WQ0011244_2023 Residual Annual Report_20240228 (2)

Initial Review
Reviewer
nathaniel.thorn burg
Is this submittal an application? (Excluding additional information.) *
Yes No
If not an application what is the submittal type?* Annual Report
Residual Annual Report
Additional Information
Other
Annual Report Year* 2023
Permit Number (IR) * WQ0011244
Applicant/Permittee City of Oxford
Email Notifications
Does this need review by the hydrogeologist? * Yes No
Regional Office Raleigh
CO Reviewer
Admin Reviewer Wanda Gerald

Submittal Form
Project Contact Information
Please provide information on the person to be contacted by NDB Staff regarding electronic submittal, confirmation of receipt, and other correspondence.
Name* Lysa Finnerty
Email Address*
[e-mail]
Project Information
.........................
Application/Document Type*
New (Fee Required)
Modification - Major (Fee Required)
Renewal with Major Modification (Fee
Required)
Annual Report
Additional Information
Other
Phone Number*
4105376150
Modification - Minor
Renewal
GW-59, NDMR, NDMLR, NDAR-1,
N DAR-2
Residual Annual Report
Change of Ownership
We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form.
https://edoes.deq.nc.gov/Forms/NonDischarge_Monitoring_Report
Permit Type:*
Wastewater Irrigation
High -Rate Infiltration
Other Wastewater
Reclaimed Water
Closed -Loop Recycle
Residuals
Single -Family Residence Wastewater
Other
Irrigation
Permit Number:*
WQ0011244
Has Current Existing permit number
Applicant/Permittee Address*
435 Williams Court, Ste 100, Baltimore, MD 21220
Facility Name*
City of Oxford Class B Residuals Program
Please provide comments/notes on your current submittal below.
Submission of the 2023 Annual Report for City of Oxford, NC
At this time, paper copies are no longer required. If you have any questions about what is required, please contact Nathaniel Thornburg
at [e-mail].
Please attach all information required or requested for this submittal to be reviewed here.
(Application Form, Engineering Plans, Specifications, Calculations, Etc.)
Oxford NC 2023 Annual Report FINAL.pdf 18.55MB
Upload only 1 PDF document (less than 250 MB). Multiple documents must be combined into one PDF file unless file is larger
than upload limit.
* By checking this box, I acknowledge that I understand the application will not be accepted for pre -review until the fee (if required) has
been received by the Non -Discharge Branch. Application fees must be submitted by check or money order and made payable to the
North Carolina Department of Environmental Quality (NCDEQ). I also confirm that the uploaded document is a single PDF with all parts
of the application in correct order (as specified by the application).
Mail payment to:
NCDEQ — Division of Water Resources
Attn: Non -Discharge Branch
1617 Mail Service Center
Raleigh, NC 27699-1617
Signature
Alva �Cit'wt%tl�
Submission Date 2/28/2024

435 Williams Court, Suite 100
Baltimore, MD 21220
www.synagro.com
FEBRUARY 28, 2024
NCDEQ
Division of Water Resources
Information Processing Unit
1617 Mail Service Center
Raleigh, NC 27699-1617
Re: 2023 Annual Report for Permit No. WQ0011244
Dear NCDEQ:
SYNAGRO
Synagro is submitting one electronic copy of the above referenced report on behalf of the City
of Oxford, NC.
If you have any questions or need additional information, please do not hesitate to contact Amy
Ratliff at [phone] or Adam Brigman at [phone].
Sincerely,
WIN w-VEL&P-M.Alm
Derrick Shivar
Environmental Compliance Manager
Enclosures
cc: Amy Ratliff, City of Oxford
YOUR PARTNER FORA CLEANER, GREENERWORLD

CITY OF OXFORD, NC
RESIDUALS LAND APPLICATION PROGRAM
Permit No. WQ0011244
2023 ANNUAL REPORT

City of Oxford, NC
Residuals Land Application Program
2023 Annual Report
TABLE OF CONTENTS
1. Certification Form and Annual Operations Summary
2. Annual Residual Sampling Summary Forms and Residuals
Analyses
3. Annual Land Application Field Summary Forms
4. TCLP Analysis
5. Pathogen ReductionNector Attraction Reduction
6. Soil pH & Lime Application Records
7. Soil Analyses

SECTION 1

ANNUAL LAND APPLICATION CERTIFICATION FORM
WQ Permit #: W00011244 County Granville Year 2023
Facility Name (as shown on permit) City of Oxford WWTP NPDES No. NCO025054
Land Application Operator Synasro Phone# [phone]
Land application of residuals as allowed by the above permit occurred during the past calendar year?
X YES NO. If NO, skip Part A, and Part B and proceed to Part C. Also, if residuals were generated but not land applied,
please attach an explanation on how the residuals were handled.
Part A — Residuals Application Summary:
Total number of application fields in the permit: 21
Total number of fields utilized for land application during the year: 6
Total amount of dry tons applied during the year for all application sites: 456.81
Total number of acres utilized for land application during the year: 164.30
Part B — Annual Compliance Statement:
Facility was compliant during calendar year 2023 with all conditions of the land application permit (including but not limited to items
1-13 below) issued by the Division of Water QualityX YES NO.
If no, please provide a written description why the facility was not compliant, the dates, and explain corrective action taken.
l . Only residuals approved for this permit were applied to the permitted sites.
2. Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or the
limit specified in the permit.
3. Annual soils analysis was performed on each site receiving residuals during the past calendar year and three (3) copies of
laboratory results are attached.
4. Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5. All other monitoring was performed in accordance with the permit and reported during the year as required and three (3)
copies of certified laboratory results are attached.
6. The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T . 1105(a) or the Pollutant Loading
Rates in 15A NCAC 02T .I 105(b) (Applicable to 40 CFR Part 503 regulated facilities).
7. All general requirements as specified in the Land Application Permit were complied with (applicable to 40 CFR Part 503
regulated facilities).
8. All monitoring and reporting requirements in 15A NCAC 02T .1111 were complied with (applicable to 40 CFR Part 503
regulated facilities).
9. All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Quality.
10. No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
11. Vegetative cover was maintained and proper crop management was performed on each site receiving residuals, as specified
in the permit.
12. No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13. All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C — Certification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate, and complete. 1
am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for
knowing violations."
Amy Ratlifff, City Engineer
Permitt me and Tit (type or print)
2/28/2024
ignature of Preparer* Date
(if different from Permittee)
J I ?tvwd 2/28/2024
gnature of Permitte Date
2/l /2024
Sign PMd AWIier Date
(if different fro Permittee anPreparer)
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 02T .1102 (26) DENR FORM ACF (12/2006)

OPERATIONS SUMMARY - LAND APPLICATION - NORTH CAROLINA
ALL COUNTIES - ALL SITES
DATE RANGE: 1/1/2023 - 12/31/2023
OXFORD,NC
OXFORD, NC AEROB. DIGESTED LIQUID
MONTH/YEAR
AMOUNT
UNIT
DRY TONS
UNIT
DRY METRIC TONS
May 2023
576,600.00
G
106.52
D
96.61
July 2023
483,600.00
G
58.89
D
53.41
August 2023
378,200.00
G
46.05
D
41.77
October 2023
2,015,000.00
G
245.35
D
222.54
TOTAL
Units Key: D - Dry Tons; G — Gallons; W — Wet Tons; Y — Cubic Yards
Report Date: 1/23/2024 8:40:24 PM
3,453,400.00 G 456.81 D 414.32

SECTION 2

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B
WQ Permit Number: WQ0011244 Laboratory:
Facility Name: OXFORD, NC Waypoint Analytical Virginia Inc.
Residual Source WQ # or
NPDES#: NCO025054
WWTP Name: OXFORD
Residual Analysis Data
Product Type
Sample or Composite Date
AEDLIQ
03/13/23
AEDLIQ
05/03/23
AEDLIQ
08/02/23
AEDLIQ
10/12/23
AEDLIQ
12/06/23
Parameter (mg/kg dry weight)
Ceiling Conc.
Limit
Percent Solids (%)
NA
3.04
4.43
2.92
3.49
1.59
Arsenic
75
<16.7
<2.89
<17.2
<14.3
<5.34
Cadmium
85
<3.33
<0.578
<3.45
<2.86
<3.13
Copper
4300
527
173
607
546
550
Chromium
NA
28.6
7.63
50.7
36.6
30.5
Lead
840
28.8
8.5
39.3
26.1
31.4
Mercury
57
<6.37
<1.01
<5.97
<4.8
<1.41
Molybdenum
75
8.53
2.39
11.8
11.2
9.75
Nickel
420
12.3
3.14
22.5
16.3
15.3
Selenium
100
<16.7
<2.89
<17.2
<14.3
<6.44
Zinc
7500
2100
665
2240
1880
1980
Total Phosphorus
NA
21200
6300
22600
21000
22700
TKN
NA
59300
19100
63800
197000
36600
Ammonia -Nitrogen
NA
7230
896
17400
8060
<6250
Nitrate and Nitrite
NA
<167
29.2
<172
<143
565
For surface disposal facilities the ceiling concentration limits listed in this form are not applicable. Reference the individual permit for metals limits.
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified
personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the
possibility ones and impriso!ynent for knowing violations."
2/28/2024
44nature of Preparer* Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15 A NCAC 2T.1102(26) DENR FORM RSSF (12/2006)
Printed: 1 /24/2024 5:53:15 PM For: 2049 01

ANNUAL RESIDUAL SAMPLING SUMMARY FORM - B
Report all sampling analysis results for parameters not listed in FORM RSSF that are part of the WQ permit or were analyzed for over the past
calendar year. Use additional forms as needed.
WO Permit Number:
W00011244 Laboratory:
Facility Name:
OXFORD, NC Waypoint Analytical Virginia Inc.
Residual Source
NPDES # or WQ#:
NCO025054
WWTP Name:
OXFORD
Residual Analysis Data
Product Type
AEDLIQ
AEDLIQ
AEDLIQ
AEDLIQ
AEDLIQ
Sample or Composite Date
03/13/23
05/03/23
08/02/23
10/12/23
12/06/23
Parameters (mg/kg dry weight)
Aluminium
38000
11600
47600
42000
42300
Calcium
16800
4990
18900
17000
18200
Magnesium
3430
925
4140
4140
4410
pH (s.u.)
6.70
7.10
7.00
9.00
7.50
Potassium
3200
734
3480
3000
3430
Sodium
2010
380
2560
1940
3850
PAN
19412
5931
22786
60813
14679
SAR (Ratio)
0.6422
0.5378
0.7489
0.6446
0.8352
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordiance with a system designed to assure that qualified
personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the
possiz0f
imprison nt for knowing violations."
2/28/2024
ature Preparer " Date
Treparer is defined in 40 CFR Part 503.9(r) and 15 A NCAC 2T.1102(26)
Printed: 1/24/2024 5:58:04 PM For: 2049 01 DENR FORM RSSF-B (1212006)

Waypointo
ANALYTICAL
3/22/2023
Synagro Central LLC/ Oxford
Mary Brewer
284 Boger Road
Mocksville, NC, 27028
Ref: Analytical Testing
Report Number: 23-073-0002
Project Description: Oxford WWTP
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
www.waypointanalytical.com
Dear Mary Brewer:
Waypoint Analytical Virginia, Inc. received sample(s) on 3/14/2023 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information
Sincerely,
&;'-� ­AldA�
Brandi Watson
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 1 of 7

•
7621 Whitepine Road, Richmond, VA 23237
Waypoint
Main 804-743-9401 0 Fax [phone]
ANALYTICAL www.waypointanalytical.com
Sample Summary Table
Report Number: 23-073-0002
Client Project Description: Oxford WWTP
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
61367
Lagoon
Solids
03/13/2023
11:15
03/14/2023
61367
Lagoon
Solids
03/13/2023
11:15
03/14/2023
61367
Lagoon
Solids
03/13/2023
11:15
03/14/2023
61367
Lagoon
Solids
03/13/2023
11:15
03/14/2023
61367
Lagoon
Solids
03/13/2023
11:15
03/14/2023
61367
Lagoon
Solids
03/13/2023
11:15
03/14/2023
61367
Lagoon
Solids
03/13/2023
11:15
03/14/2023
61367
Lagoon
Solids
03/13/2023
11:15
03/14/2023
SM-4500-NH3C
WP MTN
9045D
WP MTN
4500NO3F-2011
WP MTN
6010D
WP MTN
SW-7471B
WP MTN
SM-4500-NH3C-TKN
WP MTN
SM-2540G
WP MTN
WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN
Page 2 of 7

WayP
�' 7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 Fax [phone]
ANALYTICAL www.waypointanalytical.com
46478
Synagro Central LLC/ Oxford Project Oxford WWTP
Mary Brewer Report Date : 03/22/2023
284 Boger Road Information : Received : 03/14/2023
Mocksville , NC 27028
Brandi Watson
Report Number : 23-073-0002 REPORT OFANALYSIS
Lab No : 61367 Matrix: Solids
Sample ID : Lagoon Sampled: 3/13/2023 11:15
Test Results Units MQL DF Date / Time By Analytical
Analyzed Method
Moisture
97.0
%
0.010
1
03/19/2317:47
CJD
SM-2540G
Sulfur
7670
mg/Kg -
dry
333
1
03/18/23 08:46
BKN
6010D
Calcium
16800
mg/Kg -
dry
1670
1
03/20/23 19:22
JTR
6010D
Aluminum
38000
mg/Kg -
dry
167
1
03/18/23 08:46
BKN
6010D
Manganese
540
mg/Kg -
dry
16.7
1
03/18/23 08:46
BKN
6010D
Organic N
52100
mg/Kg -
dry
8333
1
03/21/23 11:00
CALCULATION
Nickel
12.3
mg/Kg -
dry
8.33
1
03/18/23 08:46
BKN
6010D
Lead
28.8
mg/Kg -
dry
10.0
1
03/18/23 08:46
BKN
6010D
Arsenic
<16.7
mg/Kg -
dry
16.7
1
03/18/23 08:46
BKN
6010D
Selenium
<16.7
mg/Kg -
dry
16.7
1
03/18/23 08:46
BKN
6010D
Test
Results
Units
MQL
DF
Date / Time
By
Analytical
Analyzed
Method
Total Solids
3.04
%
0.010
1
03/19/23 17:47
CJD
SM-2540G
Phosphorus
21200
mg/Kg -
dry
167
1
03/18/23 08:46
BKN
6010D
Copper
527
mg/Kg -
dry
16.7
1
03/18/23 08:46
BKN
6010D
Total Kjeldahl Nitrogen
Qualifiers/ DF Dilution Factor
Definitions
59300 mg/Kg - dry 8330 1 03/21/23 11:00 JPJ ;M-4500-NH3C-TKI`
MQL Method Quantitation Limit
Page 3 of 7

WayPANALYTICAL
46478
Synagro Central LLC/ Oxford Project
Mary Brewer
284 Boger Road Information
Mocksville , NC 27028
Report Number : 23-073-0002
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
www.waypointanalytical.com
Oxford WWTP
REPORT OFANALYSIS
Report Date : 03/22/2023
Received : 03/14/2023
Brandi Watson
Lab No : 61367
Sample ID : Lagoon
Matrix: Solids
Sampled: 3/13/2023 11:15
Potassium
3200
mg/Kg -
dry
333
1
03/20/23 19:22
JTR
6010D
Magnesium
3430
mg/Kg -
dry
167
1
03/18/23 08:46
BKN
6010D
Sodium
2010
mg/Kg -
dry
833
1
03/18/23 08:46
BKN
6010D
Iron
14900
mg/Kg -
dry
333
1
03/20/23 19:22
JTR
6010D
Zinc
2100
mg/Kg -
dry
41.7
1
03/20/23 19:22
JTR
6010D
Ammonia Nitrogen
7230
mg/Kg -
dry
3330
1
03/21/23 15:20
JPJ
SM-4500-NH3C
Nitrate+Nitrite-N
<167
mg/Kg -
dry
167
1
03/21/23 15:09
ZBD
4500NO3F-2011
Cadmium
<3.33
mg/Kg -
dry
3.33
1
03/18/23 08:46
BKN
6010D
Chromium
28.6
mg/Kg -
dry
8.33
1
03/18/23 08:46
BKN
6010D
Mercury
<6.37
mg/Kg -
dry
6.37
1
03/20/23 14:32
FDS
SW-7471B
pH
6.7
S.U.
1
03/17/2316:25
SAR
9045D
Molybdenum
8.53
mg/Kg -
dry
8.33
1
03/18/23 08:46
BKN
6010D
Qualifiers/ DF Dilution Factor
Definitions
MQL Method Quantitation Limit
Page 4 of 7

Waypointo
ANALYTICAL
Client: Synagro Central LLC/ Oxford
Project: Oxford WWTP
Lab Report Number: 23-073-0002
Date: 3/22/2023
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
www.waypointanalytical.com
CASE NARRATIVE
Metals Analysis Method 601 OD
Sample 81088 (UOSA Pellet 1 M 23-2)
Analyte: Aluminum
QC Batch No: 1-671023/1-670068
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 81088 (UOSA Pellet 1 M 23-2)
Analyte: Calcium
QC Batch No: 1-671023/1-670068
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 81088 (UOSA Pellet 1 M 23-2)
Analyte: Iron
QC Batch No: 1-671023/1-670068
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 81088 (UOSA Pellet 1 M 23-2)
Analyte: Potassium
QC Batch No: 1-671023/1-670068
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Sample 81088 (UOSA Pellet 1 M 23-2)
Analyte: Phosphorus
QC Batch No: 1-671023/1-670068
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Page 5 of 7

WayPAoInt..
NALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
www.waypointanalytical.com
Shipment Receipt Form
Customer Number: 46478
Customer Name: Synagro Central LLC/ Oxford
Report Number: 23-073-0002
Shipping Method
0 Fed Ex 0 US Postal 0 Lab
0 UPS 0 Client 0 Courier
0 Other:
Thermometer ID:
Shipping container/cooler uncompromised?
* Yes
0 No
Number of coolers/boxes received
Custody seals intact on shipping container/cooler?
0 Yes
0 No
Not Present
Custody seals intact on sample bottles?
0 Yes
0 No
Not Present
Chain of Custody (COC) present?
# Yes
0 No
COC agrees with sample label(s)?
# Yes
0 No
COC properly completed
# Yes
0 No
Samples in proper containers?
# Yes
0 No
Sample containers intact?
# Yes
0 No
Sufficient sample volume for indicated test(s)?
# Yes
0 No
All samples received within holding time?
# Yes
0 No
Cooler temperature in compliance?
# Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
# Yes
0 No
Water - Sample containers properly preserved
Yes
0 No
0 N/A
Water - VOA vials free of headspace
0 Yes
0 No
N/A
Trip Blanks received with VOAs
0 Yes
0 No
N/A
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
0 N/A
F_ High concentration container (48 hr)
F_ High concentration pre -weighed (methanol -14 d)
F_ Low concentration EnCore samplers (48 hr)
F_ Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included? 0 Yes * No
Comments:
Signature: IDavid Lennon Date & Time: 03/14/2023 09:19:31
Page 6 of 7

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Page 7 of 7

Waypointo
ANALYTICAL
5/15/2023
Synagro Central LLC/ Oxford
Mary Brewer
284 Boger Road
Mocksville, NC, 27028
Ref: Analytical Testing
Report Number: 23-124-0015
Project Description: Oxford WWTP
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
www.waypointanalytical.com
Dear Mary Brewer:
Waypoint Analytical Virginia, Inc. received sample(s) on 5/4/2023 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information
Sincerely,
&;'-� ­AldA�
Brandi Watson
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 1 of 6

•
7621 Whitepine Road, Richmond, VA 23237
Waypoint
Main 804-743-9401 0 Fax [phone]
ANALYTICAL www.waypointanalytical.com
Sample Summary Table
Report Number: 23-124-0015
Client Project Description: Oxford WWTP
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
61940
Oxford WWTP
Solids
05/03/2023 08:20
05/04/2023
61940
Oxford WWTP
Solids
05/03/2023 08:20
05/04/2023
61940
Oxford WWTP
Solids
05/03/2023 08:20
05/04/2023
61940
Oxford WWTP
Solids
05/03/2023 08:20
05/04/2023
61940
Oxford WWTP
Solids
05/03/2023 08:20
05/04/2023
61940
Oxford WWTP
Solids
05/03/2023 08:20
05/04/2023
61940
Oxford WWTP
Solids
05/03/2023 08:20
05/04/2023
61940
Oxford WWTP
Solids
05/03/2023 08:20
05/04/2023
SM-4500-NH3C
WP MTN
9045D
WP MTN
4500NO3F-2011
WP MTN
6010D
WP MTN
SW-7471B
WP MTN
SM-4500-NH3C-TKN
WP MTN
SM-2540G
WP MTN
WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN
Page 2 of 6

WayPANALYTICAL
46478
Synagro Central LLC/ Oxford Project
Mary Brewer
284 Boger Road Information
Mocksville , NC 27028
Report Number : 23-124-0015
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
www.waypointanalytical.com
Oxford WWTP Original Report Date : 05/15/2023
Revised Report Date: 05/18/2023
Received : 05/04/2023
REPORT OFANALYSIS
Lab No : 61940
Sample ID : Oxford WWTP
Matrix: Solids
Sampled: 5/3/2023 8:20
Test
Results
Units
MQL
DF
Date / Time
By
Analytical
Analyzed
Method
Total Solids
4.43
%
0.010
1
05/17/23 16:45
JLS
SM-2540G
Total Kjeldahl Nitrogen
19100
mg/Kg -
dry
1450
1
05/08/23 10:30
JPJ ;M-4500-NH3C-TKI`
Phosphorus
6300
mg/Kg -
dry
28.9
1
05/09/23 22:14
BKN
6010D
Potassium
734
mg/Kg -
dry
57.8
1
05/09/23 22:14
BKN
6010D
Sulfur
2450
mg/Kg -
dry
57.8
1
05/09/23 22:14
BKN
6010D
Calcium
4990
mg/Kg -
dry
289
1
05/09/23 22:14
BKN
6010D
Magnesium
925
mg/Kg -
dry
28.9
1
05/09/23 22:14
BKN
6010D
Sodium
380
mg/Kg -
dry
145
1
05/09/23 22:14
BKN
6010D
Iron
4540
mg/Kg -
dry
57.8
1
05/09/23 22:14
BKN
6010D
Manganese
170
mg/Kg -
dry
2.89
1
05/09/23 22:14
BKN
6010D
Copper
173
mg/Kg -
dry
2.89
1
05/09/23 22:14
BKN
6010D
Zinc
665
mg/Kg -
dry
7.23
1
05/09/23 22:14
BKN
6010D
Organic N
18180
mg/Kg -
dry
1445
1
05/08/23 10:30
DH
CALCULATION
Nitrate +N itrite-N
29.2
mg/Kg -
dry
28.9
1
05/08/23 15:16
ZBD
4500NO3F-2011
Nickel
3.14
mg/Kg -
dry
1.45
1
05/09/23 22:14
BKN
6010D
Mercury
<1.01
mg/Kg -
dry
1.01
1
05/08/23 13:28
FDS
SW-7471B
Selenium
<2.89
mg/Kg -
dry
2.89
1
05/09/23 22:14
BKN
6010D
pH
7.1
S.U.
1
05/10/2316:30
CNB
9045D
Qualifiers/ DF Dilution Factor MQL Method Quantitation Limit
Definitions
Page 3 of 6

WayP
�' 7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 Fax [phone]
ANALYTICAL www.waypointanalytical.com
46478
Synagro Central LLC/ Oxford Project Oxford WWTP Original Report Date : 05/15/2023
Mary Brewer Revised Report Date: 05/18/2023
284 Boger Road Information : Received : 05/04/2023
Mocksville , NC 27028
Report Number : 23-124-0015 REPORT OFANALYSIS
Lab No : 61940 Matrix: Solids
Sample ID : Oxford WWTP Sampled: 5/3/2023 8:20
Test Results Units MQL DF Date / Time By Analytical
Analyzed Method
Ammonia Nitrogen
Aluminum
Arsenic
Cadmium
Chromium
Lead
Molybdenum
Analytical Method: SM-2540G
Test
896
mg/Kg
- dry
578
11600
mg/Kg
- dry
28.9
<2.89
mg/Kg
- dry
2.89
<0.578
mg/Kg
- dry
0.578
7.63
mg/Kg
- dry
1.45
8.50
mg/Kg
- dry
1.73
2.39
mg/Kg
- dry
1.45
Results Units MQL
1 05/09/2311:00
CLP
SM-4500-NH3C
1 05/09/23 22:14
BKN
6010D
1 05/09/23 22:14
BKN
6010D
1 05/09/23 22:14
BKN
6010D
1 05/09/23 22:14
BKN
6010D
1 05/09/23 22:14
BKN
6010D
1 05/09/23 22:14
BKN
6010D
DF Date / Time By Analytical
Analyzed Batch
Moisture 82.7 % 0.010 1 05/10/2316:25 JLS L681249
Qualifiers/ DF Dilution Factor
Definitions
MQL Method Quantitation Limit
Page 4 of 6

WayPAoInt..
NALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
www.waypointanalytical.com
Shipment Receipt Form
Customer Number: 46478
Customer Name: Synagro Central LLC/ Oxford
Report Number: 23-124-0015
Shipping Method
0 Fed Ex 0 US Postal 0 Lab
0 UPS 0 Client 0 Courier
0 Other:
Thermometer ID:
Shipping container/cooler uncompromised?
* Yes
0 No
Number of coolers/boxes received
Custody seals intact on shipping container/cooler?
0 Yes
0 No
Not Present
Custody seals intact on sample bottles?
0 Yes
0 No
Not Present
Chain of Custody (COC) present?
# Yes
0 No
COC agrees with sample label(s)?
# Yes
0 No
COC properly completed
# Yes
0 No
Samples in proper containers?
# Yes
0 No
Sample containers intact?
# Yes
0 No
Sufficient sample volume for indicated test(s)?
# Yes
0 No
All samples received within holding time?
# Yes
0 No
Cooler temperature in compliance?
# Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
# Yes
0 No
Water - Sample containers properly preserved
Yes
0 No
0 N/A
Water - VOA vials free of headspace
0 Yes
0 No
N/A
Trip Blanks received with VOAs
0 Yes
0 No
N/A
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
0 N/A
F_ High concentration container (48 hr)
F_ High concentration pre -weighed (methanol -14 d)
F_ Low concentration EnCore samplers (48 hr)
F_ Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included? 0 Yes * No
Comments:
Signature: IDavid Lennon Date & Time: 05/04/2023 13:12:55
Page 5 of 6

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Waypointo
ANALYTICAL
8/18/2023
Synagro Central LLC/ Oxford
Mary Brewer
284 Boger Road
Mocksville, NC, 27028
Ref: Analytical Testing
Report Number: 23-215-0009
Project Description: Oxford
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
www.waypointanalytical.com
Dear Mary Brewer:
Waypoint Analytical Virginia, Inc. received sample(s) on 8/3/2023 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information
Sincerely,
&;'-� ­AldA�
Brandi Watson
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 1 of 7

•
7621 Whitepine Road, Richmond, VA 23237
Waypoint
Main 804-743-9401 0 Fax [phone]
ANALYTICAL www.waypointanalytical.com
Sample Summary Table
Report Number: 23-215-0009
Client Project Description: Oxford
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
63010
Lagoon
Solids
08/02/2023
11:42
08/03/2023
63010
Lagoon
Solids
08/02/2023
11:42
08/03/2023
63010
Lagoon
Solids
08/02/2023
11:42
08/03/2023
63010
Lagoon
Solids
08/02/2023
11:42
08/03/2023
63010
Lagoon
Solids
08/02/2023
11:42
08/03/2023
63010
Lagoon
Solids
08/02/2023
11:42
08/03/2023
63010
Lagoon
Solids
08/02/2023
11:42
08/03/2023
63010
Lagoon
Solids
08/02/2023
11:42
08/03/2023
SM-4500-NH3C
WP MTN
9045D
WP MTN
4500NO3F-2016
WP MTN
6010D
WP MTN
SW-7471B
WP MTN
SM-4500-NH3C-TKN
WP MTN
SM-2540G
WP MTN
WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN
Page 2 of 7

WayPANALYTICAL
46478
Synagro Central LLC/ Oxford Project Oxford
Mary Brewer
284 Boger Road Information
Mocksville , NC 27028
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
www.waypointanalytical.com
Report Date : 08/18/2023
Received : 08/03/2023
Brandi Watson
Report Number : 23-215-0009 REPORT OFANALYSIS
Lab No : 63010 Matrix: Solids
Sample ID : Lagoon Sampled: 8/2/2023 11:42
Test Results Units MQL DF Date / Time By Analytical
Analyzed Method
Moisture
97.1
%
0.010
1
08/08/2316:25
CJR
SM-2540G
Sulfur
11000
mg/Kg -
dry
345
1
08/08/23 21:47
TJS
6010D
Calcium
18900
mg/Kg -
dry
1720
1
08/08/23 21:47
TJS
6010D
Aluminum
47600
mg/Kg -
dry
172
1
08/08/23 21:47
TJS
6010D
Manganese
614
mg/Kg -
dry
17.2
1
08/08/23 21:47
TJS
6010D
Organic N
46380
mg/Kg -
dry
8621
1
08/15/23 10:00
CALCULATION
Nickel
22.5
mg/Kg -
dry
8.62
1
08/08/23 21:47
TJS
6010D
Lead
39.3
mg/Kg -
dry
10.3
1
08/08/23 21:47
TJS
6010D
Arsenic
<17.2
mg/Kg -
dry
17.2
1
08/08/23 21:47
TJS
6010D
Selenium
<17.2
mg/Kg -
dry
17.2
1
08/08/23 21:47
TJS
6010D
Test
Results
Units
MQL
DF
Date / Time
By
Analytical
Analyzed
Method
Total Solids
2.92
%
0.010
1
08/08/23 16:25
CJR
SM-2540G
Phosphorus
22600
mg/Kg -
dry
172
1
08/08/23 21:47
TJS
6010D
Copper
607
mg/Kg -
dry
17.2
1
08/08/23 21:47
TJS
6010D
Total Kjeldahl Nitrogen
Qualifiers/ DF Dilution Factor
Definitions
63800 mg/Kg - dry 8620 1 08/15/23 10:00 JPJ ;M-4500-NH3C-TKI`
MQL Method Quantitation Limit
Page 3 of 7

WayPANALYTICAL
46478
Synagro Central LLC/ Oxford Project Oxford
Mary Brewer
284 Boger Road Information
Mocksville , NC 27028
Report Number : 23-215-0009
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
www.waypointanalytical.com
REPORT OFANALYSIS
Report Date : 08/18/2023
Received : 08/03/2023
Brandi Watson
Lab No : 63010
Sample ID : Lagoon
Matrix: Solids
Sampled: 8/2/2023 11:42
Potassium
3480
mg/Kg -
dry
345
1
08/08/23 21:47
TJS
6010D
Magnesium
4140
mg/Kg -
dry
172
1
08/08/23 21:47
TJS
6010D
Sodium
2560
mg/Kg -
dry
862
1
08/08/23 21:47
TJS
6010D
Iron
16300
mg/Kg -
dry
345
1
08/08/23 21:47
TJS
6010D
Zinc
2240
mg/Kg -
dry
43.1
1
08/08/23 21:47
TJS
6010D
Ammonia Nitrogen
17400
mg/Kg -
dry
3450
1
08/17/23 14:30
JPJ
SM-4500-NH3C
Nitrate+Nitrite-N
<172
mg/Kg -
dry
172
1
08/07/23 14:35
CLP
4500NO3F-2016
Cadmium
<3.45
mg/Kg -
dry
3.45
1
08/08/23 21:47
TJS
6010D
Chromium
50.7
mg/Kg -
dry
8.62
1
08/08/23 21:47
TJS
6010D
Mercury
<5.97
mg/Kg -
dry
5.97
1
08/08/23 11:53
FDS
SW-7471B
pH
7.0
S.U.
1
08/10/2315:55
ANV
9045D
Molybdenum
11.8
mg/Kg -
dry
8.62
1
08/08/23 21:47
TJS
6010D
Qualifiers/ DF Dilution Factor
Definitions
MQL Method Quantitation Limit
Page 4 of 7

Waypointo
ANALYTICAL
Client: Synagro Central LLC/ Oxford
Project: Oxford
Lab Report Number: 23-215-0009
Date: 8/17/2023
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
www.waypointanalytical.com
CASE NARRATIVE
Metals Analysis Method 601 OD
Sample 63010 (Lagoon)
Analyte: Zinc
QC Batch No: 1-697634/1-697089
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Page 5 of 7

WayPAoInt..
NALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
www.waypointanalytical.com
Shipment Receipt Form
Customer Number: 46478
Customer Name: Synagro Central LLC/ Oxford
Report Number: 23-215-0009
Shipping Method
0 Fed Ex 0 US Postal 0 Lab
0 UPS 0 Client 0 Courier
0 Other:
Thermometer ID:
Shipping container/cooler uncompromised?
* Yes
0 No
Number of coolers/boxes received
Custody seals intact on shipping container/cooler?
0 Yes
0 No
Not Present
Custody seals intact on sample bottles?
0 Yes
0 No
Not Present
Chain of Custody (COC) present?
# Yes
0 No
COC agrees with sample label(s)?
# Yes
0 No
COC properly completed
# Yes
0 No
Samples in proper containers?
# Yes
0 No
Sample containers intact?
# Yes
0 No
Sufficient sample volume for indicated test(s)?
# Yes
0 No
All samples received within holding time?
# Yes
0 No
Cooler temperature in compliance?
# Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
# Yes
0 No
Water - Sample containers properly preserved
0 Yes
0 No
N/A
Water - VOA vials free of headspace
0 Yes
0 No
N/A
Trip Blanks received with VOAs
0 Yes
0 No
N/A
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
0 N/A
F_ High concentration container (48 hr)
F_ High concentration pre -weighed (methanol -14 d)
F_ Low concentration EnCore samplers (48 hr)
F_ Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included? 0 Yes * No
Comments:
Signature: IDavid Lennon Date & Time: 08/03/2023 10:53:20
Page 6 of 7

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Page 7 of 7
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Waypointo
ANALYTICAL
10/24/2023
Synagro Central LLC/ Oxford
Mary Brewer
284 Boger Road
Mocksville, NC, 27028
Ref: Analytical Testing
Report Number: 23-286-0001
Project Description: Oxford WWTP
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
www.waypointanalytical.com
Dear Mary Brewer:
Waypoint Analytical Virginia, Inc. received sample(s) on 10/13/2023 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information
Sincerely,
&;'-� ­AldA�
Brandi Watson
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 1 of 7

Waypoint
ANALYTICAL
Report Number: 23-286-0001
Client Project Description: Oxford WWTP
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
www.waypointanalytical.com
Sample Summary Table
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
63733
Oxford WWTP
Solids
10/12/2023 07:08
10/13/2023
63733
Oxford WWTP
Solids
10/12/2023 07:08
10/13/2023
63733
Oxford WWTP
Solids
10/12/2023 07:08
10/13/2023
63733
Oxford WWTP
Solids
10/12/2023 07:08
10/13/2023
63733
Oxford WWTP
Solids
10/12/2023 07:08
10/13/2023
63733
Oxford WWTP
Solids
10/12/2023 07:08
10/13/2023
63733
Oxford WWTP
Solids
10/12/2023 07:08
10/13/2023
63733
Oxford WWTP
Solids
10/12/2023 07:08
10/13/2023
SM-4500-NH3C
WP MTN
9045D
WP MTN
4500NO3F-2016
WP MTN
6010D
WP MTN
SW-7471B
WP MTN
SM-4500-NH3C-TKN
WP MTN
SM-2540G
WP MTN
WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN
Page 2 of 7

WayPANALYTICAL
46478
Synagro Central LLC/ Oxford Project
Mary Brewer
284 Boger Road Information
Mocksville , NC 27028
Report Number : 23-286-0001
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
www.waypointanalytical.com
Oxford WWTP
REPORT OFANALYSIS
Report Date : 10/24/2023
Received : 10/13/2023
Brandi Watson
Lab No : 63733
Sample ID : Oxford WWTP
Matrix: Solids
Sampled: 10/12/2023 7:08
Test
Results
Units
MQL
DF
Date / Time
By
Analytical
Analyzed
Method
Moisture
96.5
%
0.010
1
10/18/2316:14
CAH
SM-2540G
Potassium
3000
mg/Kg -
dry
286
1
10/19/23 00:50
BKN
6010D
Sulfur
10300
mg/Kg -
dry
286
1
10/19/23 00:50
BKN
6010D
Calcium
17000
mg/Kg -
dry
1430
1
10/19/23 00:50
BKN
6010D
Magnesium
4140
mg/Kg -
dry
143
1
10/19/23 00:50
BKN
6010D
Sodium
1940
mg/Kg -
dry
714
1
10/19/23 00:50
BKN
6010D
Iron
16000
mg/Kg -
dry
286
1
10/19/23 00:50
BKN
6010D
Aluminum
42000
mg/Kg -
dry
143
1
10/19/23 00:50
BKN
6010D
Manganese
683
mg/Kg -
dry
14.3
1
10/19/23 00:50
BKN
6010D
Copper
546
mg/Kg -
dry
14.3
1
10/19/23 00:50
BKN
6010D
Zinc
1880
mg/Kg -
dry
35.7
1
10/19/23 00:50
BKN
6010D
Cadmium
<2.86
mg/Kg -
dry
2.86
1
10/19/23 00:50
BKN
6010D
Chromium
36.6
mg/Kg -
dry
7.14
1
10/19/23 00:50
BKN
6010D
Nickel
16.3
mg/Kg -
dry
7.14
1
10/19/23 00:50
BKN
6010D
Lead
26.1
mg/Kg -
dry
8.57
1
10/19/23 00:50
BKN
6010D
Arsenic
<14.3
mg/Kg -
dry
14.3
1
10/19/23 00:50
BKN
6010D
Mercury
<4.80
mg/Kg -
dry
4.80
1
10/19/23 11:14
FDS
SW-7471B
Selenium
<14.3
mg/Kg -
dry
14.3
1
10/19/23 00:50
BKN
6010D
Molybdenum
11.2
mg/Kg -
dry
7.14
1
10/19/23 00:50
BKN
6010D
Qualifiers/ DF Dilution Factor
Definitions
MQL Method Quantitation Limit
Page 3 of 7

�'
WayP
7621 Whitepine
Road, Richmond, VA 23237
Main 804-743-9401 Fax [phone]
ANALYTICAL
www.waypointanalytical.com
46478
Synagro Central LLC/ Oxford
Project
Oxford WWTP
Mary Brewer
Report Date : 10/24/2023
284 Boger Road
Information :
Received : 10/13/2023
Mocksville , NC 27028
Brandi Watson
Report Number : 23-286-0001
REPORT OFANALYSIS
Lab No : 63733
Matrix: Solids
Sample ID : Oxford WWTP
Sampled: 10/12/2023 7:08
Test
Results
Units
MQL
DF Date / Time
By Analytical
Analyzed
Method
Ammonia Nitrogen
8060
mg/Kg - dry
2860
1 10/23/23 08:58
JPJ SM-4500-NH3C
Nitrate+Nitrite-N
<143
mg/Kg - dry
143
1 10/19/23 12:11
CLP 4500NO3F-2016
Organic N
188800
mg/Kg - dry
7143
1 10/20/23 11:40
CALCULATION
pH
9.0
S.U.
1 10/19/2316:10
CNB 9045D
Total Solids
3.49
%
0.010
1 10/18/23 16:14
CAH SM-2540G
Total Kjeldahl Nitrogen
197000
mg/Kg - dry
7140
1 10/20/23 11:40
JPJ ;M-4500-NH3C-TKI`
Phosphorus
21000
mg/Kg - dry
143
1 10/19/23 00:50
BKN 6010D
Qualifiers/ DF Dilution Factor
Definitions
MQL Method Quantitation Limit
Page 4 of 7

Waypointo
ANALYTICAL
Client: Synagro Central LLC/ Oxford
Project: Oxford WWTP
Lab Report Number: 23-286-0001
Date: 10/23/2023
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
www.waypointanalytical.com
CASE NARRATIVE
Metals Analysis Method 601 OD
Sample 94539 (ST230CT01-03-001)
Analyte: Aluminum
QC Batch No: L711845/L711469
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 94539 (ST230CT01-03-001)
Analyte: Calcium
QC Batch No: L711845/L711469
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 94539 (ST230CT01-03-001)
Analyte: Potassium
QC Batch No: L711845/L711469
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 94539 (ST230CT01-03-001)
Analyte: Sulfur
QC Batch No: L711845/L711469
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Solids Total Mercury Analysis - CVAA Method 7471A
Sample 94759 (Bio-solids Class A)
Analyte: Mercury
QC Batch No: L711917/L711724
The matrix spike, matrix spike duplicate and the post digestion spike were all outside of the quality control
acceptance ranges. Matrix interference is suspected
Page 5 of 7

WayPAoInt..
NALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
www.waypointanalytical.com
Shipment Receipt Form
Customer Number: 46478
Customer Name: Synagro Central LLC/ Oxford
Report Number: 23-286-0001
Shipping Method
0 Fed Ex 0 US Postal 0 Lab
0 UPS 0 Client 0 Courier
0 Other:
Thermometer ID:
Shipping container/cooler uncompromised?
* Yes
0 No
Number of coolers/boxes received
Custody seals intact on shipping container/cooler?
0 Yes
0 No
Not Present
Custody seals intact on sample bottles?
0 Yes
0 No
Not Present
Chain of Custody (COC) present?
# Yes
0 No
COC agrees with sample label(s)?
# Yes
0 No
COC properly completed
# Yes
0 No
Samples in proper containers?
# Yes
0 No
Sample containers intact?
# Yes
0 No
Sufficient sample volume for indicated test(s)?
# Yes
0 No
All samples received within holding time?
# Yes
0 No
Cooler temperature in compliance?
# Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
# Yes
0 No
Water - Sample containers properly preserved
0 Yes
0 No
N/A
Water - VOA vials free of headspace
0 Yes
0 No
N/A
Trip Blanks received with VOAs
0 Yes
0 No
N/A
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
0 N/A
F_ High concentration container (48 hr)
F_ High concentration pre -weighed (methanol -14 d)
F_ Low concentration EnCore samplers (48 hr)
F_ Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included? 0 Yes * No
Comments:
Signature: IDavid Lennon Date & Time: 10/13/2023 11:27:21
Page 6 of 7

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lium
-OEM
DUE
FM
ulmm�
Page 7 of 7

Waypointo
ANALYTICAL
1 /2/2024
Synagro Central LLC/ Oxford
Mary Brewer
284 Boger Road
Mocksville, NC, 27028
Ref: Analytical Testing
Report Number: 23-341-0005
Project Description: Project Location:Oxford
Sample Location:Lagoon
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
www.waypointanalytical.com
Dear Mary Brewer:
Waypoint Analytical Virginia, Inc. received sample(s) on 12/7/2023 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information
Sincerely,
& " 0 " -Ab " '� (--, "
Brandi Watson
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 1 of 9

Waypointo
ANALYTICAL
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 Fax [phone]
www.waypointanalytical.com
Certification Summary
Laboratory ID: WP MTN: Waypoint Analytical, LLC., Memphis, TN
State
Program
Lab ID
Expiration Date
Alabama
State Program
40750
02/29/2024
Arkansas
State Program
88-0650
02/07/2024
California
State Program
2904
06/30/2024
Florida
State Program
- NELAP
E871157
06/30/2024
Georgia
State Program
C044
11/14/2025
Georgia
State Program
04015
06/30/2024
Illinois
State Program
- NELAP
200078
10/31/2024
Kentucky
State Program
80215
06/30/2024
Kentucky
State Program
KY90047
12/31/2024
Louisiana
State Program
- NELAP
LA037
12/31/2024
Louisiana
State Program
- NELAP
04015
06/30/2024
Mississippi
State Program
MS
11/14/2025
North Carolina
State Program
47701
07/31/2024
North Carolina
State Program
415
12/31/2023
Pennsylvania
State Program
- NELAP
68-03195
05/31/2024
South Carolina
State Program
84002
06/30/2024
Tennessee
State Program
02027
11/14/2025
Texas
State Program
- NELAP
T104704180
09/30/2024
Virginia
State Program
00106
06/30/2024
Virginia
State Program
- NELAP
460181
09/14/2024
Page 1 of 1 00009/23-341-0005
Page 2 of 9

•
7621 Whitepine Road, Richmond, VA 23237
Waypoint
Main 804-743-9401 0 Fax [phone]
ANALYTICAL www.waypointanalytical.com
Sample Summary Table
Report Number: 23-341-0005
Client Project Description: Project Location:Oxford
Sample Location:Lagoon
Lab No
Client Sample ID
Matrix
Date Collected
Date Received
Method
Lab ID
64077
Oxford
Solids
12/06/2023 14:22
12/07/2023
64077
Oxford
Solids
12/06/2023 14:22
12/07/2023
SM-4500-NH3C
WP MTN
64077
Oxford
Solids
12/06/2023 14:22
12/07/2023
SW-7471B
WP MTN
64077
Oxford
Solids
12/06/2023 14:22
12/07/2023
4500NO3F-2016
WP MTN
64077
Oxford
Solids
12/06/2023 14:22
12/07/2023
6010D
WP MTN
64077
Oxford
Solids
12/06/2023 14:22
12/07/2023
6020B
WP MTN
64077
Oxford
Solids
12/06/2023 14:22
12/07/2023
SM-4500-NH3C-TKN
WP MTN
64077
Oxford
Solids
12/06/2023 14:22
12/07/2023
9045D
WP MTN
64077
Oxford
Solids
12/06/2023 14:22
12/07/2023
SM-2540G
WP MTN
WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN
Page 3 of 9

WayPANALYTICAL
46478
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
www.waypointanalytical.com
Synagro Central LLC/ Oxford Project Project Location:Oxford
Mary Brewer
284 Boger Road Information : Sample Location:Lagoon
Mocksville , NC 27028
Report Number : 23-341-0005
REPORT OFANALYSIS
Report Date : 01/02/2024
Received : 12/07/2023
Brandi Watson
Lab No : 64077
Matrix: Solids
Sample ID : Oxford
Sampled:
12/6/2023
14:22
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Method
Moisture
98.4
%
0.010
1
12/08/2316:00
CAH
SM-2540G
Aluminum
42300
mg/Kg -
dry
291
313
1
12/14/23 01:22
TJS
6010D
Arsenic
<5.34
mg/Kg -
dry
5.34
15.6
5
12/29/23 22:37
CPW
6020B
Cadmium
<3.13
mg/Kg -
dry
3.13
6.25
1
12/14/23 01:22
TJS
6010D
Calcium
18200
mg/Kg -
dry
2420
3130
1
12/14/23 01:22
TJS
6010D
Chromium
30.5
mg/Kg -
dry
15.6
15.6
1
12/14/23 01:22
TJS
6010D
Copper
550
mg/Kg -
dry
18.8
31.3
1
12/14/23 01:22
TJS
6010D
Iron
16300
mg/Kg -
dry
534
625
1
12/14/23 01:22
TJS
6010D
Mercury
<1.41
mg/Kg -
dry
1.41
11.7
1
12/13/23 11:58
FDS
SW-7471B
Lead
31.4
mg/Kg -
dry
12.5
18.8
1
12/14/23 01:22
TJS
6010D
Magnesium
4410
mg/Kg -
dry
163
313
1
12/14/23 01:22
TJS
6010D
Manganese
675
mg/Kg -
dry
21.9
31.3
1
12/14/23 01:22
TJS
6010D
Molybdenum
9.753
mg/Kg -
dry
9.38
15.6
1
12/14/23 01:22
TJS
6010D
Nickel
15.33
mg/Kg -
dry
9.38
15.6
1
12/14/23 01:22
TJS
6010D
Phosphorus
22700
mg/Kg -
dry
175
313
1
12/14/23 01:22
TJS
6010D
Potassium
3430
mg/Kg -
dry
388
625
1
12/14/23 01:22
TJS
6010D
Selenium
<6.44
mg/Kg -
dry
6.44
15.6
5
12/29/23 22:37
CPW
6020B
Sodium
3850
mg/Kg -
dry
813
1560
1
12/14/23 01:22
TJS
6010D
Sulfur
11100
mg/Kg -
dry
325
625
1
12/14/23 01:22
TJS
6010D
Zinc
1980
mg/Kg -
dry
53.1
78.1
1
12/14/23 01:22
TJS
6010D
pH
7.5 L
S.U.
1
12/11/23 17:05
CNB
9045D
Ammonia Nitrogen
<6250
mg/Kg -
dry
6250
1
12/21/23 11:25
JPJ
SM-4500-NH3C
Total Kjeldahl Nitrogen
36600
mg/Kg -
dry
15600
1
12/20/23 10:21
JPJ ;M-4500-NH3C-TKI`
Qualifiers/ B
Analyte detected in blank
DF
Dilution Factor
Definitions J
Estimated value
L
Limit Exceeded
MQL
Method Quantitation Limit
Page 4 of 9

�'
WayP
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 Fax [phone]
ANALYTICAL
www.waypointanalytical.com
46478
Synagro Central LLC/ Oxford
Project
Project Location:Oxford
Mary Brewer
Report Date : 01/02/2024
284 Boger Road
Information : Sample Location:Lagoon
Received : 12/07/2023
Mocksville , NC 27028
Brandi Watson
Report Number : 23-341-0005
REPORT OFANALYSIS
Lab No : 64077
Matrix: Solids
Sample ID : Oxford
Sampled: 12/6/2023 14:22
Test
Results
Units MDL
MQL DF Date / Time By Analytical
Analyzed Method
Organic N
36630
mg/Kg - dry
15630 1 12/20/23 10:21 CALCULATION
Nitrate+Nitrite-N
565
mg/Kg - dry
313 1 12/15/23 10:13 CLP 4500NO3F-2016
Total Solids
1.59
%
0.010 1 12/08/23 16:00 CAH SM-2540G
Qualifiers/ B Analyte detected in blank
Definitions J Estimated value
MQL Method Quantitation Limit
DF Dilution Factor
L Limit Exceeded
Page 5 of 9

WayPAoInt..
NALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
www.waypointanalytical.com
Shipment Receipt Form
Customer Number: 46478
Customer Name: Synagro Central LLC/ Oxford
Report Number: 23-341-0005
Shipping Method
0 Fed Ex 0 US Postal 0 Lab
0 UPS 0 Client 0 Courier
0 Other:
Thermometer ID:
Shipping container/cooler uncompromised?
* Yes
0 No
Number of coolers/boxes received
Custody seals intact on shipping container/cooler?
0 Yes
0 No
Not Present
Custody seals intact on sample bottles?
0 Yes
0 No
Not Present
Chain of Custody (COC) present?
# Yes
0 No
COC agrees with sample label(s)?
# Yes
0 No
COC properly completed
# Yes
0 No
Samples in proper containers?
# Yes
0 No
Sample containers intact?
# Yes
0 No
Sufficient sample volume for indicated test(s)?
# Yes
0 No
All samples received within holding time?
# Yes
0 No
Cooler temperature in compliance?
# Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
# Yes
0 No
Water - Sample containers properly preserved
0 Yes
0 No
N/A
Water - VOA vials free of headspace
0 Yes
0 No
N/A
Trip Blanks received with VOAs
0 Yes
0 No
N/A
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
0 N/A
F_ High concentration container (48 hr)
F_ High concentration pre -weighed (methanol -14 d)
F_ Low concentration EnCore samplers (48 hr)
F_ Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included? 0 Yes * No
Comments:
Signature: IDavid Lennon Date & Time: 12/07/2023 11:26:10
Page 6 of 9

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Page 7 of 9
I
fv
m
C7 X
I
►i

Waypoint.
ANALYTICAL
12/07/2023 13:39:26
Export Batch Report
Export Batch Id : 4330E
TO: Waypoint Analytical - TN
2790 Whitten Road
Memphis, TN 38133
901-213-2400
Report No Due Date
23-341-0004 12/20/2023
23-341-0004 12/20/2023
23-341-0004 12/20/2023
23-341-0004 12/20/2023
23-341-0004 12/20/2023
23-341-0004 12/20/2023
23-341-0004 12/20/2023
23-341-0005 12/20/2023
23-341.0005 12/20/2023
23-341-0005 12/20/2023
23-341-0005 12/20/2023
23-341-0005 12/20/2023
23-341-0005 12/20/2023
23-341-0005 12/20/2023
23-341-0005 12/20/2023
23-341-0006 12/20/2023
23-341-0006 12/20/2023
23-341-0006 12/20/2023
23-341-0006 12120/2023
23-341-0006 12/20/2023
23-341-0006 12/20/2023
23-341-0006 12/20/2023
23-341-0006 12/20/2023
23-341-0007 12/20/2023
23-341-0007 12/20/2023
23-341-0007 12/20/2023
23-341-0007 12/20/2023
Rjjjh Mi1.tER
Lab N4 Method No
SOL
6407 SM-254OG
SOL
64076 SM-4500-NH3C
SOL
64076 SM-4500-NH3C-TKN
SOL
64076 SM-4500-NO3F
SOL
64076 SW-6010D
SOL
W76 SW-7471A
SOL
64076 SW-9045D
SOL
640714
M-2540G
SOL
64077 5M-4500-NH3C
SOL
64077 SM-4500-NH3C-TKN
SOL
64077 SM-4500-1103F
SOL
64077 SW-6010D
SQL
64077 SW-60208
SOL
64077 SW-7471A
SOL
64077 SW-9045❑
SOL
64078'/SM-254QG
SOL
64078 SM-4500-NH3C
SOL
64078 SM-4500-NH3C-TKN
SOL
64078 SM-4500•NO3F
SOL
64078 SW-6010D
SOL
64078 SW-60208
SOL
64078 SW-7471A
SOL
64078 SW-9045D
SOL
64079 SM-254OG
SOL
64079V`SM-4500-NH3C
SOL
64079 SM-4500-NH3C-TKN
SOL
64079 SM-4500-NO3F
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Page 1 of 2
Created: 12/7/2023 13: 39 :16
Computer: WPALMS-019
User: David Lennon
From: Waypoint Analytical Virginia, Inc.
7621 Whitepine Rd.
Richmond, VA 23237
804-743-9401
Fee Code Descriotion
SLWESTM
SLWESTM
SLWESTM
SLWESTM
SLWESTM
SLWESTM
SLWESTM
SYN-1
SYN-1
SYN-1
SYN-1
SYN-1
SYN•1
SYN-1
SYN-1
SYN-1
SYN-1
SYN-1
SYN-1
SYN-1
SYN-1
SYN-1
SYN-1
SYN-1
SYN-1
SYN-1
SYN-1
Sampled By
Method of Shipment
Blank / Cooler T nit
T{ `
Remarks
Relinquished By (sign)
Date / Time
Received By (sign)
Date / Time
Relinquished By (sign)
Date / Time
Recel d By {sin
Date / Time
� A
0�5 {V
Page 8 of 9

Waypointo
ANALYTICAL
12/07/2023 13:39:26
Export Batch Report
Export Batch Id : 4330E
To: Waypoint Analytical - TN
2790 Whitten Road
Memphis, TN 38133
901-213-2400
Report No Due Date B11j!
Matrix
Lab No
Method No
23-341-0007 12/20/2023
SOL
64079
SW-60100
23-341-0007 12/20/2023
SOL
64079
SW-60208
23-341-0007 12/20/2023
SOL
64079
SW-7471A
23-341-0007 12/20/2023
SOL
64079
SW-90451)
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax $04-271-6446
www.waypointanalytical.com
Page 2 of 2
Created: 12/7/2023 13:39:16
Computer: WRALMS-019
User: David Lennon
From: Waypoint Analytical Virginia, Inc.
7621 Whitepine Rd.
Richmond, VA 23237
804-743-9401
fee Code Qgscription
SYN-1
SYN-1
SYN-1
SYN-1
Sampled By
Method of Shipment
Blank / Cooler Temp.
Remarks
Relinquished By (sign)
Date / Time
Received 8y (sign)
Date / Time
Relinquished By (sign)
Date / Time
Received By (sign)
Date / Time
Page 9 of 9

SECTION 3

FACILITY NAME: OXFORD, NC
LAND OWNER: TONI H. DENNY
OPERATOR: EDWARD DENNY
CROP 1 NAME: FESCUE HAY (FSH)
RESIDUAL SOURCE(S): * See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
WQ PERMIT M WQ0011244 FIELD#: NC-GR-00004-0-0002-
ANNUAL DRY TONS APPLIED: 15.85 SITE #: NC GR 00004
PREDOMINANT SOIL SERIES: GEORGEVILLE
CROP 1 MAX. PAN: 211 CROP 2 NAME:
ACRES UTILIZED: 8.5
ACRES PERMITTED: 8.5
CATION EXCHANGE CAPACITY (NON-503):
CROP 2 MAX. PAN:
Page: 1
Date or
Month
Gallons (G)
or Cubic Yards (Y)
or Wet Tons (W)
%
Solids
Dry Tons/Ac
Residual
Source
Site
Cond.
Dry, Wet,
Moist
Precip
Past 24 Hrs.
Inches
Application
Method*
Volati-
lization
Rate**
Mineral-
ization
Rate***
TKN
mg/kg
Ammonia
Nitrogen
mg/kg
Nitrate
and Nitrite
ng/kg
-
PAN Applied
(Ibs/acre)
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Crop 1
Crop 2
Amount
UOM
10/16/2023
Oct-23
130,200.00
130,2001.00
(G)
(G)
mm2.920
1.865
OXAEDL
DRY
0-<1/2—
SUR
0.5
0.30
63,800.00
17,400.00
72.00
84.998
FSH
Total 1.865
AS
Annual Ibs/acre Applied 0.064
Ibs/acre Applied 0.367
CU CR
264 0.189 1 0.1
18.609 1 2.474 1 1
HG NI SE ZN
022 0044 I 0.084 0 064 8.356
0,067 1 0,358 1 0.912 1 0.422
Date
Permit PAN Limit (Ibs/acre) 1st Crop` _ 1
Federal C.P L R. (Ibs/acre) ** * 36.6 1 34.8 1 339 0 _ 267.9 1 15.0 _ 375.0 1 89.0 1 2,500.0
OXAEDL = OXFORD, NC AEROB. DIGESTED LIQUID
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am
aware that there are significant penalties for sub ing false information, including the possibility of fines and imprisonment for knowing violations."
IGN T E OF LAND APPLIER dATE
NR = Not Reported or Not Required *** Mineralization Rates: Compost-0.1, Anaerobically digested-0.2, Aerobically digested-0.3, Raw Sludge-0.4
* Application Method: SUR - Surface, [NJ - Injection, SURIN - Incorporation **** C.P.L.R.: Cumulative Pollutant Loading Rate
** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 ***** See Site pH & Lime Application Records Section of Report
Printed: 1/24/2024 DENR FORM FSF (12/2006)

FACILITY NAME: OXFORD, NC
LAND OWNER: EDWARD DENNY
OPERATOR: EDWARD DENNY
CROP 1 NAME: FESCUE HAY (FSH)
RESIDUAL SOURCE(S): * See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
WQ PERMIT #: WQ0011244 FIELD#: NC-GR-00004-0-0003-
ANNUAL DRY TONS APPLIED: 132.87 SITE #: NC GR 00004
PREDOMINANT SOIL SERIES: GEORGEVILLE
CROP 1 MAX. PAN: 211 CROP 2 NAME:
ACRES UTILIZED: 52.5
ACRES PERMITTED: 52.5
CATION EXCHANGE CAPACITY (NON-503):
CROP 2 MAX. PAN:
Page: 1
Date or
Month
Gallons (G)
or Cubic Yards (Y)
or Wet Tons (W)
Amount UOM
%
Solids
Dry Tons/AC
Residual
Source
Site
Cond.
Dry, Wet,
Moist
Precip
Past 24 Hrs.
Inches
Application
Method*
Volati-
lization
Rate**
Mineral-
ization
Rate***
TKN
mg/kg
Ammonia
Nitrogen
mg/kg
Nitrate
and Nitrite
rng/kg
PAN Applied
(lbs/acre)
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Crop 1
Crop 2
10/9/2023
167,400.00. .(G)
2.9.....,
20
0.386
OXAEDL
DRY
0-<1/2""
SUR
0.5
0.30
63,800.00
17,400.00
172.00
17.693
FSH
10/10/2023
223,200.00 (G)
2.920
0.518
OXAEDL
DRY
0-<1/2""
SUR
0.5
0.30
63,800.00
17,400.00
172.00
23.591
FSH
10/11/2023
248,000.00 (G)
2.920
0,575
OXAEDL
DRY
0-<1/2""
SUR
0.5
0.30
63,800,00
17,400.00
172.00
26.213
FSH
10/12/2023
241,800.00 (G)
2,920
0.561
OXAEDL
DRY
0-<1/2""
SUR
0.5
0.30
63,800.00
17,400.00
172.00
25.557
FSH
10/13/2023
173,600.00 (G)
2.920
0.403
OXAEDL
DRY
0-<1/2"
SUR
0.5
0.30
63,800.00
17,400.00
172.00
18.349
FSH
10/16/2023
37,200.00 (G)
2.920
0.086
OXAEDL
DRY
0-<1/2""
SUR
0.5
0.30
63,800.00
17,400.00
172.00
3.932
FSH
Oct-23
1,091,200.00
1.
Total 2.531 -.1
OXAEDL = OXFORD, NC AEROB. DIGESTED LIQUID
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am
aware that there are significant penalties foy'submitting false information, including the possibility of fines and imprisonment for knowing violations."
1 2/22y
GNA R LAND APPLIER DATE
ATE
=Not Reported or Not Required *** Mineralization Rates: Compost-0.1, Anaerobically digested-0.2, Aerobically digested-0.3, Raw Sludge-0.4
* Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation **** C.P.L.R.: Cumulative Pollutant Loading Rate
** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 ***** See Site pH & Lime Application Records Section of Report
Printed: 1/24/2024 DENR FORM FSF (12/2006)

FACILITY NAME: OXFORD, NC
LAND OWNER: RED HILL PLANTATION LLC
OPERATOR: JAKE ISLEY
CROP 1 NAME: FESCUE HAY (FSH)
RESIDUAL SOURCE(S): * See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
WQ PERMIT #: WQ0011244 FIELD#: NC-GR-00060-0-0001-
ANNUAL DRY TONS APPLIED: 89.84 SITE #: NC GR 00060
PREDOMINANT SO] L SERIES: IREDELL
CROP 1 MAX. PAN: 121 CROP 2 NAME:
ACRES UTILIZED: 43.3
ACRES PERMITTED: 43.3
CATION EXCHANGE CAPACITY (NON-503):
CROP 2 MAX. PAN:
Page: 1
Gallons
Site
Name of Crop Type
or Cubic Yards (Y)
Cond.
Precip
Volati-
Mineral-
Ammonia
Nitrate
PAN Applied
Receiving Residual
Date or
or Wet Tons (W)
%
Residual
Dry, Wet,
Past 24 Hrs.
Application
lization
ization
TKN
Nitrogen
and Nitrite
(lbs/acre)
Application
Crop 1
Crop 2
1
CFSH
2
CropM
Month
Solids
Dry Tons/Ac
Source
Moist
Inches
tl
a^y
Method*
Rate**
Rate
-
Amount
UOM
10/17/2023
204,600.00
(G)
2.920
OXAEDL
_
DRY
mm
0 <1/2
0.575
SUR
0.5
0.30
0/k 00
63, 0
17 400.00
172/kg
10/18/2023
204,600.00
(G)
2.920
0.575
OXAEDL
DRY
0-<1/2""
SUR
0.5
0.30
63,800,00
17,400.00
172.00
26.220
FSH
10/19/2023
204,600.00
(G)
2.920
0.575
OXAEDL
DRY
0-<1/2""
SUR
0.5
0.30
63,800.00
17,400.00
172.00
26.220
FSH
10/20/2023
124,000.00
(G)
2,920
0.349
OXAEDL
DRY
0-<1/2""
SUR
0.5
0.30
63,800.00
17,400.00
172.00
15.891
FSH
Oct-23
737,800.00
(G)
Total 2.074
OXAEDL = OXFORD, NC AEROB. DIGESTED LIQUID
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered slid evaluated the information submitted. I am
aware that there are significant penalties for subs ' in false information, including the possibility of fines and imprisonment fo knowing violations."
S E O L APPLIER I DATE
NR = Not Reported or Not Required *** Mineralization Rates: Compost-0.1, Anaerobically digested-0.2, Aerobically digested-0.3, Raw Sludge-0.4
* Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation **** C.P.L.R.: Cumulative Pollutant Loading Rate
** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 ***** See Site pH & Lime Application Records Section of Report
Printed: 1/24/2024 DENR FORM FSF (12/2006)

FACILITY NAME: OXFORD, NC
LAND OWNER: RED HILL PLANTATION LLC
OPERATOR: JAKE ISLEY
CROP 1 NAME: FESCUE HAY (FSH)
RESIDUAL SOURCE(S): * See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
WQ PERMIT#: WQ0011244 FIELD#: NC-GR-00060-0-0002-
ANNUAL DRY TONS APPLIED: 111.73 SITE #: NC GR 00060
PREDOMINANT SOIL SERIES: LIGNUM
CROP 1 MAX. PAN: 190 CROP 2 NAME:
ACRES UTILIZED: 31.9
ACRES PERMITTED: 31.9
CATION EXCHANGE CAPACITY (NON-503):
CROP 2 MAX. PAN:
Page: 1
Gallons (G)
Site
Name of Crop Type
or Cubic Yards (Y)
Cond.
Precip
Volati-
Mineral-
Ammonia
Nitrate
PAN Applied
Receiving Residual
Date or
or Wet Tons (W)
%
Residual
Dry, Wet,
Past 24 Hrs.
Application
lization
ization
TKN
Nitrogen
and Nitrite
(Ibs/acre)
Application
Month
Solids
Dry Tons/Ac
Source
Moist
Inches
Method*
Rate**
Rate***
mg/kg
�mgrkg
mg/kg
Amount
UOM
Crop 1
15,D99
Crop 2
Crop 1RCrop
FSH
2
7/25/2023
86,800.00
(G)
2.920
0.331
OXAEDL
DRY
0-<1/2"
SUR
p-0.5
0.30
63,800.00
17,400.00
172.00
7/26/2023
117,800.00
(G)
2.920
0.450
OXAEDL
DRY
0-<1/2""
SUR
1 0.5
0.30
63,800.00
17,400.00
172XO
20.491
FSH
7/27/2023
111,600.00
(G)
2.920
0.426
OXAEDL
DRY
0-<1/2""
SUR
0.5
0.30
63.800.00
17,400.00
172.00
19.413
FSH
7/28/2023
68,200.00
(G)
2.920
0.260
OXAEDL
DRY
0-<1/2""
SUR
0.5
0.30
63,800,00
17,400.00
172.00
11.863
FSH
7/31/2023
99,200.00
(G)
2.920
0.379
OXAEDL
DRY
0-1/2
SUR
0.5
0.30
63,800.00
17,400.00
172.00
17.256
FSH
Jul-23
483,600.00
(G)
_
8/1/2023
130,200.00
(G)
2.920
0.497
OXAEDL
MOIST
0-<1/Z
SUR
0.5
0.30
63,800.00
17,400.00
172.00
22.648
FSH
8/2/2023
111,600.00
(G)
2.920
0.426
OXAEDL
DRY
0-<1/2""
SUR
0.5
0.30
63,800.00
17,400.00
172.00
19.413
FSH
8/3/2023
124,000.00
(G)
2.920
0.473
OXAEDL
DRY
0-<1/2"
SUR
0.5
0.30
63,800.00
17,400.00
172.00
21.570
FSH
8/4/2023
12,400.00
(0)
2.920
0.047
OXAEDL
DRY
0-<1/2"
SUR
0.6
0.30
63,800.00
17,400.00
172.00
2.157
FSH
Aug-23
378,200.00
(G)
10/19/2023
31,000.00
(G)
2.920
0.118
OXAEDL
DRY
0-<112""
SUR
0.5
0.30
63,800.00
17,400.00
172.00
5.392
FSH
10/20/2023
24,800.00
(G)
2,920
D.095
OXAEDL
DRY
0-<1/2""
SUR
0.5
0.30
63,800.00
17,400.00
172.00
4.314
FSH
Oct-23
55,800.00
(G)
Total 3.502
E ZIN
Annual Ibd s/acre Applied OA121 0.024 4 252 0 355 10 275 0 042 0.083 0 N58 OS lied
21 15. 91 158.314 Date rme AppLbs/Ac
re Applied 0.627 1 0.167 29.859 4.287 -_ 3.459 0.113 1 0.711 1 1.564 1 0.779 - 135.186
(Its/acre) St Crop;
Federal C.P.L.R. (Ibs/acre)*** 36.6 34.8 1 1,339.0 ! + 267.9 1 15.0 j 375.0 1 89012,500.0
OXAEDL = OXFORD, NC AEROB. DIGESTED LIQUID ! �1
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am
aware that there are significant penalties fors bmi ing false information, vnding the possibility of fines and imprisomn for k lowing violations."
IG RE 0 LA PPLIER DATE
NR = Not Reported or Not Required *** Mineralization Rates: Compost-0.1, Anaerobically digested-0.2, Aerobically digested-0.3, Raw Sludge-0.4
* Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation *'** C.P.L.R.: Cumulative Pollutant Loading Rate
** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 *** * See Site pH & Lime Application Records Section of Report
Printed: 1/24/2024 DENR FORM FSF (12/2006)

FACILITY NAME. OXFORD, NC
LAND OWNER: RED HILL PLANTATION LLC
OPERATOR: JAKE ISLEY
CROP 1 NAME: FESCUE HAY (FSH)
RESIDUAL SOURCE(S): * See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
WQ PERMIT #: WQ0011244 FIELD#: NC-GR-00060-0-0003-
ANNUAL DRY TONS APPLIED: 60.70 SITE #: NC GR 00060
PREDOMINANT SOIL SERIES: ENON
CROP 1 MAX. PAN: 194 CROP 2 NAME:
ACRES UTILIZED: 16.2
ACRES PERMITTED: 16.2
CATION EXCHANGE CAPACITY (NON-503):
CROP 2 MAX. PAN:
Page: 1
Date or
Month
Gallons (G)
or Cubic Yards (Y)
or Wet Tons (W)
Amount UOM
%
Solids
Dry Tons/Ac
Residual
Source
Sitem
Cond.
Dry, Wet,
Moist
Precip
Past 24 Hrs.
Inches
Application
Method*
Volati-
[ lization
Rate—
Mineral-
ization
Rate***
TKN
mg/kg
Ammonia
Nitrogen
mg/kg
Nitrate
and Nitrite
mg/kg
)
PAN Applied
(lbs/acre)
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Crop 1
Crop 2
5/23/2023
68,200.00
(G)
4.430
0.778
OXAEDL
DRY
0-<1/2""
SUR
0.5
0.30
19,100.00
896.00
29.20
9.225
FSH
5/24/2023
105,400.00
(G)
4.430
1.202
OXAEDL
DRY
0-<1/2""
SUR
0.5
0.30
19,100.00
896.00
29.20
14.257
FSH
5/25/2023
93,000.00
(G)
4.430
1.060
OXAEDL
DRY
0-<1/2""
SUR
0.5
0.30
19,100.00
896.00
29.20
12.580
FSH
5/26/2023
62,000.00
(G)
4.430
0.707
OXAEDL
DRY
0-<1/2""
SUR
0.5
0.30
19,100.00
896.00
29.20
8.387
FSH
May-23
328,600.00
(G)
Total 3.747 1 otai 44.44u u.uuu
OXAEDL = OXFORD, NC AEROB. DIGESTED LIQUID
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am
aware that there are significant penalties for submitting false informatio , including the possibility of fines and imprisonment for knowing violations."
'f 2 12 6 Y
,IXG ATURE OF LAND APPLIER DATE
NR = Not Reported or Not Required *** Mineralization Rates: Compost-0.1, Anaerobically digested-0.2, Aerobically digested-0.3, Raw Sludge-0.4
* Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation **** C.P.L.R.: Cumulative Pollutant Loading Rate
** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 ***** See Site pH & Lime Application Records Section of Report
Printed: 1/24/2024 DENR FORM FSF (12/2006)

FACILITY NAME: OXFORD, NC
LAND OWNER: RED HILL PLANTATION LLC
OPERATOR: JAKE ISLEY
CROP 1 NAME: FESCUE HAY (FSH)
RESIDUAL SOURCE(S): * See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
WQ PERMIT #: WQ0011244 FIELD#: NC-GR-00060-0-0004-
ANNUAL DRY TONS APPLIED: 45.81 SITE M NC GR 00060
PREDOMINANT SOIL SERIES: ENON
CROP 1 MAX. PAN: 194 CROP 2 NAME:
ACRES UTILIZED: 11.9
ACRES PERMITTED: 11.9
CATION EXCHANGE CAPACITY (NON-503):
CROP 2 MAX. PAN:
Page: 1
V Gallons (G�)
Site
_ -
Name of Crop Type
or Cubic Yards (Y)
Cond.
Precip
Volati-
Mineral-
Ammonia
Nitrate
PAN Applied
Receiving Residual
Date or
or Wet Tons (W)
%
Residual
Dry, Wet,
Past 24 Hrs.
Application
lization
ization
TKN
Nitrogen
and Nitrite
(Ibs/acre)
Application
Month
Solids
..�.....30,_
Dry Tons/Ac
Source
Moist
Inches
Method*
Rate**
Rate-
mg/kg
mg/kg
nng/kg
Amount
UOM
Crop 1
Crop 2
Crop 1
Crop 2
5/25/2023
6,200.00
(G)
4.4
0.096
OXAEDL
DRY
0-<1/2"
SUR
0.5
0,30
19,100.00
896.00
29.20
1.142
FSH
5/26/2023
55,800.00
(G)
4.430
0.866
OXAEDL
DRY
0-<1/2""
SUR
0.5
0.30
19,100.00
896.00
29.20
10.275
FSH
5/30/2023
86,800.00,
(G)
4.430
1.347
OXAEDL
DRY
0-<1/2""
SUR
0.5
0.30
19,100.00
896.00
29.20
15.984
FSH
5/31/2023
99,200.00
(G)
4,430
1.540
OXAEDL
DRY
0-<1/2""
SUR
0.5
0.30
19,100.00
896.00
29.20
18.267
FSH
May-23 1
248,000.00
(G)
Total 3.849 Total 45.668 0.000
AS CD CU CR PB HG MO NI SE ZN P Lime Applied
LAInual Ibs/acre Applied 0.022 0.004 1.332 0.0059 0.065 0.008 1 0.018 0.024 0.022 5.120 48,508 _ Date Lbs/Ac
Cumulative Ibs/acre Applied 0.361 0.100 18.619 2.889 1.210 0.053 0.359 T 0.902 0.438 84.695
Permit PAN Limit (Ibs/acre) 1st Cropi 194
Federal C.P.L.R. (Ibs/acre)**** 36.6 1 34.8 1,339.0 267.9 1 15.0 375.0 1 89.0 1 2,son n
OXAEDL = OXFORD, NC AEROB. DIGESTED LIQUID
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am
aware that there are significant penalties fo7tibm* ing false information, including the possibility of fines and imprisonment for knowing violations."
2-0 Y�
Z,-"SIC4KTURE1&rLAND APPLIER I DA E
NR = Not Reported or Not Required **' Mineralization Rates: Compost-0.1, Anaerobically digested-0.2, Aerobically digested-0.3, Raw Sludge-0.4
* Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation **** C.P.L.R.: Cumulative Pollutant Loading Rate
** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 *"*** See Site pH & Lime Application Records Section of Report
Printed: 1/24/2024 DENR FORM FSF (12/2006)

SECTION 4

SUMM111
ENVIRONMENTAL TECHN❑LOMZ3. INC
ArrzrJy0ca1 Laboralorfas
January 07, 2022
Ryan Copeland
Synagro
284 Boger Rd.
Mocksville, NC 27028
TEL: [phone]
FAX: [phone]
RE: Oxford
Dear Ryan Copeland:
Summit Environmental Technologies, Inc.
3310 Win St.
Cuyahoga Falls, Ohio 44223
TEL: [phone] FAX.- [phone]
Wehsite: http://www.settek.com
Order No.: 21121829
Summit Environmental Technologies, Inc. received 1 sample(s) on 12/29/2021 for the
analyses presented in the following report.
There were no problems with the analytical events associated with this report unless noted
in the Case Narrative.
Quality control data is within laboratory defined or method specified acceptance limits
except where noted.
If you have any questions regarding these tests results, please feel free to call the
laboratory.
Sincerely,
Jennifer Woolf
Project Manager
3310 Win St.
Cuyahoga Falls, Ohio 44223
Arkansas 88-0735, California 2943, Colorado, Connecticut PH-0108, Florida NELAC E87688, Idaho OH00923, Illinois 200061, Indiana C-OH-13, Kansas
E-10347, Kentucky (Underground Storage Tank) 3, Kentucky 90146, Maryland 339, Michigan 9988, Minnesota 1780279, Nevada OH009232020-1, New
Hampshire 2996, New Jersey OH006, New York 11777, North Carolina 39705 and 631, North Dakota R-201, Ohio DW, Ohio VAP C1,0052, Oklahoma
2019-155, Oregon OH2O0001, Pennsylvania 011, Rhode Island LA000317, South Carolina 92016001, Texas T104704466-19-16, Utah OH009232020-12,
Virginia VELAP 10381, West Virginia 9957C
Page 1 of 34

SUMMIY Summit Environmental Technologies, Inc. Case Narrative
3310 Win St.
ENVIRONMENTAL TEC„HQLOG4r;S,INC. Cuyahoga Falls, Ohio44223 WO#: 21121829
Arralyi9cal Laboralorlas TEL: [phone] FAX.- [phone]
Wehsite: http://www.settek.com Date: 1/7/2022
CLIENT: Synagro
Project: Oxford
WorkOrder Narrative:
21121829: This report in its entirety consists of the following documents: Cover Letter, Case Narrative,
Analytical Results, QC Summary Report, Applicable Accreditation Information, Chain -of -Custody,
Cooler Receipt Form, and other applicable forms as necessary. All documents contain the Summit
Environmental Technologies, Inc., Work Order Number assigned to this report.
Summit Environmental Technologies, Inc., holds the accreditations/certifications listed at the bottom of
the cover letter that may or may not pertain to this report. Please refer to the "Accreditation Program
Analytes Report" for accredited analytes list.
The information contained in this analytical report is the sole property of Summit Environmental
Technologies, Inc. and that of the customer. It cannot be reproduced in any form without the consent of
Summit Environmental Technologies, Inc. or the customer for which this report was issued. The results
contained in this report are only representative of the samples received. Conditions can vary at different
times and at different sampling conditions. Summit Environmental Technologies, Inc. is not responsible
for use or interpretation of the data included herein.
All results for Solid Samples are reported on an "as received" or "wet weight" basis unless indicated as
"dry weight" using the "-dry" designation on the reporting units.
This report is believed to meet all of the requirements of the accrediting agency, where applicable. Any
comments or problems with the analytical events associated with this report are noted below.
Analytical Sequence Sample Notes:
21121829-OOIA MTL-TCLP-7(6010D): LCS-54130 exhibits high recovery for Silver. Sample is ND
for this analyte.
21121829-OOIA TCLP-SVOC_8270E: Corresponding MS/MSD exhibited high RPD for
Hexachlorobutadiene and Hexachloroethane due to suspected sample inhomogeneity. Individual
MS/MSD percent recoveries are within acceptable criteria. Possible low bias for Pyridine due to low
recovery in LCS-54159.
Analytical Sequence QC Notes:
LCS-54130 Mtl-TCLP-7(6010): LCS-54130 exhibits high recovery for Silver. Associated samples are
ND for this analyte.
Original
Page 2 of 34

SUMMIY Summit Environmental Technologies, Inc. Case Narrative
3310 Win St.
ENVIRONMENTAL TEC„HQLOG4r;S,INC. Cuyahoga Falls, Ohio44223 Wo#: 21121829
Arralyi9cal Laboralorlas TEL: [phone] FAX.- [phone]
Wehsite: http://www.settek.com Date: 1/7/2022
CLIENT: Synagro
Project: Oxford
CCV 40ppm SVOC-MSTR S(8270): CCV exhibited low recoveries for several analytes. Possible low
bias in associated samples for these compounds. Analytes demonstrated adequate sensitivity in RLC.
MB-54159 SVOC-BNA_TCLP(8270): Possible low bias for Pyridine due to low recovery in LCS-
54159.
LCS-54159 SVOC-BNA_TCLP(8270): LCS-54159 exhibited low recovery for Pyridine. Possible low
bias in associated samples for this analyte.
21121829-OOIAMS/MSD TCLP-SVOC_8270E: MS/MSD exhibited high RPD for
Hexachlorobutadiene and Hexachloroethane due to suspected sample inhomogeneity. Individual
MS/MSD percent recoveries are within acceptable criteria. Possible low bias for Pyridine due to low
recovery in LCS-54159.
LCS-54135 TCLP-SV0C-CPEST_TCLP(8081): P: RPD between confirmation column is greater than
40%.
Original
Page 3 of 34

�� Summit Environmental Technologies, In Qualifiers and Acronyms
SU3310 Win S
Ekiwlt OMM@N-rALTECHN❑LOG{r,S,INC Cuyahoga Falls, Ohio442� WO#: 21121829
Arraly0cal Laboralorlas TEL: [phone] FAX.- (330) 253-446
Wehsite: httn:11www.settek.co Date: 1/7/2022
These commonly used Qualifiers and Acronyms may or may not be present in this report.
Qualifiers
U The compound was analyzed for but was not detected.
J The reported value is greater than the Method Detection Limit but less than the Reporting Limit.
H The hold time for sample preparation and/or analysis was exceeded.
D The result is reported from a dilution.
E The result exceeded the linear range of the calibration or is estimated due to interference.
MC The result is below the Minimum Compound Limit.
The result exceeds the Regulatory Limit or Maximum Contamination Limit.
in Manual integration was used to determine the area response.
d Manual integration in which peak was deleted
N The result is presumptive based on a Mass Spectral library search assuming a 1:1 response.
P The second column confirmation exceeded 25% difference.
C The result has been confirmed by GC/MS.
X The result was not confirmed when GC/MS Analysis was performed.
B/MB+ The analyte was detected in the associated blank.
G The ICB or CCB contained reportable amounts of analyte.
QC-/+ The CCV recovery failed low () or high (+).
R/QDR The RPD was outside of accepted recovery limits.
QL-/+ The LCS or LCSD recovery failed low () or high (+).
QLR The LCS/LCSD RPD was outside of accepted recovery limits.
QM-/+ The MS or MSD recovery failed low () or high (+).
QMR The MS/MSD RPD was outside of accepted recovery limits.
QV-/+ The ICV recovery failed low () or high (+).
S The spike result was outside of accepted recovery limits.
Z Deviation; A deviation from the method was performed; Please refer to the Case Narrative for
additional information
Acronyms
ND
Not Detected
RL
Reporting Limit
QC
Quality Control
MDL
Method Detection Limit
MB
Method Blank
LOD
Level of Detection
LCS
Laboratory Control Sample
LOQ
Level of Quantitation
LCSD
Laboratory Control Sample Duplicate
PQL
Practical Quantitation Limit
QCS
Quality Control Sample
CRQL
Contract Required Quantitation Limit
DUP
Duplicate
PL
Permit Limit
MS
Matrix Spike
RegLvl
Regulatory Limit
MSD
Matrix Spike Duplicate
MCL
Maximum Contamination Limit
RPD
Relative Percent Different
MinCL
Minimum Compound Limit
ICV
Initial Calibration Verification
RA
Reanalysis
ICB
Initial Calibration Blank
RE
Reextraction
CCV
Continuing Calibration Verification
TIC
Tentatively Identified Compound
CCB
Continuing Calibration Blank
RT
Retention Time
PLC
Reporting Limit Check
CF
Calibration Factor
DF
Dilution Factor
RF
Response Factor
This list of Qualifiers and Acronyms reflects the most commonly utilized Qualifiers and Acronyms for reporting.
Please refer to the Analytical Notes in the Case Narrative for any Qualifiers or Acronyms that do not appear in this
list or for additional information regarding the use of these Qualifiers on reported data.
Original
Page 4 of 34

MM' EF Summit Environmental Technologies, Inc. Workorder
SU3310 Win St.
ENVIR619MEWALTEe-HRpl,OGNUS,IPlC Cuyahoga Falls, Ohio44223 Sample Summary
Arraly0cal Laboralonor. TEL: [phone] FAX.- [phone] WO#: 21121829
Wehsite: http://www.settek.com 07-Jan-22
CLIENT: Synagro
Project: Oxford
Lab SampleID Client Sample ID Tag No Date Collected Date Received Matrix
21121829-001 Lagoon- Oxford 12/28/2021 12/29/2021 10:30:00 AM Solid
Page 5 of 34

SUMMIT
Summit Environmental Technologies, Inc.
3310 Win St.
DATES REPORT
ENVIRONMENTAL TECHN❑ L0G1E5, IrJG
Cuyahoga Falls, Ohio 44223
WO#: 21121829
ArWyft cal taboralonas
TEL: [phone] FAX.- [phone]
Wehsite: http://www.settek.com
07-Jan-22
Client:
Synagro
Proj ect:
Oxford
Sample ID
Client Sample ID Collection Date Matrix Test Name Leachate Date
Prep Date Analysis Date
21121829-OOIA Lagoon- Oxford 12/28/2021 Solid Ignitability of Solids (SW-846: 1030)
1/3/2022 11:54:57 AM
pH (SW9045D)
1/3/2022 12:57:48 PM
Reactive Cyanide (9014/7.3.32)-Solid
1/5/2022 2:13:00 PM
Reactive Sulfide (9034)/7.3.42
1/5/2022 2:13:00 PM
TCLP Herbicides by EPA 832113
1/6/2022 11:00:00 PM
TCLP Mercury Analysis (SW1311/7471/3/2022 4:00:00 PM
1/5/2022 10:15:00 AM 1/5/2022 4:23:00 PM
TCLP Metals Analysis (SW1311/6010:1/3/2022 4:00:00 PM
1/4/2022 12:30:24 PM 1/5/2022 10:15:00 AM
TCLP Pesticides Analysis (SW1311/8(1/3/2022 4:00:00 PM
1/4/2022 3:07:00 PM 1/5/2022 5:10:00 PM
TCLP Pesticides Analysis (SW1311/8(1/3/2022 4:00:00 PM
1/4/2022 3:07:00 PM 1/5/2022 5:10:00 PM
TCLP Semi-Volatiles Analysis 1/3/2022 4:00:00 PM
1/5/2022 11:46:00 AM 1/6/2022 4:12:00 PM
(SW1311/8270)
TCLP Volatiles Analysis
1/4/2022 3:48:00 PM
Original
Page 6 of 34

Summit Environmental Technologies, Inc.
SUMMIT 3310 Win St.
ENVITtONMENTALTECHNQLOGIE$,IRC Cuyahoga Falls, Ohio44223
Arralyt9cal Laboralorfas TEL: [phone] FAX. [phone]
Website: http://�i,-"-m,.settek.coin
Analytical Report
(base report)
WO#: 21121829
Date Reported: 1/7/2022
CLIENT: Synagro Tag Number:
Matrix: SOLID Collection Date: 12/28/2021
Lab ID: 21121829-OOIA
Project: Oxford
Client Sample ID Lagoon- Oxford
Analyses Result RL Qual Units DF Date Analyzed
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
TCLP MERCURY ANALYSIS (SW1311/7470)
TCLP Mercury
ND 0.00200 mg/L
SW7470A SW7470A Analyst: KLC
1 1/5/2022 4:23:00 PM
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
SW6010
SW301OA Analyst: MSK
TCLP METALS ANALYSIS (SW1311/6010)
TCLP Arsenic(As)
ND
0.500
mg/L
1
1/5/2022 10:15:00 AM
TCLP Barium(Ba)
ND
5.00
mg/L
1
1/5/2022 10:15:00 AM
TCLP Cadmium(Cd)
ND
0.100
mg/L
1
1/5/2022 10:15:00 AM
TCLP Chromium(Cr)
ND
0.200
mg/L
1
1/5/2022 10:15:00 AM
TCLP Lead(Pb)
ND
0.500
mg/L
1
1/5/2022 10:15:00 AM
TCLP Selenium(Se)
ND
0.0500
mg/L
1
1/5/2022 10:15:00 AM
TCLP Silver(Ag)
ND
0.500
QL+ mg/L
1
1/5/2022 10:15:00 AM
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
SW8270
SW351OC Analyst: SFG
TCLP SEMI-VOLATILES ANALYSIS (SW1311/8270)
1,4-Dichlorobenzene
ND
0.200
mg/L
2
1/6/2022 4:12:00 PM
2,4,5-Trichlorophenol
ND
0.500
mg/L
2
1/6/2022 4:12:00 PM
2,4,6-Trichlorophenol
ND
0.500
mg/L
2
1/6/2022 4:12:00 PM
2,4-Dinitrotoluene
ND
0.100
mg/L
2
1/6/2022 4:12:00 PM
Cresols, Total
ND
10.0
mg/L
2
1/6/2022 4:12:00 PM
Hexachloro-1,3-butadiene
ND
0.0400
QMR mg/L
2
1/6/2022 4:12:00 PM
Hexachlorobenzene
ND
0.100
mg/L
2
1/6/2022 4:12:00 PM
Hexachloroethane
ND
0.200
QMR mg/L
2
1/6/2022 4:12:00 PM
Nitrobenzene
ND
0.200
mg/L
2
1/6/2022 4:12:00 PM
Pentachlorophenol
ND
0.500
mg/L
2
1/6/2022 4:12:00 PM
Pyridine
ND
0.500
QL- mg/L
2
1/6/2022 4:12:00 PM
Surr: 2-Fluorophenol
71.2
10 - 157
%Rec
2
1/6/2022 4:12:00 PM
Surr: Phenol-d6
74.9
10 - 169
%Rec
2
1/6/2022 4:12:00 PM
Surr: Nitrobenzene-d5
68.3
32.1 - 130
%Rec
2
1/6/2022 4:12:00 PM
Surr: 2,4,6-Tribromophenol
75.3
45.4 - 166
%Rec
2
1/6/2022 4:12:00 PM
Surr: 2-Fluorobiphenyl
65.2
35.7 - 130
%Rec
2
1/6/2022 4:12:00 PM
Surr: p-Terphenyl-d14
98.8
70 - 145
%Rec
2
1/6/2022 4:12:00 PM
Qualifiers: B Analyte detected in the associated Method Blank
E Value above quantitation range
H Holding times for preparation or
analysis exceeded
M Manual Integration
used to determine area response
MC Value is below Minimum Compound
Limit.
N Tentatively identified compounds
ND Not Detected
OGI
P Second column confirmation exceeds
PL Permit Limit
Original
R RPD outside accepted recovery limits
RL Reporting Detection Limit
Page 7 of 34

Summit Environmental Technologies, Inc.
SU3310 Win St.
MMIT
Analytical Report
ENVI110NMENTAL1rECHNQL0GIE$,IRC
Cuyahoga Falls, Ohio44223
(base report)
Arrafyt9caf Laboralorfas TEL: (330)
253-8211 FAX. [phone]
WO#: 21121829
Website: http://www.settek.com
Date Reported: 1/7/2022
CLIENT: Synagro
Tag Number:
Matrix: SOLID
Collection Date:
12/28/2021
Lab ID: 21121829-OOIA
Project: Oxford
Client Sample ID Lagoon- Oxford
Analyses Result
RL
Qual Units
DF
Date Analyzed
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
SW8081
SW351OC Analyst: CSS
TCLP PESTICIDES ANALYSIS (SW1311/8081)
Chlordane, total ND
0.0250
mg/L
10
1/5/2022 5:10:00 PM
Toxaphene ND
0.0500
mg/L
10
1/5/2022 5:10:00 PM
Endrin ND
0.00500
mg/L
10
1/5/2022 5:10:00 PM
gamma-BHC ND
0.00500
mg/L
10
1/5/2022 5:10:00 PM
Heptachlor ND
0.00500
mg/L
10
1/5/2022 5:10:00 PM
Heptachlor epoxide ND
0.00500
mg/L
10
1/5/2022 5:10:00 PM
Methoxychlor ND
0.00500
mg/L
10
1/5/2022 5:10:00 PM
Surr: TCMX 73.2
10 - 119
%Rec
10
1/5/2022 5:10:00 PM
Surr: DCB 85.5
10 - 119
%Rec
10
1/5/2022 5:10:00 PM
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
SW8321
Analyst: RIS
TCLP HERBICIDES BY EPA 8321 B
2,4-D ND
0.500
mg/L
50
1/6/2022 11:00:00 PM
2,4,5-TP ND
0.500
mg/L
50
1/6/2022 11:00:00 PM
Surr: 2,4-Dichlorophenylacetic aci 99.2
70 - 130
%Rec
50
1/6/2022 11:00:00 PM
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
SW8260
SW1311M Analyst: NAW
TCLP VOLATILES ANALYSIS
1,1-Dichloroethene ND
0.500
mg/L
100
1/4/2022 3:48:00 PM
1,2-Dichloroethane ND
0.500
mg/L
100
1/4/2022 3:48:00 PM
MEK ND
10.0
mg/L
100
1/4/2022 3:48:00 PM
Benzene ND
0.500
mg/L
100
1/4/2022 3:48:00 PM
Carbon tetrachloride ND
0.500
mg/L
100
1/4/2022 3:48:00 PM
Chlorobenzene ND
5.00
mg/L
100
1/4/2022 3:48:00 PM
Chloroform ND
0.500
mg/L
100
1/4/2022 3:48:00 PM
Tetrachloroethene ND
0.500
mg/L
100
1/4/2022 3:48:00 PM
Trichloroethene ND
0.500
mg/L
100
1/4/2022 3:48:00 PM
Vinyl chloride ND
0.200
mg/L
100
1/4/2022 3:48:00 PM
Surr: 4-Bromofluorobenzene 98.9
70 - 130
%Rec
100
1/4/2022 3:48:00 PM
Surr: Di brom ofl uorom ethane 100
70 - 130
%Rec
100
1/4/2022 3:48:00 PM
Surr: Toluene-d8 99.9
70 - 130
%Rec
100
1/4/2022 3:48:00 PM
Qualifiers: B Analyte detected in the associated Method Blank
E Value above quantitation range
H Holding times for preparation or analysis exceeded
M Manual Integration
used to determine area response
MC Value is below Minimum Compound Limit.
N Tentatively identified compounds
ND Not Detected
OGI
P Second column confirmation exceeds
PL Permit Limit
Original
R RPD outside accepted recovery limits
RL Reporting Detection
Limit
Page 8 of 34

MMIT
Summit Environmental Technologies, Inc. Analytical Report
SU3310 Win St.
ENVIRONMENTAL TECHNQLOG4E$,IRC Cuyahoga Falls, Ohio44223 (base report)
Arrafyt9caf Laboralorfas TEL: [phone] FAX.- [phone] WO#: 21121829
Website: http://www.settek.com Date Reported: 1/7/2022
CLIENT: Synagro Tag Number:
Matrix: SOLID Collection Date: 12/28/2021
Lab ID: 21121829-OOIA
Project: Oxford
Client Sample ID Lagoon- Oxford
Analyses Result
RL Qual Units
DF
Date Analyzed
RCISOLID-W/ IGNITABILITY1030
SW9014
Analyst: MS
REACTIVE CYANIDE (9014/7.3.3.2)-SOLID
Cyanide, Reactive ND
0.495 mg/Kg
1
1/5/2022 2:13:00 PM
RCISOLID-W/ IGNITABILITY1030
SW1030
Analyst: ALT
IGNITABILITY OF SOLIDS (SW-846: 1030)
Ignitability nonflammable
mm/sec
1
1/3/2022 11:54:57 AM
RCISOLID-W/ IGNITABILITY1030
SW9045D
Analyst: ALT
PH (SW9045D)
pH 7.2
s.u.@19.1C
1
1/3/2022 12:57:48 PM
RCISOLID-W/ IGNITABILITY1030
SW9034
Analyst: MS
REACTIVE SULFIDE (9034)/7.3.4.2
Sulfide, Reactive ND
25.0 mg/Kg
1
1/5/2022 2:13:00 PM
Qualifiers: B
Analyte detected in the associated Method Blank
H
Holding times for preparation or analysis exceeded
MC
Value is below Minimum Compound Limit.
ND
Not Detected
P
Second column confirmation exceeds
R
RPD outside accepted recovery limits
E Value above quantitation range
M Manual Integration used to determine area response
N Tentatively identified compounds
OGl
PL Permit Limit Original
RL Reporting Detection Limit
Page 9 of 34

Summit Environmental Technologies, Inc.
Accreditation
Program
MM'EF
frSU3310 Win St.
Anal tes Report
Y
ENwIROMMEWALYECHNOL.OG{r,S,INC
Cuyahoga Falls, Ohio44223
Y
Arralytical Laboralorlas
TEL: [phone] FAX.- [phone]
WO#:
21121829
Wehsite: http://www.settek.com
07-Jan-22
Client: Synagro
State: NW
Project: Oxford
Program Name: NC_WW_SCM
Sample ID Matrix
Test Name
Analyte
Status
21121829-OOIA Solid
Ignitability of Solids (SW-846: 1030)
Ignitability
A
Solid
pH (SW9045D)
Hydrogen Ion (pH)
A
Solid
Reactive Cyanide (9014/7.3.32)-Solid
Cyanide, Reactive
U
Solid
Reactive Sulfide (9034)/7.3.42
Sulfide, Reactive
U
Solid
TCLP Herbicides by EPA 8321B
2,4,5-TP
A
Solid
TCLP Herbicides by EPA 8321B
2,4-D
A
Solid
TCLP Mercury Analysis (SW1311/7470)
Mercury
A
Solid
TCLP Metals Analysis (SW1311/6010)
Arsenic
A
Solid
TCLP Metals Analysis (SW1311/6010)
Barium
A
Solid
TCLP Metals Analysis (SW1311/6010)
Cadmium
A
Solid
TCLP Metals Analysis (SW1311/6010)
Chromium
A
Solid
TCLP Metals Analysis (SW1311/6010)
Lead
A
Solid
TCLP Metals Analysis (SW1311/6010)
Selenium
A
Solid
TCLP Metals Analysis (SW1311/6010)
Silver
A
Solid
TCLP Pesticides Analysis (SW1311/8081)
Chlordane, total
A
Solid
TCLP Pesticides Analysis (SW1311/8081)
Endrin
A
Solid
TCLP Pesticides Analysis (SW1311/8081)
gamma-BHC
A
Solid
TCLP Pesticides Analysis (SW1311/8081)
Heptachlor
A
Solid
TCLP Pesticides Analysis (SW1311/8081)
Heptachlor epoxide
A
Solid
TCLP Pesticides Analysis (SW1311/8081)
Methoxychlor
A
Solid
TCLP Pesticides Analysis (SW1311/8081)
Toxaphene
A
Solid
TCLP Semi-Volatiles Analysis (SW1311/8270)
1,4-Dichlorobenzene
A
Solid
TCLP Semi-Volatiles Analysis (SW1311/8270)
2,4,5-Trichlorophenol
A
Solid
TCLP Semi-Volatiles Analysis (SW1311/8270)
2,4,6-Trichlorophenol
A
Solid
TCLP Semi-Volatiles Analysis (SW1311/8270)
2,4-Dinitrotoluene
A
Solid
TCLP Semi-Volatiles Analysis (SW1311/8270)
Cresols, Total
A
Solid
TCLP Semi-Volatiles Analysis (SW1311/8270)
Hexachlorobenzene
A
Solid
TCLP Semi-Volatiles Analysis (SW1311/8270)
Hexachlorobutadiene
A
Solid
TCLP Semi-Volatiles Analysis (SW1311/8270)
Hexachloroethane
A
Solid
TCLP Semi-Volatiles Analysis (SW1311/8270)
Nitrobenzene
A
Solid
TCLP Semi-Volatiles Analysis (SW1311/8270)
Pentachlorophenol
A
Solid
TCLP Semi-Volatiles Analysis (SW1311/8270)
Pyridine
A
Original # 1
Page 10 of 34

Summit Environmental Technologies, Inc.
Accreditation
Program
MM'EF
frSU3310 Win St.
Anal tes Report
Y
ENVIROMMEWAL IrECHHOL,t
01ES, INC Cuyahoga Falls, Ohio 44223
Y
Arraly0cal Laboralorlas
TEL: [phone] FAX.- [phone]
WO#:
21121829
Wehsite: http://www.settek.com
07-Jan-22
Client: Synagro
State: NW
Project: Oxford
Program Name: NC_WW_SCM
Sample ID Matrix
Test Name
Analyte
Status
21121829-OOIA Solid
TCLP Volatiles Analysis
1,1-Dichloroethene
A
Solid
TCLP Volatiles Analysis
1,2-Dichloroethane
A
Solid
TCLP Volatiles Analysis
2-Butanone
A
Solid
TCLP Volatiles Analysis
Benzene
A
Solid
TCLP Volatiles Analysis
Carbon tetrachloride
A
Solid
TCLP Volatiles Analysis
Chlorobenzene
A
Solid
TCLP Volatiles Analysis
Chloroform
A
Solid
TCLP Volatiles Analysis
Tetrachloroethene
A
Solid
TCLP Volatiles Analysis
Trichloroethene
A
Solid
TCLP Volatiles Analysis
Vinyl chloride
A
Original # 1
Page 11 of 34

Summit Environmental Technologies, Inc.
SUMMIT 3310 Win St.
ENVIRONMEWAL rECHN❑ LQgir,-3, INCCuyahoga Falls, Ohio 44223
Arrafyt�cal iaboralorfas TEL: [phone] FAX.- [phone]
Website: http://`h,-"-m,.settek.com
QC SUMMARY REPORT
WO#: 21121829
07-Jan-22
Client: Synagro
Proj ect: Oxford BatchID: 54121
Sample ID: MB-54121
SampType: MBLK
TestCode: TCLP-VOC-M Units: mg/L
Prep Date:
RunNo: 138473
client ID: PBS
Batch ID: 54121
TestNo: SW8260 SW1311M
Analysis Date: 1/4/2022
SegNo: 3654619
analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
1,1-Dichloroethene
ND
0.500
1,2-Dichloroethane
ND
0.500
MEK
ND
10.0
Benzene
ND
0.500
Carbon tetrachloride
ND
0.500
Chlorobenzene
ND
5.00
Chloroform
ND
0.500
Tetrachloroethene
ND
0.500
Trichloroethene
ND
0.500
Vinyl chloride
ND
0.200
Surr: 4-Bromofluorobenzene
4910
Surr: Dibromofluoromethane
5030
Surr: Toluene-d8
5010
5000 98.1 70 130
5000 101 70 130
5000 100 70 130
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal)
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected OGl P Second column confirmation exceeds Original
PL Permit Limit R RPD outside accepted recovery limits RL Reporting Detection Limit
Page 12 of 34

Summit Environmental Technologies, Inc.
SUMMIT 3310 Win St.
ENVIRONMEWAL rECHN❑ LQgir,-3, INCCuyahoga Falls, Ohio 44223
Arrafyt�cal iaboralorfas TEL: [phone] FAX.- [phone]
Website: http://`h,-"-m,.settek.com
QC SUMMARY REPORT
WO#: 21121829
07-Jan-22
Client: Synagro
Proj ect: Oxford BatchID: 54121
Sample ID: 21121829-001AMS
SampType: MS
TestCode: TCLP-VOC-M Units: mg/L
Prep Date:
RunNo: 138473
Client ID: Lagoon- Oxford
Batch ID: 54121
TestNo: SW8260 SW1311M
Analysis Date: 1/4/2022
SegNo: 3654625
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
1,1-Dichloroethene
1.85
0.500
2.00
0
92.6
13.6
202
1,2-Dichloroethane
1.74
0.500
2.00
0
86.9
55.7
138
MEK
ND
10.0
10.0
0
96.9
65.3
118
Benzene
1.79
0.500
2.00
0
89.7
49.2
145
Carbon tetrachloride
1.82
0.500
2.00
0
90.9
26.7
156
Chlorobenzene
ND
5.00
2.00
0
89.7
33.7
159
Chloroform
1.80
0.500
2.00
0
90.2
48.5
145
Tetrachloroethene
1.76
0.500
2.00
0
87.8
19.2
191
Trichloroethene
1.74
0.500
2.00
0
87.1
38.4
167
Vinyl chloride
1.60
0.200
2.00
0
80.0
27.3
161
Surr:4-Bromofluorobenzene
5190
5000
104
91.7
109
Surr: Dibromofluoromethane
5000
5000
100
75.5
118
Surr: Toluene-d8
5000
5000
100
94.1
105
Sample ID: 21121829-001AMSD
SampType: MSD
TestCode: TCLP-VOC-M Units: mg/L
Prep Date:
RunNo: 138473
Client ID: Lagoon- Oxford
Batch ID: 54121
TestNo: SW8260 SW1311M
Analysis Date: 1/4/2022
SegNo: 3654626
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
1,1-Dichloroethene
1.86 0.500
2.00 0 93.1
13.6
202
1.85 0.539
25
1,2-Dichloroethane
1.78 0.500
2.00 0 88.9
55.7
138
1.74 2.33
25
MEK
ND 10.0
10.0 0 88.9
65.3
118
0 0
25
Benzene
1.82 0.500
2.00 0 90.9
49.2
145
1.79 1.33
25
Qualifiers: B
Analyte detected in the associated Method Blank
E
Value above quantitation range
H
Holding times for preparation or anal)
J
Analyte detected below quantitation limits
M
Manual Integration used to determine area
response
MC
Value is below Minimum Compound
Original
ND
Not Detected
OGI
P
Second column confirmation exceeds
PL
Permit Limit
R
RPD outside accepted recovery limits
RL
Reporting Detection Limit
Page 13 of 34

Summit Environmental Technologies, Inc.
SUMMIT 3310 Win St.
ENVIRONMEWAL rECHN❑ LQgir,_3, INCCuyahoga Falls, Ohio 44223
Arrafyt�cal iaboralorfas TEL: [phone] FAX. [phone]
Website: http://`h,-"-m,.settek.com
QC SUMMARY REPORT
WO#: 21121829
07-Jan-22
Client: Synagro
Proj ect: Oxford BatchID: 54121
Sample ID: 21121829-001AMSD
SampType: MSD
TestCode: TCLP-VOC-M Units: mg/L
Prep Date:
RunNo: 138473
client ID: Lagoon- Oxford
Batch ID: 54121
TestNo: SW8260 SW1311M
Analysis Date: 1/4/2022
SegNo: 3654626
analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
Carbon tetrachloride
1.81
0.500
2.00
0
90.6
26.7
156
1.82
0.331
25
Chlorobenzene
ND
5.00
2.00
0
90.9
33.7
159
0
0
25
Chloroform
1.83
0.500
2.00
0
91.3
48.5
145
1.80
1.16
25
Tetrachloroethene
1.77
0.500
2.00
0
88.6
19.2
191
1.76
0.851
25
Trichloroethene
1.79
0.500
2.00
0
89.3
38.4
167
1.74
2.55
25
Vinyl chloride
1.61
0.200
2.00
0
80.4
27.3
161
1.60
0.437
25
Surr:4-Bromofluorobenzene
5140
5000
103
91.7
109
0
25
Surr: Dibromofluoromethane
4960
5000
99.3
75.5
118
0
25
Surr: Toluene-d8
5020
5000
100
94.1
105
0
25
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal)
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected OGI P Second column confirmation exceeds Original
PL Permit Limit R RPD outside accepted recovery limits RL Reporting Detection Limit
Page 14 of 34

Summit Environmental Technologies, Inc.
SUMMIT 3310 Win St.
ENVIRONMEWAL rECHN❑ LQgir,-3, INCCuyahoga Falls, Ohio 44223
Arrafyt�cal iaboralorfas TEL: [phone] FAX.- [phone]
Website: http://`h,-"-m,.settek.com
QC SUMMARY REPORT
WO#: 21121829
07-Jan-22
Client: Synagro
Proj ect: Oxford BatchID: 54130
Sample ID: MB-54130
SampType: MBLK
TestCode: Mtl-TCLP-7(6 Units: mg/L
Prep Date: 1/4/2022
RunNo: 138477
Client ID: PBS
Batch ID: 54130
TestNo: SW6010 SW3010A
Analysis Date: 1/5/2022
SegNo: 3654836
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
TCLP Arsenic(As)
ND
0.500
TCLP Barium(Ba)
ND
5.00
TCLP Cadmium(Cd)
ND
0.100
TCLP Chromium(Cr)
ND
0.200
TCLP Lead(Pb)
ND
0.500
TCLP Selenium(Se)
ND
0.0500
TCLP Silver(Ag)
ND
0.500
Sample ID: LCS-54130
SampType: LCS
TestCode: Mtl-TCLP-7(6 Units: mg/L
Prep Date: 1/4/2022
RunNo: 138477
Client ID: LCSS
Batch ID: 54130
TestNo: SW6010 SW3010A
Analysis Date: 1/5/2022
SegNo: 3654837
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
TCLP Arsenic(As)
1.87
0.500
2.000
0
93.7
80
120
TCLP Barium(Ba)
ND
5.00
2.000
0
97.5
80
120
TCLP Cadmium(Cd)
1.96
0.100
2.000
0
98.0
80
120
TCLP Chromium(Cr)
1.99
0.200
2.000
0
99.6
80
120
TCLP Lead(Pb)
1.97
0.500
2.000
0
98.3
80
120
TCLP Selenium(Se)
1.90
0.0500
2.000
0
95.0
80
120
TCLP Silver(Ag)
2.41
0.500
2.000
0
120
80
120 S
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal)
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected OGI P Second column confirmation exceeds Original
PL Permit Limit R RPD outside accepted recovery limits RL Reporting Detection Limit
Page 15 of 34

MM'T Summit Environmental Technologies, Inc. QC SUMMARY REPORT
SU3310 Win St.
ENVIRONMEWAL rECHN❑ LQgir,-3, INCCuyahoga Falls, Ohio 44223 WO#: 21121829
Arrafyt�cal iaboralorfas TEL: [phone] FAX.- [phone]
Website: http://www.settek.com 07-Jan-22
Client: Synagro
Proj ect: Oxford BatchID: 54130
Sample ID: 22010028-001AMS
SampType: MS
TestCode: Mtl-TCLP-7(6 Units: mg/L
Prep Date: 1/4/2022
RunNo: 138477
Client ID: Batch=
Batch ID: 54130
TestNo: SW6010 SW3010A
Analysis Date: 1/5/2022
SegNo: 3654839
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
TCLP Arsenic(As)
1.86
0.500
2.000
0
93.1
70
130
TCLP Barium(Ba)
ND
5.00
2.000
2.987
101
70
130
TCLP Cadmium(Cd)
1.83
0.100
2.000
0.02550
90.3
70
130
TCLP Chromium(Cr)
1.89
0.200
2.000
0.05730
91.8
70
130
TCLP Lead(Pb)
1.80
0.500
2.000
0
90.2
70
130
TCLP Selenium(Se)
2.02
0.0500
2.000
0
101
70
130
TCLP Silver(Ag)
2.44
0.500
2.000
0
122
70
130 QL+
Sample ID: 22010028-001AMSD
SampType: MSD
TestCode: Mtl-TCLP-7(6 Units: mg/L
Prep Date: 1/4/2022
RunNo: 138477
Client ID: Batch=
Batch ID: 54130
TestNo: SW6010 SW3010A
Analysis Date: 1/5/2022
SegNo: 3654840
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
TCLP Arsenic(As)
1.90
0.500
2.000
0
94.9
70
130
1.862
1.93
20
TCLP Barium(Ba)
5.14
5.00
2.000
2.987
107
70
130
4.998
2.69
20
TCLP Cadmium(Cd)
1.83
0.100
2.000
0.02550
90.4
70
130
1.832
0.104
20
TCLP Chromium(Cr)
1.91
0.200
2.000
0.05730
92.5
70
130
1.893
0.768
20
TCLP Lead(Pb)
1.81
0.500
2.000
0
90.7
70
130
1.804
0.498
20
TCLP Selenium(Se)
2.05
0.0500
2.000
0
103
70
130
2.015
1.85
20
TCLP Silver(Ag)
2.47
0.500
2.000
0
123
70
130
2.439
1.20
20 QL+
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal)
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected OGl P Second column confirmation exceeds Original
PL Permit Limit R RPD outside accepted recovery limits RL Reporting Detection Limit
Page 16 of 34

MM'T Summit Environmental Technologies, Inc. QC SUMMARY REPORT
SU3310 Win St.
ENVIRONMEWAL rECHN❑ LQgir,-3, INCCuyahoga Falls, Ohio 44223 WO#: 21121829
Arrafyt�cal iaboralorfas TEL: [phone] FAX.- [phone]
Website: http://www.settek.com 07-Jan-22
Client: Synagro
Proj ect: Oxford BatchID: 54135
Sample ID: 21121937-001ams
SampType: MS
TestCode: TCLP-SVOC- Units: mg/L
Prep Date: 1/4/2022
RunNo: 138567
Client ID: Batch=
Batch ID: 54135
TestNo: SW8081 SW3510C
Analysis Date: 1/5/2022
SegNo: 3657280
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Chlordane, total
ND
0.0250
0.0200
0
65.6
70
130 S
Endrin
0.00676
0.00500
0.0100
0
67.6
10
224
gamma-BHC
0.00639
0.00500
0.0100
0
63.9
10
192
Heptachlor
0.00636
0.00500
0.0100
0
63.6
10
197
Heptachlor epoxide
0.00664
0.00500
0.0100
0
66.4
10
208
Methoxychlor
0.00652
0.00500
0.0100
0
65.2
10
251
Surr: TCMX
11.4
20.00
56.8
10
157
Surr: DCB
14.1
20.00
70.7
10
194
Sample ID: 21121937-001amsd
SampType: MSD
TestCode: TCLP-SVOC- Units: mg/L
Prep Date: 1/4/2022
RunNo: 138567
Client ID: Batch=
Batch ID: 54135
TestNo: SW8081 SW3510C
Analysis Date: 1/5/2022
SegNo: 3657281
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Chlordane, total
ND
0.0250
0.0200
0
86.5
70
130
0
0
30
Endrin
0.00903
0.00500
0.0100
0
90.3
10
224
0.00676
28.8
30
gamma-BHC
0.00812
0.00500
0.0100
0
81.2
10
192
0.00639
23.8
30
Heptachlor
0.00770
0.00500
0.0100
0
77.0
10
197
0.00636
19.1
30
Heptachlor epoxide
0.00858
0.00500
0.0100
0
85.8
10
208
0.00664
25.5
30
Methoxychlor
0.00831
0.00500
0.0100
0
83.1
10
251
0.00652
24.1
30
Surr: TCMX
13.5
20.00
67.3
10
157
0
Surr: DCB
16.6
20.00
82.8
10
194
0
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal)
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected OGI P Second column confirmation exceeds Original
PL Permit Limit R RPD outside accepted recovery limits RL Reporting Detection Limit
Page 17 of 34

Summit Environmental Technologies, Inc.
SUMMIT 3310 Win St.
ENVIRONMEWAL rECHN❑ LQgir,_3, INCCuyahoga Falls, Ohio 44223
Arrafyt�cal iaboralorfas TEL: [phone] FAX. [phone]
Website: http://`h,-"-m,.settek.com
QC SUMMARY REPORT
WO#: 21121829
07-Jan-22
Client: Synagro
Proj ect: Oxford BatchID: 54159
Sample ID: 21121829-001AMS
SampType: MS
TestCode: TCLP-SVOC_ Units: mg/L
Prep Date: 1/5/2022
RunNo: 138561
client ID: Lagoon- Oxford
Batch ID: 54159
TestNo: SW8270 SW3510C
Analysis Date: 1/6/2022
SegNo: 3658451
analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
1,4-Dichlorobenzene
0.437
0.200
0.8000
0
54.6
15.2
124
2,4,5-Trichlorophenol
0.628
0.500
0.8000
0
78.6
30.6
152
2,4,6-Trichlorophenol
0.609
0.500
0.8000
0
76.1
27.6
150
2,4-Dinitrotoluene
0.700
0.100
0.8000
0
87.5
58
141
o-Cresol
0.570
0.500
0.8000
0
71.3
26.9
132
Cresols, Total
ND
10.0
1.600
0
74.4
27.6
132
Hexachloro-1,3-butadiene
0.431
0.0400
0.8000
0
53.8
10
156
Hexachlorobenzene
0.685
0.100
0.8000
0
85.7
54.3
142
Hexachloroethane
0.423
0.200
0.8000
0
52.8
1.92
131
Nitrobenzene
0.622
0.200
0.8000
0
77.8
21
135
Pentachlorophenol
0.678
0.500
0.8000
0
84.7
47.4
134
Pyridine
ND
0.500
0.8000
0
21.2
10
130
Surr:2-Fluorophenol
0.659
1.000
65.9
9.77
146
Surr: Phenol-d6
0.746
1.000
74.6
20.7
130
Surr: Nitrobenzene-d5
0.629
1.000
62.9
13.9
156
Surr: 2,4,6-Tribromophenol
0.901
1.000
90.1
27.3
183
Surr:2-Fluorobiphenyl
0.698
1.000
69.8
21.4
153
Surr: p-Terphenyl-d14
1.08
1.000
108
54.8
154
QMR
QMR
m, QL-
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal)
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected OGl P Second column confirmation exceeds Original
PL Permit Limit R RPD outside accepted recovery limits RL Reporting Detection Limit
Page 18 of 34

Summit Environmental Technologies, Inc.
SUMMIT 3310 Win St.
ENVIRONMEWAL rECHN❑ LQgir,-3, INCCuyahoga Falls, Ohio 44223
Arrafyt�cal iaboralorfas TEL: [phone] FAX.- [phone]
Website: http://`h,-"-m,.settek.com
QC SUMMARY REPORT
Client: Synagro
Proj ect: Oxford BatchID: 54159
WO#: 21121829
07-Jan-22
Sample ID: 21121829-001AMSD
SampType: MSD
TestCode: TCLP-SVOC_ Units: mg/L
Prep Date: 1/5/2022
RunNo: 138561
Dient ID: Lagoon- Oxford
Batch ID: 54159
TestNo: SW8270 SW3510C
Analysis Date: 1/6/2022
SegNo: 3658452
4nalyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
1,4-Dichlorobenzene
0.572
0.200
0.8000
0
71.5
15.2
124
0.4368
26.7
30
2,4,5-Trichlorophenol
0.776
0.500
0.8000
0
97.0
30.6
152
0.6284
21.0
30
2,4,6-Trichlorophenol
0.778
0.500
0.8000
0
97.3
27.6
150
0.6088
24.5
30
2,4-Dinitrotoluene
0.829
0.100
0.8000
0
104
58
141
0.7000
16.9
30
o-Cresol
0.727
0.500
0.8000
0
90.9
26.9
132
0.5704
24.1
30
Cresols, Total
ND
10.0
1.600
0
94.2
27.6
132
0
0
30
Hexachloro-1,3-butadiene
0.590
0.0400
0.8000
0
73.7
10
156
0.4308
31.1
30 R
Hexachlorobenzene
0.790
0.100
0.8000
0
98.7
54.3
142
0.6852
14.2
30
Hexachloroethane
0.573
0.200
0.8000
0
71.6
1.92
131
0.4228
30.1
30 R
Nitrobenzene
0.746
0.200
0.8000
0
93.2
21
135
0.6220
18.1
30
Pentachlorophenol
0.818
0.500
0.8000
0
102
47.4
134
0.6776
18.8
30
Pyridine
ND
0.500
0.8000
0
20.4
10
130
0
0
30 m,QL-
Surr:2-Fluorophenol
0.816
1.000
81.6
9.77
146
0
Surr: Phenol-d6
0.946
1.000
94.6
20.7
130
0
Surr: Nitrobenzene-d5
0.872
1.000
87.2
13.9
156
0
Surr:2,4,6-Tribromophenol
1.18
1.000
118
27.3
183
0
Surr:2-Fluorobiphenyl
0.862
1.000
86.2
21.4
153
0
Surr: p-Terphenyl-d14
1.27
1.000
127
54.8
154
0
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal)
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected OGl P Second column confirmation exceeds Original
PL Permit Limit R RPD outside accepted recovery limits RL Reporting Detection Limit
Page 19 of 34

Summit Environmental Technologies, Inc.
SUMMIT 3310 Win St.
ENVIRONMEWAL rECHN❑ LQgir,-3, INCCuyahoga Falls, Ohio 44223
Arrafyt�cal iaboralorfas TEL: [phone] FAX.- [phone]
Website: http://`h,-"-m,.settek.com
QC SUMMARY REPORT
WO#: 21121829
07-Jan-22
Client: Synagro
Proj ect: Oxford BatchID: 54159
Sample ID: MB-54159
SampType: MBLK
TestCode: SVOC-BNA_T Units: mg/L
Prep Date: 1/5/2022
RunNo: 138561
client ID: PBS
Batch ID: 54159
TestNo: SW8270 SW3510C
Analysis Date: 1/6/2022
SegNo: 3656928
analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
1,4-Dichlorobenzene
ND
0.100
2,4,5-Trichlorophenol
ND
0.250
2,4,6-Trichlorophenol
ND
0.250
2,4-Dinitrotoluene
ND
0.0500
o-Cresol
ND
0.250
Cresols, Total
ND
5.00
Hexachloro-1,3-butadiene
ND
0.0200
Hexachlorobenzene
ND
0.0500
Hexachloroethane
ND
0.100
Nitrobenzene
ND
0.100
Pentachlorophenol
ND
0.250
Pyridine
ND
0.250
Surr: 2-Fluorophenol
0.621
Surr: Phenol-d6
0.678
Surr: Nitrobenzene-d5
0.605
Surr: 2,4,6-Tribromophenol
0.812
Surr: 2-Fluorobiphenyl
0.659
Surr: p-Terphenyl-d14
1.06
1.000
62.1
10
135
1.000
67.8
10
161
1.000
60.5
16.8
150
1.000
81.2
32.5
179
1.000
65.9
34
133
1.000
106
60.8
163
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal)
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected OGI P Second column confirmation exceeds Original
PL Permit Limit R RPD outside accepted recovery limits RL Reporting Detection Limit
Page 20 of 34

Summit Environmental Technologies, Inc.
SUMMIT 3310 Win St.
ENVIRONMEWAL rECHN❑ LQgir,-3, INCCuyahoga Falls, Ohio 44223
Arrafyt�cal iaboralorfas TEL: [phone] FAX.- [phone]
Website: http://`h,-"-m,.settek.com
QC SUMMARY REPORT
WO#: 21121829
07-Jan-22
Client: Synagro
Proj ect: Oxford BatchID: 54159
Sample ID: LCS-54159
SampType: LCS
TestCode: SVOC-BNA_T Units: mg/L
Prep Date: 1/5/2022
RunNo: 138561
client ID: LCSS
Batch ID: 54159
TestNo: SW8270 SW3510C
Analysis Date: 1/6/2022
SegNo: 3656929
analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
1,4-Dichlorobenzene
0.411
0.100
0.8000
0
51.4
46
130
2,4,5-Trichlorophenol
0.665
0.250
0.8000
0
83.1
62.5
131
2,4,6-Trichlorophenol
0.646
0.250
0.8000
0
80.8
57.9
136
2,4-Dinitrotoluene
0.674
0.0500
0.8000
0
84.2
69.4
132
o-Cresol
0.581
0.250
0.8000
0
72.6
55.9
130
Cresols, Total
ND
5.00
1.600
0
73.9
57.9
ill
Hexachloro-1,3-butadiene
0.472
0.0200
0.8000
0
59.0
38.3
130
Hexachlorobenzene
0.679
0.0500
0.8000
0
84.8
69.1
130
Hexachloroethane
0.422
0.100
0.8000
0
52.7
36.3
130
Nitrobenzene
0.572
0.100
0.8000
0
71.5
52.1
130
Pentachlorophenol
0.644
0.250
0.8000
0
80.5
60.9
133
Pyridine
ND
0.250
0.8000
0
4.38
10
130
Surr: 2-Fluorophenol
0.694
1.000
69.4
10
135
Surr: Phenol-d6
0.830
1.000
83.0
10
161
Surr: Nitrobenzene-d5
0.735
1.000
73.5
16.8
150
Surr:2,4,6-Tribromophenol
1.09
1.000
109
32.5
179
Surr:2-Fluorobiphenyl
0.835
1.000
83.5
34
133
Surr: p-Terphenyl-dl4
1.16
1.000
116
60.8
163
m
S
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal)
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected OGl P Second column confirmation exceeds Original
PL Permit Limit R RPD outside accepted recovery limits RL Reporting Detection Limit
Page 21 of 34

SUMM'T
Summit Environmental Technologies, Inc.
3310 Win St.
QC SUMMARY REPORT
ENVIRONMEWAL rECHN❑ Lggir,-3, INCCuyahoga
Falls, Ohio 44223
WO#: 21121829
Arrafyt�cal iaboralorfas
TEL: [phone] FAX.- [phone]
Website: http://www.settek.com
07-Jan-22
Client:
Synagro
Proj ect:
Oxford
BatchID: 54160
TCLP Mercury ND 0.00200
TCLP Mercury 0.00421 0.00200 0.00400 0 105 80 120
Sample ID: 22010019-005AMS
SampType: MS
TestCode: HG_TCLP(74 Units: PPM
Prep Date: 1/5/2022
RunNo: 138509
Client ID: Batch=
Batch ID: 54160
TestNo: SW7470A SW7470A
Analysis Date: 1/5/2022
SegNo: 3655919
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
TCLP Mercury
0.00452 0.00200 0.00400 0 113 75 125
Qualifiers: B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
PL Permit Limit
E Value above quantitation range H Holding times for preparation or anal)
M Manual Integration used to determine area response MC Value is below Minimum Compound
OGI P Second column confirmation exceeds
R RPD outside accepted recovery limits RL Reporting Detection Limit
Original
Page 22 of 34

Summit Environmental Technologies, Inc.
SUMMIT 3310 Win St.
ENVIRONMEWAL rECHN❑ Lggir,-3, INCCuyahoga Falls, Ohio 44223
Arrafyt�cal iaboralorfas TEL: [phone] FAX.- [phone]
Website: http://`h,-"-m,.settek.com
QC SUMMARY REPORT
WO#: 21121829
07-Jan-22
Client: Synagro
Project: Oxford BatchID: R138381
Sample ID: LCS-R138381
SampType: LCS
TestCode: Ignitability_S Units: mm/sec
Prep Date:
RunNo: 138381
Client ID: LCSS
Batch ID: R138381
TestNo: SW1030
Analysis Date: 1/3/2022
SegNo: 3652816
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
Ignitability
8.56
7.240 0 118 70 130
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal)
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected OGl P Second column confirmation exceeds Original
PL Permit Limit R RPD outside accepted recovery limits RL Reporting Detection Limit
Page 23 of 34

Summit Environmental Technologies, Inc.
SUMMIT 3310 Win St.
ENVIRONMEWAL rECHN❑ LQgir,-3, INCCuyahoga Falls, Ohio 44223
Arrafyt�cal iaboralorfas TEL: [phone] FAX.- [phone]
Website: http://`h,-"-m,.settek.com
QC SUMMARY REPORT
WO#: 21121829
07-Jan-22
Client: Synagro
Project: Oxford BatchID: R138384
Sample ID: LCS-R138384
SampType: LCS
TestCode: pH_Oil(9045D Units: s.u.@19.2C
Prep Date:
RunNo: 138384
Client ID: LCSW
Batch ID: R138384
TestNo: SW9045D
Analysis Date: 1/3/2022
SegNo: 3652889
Analyte
Result
PQL SPK value SPK Ref Val %REC
Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
pH
7.0
7.0 0 101 90 110
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal)
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected OGl P Second column confirmation exceeds Original
PL Permit Limit R RPD outside accepted recovery limits RL Reporting Detection Limit
Page 24 of 34

MM'T Summit Environmental Technologies, Inc. QC SUMMARY REPORT
SU3310 Win St.
ENVIRONMEWAL rECHN❑ Lggir,-3, INCCuyahoga Falls, Ohio 44223 WO#: 21121829
Arrafyt�cal iaboralorfas TEL: [phone] FAX.- [phone]
Website: http://www.settek.com 07-Jan-22
Client: Synagro
Project: Oxford BatchID: R138384
Sample ID: LCS-R138384
SampType: LCS
TestCode: pH_DW(4500- Units: s.u.@19.1C
Prep Date:
RunNo: 138384
Client ID: LCSW
Batch ID: R138384
TestNo: SW9045D
Analysis Date: 1/3/2022
SegNo: 3652878
Analyte
Result
PQL SPK value SPK Ref Val %REC
Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
pH 7.0 7.0 0 101 98.6 101.4
Sample ID: 21121677-001ADUP
SampType: DUP
TestCode: pH_DW(4500- Units: s.u.@19.6C
Prep Date:
RunNo: 138384
Client ID: Batch=
Batch ID: R138384
TestNo: SW9045D
Analysis Date: 1/3/2022
SegNo: 3652880
Analyte
Result
PQL SPK value SPK Ref Val %REC
Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
pH 7.8
Qualifiers: B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
PL Permit Limit
7.8 0.3 5 H
E Value above quantitation range H Holding times for preparation or anal)
M Manual Integration used to determine area response MC Value is below Minimum Compound
OGI P Second column confirmation exceeds
R RPD outside accepted recovery limits RL Reporting Detection Limit
Original
Page 25 of 34

MM'T Summit Environmental Technologies, Inc. QC SUMMARY REPORT
SU3310 Win St.
ENVIRONMEWAL rECHN❑ LQgir,-3, INCCuyahoga Falls, Ohio 44223 WO#: 21121829
Arrafyt�cal iaboralorfas TEL: [phone] FAX.- [phone]
Website: http://www.settek.com 07-Jan-22
Client: Synagro
Project: Oxford BatchID: R138423
Sample ID: LCS
SampType: LCS
TestCode: VOC-MSTR_ Units: %Rec
Prep Date:
RunNo: 138423
Client ID: LCSW
Batch ID: R138423
TestNo: SW8260
Analysis Date: 1/3/2022
SegNo: 3653693
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Surr: 4-Bromofluorobenzene
50.5
50.00
101
70
130
Surr: Dibromofluoromethane
49.8
50.00
99.7
70
130
Surr: Toluene-d8
50.0
50.00
100
70
130
Sample ID: MB
SampType: MBLK
TestCode: VOC-MSTR_ Units: %Rec
Prep Date:
RunNo: 138423
Client ID: PBW
Batch ID: R138423
TestNo: SW8260
Analysis Date: 1/3/2022
SegNo: 3653694
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Surr:4-Bromofluorobenzene 48.5 50.00 97.0 70 130
Surr: Dibromofluoromethane 49.6 50.00 99.3 70 130
Surr: Toluene-d8 49.9 50.00 99.9 70 130
Qualifiers: B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
PL Permit Limit
E Value above quantitation range H Holding times for preparation or anal)
M Manual Integration used to determine area response MC Value is below Minimum Compound
OGl P Second column confirmation exceeds
R RPD outside accepted recovery limits RL Reporting Detection Limit
Original
Page 26 of 34

SUMM'T
Summit Environmental Technologies, Inc.
3310 Win St.
QC SUMMARY REPORT
ENVIRONMEWAL rECHN❑ LQgir,-3, INCCuyahoga
Falls, Ohio 44223
WO#: 21121829
Arrafyt�cal iaboralorfas
TEL: [phone] FAX.- [phone]
Website: http://www.settek.com
07-Jan-22
Client:
Synagro
Project:
Oxford
BatchID: R138520
Sulfide, Reactive ND 25.0
Sulfide, Reactive 2080 25.0 2210 0 94.1 85 115
Sulfide, Reactive 2170 25.0 2210 0 98.2 80 120
Sample ID: 21121829-001AMSD
SampType: MSD
TestCode: Sulfide,React Units: mg/Kg
Prep Date:
RunNo: 138520
Client ID: Lagoon- Oxford
Batch ID: R138520
TestNo: SW9034
Analysis Date: 1/5/2022
SegNo: 3655854
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
Sulfide, Reactive
2110 25.0
2210 0 95.5 80
120
2170 2.80 30
Qualifiers: B
Analyte detected in the associated Method Blank
E
Value above quantitation range
H
Holding times for preparation or anal)
J
Analyte detected below quantitation limits
M
Manual Integration used to determine area response
MC
Value is below Minimum Compound
Original
ND
Not Detected
OGI
P
Second column confirmation exceeds
PL
Permit Limit
R
RPD outside accepted recovery limits
RL
Reporting Detection Limit
Page 27 of 34

Summit Environmental Technologies, Inc.
SUMMIT 3310 Win St.
ENVIRONMEWAL rECHN❑ Lggir,-3, INCCuyahoga Falls, Ohio 44223
Arrafyt�cal iaboralorfas TEL: [phone] FAX.- [phone]
Website: http://`h,-"-m,.settek.com
QC SUMMARY REPORT
WO#: 21121829
07-Jan-22
Client: Synagro
Project: Oxford BatchID: R138520
Sample ID: 21121829-001AMSD
SampType: MSD
TestCode: Sulfide,React Units: mg/Kg
Prep Date:
RunNo: 138520
Dient ID: Lagoon- Oxford
Batch ID: R138520
TestNo: SW9034
Analysis Date: 1/5/2022
SegNo: 3655854
4nalyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal)
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected OGl P Second column confirmation exceeds Original
PL Permit Limit R RPD outside accepted recovery limits RL Reporting Detection Limit
Page 28 of 34

SUMM'T
Summit Environmental Technologies, Inc.
3310 Win St.
QC SUMMARY REPORT
ENVIRONMEWAL rECHN❑ LQgir,-3, INCCuyahoga
Falls, Ohio 44223
WO#: 21121829
Arrafyt�cal iaboralorfas
TEL: [phone] FAX.- [phone]
Website: http://www.settek.com
07-Jan-22
Client:
Synagro
Project:
Oxford
BatchID: R138543
Cyanide, Reactive ND 0.490
Cyanide, Reactive 10.4 0.490 10.00 0 104 85 115
Cyanide, Reactive ND 0.490 0.5000 0 57.8 50 150
Sample ID: 21121829-001AMS
SampType: MS
TestCode: Cyanide,Rea Units: mg/Kg
Prep Date:
RunNo: 138543
Client ID: Lagoon- Oxford
Batch ID: R138543
TestNo: SW9014
Analysis Date: 1/5/2022
SegNo: 3656339
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
Cyanide, Reactive
10.2 0.490
10.00 0 102 75
125
Qualifiers: B
Analyte detected in the associated Method Blank
E Value above quantitation range
H
Holding times for preparation or anal)
J
Analyte detected below quantitation limits
M Manual Integration used to determine area response
MC
Value is below Minimum Compound
Original
ND
Not Detected
OGI
P
Second column confirmation exceeds
PL
Permit Limit
R RPD outside accepted recovery limits
RL
Reporting Detection Limit
Page 29 of 34

MM'T Summit Environmental Technologies, Inc. QC SUMMARY REPORT
SU3310 Win St.
ENVIRONMEWAL rECHN❑ LQgir,-3, INCCuyahoga Falls, Ohio 44223 WO#: 21121829
Arrafyt�cal iaboralorfas TEL: [phone] FAX.- [phone]
Website: http://www.settek.com 07-Jan-22
Client: Synagro
Project: Oxford BatchID: R138543
Sample ID: 21121829-001AMS
SampType: MS
TestCode: Cyanide,Rea Units: mg/Kg
Prep Date:
RunNo: 138543
Client ID: Lagoon- Oxford
Batch ID: R138543
TestNo: SW9014
Analysis Date: 1/5/2022
SegNo: 3656339
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Sample ID: 21121829-001AMSD
SampType: MSD
TestCode: Cyanide,Rea Units: mg/Kg
Prep Date:
RunNo: 138543
Client ID: Lagoon- Oxford
Batch ID: R138543
TestNo: SW9014
Analysis Date: 1/5/2022
SegNo: 3656342
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Cyanide, Reactive 10.2 0.485 10.00 0 102 75 125 10.24 0.649 10
Qualifiers: B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
PL Permit Limit
E Value above quantitation range H Holding times for preparation or anal)
M Manual Integration used to determine area response MC Value is below Minimum Compound
OGl P Second column confirmation exceeds
R RPD outside accepted recovery limits RL Reporting Detection Limit
Original
Page 30 of 34

SUMM'T
Summit Environmental Technologies, Inc.
3310 Win St.
QC SUMMARY REPORT
ENVIRONMEWAL rECHN❑ LQgir,-3, INCCuyahoga
Falls, Ohio 44223
WO#: 21121829
Arrafyt�cal iaboralorfas
TEL: [phone] FAX.- [phone]
Website: http://www.settek.com
07-Jan-22
Client:
Synagro
Project:
Oxford
BatchID: R138608
2,4-D ND 0.0100
2,4,5-TP ND 0.0100
Surr: 2,4-Dichlorophenylacetic acid 0.970 1.000 97.0 70 130
2,4-D
0.294
0.0100 0.3000
0 98.1
60.5
141
2,4,5-TP
0.274
0.0100 0.3000
0 91.3
68.3
144
Surr: 2,4-Dichlorophenylacetic acid
2.66
3.000
88.8
70
130
Sample ID: 21121829-001AMS
SampType: MS
TestCode: TCLP-SVOC- Units: mg/L
Prep Date:
RunNo: 138608
Client ID: Lagoon- Oxford
Batch ID: R138608
TestNo: SW8321
Analysis Date: 1/6/2022
SegNo: 3658402
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
2,4-D
15.2 0.500
15.00 0 101 60.5
141
2,4,5-TP
14.4 0.500
15.00 0 96.3 68.3
144
Surr: 2,4-Dichlorophenylacetic acid 137
150.0 91.6 70
130
Qualifiers: B
Analyte detected in the associated Method Blank
E
Value above quantitation range
H
Holding times for preparation or anal)
J
Analyte detected below quantitation limits
M
Manual Integration used to determine area response
MC
Value is below Minimum Compound
Original
ND
Not Detected
OGI
P
Second column confirmation exceeds
PL
Permit Limit
R
RPD outside accepted recovery limits
RL
Reporting Detection Limit
Page 31 of 34

MM'T Summit Environmental Technologies, Inc. QC SUMMARY REPORT
SU3310 Win St.
ENVIRONMEWAL rECHN❑ LQgir,-3, INCCuyahoga Falls, Ohio 44223 WO#: 21121829
Arrafyt�cal iaboralorfas TEL: [phone] FAX.- [phone]
Website: http://www.settek.com 07-Jan-22
Client: Synagro
Project: Oxford BatchID: R138608
Sample ID: 21121829-001AMSD
SampType: MSD
TestCode: TCLP-SVOC- Units: mg/L
Prep Date:
RunNo: 138608
Client ID: Lagoon- Oxford
Batch ID: R138608
TestNo: SW8321
Analysis Date: 1/7/2022
SegNo: 3658403
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
2,4-D 14.4 0.500 15.00 0 96.1 60.5 141 15.16 5.04 30
2,4,5-TP 13.6 0.500 15.00 0 90.7 68.3 144 14.44 5.92 30
Surr: 2,4-Dichlorophenylacetic acid 131 150.0 87.3 70 130 0 0
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal)
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected OGI P Second column confirmation exceeds Original
PL Permit Limit R RPD outside accepted recovery limits RL Reporting Detection Limit
Page 32 of 34

�� � � Summit Environmental Technologies, Inc.
SU3310 Win St.
ENVIRONMENTAL TECHNOLOQH�S.IfiC Cuyahoga Falls, Ohio44223 Sample Log -In Check List
Arrafocaf Laboralorias TEL: [phone] FAX.- [phone]
Website: http://`h,,",m,.settek.com
Client Name: SYN-NC-27028 Work Order Number: 21121829 RcptNo: 1
Logged by: Christina N. Jager
Completed By: Jacqueline Rasile
Reviewed By: Jennifer Woolf
12/29/2021 10:30:00 AM
12/29/2021 2:29:21 PM
12/29/2021 6:07:51 PM
Chain of Custody
1. Is Chain of Custody complete? Yes ❑ No ❑d Not Present ❑
2. How was the sample delivered? FedEx
Lop In
3. Coolers are present? Yes ❑d No ❑ NA ❑
4. Shipping container/cooler in good condition? Yes d❑ No ❑
Custody seals intact on shipping container/cooler? Yes ❑ No ❑ Not Present V
No. Seal Date: Signed By:
5. Was an attempt made to cool the samples? Yes ❑d No ❑ NA ❑
6. Were all samples received at a temperature of >0° C to 6.0°C Yes ❑d No ❑ NA ❑
7. Sample(s) in proper container(s)? Yes ❑d No ❑
8. Sufficient sample volume for indicated test(s)? Yes ❑d No ❑
9. Are samples (except VOA and ONG) properly preserved? Yes ❑d No ❑
10. Was preservative added to bottles? Yes ❑ No ❑d NA ❑
11. Is the headspace in the VOA vials less than 1/4 inch or 6 mm?
Yes
❑
No ❑ No VOA Vials ❑�
12. Were any sample containers received broken?
Yes
❑
No ❑d
13. Does paperwork match bottle labels?
Yes
No ❑
(Note discrepancies on chain of custody)
14. Are matrices correctly identified on Chain of Custody?
Yes
❑d
No ❑
15. Is it clear what analyses were requested?
Yes
❑d
No ❑
16. Were all holding times able to be met?
Yes
No ❑
(If no, notify customer for authorization.)
Special Handling (if applicable)
17. Was client notified of all discrepancies with this order?
Yes
❑
No ❑ NA V
Person Notified: Date:
By Whom: Via: ❑ eMail ❑ Phone ❑ Fax ❑ In Person
Regarding:
Client Instructions:
18. Additional remarks:
NC per email
project address not included
Cooler Information
Cooler No
Temp °C
Condition
I Seal Intact
Seal No
Seal Date
Signed By
1
10.6
Goodl
Not Present
Page 34 of 34

SECTION 5

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Oxford WWTP WQ Permit Number: WQ0011244
WWTP Name: Oxford WWTP NPDES Number: NCO025054
Monitoring Period: From 1/1/2023 To 3/31/2023
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. 1/A (time/temp) Alt. 2/13 (Alk Treatment) Alt. 3/C (Prior Testing)
Alt. 4/D (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic
Beta Ray Gamma Ray Pasteurization
Class B:
Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying Composting Aerobic Digestion
Anaerobic Digestion
If annlieahle to alternative performed (Class A or Class B) comnlete the following monitoring data:
Parameter
Allowable Level in Sludge
Pathogen Density
No. of
Frequency
Sample
Analytical
Excee-
of
Type
Technique
Minimum Geo. Mean Maximum Units
dences
Analysis
Fecal
2x 10 to the 61h
MPN
MPN/g
Coliform
power per gram
of total solids
5,091
6,671
7,729
CFU/g
0
4 /Yr
grab
SM9222D
CFU
1000 MPN per gram of
MPN/g
total solids (dry weight)
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed:
0 tion/Alt. 1
Option/Alt.2
Option/Alt. 3
Option/Alt.4
(V S reduction)
(40-day bench)
(30-day bench) X
(Spec. 02 uptake)
Option/Alt. 5
Option/Alt. 6
Option/Alt. 7
Option/Alt. 8
(I 4-Day Aerobic)
(Alk Stabilization)
(Drying — Stable)
(Drying — Unstable)
Option/Alt. 9
Option/Alt. 10
(Injection)
(Incorporation)
No vector attraction reduction alternatives
were performed
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met."
"I certify, under penalty of law, that the ppathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an
_ explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified
personnel properly gather and evaluate the information used to deterniine that the pathogen and vector attraction reduction requirements have
been met. I am aware that there are significant penalties for false certification including fine and imprisonment."
Antoine Lewis, WWTP Superintendent
Prepa Name and 'tle (type or print)
2/28/2024
Signature of Preparer* Date
Land Applier Name and Title (if applicable) (type or print)
Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26)

Meritech, Inc.
Environmental Laboratory
Laboratory Certification No.165
- s.r
Page 1
Contact: Alex Fox Report Date: 1/17/2023
Client: Synagro
284 Boger Road Project: Oxford WWTP
Mocksville, NC 27028 Date Sample Rcvd: 1/10/2023
Meritech Work Order # 01102336 Sample: Lagoon 1 Grab 1/10/23
Parameters Results Analysis Date Reporting Limit Method
% Total Solids 2.42 % 1/12/23 0-100 % SM 2540B
Fecal Coliform (Sludge) 7,513 CFU/g dry wt 1/10/23 130 CFU/g dry wt SM 9222D
Meritech Work Order #
01102337 Sample: Lagoon 2 Grab
1/10/23
Parameters
Results Analysis Date
Reporting Limit
Method
% Total Solids
2.51 % 1/12/23
0-100 %
SM 2540B
Fecal Coliform (Sludge)
6,520 CFU/g dry wt 1/10/23
130 CFU/g dry wt
SM 9222D
Meritech Work Order #
01102338 Sample: Lagoon 3 Grab
1/10/23
Parameters
Results Analysis Date
Reporting Limit
Method
% Total Solids
2.49 % 1/12/23
0-100 %
SM 2540B
Fecal Coliform (Sludge)
6,572 CFU/g dry wt 1/10/23
130 CFU/g dry wt
SM 9222D
Meritech Work Order #
01102339 Sample: Lagoon 4 Grab
1/10/23
Parameters
Results Analysis Date
Reporting Limit
Method
% Total Solids
2.48 % 1/12/23
0-100 %
SM 2540B
Fecal Coliform (Sludge)
6,048 CFU/g dry wt 1/10/23
130 CFU/g dry wt
SM 9222D
Meritech Work Order #
01102340 Sample: Lagoon 5 Grab
1/10/23
Parameters
Results Analysis Date
Reporting Limit
Method
% Total Solids
2.50 % 1/12/23
0-100 %
SM 2540B
Fecal Coliform (Sludge)
5,091 CFU/g dry wt 1/10/23
130 CFU/g drywt
SM 9222D
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

Meritech, Inc.
Environmental Laboratory
Laboratory Certification No.165
Contact: Alex Fox
Client: Synagro
284 Boger Road
Mocksville, NC 27028
Meritech Work Order # 01102341 Sample: Lagoon 6 Grab
Parameters Results Analysis Date
% Total Solids 2.47 % 1/12/23
Fecal Coliform (Sludge) 7,729 CFU/g dry wt 1/10/23
Meritech Work Order # 01102342 Sample: Lagoon 7 Grab
Parameters Results Analysis Date
% Total Solids 2.49 % 1/12/23
Fecal Coliform (Sludge) 7,667 CFU/g dry wt 1/10/23
Page 2
Report Date: 1/17/2023
Project: Oxford WWTP
Date Sample Rcvd: 1/10/2023
1/10/23
Reporting Limit Method
0-100 % SM 2540E
130 CFU/g dry wt SM 9222D
1/10/23
Reporting Limit Method
0-100 % SM 2540E
130 CFU/gdrywt SM9222D
I hereby certify that I have reviewed and approve these data. D, "�" �
Laboratory Representative
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

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Meritech, Inc.
Environmental Laboratory
Laboratory Certification No.165
Contact: Ryan Copeland Report Date: 2/15/2023
Client: Synagro
284 Boger Road Project: Oxford
MocksviIle, NC 27028 Date Sample Rcvd. 1/10/2023
Vector Attraction Reduction Aerobically Digested Sludge 30 Day Test
Meritech Work Order # 01102335 Sample: Oxford Effluent Composite 1/10/23
Total Solids Volatile Solids n Volatile Solids
Week 1 0.95 0.57 0.604
Week 2
0.95
0.59
0.627
Week 3
0.98
0.58
0.597
Week 4
0.90
0.53
0.591
Week 5
0.71
0.44
0.615
Van Kleeck Reduction (%): -5.15
I hereby certify that have reviewed and approve these data. p is Wa rC it,
Laboratory Representative
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

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ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Oxford WWTP WQ Permit Number: W00011244
WWTP Name: Oxford WWTP NPDES Number: NCO025054
Monitoring Period: From 4/l/2023 To 6/30/2023
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. 1/A (time/temp) Alt. 2/13 (Alk Treatment) Alt. 3/C (Prior Testing)
Alt. 4/1) (No Prior Test) _ _ _ _ Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic
Beta Ray Gamma Ray Pasteurization
Class B:
Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying Composting Aerobic Digestion
Anaerobic Digestion
If nnnlienhle to alternative nerformed (Class A or Class Rl comnlete the followino monitoring data:
Parameter
Allowable Level in Sludge
Pathogen Density
No. of
Frequency
Sample
Analytical
Excee-
of
Type
Technique
Minimum Geo. Mean Maximum Units
dences
Analysis
Fecal
2x 10 to the 61h
MPN
MPN/g
Coliform
power per gram
of total solids
508
643
1,045
CFU/g
0
4 /Yr
grab
SM9222D
CFU
1000 MPN per gram of
MPN/g
total solids (dry weight)
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed:
0ption/Alt. 1
Option/Alt. 2
Option/Alt. 3 Option/Alt. 4
(V S reduction)
(40-day bench)
(30-day bench) X (Spec. 02 uptake)
Option/Alt. 5
Option/Alt. 6
Option/Alt. 7 Option/Alt. 8
(I 4-Day Aerobic)
(Alk Stabilization)
(Drying — Stable) (Drying — Unstable)
Option/Alt. 9
Option/Alt. 10
(Injection)
(Incorporation)
No vector attraction reduction alternatives were performed
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified
personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have
been met. I am aware that there are significant penalties for false certification including fine and imprisonment."
Antoine Lewis, WWTP Superintendent
Prepare and (type or print)
.— 2/28/2024
�gnature of Preparer* Date
Land Applier Name and Title (if applicable) (type or print)
Signature of Land Applier (if applicable)
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26)
Date

Meritech, Inc.
Environmental Laboratory
' Laboratory Certification No. 165
,or
Page 1
Contact: Ryan Copeland Report Date: 5/22/2023
Client: Synagro
284 Boger Road Project: Oxford
Mocksville, NC 27028 Date Sample Rcvd: 5/11/2023
Meritech Work Order # 05112361
Sample: Ox 1 Grab
Results Analysis ate
5/11/23
IMMI-Mil M, TMEMEMMur IIN
%Total Solids 1.74 % 5/12/23 0-100 % SM 2540B
Fecal Coliform (Class B Sludge) 1,045 CFU/g dry wt 5/11/23 130 CFU/g dry wt SM 9222D
Meritech Work Order # 05112362 Sample: Ox 2 Grab 5/11/23
Parameters Results Analysis Date Retorting Limit Method
% Total Solids 1.72 % 5/12/23 0-100 % SM 2540B
Fecal Coliform (Class B Sludge) 528 CFU/g dry wt 5/11/23 130 CFU/g dry wt SM 9222D
Meritech Work Order # 05112363 Sample: Ox 3 Grab 5/11/23
Parameters
Total Solids
Fecal Coliform (Class B Sludge)
Resul AnalysiS DateMethod
1.76 % 5/12/23
<516 CFU/g dry wt 5/11/23
0-100 %
516 CFU/g dry wt
SM 2540B
SM 9222D
Meritech Work Order #
05112364 Sample: Ox 4 Grab
5/11/23
Parameters
Results Analysis late
Reporting Limit
Method
% Total Solids
1.74 % 5/12/23
0-100 %
SM 2540B
Fecal Coliform (Class B Sludge)
1,045 CFU/g dry wt 5/11/23
130 CFU/g dry wt
SM 9222D
Meritech Work Order #
05112365 Sample: Ox 5 Grab
5/11/23
Parameters
Results Analysis Date
Reporting Limit
Method
% Total Solids
1.79 % 5/12/23
0-100 %
SM 2540B
Fecal Coliform (Class B Sludge)
<508 CFU/g dry wt 5/11/23
508 CFU/g dry wt
SM 9222D
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

Meritech, Inc.
Environmental Laboratory
Laboratory Certification No. 165
Contact: Ryan Copeland
Client: Synagro
284 Boger Road
Mocksville, NC 27028
Meritech Work Order # OS112366
Sample: Ox 6 Grab
$esUlts Analysis Date
Page 2
Report Date: 5/22/2023
Project: Oxford
Date Sample Rcvd: 5/11/2023
5/11/23
Reporting Limit Method
% Total Solids 1,74 % 5/12/23 0-100 % SM 2540E
Fecal Coliform (Class B Sludge) <522 CFU/g dry wt 5/11/23 522 CFU/g dry wt SM 9222D
Meritech Work Order # 05112367 Sample: Ox 7 Grab 5/11/23
Parameters its Analysis Date Reporting Limi Method
% Total Solids 1.77 % 5/12/23 0-100 % SM 2540B
Fecal Coliform (Class B Sludge) <574 CFU/g dry wt 5/11/23 574 CFU/g dry wt SM 9222D
I hereby certify that I have reviewed and approve these data. � a— -I CL H1" al)
Laboratory Representative
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

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Meritech, Inc.
Environmental Laboratory
AM Laboratory Certification No. 165
Contact: Ryan Copeland Report Date: 6/19/2023
Client: Synagro
284 Boger Road Project: Oxford
Mocksville, NC 27028 Date Sample Rcvd: 5/11/2023
Vector Attraction Reduction / Aerobically Digested Sludge (30 Day Test)
Meritech Work Order # 05112368 Sample: Oxford Effluent Composite 5/11/23
Total Solids Volatile Solids %n Volatile Solids
Week 1 1.12 0.66 0.591
Week 2
1.00
0.61
0.610
Week 3
1.05
0.62
0.592
Week 4
0.79
0.48
0.612
Week 5
0.80
0.47
0.581
Van Kleeck Reduction (%): 4.13
I hereby certify that I have reviewed and approve these data.
Laboratory Representative
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

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ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Oxford WWTP WQ Permit Number: WQ0011244
WWTP Name: Oxford WWTP NPDES Number: NCO025054
Monitoring Period: From 7/l/2023 To 9/30/2023
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. 1/A (time/temp) Alt. 2/B (Alk Treatment) Alt. 3/C (Prior Testing)
Alt. 4/1) (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic
Beta Ray Gamma Ray Pasteurization
Class B:
Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying Composting Aerobic Digestion
Anaerobic Digestion
If annlirnhle to alternative nerformed (Class A or Class Rl comnlete the fnilnw•inv monitarinv data:
Parameter
Allowable Level in Sludge
Pathogen Density
No. of
Frequency
Sample
Analytical
Excee-
of
Type
Technique
Minimum Geo. Mean Maximum Units
dences
Analysis
Fecal
2x 10 to the 61
MPN
MPN/g
Coliform
power per gram
of total solids
228
256
461
CFU/g
0
4 /Yr
grab
SM9222D
CFU
1000 MPN per gram of
MPN/g
total solids (dry weight)
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed:
0 tion/Alt. 1
Option/Alt.2
Option/Alt.3 Option/Alt.4
(VS reduction)
(40-day bench)
(30-day bench) X (Spec. 02 uptake)
Option/Alt. 5
Option/Alt. 6
Option/Alt. 7 Option/Alt. 8
(14-Day Aerobic)
(Alk Stabilization)
(Drying — Stable) (Drying — Unstable)
Option/Alt. 9
Option/Alt. 10
(Injection)
(Incorporation)
No vector attraction reduction alternatives were performed
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement in CFR 503.33/15A NCAC 02T.1 107 have not been met." (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified
personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have
been met. I am aware that there are significant penalties for false certification including fine and imprisonment."
Antoine Lewis, WWTP Superintendent
Pm repa ae a itle (type or print)
2/28/2024
Signature of Preparer* Date
Land Applier Name and Title (if applicable) (type or print)
Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26)

Meritech, Inc.
Environmental Laboratory
�.� Laboratory Certification No. 165
Page 1
Contact: Alex Fox Report Date: 10/4/2023
Client: Synagro
284 Boger Road Project: Oxford WWTP
Mocksville, NC 27028 Date Sample Rcvd: 9/28/2023
Meritech Work Order # 09282336
Parameters
Sample: OX 1 Grab
Results Analysis Date
9/28/23
Reporting Limit Method
Total Solids
3.84 %
9/28/23
0-100 %
SM 2540B
Fecal Coliform (Sludge)
<237 CFU/g dry wt
9/28/23
237 CFU/g dry wt
SM 9222D
Meritech Work Order #
09282337 Sample:
OX 2 Grab
9/28/23
Parameters
Results
Analysis Date
ReportinLF Limit
Method
%Total Solids
3.95 %
9/28/23
0-100 %
SM 2540E
Fecal Coliform (Sludge)
<230 CFU/g dry wt
9/28/23
230 CFU/g dry wt
SM 9222D
Meritech Work Order #
09282338 Sample:
OX 3 Grab
9/28/23
Parameters
Results
Analysis Date
Reporting Limit
Method
% Total Solids
3.90 %
9/28/23
0-100 %
SM 2540B
Fecal Coliform (Sludge)
<233 CFU/g dry wt
9/28/23
233 CFU/g dry wt
SM 9222D
Meritech Work Order # 09282339
Parameters
Sample: OX 4 Grab
Results Analysis Date
9/28/23
Reporting Limit Method
% Total Solids
398 %
9/28/23
0-100 %
SM 2540B
Fecal Coliform (Sludge)
<228 CFU/g dry wt
9/28/23
228 CFU/g dry wt
SM 9222D
Meritech Work Order ## 09282340
Parameters
% Total Solids
Fecal Coliform (Sludge)
Sample: OX 5 Grab
Results Analysis Date
3.94 % 9/28/23
461 CFU/g dry wt 9/28/23
9/28/23
Reporting Limit Method
0-100 % SM 2540B
130 CFU/g dry wt SM 9222D
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

Meritech, Inc,
Environmental Laboratory
Laboratory Certification No. 165
Contact: Alex Fox
Client: Synagro
284 Boger Road
Mocksville, NC 27028
Page 2
Report Date: 10/4/2023
Project: Oxford WWTP
Date Sample Rcvd: 9/28/2023
Meritech Work Order # 09282341 Sample: OX 6 Grab 9/28/23
Parameters Results Analysis Date Reporting Limit Method
%Total Solids 3.94 % 9/28/23 0-100 % SM 2540B
Fecal Coliform (Sludge) <231 CFU/g dry wt 9/28/23 231 CFU/g dry wt SM 9222D
Meritech Work Order # 09282342 Sample: OX 7 Grab 9/28/23
Parameters Results Analysis Date Reporting Limit Method
% Total Solids 3.95 % 9/28/23 0-100 % SM 2540B
Fecal Coliform (Sludge) <230 CFU/gdry wt 9/28/23 230 CFU/gdrywt SM 9222D
I hereby certify that I have reviewed and approve these data. G:�"
Laboratory Representative
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

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Contact: Ryan Copeland
Client: Synagro
284 Boger Road
Mocksville, NC 27028
Meritech, Inc.
Environmental Laboratory
Laboratory Certification No. 165
Report Date: 11/6/2023
Project: Oxford
Date Sample Rcvd: 9/28/2023
Vector Attraction Reduction Aerobically Digested Sludge 30 Day Test
Meritech Work Order # 09282335
Total Solids
Week 1 1.05
Week 2 0.97
Week 3 0.86
Week 4 0.82
Week 5 0.77
Sample; Oxford Effluent Composite 9/28/23
Volatile Solids % Volatile Solids
0.62 0.590
0.58 0.596
0.52 0.601
0.47 0.576
0.45 0.584
Mass Balance Equation = 1.05% Volatile Solids Reduction as per EPA Part 503 Biosolids Rule
Van Kleeck Reduction (%): 2.52
I hereby certify that I have reviewed and approve these data.
Laboratory Representative
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

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ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
FacilityName: City Of Oxford WWTP WQ Permit Number: WQ0011244
WWTP Name: Oxford WWTP NPDES Number: NC 0025054
Monitoring Period: From 10/1/2023 To 12/31/2023
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. 1/A (time/temp) Alt. 2B (Alk Treatment) Alt. 3/C (Prior Testing)
Alt. 4/1) (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic
Beta Ray Gamma Ray Pasteurization
Class B:
Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying Composting Aerobic Digestion
Anaerobic Digestion
If annlirahla to alternatives narfnrmad 149acc A nr r1acc Rl rmmnlafa 1-ha fnll—na mnnitnrina data•
Parameter
Allowable Level in Sludge
Pathogen Density
No. of
Frequency
Sample
Analytical
Excee-
of
Type
Technique
Minimum Geo. Mean Maximum Units
dences
Analysis
Fecal
2x 10 to the 61h
MPN
MPN/g
Coliform
power per gram
of total solids
258
266
267
CFU/g
0
4 /Yr
Grab
9222D
CFU
1000 MPN per gram of
MPN/g
total solids (dry weight)
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed:
0ption/Alt. 1
Option/Alt. 2
Option/Alt. 3 Option/Alt. 4
(VS reduction)
(40-day bench)
(30-day bench) X (Spec. 02 uptake)
Option/Alt. 5
Option/Alt. 6
Option/Alt. 7 Option/Alt. 8
(I4-DayAerobic)
(Alk Stabilization)
(Drying — Stable) (Drying — Unstable)
Option/Alt. 9
Option/Alt. 10
(Injection)
(Incorporation)
No vector attraction reduction alternatives were performed
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met."
"I certify, under penalty of law, that the ppathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified
personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have
been met. I am aware that there are significant penalties for false certification including fine and imprisonment."
Antoine Lewis, WWTP Superintendent
Prepare and Titl pe or print)
2/28/2024
tgnature of Preparer* Date
Land Applier Name and Title (if applicable) (type or print)
Signature of Land Applier (if applicable)
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26)
Date

Meritech, Inc.
Environmental Laboratory
Laboratory Certification No.165
Contact: Alex Fox
Client: Synagro
284 Boger Road
Mocksville, NC 27028
Page 1
Report Date: 12/14/2023
Project: Oxford WWTP
Date Sample Rcvd: 12/7/2023
Meritech Work Order #
12072313 Sample: OX 1 Grab
12/7/23
Parameters
Results Analysis Date
Reporting Limit
Method
% Total Solids
3.40 % 12/8/23
0-100 %
SM 2540B
Fecal Coliform (Sludge)
<267 CFU/g dry wt 12/7/23
267 CFU/g dry wt
SM 9222D
Meritech Work Order #
12072314 Sample: OX 2 Grab
12/7/23
Parameters
Results Analysis Date
Reporting Limit
Method
% Total Solids
3.44 % 12/8/23
0-100 %
SM 2540B
Fecal Coliform (Sludge)
<264 CFU/g dry wt 12/7/23
264 CFU/g dry wt
SM 9222D
Meritech Work Order #
12072315 Sample: OX 3 Grab
12/7/23
Parameters
Results Analysis Date
Reporting Limit
Method
% Total Solids
3.40 % 12/8/23
0-100 %
SM 2540B
Fecal Coliform (Sludge)
<267 CFU/g dry wt 12/7/23
267 CFU/g dry wt
SM 9222D
Meritech Work Order #
12072316 Sample: OX 4 Grab
12/7/23
Parameters
Results Analysis Date
Reporting -Limit
Method
% Total Solids
3.42 % 12/8/23
0-100 %
SM 2540B
Fecal Coliform (Sludge)
<266 CFU/g dry wt 12/7/23
266 CFU/g dry wt
SM 9222D
Meritech Work Order #
12072317 Sample: OX 5 Grab
12/7/23
Parameters
Results Analysis Date
Reporting Limit
Method
% Total Solids
3.40 % 12/8/23
0-100 %
SM 2540B
Fecal Coliform (Sludge)
<267 CFU/g dry wt 12/7/23
267 CFU/g dry wt
SM 9222D
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

Meritech, Inc.
Environmental Laboratory
Laboratory Certification No. 165
Contact: Alex Fox
Client: Synagro
284 Boger Road
Mocksville, NC 27028
Meritech Work Order # 12072318 Sample: OX 6 Grab
Parameters Results Analysis Date
% Total Solids 3.41 % 12/8/23
Fecal Coliform (Sludge) <267 CFU/g dry wt 12/7/23
Meritech Work Order # 12072319 Sample: OX 7 Grab
Parameters Results Analysis Date
% Total Solids 3.53 % 12/8/23
Fecal Coliform (Sludge) 258 CFU/g dry wt 12/7/23
Page 2
Report Date: 12/14/2023
Project: Oxford WWTP
Date Sample Rcvd: 12/7/2023
12/7/23
Reporting Limit Method
0-100 % SM 2540E
267 CFU/g dry wt SM 9222D
12/7/23
Reporting Limit Method
0-100 % SM 2540B
230 CFU/g dry wt SM 9222D
I hereby certify that I have reviewed and approve these data. ,Am acwjAcLnL -�
Laboratory Representative
642 Tamco Road, Reidsville, forth Carolina 27320
tel.[phone] fax.[phone]

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Meritech, Inc.
Environmental Laboratory
Laboratory Certification No. 165
Contact: Ryan Copeland Report Date: 1/8/2024
Client: Synagro
284 Boger Road Project: Oxford
Mocksville, NC 27028 Date Sample Rcvd: 12/7/2023
Vector Attraction Reduction Aerobically Digested Sludge 30 Day Test
Meritech Work Order # 12072320 Sample: Oxford Effluent Composite 12/7/23
Total Solids Volatile Solids Volatile Solids
Week 1 0.99 0.57 0.570
Week 2 0.99 0.58 0.588
Week 3 1.01 0.60 0.598
Week 4 0.89 0.53 0.602
Week 5 0.98 0.61 0.620
Van Kleeck Reduction (%): -22.86
I hereby certify that I have reviewed and approve these data. g��
Laboratory Representative
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]
i f j7I I fw� f I I I I I 1 I -1—�1-R I I=- -R

SECTION 6

Agricultural Lime Application Log
Year: 2023
Project: OXFORD
Field
(state -county -site -field code)
Soil pH
Lime Requirement
(from soil analysis)l
Tons/Acre
Applied
Date Applied
NC-GR-04-02
tons ac.
NC-GR-04-03
7.7
0.0 tons/ac.
NC-GR-60-01
7.6
0.0 tons/ac.
NC-GR-60-02
6.6
0.0 tons/ac.
NC-GR-60-03
6.6
0.0 tons/ac.
NC-GR-60-04
5.8
0.0 tons/ac.

SECTION 7

NCDA&CS Agronomic Division Phone: [phone] Website: www.ncagr.gov/Divisions/Agronomic-Services Report No. FY24-SL018909
k5i I"14'4+;4
Client:
Eddy Denny
Advisor:
Ryan Copeland
Predictive
6633 Old Roxboro Rd
SYNAGRO
°± f'
Oxford, NC 27565
284 Boger Road
�- Soil Report Mehlich-3 Extraction
Mocksville, NC 27028
Sampled County : Granville
_
Soil Testing Section
Sampled: Received: 11/22/2023 Completed: 01/24/2024 Farm: GR-4
Client ID:
422576
Advisor
ID: 499503
Sample ID: GR42
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre) N P2O5
K2O
Mg S
Mn
Zn
Cu
B
Information
Lime History:
1-Fescue/OGrass/Tim, M 0.0 120-200 0
20
0 0
0
0
0
0
Note: 12
2- Fescue/OGrass/Tim, M 0.0 120-200 0
20
0 0
0
0
0
0
Note: 12
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class:
Mineral
HM% W/V CEC BS% Ac pH P-1 K-1 Ca% Mg%
S-1 Mn-I
Mn-All Mn-Al2
Zn-I
Zn-AI
Cu-I
Na ESP SS-1 NO3-N
0.46 1.08 8.5 89 0.9 6.5 227 65 65 20
45 250
160 160
401
401
867
0.0
Sample ID: GR43
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre) N P2O5
K2O
Mg S
Mn
Zn
Cu
B
Information
Lime History:
1 -Fescue/OGrass/Tim, M 0.0 120-200 30
90
0 0
pH$
0
0
0
Note: 12 Note: $
2 - Fescue/OGrass/Tim, M 0.0 120-200 30
90
0 0
pH$
0
0
0
Note: 12 Note: $
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class:
Mineral
HM% W/V CEC BS% Ac pH P-1 K-1 Ca% Mg%
S-1 Mn-I
Mn-All Mn-AI2
Zn-I
Zn-AI
Cu-I
Na ESP SS-1 NO3-N
0.18 1.02 13.1 100 0.0 7.7 45 23 92 7
33 1882 1121 1121
136
136
260
0.1 1
North Carolina
Tcbwim Truk f and Ctwinlsskm
Reprogramming of the laboratory -information -management system that makes this report possible is being funded
through a grant from the North Carolina Tobacco Trust Fund Commission.
Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
- Steve Troxler, Commissioner of Agriculture

NCDA&CS Agronomic Division Phone: [phone] Website: www.ncagr.gov/Divisions/Agronomic-Services
Report No. FY24-SL018909
Eddy Denny
Page 2 of 2
Understanding the Soil Report: explanation of measurements, abbreviations and units
Recommendations
Report Abbreviations
Ac
exchangeable acidity
Lime
B
boron
If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either
BS%
% CEC occupied by basic
ton/acre or Ib/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting.
cations
For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 to 75 Ib/1000 sq ft)
Ca%
% CEC occupied by calcium
at one time, even if the report recommends more. You can apply the rest in similar increments every six months until the
CEC
cation exchange capacity
full rate is applied. If Mg is recommended and lime is needed, use dolomitic lime.
Cu-I
copper index
ESP
exchangeable sodium percent
Fertilizer
HM%
percent humic matter
Each nutrient recommendation for field crops or other large areas are listed separately in units of lb/acre unless
K-1
potassium index
otherwise specified. Recommendations for N (and sometimes for B) are based on research/field studies for the crop
K20
potash
being grown, not on soil test results. Recommendations for K and P will depend on K-1 and P-1 soil test results and the
Mg%
% CEC occupied by magnesium
crop to be grown. Generally, at K-1 and P-1 values > 50, recommendations will be minimal. If Mg is needed and no lime is
MIN
mineral soil class
recommended, 0-0-22 (11.5% Mg) is an excellent source; 175 to 250 lb/acre alone or in a fertilizer blend will usually
Mn
manganese
satisfy crop needs. Soluble salt levels (SS-1) appear only on reports for diagnostic/problem samples.
Mn-All
Mn-availability index for crop 1
Mn-Al2
Mn-availability index for crop 2
Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z
Mn-I
manganese index
notations appear on the soil report in the recommendation section, refer to NCDA&CS
M-0
mineral -organic soil class
$Note: Secondary Nutrients and Micronutrients. Various NCDA&CS crop notes also address lime and fertilizer needs.
N
nitrogen
Na
sodium
Recommendations for small areas, such as home lawns/gardens, are listed in units of Ib/1000 sq ft. If you cannot find
NO3-N
nitrate nitrogen
the exact fertilizer grade recommended on the report, visit NCDA&CS Fertilizer Substitutions to find information that may
ORG
pH pH
organic soil class
current soil pH
help you choose a comparable alternate. For more information, read NCSU publication,
phosphorus index
A Homeowner's Guide to Fertilizer. In general, homeowners do not need to be concerned about micronutrients.
P-1
phosphate
S-1
sulfur index
Test Results
SS-1
soluble salt index
W/V
weight per volume
The first seven parameters [soil class, HM%, W/V, CEC, BS%, Ac and pH] describe the soil and its degree of acidity.
Zn-AI
zinc availability index
The remaining 16 parameters [P-I, K-I, Ca%, Mg%, Mn-I, Mn-All, Mn-AI2, Zn-I, Zn-AI, Cu-I, S-I, SS -I, Na, ESP, SS -I,
NO3-N (not routinely available)] indicate levels of plant nutrients or other fertility measurement. Visit NCDA&CS
Understand Your Report for more information.

NCDA&CS Agronomic Division Phone: [phone] Website: www.ncagr.gov/Divisions/Agronomic-Services Report No. FY24-SL018906
k5i I"14'4+;4
Client:
Jake Isley
Advisor:
Ryan Copeland
Predictive
4520 Townsville Rd
SYNAGRO
°± f'
Bullock, NC 27507
284 Boger Road
�- Soil Report Mehlich-3 Extraction
Mocksville, NC 27028
Sampled County : Granville
_
Soil Testing Section
Sampled: Received: 11/22/2023 Completed: 01/24/2024 Farm: GR-60
Client ID:
451747
Advisor
ID: 499503
Sample ID: GR601
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre) N P2O5
K2O
Mg S
Mn
Zn
Cu
B
Information
Lime History:
1 -Fescue/OGrass/Tim, M 0.0 120-200 10
90
0 0
pH$
0
0
0
Note: 12 Note: $
2 - Fescue/OGrass/Tim, M 0.0 120-200 10
90
0 0
pH$
0
0
0
Note: 12 Note: $
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class:
Mineral
HM% W/V CEC BS% Ac pH P-1 K-1 Ca% Mg%
S-1 Mn-I
Mn-All Mn-Al2
Zn-I
Zn-AI
Cu-I
Na ESP SS-1 NO3-N
0.22 0.96 13.3 100 0.0 7.5 58 25 92 7
37 1554 926 926
152
152
243
0.1 1
Sample ID: GR602
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre) N P2O5
K2O
Mg S
Mn
Zn
Cu
B
Information
Lime History:
1 -Fescue/OGrass/Tim, M 0.0 120-200 0
30
0 0
pH$
0
0
0
Note: 12 Note: $
2 - Fescue/OGrass/Tim, M 0.0 120-200 0
30
0 0
pH$
0
0
0
Note: 12 Note: $
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class:
Mineral
HM% W/V CEC BS% Ac pH P-1 K-1 Ca% Mg%
S-1 Mn-I
Mn-All Mn-AI2
Zn-I
Zn-AI
Cu-I
Na ESP SS-1 NO3-N
0.51 1.10 8.1 90 0.8 6.6 190 55 67 19
41 297
186 186
311
311
740
0.1 1
North Carolina
Tai wLv Truk f and Ctwinlsskm
Reprogramming of the laboratory -information -management system that makes this report possible is being funded
through a grant from the North Carolina Tobacco Trust Fund Commission.
Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
- Steve Troxler, Commissioner of Agriculture

NCDA&CS Agronomic Division Phone: [phone] Website: www.ncagr.gov/Divisions/Agronomic-Services
Report No.
FY24-SL018906
Jake Isley
Page 2 of 3
Sample ID: GR603
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P2O5
K2O
Mg
S
Mn
Zn
Cu
B
Information
Lime History:
1 -Fescue/OGrass/Tim, M 0.0
120-200 0
20
0
0
pH$
0
0
0
Note: 12 Note: $
2 - Fescue/OGrass/Tim, M 0.0
120-200 0
20
0
0
pH$
0
0
0
Note: 12 Note: $
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class:
Mineral
HM% W/V CEC BS% Ac pH P-1 K-1
Ca% Mg%
S-1
Mn-I
Mn-All
Mn-Al2
Zn-I
Zn-AI
Cu-I
Na
ESP
SS-1 NO3-N
0.51 1.12 8.4
91 0.8 6.6 308 67
70 17
39
270
169
169
598
598
506
0.1
1
Sample ID: GR604
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P2O5
K2O
Mg
S
Mn
Zn
Cu
B
Information
Lime History:
1-Fescue/OGrass/Tim, M 0.4
120-200 50
0
0
0
0
0
0
0
Note: 12
2- Fescue/OGrass/Tim, M 0.0
120-200 50
0
0
0
0
0
0
0
Note: 12
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class:
Mineral
HM% W/V CEC BS% Ac pH P-1 K-1
Ca% Mg%
S-1
Mn-I
Mn-All
Mn-AI2
Zn-I
Zn-AI
Cu-I
Na
ESP
SS-1 NO3-N
0.60 0.96 7.6
81 1.4 5.8 35 85
55 20
56
717
447
447
153
153
135
0.1
1

NCDA&CS Agronomic Division Phone: [phone] Website: www.ncagr.gov/Divisions/Agronomic-Services
Report No. FY24-SL018906
Jake Isley
Page 3 of 3
Understanding the Soil Report: explanation of measurements, abbreviations and units
Recommendations
Report Abbreviations
Ac
exchangeable acidity
Lime
B
boron
If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either
BS%
% CEC occupied by basic
ton/acre or Ib/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting.
cations
For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 to 75 Ib/1000 sq ft)
Ca%
% CEC occupied by calcium
at one time, even if the report recommends more. You can apply the rest in similar increments every six months until the
CEC
cation exchange capacity
full rate is applied. If Mg is recommended and lime is needed, use dolomitic lime.
Cu-I
copper index
ESP
exchangeable sodium percent
Fertilizer
HM%
percent humic matter
Each nutrient recommendation for field crops or other large areas are listed separately in units of lb/acre unless
K-1
potassium index
otherwise specified. Recommendations for N (and sometimes for B) are based on research/field studies for the crop
K20
potash
being grown, not on soil test results. Recommendations for K and P will depend on K-1 and P-1 soil test results and the
Mg%
% CEC occupied by magnesium
crop to be grown. Generally, at K-1 and P-1 values > 50, recommendations will be minimal. If Mg is needed and no lime is
MIN
mineral soil class
recommended, 0-0-22 (11.5% Mg) is an excellent source; 175 to 250 lb/acre alone or in a fertilizer blend will usually
Mn
manganese
satisfy crop needs. Soluble salt levels (SS-1) appear only on reports for diagnostic/problem samples.
Mn-All
Mn-availability index for crop 1
Mn-Al2
Mn-availability index for crop 2
Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z
Mn-I
manganese index
notations appear on the soil report in the recommendation section, refer to NCDA&CS
M-0
mineral -organic soil class
$Note: Secondary Nutrients and Micronutrients. Various NCDA&CS crop notes also address lime and fertilizer needs.
N
nitrogen
Na
sodium
Recommendations for small areas, such as home lawns/gardens, are listed in units of Ib/1000 sq ft. If you cannot find
NO3-N
nitrate nitrogen
the exact fertilizer grade recommended on the report, visit NCDA&CS Fertilizer Substitutions to find information that may
ORG
pH pH
organic soil class
current soil pH
help you choose a comparable alternate. For more information, read NCSU publication,
phosphorus index
A Homeowner's Guide to Fertilizer. In general, homeowners do not need to be concerned about micronutrients.
P-1
phosphate
S-1
sulfur index
Test Results
SS-1
soluble salt index
W/V
weight per volume
The first seven parameters [soil class, HM%, W/V, CEC, BS%, Ac and pH] describe the soil and its degree of acidity.
Zn-AI
zinc availability index
The remaining 16 parameters [P-I, K-I, Ca%, Mg%, Mn-I, Mn-All, Mn-AI2, Zn-I, Zn-AI, Cu-I, S-I, SS -I, Na, ESP, SS -I,
NO3-N (not routinely available)] indicate levels of plant nutrients or other fertility measurement. Visit NCDA&CS
Understand Your Report for more information.