WQ0039924_2023 Residual Annual Report_20240226 (2)

Initial Review
Reviewer
nathaniel.thorn burg
Is this submittal an application? (Excluding additional information.) *
Yes No
If not an application what is the submittal type?* Annual Report
Residual Annual Report
Additional Information
Other
Annual Report Year* 2023
Permit Number (IR) * WQ0039924
Applicant/Permittee Marcal Cordova LLC
Email Notifications
Does this need review by the hydrogeologist? * Yes U No
Regional Office Fayetteville
CO Reviewer
Admin Reviewer Wanda Gerald

Submittal Form
Project Contact Information
Please provide information on the person to be contacted by NDB Staff regarding electronic submittal, confirmation of receipt, and other correspondence.
Name* Robert T. Branch
Email Address*
[e-mail]
Project Information
.........................
Application/Document Type*
New (Fee Required)
Modification - Major (Fee Required)
Renewal with Major Modification (Fee
Required)
Annual Report
Additional Information
Other
Phone Number*
3363129007
Modification - Minor
Renewal
GW-59, NDMR, NDMLR, NDAR-1,
N DAR-2
Residual Annual Report
Change of Ownership
We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form.
https://edoes.deq.nc.gov/Forms/NonDischarge_Monitoring_Report
Permit Type:*
Wastewater Irrigation
High -Rate Infiltration
Other Wastewater
Reclaimed Water
Closed -Loop Recycle
Residuals
Single -Family Residence Wastewater
Other
Irrigation
Permit Number:*
WQ0039924
Has Current Existing permit number
Applicant/Permittee Address*
126 First Street Cordova, NC 28330
Facility Name*
Marcal Cordova Class A Residuals Program
Please provide comments/notes on your current submittal below.
At this time, paper copies are no longer required. If you have any questions about what is required, please contact Nathaniel Thornburg
at [e-mail].
Please attach all information required or requested for this submittal to be reviewed here.
(Application Form, Engineering Plans, Specifications, Calculations, Etc.)
MC —AR _2023_complete_signed.pdf 10.7MB
Upload only 1 PDF document (less than 250 MB). Multiple documents must be combined into one PDF file unless file is larger
than upload limit.
* By checking this box, I acknowledge that I understand the application will not be accepted for pre -review until the fee (if required) has
been received by the Non -Discharge Branch. Application fees must be submitted by check or money order and made payable to the
North Carolina Department of Environmental Quality (NCDEQ). I also confirm that the uploaded document is a single PDF with all parts
of the application in correct order (as specified by the application).
Mail payment to:
NCDEQ — Division of Water Resources
Attn: Non -Discharge Branch
1617 Mail Service Center
Raleigh, NC 27699-1617
Signature
Submission Date 2/26/2024

2023 ANNUAL REPORT
MARCAL CORDOVA, LLC
FIBER CLAY RESIDUAL
CORDOVA, NORTH CAROLINA
CLASS A
PERMIT #WQ0039924
p "Irm. fasTro ro m-wm
126 First Street
Cordova, N.C. 28330
W!, m-rim-WWWWWW"
1735 Heckle Blvd. Suite 103-291
Rock Hill SC, 29732

row I I - 11 1 1
REMPTIRTIRMUM
PHONE [phone]
1.0- lUtIMES MIA 1
Division of Water Resources
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
Reference: 2023 CLASS A LAND APPLICATION ANNUAL REPORT
Marcal Cordova, LLC. (Formerly von Drehle Corporation)
Cordova, North Carolina
Permit No. WQ0039924
BR&S Project No. 2014-110
lip P P 011; 11M
VCIZVOMWIC PCIIIIIPWIIII UCHUI-17VI ETIdICUI U191111CIVI'd, LLU I+F UICIF laclimy III
This report includes: Distribution and Marketing Certification and Summary Fonn. Distributions
were made from January through December during 2023. These distributions totaled 61,348.68
wet tons (21,370.36 dry tons). These applications were surface spread and incorporated into the
soil.
If any further information is required regarding this land application program, please do n
hesitate to contact me at [phone]. 1
Mom
Robert T. Ilk L.S.S.
64 v/1 esi&zl dievtim

TABLE OF CONTENTS
SECTION NO. TITLE
Distribution and Marketing Certification and Summary
Forms
II Annual Residual Sampling Summary Form
III Residual Analysis Lab Sheets
IV Toxicity Characteristics Leaching Procedure
(TCLP) Analysis Report
V Pathogen and Vector Attraction Reduction
Forms
VI Pathogen and Vector Attraction Reduction Documentation

DISTRIBUTION AND MARKETING CERTIFICATION AND SUMMARY FORM

CLASS A ANNUAL DISTRIBUTION AND MARKETING/ SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM
WQ PERMIT #: WQ0039924 FACILITY NAME: Marcal Cordova, LLC
PHONE: [phone] COUNTY: Richmond OPERATOR: Bio-Nomic Services, Inc.
FACILITY TYPE (please check one): Surface Disposal (complete Part A (Source(s) and "Residual In" Volume only) and Part C)
❑ Distribution and Marketing (complete Parts A, B, and C)
Was the facility in operation during the past calendar year? Yes 21 No If No skip parts A, B, C and certify form below
Part A*: Part B*:
Sources(s) (include NPDES # if Volume (dry tons) Recipient Information
Month applicable) Amendment/ Residual In Product Out Name(s) Volumed tons) Intended use
Bulking Agent
January 1,620.11 1,620.11 1,620.11 Soil Amendment
February 1,561.35 1,561.35 1,561.35 Soil Amendment
March 2,019.46 2,019.46 2,019.46 Soil Amendment
April 1,962.04 1,962.04 1,962.04 Soil Amendment
May 2,499.89 2,499.89 2,499.89 Soil Amendment
June 1,959.05 1,959.05 1,959.05 Soil Amendment
July 1,670.90 1,670.90 1,670.90 Soil Amendment
August 2,277.29 2,277.29 2,277.29 Soil Amendment
September 1,507.54 1,507.54 1,507.54 Soil Amendment
October 1,731.40 1,731.40 1,731.40 Soil Amendment
November 909.40 909.40 909.40 Soil Amendment
December 1,651.92 1,651.92 1,651.92 Soil Amendment
Total from FORM DMSDF (sup) 0 0.00 0.00 0.00
..........................
6 0 36 370 0 21 t d l Totals: A ..........................
nnua(dry tons): ,.21,37.3
I I ......................... 21,370.36
Amendment(s) used: I Bulking Agent(s) used:
If more space is required, attach additional information sheets (FORM DMSDF (supp)): Total Number of Form DMSDF (Supp)l
Part C:
Facility was compliant during the past calendar year with all conditions of the land application El Yes
permit (including but not limited to items 1-3 below) issued by the Division of Water Quality: 11 No P, If No, Explain in Narritive
1. All monitoring was done in accordance with the permit and reported for the year as required and three (3) copies of certified laboratory results are attached.
2. All operation and maintenance requirements were compiled with or, in the case of a deviation, prior authorization was received from the Division of Water Quality.
3. No contravention of Ground Water Quality Standards occurred at a monitoring well.
!(0/Z
Signat-ure of P�--- en,t'ee Date Sil-riat- re of 1�-enare- Date
(if dffl Pe_it ferent Erom.
"Preparer is def-fined in 40 0--R -Part 503.9(r) and 15A NCAC 2'T .1102 (26)

ANNUAL RESIDUAL SAMPLING SUMMARY FORM

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RESIDUAL ANALYSIS LAB SHEETS

Facility:
Mareal Corporation
Source:
Marcal Paper
Location:
Cordova, North Carolina
Contractor:
Bio-Nomic Services
Type of Analysis:
Industrial
Report No:
me 2023-1 W
Date Sampled:
12/12/2022
Date Reported:
12/21/2022
Reporting Period:
Jan-23
Parameter
%
PPM
EPA
Dry Weight
Monthly Limits
Solids
40.60
Nitrogen (TKN)
0.102
1,020.000
Phosphorus
0.011
106.000
Potassium
0.007
69.200
Sulfate
0.000
Calcium
20.500
205,000.000
Magnesium
0.259
2,590.000
Sodium
0.075
749.000
Iron
---
Aluminum
---
1)580.000
Manganese
---
Copper
---
41.900
1,500
Zinc
---
65.000
2,800
Ammonia Nitrogen
0.025
246.000
Nitrate N / Nitrite N
---
24.6000
Cadmium
---
0.2460
39
Chromium
---
1,200
Nickel
---
1.4200
420
Lead
---
3.2000
300
Arsenic
---
6.1600
41
Mercury
---
0.3370
17
Selenium
---
12.3000
100
pH
7.500
Calcium Carbonate Eq.
0.0000
Organic Nitrogen
0.077
Molybdenum
---
3.8400
75
vailable P205

Industrial
Marcal Paper
Cordova, North Carolina
Jan-23
Date Reported: 12/21/2022 Report No: me 2023-1 W
Note All Units in Pounds Per Dry Ton
I Or V rz r, I W ra f=.,
I I �41
Physical Characteristics
% Solids
40.60
pH
7.500
Min Rate
0.400
I Or VT M,
0 0 MR. ?, IT I �1
oil

Way intri.
I PARTICAL
iFA%7?ZW4
Mr. Bob Branch
1735 Heckle Blvd
Suite 103-291
Rock Hill, SC, 29732
Ref: Analytical Testing
Lab Report Number: 22-347-0006
Client Project Description: Sludge Testing
Project: 2014-10
Von Drehle
Cordova, NC
tilli
Main 901.213.2400 1 Fax [phone]
www.waypointanalytical.com
Dear Mr. Bob Branch:
Waypoint Analytical, LLC. received sampli on 12/13/2022 for the analyses presented in the following report.
IRWIN
It♦I 1 1.11111100111111 1:4 Ir
"Wi i -1 - I I a 11106111111,111W1111 :*'111616"M .16.10
"i Em -a . .16 AiaFdr1IeLeI`5 I'l-11re6t- __
POP
(including 40 CFR 136 Method Update Rule May 2021) and NELAC unless otherwise indicated. Any parameter
for which the laboratory is not officially NELAP accredited is indicated by a '—'symbol. These are not included in
the scope because NELAP accreditation is either not available or has not been applied for. Additional
certifications may be held/are available for parameters, where NELAP accreditation is not required or applicable.
A full list of certifications is available upon request.
Refer to sample analysis time for confirmation of holding time compliance.
WAS 1101101 -0 0 41 0 1
A I;WrM Iiii IIIIJ1111101:00111112111 Ib"MrA01111A
11 1 , i J
11.!- i! 111111111! 1•ire!. ll! 11
Connie Cook
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 1,. cf 10

Way int
1 RTICAL
Project Manager
www.waypointanalytical.com
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 2 of .1.0

Wayp l`
ato
.. , .Jklip�« «
. - i J - M.
Main 901.213.2400 0 Fax [phone]
www.waypointanalytical.com
State
Program
Lab ID
Expiration Cate
Alabama
State Program
40750
2/28/2023
Arkansas
State Program
8-060
02/07/2023
California
State Program
290
06/30/2023
Florida
State Program - NELAP
E871157
06/30/202
Georgia
State Program
C044
02/18/2023
Georgia
State Program
0015
06/30/2023
Illinois
State Program - NELAP
20007
10/10/202
Kentucky
State Program
80215
06/30/2023
Kentucky
State Program
KY90047
12/31/2022
Louisiana
State Program - NELAP
LA037
12/31/2022
Louisiana
State Program - NELAP
04015
06/30/2023
Mississippi
State Program
MS
02/11/202
North Carolina
State Program
47701
07/31/2023
North Carolina
State Program
415
12/31/2022
Pennsylvania
State Program - NELAP
6-015
05/31/2023
South Carolina
State Program
84002
06/30/2023
Tennessee
State Program
02027
02/11/2023
Texas
State Program - NELAP
T107010
09/30/2022
Virginia
State Program
00106
06/30/2023
Virginia
State Program - NELAP
460181
09/14/2023
Page 1 of 1 00001/22-347-0006
Page 3 of 10

Client Project Description: Sludge Testing
Project: 2014-10
Von Drehle
Cordova, NC
Lab No Client Sample ID MatrZ
82159 VD Solids 12/12/2022 13:15 12/13/2022
Page 4 of 1.0

Way nt(b
11 PM�TICAL
Project: Sludge Testing
Lab Report Number: 22-347-0006
Date: 12/21/2022
V'14
Main 901.213.2400 ' Fax 901.213.244t
www.waypointanalytical.com
X111 :1111 1 T-11 V X11% Il kyj
Metals Analysis Method 6010D
Sample 95900 (SB-126-1)
Analyte: Aluminum
QC Batch No: L655058/1-654036
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 82159 (VD)
Analyte: Arsenic
QC Batch No: L654830/L654036
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Sample 95900 (SB-126-1)
Analyte: Calcium
QC Batch No: 1-655058/1-654036
The matrix spike and/or the matrix spike duplicate was outside aquality control acceptance ranages. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 95900 (SB-126-1)
Analyte: Potassium
QC Batch No: 1-655058/1-654036
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranapes. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 95900 (SB-126-1)
Analyte: Magnesium
QC Batch No: 1-654830/1-654036
The matrix spike and/or the matrix spike duplicate was outside aqualitit control acceptance ran
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 95900 (SB-126-1)
Analyte: Molybdenum
QC Batch No: L654830/1-654036
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Sample 95900 (SB-126-1)
Analyte: Phosphorus
QC Batch No: 1-654830/1-654036
The matrix s9ike and/or the matrix spike duplicate was outside quality control acceptance ran•
' es. A dilution te'l
was performed and passed quality control acceptance ranges. No matrix interference is suspected. M
Sample 95900 (SB-126-
Analyte: Lead I
Page 5 of 10

Waypoint(2)
ANALYTICAL
QC Batc!51o: 1-654830/1-654036
ranges. Matrix interference is suspected.
Sample 82159 (VD)
Analyte: Selenium
QC Batch No: 1-6548301654036
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Sample 95900 (SB-126-1)
Analyte: Selenium
QC Batch No: 1-654830/1-654036
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Sample 95900 (SB-126-1)
Analyte: Selenium
QC Batch No: 1-655058/1-654036
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Page 6 of 10

WaN Fii,- nt.Q
1C
22972
Branch Residuals and Soils LLC
Mr. Bob Branch
1735 Heckle Blvd
Suite 103-291
Rock Hill , SC 29732
Report Number: 22-347-0006
an
Project Sludge Testing
Information : Project: 2014-10
Von Drehle
Main 901.213.2400 0 Fax [phone],
www.waypointanalytical.com
REPoR TAL Y515
Results Units MQL
Matrix: Solids
Sampled: 12/12/2022 13:1S
DF Date / Time By Analytical
Analyzed Method
Neutralizing Value (%CCE)
<0.1
%
OA
1
12/20/22 08:56
DXT
AOAC 955.01
Moisture
59.4
%
0.010
1
12/16/22 15:44
FMM
2540G-2011
Ammonia Nitrogen
<246
mg/Kg - dry
246
1
12/20/22 14:00
JPJ
4500NH3C-2011
Nitrate (NO3-N)
<24.6
mg/Kg - dry
24.6
10
12/16/22 17:43
SRI
9056A
Nitrite (NO2-N)
<24.6
mg/Kg - dry
24.6
10
12/16/22 17:43
SRJ
9056A
Nitrate+Nitrite-N
<24.6
mg/Kg - dry
24.6
10
12/16/22 17:43
9056A
pH
7®
S.U.
1
12/20/22 14:53
DRS
9045D
Total Solids
40.6
%
0.010
1
12/16/22 15:44
FMM
2540G-2011
Total Kjeldahl Nitrogen
1020
mg/Kg - dry
421
1
12/21/22 10:47
CLP
4500NORGD-2011
Phosphorus
106
mg/Kg - dry
12.3
1
12/20/22 00:35
TJS
6010D
Aluminum
1580
mg/Kg - dry
12.3
1
12/20/22 00:35
OK N
6010D
Arsenic
<6.16
mg/Kg - dry
6.16
5
12/20/22 21:48
BKN
6010D
Cadmium
<0.246
mg/Kg - dry
0.246
1
12/20/22 00:35
TIS
6010D
Calcium
205000
mg/Kg - dry
6160
50
12/20/22 22:03
BKN
6010D
Copper
41®
mg/Kg - dry
1.23
1
12/20/22 00:35
TIS
6010D
Lead
3.20
mg/Kg - dry
0.738
1
12/20/22 00:35
TIS
6010D
Magnesium
2590
mg/Kg - dry
12.3
1
12/20/22 00:35
TIS
6010D
Mercury
<0.337
mg/Kg - dry
0.337
1
12/16/22 11:13
FDS
7471A
Molybdenum
3®4
mg/Kg - dry
0.615
1
12/20/22 00:35
TIS
6010D
Nickel
1.42
mg/Kg - dry
0.615
1
12/20/22 00:35
TIS
6010D
Potassium
69.2
mg/Kg - dry
24.6
1
12/20/22 00:35
BKN
6010D
Selenium
< 12.3
mg/Kg - dry
12.3
10
12/21/22 14:24
TIS
6010D
Sodium
749
mg/Kg - dry
61.6
1
12/20/22 00:35
TIS
6010D
Qualifiers/ DF
Dilution Factor
MQL Method Quantitation Limit
Definitions
Page 7 oE 1.0

0 2790 Whitten Road, Memphis, TN 38133
Waypoint. Main 901.213.2400 0 Fax [phone]
ANALYTICAL www.waypointanalytical.com
22972
Branch Residuals and Soils LLC Project Sludge Testing
Mr. Bob Branch Report Date 12/21/2022
1735 Heckle Blvd Information : Project: 2014-10 Received 12/13/2022
Suite 103-291 Von Drehle
Rock Hill , SC 29732
Report Number: 22-347-0006
Lab No : 82159
Sample ID : VD
M
M
Qualifiers/ DF Dilution Factor
Definitions
r;V4�100Tq
Matrix: Solids
&=114r IO;
MOL DF Date / Time By Analytical
Analyzed Method
65.0 mg/Kg - dry
Z rolll I 10 9 ONG �0- "' - W
Page 8 cE 10

� * I
0 F-W-1AAA1 WA I
Customer Number: 22972
Customer Name: Branch Residuals and Soils LLC
Report Number: 22-347-0006
tog[#
Main 901.213.2400 0 Fax [phone]
www.waypointanalytical.com
Fed Ex US Postal Lab
0 UPS Client Courier
Other :
Thermometer ID:
I
Shipping container/cooler uncompromised?
0 Yes
No
.................
Number of coolers/boxes received
1
Custody seals intact on shipping container/cooler?
Yes
No
0 Not Present
Custody seals intact on sample bottles?
Yes
No
0 Not Present
Chain of Custody (COC) present?
0 Yes
No
COG agrees with sample label(s)?
0 Yes
No
COC properly completed
0 Yes
No
Samples in proper containers?
0 Yes
No
Sample containers intact?
0 Yes
No
Sufficient sample volume for indicated test(s)?
0 Yes
No
All samples received within holding time?
0 Yes
No
Cooler temperature in compliance?
0 Yes
No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
0 Yes
No
Water - Sample containers properly preserved
Yes
No
0 N/A
Water - VOA vials free of headspace
Yes
No
0 N/A
Trip Blanks received with VOAs
Yes
No
0 N/A
Soil VOA method 5035 — compliance criteria met
Yes
No
0 N/A
High concentration container (48 hr)
High concentration pre -weighed (methanol -14 d)
Low concentration Enor e samplers (48 hr)
Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included?
Yes
0 No

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Page 10 of 10

Facility:
Marcal Corporation
Source:
Marcal Paper
Location:
Cordova, North Carolina
Contractor:
io-Nomic Services
Type of Analysis:
Industrial
Report No:
me 2023-2
Date Sampled:
1/24/2023
Date Reported:
2/6/2023
Reporting Period:
Feb-23
Parameter
%
PPM
EPA -
Dry Weight
Monthly Limits
Solids
40.40
Nitrogen (TKN)
0.127
1,270.000
Phosphorus
0.010
103.000
Potassium
0.008
80.400
Sulfate
0.000
Calcium
20.100
201,000.000
Magnesium
0.292
2,920.000
Sodium
0.059
587.000
Iron
---
Aluminum
---
1,580.000
Manganese
---
Copper
---
40.100
1,500
Zinc
---
74.300
2,800
Ammonia Nitrogen
0.025
248.000
Nitrate N / Nitrite N
---
24.8000
Cadmium
---
0.2480
39
Chromium
---
1,200
Nickel
---
1.4600
420
Lead
---
0.7420
300
Arsenic
---
2.3600
41
Mercury
---
0.3490
17
Selenium
---
4.8000
100
pH
7.600
Calcium Carbonate Eq. *
0.0000
Organic Nitrogen
0.102
Molybdenum
---
3.4700
75
Chloride
Boron
Available P205

Industrial
Marcal Paper
Cordova, North Carolina
Feb-23
Date Reported: 2/6/2023 Report No: me 2023-2 W
Note All Units in Pounds Per Dry Ton
Macro Nutrients Physical Characteristics
6vj I Z
Secondary Nutrients
Magnesium
I •c
% Solids
40.40
pH
7.600
Min Rate
0.400
��
a

Wayp int (D
Mr. Bob Branch
1735 Heckle B71vd I
Suite 103-291
Rock Hill, SC, 29732
Ref: Analytical Testing
Lab Report Number: 23-025-0087
Client Project Description: Von Drehle
Project #2014-110
ag
Main 901.213.2400 0 Fax [phone]
www.waypointanalytical.com
Dear Mr. Bob Branch:
Waypoint Analytical, LLC. received sample(s) on 1/25/2023 for the analyses presented in the following report.
-------------
cermicationts maj Ue liela/ or parameYerz77ffrGTG-M=A??I- n is not req Irel or app ME
A full list of certifications is available upon request.
I i . I I . . I ^ 1 0 1 - . - . I 1 0 1, . . . I I . I
11;A101KIK012111d ving] KOIE LOIL0111REIII V-AKOJ 1011r.1110
the samples included in this report.
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 1 of 8

'Ont,(2)
WaPMTICAL«
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f f. f M f• ',, f is
! ! 4
State
Program
Lab ID
Expiration Date
Alabama
State Program
40750
02/28/2023
Arkansas
State Program
8-060
02/07/2023
California
State Program
2904
06/30/2023
Florida
State Program - NELAP
E871157
0/30/2023
Georgia
State Program
C044
02/18/2023
Georgia
State Program
04015
06/30/2023
Illinois
State Program - NELAP
2007
10/10/2023
Kentucky
State Program
80215
06/30/2023
Kentucky
State Program
KY90047
12/31/223
Louisiana
State Program - NELAP
L037
12/31/2023
Louisiana
State Program - NELAP
0015
06/30/2023
Mississippi
State Program
MS
02/11/2023
North Carolina
State Program
47701
07/31/2023
North Carolina
State Program
415
12/31/2023
Pennsylvania
State Program - NELAP
6-015
05/31/2023
South Carolina
State Program
84002
06/30/2023
Tennessee
State Program
0027
11/14/2025
Texas
State Program - NELAP
T1070180
0/30/2023
Virginia
State Program
00106
06/30/2023
Virginia
State Program - NELAP
46011
09/14/2023
Page 1 of 1 00001 r23-025-0087
Page 2 of 8

0 (2)
Waypoint,
ANALYTICAL
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 ' Fax [phone]
www.waypointanalytical.com
Sample Summary Table
Report Number: 23-025-0087
Client Project Description: Von Drehle
Project #2014-110
Lab No Client Sample ID Matrix Date Collected Date Received
97226 VD Solids 01/24/2023 12:45 01/25/2023
Page 3 ci�f 9

0
k TAIN191
Project: Von Drehle
Lab Report Number: 23-025-0087
Date: 2/6/2023
Main 901.213.2400 * Fax [phone]
www.waypointanalytical.com
WTIIVW[Tud��
Metals Analysis Method 6010D
Sample 98832
Analyte: Aluminum
QC Batch No: 1-661330/1-661089
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 98832
Analyte: Arsenic
QC Batch No: L661330/1-661089
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Sample 98832
Analyte: Calcium
QC Batch No: 1-661330/1-661089
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 98832
Analyte: Potassium
QC Batch No: 1-661330/1-661089
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 98832
Analyte: Lead
QC Batch No: 1-661330/1-661089
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Anions by Ion Chromatography Method 9056A
QC Batch No: 1-661123/1-660684
The sample was diluted due to the nature of the sample matrix. Reporting limits have been adjusted accordingly.
Page 4 of B

Waypoint.(b
22972
Branch Residuals and Soils LLC
Mr. Bob Branch
1735 Heckle Blvd
Suite 103-291
Rock Hill , SC 29732
lim
Main 901.213.2400 0 Fax [phone]
www.waypointanalytical.com
Project Von Drehle
Information : Project #2014-110
REPoRrOFANALYSIS
Results Units MQL
Matrix: Solids
Sampled: 1/24/2023 12:45
DF Date / Time By Anal ical
Analyzed Method
Neutralizing Value (%CCE)
9®4
%
0.1
1
01/30/23 11:15
HBT
AOAC 955.01
Moisture
S9.6
%
0.010
1
01/27/23 16:10
FMM
2540G-2011
Ammonia Nitrogen
<248
mg/Kg - dry
248
1
02/03/23 13:30
CLP
4500NH3C-2011
Nitrate (NO3-N)
<248
mg/Kg - dry
248
100
01/27/23 15:34
SRI
9056A
Nitrite (NO2-N)
<24.8
mg/Kg - dry
24,8
10
01/27/23 15:21
SRI
9056A
Nitrate+ N itrite-N
<24.8
mg/Kg - dry
24.8
10
01/27/23 15:21
9056A
pH
®6
S.U.
1
02/03/23 15:43
SAR
9045D
Total Solids
40.4
%
0.010
1
01/27/23 16:10
FMM
2540G-2011
Total Kjeldahl Nitrogen
1270
mg/Kg - dry
124
1
01/27/23 12:14
ANH
4500NORGD-2011
Phosphorus
103
mg/Kg - dry
12.4
1
01/31/23 02:53
JTR
6010D
Aluminum
1580
mg/Kg - dry
12.4
1
01/31/23 02:53
JTR
6010D
Arsenic
2.36
mg/Kg - dry
1,24
1
01/31/23 02:53
JTR
6010D
Cadmium
<0.248
mg/Kg - dry
0.248
1
01/31/23 02:53
JTR
6010D
Calcium
201000
mg/Kg - dry
2480
20
01/31/23 16:56
JTR
6010D
Copper
®1
mg/Kg - dry
1.24
1
01/31/23 02:53
JTR
6010D
Lead
<0.742
mg/Kg - dry
0.742
1
01/31/23 02:53
JTR
60100
Magnesium
2920
mg/Kg - dry
12.4
1
01/31/23 02:53
JTR
60100
Mercury
<0.349
mg/Kg - dry
0.349
1
01/30/23 15:49
JTR
7471A
Molybdenum
3®7
mg/Kg - dry
0.618
1
01/31/23 02:53
JTR
6010D
Nickel
1.46
mg/Kg - dry
0.618
1
01/31/23 02:53
JTR
6010D
Potassium
®4
mg/Kg - dry
24.8
1
01/31/23 02:53
JTR
6010D
Selenium
4.80
mg/Kg - dry
1.24
1
01/31/23 02:53
JTR
6010D
Sodium
S87
mg/Kg - dry
61.9
1
01/31/23 02:53
JTR
6010D
(tualifiers/ DF Dilution Factor
Definitions
Page 5 of 6

C) 2790 Whitten Road, Memphis, TN 38133
Waypoint. Main 01.213.2400 0 Fax [phone]
ANALYTICAL www.waypointanalytical.com
22972
Branch Residuals and Solis LLC Project Von Drehle
Mr. Bob Branch Report Date 02/06/2023
1735 Heckle Blvd Information : Project #2014-110 Received 01/25/2023
Suite 103-291
Rock Hill , SC 29732
Report Number: 23-025-0087
Lab No : 97226
Sample ID: VD
NMI
Qualifiers/ DF Dilution Factor
Definitions
Matrix: Solids
Sampled: 1/24/2023 12:4S
Results Units MOL DF Date / Time By Analytical
Analyzed Method
74.3 mg/Kg - dry 3.09 1 01/31/23 02:53 ITR 6010D
Page 5 of 6

0 2790 Whitten Road, Memphis, TN 38133
Waypoint Main 901.213.2400 * Fax [phone]
ANALYTICAL www.waypointanalytical.com
aM7X-zMMUM3M=-
Customer Number: 22972
Customer Name: Branch Residuals and Solis LI-C
Report Number: 23-025-0087
Shipping Method
Fed Ex US Postal Lab
41 UPS Client Courier
Other
Thermometer ID:
100
Shipping container/cooler uncompromised?
0 Yes
No
Number of coolers/boxes received
1
Custody seals intact on shipping container/cooler?
Yes
No
0 Not Present
Custody seals intact on sample bottles?
Yes
No
0 Not Present
Chain of Custody (COC) present?
0 Yes
No
COC agrees with sample labei(s)?
0 Yes
No
COC properly completed
0 Yes
No
Samples in proper containers?
0 Yes
No
Sample containers intact?
0 Yes
No
Sufficient sample volume for indicated test(s)?
0 Yes
No
All samples received within holding time?
0 Yes
No
Cooler temperature in compliance?
0 Yes
No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
0 Yes
No
Water - Sample containers properly preserved
Yes
No
40 N/A
Water - VOA vials free of headspace
Yes
No
0 N/A
Trip Blanks received with As
Yes
No
0 N/A
Soil VOA method 5035 — compliance criteria met
Yes
No
0 N/A
High concentration container (48 hr)
High concentration pre -weighed (methanol -14 d)
Low concentration EnCore samplers (48 hr)
Low conc pre -weighed vials (Sod is -14 d)
Special precautions or instructions included?
Comments:
Yes
0 No
MFEMM��=-

sz a
0
w +aro mu
w u+
L u W q A„
�u z ae Eu
C w w a® x x a s E Ic,r^ u
w I
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r .W
z
�a .� E I]; .,
wa � E
`a: E E
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AL
ro 2 E E E
B'3 aC 6+ ...J 49 M = i—
a.
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A
Y-- - ------- -- - - -- - -------- Ll
W E
2 :. w ! / °
12
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�
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ail is;aNl Xplew
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1.3
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�^ d ,r Apq

Facility:
Marcal Corporation
Source:
Marcal Paper
Location:
Cordova, North Carolina
Contractor:
Bio-Nomic Services
Type of Analysis:
Industrial
Report No:
me 2023-3 W
Date Sampled:
2/20/2023
Date Reported:
3/6/2023
Reporting Period:
Mar-23
Parameter
%
Solids
35.30
Nitrogen (TKN)
0.128
Phosphorus
0.013
Potassium
0.009
Sulfate
Calcium
19.500
Magnesium
0.220
Sodium
0.067
Iron
---
Aluminum
---
Manganese
---
Copper
---
Zinc
---
Ammonia Nitrogen
0.028
Nitrate N / Nitrite N
---
Cadmium
---
Chromium
---
Nickel
---
Lead
---
Arsenic
Mercury
---
Selenium
---
pH
7.300
Calcium Carbonate Eq.
Organic Nitrogen
0.100
•
I i• to) I
&V I Mrs—=0 -�'
PPM EPA
i Weight Monthly Limits
111
11

Industrial
Marcal Paper
Cordova, North Carolina
Mar-23
Date Reported: 3/6/2023 Report No: me 2023-3 W
Note All Units in Pounds Per Dry Ton
im.mrsam7m
Wwj
Secondary Nutrients
A 1 41 loop$
11
Manganese
Physical Characteristics
0 Solids
35.30
pH
7.300
Min Rate
0.400
I Of -T mo,
�10
�1 Min
-W

Way
I PARTICAL
Mr. Bob Branch
173�5 Heckle Blvd
I
Suite 103-291
Rock Hill, SC, 29732
1\ef: Analytical Testing
Lab Report Number: 23-053-0077
Client Project Description: Sludge Testing
Dear Mr. Bob Branch:
Main 901.213.2400 1 Fax [phone]
www.waypointanalytical.com
00 0 �10 zwulw 10111114111OW11111 IN 91 110114111 w"
E-Iv'ps IZE'l V-1 1;1 sual igm g1l ffl. 6 a 9 ........
W on 1
=01IF IS 111dj Ale I CLAP eo
A full list of certifications is available upon request.
1.4111110,1111 W111111991"W"N' NOW, im" OW1,111161 101111W M-Ilowill"
IWAV-1011111VVI gly'OL-2411 r-Amasiol 1111 rugLO111.41M LOIL011 lIIisil 1011ral I
the samples included in this report.
Norst 0=1 � in, rOTH71-1 MO,
M=
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 3. of 10

Way * to
Pa It f L ,...
111:1111 1 i... I� .I
www.waypointanalytical.com
State
Program
Lab ID
Expiration Date
Alabama
State Program
40750
02/2/2024
Arkansas
State Program
-0650
02/07/2024
California
State Program
2904
06/30/2023
Florida
State Program - NELAP
E871157
0/30/2023
Georgia
State Program
C044
11/1/2025
Georgia
State Program
0401
06/0/2023
Illinois
State Program - NELAP
20007810/10/202
Kentucky
State Program
80215
06/30/2023
Kentucky
State Program
KY90047
12/31/2023
Louisiana
State Program - NELAP
L037
12/31/2023
Louisiana
State Program - NELAP
04015
06/0/2023
Mississippi
State Program
MS
02/11/2023
North Carolina
State Program
47701
07/31/2023
North Carolina
State Program
415
12/1/2023
Pennsylvania
State Program - NELAP
6-0315
05/31/2023
South Carolina
State Program
84002
06/30/2023
Tennessee
State Program
007
11/14/2025
Texas
State Program - NELAP
T1070410
0/30/2023
Virginia
State Program
00106
6/0/2023
Virginia
State Program - NELAP
460181
0/1/2023
Page 1 of 1 0000123-053-0077

Client Project Description: Sludge Testing
Lab No Client Sample ID Matrix
Date Collected Date Received
Solids 02/20/2023 13:30
02/22/2023
Page 3 of 2.0

Wayp int(D
"i TICiL
Project: Sludge Testing
Lab Report Number: 23-053-0077
Main 901.213.2400 ' Fax [phone]
www.waypointanalytical.com
CASE NARRATIVE
Metals Analysis Method 6010D
Sample 90770
QC Batch No: L666340/L665814
One or more Internal Standards are outside method acceptance criteria. Re -analysis and/or sample dilutions are
required.
Sample 90770
Analyte: Aluminum
QC Batch No: L666340/L665814
The matrix spike, matrix spike duplicate and the dilution test were all outside of the quality control acceptance
ranges. Matrix interference is suspected.
Sample 90770
Analyte: Aluminum
QC Batch No: L666993/L665814
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 90770
Analyte: Arsenic
QC Batch No: L666340/L665814
The matrix spike, matrix spike duplicate and the dilution test were all outside of the quality control acceptance
ranges. Matrix interference is suspected.
Sample 90770
Analyte: Arsenic
QC Batch No: L666637/L665814
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Sample 90770
Analyte: Calcium
QC Batch No: L666637/L665814
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 90770
Analyte: Potassium
QC Batch No: L666637/L665814
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
. if - 10
u Mw MMILTA .
Paqe 4 of 1.0

0 0 0
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 ' Fax [phone]
www.waypointanalytical.com
QC Batch No: 1-666340/1-665814
TJILP-#-2 19.1-kr-A
ranges. Matrix interference is suspected.
Sample 90770
Analyte: Magnesium
QC Batch No: L666637/L665814
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 90770
Analyte: Nickel
QC Batch No: 1-666340/1-665814
The matrix spike, matrix spike duplicate and the dilution test were all outside of the quality control acceptance
ranges. Matrix interference is suspected.
Sample 90770
Analyte: Phosphorus
QC Batch No: L666637/L665814
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 90770
Analyte: Lead
QC Batch No: L666340/L665814
The matrix spike, matrix spike duplicate and the dilution test were all outside of the quality control acceptance
ranges. Matrix interference is suspected.
Sample 90770
Analyte: Lead
QC Batch No: L666637/L665814
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Sample 90770
Analyte: Selenium
QC Batch No: 1-666340/1-665814
The matrix spike, matrix spike duplicate and the post digestion spike were all outside of the quality control
acceptance ranges. Matrix interference is suspected
Sample 90770
Analyte: Zinc
QC Batch No: 1-666340/1-665814
The matrix spike, matrix spike duplicate and the dilution test were all outside of the quality control acceptance
ranges. Matrix interference is suspected.
Sample 90770
Analyte: Zinc
QC Batch No: 1-666637/1-665814
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Page 5 of 10

! 0 1
0 FAI I
Main 901.213.2400 1 Fax [phone]
www.waypointanalytical.com
Solids Total Mercury Analysis - CVAA Method 7471A
Sample 99714
Analyte: Mercury
QC Batch No: 1-666799/1-666619
The matrix spike, matrix spike duplicate and the post digestion spike were all outside of the quality control
acceptance ranges. Matrix interference is suspected
Page 6 oE 10

Report Number: 23-053-0077
Matrix: Solids
Test
Results
Units
MOL
QF
Date /Time
By
Analytical
Analyzed
Method
Neutralizing Value (%CCE)
48.2
96
D.1
1
03/01/2311:15
H8T
4OAC955.D1
Moisture
64,7
96
0.810
1
03/33/3315:45
FMM
254OG-2011
Ammonia Nitrogen
<283
mg/Kg 'dry
283
1
03y04/23 14:30
]P]
450ONH3C'2011
N|traUe(NO3-N)
<28.3
mg/Kg-dm
28.3
10
02/27/23 10:39
S0
9066A
N|tMhe(NO2'N)
<203
mg/Kg 'dry
28.3
10
02/37y23 18:39
SFO
9056A
Nitrate+N|trihe'N
<I03
mg/Kg 'dry
28.3
10
02/27/23 18:39
9056A
pH
7.3
S.U.
1
03/28/2316:00
6AR
9045D
Total Solids
35.3
%
0.010
1
02/23V23 15:45
PMM
254UG-3011
Total Kje|dah|Nitrogen
1280
mg/Kg dry
1*2
1
03/38/23 14:39
ANH
4580NORGQ-2011
Phosphorus
131
mg/Kg-dry
1*.2
1
03/27/2328:04
T]S
6010D
Aluminum
1750
mg/Ng-dry
14.2
1
03/25/3383:42
]TR
6010D
Arsenic
4,82
mg/Ng-dry
1AI
1
03/26y2388:42
T]5
6010D
Cadmium
<0.283
mg/Kg 'dry
0183
1
0I/25y2303:4I
TJ5
6010D
Calcium
195000
mg/Kg 'dry
14200
100
02/I7/2320:10
T]5
6010D
Copper
46.S
mg/Kg -dry
1.42
z
0I/25/2383:*2
lu5
uDzOo
Lead
<0.849
mg/Kg-dry
0.849
1
0425/2383:42
T]S
6010Q
Magnesium
2200
mg/Kg dry
14.2
1
02/25/2383:43
TJ5
8010D
Mercury
<0.504
mg/Kg-dry
0.504
1
02Y28/23 15:23
FIDS
7471A
Molybdenum
4.62
mg/Ng-dry
O.708
1
02/35/2383:43
T]5
8010n
M|che|
2.28
mg/Kg 'dry
0.700
1
02/35y2383:42
l]S
6010D
Potassium
91,5
mg/Kg 'dry
28.3
1
02/27y2320:04
T]S
6010D
Selenium
2.48
mg/Kg 'dry
142
1
02/25/2303:42
T]G
6010D
Sodium
666
mg/Kg 'dry
70.8
1
02/25/2303:42
T35
60100
Qualifiers/ DF Dilution Factor
DefinitioTs
Page 7 of 10

Report Number: 23-053-0077
Lab No : 90492
Sample ID : VD
Test
No
Qualifiers/ DF Dilution Factor
Definitions
WA*t
Main 901.213.2400 0 Fax [phone]
www.waypointanalytical.com
Matrix: Solids
Sampled: 2/20/2023 13:30
Results Units MOIL DIF Date / Time By Analytical
Analyzed Method
73.9 mg/Kg - dry 3.54 1 02/25/23 03:42 TIS 6010D
Page 8 of I.G

Main 901.213.2400 0 Fax [phone]
www.waypointanalytical.com
Shipment Receipt Form
Customer Number: 22972
Customer Name: Branch Residuals and Solis L
Report Number: 23-053-0077 1
EM MW12J=
Fed Ex US Postal Lab
Other :
0 UPS Client Courier
ThermometerID:
�137_
Shipping container/cooler uncompromised?
0 Yes
No
Number of coolers/boxes received
1
Custody seals intact on shipping container/cooler?
Yes
No
0 Not Present
Custody seals intact on sample bottles?
Yes
No
0 Not Present
Chain of Custody (CC) present?
40 Yes
No
COC agrees with sample label(s)?
41 Yes
No
CC properly completed
0 Yes
No
Samples in proper containers?
0 Yes
No
Sample containers intact?
40 Yes
No
Sufficient sample volume for indicated test(s)?
0 Yes
No
All samples received within holding time?
0 Yes
No
Cooler temperature in compliance?
0 Yes
No
Cooler/Samples arrived at the laboratory on ice.
0 Yes
No
Samples were considered acceptable as cooling
process had begun.
Water ® Sample containers properly preserved
Yes
No
0 N/A
Water - VOA vials free of headspace
Yes
No
0 N/A
Trip Blanks received with VOAs
Yes
No
0 N/A
Soil VOA method 5035 ® compliance criteria met
Yes
No
0 N/A
High concentration container (48 hr)
Low concentration EnCore samplers (48 hr)
High concentration pre -weighed (methanol -14 d)
Low conc pre -weighed vials (Sod is ®1 d)
Special precautions or instructions included?
Yes
0 No
I

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n V
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M
E
0
p
c C,
cc M
C�
mw
o
U
a
a
a
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m
mm.a
4
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0
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own °
r
0
0
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aj
'E
a.
Paste
10
of
10

Solids
Potassium
Sulfate
Calcium
Sodium
Iron
Aluminum
Manganese
Zinc
Ammonia Nitrogen
Nitrate N / Nitrite N
Cadmium
Chromium
Nickel
Lead
Arsenic
alcium Carbonate Eq.
rganic Nitrogen
[olvbdenum
oron
vailable P2O5
Marcal Corporation
Marcal Paper
Cordova, North Carolina
io-Nomic Services
Industrial
e 2023-4
3/13/2023
3/22/2023
Apr-23
% PP
ry Wei
36.60
0.134
0.011
0.007
1
11
111
I11
1 11
1.5800
1.1000
1.3700
0.5140
1.3700
Ozf�Z�I��iI�Iili:
EPA
Monthly Limits

Industrial
Marcal Paper
Cordova, North Carolina
Apr-23
Date Reported: 3/22/2023 Report No: me 2023-4 W
Note All Units in Pounds Per Dry Ton
1OFTM, mWrlm'
Secondary Nutrients
Physical Characteristics
% Solids
36.60
pH
7.400
Min Rate
0.400
LVj M NT,

Waypoint.(2)
ANALYTICAL
Bob Branch c 1
1735 Heckle Blvd
S it
uite 103-291
Rock Hill, SC, 29732
NO: Analytical Testing
Lab Report Number: 23-073-0053
Client Project Description: Project #2014-111
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 Fax [phone]
www.waypointanalytical.com
Dear Mr. Bob Branch:
Waypoint Analytical, LLC. received sample(s) on 3/14/2023 for the analyses presented in the following report.
09NO-ON11 "N' 11111 ONION*
r-Kol rul
--l"I Lolls
,Ilr ,1411;nylolol EV441pr�&
the samples included in this report.
MMEM
=- .5 zoaa'. wo FAM-Emk-aKEEME�
1. 1 - I - - 6��R 11:11 Iff iiiIii.fil I I I I!!, I I I I I I I I I � I I I lI F11I, =.4 it
Page 1 oE 9

*1
Main 't; 411' Fax [phone]
www.waypointanalytical.com
State
Program
Lab ID
Expiration Date
Alabama
State Program
40750
2/2/224
Arkansas
State Program
8-0650
02/07/2024
California
State Program
2904
06/30/2023
Florida
State Program - NELAP
E871157
06/30/2023
Georgia
State Program
C044
11/14/202
Georgia
State Program
04015
0/0/2023
Illinois
State Program - NELAP
20007
10/10/2023
Kentucky
State Program
80215
06/30/2023
Kentucky
State Program
KY90047
1/1/2023
Louisiana
State Program - NELAP
LA037
12/31/202
Louisiana
State Program - NELAP
0015
06/30/203
Mississippi
State Program
MS
02/11/2023
North Carolina
State Program
47701
07/31/202
North Carolina
State Program
415
12/31/023
Pennsylvania
State Program - NELAP
68-03195
05/1/2023
South Carolina
State Program
84002
0/30/2023
Tennessee
State Program
02027
11 /14/02
Texas
State Program - NELAP
T104704180
09/30/202
Virginia
State Program
00106
06/30/023
Virginia
State Program - NELAP
46011
09/14/202
Page 1 of 1 0000123-073-0053

(D 2790 Whitten Road, Memphis, TN 38133
Waypoint. Main 901.213.2400 1 Fax [phone]
ANALYTICAL www.waypointanalytical.com
Sample Summary Table
Report Number: 23-073-0053
Client Project Description: Project #2014-110
Lab No Client Sample ID Matrix
98991 VD Solids
03/13/2023 12:24
03/14/2023
Page 3 of 9

Way int(b
I PARTICAL
Project: Project #2014-110
Lab Report Number: 23-073-0053
Date: 3/22/2023
Main 9000 1.213.24' Fax [phone]
www.waypointanNi
alytical.com
F—VZTZ1'L% d kyl
Metals Analysis Method 6010D
Sample 99896 (SS-4, 0'-3')
Analyte: Aluminum
QC Batch No: 1-671277/1-670200
61 ow tonce ranies, A dilution te-st - -4
a - 1 0 ps uwym k, Lon I fivig 1 La I Elm I L.-d 1;1 m7,0 &-Mm &I aga"g-14
Sample 99896 (SS-4, 0'-3')
Analyte: Arsenic
QC Batch No: 1-671023/1-670200
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Sample 99896 (SS-4, 0'-3')
Analyte: Magnesium
QC Batch No: 1-671023/1-670200
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 99896 (SS-4, 0'-3')
Analyte: Phosphorus
QC Batch No: 1-671023/1-670200
es. A dilution tes)
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 99896 (SS-4, 0'-3')
Analyte: Selenium
QC Batch No: 1-671023/1-670200
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Solids Total Mercury Analysis - CVAA Method 7471A
Sample 90250 (White Bluff WWTP: Sludge)
Analyte: Mercury
QC Batch No: 1-671176/1-670913
The matrix soke- matrix s%ike du ' �licateandthe%ost i,.oestion s�tike were all outside of the �eualitp control
acceptance ranges. Matrix interference is suspected
Anions by Ion Chromatography Method 9056A
Sample 98991 (VD)
QC Batch No: 1-670716/1-670499
The sample was diluted due to the nature of the sample matrix. Reporting limits have been adjusted accordingly.

Waypoint (20
ANALYTICAL
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 " Fax [phone]
www.waypointanalytical,com
Page 5 of 9

"A.141k
Main 901.213.2400 0 Fax [phone]
www.waypointanalytical.com
Report Number: 23-073-0053
Lab No : 98991
Sample ID : VD
Matrix: Solids
Sampled: 3/13/2023 12:24
Test
Results
Units
MOL
DF
Date / Time
By
Analytical
Analyzed
Method
Neutralizing Value (%CCE)
24.8
%
OA
1
03/22/23 10:53
DXT
AOAC 955.01
Moisture
3®4
%
0.010
1
03/19/23 17:47
CID
254OG-2011
Ammonia Nitrogen
473
mg/Kg - dry
273
1
03/22/23 10:00
JPJ
4500NH3C-2011
Nitrate (NO3-N)
<27.3
mg/Kg - dry
27.3
10
03/17/23 19:12
SRI
9056A
Nitrite (NO2-N)
<27.3
mg/Kg - dry
27.3
10
03/17/23 19:12
SRJ
9056A
Nitrate+Nitrite-N
< 27.3
mg/Kg - dry
27.3
10
03/17/23 19:12
9056A
pH
7®
SM.
1
03/15/23 15:50
SAR
9045D
Total Solids
36.6
%
0.010
1
03/19/23 17:47
CID
254OG-2011
Total Kjeldahl Nitrogen
1340
mg/Kg - dry
137
1
03/21/23 14:21
ANH 4500NORGD-2011
Phosphorus
112
mg/Kg - dry
13.7
1
03/21/23 05:36
JTR
6010D
Aluminum
1660
mg/Kg - dry
13.7
1
03/21/23 05:36
ITR
6010D
Arsenic
<1.37
mg/Kg - dry
1.37
1
03/21/23 05:36
ITR
6010D
Cadmium
<0.273
mg/Kg - dry
0.273
1
03/21/23 05:36
ITR
6010D
Calcium
167000
mg/Kg - dry
13700
100
03/21/23 20:18
TIS
6010D
Copper
18.1
mg/Kg - dry
1.37
1
03/21/23 05:36
ITR
6010D
Lead
1®
mg/Kg - dry
0.819
1
03/21/23 05:36
ITR
6010D
Magnesium
2150
mg/Kg - dry
13.7
1
03/21/23 05:36
ITR
6010D
Mercury
<0.514
mg/Kg - dry
0.514
1
03/21/23 13:28
FDS
7471A
Molybdenum
4.37
mg/Kg - dry
0.683
1
03/21/23 05:36
ITR
6010D
Nickel
1.58
mg/Kg - dry
0.683
1
03/21/23 05:36
ITR
6010D
Potassium
70®
mg/Kg - dry
27.3
1
03/21/23 05:36
ITR
6010D
Selenium
< 1.37
mg/Kg - dry
137
1
03/21/23 05:36
ITR
6010D
Sodium
842
mg/Kg - dry
683
1
03/21/23 05:36
ITR
6010D
Qualifiers/ DF Dilution Factor
Definitions

Report Number: 23-073-0053
Lab No : 98991
Sample ID: VD,
Test
No
Main 901.213.2400 0 Fax [phone]
www.waypointanalytical.com
mmml��
Matrix: Solids
Sampled: 3/1312023 12:24
Results Units MOIL DF Date / Time By AnaWlcal
Analyzed Method
175 mg/Kg - dry 3.42 1 03/21/23 05:36 JTR 6010D
Qualifiers/ DF Dilution Factor MQL Method Quantitation Limit
Definitions
Page 7 of 9

Waypoint(2)
ANALYTICAL
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 * Fax [phone]
www.waypointanalytical.com
Shipment Receipt Form
Customer Number: 22972
Customer Name: Branch Residuals and Soils LLC
Report Number: 23-073-0053
Shipping Method
Fed Ex US Postal Lab Other:
0 UPS Client Courier Thermometer ID: �1'3'6
Shipping container/cooler uncompromised?
-----------------------
0 Yes
No
Number of coolers/boxes received
Custody seals intact on shipping container/cooler?
Yes
- -- -- --------------------
No
--
0 Not Present
-
Custody seals intact on sample bottles?
--
Yes
N
----------------------------
0 Not Present
Chain of Custody (COC) present?
0 Yes
No
COC agrees with sample label(s)?
0 Yes
No
COC properly completed
0 Yes
No
Samples in proper containers?
0 Yes
-- ------- ------
No
-----
Sample containers intact?
11
0 Yes
No
Sufficient sample volume for indicated test(s) ?
0 Yes
No
All samples received within holding time?
0 Yes
No
Cooler temperature in compliance?
0 Yes
No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
0 Yes
No
Water - Sample containers properly preserved
Yes
No
0 N/A
Water - VOA vials free of headspace
Yes
No
0 N/A
Trip Blanks received with VOAs
Yes
No
Soil VOA method 5035 — compliance criteria met
Yes
No
------------------
High concentration container (48 hr)
High concentration pre -weighed (methanol -14 d)
Low concentration EnCore samplers (48 hr)
Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included?
Yes
0 No
Signature: Makayla Weaver Date & Time: 03/14/2023 10:58:39

Ott
3

Facility:
Marcal Corporation
Source:
Mareal Paper
Location:
Cordova, North Carolina
Contractor:
Bio-Nomic Services
Type of Analysis:
Industrial
Report No:
me 2023-5 W
Date Sampled:
4/17/2023
Date Reported:
4/28/2023
Reporting Period:
May-23
Parameter
% PP M EPA
Solids
41.60
Nitrogen (TKN)
0.128
1,280.000
Phosphorus
0.012
119.000
Potassium
0.007
73.600
Sulfate
0.000
Calcium
19.700
197,000.000
Magnesium
0.216
2,160.000
Sodium
0.066
656.000
Iron
---
Aluminum
---
1,600.000
Manganese
---
Copper
---
17.400 1,500
Zinc
---
114.000 2,800
Ammonia Nitrogen
0.031
310.000
Nitrate N / Nitrite N
---
24.0000
Cadmium
---
0.0240 39
Chromium
1,200
Nickel
---
1.3600 420
Lead
---
1.7800 300
Arsenic
---
2.1400 41
Mercury
---
0.4300 17
Selenium
---
12.0000 100
pH
7.500
Calcium Carbonate Eq.
52.500
525,000.0000
Organic Nitrogen
0.097
Molybdenum
---
4.83001 75
Chloride
Boron
Available P205

Industrial
Marcal Paper
Cordova, North Carolina
May-23
Date Reported: 4/28/2023 Report No: me 2023-5 W
Note All Units in Pounds Per Dry Ton
Macro Nutrients Physical Characteristics
z =--mmig
1 Ill
% Solids
41.60
pH
7.500
Min Rate
0.400
I UT

Waypoint(b
ANALYTICAL
Iff
Mr. Bob Branch
1735 Heckle Blvd
Suite 103-291
Rock Hill, SC, 29732
Ref: Analytical Testing
Lab Report Number: 23-108-0184
Client Project Description: Project #2014-110
Dear Mr. Bob Branch:
2790 Whitten Road, Memphis, TIN 38133
Main 901.213.2400 0 Fax [phone]
www.waypointanalytical.com
mayZe neia/are 5111hauie upir A;E1rUmFier&,11"'fl—F1TwA)!CAr- acci-FITUT1771 r=1#1t-rEATwFi IF G—A=Alfre—
A full list of certifications is available upon request.
TM-71
1RAgIgOISIM] 101mr-1 girws.211 ljoldwol ilia 11011ma
I I RRI fue-t5--dr -e-1 -eTAJT#Tr I #Tf'Cf1-f'CfS---
the samples included in this report.
us=
Page 1 of 8

�f1.. f
• I
State
Program
Lab ID
Expiration Date
Alabama
State Program
40750
02/ /2024
Arkansas
State Program
-0650
02/07/2024
California
State Program
290
06/30/202
Florida
State Program - NELAP
E71157
6/30/2023
Georgia
State Program
C04
11/14/2025
Georgia
State Program
04015
06/30/2023
Illinois
State Program - NELAP
20007
1/10/2023
Kentucky
State Program
80215
06/30/2023
Kentucky
State Program
KY90047
12/1/203
Louisiana
State Program - NELAP
L037
12/31/2023
Louisiana
State Program - NELAP
04015
0/30/2023
Mississippi
State Program
MS
11/1/2025
North Carolina
State Program
47701
07/31/2023
North Carolina
State Program
415
12/31/2023
Pennsylvania
State Program - NELAP
6-03195
05/31/2024
South Carolina
State Program
84002
06/30/2023
Tennessee
State Program
02027
11/14/2025
Texas
State Program - NELAP
T1070410
0/30/202
Virginia
State Program
00106
06//023
Virginia
State Program - NELAP
46011
09/1/2023
Page 1 of 1 00001 /23-108-0184
Page 2 of 8

(D 2790 Whitten Road, Memphis, TN 38133
Waypoint. Main 901.213.2400 0 Pax 901.213.2442
ANALYTICAL www.waypointanalytical.com
Sample Summary Table
Report Number: 23-108-0184
Client Project Description: Project #2014-110
Lab No Client Sample ID
Matrix Date Collected Date Received
Solids 04/17/2023 11:50 04/18/2023
Page .3 of 8

b
ANALYTICAL
Project: Project #2014-110
Lab Report Number: 23-108-0184
D. 4/28/2023
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 * Fax [phone]
www.waypointanalytical.com
WXIAFNAOIO�
Metals Analysis Method 6010D
Sample 98538
Analyte: Aluminum
QC Batch No: 1-678073/1-677142
-AAQ&W!. P--J
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 98538
Analyte: Aluminum
QC Batch No: 1-678312/1-677142
-A-dkdhv,�-R)
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 98538
Analyte: Potassium
QC Batch No: 1-677789/1-677142
The matrix spike and/or the matrix sn,'ke duplicate was outside quality control acceptance rannes. A dilution tesl
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 98379 (M)
Analyte: Selenium
QC Batch No: L677789/L677142
This analyte was analyzed at a dilution due to IC interference/matrix interference.
Anions by Ion Chromatography Method 9056A
Sample 98379 (M)
QC Batch No: 1-677522/1-677272
The sample was diluted due to the nature of the sample matrix. Reporting limits have been adjusted accordingly.

ff-T-T*Rwnffl. �01 �T
an
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 Fax [phone]
www.waypointanalytical.com
23r r
Matrix: Solids
Sampled: 4/17/2023 11:50
-esults Units MOIL DF Date / Time By Analytical
Analyzed Method
Neutralizing Value (%CCE)
52.S
%
0.1
1
04/28/23 10:13
DXT
AOAC 955.01
Moisture
58.4
%
0.010
1
04/21/23 16:40
JILS
2540G-2011
Ammonia Nitrogen
310
mg/Kg - dry
240
1
04/24/23 12:00
CLP
4500NH3C-2011
Nitrate (NO3-N)
<24.0
mg/Kg - dry
24.0
10
04/20/23 16:43
SRI
9056A
Nitrite (NO2-N)
<24.0
mg/Kg - dry
24.0
10
04/20/23 16:43
SRJ
9056A
Nitrate+Nitrite-N
<24.0
mg/Kg - dry
24.0
10
04/20/23 16:43
9056A
pH
7.S
SM.
1
04/25/23 16:30
CN13
9045D
Total Solids
41.6
%
0,010
1
04/21/23 16:40
ILS
2540G-2011
Total Kjeldahl Nitrogen
1280
mg/Kg - dry
498
1
04/20/23 14:57
ANH
4500NORGD-2011
Phosphorus
119
mg/Kg - dry
12.0
1
04/22/23 02:28
TJS
6010D
Aluminum
1600
mg/Kg - dry
12.0
1
04/22/23 02:28
TJS
6010D
Arsenic
2.14
mg/Kg - dry
1.20
1
04/22/23 02:28
TJS
6010D
Cadmium
<0.240
mg/Kg - dry
0.240
1
04/22/23 02:28
TJS
6010D
Calcium
197000
mg/Kg - dry
1200
10
04/24/23 19:07
BKN
6010D
Copper
17®
mg/Kg - dry
1.20
1
04/22/23 02:28
TJS
6010D
Lead
1.78
mg/Kg - dry
0.721
1
04/22/23 02:28
TJS
6010D
Magnesium
2160
mg/Kg - dry
12.0
1
04/22/23 02:28
TJS
6010D
Mercury
<0.430
mg/Kg - dry
0.430
1
04/20/23 13:10
FDS
7471A
Molybdenum
4.83
mg/Kg - dry
0.600
1
04/22/23 02:28
TJS
6010D
Nickel
1.36
mg/Kg - dry
0.600
1
04/22/23 02:28
TJS
6010D
Potassium
73®
mg/Kg - dry
24.0
1
04/22/23 02:28
TJS
6010D
Selenium
< 12.0
mg/Kg - dry
12.0
10
04/26/23 02:26
BKN
6010D
Sodium
656
mg/Kg - dry
60.1
1
04/22/23 02:28
TJS
6010D
Qualifiers/ DF
Dilution Factor
MQL
Method Quantitation Limit
Definitions

Report Number : 23-108-0184
Lab No : 98379
Sample ID: M
Test
M
2790 Whitten Road, Memphis, TIN 38133
Main 901.213.2400 0 Fax [phone]
www.waypointanalytical.com
0 0 #
74 7*7.TZo7Y.,TA7-74Tf45l
Matrix: Solids
Sampled: 4/17/2023 11:50
Results Units MQL DF Date / Time By Analytical
Analyzed Method
114 mg/Kg - dry 3.00 1 04/22/23 02:28 TIS 6010D
Qualifiers/ DF Dilution Factor MQL Method Quantitation Limit
Definitions
Page 6 of 8

(D 2790 Whitten Road, Memphis, TN 38133
Waypoint, Main 901.213.2400 * Fax [phone]
ANALYTICAL www.waypointanalytical.com
EMMMU= }
Customer Number: 22972
Customer Name: Branch Residuals and Solis LLC
Report Number: 23-108-0184
Shipping Method
Fed Ex US Postal Lab
0 UPS Client Courier
Other
Thermometer ID:
Shipping container/cooler uncompromised?
0 Yes
No
Number of coolers/boxes received
1
Custody seals intact on shipping container/cooler?
Yes
No
0 Not Present
Custody seals intact on sample bottles?
Yes
No
0 Not Present
Chain of Custody (COC) present?
0 Yes
No
COC agrees with sample label(s)?
0 Yes
No
COC properly completed
0 Yes
No
Samples in proper containers?
0 Yes
No
Sample containers intact?
0 Yes
No
Sufficient sample volume for indicated test(s)?
0 Yes
No
All samples received within holding time?
0 Yes
No
Cooler temperature in compliance?
0 Yes
No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
0 Yes
No
Water - Sample containers properly preserved
Yes
No
0 N/A
Water - VOA vials free of headspace
Yes
No
0 N/A
Trip Blanks received with VOAs
Yes
No
0 N/A
Soil VOA method 5035 — compliance criteria met
Yes
No
0 N/A
High concentration container (48 hr)
High concentration pre -weighed (methanol -14 d)
Low concentration nCore samplers (48 hr)
Low cone pre -weighed vials (Sod is -14 d)
Special precautions or instructions included?
Yes
0 No
Date & Time: 04/18/2023 15:09:51
Page 7 of 9

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C6
>
E
-Z 0
I
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z
0
t
At
v
CO
L)
83
C)
C:
E
E
c
m
z M
C)
z'
co Of
CL (N
I
L
X_
Page 8 of 8

Facility:
Marcal Corporation
Source:
Marcal Paper
Location:
Cordova, North Carolina
Contractor:
io-Nomic Services
Type of Analysis:
Industrial
Report No:
me 2023-6
Date Sampled:
5/16/2023
Date Reported:
5/25/2023
Reporting Period:
Jun-2-3
Parameter
%
PPM
EPA
Dry Weight
Monthly Limits
Solids
34.90
Nitrogen (TKN)
0.136
1,360.000
Phosphorus
0.008
77.400
Potassium
0.007
68.800
Sulfate
0.000
Calcium
19600
196,000.000
Magnesium
0.186
1,860.000
Sodium
0.074
736.000
Iron
---
Aluminum
___
1,500.000
Manganese
---
Copper
---
14.600
1,500
Zinc
---
120.000
2,800
Ammonia Nitrogen
0.035
352.000
Nitrate N / Nitrite N
---
28.7000
Cadmium
___
0.2870
39
Chromium
___
1,200
Nickel
___
1.6600
420
Lead
___
2.5100
300
Arsenic
___
1.4300
41
Mercury
___
0.5270
17
Selenium
---
7.1600
100
pH
6.700
Calcium Carbonate Eq. *
23.500
235,000.0000
Organic Nitrogen
0.101
Molybdenum
___
1.84001
75
Chloride
Boron
Available P205

Industrial
Marcal Paper
Cordova, North Carolina
Jun-23
Date Reported: 5/25/2023 Report No: me 2023-6 W
Note All Units in Pounds Per Dry Ton
Macro Nutrients Physical Characteristics
6w.1 9 &1 M-
Secondary Nutrients
% Solids
Secondary Nutrients
% Solids
34.90
pH
6.700
Min Rate
0.400
rur 1 -7 M.,
�Lrj Nft I I
LVj no 0 -T,

2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 Fax [phone]
www.waypointanalytical.com
Mr. Bob Branch
1735 Heckle Blvd
Suite 103-291
Rock Hill, SC, 29732
Ref: Analytical Testing
Lab Report Number: 23-137-0046
Client Project Description: Sludge Testing - 2014-1
Dear Mr. Bob Branch:
Waypoint Analytical, LLC. received sample(s) on 5/17/2023 for the analyses presented in the following report.
N W" OW W 111111"i'I'liffil
1;&41
F-115 M I I rM J no annoralm
4 0 0 0
the samples included in this report.
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 1 of 9

Way
RTICAL
"�.1 f �1
Main 901.213.2400 90I G44M
Nwww.waypointanalytical.coml
State
Program
Lab ID
Expiration Date
Alabama
State Program
40750
02/29/2024
Arkansas
State Program
-0650
02/7/2024
California
State Program
2904
06/30/2023
Florida
State Program - NELAP
E871157
06/30/2023
Georgia
State Program
C044
11/14/2025
Georgia
State Program
0015
06/30/2023
Illinois
State Program - NELAP
200078
10/10/2023
Kentucky
State Program
80215
06/30/2023
Kentucky
State Program
KY90047
12/31/2023
Louisiana
State Program - NELAP
L037
12/31/2023
Louisiana
State Program - NELAP
0015
06/30/2023
Mississippi
State Program
MS
11/14/2025
North Carolina
State Program
47701
07/1/202
North Carolina
State Program
415
12/31/2023
Pennsylvania
State Program - NELAP
6-01
05/31/224
South Carolina
State Program
84002
06/30/2023
Tennessee
State Program
007
11/14/2025
Texas
State Program - NELAP
T107010
0/30/2023
Virginia
State Program
00106
06/30/2023
Virginia
State Program - NELAP
46011
0/1/2023
Page 1 of 1 00001/23-137-0046
Page 2 of

(D 2790 Whitten Road, Memphis, TN 38133
Waypoint. Main 901.213.2400 0 Fax [phone]
ANALYTICAL www.waypointanalytical.com
Sample SummarV Table
Report Number: 23-137-0046
Client Project Description: Sludge Testing - 2014-110
Lab No Client Sample ID Matrix Date Collected Date Received
94919 M Solids 05/16/2023 13:00 05/17/2023

Way nt,(2)
11 PARTICAL
Project: Sludge Testing - 2014-110
Lab Report Number: 23-137-0046
D. 5/25/2023
W41
Main 901.213.2400 0 Fax 901.213.ii
2440
www.waypointanalytical.com
Metals Analysis Method 6010D
Sample 94919 (M)
Analyte: Aluminum
QC Batch No: 1-683237/1-682624
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 94919 (M)
Analyte: Calcium
QC Batch No: L683571/L682624
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 94919 (M)
Analyte: Potassium
QC Batch No: L683237/L682624
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Sample 94919 (M)
Analyte: Selenium
QC Batch No: L683571/L682624
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Sample 94919 (M)
Analyte: Zinc
QC Batch No: L683237/L682624
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Solids Total Mercury Analysis - CVAA Method 7471A
Sample 94919 (M)
Analyte: Mercury
QC Batch No: 1-683393/1-683123
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Anions by Ion Chromatography Method 9056A
Sample 94919 (M)
QC Batch No: 1-683557/1-683362
The sample was diluted due to the nature of the sample matrix. Reporting limits have been adjusted accordingly.
Page 4 of 9

Way int.,(2)
I PARTICAL
Page 5 of 9

Lab mo: 94919
Sample ID: M
Matrix: Solids
Test
Results
Unite
MOIL
DIF
Date /Time
By
Analytical
Analyzed
Method
Neutralizing Value (%CC2)
23.5
%
O.1
1
05/23/2311:58
DxT
AOAC9SS.O1
Moisture
65.1
96
0.010
1
05/33V2316:20
JB
254QG'2011
Ammonia Nitrogen
352
mg/Kg-dry
207
1
05725/33 14:28
]P]
450ONH3E2811
N|trabe(NO3'N)
<28J
mg/Kg-dry
28.7
10
05/22/3323:23
SFO
9056A
N|tdbe(M02-N)
<28.7
mg/Kg 'dry
28.7
10
05/22/2323:23
SR]
9058A
N|trabe+NitMte-N
<28.7
mg/Kg 'dry
28.7
10
05/22/2323:23
9856A
pH
6.7
s.u.
1
05/24V2317:05
CNG
9045D
Total Solids
34.9
9*
0.010
z
05/23/23 18:20
zLS
254OG'2011
Total Kje|dah| Nitrogen
1360
mg/Kg-dry
143
1
05/18/23 13:14
ANH
4500NORGD-2811
Phosphorus
77.4
mg/Kg 'dry
14.3
1
85/20/2307:13
BKN
6810D
Aluminum
1500
mg/Kg 'dry
14.3
1
05/I0/2307:13
BKN
6010D
Arsenic
<1.1]
mg/Kg 'dry
1.43
1
057202307:13
BKN
6010D
Cadmium
«0.287
mg/Kg 'dry
0.287
1
05/20/2307:13
BKN
60100
Calcium
196000
mg/Kg-dry
14300
100
05/22/23 21:11
BKN
6010D
Copper
14.6
mg/Kg-dry
1.43
1
05/202387:13
BKN
6010D
Lead
2,51
mg/Kg-dry
0.859
1
05/38/2307:13
BKN
6018B
Magnesium
1860
mg/Kg 'dry
14.3
1
05/28/23 07:13
BKN
8010D
Mercury
^8.527
mg/Kg 'dry
0.537
1
05/22/23 12:32
F06
7471A
Molybdenum
1,84
mg/Kg-dry
0.716
1
05/20/2307:13
BKN
8018D
Nickel
1,66
mg/Ky-dry
0.716
1
05/20/23 07:13
BKN
68100
Potassium
68.8
mg/Kg-dry
28.7
1
85/20/2307:13
BKN
6010D
Selenium
<7.18
mg/Kg-dry
7.16
S
05/22/2320:35
BKN
6010D
Sodium
736
mg/Kg-dry
71.6
1
85/20/2307:13
BKN
6010Q
Qualifiers/ DF Dilution Factor
Definitions
Page 6 of 5

Report Number: 23-137-0046
Lab No : 94919
Sample ID : IM
uml
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 " Fax [phone]
www.waypointanalytical.com
Sludge Testing - 2014-110
Matrix: Solids
Sampled: 5/16/2023 13:00
Results Units MCIL DF Date / Time By Analytica
Analyzed Methof:-I
120 mg/Kg - dry 3.58 1 05/20/23 07:13 BKN 6010D
Qualifiers/ DF Dilution Factor MQL Method Quantitation Limit
Definitions I

Wayp into�
, Ri TICAL
Main 901.213.2400 * Fax [phone]—Af,
www.waypointanalytical.com
Shipment Receipt Form
Customer Number: 22972
Customer Name: Branch Residuals and Soils LLC
Report Number: 23-137-0046
Shipping Method
Fed Ex US Postal Lab Other
0 UPS Client Courier Thermometer ID: Y1,
Shipping container/cooler uncompromised?
Yes
No
Number of coolers/boxes received
Custody seals intact on shipping container/cooler?
Yes
No
0 Not Present
Custody seals intact on sample bottles?
Yes
No
0 Not Present
Chain of Custody (COC) present?
0 Yes
No
COC agrees with sample label(s)?
0 Yes
No
CC properly completed
Yes
0 No
Samples in proper containers?
0 Yes
No
Sample containers intact?
0 Yes
No
Sufficient sample volume for indicated test(s)?
0 Yes
No
All samples received within holding time?
0 Yes
No
Cooler temperature in compliance?
0 Yes
No
Cooler/Samples arrived at the laboratory on ice.
0 Yes
No
Samples were considered acceptable as cooling
process had begun.
Water - Sample containers properly preserved
Yes
No
0 N/A
Water - VOA vials free of headspace
Yes
No
0 N/A
Trip Blanks received with As
Yes
No
0 N/A
Soil VOA method 5035 ® compliance criteria met
Yes
No
0 N/A
High concentration container (48 hr)
Low concentration EnCore
samplers (48 hr)
High concentration pre -weighed (methanol -14 d)
Low cone pre -weighed vials (Sod is -14 d)
Special precautions or instructions included?
Yes
0 No
Comments:
Signature: Carleen Qualls Date & Time: 05/17/2023 11:58:09

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Facility:
Marcal Corporation
Source:
Marcal Paper
Location:
Cordova, North Carolina
Contractor:
Bio-Nomic Services
Type of Analysis:
Industrial
Report No:
me 2023-7 W
Date Sampled:
6/27/2023
Date Reported:
7/10/2023
Reporting Period:
Jul-23
Parameter
%
PPM
EPA
Dry Weight
Monthly Limits
Solids
32.50
Nitrogen (TKN)
0.137
1,370.000
Phosphorus
0.012
124.000
Potassium
0.010
97.500
Sulfate
0.000
Calcium
18.600
186,000.000
Magnesium
0.203
2,030.000
Sodium
0.088
877.000
Iron
---
Aluminum
---
1,660.000
Manganese
---
Copper
---
14.400
1,500
Zinc
---
92.300
2,800
Ammonia Nitrogen
0.031
308.000
Nitrate N / Nitrite N
---
30.8000
Cadmium
---
0.3080
39
Chromium
---
1,200
Nickel
---
1.2300
420
Lead
---
0.9230
300
Arsenic
---
3.0200
41
Mercury
---
0.5630
17
Selenium
---
1.5400
100
pH
7.600
Calcium Carbonate Eq.
41.700
417,000.0000
Organic Nitrogen
0.106
Molybdenum
---
5.3200
75

Industrial
Marcal Paper
Cordova, North Carolina
Jul-23
Date Reported: 7/10/2023 Report No: me 2023-7 W
Note All Units in Pounds Per Dry Ton
UMMUNMMI W
111
0 �41
Physical Characteristics
% Solids
32.50
pH
7.600
Min Rate
0.400
�411 Cr.) I
0 0 My, F. We I �,
M LVI

Waypoint(b
ANALYTICAL
NEWOW
Mr. Bob Branch
1735 Heckle Blvd
Suite 103-291
Rock Hill, SC, 29732
Ref: Analytical Testing
Lab Report Number: 23-179-0089
Client Project Description: Sludge Testing
Project #2014-110
Dear Mr. Bob B,offranch:
. f- 41 -,.Q1Vfir-9U-L-r1r. .................
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 Fax [phone]
www.waypointanalytical.com
Plillill;1lip
stage (refer to the chain of custody) results apply to the sample as received.
A full list of certifications is available upon request.
A.11101111 "IN 111191,1111111601w, a . , I . . . 4 10 0 4
ligy4r4sumcgi 101rw] mg06241 ly-Alsigisiolling muellwalm 1011611AVE41 V-K4K*1 11411ria ^
4 N Z . .00 0 0 . 0 1 .1 16 0
411011 W wz Z
It: X; at . I I I a T111-1111111 &I'll
Page 1. of 9

IY�"dil
• 0 0
www.waypointanalytical.com
State
Program
Lab ID
Expiration Cate
Alabama
State Program
40750
02/29/2024
Arkansas
State Program
8-060
02/07/2024
California
State Program
290
0/30/2023
Florida
State Program - NELAP
E871157
0/30/2024
Georgia
State Program
C044
11/1/2025
Georgia
State Program
04015
06/30/2024
Illinois
State Program - NELAP
2007
10/10/203
Kentucky
State Program
80215
0/30/2024
Kentucky
State Program
KY90047
12/31/2023
Louisiana
State Program - NELAP
L037
12/31/2023
Louisiana
State Program - NELAP
04015
06/30/2024
Mississippi
State Program
MS
11/14/2025
North Carolina
State Program
47701
07/31/2023
North Carolina
State Program
415
12/31/2023
Pennsylvania
State Program - NELAP
6-03195
05/1/2024
South Carolina
State Program
84002
06/0/202
Tennessee
State Program
0027
11/14/2025
Texas
State Program - NELAP
T107010
09/30/2023
Virginia
State Program
00106
06/30/2024
Virginia
State Program - NELAP
46011
0/14/2023
Page 1 of 1 00001/23-179-0039
Page 2 of 9

Client Project Description: Sludge Testing
Project #2014-110
Lab No Client Sample ID Matrix
94072 M Solids 06/27/2023 13:20 06/28/2023
Page 3 of 9

Way int
1 RTICAL
Project: Sludge Testing
Lab Report Number: 23-179-0089
Date: 7/10/2023
kX4411
Main 901.213.2400 1 Fax [phone]
www.waypointanalytical.com
W-11*411121 F-11 N ZT-11% 0 LVA
Metals Analysis Method 6010D
Sample 94357 (CM SWARIF 23-1)
Analyte: Arsenic
QC Batch No: L691398/1-690494
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Sample 94357 (CM SWARF 23-1)
Analyte: Calcium
QC Batch No: 1-691398/1-690494
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Sample 94357 (CM SWARF 23-1)
Analyte: Cadmium
QC Batch No: 1-691398/1-690494
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Sample 94357 (CM SWARF 23-1)
Analyte: Copper
QC Batch No: 1-691398/1-690494
61,1 Iiiix I r jh� mi rix i ike d Ilicate was outside ualit control acceRtance ran es. A dilution test g 0
K;] 101111 NUO 1VI its 0 IN&NI;1I ILI If r-I 1 IV t.71 ;J .1 K-7A U'rW -Afi*11141to 1[ 17 IL -If& 1011g4m
Sample 94357 (CM SWARF 23-1)
Analyte: Potassium
QC Batch No: 1-691398/1-690494
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Sample 94357 (CM SWARF 23-1)
Analyte: Molybdenum
QC Batch No: 1-691398/1-690494
UR-�M2JWX SX,
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Page 4 of 9

0 (D
Waypoint
-719 IK I Its morarvis as I I n I I I VALOJ 114 Im K;
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 ' Fax [phone]
www.waypointanalytical.com
Sample 94357 (CM SWARF 23-1)
Analyte: Lead
QC Batch No: 1-691398/1-690494
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Sample 94357 (CM SWA 23-1)
Analyte: Selenium
QC Batch No: 1-691398/1-690494
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Page 5 of 9

(2) 2790 Whitten Road, Memphis, TN 38133
Waypoint. Main 91.13.2400 0 Fax [phone]
ANALYTICAL www.waypointanalytical.com
22972
Branch Residuals and Soils LLC Project Sludge Testing
Mr. Bob Branch Report Date 07/10/2023
1735 Heckle Blvd Information : Project #2014-110 Received 06/28/2023
Suite 103-291
Rock Hill , SC 29732
Report Number: 23-179-0089
Lab No : 94072
Sample ID: M
im,
W##OOJJARIZI TJZ T4 2cl M
Matrix: Solids
Sampled: 6/27/2023 13:20
Results Units MOL DF Date / Time By Analytical
Analyzed Method
Neutralizing Value (%CCE)
41.7
%
0.1
1
07/07/23 11:15
DXT
AOAC 955.01
Moisture
67.5
%
0.010
1
07/03/23 18:26
KDO
2540G-2011
Ammonia Nitrogen
<308
mg/Kg - dry
308
1
07/06/23 15:00
JPJ
4500NH3C-2011
Nitrate (NO3-N)
<30A
mg/Kg - dry
30.8
10
07/10/23 09:11
NFP
9056A
Nitrite (NO2-N)
<30.8
mg/Kg - dry
30.8
10
07/10/23 09:11
NFP
9056A
Nitrate+Nitrite-N
<30.8
mg/Kg - dry
30.8
10
07/10/23 09:11
9056A
pH
7®
SM.
1
07/05/23 11:48
CNB
9045D
Total Solids
32.5
%
0.010
1
07/03/23 18:26
KDO
2540G-2011
Total Kjeldahl Nitrogen
1370
mg/Kg - dry
422
1
07/03/23 16:40
AN H 4500NORGD-2011
Phosphorus
124
mg/Kg - dry
15.4
1
07/03/23 19:45
BKN
6010D
Aluminum
1660
mg/Kg - dry
15.4
1
07103/23 19:45
BKN
6010D
Arsenic
3®2
mg/Kg - dry
1.54
1
07/03/23 19:45
BKN
6010D
Cadmium
<0.308
mg/Kg - dry
0308
1
07/03/23 19:45
BKN
6010D
Calcium
186000
mg/Kg - dry
3080
20
07/05/23 17:59
BKN
6010D
Copper
14.4
mg/Kg - dry
1.54
1
07/03/23 19:45
BKN
6010D
Lead
<0.923
mg/Kg - dry
0.923
1
07/03/23 19:45
BKN
6010D
Magnesium
2030
mg/Kg - dry
15.4
1
07/03/23 19:45
BKN
6010D
Mercury
<0.563
mg/Kg - dry
0.563
1
06/30/23 11:06
FDS
7471A
Molybdenum
5.32
mg/Kg - dry
0.769
1
07/03/23 19:45
BKN
6010D
Nickel
1.23
mg/Kg - dry
0.769
1
07/03/23 19:45
BKN
6010D
Potassium
7®
mg/Kg - dry
30.8
1
07/03/23 19:45
BKN
6010D
Selenium
<1.54
mg/Kg - dry
1.54
1
07/03/23 19:45
BKN
6010D
Sodium
877
mg/Kg - dry
76.9
1
07/03/23 19:45
BKN
6010D
Qualifiers/ DF
Dilution Factor
MQL Method Quantitation Limit
Definitions
Page 6 of 9

(2) 2790 Whitten Road, Memphis, TN 38133
Waypoint. Main 1.21.200 0 Fax [phone]
ANALYTICAL www.waypointanalytical.com
22972
Branch Residuals and Soils LLC Project Sludge Testing
Mr. Bob Branch Report Date 07/10/2023
1735 Heckle Blvd Information : Project #2014-110 Received 06/28/2023
Suite 103-291
Rock Hill , SC 29732
Xeport Number: 23-179-0089 REPORT OFANAL YSIS
Lab No : 94072 Matrix: Solids
Sample ID : M Sampled: 6/27/2023 13:20
Test Results Units MOL DF Date / Time By Analytical
Analyzed Method
Zinc 92.3 mg/Kg - dry 3.85 1 07/03/23 19:45 BKN 6010D
i[malifiers/ DF Dilution Factor
Definitions
0
11age 7 of 9

Main 901.213.2400 0 Fax [phone]
wwwmaypontanay ca.com
Customer Number: 22972 1
Customer Name: Branch Residuals and Soils L
Report Number: 23-179-0089 1
Fed Ex US Postal Lab
Other
0 UPS Client Courier
Thermometer ID:
Shipping container/cooler uncompromised?
0 Yes
No
Number of coolers/boxes received
1
Custody seals intact on shipping container/cooler?
Yes
No
0 Not Present
Custody seals intact on sample bottles?
Yes
No
0 Not Present
Chain of Custody (COC) present?
0 Yes
No
COC agrees with sample label(s)?
0 Yes
No
COC properly completed
0 Yes
No
Samples in proper containers?
0 Yes
No
Sample containers intact?
0 Yes
No
Sufficient sample volume for indicated test(s)?
0 Yes
No
All samples received within holding time?
0 Yes
No
Cooler temperature in compliance?
0 Yes
No
Cooler/Samples arrived at the laboratory on ice.
0 Yes
No
Samples were considered acceptable as cooling
process had begun.
Water - Sample containers properly preserved
Yes
No
411 N/A
Water - VOA vials free of headspace
Yes
No
40 N/A
Trip Blanks received with VOAs
Yes
No
40 N/A
Soil VOA method 5035 ® compliance criteria met
Yes
No
0 N/A
High concentration container (48 hr)
Low concentration EnCore samplers (48 hr)
High concentration pre -weighed (methanol -14 d)
Low conc pre -weighed vials (Sod is -14 d)
Special precautions or instructions included?
Yes
0 No
MMMMGE=F,M7MM
-071177�j �,*X
1�11111M

SP!IOS%
qd'nopo'sv
.......................... . . . .....

Marcal Corporation
arcal Paper
Cordova, North Carolina
io-Nomic Services
Industrial
me 2023-8
8/1/2023
8/10/2023
Solids
Potassium
Sulfate
Calcium
Sodium
Iron
Aluminum
Manganese
Ammonia Nitrogen
Nitrate N / Nitrite N
Cadmium
Chromium
Nickel
Lead
Arsenic
Selenium
Calcium Carbonate Eq.
Orizanic Nitrogen
Molybdenum
Chloride
Boron
Available P2O5
415.000
107.0000
0.4150
EPA
Monthly Limits
75

Industrial
Marcal Paper
Cordova, North Carolina
Aug-23
Date Reported: 8/10/2023 Report No: me 2023-8 W
Note All Units in Pounds Per Dry Ton
1UTVrq71Wxmr". ml,
Secondary Nutrients
tool$111
Physical Characteristics
% Solids 24.10
pH 8.800
Min Rate 0.400
Physical Characteristics
% Solids 24.10
pH 8.800
Min Rate 0.400
ON m 01 IT,

Waypoint(2)
ANALYTICAL
Mr. Bob Branch
1735 Heckle Blvd
Suite 103-291
Rock Hill, SC, 29732
Ref: Analytical Testing
Lab Report Number: 23-214-0099
Client Project Description: Cordova, NC
Project #2014-110
Dear Mr. Bob Branch:
2790 Whitten Road, Memphis, TIN 38133
Main 901.213.2400 0 Fax [phone]
www.waypointanalytical.com
ETA
b-Igg LZRI 1z] V.] Stang I lZRIM 1g] lagc Role mtels VJE V-gll I I $14iVA1424 11;Ivy I III *J rR;&2r-14gd
CUUMIGallullb [11dy Ue nelware -&I'dildule lur PdranTe lAr-Leir
A full list of certifications is available upon request.
NO 0 . . 11 ^ - N A I , •1 0 0 0 ^ . . . I - I .
A.11111111110 111WORMINIVIT4,
1111,711 1�1 bf!m1:11, npp�ii the samples included in this report.
§M=
4�1 A

Main ' t14N 1' Fax S I -2440
www.waypointanalytical.com
State
Program
Lab ID
Expiration Date
Alabama
State Program
40750
02/29/2024
Arkansas
State Program
8-0650
02/7/04
California
State Program
2904
0/0/04
Florida
State Program - NELAP
E871157
0/0/4
Georgia
State Program
C044
11/1/205
Georgia
State Program
04015
06/30/204
Illinois
State Program - NELAP
200078
10/1/03
Kentucky
State Program
80215
06/30/204
Kentucky
State Program
KY90047
1/31/02
Louisiana
State Program - NELAP
LA037
12/31/2023
Louisiana
State Program - NELAP
04015
06/30/2024
Mississippi
State Program
MS
11/14/5
North Carolina
State Program
47701
07/1/2024
North Carolina
State Program
415
12/1/23
Pennsylvania
State Program - NELAP
68-03195
0/1/024
South Carolina
State Program
84002
06/0/203
Tennessee
State Program
02027
11/14/2025
Texas
State Program - NELAP
T104704180
09/30/2023
Virginia
State Program
00106
0/0/204
Virginia
State Program - NELAP
460181
09/14/03
Page 1 of 1 00001,123-214-0099
Page 2 of 1.0

W.(b
•
oint
ANALYTICAL
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 Fax [phone]
www.waypointanalytical.com
Sample Summary Table
Report Number: 23-214-0099
Client Project Description: Cordova, NC
Project 2014-110
Lab No Client Sample ID Matrix Date Collected Date Received
89066 MA Solids 08/01/202313:17 08/02/2023
89067 M Solids 08/01/202313:25 08/02/2023

Waypointo
ANALYTICAL
Client: Branch Residuals and Soils LLC
Project: Cordova, NC
Lab Report Number: 23-214-0099
Date: 8/10/2023
2790 Whiften Road, Memphis, TN 38133
Main gV2.2z3.Z4V0"Fax goz.2z3.2440
www^waypmimunna|ydcatcom
CASE NARRATIVE
Metals Analysis Method 6010D
Sample 89326
Anakyte:Aluminum
OCBatch No: LGS737i/LG3G7O7
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. Nomatrix interference imsuspected.
Sample8932
Anokda:Cokcium
C\CBatch No:LGQ7OQ7/LGQG7O7
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. Nomatrix interference iesuspected.
Sample 89326
Analyte: Magnesium
QC Batch No: 1-697097/1-696707
-A tel,
Anions by Ion Chromatography Method 9056A
Sample 88223 (East POTW)
QC Batch No: 1-697499/1-697460
Sample 89066 (MA)
QC Batch No: 1-697499/1-697460
ease 4 of 10

0 (D
Wawoint.
ANALY I K►
-
22972
Branch Residuals and Soils LLC
Mr. Bob Branch
1735 Heckle Blvd
Cuite 103-291
Rock Hill , SC 29732
Main 901.213.2400 0 Fax [phone]
www.waypointanalytical.com
Project Cordova, NC
Information : Project #2014-110
Report Number: 23-214-0099 REPoR r OF A NA L Y515
Lab No : 89066 Matrix: Solids
Sample ID: MA Sampled: 8/1/2023 13:17
Test Results Units MOIL DF Date / Time By Analytical
Analyzed Method
Total Organic Carbon
10.0
%
0.05
1
08/10/23 11:30
AAB
WALK -BLACK
Neutralizing Value (%CCE)
45®
%
0.1
1
08/06/23 14:45
DXT
AOAC 955.01
Moisture
7S.9
%
0.010
1
08/02/23 17:53
KDO
254OG-2011
Ammonia Nitrogen
<415
mg/Kg - dry
415
1
08/09/23 11:00
JPJ
4500NH3C-2011
Nitrate (NO3-N)
< 107
mg/Kg - dry
107
10
08/09/23 10:07
SDS
9056A
Nitrite (NO2-N)
< 107
mg/Kg - dry
107
10
08/09/23 10:07
SDS
9056A
Nitrate+ Nitrite-N
< 107
mg/Kg - dry
107
10
08/09/23 10:07
9056A
PH
8.8
S.U.
1
08/03/23 15:25
CNB
9045D
Total Solids
24.1
%
0.010
1
08/02/23 17:53
KDO
254OG-2011
Total Kjeldahl Nitrogen
4090
mg/Kg - dry
1660
1
08/04/23 15:28
ANH
4500N0RGD-2011
Phosphorus
228
mg/Kg - dry
20.7
1
08/04/23 18:40
TIS
6010D
Aluminum
2640
mg/Kg - dry
20.7
1
08/04/23 18:40
TIS
6010D
Arsenic
<2.07
mg/Kg - dry
2.07
1
08/04/23 18:40
TIS
6010D
Cadmium
<0.415
mg/Kg - dry
0.415
1
08/04/23 18:40
TIS
6010D
Calcium
68500
mg/Kg - dry
1040
5
08/07/23 13:19
TIS
6010D
Copper
24.8
mg/Kg - dry
2.07
1
08/04/23 18:40
TIS
6010D
Lead
4.69
mg/Kg - dry
1.24
1
08/04/23 18:40
TIS
6010D
Magnesium
1470
mg/Kg - dry
20.7
1
08/04/23 18:40
TIS
6010D
Mercury
<0.793
mg/Kg - dry
0.793
1
08/04/23 10:45
FDS
7471A
Molybdenum
®7
mg/Kg - dry
1.04
1
08/04/23 18:40
TIS
6010D
Nickel
2®4
mg/Kg - dry
1.04
1
08/04/23 18:40
TIS
6010D
Potassium
isi
mg/Kg - dry
41.5
1
08/04/23 18:40
TIS
6010D
Selenium
<2.07
mg/Kg - dry
2.07
1
08/04/23 18:40
TIS
6010D
!Lualifiers/ DF Dilution Factor
Definitions
I
Page 5 of 10

V r
Yamooint(I
ANALYTICAL
22972
Branch Residuals and Soils LLC
Mr. Bob Branch
1735 Heckle Blvd
Suite 103-291
Rock Hill , SC 29732
Report Number: 23-214-0099
Lab No : 89066
Sample ID: MA
fim
N
Main 901.213.2400 0 Fax [phone]
www.waypointanalytical.com
Project Cordova, NC
Information : Project #2014-110
W4,70 ��f W11,61`4
1050 mg/Kg - dry 104
65.6 mg/Kg - dry 5.19
0 0 R.
Matrix: Solids
Sampled: 8/1/2023 13:17
DF Date / Time By Analytical
Analyzed Method
1 08/04/23 18:40 US 60101
1 08/04/23 1840 TIS 60101F,
Qualifiers/ DF Dilution Factor MQL Method Quantitation Limit
Definitions
Page 6 of 10

Waypoint.
ANALYTICAL
22972 1
Main 901.213.2400 0 Fax [phone]
www.waypointanalytical.com
Branch Residuals and Soils LLC project Cordova, NC
Mr. Bob Branch
1735 Heckle Blvd Information : Project #2014-110
Suite 103-291
Rock Hill , SC 29732
port Number :23-214-0099 REPORT OFANAL YSIS
Lab No : 89067 Matrix: Solids
Sample ID: M Sampled: 8/1/2023 13:25
Test Results Units MOL DF Date / Time By Analytical
Analyzed Method
Total Organic Carbon
11.1
%
0.05
1
08/10/23 11:30
AAB
WALK -BLACK
Neutralizing Value (%CCE)
22.5
%
0.1
1
08/06/23 14:45
DXT
AOAC 955.01
Moisture
61.5
%
0.010
1
08/02/23 17:53
KDO
2540G-2011
Ammonia Nitrogen
<260
mg/Kg - dry
260
1
08/09/23 11:00
JPJ
4500NH3C-2011
Nitrate (NO3-N)
<26.0
mg/Kg - dry
26.0
10
08/07/23 17:05
SDS
9056A
Nitrite (NO2-N)
<26.0
mg/Kg - dry
26.0
10
08/07/23 17:05
SDS
9056A
Nitrate+ Nitrite-N
<26.0
mg/Kg - dry
26.0
10
08/07/23 17:05
9056A
pH
7®
S.U.
1
08/03/23 15:25
CNB
9045D
Total Solids
38.5
%
0.010
1
08/02/23 17:53
KDO
2540G-2011
Total Kjeldahl Nitrogen
Isso
mg/Kg - dry
979
1
08/04/23 15:31
ANH
4500NORGD-2011
Phosphorus
11S
mg/Kg - dry
13.0
1
08/04/23 18:45
TIS
6010D
Aluminum
1960
mg/Kg - dry
13.0
1
08/04123 18:45
TJS
6010D
Arsenic
1.97
mg/Kg - dry
1.30
1
08/04/23 18:45
TIS
6010D
Cadmium
<0.260
mg/Kg - dry
0.260
1
08/04/23 18:45
TIS
6010D
Calcium
185000
mg/Kg - dry
1300
10
08/07/23 13:25
TIS
6010D
Copper
18.7
mg/Kg - dry
1.30
1
08/04/23 18:45
TIS
6010D
Lead
0.831
mg/Kg - dry
0379
1
08/04/23 18:45
TIS
6010D
Magnesium
IL900
mg/Kg - dry
13.0
1
08104/23 18:45
TIS
6010D
Mercury
<0.444
mg/Kg - dry
0.444
1
08/04/23 10:46
FDS
7471A
Molybdenum
4.42
mg/Kg - dry
0.649
1
08/04/23 18:45
TIS
6010D
Nickel
1.26
mg/Kg - dry
0.649
1
08/04/23 18:45
TIS
6010D
Potassium
64.7
mg/Kg - dry
26.0
1
08/04/23 18:45
TIS
6010D
Selenium
< 1.30
mg/Kg - dry
1.30
1
08/04/23 18:45
TIS
6010D
Qualifiers/ DF
Dilution Factor
MQL Method Quantitation Limit
Definitions
Page 7 of :1.0

(2) 2790 Whitten Road, Memphis, TN 38133
Waypoint. Main 901.21.2400 0 Fax [phone]
ANALYTICAL www.waypointanalytical.com
22972
Branch Residuals and Soils LLC Project Cordova, NC
Mr. Bob Branch Report Date 08/10/2023
1735 Heckle Blvd Information : Project #2014-110 Received 08/02/2023
Suite 103-291
Rock Hill , SC 29732
Report Number: 23-214-0099
Lab No : 89067
Sample ID: M
km
IN
Matrix: Solids
Sampled: 8/1/2023 13:25
Results Units MOL
DF Date / Time By
Analytical
Analyzed
Method
979 mg/Kg - dry 64.9
1 08/04/23 18:45 TIS
6010D
87.0 mg/Kg - dry 3.25
1 08/04/23 18:45 TIS
6010D
Qualifiers/ DF Dilution Factor MQL Method Quantitation Limit
DefiTIUOTS

0 0* 1
VAI g VAI WA I
Customer Number: 22972
Customer Name: Branch Residuals and Solis LILC
Report Number: 23-214-0099
MA9
Main 901.213.2400 * Fax [phone]
www.waypointanalytical.com
Fed Ex US Postal Lab Other : I
0 UPS Client Courier Thermometer ID: 1'3­5
Shipping container/cooler uncompromised?
Yes
No
Number of coolers/boxes received
1"
Custody seals intact on shipping container/cooler?
Yes
No 0 Not Present
Custody seals intact on sample bottles?
Yes
No 0 Not Present
Chain of Custody (COC) present?
0 Yes
No
COC agrees with sample label(s)?
0 Yes
No
COC properly completed
0 Yes
No
Samples in proper containers?
0 Yes
No
Sample containers intact?
0 Yes
No
Sufficient sample volume for indicated test(s)?
0 Yes
No
All samples received within holding time?
0 Yes
No
Cooler temperature in compliance?
0 Yes
No
Cooler/Samples arrived at the laboratory on ice.
0 Yes
No
Samples were considered acceptable as cooling
process had begun.
Water - Sample containers properly preserved
Yes No 0 N/A
Water - VOA vials free of headspace
Yes No 0 N/A
Trip Blanks received with VOAs
Yes No 0 N/A
Soil VOA method 5035 — compliance criteria met
Yes No 0 N/A
High concentration container (48 hr)
Low concentration EnCore samplers (48 hr)
High concentration pre -weighed (methanol -14 d)
Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included?
Yes 0 No
NMM

m
0
U)
at A
ti
sp!los%
s�
14-W, R
I
sjau!ejuo:) jo jaqwnN
r,
0 u
2
c m
CL
I
I
m
i
�
a
BS
CodM�
Z
W
'@
cc
Z
w
E

Facility:
Marcal Corporation
Source:
Marcal Paper
Location:
Cordova, North Carolina
Contractor:
Bio-Nomic Services
Type of Analysis:
Industrial
Report No:
me 2023-9 W
Date Sampled:
9/12/2023
Date Reported:
9/25/2023
Reporting Period:
Sep-23
Parameter
%
PPM
EPA
Dry Weight
Monthly Limits
Solids
35.70
Nitrogen (TKN)
0.303
3,030.000
Phosphorus
0.020
196.000
Potassium
0.012
122.000
Sulfate
0.000
Calcium
3.030
30,300.000
Magnesium
0.102
1,020.000
Sodium
0.079
790.000
Iron
---
Aluminum
---
2,250.000
Manganese
---
Copper
---
22.900
1,500
Zinc
---
48.200
2,800
Ammonia Nitrogen
0.031
311.000
Nitrate N / Nitrite N
---
28.0000
Cadmium
---
0.2800
39
Chromium
---
1,200
Nickel
---
2.4600
420
Lead
---
3.8100
300
Arsenic
---
1.4000
41
Mercury
---
0.5240
17
Selenium
---
1.4000
100
pH
7.100
Calcium Carbonate Eq.
28.900
289,000.0000
Organic Nitrogen
0.272
Molybdenum
0.7000
75

Industrial
Marcal Paper
Cordova, North Carolina
Sep-23
Date Reported: 9/25/2023 Report No: me 2023-9 W
Note All Units in Pounds Per Dry Ton
1UTT.W70Wmrjf- ml,
qlz
�W.V111
Physical Characteristics
% Solids
Physical Characteristics
% Solids
35.70
pH
7.100
Min Rate
0.400
13r-T M
moril"Iffiff- �11

0 P 0 1
, zyff�"WA N
ch
*�MM2W
Mr. Bob Branch
173�5 Heckle Blvd
it
Suite 103-291
Rock Hill, SC, 29732
'Nef: Analytical Testing
Lab Report Number: 23-256-0067
Client Project Description: Marcal Cordova, NC
Project #2014-110
2790 Whitten Road, Memphis, TIN 38133
Main 901.213.2400 0 Fax [phone]
www.waypointanalytical.com
Dear Mr. Bob Branch:
Waypoint Analytical, LLC. received sample(s) on 9/13/2023 for the analyses presented in the following report.
LMM=rls 11IN3, OU MGM -.27affMMMOr paraTneier&,_J;r
A full list of certifications is available upon request.
14.1111411111"N 19"'Ing-Inou"
1411-7116VIIII41 rlim IIIOJ [oil
I U, 4 111111IFTI ITITIVITIM11111111 11!11� 1� ; nmlln'mr'-'M� M"
§M=
•I'd11
liamIzA - -
-V#IrAm T-F
I pr;wj
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
e 4
Elf
" P4
Page 1 oE 8

Main �1 Mf full, Fax f11 44►
9II
www.waypointanalytical.com
State
Program
Lab ID
Expiration Date
Alabama
State Program
40750
0/9/024
Arkansas
State Program
8-0650
02/7/2024
California
State Program
2904
0/30/2024
Florida
State Program - NELAP
E871157
06/30/2024
Georgia
State Program
C044
11/1/205
Georgia
State Program
04015
0/0/2024
Illinois
State Program - NELAP
20007
10/31/224
Kentucky
State Program
80215
0/30/2024
Kentucky
State Program
KY90047
12/1/202
Louisiana
State Program - NELAP
LA037
12/31/02
Louisiana
State Program - NELAP
04015
0/30/24
Mississippi
State Program
MS
11/14/2025
North Carolina
State Program
47701
07/31/24
North Carolina
State Program
415
1/31/2023
Pennsylvania
State Program - NELAP
68-03195
05/31/2024
South Carolina
State Program
84002
06/30/2023
Tennessee
State Program
02027
11/1/05
Texas
State Program - NELAP
T10704180
0/30/2023
Virginia
State Program
00106
/3/024
Virginia
State Program - NELAP
460181
0/14/2024
Page 1 of 1 00001/23-256-0067
Page ge 2 e'.>:f 8

2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 1 Fax [phone]
www.waypointanalytical.com
Sample Summary Table
Report Number: 23-256-0067
Client Project Description: Marcal Cordova, NC
Project #2014-110
Lab No Client Sample ID Matrix Date Collected Date Received
81777 M Solids 09/12/2023 12:40 09/13/2023
Page 3 of 8

Waypointo
at
Lwa- nT%"TN
Project: Marcal Cordova, NC
Lab Report Number: 23-256-0067
D. 9/25/2023
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 1 Fax [phone]
www.waypointanalytical.com
&�,►I --. -. �-- �
Metals Analysis
Sample 81456 (#5)
Analyte: Aluminum
QC Batch No: 1-704590/1-704238
'Legur --wilmer rilklor-g-1wk w I I I L*I;A b
Sample 81456 (#5)
Analyte: Calcium
QC Batch No: 1-704590/1-704238
AROW"Op- WIN-
LIAP 92 1011 Lai I a I Me 1V 1 a 10 0 IV Mcr4v ILO I I N 111 V'=* I a 14 K 0 1 1r. 0 . I
Sample 81456 (#5)
Analyte: Potassium
QC Batch No: 1-704947/1-704238
ww'9144ii-"W"i, V, W, IN411"Op- WNW- Ai" 189,
Sample 81456 (#5)
Analyte: Sodium
QC Batch No: 1-704590/1-704238
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Sample 81456 (#5)
Analyte: Phosphorus
QC Batch No: 1-704590/1-704238
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution te
was performed and passed quality control acceptance ranges. No matrix interference is suspected. I
Page 4 of B

W a N 0 (2)
avwloint.
ANALYTIC
22972
Branch Residuals and Soils LLC
Mr. Bob Branch
1735 Heckle Blvd
iuite 103-291
Rock Hill , SC 29732
Report Number :23-256-0067
w.-Loam, An'
Main 901.213.2400 0 Fax 901.213.244f
www.waypointanalytical.com
Project Marcal Cordova, NC
Information : Project #2014-110
M 7-oT-TZP7Y-,TTT4Tf45l
Lab No : 81777 Matrix: Solids
Sample ID: M Sampled: 9/12/2023 12:40
Test Results Units MOL DF Date / Time By Analytical
Analyzed Method
Neutralizing Value (%CCE)
28.9
%
0.1
1
09/22/23 14:26
DXT
AOAC 955.01
Moisture
64.3
%
0.010
1
09/14/23 15:12
CAH
2540G-2011
Ammonia Nitrogen
311
mg/Kg - dry
280
1
09/22/23 12:40
JPJ
4500NH3C-2011
Nitrate (NO3-N)
<28.0
mg/Kg - dry
28.0
10
09/14/23 20:16
SDS
9056A
Nitrite (NO2-N)
<28.0
mg/Kg - dry
28.0
10
09/14/23 20:16
SDS
9056A
Nitrate+ N itrite-N
<28.0
mg/Kg - dry
28.0
10
09/14/23 20:16
9056A
pH
7.1
S.U.
1
09/15/23 14:49
CNB
9045D
Total Solids
35.7
%
0.010
1
09/14/23 15:12
CAH
2540G-2011
Total Kjeldahl Nitrogen
3030
mg/Kg - dry
849
1
09/15/23 14:22
ANH 4500NORGD-2011
Phosphorus
196
mg/Kg - dry
14.0
1
09/15/23 03:38
BKN
6010D
Aluminum
2250
mg/Kg - dry
14.0
1
09/15/23 03:38
BKN
6010D
Arsenic
< 1.40
mg/Kg - dry
1.40
1
09/15/23 03:38
BKN
6010D
Cadmium
<0.280
mg/Kg - dry
0.280
1
09/15/23 03:38
BKN
6010D
Calcium
30300
mg/Kg - dry
700
5
09/18/23 15:07
ITR
6010D
Copper
22®
mg/Kg - dry
1.40
1
09/15/23 03:38
BKN
6010D
Lead
3.81
mg/Kg - dry
0.840
1
09/15/23 03:38
BKN
6010D
Magnesium
1020
mg/Kg - dry
14.0
1
09/15/23 03:38
BKN
6010D
Mercury
<0.524
mg/Kg - dry
0.524
1
09/15/23 11:15
MRE
7471A
Molybdenum
<0.700
mg/Kg - dry
0.700
1
09/15/23 22:56
BKN
6010D
Nickel
2®
mg/Kg - dry
0.700
1
09/15/23 03:38
BKN
6010D
Potassium
122
mg/Kg - dry
28.0
1
09/15/23 22:56
BKN
6010D
Selenium
< 1.40
mg/Kg - dry
1.40
1
09/15/23 03:38
BKN
6010D
Sodium
790
mg/Kg - dry
70.0
1
09/15/23 03:38
BKN
6010D
Qualifiers/ DF
Dilution Factor
MQL Method Quantitation Limit
Definitions
Page 5 of 5

(2) 2790 Whitten Road, Memphis, TN 38133
Waypoint. Main 91.213.2400 0 Fax [phone]
ANALYTICAL www.waypointanalytical.com
22972
Branch Residuals and Soils LLC Project Marcal Cordova, NC
Mr. Bob Branch Report Date 09/25/2023
1735 Heckle Blvd Information : Project #2014-110 Received 09/13/2023
Suite 103-291
Rock Hill , SC 29732
Report Number: 23-256-0067
Lab No : 81777
Sample ID : M
mm
Jualifiers/ DF Dilution Factor
Definitions
0
48.2 mg/Kg - dry 3.50
Matrix: Solids
Sampled: 9/12/2023 12:40
XF Date / Time By Analytical
Analyzed Method
&i w
Page G of 8

(2) 2790 Whitten Road, Memphis, TN 381
Waypoint, Main 901.213.2400 0 Fax [phone]
ANALYTICAL www.waypointanalytical.clo
MMMUMM=-
Customer Number: 22972
Customer Name: Branch Residuals and Soils LLC
Report Number: 23-256-0067
Shipping Method
Fed Ex US Postal Lab
0 UPS Client Courier
Other
Thermometer ID:
�1
Shipping container/cooler uncompromised?
0 Yes
No
Number of coolers/boxes received
I
Custody seals intact on shipping container/cooler?
Yes
No
0 Not Present
Custody seals intact on sample bottles?
Yes
No
0 Not Present
Chain of Custody (COC) present?
0 Yes
No
COC agrees with sample label(s)?
0 Yes
No
COC properly completed
0 Yes
No
Samples in proper containers?
40 Yes
No
Sample containers intact?
0 Yes
No
Sufficient sample volume for indicated test(s)?
0 Yes
No
All samples received within holding time?
0 Yes
No
Cooler temperature in compliance?
0 Yes
No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
0 Yes
No
Water - Sample containers properly preserved
0 Yes
No
N/A
Water - VOA vials free of headspace
Yes
No
0 N/A
Trip Blanks received with VOAs
Yes
No
0 N/A
Soil VOA method 5035 — compliance criteria met
Yes
No
0 N/A
High concentration container (48 hr)
High concentration pre -weighed (methanol -14 d)
Low concentration Enor e samplers (48 hr)
Low cone pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included?
Yes
0 No
I I 5
Signature: Makayla Weaver Date & Time: 09/13/2023

E E
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Page
8
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8

Facility:
Marcal Corporation
Source:
Marcal Paper
Location:
Cordova, North Carolina
Contractor:
Bio-Nomic Services
Type of Analysis:
Industrial
Report No:
me 2023-10 W
Date Sampled:
10/3/2023
Date Reported:
10/8/2023
Reporting Period:
Oct-23
Parameter
%
PPM
Dry Weight
Solids
29.10
Nitrogen (TKN)
0.409
4,090.000
Phosphorus
0.027
270.000
Potassium
0.019
187.000
Sulfate
0.000
Calcium
4.540
45,400.000
Magnesium
0.154
1,540.000
Sodium
0.098
979.000
Iron
---
Aluminum
---
2,940.000
Manganese
---
Copper
---
32.400
Zinc
---
58.100
Ammonia Nitrogen
0.034
344.000
Nitrate N / Nitrite N
---
34.4000
Cadmium
---
0.3440
Chromium
---
Nickel
---
3.0300
Lead
---
5.5700
Arsenic
---
1.7200
Mercury
---
0.5770
Selenium
---
1.7200
pH
6.600
Calcium Carbonate Eq.
9.900
99,000.0000
Organic Nitrogen
0.375
Molybdenum
---
1.4700
Pon
EPA
Monthly Limits
an
9M
IN

Industrial
Marcal Paper
Cordova, North Carolina
Oct-23
Date Reported: 10/8/2023 Report No: me 2023-10 W
Note All Units in Pounds Per Dry Ton
lurrim0wommr. ml,
rs Wa
Physical Characteristics
% Solids
29.10
pH
6.600
Min Rate
0.400
lurf-T m�'
Emm"111
MOTION=

Waypoint(b
ANALYTICAL
Mr. Bob Branch
1735 Heckle Blvd
Suite 103-291
Rock Hill, SC, 29732
Ref: Analytical Testing
Lab Report Number: 23-277-0125
Client Project Description: Marcal Cordova, NC
Project #2014-110
Dear ffir. Bob Branch:
nmr=
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 Fax [phone]
www.waypointanalytical,cam
stage (refer to the chain of custody) results apply to the sample as received.
acureultailull 15 11UL req`11tRn_OLAPV1LGBnLe_
certifications may De neia/are avaAaDie T r parameters, w e
A full list of certifications is available upon re•uest.
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only t�
the samples included in this report.
01 M.•
-
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
1 1"'U
b P0,
�IIIIIIIIIIM

Waypointo
ANALYTICAL
2790 Whitten Road, Memphis, TN 3133
Main 901.213.2400 0 Fax [phone]
www.waypointanalytical.com
�. .I i .1�111 I 1 11 1 MKOALUMa3am
State
Program
Lab ID
Expiration Date
Alabama
State Program
40750
0/2/4
Arkansas
State Program
88-0650
0/07/024
California
State Program
2904
0/0/024
Florida
State Program - NELAP
E871157
0/0/04
Georgia
State Program
C044
11/1/025
Georgia
State Program
04015
06/30/024
Illinois
State Program - NELAP
200078
10/1/204
Kentucky
State Program
80215
0/0/024
Kentucky
State Program
KY90047
1/31/023
Louisiana
State Program - NELAP
LA037
1/1/2023
Louisiana
State Program - NELAP
04015
0/30/04
Mississippi
State Program
MS
11/14/02
North Carolina
State Program
47701
07/31/04
North Carolina
State Program
415
1/31/03
Pennsylvania
State Program - NELAP
68-03195
0/31/2024
South Carolina
State Program
84002
0/0/024
Tennessee
State Program
02027
11/1/205
Texas
State Program - NELAP
T104704180
09/30/2024
Virginia
State Program
00106
06/30/2024
Virginia
State Program - NELAP
460181
09/14/2024
Page 1 of 1 00001 /23-277-0125
Page 2 of

Client Project Description: Marcal Cordova, NC
Project #2014-110
Lab No Client Sample ID Matrix Date Collected Date Received
98313 M Solids 10/03/2023 13:25 10/04/2023
Page 3 of 9

0
Project: Marcal Cordova, NC
Lab Report Number: 23-277-0125
D. 10/18/2023
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 ' Fax [phone]
www.waypointanalytical.com
CaF�*k' F-11 N XI% 11 LN
Metals Analysis Method 6010D
Sample 98565
Analyte: Aluminum
QO Batch No: 1-709473/1-708892
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 98565
Analyte: Calcium
QC Batch No: 1-709473/1-708892
W-6 iiv Vilutil -1 tpqt
W M-09
Sample 98565
Analyte: Potassium
QC Batch No: 1-709473/1-708892
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Sample 98565
Analyte: Potassium
QC Batch No: 1-71002408892
licite �was outside ualit control acce4tance ranies. dilution test
61 AAIW'W"- wiiwil -16;w wiww � i.
Ver. 62 GrA I LO I I a ONIO Jr. I Rom It, 61;rAe lull n I I I VAOL41 III M a; M - 0 . 2 ' . 1 4
Sample 98565
Analyte: Magnesium
QC Batch No: 1-709473/1-708892
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 98565
Analyte: Sodium
QC Batch No: 1-709473/1-708892
�11'g i nges. dilution test 141LO]IN -0 1 14�RJCJW L LOA 11 M14 1 P29 I I It-7111A7 L-71 I Lft;M F-JIM I &191�11"uls H
Sample 98565
Analyte: Phosphorus
QC Batch No: 1-709731/1-708892
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Solids Total Mercury Analysis - CVAA Method 7471A
Sample 97716 (Annual Sludge)
Analyte: Mercury
�IlllllWl

WaypRint(2)
A ALYTICAL
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 * Fax [phone]
www.waypointanalytical.com
QC Batch No: 1-709569/1-709290
ity control acceptance •- A ••
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Anions by Ion Chromatography Method 9056A
• 98313 (M)
QC Batch No: 1-709346/1-709244
The sample was diluted due to the nature • the sample matrix. Reporting limits have •' adjusted accordingly.
Sample •..
QC Batch No: 1-709346/1-709244
The • was diluted • to the nature • the sample matrix. Reporting limits have •- adjusted accordingly.
Page 5 of 9

(2) 2790 Whitten Road, Memphis, TN 38133
Waypoint. Main 901.213.2400 0 Fax [phone]
ANALYTICAL www.waypointanalytical.com
22972
Branch Residuals and Soils LLC Project Marcal Cordova, NC
Mr. Bob Branch Report Date 10/18/2023
1735 Heckle Blvd Information : Project #2014-110 Received 10/04/2023
Suite 103-291
Rock Hill , SC 29732
Report Number: 23-277-0125 REPORT OFANAL YSIS
Lab No : 98313 Matrix: Solids
Sample ID: M Sampled: 10/3/2023 13:25
Test Results Units MOL DF Date / Time By Analytical
Analyzed Method
Neutralizing Value (%CCE)
9.9
%
0.1
1
10/11/23 14:31
DXT
AOAC 955.01
Moisture
70.9
%
0,010
1
10/06/23 16:00
CAH
2540G-2011
Ammonia Nitrogen
<344
mg/Kg - dry
344
1
10/18/23 14:37
JPJ
4500NH3C-2011
Nitrate (NO3-N)
<34.4
mg/Kg - dry
34.4
10
10/06/23 15:08
HMQ
9056A
Nitrite (NO2-N)
<34.4
mg/Kg - dry
34.4
10
10/06/23 15:08
HMQ
9056A
Nitrate+ Nitrlte-N
<34.4
mg/Kg - dry
34.4
10
10/06/23 15:08
9056A
pH
6.6
SM.
1
10/06/23 16:07
CNB
9045D
Total Solids
29.1
%
0.010
1
10/06/23 16:00
CAH
2540G-2011
Total Kjeldahl Nitrogen
4090
mg/Kg - dry
1260
1
10/06/23 12:03
ANH
4500NORGD-2011
Phosphorus
270
mg/Kg - dry
17.2
1
10/06/23 23:56
TJS
6010D
Aluminum
2940
mg/Kg - dry
17.2
1
10/06/23 23:56
BKN
6010D
Arsenic
< 1.72
mg/Kg - dry
1.72
1
10/06/23 23:56
BKN
6010D
Cadmium
<0.344
mg/Kg - dry
0.344
1
10/06/23 23:56
BKN
6010D
Calcium
45400
mg/Kg - dry
859
5
10/09/23 14:07
TIS
6010D
Copper
2®
mg/Kg - dry
132
1
10/06/23 23:56
BKN
6010D
Lead
5.57
mg/Kg - dry
1.03
1
10/06/23 23:56
BKN
6010D
Magnesium
1540
mg/Kg - dry
17.2
1
10/06/23 23:56
BKN
6010D
Mercury
<0,577
mg/Kg - dry
0.577
1
10/09/23 11:52
MRE
7471A
Molybdenum
1.47
mg/Kg - dry
0.859
1
10/06/23 23:56
BKN
6010D
Nickel
3.03
mg/Kg - dry
0.859
1
10/06/23 23:56
BKN
6010D
Potassium
187
mg/Kg - dry
34.4
1
10/06/23 23:56
BKN
6010D
Selenium
< 1.72
mg/Kg - dry
1.72
1
10/06/23 23:56
BKN
6010D
Sodium
979
mg/Kg - dry
85.9
1
10/06/23 23:56
BKN
6010D
Qualifiers/ DF Dilution Factor
Definitions
L�MTIW�.
Page 5 of 9

(0 2790 Whitten Road, Memphis, TN 38133
Waypoint. Main 91.21.200 0 Fax [phone]
ANALYTICAL www.waypointanalytical.com
22972
Branch Residuals and Soils LLC Project Marcal Cordova, NC
Mr. Bob Branch Report Date 10/18/2023
1735 Heckle Blvd Information : Project #2014-110 Received 10/04/2023
Suite 103-291
Rock Hill , SC 29732
Report Number: 23-277-0125
Lab No : 98313
Sample ID: M
LMI
M Mi
Matrix: Solids
Sampled: 10/3/2023 13:2S
Results Units MOL DF Date / Time By Analytical
Analyzed Method
58.1 my/Kq - dry 4.30 1 10/06/23 23:56 BKN 6010D
Page '7 of 9

Wayp Rint(b
►TICAL
Customer Number: 22972
Customer Name: Branch Residuals and Solis LILC
Report Number: 23-277-0125
Mu
Main 901.213.2400 * Fax 9ate 1.213.2440
www.waypointanalytical.com
MT.-IMML=
Fed Ex US Postal Lab
Other :
I
0 UPS Client Courier
Thermometer :I
1
Shipping container/cooler uncompromised?
* Yes
No
Number of coolers/boxes received
1
Custody seals intact on shipping container/cooler?
Yes
No
0 Not Present
Custody seals intact on sample bottles?
Yes
No
0 Not Present
Chain of Custody (COC) present?
0 Yes
No
COC agrees with sample label(s)?
0 Yes
No
COC properly completed
0 Yes
No
Samples in proper containers?
0 Yes
No
Sample containers intact?
0 Yes
No
Sufficient sample volume for indicated test(s)?
0 Yes
No
All samples received within holding time?
0 Yes
No
Cooler temperature in compliance?
0 Yes
No
Cooler/Samples arrived at the laboratory on ice.
0 Yes
No
Samples were considered acceptable as cooling
process had begun.
Water - Sample containers properly preserved
Yes
No
0 N/A
Water - VOA vials free of headspace
Yes
No
0 N/A
Trip Blanks received with VOAs
Yes
No
0 N/A
Soil VOA method 5035 — compliance criteria met
Yes
No
0 N/A
High concentration container (48 hr)
Low concentration EnCore samplers (48 hr)
High concentration pre -weighed (methanol -14 d)
Low conc pre -weighed vials (Sod is - 14 d)
Special precautions or instructions included?
Yes
0 No
I
MI�Ml

Solids
rotassium
Sulfate
Calcium
Magnesiun
Sodium
Iron
Aluminum
Ammonia Nitrogen
Nitrate N / Nitrite N
Cadmium
Chromium
Nickel
Lead
Selenium
pH
Calcium Carbonate
®reanlc Nitrogen
Chloride
Boron
Available P205
Marcal Corporation
Marcal Paper
Cordova, North Carolina
io-Nonuc Services
Industrial
me 2023-11
11/8/2023
11/21/2023
Nov-23
% PP
ry Weight
87,000.0000
1.1200
EPA
Monthly Limits
75

Industrial
Marcal Paper
Cordova, North Carolina
Nov-23
Date Reported: 11/21/2023 Report No: me 2023-11 W
Note All Units in Pounds Per Dry Ton
Macro Nutrients Physical Characteristics
111
% Solids
29.00
pH
7.300
Min Rate
0.400
10777T

Waypoint(b
ANALYTICAL
11/21/2023
Branch Residuals and Soils LLC
Mr. Bob Branch
1735 Heckle Blvd
Suite 103-291
Rock Hill, SC, 29732
Ref: Analytical Testing
Lab Report Number: 23-313-0153
Client Project Description: Marcal Cordova, NC
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 Fax [phone]
www.waypointanalytical.com
Dear Mr. Bob Branch:
Waypoint Analytical, LLC. received sample(s) on 11/9/2023 for the analyses presented in the following report.
UMTfM"cT= May OU MOZIU-MRAdum 097,el
A full list of certifications is available upon request.
the samples included in this report.
•0
IjUMEMNITA 0 ,
Page 2. of 8

*5 �r
Main 'li 4Mf 0 Fax [phone]
www.waypointanalytical.com
State
Program
Lab ID
Expiration Date
Alabama
State Program
40750
02/2/2024
Arkansas
State Program
8-0650
0/07/2024
California
State Program
2904
0/30/2024
Florida
State Program - NELAP
E71157
0/30/024
Georgia
State Program
C044
11/1/2025
Georgia
State Program
04015
0/30/2024
Illinois
State Program - NELAP
200078
10/31/224
Kentucky
State Program
80215
06/30/2024
Kentucky
State Program
KY90047
1/31/023
Louisiana
State Program - NELAP
LA037
1/31/202
Louisiana
State Program - NELAP
04015
06/0/4
Mississippi
State Program
MS
11/14/2025
North Carolina
State Program
47701
07/1/2024
North Carolina
State Program
415
12/31/202
Pennsylvania
State Program - NELAP
68-03195
05/1/2024
South Carolina
State Program
84002
06/30/202
Tennessee
State Program
02027
11/14/22
Texas
State Program - NELAP
T104704180
09/0/024
Virginia
State Program
00106
0/30/024
Virginia
State Program - NELAP
46011
0/1/2024
Page 1 of 1 00001 23-313-0153
Page 2 cff 6

0 (2)
Waypoint,
ANALYTICAL
�1—
Client Project Description:
Lab No Client Sample ID
89319 M
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 Fax [phone]
www.waypointanalytical.com
Sample Summary Table
23-313-0153
Marcal Cordova, NC
Matrix
Solids
=?-yon-
11/08/2023 12:30
lJuTTZ-T1T-T=-
11/09/2023

Waypoint(2)
ANALYTICAL
lot
Project: Marcal Cordova, NC
Lab Report Number: 23-313-0153
D. 11/21/2023
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 Fax 901.213.244D
www.waypointanalytical.com
CASE NARRATIVE
Metals Analysis Method 6010D
Sample 63921 (4)
Analyte: Aluminum
QC Batch No: 1-717129/1-716429
T—XP--n?tdx-%fte 2 11
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Anions by Ion Chromatography Method 9056A
Sample 89319 (M)
QC Batch No: 1-717814/1-717576
The saMDle was diluted due to the nature of the samDle matrix. ReDorting limits have been adiusted accordiaqj)�.
Sample 90680 (B-02)
QC Batch No: 1-717814/1-717576
T�e sangle

2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 1 Fax [phone]
www.waypointanalytical.com
Z"M- FCOTO
Report Number : 23-313-0153 REPoRrOFANALYSIS
Lab No : 89319 Matrix: Solids
Sample ID : M Sampled: 11/8/2023 12:30
Test Results Units MOIL DF Date / Time By Analytical
Analyzed Method
Neutralizing Value (%CCE)
8.7
%
0.1
1
11/21/23 09:58
DXT
AOAC 955.01
Moisture
71.0
%
0.010
1
11/10/23 16:14
CAH
2540G-2011
Ammonia Nitrogen
< 345
mg/Kg ® dry
345
1
11/16/23 10:48
JPJ
4500NH3C-2011
Nitrate (NO3-N)
<34.5
mg/Kg ® dry
34.5
10
11/16/23 12:58
HMQ
9056A
Nitrite (NO2-N)
<34,5
mg/Kg ® dry
34.5
10
11/16/23 12:58
HMQ
9056A
Nitrate+ N itrite-N
<34.5
mg/Kg ® dry
34.5
10
11/16/23 12:58
9056A
pH
7.3
SM.
1
11/14/23 17:00
CN13
9045D
Total Solids
29.0
%
0.010
1
11/10/23 16:14
CAH
2540G-2011
Total Kjeldahl Nitrogen
3170
mg/Kg ® dry
1180
1
11/14/23 13:50
ANH
4500NORGD-2011
Phosphorus
233
mg/Kg ® dry
17.2
1
11/14/23 18:56
BKN
6010D
Aluminum
3860
mg/Kg ® dry
17.2
1
11114/23 18:56
BKN
6010D
Arsenic
<1.72
mg/Kg ® dry
1.72
1
11114/23 18:56
BKN
6010D
Cadmium
<0.345
mg/Kg ® dry
0.345
1
11/14/23 18:56
BKN
6010D
Calcium
30700
mg/Kg ® dry
172
1
11/14/23 18:56
BKN
6010D
Copper
23.0
mg/Kg ® dry
1.72
1
11/14/23 18:56
BKN
6010D
Lead
4.86
mg/Kg ® dry
1.03
1
11/14/23 18:56
BKN
6010D
Magnesium
1140
mg/Kg ® dry
17.2
1
11/14/23 18:56
BKN
6010D
Mercury
<0.631
mg/Kg ® dry
0.631
1
11/13/23 11:14
FDS
7471A
Molybdenum
1.12
mg/Kg ® dry
0.862
1
11/14/23 18:56
BKN
6010D
Nickel
3.17
mg/Kg ® dry
0.862
1
11/14/23 18:56
BKN
6010D
Potassium
160
mg/Kg ® dry
34.5
1
11/14/23 18:56
BKN
6010D
Selenium
<1.72
mg/Kg ® dry
1.72
1
11/14/23 18:56
BKN
6010D
Sodium
1030
mg/Kg ® dry
86.2
1
11/14/23 18:56
BKN
6010D
Qualifiers/ DF
Dilution Factor
MQL Method Quantitation Limit
Definitions
Page S of 8

Way *nt.(I)
PANALYTICAL
22972
Branch Residuals and Soils LLC Project
Mr. Bob Branch
1735 Heckle Blvd Information
Suite 103-291
Rock Hill , SC 29732
Report Number: 23-313-0153
Lab No : 89319
Sample ID : M
Test
Main 901.213.2400 0 Fax [phone]
www.waypointanalytical.com
ORTWITITOWWR
r-T4-1#T-TZPT—Z-,TTT4Y3Ti
Matrix: Solids
Sampled: 11/8/2023 12:30
Results Units MOL DF Date / Time By Analytical
Analyzed Method
52.1 mg/Kg - dry 4.31 1 11/14/23 18:56 BKN 6010D
Qualifiers/ DF Dilution Factor MQL Method Quantitation Limit
Definitions I
Pa.<.3e 6 of 8

2790 Whitten Road, Memphis, TN 381
WaypointO Main 901.213.2400 0 Fax [phone]
ANALYTICAL www.waypointanalytical.clo
1_0 , =0MMUM
Customer Number: 22972
Customer Name: Branch Residuals and Solis LLC
Report Number: 23-313-0153
Shipping Method
Fed Ex US Postal Lab
40 UPS Client Courier
Other
Thermometer ID:
Shipping container/cooler uncompromised?
40 Yes
No
Number of coolers/boxes received
1
Custody seals intact on shipping container/cooler?
Yes
No
40 Not Present
Custody seals intact on sample bottles?
Yes
No
0 Not Present
Chain of Custody (COC) present?
0 Yes
No
COC agrees with sample label(s)?
0 Yes
No
COC properly completed
0 Yes
No
Samples in proper containers?
0 Yes
No
Sample containers intact?
0 Yes
No
Sufficient sample volume for indicated test(s)?
0 Yes
No
All samples received within holding time?
0 Yes
No
Cooler temperature in compliance?
40 Yes
No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
0 Yes
No
Water - Sample containers properly preserved
Yes
No
0 N/A
Water - VOA vials free of headspace
Yes
No
0 N/A
Trip Blanks received with VOAs
Yes
No
0 N/A
Soil VOA method 5035 — compliance criteria met
Yes
No
0 N/A
High concentration container (48 hr)
High concentration pre -weighed (methanol -14 d)
Low concentration Enor e samplers (48 hr)
Low conc pre -weighed vials (Sod is -14 d)
Special precautions or instructions included?
Comments:
Yes
0 No
Signature: Makayla Weaver Date & Time: 11/09/2023 15:42:56

m
c
-----
-------
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Page 8, of 8

Facility:
Marcal Corporation
Source:
Marcal Paper
Location:
Cordova, North Carolina
Contractor:
io-Nomic Services
Type of Analysis:
Industrial
Report No:
me 2023-12
Date Sampled:
12/5/2023
Date Reported:
12/18/2023
Reporting Period:
Dec-23
Parameter
%
PPM
EPA
Dry Weight
Monthly Limits
Solids
37.70
Nitrogen (TKN)
0.167
1,670.000
Phosphorus
0.006
61.300
Potassium
0.008
79.600
Sulfate
0.000
Calcium
19.000
190,000.000
Magnesium
0.206
2,060.000
Sodium
0.091
912.000
Iron
---
Aluminum
---
1,890.000
Manganese
---
Copper
---
20.900
1,500
Zinc
---
115.000
2,800
Ammonia Nitrogen
0.027
265.000
Nitrate N / Nitrite N
---
10.6000
Cadmium
---
1.3300
39
Chromium
---
1,200
Nickel
___
0.8220
420
Lead
---
0.7950
300
Arsenic
---
3.5300
41
Mercury
---
0.4880
17
Selenium
___
13.3000
100
pH
7.800
Calcium Carbonate Eq. *
50.700
507,000.0000
Organic Nitrogen
0.141
Molybdenum
---
6.6300
75
Chloride
Boron
Available P2O5

Industrial
Marcal Paper
Cordova, North Carolina
Dec-23
Date Reported: 12/18/2023 Report No: me 2023-12 W
Note All Units in Pounds Per Dry Ton
lurrWroluff ofM
WIN
Physical Characteristics
% Solids
Physical Characteristics
% Solids
37.70
pH
7.800
Min Rate
0.400
Or fM 17,
174 M MIT, MI

Waypointo
ANALYTICAL
Ref: Analytical Testing
Lab Report Number: 23-340-0151
Client Project Description: Cordova, NC
Project # 2014-110
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 Fax [phone]
www.waypointanalytical.com
Dear Mr. Bob Branch:
Waypoint Analytical, LLC. received sample(s) on 12/6/2023 for the analyses presented in the following report.
1100101
mvp r-z'JrAr4 MILS24 1r-KOJ Ig 11 OR*] K91IM911 Q--11 I R-2; 14141 kTA14z11VJRV1 HIC 174;&m IVIPM
LAMMUdL1441b Indy se nout/are STRASTIM-3-71artvar- aMr
A full list of certifications is available upon request.
.4.1 111111 111.0 low 911 will I - .0 0 . 0
1111fill or"llawliellho I&NIINWIPIN11
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
0 'S a 00
&&MI'm
ITIVIVIP 111711MII§511111� 1111 11
I10
Page :11. of 9

Waypdint.(2)
ANALYTICAL
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 ° Fax [phone]
www.waypointanalytical.com
State
Program
Lab ID
Expiration Date
Alabama
State Program
40750
0/9/24
Arkansas
State Program
8-0650
0/07/04
California
State Program
2904
06/0/204
Florida
State Program - NELAP
E871157
06/30/2024
Georgia
State Program
C044
11/1/205
Georgia
State Program
04015
06/30/2024
Illinois
State Program - NELAP
200078
10/31/04
Kentucky
State Program
80215
06/30/04
Kentucky
State Program
KY90047
12/31/23
Louisiana
State Program - NELAP
LA037
1/31/03
Louisiana
State Program - NELAP
04015
0/30/4
Mississippi
State Program
MS
11/14/202
North Carolina
State Program
47701
07/1/04
North Carolina
State Program
415
1/1/2023
Pennsylvania
State Program - NELAP
68-03195
05/1/04
South Carolina
State Program
84002
06/0/04
Tennessee
State Program
02027
11/14/025
Texas
State Program - NELAP
T104704180
09/30/2024
Virginia
State Program
00106
06/30/02
Virginia
State Program - NELAP
460181
0/1/202
Page 1 of 1 00001 r23-340-0151

(D
2790 Whitten Road, Memphis, TN 38133
Waypoint,Main 901.213.2400 1 Fax [phone]
ANALYTICAL www.waypointanalytical.com
Sample Summary Table
Report Number: 23-30-0151
Client Project Description: Cordova, NC
Project # 2014-110
Lab No Client Sample ID Matrix Date Collected Date Received
88384 M Solids 12/05/202313:23 12/06/2023
Page 3 of 9

0 D
Waypoint
ANALYTICAL
Project: Cordova, NC
Lab Report Number: 23-340-0151
D. 12/18/2023
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 1 Fax [phone]
www.waypointanalytical.com
CASE NARRATIVE
Metals Analysis Method 6010D
Sample 90089(SB-6@10-15)
Analyte: Aluminum
QC Batch No: 1-721810/1-7211234
I ri _11. A dilution test
Al alwaiw� "111
kyr��s fig I m I I I L7-11 1p 11 tom OvE;1-.r-
Sample 90089(SB-6@10-15)
Analyte: Arsenic
QC Batch No: 1-721612/1-721234
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Sample 88384 (M)
Analyte: Cadmium
QC Batch No: 1-721612/1-721234
This analyte was analyzed at a dilution due to IC interference/matrix interference.
Sample 90089 (SB-6@10-15)
Analyte: Copper
QC Batch No: 1-721612/1-721234
TXe—n2Wx-s�01tR
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 90089(SB-6@10-15)
Analyte: Potassium
QC Batch No: 1-721612/1-7211234
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranpe% A dilution te�l
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 88384 (M)
Analyte: Molybdenum
QC Batch No: 1-721612/1-721234
This analyte was analyzed at a dilution due to I interference/matrix interference.
Sample 90089(SB-6@10-15)
Analyte: Molybdenum
QC Batch No: 1-721612/1-721234
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
. 1 0 - * 10 ; I '. 0 0 1
F-1 MIN pr JM:11 0 0 0
Page 4 of 9

2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400' Fax [phone]
www.waypointanalytical.com
QC Batch No: 1-721612/1-721234
I
LOW"W'619WO i6whIPIA
Sample 90089(SB-6@10-15)
Analyte: Lead
QC Batch No: 1-7216112/1-721234
Sample 88384 (M)
Analyte: Selenium
QC Batch No: 1-721612/1-721234
Sample 90089(SB-6@10-15)
Analyte: Selenium
QC Batch No: 1-721612/1-721234
tXA�ZOZZ-�Z2G VAQUZ
digestion spike was performed and passed quality control acceptance ranges. No matrix interference i
suspected. I
Anions by Ion Chromatography Method 9056A
Sample 88384 (M)
QC Batch No: 1-722888/1-722002
The sample was diluted due to the nature of the sample matrix. Reporting limits have been adjusted accordingly.
Sample 88887
QC Batch No: 1-722888/1-722002
The sample was diluted due to the nature of the sample matrix. Reporting limits have been adjusted accordingly.
Page 5 of 9

Waypoint.
ANALYTICAL
22972 1
Main 901.213.2400 0 Fax [phone]
www.waypointanalytical.com
Branch Residuals and Soils LLC Project Cordova, NC
Mr. Bob Branch
1735 Heckle Blvd Information : Project # 2014-110
Suite 103-291
Rock Hill , SC 29732
Xeport Number: 23-340-0151 REPoRrOFANALYSIS
Lab No : 88384 Matrix: Solids
Sample ID: M Sampled: 12/5/2023 13:23
Test Results Units MOL DF Date / Time By Analytical
Analyzed Method
Neutralizing Value (%CCE)
50.7
%
0.1
1
12/14/23 14:30
DXT
ACAC 955.01
Moisture
2®
%
0.010
1
12/07/23 16:05
CAH
2540G-2011
Ammonia Nitrogen
<265
mg/Kg - dry
265
1
12/14/23 12:23
JPJ
4500NH3C-2011
Nitrate (NO3-N)
< 10.6
mg/Kg - dry
10.6
10
12/12/23 18:28
NFP
9056A
Nitrite (NO2-N)
< 10.6
mg/Kg - dry
10.6
10
12/12/23 18:28
NFP
9056A
Nitrate+Nitrite-N
< 10.6
mg/Kg - dry
10.6
10
12/12/23 18:28
9056A
PH
7®
SM.
1
12/07/23 13:00
RDP
9045D
Total Solids
37.7
%
0.010
1
12/07/23 16:05
CAH
2540G-2011
Total Kjeldahl Nitrogen
1670
mg/Kg - dry
671
1
12/15/23 11:06
AN H 4500NORGD-2011
Phosphorus
61.3
mg/Kg - dry
13.3
1
12/08/23 19:50
TJS
6010D
Aluminum
1890
mg/Kg - dry
13.3
1
12/08/23 19:50
TJS
6010D
Arsenic
3.53
mg/Kg - dry
1.33
1
12/08/23 19:50
TJS
6010D
Cadmium
< 1.33
mg/Kg - dry
1.33
5
12/11/23 21:28
TJS
6010D
Calcium
190000
mg/Kg - dry
1330
10
12/11/23 21:33
TJS
6010D
Copper
20.9
mg/Kg - dry
1.33
1
12/08/23 19:50
TJS
6010D
Lead
<0.795
mg/Kg - dry
0.795
1
12/08/23 19:50
TJS
6010D
Magnesium
2060
mg/Kg - dry
13.3
1
12/08/23 19:50
TJS
6010D
Mercury
<0.488
mg/Kg - dry
0.488
1
12111/23 11:07
FDS
7471A
Molybdenum
< 6.63
mg/Kg - dry
6.63
10
12/11/23 21:33
TJS
6010D
Nickel
0.822
mg/Kg - dry
0.663
1
12/08/23 19:50
TJS
6010D
Potassium
79.6
mg/Kg - dry
26.5
1
12/08/23 19:50
TJS
6010D
Selenium
< 13.3
mg/Kg - dry
13.3
10
12/11/23 21:33
TJS
6010D
Sodium
912
mg/Kg - dry
66.3
1
12/08/23 19:50
TJS
6010D
Qualifiers/ DF
Dilution Factor
MQL Method Quantitation Limit
Definitions
Page 6 of 9

Q) 2790 Whitten Road, Memphis, TN 38133
Waypoint Main 91.213.2400 0 Fax [phone]
ANALYTICAL www.waypointanalytical.com
22972
Branch Residuals and Soils LLC Project Cordova, NC
Mr. Bob Branch Report Date 12/18/2023
1735 Heckle Blvd Information : Project # 2014-110 Received 12/06/2023
Suite 103-291
Rock Hill , SC 29732
Report Number: 23-340-0151
Lab No : 88384
Sample ID: M
On
Io
Matrix: Solids
cri It
Results Units MOL DF Date / Time By Analytical
Analyzed Method
115 mg/Kg - dry 3.32 1 12/08/23 19:50 TIS 6010D
Qualifiers/ DF Dilution Factor MQL Method Quantitation Limit
Definitions
Page 7 of 9

Way int,(D
I PARTICAL
Customer Number: 22972 1
Customer Name: Branch Residuals and Solis L
Report Number: 23-340-0151 1
01VOwt
Main 901.213.2400 * Fax 90MI 1.213.2440
www.waypointanalytical.com
Fed Ex US Postal Lab Other :
0 UPS Client Courier Thermometer ID: 137
Shipping container/cooler uncompromised?
..............
Number of coolers/boxes received
--------- --------- ---------
Custody seals intact on sample bottles?
--------------
Ohainof Custody (COC) present? ...............
COC agrees with sample label(s)?
0 Yes
No
..................................
Yes
No 0 Not Present
Yes
No 0 Not Present
0 Yes
No
do Yes
No
COC properly completed
0 Yes
No
Samples in proper containers?
0 Yes
No
Sample containers intact?
0 Yes
No
Sufficient sample volume for indicated test(s)?
0 Yes
N*
All samples received within holding time?
0 Yes
No
Cooler in compliance?
0 Yes
No
-temperature
Cooler/Samples arrived at the laboratory on ice.
0 Yes
No
Samples were considered acceptable as cooling
process had begun . ...............
Water - Sample containers properly preserved
0 Yes
No N/A
Water - VOA vials free of headspace
Yes
No 0 N/A
Trip Blanks received with VOAs
--------------------------------------------
Yes
No 0 N/A
Soil VOA method 5 035 — compliance criteria met
Yes
No 0 N/A
High concentration container (48 hr)
Low concentration EnCore samplers (48 hr)
High concentration pre -weighed (methanol -14 d)
Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included?
Yes
0 No
I 11TOMMM-F=

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Page 9 of 9

TOXICITY CHARACTERISTICS LEACHING PROCEDURE
(TCLP) ANALYSIS REPORT

Branch p mm W /Bob Branch
Date of Report. Feb 17, 2023
'1735 p....peckl p Blvd Suite '103-2 1
Customer PO M
Rock p..fll SC 2 732
Customer ID: 15060009
ttermtlo n:
Report M 2 23-01553
Project ID: &udge...von Drehle
OL b p mmmp l ID:
ry m rvrvrv. M mm ....................................... -,—
Collect DateMirne Matirix Sampled by
23-03 17 Site: SWdge VD
1/24/2023
12:45 PM SoHdOudgeMe nt
"rest
Method
Results
Date r� My . d
Total Solids
SM 2540 um
4 . %
02/ 212023
hloii°d ne (TCLP)
S -846a 808D um
0.02 rn'n /L
01/26/2 23
I rmdrprn (TCLP)
S -846 8081 um
<0.00 65 m/L
01/26/2 23
p lept clhlor (TCLP)
S -B46 8081 mm
<0,0 05 rrn /L
01126/2023
p...11eptachlor epoxlde (TCLP)
wW-8468081 B
<0. 005n"rm /L
01/26/2-02.3
Und n (TCLP)
SW-846 8081 rm
<0 0005 rn /L
01/ 612023
Methoxychlor° (..p.. LP)
W-846 8081 B
<LR 0 5 rn'n /L
01/26/202.3
Toxaph ru (TCLP)
SM8468081 B
<0.051rrng/L
01/25/2 2.3
2,4,5- P (TCLP)
S W-846 8155 A
<0 ,003 rmm /L
01126/2023
2,4-ID (1i' p...P)
SW 846 8151 A
<0.0 3 umme /L
01/26/2023
1 „4d'.)ichlmmrrmbenze n (TCLP)
SSW-846 8270 E
<OMO rang/L
01/ 7/2 23
2 4 5-TrichloropI"m6?nol (TCLP)
S -846 8270 E
0. S0 nmmq/L.
01/27/2023
2,4,6-1f r'ichlorophenoII (TCLP)
SW-845 8270 E
<0.050 mgIl..
01127/2023
2,4-Dpamptrrmt6lm»u rm ('t..CLP)
S-8468270 E
<0.050 mg/L
01/27/2 2
Cresol (TCLP)
W-846 8270 E
<0.050 umm /L
0112.7/22 23
Hexac oii-o-1 ,3-but dp rn (TO P)
S W..846 8270 E
<0.050 r'rng/L
1/2 7 /2023
p....p 9mllorobenz rn (1" LP)
SW...846 8270 E
<0..050 mg/If....
01 /271202.3
Hexac oro ttm lrm (TCLP)
S -846 8270 E
<0.050 rang/l,
1127/2023
nmm + rp- resom (TCLP)
SW 846 8270 E
<0.050 mg/L
01 /27/2023
Nptrrmtmeriaene ("r(.'LP)
-846 8270 IE
<0.050 rrn /p....
01127/2023
mm- resol(T L)
-8468270E
<'0.05 rmm /L
1/27/2023
Pernt hlorop he nol (r LP)
S -846 8270 IC
<0 250 rrrm /L
01/27/2 23
Pyr6 n (TCLP)
SW-846 8270 E
<0,050 ummg/L
01/27/2023
M-I pclhporoettmylen (T LII)
SW/4r-845Me&II'od54260D
<0.0'tRlg/L.
2/ /2 23
1,2-IDpamtnloro than cr LFI)
S -B46 Method 82600
< 0,01 rvm /L
21 /2023
Benzene (TCLP)
SW..84mm Whod 8; 60D
< 0,01 Nmm /L
2/ /2023

Branch ResiduaWBob Branch
Date of Report: Feb 17, 2023
1735 iecWe BW SUfte 103-291
Customer PO #:
Rock I WI SC 29732
Customer ID: 15060009
Afteomfiorr
Report #: 2023-01563
Project ID: &udge-von DireNe
Carbon Tetracl"mbride (I"GI FI)
SW 846 Meffind 8260D
< 0. 01 rl"Bg/[-
2/9/2023
Chlordbenzene (I CI FI)
SW-1146 Methad 8250D
< 0 01 nign
2/9/2023
Chbroforni (I U .P)
SW-846 Method 8260D
,: 0.01 rngn
2/9/2023
Mefl-,uyp ethyketone (TU
SW-846 Method 8260D
< 0.05 nig/L
2/9/2023
Tetraclhbiroeft�eriie (TCLFI)
SW-846 Method 8260D
< 0.01 rng/I
2/9/2023
Trichbroethylene (TU P)
SW-84h Method 8260D
< 0.01 nig/L.
219/2023
Virtyll Chbride (,rcL..,i,::,)
SW-846 Method 8260D
< 0.01 rngA
2/9/2.,023
RU
SOW 4500 Vq D 2016
Suffide SM 4500 S D
PpSW 845 Method 9045D
Resuft esfirnated, Anyzed out of 15 minutes Wd fume,
rci p Metals
,rO.8 rwnlsec ()1/27/2.023
3.80 rng/kg 01131/2023
0.83 nigA(g 02/01/2023
3.1 UInRS 02/14/2023
Arsenor c ("rCL.JP)
EPA 2007, Rev 4 4, 1994
<1.0 Mgn
01/3012023
Bark= ( rCL.l::))
EPA 200 7, Rev 4 4, 1994
<I.Onng/p
01/3012.023
Cadmium cru P)
EPA 200 7, Rev 44, 1994
< 1.0 rng/p
0,1/30/2.023
0"irorniurn ( FCpP)
EPA 200 7, Rev 4 4, 1994
< 1,0 mgfl
01/30/2023
ead cru FI)
EPA 200 7, Rev 4 4,1994
<1.0 rng/p
01/30/2023
Sepenh..irn ("I"CLP)
EPA 200 7, Rev 4 4, 1994
<1 .0 rng/L
0113012023
Sheii-, (I UP)
EPA 200 7, Rev 4 4� 1994
< 1 . 0 rng/11
01/30/2-023
Mercury crcLP)
. ....... . .
EPA 245.
<0.0002 rng/L
01/27/2023
................... ............................................
Comment:
FReviewed by,
. . ................ ......... . ... . . ...... . . . .... . ... .... . ..............................
—.1'..,..—..—... .. . ................................................ . ....... . .........................
. ..........
....... ��/ ..........

6602VVIindmiUVilay
@N|nn��ton,0K' 2Q405
9I0, 3 g 2 O2 2 3
OienL Oate� '%S� Repo�Number_
R i f
(ES
El
110
*TOcA/obU|esare Pill aiUmoo[ana|ysisandecordcdondhe��nchsheo�
|** Baclleriasamp|esare checkedhorOh|orIII lie aOtimeo[ana|\misand recondcdon11hebenchshee�
C1]l P4M E III �, 5;

I
ME

PATHOGEN AND VECTOR
ATTRACTION REDUCTION FORMS

PATHOGEN REDUCTION AND VECTOR ATTRACTION REDUCTION
The current permit, WQ0039924, does not have vector attraction requirements but does have Class
A requirements for pathogens. These forms are marked to reflect these requirements.

110101111 1 11PI[
Facility Name: Marcal Cordova, LLC WQ Permit Number: WQ0039924
WWTP Name: Cordova Facility NPDES Number: NA
Monitoring Period: From 1/1/2023 To 1/31/2023
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
�60�, Alt. A (time/temp) L] Alt B (Alk Treatment) L1 Alt. C (Prior Testing) 21 1
Alt.D (No Prior Test) L1 Process to Further Reduce Pathogens
IN I 111 11 11 111 1 1 111 1 11 11 11 1 1 11 111 11 1 11 11 111 111 1 11 1
1 111111 1 11 illi�ill�l I ii ��! �11 11 11 �
li 1, 1 l � �� 1111 11 11 U1111011 I MUMMZUOE��
Heat Drving■
Heat Treatment[]
Gamnia_Ray Pasteurization El - -------- -------------------- - ----------
1.31MINEW!,
Stabilization 13 1
robic Digestion 0 :
TIM III MTMPI "Im.
Parameter
I= me
2 x 10 to the MPN
6th power
per gram of CFU
total solids
1000 mpn per gram
of total solid (dry
gArm.'r,",
Pathogen Density
M, ME, MIMI I MY W11
ilmonella bacteria 3 MPN per 4 grams I MPN/ 4
(in lieu of fecal total solid (dry <_ 0.6 NA <_ 0.7
Grams
.
............
..........
..........
..........
..............
.............. ..............
............. ............
)110 ing monitoring data:
ber o um e— Af Frequency— Sample Yt1( Tech -
is
Excee- of Anal Type A-nrpc Ys [ypnal I n;nm-
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed:
Alt. 1 (VS reduction) El Alt. 2 (40-day bench) Alt. 3 (30-day bench) jAlt. 4 (Spec. 0, uptake) U
Alt. 5 (14-Day Aerobic) Alt. 6 (Alk. Stabilization El Alt 7 (Drying - Stable) jAlt. 8 (Drying - Unstable) 0
Alt. 9 (Injection) Alt. 10 (Incorporation) [I No vector attraction reduction alternatives were performed El
CERTIFICATION STATEMENT (please check the appropriate statement)
I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note
if you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Mr. Mitchell Luckie, Systems Engineer ORC
Preparer Name and Title ce or print) Land Applier Name and Title (if applicable) (type or print)
�/_z 2-v- 0
Signature of Preparer* Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF02T(12/2006)

�-1106111K U a 1 1,1111 1, 111, 11, f 11 11111
I- -•111 1� I ►JF�11 111 , 1
Facility Name: Marcal Cordova, LLC WQ Permit Number:
WWTP Name: Cordova Facility NPDES Number:
Monitoring Period: From 2/l/2023 To 2/28/2023
Pathogen Reduction (15A NCAC 02T.1106) - Please indicate level achieved and alternative
Alt. A (time/temp) ■ Alt B (Alk Treatment)LI ....... W.-IIHMI
Alt.D (No Prior Test) El Process to Further Reduce Pathog
----------------
W1 RINW, �7 1+
Heat Drviniz U Heat Treatment
F,
- ----------
Gamma Rav■ Pasteurization 11
Lime Stabilization■
Anaerobic Digestion D
Ti-TWIN lot M.,
Allowable Level =
in Sludge ITWI
1 ♦ - "11 11
WWWO1411 3U=0-vTRM3U=,
-ss-B-only)-indicate-"Pi-ocess to Significantly Reduce_�.
ml�-- ■ Comi)ostirau=6�
FFWW.TTML41 FM '-jY i =so i U M- = (I I L2AULF-IgLoW
Ill Pathogen Density NO -
ONE=
■
Tech-
01mrsm.-M. X�T ,W�
(in lieu of fecal total solid (dry
coliforin)EMMEEMEN
Vector Attraction Reduction (15A NCAC 02T.1107) - Please indicate alternative performed:
Alt. 1 (VS reduction) 11 'Alt. 2 (40-day bench) D Alt. 3 (30-day bench) [I Alt. 4 (Spec. 02 uptake) D
Alt. 5 (14-Day Aerobic) 11 Alt. 6 (Alk. StabilizationD Alt 7 (Drying - Stable) [I Alt. 8 (Drying - Unstable) 0
It. 9 (Injection) El : Alt. 10 (Incorporation) D No vector attraction reduction alternatives were performed Rl
CERTIFICATION STATEMENT (please check the appropriate statement)
I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T.1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note
if you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Preparer Name an T' le e or print) Land Applier Name and Title (if applicable)(type or print)
Signature of Preparer* Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 02T (12/2006)

Facility Name: Marcal Cordova, LLC WQ Permit Number: WQ0039924
WWTP Name: Cordova Facility NPDES Number: NA
Monitoring Period: From 3/l/2023 To 3/31/2023
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A: Alt. A (time/temp) Alt B (Alk Treatment) El Alt. C (Prior Testing) 21
.................... ...........
..................... ...........
....................... I Alt.D (No Prior Test) 0 Process to Further Reduce Pathogens 0
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
'Compost El Heat Drying L1 Heat TreatmentO TheniiophilicL]
.............. ..............
..............
Beta Rav 13 Gamma Rav 11 Pasteurization El
Class B: Wt. (1) Fecal Density El
,pplicable to alternative performed (CE
ie Stabilization L1Air
aerobic Digestion L1
ipplicable to alternative performed
Parameter Allowable Level
in Sludge
Minin
2 x 10 to the MPN
6th power
per gram of CFU
total solids
1000 mpn per gram
of total solid (dry
ITU1.
F.111
imly) indicate "Process to Significantly Reduce Pathogens" -
■Composting D ■
rm's ZZ, 11=0 W41
Pathogen Density
)Ilowing monitoring data:
um5er of Frequency Sample Analyti(
Excee- Tech -
of Analysis Type
&-nrpc I I ninin.
Salmonella bacteria 3 MPN per 4 grams MPN/ 4 EPA
(in lieu of fecal total solid (dry < 0.7 NA < 0.8 Grams 0 Monthly Grab 1682
coliformweight)
Vector Attraction Reduction (15A NCAC 02T.1107) - Please indicate alternative performed:
Alt. 1 (VS reduction) El Alt. 2 (40-day bench) L3 Alt. 3 (30-day bench) Alt. 4 (Spec. 02 uptake) Ll
Alt. 5 (14-Day Aerobic) 13 Alt. 6 (Alk. Stabilization[] Alt 7 (Drying - Stable) El 1Alt. 8 (Drying - Unstable) 0
Alt. 9 (Injection) L1 Alt. 10 (Incorporation) L3 No vector attraction reduction alternatives were performed R1
CERTIFICATION STATEMENT (please check the appropriate statement)
21 1 certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T.1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
L3 "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note
if you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Mr. Mitchell Luckie, Systems Engineer ORC
Preparer Name and Title (type or print) Land Applier Name and Title (if applicable) (type or print)
Signature of Preparer* Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 02T (12/2006)

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Marcal Cordova, LLC WQ Permit Number: WQ0039924
WWTP Name: Cordova Facility NPDES Number: NA
Monitoring Period: From 4/l/2023 To 4/30/2023
Pathogen Reduction (15A NCAC 02T AK
�SIFR Alt. A (time/temp) ---I
N Alt.D (No Prior Test) 0
If aDDlicable to alternative Derformed (ClassJ
■Heat Drying 0
�61 rm;= F.-I Fm all Em 1 valm
If applicable to alternative performed
Lime Stabilization El
Anaerobic Digestion El
If applicable to alternative perforn
2 x 10 to the MPN
6th power
per gram of CFU
total solids
1000 mpn per gram
of total solid (dry
� - Please indicate level achieved and alternative performed:
Alt B (Alk Treatment) L3 Alt. C (Prior Testing) 21_
�11 Process to Further Reduce Pathogens■
tinlv) indicate "Process to Further Reduce Pathogens":
I
Heat TreatmentEl Thermophilic L3
Pasteurization E3
mly) indicate "Process to Significantly Reduce Pathogens":
■Composting E3
Pathogen Density
lete the following monitoring data:
Num er o Frequency I Sample Analyh(
Excee- Tech -
Units of AnalysisType
Salmonella bacteria 3 MPN per 4 grams I MPNI 4 EPA
(in lieu of fecal total solid (dry :5 0.7 NA 0.8 Grams 0 Monthly Grab 1682
colifon-n) weight) I
Vector Attraction Reduction (15A NCAC 02T.1107) - Please indicate alternative performed:
Alt. 1 (VS reduction) 0 Alt. 2 (40-day bench) L3 Alt. 3 (30-day bench) [] Alt. 4 (Spec. 0, uptake)
T. 5 (14-Day Aerobic) Alt. 6 (Alk. Stabilization El Alt 7 (Drying - Stable) El 1Alt. 8 (Drying - Unstable) 0
Alt. 9 (Injection) Alt. 10 (Incorporation) L1 No vector attraction reduction alternatives were performed
CERTIFICATION STATEMENT (please check the appropriate statement)
I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T.1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
13 "1 certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note
if you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Mr. Mitchell Luckie, Systems Engineer ORC
Preparer Name and id (type or print) Land Applier Name and Title (if applicable) (type or print)
Signature of Preparer* Date Signature of Land Applier (if applicable)
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)

ANNUALPATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02TRules)
Facility Name: Marcal Cordova, LLC WQ Permit Number: WQ0039924
TP Name: Cordova Facility NPDES Number: NA
Monitoring Period: From 5/1/2023 To 5/31/2023
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A: Alt. A (time/temp) Alt B (Alk Treatment) Alt. C (Prior Testing) 21
A1t.D (No Prior Test) 0 Process to Further Reduce Pathogens
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost ❑ Heat Drying 0 Heat Treatment❑ Thennophilic❑
Beta Ray 01 Gamina Ray 0 Pasteurization 0 .....
Class : jAlt. (1) Fecal Density Ll I Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Path
Lime Stabilization El Air Drying ❑ Composting 11 jAerobic E
Anaerobic Digestion El
If applicable to alternative performed (Class A or Class ) c4
Parameter Allowable Level Pathogen Density
in Sludge Minimu Geo. MeanlMaxiint
2 x 10 to the MPN
6th power
per gram of CFU
Fecal Coliform total solids
1000 mpn per gram
of total solid (dry
lete the following monitoring data:
Number o Frequency Sample na ytu
Excee- Tech -
Units r1--c Of Analysis Type nimta
Salmonella bacteria 3 MPN per 4 grams
(in lieu of fecal total solid (dry c 0.7 NA C 0.6 GPN/is 0 Monthly Grab 1682
coliform wei ht
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed:
Alt.1 (VS reduction) 11 Alt. 2 (40-day bench) 0 Alt. 3 (30-day bench) Alt. 4 (Spec. O, uptake)
Alt. 5 (14-Day Aerobic) 11 Alt. 6 (Alk. Stabilization[] Alt 7 (Drying - Stable) Ej Alt. 8 (Drying - Unstable)
Alt. 9 (Injection) Ll Alt. 10 (Incorporation) El No vector attraction reduction alternatives were performed 21
CERTIFICATION STATEMENT (please check the appropriate statement)
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note
if you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Mr. Mitchell Luckie, Systems Engineer ORC
rearer Name
p and Title (type or print) Land Applier Name and Title (if applicable)(type or print)
100
Signature of Preparer* Date Signature of Land Applier (if applicable)
R
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)

UWU��,1�10114 '! 1 0 1 "i � li III; i � 113,11 11 [ i 11 11,15 [GRA=',
Facility Name: Marcal Cordova, LLC WQ Permit Number: WQ0039924
WWTP Name: Cordova Facility NPDES Number: NA
Monitoring Period: From 6/1/2023 To 6/30/2023
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A: Alt. A (time/temp) Alt B 'Alk Treatment) U Alt. C (Prior Testing)
Alt. D (No Prior Test) Process to Further Reduce Pathogens
If app,licable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
-compost Heat Drying L1 Heat Treaty Thennophil�� .... ..
Beta Ray 01 Gamma Ray L1 Pasteurization El
Class B: jAlt. (1) Fecal Density D I Alt. (2) Process to Sign
ificantly Reduce Pathogens Li
f applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
,ime Stabilization El Air D!jing D Composting El jAerobic Digestion L1
.......... ...... ... .
.......... .
anaerobic Digestion D
applicable to alternative performed (Class A or Class B) complete the following monitoring data:
Allowable 11 Level Pathoica
gen Density N—um per ot I Frequency Sample Anal
Parameter I in Sludge Exce,- of Type Tech -
in Mean Unitsf Ali
� I �;nllp
= K one
2 x 10 to the MPN
6th power
per gram of CFU
total solids
1000 mpn per gram
of total solid (dry
Salmonella bacteria 3 MPN per 4 grams I N/ 4 � I (in lieu of fecal total solid (dry < 0-7 NA MP0.8 0 Monthly Grab 1682
Gams
Vector Attraction Reduction (15A NCAC 02T.1107) - Please indicate alternative performed:
Alt. 1 (VS reduction) Alt. 2 (40-day bench) Ll Alt. 3 (30-day bench) Alt. 4 (Spec. 0-) uptake) D
Alt. 5 (14-Day Aerobic) El Alt. 6 (Alk. StabilizationEl Alt 7 (Drying - Stable) 1Alt. 8 (Drying Unstable) L1
Alt. 9 (Injection) D Alt. 10 (Incorporation) El No vector attraction reduction alternatives were perfon-ned R1
CERTIFICATION STATEMENT (please check the appropriate statement)
I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T.1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note
if you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Mr. Mitchell Luckie, Systems Engineer ORC
Preparer Name and Title (type or print) Land Applier Name and Title if applicable) (type or print)
e�
'
Signature of Preparer* Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 02T (12/2006)

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Marcal Cordova, LLC WQ Permit Number: WQ0039924
WWTP Name: Cordova Facility NPDES Number: NA
Monitoring Period: From 7/l/2023 To 7/31/2023
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A: Alt. A (time/temp) Alt B (Alk Treatment) El Alt. C (Prior Testing) n%o
.................... .................... Alt.D (No Prior Test) Process to Further Reduce Pathogens
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
.......... ...........
Compost Heat Drying L3 Heat Treatment[] Therniophilic 0
.......... ..........
............. .. ...........
............. .. ...........
Beta Ray 01 Gamma Ray Pasteurization
TMI 0 1,171 UTO 011111
Lime Stabilization 0— CoMp2stiniz El
Anaerobic Digestion 0
111P M11 tM. 11rX MO. IMM! M. M. MIM,
. 0 .0 - . . I- Pathogen Density
2 x 10 to the IMPN
6th power
per gram of CFU
Fecal Coliforin total solids
1000 mpn per gram
of total solid (dry
lete the following monitoring data:
um er o I Frequency Sample na ytic
Excee- Tech -
Units A—Ppcof Analysis I Type .;n—
Salmonella bacteria 3 MPN per 4 grams MPN/ 4 EPA
(in lieu of fecal total solid (dry :5 0.8 NA < 0.8 Grams 0 Monthly Grab 1682
colifbrmweiht�
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed:
Alt. 1 (VS reduction) Alt. 2 (40-day bench) Alt. 3 (30-day bench) Alt. 4 (Spec. 0? uptake)
Alt. 5 (14-Day Aerobic) Alt. 6 (Alk. StabilizationD Alt 7 (Drying - Stable) 1Alt. 8 (Drying - Unstable)
Alt. 9 (Injection) Alt. 10 (Incorporation) 0 No vector attraction reduction alternatives were performed
CERTIFICATION STATEMENT (please check the appropriate statement)
1 certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T.1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note
if you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Mr. Mitchell Luckie, Systems Engineer ORC
Preparer Name and Tith�jtype (jr pi�mt) Land Applier Name and Title (if applicable) (type or print)
Signature of Preparer* Date Signature of Land Applier (if applicable)
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
M11 I.
1-.4120A-.4 IVA man-vallyA KI Eam

Facility Name: Marcal Cordova, LLC
WWTP Name: Cordova Facility
M1nit1rin2 Period: From 8/1/2023
Pathogen Reduction (15A NCAC 02T.11Ti
Alt. A (time/temp) 11 1
Alt.D (No Prior Test)■
Heat Drying
WQ Permit Number: WQ0039924
NPDES Number: NA
To 8/31/2023
i - Please indicate level achieved and alternative performed:
Alt B (Alk Treatment) U I Alt. C (Prior Testing)
Process to Further Reduce Pathogens
)nlv) indicate "Process to Further Reduce Pathogens":
Heat Treatment[] Thennophilic 0
Pasteurization
�OWM',=Alt. (1) Fecal Density D W.04WOPA111, %4W4n=- :m 0 -
Lime Stabilization
Anaerobic Digestion El
I. MM tmo -11 - 01WI (;a a
Pathogen Density
Lwow
2 x 10 to the IMPN
6th power
per gram of CFU
Fecal Coliform total solids
1000 mpn per gram
of total solid (dry
dmonella bacteria 3 MPN per 4 grams I MPN/ 4
(in lieu of fecal total solid (dry 5 0.6 NA < 0.7
I Grams
M=
fflowing monitoring data:
amber ot Frequency SampleA —na- Wi
Excee- Tech -
of Analysis Type
rlpnrpq I I ninup
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed:
Alt. 1 (VS reduction) Alt. 2 (40-day bench) Alt. 3 (30-day bench) jAlt. 4 (Spec. 0, uptake)
t—
Alt. 5 (14-Day Aerobic) Alt. 6 (Alk. StabilizationEl Alt 7 (Drying - Stable) JAIL 8 (Drying - Unstable)
Alt. 9 (Injection) Alt. 10 (Incorporation) El No vector attraction reduction alternatives were performed
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note
if you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Mr.Mitchell Luckie, Systems Engineer ORC
Preparer Name and Title (type,W . 0 Land Applier Name and Title (if applicable) (type or print)
......... ..
Signature of Preparer* Date Signature of Land Applier (if applicable)
IM
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)

Facility Name: Marcal Cordova, LLC
TP Name: Cordova Facility
Monitoring Period: From 9/l/2023
Pathogen Reduction (15A NCAC 02T .110E
Class A: Alt. A (time/temp)
A1t.D (No Prior Test)
If applicable to alternative performed (Class A
Compost Heat Drying
Beta Ray DI Gamma Rav
WQ Permit Number: WQ0039924
NPDES Number: NA
1 r 9/30/2023
I - Please indicate level achieved and alternative pe
Alt B (Alk Treatment) Alt. C (Prior Testing)
Process to Further Reduce Pathogens
)nh) indicate "Process to Further Reduce Pathogens":
Heat Treatment[] ThermophilicC
Pasteurization El
Class : jAlt. (1) Fecal Density ❑ I Alt. (2) Process to Signifi
If applicable to alternative performed (Class B only) indicate "Process to'
Lime Stabilization 11 1 Air Drying ❑ 1 Como(
rea:
I
n❑
Anaerobic Digestion El
............
If applicable to alternative performed (Class A or Class ) complete the following monitoring data:
Allowable Level Pathogen Density um er o Frequency Sample Analytic
Parameter Excee- Tech -
in Sludge inimu Geo. Mean aximu Units of Analysis Type
rienrPc niniv-
2 x 10 to the MPN
6th power
per gram of CFU
Fecal Coliform total solids
1000 mpn per gram
of total solid (dry
fly Reduce Pathogens
ificantly Reduce Path
❑ lAerobic E
Salmonella bacteria 3 MPN per 4 grams
(in lieu of fecal total solid (dry C 0.7 NA C 1.0 Grams 0 Monthly Grab 1682
coliform) wei ht
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed:
Alt.1 (VS reduction) Alt. 2 (40-day bench) Ll Alt. 3 (30-day bench) Alt. 4 (Spec. O, uptake)
Alt. 5 (14-Day Aerobic) Alt. 6 (Alk. Stabilization❑ Alt 7 (Drying - Stable) Alt. 8 (Drying - Unstable)
Alt. 9 (Injection) Alt. 10 (Incorporation) No vector attraction reduction alternatives were performed I)
CERTIFICATION STATEMENT (please check the appropriate statement)
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02 .1107 have not been met." (Please note
if you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Mr.Mitchell Luckie, Systems Engineer ORC
Preparer Name and Title (type or pr. t) Land Applier Name and Title (if applicable)(type or print)
Z� l/
Signature of Preparer* Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)

113111!011K - 1 l�i 110-loilririIlN� 1,111'' 111 11 1:111 111 1, 1 �I I JIRI�I��' - - 1 - I 1 1 11, 1' 1 111 1111 D
Facility Name: Marcal Cordova, LLC WQ Permit Number:
WWTP Name: Cordova Facility NPDES Number:
Monitoring Period: From 10/1/2023 To 10/31/2023
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative
Class A: Alt. A (time/temp) U Alt B (Alk Treatment) El Alt. C (Prior Testis
...................
................... Alt.D (No Prior Test) Process to Further Reduce Patiiop
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogen
Compost Heat Drying 11 Heat Treatment[] Therniophill
Beta Ray El Gamma Ray 0 Pasteurization
Class B: ]Alt. (:1:)::Fecal Density LJ I Alt (2) Process to Significan
tly y Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Path
Lime Stabilization El Air Drying El I Composting 0 jAerobic D
Anaerobic Digestion U
gollims! pt,
-fierformed■
If applicable to alternative performed (Class A or Class B) complete the following monitoring data:
Allowable Level Pathogen Density un`i er 0 Frequency SaI Analytic
Parameter --- Excee- Tech -
in Sludge m�Geo. MearilmaximutrIl Units� , "P of Analysis Type
I r17F-nf-Pc ninny
2 x 10 to the IMPN
6th power
per gram of CFU
Fecal Coliform. total solids L
1000 mpn per gram
of total solid (dry
Salmonella bacteria 3 MPN per 4 grams (in lieu of fecal total solid (dry < 0.9 NA <_ 1.0 MPN/0 Monthly Grab 1682
coliform) weights
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed:
Alt. 1 (VS reduction) Alt. 2 (40-day bench) 0 Alt. 3 (30-day bench) Alt. 4 (Spec. 0, uptake)
Alt. 5 (14-Day Aerobic) Alt. 6 (Alk. StabilizationEl Alt 7 (Drying - Stable) 1Alt. 8 (Drying - Unstable)
Alt. 9 (Injection) Alt. 10 (Incorporation) U No vector attraction reduction alternatives were performed [YJ
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note
if you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Mr.Mitchell Luckie, Systems Engineer ORC
Preparer Name and Title (type orprint) Land Applier Name and Title (if applicable) (type or print)
Signature of Preparer* Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 02T (12/2006)

I "1 11111 Qfl['�-J]Rin�� �11.�Ijj �19
Facility Name: Marcal Cordova, LLC WQ Permit Number: WQ0039924
WWTP Name: Cordova Facility NPDES Number: NA
Monitoring Period: From ll/l/2023 To 11/30/2023
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative pe
Class A: Alt. A (time/temp) [I I Alt B (Alk Treatment) Ll Alt. C (Prior Testing)
Alt.D (No Prior Test) C1 Process to Further Reduce Pathogens
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying 0 1 Heat Treatment[] TherniophilicE
Beta Ray Gamma Rav El I Pasteurization 13
Class B: jAlt. (1) Fecal Density L3 I Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathc
Lime Stabilization El Air Drying El Composting . D jAerobic Di
Anaerobic Digestion D
If applicable to alternative performed (Class A or Class B) complete the following monitorin
Allowable Level Pathogen Density Number of Frequency
Parameter I Excee-
in Sludge MinimumlGeo. MeanMaximun� Units of Analysis
I ;� A ---- I
2 x 10 to the MPN
6th power
per gram of CFU
Fecal Coliform total solids
1000 mpn per gram
of total solid (dry
g data:
Sample Analytic
Tech -
Type I ninup
Salmonella bacteria 3 MPN per 4 grams GPanls
EPA(in lieu of fecal total solid (dry 0.9 NA <0.9 0 Monthly Grabcolifon-n2 weight1682
Vector Attraction Reduction (15A NCAC 02T.1107) - Please indicate alternative performed:
Alt. 1 (VS reduction) Alt. 2 (40-day bench) 0 Alt. 3 (30-day bench) Alt. 4 (Spec. 0-) uptake) LJ
Alt. 5 (14-Day Aerobic) Alt. 6 (Alk. StabilizationEl Alt 7 (Drying - Stable) 1Alt. 8 (Drying - Unstable) 13
Alt. 9 (Injection) D Alt. 10 (Incorporation) El No vector attraction reduction alternatives were performed 5d
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T.1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note
if you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Mr.Mitchell Luckie, Systems Engineer ORC
Preparer Name and Title (type or print) Land Applier Name and Title (if applicable)(type or print)
Signature of Preparer* Date Signature of Land Applier (if applicable)
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
RM

Facility Name: Marcal Cordova, LLC WQ Permit Number: WQ0039924
WWTP Name: Cordova Facility NPDES Number: NA
Monitoring Period: From 12/1/2023 To 12/31/2023
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A: Alt. A (time/temp) [j Alt B (Alk Treatment) Alt. C (Prior Testing)
................. .... .
................. Alt. D (No Prior Test) Process to Further Reduce Pathogens
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying El Heat TreatmentEl Therniophilicl]
Beta Rav Gamma Rav Pasteurization
Class B: JAR. (1) Fecal Densi
.pplicable to alternative performed
ie Stabilization El
aerobic Digestion D
applicable to alternative perform
Parameter Allowable Level
I in Sludge 6 1
Fecal Coliform
2 x 10 to the MPN
6th power
per gram of CFU
total solids
1000 mpn per gram
of total solid (dry
ty ❑ Alt. (2) Process to Significantly Reduce Pathogen
(Class B only) indicate "Process to Significantly Reduce 3 Pati
Air Drying El Composting El [Aerobic
ied (Class A or Class B) complete the following monitor
APathogen Density Number of Frequency
: Excee-
.nimGeo. MeanlMaximu Unitsi 4of Analysis
®e 1
S L]
ogens":
Di
gestion L3
.......... ..
ing data:
ISample Analyt ca
Type Tech -
I niniu-
Salmonella bacteria 3 MPN per 4 grams I I NI s
I682PA(in lieu of fecal total solid (dry <GP
am0.6 1 NA :5 0.7 0 Monthly I Grab I
r1
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed:
Alt. 1 (VS reduction) Alt. 2 (40-day bench) El Alt. 3 (30-day bench) Alt. 4 (Spec. 0-, uptake) 0
Th. 5 (14-Day Aerobic) Alt. 6 (Alk. Stabilization[] Alt 7 (Drying - Stable) 1Alt. 8 (D - rying - Unstable)
Alt. 9 (Injection) Alt. 10 (Incorporation) El No vector attraction reduction alternatives were performed R1
CERTIFICATION STATEMENT (please check the appropriate statement)
21 "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
El "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note
if you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Mr.Mitchell Luckie, Systems Engineer ORC
Preparer Name and Title ( De or print) Land Applier Name and Title (if applicable)(type or print)
rJ
Signature of Preparer* Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)

PATHOGEN AND VECTOR
ATTRACTION REDUCTION DOCUMENTATION

PATHOGEN REDUCTION AND VECTOR
ATTRACTION REDUCTION DOCUMENTATION
requirementsThe current permit, WQ0039924, does not have vector attraction requirements but does have Class
og- Documentation is attached to reflect these

Marcal Cordova, LLC
Cordova, NC
City of Rockingham IUP 0015
Jan-23
Biological Consulting Services
Laub 9,:
Da"te"'An"ad 'Zed,
y
Iftfithat V 1 o S: I' Ola
t oftary �:Sai na.
Sc value Mone
MPN- r,jW pe
y
2212134
12/16/22
< 0.07
< 0.6
2212135
12/16/22
< 0.07
< U
2212136
12/16/22
s O07
5 0.6
2212137
12/16/22
< 0.07
5 0.7
2212138
12/16/22
< 0.07
<' O.6
2212139
12/16/22
0.07
0.6
2212140
12/16/22
0.07
0.7
Exceedances U
All Samples are less then 3 MPN per 4 grams dry weight. Samples meet Class A pathogen
requirement for distribution.
Data provided in this summary have been used for the values reported on the Monthly Pathogen
and Vector Attraction Reduction Forms for Class A option.

Inc. BIOLOGICAL CONSULTING SERVICES
OF NORTH FLORIDA, INC.
December 20, 2022
Robert Branch
Branch Residuals and Soils
1735 Heckle Blvd. Suite 103-291
Rockhill SC 29732
336-312-9007
[e-mail]
Client ID: VD1, VD2, VD3, VD4, VD5, VD6, VD7
Analysis Method
Salmonella EPA 1682; BCS SOP M-4 (IS017025 and TNI Accredited)
Following, you will find our report on the results of the analysis conducted on the referenced samples -
Should you have any questions, please do not hesitate to contact me.
Sincerely,
Bonnie Mull, MPH
Page I of 8
Final Report BCS ID 2212134, 2212135, 2212136, 2212137, 2212138, 2212139, 2212140
BCS LABORATORIES, INC. — GAINESVILLE
4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609
TEL. [phone], FAx. [phone]
WWW,MICROBIOSERVICES.COM
FLDOH E82924, ISO 17025:2017 L2422, PAIDEP: 68-03950, AZDHS:AZO820, EPA FLO 1 147
THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES
/-7A

Client: Branch Residuals and Soils
Analysis: Salmonella
Project Name: 2014-110
Client Sample ID: VD1
Sample Date/Time: December 12, 2022 1:03
BCS Sample ID: 2212134 Sample Description: biosolid
Date Received: December 13, 2022 11:20 Amount Submitted:100 ml BCS bottle % Solids: 41.9
Amount Analyzed: 3.01E+01 g Receipt Temperature: 0.9 deg C Preserved: Yes
Analysis Start: December 13, 2022 11:35 Analysis Stop Date: December 16, 2022 11:00
Analyst: Nelson Luque, B.S. Qualifier: U
Primary Value: !90.07 Salmonella MPN/mL sample analyzed
Secondary Value: :90.6 Salmonella MPN/4 dry grams
Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's
detection limit for the amount of sample analyzed as per the method's standard reporting units
Client: Branch Residuals and Soils
Analysis: Salmonella
Project Name: 2014-110
Client Sample ID: VD2
BCS Sample ID: 2212135 Sample Description: biosolid
Date Received: December 13, 2022 11:20 Amount Submitted: 100 ml BCS bottle % Solids: 39.9
Amount Analyzed: 3.00E+01 g Receipt Temperature: 0.9 deg C Preserved: Yes
Analysis Start: December 13, 2022 11:35 Analysis Stop Date: December 16, 2022 11:00
Analyst: Nelson Luque, B.S. Qualifier: U
Primary Value: :50.07 Salmonella MPN/mL sample analyzed
Secondary Value: 50.7 Salmonella MPN/4 dry grams
Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's
detection limit for the amount of sample analyzed as per the method's standard reporting units
Page 2 of R
Final Report BCS ID 2212134, 2212135, 2212136, 2212137, 2212138, 2212139, 2212140
BCS LABORATORIES, INC. °— GAINESVILLE
4609 NW 6TI-I STREET, STE. A, GAINESVILLE, FLORIDA 32609
TEL. [phone], FAx. [phone]
WWW.MICROBIOSERVICES.COM
FLDOH E82924, ISO17025:2017 L2422, PA®EP: 68-03950, AZDHS:AZO820, EPA FLO1 147
THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL., WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES
lbl
HaC-MA A16
//i .

Client: Branch Residuals and Soils
Analysis: Salmonella
Project Name: 2014-110
Client Sample ID: VD3
Sample Date/Time: December 12, 2022 1:09
BCS Sample ID: 2212136 Sample Description: biosolid
Date Received: December 13, 2022 11:20 Amount Submitted:100 ml BCS bottle % Solids: 40.2
Amount Analyzed: 2.99E+01 g Receipt Temperature: 0.9 deg C Preserved: Yes
Analysis Start: December 13, 2022 11:35 Analysis Stop Date: December 16, 2022 11:00
Analyst: Nelson Luque, B.S. Qualifier: U
Primary Value: 150.07 Salmonella MPN/mL sample analyzed
Secondary Value: 150.6 Salmonella MPN/4 dry grams
Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's
detection limit for the amount of sample analyzed as per the method's standard reporting units
Client: Branch Residuals and Soils
Analysis: Salmonella
Project Name: 2014-110
Client Sample ID: VD4
BCS Sample I: 2212137 Sample Description: biosolid
Date Received: December 1, 2022 11:20 Amount Submitted:100 ml BCS bottle % Solids: 39.5
Amount Analyzed: 3.01E+01 g Receipt Temperature: 0.9 deg C Preserved: Yes
Analysis Start: December 13, 2022 11:35 Analysis Stop Date: December 16, 2022 11:00
Analyst: Nelson Luque, B.S. Qualifier: U
Primary Value: 150.07 Salmonella MPN/L sample analyzed
Secondary Value: :50.7 Salmonella MPN/4 dry grams
Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's
detection limit for the amount of sample analyzed as per the method's standard reporting units
Page 3 of &
Final Report BCS ID 2212134, 2212135, 2212136, 2212137, 2212138, 2212139, 2212140
BCS LABORATORIES, INC. — GAINESVILLE
4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 5260
TEL. [phone], FAx. [phone]
WWWMICROBIOSERVICES.COM
ELDOH E82924, ISO 1702 5:2017 L2422, PADEP: 68-03950, AZDH S:AZO820, EPA FL_O 1 147
THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL., WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES
it 4

Client: Branch Residuals and Soils
Analysis: Salmonella
Project Name: 2014-110
Client Sample ID: VD5
Sample Date/Time: December 12, 2022 IAA
BCS Sample ID: 2212138 Sample Description: biosolid
Date Received: December 13, 2022 11:20 Amount Submitted:100 ml BCS bottle % Solids: 40.6
Amount Analyzed: 3.01E+01 g Receipt Temperature: 0.9 deg C Preserved: Yes
Analysis Start: December 13, 2022 11:35 Analysis Stop Date: December 16, 2022 11:00
Analyst: Nelson Luque, B.S. Qualifier: U
Primary Value: 150.07 Salmonella MPN/mL sample analyzed
Secondary Value: 50.6 Salmonella MPN/4 dry grams
Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's
detection limit for the amount of sample analyzed as per the method's standard reporting units
Client: Branch Residuals and Soils
Analysis: Salmonella
Project Name: 2014-110
Client Sample ID: V6
�. r-
BCS Sample ID: 2212139 Sample Description: biosolid
Date Received: December 13, 2022 11:20 Amount Submitted:100 ml BCS bottle % Solids: 40.3
Amount Analyzed: 3.00E+01 g Receipt Temperature: 0.9 deg C Preserved: Yes
Analysis Start: December 13, 2022 11:5 Analysis Stop Date: December 16, 2022 11:00
Analyst: Nelson Luque, B.S. Qualifier: U
Primary Value: :50.07 Salmonella MPN/mL sample analyzed
Secondary Value: :50.6 Salmonella MPN/4 dry grams
Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's
detection limit for the amount of sample analyzed as per the method's standard reporting units
Page 4 of 8
Final Report BCS ID 2212134, 2212135, 2212136, 2212137, 2212138, 2212139, 2212140
BCS LABORATORIES, INC. — GAINESVILLE
4609 NW STI-I STREET, STE. A, GAaINESVILLE, FLORIDA 3260
TEL. [phone], FAx. [phone]
WWW.MICROBIOSERVICES.COM
FL®®I—I E82924, ISO 17025:2017 L2422, PA®EP: 63D50, AZDHS:AZO820, EPA FL01 147
THIS REPORT SHALL NOT BE REPRODUCE®, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES
RaC-MRA AAM l '
1i 0

Client: Branch Residuals and Soils
Analysis: Salmonella
Project Name: 2014-110
Client Sample ID: VD7 Sample Date/Time: December 12, 2022 1:22
BCS Sample ID: 2212140 Sample Description: biosolid
Date Received: December 13, 2022 11:20 Amount Submitted:100 ml BCS bottle % Solids: 39.7
Amount Analyzed: 3.00E+01 g Receipt Temperature: 0.9 deg C Preserved: Yes
Analysis Start: December 13, 2022 11:35 Analysis Stop Date: December 16, 2022 11:00
Analyst: Nelson Luque, B.S. Qualifier: U
Primary Value: :50.07 Salmonella MPN/mL sample analyzed
Secondary Value: <_0.7 Salmonella MPN/4 dry grams
Analysis Notes: Undetected: Analyse was not detected in the sample analyzed; Value represents the method's
detection limit for the amount of sample analyzed as per the method's standard reporting units
Page 5 of R
Final Report BCS I® 2212134, 2212135, 2212136, 2212137, 2212138, 2212139, 2212140
BCS LABORATORIES, INC. — GAINESVILLE
4609 NW 6T"{ STREET, STE. A, GAINESVIL.LE, FLORIDA 32609
TEL. [phone], F (52) 577-5630
WWW.MICROBIOSERVICES.COM
F'LDOH E82024, ISO17025:2017 L2422, PA®EP: 68-03950, DHS:AZO820, EPA EL.O 1 147
THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF ECG LABORATORIES
1I 6 p
�i IrJL�

Client: Branch Residuals and Soils
Project: 2014-110
Method Detection Limit: 1 microorganism/ unit weight or volume analyzed
Practical Quantitation Limit: 1 microorganism/ unit weight or volume analyzed
Report Notes:
Custody Seal Condition: Not Present
Sample(s) were received well preserved and in excellent condition. Sample(s) were analyzed following receipt
as per the described analytical methodology. End of report notes.
Page 6 of 8
Final Report BCS ID 2212134, 2212135, 2212136, 2212137, 2212138, 2212139, 2212140
BCC LABORATORIES, INC. — GAINESVILLE
4609 NVV 6`fH STREET, STE. A, GAINESVIL.LE, FLORIDA 32609
TEL. (352) 377®272, FAX. [phone] VVVVW.MICROBIOSERVICES.COM
FLDOH E82924, ISO 17025:2017 L.2422, FADER. 6&03950, AZD i :AZC7820,EPA F'L O 1 147
THIS REPORT SHALL NOTBE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCC LABORATORIES
ilaC-WA A&B,
ie. �� f�r���j'b

I certify that I have examined and I am familiar with the information submitted herein. The results pertain only
to sample(s) identified and their condition at time of receipt. Based on my inquiry of the individuals
responsible for the analysis, I believe the data to be true, accurate, and complete. Sampling and field data was
obtained from submitted documents. The analysis was authorized and commissioned by the client. The
resulting data are representative of the analysis conducted on the material/samples/articles provided by the
client (or client's representative) and it's/their condition at the time of analysis. The sample(s) were analyzed
in accordance with the appropriate method , however due to the inherent limitations of the methods,
microorganisms may avoid detection. BCS Laboratories offers no express or implied warranties concerning
the quality, safety, and/or purity of any sample, batch, source, or the process they are derived from. Quality
assurance controls were performed as outlined in the method and as per Good Laboratory Practices. The
analysis and results presented in this report meet the requirements of the standards of The NELAC Institute
(TNI), ISO 17025, and the FL DOH Environmental Laboratory Certification Program, as applicable unless
otherwise noted.
Date: December 20, 222
Page 7 of 8
Final Report BCS ID 2212134, 2212135, 2212136, 2212137, 2212136, 2212139, 2212140
BCS LABORATORIES, INC. — GAINESVILLE
4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32600
TEL. [phone], FAx. [phone]
WWW.MICROBIOSERVICES.COM
FLDOH E82924, ISO 17025:2017 L2422, FADER 68-039 a0, AZDHS;AZO820, EFTA F'LO1 147
THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT" OF BCS LABORATORIES
I -MA
� �� )

DATA QUALIFIER CODES
SYMBOL MEANING
B Results based on counts outside the acceptable range.
X Sample received without prior notification or delayed delivery. Analysis performed outside of
associated method required QC data set (1 QC data set per 20 samples per 168 hours).
I Value is between the laboratory method detection limit & the practical quantitation limit.
J1 The sample matrix interfered with the ability to make any accurate determination.
J2 No Quality Control criteria exist for the component.
J3 The data are questionable because of improper laboratory orfield protocols.
L Off scale high. Actual value is known to be greaterthan value given.
N Presumptive evidence for the presence of material. There is an indication that the analyte is
present, but the confirmation requirement was not met.
0 Sampled, but analysis not performed.
Q Sample held beyond the accepted holding time.
U Indicates that the compound was analyzed for but not detected. The specified component was
not detected. The reported value is the method detection limit.
V Analyte was detected in both sample and the method blank. Data may not be accurate.
Y Laboratory analysis was from an improperly preserved sample; the data may not be accurate
Z Too many colonies present (TNTC); the numeric value given represents the upper end of the
value that can be determined based on the volume.
7 Data are rejected and should not be used. QC data for analyte did not meet acceptance criteria.
Presence or absence of analyte could not be confirmed.
** Not reported due to interference.
A Sampling container supplied by client. Sterility can not be confirmed by BCS.
# BCS Lab specific qualifier. See laboratory analysis notes.
Page B of
Final Report BCS ID 2212134, 2212135, 2212136, 2212137, 2212138, 2212139, 2212140
BCS LABORATORIES, INC. — GAINESVILLE
4609 NW 6TH STREET,STEE. A, GAINESVILLE, FL.ORIDA 260
TEL. (3 2) 377-�^2 2, F , (3 2) 377-5630
WWW.MICROBIOSERVICES.COM
F'LDOH E82924, ISO 17025:2017 L2422, PAIOEP: 68-03950, AZDHS:AZOE20, EPA F'L.O 1 147
THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES
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Marcal Cordova, LLC
Cordova, NC
City of Rockingham IUP O015
Feb-23
Biological Consulting Services
Date Ahol-pe
PriMAr,
MW
2301246
1/30/23
2301247
2/28/23
2301248
2/28/23
2301249
2/28/23
2301250
2/28/23
2301251
2/28/23
2301252
2/28/23
Der MI
Exceedances
All Samples are less then 3 MPN per 4 grams dry weight. Samples meet Class A pathogen
requirement for distribution.
Data provided in this summary have been used for the values reported on the Monthly Pathogen
and Vector Attraction Reduction Forms for Class A option.

Boologucal Consul'Ung Services v
Of Norlh Florida, InC.
Robert Branch
Branch Residuals and Soils
1735 Heckle Blvd. Suite 103-291
Rockhill SC 29732
336-312-9007
[e-mail]
Client ID: VD1, VD2, VD3, VD4, VD5, VD6, VD7
We have completed the analysis of the submitted samples as outlined below.
Project Name: Von Drehle Cordova NC
Analysis Method
Salmonella EPA 1682; BCS SOP M-4 (ISO17025 and TNI Accredited)
TE -ffflfi I L - - , .. I rp'1777
lovring, you wl I ow cepm F-WiTdT?STb LUI IUULL%:U U,1 I Ul- i
Should you have any questions, please do not hesitate to contact me.
Sincerely,
Bonnie Mull, MPH
Laboratory Operations Manager
Page 1 of 8
Final Report BCS ID 2301246, 2301247, 2301248, 2301249, 2301250, 2301251, 2301252
BCS LABORATORIES, INC. — GAINESVILLE
4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609
TEL. [phone], FAx. [phone]
WWW.MICROBIOSERVICES.COM
FLDOH E82924, ISO 17025:2017 L2422, PADEP: 68-03950, AZDHS:AZ0820, EPA FLO 1 147
THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES
ilaC-URA

Client: Branch Residuals and Soils
Analysis: Salmonella
Project Name: Von Drehle Cordova NC
Client Sample ID: VDI
Sample Date/Time: January 24, 2023 12:40
BCS Sample ID: 2301246 Sample Description: Biosolid
Date Received: January 25, 2023 10:12 Amount Submitted: 100 mL BCS bottle %Solids: 40.5
Amount Analyzed: 2.99E+01 g Receipt Temperature: 2.0 deg C Preserved: Yes
Analysis Start: January 25, 2023 10:30 Analysis Stop Date: January 30, 2023 14:00
Analyst: Wei -yea Hsu, M.S. Qualifier: U
Primary Value: :50.07 Salmonella MPN/mL sample analyzed
Secondary Value: :50.6 Salmonella MPN/4 dry grams
Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's
detection limit for the amount of sample analyzed as per the method's standard reporting units
Client: Branch Residuals and Soils
Analysis: Salmonella
Project Name: Von Drehle Cordova NC
Client Sample ID: VD2
Z,115A11�
BCS Sample ID: 2301247 Sample Description: Biosolid
Date Received: January 25, 2023 10:12 Amount Submitted: 100 mL BCS bottle %Solids: 39.4
Amount Analyzed: 3.01E+01 g Receipt Temperature: 2.0 deg C Preserved: Yes
Analysis Start: January 25, 2023 10:30 Analysis Stop Date: January 30, 2023 14:00
Analyst: Wei -yea Hsu, M.S. Qualifier: U
Primary Value: 50.07 Salmonella MPN/mL sample analyzed
Secondary Value: :50.7 Salmonella MPN/4 dry grams
Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's
detection limit for the amount of sample analyzed as per the method's standard reporting units
Page 2 of 8
Final Report BCS ID 2301246, 2301247, 2301248, 2301249, 2301250, 2301251, 2301252
BCS LABORATORIES, INC. — GAINESVILLE
4609 NW 6TH STREET', STE. A, GAINESVILLE, FLORIDA 32609
TEL. [phone], FAx [phone]
MICROBIOSERVICES.COM
FLDOH E82924, ISO 17025:2017 L-2422, PADEP: 68-03950, AZDHS:AZO820, EPA FLO 1 147
THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES

Client: Branch Residuals and Soils
Analysis: Salmonella
Project Name: Von Drehle Cordova NC
Client Sample ID: VD3
Sample Date/Time: January 24, 2023 12:35
BCS Sample ID: 2301248 Sample Description: Biosolid
Date Received: January 25, 2023 10:12 Amount Submitted: 100 mL BCS bottle %Solids: 30.2
Amount Analyzed: 3.01E+01 g Receipt Temperature: 2.0 deg C Preserved: Yes
Analysis Start: January 25, 2023 10:30 Analysis Stop Date: January 30, 2023 14:00
Analyst: Wei -yea Hsu, M.S. Qualifier: U
Primary Value: 50.07 Salmonella MPN/mL sample analyzed
Secondary Value: :50.9 Salmonella MPN/4 dry grams
Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's
detection limit for the amount of sample analyzed as per the method's standard reporting units
Client: Branch Residuals and Soils
Analysis: Salmonella
Project Name: Von Drehle Cordova NC
Client Sample ID: VD4
zlvwffq!��,
BCS Sample ID: 2301249 Sample Description: Biosolid
Date Received: January 25, 2023 10:12 Amount Submitted: 100 mL BCS bottle %Solids: 40.2
Amount Analyzed: 3.00E+01 g Receipt Temperature: 2.0 deg C Preserved: Yes
Analysis Start: January 25, 2023 10:30 Analysis Stop Date: January 30, 2023 14:00
Analyst: Wei -yea Hsu, M.S. Qualifier: U
Primary Value: 150.07 Salmonella MPN/mL sample analyzed
Secondary Value: :50.6 Salmonella MPN/4 dry grams
Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's
detection limit for the amount of sample analyzed as per the method's standard reporting units
Page 3 of 8
final Report BCS ID 2301246, 2301247, 2301248, 2301249, 2301250, 2301251, 2301252
BCS LABORATORIES, INC. — GAINESVILLE
4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609
TEL. [phone], FAx. [phone]
WWW,MICROBIOSERVICES.COM
FLDOH E82924, ISO 17025:2017 L2422, PARE P: 68-03950, AZDHS:A-ZO820, EPA FLO 1 147
THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LAE30RATORIES
11EIC-MA Ai&B
Mir
N

Client: Branch Residuals and Soils
Analysis: Salmonella
Project Name: Von Drehle Cordova NC
Client Sample ID: VD5
Sample Date/Time: January 24, 2023 12:19
BCS Sample ID: 2301250 Sample Description: Biosolid
Date Received: January 25, 2023 10:12 Amount Submitted: 100 mL BCS bottle %Solids: 36.7
Amount Analyzed: 3.00E+01 g Receipt Temperature: 2.0 deg C Preserved: Yes
Analysis Start: January 25, 2023 10:30 Analysis Stop Date: January 30, 2023 14:00
Analyst: Wei -yea Hsu, M.S. Qualifier: U
Primary Value: :50.07 Salmonella MPN/mL sample analyzed
Secondary Value: :50.7 Salmonella MPN/4 dry grams
Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's
detection limit for the amount of sample analyzed as per the method's standard reporting units
Client: Branch Residuals and Soils
Analysis: Salmonella
Project Name: Von Drehle Cordova NC
Client Sample ID: VD6
BCS Sample ID: 2301251 Sample Description: Biosolid
Date Received: January 25, 2023 10:12 Amount Submitted: 100 mL BCS bottle %Solids: 39.2
Amount Analyzed: 3.01E+01 g Receipt Temperature: 2.0 deg C Preserved: Yes
Analysis Start: January 25, 2023 10:30 Analysis Stop Date: January 30, 2023 14:00
Analyst: Wei -yea Hsu, M.S. Qualifier: U
Primary Value: :50.07 Salmonella MPN/mL sample analyzed
Secondary Value: :50.7 Salmonella MPN/4 dry grams
Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's
detection limit for the amount of sample analyzed as per the method's standard reporting units
Page 4 of 8
firial Report BCS ID 2301246, 2301247, 2301248, 2301249, 2301250, 2301251, 2301252
BCS LABORATORIES, INC. -®' GAINESVILLE
4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609
TEL. [phone], FAx. [phone]
WWW.MICROBIOSERVICES.COM
FLDOH E82924, ISO 17025:2017 L2422, PADEP: 68-03950, AZDHS:AZO820, EPA FLO 1 147
THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF 8CS LAEIORATORIES
AAAB
11ZIC-NIRA

Client: Branch Residuals and Soils
Analysis: Salmonella
Project Name: Von Oreh|eCordova N[
Client Sample ID: VD7 Sample Date/Time: January 24, 2023 12:25
B[SSample ID: 2301252 Sample Description: Bioso|id
Date Received: January 2S,ZO23 10:12 Amount Submitted: 10]mL8[5bottle 96SoUds: 54.0
Amount Analyzed: 3.00E+01 g Receipt Temperature: 2.0 deg Preserved: Yes
Analysis Start: January 2S,ZO2] 10:30 Analysis Stop Date: January SO,3O2] 14:00
Analyst: Wei -yea Hsu, M.S. Qualifier: U
Primary Value: :50.07 Salmonella MPN/mLsample analyzed
Secondary Value: 50.4 Salmonella K8P0/4dry grams
Analysis Notes: Undetected: Ana|ytevvas not detected inthe sample analyzed; Value represents the method's
detection limit for the amount of sample analyzed as per the method's standard reporting units
pagesofa
BCS LABORATORIES, INC. --GAlNESV!LLE
4609 NyV6THSTREET, STE.A`GA|wEsvLLE.FLORIDA 32609
TEL[phone].F*)c(352)377-563(]
WYVW.M(CROB((3SERV(CES.COM
FLDOHE82924.ISO 17025:2017L2422.PADEP: 66-0395Q.AZQHS:AZO820.EPA FLD1147
THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRrrrEN CONSENT OF BCS LABORATORIES
���
� ..__.
^ .^.. b

Client: Branch Residuals and Soils
Project: Von Drehle Cordova NC
Method Detection Limit: 1 microorganism/ unit weight or volume analyzed
Practical Quantitation Limit: 1 microorganism/ unit weight or volume analyzed
Report Notes: Custody Seal Condition: Not Present
Sample(s) were received well preserved and in excellent condition. Sample(s) were analyzed following receipt
as per the described analytical methodology. End of report notes.
Page 6 of $
Final Report BC5 10 2301246, 2301247, 2301248, 2301249, 2301250, 2301251, 2301252
BCS LABORATORIES, INC. — GAINES'VIL.L.E:
4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 3260
TEL. [phone], FAX, (352) 77-5630
MICROBIOSERVICES.COM
FLDOH E82924, ISO1'7025:2017 L2422, PA[ EP:68-039 0, AZDHS:AZO82 1, EPA FLO1 147
THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES
111m

I certify that I have examined and I am familiar with the information submitted herein. The results pertain only
to sample(s) identified and their condition at time of receipt. Based on my inquiry of the individuals
responsible for the analysis, I believe the data to be true, accurate, and complete. Sampling and field data was
obtained from submitted documents. The analysis was authorized and commissioned by the client. The
resulting data are representative of the analysis conducted on the material/samples/articles provided by the
client (or client's representative) and it's/their condition at the time of analysis. The sample(s) were analyzed
in accordance with the appropriate method , however due to the inherent limitations of the methods,
microorganisms may avoid detection. BCS Laboratories offers no express or implied warranties concerning
the quality, safety, and/or purity of any sample, batch, source, or the process they are derived from. Quality
assurance controls were performed as outlined in the method and as per Good Laboratory Practices. The
analysis and results presented in this report meet the requirements of the standards of The NELAC Institute
(TNI), ISO 17025, and the FL DOH Environmental Laboratory Certification Program, as applicable unless
otherwise noted.
Signature of LaboratoryDirector/Authorized Rep Date: January 31,
2023
Page 7 of 8
Final Report BCS ID 2301246, 2301247, 2301248, 2301249, 2301250, 2301251, 2301252
BCS LABORATORIES, INC. — GAINESVIL.L E
4609 NW 6TH STREET, STE. A, GAINESVILL.E, FLORIDA 32609
`['EL. [phone], F'AK (2) 377-5630
WWW.MICROBIOSERVICES.COM
FLDOFI S82924, ISO 17025:2017 L.2422, PADEP: 68-03950, AZDHS.AZ O820, EPA F'LO 1 147
THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT" THE WRiT-rE N CONSENT OF BCS LABORATORIES
1l-Es
ftarli

SYMBOL�Y
B Results based on counts outside the acceptable range.
X Sample received without prior notification or delayed delivery. Analysis performed outside of
associated method required QC data set (1 QC data set per 20 samples per 168 hours).
I Value is between the laboratory method detection limit & the practical quantitation limit.
J1 The sample matrix interfered with the ability to make any accurate determination.
J2 No Quality Control criteria exist for the component.
J3 The data are questionable because of improper laboratory or field protocols.
L Off scale high. Actual value is known to be greaterthan value given.
N Presumptive evidence forthe presence of material. There is an indication thatthe analyte is
present, but the confirmation requirement was not met.
O Sampled, but analysis not performed.
Q Sample held beyond the accepted holding time.
U Indicates that the compound was analyzed for but not detected. The specified component was
not detected. The reported value is the method detection limit.
V Analyte was detected in both sample and the method blank. Data may not be accurate.
Y Laboratory analysis was from an improperly preserved sample; the data may not be accurate
Z Too many colonies present (TNTC); the numeric value given represents the upper end of the
value that can be determined based on the volume.
7 Data are rejected and should not be used. QC data for analyte did not meet acceptance criteria.
Presence or absence of analyte could not be confirmed.
** Not reported due to interference.
A Sampling container supplied by client. Sterility can not be confirmed by BCS.
# BCS Lab specific qualifier. See laboratory analysis notes.
Page B of 6
Final Report BCS ID 2301246, 2301247, 2301248, 2301249, 2301250, 2301251, 2301252
BCS LABORATORIES, INC.. — GAINESVILLE
4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 3260
TEL. (52) :377- 272, FAx. [phone]
WWW.MICROBIOSERVICES.COM
FLDOH F82 924, ISO 17025:201 T L2422, PADEP: 68-0395 i, AZDHS:AZ0820, EPA F LO 1 147
THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES

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Marcal Cordova, LLC
Cordova, NC
City of Rockingham IUP 00:15
Mar-23
Biological Consulting Services
Lab;
d::
ri, A
2302192
2/28/23
2302193
2/28/23
2302194
2/28/23
2302195
2/28/23
2302196
2/28/23
2302197
2/28/2=
2302198
2/28/23
1
Y yalue NOW*
WNver W. MPN
Exceedances
'rants 01 ky
KIM
All Samples are less then 3 MPN per 4 grams dry weight. Samples meet Class A pathogen
requirement for distribution.
Data provided in this summary have been used for the values reported on the Monthly Pathogen
and Vector Attraction Reduction Forms for Class A option.

Boologocal,
x
•Of North Florida, Inc.
Consulting services
Robert Branch
Branch Residuals and Soils
1735 Heckle Blvd. Suite 103-291
Rockhill SC 29732
336-312-9007
[e-mail]
Client ID: VDI, VD2, VD3, VD4, VD5, VD6, VD7
mr-Ig "M MMILT.Tr M,
FWaIrl-WIFE 7MINK11f, EMN
Analysis Method
Salmonella EPA 1682; BCS SOP M-4 (ISO17025 and TNI Accredited)
Should you have any questions, please do not hesitate to contact me.
Page 1 of 8
Final Report BCS ID 2302192, 2302193, 2302194, 2302195, 2302196, 2302197, 2302198
BCS LABORATORIES, INC. — GAINESVILLE
4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609
TEL. [phone], FAx. [phone]
WWW.MICROBIOSERVICES,COM
FLDOH E82924, ISO 17025:2017 L2422, PADEP: 68-03950, AZDHS:AZO820, EPA FLO 1 147
THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRrT-TEN CONSENT OF BCS LABORATORIES
KIWI%
11aC-MRA AAB R#'o 7

Client: Branch Residuals and Soils
Analysis: Salmonella
Project Name: 2014-110
Client Sample ID: VDI Sample Date/Time: February 21, 2023 13:20
BCS Sample ID: 2302192 Sample Description: Biosolid
Date Received: February 22, 2023 10:00 Amount Submitted: 100 ml BCS bottle %Solids: 35.0
Amount Analyzed: 3.01E+01 g Receipt Temperature: 3.7 deg C Preserved: Yes
Analysis Start: February 22, 2023 11:00 Analysis Stop Date: February 28, 2023 11:00
Analyst: Erika DiPasquale, B.S. Qualifier: U
Primary Value: 50.07 Salmonella MPN/mL sample analyzed
Secondary Value: !90.7 Salmonella MPN/4 dry grams
Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's
detection limit for the amount of sample analyzed as per the method's standard reporting units
Client: Branch Residuals and Soils
Analysis: Salmonella
ZMMM023��
r.RIPTIRIffm
BCS Sample ID: 2302193 Sample Description: Biosolid
Date Received: February 22, 2023 10:00 Amount Submitted: 100 ml BCS bottle %Solids: 33.7
Amount Analyzed: 3.01E+01 g Receipt Temperature: 3.7 deg C Preserved: Yes
Analysis Start: February 22, 2023 11:00 Analysis Stop Date: February 28, 2023 11:00
Analyst: Erika DiPasquale, B.S. Qualifier: U
Primary Value: 50.07 Salmonella MPN/mL sample analyzed
Secondary Value: 50.8 Salmonella MPN/4 dry grams
Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's
detection limit for the amount of sample analyzed as per the method's standard reporting units
Page 2 of 8
hnal Report BCS ID 23021.92, 23021.93, 2302194, 2302195, 2302196, 2302197, 2302198
BCS LABORATORIES, INC. — GAINESVILLE
4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609
TEL. [phone], FAx. [phone]
WWW.MICROBIOSERVICES.COM
FLDOH E82924, ISO 17025:2017 L2422, PADEP: 68-03950, AZDHS:AZ0820, EPA FLO 1 147
THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES
rKcf*,
08r--MA —AAM 1

Client: Branch Residuals and Soils
Analysis: Salmonella
Project Name: 2014-110
Client Sample ID: VD3
BCS Sample ID: 2302194
Sample Date/Time: February 21, 2023 13:24
Date Received: February 22, 2023 10:00 Amount Submitted: 100 ml BCS bottle %Solids: 35.3
Amount Analyzed: 2.99E+01 g Receipt Temperature: 3.7 deg C Preserved: Yes
Analysis Start: February 22, 2023 11:00 Analysis Stop Date: February 28, 2023 11:00
Analyst: Erika DiPasquale, B.S. Qualifier: U
Primary Value: :50.07 Salmonella MPN/mL sample analyzed
Secondary Value: :50.7 Salmonella MPN/4 dry grams
Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's
detection limit for the amount of sample analyzed as per the method's standard reporting units
Client: Branch Residuals and Soils
Analysis: Salmonella
Project Name: 2014-114
Client Sample ID: VD4
BCS Sample ID: 2302195 Sample Description: Biosolid
Date Received: February 22, 2023 10:00 Amount Submitted: 100 ml BCS bottle %Solids: 35.3
Amount Analyzed: 3.01E+01 g Receipt Temperature: 3.7 deg C Preserved: Yes
Analysis Start: February 22, 2023 11:00 Analysis Stop Date: February 28, 2023 11:00
Analyst: Erika DiPasquale, B.S. Qualifier: U
Primary Value: :50.07 Salmonella MPN/mL sample analyzed
Secondary Value: :50.7 Salmonella MPN/4 dry grams
Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's
detection limit for the amount of sample analyzed as per the method's standard reporting units
Page 3 of 8
final Report BCS ID 23021.92, 23021.93, 23021.94, 2302195, 2302196, 2302197, 2302198
BCS L-AE30RATORIES, INC. - GAINESVILLE
4609 NW 6T+q STREET, STE, A, GAINESVILLE, FLORIDA 32609
TEL. [phone], FAx. [phone]
VVWW.MICROBIOSERVICES.COM
FLDOH E82924, ISO 1 7025:201 7 L2422, PADEP: 68-03950, AZDHS:AZO820, EPA FLO 1 147
THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES
1121C-MA

Client: Branch Residuals and Soils
Analysis: Salmonella
Project Name: 2014-110
Client Sample ID: VD5
Sample Date/Time: February 21, 2023 13:26
BCS Sample ID: 2302196 Sample Description: Biosolid
Date Received: February 22, 2023 10:00 Amount Submitted: 100 ml BCS bottle %Solids: 35.3
Amount Analyzed: 2.99E+01 g Receipt Temperature: 3.7 deg C Preserved: Yes
Analysis Start: February 22, 2023 11:00 Analysis Stop Date: February 28, 2023 11:00
Analyst: Erika DiPasquale, B.S. Qualifier: U
Primary Value: :50.07 Salmonella MPN/mL sample analyzed
Secondary Value: 50.7 Salmonella MPN/4 dry grams
Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's
detection limit for the amount of sample analyzed as per the method's standard reporting units
Client: Branch Residuals and Soils
Analysis: Salmonella
Project Name: 2014-110
Client Sample ID: VD6
FRI17911MW
BCS Sample ID: 2302197 Sample Description: Biosolid
Date Received: February 22, 2023 10:00 Amount Submitted: 100 ml BCS bottle %Solids: 37.7
Amount Analyzed: 3.01E+01 g Receipt Temperature: 3.7 deg C Preserved: Yes
Analysis Start: February 22, 2023 11:00 Analysis Stop Date: February 28, 2023 11:00
Analyst: Erika DiPasquale, B.S. Qualifier: U
Primary Value: 150.07 Salmonella MPN/mL sample analyzed
Secondary Value: 50.7 Salmonella MPN/4 dry grams
Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's
detection limit for the amount of sample analyzed as per the method's standard reporting units
Page 4 of 8
Finil Report BCS ID 2302192, 23021.93, 23021.94, 2302195, 2302196, 2302197, 2302198
BCS LABORATORIES, INC. - GAINESVILLE
4609 NW 6TH STREET, STE, A, GAINESVILLE, FLORIDA 32609
TEL. [phone], FAx. [phone]
WWW.MICROBIOSERVICES.COM
FLDOH E82924, ISO 17025:2017 L2422, PADEP: 68-03950, AZDHS:AZO820, EPA FLO 1 147
THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES
lad -MA
AI&B

Client: Branch Residuals and Soils
Analysis: Salmonella
Project Name: 2014-110
Client Sample ID: VD7 Sample Date/Time: February 21, 2023 13:30
BCS Sample ID: 2302198 Sample Description: Biosolid
Date Received: February 22, 2023 10:00 Amount Submitted: 10 ml BCS bottle %Solids: 38.0
Amount Analyzed: 3.01E+01 g Receipt Temperature: 3.7 deg C Preserved: Yes
Analysis Start: February 22, 2023 11:00 Analysis Stop Date: February 28, 2023 11:00
Analyst: Erika DiPasquale, B.S. Qualifier: U
Primary Value: :50.07 Salmonella MPN/mL sample analyzed
Secondary Value: :50.7 Salmonella MPN/4 dry grams
Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's
detection limit for the amount of sample analyzed as per the method's standard reporting units
Page 5 of 8
Final Report BCS ID 2302192, 2302193, 2302194, 2302195, 2302196, 2302197, 2302198
BCS LABORATORIES, INC. - GAINESVILLE
4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609
rEL. [phone], FAx. [phone]
WWW.MICROBIOSERVICES.COM
FLDOH E82924, ISO 17025:2017 L2422, PADEP: 68-03950, AZDHS:AZO820, EPA FLO 1 147
THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES
llaC-VP,A _A40
I7.

Client: Branch Residuals and Soils
Project: 2014-110
Method Detection Limit: 1 microorganism/ unit weight or volume analyzed
Practical Quantitation Limit: 1 microorganism/ unit weight or volume analyzed
Report Notes: Custody Seal Condition: Not Present
Sample(s) were received well preserved and in excellent condition. Sample(s) were analyzed following receipt
as per the described analytical methodology. End of report notes.
Page 6 of $
Final Report BCS ID 2302192, 2302193, 2302194, 2302195, 2302196, 2302197, 2302198
BCS LABORATORIES, INC. GAINESVILLE
4609 NW STH STREET, STE. A, GAINESVILLE, FLORIDA 32609
["EL. (52) 377-9272, FAx. [phone]
MIC ROBIOSERVICES.COM
I:-'LDOI-i E82824, ISO17025:201'7 L2422, PADEP: 68-088 0, AM-iS:AZO820, EPA F"LO1 147
THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRn-rEN CONSENT OF BC;S LABORATORIES
AJAB
tf
RaC-MRAI
ws
�r of k, A

I certify that I have examined and I am familiar with the information submitted herein. The results pertain only
to sample(s) identified and their condition at time of receipt. Based on my inquiry of the individuals
responsible for the analysis, I believe the data to be true, accurate, and complete. Sampling and field data was
obtained from submitted documents. The analysis was authorized and commissioned by the client. The
resulting data are representative of the analysis conducted on the material/samples/articles provided by the
client (or client's representative) and it's/their condition at the time of analysis. The sample(s) were analyzed
in accordance with the appropriate method , however due to the inherent limitations of the methods,
microorganisms may avoid detection. BCS Laboratories offers no express or implied warranties concerning
the quality, safety, and/or purity of any sample, batch, source, or the process they are derived from. Quality
assurance controls were performed as outlined in the method and as per Good Laboratory Practices. The
analysis and results presented in this report meet the requirements of the standards of The NELAC Institute
(TNI), ISO 17025, and the FL DOH Environmental Laboratory Certification Program, as applicable unless
otherwise noted.
Signature of Laboratory Director/Authorized Rep. Date: February 28, 2023
Page 7 of &
Final Report BCS 10 2302192, 2302193, 2302194, 2302195, 2302196, 2302197, 2302198
BCS BOF XI"ORIE S, INC. — GAINESVILLE
4609 NW 6TF-d STREET, STE. A, GAINE VILI...E, F'LORIDA 32609
1"EL. (352) 77- 272, F (52) 77- 6 ®
FLDOH E82924, I S017025:2017 L2422, PADEP: 58-03950, AZDHS:AZO820, EPA FLO1 147
THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT oF- BCS LABORATORIES
HaC-MRA- l
4f
11 al

DATA QUALIFIER CODES
SYMBOL MEANING
B Results based on counts outside the acceptable range.
X Sample received without prior notification or delayed delivery. Analysis performed outside of
associated method required QC data set (1 QC data set per 20 samples per 168 hours).
I Value is between the laboratory method detection limit & the practical quantitation limit.
J1 The sample matrix interfered with the ability to make any accurate determination.
J2 No Quality Control criteria exist for the component.
J3 The data are questionable because of improper laboratory or field protocols.
L Off scale high. Actual value is known to be greater than value given.
N Presumptive evidence for the presence of material. There is an indication that the analyte is
present, but the confirmation requirement was not met.
O Sampled, but analysis not performed.
Q Sample held beyond the accepted holding time.
U Indicates that the compound was analyzed for but not detected. The specified component was
not detected. The reported value is the method detection limit.
V Analyte was detected in both sample and the method blank. Data may not be accurate.
Y Laboratory analysis was from an improperly preserved sample; the data may not be accurate
Z Too many colonies present (TNTC); the numeric value given represents the upper end of the
value that can be determined based on the volume.
7 Data are rejected and should not be used. QC data for analyte did not meet acceptance criteria.
Presence or absence of analyte could not be confirmed.
** Not reported due to interference.
A Sampling container supplied by client. Sterility can not be confirmed by BCS.
# BCS Lab specific qualifier. See laboratory analysis notes.
Page 8 of B
FirW Report BCS M 2.302.192., 2302.193, 2.302194, 2302195, 2302196, 2302197, 2302198
BCS L..AIm34: RATC_ RIIIE: S, Nc....... GANIf::SiCll....lf....lEm:
4609 NW GTH STREF.7, STE. A, GAINE S'VEC iL.E, FL OFRI111)A 3260
..I..EL.. (352) 377- 272. FAx. [phone]
VTWW.WCF:R0B10SE1FRVCE .C®M
F= LE: OF1 E 2924, ESO 1 '7025:2017 L2422, F IADEP: 8-0395 J, AZf. HS:AZ0820. E:::F IA F-'k-01 147
'rHIS REPORT'SHALL R)OTBE REPRODUCED, EXCF.P1r IN Ff. I L, WITHour our rHE WRITTEN CONSENT OF BCS LARH ORATCbMES

I
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No of containers/units shipi:
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2302198
02127J2023 11000
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Cryptosporidium & Giardia
�,1'Fecal coliform
1�lelminth Ova
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0

areal Cordova, LLC
Cordova, NC
City of Rockingham lCP 001
Apr-23
Biological Consulting Services
Lab*
2303179
Date Analyzed
3/17/23
Primary Value`Salmonella
MPN per tnl
< 0.07'
S condArv. Value Salmonella
MP per 4 gxa is Dry
< 0.7
2303180
3/17/23
<; 0.07
0.7
2303181
3/17/23
� 0.07
5.0.7
2303182
3/17/23
_. 0.07
0.7
2303183
3/17/23
0.07
0,8
2303184
3/17/23
' 0„07
!S 0.7
2303185
3/17/23
< 0.07
M
xeeedanees
All Samples are less then 3 MPN per 4 grams dry weight. Samples meet Class A pathogen
requirement for distribution.
i' i s i w. 1

Boolog"cal Consulting Services
• Florida,
Robert ranch
Branch Residuals and Soils
1735 Heckle Blvd. Suite103-291
ocill SC 29732
36-1-7
[e-mail]
Client ID: VDI, 5, VD6, VD7
BCS ID: 2303179, 20310, 230311, 230312, 230313, 230314, 23015
Dear Robert Branch,
e have completed the analysis of the submitted samples as outlined below.
• 0 95
Analysis Method
Salmonella EPA 1 2; BCS SOP - (ISO17025 and T I Accredited)
Should you have any questions, please do not hesitate to contact me.
Bonnie Mull, MPH
Laboratory Operations Manager
Page 1 of 8
Final Report BCS ID 2303179, 2303180, 2303181, 2303182, 2303183, 23031.84, 2303185
BCS LAE30RATORIES, INC::. --- GAINE SVIL.L.E
4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32509
TEL-. [phone], FAX. [phone]
WWW,MICROBIOSERVICES.COM
F'LDOH E82924, ISO 17025:2017 L242 , PADEP: 68-03950, AZDHS:A-Z0820, EFTA F'L01 147
'THIS REPORT SHALL NOT BE RE:PRor:)UCE7, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES
ccar
„Y
ilaC-MRA

Client: Branch Residuals and Soils
Analysis: Salmonella
Project Name: Cordova
Client Sample ID: VDI
BCS Sample ID: 2303179 Sample Description: Biosolid
Date Received: March 14, 2023 10:27 Amount Submitted: 100 mL BCS bottle %Solids: 36.1
Amount Analyzed: 3.00E+01 g Receipt Temperature: 0.6 deg C Preserved: Yes
Analysis Start: March 14, 2023 11:00 Analysis Stop Date: March 17, 2023 11:00
Analyst: Erika DiPasquale, B.S. Qualifier: U
Primary Value: :50.07 Salmonella MPN/mL sample analyzed
Secondary Value: :50.7 Salmonella MPN/4 dry grams
Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's
detection limit for the amount of sample analyzed as per the method's standard reporting units
Client: Branch Residuals and Soils
Analysis: Salmonella
Project Name: Cordova
Client Sample ID: VD2
BCS Sample I: 2303180 Sample Description: Biosolid
Date Received: March 14, 2023 10:27 Amount Submitted: 100 mL BCS bottle %Sofids: 36.1
Amount Analyzed: 3.01E+01 g Receipt Temperature: 0.6 deg C Preserved: Yes
Analysis Start: March 14, 2023 11:00 Analysis Stop Date: March 17, 2023 11:00
Analyst: Erika DiPasquale, B.S. Qualifier: U
Primary Value: :50.07 Salmonella MPN/mL sample analyzed
Secondary Value: :50.7 Salmonella MPN/4 dry grams
Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's
detection limit for the amount of sample analyzed as per the method's standard reporting units
Page 2 of 8
Final Report BCS M 2303179, 2303180, 2303181, 2303182, 2303183, 2303184, 2303185
BCS I ABORATORI ES, lINC . ......... GAHNESVLLE
4609 NW 6TF-i S"rF:u: ' ET, S-rE. A, GANESVILLE, FLORDA 32609
TEIL.. [phone], FAx. [phone]
WWW.MCIROBIOSERVnCES.COM
FLDOi--i E82924, SO 170252017 11 2422, F"AlDrE " P: 68-03950, AZDf-iSAEF ZO820, If FLO 0 147
THIS REPORT SHALL NOTBE REPRODUCED, EXCEPT IN FULL, WITHOUT -rHEWRrr-rEN CONSENT OF BCS LABORATORIES
,e aCw, 9%
HaC-MRA AJAB

Client: Branch Residuals and Soils
Analysis: Salmonella
Project Name: Cordova
Client Sample ID: VD3
Sample Date/Time: March 13, 2023 12:18
BCS Sample ID: 2303181 Sample Description: Biosolid
Date Received: March 14, 2023 10:27 Amount Submitted: 100 mL BCS bottle %Solids: 35.9
Amount Analyzed: 3.00E+01 g Receipt Temperature: 0.6 deg C Preserved: Yes
Analysis Start: March 14, 2023 11:00 Analysis Stop Date: March 17, 2023 11:00
Analyst: Erika DiPasquale, B.S. Qualifier: U
Primary Value: :50.07 Salmonella MPN/mL sample analyzed
Secondary Value: 50-7 Salmonella MPN/4 dry grams
Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's
detection limit for the amount of sample analyzed as per the method's standard reporting units
Client: Branch Residuals and Soils
Analysis: Salmonella
Project Name: Cordova
Client Sample ID: VD4
BCS Sample ID: 2303182 Sample Description: Biosolid
Date Received: March 14, 2023 10:27 Amount Submitted: 100 mL BCS bottle %Solids: 36.5
Amount Analyzed: 3.01E+01 g Receipt Temperature: 0.6 deg C Preserved: Yes
Analysis Start: March 14, 2023 11:00 Analysis Stop Date: March 17, 2023 11:00
Analyst: Erika DiPasquale, B.S. Qualifier: U
Primary Value: 50.07 Salmonella MPN/mL sample analyzed
Secondary Value: 50.7 Salmonella MPN/4 dry grams
Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's
detection limit for the amount of sample analyzed as per the method's standard reporting units
Page 3 of 8
Final Report BCS ID 2303179, 2303180, 2303181, 2303182, 2303183, 2303184, 2303185
BCS LABORATORIES, INC. - GAINESVILLE
4609 NW 6TI--1 STREET, STE. A, GAINESVILLE, F-­L0RIDA 32609
TEL. [phone], FAx [phone]
VVWW.MICROBIOSERVICES.COM
FLDOH E82924, ISO 17025:2017 L2422, PADEP: 68-03950, AZDHS:AZ0820, EPA FL01 147
THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES

Client: Branch Residuals and Soils
Analysis: Salmonella
Project Name: Cordova
Client Sample ID: VD5
BCS Sample ID:
Date Received:
Amount Analyzed
Analysis Start:
Analyst:
Primary Value:
Secondary Value:
Analysis Notes:
Sample Date/Time: March 13, 2023 12:21
2303183 Sample Description: Biosolid
March 14, 2023 10:27 Amount Submitted: 100 mL BCS bottle %Solids: 36.5
2.99E+01 g Receipt Temperature: 0.6 deg C Preserved: Yes
March 14, 2023 11:00 Analysis Stop Date: March 20, 2023 11:00
Erika DiPasquale, B.S. Qualifier: None
0.07 Salmonella MPN/mL sample analyzed
0.8 Salmonella MPN/4 dry grams
Client:
Branch Residuals and Soils
Analysis:
Salmonella
Project Name:
Cordova
Client Sample ID:
VD6 Sample Date/Time: March 13, 2023 12:22
BCS Sample ID:
2303184 Sample Description: Biosolid
Date Received:
March 14, 2023 10:27 Amount Submitted: 100 mL BCS bottle %Solids: 37.6
Amount Analyzed:
3.01E+01 g Receipt Temperature: 0.6 deg C Preserved: Yes
Analysis Start:
March 14, 2023 11:00 Analysis Stop Date: March 17, 2023 11:00
Analyst:
Erika DiPasquale, B.S. Qualifier: U
Primary Value:
50.07 Salmonella MPN/mL sample analyzed
Secondary Value:
50.7 Salmonella MPN/4 dry grams
Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's
detection
limit for the amount of sample analyzed as per the method's standard reporting units
Page 4 of 8
Fonal Report BCS ID 2303179, 2303180, 2303181, 2303182, 2303183, 2303184, 2303185
BCS LABORAl"ORIES, INC..- GAINESVILLE
4609 NW ISTii STREET, STE. A, GAINESVILLE, FLORIDA 32609
TEL. [phone], FAx. [phone]
WWW.MICROBOSERVICES.COM
FLDOH E82924, ISO 17025:2017 L2422, PADEP: 68-03950, AZDHS:AZO820, EPA FLO 1 147
THIS REPORT S14ALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES
A10AB
flar--WA
I

Client: Branch Residuals and Soils
Analysis: Salmonella
Project Name: Cordova
Client Sample ID: VD7 Sample Date/Time: March 13, 2023 12:23
BCS Sample ID: 2303185 Sample Description: Biosolid
Date Received: March 14, 2023 10:27 Amount Submitted: 100 mL BCS bottle %Solids: 36.1
Amount Analyzed: 3.01E+01 g Receipt Temperature: 0.6 deg C Preserved: Yes
Analysis Start: March 14, 2023 11:00 Analysis Stop Date: March 17, 2023 11:00
Analyst: Erika DiPasquale, B.S. Qualifier: U
Primary Value: :50.07 Salmonella MPN/mL sample analyzed
Secondary Value: :50.7 Salmonella MPN/4 dry grams
Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's
detection limit for the amount of sample analyzed as per the method's standard reporting units
Page 5 of 8
Final Report BCS ID 2303179, 2303180, 2303181, 2303182, 2303183, 2303184, 2303185
BCS I Aii:IOFRATORES, INC......... GAINESV�LIL.E
4609 NW 6TF-i STREET, STE. A, GAIINESVlf UIE, F11 ORl[)A 32609
TEL. [phone], FAx. [phone]
VVVJW.MICi:ROBI�OSII:"RV10ES.COM
F:'LD0H I1E82924, lSO 17025:20 17 11-2422, PA[DEP: 68-03950, AZED1-SAW820, 11::' PA F-1-01 147
THIS REPORr SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES
JIBC-MRA �/d

Client: Branch Residuals and Soils
Project: Cordova
Method Detection Limit: 1 microorganism/ unit weight or volume analyzed
Practical Quantitation Limit: 1 microorganism/ unit weight or volume analyzed
Report Notes: Custody Seal Condition: Not Present
Sample(s) were received well preserved and in excellent condition. Sample(s) were analyzed following receipt
as per the described analytical methodology. End of report notes.
Flage 6 of 8
Final Report BCS ID 2303179, 2303180, 2303181, 2303182, 2303183, 2303184, 2303185
BCS LABORATOR�ES, liNc. GAft[:::'SVlL1 E-
4609 NW 61-1-1 S7F2E11-7, STE. A, GAINESVILLE, FLORIDA 32609
Ti:"i,.... [phone], FAx. [phone]
WWW.MlC1FR0B1OS1[:. " RVICES.COM
FLDOH E82924, ISO 1"7025:20 17 L2422, PADER 68-03950, AZDHS:AZ0820, EPA FLOI 147
THIS REPORT SHALL NOTBE REPRODUCED, EXCEPT IN FULL, WITHOU"i"THE WRrr7EN CONSENT OF BC I-ABORAxORIES
ilaC-NRA
M
d
24
�W

I certify that I have examined and I am familiar with the information submitted herein. The results pertain only
to sample(s) identified and their condition at time of receipt. Based on my inquiry of the individuals
responsible for the analysis, I believe the data to be true, accurate, and complete. Sampling and field data was
obtained from submitted documents. The analysis was authorized and commissioned by the client. The
resulting data are representative of the analysis conducted on the material/samples/articles provided by the
client (or client's representative) and it's/their condition at the time of analysis. The sample(s) were analyzed
in accordance with the appropriate method , however due to the inherent limitations of the methods,
microorganisms may avoid detection. BCS Laboratories offers no express or implied warranties concerning
the quality, safety, and/or purity of any sample, batch, source, or the process they are derived from. Quality
assurance controls were performed as outlined in the method and as per Good Laboratory Practices. The
analysis and results presented in this report meet the requirements of the standards of The NELAC Institute
(TNI), ISO 17025, and the FL DOH Environmental Laboratory Certification Program, as applicable unless
otherwise noted.
Date: March 21, 2023
Page 7 of 8
Final Report RO.S ID 2303179, 2303130, 2303181, 2.303182, 2303133, 2303184„ 2303185
BC S q....AE3ORATORF ES, iNC. -- GAW1-`SViL.I1....lE::
4609 NW 6TFf S TFREET, S..r..r;::~. A, GANYrMESVILLE, FLC3ROIF A 32609
FE[.... (352) 77-9272, FAX. [phone]
WWW.M�CROBlOSEI[:RVIICES.COM
F° LC:: OFi E82924, ISO 1 "7025:2017 L2422, PADEF': 68-039 0, AZDH :AZO82 3, € PA F1....01 147
.C.HIS REPORTSHALL NOT BE REPRODUCED, EXCEPT IN F UI...L., wYTHOUT'THE WRrTi'EN CONSENT OF BC5 L.AF30RATC3R s
a"
H- A ror

SYMBOL MEANING
B Results based on counts outside the acceptable range.
X Sample received without prior notification or delayed delivery. Analysis performed outside of
associated method required QC data set (1 QC data set per 20 samples per 168 hours).
I Value is between the laboratory method detection limit & the practical quantitation limit.
J1 The sample matrix interfered with the ability to make any accurate determination.
J2 No Quality Control criteria exist for the component.
J3 The data are questionable because of improper laboratory or field protocols.
L Off scale high. Actual value is known to be greater than value given.
N Presumptive evidence for the presence of material. There is an indication that the analyte is
present, but the confirmation requirement was not met.
O Sampled, but analysis not performed.
Q Sample held beyond the accepted holding time.
U Indicates that the compound was analyzed for but not detected. The specified component was
not detected. The reported value is the method detection limit.
V Analyte was detected in both sample and the method blank. Data may not be accurate.
Y Laboratory analysis was from an improperly preserved sample; the data may not be accurate
Z Too many colonies present (TNTC); the numeric value given represents the upper end of the
value that can be determined based on the volume.
7 Data are rejected and should not be used. QC data for analyte did not meet acceptance criteria.
Presence or absence of analyte could not be confirmed.
** Not reported due to interference.
A Sampling container supplied by client. Sterility can not be confirmed by BCS.
# BCS Lab specific qualifier. See laboratory analysis notes.
Page 8 of 3
Finial Resort BCS iD 2303179, 2.303180, 2303181, 2.303182., 2303183, 2303184, 2.303185
BCS LABORATORIES, INC......... GAINESVILLE
4609 NW 6` H OTIRELT, S..T..IE:-. A, GAINESVIII-LIES:, ih�� LOE2 DA 32609
TIE.L.. (35 ) 377 9272, FAx, ( a ) 377-5630
R...D01-{ E82.924, ISO17025:2017 L2422, If::sADEI::a: 58-03950, AZD1 G:A O820, EPA FLO1 147
.'T_Ha S REPORT SHALL NOT BE: REPROr:)UCED, EXCEPT IN F'UI...IL., WITHOUT "fl-CE WRITTEN CONSENT C3V� BCS LABORATORIES
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Cordova, NC
1 "" ' 3..
Biological Consulting Services
Lab #
Date Analyzed`
Prlmar V. ..lmonella� i
Secondary Yalu salmonella
LPN per ml . l
:MP1V per 4 gxarns;D�
2304210
4/25/23
< 0.07
-0.6
2304211
4/25/23
0.07
< 0.6
2304212
4/25/23
< 0.07
5 0.6
2304213
4/25/23
" 0,07
U
2304214
4/25/23
0.07
< 0.6
2304215
4/25/23
< 0.07
0.7
2304216
4/25/23
< 0.07
< 0.6
E ceedances
}
All Samples are less then 3 MPN per 4 grams dry weight. Samples meet Class A pathogen
requirement for distribution.
VectorData provided in this summary have been used for the values reported on the Monthly Pathogen
and Reduction i

Biological Consulting Services
k V1 %
Of North Florida, Inc.
omlmomi
Robert Branch
%,ranch Residuals and Soils
1735 Heckle Blvd. Suite 103-291
Nockhill SC 29732
336-312-9007
[e-mail]
Client ID: M1, M2, M3, M4, M5, M6, M7
We have completed the analysis of the submitted samples as outlined below.
Project Name: Marcal Cordova NC
Analysis Method
Salmonella EPA 1682; BCS SOP M-4 (ISO17025 and TNI Accredited)
-1 , PTIT"Irl"T T 1 21 ... '?M1;t'WMYJ
Should you have any questions, please do not hesitate to contact me.
Sincerely,
Bonnie Mull, MPH
Laboratory Operations Manager
Page I of 8
Final Report BCS ID 2304210, 2304211, 2304212, 2304213, 2304214, 2304215, 2304216
BCS LABORATORIES, INC. — GAINESVILLE
4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609
TEL. [phone], FAX. [phone]
WWW.MICROBIOSERVICES.COM
FLDOH E82924, ISO 17025:2017 L-2422, PAIDEP: 68-03950, AZDHS:AZO820, EPA FLO 1 147
THIS REPORT SHALL NOT` BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES
AJAB
ilaC-MRA iv'

Client: Branch Residuals and Soils
Analysis: Salmonella
Project Name: Marcal Cordova NC
Client Sample ID: MI
BCS Sample ID: 2304210 Sample Description: Biosolid
Date Received: April 18, 2023 9:51 Amount Submitted: 100 mL BCS bottle %Solids: 40.2
Amount Analyzed: 2.99E+01 g Receipt Temperature: 4.9 deg C Preserved: Yes
Analysis Start: April 18, 2023 10:15 Analysis Stop Date: April 25, 2023 11:30
Analyst: Wei -yea Hsu, M.S. Qualifier: U
Primary Value: :50.07 Salmonella MPN/mL sample analyzed
Secondary Value: :50.6 Salmonella MPN/4 dry grams
Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's
detection limit for the amount of sample analyzed as per the method's standard reporting units
Client: Branch Residuals and Soils
Analysis: Salmonella
Project Name: Marcal Cordova NC
Client Sample ID: M2
BCS Sample ID: 2304211 Sample Description: Biosolid
Date Received: April 18, 2023 9:51 Amount Submitted: 100 mL BCS bottle %Solids: 40.7
Amount Analyzed: 3.00E+01 g Receipt Temperature: 4.9 deg C Preserved: Yes
Analysis Start: Aprill8,2023 10:15 Analysis Stop Date: April 25, 2023 11:30
Analyst: Wei -yea Hsu, M.S. Qualifier: U
Primary Value: 150.07 Salmonella MPN/mL sample analyzed
Secondary Value: 50.6 Salmonella MPN/4 dry grams
Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's
detection limit for the amount of sample analyzed as per the method's standard reporting units
Page 2 of 8
Fwal Report BCS ID 2304210, 2304211, 2304212, 2304213, 2304214, 2304215, 2304216
BCS LABORATORIES, INC . ........ GAINESVILLE
4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609
TEL. [phone], FAx. [phone]
MICROBIC SERVICE
FLDOH E82924, ISO 1702 5:20 17 L2422, PADEP: 68-03950, AZDHS:AZO820, EPA FLO 1 147
THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES
llaC-MA _,A1,0A0
7,
a, V011,

Client: Branch Residuals and Soils
Analysis: Salmonella
Project Name: Marcal Cordova NC
Client Sample ID: M3
BCS Sample ID: 2304212 Sample Description: Biosolid
Date Received: April 18, 2023 9:51 Amount Submitted: 100 mL BCS bottle %Solids: 40.4
Amount Analyzed: 3.01E+01 g Receipt Temperature: 4.9 deg C Preserved: Yes
Analysis Start: April 18,2023 10:15 Analysis Stop Date: April 25, 2023 11:30
Analyst: Wei -yea Hsu, M.S. Qualifier: U
Primary Value: :50.07 Salmonella MPN/mL sample analyzed
Secondary Value: 50.6 Salmonella MPN/4 dry grams
Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's
detection limit for the amount of sample analyzed as per the method's standard reporting units
Client: Branch Residuals and Soils
Analysis: Salmonella
Project Name: Marcal Cordova NC
Client Sample ID: M4
WOURR1411070
BCS Sample ID: 2304213 Sample Description: Biosolid
Date Received: April 18, 2023 9:51 Amount Submitted: 100 m L BCS bottle %Solids: 36.3
Amount Analyzed: 3.01E+01 g Receipt Temperature: 4.9 deg C Preserved: Yes
Analysis Start: April l8,2023 10:15 Analysis Stop Date: April 25, 2023 11:30
Analyst: Wei -yea Hsu, M.S. Qualifier: U
Primary Value: :50.07 Salmonella MPN/mL sample analyzed
Secondary Value: 50.7 Salmonella MPN/4 dry grams
Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's
detection limit for the amount of sample analyzed as per the method's standard reporting units
Page 3 of 8
Final Report BCS ID 2304210, 2304211, 230421.2, 230421.3, 230421.4, 2304215, 2304216
BCS LABORATORIES, INC. - GAINESVILLE
4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609
T'EL. [phone], FA)c [phone]
WWW.MICROBIOSERVICES.COM
FLDOH E82924, ISO 17025:2017 L2422, PADEP: 68-03950, AZDHS:AZ0820, EPA FLO 1 147
THIS REPORT SHAL.L. NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF E3CS LABORATORIES
lxcft,
Ai&B
J1,3C-MP,A

Client: Branch Residuals and Soils
Analysis: Salmonella
Project Name: Marcal Cordova NC
Client Sample ID: M5
BCS Sample I D: 2304214
Date Received: April 18, 2023 9:51
Sample Description: Biosolid
Amount Submitted: 100 mL BCS bottle %Solids: 40.9
Amount Analyzed: 3.00E+01 g Receipt Temperature: 4.9 deg C Preserved: Yes
Analysis Start: April 18, 2023 10:15 Analysis Stop Date: April 25, 2023 11:30
Analyst: Wei -yea Hsu, M.S. Qualifier: U
Primary Value: :50.07 Salmonella MPN/mL sample analyzed
Secondary Value: :50.6 Salmonella MPN/4 dry grams
Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's
detection limit for the amount of sample analyzed as per the method's standard reporting units
Client: Branch Residuals and Soils
Analysis: Salmonella
Project Name: Marcal Cordova NC
Client Sample ID: M6
. 0 - 0
�1104: M.
FTMT#=Wx1Tff!9 Ma
Analysis Start:
Analyst:
2.99E+01 g
April 18, 2023 10:15
Wei -yea Hsu, M.S.
-Alieceipt Temperature: 4.9 deg C Preserved: Ye2
Analysis Stop Date: April 25, 2023 11:30
74M
Primary Value: :50.07 Salmonella MPN/mL sample analyzed
Secondary Value: 50.7 Salmonella MPN/4 dry grams
Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's
detection limit for the amount of sample analyzed as per the method's standard reporting units
Page 4 of 8
Final Report BCS ID 2304210, 230421.1, 2304212, 2304213, 2304214, 2304215, 2304216
BCS LABORATORIES, INC. — GAINESVILLE
4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609
TEL. [phone], FAx. [phone]
WWW.MICROBIOSERVICES.COM
FLDOH E82924, ISO 17025:2017 L2422, PADEP: 68-03950, AZDHS:AZO820, EPA FLO 1 147
THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES
HaC-MRA AJAB

Client: Branch Residuals and Soils
Analysis: Salmonella
Project Name: Marcal Cordova NC
Client Sample ID: M7
BCS Sample ID: 2304216 Sample Description: Biosolid
Date Received: April 18, 2023 9:51 Amount Submitted: 100 m L BCS bottle %Solids: 41.8
Amount Analyzed: 3.00E+01 g Receipt Temperature: 4.9 deg C Preserved: Yes
Analysis Start: April 18,2023 10:15 Analysis Stop Date: April 25, 2023 11:30
Analyst: Wei -yea Hsu, M.S. Qualifier: U
Primary Value: :50.07 Salmonella MPN/mL sample analyzed
Secondary Value: :50.6 Salmonella MPN/4 dry grams
Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's
detection limit for the amount of sample analyzed as per the method's standard reporting units
Page 5 of 8
Final Report BCS ID 2304210, 2304211, 2304212, 2304213, 2304214, 2304215, 2304216
BCS L.-ABORAI"ORIES, INC. — GAINESVILLE
4609 NW 6TI1 STREE7, STE. A, GAINESVILLE, FLORIDA 32609
["EL. [phone], FAx. [phone]
WWWMICROBIOSERVICES.COM
FLDOH E82924, ISO 17025:2017 L2422, PADEP: 68-03950, AZDHS:AZ0820, EPA FL01 147
THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE. WRITTEN CONSENT OF BCS LABORATORIES
HaC-���7
MRA
1:7 1

Client: Branch Residuals and Soils
Project: K8arca|Cordova N[
Method Detection Limit: 1microorganism/ unit weight orvolume analyzed
Practical OuantitationLimit: 1microorganism/ unit weight orvolume analyzed
Report Notes: Custody Seal Condition: Not Present
Samp|e(s)were received well preserved and inexcellent condition. Samp|e(s)were analyzed following receipt
asper the described analytical methodology. End ofreport notes.
_
Page aofm
BCSLABORATORIES, INC. —GAINEBVILLE
4609 NVV6TxSTREET, STE. A, GA|msSvLLs.FLOR/oA 32609
TEL[phone].F/x.(352)377'5630
WVW.M|CROB|OSERV|CES.COM
FLDOHEB2924.|S017O25:2017L2422.PADEP: 6B-0395D.AZDHB:AZO82Q.EPA FLQ1147
THIS REPORTSHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES
��W��
�aCf�0\ ~~~

I certify that I have examined and I am familiar with the information submitted herein. The results pertain only
to sample(s) identified and their condition at time of receipt. Based on my inquiry of the individuals
responsible for the analysis, I believe the data to be true, accurate, and complete. Sampling and field data was
obtained from submitted documents. The analysis was authorized and commissioned by the client. The
resulting data are representative of the analysis conducted on the material/samples/articles provided by the
client (or client's representative) and it's/their condition at the time of analysis. The sample(s) were analyzed
in accordance with the appropriate method , however due to the inherent limitations of the methods,
microorganisms may avoid detection. BCS Laboratories offers no express or implied warranties concerning
the quality, safety, and/or purity of any sample, batch, source, or the process they are derived from. Quality
assurance controls were performed as outlined in the method and as per Good Laboratory Practices. The
analysis and results presented in this report meet the requirements of the standards of The NELAC Institute
(TNI), ISO 17025, and the FL DOH Environmental Laboratory Certification Program, as applicable unless
otherwise noted.
;i
Signature of Laboratory Director/Authorized Rep. Date: April 27, 2023
Page 7 of 6
Final Report RCS ID 2304210, 2304211, 2304212, 230421.3, 2304214, 2304215, 2304216
BCC LABORATORIES, INC. •— GAINESVILLE
4609 NW 6TH STREET, STE.. A, GAINE.SVILLE., FLORIDA 3260
TEL. [phone], FAX. [phone]
VVWW.MICROBIOSERVICES.COM
F"LDOH E82924, ISO 1702 5:2017 L2422, PADEP: 68-03950, AZDHS:AZ0820, EPA FLO 1 147
THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BC:S LABORATORIES
11- , w 614
zj b

SYMBOL MEANING
B Results based oncounts outside the acceptable range.
Sample received without prior notification or delayed delivery. Analysis performed outside of
associated method required QC data set (I QC data set per 20 samples per 168 hours).
| Value is between the laboratory method detection limit & the practical quantitation limit.
]1 The sample matrix interfered with the ability to make any accurate determination.
]2 NoQuality Control criteria exist for the component.
]S The data are questionable because of improper laboratory or field protocols.
L Off scale high. Actual value isknown tobegreaterthanvalue given.
N Presumptive evidence forthe presence of material. There is an indication thatthe analyte is
present, but the confirmation requirement was not met.
O Sampled, but analysis not performed.
O Sample held beyond the accepted holding time.
U Indicates that the compound was analyzed for but not detected. The specified component was
not detected. The reported value isthe method detection limit.
V Ana|ytewas detected inboth sample and the method blank. Data may not be accurate.
Y Laboratory analysis was from an improperly preserved sample; the data may not be accurate
Z '
Too many colonies present (TNTC); the numeric value given represents the upper end of the
value that can bedetermined based onthe volume.
? re
jected
Presence orabsence ofana|ytecould not beconfirmed.
** Not reported due 1ointerference.
^ Sampling container supplied by client. Sterility can not be confirmed by B[5.
# B[S Lab specific qualifier. See laboratory analysis notes.
Page auvo
BCSLABORA-FOR|ES.INC. —GAINEBVLLE
4609NVV6TH STREET, ETE.A.GAIwsSvLLE.FLORIDA 32609
TEL�C552>377-9272.FAX. (352)377'563O
VVWW.M[CROB(OSEBV|CES.COK«
FLDOHE82924.ISO 17D25:2017L2422.PADEP: 6B-0395g.AZOHS:4ZOB2D.EPA FLO1?47
THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES
AtIAB
~_
*���0�

Date Sampled
Time Sampled
MEN
MEN mom
mom
0
NNEM
M
MEMO
NTempe
rature at collection
-
thiosulfate added
mom no WSodium
MENNEN
1f;;41 �
MENNEN
in
ME11"IM112
MENNEN
ME
MMMMMMMMN!
Drinking Water
M Bloom
No MEN
Ja
—WIN
Branch Residuals and Soils
10. 110*41M.07—sm"M M.
-j
M7
2304216
fD
04118/20239:51
Fecal coliform
'X, ro
ID ID
Helminth Ova
',�almonella
03 OM
spp/,;�
2 �<
CD In
@
�Total Coliform
0 SL
KS.
R
0
w—
— ------- — --- — ---
Plate Count Bacteria (HPC)
@ @
n
n
t
M
:r
;.
i. ------- - - ---
i '
I egionella CDC method
15 g C4, M
5: - Ci
CIO
U,
r "
ri . 0 2
ia V, a
0 ::
-11 .
-Enterococcus IDEXX
or-,
"
;r
0
CIA
0
0
0
Yeast and Mold
0
CA
1615 RT-qPCR tests..
Branch Residuals and Soils
-_EPA
--.-
I
6 __L1
CL
M4
z z 1
2304213
OV1812023 9:51
RUSH TAT (Fee Applies)

Marcal Cordova, LLC
Cordova, NC
City ofllockingham [UP 0015
Jun-23
Biological Consulting. Services
Lab #€
Date Analysed
Primary Value Salmonella
Secondary Value �almonellat
MPN pet- ml '
�IPIV per 4 grams;1)
.0.8
2305237
5/20,/23
< 0.07
_
2305238
5/20/23
0.07:0.8
2305239
5/20/23
< 0,07
0.8
2305240
5/20/23
10.07
< 0.7
2305241
5/20/23
:: 0.07
�, 0.8
2305242
5/20/23
0.07
C1.8
2305243
5/20/23
0.07
0.7
E ceedances
All Samples are less then 3 MPN per 4 grams dry weight. Samples meet Class A pathogen
requirement for distribution.
Data provided in this summary have been used for the values oMonthly Pathogen
Reductionand Vector Attraction option.

Boological Consulting Services
"V 1Y 1
Of North Florida, Inc.
May 23, 2023
Robert Branch
Branch Residuals and Soils
1735 Heckle Blvd. Suite 103-291
Rockhill SC 29732
336-312-9007
[e-mail]
Client ID: M1, M2, M3, M4, M5, M6, M7
BCSID: 2305237,2305238,2305239,2305240,2305241,2305242,2305243
Dear Robert Branch,
We have completed the analysis of the submitted samples as outlined below.
Analysis Method
Salmonella EPA 1682; BCS SOP M-4 (ISO17025 and TNI Accredited)
Should you have any questions, please do not hesitate to contact me.
Sincerely,
Bonnie Mull, MPH
Laboratory Operations Manager
Page I of 8
Final Report BCS ID 2305237, 2305238, 2305239, 2305240, 2305241, 2305242, 2305243
BCS LABORATORIES, INC. — GAINESVILLE
4609 NW 6T'FI STREET, STE. A, GAINESVILLE, FLORIDA 32609
TEL. [phone], FAX- [phone]
WWW.MICROBIOSERVICES.COM
FLDOH E82924, ISO 17025:2017 1-2422, PADEP: 68-03950, AZDHS:AZO820, EPA FLO 1 147
THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT T14E WRITTEN CONSENT OF BCS LABORATORIES
RZIG-MRA

Client: Branch Residuals and Soils
Analysis: Salmonella
Project Name: Marcal Cordova NC
Client Sample ID: M1
BCS Sample ID: 2305237
Date Received: May 17, 2023 9:50
Amount Analyzed: 3.01E+01 g
Analysis Start: May 17, 2023 10:32
Analyst: Catherine Dixon, B.S.
-Neceipt Temperature: 0.5 deg C Preserved: Yes
Analysis Stop Date: May 20, 2023 10:21
Primary Value: :50.07 Salmonella MPN/mL sample analyzed
Secondary Value: :50.8 Salmonella MPN/4 dry grams
Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's
detection limit for the amount of sample analyzed as per the method's standard reporting units
Client: Branch Residuals and Soils
Analysis: Salmonella
Project Name: Marcal Cordova NC
BCS Sample ID:
Date Received:
eloub w10,2 &;I& 'I,
Analysis Start:
Analyst: I
May 17, 2023 9:50
3.01E+01 g
May 17, 2023 10:32
Cat'ieri-te
I
07�11 10111
FT1705M M,
Receipt Temperature: 0.5 deg C Preserved: Yes
Analysis Stop Date: May 20, 2023 10:21
Primary Value: :50.07 Salmonella MPN/mL sample analyzed
Secondary Value: 50.8 Salmonella MPN/4 dry grams
Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's
detection limit for the amount of sample analyzed as per the method's standard reporting units
Page 2 of 8
Final Report BCS ID 2305237, 2305238, 2305239, 2305240, 2305241, 2305242, 2305243
BCC LABORATORIES, INC. — GAINESVILLE
4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609
TEL. [phone], FAx- [phone]
WWW.MICROBIOSERVICE'.S.COO
FLDOH E82924, ISO 17025:2017 L2422, PADEP: 68-03950, AZDHS:AZO820, EPA FLO 1 147
THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT oF BCS LABORATORIES
RaC-MRA -AJA0

Client: Branch Residuals and Soils
Analysis: Salmonella
Project Name: Marcal Cordova NC
Client Sample ID: M3
BCS Sample ID: 2305239 Sample Description: biosolid
Date Received: May 17, 2023 9:50 Amount Submitted: 100 ml BCS bottle %Solids: 33.6
Amount Analyzed: 2.99E+01 g Receipt Temperature: 0.5 deg C Preserved: Yes
Analysis Start: May 17, 2023 10:32 Analysis Stop Date: May 20, 2023 10:21
Analyst: Catherine Dixon, B.S. Qualifier: U
Primary Value: :50.07 Salmonella MPN/mL sample analyzed
Secondary Value: 50.8 Salmonella MPN/4 dry grams
Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's
detection limit for the amount of sample analyzed as per the method's standard reporting units
Client: Branch Residuals and Soils
Analysis: Salmonella
Project Name: Marcal Cordova NC
Client Sample ID: M4
krf�lffl
BCS Sample ID: 2305240 Sample Description: biosolid
Date Received: May 17, 2023 9:50 Amount Submitted: 100 ml BCS bottle %Solids: 36.9
Amount Analyzed: 3.01E+01 g Receipt Temperature: 0.5 deg C Preserved: Yes
Analysis Start: May 17, 2023 10:32 Analysis Stop Date: May 20, 2023 10:21
Analyst: Catherine Dixon, B.S. Qualifier: U
Primary Value: 50.07 Salmonella MPN/mL sample analyzed
Secondary Value: 50.7 Salmonella MPN/4 dry grams
Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's
detection limit for the amount of sample analyzed as per the method's standard reporting units
Page 3 of 8
Final Report BCS ID 2305237, 2305238, 2305239, 2305240, 2305241, 2305242, 2305243
BCS LABORATORIES, INC. — GAINESVILLE
4609 NVV 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609
TEL. [phone], FAX. [phone]
WWW.MICROBIOSERVICES.COM
FLDOH E82924, ISO 17025:2017 L2422, PADEP: 68-03950, AZDHS:AZO820, EPA FLO 1 147
THIS REPORTSHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES
RaC-WA

Client:
Branch Residuals and Soils
Analysis:
Salmonella
Project Name:
Marcal Cordova NC
Client Sample ID:
M5 Sample Date/Time: May 16, 2023 12:52
BCS Sample ID:
2305241 Sample Description: biosolid
Date Received:
May 17, 2023 9:50 Amount Submitted: 100 ml BCS bottle %Solids: 32.0
Amount Analyzed:
3.01E+01 g Receipt Temperature: 0.5 deg C Preserved: Yes
Analysis Start:
May 17, 2023 10:32 Analysis Stop Date: May 20, 2023 10:21
Analyst:
Catherine Dixon, B.S. Qualifier: U
Primary Value:
:50.07 Salmonella MPN/mL sample analyzed
Secondary Value:
50.8 Salmonella MPN/4 dry grams
Analysis Notes: Undetected:
Analyte was not detected in the sample analyzed; Value represents the method's
detection limit for the amount of sample analyzed as per the method's standard reporting units
Client:
Branch Residuals and Soils
Analysis:
Salmonella
Project Name:
Marcal Cordova NC
Client Sample ID:
M6 Sample Date/Time: May 16, 2023 12:53
BCS Sample ID:
2305242 Sample Description: biosolid
Date Received:
May 17, 2023 9:50 Amount Submitted: 100 ml BCS bottle %Solids: 34.0
Amount Analyzed:
3.01E+01 g Receipt Temperature: 0.5 deg C Preserved: Yes
Analysis Start:
May 17, 2023 10:32 Analysis Stop Date: May 20, 2023 10:21
Analyst:
Catherine Dixon, B.S. Qualifier: U
Primary Value:
150.07 Salmonella MPN/mL sample analyzed
Secondary Value:
50.8 Salmonella MPN/4 dry grams
Analysis Notes: Undetected:
Analyte was not detected in the sample analyzed; Value represents the method's
detection limit for the amount of sample analyzed as per the method's standard reporting units
Page 4 of 8
Final Report BCS ID 2305237, 2305238, 2305239, 2305240, 2305241, 2305242, 2305243
BCS LABORATORIES, INC. - GAINESVILLE
4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609
TEL. [phone], FAx- [phone]
WWW.MICROBIOSERVICES.COM
FLDOH E62924, ISO 17025:2017 L2422, PADEP: 68-03950, AZDHS:AZO820, EPA FLO 1 147
THIS REPORT SHALL NOT BE REPRODUCED. EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES
RaC-MRA AJAB
"Po

Client: Branch Residuals and Soils
Analysis: Salmonella
Project Name: Marcm|[ordova N[
Client Sample |D: K87 Sample Date/Time: May 16 3023 12:58
B[SSample ID: 2305I43 Sample Description: bioso|id
Date Received: May 17,2O23 9:50 Amount Submitted: 1QOm|B[Sbottle %So|ids: 35.8
Amount Analyzed: 3.01E+01 g Receipt Temperature: 0.6 deg[ Preserved: Yes
Analysis Start: May 17,2O23 10:32 Analysis Stop Date: May J1,2OZ3 10:09
Analyst: Catherine Dixon, B.S. Qualifier: U
Primary Value: 150.07 Salmonella MPN/mLsample analyzed
Secondary Value: :50J Salmonella K4PM/4dry grams
Analysis Motes: Undetected: Ana|yte was not detected in the sample analyzed; Value represents the method's
detection limit for the amount of sample analyzed as per the method's standard reporting units
Page soxw
BCSLABORATORIES, INC. —GANESVILLE
4609 NW 6THSTREET, BTE.4+GmmEsv|LLE.FLORIDA 32609
TEL(352) 377'9272.FAx-[phone]
VY\NW.M(CRCJB|OSERV|CEB.CC)x&
FLDOHE82924.ISO 17O25:2017L2422.PADEP: 68-0395O.4ZDHS:/ZDB20.EPA FLD1 147
THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES
'
' �
���^���.�

Client: Branch Residuals and Soils
Project: Marcal Cordova NC
Method Detection Limit: 1 microorganism/ unit weight or volume analyzed
Practical Quantitation Limit: 1 microorganism/ unit weight or volume analyzed
Report Notes: Custody Seal Condition: Not Present
Sample(s) were received well preserved and in excellent condition. Sample(s) were analyzed following receipt
as per the described analytical methodology. End of report notes.
Page 6 of &
Final Report PC5 ID 2305237, 2305238, 2305239, 2305240, 2305241, 2305242, 2305243
BCS LABORATORIES, INC:. --- GAINESVILLE
4609 NW 6TH STREET, STE. A, G AINESVILLE, FLORIDA 32609
TEL. [phone], FAx. (3 s2) 377-563 7
WWW.MICROBIOSERVICES.COM
F"LDOH E82924, ISO 17025:2017 L2422, PADEP: 68-039 0, AZDHS: _. O82 0, EPA F'LO 1 147
TmS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUTTHE WRITTEN CONSENT OF BC;S LABORATORIES
1x aka se ..,,, ..... �
u
1 „P

I certify that I have examined and I am familiar with the information submitted herein. The results pertain only
to sample(s) identified and their condition at time of receipt. Based on my inquiry of the individuals
responsible for the analysis, I believe the data to be true, accurate, and complete. Sampling and field data was
obtained from submitted documents. The analysis was authorized and commissioned by the client. The
resulting data are representative of the analysis conducted on the material/samples/articles provided by the
client (or client's representative) and it's/their condition at the time of analysis. The sample(s) were analyzed
in accordance with the appropriate method , however due to the inherent limitations of the methods,
microorganisms may avoid detection. BCS Laboratories offers no express or implied warranties concerning
the quality, safety, and/or purity of any sample, batch, source, or the process they are derived from. Quality
assurance controls were performed as outlined in the method and as per Good Laboratory Practices. The
analysis and results presented in this report meet the requirements of the standards of The NELAC Institute
(TNI), ISO 17025, and the FL DOH Environmental Laboratory Certification Program, as applicable unless
otherwise noted.
�l
Signature of Laboratory Director/Authorized Rep Date: May 23, 2023
Page 7 of E
Final Report BCS ID 2305237, 2305238, 2305239, 2305240, 2305241, 2305242, 2305243
BCS LABORATORIES, INC. —° GAINESVILLE
4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 02600
TEL. [phone], HAS. [phone]
WWW.MICROBIOSERVICES.COM
F'LDOH E82924, ISO 17025:201 7 L2422, FADER 68-03950, AZDHS:AZO820, EPA F'LO1 147
THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES
flaC-MRA

SYMBOL MEANING
B Results based on counts outside the acceptable range.
X Sample received without prior notification or delayed delivery. Analysis performed outside of
associated method required QC data set (1 QC data set per 20 samples per 168 hours).
I Value is between the laboratory method detection limit & the practical quantitation limit.
J1 The sample matrix interfered with the ability to make any accurate determination.
J2 No Quality Control criteria exist for the component.
J3 The data are questionable because of improper laboratory or field protocols.
L Off scale high. Actual value is known to be greaterthan value given.
N Presumptive evidence forthe presence of material. There is an indication that the analyte is
present, but the confirmation requirement was not met.
O Sampled, but analysis not performed.
Q Sample held beyond the accepted holding time.
U Indicates that the compound was analyzed for but not detected. The specified component was
not detected. The reported value is the method detection limit.
V Analyte was detected in both sample and the method blank. Data may not be accurate.
Y Laboratory analysis was from an improperly preserved sample; the data may not be accurate
Z Too many colonies present (TNTC); the numeric value given represents the upper end of the
value that can be determined based on the volume.
7 Data are rejected and should not be used. QC data for analyte did not meet acceptance criteria.
Presence or absence of analyte could not be confirmed.
** Not reported due to interference.
A Sampling container supplied by client. Sterility can not be confirmed by BCS.
# BCS Lab specific qualifier. See laboratory analysis notes.
Page 8 of 8
Final Report BCS ID 2305237, 2305238, 2305239, 2305240, 2305241, 2305242, 2305243
BCS LABORATORIES, INC. — GAINESVILLE
4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609
TEL. (:352) 77-0272, FAx. [phone]
WWW.MICROBIOSERVICES.COM
F'LDOFI E62924, ISO 17025:2017 L2422, PADEP: 68-03 S0, AZDHS:AZO820, EPA F'LO 1 147
THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN PULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES
AAB
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Mareal Cordova, Elf,;"
Cordova, NC
City of Rockingham ICP' 001
Jul-23
Biological Consulting Services
Date Analyzed
Pr nary V,a u- Salm l at'
MPN per aril
Sect) dAry Value Silrnonella'
NIP l� !per 4 grams(Dry
2306298
7/3/23
< 0.07
0.8
2306299
7/3/23
< 0.07
< 0.8
2306300
7/3/23
< 0.07
< 0.8
2306301
7/3/23
< 0.07
< 0.8
2306302
7/3/23
m 0.07
0.8
2306303
7/3/23
5 0.07
0.8
2306304
7/3/23
<". 0.07
< 0.8
Exeeedanees 0'
All Samples are less then 3 MPN per 4 grams dry weight. Samples meet Class A pathogen
requirement for distribution.
VectorData provided in this summary have been used for the values reported on the Arionthly Pathogen -
Reduction i

Mological -V
Of North Florida, Inc.
Consulting Services
Robert Branch
Branch Residuals and Soils
1735 Heckle Blvd. Suite 103-291
Rockhill SC 29732
336-312-9007
[e-mail]
Client ID: M1, M2, M3, M4, M5, M6, M7
11, naTe compieteo ne ana-
Project Name: Marcal Cordova NC
Analysis Method
Salmonella EPA 1682; BCS SOP M-4 (ISO17025 and TNI Accredited)
Sincerely,
Bonnie Mull, MPH
Laboratory Operations Manager
Page 1 of 8
Final Report BCS ID 2306298, 2306299, 2306300, 2306301, 2306302, 2306303, 2306304
BCS LABORATORIES, INC. — GAINESVILLE
4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609
TEL. [phone], FAX. [phone]
WWW.MICROBIOSERVICES.COM
I:-'LDOH E82924, ISO 17025:2017 L2422, PADEP: 68-03950, AZDHS:AZO820, EPA FLO 1 147
THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES
we
HaC-MRA A&B

Client: Branch Residuals and Soils
Analysis: Salmonella
Project Name: Marcal Cordova NC
Client Sample ID: M1 Sample Date/Time: June 27, 2023 12:50
BCS Sample ID: 2306298 Sample Description: biosolid
Date Received: June 28, 2023 9:53 Amount Submitted:100 ml BCS bottle % Solids: 32.9
Amount Analyzed: 3.01E+01 g Receipt Temperature: 4.4 deg C Preserved: Yes
Analysis Start: June 28, 2023 10:30 Analysis Stop Date: July 03, 2023 12:17
Analyst: Catherine Dixon, B.S. Qualifier: U
Primary Value: :50.07 Salmonella MPN/mL sample analyzed
Secondary Value: :50.8 Salmonella MPN/4 dry grams
Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's
detection limit for the amount of sample analyzed as per the method's standard reporting units
Client: Branch Residuals and Soils
Analysis: Salmonella
ProjectName: Marcal Cordova NC
Client Sample I: M2 Sample Date/Time: June 27, 2023 1:51
BCS Sample I: 2306299 Sample Description: biosolid
Date Received: June 28, 2023 9:53 Amount Submitted: 1 ml BCS bottle % Solids: 31.4
Amount Analyzed: 2.99E+01 g Receipt Temperature: 4.4 deg C Preserved: Yes
Analysis Start: June 28, 22 10:30 Analysis Stop Date: July 0, 202 1:17
Analyst: Catherine Dixon, B.S.Qualifier: U
Primary Value: :50.07 Salmonella /mL sample analyzed
Secondary Value: 50.8 Salmonella MPN/4 dry grams
Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's
detection limit for the amount of sample analyzed as per the method's standard reporting units
Page 2 of 8
Final Report BCS I® 2306298, 2306299, 2306300, 2306301, 2306302, 2306303, 2306304
BCS LABORATORIES, INC. — GAINESVILLE
4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 3260
TEL. [phone], F (352) 377- 630
WWW.MICROBIOSERVICES.COM
FLDOH E132924, ISO 1702 s:2017 L2422, PADEP. 68-039 s0, AZDHS:AZO820, EPA FLO 1 147
THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHi7'.. T THE WRITTEN CONSENT OF BCS LABORATORIES
11s
pro'

Client: Branch Residuals and Soils
Analysis: Salmonella
Project Name: Marcal Cordova NC
Client Sample ID: M3
Sample Date/Time: June 27, 2023 12:53
BCS Sample ID: 2306300 Sample Description: biosolid
Date Received: June 28, 2023 9:53 Amount Submitted:100 ml BCS bottle % Solids: 31.5
Amount Analyzed: 3.00E+01 g Receipt Temperature: 4.4 deg C Preserved: Yes
Analysis Start: June 28, 2023 10:30 Analysis Stop Date: July 03, 2023 12:17
Analyst: Catherine Dixon, B.S. Qualifier: U
Primary Value: :50.07 Salmonella MPN/mL sample analyzed
Secondary Value: :90.8 Salmonella MPN/4 dry grams
Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's
detection limit for the amount of sample analyzed as per the method's standard reporting units
Client: Branch Residuals and Soils
Analysis: Salmonella
Project Name: Marcal Cordova NC
Client Sample I:
• �,
BCS Sample I: 23001 Sample Description: biosolid
Date Received: June 28, 2023 9:53 Amount Submitted: 10 ml BCS bottle % Solids: 31.8
Amount Analyzed: 3.00E+1 g Receipt Temperature: 4.4 deg C Preserved: Yes
Analysis Start: June 28, 202 10:30 Analysis Stop ate: July 03, 202 12:17
Analyst: Catherine Dixon, B.S.Qualifier: U
Primary Value: 5.07 Salmonella /L sample analyzed
Secondary Value: 0.8 Salmonella MPN/4 dry grams
AnalysisNotes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's
detection limit for the amount of sample analyzed as per the method's standard reporting units
Page 3 of 6
Rnal Report BCS I0 2306298, 2306299, 2306300, 2306301, 2306302, 2306303, 2306304
BCS LABORATORIES, INC. — GAINESVILLE
4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609
TEL. [phone], FAx. [phone]
WWW.MICROBIOSERVICES.COM
FLDOH EE2924, ISO 17025:2017 L2422, PADEP: 68-03950, AZDHS:AZO820, EPA FLO 1 147
THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN PULL. WITHOUT THE `✓ BITTEN CONSENT OF BCS LABORATORIES
AAAB
NaC-MRA

Client: Branch Residuals and Soils
Analysis: Salmonella
Project Name: Marcal Cordova NC
Client Sample ID: M5
Sample Date/Time: June 27, 2023 12:57
BCS Sample ID: 2306302 Sample Description: biosolid
Date Received: June 28, 2023 9:53 Amount Submitted:100 ml BCS bottle % Solids: 32.5
Amount Analyzed: 2.99E+01 g Receipt Temperature: 4.4 deg C Preserved: Yes
Analysis Start: June 28, 2023 10:30 Analysis Stop Date: July 03, 2023 12:17
Analyst: Catherine Dixon, B.S. Qualifier: U
Primary Value: 50.07 Salmonella MPN/mL sample analyzed
Secondary Value: :50.8 Salmonella MPN/4 dry grams
Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's
detection limit for the amount of sample analyzed as per the method's standard reporting units
Client: Branch Residuals and Soils
Analysis: Salmonella
Project Name: Marcal Cordova NC
Client Sample I: M6
CS Sample ID: 2306303 Sample Description: biosolid
Date Received: June 2, 20 9:53 Amount Submitted: 1 ml BCS bottle % Solids: 31.4
Amount Analyzed: 3.00E+01 g Receipt Temperature: 4.4 deg C Preserved: Yes
Analysis Start: June 28, 2023 10:30 Analysis Stop Date: July OS, 2023 13:44
Analyst: Catherine Dixon, B.S.Qualifier: U
Primary Value: :50.07 Salmonella /L sample analyzed
Secondary Value: 50.8 5almonellaMPN/4 dry grams
Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's
detection limit for the amount of sample analyzed as per the method's standard reporting units
Page 4 of B
Final Report BCS ID 2306298, 2306299, 2306300, 2306301, 2306302, 2306303, 2306304
BCS LABORATORIES, INC. - GAINESVILLE
4609 NW 6TH .STREET, STE. A, GAINESVILLE, FLORIDA 32609
TEL. [phone], FAx. [phone]
WWW.MICROBIOSERVICES.COM
F'LDOH E 2924, ISO 17025:2017 L2422, PADEP: 68-03950, AZDHS:AZO820, EPA F'LO 1 147
THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, wITHOUT'T'HE WRITTEN CONSENT OF BCS LABORATORIES
ilea
i"

Client: Branch Residuals and Soils
Analysis: Salmonella
Project Name: K8anca|Cordova N[
Client Sample ID: M7
B[S Sample ID: 2306304 Sample Description: biosoid
Date Received: June 28,2O23 9:53 Amount Submitted: 1OOm|B[Sbottle 0So|ids: 31.6
Amount Analyzed: 38OE+01Q Receipt Temperature: 4.4deg [ Preserved: Yes
Analysis Start: June Z8,2OZ3 10g0 Analysis Stop Date: July O],ZD23 13:17
Analyst: Catherine Dixon, B.S. Qualifier: U
Primary Value: :50.07 Salmonella MP0/mLsample analyzed
Secondary Value: 150.8 Salmonella MP0/4 dry grams
Analysis Notes: Undetected: Ana(ytevvas not detected in the sample analyzed; Value represents the method's
detection limit for the amount of sample analyzed as per the method's standard reporting units
Page sofa
E3CSLABORATORIES, INC. --GA|NESV|LLE
4609P4W 6TxSTREET, STE. A, GmmESvLLE.FLORIDA 32609
TEL. [phone].FAx-(352)377'563D
VVWW.M[CROB|OSER\/|CES.COM
FLDO8E82924.ISO ?7Q25:2V17L2422.pADEF: 68'03950.AZDHS:AZO820.EPA FLO1147
THIS REPORT SHALL NOT BsREPRODUCED, EXCEPT /mFULL, WITHOUT THE we/rrswCONSENT oreCS LxooeATOn/ss
I Kok,
. ` &
,__�__,iv

Client: Branch Residuals and Soils
Project: Marcal Cordova NC
Method Detection Limit: 1 microorganism/ unit weight or volume analyzed
Practical Quantitation Limit: 1 microorganism/ unit weight or volume analyzed
Report Notes: Custody Seal Condition: Not Present
Sample(s) were received well preserved and in excellent condition. Sample(s) were analyzed following receipt
as per the described analytical methodology. End of report notes.
Page 6 of B
Final Report BC5 ID 2306298, 2306299, 2306300, 2306301, 2306302, 2306303, 2306304
IBC i LABORATORIES, INC. —° GAINE: SVIL.L.E
4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609
TEL. [phone], FAQ. (3 a2) 77-5630
WWW.MICROBIOSERVICES.COM
FLCBOH E82924, ISO17025:2017 L2422, PADEP: 68-039 0, AZDHS:AZO820, EPA FLO1 147
THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCC LABORATORIES
it- . A ��

I certify that I have examined and I am familiar with the information submitted herein. The results pertain only
to sample(s) identified and their condition at time of receipt. Based on my inquiry of the individuals
responsible for the analysis, I believe the data to be true, accurate, and complete. Sampling and field data was
obtained from submitted documents. The analysis was authorized and commissioned by the client. The
resulting data are representative of the analysis conducted on the material/samples/articles provided by the
client (or client's representative) and it's/their condition at the time of analysis. The sample(s) were analyzed
in accordance with the appropriate method , however due to the inherent limitations of the methods,
microorganisms may avoid detection. BCS Laboratories offers no express or implied warranties concerning
the quality, safety, and/or purity of any sample, batch, source, or the process they are derived from. Quality
assurance controls were performed as outlined in the method and as per Good Laboratory Practices. The
analysis and results presented in this report meet the requirements of the standards of The NELAC Institute
(TNI), ISO 17025, and the FL DOH Environmental Laboratory Certification Program, as applicable unless
otherwise noted.
r
Signature of Laboratory Director/Authorized Rep. Date: July 10, 2023
Page 7 of 8
Final Report BCS ID 2306298, 2306299, 2306300, 2306301, 2306302, 2306303, 2306304
BCS LABORATORIES, INC. — GAINESVILLE
4609 NW 6TH STREET, CTE. A, GAINESVILLE, FLORIDA 32609
TEL. [phone], FAX. [phone]
WWW.MICROBIOSERVICES.COM
FLC>OH E82924, ISO 1702 a:2017 L2422, PADEP: 8-03 0, AZDHS:AZ0820, EPA FLO 1 147
THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES
,,yy
,° Ja(lIU

B Results based on counts outside the acceptable range.
X Sample received without prior notification or delayed delivery. Analysis performed outside of
associated method required QC data set (1 QC data set per 20 samples per 168 hours).
I Value is between the laboratory method detection limit & the practical quantitation limit.
J1 The sample matrix interfered with the ability to make any accurate determination.
J2 No Quality Control criteria exist forthe component.
J3 The data are questionable because of improper laboratory orfield protocols.
L Off scale high. Actual value is known to be greater than value given.
N Presumptive evidence forthe presence of material. There is an indication that the analyte is
present, but the confirmation requirement was not met.
O Sampled, but analysis not performed.
Q Sample held beyond the accepted holding time.
U Indicates that the compound was analyzed for but not detected. The specified component was
not detected. The reported value is the method detection limit.
V Analyte was detected in both sample and the method blank. Data may not be accurate.
Y Laboratory analysis was from an improperly preserved sample; the data may not be accurate
Z Too many colonies present (TNTC); the numeric value given represents the upper end of the
value that can be determined based on the volume.
7 Data are rejected and should not be used. QC data for analyte did not meet acceptance criteria.
Presence or absence of analyte could not be confirmed.
** Not reported due to interference.
^ Sampling container supplied by client. Sterility can not be confirmed by BCS.
# BCS Lab specific qualifier. See laboratory analysis notes.
Page & of &
Final Report BCS ID 2306298, 2306299, 2306300, 2306301, 2306302, 2306303, 2306304
BCS LABORATORIES, INC. — GAINESVILLE
4609 NW 6TH STREET, STE. A, GAINE SVILLE, FLORIDA 32609
TEL. [phone], FAQ. [phone]
WWW.MICROBIOSERVICES.COM
FLDOH E82924, ISO 17025:2017 L2422, PADEP: 68-03950, AZDHS:AZO820, EPA FLO 1 147
THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES
it -t:7
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RUSH TAT (Fee Applies)
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Marcal Cordova, LLC
Cordova, NC
City of Rockingham IUP 0015
Aug-23
Biological Consulting Services
Lab'.9
Date analyzed
Primary Value Salmonella
MPN per ml
Secondar -,Value Salmonella'
MPN per 4 grams Dry
2308024
8/08/23
< 0.07
< 0.7
2308025
8/08/23
< 0.07
< 0.7
2308026
8/08/23
< 0.07
<_ 0.7
2308027
8/08/23
< 0.07
< 0.6
2308028
8/08/23
< 0.07
< 0.7
2308029
8/08/23
< 0.07
< 0.7
2308030
8/08/23
< 0.07
< 0.7
Exceedances 1 U
All Samples are less then 3 MPN per 4 grams dry weight. Samples meet Class A pathogen
requirement for distribution.
ReductionData provided in this summary have been used for the values reported on the Monthly Pathogen
and Vector Attraction i

A'
Biological Consulting Services
Of North Florida, Inc.
Robert Branch
Branch Residuals and Soils
1735 Heckle Blvd. Suite 103-291
Rockhill SC 29732
336-312-9007
[e-mail]
Client ID: M1, M2, M3, M4, M5, M6, M7
�*Illalyz ffJ2LL0E+-W1 I
We have completed the analysis of the submitted samples as outlined below.
Project Name: 2014-110
Analysis Method
Salmonella EPA 1682; BCS SOP M-4 (ISO17025 and TNI Accredited)
IV I I'll' Urt&-j"VI-Ir - . r r rfC-cfffcff;'b�-C#FrF*1 Tr ITT 717,7P -Ycn I rAYM
Should you have any questions, please do not hesitate to contact me.
Bonnie Mull, MPH
Laboratory Operations Manager
Page 1 of 8
Final Report BCS ID 2308024, 2308025, 2308026, 2308027, 2308028, 2308029, 2308030
BCS LABORATORIES, INC. — GAINESVILLE
4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609
TEL. [phone], FAx. [phone]
WWW.MICROBIOSERVICES.COM
FLDOH E82924, ISO 17025:2017 1-2422, PADEP: 68-03950, AZDHS:AZO820, EPA FLO 1 147
THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES
11ac-MRA 7N

Client: Branch Residuals and Soils
Analysis: Salmonella
Project Name: 2014-110
Client Sample ID: M1
9ME931M
BCS Sample ID: 2308024 Sample Description: biosolid
Date Received: August 02, 2023 10:01 Amount Submitted: 100 ml BCS bottle %Solids: 38.8
Amount Analyzed: 2.99E+01 g Receipt Temperature: 2.2 deg C Preserved: Yes
Analysis Start: August 02, 2023 12:59 Analysis Stop Date: August 08, 2023 9:38
Analyst: Catherine Dixon, B.S. Qualifier: U
Primary Value: :50.07 Salmonella MPN/mL sample analyzed
Secondary Value: 50.7 Salmonella MPN/4 dry grams
Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's
detection limit for the amount of sample analyzed as per the method's standard reporting units
Client: Branch Residuals and Soils
Analysis: Salmonella
Project Name: 2014-110
Client Sample ID: M2
131EMEEM
BCS Sample ID: 2308025 Sample Description: biosolid
Date Received: August 02, 2023 10:01 Amount Submitted: 100 ml BCS bottle %Solids: 37.2
Amount Analyzed: 199E+01 g Receipt Temperature: 2.2 deg C Preserved: Yes
Analysis Start: August 02, 2023 12:59 Analysis Stop Date: August 08, 2023 9:38
Analyst: Catherine Dixon, B.S. Qualifier: U
Primary Value: 50.07 Salmonella MPN/mL sample analyzed
Secondary Value: 50.7 Salmonella MPN/4 dry grams
Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's
detection limit for the amount of sample analyzed as per the method's standard reporting units
Page 2 of 8
Final Report BCS ID 2308024, 2308025, 2308026, 2308027, 2308028, 2308029, 2308030
BCS LABORATORIES, INC. - GAINESVILLE
4609 NW 6TH STREET', STE. A, GAINESVILLE, FLORIDA 32609
TEL. [phone], FAx. [phone]
WWW.MICROBIOSERVICE S.COM
FLDOH E82924, ISO 17025:2017 L2422, RADER: 68-03950, AZDHSAZO82O, EPA FLO 1 147
THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES
11 1
HaC-MRA
0
!

Client: Branch Residuals and Soils
Analysis: Salmonella
Project Name: 2014-110
Client Sample ID: M3
r.
ME911M
BCS Sample ID: 2308026 Sample Description: biosolid
Date Received: August 02, 2023 10:01 Amount Submitted: 100 ml BCS bottle %Solids: 38.1
Amount Analyzed: 3.01E+01 g Receipt Temperature: 2.2 deg C Preserved: Yes
Analysis Start: August 02, 2023 12:59 Analysis Stop Date: August 08, 2023 9:38
Analyst: Catherine Dixon, B.S. Qualifier: U
Primary Value: :50.07 Salmonella MPN/mL sample analyzed
Secondary Value: 150.7 Salmonella MPN/4 dry grams
Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's
detection limit for the amount of sample analyzed as per the method's standard reporting units
Client: Branch Residuals and Soils
Analysis: Salmonella
Project Name: 2014-110
Client Sample ID: M4
BCS Sample ID: 2308027 Sample Description: biosolid
Date Received: August 02, 2023 10:01 Amount Submitted: 100 ml BCS bottle %Solids: 42.2
Amount Analyzed: 3.00E+01 g Receipt Temperature: 2.2 deg C Preserved: Yes
Analysis Start: August 02, 2023 12:59 Analysis Stop Date: August 08, 2023 9:38
Analyst: Catherine Dixon, B.S. Qualifier: U
Primary Value: :50.07 Salmonella MPN/mL sample analyzed
Secondary Value: :50.6 Salmonella MPN/4 dry grams
Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's
detection limit for the amount of sample analyzed as per the method's standard reporting units
Page 3 of 8
Final Report BCS ID 2308024, 2308025, 2308026, 2308027, 2308028, 2308029, 2308030
BCS LABORATORIES, INC. - GAINESVILLE
4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609
TEL. [phone], FAx. [phone]
WWW.MICROBIOSERVICES.COM
FLDOH E82924, ISO 17025:2017 L2422, PADEP: 68-03950, AZDI-IS:AZO820, EPA FLO 1 147
THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES
At&B
RaC-MRA

Client:
Branch Residuals and Soils
Analysis:
Salmonella
Project Name:
2014-110
Client Sample ID:
M5
BCS Sample ID:
2308028
Date Received:
August 02, 2023 10:01
Amount Analyzed: 3.01E+01 g
Analysis Start:
August 02, 2023 12:59
Analyst:
Catherine Dixon, B.S.
Sample Description: biosolid
Amount Submitted: 100 ml BCS bottle %Solids: 37.7
'Neceipt Temperature: 2.2 deg C Preserved: Yes
Analysis Stop Date: August 08, 2023 9:38
Qualifier: U
Primary Value: :50.07 Salmonella MPN/mL sample analyzed
Secondary Value: :50.7 Salmonella MPN/4 dry grams
Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's
detection limit for the amount of sample analyzed as per the method's standard reporting units
Client: Branch Residuals and Soils
Analysis: Salmonella
Project Name: 2014-110
Client Sample ID: M6
BCS Sample ID: 2308029 Sample Description: biosolid
Date Received: August 02, 2023 10:01 Amount Submitted: 100 ml BCS bottle %Solids: 37.4
Amount Analyzed: 3.00E+01 g Receipt Temperature: 2.2 deg C Preserved: Yes
Analysis Start: August 02, 2023 12:59 Analysis Stop Date: August 08, 2023 9:38
Analyst: Catherine Dixon, B.S. Qualifier: U
Primary Value: :50.07 Salmonella MPN/mL sample analyzed
Secondary Value: :50.7 Salmonella MPN/4 dry grams
Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's
detection limit for the amount of sample analyzed as per the method's standard reporting units
Page 4 of 8
Final Report BCS ID 2308024, 2308025, 2308026, 2308027, 2308028, 2308029, 2308030
BCS LABORATORIES, INC. — GAINESVILLE
4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609
TEL. [phone], FAx. [phone]
WWW.MICROBIOSERVICES.COM
FLDOH E82924, ISO 17025:2017 L2422, PADEP: 68-03950, AZDHS:AZO820, EPA FLO 1 147
THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES
7N
RaC-MRA

Client: Branch Residuals and Soils
Analysis: Salmonella
Project Name: 2014'110
Client Sample ID: K47 Sample Date/Time:August O1,3O23 13:34
B[SSample ID: 2]080]0 Sample Description: biosoid
Date Received: August O3,3O23 10:01 Amount Submitted: 1OOm|B[Sbottle %So|ids: 38.6
Amount Analyzed: 3.00E+01 g Receipt Temperature: 2.2 deg[ Preserved: Yes
Analysis Start: August OZ,2OZ3 12:59 Analysis Stop Date: August O8,2OZ3 9:38
Analyst: Catherine Dixon, B.S. Qualifier: U
Primary Value: g0.07 Salmonella W4P0/mLsample analyzed
Secondary Value: :50J Salmonella MPN/4dry grams
Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's
detection limit for the amount of sample analyzed as per the method's standard reporting units
_
Page soxo
BCSLABORATORIES, INC. —GANESVILLE
4609NW 6TxSTREET, STE. A, GAINESvLLE.FuoR/oA 32609
TEL. (352)377^9272.FAK(352)377'563O
WwW.M{CROBlOSERV!CES.CO&4
FLDC)HEB2924.ISO 77025:2017L2422.PADEP: 68-Q385V.AZDHS:AZOB20.EPA FLO1147
THIS REPORT SHALL NOT BEREPRODUCED, cxcEpT/wFULL, w�HourTHE wnnTsN ComssmroF ECsL�Onxromss
&

Client: Branch Residuals and Soils
Project: 2014-110
Method Detection Limit: 1 microorganism/ unit weight or volume analyzed
Practical Quantitation Limit: 1 microorganism/ unit weight or volume analyzed
Report Notes: Custody Seal Condition: Not Present
Sample(s) were received well preserved and in excellent condition. Sample(s) were analyzed following receipt
as per the described analytical methodology. End of report notes.
Page 6 of $ _.
Final Report BCC ID 2308024, 2308025, 2308026, 2308027, 2308028, 2308029, 2308030
BCS LABORATORIES, INC. — GAINESVILLE
4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609
TEL. [phone], I"AK (a2) 77-5630
WWW.MICROBIOSERVICES.COM
FL. DOH E82924, ISO 17025:2017 L2422, PADEP: 68-03950, DF IS:AZC3520, EPA FLO 1 147
THIS REPORT SHALL NOT BE REPRODUCED. EXCEPT IN FULL WITHOUT THE WRITTEN CONSENT OF ECS LABORATORIES
HaC- r

I certify that I have examined and I am familiar with the information submitted herein. The results pertain only
to sample(s) identified and their condition at time of receipt. Based on my inquiry of the individuals
responsible for the analysis, I believe the data to be true, accurate, and complete. Sampling and field data was
obtained from submitted documents. The analysis was authorized and commissioned by the client. The
resulting data are representative of the analysis conducted on the material/samples/articles provided by the
client (or client's representative) and it's/their condition at the time of analysis. The sample(s) were analyzed
in accordance with the appropriate method , however due to the inherent limitations of the methods,
microorganisms may avoid detection. BCS Laboratories offers no express or implied warranties concerning
the quality, safety, and/or purity of any sample, batch, source, or the process they are derived from. Quality
assurance controls were performed as outlined in the method and as per Good Laboratory Practices. The
analysis and results presented in this report meet the requirements of the standards of The NELAC Institute
(TNI), ISO 17025, and the FL DOH Environmental Laboratory Certification Program, as applicable unless
otherwise noted.
• . ..., . . _ . . • .
Date: August 08, 2023
Page 7 of 8
Final Report BCS ID 230€3024, 2308025, 2308026, 2308027, 2308028, 2308029, 2308030
BCS I_.ABORA-rol'RIES, INC. - GAINESVILLE
4609 NW 6TH STREET, STE. A, GAINE•SVILLE, FLORIDA 32609
T'E.L. [phone], FAx. [phone]
WWW.MICROBIOSERVICES.COM
FLDCOH E€ 2924, IE017025:2017 L2422, PADEP: 68-03950, AZDF-IS:AZO82O, EPA FLO1 147
THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES
,. „ blu",(,
�

r, •i XceLLM
SYMBOL MEANING
B Results based on counts outside the acceptable range.
X Sample received without prior notification or delayed delivery. Analysis performed outside of
associated method required QC data set (1 QC data set per 20 samples per 168 hours).
I Value is between the laboratory method detection limit & the practical quantitation limit.
J1 The sample matrix interfered with the ability to make any accurate determination.
J2 No Quality Control criteria exist forthe component.
J3 The data are questionable because of improper laboratory orfield protocols.
L Off scale high. Actual value is known to be greaterthan value given.
N Presumptive evidence forthe presence of material. There is an indication thatthe analyte is
present, but the confirmation requirement was not met.
O Sampled, but analysis not performed.
Q Sample held beyond the accepted holding time.
U Indicates that the compound was analyzed for but not detected. The specified component was
not detected. The reported value is the method detection limit.
V Analyte was detected in both sample and the method blank. Data may not be accurate.
Y Laboratory analysis was from an improperly preserved sample; the data may not be accurate
Z Too many colonies present (TNTC); the numeric value given represents the upper end of the
value that can be determined based on the volume.
7 Data are rejected and should not be used. QC data for analyte did not meet acceptance criteria.
Presence or absence of analyte could not be confirmed.
** Not reported due to interference.
A Sampling container supplied by client. Sterility can not be confirmed by BCS.
# BCS Lab specific qualifier. See laboratory analysis notes.
Page 8 of B
Final Report BCS I® 2308024, 2308025, 2308026, 2308027, 2308028, 2308029, 2308030
BCS LABORATORIES, INC. --° GAINE SVILLE
4609 NW CTH STREET, STE. A, GAINESVILLE, FLORIDA 32609
TEL. [phone], I~AK (352) 77-5630
FLDOH 5 2924, ISO 1702 5:20l 7 L2422, PADEP: 68-03950, AZDHS:AZO820, EPA FLO t 147
THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES
ABC- RA

M
M
0
911
M
0
MEN M NINE
Date Sampled
FTime Sampled
I------ ---- -- -
No. of containers shipped
Field Filtered
pH at collection
NNN'Temperature
at collection
MENNEENINaThiosulfate
I
MENE
NUOther
(specify).
MENLWastewater
-------- -----
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Branch Residuals and Soil,
M4
2308027
08/02/2023 10:0l
Branch Residuals and Soils
M5
2308028
08/02/2023 10:01
JIMMEAKI - - - - - -
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9/16/23
9/16/23
9/16/23
9/16/23
9/16/23
9/16/23
9/16/23
Marcal Cordova, LLC
Cordova, NC
City of Rockingham IUP 001.5
Sep-23
Primary Value Salmonella $666-
MPN per.
Exceedances
ner 4 2iriams D.rv::
All Samples are less then 3 MPN per 4 grams dry weight. Samples meet Class A pathogen
requirement for distribution.
Data provided in this summary have been used for the values reported on the Monthly Pathogen
and Vector Attraction Reduction Forms for Class A option.

Biologocal Consulting Servo v I ices
'I4ow- Of North Florida, Inc.
Robert Branch
1735 Heckle Blvd. Suite 103-291
Rockhill SC 29732
336-312-9007
[e-mail]
Client ID: M1, M2, M3, M4, M5, M6, M7
Dear Robert Branch,
We have completed the analysis of the submitted samples as outlined below.
Project Name: 2014.110
Analysis Method
Salmonella EPA 1682; BCS SOP M-4 (ISO17025 and TNI Accredited)
011141,11'Ing, 'J"PT '1111 it o 11- re wo I-E Yn-17 e 41 C 1,= =13117rfe—i
Should you have any questions, please do not hesitate to contact me.
Bonnie Mull, MPH
Laboratory Operations Manager
Page I of 8
Final Report BCS ID 2309088, 2309089, 2309090, 2309091, 2309092, 2309093, 2309094
BCS LABORATORIES, INC. — GAINESVILLE
4609 NW ISTH STREET, STE. A, GAINESVILLE, FLORIDA 32609
TEL. [phone], FAX. [phone]
WWW.MICROBIOSERVICES.COM
FLDOH E82924, ISO 17025:2017 L2422, PADEP: 68-03950, AZDHS:AZO820, EPA FLO 1 147
THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES
ilac-mm

Client: Branch Residuals and Soils
Analysis: Salmonella
Project Name: 2014.110
Client Sample ID: M1
BCS Sample ID: 2309088
Date Received: September 13, 2023 9:5
Amount Analyzed: 2.99E+01 g
Analysis Start: September 13, 2023 11:1
RMATINMEMEN
Sample Description: Biosolid
Amount Submitted: 100 ml bottle %Solids: 371
Receipt Temperature: 3.3 deg C Preserved: Yes
Analysis Stop R. September 16, 2023 13:02
Analyst: Catherine Dixon, B.S. Qualifier: U
Primary Value: :50.07 Salmonella MPN/mL sample analyzed
Secondary Value: 50.7 Salmonella MPN/4 dry grams
Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's
detection limit for the amount of sample analyzed as per the method's standard reporting units
Client:
Branch Residuals and Soils
Analysis:
Salmonella
Project Name:
2014.110
Client Sample ID:
M2
BCS Sample ID:
2309089
Date Received:
September 13, 2023 9:53
Amount Analyzed:
2.99E+01 g
Analysis Start:
September 13, 2023 11:12
r-J5M1�lllMll
Sample Description: Biosolid
Amount Submitted: 100 ml bottle %Solids: 27.2
Receipt Temperature: 3.3 deg C Preserved: Yes
Analysis Stop Date: September 16, 2023 13:02
Analyst: Catherine Dixon, B.S. Qualifier: U
Primary Value: 50.07 Salmonella MPN/mL sample analyzed
Secondary Value: :51.0 Salmonella MPN/4 dry grams
Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's
detection limit for the amount of sample analyzed as per the method's standard reporting units
Page 2 of 8
Final Report BCS ID 2309088, 2309089, 2309090, 2309091, 2309092, 2309093, 2309094
BCS LABORATORIES, INC. — GAINESVILLE
4,609 NW ISTH STREET, STE. A, GAINESVILLE, FLORIDA 32609
TEL. [phone], FAX. [phone]
WWW.MICROBIOSERVICES.COM
FLDOH E82924, ISO 17025:2017 L2422, FADER 68-03950, AZDHS:AZO820, EPA FLO 1 147
THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES
AM
11aC-MRA

Client: Branch Residuals and Soils
Analysis: Salmonella
Project Name: 2014.110
Client Sample ID: M3
Sample Date/Time: September 12, 2023 12:43
BCS Sample ID: 2309090 Sample Description: Biosolid
Date Received: September 13, 2023 9:53 Amount Submitted:100 ml bottle % Solids: 39.5
Amount Analyzed: 3.00E+01 g Receipt Temperature: 3.3 deg C Preserved: Yes
Analysis Start: September 13, 2023 11:12 Analysis Stop Date: September 16, 2023 13:02
Analyst: Catherine Dixon, B.S. Qualifier: U
Primary Value: :50.07 Salmonella MPN/mL sample analyzed
Secondary Value: 50.7 Salmonella MPN/4 dry grams
Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's
detection limit for the amount of sample analyzed as per the method's standard reporting units
Client: Branch Residuals and Soils
Analysis: Salmonella
Project Name: 201.11
Client Sample I
BCS Sample I: 201 Sample Description: Biosolid
Date Received: September 1, 2023 9:53 Amount Submitted: 10 ml bottle % Solids: 26.
Amount Analyzed: 3.00E+1 g Receipt Temperature: 3.3 deg C Preserved: Yes
Analysis Start: September 1, 2023 11:12 Analysis Stop Date: September 1, 22 13:0
Analyst: Catherine Dixon, B.S.Qualifier: U
Primary Value: :50.07 Salmonella N/mL sample analyzed
Secondary Value: 51.0 Salmonella MPN/4 dry grams
Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's
detection limit for the amount of sample analyzed as per the method's standard reporting units
Page 3 of 9
F4,,al Report BCS ICE 2309088, 2309089, 2309090, 2309091, 2309092, 2309093, 2309094
BCS LABORATORIES, INC. -- GAINESVILLE
4609 NW 6TH STREET, STE. A, GAINE SVILLE, FLORIDA 32609
TEL. [phone], F"AK (S 2) 3 7"7-S6 0
WWW.MICROBIOSERVICES.COM
F'LDOH E82924, ISO 1 702 s:2017 L.2422, PADEP: 68-039 s0, A7-DHS:AZO820, EPA F'LO 1 147
THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES
r "
i16C- RA
" ,

Client: Branch Residuals and Soils
Analysis: Salmonella
Project Name: 2014.110
Client Sample ID: M5
Sample Date/Time: September 12, 2023 12:46
BCS Sample ID: 2309092 Sample Description: Biosolid
Date Received: September 13, 2023 9:53 Amount Submitted:100 ml bottle % Solids: 30.4
Amount Analyzed: 3.01E+01 g Receipt Temperature: 3.3 deg C Preserved: Yes
Analysis Start: September 13, 2023 11:12 Analysis Stop Date: September 16, 2023 13:02
Analyst: Catherine Dixon, B.S. Qualifier: U
Primary Value: 50.07 Salmonella MPN/mL sample analyzed
Secondary Value: :50.9 Salmonella MPN/4 dry grams
Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's
detection limit for the amount of sample analyzed as per the method's standard reporting units
Client: Branch Residuals and Soils
Analysis: Salmonella
Project Name: 201.11
Client Sample I: M6
BCS Sample I: 2309093 Sample Description: Biosolid
Date Received: September 13, 203 9:53 Amount Submitted: 1 ml bottle % Solids: 37.9
Amount Analyzed: 3.00E+1 g Receipt Temperature: 3.3 deg C Preserved: Yes
Analysis Start: September 1, 202 11:12 Analysis Stop Date: September 1, 2023 1:2
Analyst: Catherine Dixon, B.S.Qualifier:
Primary Value: 5.07 Salmonella /L sample analyzed
Secondary Value: 50.7 Salmonella MPN/4 dry grams
Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's
detection limit for the amount of sample analyzed as per the method's standard reporting units
Page 4 of 8
BCS LABORATORIES, INC. -- GAINE SVILLE
4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609
TEL. [phone], FAx. [phone]
WWW.MICROBIOSERVICES.COM
F'LI7t; H E32924, ISO 17025:2017 L.2422, FADER 68-03950, AZDHS:AZO820, EPA F°LO 1 147
THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES
1a-
d1 11,

Client: Branch Residuals and Soils
Analysis: Salmonella
Project Name: 2014.110
Client Sample ID: M7 Sample Date/Time: September 12, 2023 12:48
B[SSample ID: 2389094 Sample Description: Bioso\id
Date Received: September 1],2O23 9:53 Amount Submitted: 1OOmn|bottle V6So|ids: 26.8
Amount Analyzed: 2.99E+01R Receipt Temperature: 3.3 deg Preserved: Yes
Analysis Start: September 13,3O33 11:12 Analysis Stop Date: September 16'2O2] 13:02
Analyst: Catherine Dixon, B.S. Qualifier: U
Primary Value: :50.07 Salmonella MPN/mLsample analyzed
Secondary Value: :51.0 Salmonella K4PN/4dry grams
Analysis Notes: Undetected: Ana|ytewas not detected inthe sample analyzed; Value represents the method's
detection limit for the amount of sample analyzed as per the method's standard reporting units
E]CSLABORATORIES, INC. --GA|NESV|LLE
4609NVV6TH STREET, ETE.A.GAImESvLLE.FLORIDA 32609
TEL[phone].FAx.[phone]
WuVYv.%«[CROB|OBERY(CES.COyw
FLDOHE82924.ISO 170252017L2422.P4DEP: 68-03950.AZO8S:AZOG2O.EPA FU01147
THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES
'_—_-~. � ^

Client: Branch Residuals and Soils
Project: 2014.110
Method Detection Limit: 1 microorganism/ unit weight or volume analyzed
Practical Quantitation Limit: 1 microorganism/ unit weight or volume analyzed
Report Notes: Custody Seal Condition: Not Present
Sample(s) were received well preserved and in excellent condition. Sample(s) were analyzed following receipt
as per the described analytical methodology. End of report notes.
Page 6 of 8
Final Report BCS ID 2309088, 2309089, 2309090, 2309091, 2309092, 2309093, 2309094
BCS LABORATORIES, INC. — GAINESVILLE
4609 NW 6TH STREET, STE. A, GAINES`,PILLE, FLORIDA 32609
TEL. [phone], FAx. [phone]
MICRt BIOSERVICES.COM
F'LDOH E82924, ISO 17025:2017 L2422, PADEP: 68-03 s0, AZDHS:AZ0820, EPA F'LO 1 147
THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL., WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES
PPG-MRA AJAB
' �

I certify that I have examined and I am familiar with the information submitted herein. The results pertain only
to sample(s) identified and their condition at time of receipt. Based on my inquiry of the individuals
responsible for the analysis, I believe the data to be true, accurate, and complete. Sampling and field data was
obtained from submitted documents. The analysis was authorized and commissioned by the client. The
resulting data are representative of the analysis conducted on the material/samples/articles provided by the
client (or client's representative) and it's/their condition at the time of analysis. The sample(s) were analyzed
in accordance with the appropriate method , however due to the inherent limitations of the methods,
microorganisms may avoid detection. BCS Laboratories offers no express or implied warranties concerning
the quality, safety, and/or purity of any sample, batch, source, or the process they are derived from. Quality
assurance controls were performed as outlined in the method and as per Good Laboratory Practices. The
analysis and results presented in this report meet the requirements of the standards of The NELAC Institute
(TNI), ISO 17025, and the FL DOH Environmental Laboratory Certification Program, as applicable unless
otherwise noted.
MMEMEMMIUM
Page 7 of 8
Final Report BCS ID 2309088, 2309089, 2309090, 2309091., 2309092, 2309093, 2309094
BCS LABORA70RIES, INC. --- GAINE VILLE
4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609
TEL. (O 2) 377-9272, FAX. [phone]O
WWW.MICROBIOSERVICES.COM
F LDOH E82924, ISO 1 "7O25:201 "7 L24 22, RADER 68-03950, AZDFAS:AZO820, EPA FLO 1 147
THIS REPOR"r SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE. WRITTEN CONSENT OF BCS LABORATORIES
RaC-MRA

SYMBOL MEANING
B Results based on counts outside the acceptable range.
X Sample received without prior notification or delayed delivery. Analysis performed outside of
associated method required QC data set (1 QC data set per 20 samples per 168 hours).
I Value is between the laboratory method detection limit & the practical quantitation limit.
J1 The sample matrix interfered with the ability to make any accurate determination.
J2 No Quality Control criteria exist for the component.
J3 The data are questionable because of improper laboratory or field protocols.
L Off scale high. Actual value is known to be greaterthan value given.
N Presumptive evidence forthe presence of material. There is an indication thatthe analyte is
present, but the confirmation requirement was not met.
O Sampled, but analysis not performed.
Q Sample held beyond the accepted holding time.
U Indicates that the compound was analyzed for but not detected. The specified component was
not detected. The reported value is the method detection limit.
V Analyte was detected in both sample and the method blank. Data may not be accurate.
Y Laboratory analysis was from an improperly preserved sample; the data may not be accurate
Z Too many colonies present (TNTC); the numeric value given represents the upper end of the
value that can be determined based on the volume.
7 Data are rejected and should not be used. QC data for analyte did not meet acceptance criteria.
Presence or absence of analyte could not be confirmed.
** Not reported due to interference.
A Sampling container supplied by client. Sterility can not be confirmed by BCS.
# BCS Lab specific qualifier. See laboratory analysis notes.
Page R of B
Final Report BCS ID 2309088, 2309089, 2309090, 2309091, 2309092, 2309093, 2309094
BCS LABORATORIES, INC. — GAINESVIL.L.E
4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 3260
TEL. [phone], F (S2) 77- 630
WWW.MICROBIOSERVICES.COM
FLDOH E82924, ISO 17025:2017 L2422, PADEP: 68-0395 , DHS: _ OS20, EPA FLO 1 147
THIS REPORT SHALL. NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES
HaC A

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Marcal Cordova, LLC
Cordova, NC
City of Rockingham IUP 0015
Oct-23
Biological Consulting Smites
Lab
Date AMalY d�
P I..m'arYVa ne"aIm -aSecondary
PN per nd
Value
MPN,:,per 4 gi
2310015
10/7/23
.<. 0.07
< 0.9
2310016
9/24/22
!S 0.07
0.9
2310017
9/24/22
< 0.07
< 0.9
2310018
9/24/22
< 0.07
0.9
2310019
9/24/22
< 0.07
1.0
2310020
9/24/22
< 0.07
........
< 0.9
........
2310021
9/24/22
0.07
:S 0.9
Exceedances
All Samples are less then 3 MPN per 4 grams dry weight. Samples meet Class A pathogen
requirement for distribution.
Ha
Data provided in this summary have been used for the values reported on the Monthly Pathogen
and Vector Attraction Reduction Forms for Class A option.

Ix fflolog'cal Consulting Services
I Of North Florida, Inc.
Robert Branch
Branch Residuals and Soils
1735 Heckle Blvd. Suite 103-291
Rockhill SC 29732
336-312-9007
[e-mail]
Client ID: M1, M2, M3, M4, M5, M6, M7
We have completed the analysis of the submitted samples as outlined below.
Project Name: 2014-110 Cordova NC
Analysis Method
Salmonella EPA 1682; BCS SOP M-4 (ISO17025 and TNI Accredited)
Sincerely,
III '�
Bonnie Mull, MPH
Laboratory Operations Manager
Page I of 8
Final Report BCS ID 2310015, 2310016, 2310017, 2310018, 2310019, 2310020, 2310021
BCS LABORATORIES, INC. — GAINESVILL.E
4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609
TEL. [phone], FAx. [phone]
WWW.MICROBIOSERVICES.COM
FIL DOH E82924, ISO 17025:2017 L2422, PA DEP 68-03950, AZ DHS AZO820, EPA FLO 1 147
THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES
HaC-MRA ,API �W

Client: Branch Residuals and Soils
Analysis: Salmonella
Project Name: JD14-11OCordova N[
Client Sample ID: MI
BCSSample ID: 2310015 Sample Description: Bioso|id
Date Received: OctoberO4 2023 10:02 Amount Submitted: 1OOmL8[Sbottle 965dids: 29.6
Amount Analyzed: I01E+01 g Receipt Temperature: 5.7 deg[ Preserved: Yes
Analysis Start: OctoberO4 2023 11:12 Analysis Stop Date: October O7,2O2] 10:19
Analyst: Catherine Dixon, B.S. Qualifier: U
Primary Value: :50.07 Salmonella MPN/mLsamp|e analyzed
Secondary Value: 150.9 Salmonella K8PN/4 dry grams
Analysis Notes: Undetected: Ana|ytewas not detected in the sample analyzed; Value represents the method's
detection limit for the amount of sample analyzed as per the method's standard reporting units
Client: Branch Residuals and Soils
Analysis: Salmonella
Project Name: 2Dl4-1IDCordova NC
Client Sample ID: M2
8CS Sample ID: 2310016 Sample Description: Bioso|id
Date Received: Oc1oberU4 2023 18:02 Amount Submitted: 10]mL8CSbottle 96So|idc 29.8
Amount Analyzed: 3.DOE+01 g Receipt Temperature: 5.7 deg C Preserved: Yes
Analysis Start: Oc1oherO4, 2023 11:12 Analysis Stop Date: October D7,2Q23 10:19
Analyst: Catherine Dixon, B.S. Qualifier: U
Primary Value: 150.07 Salmonella MP0/mLsample analyzed
Secondary Value: 50.9 Salmonella K8PN/4dry grams
Analysis Notes: Undetected: Ana|ytexvas not detected in the sample analyzed; Value represents the method's
detection limit for the amount ofsample analyzed asper the method's standard reporting units
-- -
E]CS LABORATORIES, INC. —GAINESVLLE
4609NVV6TH STREET, STE.A,GA0ESvLLE.FLORIDA 32609
TEL.[phone].FAx.[phone]
mWYV.M|CROB|OBERV|CES.CO;m
FLDOH EB2924.ISO 17Q252OJ7L2422.PADEP6B-0395D.AZ DHS AZOB2O.EPA FLQ1147
THIS REPORT SHALL NOT BE REPRODUCED. EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABon^TOn/ss
'__---A
~~''^~

Client: Branch Residuals and Soils
Analysis: Salmonella
Project Name: 2014-110 Cordova NC
Client Sample ID: M3
BCS Sample ID: 2310017 Sample Description: Biosolid
Date Received: October 04, 2023 10:02 Amount Submitted: 100 mL BCS bottle %Solids: 30.5
Amount Analyzed: 3.01E+01 g Receipt Temperature: 5.7 deg C Preserved: Yes
Analysis Start: October 04, 2023 11:12 Analysis Stop Date: October 07, 2023 10:19
Analyst: Catherine Dixon, B.S. Qualifier: U
Primary Value: :50.07 Salmonella MPN/mL sample analyzed
Secondary Value: !M9 Salmonella MPN/4 dry grams
Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's
detection limit for the amount of sample analyzed as per the method's standard reporting units
Client: Branch Residuals and Soils
Analysis: Salmonella
Project Name: 2014-110 Cordova NC
Client Sample ID: M4
i
BCS Sample ID: 2310018 Sample Description: Biosolid
Date Received: October 04, 2023 10:02 Amount Submitted: 100 mL BCS bottle %Solids: 27.6
Amount Analyzed: 3.01E+01 g Receipt Temperature: 5.7 deg C Preserved: Yes
Analysis Start: October 04, 2023 11:12 Analysis Stop Date: October 07, 2023 10:19
Analyst: Catherine Dixon, B.S. Qualifier: U
Primary Value: :50.07 Salmonella MPN/mL sample analyzed
Secondary Value: 50.9 Salmonella MPN/4 dry grams
Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's
detection limit for the amount of sample analyzed as per the method's standard reporting units
Page 3 of 8
Final Report BCS ID 2310015, 2310016, 2310017, 2310018, 2310019, 2310020, 2310021
BCS LABORATORIES, INC. — GAINESVILLE
4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609
TEL. [phone], FAx. [phone]
WWW.MICROBIOSERVICES.COM
FL DOH E82924, ISM 7025:2017 L2422, FIA DPP 68-03950, AZ DHS AZO820, EPA PLO 1 147
THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES
A&B
OKI'
01

Client: Branch Residuals and Soils
Analysis: Salmonella
Project Name: 2014-110 Cordova NC
Client Sample ID: M5
BCS Sample ID: 2310019 Sample Description: Biosolid
Date Received: October 04, 2023 10:02 Amount Submitted: 100 mL BCS bottle %Solids: 25.8
Amount Analyzed: 2.99E+01 g Receipt Temperature: 5.7 deg C Preserved: Yes
Analysis Start: October 04, 2023 11:12 Analysis Stop Date: October 07, 2023 10:19
Analyst: Catherine Dixon, B.S. Qualifier: U
Primary Value: :50.07 Salmonella MPN/mL sample analyzed
Secondary Value: :51.0 Salmonella MPN/4 dry grams
Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's
detection limit for the amount of sample analyzed as per the method's standard reporting units
Client: Branch Residuals and Soils
Analysis: Salmonella
Project Name: 2014-110 Cordova NC
Client Sample ID: M6
MITIM
BCS Sample ID: 2310020 Sample Description: Biosolid
Date Received: October 04, 2023 10:02 Amount Submitted: 100 mL BCS bottle %Solids: 30.2
Amount Analyzed: 3.00E+01 g Receipt Temperature: 5.7 deg C Preserved: Yes
Analysis Start: October 04, 2023 11:12 Analysis Stop Date: October 07, 2023 10:19
Analyst: Catherine Dixon, B.S. Qualifier: U
Primary Value: :50.07 Salmonella MPN/mL sample analyzed
Secondary Value: :50.9 Salmonella MPN/4 dry grams
Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's
detection limit for the amount of sample analyzed as per the method's standard reporting units
Page 4 of 8
Fsnal Report BCS ID 231003.5, 231.0016, 2310017, 2310018, 231.0019, 2310020, 2310021
BCS LABORAT'ORIES, INC. - GAINESVILLE
4609 NW 6TF1 STREET, STE. A, GAINESVILLE, FLORIDA 32609
-rEL. [phone], FAx. [phone]
WWW.MICROBIOSERVICES.COM
FL DOH E82924, ISO 17025:2017 L2422, PA [REF' 68-03950, AZ DHS AZO820, EPA FLO 1 147
THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THEWRmi-EN CONSENT OF BCS LABORATORIES
flaC-MRA
11110,
'll, M77

Client: Branch Residuals and Soils
Analysis: Salmonella
Project Name: JOI4'lIOCordova N[
Client Sample ID: W47 Sample Date/Tme:October O3,2O23 13:27
B[SSample |D: 2310021 Sample Description: Biosoid
Date Received: October 04 2023 10:02 Amount SubmK1ed:1OO mL 8[S bottle % 5o|ids: 27.4
Amount Analyzed: 2.99E+01 B Receipt Temperature: 5.7 deg Preserved: Yes
Analysis Start: October O4,JO23 11:12 Analysis Stop Date: October O7,2OJ] 10:19
Analyst: Catherine Dixon, B.S. Qualifier: U
Primary Value: :50.07 Salmonella MP0/mLsamp|e analyzed
Secondary Value: 50.9 Salmonella W1PN/4 dry grams
Analysis Notes: Undetected: Ana|ytexvas not detected inthe sample analyzed; Value represents the method's
detection limit for the amount of sample analyzed as per the method's standard reporting units
Page soxo
EBCSLABORATORIES, INC. --GAiNESV(LLE
4609 NVV6THSTREET, STE.A, GewESvLLE.FLOe|DA 32609
TEL[phone].Ffx.<352>377'5630
\&'WW.yM}CROB((JSERV|CES.COM
FLDOH E82924.ISO 17O25:2D77L2422.PADEP6B{}395Q.AZQHSAZDB2O.EPA FLO1147
THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LAeonxron/ss
�
HaC-MRA

Client: Branch Residuals and Soils
Project: JO14'l1OCordova N[
Method Detection Limit: lmicroorganism/ unit weight orvolume analyzed
Practical CWanUtation Limit: 1 microorganism/ unit weight orvolume analyzed
Report Notes: Custody Seal Condition: Not Present
5amp|e(s)xveve received well preserved and in excellent condition. Samp|e(s)were analyzed following receipt
asper the described analytical methodology. End ofreport notes.
Page sofu
BCS LABORATORIES, INC. ~~GAINESV|LLE
4609 NVV6TeSTREET, STE.A'GA|NESvLLE.FLORIDA 32609
TEL. [phone].Ffx.(352)377'563C)
VV8pW84|CROB|OBERV|CES.COWY
FLDOH EB2924.ISO l70252077L2422.PADEP6B-03950.AZ[}HS/ZO82D.EPA FU]1147
THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCeLABonmmzn/ss
d
RaC-MRA� ^~���^��_�'�

I certify that I have examined and I am familiar with the information submitted herein. The results pertain only
to sample(s) identified and their condition at time of receipt. Based on my inquiry of the individuals
responsible for the analysis, I believe the data to be true, accurate, and complete. Sampling and field data was
obtained from submitted documents. The analysis was authorized and commissioned by the client. The
resulting data are representative of the analysis conducted on the material/samples/articles provided by the
client (or client's representative) and it's/their condition at the time of analysis. The sample(s) were analyzed
in accordance with the appropriate method , however due to the inherent limitations of the methods,
microorganisms may avoid detection. BCS Laboratories offers no express or implied warranties concerning
the quality, safety, and/or purity of any sample, batch, source, or the process they are derived from. Quality
assurance controls were performed as outlined in the method and as per Good Laboratory Practices. The
analysis and results presented in this report meet the requirements of the standards of The NELAC Institute
(TNI), ISO 17025, and the FL DOH Environmental Laboratory Certification Program, as applicable unless
otherwise noted.
.M-M Mon -• -.
Date: October 09, 2023
Page 7 of g
Final Report BCS ID 2310015, 2310016, 2310017, 2310018, 2310019, 2310020, 2310021
BCS LABORATORIES, INC. -- GAINE.SVIL.LE:
4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609
TEL. [phone], FAx. [phone]
WWW.MICROBIOSERVICES.COM
FL DOH E82924, ISO 1702 :2017 L2422, PA C EP 68-03950, AZ DHS AZ0820, EPA F'LO 1 147
THIS REPORT SMALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WR17rEN CONSENT OF BCS LABORATORIES
Rae-m
®M1

B Results based on counts outside the acceptable range.
X Sample received without prior notification or delayed delivery. Analysis performed outside of
associated method required QC data set (1 QC data set per 20 samples per 168 hours).
I Value is between the laboratory method detection limit & the practical quantitation limit.
J1 The sample matrix interfered with the ability to make any accurate determination.
J2 No Quality Control criteria exist for the component.
J3 The data are questionable because of improper laboratory or field protocols.
L Off scale high. Actual value is known to be greaterthan value given.
N Presumptive evidence forthe presence of material. There is an indication thatthe analyte is
present, butthe confirmation requirement was not met.
O Sampled, but analysis not performed.
Q Sample held beyond the accepted holding time.
U Indicates that the compound was analyzed for but not detected. The specified component was
not detected. The reported value is the method detection limit.
V Analyte was detected in both sample and the method blank. Data may not be accurate.
Y Laboratory analysis was from an improperly preserved sample; the data may not be accurate
Z Too many colonies present (TNTC); the numeric value given represents the upper end of the
value that can be determined based on the volume.
7 Data are rejected and should not be used. QC data for analyte did not meet acceptance criteria.
Presence or absence of analyte could not be confirmed.
** Not reported due to interference.
A Sampling container supplied by client. Sterility can not be confirmed by BCS.
# BCS Lab specific qualifier. See laboratory analysis notes.
Page 8 of 8
Final Report BCS I0 2310015, 2310016, 2310017, 2310018, 2310019, 2310020, 2310021
BCS LABORA-170RIES, INC. —° GAINESVIL.LE
4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609
TEL. [phone], FAX. [phone]
WWW.MICROBIOSERVICES.COM
FL DOH E82924, ISO 1702 :2017 L2422, PA DEP 68-03950, AZ DHS AZ O820, EPA F'LO1 147
THIS REPORT SHALL, NOT BE REPRCOCDUCED EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS L.ABCRATYORIES

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i1./0412023 10:02

Mareal. Cordova, LLC
Cordova, NC
City of Rockingham IUP 001
Nov-23
Biological Consulting Services
Lab
Date Analysed;
Primary value Salmonella
MPN per ml
Secondary value
dot N peer 4 gr
2311093
11/14/23
< 0.07
< 0.9_
2311094
11/14/23
75 0.07
f� 0.9
2311095
11/14J23
: 0.07
0.9
2311096
11/14J23
< 0.07
0,9
2311097
11J14J23
< 0.07
< 0.9
231109
11/14/23
< 0.07
< 0.9
2311099
11J14/23
< 0,07
:� 0.9
Exceedanees 1}
"
All Samples are less then 3 MPN per 4 grams dry weight. Samples meet Class A pathogen
requirement for distribution.
Data provided in this summary have b.. used for the values reported on the Monthly Pathogen
Vectorand

Y
d I ""' Biological Consulting Services
X
Of North Florida, Inc.
Robert Branch
Branch Residuals and Soils
1735 Heckle Blvd. Suite 103-291
Rockhill SC 29732
336-312-9007
[e-mail]
Client ID: M1, M2, M3, M4, M5, M6, M7
Dear Robert Branch,
We have completed the analysis of the submitted samples as outlined below.
Project Name: Marcal Cordova NC
Analysis Method
Salmonella EPA 1682; BCS SOP M-4 (IS017025 and TNI Accredited)
r7p - .—Ep 7 -- —TrITTI #M-re-,tFPTFi7-7r?'L III• - re-tTre
Should you have any questions, please do not hesitate to contact me.
Sincerely,
Bonnie Mull, MPH
Laboratory Operations Manager
Page I of 8
Final Report BCS ID 2311093, 2311094, 2311095, 2311096, 2311097, 2311098, 2311099
BCS LABORATORIES, INC. — GAINESVILLE
4609 NW 6TH STREET, CTE. A, GAINESVILLE, FLORIDA 32609
TEL. [phone], FAX. [phone]
WWW.MICROBIOSERVICES.COM
FL DOH E82924, ISO 17025:2017 L2422, PA DEP 68-03950, AZ. DHS AZO820, EPA FLO 1 147
THIS REPORT SHALL NOT BE REPRODUCED. EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES
HaG-MRA —AA40

Client: Branch Residuals and Soils
Analysis: Salmonella
Project Name: Marcal Cordova NC
Client Sample ID: M1
7-1105'�M
BCS Sample ID: 2311093 Sample Description: Biosolid
Date Received: November 09, 2023 9:57 Amount Submitted: 100 mL BCS bottle %Solids: 29.3
Amount Analyzed: 2.99E+01 g Receipt Temperature: 3.0 deg C Preserved: Yes
Analysis Start: November 09, 2023 11:11 Analysis Stop Date: November 14, 2023 9:44
Analyst: Catherine Dixon, B.S. Qualifier: U
Primary Value: :50.07 Salmonella MPN/mL sample analyzed
Secondary Value: :50.9 Salmonella MPN/4 dry grams
Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's
detection limit for the amount of sample analyzed as per the method's standard reporting units
Client: Branch Residuals and Soils
Analysis: Salmonella
Project Name: Marcal Cordova NC
Client Sample ID: M2
BCS Sample ID: 2311094 Sample Description: Biosolid
Date Received: November09,2023 9:57 Amount Submitted: 100 mL BC5 bottle %Solids: 29.4
Amount Analyzed: 3.00E+01 g Receipt Temperature: 3.0 deg C Preserved: Yes
Analysis Start: November09,2023 11:11 Analysis Stop Date: November14,2023 9:44
Analyst: Catherine Dixon, B.S. Qualifier: U
Primary Value: 50.07 Salmonella MPN/mL sample analyzed
Secondary Value: :50.9 5almonellaMPN/4 dry grams
Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's
detection limit for the amount of sample analyzed as per the method's standard reporting units
Page 2 of 8
final Report BCS ID 2311093, 2311094, 2311095, 2311096, 2311097, 2311098, 2311099
BCS LABORATORIES, INC. — GAINESVILLE
4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609
TEL. [phone], FA)c [phone]
WWW.MICROBIOSERVICES.COM
FL DOH E82924, ISO 17025:2017 L2422, PA CEP 68-03950, AZ DHS AZ0820, EPA FLO 1 147
THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL. WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES
ilBC-MRA
4.", *m: v i',/"
4@

Client: Branch Residuals and Soils
Analysis: Salmonella
Project Name: Marcal Cordova NC
Client Sample ID: M3
BCS Sample ID: 2311095 Sample Description: Biosolid
Date Received: November 09, 2023 9:57 Amount Submitted: 100 mL BCS bottle %Solids: 29.5
Amount Analyzed: 3.01E+01 g Receipt Temperature: 3.0 deg C Preserved: Yes
Analysis Start: November 09, 2023 11:11 Analysis Stop Date: November 14, 2023 9:44
Analyst: Catherine Dixon, B.S. Qualifier: U
Primary Value: :50.07 Salmonella MPN/mL sample analyzed
Secondary Value: 150.9 Salmonella MPN/4 dry grams
Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's
detection limit for the amount of sample analyzed as per the method's standard reporting units
Client: Branch Residuals and Soils
Analysis: Salmonella
Project Name: Marcal Cordova NC
Client Sample ID: M4
.110113%
BCS Sample ID: 2311096 Sample Description: Biosolid
Date Received: November 09, 2023 9:57 Amount Submitted: 100 mL BCS bottle %Solids: 29.6
Amount Analyzed: 3.01E+01 g Receipt Temperature: 3.0 deg C Preserved: Yes
Analysis Start: November09,2023 11:11 Analysis Stop Date: November14,2023 9:44
Analyst: Catherine Dixon, B.S. Qualifier: U
Primary Value: :50.07 Salmonella MPN/mL sample analyzed
Secondary Value: :50.9 Salmonella MPN/4 dry grams
Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's
detection limit for the amount of sample analyzed as per the method's standard reporting units
Page 3 of 8
I'mal Report BCS ID 2311093, 2311094, 2311095, 2311096, 2311097, 2311098, 2311099
BCS LABORATORIES, INC. - GAINESVILLE
4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609
TEL. [phone], FA)c [phone]
WWW.MICROBIOSERVICES.COM
FL DOH E82924, ISO 17025:2017 L2422, PA DEP 68-03950, AZ DIS AZO820, EPA FLO 1 147
THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LAE30RATORIES
MC-MRA

Client: Branch Residuals and Soils
Analysis: Salmonella
Project Name: Marcal Cordova NC
Client Sample ID: M5
-TEIT-1911MEW,
BCS Sample ID: 2311097 Sample Description: Biosolid
Date Received: November 09, 2023 9:57 Amount Submitted: 100 ml- BCS bottle %Solids: 29.9
Amount Analyzed: 3.00E+01 g Receipt Temperature: 3.0 deg C Preserved: Yes
Analysis Start: November 09, 2023 11:11 Analysis Stop Date: November 14, 2023 9:44
Analyst: Catherine Dixon, B.S. Qualifier: U
Primary Value: 150.07 Salmonella MPN/mL sample analyzed
Secondary Value: 50.9 Salmonella MPN/4 dry grams
Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's
detection limit for the amount of sample analyzed as per the method's standard reporting units
Client: Branch Residuals and Soils
Analysis: Salmonella
Project Name: Marcal Cordova NC
Client Sample ID: M6
r..7 r: � W.
BCS Sample ID: 2311098 Sample Description: Biosolid
Date Received: November09,2023 9:57 Amount Submitted: 100 mL BCS bottle %Solids: 30.2
Amount Analyzed: 2.99E+01 g Receipt Temperature: 3.0 deg C Preserved: Yes
Analysis Start: November 09,2023 11:11 Analysis Stop Date: November14,2023 9:44
Analyst: Catherine Dixon, B.S. Qualifier: U
Primary Value: :50.07 Salmonella MPN/mL sample analyzed
Secondary Value: :50.9 Salmonella MPN/4 dry grams
Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's
detection limit for the amount of sample analyzed as per the method's standard reporting units
Page 4 of 8
Final Report BCS ID 2311093, 2311094, 2311095, 2311096, 2311097, 2311098, 2311099
BCS LABORATORIES, INC. — GAINESVILLE
4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609
TEL— [phone], FAx. [phone]
WWW.MICROBIOSERVICES.COM
FL DCH E82924, ISO 17025:2017 L2422, PA DER 68-03950, AZ DHS AZ0820, EPA FLO 1 147
THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT' THE. WRITTEN CONSENT OF BCS LABORATORIES
7, %
OBC-MRA
aw

Client: Branch Residuals and Soils
Analysis: Sohnone8o
Project Name: Marca|Cordova N[
Client Sample ID: M7 Sample Date/Time: November 08, 2023 12:30
B[SSample ID: 2911099 Sample Description: Bioso|id
Date Received: November09 2O2] 9:57 Amount Submitted: 18OmL8[Sbottle %Gdids: 29.7
Amount Analyzed: 3.00E+01 g Receipt Temperature: 3.0 deg Preserved: Yes
Analysis Start: November O9,JO23 I1:11 Analysis Stop Date: November 14,JOI] 9:44
Analyst: Catherine Dixon, B.S. Qualifier: U
Primary Value: 150.07 Salmonella [NPN/mLsample analyzed
Secondary Value: g0.9 Salmonella K8PN/4dry grams
Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's
detection limit for the amount of sample analyzed as per the method's standard reporting units
E3CS LABORATORIES, INC. --GANESV)LLE
4609 NVV6TeSTREET, STE. A, GAINESvLLs.FLQR|oA 32609
TEL(352) 377`9272.FAx.[phone]
90WW.M«|CRC)B|OSERV|CES.COM
FLDOH E82924.ISO Y7Q25:20Y7L2422.PADEP68-0395O.AZ[>HSAZO82D.EPA FLO)147
THIS REPORT SHALL NOT BE REPRODUCED. EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LxaoRmmzn/ss
AM
RaC-MBAfill

Client: Branch Residuals and Soils
Project: Marcal Cordova NC
Method Detection Limit: 1 microorganism/ unit weight or volume analyzed
Practical Quantitation Limit: 1 microorganism/ unit weight or volume analyzed
Report Notes: Custody Seal Condition: Not Present
Sample(s) were received well preserved and in excellent condition. Sample(s) were analyzed following receipt
as per the described analytical methodology. End of report notes.
Page 6 of 8
Final Report 6CS ID 2311093, 2311094, 2311095, 2311096, 2311097, 2311098, 2311099
BCS LABORATORIES, INC. --- GAINESVILL.E
4609 IOW 6TFI STREET, STE. A, GAINESVILLE, FLORIDA 32609
TEL. [phone], FAx. [phone]
MICROBIB aERVICES.COM
FL DOH E82924, ISO 1 702 a:2017 L.2422. PA DEP 68-03950, AZ DHS AZO820, EPA FLO 1 147
THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES
-A&B�

I certify that I have examined and I am familiar with the information submitted herein. The results pertain only
to sample(s) identified and their condition at time of receipt. Based on my inquiry of the individuals
responsible for the analysis, I believe the data to be true, accurate, and complete. Sampling and field data was
obtained from submitted documents. The analysis was authorized and commissioned by the client. The
resulting data are representative of the analysis conducted on the material/samples/articles provided by the
client (or client's representative) and it's/their condition at the time of analysis. The sample(s) were analyzed
in accordance with the appropriate method , however due to the inherent limitations of the methods,
microorganisms may avoid detection. BCS Laboratories offers no express or implied warranties concerning
the quality, safety, and/or purity of any sample, batch, source, or the process they are derived from. Quality
assurance controls were performed as outlined in the method and as per Good Laboratory Practices. The
analysis and results presented in this report meet the requirements of the standards of The NELAC Institute
(TNI), ISO 17025, and the FL DOH Environmental Laboratory Certification Program, as applicable unless
otherwise noted.
• • r .rr r �: r r •• `-•
�Date: November 14, 2023
Page 7 of B
Final Report BCS Ira 2311.093, 231.1094, 2311095, 2311096, 2311097, 2311.098, 2311.099
BCS LABORATORIES, INC. -- GAINESVILLE
4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609
TEL. [phone], FAx. [phone]
WWW.MICROBIOSERVICES.COM
F L DOH E82 24, ISO 1702 a 2017 L242Z PA CHEF' 68-03950, AZ DHS AZO82 0, EPA FLO 1 147
THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN! CONSENT OF BCS LAsOFRATORIES

r� ' • •rSYMBOL MEANING
B Results based on counts outside the acceptable range.
X Sample received without prior notification or delayed delivery. Analysis performed outside of
associated method required QC data set (1 QC data set per 20 samples per 168 hours).
I Value is between the laboratory method detection limit & the practical quantitation limit.
J1 The sample matrix interfered with the ability to make any accurate determination.
12 No Quality Control criteria exist forthe component.
13 The data are questionable because of improper laboratory orfield protocols.
L Off scale high. Actual value is known to be greaterthan value given.
N Presumptive evidence forthe presence of material. There is an indication thatthe analyte is
present, butthe confirmation requirement was not met.
O Sampled, but analysis not performed.
Q Sample held beyond the accepted holding time.
LI Indicates that the compound was analyzed for but not detected. The specified component was
not detected. The reported value is the method detection limit.
V Analyte was detected in both sample and the method blank. Data may not be accurate.
Y Laboratory analysis was from an improperly preserved sample; the data may not be accurate
2 Too many colonies present (TNTC); the numeric value given represents the upper end of the
value that can be determined based on the volume.
7 Data are rejected and should not be used. QC data for analyte did not meet acceptance criteria.
Presence or absence of analyte could not be confirmed.
** Not reported due to interference.
A Sampling container supplied by client. Sterility can not be confirmed by BCS.
BCS Lab specific qualifier. See laboratory analysis notes.
Page 8 of B
Final Report BCS ID 2311093, 2311094, 2311095, 2311096, 2311097, 2311098, 2311099
BCS LABORATORIES, INC. — GAINESVILLE
4600 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609
TEL. [phone], FAx. [phone]
WWW.MICROBIOSERVICES.COM
FL DOH E82924, ISO 17025:2017 L..2422, PA DEP 68-03 50, AZ D I S AZO820, EPA. FLO 1 147
THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES
PaC-MA

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Marcal Cordova, LLC
Cordova, NC
City of Rockingham IUP 0015
D,ec-23
Biological Consulting Services
ah: -9"
Date AftaIy qd
Trim"Ary Value Sal' nell
:
MPNper MI
Se c6ndary Value
APN er::4,
2312045
12/9/23
0.07
03
2312046
12/9/23
0.07
0.7
2312047
12/9/23
< 0.07x
07
2312048
12/9/23
<.-0.07
0.7
2312049
12/9/23
<0.07
< 0.7
2312050
12/9/23
<1 0.07
0.6
2312051
12/9/23
< 0.07
0.6
Exceedances
All Samples are less then 3 MPN per 4 grams dry weight. Samples meet Class A pathogen
requirement for distribution.
raw
Data provided in this summary have been used for the values reported on the 17ionthly Pathogen
and Vector Attraction Reduction Forms for Class A option.

Biological
®
Of North Florida, Inc.
Consulting Services
Robert Branch
Branch Residuals and Soils
1735 Heckle Blvd. Suite 103-291
Rockhill SC 29732
336-312-9007
[e-mail]
Client ID: M1, M2, M3, M4, M5, M6, M7
BCS ID: 2312045,2312046,2312047,2312048,2312049,2312050,2312051
Dear Robert Branch,
We have completed the analysis of the submitted samples as outlined below.
Analysis Method
Salmonella EPA 1682; BCS SOP M-4 (ISO17025 and TNI Accredited)
Should you have any questions, please do not hesitate to contact me.
Sincerely,
Bonnie Mull, MPH
Laboratory Operations Manager
Page I of 8
Final Report BCS ID 2312045, 2312046, 2312047, 2312048, 2312049, 2312050, 2312051
BCS LABORATORIES, INC, — GAIN ESVILLE
4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609
TEL. [phone], FAx. [phone]
WWW.MICROBIOSERVICES.COM
FL DOH E82924, ISO 17025:2017 L2422, PA DEP 68-03950, AZ DHS AZO820, EPA FLO 1 147
THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES
A&B
VaC-WA

Client: Branch Residuals and Soils
Analysis: Salmonella
Project Name: Marcal Cordova NC
Client Sample ID: M1 Sample Date/Time: December OS, 2023 13:04
BCS Sample ID: 2312045 Sample Description: biosolid
Date Received: December 06, 2023 10:18 Amount Submitted: 100 mL BCS bottle %Solids: 38.9
Amount Analyzed: 3.01E+01 g Receipt Temperature: 1.3 deg C Preserved: Yes
Analysis Start: December 06, 2023 11:45 Analysis Stop Date: December 09, 2023 9:23
Analyst: Catherine Dixon, B.S. Qualifier: U
Primary Value: :50.07 Salmonella MPN/mL sample analyzed
Secondary Value: :50.7 Salmonella MPN/4 dry grams
Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's
detection limit for the amount of sample analyzed as per the method's standard reporting units
Client: Branch Residuals and Soils
Analysis: Salmonella
Project Name: Marcal Cordova NC
Client Sample ID: M2 Sample Date/Time: December 05, 2023 13:06
BCS Sample ID: 2312046 Sample Description: biosolid
Date Received: December 06, 2023 10:18 Amount Submitted: 100 mL BCS bottle %Solids: 37.1
Amount Analyzed: 3.00E+01 g Receipt Temperature: 1.3 deg C Preserved: Yes
Analysis Start: December 06, 2023 11:45 Analysis Stop Date: December 09, 2023 9:23
Analyst: Catherine Dixon, B.S. Qualifier: U
Primary Value: :50.07 Salmonella MPN/mL sample analyzed
Secondary Value: 50.7 Salmonella MPN/4 dry grams
Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's
detection limit for the amount of sample analyzed as per the method's standard reporting units
Page 2 of 8
hnal Report BCS ID 231.2045, 231.2046, 2312047, 231.2048, 231.2049, 23120S0, 2312051.
BCS LABORATORIES, INC. - GAINESVILLE
4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609
TEL. [phone], FAX. [phone]
WWW.MICROBIB SERVICES.COM
FL DOH E82924, ISO 17025:2017 L2422, PA DEP 6&03950, AZ DHS AZO820, EPA FLO 1 147
THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES
HaC-MRA

Client: Branch Residuals and Soils
Analysis: Salmonella
Project Name: Marcal Cordova NC
Client Sample ID: M3 Sample Date/Time: December 05, 2023 13:09
BCS Sample ID: 2312047 Sample Description: biosolid
Date Received: December 06, 2023 10:18 Amount Submitted:100 mL BCS bottle % Solids: 37.3
Amount Analyzed: 3.00E+01 g Receipt Temperature: 1.3 deg C Preserved: Yes
Analysis Start: December 06, 2023 11:45 Analysis Stop Date: December 09, 2023 9:23
Analyst: Catherine Dixon, B.S. Qualifier: U
Primary Value: 50.07 Salmonella MPN/mL sample analyzed
Secondary Value: 150.7 Salmonella MPN/4 dry grams
Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's
detection limit for the amount of sample analyzed as per the method's standard reporting units
Client: Branch Residuals and Soils
Analysis: Salmonella
ProjectName: Marcal Cordova NC
Client Sample I Sample Date/Time: December 05, 2023 13:1
CS Sample ID: 2312048 SampleDescription: biosolid
Date Received: December 06, 2023 10:18 Amount Submitted: 1 L BCS bottle % Solids: 40.4
Amount Analyzed: 3.01E+1 g Receipt Temperature: 1.3 degC Preserved: Yes
Analysis Start: December 06, 2023 11:45 Analysis Stop ate: December 09, 2023 9:23
Analyst: Catherine Dixon, B.S.Qualifier:
Primary Value: :50.7 Salmonella /L sample analyzed
Secondary Value: 5.7 Salmonella MPN/4 dry grams
AnalysisNotes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's
detection limit for the amount of sample analyzed as per the method's standard reporting units
Page 3 of R
Rnal Report BCS ID 2312045, 2312046, 2312047, 2312048, 2312049, 2312050, 231.2051
BCS LABORATORIES, INC`.. •— GAINE:SVIL.LE.
4609 NW 6TH STREET, STET. A, GAINESVILLE, FLORIDA 32609
TEL. [phone], FAx. [phone]
WWW.MICROBIOSERVICES.COM
FL DOH E82924, ISO 1702 5:201 7 L.2422, PA C EP 68-03950, AZ DHS AZO820, EPA FLO 1 147
THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES
flac-MRA. "
t�"""
%Ij

Client: Branch Residuals and Soils
Analysis: Salmonella
Project Name: Marcal Cordova NC
Client Sample ID: M5
Sample Date/Time: December 05, 2023 13:15
BCS Sample ID: 2312049 Sample Description: biosolid
Date Received: December 06, 2023 10:18 Amount Submitted:100 mL BCS bottle % Solids: 37.9
Amount Analyzed: 2.99E+01 g Receipt Temperature: 1.3 deg C Preserved: Yes
Analysis Start: December 06, 2023 11:45 Analysis Stop Date: December 09, 2023 9:23
Analyst: Catherine Dixon, B.S. Qualifier: U
Primary Value: 50.07 Salmonella MPN/mL sample analyzed
Secondary Value: 50.7 Salmonella MPN/4 dry grams
Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's
detection limit for the amount of sample analyzed as per the method's standard reporting units
Client: Branch Residuals and Soils
Analysis: Salmonella
Project Name: Marcal Cordova NC
Client Sample I
BCS Sample ID: 2312050 SampleDescription: biosolid
Date Received: December 06, 2023 10:18 Amount Submitted: 1 mL BCS bottle % Solids: 40.2
Amount Analyzed: 2.99E+1 g Receipt Temperature: 1.3 deg C Preserved: Yes
Analysis Start: December 06, 223 11:5 Analysis Stop ate: December 09, 223 :2
Analyst: Catherine Dixon, B.S.Qualifier: U
Primary Value: 5.7 Salmonella /mL sample analyzed
Secondary Value: :50.6 Salmonella MPN/4 dry grams
Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's
detection limit for the amount of sample analyzed as per the method's standard reporting units
Page 4 of B
Hnal Report BCS ICI 2312045, 2312046, 2312047, 2312048, 2312049, 2312050, 2312051
BCS L,ABORAT'ORIE S, INC:. --- GAINE.SVIL.L.E
4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 52609
T'EL. (352) 37 7-9272, FAx. (:352) 7 7-5630
WWW.MICROBIOSERVICES.COM
FL DOH E82924, ISO 17025:201 7 L_2422, PA DEP 68-03950, AZ DHS AZO820, EPA FLO1 147
THIS REPORT SHALL. NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES
HaC- . A
r r„ro

Client: Branch Residuals and Soils
Analysis: Salmonella
Project Name: PNarca|Cordova N[
Client Sample ID: K87 Sample Date/Tme:December O5,2DI3 13:20
B[SSample ID: 3312051 Sample Description: bioso|id
Date Received: December OG,2O2] 10:I8 Amount Submitted: 1OOmLB[5bottle %So|ids: 40.4
Amount Analyzed: 3.01E+01 Q Receipt Temperature: 1.3 deg[ Preserved: Yes
Analysis Start: December O6,ZOJ3 11:45 Analysis Stop Date: December O9^2OZ3 9:I3
Analyst: Catherine Dixon, B.S. Qualifier: U
Primary Value: 158.07 Salmonella K4PN/mLsample analyzed
Secondary Value: 150.6 Salmonella MPN/4dry grams
Analysis Notes: Undetected: Ana(yte was not detected in the sample analyzed; Value represents the method's
detection limit for the amount of sample analyzed as per the method's standard reporting units
BCS LABORATORIES, INC. --GAINESV|LLE
4609 NW 6THSTREET, STE. A, GAIwESvLLE.FLQR|DA 32609
TEL(352) 377'9272.FA)c(352)377-5630
WWW.K8|CROB|OSERV|CES.COM
FLDOH E82924.ISO 17025:2017L2422.PA DEP6B-0395O.AZDHSAZO82O.EPA FLD1147
THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES
51

Client: Branch Residuals and Soils
Project: Marcal Cordova NC
Method Detection Limit: 1 microorganism/ unit weight or volume analyzed
Practical Quantitation Limit: 1 microorganism/ unit weight or volume analyzed
Report Notes: Custody Seal Condition: Not Present
Sample(s) were received well preserved and in excellent condition. Sample(s) were analyzed following receipt
as per the described analytical methodology. End of report notes.
Page G of 3
Final Report BC5 ID 2312045, 2312046, 2312047, 2312048, 2312049, 2312050, 2312051
BCC LABORATORIES, INC. — GAINESVILLE
4509 NW 6TH STREET, STE. A, GAINE SVILLE, FLORIDA 32609
TEL. [phone], FAX. [phone]
WWW.MICROBIOSERVICES.COM
FL DOH E52924, ISO 17025:2017 L2422, PA DER 68-03950, AZ DHS AZI EF'A 1= L01 147
THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BC;S LABORATORIES
„g u

I certify that I have examined and I am familiar with the information submitted herein. The results pertain only
to sample(s) identified and their condition at time of receipt. Based on my inquiry of the individuals
responsible for the analysis, I believe the data to be true, accurate, and complete. Sampling and field data was
obtained from submitted documents. The analysis was authorized and commissioned by the client. The
resulting data are representative of the analysis conducted on the material/samples/articles provided by the
client (or client's representative) and it's/their condition at the time of analysis. The sample(s) were analyzed
in accordance with the appropriate method , however due to the inherent limitations of the methods,
microorganisms may avoid detection. BCS Laboratories offers no express or implied warranties concerning
the quality, safety, and/or purity of any sample, batch, source, or the process they are derived from. Quality
assurance controls were performed as outlined in the method and as per Good Laboratory Practices. The
analysis and results presented in this report meet the requirements of the standards of The NELAC Institute
(TNI), ISO 17025, and the FL DOH Environmental Laboratory Certification Program, as applicable unless
otherwise noted.
Date: December 09, 2023
Page 7 of B
Final Report BCS ID 2312045, 2312046, 2312047, 2312048, 2312049, 2312050, 2312051
BCS LABORATORIES, INC. —° GAINESVILLE
460NW 6TI-I STREET, STE. A, GAINESVILLE, FLORIDA 32609
TEL. (O s2) 377-9272, FAX. [phone]
WWWMICROBIOSERVICES.COM
FL DOH E.822 24, ISO 1702 :2017 L2422, PA DEP 68-03950, AZ DHE AZ.0820, EPA FLO 1 147
THIS REPORT .SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES
iia - A t,

• I
SYMBOL MEANING
B Results based on counts outside the acceptable range.
X Sample received without prior notification or delayed delivery. Analysis performed outside of
associated method required QC data set (1 QC data set per 20 samples per 168 hours).
I Value is between the laboratory method detection limit & the practical quantitation limit.
J1 The sample matrix interfered with the ability to make any accurate determination.
J2 No Quality Control criteria exist for the component.
J3 The data are questionable because of improper laboratory or field protocols.
L Off scale high. Actual value is known to be greaterthan value given.
N Presumptive evidence forthe presence of material. There is an indication that the analyte is
present, but the confirmation requirement was not met.
O Sampled, but analysis not performed.
Q Sample held beyond the accepted holding time.
U Indicates that the compound was analyzed for but not detected. The specified component was
not detected. The reported value is the method detection limit.
V Analyte was detected in both sample and the method blank. Data may not be accurate.
Y Laboratory analysis was from an improperly preserved sample; the data may not be accurate
Z Too many colonies present (TNTC); the numeric value given represents the upper end of the
value that can be determined based on the volume.
? Data are rejected and should not be used. QC data for analyte did not meet acceptance criteria.
Presence or absence of analyte could not be confirmed.
** Not reported due to interference.
A Sampling container supplied by client. Sterility can not be confirmed by BCS.
# BCS Lab specific qualifier. See laboratory analysis notes.
Page 8 of 8
Final Report BCS ID 2312045, 2312046, 2312047, 2312048, 2312049, 2312050, 2312051
BCS LABORATORIES, INC. GAINEa'VIL.L.E
4609 NW 6TH...a-TREET, STE. A, GAINESVILLE, FLORIDA 32609
TEL. [phone], FAX. [phone]
FL. DOH E82924, ISO 17025 2017 L2422, PA DEP 68-0395 , AZ DHS AZO820, EFTA FLO1 147
THIS REPORT SHALL NOT BE REPRODUCED., EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES
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