223 Lab ` 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 ' 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 ' 910.3475843 Lab/Fax
[e-mail]
Date of Report: Aug 21, 2023
Customer PO #:
Customer ID: 15060009
Report #: 2023-17785
Project ID: Pilgrim's - Sanford
Collect Date/Time Matrix Sampled by
8/9/2023 10:36 AM Solid/Sludge Client
Test Method Results Date Analyzed
Total Solids (%) SM 2540 B 1.85 % 08/10/2023
Fecal Density SM 9221C E-2014 <98 MPN/g 08/09/2023
Lab ID Sample ID: Collect DatefTime Matrix Sampled by
2343772 Site: ps2 8/9/2023 10 39 AM Solid/Sludge Client
Test Method Results Date Analyzed
Total Solids (%) SM 2540 B 1.75 % 08/10/2023
Fecal Density SM 9221C E-2014 <103 MPN/g 08/09/2023
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
2343773 Site: psi 8/9/2023 10:42 AM Solid/Sludge Client
Test
Method
Results Date Analyzed
Total Solids (%)
SM 2540 B
1.97 % 08/10/2023
Fecal Density
SM 9221C E-2014
<92 MPN/g 08/09/2023
Lab ID Sample ID:
Collect DatelTime
Matrix Sampled by
23-43774 Site: ps4
8/9/2023 10:45 AM
Solid/Sludge Client
Test
Method
Results Date Analyzed
Total Solids (%)
SM 2540 B
1.86 % 08/10/2023
Fecal Density
SM 9221C E•2014
<97 MPN/g 08/09/2023
Lab ID Sample ID:
Collect Date/Time
Matrix Sampled by
23-43775 Site: ps5
8/9/2023 10:48 AM
Solid/Sludge Client
Test
Method
Results Date Analyzed
Total Solids (%)
SM 2540 B
2.09 % 08/10/2023
Fecal Density
SM 9221C E-2014
<87 MPN/g 08/09/2023
Report #. 2023-17785 Page 1 of 2

Environmental Chemists, Inc.
envirochem
ANALYTICAL & CONSULTING CHEMISTS
6602 Windmill Way, Wilmington, NC 28405 ' 910.392.0223 Lab ' 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 ' 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 ' 910.347.5843 Lab/Fax
infoC&environmentalchemists.com
Branch Residuals/Bob Branch Date of Report: Aug 21, 2023
1735 Heckle Blvd Suite 103-291 Customer PO #:
Rock Hill SC 29732 Customer ID: 15060009
Attention: Report #: 2023-17785
Project ID: Pilgrim's - Sanford
Lab lD Sample ID: Collect Date/Time Matrix Sampled by
23-43776 Site: ps6
8/9/2023 10:51 AM Solid/Sludge Client
Test Method Results Date Analyzed
Total Solids (%)
SM 2540 B
1.83 % 08/10/2023
Fecal Density SM 9221C E-2014 <99 MPN/g 08/09/2023
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
23-43777 Site: ps7
8/9/2023 10.54 AM Solid/Sludge Client
Test Method Results Date Analyzed
Total Solids (%)
Fecal Density
Comment:
Reviewed by:
SM 2540 S
SM 9221 C E-2014
1.92 %
<94 MPN/g
08/10/2023
08/09/2023
Report # 2023-17785 Page 2 of 2

Environmental Chemist, Inc., Wilmington, NC Lab #94
6602 Windmill Way
Wilmington, NC 28405
910 392 0223
Sample Receipt Checklist
Client: r1C:YIT-u,9_� t A uLa[ S Date: b '"I E�
Report Number. _ 2023-
Receipt of sample:
❑ YES ❑
ECHEM Pickup Client Delivery ❑ UPS ❑ Fed EX ❑ Other ❑
NO
O N/A
1. Were custody seals present on the cooler?
❑ YES
❑ NO
O N/A
2. If custody seals were present, were they intact/unbroken?
Original temperature upo i receipt "C Corrected temperatur, upon r_,r ip; C
How temperature taken: ❑
Temperature Blank 0 Against Bottles
IR Gun ID: Thomas Traceable S/fV 2i0886869 IR Gun Correction Factor 'C: 0.0
O YES
❑x
❑ NO
3. If temperature of cooler exceeded 6°C, was Project Mgr./QA notified?
YES
❑O
❑ NO
4. Were proper custody procedures (relinquished/received) followed?
YES
❑ NO
5. Were sample ID's listed on the COC?
E9 YES
❑ NO
6. Were samples ID's listed on sample containers?
I] YES
❑ NO
7. Were collection date and time listed on the COC?
❑O YES
❑ NO
8. Were tests to be performed listed on the COC?
❑x YES
❑ NO
9. Did samples arrive in proper containers for each test?
59 YES
❑ NO
10. Did samples arrive in good condition for each test?
Z YES
❑ NO
11. Was adequate sample volume availableT
YES
❑
❑ NO
12. Were samples received within proper holding time for requested tests?
YES
❑ NO
113. Were acid preserved samples received at a pH of <2?
❑ YES
❑ NO
14. Were cyanide samples received at a pH >12?
❑ YES
❑ NO
15. Were sulfide samples received at a pH >9?
❑ YES
❑ YES
❑ NO
❑
16. Were NH3/TKN/Phenol received at a chlorine residual of <0.5 m/L? **
❑
NO
11. Were Sulfide/Cyanide received at a chlorine residual of <0.5 m/L?
YES ❑ NO
18. Were orthophosphate samples filtered in the field within 15 minutes?
* TOC/Volatiles are pH checked at time of analysis and recorded on the benchsheet.
** Bacteria samples are checked for Chlorine at time of analysis and recorded on the benchsheet.
Sample Preservation:
(Must be completed for any samples) incorrect( Y preserved or with headspace)
Sample(s)
by adding (circle one):
were received incorrectly preserved and were adjusted accordingly
H2SO4 HNO3 NCI
NaOH
Time of preservation:
If more than one preservative is needed, notate in comments below
Note: Notify customer service immediately
for incorrectly preserved samples. obtain anew sample or
notify the state lab if directed to analyzed by the customer. who was notified, date and time:
Volatiles Sample(s)
were received with headspace
COMMENTS:
DOC. QA.002 Rev 1

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SOIL ANALYSIS REPORT

SOIL ANALYSIS REPORT
Soil samples are not required to be included in this annual report, according to the current permit.
Pilgrim's Pride will have these samples available for review if desired by the NCDEQ Regional
office.

2023 APPLICATION SUMMARY TABLE

Icon Icon I
W
A
G O 000
r. N
110 N M

2023 APPLICATION CONDITION SUMMARIES

Pilgrim's Pride WTP
Sanford, North Carolina
Denali Water Solutions
WQ0028653
Annual 2023
Water Treatment Plant
Farmer: Pilgrim's Pride
Acres: 7.14
Site/Tract: 1
Application Method: Surface
Field: 1
Percent Solids : 1.58
Residual Report No.: 23-222-0072
Crop: Fescue
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
9/25/23
1
58,000.0
Dry
warm
0.00
9/26/23
1
98,600.0
Dry
Cool
0.00
9/27/23
1
104,400.0
Dry
Cool
0.00
Total Gallons
261;000.0

Pilgrim's Pride WTP
Sanford, North Carolina
Denali Water Solutions
WQ0028653
Annual 2023
Water Treatment Plant
Farmer: Pilgrim's Pride
Acres: 16.01
Site/Tract: 1
Application Method: Surface
Field: 3
Percent Solids : 1.58
Residual Report No.: 23-222-0072
Crop: Fescue
. . .........
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
9/26/23
3
203,000.0
Dry
Cool
0.00
9/27/23
3
104,400.0
Dry
Cool
0.00
9/28/23
3
75,400.0
Dry
Cool
0.01
Total Gallons
382,800,0