WQ0009477_2023 Residual Annual Report_20240226 (2)

Initial Review
Reviewer
nathaniel.thorn burg
Is this submittal an application? (Excluding additional information.) *
Yes No
If not an application what is the submittal type?* Annual Report
Residual Annual Report
Additional Information
Other
Annual Report Year* 2023
Permit Number (IR) * WQ0009477
Applicant/Permittee Cascades Tissue Group - North Carolina, A Division of Cascades Holding US, Inc.
Email Notifications
Does this need review by the hydrogeologist? * Yes OO No
Regional Office Fayetteville
CO Reviewer
Admin Reviewer Wanda Gerald

Submittal Form
Project Contact Information
Please provide information on the person to be contacted by NDB Staff regarding electronic submittal, confirmation of receipt, and other correspondence.
Name* Michael Hurst
Email Address*
[e-mail]
Project Information
.........................
Application/Document Type*
New (Fee Required)
Modification - Major (Fee Required)
Renewal with Major Modification (Fee
Required)
Annual Report
Additional Information
Other
Phone Number*
9108954033
Modification - Minor
Renewal
GW-59, NDMR, NDMLR, NDAR-1,
N DAR-2
Residual Annual Report
Change of Ownership
We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form.
https://edoes.deq.nc.gov/Forms/NonDischarge_Monitoring_Report
Permit Type:*
Wastewater Irrigation
High -Rate Infiltration
Other Wastewater
Reclaimed Water
Closed -Loop Recycle
Residuals
Single -Family Residence Wastewater
Other
Irrigation
Permit Number:*
WQ0009477
Has Current Existing permit number
Applicant/Permittee Address*
805 Midway Road Rockingham, NC 28379
Facility Name*
Cascades Tissue Group Class A Residuals Program
Please provide comments/notes on your current submittal below.
At this time, paper copies are no longer required. If you have any questions about what is required, please contact Nathaniel Thornburg
at [e-mail].
Please attach all information required or requested for this submittal to be reviewed here.
(Application Form, Engineering Plans, Specifications, Calculations, Etc.)
Cascades Land Application 2023 Annual Report
8.89MB
WQ0009477 Feb 2024.pdf
Upload only 1 PDF document (less than 250 MB). Multiple documents must be combined into one PDF file unless file is larger
than upload limit.
* By checking this box, I acknowledge that I understand the application will not be accepted for pre -review until the fee (if required) has
been received by the Non -Discharge Branch. Application fees must be submitted by check or money order and made payable to the
North Carolina Department of Environmental Quality (NCDEQ). I also confirm that the uploaded document is a single PDF with all parts
of the application in correct order (as specified by the application).
Mail payment to:
NCDEQ — Division of Water Resources
Attn: Non -Discharge Branch
1617 Mail Service Center
Raleigh, NC 27699-1617
Signature
Submission Date 2/26/2024

OL
Cascades Tissue Group — North Carolina
A Division of Cascades Holding US Inc.
805 Midway Road, P.O. Box 578, Rockingham, NC 28380 USA
cascades
Phone: [phone] Fax: [phone]
www.cascades.com * [e-mail]
Date: Feb 1 ,2024
To: State of North Carolina Department of Environment and Natural Resources
Division of Water Quality
Aquifer Protection Section
Land Application Unit
512 N Salisbury St.
Raleigh, North Carolina 27604
1-919-807-6300
From: Brandt Steele-ORC and Preparer of 2023 Annual Report
Cascades Tissue Group -North Carolina, a division of Cascades Holding US Inc.
805 Midway Road
Rockingham, NC 28379
1-910-895-4033 EXT 74280
1-910-895-1877 Fax
Michael Hurst(d-)Cascades.com
Permit # WQ0009477
Subject: Land Application Annual Report Cover Letter
Forms Included:
Annual Land Application Certification Form DENR Form ACF
Elwood Black PH D Letter on Field Application
Elwood Black PH D Pan Calculation for Cascades Biosolids
Excel Spreadsheets on Farmers, Field #, Address, Rain Data, Crops, If K Soil, % Solids, Acres, Wet Tons,
Dry Tons, Dry tons per Acre, Long and Latitudes and Water Shed info.
DENR Form DMSDF and Additional Supplementals
DENR Form RSSF
DENR Form RSSF-B
Lab Results
TCLP, Ignitability, Reactivity, & Corrosivity
DENR Form PVRF 2T
Letter on Vector Reduction
Page 1 of 2

Subject: Land Application Annual Report Cover Letter.
Cascades had 1 ORC and 1 Backup ORC. Karen Bellamy ORC and Brandt Steele -Backup. Jacob Groth
left Cascades the beginning of 2023. Brandt Steele and Jacob Groth both completed the necessary field
inspections in 2023.We have Two to three employees that will be attending NC State University Training in
2024 and will take the exam shortly after. Karen Bellamy will be retiring Jan 31,2024. Michael Hurst will be
handling the taking over the Environmental Position on Feb1,2024. Brandt Steele will be the Temporary
ORC until one of our personally completes the training and test.
Field Inspections where conducted, equipment calibration, PM work on equipment and ORC and backup
ORC performed required inspections for the year.
Karen Bellamy attended Rural Water Association Training in 2023 for our Continuing Education Contact
Hours.
Dr. Elwood Black continues to work closely with our land application Program.
Advanced Residuals had one incident in 2023. Truck turned over in Laurinburg. The State was notified, and
pictures and letter sent.
2023- Challenging year difficulty getting parts for equipment and heavy rains have also been an issue.
Cascades and Advanced Residuals have worked hard to make sure we have a good program that is
Environmentally Friendly and benefits the farmers. We have gotten a lot of positive feedback from farmers.
Bill Young is the Project Manager for Advanced Residuals project at Cascades. Bill Young has worked as
Project Manager several years ago and is back as project manger again.
Pathogen and Vector Reduction aren't required on by our Permit. Several of the heavy metals have also
been removed from our permit since levels have been extremely low for over 12 years.
We also have testing performed by Department of Agronomics, so the farmers can have access to
information.

ANNUAL LAND APPLICATION CERTIFICATION FORM
WQ Permit#: WQ0009477 County: Richmond Year:
2023
Facility Name (as shown on permit):
- Land Application Operator:
Cascades Tissue Group -North Carolina, a division of Cascades Holding US
Brandt Steele
Inc.
Phone: [phone]
L;Lan application of residuals as allowed by the permit occurred during the past calendar year?
Yes ❑ No - If No, skip Part A, and Part B and proceed to Part C. Also, If residuals were
generated but not land applied, please attach an explanation on how the residuals were handled.
Part A - Residuals Application Summary:
Total number of application fields in thepermit:
Total number of fields utilized for land application during the year:
Total amount of dry tons applied during the year for all application sites:
20910.34089
Total number of acres utilizes for land application during the year:
Part B - Annual Comniance Statement:
Facility was compliant during calendar year 2023 with all conditions of the land application permit
(including but not limited to items 1-13 below) issued by the Division of Water Quality. V es ❑ No
If no please, provide a written description why the facility was not compliant, the dates, and explain corrective action
taken.
1) Only residuals approved for this permit were applied to the permitted sites.
2) Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or the
limit specified in the permit.
3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies of
laboratory results are attached.
4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5) All other monitoring was performed in accordance with the permit and reported during the year as required and three (3)
copies of certified laboratory results are attached.
6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .I 105(a) or the Pollutant Loading
Rates in 15A NCAC 02T .I 105(b) (applicable to 40 CFR Part 503 regulated facilities).
7) All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part
503 regulated facilities).
8) All monitoring and reporting requirements in 15A NCAC 02T .1 I I I were complied with (applicable to 40 CFR Part 503
regulated facilities).
9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Quality.
10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
11) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as specified
in the permit.
12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13) All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C - Certification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate,
and complete. I am aware that there are significant penalties for submitting false information, including the possibility
of fines and imprisonment for knowing violations."
Michael Hurst Environmental ManagerZL I I
#JL1 Z
Permittee Name and Title (type or print) Signature of Permittee )ate
B l Ii�
Signature of Prepare ' Date Signature I'a 16, E)plier Date
(if different from Permittee) (if different from Permittee and Preparer)
* Preparer is defined in 40 CFR Part 503.9 (r) and 15A NCAC 02T .1102 (26)
DENR FORM ACF (12/2006)

Feb 1, 2024
Cascades Tissue Group
PO Box 578
Rockingham, NC 2380
Attention: Michael Hurst -Environmental Manager
Dear Michael Hurst and Brandt Steele:
From Jan 1,2023 Thru Dec 31, 2023, Fiber Clay was distributed only to agricultural land.
No Farm field received Fiber Clay in a continuous year- to year application as defined by the
North Carolina Department of Environmental Quality respective to permit WQ0009477.
These statements are based on information reported by Advanced Residuals Management.
Elwood Black, Ph. D.-Soils

Date 1/31/2024
Subject: PAN calculation
The Plant Available Nitrogen (PAN) calculation is widely used to estimate the N that
will be available to a crop from the biosolids. The carbon to nitrogen ratio in biosolids
is commonly less than 20:1 and net mineralization of N from the biosolids occurs.
The mineralization's refers to the transformation of organic N to inorganic N which is
in a plant available form. For materials with a C:N of less than 20:1 the PAN provides
a good estimate of the N that may be available to the plant.
However for materials like the Cascades soil additive, which have a C:N greater than
30:1, the PAN calculation is not appropriate. Instead of mineralization, N
immobilization occurs. For crop production, immobilization is a loss of plant available
N. As a result farmers need to apply additional N to offset the N that will be
immobilized as the soil microorganisms assimilate the fiber.
The PAN should be 0.
Elwood Black, Ph.D. - Soils

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aceAnalytical
www.pacelabs.com
January 25, 2023
Ms. Karen Bellamy
Cascades Tissue Group -NC
805 Midway Road
PO Box 578
Rockingham, NC 28380
RE: Project: January Monthly
Pace Project No.: 92645991
Dear Ms. Bellamy:
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
[phone]
Enclosed are the analytical results for sample(s) received by the laboratory on January 10, 2023. The results relate only to
the samples included in this report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless
otherwise footnoted.
Some analyses were subcontracted outside of the Pace Network. The test report from the external subcontractor is
attached to this report in its entirety.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Asheville
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Tyriek Hooks
[e-mail]
[phone]
Project Manager
Enclosures
cc: Cascades Tissue Group- Rockingham, Divsion of
Cascades Holding US Inc.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 1 of 21

aceAnalyfical
www.pacelabs.com
Project: January Monthly
Pace Project No.: 92645991
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
[phone]
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Laboratory ID: 99006
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
CERTIFICATIONS
South Carolina Certification #: 99006001
South Carolina Drinking Water Cent. #: 99006003
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Louisiana DoH Drinking Water #: LA029
Virginia/VELAP Certification #: 460221
South Carolina Laboratory ID: 99030
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 21

aceAnalytical
www.paceiabs.com
i
Project: January Monthly
Pace Project No.: 92645991
Lab ID Sample ID
SAMPLE SUMMARY
Matrix Date Collected Date Received
92645991001 SLUDGE Solid 01/10/23 08:40 01/10/23 09:25
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
[phone]
Page 3 of 21

aceAnalytical
www.pacelabs.com
ANALYTICAL RESULTS
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
[phone]
Project: January Monthly
Pace Project No.. 92645991
Sample: SLUDGE
Lab ID: 92645991001 Collected: 01/10/23 08:40 Received: 01/10/23 09:25 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters
Results Units Limit MDL
DF Prepared
Analyzed CAS No. Qual
6010 MET ICP
Analytical Method: EPA 601 OD Preparation Method: EPA 3050E
Pace Analytical Services - Asheville
Calcium
196000 mg/kg 548 110
10 01/11/23 09:58
01/17/23 16:33 7440-70-2
Copper
16.9 mg/kg 11.0 0.55
1 01/11/23 09:58
01/16/23 18:48 7440-50-8
Magnesium
1580 mg/kg 21.9 0.55
1 01/11/23 09:58
01/16/23 18:48 7439-95-4
Nickel
ND mg/kg 1.1 0.55
1 01/11/23 09:58
01/16/23 18:48 7440-02-0
Zinc
97.2 mg/kg 2.2 1.1
1 01/11/23 09:58
01/16/23 18:48 7440-66-6
254OG Total Percent Solids
Analytical Method: SM 2540G-2011
Pace Analytical Services - Charlotte
Total Solids
43.0 % 0.10 0.000010
1
01/11/23 17:12
Percent Moisture
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
57.0 % 0.10 0.10
1
01/11/23 17:05 N2
9.045 pH Soil
Analytical Method: EPA 9045D
Pace Analytical Services - Asheville
pH at 25 Degrees C
7.4 Std. Units 0.10 0.10
1
01 /18/23 16:59 H3
Plant Available Nitrogen
Analytical Method: None
Pace Analytical Services - Asheville
Plant Available Nitrogen
510 mg/kg
1
01/18/23 18:03 N2
Total Nitrogen Calculation
Analytical Method: TKN+NO3+NO2 Calculation
Pace Analytical Services - Asheville
Nitrogen
1700 mg/kg 40.0 20.0
1
01/18/2318:09 7727-37-9
350.1 Ammonia
Analytical Method: EPA 350.1 Rev 2.0 1993 Mod.
Preparation Method: EPA 350.1 Rev 2.0 1993 Mod.
Pace Analytical Services -Asheville
Nitrogen, Ammonia
ND mg/kg 20.4 20.4
1 01/17/2310:31
01/18/2312:23 7664-41-7
351.2 Total Kjeldahl Nitrogen
Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993
Pace Analytical Services - Asheville
Nitrogen, Kjeldahl, Total
1700 mg/kg ill 55.3
1 01/16/23 17:12
01/17/23 05:20 7727-37-9
353.2 Nitrogen, NO2/NO3
Analytical Method: EPA 353.2 Rev 2.0 1993 Preparation Method: EPA 353.2 Rev 2.0 1993
Pace Analytical Services - Asheville
Nitrogen, NO2 plus NO3
ND mg/kg 9.1 4.5
1 01/10/23 23:07
01/11/23 00:56
Nitrogen, Nitrate
ND mg/kg 9.1 4.5
1 01/10/23 23:07
01/11/23 00:56 14797-55-8
Nitrogen, Nitrite
ND mg/kg 9.1 2.3
1 01/10/2323:07
01/11/2300:56 14797-65-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /25/2023 03:53 PM without the written consent of Pace Analytical Services, LLC. Page 5 of 21

Waypoint-(D
ANALYTICAL
1 /20/2023
Pace Analytical Labs Charlotte
Tyriek Hooks
9800 Kindey Ave
Huntersville, NC, 28078
Ref: Analytical Testing
Report Number: 23-012-0005
Project Description: 92645991
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Dear Tyriek Hooks:
Waypoint Analytical Virginia, Inc. received sample(s) on 1/12/2023 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Brandi Watson
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 17 of 21
Page 1 of 5

(2)
7621 Whitepine Road, Richmond, VA 23237
Waypoint,
Main 804-743-9401 ° Fax [phone]
ANALYTICAL www.waypointanalytical.com
Sample Summary Table
Report Number: 23-012-OOOS
Client Project Description: 92645991
Lab No
Client Sample ID
Matrix
Date Collected
Date Received
Method
Lab ID
60388
Sludge
Solids
01/10/2023 08:40
01/12/2023
60388
Sludge
Solids
O1/10/2023 08:40
01/12/2023
SM-2540G
WP MTN
60388
Sludge
Solids
01/10/2023 08:40
01/12/2023
SM-4500-NH3C-TKN
WP MTN
60388
Sludge
Solids
01/10/2023 08:40
01/12/2023
AOAC 955.01
WP MTN
WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN
Page 2 of 5
Page 18 of 21

WayPA� nt.
NALYTICAL
11769
Pace Analytical Labs Charlotte Project 92645991
Tyriek Hooks
9800 Kindey Ave Information
Huntersville , NC 28078
Report Number : 23-012-0005 REPORTOF.4
Lab No : 60388
Sample ID : Sludge
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.corn
Report Date ; 01/20/2023
Received : 01/12/2023
Brandi Watson
VA YSlS
Matrix: Solids
Sampled: 1/10/2023 8:40
Test
Results
Units
MQL
DF Date / Time
Analyzed
By
Analytical
Method
Total Solids
42.8
%
0.010
1 01/13/23 15:50
FMM
SM-254OG
Total Kjeldahl Nitrogen
2870
mg/Kg - dry
584
1 01/19/23 05:30
JPJ ;M-4500-NH3C-TKP
Calcium Carbonate Equivalent
44.2
%
0.1
1 01/17/23 10:30
HBT
AOAC 955.01
Total Volatile Solids
48.6
%
0.010
1 01/13/23 15:50
FMM
SM-254OG
C/N RATIO
98
Ratio
0
1 01/13/23 15:50
CALCULATION
Test
Results
Units
MQL
DF Date / Time
By
Analytical
Analyzed
Method
Carbon (TOC)
28.3
%
0.010
1 01/13/23 15:50
CALCULATION
Analytical Method: SM-2540G
Test
Results
Units
MQL
DF Date / Time
By
Analytical
Analyzed
Batch
Moisture 57.2 % 0.010 1 01/13/23 15:50 FMM L658536
Qualifiers/ DF Dilution Factor
Definitions
MQL Method Quantitation Limit
Page 3 of 5
Page 19 of 21

aceAnalytical
www.pacelabs.com
March 03, 2023
Ms. Karen Bellamy
Cascades Tissue Group -NC
805 Midway Road
PO Box 578
Rockingham, NC 28380
RE: Project: February
Pace Project No.: 92651388
Dear Ms. Bellamy:
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
[phone]
Enclosed are the analytical results for sample(s) received by the laboratory on February 09, 2023. The results relate only
to the samples included in this report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless
otherwise footnoted.
Some analyses were subcontracted outside of the Pace Network. The test report from the external subcontractor is
attached to this report in its entirety.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Asheville
• Pace Analytical Services - Charlotte
• Pace Analytical Services - Peachtree Corners, GA
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Tyriek Hooks
[e-mail]
[phone]
Project Manager
Enclosures
cc: Cascades Tissue Group- Rockingham, Divsion of
Cascades Holding US Inc.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 1 of 20

_ ;a'ceAnalytical'
www.pacolabs.com
Project: February
Pace Project No.: 92651388
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
[phone]
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Laboratory ID: 99006
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
Pace Analytical Services Peachtree Corners
110 Technology Pkwy, Peachtree Corners, GA 30092
Florida DOH Certification #: E87315
Georgia DW Inorganics Certification #: 812
CERTIFICATIONS
South Carolina Certification #: 99006001
South Carolina Drinking Water Cert. #: 99006003
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Louisiana DoH Drinking Water #: LA029
Virginia/VELAP Certification #: 460221
South Carolina Laboratory ID: 99030
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
North Carolina Certification #: 381
South Carolina Certification #: 98011001
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 20

aceAnalytical
www.pacelabs.com
Project: February
Pace Project No.: 92651388
Lab ID Sample ID
SAMPLE SUMMARY
Matrix Date Collected Date Received
92651388001 CASCADES Solid 02/09/23 08:00 02/09/23 10:40
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
[phone]
Page 3 of 20

aceAnalytical
www.pacelabs.com
ANALYTICAL RESULTS
Project: February
Pace Project No.: 92651388
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
[phone]
Sample: CASCADES Lab ID: 92651388001 Collected: 02/09/23 08:00 Received: 02/09/23 10:40 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
6010D ATL ICP
Analytical Method: EPA 601OD Preparation Method: EPA 3050B
Pace Analytical Services - Peachtree Corners, GA
Calcium
177000 mg/kg 1170 149
10 02/21/23 15:10
02/22/2316:01 7440-70-2
Copper
17.1 mg/kg 4.7 1.9
1 02/21/23 15:10
02/22/23 00:09 7440-50-8
Magnesium
2480 mg/kg 5.8 3.3
1 02/21/23 15:10
02/22/23 00:09 7439-95-4
Nickel
1.5J mg/kg 2.3 0.57
1 02/21/23 15:10
02/22/23 00:09 7440-02-0
Zinc
76.4 mg/kg 3.5 3.2
1 02/21/23 15:10
02/22/23 00:09 7440-66-6
2540G Total Percent Solids
Analytical Method: SM 2540G-2011
Pace Analytical Services - Charlotte
Total Solids
42.7 % 0.10 0.000010
1
02/09/23 17:38
Percent Moisture
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
57.3 % 0.10 0.10
1
02/09/23 17:31 N2
9045 pH Soil
Analytical Method: EPA 9045D
Pace Analytical Services - Asheville
pH at 25 Degrees C
7.6 Std. Units 0.10 0.10
1
02/16/23 15:24 H3
Plant Available Nitrogen
Analytical Method: None
Pace Analytical Services -Asheville
Plant Available Nitrogen
495 mg/kg
1
02/24/23 06:34 N2
Total Nitrogen Calculation
Analytical Method: TKN+NO3+NO2 Calculation
Pace Analytical Services - Asheville
Nitrogen
1650 mg/kg 40.0 20.0
1
02/17/2311:44 7727-37-9
350.1 Ammonia
Analytical Method: EPA 350.1 Rev 2.0 1993 Mod.
Preparation Method: EPA 350.1 Rev 2.0 1993 Mod.
Pace Analytical Services -Asheville
Nitrogen, Ammonia
ND mg/kg 22.5 22.5
1 02/14/23 14:22
02/15/23 12:27 7664-41-7
351.2 Total Kjeldahl Nitrogen
Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993
Pace Analytical Services - Asheville
Nitrogen, Kjeldahl, Total
1650 mg/kg 117 58.5
1 02/14/23 18:28
02/15/23 05:08 7727-37-9
353.2 Nitrogen, NO2/NO3
Analytical Method: EPA 353.2 Rev 2.0 1993 Preparation Method: EPA 353.2 Rev 2.0 1993
Pace Analytical Services - Asheville
Nitrogen, NO2 plus NO3
ND mg/kg 9.2 4.6
1 02/09/23 23:05
02/10/23 00:54
Nitrogen, Nitrate
ND mg/kg 9.2 4.6
1 02/09/23 23:05
02/10/23 00:54 14797-55-8
Nitrogen, Nitrite
ND mg/kg 9.2 2.3
1 02/09/23 23:05
02/10/23 00:54 14797-65-0
Date: 03/03/2023 05:12 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 5 of 20

0 (2)
Waypoint
ANALYTICAL
2/23/2023
Pace Analytical Labs Charlotte
Tyriek Hooks
9800 Kindey Ave
Huntersville, NC, 28078
Ref: Analytical Testing
Report Number: 23-044-0003
Project Description: Tyriek Hooks
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Dear Tyriek Hooks:
Waypoint Analytical Virginia, Inc. received sample(s) on 2/13/2023 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Brandi Watson
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 16 of 20
Page 1 of 5

(D
Waypoint 7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
ANALYTICAL www.waypointanalytical.com
Sample Summary Table
Report Number: 23-044-0003
Client Project Description: Tyriek Hooks
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
60775
Cascades
Solids
60775
Cascades
Solids
60775
Cascades
Solids
60775
Cascades
Solids
WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN
02/09/2023 08:00 02/13/2023
02/09/2023 08:00 02/13/2023
02/09/2023 08:00 02/13/2023
02/09/2023 08:00 02/13/2023
SM-2540G WP MTN
SM-4500-NH3C-TKN WP MTN
AOAC 955.01 WP MTN
Page 2 of 5
Page 17 of 20

0
Waypoint.
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
ANALYTICAL
www.waypointanalytical.com
11769
Pace Analytical Labs Charlotte
Project
Tyriek Hooks
Tyriek Hooks
Report Date ; 02/23/2023
9800 Kindey Ave
Information :
Received : 02/13/2023
Huntersville , NC 28078
Brandi Watson
Report Number: 23-044-0003
REPORT OFANALYSlS
Lab No : 60775
Matrix: Solids
Sample ID : Cascades
Sampled: 2/9/2023 8:00
Test
Results
Units
MQL
DF Date / Time
By Analytical
Analyzed
Method
Total Solids
43.0
%
0.010
1 02/16/23 15:55
FMM SM-254OG
Total Kjeldahl Nitrogen
7880
mg/Kg - dry
581
1 02/22/23 09:00
JPJ ')M-4500-NH3C-TKP
Calcium Carbonate Equivalent
48.7
%
0.1
1 02/17/23 14:16
HBT AOAC 955.01
Total Volatile Solids
47.6
%
0.010
1 02/16/23 15:55
FMM SM-254OG
C/N RATIO
35
Ratio
0
1 02/16/23 15:55
CALCULATION
Test
Results
Units
MQL
DF Date / Time
By Analytical
Analyzed
Method
Carbon (TOC)
27.7
%
0.010
1 02/16/23 15:55
CALCULATION
Analytical Method: SM-2540G
Test
Results
Units
MQL
DF Date / Time
By Analytical
Analyzed
Batch
Moisture
57.0
%
0.010
1 02/16/23 15:55
FMM L664521
Qualifiers/ DF Dilution Factor MQL Method Quantitation Limit
Definitions
Page 18 of 20
Page 3 of 5

aceAnalyfical
www.pacelabs.com
April 13, 2023
Ms. Karen Bellamy
Cascades Tissue Group -NC
805 Midway Road
PO Box 578
Rockingham, NC 28380
RE: Project: March
Pace Project No.: 92655494
Dear Ms. Bellamy:
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
[phone]
Enclosed are the analytical results for sample(s) received by the laboratory on March 07, 2023. The results relate only to
the samples included in this report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless
otherwise footnoted.
Some analyses were subcontracted outside of the Pace Network. The test report from the external subcontractor is
attached to this report in its entirety.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Asheville
• Pace Analytical Services - Charlotte
• Pace Analytical Services - Peachtree Corners, GA
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Tyriek Hooks
[e-mail]
[phone]
Project Manager
Enclosures
cc: Cascades Tissue Group- Rockingham, Divsion of
Cascades Holding US Inc.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 1 of 20

aceAnalytical
www.pacelabs.com
Project: March
Pace Project No.: 92655494
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
[phone]
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Laboratory ID: 99006
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
Pace Analytical Services Peachtree Corners
110 Technology Pkwy, Peachtree Corners, GA 30092
Florida DOH Certification #: E87315
Georgia DW Inorganics Certification #: 812
CERTIFICATIONS
South Carolina Certification #: 99006001
South Carolina Drinking Water Cert. #: 99006003
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Louisiana DoH Drinking Water #: LA029
VirginiaNELAP Certification #: 460221
South Carolina Laboratory ID: 99030
South Carolina Certification #: 99030001
VirginiaNELAP Certification #: 460222
North Carolina Certification #: 381
South Carolina Certification #: 98011001
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 20

aceAnalytical
www.pacelabs.com
Project: March
Pace Project No.. 92655494
Lab ID Sample ID
SAMPLE SUMMARY
Matrix Date Collected Date Received
92655494001 SLUDGE Solid 03/06/23 08:50 03/07/23 10:30
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
[phone]
Page 3 of 20

aceAnalytical
! www.pacelabs.com
ANALYTICAL RESULTS
Project: March
Pace Project No.: 92655494
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
(919)8344984
Sample: SLUDGE Lab ID: 92655494001 Collected: 03/06/23 08:50 Received: 03/07/23 10:30 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No.
Qual
601 OD ATL ICP
Analytical Method: EPA 601 OD Preparation Method: EPA 3050E
Pace Analytical Services - Peachtree Corners, GA
Calcium
151000 mg/kg 57.1 7.3 1 03/16/23 11:04
03/22/23 00:27 7440-70-2
Copper
19.4 mg/kg 2.3 0.92 1 03/16/23 11:04
03/22/23 00:27 7440-50-8
Magnesium
1770 mg/kg 2.9 1.6 1 03/16/23 11:04
03/22/23 00:27 7439-95-4
Nickel
1.1J mg/kg 1.1 0.28 1 03/16/23 11:04
03/22/23 00:27 7440-02-0
Zinc
71.2 mg/kg 1.7 1.6 1 03/16/23 11:04
03/22/23 00:27 7440-66-6
254OG Total Percent Solids
Analytical Method: SM 2540G-2011
Pace Analytical Services - Charlotte
Total Solids
43.2 % 0.10 0.000010 1
03/07/23 17:03
Percent Moisture
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
56.9 % 0.10 0.10 1
03/07/23 16:57
N2
9045 pH Soil
Analytical Method: EPA 9045D
Pace Analytical Services - Asheville
pH at 25 Degrees C
7.1 Std. Units 0.10 0.10 1
03/15/23 16:03
H3
Plant Available Nitrogen
Analytical Method: None
Pace Analytical Services -Asheville
Plant Available Nitrogen
672 mg/kg 1
03/20/23 07:24
N2
Total Nitrogen Calculation
Analytical Method: TKN+NO3+NO2 Calculation
Pace Analytical Services - Asheville
Nitrogen
2240 mg/kg 40.0 20.0 1
03/20/23 07:21 7727-37-9
350.1 Ammonia
Analytical Method: EPA 350.1 Rev 2.0 1993 Mod. Preparation Method: EPA 350.1 Rev 2.0 1993 Mod.
Pace Analytical Services - Asheville
Nitrogen, Ammonia
ND mg/kg 22.7 22.7 1 03/09/23 14:58
03/10/23 13:25 7664-41-7
351.2 Total Kjeldahl Nitrogen
Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993
Pace Analytical Services - Asheville
Nitrogen, Kjeldahl, Total
2240 mg/kg 211 105 1 03/17/23 16:40
03/18/23 04:22 7727-37-9
353.2 Nitrogen, NO2/NO3
Analytical Method: EPA 353.2 Rev 2.0 1993 Preparation Method: EPA 353.2 Rev 2.0 1993
Pace Analytical Services - Asheville
Nitrogen, NO2 plus NO3
ND mg/kg 9.2 4.6 1 03/07/23 22:29
03/08/23 00:56
Nitrogen, Nitrate
ND mg/kg 9.2 4.6 1 03/07/23 22:29
03/08/23 00:56 14797-55-8
Nitrogen, Nitrite
ND mg/kg 9.2 2.3 1 03/07/23 22:29
03/08/23 00:56 14797-65-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/13/2023 05:07 PM without the written consent of Pace Analytical Services, LLC. Page 5 of 20

Waypoint �
ANALYTICAL
4/13/2023
Pace Analytical Labs Charlotte
Tyriek Hooks
9800 Kindey Ave
Huntersville, NC, 28078
Ref: Analytical Testing
Report Number: 23-069-0008
Project Description: 92655494 March
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Dear Tyriek Hooks:
Waypoint Analytical Virginia, Inc. received sample(s) on 3/10/2023 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information
Sincerely,
Brandi Watson
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 16 of 20
Page 1 of 5

(2)
Waypoint.
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
ANALYTICAL
www.waypointanalytical.com
Sample Summary Table
Report Number: 23-069-0008
Client Project Description: 92655494 March
Lab No Client Sample ID
Matrix
Date Collected
Date Received Method
Lab ID
61326 Sludge 92655494001
Solids
03/06/2023 08:50
03/10/2023
61326 Sludge 92655494001
Solids
03/06/2023 08:50
03/10/2023 SM-2540G
WP MTN
61326 Sludge 92655494001
Solids
03/06/2023 08:50
03/10/2023 SM-4500-NH3C-TKN
WP MTN
61326 Sludge 92655494001
Solids
03/06/2023 08:50
03/1O/2023 AOAC 955.01
WP MTN
WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN
Page 2 of 5
Page 17 of 20

r •
7621 Whitepine Road, Richmond, VA 23237
Waypoint.
Main 804-743-9401 ° Fax [phone]
ANALYTICAL www.waypointanalytical.com
11769
Pace Analytical Labs Charlotte Project 92655494 March
Tyriek Hooks Report Date : 04/13/2023
9800 Kindey Ave Information : Received : 03/10/2023
Huntersville , NC 28078
Brandi Watson
Report Number : 23-069-0008 REPORT OFANAL YSIS
Lab No : 61326 Matrix: Solids
Sample ID : Sludge 92655494001 Sampled: 3/6/2023 8:50
Test Results Units MQL DF Date / Time By Analytical
Analyzed Method
Total Solids
Total Kjeldahl Nitrogen
Calcium Carbonate Equivalent
Total Volatile Solids
C/N RATIO
Test
Carbon (TOC)
Analytical Method: SM-254OG
Test
39.5 H
%
0.010
1
03/16/23 17:06
CID
SM-2540G
12800
mg/Kg - dry
633
1
03/17/23 09:30
CLP ;M-4500-NH3C-TKP
55.6
%
0.1
1
03/16/23 10:43
HBT
AOAC 955.01
49.9 H
%
0.010
1
03/16/23 17:06
CJD
SM-2540G
23
Ratio
0
1
03/16/23 17:06
CALCULATION
Results
Units
MQL
DF
Date / Time
By
Analytical
Analyzed
Method
29.0
%
0.010
1
03/16/23 17:06
CALCULATION
Results Units MQL DF Date / Time By Analytical
Analyzed Batch
Moisture 60.5 H % 0.010 1 03/16/23 17:06 CID L670315
Qualifiers/ DF Dilution Factor H Beyond holding time
Definitions MQL Method Quantitation Limit
Page 18 of 20
Page 3 of 5

aceAnalytical
www.pacelabs.com
May 02, 2023
Ms. Karen Bellamy
Cascades Tissue Group -NC
805 Midway Road
PO Box 578
Rockingham, NC 28380
RE: Project: APRIL
Pace Project No.: 92662175
Dear Ms. Bellamy:
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
[phone]
Enclosed are the analytical results for sample(s) received by the laboratory on April 13, 2023. The results relate only to the
samples included in this report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless
otherwise footnoted.
Some analyses were subcontracted outside of the Pace Network. The test report from the external subcontractor is
attached to this report in its entirety.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Asheville
• Pace Analytical Services - Charlotte
• Pace Analytical Services - Peachtree Corners, GA
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Tyriek Hooks
tyriek. [e-mail]
[phone]
Project Manager
Enclosures
cc: Cascades Tissue Group- Rockingham, Divsion of
Cascades Holding US Inc.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 1 of 21

aceAnalytical
www.paceiabs.com
Project: APRIL
Pace Project No.: 92662175
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
[phone]
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Laboratory ID: 99006
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
Pace Analytical Services Peachtree Corners
110 Technology Pkwy, Peachtree Corners, GA 30092
Florida DOH Certification #: E87315
Georgia DW Inorganics Certification #: 812
CERTIFICATIONS
South Carolina Certification #: 99006001
South Carolina Drinking Water Cert. #: 99006003
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Louisiana DoH Drinking Water #: LA029
Virginia/VELAP Certification #: 460221
South Carolina Laboratory ID: 99030
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
North Carolina Certification #: 381
South Carolina Certification #: 98011001
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 21

aceAnalytical
www.pacelabs.com
Project: APRIL
Pace Project No.: 92662175
Lab ID Sample ID
92662175001 SLUDGE
SAMPLE SUMMARY
Matrix Date Collected Date Received
Solid 04/13/23 08:20 04/13/23 09:52
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
[phone]
Page 3 of 21

_ aceAnalytical
www.pacelabs.com
ANALYTICAL RESULTS
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
[phone]
Project: APRIL
Pace Project No.: 92662175
Sample: SLUDGE
Lab ID: 92662175001 Collected: 04/13/23 08:20 Received: 04/13/23 09:52 Matrix: Solid
Results reported on a "dry weight"
basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters
Results Units Limit MDL DF Prepared
Analyzed CAS No. Qual
6010D ATL ICP
Analytical Method: EPA 6010D Preparation Method: EPA 3050B
Pace Analytical Services - Peachtree Corners, GA
Calcium
200000 mg/kg 1270 161 20 04/19/23 16:00
04/24/2310:48 7440-70-2
Copper
19.7 mg/kg 2.5 1.0 1 04/19/23 16:00
04/20/23 20:07 7440-50-8
Magnesium
1680 mg/kg 3.2 1.8 1 04/19/23 16:00
04/20/23 20:07 7439-95-4
Nickel
1.3J mg/kg 1.3 0.31 1 04/19/23 16:00
04/20/23 20:07 7440-02-0
Zinc
69.7 mg/kg 1.9 1.7 1 04/19/23 16:00
04/20/23 20:07 7440-66-6
254OG Total Percent Solids
Analytical Method: SM 2540G-2011
Pace Analytical Services - Charlotte
Total Solids
39.2 % 0.10 0.000010 1
04/14/23 00:05
Percent Moisture
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
60.8 % 0.10 0.10 1
04/13/23 23:57 N2
9045 pH Soil
Analytical Method: EPA 9045D
Pace Analytical Services - Asheville
pH at 25 Degrees C
7.5 Std. Units 0.10 0.10 1
04/17/23 16:20 H3
Plant Available Nitrogen
Analytical Method: None
Pace Analytical Services - Asheville
Plant Available Nitrogen
471 mg/kg 1
05/01/23 20:00 N2
Total Nitrogen Calculation
Analytical Method: TKN+NO3+NO2 Calculation
Pace Analytical Services - Asheville
Nitrogen
1570 mg/kg 40.0 20.0 1
04/18/23 21:22 7727-37-9
350.1 Ammonia
Analytical Method: EPA 350.1 Rev 2.0 1993 Mod. Preparation Method: EPA 350.1 Rev 2.0 1993 Mod.
Pace Analytical Services -Asheville
Nitrogen, Ammonia
ND mg/kg 24.1 24.1 1 04/29/23 12:15
04/29/23 13:40 7664-41-7
351.2 Total Kjeldahl Nitrogen
Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993
Pace Analytical Services -Asheville
Nitrogen, Kjeldahl, Total
1570 mg/kg 121 60.7 1 04/17/23 15:12
04/18/23 04:28 7727-37-9
353.2 Nitrogen, N021NO3
Analytical Method: EPA 353.2 Rev 2.0 1993 Preparation Method: EPA 353.2 Rev 2.0 1993
Pace Analytical Services -Asheville
Nitrogen, NO2 plus NO3
ND mg/kg 10.1 5.1 1 04/13/23 22:39
04/14/23 00:10
Nitrogen, Nitrate
ND mg/kg 10.1 5.1 1 04/13/23 22:39
04/14/23 00:10 14797-55-8
Nitrogen, Nitrite
ND mg/kg 10.1 2.5 1 04/13/23 22:39
04/14/23 00:10 14797-65-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/02/2023 05:11 PM without the written consent of Pace Analytical Services, LLC. Page 5 of 21

(2)
WayPA� i nt .
NALYTICAL
4/28/2023
Pace Analytical Labs Charlotte
Tyriek Hooks
9800 Kindey Ave
Huntersville, NC, 28078
Ref: Analytical Testing
Report Number: 23-108-0004
Project Description: 92662175 Sludge
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Dear Tyriek Hooks:
Waypoint Analytical Virginia, Inc. received sample(s) on 4/18/2023 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information
Sincerely,
Brandi Watson
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 17 of 21
Page 1 of 5

•
7621 (2) Whitepine Road, Richmond, VA 23237
Waypoint,
Main 804-743-9401 ° Fax [phone]
ANALYTICAL www.waypointanalytical.com
Sample Summary Table
Report Number: 23-108-0004
Client Project Description: 92662175 Sludge
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
61808
Sludge
92662175001
Solids
61808
Sludge
92662175001
Solids
61808
Sludge
92662175001
Solids
61808
Sludge
92662175001
Solids
WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN
04/13/2023 08:20
04/18/2023
04/13/2023 08:20
04/18/2023
04/13/2023 08:20
04/18/2023
04/13/2023 08:20
04/18/2023
SM-2540G WP MTN
SM-4500-NH3C-TKN WP MTN
AOAC 955.01 WP MTN
Page 2 of 5
Page 18 of 21

■
Waypoint,
7621 Whitepine
Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
ANALYTICAL
www.waypointanalytical.com
11769
Pace Analytical Labs Charlotte
Project
92662175 Sludge
Tyriek Hooks
Report Date : 04/28/2023
9800 Kindey Ave
Information :
Received : 04/18/2023
Huntersville , NC 28078
Brandi Watson
Report Number : 23-108-0004
REPORT OFANAL YSIS
Lab No : 61808
Matrix: Solids
Sample ID : Sludge 92662175001
Sampled: 4/13/2023 8:20
Test
Results
Units
MOL
DF Date / Time
By Analytical
Analyzed
Method
C/N RATIO
33
Ratio
0
1 04/20/23 15:53
CALCULATION
Test
Results
Units
MQL
DF Date / Time
By Analytical
Analyzed
Method
Carbon (TOC)
27.4
%
0.010
1 04/20/23 15:53
CALCULATION
Total Solids
38.3
%
0.010
1 04/20/23 15:53
JLS SM-2540G
Analytical Method: SM-2540G
Test
Results
Units
MQL
DF Date / Time
By Analytical
Analyzed
Batch
Moisture
61.7
%
0.010
1 04/20/23 15:53
JLS L677392
Total Kjeldahl Nitrogen
Calcium Carbonate Equivalent
Total Volatile Solids
Qualifiers/ OF Dilution Factor
Definitions
8300
mg/Kg - dry
653
48.6
%
0.1
47.1
%
0.010
1 04/24/23 10:00 CLP ;M-4500-NH3C-TKP
1 04/27/23 09:43 DXT AOAC 955.01
1 04/20/23 15:53 JLS SM-2540G
MQL Method Quantitation Limit
Page 3 of S
Page 19 of 21

117?ceAnalyfical'
www.pacelabs.cem
May 23, 2023
Ms. Karen Bellamy
Cascades Tissue Group -NC
805 Midway Road
PO Box 578
Rockingham, NC 28380
RE: Project: May
Pace Project No.: 92666463
Dear Ms. Bellamy:
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
[phone]
Enclosed are the analytical results for sample(s) received by the laboratory on May 09, 2023. The results relate only to the
samples included in this report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless
otherwise footnoted.
Some analyses were subcontracted outside of the Pace Network. The test report from the external subcontractor is
attached to this report in its entirety.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Asheville
• Pace Analytical Services - Charlotte
• Pace Analytical Services - Peachtree Corners, GA
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Tyriek Hooks
[e-mail]
[phone]
Project Manager
Enclosures
cc: Cascades Tissue Group- Rockingham, Divsion of
Cascades Holding US Inc.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 1 of 20

17;a'ceAnalytical'
/ www.pacelabs.com
Project: May
Pace Project No.. 92666463
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
[phone]
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Laboratory ID: 99006
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
Pace Analytical Services Peachtree Corners
110 Technology Pkwy, Peachtree Corners, GA 30092
Florida DOH Certification #: E87315
Georgia DW Inorganics Certification #: 812
CERTIFICATIONS
South Carolina Certification #: 99006001
South Carolina Drinking Water Cert. #: 99006003
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Louisiana DoH Drinking Water#: LA029
Virginia/VELAP Certification #: 460221
South Carolina Laboratory ID: 99030
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
North Carolina Certification #: 381
South Carolina Certification #: 98011001
Virginia Certification #: 460204
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 20

aceAnalytical
www.paceiabs.com
Project: May
Pace Project No.: 92666463
Lab ID Sample ID
SAMPLE SUMMARY
Matrix Date Collected Date Received
92666463001 CASCADES Solid 05/09/23 08:35 05/09/23 09:30
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
[phone]
Page 3 of 20

/�?aceAnalytical
www.pacelabs.com
ANALYTICAL RESULTS
Project: May
Pace Project No.: 92666463
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
[phone]
Sample: CASCADES Lab ID: 92666463001 Collected: 05/09/23 08:35 Received: 05/09/23 09:30 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
6010D ATL ICP
Analytical Method: EPA 6010D Preparation Method: EPA 3050B
Pace Analytical Services - Peachtree Corners, GA
Calcium
174000 mg/kg 1030 130
5 05/10/23 11:35
05/11/2315:34 7440-70-2
Copper
26.2 mg/kg 8.2 3.3
1 05/10/23 11:35
05/10/23 21:41 7440-50-8
Magnesium
2550 mg/kg 10.3 5.8
1 05/10/23 11:35
05/10/23 21:41 7439-95-4
Nickel
1.1J mg/kg 4.1 1.0
1 05/10/23 11:35
05/10/23 21:41 7440-02-0
Zinc
83.3 mg/kg 6.2 5.6
1 05/10/23 11:35
05/10/23 21:41 7440-66-6
2540G Total Percent Solids
Analytical Method: SM 2540G-2011
Pace Analytical Services - Charlotte
Total Solids
44.3 % 0.10 0.000010
1
05/09/23 16:44
Percent Moisture
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
55.7 % 0.10 0.10
1
05/09/23 16:37 N2
9045 pH Soil
Analytical Method: EPA9045D
Pace Analytical Services - Asheville
pH at 25 Degrees C
7.9 Std. Units 0.10 0.10
1
05/19/23 12:22 H3
Plant Available Nitrogen
Analytical Method: None
Pace Analytical Services -Asheville
Plant Available Nitrogen
468 mg/kg
1
05/19/23 16:00 N2
Total Nitrogen Calculation
Analytical Method: TKN+NO3+NO2 Calculation
Pace Analytical Services - Asheville
Nitrogen
1560 mg/kg 40.0 20.0
1
05/19/2315:57 7727-37-9
350.1 Ammonia
Analytical Method: EPA 350.1 Rev 2.0 1993 Mod.
Preparation Method: EPA 350.1 Rev 2.0 1993 Mod.
Pace Analytical Services - Asheville
Nitrogen, Ammonia
ND mg/kg 20.9 20.9
1 05/16/23 15:20
05/17/23 12:07 7664-41-7
351.2 Total Kjeldahl Nitrogen
Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993
Pace Analytical Services - Asheville
Nitrogen, Kjeldahl, Total
1560 mg/kg 103 51.3
1 05/18/23 16:22
05/19/23 06:41 7727-37-9
353.2 Nitrogen, NO2/NO3
Analytical Method: EPA 353.2 Rev 2.0 1993 Preparation Method: EPA 353.2 Rev 2.0 1993
Pace Analytical Services - Asheville
Nitrogen, NO2 plus NO3
ND mg/kg 8.8 4A
1 05/09/23 23:22
05/10/23 01:00
Nitrogen, Nitrate
ND mg/kg 8.8 4A
1 05/09/23 23:22
05/10/23 01:00 14797-55-8
Nitrogen, Nitrite
ND mg/kg 8.8 2.2
1 05/09/23 23:22
05/10/23 01:00 14797-65-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/23/2023 05:58 PM without the written consent of Pace Analytical Services, LLC. Page 5 of 20

WayR?unt.(2)YTICAL
5/17/2023
Pace Analytical Labs Charlotte
Tyriek Hooks
9800 Kindey Ave
Huntersville, NC, 28078
Ref: Analytical Testing
Report Number: 23-130-0002
Project Description: 92666463
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Dear Tyriek Hooks:
Waypoint Analytical Virginia, Inc. received sample(s) on 5/10/2023 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Brandi Watson
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 16 of 20
Page 1 of 5

Waypoint.(2)
ANALYTICAL
Report Number: 23-130-0002
Client Project Description: 92666463
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Sample Summary Table
Lab No
Client Sample ID
Matrix
Date Collected
Date Received
Method
Lab ID
61963
Cascades
Solids
05/09/2023 08:55
05/10/2023
61963
Cascades
Solids
05/09/2023 08:55
05/10/2023
SM-2540G
WP MTN
61963
Cascades
Solids
05/09/2023 08:55
05/10/2023
SM-4500-NH3C-TKN
WP MTN
61963
Cascades
Solids
05/09/2023 08:55
05/10/2023
AOAC 955.01
WP MTN
WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN
Page 17 of 20
Page 2 of 5

0
■
Waypoint.
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
ANALYTICAL
www.waypointanalytical.com
11769
Pace Analytical Labs Charlotte
Project
92666463
Tyriek Hooks
Report Date : 05/17/2023
9800 Kindey Ave
Information :
Received : 05/10/2023
Huntersville , NC 28078
Brandi Watson
Report Number : 23-130-0002
REPORT OFANAL
YSIS
Lab No : 61963
Matrix: Solids
Sample ID : Cascades
Sampled: 5/9/2023 8:55
Test
Results
Units
MQL
DF Date / Time By Analytical
Analyzed Method
C/N RATIO
250
Ratio
0
1 05/12/23 07:10 CALCULATION
Test
Results
Units
MQL
DF Date / Time By Analytical
Analyzed Method
Carbon (TOC)
46.3
%
0.010
1 05/15/23 16:20 CALCULATION
Total Solids
75.1
%
0.010
1 05/15/23 16:20 JLS SM-2540G
Analytical Method: SM-2540G
Test
Results
Units
MQL
DF Date / Time By Analytical
Analyzed Batch
Moisture
24.9
%
0.010
1 05/15/23 16:20 JLS L682107
Total Kjeldahl Nitrogen
Calcium Carbonate Equivalent
Total Volatile Solids
Qualifiers/ DF Dilution Factor
Definitions
1840
mg/Kg - dry
333
44.9
%
0.1
79.7
%
0.010
1 05/12/23 07:10 JPJ ;M-4500-NH3C-TKP
1 05/16/23 11:15 DXT AOAC 955.01
1 05/15/23 16:20 JLS SM-2540G
MQL Method Quantitation Limit
Page 3 of 5
Page 18 of 20

ace
July 17, 2023
Ms. Karen Bellamy
Cascades Tissue Group -NC
805 Midway Road
PO Box 578
Rockingham, NC 28380
RE: Project: JUNE
Pace Project No.: 92672816
Dear Ms. Bellamy:
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
[phone]
Enclosed are the analytical results for sample(s) received by the laboratory on June 15, 2023. The results relate only to the
samples included in this report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless
otherwise footnoted.
Some analyses were subcontracted outside of the Pace Network. The test report from the external subcontractor is
attached to this report in its entirety.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Asheville
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
C (' wYl .jai anti
Angela Baioni for
Tyriek Hooks
[e-mail]
[phone]
Project Manager
Enclosures
cc: Cascades Tissue Group- Rockingham, Divsion of
Cascades Holding US Inc.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 1 of 21

Project: JUNE
Pace Project No.: 92672816
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
[phone]
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Laboratory ID: 99006
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
CERTIFICATIONS
South Carolina Certification #: 99006001
South Carolina Drinking Water Cert. #: 99006003
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Louisiana DoH Drinking Water #: LA029
VirginiaNELAP Certification #: 460221
South Carolina Laboratory ID: 99030
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 21

Project: JUNE
Pace Project No.: 92672816
Lab ID Sample ID
SAMPLE SUMMARY
Matrix Date Collected Date Received
92672816001 SLUDGE SAMPLES Solid 06/15/23 08:30 06/15/23 09:55
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
[phone]
Page 3 of 21

ace
ANALYTICAL RESULTS
Project: JUNE
Pace Project No.: 92672816
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
[phone]
Sample: SLUDGE SAMPLES Lab ID: 92672816001 Collected: 06/15/23 08:30 Received: 06/15/23 09:55 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Analytical Method: EPA 601 OD Preparation Method: EPA 3050B
Pace Analytical Services - Asheville
Calcium
159000 mg/kg 1220
152
25
06/22/2314:41
06/27/2318:25 7440-70-2
Copper
14.4 mg/kg 9.8
0.27
1
06/22/2314:41
06/26/2315:48 7440-50-8
Magnesium
1710 mg/kg 19.6
4.4
1
06/22/2314:41
06/26/2315:48 7439-95-4
Nickel
1.1 mg/kg 0.98
0.29
1
06/22/2314:41
06/26/2315:48 7440-02-0
Zinc
81.9 mg/kg 2.0
0.77
1
06/22/2314:41
06/26/2315:48 7440-66-6
254OG Total Percent Solids
Analytical Method: SM 254OG-2011
Pace Analytical Services - Charlotte
Total Solids
41.3 % 0.10
0.000010
1
06/20/23 15:09
Percent Moisture
Percent Moisture
9045 pH Soil
pH at 25 Degrees C
Plant Available Nitrogen
Plant Available Nitrogen
Total Nitrogen Calculation
Nitrogen
350.1 Ammonia
Nitrogen, Ammonia
351.2 Total Kjeldahl Nitrogen
Nitrogen, Kjeldahl, Total
353.2 Nitrogen, NO2/NO3
Nitrogen, NO2 plus NO3
Nitrogen, Nitrate
Nitrogen, Nitrite
Date: 07/17/2023 06:17 PM
Analytical Method: SW-846
Pace Analytical Services - Charlotte
58.7 % 0.10 0.10 1 06/20/2315:00
Analytical Method: EPA 9045D
Pace Analytical Services - Asheville
7.6 Std. Units 0.10 0.10 1 06/20/23 13:40
Analytical Method: None
Pace Analytical Services - Asheville
459 mg/kg 1 06/29/2314:21
Analytical Method: TKN+NO3+NO2 Calculation
Pace Analytical Services - Asheville
1530 mg/kg 40.0 20.0 1 06/26/2313:43 7727-37-9
Analytical Method: EPA 350.1 Rev 2.0 1993 Mod. Preparation Method: EPA 350.1 Rev 2.0 1993 Mod.
Pace Analytical Services - Asheville
ND mg/kg 22.9 22.9 1 06/28/2310:39 06/29/2313:00 7664-41-7
Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993
Pace Analytical Services - Asheville
1530 mg/kg 128 63.8 1 06/16/23 14:05 06/17/23 08:12 7727-37-9
Analytical Method: EPA 353.2 Rev 2.0 1993 Preparation Method: EPA 353.2 Rev 2.0 1993
Pace Analytical Services - Asheville
N2
H3
N2
M1
ND mg/kg 9.6 4.8 1 06/15/23 22:13 06/15/23 23:46
ND mg/kg 9.6 4.8 1 06/15/23 22:13 06/15/23 23:46 14797-55-8
ND mg/kg 9.6 2.4 1 06/15/23 22:13 06/15/23 23:46 14797-65-0 M1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 5 of 21

WayPA�int
[CAL
7/3/2023
Pace Analytical Labs Charlotte
Tyriek Hooks
9800 Kindey Ave
Huntersville, NC, 28078
Ref: Analytical Testing
Report Number: 23-172-0001
Project Description: 92672816
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Dear Tyriek Hooks:
Waypoint Analytical Virginia, Inc. received sample(s) on 6/21/2023 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information
Sincerely,
Q
Brandi Watson
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 17 of 21
Page 1 of 5

(D
Waypoint. 7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
ANALYTICAL www.waypointanalytical.com
Sample Summary Table
Report Number: 23-172-0001
Client Project Description: 92672816
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
62354
92672816001
Solids
62354
92672816001
Solids
62354
92672816001
Solids
62354
92672816001
Solids
WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN
06/15/2023 08:30
06/21/2023
06/15/2023 08:30
06/21/2023
06/15/2023 08:30
06/21/2023
06/15/2023 08:30
06/21/2023
SM-2540G
WP MTN
SM-4500-NH3C-TKN
WP MTN
AOAC 955.01
WP MTN
Page 2 of 5
Page 18 of 21

Waypointo
ANALYTICAL
11769
Pace Analytical Labs Charlotte Project 92672816
Tyriek Hooks
9800 Kindey Ave Information
Huntersville , NC 28078
Report Number : 23-172-0001 REPORTOFi
Lab No : 62354
Sample ID : 92672816001
Test Results Units
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Report Date : 07/03/2023
Received : 06/21/2023
Brandi Watson
VALYSIS
Matrix: Solids
Sampled: 6/15/2023 8:30
MQL DF Date / Time By Analytical
Analyzed Method
Total Solids
41.4 H
%
0.010
1
06/23/23 16:35
KDO
SM-254OG
Total Kjeldahl Nitrogen
3410
mg/Kg - dry
604
1
06/30/23 11:00
JPJ ')M-4500-NH3C-TKP
Calcium Carbonate Equivalent
40.9
%
0.1
1
06/29/23 15:30
DXT
AOAC 955.01
Total Volatile Solids
53.8 H
%
0.010
1
06/23/23 16:35
KDO
SM-2540G
C/N RATIO
92
Ratio
0
1
06/23/23 16:35
CALCULATION
Test
Results
Units
MQL
DF
Date / Time
By
Analytical
Analyzed
Method
Carbon (TOC)
31.3
%
0.010
1
06/23/23 16:35
CALCULATION
Analytical Method: SM-254OG
Test
Results
Units
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
Moisture 58.6 H % 0.010 1 06/23/23 16:35 KDO L689556
Qualifiers/ DF Dilution Factor
Definitions MQL Method Quantitation Limit
H Beyond holding time
Page 19 of 21
Page 3 of 5

ace
July 20, 2023
Ms. Karen Bellamy
Cascades Tissue Group -NC
805 Midway Road
PO Box 578
Rockingham, NC 28380
RE: Project: SLUDGE
Pace Project No.: 92675970
Dear Ms. Bellamy:
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
[phone]
Enclosed are the analytical results for sample(s) received by the laboratory on July 06, 2023. The results relate only to the
samples included in this report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless
otherwise footnoted.
Some analyses were subcontracted outside of the Pace Network. The test report from the external subcontractor is
attached to this report in its entirety.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Asheville
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
k&q�
Tyriek Hooks
[e-mail]
[phone]
Project Manager
Enclosures
cc: Cascades Tissue Group- Rockingham, Divsion of
Cascades Holding US Inc.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 1 of 20

Project: SLUDGE
Pace Project No.: 92675970
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
[phone]
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Laboratory ID: 99006
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
CERTIFICATIONS
South Carolina Certification #: 99006001
South Carolina Drinking Water Cert. #: 99006003
Florida/NELAP Certification #: E87627
Kentucky UST Certification M 84
Louisiana DoH Drinking Water#: LA029
VirginiaNELAP Certification #: 460221
South Carolina Laboratory ID: 99030
South Carolina Certification #: 99030001
VirginiaNELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 20

Project: SLUDGE
Pace Project No.: 92675970
Lab ID Sample ID
92675970001 SLUDGE
SAMPLE SUMMARY
Matrix Date Collected Date Received
Solid 07/06/23 08:00 07/06/23 11:56
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
[phone]
Page 3 of 20

ace
ANALYTICAL RESULTS
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
[phone]
Project: SLUDGE
Pace Project No.. 92675970
Sample: SLUDGE
Lab ID: 92675970001 Collected: 07/06/23 08:00 Received: 07/06/23 11:56 Matrix: Solid
Results reported on a "dry weight"
basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters
Results Units Limit MDL DF Prepared Analyzed CAS No.
Qua]
6010 MET ICP
Analytical Method: EPA 6010D Preparation Method: EPA 3050B
Pace Analytical Services - Asheville
Calcium
205000 mg/kg 3800 474 100 07/07/23 09:37 07/11/23 15:09 7440-70-2
Copper
19.4 mg/kg 7.6 0.21 1 07/07/23 09:37 07/09/23 19:10 7440-50-8
Magnesium
2320 mg/kg 15.2 3.4 1 07/07/23 09:37 07/09/23 19:10 7439-95-4
Nickel
1.4 mg/kg 0.76 0.22 1 07/07/23 09:37 07/09/23 19:10 7440-02-0
Zinc
172 mg/kg 1.5 0.60 1 07/07/23 09:37 07/09/23 19:10 7440-66-6
2540G Total Percent Solids
Analytical Method: SM 2540G-2011
Pace Analytical Services - Charlotte
Total Solids
37.0 % 0.10 0.000010 1 07/06/23 18:03
Percent Moisture
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
63.1 % 0.10 0.10 1 07/06/23 17:56
N2
9045 pH Soil
Analytical Method: EPA 9045D
Pace Analytical Services - Asheville
pH at 25 Degrees C
7.4 Std. Units 0.10 0.10 1 07/11/23 10:03
H3
350.1 Ammonia
Analytical Method: EPA 350.1 Rev 2.0 1993 Mod. Preparation Method: EPA 350.1 Rev 2.0 1993 Mod.
Pace Analytical Services - Asheville
Nitrogen, Ammonia
ND mg/kg 23.3 23.3 1 07/14/23 16:07 07/15/23 11:38 7664-41-7
351.2 Total Kjeldahl Nitrogen
Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993
Pace Analytical Services - Asheville
q(L
Nitrogen, Kjeldahl, Total
1330 mg/kg 113 56.4 1 07/17/23 18:10 07/18/23 03:29 7727-37-9
M1 g
1r
7 pzh-
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/20/2023 04:49 PM without the written consent of Pace Analytical Services, LLC. Page 5 of 20

WayPAoint.
NALYTICAL
7/17/2023
Pace Analytical Labs Charlotte
Tyriek Hooks
9800 Kindey Ave
Huntersville, NC, 28078
Ref: Analytical Testing
Report Number: 23-188-0004
Project Description: 92675970
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Dear Tyriek Hooks:
Waypoint Analytical Virginia, Inc. received sample(s) on 7/7/2023 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information
Sincerely,
Brandi Watson
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 16 of 20
Page 1 of 5

Waypoint, 7621 (2) Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
ANALYTICAL www.waypointanalytical.com
Sample Summary Table
Report Number: 23-188-0004
Client Project Description: 92675970
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
62584
Sludge
Solids
62584
Sludge
Solids
62584
Sludge
Solids
62584
Sludge
Solids
WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN
07/06/2023 08:00 07/07/2023
07/06/2023 08:00 07/07/2023
07/06/2023 08:00 07/07/2023
07/06/2023 08:00 07/07/2023
SM-2540G WP MTN
SM-4500-NH3C-TKN WP MTN
AOAC 955.01 WP MTN
Page 2 of 5
Page 17 of 20

Waypoint(2)
ANALYTICAL
11769
Pace Analytical Labs Charlotte Project 92675970
Tyriek Hooks
9800 Kindey Ave Information
Huntersville , NC 28078
Report Number: 23-188-0004 REPORTOFA
Lab No : 62584
Sample ID: Sludge
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Report Date : 07/17/2023
Received : 07/07/2023
(Jl�
Brandi Watson
VALY515
Matrix: Solids
Sampled: 7/6/2023 8:00
Test
Results
Units
MQL
DF Date / Time
Analyzed
By
Analytical
Method
Total Solids
52.6
%
0.010
1 07/13/23 18:30
KDO
SM-2540G
Total Kjeldahl Nitrogen
29800
mg/Kg - dry
475
1 07/13/23 08:30
JPJ ;M-4500-NH3C-TKP
Calcium Carbonate Equivalent
54.2
%
0.1
1 07/14/23 10:11
DXT
AOAC 955.01
Total Volatile Solids
31.9
%
0.010
1 07/13/23 18:30
KDO
SM-2540G
C/N RATIO
6
Ratio
0
1 07/13/23 08:30
CALCULATION
Test
Results
Units
MQL
DF Date / Time
By
Analytical
Analyzed
Method
Carbon (TOC)
18.5
%
0.010
1 07/13/23 18:30
CALCULATION
Analytical Method: SM-254OG
Test
Results
Units
MOL
DF Date / Time
By
Analytical
Analyzed
Batch
Moisture 47.4 % 0.010 1 07/13/23 18:30 KDO L692437
Qualifiers/ DF Dilution Factor
Definitions
MQL Method Quantitation Limit
Page 3 of 5
Page 18 of 20

�ce
July 19, 2023
Ms. Karen Bellamy
Cascades Tissue Group -NC
805 Midway Road
PO Box 578
Rockingham, NC 28380
RE: Project: SLUDGE
Pace Project No.: 92677873
Dear Ms. Bellamy:
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
[phone]
Enclosed are the analytical results for sample(s) received by the laboratory on July 18, 2023. The results relate only to the
samples included in this report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless
otherwise footnoted.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Asheville
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Tyriek Hooks
[e-mail]
[phone]
Project Manager
Enclosures
cc: Cascades Tissue Group- Rockingham, Divsion of
Cascades Holding US Inc.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 1 of 12

-"P
(- ace
Project: SLUDGE
Pace Project No.: 92677873
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
[phone]
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Laboratory ID: 99006
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
CERTIFICATIONS
South Carolina Certification #: 99006001
South Carolina Drinking Water Cert. #: 99006003
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Louisiana DoH Drinking Water#: LA029
VirginiaNELAP Certification #: 460221
South Carolina Laboratory ID: 99030
South Carolina Certification #: 99030001
VirginiaNELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 12

ace
Project: SLUDGE
Pace Project No.: 92677873
Lab ID Sample ID
SAMPLE SUMMARY
Matrix Date Collected Date Received
92677873001 CASCADES SLUDGE Solid 07/18/23 06:20 07/18/23 10:58
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
[phone]
Page 3 of 12

( A"qa ce,
ANALYTICAL RESULTS
Project: SLUDGE
Pace Project No.: 92677873
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
[phone]
Sample: CASCADES SLUDGE Lab ID: 92677873001 Collected: 07/18/23 06:20 Received: 07/18/23 10:58 Matrix: Solid
Results reported on a "dry weight' basis and are adjusted forpercent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qua]
Percent Moisture
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
56.5 % 0.10 0.10 1 07/18/23 16:55 N2
Plant Available Nitrogen
Analytical Method: None
Pace Analytical Services -Asheville
Plant Available Nitrogen
369 mg/kg 1 07/22/23 11:51 N2
Total Nitrogen Calculation
Analytical Method: TKN+NO3+NO2 Calculation
Pace Analytical Services -Asheville
Nitrogen
1230 mg/kg 40.0 20.0 1 07/22/2311:58 7727-37-9
350.1 Ammonia
Analytical Method: EPA 350.1 Rev 2.0 1993 Mod. Preparation Method: EPA 350.1 Rev 2.0 1993 Mod.
Pace Analytical Services -Asheville
Nitrogen, Ammonia
ND mg/kg 21.7 21.7 1 07/19/23 16:12 07/20/23 12:10 7664-41-7
351.2 Total Kjeldahl Nitrogen
Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993
Pace Analytical Services -Asheville
Nitrogen, Kjeldahl, Total
1230 mg/kg 92.0 46.0 1 07/21/23 17:13 07/22/23 05:38 7727-37-9
353.2 Nitrogen, NO2/NO3
Analytical Method: EPA 353.2 Rev 2.0 1993 Preparation Method: EPA 353.2 Rev 2.0 1993
Pace Analytical Services - Asheville
Nitrogen, NO2 plus NO3
ND mg/kg 8.9 4.5 1 07/18/23 22:13 07/18/23 23:45
Nitrogen, Nitrate
ND mg/kg 8.9 4.5 1 07/18/23 22:13 07/18/23 23:45 14797-55-8
Nitrogen, Nitrite
ND mg/kg 8.9 2.2 1 07/18/23 22:13 07/18/23 23:45 14797-65-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/02/2023 06:00 PM without the written consent of Pace Analytical Services, LLC Page 5 of 14

ace
October 05, 2023
Ms. Karen Bellamy
Cascades Tissue Group -NC
805 Midway Road
PO Box 578
Rockingham, NC 28380
RE: Project: AUGUST
Pace Project No.: 92683365
Dear Ms. Bellamy:
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
[phone]
Enclosed are the analytical results for sample(s) received by the laboratory on August 17, 2023. The results relate only to
the samples included in this report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless
otherwise footnoted.
Some analyses were subcontracted outside of the Pace Network. The test report from the external subcontractor is
attached to this report in its entirety.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Asheville
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Tyriek Hooks
[e-mail]
704-977-0947
Project Manager
Enclosures
cc: Cascades Tissue Group- Rockingham, Divsion of
Cascades Holding US Inc.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 1 of 21

CERTIFICATIONS
Project: AUGUST
Pace Project No.: 92683365
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
[phone]
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
South Carolina Certification #: 99006001
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
South Carolina Drinking Water Cert. #: 99006003
North Carolina Drinking Water Certification #: 37706
Florida/NELAP Certification #: E87627
North Carolina Field Services Certification #: 5342
Kentucky UST Certification #: 84
North Carolina Wastewater Certification #: 12
Louisiana DoH Drinking Water #: LA029
South Carolina Laboratory ID: 99006
Virginia/VELAP Certification #: 460221
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
South Carolina Laboratory ID: 99030
Florida/NELAP Certification #: E87648
South Carolina Certification #: 99030001
North Carolina Drinking Water Certification #: 37712
Virginia/VELAP Certification #: 460222
North Carolina Wastewater Certification #: 40
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 21

ace
Project: AUGUST
Pace Project No.. 92683365
Lab ID Sample ID
92683365001 SLUDGE
SAMPLE SUMMARY
Matrix Date Collected Date Received
Solid 08/17/23 08:30 08/17/23 08:34
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
[phone]
Page 3 of 21

Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
[phone]
ANALYTICAL RESULTS
Project: AUGUST
Pace Project No.: 92683365
Sample: SLUDGE Lab ID: 92683365001 Collected: 08/17/23 08:30 Received: 08/17/23 08:34 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qua[
254OG Total Percent Solids Analytical Method: SM 254OG-2011
Pace Analytical Services - Charlotte
Total Solids 41.5 % 0.10 0.000010 1 08/18/23 14:30
Percent Moisture Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture 58.5 % 0.10 0.10 1 08/18/23 14:19 N2
9045 pH Soil Analytical Method: EPA 9045D
Pace Analytical Services - Asheville
pH at 25 Degrees C 7.5 Std. Units 0.10 0.10 1 08/29/23 13:00 H1
Plant Available Nitrogen Analytical Method: None
Pace Analytical Services -Asheville
Plant Available Nitrogen 67.8 mg/kg 1 08/27/23 15:16 N2
Total Nitrogen Calculation Analytical Method: TKN+NO3+NO2 Calculation
Pace Analytical Services -Asheville 1�0
Nitrogen 226 mg/kg 40.0 20.0 1 08/2312314:15 7727-37-9 M.0 /
v
350.1 Ammonia Analytical Method: EPA 350.1 Rev 2.0 1993 Mod. Preparation Method: EPA 350.1 Rev 2.0 1993 Mod.
Pace Analytical Services - Asheville
Nitrogen, Ammonia ND mg/kg 22.8 22.8 1 08/24/23 08:32 08/24/23 12:42 7664-41-7
351.2 Total Kjeldahl Nitrogen Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993
Pace Analytical Services -Asheville
Nitrogen, Kjeldahl, Total 226 mg/kg 105 52.4 1 08/22/23 00:32 08/23/23 03:26 7727-37-9
353.2 Nitrogen, NO2/NO3 Analytical Method: EPA 353.2 Rev 2.0 1993 Preparation Method: EPA 353.2 Rev 2.0 1993 W_
Pace Analytical Services - Asheville
Nitrogen, NO2 plus NO3 ND mg/kg 9.6 4.8 1 08/18/23 00:02 08/18/23 01:54
Nitrogen, Nitrate ND mg/kg 9.6 4.8 1 08/18/23 00:02 08/18/23 01:54 14797-55-8
Nitrogen, Nitrite ND mg/kg 9.6 2.4 1 08/18/23 00:02 08/18/23 01:54 14797-65-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/05/2023 05:12 PM without the written consent of Pace Analytical Services, LLC. Page 5 of 21

a
WayRgunt
YTICAL
9/6/2023
Pace Analytical Labs Charlotte
Tyriek Hooks
9800 Kindey Ave
Huntersville, NC, 28078
Ref: Analytical Testing
Report Number: 23-233-0005
Project Description: 92683365 August
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Dear Tyriek Hooks:
Waypoint Analytical Virginia, Inc. received sample(s) on 8/21/2023 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Brandi Watson
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 16 of 21
Page 1 of 6

(2)
7621 Whitepine Road, Richmond, VA 23237
Waypoint,
Main 804-743-9401 ° Fax [phone]
ANALYTICAL www.waypointanalocal.com
Sample Summary Table
Report Number:
23-233-0005
Client Project Description:
92683365 August
Lab No Client Sample ID
Matrix
Date Collected
Date Received
Method
Lab ID
63127 Sludge 92683365001
Solids
08/17/2023 08:30
08/21/2023
63127 Sludge 92683365001
Solids
08/17/2023 08:30
08/21/2023
SM-2540G
WP MTN
63127 Sludge 92683365001
Solids
08/17/2023 08:30
08/21/2023
SM-4500-NH3C-TKN
WP MTN
63127 Sludge 92683365001
Solids
08/17/2023 08:30
08/21/2023
6010D
WP MTN
63127 Sludge 92683365001
Solids
08/17/2023 08:30
08/21/2023
AOAC 955.01
WP MTN
WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN
Page 2 of 6
Page 17 of 21

7621 0 Whitepine Road, Richmond, VA 23237
Waypoint,
Main 804-743-9401 ° Fax [phone]
ANALYTICAL www.waypointanalytical.com
11769
Pace Analytical Labs Charlotte Project 92683365 August Original Report Date : 09/06/2023
Tyriek Hooks Revised Report Date: 10/05/2023
9800 Kindey Ave Information : Received : 08/21/2023
Huntersville , NC 28078
Report Number : 23-233-0005 REPORT OFANAL YSIS
Lab No : 63127 Matrix: Solids
Sample ID : Sludge 92683365001 Sampled: 8/17/2023 8:30
Test
Results
Units
MOL
DF
Date / Time
By
Analytical
Analyzed
Method
Total Solids
29.7
%
0.010
1
08/23/23 16:50
CJR
SM-254OG
Total Kjeldahl Nitrogen
1880
mg/Kg - dry
842
1
08/25/23 12:00
JPJ iM-4500-NH3C-TKP
Calcium 154000
mg/Kg - dry
3370
20
09/28/23 11:26
TJS
6010D
Magnesium
1720
mg/Kg - dry
16.8
1
09/06/23 02:48
TJS
6010D
Copper
31.9
mg/Kg - dry
1.68
1
09/06/23 02:48
BKN
6010D
Zinc
79.8
mg/Kg - dry
4.21
1
09/06/23 02:48
BKN
6010D
Nickel
0.989
mg/Kg - dry
0.841
1
09/06/23 02:48
BKN
6010D
Calcium Carbonate Equivalent
51.4
%
0.1
1
09/01/23 11:18
DXT
AOAC 955.01
Total Volatile Solids
58.9
%
0.010
1
08/23/23 16:50
CJR
SM-254OG
C/N RATIO
180
Ratio
0
1
08/23/23 16:50
CALCULATION
Test
Results
Units
MQL
DF
Date / Time
By
Analytical
Analyzed
Method
Carbon (TOC)
34.2
%
0.010
1
08/23/23 16:50
JM
CALCULATION
Analytical Method: SM-2540G
Test
Results
Units
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
Moisture
70.3
%
0.010
1
08/23/23 16:50
CJR
L700426
Qualifiers/ DF Dilution Factor
MQL Method Quantitation Limit
Definitions
Page 18 of 21
Page 3 of 6

( A"'�a ce
October 09, 2023
Ms. Karen Bellamy
Cascades Tissue Group -NC
805 Midway Road
PO Box 578
Rockingham, NC 28380
RE: Project: September
Pace Project No.: 92688004
Dear Ms. Bellamy:
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
[phone]
Enclosed are the analytical results for sample(s) received by the laboratory on September 14, 2023. The results relate only
to the samples included in this report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless
otherwise footnoted.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Asheville
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Tyriek Hooks
[e-mail]
704-977-0947
Project Manager
Enclosures
cc: Cascades Tissue Group- Rockingham, Divsion of
Cascades Holding US Inc.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 1 of 16

Project: September
Pace Project No. 92688004
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
[phone]
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Laboratory ID: 99006
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
CERTIFICATIONS
South Carolina Certification #: 99006001
South Carolina Drinking Water Cert. #: 99006003
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Louisiana DoH Drinking Water#: LA029
VirginiaNELAP Certification #: 460221
South Carolina Laboratory ID: 99030
South Carolina Certification #: 99030001
VirginiaNELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 16

Project: September
Pace Project No.: 92688004
Lab ID Sample ID
92688004001 SLUDGE
SAMPLE SUMMARY
Matrix Date Collected Date Received
Solid 09/14/23 06:54 09/14/23 13:50
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
[phone]
Page 3 of 16

ace
ANALYTICAL RESULTS
Project: September
Pace Project No.: 92688004
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
[phone]
Sample: SLUDGE Lab ID: 92688004001 Collected: 09/14/23 06:54 Received: 09/14/23 13:50 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Analytical Method: EPA 601 OD Preparation Method: EPA 3050B
Pace Analytical Services - Asheville
Calcium
133000 mg/kg 1210 242 25 09/27/23 14:45
10/04/2316:13 7440-70-2
Copper
14.7 mg/kg 9.7 0.48 1 09/27/23 14:45
10/02/23 03:22 7440-50-8
Magnesium
1380 mg/kg 19.4 0.48 1 09/27/23 14:45
10/02/23 03:22 7439-95-4
Nickel
ND mg/kg 0.97 0.48 1 09/27/23 14:45
10/02/23 03:22 7440-02-0
Zinc
66.0 mg/kg 1.9 0.97 1 09/27/23 14:45
10/02/23 03:22 7440-66-6
7471 Mercury
Analytical Method: EPA 7471 B Preparation Method: EPA 7471 B
Pace Analytical Services - Asheville
Mercury
0.015 mg/kg 0.013 0.0081 1 09/27/2317:34
10/05/2318:19 7439-97-6
2540G Total Percent Solids
Analytical Method: SM 2540G-2011
Pace Analytical Services - Charlotte
Total Solids
41.4 % 0.10 0.000010 1
09/15/23 16:37
Percent Moisture
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
58.6 % 0.10 0.10 1
09/15/23 16:30 N2
9045 pH Soil
Analytical Method: EPA 9045D
Pace Analytical Services - Asheville
pH at 25 Degrees C
7.2 Std. Units 0.10 0.10 1
09/25/23 13:37 H3
Plant Available Nitrogen
Analytical Method: None
Pace Analytical Services - Asheville
Plant Available Nitrogen
552 mg/kg 1
09/27/23 17:02 N2
Total Nitrogen Calculation
Analytical Method: TKN+NO3+NO2 Calculation
Pace Analytical Services - Asheville
Nitrogen
1840 mg/kg 40.0 20.0 1
09/27/2316:58 7727-37-9
350.1 Ammonia
Analytical Method: EPA 350.1 Rev 2.0 1993 Mod. Preparation Method: EPA 350.1 Rev 2.0 1993 Mod.
Pace Analytical Services - Asheville
Nitrogen, Ammonia
ND mg/kg 21.5 21.5 1 09/16/23 09:46
09/16/23 13:11 7664-41-7
351.2 Total Kjeldahl Nitrogen
Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993
Pace Analytical Services - Asheville
Nitrogen, Kjeldahl, Total
1840 mg/kg 110 54.8 1 09/22/23 18:52
09/23/23 05:15 7727-37-9
353.2 Nitrogen, NO2/NO3
Analytical Method: EPA 353.2 Rev 2.0 1993 Preparation Method: EPA 353.2 Rev 2.0 1993
Pace Analytical Services - Asheville
Nitrogen, NO2 plus NO3
ND mg/kg 9.6 4.8 1 09/15/23 01:39
09/15/23 05:22
Nitrogen, Nitrate
ND mg/kg 9.6 4.8 1 09/15/23 01:39
09/15/23 05:22 14797-55-8
Nitrogen, Nitrite
ND mg/kg 9.6 2.4 1 09/15/23 01:39
09/15/23 05:22 14797-65-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/09/2023 04:17 PM
without the written consent of Pace Analytical Services, LLC.
Page 5 of 16

ace
October 09, 2023
Ms. Karen Bellamy
Cascades Tissue Group -NC
805 Midway Road
PO Box 578
Rockingham, NC 28380
RE: Project: September
Pace Project No.: 92690615
Dear Ms. Bellamy:
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
[phone]
Enclosed are the analytical results for sample(s) received by the laboratory on September 28, 2023. The results relate only
to the samples included in this report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless
otherwise footnoted.
Some analyses were subcontracted outside of the Pace Network. The test report from the external subcontractor is
attached to this report in its entirety.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Tyriek Hooks
[e-mail]
704-977-0947
Project Manager
Enclosures
cc: Cascades Tissue Group- Rockingham, Divsion of
Cascades Holding US Inc.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 1 of 10

Waypoint
ANALYTICAL
10/9/2023
Pace Analytical Labs Charlotte
Tyriek Hooks
9800 Kindey Ave
Huntersville, NC, 28078
Ref: Analytical Testing
Report Number: 23-272-0007
Project Description: Cascades Monthly Sludge
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-4401 ° Fax [phone]
www.waypointanalytical.com
Dear Tyriek Hooks:
Waypoint Analytical Virginia, Inc. received sample(s) on 9/29/2023 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information
Sincerely,
Brandi Watson
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 6 of 10
Page 1 of 5

s
7621 (2) Whitepine Road, Richmond, VA 23237
Waypoint.
Main 804-743-9401 ° Fax [phone]
ANALYTICAL www.waypointanalytical.com
Sample Summary Table
Report Number: 23-272-0007
Client Project Description: Cascades Monthly Sludge
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
63557
Sludge
Testing
Solids
63557
Sludge
Testing
Solids
63557
Sludge
Testing
Solids
63557
Sludge
Testing
Solids
WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN
09/28/2023 07:00 09/29/2023
09/28/2023 07:00 09/29/2023
09/28/2023 07:00 09/29/2023
09/28/2023 07:00 09/29/2023
SM-2540G WP MTN
SM-4500-NH3C-TKN WP MTN
AOAC 955.01 WP MTN
Page 2 of 5
Page 7 of 10

0
Waypoint,
7621 Whitepine
Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
ANALYTICAL
www.waypointanalytical.com
11769
Pace Analytical Labs Charlotte
Project
Cascades Monthly Sludge
Tyriek Hooks
Report Date : 10/09/2023
9800 Kindey Ave
Information :
Received : 09/29/2023
Huntersville , NC 28078
Brandi Watson
Report Number: 23-272-0007
REPORT OFANALYSIS
Lab No : 63557
Matrix: Solids
Sample ID : Sludge Testing
Sampled: 9/28/2023 7:00
Test
Results
Units
MQL
DF Date / Time
By Analytical
Analyzed
Method
C/N RATIO
100
Ratio
0
1 10/04/23 16:13
CALCULATION
Test
Results
Units
MQL
DF Date / Time
By Analytical
Analyzed
Method
Carbon (TOC)
29.4
%
0.010
1 10/04/23 16:13
CALCULATION
Total Solids
44.5
%
0.010
1 10/04/23 16:13
CAH SM-2540G
Analytical Method: SM-2540G
Test
Results
Units
MQL
DF Date / Time
By Analytical
Analyzed
Batch
Moisture
55.5
%
0.010
1 10/04/23 16:13
CAH L708764
Total Kjeldahl Nitrogen
Calcium Carbonate Equivalent
Total Volatile Solids
Qualifiers/ DF Dilution Factor
Definitions
2920 mg/Kg - dry 562
40.7 % 0.1
50.6 % 0.010
1 10/05/23 07:05 JPJ ;M-4500-NHX-TKP
1 10/06/23 14:28 DXT AOAC 955.01
1 10/04/23 16:13 CAH SM-2540G
MQL Method Quantitation Limit
Page 3 of 5
Page 8 of 10

Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
[phone]
December 28, 2023
Ms. Karen Bellamy
Cascades Tissue Group -NC
805 Midway Road
PO Box 578
Rockingham, NC 28380
RE: Project: October -Revised Report
Pace Project No.: 92691248
Dear Ms. Bellamy:
Enclosed are the analytical results for sample(s) received by the laboratory on October 03, 2023. The results relate only to
the samples included in this report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless
otherwise footnoted.
Some analyses were subcontracted outside of the Pace Network. The test report from the external subcontractor is
attached to this report in its entirety.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services -Asheville
• Pace Analytical Services - Charlotte
• Pace Analytical Services - Peachtree Corners, GA
Revision 1- This revision was issued on December 28, 2023. The report was reissued to add remove metal compounds
that were not requested per client's request.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Tyriek Hooks
[e-mail]
704-977-0947
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC Page 1 of 22

Pace Analytical Services, LLC
lacee
6701 Conference Drive
Raleigh, NC 27607
[phone]
December 28, 2023
Page 2
cc: Cascades Tissue Group- Rockingham, Divsion of
Cascades Holding US Inc.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 22

02
Project: October -Revised Report
Pace Project No.: 92691248
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Laboratory ID: 99006
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
Pace Analytical Services Peachtree Corners
110 Technology Pkwy, Peachtree Corners, GA 30092
Florida DOH Certification #: E87315
Georgia DW Inorganics Certification #: 812
CERTIFICATIONS
South Carolina Certification #: 99006001
South Carolina Drinking Water Cert. #: 99006003
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Louisiana DoH Drinking Water #: LA029
MrginiaNELAP Certification #: 460221
South Carolina Laboratory ID: 99030
South Carolina Certification #: 99030001
VirginiaNELAP Certification #: 460222
North Carolina Certification #: 381
South Carolina Certification #: 98011001
Virginia Certification #: 460204
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
[phone]
Page 3 of 22

Project: October -Revised Report
Pace Project No. 92691248
Lab ID Sample ID
SAMPLE SUMMARY
Matrix Date Collected Date Received
92691248001 SLUDGE SAMPLE Solid 10/03/23 08:15 10/03/23 10:40
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
[phone]
Page 4 of 22

�Ce"
ANALYTICAL RESULTS
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
[phone]
Project: October -Revised Report
Pace Project No.: 92691248
Sample: SLUDGE SAMPLE
Lab ID: 92691248001 Collected: 10/03/23 08:15 Received: 10/03/23 10:40 Matrix: Solid
Results reported on a "dry weight"
basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters
Results Units Limit MDL DF Prepared
Analyzed CAS No.
Qual
601OD ATL ICP
Analytical Method: EPA 601OD Preparation Method: EPA 3050B
Pace Analytical Services - Peachtree Corners, GA
Calcium
168000 mg/kg 772 98.2 10 10/14/23 14:01
11/01/2319:21 7440-70-2
M1
Copper
17.9 mg/kg 3.1 1.3 1 10/14/23 14:01
10/25/23 23:38 7440-50-8
M1
Magnesium
2280 mg/kg 3.9 2.2 1 10/14/23 14:01
11/01/2319:16 7439-95-4
M1
Nickel
1.4J mg/kg 1.5 0.38 1 10/14/23 14:01
11/01/2319:16 7440-02-0
Zinc
66.5 mg/kg 2.3 2.1 1 10/14/23 14:01
10/25/23 23:38 7440-66-6
M1
254OG Total Percent Solids
Analytical Method: SM 2540G-2011
Pace Analytical Services - Charlotte
Total Solids
31.9 % 0.10 0.000010 1
10/04/23 13:38
Percent Moisture
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
68.1 % 0.10 0.10 1
10/04/23 13:30
N2
9045 pH Soil
Analytical Method: EPA 9045D
Pace Analytical Services -Asheville
pH at 25 Degrees C
7.6 Std. Units 0.10 0.10 1
10/10/23 17:35
H3
Plant Available Nitrogen
Analytical Method: None
Pace Analytical Services -Asheville
Plant Available Nitrogen
801 mg/kg 1
10/16/23 10:52
N2
Total Nitrogen Calculation
Analytical Method: TKN+NO3+NO2 Calculation
Pace Analytical Services - Asheville
Nitrogen
2670 mg/kg 40.0 20.0 1
10/16/2310:48 7727-37-9
350.1 Ammonia
Analytical Method: EPA 350.1 Rev 2.0 1993 Mod. Preparation Method: EPA 350.1 Rev 2.0 1993 Mod.
Pace Analytical Services -Asheville
Nitrogen, Ammonia
ND mg/kg 26.6 26.6 1 10/13/23 10:06
10/13/23 14:22 7664-41-7
351.2 Total Kjeldahl Nitrogen
Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993
Pace Analytical Services - Asheville
Nitrogen, Kjeldahl, Total
2670 mg/kg 143 71.3 1 10/06/23 15:39
10/07/23 05:24 7727-37-9
353.2 Nitrogen, N021NO3
Analytical Method: EPA 353.2 Rev 2.0 1993 Preparation Method: EPA 353.2 Rev 2.0 1993
Pace Analytical Services - Asheville
Nitrogen, NO2 plus NO3
ND mg/kg 12.3 6.2 1 10/04/23 02:43
10/04/23 05:03
Nitrogen, Nitrate
ND mg/kg 12.3 6.2 1 10/04/23 02:43
10/04/23 05:03 14797-55-8
Nitrogen, Nitrite
ND mg/kg 12.3 3.1 1 10/04/23 02:43
10/04/23 05:03 14797-65-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/31/2024 09:33 AM without the written consent of Pace Analytical Services, LLC. Page 6 of 22

Waypoint(D
ANALYTICAL
10/18/2023
Pace Analytical Labs Charlotte
Tyriek Hooks
9800 Kindey Ave
Huntersville, NC, 28078
Ref: Analytical Testing
Report Number: 23-278-0003
Project Description: 92691248
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Dear Tyriek Hooks:
Waypoint Analytical Virginia, Inc. received sample(s) on 10/5/2023 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information
Sincerely,
Brandi Watson
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 18 of 22
Page 1 of 5

(2)
Waypoint 7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
ANALYTICAL www.waypointanalytical.com
Sample Summary Table
Report Number: 23-278-0003
Client Project Description: 92691248
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
63619 Sludge
Sample
Solids
63619 Sludge
Sample
Solids
63619 Sludge
Sample
Solids
63619 Sludge
Sample
Solids
WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN
10/03/2023 08:15
10/05/2023
10/03/2023 08:15
10/05/2023
10/03/2023 08:15
10/05/2023
10/03/2023 08:15
10/05/2023
SM-254OG
WP MTN
SM-4500-NH3C-TKN
WP MTN
AOAC 955.01
WP MTN
Page 2 of 5
Page 19 of 22

0
Waypoint
7621 Whitepine
Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
ANALYTICAL
www.waypointanalytical.com
11769
Pace Analytical Labs Charlotte
Project
92691248
Tyriek Hooks
Report Date : 10/18/2023
9800 Kindey Ave
Information :
Received = 10/05/2023
Huntersville , NC 28078
Brandi Watson
Report Number: 23-278-0003
REPOR T OF A
NA L YSIS
Lab No : 63619
Matrix: Solids
Sample ID : Sludge Sample
Sampled: 10/3/2023 8:15
Test
Results
Units
MQL
DF Date / Time By Analytical
Analyzed Method
C/N RATIO
54
Ratio
0
1 10/09/23 17:26 CALCULATION
Test
Results
Units
MQL
DF Date / Time By Analytical
Analyzed Method
Carbon (TOC)
31.5
%
0.010
1 10/09/23 17:26 CALCULATION
Total Solids
38.9
%
0.010
1 10/09/23 17:26 OR SM-2540G
Analytical Method: SM-254OG
Test
Results
Units
MQL
DF Date / Time By Analytical
Analyzed Batch
Moisture
61.1
%
0.010
1 10/09/23 17:26 OR L709658
Test
Results
Units
MQL
DF Date / Time By Analytical
Analyzed Method
Total Kjeldahl Nitrogen
5810
mg/Kg - dry
643
1 10/18/23 10:30 JPJ ;M-4500-NH3C-TKP
Calcium Carbonate Equivalent
38.3
%
0.1
1 10/11/23 14:31 DXT AOAC 955.01
Total Volatile Solids
54.1
%
0.010
1 10/09/23 17:26 OR SM-254OG
Qualifiers/ DF Dilution Factor
MQL Method Quantitation Limit
Definitions
Page 20 of 22
Page 3 of S

Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
[phone]
December 05, 2023
Ms. Karen Bellamy
Cascades Tissue Group -NC
805 Midway Road
PO Box 578
Rockingham, NC 28380
RE: Project: SLUDGE
Pace Project No.: 92697975
Dear Ms. Bellamy:
Enclosed are the analytical results for sample(s) received by the laboratory on November 09, 2023. The results relate only
to the samples included in this report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless
otherwise footnoted.
Some analyses were subcontracted outside of the Pace Network. The test report from the external subcontractor is
attached to this report in its entirety.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Asheville
• Pace Analytical Services - Charlotte
• Pace Analytical Services - Ormond Beach
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
1- n9, —
Tyriek Hooks
[e-mail]
704-977-0947
Project Manager
Enclosures
cc: Cascades Tissue Group- Rockingham, Divsion of
Cascades Holding US Inc.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 1 of 21

ace
Project: SLUDGE
Pace Project No.: 92697975
Pace Analytical Services Ormond Beach
8 East Tower Circle, Ormond Beach, FL 32174
Alaska DEC- CS/UST/LUST
Alabama Certification #: 41320
Colorado Certification: FL NELAC Reciprocity
Connecticut Certification #: PH-0216
Delaware Certification: FL NELAC Reciprocity
DoD-ANAB #:ADE-3199
Florida Certification #: E83079
Georgia Certification #: 955
Guam Certification: FL NELAC Reciprocity
Hawaii Certification: FL NELAC Reciprocity
Illinois Certification #: 200068
Indiana Certification: FL NELAC Reciprocity
Kansas Certification #: E-10383
Kentucky Certification #: 90050
Louisiana Certification #: FL NELAC Reciprocity
Louisiana Environmental Certificate #: 05007
Maine Certification #: FLO1264
Maryland Certification: #346
Massachusetts Certification #: M-FL1264
Michigan Certification #: 9911
Mississippi Certification: FL NELAC Reciprocity
Pace Analytical Services, LLC
6701 Conference Drive
CERTIFICATIONS
Missouri Certification #: 236
Montana Certification #: Cert 0074
Nebraska Certification: NE-OS-28-14
New Hampshire Certification #: 2958
New Jersey Certification M FL022
New York Certification #: 11608
North Carolina Environmental Certificate #: 667
North Carolina Certification #: 12710
North Dakota Certification #: R-216
Ohio DEP 87780
Oklahoma Certification #: D9947
Pennsylvania Certification #: 68-00547
Puerto Rico Certification #: FLO1264
South Carolina Certification: #96042001
Tennessee Certification #: TN02974
Texas Certification: FL NELAC Reciprocity
US Virgin Islands Certification: FL NELAC Reciprocity
Virginia Environmental Certification #: 460165
West Virginia Certification #: 9962C
Wisconsin Certification #: 399079670
Wyoming (EPA Region 8): FL NELAC Reciprocity
Raleigh, NC 27607
(919)8344984
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
South Carolina Certification #: 99006001
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
South Carolina Drinking Water Cert. #: 99006003
North Carolina Drinking Water Certification #: 37706
Florida/NELAP Certification #: E87627
North Carolina Field Services Certification #: 5342
Kentucky UST Certification #: 84
North Carolina Wastewater Certification #: 12
Louisiana DoH Drinking Water #: LA029
South Carolina Laboratory ID: 99006
Virginia/VELAP Certification #: 460221
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
South Carolina Laboratory ID: 99030
Florida/NELAP Certification #: E87648
South Carolina Certification #: 99030001
North Carolina Drinking Water Certification #: 37712
Virginia/VELAP Certification #: 460222
North Carolina Wastewater Certification #: 40
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 21

ace
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
[phone]
SAMPLE SUMMARY
Project: SLUDGE
Pace Project No.. 92697975
Lab ID Sample ID Matrix Date Collected Date Received
92697975001 CACADES SLUDGE SAMPLE Solid 11/09/23 08:06 11/09/23 10:31
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 3 of 21

ANALYTICAL RESULTS
Project: SLUDGE
Pace Project No.: 92697975
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
[phone]
Sample: CACADES SLUDGE Lab ID: 92697975001 Collected: 11/09/23 08:06 Received: 11/09/23 10:31 Matrix: Solid
SAMPLE
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Analytical Method: EPA 6010 Preparation Method: EPA 3050
Pace Analytical Services - Ormond Beach
Calcium
336000 mg/kg 4850 3490
20
11/20/2312:00
11/21/2310:31
7440-70-2
Copper
31.9 mg/kg 1.2 0.61
1
11/20/23 12:00
11/21/23 10:35
7440-50-8
Magnesium
3220 mg/kg 121 60.6
1
11/20/2312:00
11/21/2310:35
7439-95-4
Nickel
0.891 mg/kg 1.2 0.61
1
11/20/2312:00
11/21/2310:35
7440-02-0
Zinc
125 mg/kg 24.3 8.7
1
11/20/2312:00
11/21/2310:35
7440-66-6
254OG Total Percent Solids
Analytical Method: SM 2540G-2011
Pace Analytical Services - Charlotte
Total Solids
22.1 % 0.10 0.000010
1
11/10/23 15:40
Percent Moisture
Percent Moisture
9045 pH Soil
pH at 25 Degrees C
Plant Available Nitrogen
Plant Available Nitrogen
Total Nitrogen Calculation
Nitrogen
350.1 Ammonia
Nitrogen, Ammonia
351.2 Total Kjeldahl Nitrogen
Nitrogen, Kjeldahl, Total
353.2 Nitrogen, NO2/NO3
Nitrogen, NO2 plus NO3
Nitrogen, Nitrate
Nitrogen, Nitrite
Date: 12/05/2023 04:23 PM
Analytical Method: SW-846
Pace Analytical Services - Charlotte
77.9 % 0.10 0.10 1 11/10/2315:32
Analytical Method: EPA 9045D
Pace Analytical Services - Asheville
7.5 Std. Units 0.10 0.10 1 11/17/23 15:12
Analytical Method: None
Pace Analytical Services - Asheville
1140 mg/kg 1 11/27/2316:39
Analytical Method: TKN+NO3+NO2 Calculation
Pace Analytical Services -Asheville
3810 mg/kg 40.0 20.0 1 11/21/2313:39 7727-37-9
Analytical Method: EPA 350.1 Rev 2.0 1993 Mod. Preparation Method: EPA 350.1 Rev 2.0 1993 Mod.
Pace Analytical Services - Asheville
ND mg/kg 41.2 41.2 1 11/25/2310:39 11/25/2312:45 7664-41-7
Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993
Pace Analytical Services -Asheville
3810 mg/kg 174 87.2 1 11/15/23 20:20 11/16/23 06:47 7727-37-9
Analytical Method: EPA 353.2 Rev 2.0 1993 Preparation Method: EPA 353.2 Rev 2.0 1993
Pace Analytical Services -Asheville
N2
N2
AAHZI
ND mg/kg 17.5 8.8 1 11/09/23 22:55 11/10/23 00:33
ND mg/kg 17.5 8.8 1 11/09/23 22:55 11/10/23 00:33 14797-55-8
ND mg/kg 17.5 4.4 1 11/09/23 22:55 11/10/23 00:33 14797-65-0 M1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 5 of 21

Waypoint(D
ANALYTICAL
12/5/2023
Pace Analytical Labs Charlotte
Tyriek Hooks
9800 Kindey Ave
Huntersville, NC, 28078
Ref: Analytical Testing
Report Number: 23-318-0005
Project Description: 92697975
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Dear Tyriek Hooks:
Waypoint Analytical Virginia, Inc. received sample(s) on 11/14/2023 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Brandi Watson
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 17 of 21
Page 1 of 5

(D
7621 Whitepine Road, Richmond, VA 23237
Waypoint. Main 804-743-9401 ° Fax [phone]
ANALYTICAL www.waypointanalytical.com
Sample Summary Table
Report Number: 23-318-0005
Client Project Description: 9269797S
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
63947
Cascades Sludge Sample
Solids
11/09/2023 08:06
11/14/2023
63947
Cascades Sludge Sample
Solids
11/09/2023 08:06
11/14/2023 SM-254OG WP MTN
63947
Cascades Sludge Sample
Solids
11/09/2023 08:06
11/14/2023 SM-4500-NH3C-TKN WP MTN
63947
Cascades Sludge Sample
Solids
11/09/2023 08:06
11/14/2023 AOAC 955.01 WP MTN
WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN
Page 2 of 5
Page 18 of 21

Waypointo
ANALYTICAL
11769
Pace Analytical Labs Charlotte Project 92697975
Tyriek Hooks
9800 Kindey Ave Information :
Huntersville , NC 28078
Report Number : 23-318-0005 REPORTOFo
Lab No : 63947
Sample ID: Cascades Sludge Sample
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Report Date : 12/05/2023
Received : 11/14/2023
�/ya�i CL
Brandi Watson
VALYSIS
Matrix: Solids
Sampled: 11/9/2023 8:06
Test Results Units MQL DF Date / Time By Analytical
Analyzed Method
Total Solids
Total Kjeldahl Nitrogen
Calcium Carbonate Equivalent
Total Volatile Solids
C/N RATIO
Test
Carbon (TOC)
Analytical Method: SM-2540G
Test
40.0
%
0.010
1
11/15/2316:24
CAH
SM-254OG
2170
mg/Kg - dry
625
1
12/05/23 12:24
JPJ ')M-4500-NH3C-TKP
43.1
%
0.1
1
11/28/23 15:07
DXT
AOAC 955.01
50.8
0/0
0.010
1
11/15/2316:24
CAH
SM-254OG
140
Ratio
0
1
11/15/2316:24
CALCULATION
Results
Units
MQL
DF
Date / Time
By
Analytical
Analyzed
Method
29.5 % 0.010 1 11/15/23 16:24 CALCULATION
Results Units MQL DF Date / Time By Analytical
Analyzed Batch
Moisture 60.0 % 0.010 1 11/15/2316:24 CAH L717359
Qualifiers/ DF Dilution Factor
Definitions
MQL Method Quantitation Limit
Page 3 of 5
Page 19 of 21

Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
[phone]
January 03, 2024
Ms. Karen Bellamy
Cascades Tissue Group -NC
805 Midway Road
PO Box 578
Rockingham, NC 28380
RE: Project: December
Pace Project No.: 92702587
Dear Ms. Bellamy:
Enclosed are the analytical results for sample(s) received by the laboratory on December 07, 2023. The results relate only
to the samples included in this report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless
otherwise footnoted.
Some analyses were subcontracted outside of the Pace Network. The test report from the external subcontractor is
attached to this report in its entirety.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Asheville
• Pace Analytical Services - Charlotte
• Pace Analytical Services - Peachtree Corners, GA
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Sarah Graham for
Tyriek Hooks
[e-mail]
704-977-0947
Project Manager
Enclosures
cc: Cascades Tissue Group- Rockingham, Divsion of
Cascades Holding US Inc.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 1 of 16

�ce
Project: December
Pace Project No.. 92702587
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
[phone]
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Laboratory ID: 99006
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
Pace Analytical Services Peachtree Corners
110 Technology Pkwy, Peachtree Corners, GA 30092
Florida DOH Certification #: E87315
Georgia DW Inorganics Certification #: 812
CERTIFICATIONS
South Carolina Certification #: 99006001
South Carolina Drinking Water Cert. M 99006003
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Louisiana DoH Drinking Water* LA029
Virginia/VELAP Certification #: 460221
South Carolina Laboratory ID: 99030
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
North Carolina Certification #: 381
South Carolina Certification #: 98011001
Virginia Certification #: 460204
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 16

�ce
Project: December
Pace Project No.: 92702587
Lab ID Sample ID
SAMPLE SUMMARY
Matrix Date Collected Date Received
92702587001 CASCADES Solid 12/07/23 08:35 12/07/23 11:10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
[phone]
Page 3 of 16

�ce
ANALYTICAL RESULTS
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
[phone]
Project: December
Pace Project No.: 92702587
Sample: CASCADES
Lab ID: 92702587001 Collected: 12/07/23 08:35 Received: 12/07/23 11:10 Matrix: Solid
Results reported on a 'dry weight' basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters
Results Units Limit MDL DF Prepared
Analyzed CAS No. Qual
601 OD ATL ICP
Analytical Method: EPA 601 OD Preparation Method: EPA 3050E
Pace Analytical Services - Peachtree Corners, GA
Calcium
184000 mg/kg 1580 200 20 12/21/23 12:47
12/27/23 09:07 7440-70-2
Copper
19.3 mg/kg 3.2 1.3 1 12/21/23 12:47
12/22/23 09:32 7440-50-8
Magnesium
2110 mg/kg 3.9 2.2 1 12/21/23 12:47
12/22/23 09:32 7439-95-4
Nickel
11.4.11 mg/kg 1.6 0.39 1 12/21/23 12:47
12/22/23 09:32 7440-02-0
Zinc
220 mg/kg 2.4 2.2 1 12/21/23 12:47
12/22/23 09:32 7440-66-6
254OG Total Percent Solids
Analytical Method: SM 2540G-2011
Pace Analytical Services - Charlotte
Total Solids
31.4 % 0.10 0.000010 1
12/11/23 12:12
Percent Moisture
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
68.6 % 0.10 0.10 1
12/11/23 12:04 N2
9045 pH Soil
Analytical Method: EPA 9045D
Pace Analytical Services - Asheville
pH at 25 Degrees C
7.6 Std. Units 0.10 0.10 1
12/13/23 13:42 H3
Plant Available Nitrogen
Analytical Method: None
Pace Analytical Services - Asheville
Plant Available Nitrogen
735 mg/kg 1
12/14/23 08:26 N2
Total Nitrogen Calculation
Analytical Method: TKN+NO3+NO2 Calculation
Pace Analytical Services - Asheville
Nitrogen
2450 mg/kg 40.0 20.0 1
12/15/2317:59 7727-37-9
350.1 Ammonia
Analytical Method: EPA 350.1 Rev 2.0 1993 Mod. Preparation Method: EPA 350.1 Rev 2.0 1993 Mod.
Pace Analytical Services - Asheville
Nitrogen, Ammonia
ND mg/kg 31.2 31.2 1 12/09/23 15:28
12/12/23 07:22 7664-41-7
351.2 Total Kjeldahl Nitrogen
Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993
Pace Analytical Services - Asheville
Nitrogen, Kjeldahl, Total
2450 mg/kg 127 63.7 1 12/13/23 18:33
12/14/23 06:17 7727-37-9
353.2 Nitrogen, NO2/NO3
Analytical Method: EPA 353.2 Rev 2.0 1993 Preparation Method: EPA 353.2 Rev 2.0 1993
Pace Analytical Services -Asheville
Nitrogen, NO2 plus NO3
ND mg/kg 12.7 6.3 1 12/07/23 23:45
12/08/23 02:27
Nitrogen, Nitrate
ND mg/kg 12.7 6.3 1 12/07/23 23:45
12/08/23 02:27 14797-55-8
Nitrogen, Nitrite
ND mg/kg 12.7 3.2 1 12/07/23 23:45
12/08/23 02:27 14797-65-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /03/2024 04:36 PM without the written consent of Pace Analytical Services, LLC. Page 5 of 16

WayR?unt
ANALYTICAL
1/31/2024
Pace Analytical Labs Charlotte
Tyriek Hooks
9800 Kindey Ave
Huntersville, NC, 28078
Ref: Analytical Testing
Report Number: 24-005-0003
Project Description: 92706797
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Dear Tyriek Hooks:
Waypoint Analytical Virginia, Inc. received sample(s) on 1/5/2024 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Brandi Watson
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 12 of 18
Page 1 of 7

(DW
*���� � ��
7621 Whitepine Road, Richmond, VA 23237
a
Main 804-743-9401 ° Fax [phone]
ANALYTICAL
www.waypointanalytical.com
Sample Summary Table
Report Number: 24-005-0003
Client Project Description: 92706797
Lab No Client Sample ID
Matrix
Date Collected
Date Received Method
Lab ID
64371 Cascades Tissur Group Inc
Solids
12/29/2023 09:30
01/05/2024
64371 Cascades Tissur Group Inc
Solids
12/29/2023 09:30
01/05/2024 SM-2540G
WP MTN
64371 Cascades Tissur Group Inc
Solids
12/29/2023 09:30
01/05/2024 SM-4500-NH3C-TKN
WP MTN
64371 Cascades Tissur Group Inc
Solids
12/29/2023 09:30
01/05/2024 AOAC 955.01
WP MTN
WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN
Page 13 of 18

■
Waypoint.
7621 Whitepine
Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
ANALYTICAL
www.waypointanalocal.com
11769
Pace Analytical Labs Charlotte
Project
92706797
Tyriek Hooks
Report Date : 01/31/2024
9800 Kindey Ave
Information :
Received : 01/05/2024
Huntersville , NC 28078
Brandii Watson
Report Number : 24-005-0003
REPORT OFANALYSIS
Lab No : 64371
Matrix: Solids
Sample ID : Cascades Tissur Group Inc
Sampled: 12/29/2023 9:30
Test
Results
Units
MQL
DF Date / Time
By Analytical
Analyzed
Method
C/N RATIO
98
Ratio
0
1 01/09/24 14:00
CALCULATION
Test
Results
Units
MQL
DF Date / Time
By Analytical
Analyzed
Method
Carbon (TOC)
29.1
%
0.010
1 01/09/24 14:00
CALCULATION
Total Solids
39.2 H
%
0.010
1 01/09/24 14:00
CJR SM-2540G
Analytical Method: SM-2540G
Test
Results
Units
MQL
DF Date / Time
By Analytical
Analyzed
Batch
Moisture
60.8 H
%
0.010
1 01/09/24 14:00
CJR L726878
Test
Results
Units
MQL
DF Date / Time
By Analytical
Analyzed
Method
Total Kjeldahl Nitrogen
2980 H
mg/Kg - dry
638
1 01/30/24 10:29
JPJ ')M-4500-NH3C-TKP
Calcium Carbonate Equivalent
37.3
%
0.1
1 01/19/24 11:53
DXT AOAC 955.01
Total Volatile Solids
50.1 H
%
0.010
1 01/09/24 14:00
CIR SM-2540G
Qualifiers/ DF Dilution Factor
H Beyond holding time
Definitions MQL Method Quantitation Limit
Page 14 of 18
Page 3 of 7

summill Summit Environmental Technologies, Inc.
3310 Win St.
4U1110?- IENTdL TEfiINOLC IFS, %C Cuyahoga Falls, Ohio 44223
�,1iyfTEL: [phone] FAX: [phone]
Website: http:lAvww.settek.com
July 12, 2023
Karen Bellamy
Cascades Tissue Group - North Carolina Inc
a division of Cascades Holding US Inc.
805 Midway Road
P.O. Box 578
Rockingham, NC 28379
TEL: [phone]
FAX: [phone]
Dear Karen Bellamy: Order No.: 23070031
Summit Environmental Technologies, Inc. received 1 sample(s) on 6/30/2023 for the
analyses presented in the following report.
There were no problems with the analytical events associated with this report unless noted
in the Case Narrative.
Quality control data is within laboratory defined or method specified acceptance limits
except where noted.
If you have any questions regarding these tests results, please feel free to call the
laboratory.
Sincerely,
Holly Florea
Project Manager
3310 Win St.
Cuyahoga Falls, Ohio 44223
Arkansas 88-0735, Califomia 2943, Colorado, Connecticut PH-0108, Florida NE LAC E87688, Idaho OH00923, Illinois 200061, Indiana C-OH-13,
ISO/IEC 17025:2017 119125 L22-544, Kansas E-10347, Kentucky (Underground Storage Tank) 3, Kentucky 90146, Maryland 339, Michigan 9988,
Minnesota 1780279, Nevada OH009232020-1, New Hampshire 2996, New Jersey OH006, New York 11777, North Carolina 39705 and 631, North Dakota
R-201, Ohio DW, Ohio VAP CL0052, Oklahoma 2019-155, Oregon OH2O0001, Pennsylvania 68-01335, Rhode Island LA000317, South Carolina
92016001, Texas T104704466-19-16, Utah OH009232020-12, Virginia VELAP 10391, West Virginia 9957C
Page 1 of 10

SUMMIT Summit Environmental Technologies, Inc. Case Narrative
3310 Win St.
ENVIPONMENTA.L 7ECHNOU019S, NC. Cuyahoga Falls, Ohio 44223 WO#: 23070031
Anatyf,cal Lah,,ra.fcr'tes TEL: [phone] FAX. [phone]
Website: hrta:Ihv+vw,settekcom. Date: 7/12/2023
CLIENT: Cascades Tissue Group - North Carolina Inc
Project:
WorkOrder Narrative:
This report in its entirety consists of the following documents: Cover Letter, Case Narrative, Analytical
Results, QC Summary Report, Applicable Accreditation Information, Chain -of -Custody, Cooler
Receipt Form, and other applicable forms as necessary. All documents contain the Summit
Environmental Technologies, Inc., Work Order Number assigned to this report.
Summit Environmental Technologies, Inc., holds the accreditations/certifications listed at the bottom of
the cover letter that may or may not pertain to this report. Please refer to the "Accreditation Program
Analytes Report" for accredited analytes list.
The information contained in this analytical report is the sole property of Summit Environmental
Technologies, Inc. and that of the customer. It cannot be reproduced in any form without the consent of
Summit Environmental Technologies, Inc. or the customer for which this report was issued. The results
contained in this report are only representative of the samples received. Conditions can vary at different
times and at different sampling conditions. Summit Environmental Technologies, Inc. is not responsible
for use or interpretation of the data included herein.
All results for Solid Samples are reported on an "as received" or "wet weight" basis unless indicated as
"dry weight" using the "-dry" designation on the reporting units.
This report is believed to meet all of the requirements of the accrediting agency, where applicable. Any
comments or problems with the analytical events associated with this report are noted below.
Analytical Sequence Sample Notes:
23070031-OOIA F1ashPt_S(1010): Z = Method deviation, due to sample matrix could not stir to 250
RPM as required by the method.
Original
Page 2 of 10

SUMMIEF Summit Environmental 7'echnologies,Inc.
3310 Win St.
ENVIRONMENTAL'FECHNOLOGIFS, INC Cuyahoga Falls, Ohio 44223
Arw$ ytical Laberaforlee TEL: [phone] FAX.- [phone]
Website: http://www.settek.com
CLIENT: Cascades Tissue Group - North Carolina Inc
Project:
Lab SampleID Client Sample ID
23070031-001 Sludge
Tag No Date Collected
6/20/2023 6:10:00 AM
Workorder
Sample Summary
WO#: 23070031
12-Jul-23
Date Received Matrix
6/30/2023 1:05:00 PM Solid
Page 3 of 10

. Summit Environmental
Technologies, Inc.
WO#:
23070031
SummingO
3310 Win St.
Cuyahoga Falls, Ohio 44223
Date Reported:
7/12/2023
A R,Nyt;Caf Laborirrnes TEL: [phone] FAX: [phone]
Company: Cascades
Tissue
Group
- North Carolina I
Website: http / %,%vw.settek.com
Address: a division of Cascades Holding US Inc.
Rockingham
NC 28379
Received: 6/30/2023
Project#:
TCLP Metals
Client ID#
Lab ID# Collected Analyte
Rep Lmt Result Units
Matrix
Method
DF
RegLvl
Run
Analyst
Sludge
001 6/20/2023 TCLP Arsenic(As)
0.100 ND mg/L
Solid
EPA 6010C
1
5.00
7/4/2023
RJE
C
Sludge
001 6/20/2023 TCLP Barium(Ba)
1.00 ND mg/L
Solid
EPA 6010C
1
100
7/4/2023
RJE
C
Sludge
001 6/20/2023 TCLP Cadmium(Cd)
0.100 ND mg/L
Solid
EPA 6010C
1
1.00
7/4/2023
RJE
C
Sludge
001 6/20/2023 TCLP Chromium(Cr)
0.200 ND mg/L
Solid
EPA 6010C
1
5.00
7/4/2023
RJE
C
Sludge
001 6/20/2023 TCLP Lead(Pb)
0.100 ND mg/L
Solid
EPA 6010C
1
5.00
7/4/2023
RJE
C
Sludge
001 6/20/2023 TCLP Selenium(Se)
0.100 ND mg/L
Solid
EPA 6010C
1
1.00
7/4/2023
RJE
C
Sludge
001 6/20/2023 TCLP Silver(Ag)
0.100 ND mg/L
Solid
EPA 6010C
1
5.00
7/4/2023
RJE
C
TCLP Mercury
Client ID#
Lab ID# Collected Analyte
Rep Lmt Result Units
Matrix
Method
DF
RegLvl
Run
Analyst
Sludge
001 6/20/2023 TCLP Mercury
0.00200 ND mg/L
Solid
EPA 7470 A
1
0.200
7/3/2023
JJF
TCLP Pesticides
Client ID#
Lab ID# Collected Analyte
Rep Lmt Result Units
Matrix
Method
DF
RegLvl
Run
Analyst
Sludge
001 6/20/2023 Chlordane, total
0.00250 ND mg/L
Solid
EPA 8081 B
1
0.0300
7/11/2023
PGP
Sludge
001 6/20/2023 Toxaphene
0.00500 ND mg/L
Solid
EPA 8081 B
1
0.500
7/11/2023
PGP
Sludge
001 6/20/2023 Endrin
3.000500 ND mg/L
Solid
EPA 8081 B
1
0.0200
7/11/2023
PGP
Sludge
001 6/20/2023 gamma-BHC
3.000500 ND mg/L
Solid
EPA 8081 B
1
0.400
7/11/2023
PGP
Sludge
001 6/20/2023 Heptachlor
3.000500 ND mg/L
Solid
EPA 8081 B
1
0.00800
7/11/2023
PGP
Sludge
001 6/20/2023 Heptachlor epoxide
3.000500 ND mg/L
Solid
EPA 8081 B
1
0.00800
7/11/2023
PGP
Sludge
001 6/20/2023 Methoxychlor
J.000500 ND mg/L
Solid
EPA 8081 B
1
10.0
7/11/2023
PGP
Page 4 of 10

Summit Environmental Technologies, Inc.
V,/O#:
23070031
�' �.
sum3310
£'8UI1[LJNH1EIdTAL TLCI�'VOLC••GIFS, INr'
Win St.
Cuyahoga Falls, Ohio 44223
Date Repotted:
7/12/2023
4!7.:r+yrrcai '_aborarono-,
TEL: [phone] FAX.- [phone]
Company:
Cascades Tissue Group - North Carolina I
Website: httn:6S5vw.settek.com
Address:
a division of Cascades Holding US Inc.
Rockingham NC 28379
Received:
6/30/2023
Project#:
TCLP Volatiles
Client ID# Lab ID# Collected Analyte Rep Lint Result Units Matrix Method DF RegLvl Run Analyst
Sludge
001
6/20/2023 1,1-Dichloroethene
0.100
ND mg/L
Sludge
001
6/20/2023 1,2-Dichloroethane
0.100
ND mg/L
Sludge
001
6/20/2023 MEK
2.00
ND mg/L
Sludge
001
6/20/2023 Benzene
0.100
ND mg/L
Sludge
001
6/20/2023 Carbon tetrachloride
0.100
ND mg/L
Sludge
001
6/20/2023 Chlorobenzene
1.00
ND mg/L
Sludge
001
6/20/2023 Chloroform
0.100
ND mg/L
Sludge
001
6/20/2023 Tetrachloroethene
0.100
ND mg/L
Sludge
001
6/20/2023 Trichloroethene
0.100
ND mg/L
Sludge
001
6/20/2023 Vinyl chloride
0.0400
ND mg/L
TCLP Semi-Volatiles
Client ID# Lab ID# Collected Analyte Rep Lmt Result Units
Sludge
001
6/20/2023 1,4-Dichlorobenzene
0.0250
ND mg/L
Sludge
001
6/20/2023 2,4,5-Trichlorophenol
0.0250
ND mg/L
Sludge
001
6/20/2023 2,4,6-Trichlorophenol
0.0250
ND mg/L
Sludge
001
6/20/2023 2,4-Dinitrotoluene
0.100
ND mg/L
Sludge
001
6/20/2023 Cresols, Total
0.0500
ND mg/L
Sludge
001
6/20/2023 Hexachloro-1,3-
0.100
ND mg/L
butadiene
Sludge
001
6/20/2023 Hexachlorobenzene
0.100
ND mg/L
Sludge
001
6/20/2023 Hexachloroethane
0.0250
ND mg/L
Sludge
001
6/20/2023 Nitrobenzene
0.0250
ND mg/L
Sludge
001
6/20/2023 Pentachlorophenol
0.0250
ND mg/L
Sludge
001
6/20/2023 Pyridine
0.0250
ND mg/L
TCLP Herbicides
Client ID# Lab ID# Collected Analyte Rep Lint Result Units
Sludge 001 6/20/2023 2,4-D 0.500 ND mg/L
Sludge 001 6/20/2023 2,4,5-TP 0.500 ND mg/L
Solid
EPA 8260 B
20
Solid
EPA 8260 B
20
Solid
EPA 8260 B
20
Solid
EPA 8260 B
20
Solid
EPA 8260 B
20
Solid
EPA 8260 B
20
Solid
EPA 8260 B
20
Solid
EPA 8260 B
20
Solid
EPA 8260 B
20
Solid
EPA 8260 B
20
0.700
7/5/2023
MTG
0.500
7/5/2023
MTG
200
7/5/2023
MTG
0.500
7/5/2023
MTG
0.500
7/5/2023
MTG
100
7/5/2023
MTG
6.00
7/5/2023
MTG
0.700
7/5/2023
MTG
0.500
7/5/2023
MTG
0.200
7/5/2023
MTG
Matrix Method DF RegLvl Run Analyst
Solid
EPA 8270 C 1
Solid
EPA 8270 C 1
Solid
EPA 8270 C 1
Solid
EPA 8270 C 1
Solid
EPA 8270 C 1
Solid
EPA 8270 C 1
Solid
EPA 8270 C 1
Solid
EPA 8270 C 1
Solid
EPA 8270 C 1
Solid
EPA 8270 C 1
Solid
EPA 8270 C 1
7.50
7/7/2023
JAP
400
7/7/2023
JAP
2.00
7/7/2023
JAP
0.130
7/7/2023
JAP
200
7/7/2023
JAP
0.500
7/7/2023
JAP
0.130
7/7/2023
JAP
3.00
7/7/2023
JAP
2.00
7/7/2023
JAP
100
7/7/2023
JAP
5.00
7/7/2023
JAP
Matrix Method DF RegLvl Run Analyst
Solid EPA 8321B 50 10.0 7/3/2023 JDB
Solid EPA 8321B 50 1.00 7/3/2023 JDB
Page 5 of 10

SUMMIT
Summit Environmental Technologies, Inc.
3310 Win St.
Analytical Report
ENVIRONMENTAL TECHN0L0GIE7S, 1NC
Arai yrlcaf Laborarones
Cuyahoga Falls, Ohio 44223
TEL: [phone] FAX.- [phone]
(consolidated)
WO#: 23070031
Website: hMp.-Avmi�seftek.eom
Date Reported: 7/12/2023
CLIENT:
Cascades Tissue Group - North
Carolina Inc Collection Date:
6/20/2023 6:10:00 AM
Project:
Lab ID:
23070031-001
Matrix:
SOLID
Client Sample ID: Sludge
Analyses Result
PQL Qual Units DF
Date Analyzed
RCI
SW1010
Analyst: TAH
FLASHPOINT DETERMINATION (1010)
Flashpoint (140°F) >140
Z °F 1
7/7/2023 4:58:02 PM
NOTES:
Z = Method deviation, due to sample matrix could not stir to
250 RPM as required by the method.
RCI
SW9014
Analyst: HDJ
REACTIVE CYANIDE (9014/7.3.3.2)-SOLID
Cyanide, Reactive ND
0.385 mg/Kg 1
7/4/2023 12:00:00 PM
RCI
SW9045D
Analyst: JPN
PH (SW9045D)
pH 7.1
s.u.@23.4C 1
7/6/2023 3:00:00 PM
RCI
SW9034
Analyst: KG
REACTIVE SULFIDE (9034)/7.3.4.2
Sulfide, Reactive ND
25.0 mg/Kg 1
7/3/2023 9:20:23 AM
Qualifiers: E Value above quantitation range
M Manual Integration used to determine area response
PL Permit Limit
RL Reporting Detection Limit
I I Ito Iding times for preparation or analysis exceeded
ND Not Detected
R RPD outside accepted recovery limits
W Sample container temperature is out of limit as specified at testeode
Original
Page 6 of 10

In
u mm, Summit Environmental Technologies, 3310 Wirt' Qualifiers and Acronyms
,
EN'sr 110td1.15NTAL Tcctf�lota ir5, !NC Cuyahoga Falls, Ohio 442� WO#: 23070031
�uiytk=ai L�b7rutr�,r,i�s TEL: [phone] FAX.- (330) 253-446
Website: http://www.settek.co Date: 7/12/2023
These commonly used Qualifiers and Acronyms may or may not be present in this report
Qualifiers
U The compound was analyzed for but was not detected.
J The reported value is greater than the Method Detection Limit but less than the Reporting Limit.
H The hold time for sample preparation and/or analysis was exceeded.
D The result is reported from a dilution.
E The result exceeded the linear range of the calibration or is estimated due to interference.
MC The result is below the Minimum Compound Limit.
* The result exceeds the Regulatory Limit or Maximum Contamination Limit.
m Manual integration was used to determine the area response.
d Manual integration in which peak was deleted
N The result is presumptive based on a Mass Spectral library search assuming a 1:1 response.
P The second column confirmation exceeded 25% difference.
C The result has been confirmed by GUMS.
X The result was not confirmed when GUMS Analysis was performed.
B/MB+ The analyte was detected in the associated blank.
G The iCB or CCB contained reportable amounts of analyte.
QC-/+ The CCV recovery failed low (-) or high (+).
R/QDR The RPD was outside of accepted recovery limits.
QL-/+ The LCS or LCSD recovery failed low (-) or high (+).
QLR The LCS/LCSD RPD was outside of accepted recovery limits.
QM-/+ The MS or MSD recovery failed low (-) or high (+).
QMR The MS/MSD RPD was outside of accepted recovery limits.
QV-/+ The ICV recovery failed low (-) or high (+).
S The spike result was outside of accepted recovery limits.
Z Deviation; A deviation from the method was performed; Please refer to the Case Narrative for
additional infonnation
Acronyms
ND
Not Detected
RL
Reporting Limit
QC
Quality Control
MDL
Method Detection Limit
MB
Method Blank
LOD
Level of Detection
LCS
Laboratory Control Sample
LOQ
Level of Quantitation
LCSD
Laboratory Control Sample Duplicate
PQL
Practical Quantitation Limit
QCS
Quality Control Sample
CRQL
Contract Required Quantitation Limit
DUP
Duplicate
PL
Permit Limit
MS
Matrix Spike
RegLvl
Regulatory Limit
MSD
Matrix Spike Duplicate
MCL
Maximum Contamination Limit
RPD
Relative Percent Different
MinCL
Minimum Compound Limit
ICV
Initial Calibration Verification
RA
Reanalysis
ICB
Initial Calibration Blank
RE
Reextraction
CCV
Continuing Calibration Verification
TIC
Tentatively Identified Compound
CCB
Continuing Calibration Blank
RT
Retention Time
RLC
Reporting Limit Check
CF
Calibration Factor
DF
Dilution Factor
RF
Response Factor
This list of Qualifiers and Acronyms reflects the most commonly utilized Qualifiers and Acronyms for reporting.
Please refer to the Analytical Notes in the Case Narrative for any Qualifiers or Acronyms that do not appear in this
list or for additional information regarding the use of these Qualifiers on reported data.
Original
Page 7 of 10

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Page 8 of 10

U M M I Summit Environmental Technologies, Inc.
Ezzraor--i S 3310 Win St.
';'dll'_tdpdEpiTOL"�C}:'dOl.?A-s ,.. Cuyahoga Falls, Ohio44223 Sample Receipt Checklist
rg fon7c - TEL: [phone] FAX: [phone]
Website: httn:llwwwseftek"m
Client Name CAS-NC-28379 Work Order Number 23070031
RcptNo: 1 Date and Time Received 6/30/2023 1:05:00 PM Received by: Anthony W. Britton
Completed by Reviewed by:
Completed Date: 7/1/2023 1:02:49 PM Reviewed Date: 7/10/2023 9:40:55 AM
Carrier name: Summit
Chain of custody present?
Chain of custody signed when relinquished and received?
Chain of custody agrees with sample labels?
Are matrices correctly identified on Chain of custody?
Is it clear what analyses were requested?
Custody seals intact on sample bottles?
Samples in proper container/bottle?
Were correct preservatives used and noted?
Sample containers intact?
Sufficient sample volume for indicated test?
Were container Tables complete (ID, Pres, Date)?
All samples received within holding time?
Was an attempt made to cool the samples?
All samples received at a temp. of > 0° C to 6.0° C?
Response when temperature is outside of range:
Preservative added to bottles:
Sample Temp. taken and recorded upon receipt?
Water - Were bubbles absent in VOC vials?
Water- Was there Chlorine Present?
Water- pH acceptable upon receipt?
Are Samples considered acceptable?
Custody Seals present?
Traffic Report or Packing Lists present?
Airbill or Sticker?
Airbill No:
Sample Tags Present?
Sample Tags Listed on COC?
Tag Numbers:
Sample Condition?
Case Number: SDG:
Yes
d
No
Yes
✓
No
Yes
✓
No
Not Present
_
Yes
✓
No
Yes
No
Yes
No
Not Present
✓
Yes
V
No
Yes
No
NA
Yes
No
Yes
No
Yes
►i
No
Yes
No
Yes
No
NA
Yes
N
No
NA
Yes
No
1.8 To 1.8
°C
Yes
No
No Vials
✓
Yes
No
NA
Yes
No
NA
Yes
No
Yes
No
Yes
No
Air Bill
Sticker
Not Present
Yes
No
Yes
No
Intact Broken
SAS:
Adjusted?
Any No and/or NA (not applicable) response must be detailed in the comments section be
Leaking
Checked by
Page 9 of 10

�'� Summit Environmental Technologies, Inc.
3310 Win St.
0jENVIRONMENTAL TECHNOLOGIES, INC Cuyahoga Falls, Ohio44223 Sample Receipt Checklist
rin aly0cal L.aboraiorles TEL: [phone] FAX: [phone]
Website: htt :Ilwww.settek.com
Client Contacted? Yes No NA Person Contacted:
Contact Mode: _; Phone: Fax: Email:
Client Instructions:
Date Contacted: Contacted By:
Regarding:
CorrectiveAction:
In Person:
Comments:
Page 10 of 10

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Cascades Tissue Group -North Carolina,a division of
Facility Name: Cascades HoldingUS Inc.
WQ Permit Number:
WWTP Name: NPDES Number:
Monitoring Period: From 1/l/2023 To 12/31/2023
WQ0009477
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A: I Alt. A (time/temp) ❑
1 Alt B (Alk Treatment)❑
TAIt. C (Prior Testing)❑
A1t.D (No Prior Test) ❑
I Process to Further Reduce Pathogengs ❑
If applicable to alternative pet -formed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost ❑
Heat Drying ❑
Heat Treatment ❑ Thermo hilic ❑
Beta Ray ❑
Gamma Ray ❑
Pasteurization ❑
Class B:
JAIt. (1) Fecal Density ❑
AIt. (2) Process to Significantly Reduce Pathogens ❑
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization ❑
Air Drying ❑
Composting ❑
Aerobic Digestion ❑
Anaerobic Digestion ❑
If applicable to alternative performed (Class A or Class B) complete the following
monitoring data:
Parameter
Allowable Level
in Sludge
Pathogen Density
Number o
Excee-
dences
Frequency
of Analysis
Sample
Type
Analytical
Tech -
nique
Minimum
Geo. Mean
Maximurr
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
NA
NA
CFU
NA
NA
1000 mpn per gram
of total solid (dry
weight)
NA
NA
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per 4 grams
total solid (dry
weight)
NA
NA
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed:
Alt.1 (VS reduction) ❑
Alt. 2 (40-day bench) ❑
Alt. 3 (30-day bench) ❑
Alt. 4 (Spec. O, uptake) ❑
Alt. 5 (14-Day Aerobic) ❑
Alt. 6 (Alk. Stabilization ❑
Alt 7 (Drying - Stable) ❑
1 Alt. 8 (Drying - Unstable) ❑
Alt. 9 (Injection) ❑
Alt. 10 (Incorporation) ❑
No vector attraction reduction alternatives were performed ❑
CERTIFICATION STATEMENT (please check the appropriate statement)
❑/ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note
lykif you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance ■vith the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Brandt Steele Advanced Residuals President
Preparer Name and Title (type or print)
Signature of Pr er* Date
Bill Young Project Manager
Land A pI.er Name and T' if applicable)(type or print)
Signature of L Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 02T (12/2006)

(%L
Cascades
Date: Feb 1, 2024
From: Brandt Steele
Cascades Tissue Group - North Carolina
A Division of Cascades Holding US Inc.
805 Midway Road, Post Office Box 578
Rockingham, NC 28380 USA
Phone: [phone] Fax: [phone]
Cascades Tissue Group -North Carolina, a division of Cascades Holding US Inc.
Po Box 578 805 Midway Rd.
Rockingham, NC 28380
Phone [phone]-Ext 74280
Fax [phone]
Email: Michael Hurst __Cascades.corn
Permit: WQ0009477
Subject: Fecal Testing
Cascades Material is a lime material, so we don't perform vector reduction.
Should your office have any question please contact me at the above numbers or email.
Brandt Steele
ORC
Cascades Tissue Group -North Carolina, a division of Cascades Holding US Inc.