WQ0010689_2023 Residual Annual Report_20240228 (2)

Initial Review
Reviewer
nathaniel.thorn burg
Is this submittal an application? (Excluding additional information.) *
Yes No
If not an application what is the submittal type?* Annual Report
Residual Annual Report
Additional Information
Other
Annual Report Year* 2023
Permit Number (IR) * W00010689
Applicant/Permittee Baxter Healthcare Corporation
Email Notifications
Does this need review by the hydrogeologist? * Yes U No
Regional Office Asheville
CO Reviewer
Admin Reviewer Wanda Gerald

Submittal Form
Project Contact Information
Please provide information on the person to be contacted by NDB Staff regarding electronic submittal, confirmation of receipt, and other correspondence.
Name* Derek Bouchard
Email Address*
derek—[e-mail]
Project Information
.........................
Application/Document Type*
New (Fee Required)
Modification - Major (Fee Required)
Renewal with Major Modification (Fee
Required)
Annual Report
Additional Information
Other
Phone Number*
8287566644
Modification - Minor
Renewal
GW-59, NDMR, NDMLR, NDAR-1,
N DAR-2
Residual Annual Report
Change of Ownership
We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form.
https://edoes.deq.nc.gov/Forms/NonDischarge_Monitoring_Report
Permit Type:*
Wastewater Irrigation
High -Rate Infiltration
Other Wastewater
Reclaimed Water
Closed -Loop Recycle
Residuals
Single -Family Residence Wastewater
Other
Irrigation
Permit Number:*
WQ0010689
Has Current Existing permit number
Applicant/Permittee Address*
65 Pitts Station Road, Marion, NC 28752
Facility Name*
Baxter Healthcare Corporation Class A Residuals Program
Please provide comments/notes on your current submittal below.
At this time, paper copies are no longer required. If you have any questions about what is required, please contact Nathaniel Thornburg
at [e-mail].
Please attach all information required or requested for this submittal to be reviewed here.
(Application Form, Engineering Plans, Specifications, Calculations, Etc.)
2023 Annual Land Application Report WQ001068.pdf 1.65MB
Upload only 1 PDF document (less than 250 MB). Multiple documents must be combined into one PDF file unless file is larger
than upload limit.
* By checking this box, I acknowledge that I understand the application will not be accepted for pre -review until the fee (if required) has
been received by the Non -Discharge Branch. Application fees must be submitted by check or money order and made payable to the
North Carolina Department of Environmental Quality (NCDEQ). I also confirm that the uploaded document is a single PDF with all parts
of the application in correct order (as specified by the application).
Mail payment to:
NCDEQ — Division of Water Resources
Attn: Non -Discharge Branch
1617 Mail Service Center
Raleigh, NC 27699-1617
Signature
01-mo fflowA�il".11
Submission Date 2/28/2024

F.
February 26, 2024
Division of Water Resources
Water Quality Permitting Section
Non -Discharge Permitting Unit
1636 Mail Service Center
Raleigh, NC 27699-1636
RE: 2023 Annual Ash Report
Permit No. WQ0010689
Wood Boiler — North Cove, NC
Enclosed is the 2023 Annual Ash Distribution Report using the forms provided by NCDEQ-
DWR. Included in this report is the following information:
- Class A Annual DMSDF and Supplemental Information
- Annual Residual Sampling Summary Form and Form-B
- Ash Distribution Landowner Utilization Agreements
- Lab Sheets
There were no permit deviations during the 2023 Reporting Year.
If you have any questions or require additional information, please contact me at 828-756-6644
or at derek—[e-mail].
Sincerely
Derek Bouchard
Environmental Manager
Attachments: Annual Ash Report (3 copies)
O 9ox 3rr}, ,1 t icr,: Nl,' 28752
f28.7 5.4'9r 1

CLASS A ANNUAL D1S'YK113U'1'10.N AIND MAKKl+ IINC71 SURFACE ll15POSAL CERIAHC:A 10N AND SUMMARY MRM
WQ PERMIT #: WQ0010689 FACILITY NAME: Baxter Healthcare Corporation North Cove Steam Generation Plant Ash
PHONE: [phone] COUNTY: McDowell OPERATOR: Baxter Healthcare
FACILITY TYPE (please check one): ❑ Surface Disposal (complete Part A (Source(s) and "Residual In" Volume only) and Part C)
® Distribution and Marketing (complete Parts A, B, and C)
Was the facility in operation during the past calendar year? Yes 0 No ❑ --* If No skip parts A, B, C and certify form below
Part A*:
Part B*:
Month
Sources(s) (include NPDES # if
applicable)
Volume (dry tons)
Recipient Information
Amendment/
Bulking Agent
Residual In
Product Out
Name(s)
Volume (dry tons)
Intended use(s)
January
February
March
April
May
WQ0010699
112
550.20
662.20
See DMSDF Supp. Form
550.20
Land Application
.tune
July
August
September
October
November
4
WQ0010689
80
476.19
556.19
See DMSDF Supp, Form
476.19
Land Application
December
Total from FORM DMSDF (sup)
192
1t126,39 "
1I8<39..--
10639..
Totals:
Annual (dry tons):
192
1026.39 ..
1218.3� '
10209
Amendment(s) used: None Bulking Agent(s) used: Dry Wood Chips
* If more space is required, attach additional information sheets (FORM DMSDF (supp)): Total Number of Form DMSDF (Supp) 1
Part C:
Facility was compliant during the past calendar year with all conditions of the land application permit 0 Yes
(including but not limited to items 1-3 below) issued by the Division of Water Quality: ❑ No ip If No, Explain In Narrative
1. All monitoring was done in accordance with the permit and reported for the year as required and three (3) copies of certified laboratory results are attached.
2. All operation and maintenance requirements were compiled with or, in the case of a deviation, prior authorization was received from the Division of Water Quality.
No contravention of Ground Water Quality Standards occurred at a monitoring well.
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate and complete. I am aware that there are significant
penalties for su itting false information, including the possibility of fines and imprisonment for knowing violations."
Z/z7/Z.-1y
Signa4W of Permittee Date Signature of Preparer** Date
(if different from Permittee)
**Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM DMSDF (Supp) (12/2006)

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LU

Baxter JH[ealthcare, Corp.
2859 Old Linville Road
Marion, North Carolina 28752
Ash Distribution Utilization Agreement (Valid thru 3/30/2025), ]Baxter Copy
Baxter Healthcare, Corp., is the generator of the ash provided to e
v
the aforementioned ash is prohibited except in accordance with the i sttuctions on this sheet (Recipient). Application of
Transport: Adequate provisions steall be taken to ensure that the ing while ash is in transport transportation of aslh does not cause nuisances and hazards to public
health and safety or otherwise cause an adverse impact (e.g., transport wet ash in leak -proof trucks or cover dry ash). Spill c
Provisions must be available during transportation or land application activities. Any spill occurring or on the
application fields is the responsibility of the transporter. ) control
Stowage: The ash shall be adequately stbred to prevent wind erosion or surface runoff from carrying
use of wetting agents, berms, barriers, or tarps, may be necessary under windy or rainy conditions or if erosion or runoff cannot be
controlled. ash into any surface waters. The
Amlicatiowh: When using ash, the following shall apply. -
The ash application rates shall be limited to those that can be agronomically -justified (i.e., limited to that needed to me
liming requirements of the crops being grown on the land).
° Residual ash cake shall not be stockpiled for more than 60 days prior to land appl
Application ication et the
' Application o€ash cake residuals shall not occur within 100 feet of a public or private water supply
° of ash cake residuals shall not occur within 25 feet of surface waters such as intermittent and perennial
stream
perennial waterbodies, and wetlands.
• Copies of this Utilization Agreement, Aslh Permit No. WQOO 10689, and file Operation and Maintenance Plan shall ,
at the land application site when bulk residuals are being applied. be maintained
s
• Ash shall not be placed within one foot of the seasonal high water table or bedrock. net
• Ash shall not be applied to any site under the following conditions:
o blooded, frozen, or snow-covered or other condition causing runoff
o During precipitation events or within 24-hrs following a 0.5,, rainfall
o If the land application site does not have established vegetative cover crop
o If the application causes any nuisance conditions to adjacent property, natural resources, or wildlife
A surrhmary of the ash chemical analyses is located on page 3 of the request. information sheet. Detailed laboratory results are'
available upon
Title to the ash will transfer from Baxter Healthcare, Corp to Recipient upon delivery thereof. Thereafter, Baxter Healthcare,
Will have no responsibility and shall not be held liable by Recipient or any third party for any spill, misuse, misapplication
mishandling of the ash. Recipient acknowledges and agrees that the ash is being delivered by Baxter Healthcare, Corpto Recipient
Corp
an accommodation to Recipient. In exchange therefore, Recipient agrees to indemnify, oror other
harmless from and against any and all liability, damage, loss, cast, expense (including attorneys' fees), claim demand, ecte, C as
save and ]hold Baxter Healthcare, Corp
judgment or recovery asserted against Baxter Healthcare, Corp by any third party, including attorneys,
an
bodily injury (including death) or against
damage to property, it ,suit, action,
or other use of the ash.
p oP rty, arising from or in connection with Recipients receipt, transportation, hhandling
Signed (Ash Recipient): p„�
t� 1•ys Date:
Ash Recipient's Mailing Address: Zfi
Intended Use of Ash and Crop Type:
Expected Qty/Yr:
...y✓6 d:
Baxter Representative Sierharttm•
2 of 3

Baxter Healthcare, Corp.
2859 Old Linville Road
Marion, North Carolina 28752
Ash Distribution Utilization Agreement (Valid thru 3/30/2025), Baxter Copy
Baxter Healthcare, Corp., is the generator of the ash provided to �%� (Recipient}. Application of
the aforementioned ash is prohibited except in accordance with the instructions on tb� sheet.
_,
Transport:Adequate provisions shall n taken
and on of ash
health and safety or otherwise cause an to ensure that the transportation does not cause nuisances and hazards to public
adverse impact (e.g_, transport wet ash in leak -proof trucks or cover dry ash). Spill control
Provisions must be available during transportation or land application activities. Any spill occurring while ash is in transport or on the
application fields is the responsibility of the transporter.
Storage: The ash shall be adequately stored to prevent wind erosion or surface runoff from carrying
use of g agents, berms, barriers, or tarps, may be necessary antler windy or rainy conditions or rerosr©n ornto any rruanoff cannot be
controlled.
Application: When using ash, tine following shall apply:
* The ash application rates shall be limited to those that can be agronomically justified (i.e., limited to that needed to meet the
liming requirements of the crops being grown on the land).
• Residual ash cake shall not be stockpiled for more than 60 days prior to land application
' Application of ash cake residuals shall not occur within 144 feet of a public or private water supply
` Application of ash cake residuals shall not occur within 25 feet of surface waters such as intermittent and perennial streams,
Perennial waterbodies, and wetlands.
* Copies of this Utilization Agreement, Ash Permit No.WQ4010689, and the Operation and Maintenance flan shall be maintained
at the land application site when bulk residuals are being applied.
• Ash shall not be placed within one foot of the seasonal Irigh water table or bedrock. a
• Ash shall not be applied to any site under the fallowing conditions:
a Flooded, frozen, or snow-covered or other condition causing runoff
a During precipitation events or within 24-his following a 0.5" rainfall
o If the land application site does not have established vegetative cover crop
o If the application causes any nuisance conditions to adjacent property, natural resources, or wildlife
A summary of the ash chemical analyses is located on page 3 of the information sheet. Detailed laboratory results are available u
request,
pon
Title to the ash will transfer from Baxter Healthcare, Corp to Recipient upon delivery thereof. Thereafter, Baxter Healthcare,
will have no responsibility and shall not be held liable by Recipient or any third party for any spill, misuse, misapplication
mishandling of the ash. Recipient acknowledges and agrees that the ash is being delivered by Baxter Healthcare, Co to Recipient
Corps
an accommodation to Recipient. In exchange therefore, Recipient agrees to indemnify, or other
harmless from and against any and all liability, damage, loss, cost, expense (including attorneys' fees}, claim, demand, suitipaent as
save and hold Baxter Healthcare, Corp
judgment or recovery asserted against Baxter Healthcare, Corp by any third art
or
in (including death} or damage to roe P Y, including any governmental authority, whether for
or other use of the ash. g property, rty, arising from or in connection with Recipient's receipt, transportation, handling
Signed (Ash Recipient):
Date: _ - I-7 T 22
Ash Recipient's Mailing Address: S 7 t-/ (2 o nI A S �. a
Intended Use of Ash and Crop Type:
Expected Qty/yr: ,2 T) r,
Baxter Representative
Acres of Land: _ (j 2�
Page 2 of 3
! 7,"Z

Baxter Healthcare, Corp.
2859 Old Linville Road
Marion, North Carolina 28752
:ash Distribution Utilization Agreement (Valid thru 3/30/2025), Bauer Copy
13,.x1 r ly4calthcam, i'ca a, r, the r;cnerworn a
of the ash provided to f & '
the .,lc�rwnettticnte d aslt is prohibited exec i in with the instruction. un this shc4 !/Y (Recipient). Apl�licatian (if'al
t.
prrt�tc���u�t � deyarate provisions shall be taken to ensure that the transportation orash does not effuse nuisances and hazards (0 public
heal a and safety or other vise cause an adverse impact (c.�., transport wet ash in leak -proof trucks or cover dry ash). Spill control
pro "'ISions must he available during transportation or land application activities. Any spill occurrivL while ash i:, ill transport or on the
application fields is tlae responsibility of tkrra transporter.
Stt�r�t c: The ash shall be adequately stored to prevent wind erosion or surface runoff rrom canying ash into any surface waters. Jfhe
use of wetting; agents, terms, barriers, or tarp;;, may he necessary under windy or rainy conditions or if erasion or runoff cannot be
con(rolled.
-4pp1ieatit)ij: When €rl:irtg ash, the fiollo���ing shall apply:
p The ash apphcattic}n rates shall Ile limited to those that call be agronomically -justified (i.e., limited to that needed to rnect tfae
liming requireme13ls orthe crolas being !Town on the land).
Residual ash cake shrill not he stockpiled for more than (U days prior to land application
Application orash cake residuals shall not occur within 100 feet of a public or private water supply
• .Application of rift cake residuals shall not occur within 23 fCct of surrace waters such as intermittent and perennial streams,
perennial watcrhodic,4, and wetlands.
Copiers of this l.stilization Agreement. Ash Permit No.WQOO10689. and tile. Operation and Maintenance ]'fan shall he maii,tained
at the land atl�plication site When bulk residuals arc being applied.
® Ash shrill not l,c plsccrl withinne [oat ol•the st,nsonal high floater table or bedrock.
Aslt .shall r,ot he applied to filly site under the following conditions:
Flooded. frozen, or snow-covereu or other condition causing runoff
Durin�M pr"tpitation e vents or within 24-hrs following a ().S ' rainf,•tll
if the land application site doe not have established vegetative c ) r crop
1.1'111c application causes any nuisance conditions to ac.jaccnt property, natural resources, or wildlife
A summary c.r Ilae ash chemical anatlyscs is located on page 3 of the information sheet. Detailed lalaurttary results are m aihiblc upon
request,
I itle to the ash will transfer from Baxter Healthcare. C.`or7a to Recipient upon delivery thereof'. Thervaltcr. Bamur lleallbear'c, Corp
vN'ill have nil responsibility and shall not he held liable by Recipient or auy third party liar any .,pill, misuse, misapplication or other
mishandling of the ash. Recipient acknowledges and agree.5 that the ash is being clehvcrcd by Baxter I]calllacare. C'otp to Recipient as
an accommodation to Recipient, In �xchartge therefore, Recipient agrees to indemnify, save and hold Baxter IIcaltlacare, Corp
harmless from and against any and all liability, dam tge, loss, cost, expense (including attorneys' fees), claim, demand, suit, action,
judgment ar recovery asserted against Baxter Ilcalthcare. Corp by any third party, including any governmental authority, whether for
bodily injury (including death) or damage to property. arising from or in connection with Recipient's receipt, transportation, handling
or other use of the rift. -r
)
Signed (Ash Rcci prelit �
e
... Date: 01.21
Ash '
Reci ients Mailing'
p Address:
r
Intended Use ol'Ash and Crop Type; ° ijy tP
I3x pected t :
l Q Y%Yr: Acres of l.artd:
Baxter Representative Signature:
Page 2 of

axter Healthcare, Corp.
2859 Old Linville Road
Marion, North Carolina 28752
Asia Distributioll Utilization Agreement (Valid thru 3/30/2025), Baxter Copy
1hpYaf��rc3nctttionecl (slt�is fs tile 9cilerator rohihic c1 exceptina accordance witlllte.!�g ':vl , -__ (Recipient). Application of
provided to
p instructions on this sheet.
IrctlrspruY: Adequate provisions shall be taken to cnsure that the transportation of ash does not cause nuiswices and hazards to public
health and safety or oihcrwisc cause all adverse impact (e.g,, transport wet fish in leak -proof tnteks or cover dry ash). Spill control
provisions ntusl be available: dnrimy transportation or land application activities. Any spill occurring while ash is in transport or on the
application fields is the responsibility of the transporter.
Slrn-rrgcr; The ash shall be adequately stored to prevent wind erosion or surface runoff !font Carving aslt into any surface waters. fhc
use of wetting agents, berths, basTiers, or fares, may be necessary under windy or rainy conditions or if erosion or runoff cannot be
controlled.
fpplicrrtlurt: Wiles using ash, till foll(wing shall alzpky:
® "lie ash application rates ,hall be limited to those that can be agronomically-jx(stilicci (i.e., limited to that needed to meet the
lialing require.tte.nts of the crops being grown on the land).
9 Residual ash calve shall riot be stockpiled for more than 60 days prior to land application
V Application of ash cake residuals shall not occur within 100 fM of a public or private water supply
0 Application of atilt cake residual, shall not occur within 25 Icel of surface waters ,uoh as intermittentand perennial streams,
perennial waterhodies, and wetlands.
6 Copies of this Utilization Agreement, Ash Permit No.WQ0oi06$9, and the Operation and Maintenance flan Shall I;e. maintained
at the land application site wheat bulk residuals are being applied.
0 Asti shall not be placed within one foot of the seasonal high water table or bedrock.
® Ash shall not be applied to any site under the following conditions:
o Flooded, irozen, or snow-covered or outer condition causing rulloff
Durinf, precipitation itation events or within 24-hrs following a 0.5' ahil'all
Q If the land application site does not have established vegetative cover crop
site application causes Wry nuisance conditions to ac�jaeertt property, natural resources, ar wildlife
A suttltnury of the ash chc:ntiQal analyses is located on page; 3 of the information sheet. Detailed laboratory results arc available upon
request.
Title to the atilt ti-i11 tramsfcr frojil Baxter healthcare, C"olp to Recipient upon delivery thereof. `thereafter, Baxter llcaltheare, Corp
will have no responsibility and shall not be held liable by Recipient or any thirdparty for any spill, misuse, misapplication ar other
mishandling of the ash. Recipient acknowledges and agrees that the ash is being delivered by Baxter healthcare, Corp to Recipient as
an accommodation to Recipient. Its exchange lherclore, Recipient agrees to indentnily, save and hold Baxter Healthcare. C'orlt
harmless firom and against any and all liability, damage, loss, cost, expense (including attorneys' fees). claim, demand, suit, action,
judgment or recovery asserted against Baxter licaltheare, Corp by any third party, including any 41ovetltntental authority, whether Iiir
bodily injury (including death) or damages to property, arising from or in connection
or other use of the ash. with Recipient's rcc:aipt, transpartatit,tt, handling
Signed (Ash Recipient): ,� L
Date:
--."
Asti Recipient's Mailing Address: �1 ` , e�
Intended Use of Ash and Crop I'ylte: ,... �Z,� Z 417"� '
F;xpected QlyrYa-_
Acres cif land: {/
Baxter Representative Signature: V X
rage 2 of 3

axter Healthcare, Corp.
2859 Old Linville Road
Marion, North Carolina 28752
Ash Discributiou Utilization Agreement (Valid thru 3130/2025), Baxter Copy
Baxter ,
f' tile ash proved to
the aforementt3 ned ash lis prohibited except_, is the gencratorcin accordance with the rn °trttLtro>t �r� (Recipient).Application of'
4 s lest.
D-11ttspo}•f: Adequate provisions ~hall be taken to ensure that the transportation of ash does not cause nuisance~ and hazards to public
health and safety or otherwise cause an adverse impact (e.g., transport wet ash in teal:-prool' trucks or cover dry ash). Spill control
provisions must be available during transportation or land application activities. Any spill occurring while ash is in transport or on the
application fields is the responsibility of the transporter_
Sloruge- The ash shall be adequately stored to prevent wind erosion or surface runoff from carrying ash into any surface waters, The
use of wetting agents, berms, barriers. or saris, way be necessary under windy or rainy conditions or if erosion or runoff cannot be
co,5trolled.
,1Pi:!ic.•rttion: When using ash, the following shall apply:
• Hic ash application rates shall be limited to those that can be agronornically-justif:ted (i_e., limited to that needed to meet the
liming requirenwrits of the crops being grown on the land).
® Residual ash cake shall not hestockpiled For more than lit) days prior to land application
e Applicatic=r of ash cake residuals shall not occur within 100 feet of a public or private water supply
® Application of ash cake residuals shall not occur within 25 feet of surface waters such as intermittent and perennial streams,
perennial waterbodies, and wetlands.
. ('opic,s of this Utilizalion Agreement. Ash Pennit No.WQ0010689, and the Operation and Maintenance flan shall be maintained
at the hind application site when bulk residuals are being applied.
Ash shall not be placed within one foot ol' the seasonal high water table or bedrock.
m Ash ;hall not be applied to any site under the tillhnvirl, conditions:
Flooded. frozen. or snow-covered or other condition causing nrnoff
During precipitation events or within 24-hrs following a 0.5" rainfall
o II'the laud application site does not have established vegetative cover crop
Il'the application causes only nuisance conditions to adjacent property, natural resources, or wildlife
A scirnnlary of the ash chemical analyses is located on paste 3 of the infonnafion sheet. Detailed laboratory results are available upon
I equest.
Title to the tvsh v ih transfer firom Baxter Healthcare. Corp to Recipient upon delivery thereof. Thereafter, I3axtcr Healthcare. C'orp
will have no responsibility and shall not he held. liable by Recipient or any third party for any spill, misuse, misapplication or other
mishandling, of'the ash. Recipient acknowledges and agrees that the ash is being, delivered by Baxter llcallhcare, Corp to Recipient as
an accommodation to Recipient. In exchange therefore, Recipient agrees to indemnify, save and hold Baxter Ifealthcare, Corp
harmless from and against any and all liability, damage, tons, cast, expense; (including attorneys' fees), claim, demand, suit, action,
judgment or recovery asserted against Baxter Ilealthcarc, Corp by any third party, including any governmenial authority, whether For
bodily injury (iacltlding, death) or damage to property, arising fi"om or in connection with Recipient's receipt, transportation, handling
or other use of the ash,
i
p
Signed (Ash Recipient) ,.;
����" t,•[o� v� _,;;� Date:
Ash Recipient's Mailing Address: �` ' • ' r� 7
r '..,xr::..._d,e
intended Use of Ash and Crop ]vpe;:
Expected (tv. Nr: Acre. of L.alld:
1 ? . °l. j
Baxter Representative Signature:
Pagi: 2 of 3

Baxter 1-lealtheare, Corp.
2859 Old Linville Road
Marion, North Carolina 28752
Ash Distribution Utilization Agreenjent (Valid thru 3/30/2025), Baxter Copy
Baxter healthcare, C'097., is the generator of the ash provided to
iue; at'orcntcntioned ash iti pralaibitcd except to accordance with the iulsiruCtioue f Allplicaticut of
�a5 as tE'1us sheen
Adequate provisions shall be taken to ensure that the transportation of ash does not cause nuisances and hazards to public.
tl r, ind safety or otherwise cause an adverse iEilpac;t transport wet ash in leak -proof trucks or cover dry ash). Spill control
:1 test be available during transpo iation ur land application activities. Any spill occurring while ash is in transport or on the.
s <stran flelds is tlae responsibility of the transporter.
Shr.{fir- The ash shall be adequately stored to prevent wind erasion or surface runoft' from carrying ash into any surface waters. '[ he.
�Isc (4 wetting agents, berms, barriers, or tarps, may be necessary under windy or rainy conditions or il' trrosicm or runoff cannot be
control led.
. PPlicestion: When using, ash, t11e followinj, shall apply:
r Us, ash aappiication rates shall be limited to those that can be agronomically-jxustificd (i.e., linlitcJ to that needed to nice( the
liming rccluiremems of' the crops being grown on the land),
® Residual a,11 cake shall not be stockpiled for more than 60 days prior to land application
a Applictttiotl of ash cake residuals shall not occur within WO fect of a public; or private water supply
ArTlicaliorn oi' ash cake residuals shall rat occur -within 25 feet of surface vvatcrs such as intermittent and perennial streaun.s,
p��r;:;rinial w'uicrbcxlics. and wetlands.
0c iI)iGs crl'tliis r i;ili;�alion Agreement, Ash Permit No.WQO(ll0689, and t11e Operation and Mainmiance flan steal! he maintained
sul Cl,: ht;.ci a�,,i;0� ;; boil site when bulk residuals are being applied.
As:� vhidl no iwe placed within otae Bart ofthe Seasonal hif;h water table orbeclawk.
P„la sltt,ll �V't be applied to any site under the lirllowing, candition.s:
l !oodod, l'rozc:ll, or snow-covered or other condition caausing runoff
c= lluriulg precipitation events or within 24-hrs following a 0-5- rainfall
11'the land application site sloes not have established vegetative cover croyp
If Lhe alapfication causes atgv nuisance conditions load' acent property, natural resources, oe ca ildiife
�,a maary of tllc ash chemical analyses is to sated out page 3 of the information sheet. lhetailed laborato t'ry resntts area anal°ifc� upon
.cl:iest.
Title to the ash will transfer from I3axlcr Ileaithcare, Corp to Re ipicaut upon delivery t:horeo r. Ihereafter, Baxter Ilealthcare. Corp
will have no uesponsibility and shall not be held liable by Recipient or any third. party for any spill, nlisusc, misapplication or other
ansharldlialtw nl the; ash. Recipient ackllowlcdgcs and agrccs Mat the sash is being delivered by Baxter healthcare, Corp to Recipient as
an accoinmodai'iaal to Recipient. In exchange therefore. Recipient agrees to indemnify, save'~ and hold Baxter Healthcare, Cote
hat7nless from ,and against any and all liability. damage, loss, cast, expense (including; attorneys' fees). claim, demand, suit, actiaat,
Judi
gment or reCaVl'Fy aSSeltf'.d ilf�ainst Baxter Ilealthc'arc. COil-) by any third party, including any governmental authority, whether l:or
bodily injury (including death) or daalla���e t() prtaperty, ar
or other use of, (lie ash. ising from or in connection with Recipient's receipt, transportation, handling
Si,Wned ',Ash Recipient)
J. I.1ate: _:
r
Ash Recipient's Mailing Address:
fnictided l Ise of' Ash and ('rop'l,yp
e.
¢ �9
1:\ilC=etC(l (lytVYE:
.. __ . Ac.rcti l L and, ;
ti«xtcr itepresentalive:Sit
rature:
Page 2 of 3

Baxter Healthcare, Corp.
2859 Old Linville Road
Marion, North Carolina 28752
Asia Distribution Utilization At reemelit� (vali(1 thru 3/30/2025), Baxter Copy
tl eYaforcmenuonud ash is tt ,hibiled except in accorsiaPce +vitJt tile. iit'siru lions oat 1>!` Sheet.
.. generator of the ush rovidcd ttt
xti., a
p (Recipient), Applicatic?at of
U.
Dilnslvrf. Adeyualc prrtvisions shall be taken to ensure Iltal the trattslx,aYatian of ash does nut cause nuisattces ,and hazards to piatths
health and safety or o[hcrrv°isa cause an adverse impact[r:utsperrt wet a'h ill leak -proof trucks or cover dry ash). Spill ct*llt of
provisions must 1v available daring transportation or lane{ application Aclivilics_ Any spill occurring while a41F i
application Holds is the responsibility of the transporlcrrs in transport or on fire.
use (11' 'Pile ash shall be aduluately shred to prevent wind erasion or surface runof�� non c:traying ash into any surftce water;,.- t itr.
conro ledWelling agents, beams, barrier~. or tarps, may Ire necessary under windy nr rainy atntditiirn�s or if crsrsion or nanstlWa cat :ot he
controlled.
fpplicutinn: W€test using ash. the following' hlnallapply;
• The ash application rates shall be limited to Ihose that can Ire agrnnnrnirally-,jaraulied , Inning requirements of tire erops being grown on the land), litnuad to that nocdLd le ittect tits • Residual ash cake shall not be stockpiled for more than 60 days prior to land atpphcatiUn
• Applicatiurt of ash cake residuals shall licit occur withiat 1()() feel nf" a pohlic s=r Private tv ttcr supply
° Application of ash cake residuals Shall oat occur within 25 feel of surface• waters Such�,Is ullerntittenl and perennial snvam!"
Perennial waterbodics, and wetlands.:
• Copies of this Uliliralion Agreement, Ash Permil N(j,WQO()lpfiR+). atul the t)prtitalion stud at t€le land application silo when bulk residuals arc being applicc!. l4tiuoterr.nwu Plan Shall be maintained
• Ash sltall not be placed within one foot cif the seasonal high water table or hcsfrock.
• Ash siaall not !tc applied to any site under the le,€bowing conditions;
cr Flooded, frozen- or ~now-cavcrud or othca' condili:;-tt c„u<;in}; runot'l-
0 During precipitation eveatis or within 23-han foN,1 ,-ing a 0.5" r�Eio€isii
o If he land application site does not have eaf�-ablislted vc;getati ce cuv°c,- u sit,
If tlic application causes ally nuisance conditions t:r adjac'ant l,r�mrrr•; _ z,afI resoE,rccc. nt wifdl£Ic
A summary of 1Jte a'd' chemical analyses is located oat page 3 of tltc itt#irnnatiott xh�a t. ?h luilcc€ lalu,mimy resndts are available Igwe t
request.
"lie to the ash will transfer front 13amor licatthearc, G,3p to Rcci;,ictn upon delivery lheras: 3'hccaaftur. i3axscr ltrahJtnur.:, t-'rrrp
will have no responsibility and shall not be held liabla by € "ipiert nr any third party it=r tiny spill. rnisus .misapplication or zriiter
mishandling of file a h. Recipient acknowledges and angraes thal Ill(
aslt is heir.,, alalivcrCd by l3;taiur l lsaalthttrrc, Corp to Recipient ;r,
an acenmmcidathm fo Recipient. In exchange therefore. Recipient al;rccs ta,indcEnnil'y. serve and hold Baxter EIca[thcate. C''trrp
hamtless `innt and against. any and all liability. darnage, loss, cost, ex€tense (including anc,:ae;ys' fees}, rhaian, demand, suit. , Cn r_
judgmcni nr ructsvcry asserted against I;aster healthcare, Corp by any tltirsl party. inoludin any gatvcrmncn€;tI authctrily, tchctltcr fitr
or other
v'ic (including death) or damage fir property, arising from or in Cot�,uclion wish Rc6pient'�s re rvipt, transpor(ation, handlirtl;
nrcttha r nose of ilk ash_
Signed IAslt Recipient)
�7
Ash Recipicnl's Mailing Address::''
lnlendcd Use o£'Ash and (..'rop •Type'
f
;y
p
Baxter Rc rescrttapvu Sr tonsure: r -
;xireiLc (ityiYr:
% r r
Page ? of .3

Baxter Healthcare,, Corp.
285€1 Old LinvNic Road
Marion. North C UI.Olina 28752
Ash Distribution Utilization Agreement (Valid thrill 3130/2025), Baxter Copy
Baxter IIcalthcare, co - is tIle of
1
the aforementioned ash is pTlCllllbateillexeepi(St't, 111 rdlCe W[Ill the 1i1S11 l Il V()i] y g]]ee
�.. (Recipient). Applicaiintr ({'
DWIlsliort: Adequate provisions shall be taken In, ensure that till; lransporutdou n]';tish doc-s not "Ruse nclis: lwcs and hazar(G; uc pt il,tic
health and safety nr- otherwise cause an advcrsc inlpne€ (e.g., Iran port we€ ;rsh in leak-prte?l' il�tcks or calver dry asi]). Spill cgrllxiai
Provisions trust be available during transportation or I:and application activities. Any spill recurring While ;lsh is in € ash),
Spill
oil the
application fields is the responsibility of the transporter.
Slura,�e: 'file ash shall be adequately stored to present weld erosion; oa surjae -,c ru,loti from CIu ilug ash into any surface walels tlie
use of wetting agems, berms, harriers, or tarps, play he necessary under windy nr r aiuy cckuditi(ms Or if urosioll of rnnol'f eauEtot hu
conln,lled.
Applir'ulaplr: Wllen ll iulg ash, the follo%viing she;][ apply:
• The ash applicatirnl rate's shall be limited to th(rsc that r
t
cap he agrrnomic;ally-.jtas4]9cd (i-c., ]"relied to that needed to nle,,; ltc
lining requirements rf the crops hero"; grown on the land},
• R"c idual ash cake shall not he stockpiled for more than 60 days prior to land application -Application ofash cake residuals shall not occur withinn ]Il() feel ofa Public or private w:ucr supply Applicatinrr of ash cake residuals shall 'lot occut within 25 feet of surlaec wilted such as intcrm iltcn'•
Perennial sy;lterbodics, arld wetlands. and percnniap Nirw arnz,
• Copies of this Utilization Agreement, Aslc I vtrrrlt "io.WQjIO ilii'R°3, ant! (Ile ( Tcrltion and il;lirucnarrc ?'tan sliuli he nrlita3ilinexJ
at the Inad :tpplicatinn site when bulk residuals are being. applied.
• Ash shall not be piacrd within m.c feet ol'the sea%onal high wvale, lable or luldrocic.
• Ash sliall rlot be applied to any site under the fi,liowu)g eunditic,ns�
Hooded, frozen, air sn0w-c0A'ered oc othcramditlon eautiln�,f
During prac.ipiiai,rtt events (if wuhn, '2q-hrL trlr n11 ;ell<r,. ,ng 11 fLs" r t i
11ehe €:.red application site does not halve estabhAcd vcgcrlative
if the appl€catil?n causes any nuisance conditions it, adjtuxa;t pr<: „ t, . ❑a;t±rcl ri_,nr:rca5. or iidiifc
A summary of the ash che•rnical analyses' is i sated oil page 3 of the infominti� r< ;]less- i 3. t;lilc�i ':,,'c,r.3tc,r„ ,kaca]ts ;:re n% aiiable u, on
request.
"'Ile to the ash will transfer from Raster l lealthcare, Corp Rs Rccipiellt trpoll d::Eivel- thereof, i'hcreali(i, ]raster 1 tcalthcare,
will have no responsibility and shall not be held liable by Recipient nr ally ii;ir(1 ],arty fir u;tg sl�tlL ttlisuse, rtiisapphc.d ion or rrihet�
1Pishartdling of the ash Rec,ipicrtl acknowledgos and -Ir rues €hat the ash is hcuw dolivclvd by l3.rstsr l lcapthcnac. Corp) ur Re, -ij wiv ;t,:
an accommodation to Recipient it, ezch;Tr;ge therGl rc. Roeip:cltt ugrcrs Ica indc:rnnily..w,tve ;1nd hold ]]aster llraltlscara, C�:rrp
Ilargmen or r and -gasman any and all liability, altr c, ins, Cost, eNpcnse (inc]udlinl. attaxuaya fc(es), cl aitn, dcanand, soil, aciion-
jud bodily
inn r recovu i asserted again t iiartrr llcakf1c rrc. Corp, by ruy third Pell y, inc lu(iing 'roy go+cmnldnlcrl aulhori[y, whether liar
bodily iruse (including death} urdanl,rite to propert} t €stnst from or in (anncctiort c� ill: Re iputjl1's reccipl. Irs ]spor�ation, bane iiu.
or other ttsc of th( ash_
�-
Signed (Ash RcerpiPnt3
Ash Recipient's Mailing Address:; z
Intended Use M Ash and C.'rups "Cypc:
14
F-Mccled [hyfyr:
Baxter RcpresenLalivcSignulirra;
Page of i

Baxter Healthcare, Corp.
2859 Old Linville Road
Marion, North Carolina 28752
Ash Distribution Utilization Agreement (Valid thru 3/30/2025), Baxter Copy
Baxter Healthcare, Corp., is the generator of the ash provided to the aforementioned ash is prohibited except in accordance with the in ns of tGet�
(Recipient). Application of
health an : Adequate provisions shall be taken to ensure that the transportation of ash does not cause nuisances and hazards to public
health and safety or otherwise cause all adverse impact (e,g., transpoR wet ash in Leak -proof trucks nr cover dry ash), Spill control
Provisions must be available during transportation or land application activities. Any spill occurring while ash is in transport or on the
application fields is the responsibility of the transporter.
Sto
use Of
The ash shall be adequately stored to prevent wind erosion or surface runoff from carrying ash into any surface waters, The
use ro wetting agents, berms, barriers, or tarps, may be necessary under windy or rainy conditions ar if erosion or runoff cannot he
controlled.
Application: When using ash, the following shall apply:
• The ash application rates shall be limited to those that can be agronomically justified (i.e., limited to that needed to cc the
liming requirements of the crops being grown on the land).
• Residual ash cake shall not be stockpiled for more than 60 days prior to land application
• Application of ash cake residuals shall not occur within 100 feet of public or Private water supply
• Application of ash cape residuals shall not occur within 25 Feet of surface waters such as intermittent and perennial streams
Perennial waterbodies, and wetlands.
• Copies of this Utilization Agreement, Ash Permit 1Yo.WQ0010689, and the operation and Maintenance Plan shall
at the land application site when bulk residuals are being applied. be maintained
Ash shall not be placed within one foot of the seasonal high wafer table or bedrock.
Asir shall not be applied to any site under the following conditions:
o Flooded, frozen, or snow-covered or other condition causing runoff
o During precipitation events or within 24-hrs following a 0.5" rainfall
o If the land application site does not have established vegetative cover crop
o If the application causes any nuisance conditions to adjacent property, natural resources, or wildlife
A summary of the ash chemical analyses is located on page 3 of the information sheet. Detailed laboratory results are available upon
request
Title to the ash will transfer from Baxter healthcare, Corp to Recipient upon delivery thereof. Thereafter, Baxter Healthcare, Corp
will have no responsibility and shall not be held liable by Recipient or any third part for an
mishandling of the ash. Recipient acknowledges and agrees that the ash is being delivered by Baxttrer Healthcare, Corpr o Recipient as
an accommodation to Recipient, In exchange therefore, Recipient agrees to indemnify, save and hold Baxter Healthcare, Corp
harmless from and against any and all liability, damage, loss, cost expense (including attorneys' tees), claim, demand, suit, action,
judgment or recovery asserted against Baxter Healthcare, Corp by any third party, including any governmental authority,
bodily injury, (including death) or damage to property, arising from or in connection with Recipient's receipt transportation, handling
or other use of the ash, whether for
Signed (Ash Recipient):
Date:_L()
Ash Recipient's Mailing Address: — AV � ��2 2 ��
Intended Use of Ash and Crop Type: ,�� y o� /�
Expected Qty/Yr. � 7
---� Acres of Land: /SO
Baxter Representative Signature:
l age 2 of 3

Baxter Healthcare, Corp.
2859 Old Linville Road
Marion, North Carolina 28752
Ash Distribution Utilization Agreement (Valid thru 3/30/2025), Baxter Copy
Baxter Healthcare, Corp., is the Scneratox of the ash provided to . % the aforementioned ash is prohibited except in accardance with the instructions this sheet. %i(Recipient). Application of
Y
health and
Transport: Adequate provisions shall be taken to ensure that the transportation of ash does not cause nuisances and hazards to public
safety or otherwise cause an adverse impact (c,g., transport wet ash in leak -proof trucks or cover dry ash)_ Spill control
Provisions must be available during transportation or land application activities. Any spill occurring while ash is in transport or on the
application fields is the responsibility of the transporter.
Storage: The ash shall be adequately stoned to prevent wind erosion or surface runoff from carrying ash into any surface waters. The
use of wetting agents, berms, barriers, or tarps, may be necessary Under windy or rainy conditions or if erosion or runoff cannot be
controlled.
Application; When Using ash, the following shall apply:
• The ash application rates shall be limited to those that can be agn nornically justified (i.e., limited to that needed to meet die
liming requirements of the crops being grown on the land).
• Residual ash cake shall not be stockpiled for more than 60 days prior to land application
• Application of ash cake residuals shall not occur within 100 feet ofa public or private water supply
• Applicator of ash cake residuals shall not accur within 25 feet of surface water; such as intermittent and perennial streams,
perennial waterbodies, and wetlands.
• Copies of this Utilization Agreement, Ash permit No.WQ00f0689, and the Operation and Maintenance Plan shall be maintained
at the land application site when bulk residuals are being applied.
• Ash shall not be placed within one foot of the seasonal high water table or bedrock
• Ash shall not be applied to any site under the following conditions:
a Flooded, frozen, or snow-covered or other condition causing runoff
o During precipitation events or within 24-hrs following a 0.5" rainfall
o If the land application site does not have established vegetative cover crop
a If the application causes any nuisance conditions to adjacent property, natural resources, or wildlife
A summary of the ash chemical analyses is located on page 3 of the information sheet. Detailed laboratory results are available upon
request.
Title to the ash will transfer from Baxter Healthcare, Corp to Recipient upon delivery thereof. Thereafter, Baxter Healthcare, Corp
will have no responsibility and shall not be held liable by Recipient or any third party for any spill, misuse, misapplication or other
mishandling of the ash, Recipient acknowledges and agrees that the ash is being delivered by Baxter Healthcare, Corp to Recipient as
an accommodation to Recipient. In exchange therefore, Recipient agrees to indemnify, save and hold Baxter Healthcare, Corp
harmless from and against any and all liability, damage, loss, cost, expense (including attorneys' fees), claim, demand, suit, action,
judgment or recovery asserted against Baxter Healthcare, Corp by any third party, including any governmental authority, whether for
bodily injury (including death) or damage to property, arising from or in connection with Recipient's receipt,
or other use of the ash. P p transportation handling
Signed (Ash Recipient): Date: ? j�
Ash Recipient's Address: Q S
, -,zv1 /!t
Intended Use of Ash: n` , �' S p / l►rCr�/1 a2
Expected Qty/Yr: Acres of Land:
Baxter Representative Signature:
Page 2 of 3
Updated: January 2020

aceAnalytical
www.pacelabs.com
April 20, 2023
Mr. Ricky Styles
Baxter Healthcare
2859 Old Linville Road
Marion, NC 28752
RE: Project: Wood Boiler Ash
Pace Project No.: 92659559
Dear Mr. Styles:
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Enclosed are the analytical results for sample(s) received by the laboratory on March 29, 2023. The results relate only to
the samples included in this report. Results reported herein conform to the applicable TNIINELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Asheville
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Jonathan W Siddix for
Sarah Graham
[e-mail]
[phone]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 26

wmnalj cal
www.pacelabs.com
Project: Wood Boiler Ash
Pace Project No.: 92659559
Pace Analytical Services, LLC
9800 Kincey Ave, Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Laboratory ID: 99006
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
CERTIFICATIONS
South Carolina Certification #: 99006001
South Carolina Drinking Water Cert. #: 99006003
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Louisiana DoH Drinking Water #: LA029
VirginiaNELAP Certification #: 460221
South Carolina Laboratory ID: 99030
South Carolina Certification #: 99030001
VirginiaNELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analypcal Services, LLC. Page 2 of 26

aceAnalj6cal
www.pacelabs.com
SAMPLE ANALYTE COUNT
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project:
Pace Project No.:
Wood Boiler Ash
92669559
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92659559001
SP32923A
EPA6010D
1313131
17
PASI-A
EPA6010D
D13131
7
PASI-A
EPA6010D
DMN
1
PASI-A
EPA 7470A
NMP
1
PASI-A
EPA 74718
NMP
1
PASI-A
SW-846
KDF
1
PASI-C
EPA90460
YEG
1
PASI-A
None
MDW
1
PASI-A
TKN+NO3+NO2 Calculation
MDW
1
PASI-A
EPA 350.1 Rev 2.0 1993 Mod.
ARJ
1
PASI-A
EPA 351.2 Rev 2.0 1993
MFO
1
PASI-A
EPA 353.2 Rev 2.0 1993
MFO
3
PASI-A
EPA365.1 Rev 2.0 1993
Zip
1
PASI-A
92659559002
SP32923B
EPA6010D
0881
18
PASI-A
EPA 601OD
D8131
7
PASI-A
EPA6010D
DMN
1
PASI-A
EPA 7470A
NMP
1
PASI-A
EPA 7471B
NMP
1
PASI-A
SW-846
KDF
1
PASI-C
EPA9045D
YEG
1
PASI-A
None
MDW
1
PASI-A
TKN+NO3+NO2 Calculation
MDW
1
PASI-A
EPA 350.1 Rev 2.0 1993 Mod,
ARJ
1
PASI-A
EPA351.2 Rev 2.0 1993
MFO
1
PASI-A
EPA353.2 Rev 2.0 1993
MFO
3
PASI-A
EPA365.1 Rev 2.0 1993
Zip
1
PASI-A
PASI-A = Pace Analytical Services -Asheville
PAS I-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Servioes, LLC. Page 3 of 26

aceAna1j&ca1
www.Pacelabs.Com
ANALYTICAL RESULTS
Project: Wood Boller Ash
Pace Project No.: 92659559
Pace Analytical Services, LLC
9800 Kincey Ave, Suite 100
Huntersville, NC 28078
[phone]
Sample: SP32923A Lab ID: 92659559001 Collected: 03/28/23 09:30 Received: 03/29/23 17:32 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Analytical Method: EPA 601OD Preparation Method: EPA3050B
Pace Analytical Services -Asheville
Aluminum
8940 mg/kg
175
10
04/01/2312:30
04/18/2313:24
7429-90-5
Arsenic
ND mglkg
43.7
10
04/01/2312:30
04/1812313:24
7440-38-2
Barium
1460 mg/kg
17.5
10
04/01/2312:30
04/18/2313:24
7440-39-3
Cadmium
3.7 mg/kg
1.7
10
04/0112312:30
04/18/2313:24
7440-43-9
Calcium
114000 mglkg
437
10
04101/2312:30
04118/2313:24
7440-70-2
Chromium
17.3 mg/kg
8.7
10
04101/2312:30
04/18/2313:24
7440-47-3
Copper
132 mg/kg
87.4
10
04/01/2312:30
04/18/2313:24
7440-50-8
Iron
8570 mg/kg
874
10
04/01/2312:30
04/18/2313:24
7439-89-6
Lead
34.1 mg/kg
17.5
10
04/0112312:30
04/16/2313:24
7439-92-1
Magnesium
16600 mg/kg
175
10
04/01/2312:30
04/18/2313:24
7439-95-4
Manganese
3990 mg/kg
8.7
10
04/01/2312:30
04/1812313:24
7439-96-5
Molybdenum
ND mglkg
87.4
10
0410112312:30
04/1812313:24
7439-98-7
Nickel
17.6 mglkg
8.7
10
04/0112312:30
0411812313:24
7440-02-0
Potassium
15100 mg/kg
8740
10
04/01/2312:30
0411812313:24
7440-09-7
Selenium
ND mglkg
17.5
10
04101/2312:30
04/18/2313:24
7782-49-2
Sodium
11800 mg/kg
8740
10
04101/2312:30
04/18/2313:24
7440-23-5
Zinc
343 mg/kg
17,5
10
04/01/2312:30
04/18/2313:24
7440-66-6
6010 MET ICP, TCLP
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Leachate Method/Date: EPA 1311; 04/07/23 14:59
Initial pH: 1.76, Final pH: 2
Pace Analytical Services -Asheville
Arsenic
ND mg/L
0.050
1
04/11/23 01:26
04/18/23 01:14
7440-38-2
Barium
2.5 mg/L
0.25
1
04/11/23 01:26
04/18/23 01:14
7440-39-3
Cadmium
ND mg/L
0.0050
1
04/11/23 01:26
04/18/23 01:14
7440-43-9
Chromium
ND mg/L
0,050
1
04/11/23 01:26
04/18/23 01:14
7440-47-3
Lead
ND mg/L
0,025
1
04/11/23 01:26
04/18/23 01:14
7439-92-1
Selenium
ND mg/L
0.10
1
04/11/23 01:26
04/18/23 01:14
7782-49-2
Silver
ND mg/L
0.025
1
04/11/23 01:26
04/18/23 01:14
7440-22-4
Sodium Adsorption Ratio, SAR
Analytical Method: EPA 6010D
Pace Analytical Services -Asheville
Sodium Adsorption Ratio
12.3 meg1L
1
04/19/23 17:57
7470 Mercury, TCLP
Analytical Method: EPA 7470A Preparation Method: EPA
7470A
Leachate Method/Date: EPA 1311; 04/07/23 14:59 Initial pH: 1.76; Final
pH: 2
Pace Analytical Services - Asheville
Mercury
ND mg/L
0,00020
1
04111/2310A2
04/1212311:42
7439-97-6
7471 Mercury
Analytical Method: EPA 7471 B Preparation Method: EPA
7471 B
Pace Analytical Services -Asheville
Mercury
ND mg/kg
0.0087
1
04112/2310:07
04/12/2313:28
7439-97-6
D3
D3
D3
N2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/20/2023 10:18 AM without the written consent of Pace Analytical Services, LLC. Page 4 of 26

aceAnalytical
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ANALYTICAL RESULTS
Project: Wood Boiler Ash
Pace Project No.: 92659559
Pace Analytical Services, LLC
9800 Kincey Ave. Suite1o0
Huntersville, NC 28078
[phone]
Sample: SP32923A Lab ID: 92659559001 Collected: 03/28/23 09:30 Received: 03/29/23 17:32 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qua]
Percent Moisture Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture 50.7 % 0.10 1 03/30/23 14:15 N2
9045 pH Sall
Analytical Method: EPA 9045D
Pace Analytical Services -Asheville
pH at 25 Degrees C
9.0 Std. Units 0.10
1 04/10/23 13:13 Q
Plant Available Nitrogen
Analytical Method: None
Pace Analytical Services -Asheville
Plant Available Nitrogen
924 mg/kg
1 04/05/23 18:51 N2
Total Nitrogen Calculation
Analytical Method: TKN+NO3+NO2 Calculation
Pace Analytical Services -Asheville
Nitrogen
3080 mg/kg 40.0
1 04106/2318:56 7727-37-9
350.1 Ammonia
Analytical Method: EPA 350.1 Rev 2.0 1993 Mod.
Preparation Method: EPA 350.1 Rev 2.0 1993 Mod.
Pace Analytical Services - Asheville
Nitrogen, Ammonia
NO mglkg 19.9
1 03131/2315:20 04/01/2312:51 7664-41-7
351.2 Total Kjeldahl Nitrogen
Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993
Pace Analytical Services - Asheville
Nitrogen, Kjeldahl, Total
3080 mg/kg 88.2
1 04/03/23 18:24 04/04/23 04:51 7727-37-9
353.2 Nitrogen, NO2/NO3
Analytical Method: EPA 353.2 Rev 2.0 1993 Preparation Method: EPA 353.2 Rev 2.0 1993
Pace Analytical Services -Asheville
Nitrogen, NO2 plus NO3
ND mg/kg 8.1
1 03/29/23 22:43 03/30/23 01:35
Nitrogen, Nitrate
ND mg/kg 8.1
1 03/29/23 22:43 03/30/23 01:35 14797-55-8
Nitrogen, Nitrite
NO mg/kg 8.1
1 03/29/23 22:43 03/30/23 01:35 14797-65-0
365.1 Phosphorus, Total
Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation Method: EPA 365.1 Rev 2.0 1993
Pace Analytical Services -Asheville
Phosphorus
2290 mg/kg 37.6
20 0313112311:44 03/31/2314:41 7723-14-0
............ -
Sample: SP32923B Lab lD: 92659559002 Collected: 03/28/23 09:30 Received: 03/29/23 17:32 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual
6010 MET IC
Analytical Method: EPA 601 OD Preparation Method: EPA 3050E
Pace Analytical Services -Asheville
Aluminum
7560 mg/kg 135 10 04101/2312:30 04/1812313:27
7429-90-5
Arsenic
ND mg/kg 33.9 10 04/01/2312:30 04118/2313:27
7440-38-2 D3
Barium
1430 mg/kg 13.5 10 04/0112312:30 04/18/2313:27
7440-39-3
Cadmium
3.8 mg/kg 1.4 10 04/01/2312:30 04118/2313:27
7440-43-9
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/20/2023 10:18 AM
without the written consent of Pace Analytical Services, LLC.
Page 5 of 26

aceAnalytical
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ANALYTICAL RESULTS
Project: Wood Boiler Ash
Pace Project No.: 92659559
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: SP329238 Lab ID: 92659559002 Collected: 03/28/23 09:30 Received: 03/29/23 17:32 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted forpercent moisture, sample size and any dilutions.
Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual
6010 MET ICP
Analytical Method: EPA 601 OD Preparation Method: EPA 3050E
Pace Analytical Services - Asheville
Calcium
116000 mg/kg 339 10 04101/2312:30
04/1812313:27
7440-70-2
Chromium
16.1 mg/kg 6.8 10 04/0112312:30
04/1812313:27
7440-47-3
Copper
141 mg/kg 67.7 10 04/0112312:30
04/1812313:27
7440-50-8
Iron
7180 mg/kg 677 10 0410112312:30
04118/2313:27
7439-89-6
Lead
37.5 mglkg 13.5 10 0410112312:30
04118/2313:27
7439-92-1
Magnesium
16200 mglkg 135 10 0410112312:30
0411812313:27
7439-95-4
Manganese
3920 mglkg 6.8 10 04101/2312:30
04/1812313:27
7439-96-5
Molybdenum
ND mg/kg 67.7 10 04/01/2312:30
04/18/2313:27
7439-98-7
D3
Nickel
17.4 mglkg 6.8 10 04/01/2312:30
04/18/2313:27
7440-02-0
Potassium
16200 mg/kg 6770 10 04/01/2312:30
04/1812313:27
7440-09-7
Selenium
ND mglkg 13.5 10 0410112312:30
04/18/2313:27
7782-49-2
D3
Silver
ND mg/kg 6.8 10 04101/2312:30
04/1812313:27
7440-22-4
D3
Sodium
12900 mglkg 6770 10 04/01/2312:30
04/18/2313:27
7440-23-5
Zinc
360 mg/kg 13.5 10 04/0112312:30
04/18/2313:27
7440-66-6
6010 MET ICP, TCLP
Analytical Method: EPA 601 OD Preparation Method: EPA 3010A
Leachate Method/Date: EPA 1311; 04/07/23 14:59 Initial pH: 1.94; Final
pH: 2
Pace Analytical Services - Asheville
Arsenic
NO mg/L 0.050 1 04/11/23 01:26
04/18/23 01:18
7440-38-2
Barium
2.1 mg/L 0.25 1 04/11/23 01:26
04/18/23 01:18
7440-39-3
Cadmium
NO mg/L 0.0050 1 04/11/23 01:26
04/18/23 01:18
7440-43-9
Chromium
NO mg/L 0.050 1 04/11/23 01:26
04/18/23 01:18
7440-47-3
Lead
ND mg/L 0.025 1 04/11/23 01:26
04/18/23 01:18
7439-92-1
Selenium
ND mg/L 0.10 1 04/11/23 01:26
04/18/23 01:18
7782-49-2
Silver
ND mg/L 0.025 1 04/11/23 01:26
04/18/23 01:18
7440-22-4
Sodium Adsorption Ratio, SAR
Analytical Method: EPA 601 OD
Pace Analytical Services -Asheville
Sodium Adsorption Ratio
13.4 meq/L 1
04/20/2308:04
N2
7470 Mercury, TCLP
Analytical Method: EPA 7470A Preparation Method: EPA 7470A
Leachate Method/Date: EPA 1311, 04/07/23 14:59 Initial pH: 1.94; Final
pH: 2
Pace Analytical Services - Asheville
Mercury
ND mg/L 0.00020 1 04/11/2310:42
04/1212311:44
7439-97-6
7471 Mercury
Analytical Method: EPA 7471 B Preparation Method: EPA 7471 B
Pace Analytical Services -Asheville
Mercury
ND mg/kg 0,0085 1 04112/2310:07
04/12/2313:31
7439-97-6
Percent Moisture
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
50.8 % 0.10 1
03/30/23 14:16
N2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/20/2023 10:18 AM
without the written consent of Pace Analytical Services, LLC.
Page 6 of 26

aceAnalyfical
www.pacolsbs.com
ANALYTICAL RESULTS
Project: Wood Boiler Ash
Pace Project No.: 92659559
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: SP32923B
Lab ID: 92669559002 Collected: 03/28/23 09:30 Received: 03/29/23 17:32 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters
Results Units Report Limit DF Prepared Analyzed CAS No. Qual
9045 pH Soil
Analytical Method: EPA 9045D
Pace Analytical Services -Asheville
pH at 25 Degrees C
9.1 Std. Units 0.10 1 04/10/23 13:15 Q
Plant Available Nitrogen
Analytical Method: None
Pace Analytical Services - Asheville
Plant Available Nitrogen
1400 mg/kg 1 04/05/23 18:51 N2
Total Nitrogen Calculation
Analytical Method: TKN+NO3+NO2 Calculation
Pace Analytical Services - Asheville
Nitrogen
4680 mg/kg 40.0 1 04/05/2318:56 7727-37-9
350.1 Ammonia
Analytical Method: EPA 350.1 Rev 2.0 1993 Mod. Preparation Method: EPA 350.1 Rev 2,0 1993 Mod.
Pace Analytical Services - Asheville
Nitrogen, Ammonia
ND mglkg 17,2 1 03131/2315:20 04/0112312:52 7664-41-7
351.2 Total Kjeldahl Nitrogen
Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993
Pace Analytical Services - Asheville
Nitrogen, Kjeldahl, Total
4680 mg/kg 462 5 04/03/23 18:24 04/04/23 06:22 7727-37-9
353.2 Nitrogen, N021NO3
Analytical Method: EPA 353.2 Rev 2.0 1993 Preparation Method: EPA 353.2 Rev 2.0 1993
Pace Analytical Services -Asheville
Nitrogen, NO2 plus NO3
ND mglkg 7.9 1 03/299/23 22:43 03/30/23 01:38
Nitrogen, Nitrate
ND mglkg 7.9 1 03/29/23 22:43 03/30/23 01:38 14797-55-8
Nitrogen, Nitrite
ND mglkg 7.9 1 03/29/23 22:43 03/30/23 01:38 14797-65-0
365.1 Phosphorus, Total
Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation Method: EPA 365.1 Rev 2.0 1993
Pace Analytical Services -Asheville
Phosphorus
1860 mg/kg 39.1 20 03/31/23 11:44 03/31/23 14:42 7723-14-0
Date: 04/20/2023 10:18 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC,
Page 7 of 26

aceAnalytieal "'
www.pacelabs.com
Project:
Wood Boiler Ash
Pace Project No.:
92659559
QC Batch:
767192
QC Batch Method:
EPA 7470A
Associated Lab Samples: 92659559001, 92659559002
QUALITY CONTROL DATA
Analysis Method: EPA 7470A
Analysis Description: 7470 Mercury TCLP
Laboratory: Pace Analytical Services -Asheville
METHOD BLANK: 3981284 Matrix: Water
Associated Lab Samples: 92659559001, 92659559002
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Mercury mg/L ND 0.00020 04/1212311:24
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE: 3983482
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Mercury mg1L 0.0025 0,0029 117 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3983483 3983484
MS MSD
92661001001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Mercury mg/L ND 0.0025 0.0025 0.0028 0.0027 110 109 75-125 1
Results presented on this page are In the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/20/2023 10:18 AM without the written consent of Pace Analytical Services, LLC.
Page 8 of 26

aceAnalytical
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Project: Wood Boiler Ash
Pace Project No.: 92659559
QC Batch: 766989
QC Batch Method: EPA 7471 B
Associated Lab Samples: 92659559001, 92659559002
METHOD BLANK: 3982406
Associated Lab Samples: 92659559001, 92659559002
Parameter Units
Mercury mg/kg
QUALITY CONTROL DATA
Analysis Method: EPA 7471 B
Analysis Description: 7471 Mercury
Laboratory: Pace Analytical Services - Asheville
Matrix: Solid
Blank Reporting
Result Limit Analyzed Qualifiers
ND 0.0060 04/12/2313:17
Pace Analytical Services, LLC
9800 K€nceyAve. Suite 100
Huntersville, NO 28078
[phone]
..........
LABORATORY CONTROL SAMPLE: 3982407
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Mercury mg/kg 0.083 0.087 105 80-120
................
MATRIX SPIKE 8 MATRIX SPIKE DUPLICATE: 3982408 3982409
MS MSD
92659537001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Mercury mg/kg 0,57 0.082 0,086 0.99 0.89 514 382 75-125 10 i(MI)
Results presented on this page are in the units Indicated by the -Units- column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/20/2023 10:18 AM without the written consent of Pace Analytical Services, LLC.
Page 9 of 26

aceAnalytical
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Project: Wood Boiler Ash
Pace Project No.: 92659559
QC Batch: 765361
QC Batch Method: EPA 3050B
Associated Lab Samples: 92659559001, 92659559002
QUALITY CONTROL DATA
Analysis Method: EPA 601 OD
Analysis Description: 6010 MET
Laboratory: Pace Analytical Services -Asheville
METHOD BLANK: 3974028
Associated Lab Samples: 92659559001, 92659559002
Parameter Units
Matrix: Solid
Blank Reporting
Result Limit
Analyzed
Aluminum
mg/kg
NO
10.0
04/05/23 22:56
Arsenic
mg/kg
NO
2.5
04/05/23 22:56
Barium
mg/kg
NO
1,0
04/05/23 22:56
Cadmium
mg/kg
NO
0.10
04/05/23 22:56
Calcium
mg/kg
NO
25.0
04/05/23 22:56
Chromium
mglkg
NO
0.50
04/05/23 22:56
Copper
mglkg
NO
5.0
04/05/23 22:56
Iron
mg/kg
NO
50.0
04/05/23 22:56
Lead
mg/kg
NO
1.0
04/05/23 22:56
Magnesium
mglkg
NO
10.0
04/05/23 22:56
Manganese
mg/kg
ND
0.50
04/05/23 22:56
Molybdenum
mg/kg
NO
5.0
04/05/23 22:56
Nickel
mg/kg
ND
0.50
04/05/23 22:56
Potassium
mg/kg
NO
500
04/05/23 22:56
Selenium
mg/kg
NO
1.0
04/05/23 22:56
Sodium
mglkg
NO
500
04/05/23 22:66
Zinc
mg/kg
NO
1.0
04/05/23 22:56
Qualifiers
LABORATORY CONTROL SAMPLE:
Parameter
3974029
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
Aluminum
mglkg
500
480
96
80-120
Arsenic
mg/kg
50
45.5
91
80-120
Barium
mglkg
50
48.7
97
80-120
Cadmium
mglkg
50
48.0
96
80-120
Calcium
mglkg
500
502
100
80-120
Chromium
mglkg
50
47.9
96
80-120
Copper
mg/kg
50
48.8
98
80-120
Iron
mg/kg
500
491
98
80-120
Lead
mg/kg
50
48.7
97
80-120
Magnesium
mglkg
500
468
94
80-120
Manganese
mglkg
50
48.0
96
80-120
Molybdenum
mglkg
50
47.3
95
80-120
Nickel
mglkg
50
48.3
97
80-120
Potassium
mg/kg
500
NO
98
80-120
Selenium
mg/kg
50
43.4
87
80-120
Sodium
mg/kg
500
505
101
80-120
Zinc
mglkg
50
48.1
96
80-120
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/20/2023 10:18 AM without the written consent of Pace Analytical Services, LLC. Page 10 of 26

aceAnalytical
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QUALITY CONTROL DATA
Project: Wood Boiler Ash
Pace Project No.: 92659559
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Wuntersville, NC 28078
[phone]
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
3974030
3974031
MS
MSD
92658175001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Aluminum
mg/kg
5480
439
439
6520
6610
236
256
75-125
1 J(M1)
Arsenic
mg/kg
148
43.9
43.9
183
186
80
86
75-125
2
Barium
mg/kg
343
43.9
43.9
371
374
65
72
75-125
1 J(M1)
Cadmium
mg/kg
NO
43.9
43.9
41.2
42.0
94
96
75-125
2
Calcium
mg/kg
9590
439
439
9540
9660
-12
15
75-125
1 J(M1)
Chromium
mg/kg
87.9
43.9
43.9
136
138
109
114
75-125
2
Copper
mg/kg
297
43.9
43.9
331
332
76
79
75-125
0
Iron
mg/kg
331000
439
439
261000
328000
-18200
-617
75-125
27 J(M1),
J(RI)
Lead
mpg
76.1
43.9
43.9
113
117
84
93
75-125
3
Magnesium
mg/kg
30800
439
439
31200
31400
95
134
75-125
1 J(M1)
Manganese
mg/kg
21300
43.9
43.9
20400
20700
•2100
-1450
75-125
1 J(M1)
Molybdenum
mg/kg
NO
43.9
43.9
581
59A 1
90
92
75-125
Nickel
mg/kg
225
43.9
43.9
262
263
85
88
75-125
0
Potassium
mg/kg
NO
439
439
ND
ND
108
111
75-125
Selenium
mg/kg
NO
43.9
43.9
30.9
25.4
70
58
75-125
20 J(M1)
Sodium
mg/kg
NO
439
439
NO
ND
88
89
75-125
Zinc
mg/kg
235
43.9
43.9
264
268
65
76
75-125
2 J(M1)
Results presented on this page are in the units indicated by the "units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/20/2023 10:18 AM without the written consent of Pace Analytical Services, LLC.
Page 11 of 26

aceAnaljftal
W".pacelab"M
Project:
Wood Boiler Ash
Pace Project No.:
92659559
QC Batch:
767189
QC Batch Method:
EPA 3010A
Associated Lab Samples: 92659559001, 92659559002
METHOD BLANK: 3981284
Associated Lab Samples:
92659559001, 92659559002
Parameter
Units
Arsenic
mg/L
Barium
mg/L
Cadmium
mg1L
Chromium
mg/L
Lead
mg/L
Selenium
mg/L
Silver
mg/L
LABORATORY CONTROL. SAMPLE:
3983475
Parameter
Units
Arsenic
mg/L
Barium
mg/L
Cadmium
mg/L
Chromium
mg/L
Lead
mg/L
Selenium
mg/L
Silver
mg1L
QUALITY CONTROL DATA
Analysis Method: EPA 6010D
Analysis Description: 6010 MET TCLP
Laboratory: Pace Analytical Services - Asheville
Matrix: Water
Blank
Result
Reporting
Limit
Analyzed
ND
0.050
04/18/23 00:50
ND
0.25
04/18/23 00:50
ND
0.0050
04/18/23 00:50
ND
0.050
04/18/23 00:50
NO
0.025
04/18/23 00:50
ND
0.10
04/16/23 00:50
NO
0.025
04/18/23 00:50
Qualifiers
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Spike
LCS
LCS
%fl Rec
Conc.
Result
% Rec
Limits Qualifiers
2.5
2.5
102
80-120
2.5
2.4
97
80-120
2.5
2.4
97
80-120
2.5
2.4
97
80-120
2.5
2.4
95
80-120
2.5
2.6
102
80-120
1.2
1.2
99
80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
3983476
3983477
MS
MSD
92661001001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Arsenic
mg/L
0.0151
2.5
2.5
2.3
2.5
93
101
75-125
9
Barium
mg/L
1.8
2.5
2.5
3.9
4.3
86
99
75-125
8
Cadmium
mg/L
0.10
2.5
2.5
2.3
2.5
90
98
75-125
8
Chromium
mg/L
0.0151
2.5
2.5
2.3
2.5
90
98
75-125
8
Lead
mg/L
0.096
2.5
2.5
2.3
2.5
89
97
75-125
8
Selenium
mg/L
ND
2.5
2.5
2.3
2.6
94
102
75-125
8
Silver
mg/L
ND
1.2
1.2
1.1
1.2
90
98
75-125
8
Results presented on this page are in the units indicated by the "Units' column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/20/2023 10:18 AM without the written consent of Pace Analytical Services, LLC. Page 12 of 26

acmnalyrical
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Project: Wood Boiler Ash
Pace Project No.: 92659559
QC Batch: 764956
QC Batch Method: SW-846
Associated Lab Samples: 92659559001, 92659559002
SAMPLE DUPLICATE: 3972018
Parameter Units
Percent Moisture %
QUALITY CONTROL DATA
Analysis Method: SW-846
Analysis Description: Dry Weight/Percent Moisture
Laboratory: Pace Analytical Services - Charlotte
92659559002 Dup
Result Result RPD Qualifiers
50.8 50.4 1 N2
SAMPLE DUPLICATE: 3972020
92659388001 Dup
Parameter Units Result Result
Percent Moisture % 12.6 12.1
RPD Qualifiers
4 N2
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Results presented an this page are in the units indicated by the "Units- column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/20/2023 10:18 AM without the written consent of Pace Analytical Services, LL.C,
Page 13 of 26

aceAnaljftal
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QUALITY CONTROL DATA
Project: Wood Boiler Ash
Pace Project No.: 92659559
QC Batch: 767058 Analysis Method: EPA 9045D
QC Batch Method: EPA 9045D Analysis Description: 9045 pH
Laboratory: Pace Analytical Services - Asheville
Associated Lab Samples: 9265955900'1, 92659559002
SAMPLE DUPLICATE: 3982729
92661014001 Dup
Parameter Units Result Result RPD Qualifiers
pH at 25 Degrees C Std. Units 8.3 8.3 00
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Results presented on this page are in the units indicated by the "units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/20/2023 10:18 AM without the written consent of Pace Analytical Services, LLC.
Page 14 of 26

1(�;aneAnalXical
wlwrpaceiabs.ctlm
I
Project: Woad Boiler Ash
Pace Project No.: 92659559
QC Batch: 765257
QC Batch Method: EPA 350.1 Rev 2.0 1993 Mod.
Associated Lab Samples: 92659559001, 92659559002
METHOD BLANK: 3973592
Associated Lab Samples: 92659559001, 92659559002
Parameter Units
Nitrogen, Ammonia mglkg
QUALITY CONTROL DATA
Analysis Method:
Analysis Description:
Laboratory:
Matrix: Solid
EPA 350.1 Rev 2.0 1993 Mod.
350.1 Ammonia
Pace Analytical Services -Asheville
Blank Reporting
Result Limit Analyzed Qualifiers
ND 8.6 04/01/2312:35
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE: 3973593
Spike LCS LCS % Rea
Parameter Units Conc. Result % Rea Limits Qualifiers
Nitrogen, Ammonia mg/kg 446 441 99 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3973594 3973595
MS MSD
92659071001 Spike Spike MS MSD MS MSD % Rea
Parameter Units Result Conc. Conc. Result Result % Rea % Rec Limits RPD Qual
Nitrogen, Ammonia mg/kg ND 3320 3720 3430 3820 103 102 90-110 11 J(RI)
Results presented on this page are In the units indicated by the -Units- column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/20/2023 10:18 AM without the written consent of Pace Analytical Services, LLC. Page 15 of 26

aceAnalytical
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Project: Wood Boiler Ash
Pace Project No.: 92659559
QC Batch: 765482
QC Batch Method: EPA 351.2 Rev 2.0 1993
Associated Lab Samples: 92659559001, 92659559002
METHOD BLANK: 3974551
Associated Lab Samples: 92659559001, 92659559002
Parameter Units
Nitrogen, Kjeldahl, Total mglkg
QUALITY CONTROL DATA
Analysis Method: EPA 351.2 Rev 2.0 1993
Analysis Description: 351.2 TKN
Laboratory: Pace Analytical Services -Asheville
Matrix: Solid
Blank Reporting
Result Limit Analyzed Qualifiers
ND 50.0 04/04/23 04:39
LABORATORY CONTROL SAMPLE: 3974552
Spike LC5
Parameter Units Conc. Result
Nitrogen, Kjeldahl, Total mglkg 1000 961
Pace Analytical Services, LLC
9800 Kincey Ave, Suite 100
Huntersville, NC 28078
[phone]
LCS % Rec
% Rec Limits Qualifiers
96 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3974553
3974554
MS
MSD
92659071001 Spike
Spike
MS
MSD MS MSD % Rec
Parameter Units Result Conc.
Conc.
Result
Result % Rec % Rec Limits RPD Qual
Nitrogen, Kjeldahl, Total mglkg 46100 5960
7450
47500
57300 23 150 90-110 19 J(M1),
J(R1)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full.
Date: 04/20/2023 10:18 AM without the written consent of Pace Analytical Services, LLC.
Page 16 of 26

aceAnalytical*
tvww.paeelabscoln
QUALITY CONTROL DATA
Project: Wood Boiler Ash
Pace Project No.: 92659559
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QC Batch: 764746
Analysis Method: EPA 353.2 Rev 2.0 1993
QC Batch Method: EPA 353.2 Rev 2.0 1993
Analysis Description: 353.2 Nitrate + Nitrite
Laboratory: Pace Analytical Services - Asheville
Associated Lab Samples: 92659659001, 92659559002
METHOD BLANK: 3971086
Matrix: Solid
Associated Lab Samples: 92659559001, 92659559002
Blank Reporting
Parameter
Units
Result Limit
Analyzed Qualifiers
Nitrogen, Nitrate
mglkg
ND 4.0
03/30/23 01:33
Nitrogen, Nitrite
mg/kg
ND 4.0
03/30/23 01:33
Nitrogen, NO2 plus NO3
mg/kg
NO 4.0
03/30/23 01:33
LABORATORY CONTROL SAMPLE:
3971087
Spike LCS
LCS % Rec
Parameter
Units
Conc. Result
% Rec Limits Qualifiers
Nitrogen, Nitrate
mglkg
15 14.9
100 90-110
Nitrogen, Nitrite
mg/kg
10 10.0
100 90-110
Nitrogen, NO2 plus NO3
mg/kg
25 25.0
100 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3971088
3971089
MS MSD
92659559001
Spike Spike MS
MSD MS MSD
% Rec
Parameter
Units Result
Conc. Conc. Result
Result % Rec % Rec
Limits RPD Qual
Nitrogen, Nitrate
mg/kg ND
30.2 30 35.7
34.8 118 116
90-110 3
Nitrogen, Nitrite
mg/kg ND
20.3 19.9 21.2
20.7 99 98
90-110 2
Nitrogen, NO2 plus NO3
mg/kg ND
50.5 49.9 56.9
55.5 106 105
90-110 2
Results presented on this page are In the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/20/2023 10:18 AM without the written consent of Pace Analytical Services, LLC,
Page 17 of 26

aceAnalj cal e
www.pacalabsxam
QUALITY CONTROL DATA
Project: Wood Boiler Ash
Pace Project No.: 92659559
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QC Batch: 765021
Analysis Method: EPA 365.1 Rev 2.0 1993
QC Batch Method: EPA 365.1 Rev 2.0 1993
Analysis Description: 365.1 Phosphorus, Total
Laboratory: Pace Analytical Services - Asheville
Associated Lab Samples: 92659559001, 92659559002
METHOD BLANK: 3972470
Matrix: Solid
Associated Lab Samples: 92659559001, 92659559002
Blank Reporting
Parameter Units
Result Limit
Analyzed Qualifiers
Phosphorus mg/kg
ND 0.94
03/31/2314:18
LABORATORY CONTROL SAMPLE: 3972471
Spike LCS
LCS % Rec
Parameter Units
Conc. Result
% Rec Limits Qualifiers
Phosphorus mg/kg
47.2 48.4
103 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3972472
3972473
MS MSD
92667900001
Spike Spike MS
MSD MS MSD
% Rec
Parameter Units Result
Conc. Conc. Result
Result % Rec % Rec
Limits RPD Qual
Phosphorus mg/kg 86.8
84A 74.3 104
81.5 20 -7
90-110 24 J(M1),
J(RI)
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3972474 3972475
MS MSD
92659168001
Spike Spike MS
MSD MS MSD
% Rec
Parameter Units Result
Conc. Conc. Result
Result % Rec % Rec
Limits RPD Qual
Phosphorus mg/kg 88.6
90.9 87.6 96.2
82.7 8 -7
90-110 15 J(M1),
J(RI)
Results presented on this page are in the units indicated by the "units" column except whore an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/20/2023 10:18 AM without the written consent of Pace Analytical Services, LLC.
Page 18 of 26

aceAnalj6cal
i wwiw.lweelahs.com
1
QUALIFIERS
Project: Wood Boiler Ash
Pace Project No.: 92659559
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
MDL -Adjusted Method Detection Limit.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270, The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI -The NEL4C Institute.
ANALYTE QUALIFIERS
I The reported value is between the laboratory method detection limit and the laboratory practical quantitation limit.
D3 Sample was diluted due to the presence of high levels of non -target analytes or other matrix interference.
i(MI) Estimated Value. Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS)
recovery.
J(R1) Estimated Value. RPD value was outside control limits.
N2 The lab does not hold NELACIT'NI accreditation for this parameter but other accreditations/certifications may apply. A
complete list of accreditationslcertifications is available upon request.
Q Sample held beyond the accepted holding time. Sample was received outside EPA method holding time.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/20/2023 10:18 AM without the written consent of Pace Analytical Services, LLC, Page 19 of 26

aceAnatytica!
www.pacelabs.cam
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: Wood Boiler Ash
Pace Project No.: 92659559
Pace Analytical Services, LLC
9800 Kincey Ave, Suite 100
Huntersville, NC 28078
[phone]
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Analytical
Batch
92659559001
SP32923A
EPA 3050B
765361
EPA 601OD
765373
92659559002
SP329238
EPA 3050B
765361
EPA 6010D
765373
92659559001
SP32923A
EPA 3010A
767189
EPA 6010D
767205
92659559002
SP32923B
EPA 3010A
767189
EPA 6010D
767205
92659559001
SP32923A
EPA 60100
769100
92659559002
SP32923B
EPA 6010D
769159
92659559001
SP32923A
EPA 7470A
767192
EPA 7470A
767322
92659559002
SP32923B
EPA 7470A
767192
EPA 7470A
767322
92659559001
SP32923A
EPA 7471B
766989
EPA 74718
767541
92659559002
SP32923B
EPA 7471B
766989
EPA 74718
767541
92659559001
SP32923A
SW-846
764956
92659559002
SP32923B
SW-846
764956
92659559001
SP32923A
EPA 9045D
767058
92659559002
SP32923B
EPA 9045D
767058
92659559001
SP32923A
None
766262
92659559002
SP329238
None
766262
92659559001
SP32923A
TKN+NO3+N 02
766263
Calculation
92659559002
SP32923B
TKN+N 03+NO2
766263
Calculation
92659569001
SP32923A
EPA 350.1 Rev 2.0 1993
765257
EPA 3501 Rev 2.0 1993
765351
Mod.
Mod.
92659559002
SP32923B
EPA 350.1 Rev 2.0 1993
765257
EPA 350.1 Rev 2.0 1993
766351
Mod,
Mod.
92659559001
SP32923A
EPA 351.2 Rev 2.0 1993
765482
EPA 351.2 Rev 2.0 1993
765660
92659559002
SP32923B
EPA 351.2 Rev 2.0 1993
765482
EPA 351.2 Rev 2.0 1993
766660
92659559001
SP32923A
EPA 353.2 Rev 2.0 1993
764746
EPA 353.2 Rev 2.0 1993
764751
92659559002
SP32923B
EPA 353.2 Rev 2.0 1993
764746
EPA 353.2 Rev 2.0 1993
764751
92659559001
SP32923A
EPA 365.1 Rev 2.0 1993
765021
EPA 365.1 Rev 2.0 1993
765209
92659559002
SP32923B
EPA 365.1 Rev 2.0 1993
765021
EPA 365.1 Rev 2.0 1993
765209
Date: 04/20/2023 10:18 AM
REPORT OF LABORATORY ANALYSIS
This report shall not he reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 20 of 26

EIC#_TItle: ENV+RM4HUN1oOO83 v02 Sample Condition Upon Receipt
/��CE ' - � -
effec#ivo Date:11/14/2022 8:18:30 AM
Laboratory ,ceiviri ',$t IMpleS:
AshavVeQ EdOpEj GreenwoodEl. Hutttetsvllle ❑ Raleigh❑ Mechenlesvil#e❑ AthwteQ KemckmVille❑
Client Name: je
proyt#t. NO : 92659559
Courlert LJ Fed txc UUPS 11 LISPS ClleOn,
❑ e. ❑H1111
Commercial QPacOther ]
0-dto(lyteasI Present? ❑Yas
Nay Seals Intact? [Ives
f� ,
l'i 4kint Material: ❑ bubble Wrap ❑ Bubble BS0. 14 None ❑ Other
Tltarmottieter. -
.d Ili Gun Irl:. ��� Ty" pT ke; ,owet
Corn3tNan Forfar: to
wet
Temp: Add/Subtract ('Q
Cooler Temp CoOd0d'
USDABtgtdaliWShc (0 NgAo eater sample)
Dld satmplesoillinotolin atau*mntlne tone wlibid1ha-Uhtted StRtmv rA Nv "rr
0aitollpltiadsa Person F. wpInlnR Cgritentss
© Blue I] None
Bk4o"`Tissua Frozen?
❑Yes .�Na Cjr,jA
Temp Ihodd te above frett143a 6T
QSarnRW%wt of teniidker)& i _mples on ice, copliM process
has begun
including Ilan i l mid Poeri; Rrcd)? dMs ❑ Nti
6*1 n of CuRo0yP►rriren.
Yes
� No
� N/A
] .
SamplesArtWed w0in Hatd:41mo?
Yas
0111a
❑N/A
2,
Short Holt! Timf Aram�r,, c72 hr.)?
Yts
Oft
❑N/A
3.
Rush Turn AraundOr"fie tad?
Qres
®tie
© A
A.
SvmdantVolunie?
b
.I3NP
DH/A
S.
Correct F.ontalners V"d?.
0fm
(3N/A
6.
. -Pace ContalnersUsed?
Yes
0No
Ord/A
Contalner3lntact?Qkes
❑Ho
O
❑H/A
7.
Dissolved ads) is: SArh lea Field Filtered?
Y
C1K/A
8.
Sample Labels&E C?
©WA
5.
-Includes. QatatnmefloLmmos wrix;
_
Head ace in VOAMalaa k5-6mm ?
DYAS
ONO
A
10
Trip'Slank Present?
Oyes
ONO
A
lf.
ITri BlanitCusttld Se 1aPresent7
©Yes
ONO
&A
COMMENTS/SAMPLED
L
CLIENTt4t3T1 lot ID of�'o It corttalners
CLIENT
FtCATiDht/11ESOLtIT0l
Person cantatted: Date/Time;
Praiarct Manager SCUR l(AVIew;
"act MauaagerSRF ReVWW,
Date;
Date
Hera oats se WId? UYaS U No
Page 21 of 26

DC#_°fitle: ENV-FRM.HUNj-0083 v02 Sample Condition Upon Receipt
Effectiva Date:11/14/M2
* Check mark top half rif bax if pH and/or dathlorinatian, (s verified and
Within the:Ameptanca range.for preservation sarnples,.;
i`?c'ceptians. Vt3�, Cpiifarm, TOC, 0'R and Grease, ORO/8©is (wafer ,DDC, LLNg.
"*Batton half of box b u fish number of bottles
*'k#Check,R:un0.reserv00 Nitrates for chlorine
Frafcct; WO## : 92659559
PH-. SHO Due Date: 04/13/23
CLIENT: 92—Haxt,er
p,
is
cx.
,�
�
�
n;:
�
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'4'
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=
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L
4 r�Si:
F)p
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f6
1D6enm
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�4t
aRbY1"YG?I
Waf
0 ;
is
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+.iAiYJa
>:
rf3i
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11�:r
. ry•,
—XNf-
I
\\N\
�.
3
1
L
\dN
.A
A
NN
I
5
6,
.7
_g
9
pHAdj stment Log for Preserved Samples
5arppia ID Type of Praservatiw I pH upon receipt flake.WdSi vatlort adItisted: I lima pteserwAlon Amount Of Preservative & ' tot sr.,.
u .n
Note: Whar+evetthere isadlStrep6i y.affeetlggNorthCarolinacotn'pBaneesamples,acopyofthlsformwill6esenttotheNorthCarofir+aDENR.CertillcetkmOfficefl.e.
Out at hold, iintbrrect pres&r`pativst aut of temp, lncorrect:conthlners.
Page 22 of 26

n
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u
�a
a
cr
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u
91
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Page 23 of 26

As I .
BAXTER HEALTHCARE CORPORATION-36974006
65 PITT STATION ROAD
RECEIVING DOCK 5
MARION, NC 28752
United States
Attention of. Rickey E Styles @ WOOD BOILER
BAXTER HEALTHCARE CORPORATION
BAXTER HEALTHCARE - PAYABLES; BAS - COSTA
RICA
PO BOX 999
DEERFIELD, IL 60015
United States
Attn: ACCOUNTS PAYABLE Fax: [phone]
Addruaty
PACE INC-37677188-USD-US-560861401
CHARLOTTE
CHARLOTTE, NC 28256-9427
GET PAID ON TIME
Baxter uses a supplier platform to help make sure you are paid on time. Submitting an invoice is free and easy,
specific invoicing instructions are below. If you have questions about how to use the platform to submit your
Invoice, please email [e-mail].
To ensure payment of the Invoice, submit Invoice through one of the following:
Click this box to join the Coupa Supplier Portal (CSP)
• Utilize the Supplier Actionable Buttons included within this email
110 Wi.) .I9FrZ
PO NUMBER C01302963 CURRENCY USD
ORDER DATE 27'10312023 PAYMENT TERMS 0% Net 30
REQUESTER Rickey E Styles Days(A30)
Page 24 of 26

f1
€ ine Dc!,,4,rjl;tiara I i f J I)%jti3 l�fS �:
i
1 Pace , Ash Analysis per samples SP32923A Sr Apr 12, 2023 2 each 800.00 1.600.00
SP32923S, estimate of services $800 each
1,600.00 use
"SUPPLIER: READ ALL COMMENTS BEFORE ORDER FULFILLMENT****'
This purchase order is subject to and Incorporates Baxter's purchase order terms and conditions for Baxter's suppliers,
vendors and service providers ("Seller" or "Sellers") which can be accessed electronlcally on Baxter's web site
at hY. 0..1/%vww,baxtcr.cram � •- I .uRi2-L. �1 ,
1�131 ie's i}axter s i•f•r nurrhase-order-terms-conditions antl clicking on the TO
Terms and Conditions' for the country or by contacting the Baxter buyer listed on this order and requesting a copy be e-
mailed or faxed to you. You will be deemed to have accepted this purchase order along with Baxter's purchase order
terms and conditions when accepted by your acknowledgment or your commencement of performance, Baxter objects to
all additions, exceptions, or changes to these terms, whether contained in any printed Form of Seller or elsewhere,
unless approved by Baxter In writing. If Seller has a separate Supply or Service Agreement signed by Baxter, the terms
and conditions set forth it such Supply Agreement shall control any conflicting terms found 'n ;his purchase order or
Baxter's purchase order terms and conditions.
COMPLIANCE AND ETHICS RULES FOR BAXTER PROVIDERS
Baxter promotes fair and ethical treatment in our dealings with suppliers, We believe that a shared commitment to
conducting business In a manner consistent with high ethical standards will continue to enhance our business
relationships, For this reason, Baxter expects its suppliers to comply with the Compliance and Ethics Standards for
Baxter suppliers, These rules canbeon the Baxter website: httpsJ/www.baxter /partnerj-sgo llerslbaxter-
gA�ierS/stand ds-Baxter-suo li rs
For each unique Invoice reference number, please only submit the relevant invoice once to the accounts payable
department.
THE FOLLOWING MINIMUM REQUIREMENTS SHOULD BE MET FOR ALL INVOICES SUBMITTED BY
SUPPLIERS:
' Name and address of the supplier billing entity
Unique supplier invoice number
Correct Baxter legal entity
Do not combine invoices related to multiple Baxter entities
Invoice date
Sufficient bank account details, if applicable For electronic transfers
Item/service name, price, and quantity
Tax amount included on the Invoice
Total invoice value (in the same currency as the Purchase Order currency)
For International suppliers, VAT Registration Number of the supplier, or local equivalent (GST/HST number in
Canada)
Any country specific tax or other legal requirements
Reference a valid Baxter purchase order number, the requester name, department, or cast center code
Paper Invoices will not be accepted. Each Invoice must be attached separately in PDF format
Always send one invoice in one PDF
Invoice To,
BAXTER HEALTHCARE - PAYABLES; BAS - COSTA RICA
PO BOX 999
REERFIEL©, IL 60025
h4TS OESTE DE ENTRAOA PRINCIPAL
AVE LAS Ah1ERiCAS
CARTAGO,10111
Coda Rica
25 of 26

For queries on invoices, the Acccunts Payable department may be contacted at: E p box rservice-no�v. om sm
Page 26 of 26

�ce�
October 09, 2023
Mr. Ricky Styles
Baxter Healthcare
2859 Old Linville Road
Marion, NC 28752
RE: Project: Biomass Wood BoilerAsh 9/19
Pace Project No.: 92689229
Dear Mr. Styles:
Pace Analytical Services, LLC
9800 KinceyAve, Suite 100
Huntersville, NC 28078
[phone]
Enclosed are the analytical results for sample(s) received by the laboratory on September 20, 2023. The results relate only
to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace National - Mt. Juliet
• Pace Analytical Services - Asheville
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Jonathan W Biddix
[e-mail]
704-977-0978
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 26

ace'�'
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Biomass Wood Boiler Ash 9119
Pace Project No.: 92689229
Pace Analytical Services National
12065 Lebanon Road, Mt. Juliet, TN 37122
Alabama Certification #: 40660
Alaska Certification 17-026
Arizona Certification M AZ0612
Arkansas Certification #: 88-0469
California Certification #: 2932
Canada Certification #: 1461,01
Colorado Certification #: TNO0003
Connecticut Certification #: PH-0197
DOD Certification: #1461.01
EPA# TNO0003
Florida Certification M E87487
Georgia DW Certification M 923
Georgia Certification: NELAP
Idaho Certification #: TNO0003
Illinois Certification M 200008
Indiana Certification #: C-TN-01
Iowa Certification #: 364
Kansas Certification #: E-10277
Kentucky UST Certification #: 16
Kentucky Certification #: 90010
Louisiana Certification #: A130792
Louisiana DW Certification #: LA180010
Maine Certification #: TNO002
Maryland Certification #: 324
Massachusetts Certification #: M-TNO03
Michigan Certification #: 9958
Minnesota Certification #: 047-999-395
Mississippi Certification M TNO0003
Missouri Certification #: 340
Montana Certification #: CERT0086
Nebraska Certification #: NE-OS-15-05
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification M 12
South Carolina Laboratory ID: 99006
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification M E87648
North Carolina Drinking Water Certification M 37712
North Carolina Wastewater Certification #: 40
CERTIFICATIONS
Nevada Certification #: TN-03-2002-34
New Hampshire Certification M 2975
New Jersey Certification #: TNO02
New Mexico DW Certification
New York Certification #: 11742
North Carolina Aquatic Toxicity Certification #: 41
North Carolina Drinking Water Certification #: 21704
North Carolina Environmental Certificate #: 375
North Dakota Certification #: R-140
Ohio VAP Certification #: CL0069
Oklahoma Certification M 9915
Oregon Certification #: TN200002
Pennsylvania Certification M 68-02979
Rhode Island Certification #: LA000356
South Carolina Certification #: 84004
South Dakota Certification
Tennessee DW/Chem/Micro Certification #: 2006
Texas Mold Certification M L.ABO152
Texas Certification #: T 104704246-17-14
USDA Soil Permit #: P330-15-00234
Utah Certification #: TNO0003
Virginia Certification #: VT2006
Vermont Dept. of Health: ID# VT-2006
Virginia Certification M 460132
Washington Certification #: C847
West Virginia Certification #: 233
Wisconsin Certification #: 998093910
Wyoming UST Certification M via A2LA 2926.01
A2LA-ISO 17025 Certification #: 1461,01
A2LA-ISO 17025 Certification M 1461.02
AIHA-LAP/LLC EMLAP Certification #:100789
South Carolina Certification M 99006001
South Carolina Drinking Water Cart, #: 99006003
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Louisiana DoH Drinking Water #: LA029
VirginiaNELAP Certification #: 460221
South Carolina Laboratory ID: 99030
South Carolina Certification #: 99030001
VirginiaNELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shah not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 26

SAMPLE ANALYTE COUNT
Project: Biomass Wood Boiler Ash 9119
Pace Project No.: 92689229
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 1oo
Huntersville, NC 28078
[phone]
Lab ID Sample ID Method
Analysts
Analytes
Reported
Laboratory
92689229001 NP91923A EPA 6010D
DBB1
18
PASI-A
EPA 601OD
DBB1
7
PASI-A
EPA 7471 B
LAS
1
PAN
EPA 7470A
BM
1
PASI-A
SW-846
KDF
1
PASI-C
SM 254OG
CMK
1
PAN
EPA 9045D
YEG
1
PASI-A
None
MDW
1
PASI-A
EPA 350.1 Rev 2.0 1993 Mod.
ARJ
1
PASI-A
EPA351.2 Rev 2.0 1993
MFO
1
PASI-A
EPA 353.2 Rev 2.0 1993
MFO
3
PASI-A
EPA 365.1 Rev 2.0 1993
Zip
1
PASI-A
92689229002 NP919238 EPA 601OD
DBB1
18
PASI-A
EPA 6010D
DBB1
7
PASI-A
EPA 74718
LAS
1
PAN
EPA 7470A
BM
1
PASI-A
SW-846
KDF
1
PASI-C
SM 264OG
CMK
1
PAN
EPA 9045D
YEG
1
PASI-A
None
MDW
1
PASI-A
EPA 350.1 Rev 2.0 1993 Mod.
ARJ
1
PASI-A
EPA 351.2 Rev 2.0 1993
MFO
1
PASI-A
EPA353.2 Rev 2.0 1993
MFO
3
PASI-A
EPA 365.1 Rev 2.0 1993
Zip
1
PASI-A
PAN = Pace National - Mt. Juliet
PASI-A = Pace Analytical Services - Asheville
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 3 of 26

Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Biomass Wood Boiler Ash 9119
Pace Project No.: 92689229
Sample. NP91923A
Lab ID: 92689229001 Collected: 09/19/23 09:30 Received: 09/20/23 12:17 Matrix: Solid
Results reported on a "dry weight"
basis and are adjusted for percent moisture, sample
size and any dilutions.
Parameters
Results units Report Limit
DF Prepared
Analyzed
CAS No. Qual
6010 MET ICP
Analytical Method: EPA 601 OD Preparation Method:
EPA 3050B
Pace Analytical Services -Asheville
Aluminum
8270 mglkg 18.9
1 09/27/23 14:45
10/02/23 03:58
7429-90-5
Arsenic
Barium
NO mg/kg 4.7
1 09/27/23 14:45
10/04/2316:31
7440-38-2
Cadmium
1180 mg/kg 1.9
1 09/27/23 14:45
10/02/23 03:58
7440-39-3
Calcium
2.9 mg/kg 0.19
1 09/27/23 14:45
10/02/23 0&68
7440-43-9
Chromium
105000 mglkg 473
10 09127/2314.45
1010412316:24
7440-70-2
Copper
13.5 mglkg 0.95
1 09/27/23 14:45
10/02/23 03:58
7440-47-3
Iron
77.5 mg/kg 9.5
1 09/27/23 14:45
10/02/23 03:58
7440-50-8
Lead
6540 mg/kg 94.5
1 09/27/23 14:45
10/02/23 03:58
7439-89-6
Magnesium
23.4 mg/kg 1.9
1 09/27/23 14:45
10/02/23 0158
7439-92-1
Manganese
18800 mglkg 18.9
1 09/27/23 14:45
10/02/23 03:58
7439-95-4
Molybdenum
3590 mglkg 9.5
10 0912712314:45
10/04/2316:24
7439-96-5
Nickel
ND mglkg 94.5
10 09/27/23 14:45
10104/2316:24
7439-98-7 D3
Potassium
15.9 mg/kg 0.95
1 09/27/23 14:45
10/02/23 03:58
7440-02-0
Selenium
12700 mg/kg 945
1 09/27/23 14:45
10/02/23 03:58
7440-09-7
Silver
NO mglkg 1.9
1 09127/2314A5
10/0412316:31
7782-49-2
Sodium
NO mg/kg 0.95
1 09/27/23 14:45
10/02/23 03:58
7440-22-4
Zinc
ND mg/kg 9450
10 09/27/23 14:45
10/0412316:24
7440-23-5 D3
258 mg/kg 1.9
1 09/27/23 14:45
10/02/23 03:58
7440-66-6
6010 MET ICP, TCLP
Analytical Method: EPA6010D Preparation Method: EPA3010A
Leachate Method/Date: EPA 1311; 09/25/23 13:00 Initial pH: 6.36; Final
pH: 5
Pace Analytical Services -Asheville
Arsenic
Barium
NO mg/L 0.050
1 09/30/23 01:04
10/03/23 23:01
7440-38-2
Cadmium
2.4 mg/L 0.25
1 09/30/23 01:04
10/03/23 23:01
7440-39-3
Chromium
NO mg/L 0.0050
1 09/30/23 01:04
10/03/23 23:01
7440-43-9
Lead
NO mg/L 0.050
1 09/30/23 01:04
10/03/23 23:01
7440-47-3
Selenium
ND mg/L 0.025
1 09/30/23 01:04
10/03/23 23:01
7439-92-1
Silver
NO mg1L 0.10
1 09/30/23 01:04
10/03/23 23:01
7782-49-2
NO mg/L 0.025
1 09/30/23 01:04
10/03/23 23:01
7440-22-4
Mercury 74718
Analytical Method: EPA 7471E Preparation Method: 7471A
Pace National - Mt. Juliet
Mercury
NO mg/kg 0.0973
1 10/03/23 22:58
10/04/23 14:25
7439-97-6
7470 Mercury, TCLP
Analytical Method: EPA 7470A Preparation Method: EPA 7470A
Leachate Method/Date: EPA 1311; 09/25/23 13:00
Initial pH: 6.36; Final
pH: 5
Pace Analytical Services -Asheville
Mercury
NO mg/L 0.00020
1 10102/2312:00
10/06/2311:50
7439-97-6
Percent Moisture
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
52.1 % 0.10
1 09/22/23 14:18
N2
Date: 10/09/2023 10:06 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC,
Page 4 of 26

(-�Face­
ANALYTICAL RESULTS
Project: Biomass Wood Boller Ash 9/19
Pace Project No.: 92689229
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Sample: NP91923A Lab ID: 92689229001 Collected: 09/19/23 09:30 Received: 09/20/23 12:17 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual
Total Solids 2540 G-2011 Analytical Method: SM 254OG Preparation Method: SM 2540 G
Pace National - Mt. Juliet
Total Solids 41.1 % 1 10/03/23 10:14 10/03123 10:28
9045 pH Soil
pH at 25 Degrees C
Plant Available Nitrogen
Plant Available Nitrogen
350.1 Ammonia
Nitrogen, Ammonia
361.2 Total Kjeldahl Nitrogen
Nitrogen, Kjeldahl, Total
353.2 Nitrogen, N021NO3
Nitrogen, NO2 plus NO3
Nitrogen, Nitrate
Nitrogen, Nitrite
366.1 Phosphorus, Total
Phosphorus
Analytical Method: EPA 9045D
Pace Analytical Services -Asheville
9.2 Std. Units 0.10 1 10/04/23 12A4
Analytical Method: None
Pace Analytical Services - Asheville
765 mglkg 1 0912712317:02
Analytical Method: EPA 350.1 Rev 2.0 1993 Mod. Preparation Method: EPA 350.1 Rev 2.0 1993 Mod.
Pace Analytical Services - Asheville
NO mg/kg 19.7 1 09/2212310:18 09122/2313:25 7664-41-7
Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993
Pace Analytical Services -Asheville
2550 mg/kg 99.3 1 09/22/23 18:52 09/23/23 05:17 7727-37-9
Analytical Method: EPA 353.2 Rev 2.0 1993 Preparation Method: EPA 353.2 Rev 2.0 1993
Pace Analytical Services -Asheville
NO mg/kg 8.1 1 09/21/23 23:12 09/22/23 03:04
H3
Z
H1,H2,
M1
NO mglkg 8.1 1 09/21/23 23:12 09122/23 0104 14797-55-8
NO mg/kg 8.1 1 09/21/23 23:12 09/22/23 03:04 14797-65-0 H1,H2
Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation Method: EPA 3651 Rev 2.0 1993
Pace Analytical Services - Asheville
2650 mg/kg 41.7 20 09/2212317:06 09/25/2315:41 7723-14-0
Date: 10/09/2023 10:06 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 5 of 26

ANALYTICAL RESULTS
Project: Biomass Wood Boiler Ash 9/19
Pace Project No.: 92689229
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: NP919238 Lab ID: 92689229002 Collected: 09/19/23 09:30 Received: 09/20/23 12:17 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual
6010 MET ICP
Analytical Method. EPA 6010D Preparation Method: EPA 3050B
Pace Analytical Services -Asheville
Aluminum
10500 mg/kg
19.9
1
09/27/23 14:45
10/02/23 04:01
7429-90-5
Arsenic
ND mglkg
5.0
1
09/27/23 14:45
10104/2316:36
7440-38-2
Barium
1420 mglkg
2.0
1
09/27/23 14:45
10/02/23 04:01
7440-39-3
Cadmium
3.6 mglkg
0.20
1
09/27/23 14:45
10/02/23 04:01
7440-43-9
Calcium
123000 mglkg
498
10
09127/2314:45
10104/2316:27
7440-70-2
Chromium
17.1 mglkg
1.0
1
09/27/23 14:45
10/02/23 04:01
7440-47-3
Copper
95.1 mglkg
10
1
09/27/23 14A5
10/02/23 04:01
7440-50-8
Iron
8360 mg/kg
99.5
1
09/27/23 14:45
10/02/23 04:01
7439-89-6
Lead
28.2 mglkg
2.0
1
09/27/23 14:45
10/02/23 04:01
7439-92-1
Magnesium
23100 mg/kg
199
10
09127/2314:45
10/04/2316:27
7439-95-4
Manganese
4180 mg/kg
10
10
09/27/23 14:45
10104/2316:27
7439-96-5
Molybdenum
NO mg/kg
99.5
10
09/27/23 14:45
1010412316:27
7439-98-7
Nickel
19.4 mg/kg
1.0
1
09/27/23 14:45
10/02/23 04:01
7440-02-0
Potassium
16300 mglkg
995
1
09/27/23 14:45
10/02/23 04:01
7440-09-7
Selenium
ND mg/kg
2.0
1
09/27/23 14:45
10/04/2316:35
7782.49-2
Silver
ND mg/kg
1.0
1
09/27/23 14:45
10/02/23 04:01
7440-22-4
Sodium
ND mg/kg
9950
10
09/27/23 14:45
10/04/2316:27
7440-23-5
Zinc
324 mglkg
2.0
1
09/27/23 14:45
10/02/23 04:01
7440-66-6
6010 MET ICP, TCLP
Analytical Method: EPA 601 OD Preparation Method:
EPA 3010A
Leachate Method/Date: EPA 1311; 09/25/23 13:00 initial pH: 7.39; Final pH: 5
Pace Analytical Services - Asheville
Arsenic
ND mg/L
0.050
1
09/30/23 01:04
10/03/23 23:04
7440-38-2
Barium
2.4 mg/L
0.25
1
09/30/23 01:04
10/03/23 23:04
7440-39-3
Cadmium
NO mg/L
0.0050
1
09/30/23 01:04
10/03/23 23:04
7440-43-9
Chromium
ND mg/L
0.050
1
09/30/23 01:04
10/03/23 23:04
7440-47-3
Lead
ND mg/L
0.025
1
09/30/23 01:04
10/03/23 23:04
7439-92-1
Selenium
ND mg/L
0,10
1
09/30/23 01:04
10/03/23 23:04
7782-49-2
Silver
NO mg/L
0.025
1
09/30/23 01:04
10/03/23 23:04
7440-22-4
Mercury 7471E
Analytical Method: EPA 7471B Preparation
Method:
7471A
Pace National - Mt. Juliet
Mercury
ND mglkg
0.0927
1
10/03/23 22:58
10/04/23 14:27
7439-97-6
7470 Mercury, TCLP
Analytical Method: EPA 7470A Preparation Method: EPA 7470A
Leachate Method/Date: EPA 1311; 09/25/23 13:00
Initial
pH: 7.39; Final
pH: 5
Pace Analytical Services -Asheville
Mercury
ND mg/L
0.00020
1
10/0212312:00
10106/2311:52
7439-97-6
Percent Moisture
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
51.7 %
0,10
1
09/22/23 14:18
D3
D3
N2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/09/2023 10:06 AM without the written consent of Pace Analytical Services, LLC. Page 6 of 26

Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Biomass Wood Boiler Ash 9119
Pace Project No.: 92689229
Sample: NP91923B
Lab ID- 92689229002 Collected: 09/19/23 09:30 Received: 09/20123 12:17 Matrix: Solid
Results reported on a "dry weight"
basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters
Results Units Report Limit DF Prepared Analyzed CAS No.
Qual
Total Solids 2540 G-2011
Analytical Method: SM 254OG Preparation Method: SM 2540 G
Pace National - Mt. Juliet
Total Solids
43.2 % 1 10/03/23 10:14 10/03/23 10:28
9046 pH Soil
Analytical Method: EPA 90450
Pace Analytical Services - Asheville
pH at 25 Degrees C
9.2 Std. Units 0.10 1 10104/2312:45
H3
Plant Available Nitrogen
Analytical Method: None
Pace Analytical Services - Asheville
Plant Available Nitrogen
897 mg/kg 1 09/27/23 17:02
N2
350.1 Ammonia
Analytical Method: EPA 350.1 Rev 2.0 1993 Mod. Preparation Method: EPA 350.1 Rev 2.0 1993 Mad.
Pace Analytical Services - Asheville
Nitrogen, Ammonia
ND mglkg 19.9 1 09/22/23 10:18 09/22/23 13:27 7664-41-7
351.2 Total Kjeldahl Nitrogen
Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993
Pace Analytical Services - Asheville
Nitrogen, Kjeldahi, Total
2990 mglkg 104 1 09/22/23 18:52 09/23/23 05:18 7727-37-9
353.2 Nitrogen, N021NO3
Analytical Method: EPA 353.2 Rev 2.0 1993 Preparation Method: EPA 353.2 Rev 2.0 1993
Pace Analytical Services -Asheville
Nitrogen, NO2 plus NO3
ND mg/kg 8.0 1 09/21/23 23:12 09/22/23 03:08
H1,H2
Nitrogen, Nitrate
ND mg/kg 8.0 1 09/21/23 23:12 09/22/23 03:08 14797-66-8
Nitrogen, Nitrite
ND mg/kg 8.0 1 09/21/23 23:12 09/22/23 03:08 14797-65-0
H1,H2
365.1 Phosphorus, Total
Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation Method: EPA 365.1 Rev 2.0 1993
Pace Analytical Services - Asheville
Phosphorus
1890 mg/kg 41.4 20 0912212317:06 09/25/2315:41 7723-14-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/09/2023 10:06 AM without the written consent of Pace Analytical Services, LLC. Page 7 of 26

Project: Biomass Wood Boiler Ash 9/19
Pace Project No.: 92689229
QC Batch: 2143913
QC Batch Method: 7471A
Associated Lab Samples: 92689229001, 92689229002
METHOD BLANK: R3981847-1
Associated Lab Samples: 92689229001, 92689229002
Parameter Units
Mercury mg/kg
QUALITY CONTROL DATA
Analysis Method: EPA 7471 B
Analysis Description: Mercury 7471 B
Laboratory: Pace National - Mt. Juliet
Matrix: Solid
Blank Reporting
Result Limit Analyzed Qualifiers
ND 0.0400 10104/2313:15
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE: R3981847-2
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Mercury mglkg 0.500 0,517 103 80.0-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: R3981847-3 R3981847-4
MS MSD
L1661493-13 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Canc. Result Result % Rec % Rec Limits RPD Qua[
Mercury mg/kg ND 0.500 0.500 0.520 0.471 104 94.2 75.0-125 9.86
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right or the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/09/2023 10:06 AM without the written consent of Pace Analytical Servicesr LLC. Page 8 of 26

QUALITY CONTROL DATA
Project: Biomass Wood Boiler Ash 9119
Pace Project No.: 92689229
Pace Analytical Services, LLC
9800 Kincey Ave, Suite too
Huntersville, NC 28078
[phone]
QC Batch: 803237
Analysis Method:
EPA 7470A
QC Batch Method: EPA 7470A
Analysis Description:
7470 Mercury TCLP
Laboratory:
Pace Analytical Services - Asheville
Associated Lab Samples: 92689229001, 92689229002
METHOD BLANK: 4152921
Matrix: Water
Associated Lab Samples: 92689229001, 92689229002
Blank Reporting
Parameter Units
Result Limit
Analyzed Qualifiers
Mercury mglL
ND 0.00020 10106/2311:34
LABORATORY CONTROL SAMPLE: 4160378
Spike LCS
LCS % Rec
Parameter Units
Conc. Result
% Rec Limits Qualifiers
Mercury mg1L
0.0025 0.0027
108 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4160379 4160380
MS MSD
92689619001
Spike Spike MS
MSD MS MSD % Rec
Parameter Units Result
Conc. Conc. Result
Result % Rec % Rec Limits RPD Qua€
Mercury mglL ND
0.0025 0.0025 0.0024 0.0023 90 88 75-125 2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/09/2023 10:06 AM without the written consent of Pace Analytical Services, LLC. Page 9 of 26

Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Biomass Woad Boiler Ash 9/19
Pace Project No.: 92689229
QC Batch: 802404 Analysis Method: EPA 6010D
QC Batch Method: EPA 3050E Analysis Description: 6010 MET
Laboratory: Pace Analytical Services - Asheville
Associated Lab Samples: 92689229001, 92689229002
METHOD BLANK: 4156414
Associated Lab Samples: 92689229001, 92689229002
Parameter Units
Matrix: Solid
Blank Reporting
Result Limit
Analyzed Qualifiers
Aluminum
mglkg
ND
5.0
10/02/23 02:51
Arsenic
mg/kg
ND
1.2
10/02/23 02:51
Barium
mglkg
ND
0.50
10/02/23 02:51
Cadmium
mglkg
ND
0.050
10/02/23 02:51
Calcium
mglkg
ND
12.5
10/02/23 02:51
Chromium
mglkg
ND
0.25
10/02/23 02:51
Copper
mg/kg
ND
2.5
10/02/23 02:51
Iron
mglkg
ND
25.0
10/02/23 02:51
Lead
mglkg
ND
0.50
10/02/23 02i51
Magnesium
mg/kg
ND
5.0
10/02/23 02:51
Manganese
mg/kg
ND
0.25
10/02/23 02:51
Molybdenum
mg/kg
ND
2.5
10/02/23 02:51
Nickel
mg/kg
ND
0.25
10/02/23 02:51
Potassium
mglkg
ND
260
10/02/23 02:51
Selenium
mg/kg
ND
0,50
10/02/23 02:61
Silver
mglkg
ND
0,25
10/02/23 02:51
Sodium
mg/kg
ND
250
10/04/2315:45
Zinc
mg/kg
ND
0.50
10/02/23 02:51
LABORATORY CONTROL SAMPLE:
Parameter
4156415
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
Aluminum
mglkg
250
228
91
80-120
Arsenic
mglkg
25
21.9
88
80-120
Barium
mg/kg
25
23.8
95
80-120
Cadmium
mg/kg
25
23.7
95
80-120
Calcium
mg/kg
250
244
97
80-120
Chromium
mg/kg
25
23.4
94
80-120
Copper
mg/kg
25
23.8
95
80-120
Iron
mg/kg
250
240
96
80-120
Lead
mglkg
25
23.4
93
80-120
Magnesium
mglkg
250
223
89
80-120
Manganese
mglkg
25
23.6
95
80-120
Molybdenum
mglkg
25
23.9
95
80-120
Nickel
mglkg
25
23.8
95
80-120
Potassium
mglkg
250
ND
89
80-120
Selenium
mg/kg
25
21.2
85
80-120
Silver
mg/kg
12.5
11.6
93
80-120
Sodium
mg/kg
250
247J
99
80-120
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 10/09/2023 10:06 AM without the written consent of Pace Analytical Services, LLC. Page 10 of 26

A I
Project: Biomass Wood Boiler Ash 9119
Pace Project No.: 92689229
LABORATORY CONTROL SAMPLE: 4156415
Parameter Units
Zinc mglkg
QUALITY CONTROL DATA
Spike LCS
Conc. Result
25 23.7
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
4156416
MS
92685498001
Spike
Parameter
Units
Result
Conc.
Aluminum
mglkg
472
567
Arsenic
mglkg
NO
56.7
Barium
mglkg
304
56.7
Cadmium
mglkg
0.45
56.7
Calcium
mglkg
453000
567
Chromium
mg/kg
26.7
56.7
Copper
mg/kg
ND
56.7
Iran
mglkg
373
567
Lead
mglkg
ND
56.7
Magnesium
mg/kg
7230
567
Manganese
mg/kg
412
56.7
Molybdenum
mglkg
ND
56.7
Nickel
mglkg
9.8
66.7
Potassium
mglkg
ND
567
Selenium
mg/kg
ND
56.7
Silver
mglkg
ND
28.3
Sodium
mglkg
ND
567
Zinc
mglkg
9.2
56.7
LCS
% Rec
95
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
% Rec
Limits Qualifiers
80-120
4156417
MSD
Spike
MS
MSD
MS
MSD
% Rec
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
582
1160
1170
120
120
75-125
1
58.2
51.6
53.9
91
92
75-125
4
58.2
358
359
95
96
75-125
0
58.2
50.5
52.1
88
89
75-125
3
582
448000
455000
-968
324
75-125
2 M1
58.2
77.9
79.6
90
91
75-125
2
58.2
62.6
64.1
106
106
75-125
2
582
730
765
63
68
75-126
5 M1
58.2
50.7
52.6
89
90
75-125
4
582
7740
7780
89
93
75-125
0
58.2
463
451
90
66
75-125
3 M1
58.2
52.2
54.0
92
93
75-125
3
58.2
58.1
59.5
85
85
75-125
2
582
966
988
139
140
75-125
2 M1
58.2
48.0
49.1
81
81
75-125
2
29.1
31.5
32.6
110
111
75-125
3
582
NO
ND
76
55
75-125
M1
58.2
57.5
57.2
85
82
75-125
1
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full.
Date: 10/09/2023 10:06 AM without the written consent of Pace Analytical Services, LLC.
Page 11 of 26

QUALITY CONTROL DATA
Project: Biomass Wood Boiler Ash 9/19
Pace Project No.: 92689229
QC Batch: 802241 Analysis Method: EPA 601 OD
QC Batch Method: EPA 3010A Analysis Description: 6010 MET TCLP
Laboratory: Pace Analytical Services - Asheville
Associated Lab Samples: 92689229001, 92689229002
METHOD BLANK: 4152921
Matrix: Water
Associated Lab Samples:
92689229001, 92689229002
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Arsenic
mg/L
NO
0.050
10/03/23 22:23
Barium
mg/L
NO
0.25
10/03/23 22:23
Cadmium
mg/L
NO
0.0050
10/03/23 22:23
Chromium
mg/L
NO
0.050
10/03/23 22:23
Lead
mg/L
ND
0,025
10/03/23 22:23
Selenium
mg/L
NO
0.10
10/03/23 22:23
Silver
mg/L
NO
0.025
10/03/23 22:23
LABORATORY CONTROL SAMPLE:
4155665
Parameter
Units
Arsenic
mg/L
Barium
mg/L
Cadmium
mg/L
Chromium
mg1L
Lead
mg/L
Selenium
mg/L
Silver
mg/L
Pace Analytical Services, I l-C
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Spike
LCS
LCS
% Rec
Conc.
Result
% Rec
Limits Qualifiers
2.5
2.5
98
80-120
2.5
2.4
97
80-120
2.5
2.4
96
80-120
2.5
2.4
97
80-120
2.5
2A
96
80-120
2.5
2.6
103
80-120
1.2
1.2
99
80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
4155666
4155667
MS
MSD
92689619001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Arsenic
mg/L
ND
2.5
2.5
2.1
2.3
84
91
75-125
8
Barium
mg/L
0.66
2.5
2.5
2.7
2.9
80
88
75-125
7
Cadmium
mg/L
0.023
2.5
2.5
2.1
2.2
82
88
75-125
7
Chromium
mg/L
ND
2.5
2.5
2.1
2.2
83
89
75-125
7
Lead
mg/L
0.30
2.5
2.5
2.3
2.5
81
88
75-125
7
Selenium
mg/L
NO
2.5
2.5
2.2
2.3
86
93
75-125
7
Silver
mg/L
NO
1.2
1.2
1.0
1.1
83
88
75-125
6
Results presented on this page are In the units Indicated by the "Units' column except where an aHernate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/09/2023 10:06 AM without the written consent of Pace Analytical Services, LLC. Page 12 of 26

Pace Analytical Services, LLC
9800 Kinoey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Biomass Wood Bailer Ash 9119
Pace Project No.: 92689229
QC Batch: 801473 Analysis Method: SW-846
QC Batch Method: SW-846 Analysis Description: Dry WeightfPercent Moisture
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92689229001, 92689229002
SAMPLE DUPLICATE: 4151514
92689390001 Dup
Parameter Units Result Result RPD Qualifiers
Percent Moisture % 16.3 17.5 7 N2
SAMPLE DUPLICATE: 4151515
92689191046 Dup
Parameter Units Result Result RPD Qualifiers
Percent Moisture % 28.2 28.9 3 N2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 10/09/2023 10:06 AM without the written consent of Pace Analyticat Services, LLC.
Page 13 of 26

QUALITY CONTROL DATA
Project: Biomass Wood Boiler Ash 9119
Pace Project No.: 92689229
QC Batch: 2143400
Analysis Method:
QC Batch Method: SM 2540 G
Analysis Description:
Laboratory:
Associated Lab Samples: 92689229001, 92689229002
METHOD BLANK: R3981451-1
Matrix: Solid
Associated Lab Samples: 92689229001, 92689229002
Blank Reporting
Parameter Units
Result Limit
Total Solids %
0.00100
SM 254OG
Total Solids 2540 G-2011
Pace National - Mt. Juliet
Analyzed Qualifiers
10/03/23 10:28
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE: R3981451-2
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Total Solids % 50.0 50.0 100 85.0-115
SAMPLE DUPLICATE: R3981451-3
L1661260-01 Dup
Parameter Units Result Result RPD Qualifiers
Total Solids % 91.7 91.8 0.130
Results presented on this page are in the units indicated by the "units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/09/2023 10:06 AM without the written consent of Pace Analytical Services, LLC. Page 14 of 26

Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Biomass Wood Boiler Ash 9119
Pace Project No.: 92689229
QC Batch: 804027 Analysis Method: EPA 9045D
QC Batch Method: EPA 9045D Analysis Description: 9045 pH
Laboratory: Pace Analytical Services - Asheville
Associated Lab Samples: 92689229001, 92689229002
SAMPLE DUPLICATE: 4163974
92689191045 Dup
Parameter Units Result Result RPD Qualifiers
pH at 25 Degrees C Std. Units 6A 6,6 3 D6,H3
Results presented an this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/09/2023 10:06 AM without the written consent of Pace Analytical Services, LLC.
Page 15 of 26

Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Biomass Wood Boiler Ash 9119
Pace Project No.: 92689229
QC Batch: 801344
QC Batch Method: EPA 350.1 Rev 2.0 1993 Mod
Associated Lab Samples: 92689229001, 92689229002
QUALITY CONTROL DATA
Analysis Method: EPA 350.1 Rev 2.0 1993 Mod,
Analysis Description: 350.1 Ammonia
Laboratory: Pace Analytical Services -Asheville
METHOD BLANK: 4150847 Matrix: Solid
Associated Lab Samples: 92689229001, 92689229002
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Nitrogen, Ammonia mg/kg ND 9.4 09/22/23 13:16
LABORATORY CONTROL SAMPLE: 4150848
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Nitrogen, Ammonia mg/kg 463 472 102 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4150849 4150850
MS MSD
70270271001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Nitrogen, Ammonia mg/kg 1560 472 455 1840 2060 59 109 90-110 11 M1,R1
Results presented an this page are in the units indicated by the "units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 10/09/2023 10:06 AM without the written consent of Pace Analytical Services, LLC.
Page 16 of 26

QUALITY CONTROL DATA
Project: Biomass Wood Boiler Ash 9119
Pace Project No.: 92689229
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QC Batch: 801425
Analysis Method:
EPA 351.2 Rev 2.0 1993
QC Batch Method: EPA 351.2 Rev 2.0 1993
Analysis Description:
351.2 TKN
Laboratory:
Pace Analytical Services - Asheville
Associated Lab Samples: 92689229001, 92689229002
METHOD BLANK: 4151188
Matrix: Solid
Associated Lab Samples: 92689229001, 92689229002
Blank Reporting
Parameter Units
Result Limit
Analyzed Qualifiers
Nitrogen, Kjeldahl, Total mglkg
ND 50.0 09/23/23 05:05
LABORATORY CONTROL SAMPLE: 4161189
Spike LCS
LCS % Rec
Parameter Units
Conc. Result
% Rec Limits Qualifiers
Nitrogen, Kjeldahl, Total mglkg
1000 1020
102 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4151190 4151191
MS MSD
92688040002
Spike Spike MS
MSD MS MSD % Rec
Parameter Units Result
Conc. Conc. Result
Result % Rec % Rec Limits RPD Qual
Nitrogen, Kjeldahl, Total mglkg 44300
69000 60700 104000 87800 86 72 90-110 17 M1,R1
Results presented on this page are in the units indicated by the "Units" column except where an altemate unit Is presented to the right of the resutt.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/09/2023 10:06 AM without the written consent of Pace Analytical Services, LLC.
Page 17 of 26

Project: Biomass Wood Boiler Ash 9/19
Pace Project No.: 92689229
QC Batch: 801279
QC Batch Method: EPA 353.2 Rev 2.0 1993
Associated Lab Samples: 92689229001, 92689229002
METHOD BLANK: 4150698
Associated Lab Samples: 92689229001, 92689229002
Parameter Units
Nitrogen, Nitrate mglkg
Nitrogen, Nitrite mglkg
Nitrogen, NO2 plus NO3 mglkg
QUALITY CONTROL DATA
Analysis Method: EPA 353.2 Rev 2.0 1993
Analysis Description: 353.2 Nitrate + Nitrite
Laboratory: Pace Analytical Services - Asheville
Matrix: Solid
Blank Reporting
Result Limit Analyzed
ND 4.0 09/22/23 03:02
ND 4.0 09/22/23 03:02
ND 4.0 09/22/23 03:02
Qualifiers
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE: 4150699
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Nitrogen, Nitrate mg/kg 15 15.5 103 90-110
Nitrogen, Nitrite mglkg 10 10.1 101 90-110
Nitrogen, NO2 plus NO3 mg/kg 25 25.5 102 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
4160700
4150701
MS
MSD
92689229001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits RPD Qual
Nitrogen, Nitrate
mg/kg
NO
30.7
30.5
35.4
35.4
116
116
90-110 0
Nitrogen, Nitrite
mg/kg
ND
20.4
20.2
22,0
21.8
106
106
90-110 1 H1
Nitrogen, NO2 plus NO3
mg/kg
NO
51.1
50.9
57.5
57.2
112
112
90-110 0 H1,M1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/09/2023 10:06 AM without the written consent of Pace Analytical Services, LLC.
Page 18 of 26

QUALITY CONTROL DATA
Project: Biomass Wood Boiler Ash 9/19
Pace Project No.: 92689229
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QC Batch: 801382 Analysis Method: EPA 365.1 Rev 2.0 1993
QC Batch Method: EPA 365.1 Rev 2.0 1993 Analysis Description: 365.1 Phosphorus, Total
Laboratory: Pace Analytical Services - Asheville
Associated Lab Samples: 92689229001, 92689229002
METHOD BLANK: 4150971 Matrix: Solid
Associated Lab Samples: 92689229001, 92689229002
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Phosphorus mglkg ND 1.0 09/25/2315:32
LABORATORY CONTROL SAMPLE: 4150972
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Phosphorus mglkg 50 54.1 108 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4150973 4150974
MS MSD
92687510001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Phosphorus mg/kg 124 83.5 85 191 196 80 84 90-110 3 M1
Results presented on this page are in the units Indicated by the -Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Pace Analytical Services, LLC
9800 Kinsey Ave. Suite 100
(-�Face­
Huntersviile, NC 28078
[phone]
QUALIFIERS
Project: Biomass Wood Boiler Ash 9119
Pace Project No.: 92689229
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260,
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TN I accredited. Contact your Pace PM for the current list of accredited analytes.
TNI -The NELAC Institute.
ANALYTE QUALIFIERS
D3 Sample was diluted due to the presence of high levels of non -target analytes or other matrix interference.
D6 The precision between the sample and sample duplicate exceeded laboratory control limits.
H1 Analysis conducted outside the EPA method holding time.
H2 Extraction or preparation conducted outside EPA method holding time.
H3 Sample was received or analysis requested beyond the recognized method holding time.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
N2 The lab does not hold NELACITNI accreditation for this parameter but other accreditations/certifications may apply. A
complete list of accreditationstcertifications is available upon request.
R1 RPD value was outside control limits.
REPORT OF LABORATORY ANALYSIS
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Pace Analytical Services, LLC
9800 Kincey Ave, Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: Biomass Wood Boiler Ash 9I19
Pace Project No.: 92689229
Lab ID
Sample 1D
QC Batch Method
QC Batch
Analytical Method
Analytical
Batch
92689229001
NP91923A
EPA 3050E
802404
EPA 6010D
802507
92689229002
NP91923B
EPA 30508
802404
EPA 6010D
802507
92689229001
NP91923A
EPA 3010A
802241
EPA 6010D
803249
92689229002
NP91923B
EPA 3010A
802241
EPA 6010D
803249
92689229001
NP91923A
7471A
2143913
EPA 7471E
2143913
92689229002
NP91923B
7471A
2143913
EPA 7471B
2143913
92689229001
NP91923A
EPA 7470A
803237
EPA 7470A
803539
92689229002
NP91923B
EPA 7470A
803237
EPA 7470A
803539
92689229001
NP91923A
SW-846
801473
92689229002
NP91923B
SW-846
801473
92689229001
NP91923A
SM 2540 G
2143400
SM 254OG
2143400
92689229002
NP91923B
SM 2540 G
2143400
SM 254OG
2143400
92689229001
NP91923A
EPA 9045D
804027
92689229002
NP91923B
EPA 9045D
804027
92689229001
NP91923A
None
802498
92689229002
NP91923B
None
802498
92689229001
NP91923A
EPA 350.1 Rev 2.0 1993
801344
EPA 350.1 Rev 2.0 1993
801408
Mod.
Mod.
92689229002
NP91923B
EPA 350.1 Rev 2.0 1993
801344
EPA 350.1 Rev 2.0 1993
801408
Mod.
Mod.
92689229001
NP91923A
EPA 351.2 Rev 2.0 1993
801425
EPA 351.2 Rev 2.0 1993
801559
92689229002
NP91923B
EPA 351.2 Rev 2.0 1993
801425
EPA 351.2 Rev 2.0 1993
801669
92689229001
NP91923A
EPA 353.2 Rev 2.0 1993
801279
EPA 353.2 Rev 2.0 1993
801280
92689229002
NP91923B
EPA 353.2 Rev 2.0 1993
801279
EPA 353.2 Rev 2.0 1993
801280
92689229001
NP91923A
EPA 365.1 Rev 2.0 1993
801382
EPA 365.1 Rev 2.0 1993
801765
92689229002
NP91923B
EPA 365.1 Rev 2.0 1993
801382
EPA 365.1 Rev 2.0 1993
801765
Date: 10/09/2023 10:06 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 21 of 26

4ace,DC# Title: ENV-FRM-HUNI-0083 �02 Sample Condition Upon Receipt
ace'
iumu.vr,xn
Effective Date: 11/14/2022 8*18:30 AM
Laboratory recgMng samples:
Ashevill4Z Eden❑ Greenwood ❑ Huntersville ❑ Raleigh[] Mechanicsville❑ Atlanta❑ Kemersville❑
Sample Condition
Client Name:Upon Project #: WO# : 92689229
Ri.lx t t, '— I I
Courier. El Fed Ex UPS Ll LISPS Client
❑ Commercial ❑Pace []other; I I [
M89229
Custody Seal Present? ❑Yes Dffo Seals Intact? El Yes No f
Date/Initials Person Examining Contents; .4 ` y
Packing Material: ❑ Bubble Wrap ❑Bubble Bags ZfNone ❑ Other Biological Tissue -Frozen?
_ ;T�e�rnolreter .. _ __ _ _ _ _ .....❑Yes..._❑�ln. _i�lrr/A.
Gun ID:
Correction Factor:
Cooler Temp: -a�3 ' Add/Subtract ('C) Tem ould be above freezing to VC
+ 5amptes out of temp criteria. Samples on ice, cooling process
Cooler Temp Corrected ('C): ? 3 ] l has begun
USDA Regulated Soil (❑ N/A, water sample)
Did samples originate in a quarantine :one within the United States: CA, NY, or SC Did samples originate from a foreign source (internationally,
-L--L -- .t'J mv— 1:;K., indudinp Hawaii and Puerto Ricot? ❑Yes Elmo,
Comments/Discrepancy:
Chain of Custody Present?
gles
❑No
:1N/A
1.
Samples Arrived within Hold Time?
Yes
ONO
❑N/A
2.
Short bold Time Analysis (<72 hr.)?
es
❑ No
❑ N/A
3.
Rush Turn Around Time Rs uested7
❑ Yes
❑ N/A
4.
Sufficient Volume?
es
❑No
❑ WA
5.
Correct Containers Used?
-Pace Containers Used?
Pes
❑Yes
❑No
)a'tio
❑ WA
❑ WA
6.
Containers Intact?
❑No
❑ WA
7.
Dissolved analysis: Samples Field Filtered?
Oyes
ONO
a.
Sample Labels Match COC?
-includes Date/Time/ID/Analysis Matrix:
s
❑No
❑MIA
4.
Headspace in VOA Vials >5-6mmj?
[)Yes
❑ No
W
10.
Trip Blank Present?
Trip Blank Custody Seals Present?
❑Yes
❑Yes
❑No
❑No
A
❑
11.
COMMENTS/SAMPLE DISCREPANCY
Lot ID of split containers:
CLIENT NOTIFICATION/RESOLUTION
Person contacted:
Project Manager SCURF Review:
Project Manager SRF Review:
Date/Time:
Date:
Date:
Flela aata Isequtrear ures u rro
Page 22 of 26
nit�lfrav Irl• AOR14 Pe a 1 of '7

Ace, DC# Title: ENV-i=RM-HUN1-0083 02 Sample Condition Upon Receipt
Effective Date:1111412022 8:18:30 AM
*Check mark top half of box if pH and/or dechlorination is verified and
within the acceptance range for preservation samples,
Exceptions: VOA, Coliform, TOC, Oil and Grease, DRO/8015 (water) DOC, LLHg
* *Bottom half of box Is to list number of bottles
* * *Check all unpreserved Nitrates for chlorine
Project # ' 92689229
PH: JW5 Due Date: 10/04/23
CLIENT: 82—Baxter
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Log for Preserved Samples
Sample ID
Type of Preservative
pH upon receipt
Date preservation adjusted
Time preservation
adjusted
Amount of Preservative
added
Lot #
Note: Whenever there is a utscrepancy atte CRtng Nortn t.arorcna comp»ance samples, a COPY oT snts corm Will Oe se nc ra ure NUCUI tear LPnrta W clvn L-er,r nca,Wrr urrrLe tr.e.
out of hold, incorrect preservative, out of temp, incorrect containers. Page 23 of 26
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Page 24 of 26

BAXTER HEALTHCARE
65 PITT STATION ROAD
RECEIVING DOCK 5
MARION, NC 28752
United States
Attention of. Rickey E Styles
[phone]
BAXTER HEALTHCARE
PACE INC-37677188-USD-US-
ORPORATION
5608.6.1.4.0..1....
BAXTER HEALTHCARE
CHARLOTTE
_
PAYABLES; BAS - COSTA RICA _
_
CHARLOTTE, NC 28256-9427
PO BOX 999
[e-mail]
DEERFIELD, IL60015
United States
Attn: ACCOUNTS PAYABLE Fax:
1-866-887-7421
ET PAD QN TIME
Baxter uses a supplier platform to help make sure you are paid on time. Submitting an invoice is free and easy,
specific invoicing instructions are below. If you have questions about how to use the platform to submit your
invoice, please email [e-mail].
To ensure payment of the Invoice, submit Invoice through one of the following:
Click this box to join the Coupa Supplier Portal (CSP)
• Utilize the Supplier Actionable Buttons included within this email
PO NUMBER C01421885 CURRENCY USD
ORDER DATE 19109/2023 PAYMENT TERMS 0% Net 30
REQUESTER Rickey E Styles Days(A30)
EMAIL [e-mail] SHIPPING TERMS NIA( )
1 Pace , Ash Analysis per samples NP91923A & Sep 20, 2023 2 Each 800.00 1,600.00
NP9192313, estimate of services $800 each
1,600.00 USD
*"'"SUPPLIER: READ ALL COMMENTS BEFORE ORDER FULFILLMENT'' I I -
This purchase order is subject to and incorporates Baxter's purchase order terms and conditions for Baxter's suppliers,
vendors and service providers ("Seller" or "Sellers") which can be accessed electronically on Baxter's web site
at ittps 1/www.baxte;r.cornft2artnei's-su12�2 ersCbraxter- lc� 51 and clicking on the'PO
Terms and Conditions' for the country or by contacting the Baxter buyer listed on this order and requesting a copy be e-
mailed or faxed to you. You will be deemed to have accepted this purchase order along with Baxter's purchase order
25 of 26

terms and conditions when accepted by your acknowledgment or your commencement of performance. Baxter objects to
all additions, exceptions, or changes to these terms, whether contained in any printed form of Seller or elsewhere,
unless approved by Baxter in writing. If Seller has a separate Supply or Service Agreement signed by Baxter, the terms
and conditions set forth in such Supply Agreement shall control any conflicting terms found in this purchase order or
Baxter's purchase order terms and conditions.
COMPLIANCE AND ETHICS RULES FOR BAXTER PROVIDERS
Baxter promotes fair and ethical treatment in our dealings with suppliers. We believe that a shared commitment to
conducting business in a manner consistent with high ethical standards will continue to enhance our business
relationships. For this reason, Baxter expects its suppliers to comply with the Compliance and Ethics Standards for
Baxter suppliers. These rules can be found on the Baxter website: https://www.baxtercom/partners-suppliers/baxter-
su ppl ie rs/standa rds-ba xter-suppl iers
For each unique invoice reference number, please only submit the relevant invoice once to the accounts payable
department.
THE FOLLOWING MINIMUM REQUIREMENTS SHOULD BE MET FOR ALL INVOICES SUBMITTED BY
SUPPLIERS:
Unique supplier invoice number
Correct Baxter legal entity
Do not combine invoices related to multiple Baxter entities
Invoice date
Sufficient bank account details, if applicable for electronic transfers
Item/service name, price, and quantity
Tax amount included on the invoice
Total invoice value (in the same currency as the Purchase Order currency)
For international suppliers, VAT Registration Number of the supplier, or local equivalent (GST/HST number in
Canada)
Any country specific tax or other legal requirements
Reference a valid Baxter purchase order number, the requester name, department, or cost center code
Paper invoices will not be accepted, Each Invoice must be attached separately in POF format
Always send one invoice in one POF
Invoice To:
BAXTER HEALTHCARE - PAYABi FS; BAS - COSTA RICA
PO BOX 999
DEERFIELD, IL 60015
For queries on invoices, the Accounts Payable department may be contacted at: https://baxter.service-now.com/csm
Page 26 of 26