WQ0030998_2023 Residual Annual Report_20240229 (2)

Initial Review
Reviewer
nathaniel.thorn burg
Is this submittal an application? (Excluding additional information.) *
Yes No
If not an application what is the submittal type?* Annual Report
Residual Annual Report
Additional Information
Other
Annual Report Year* 2023
Permit Number (IR) * WQ0030998
Applicant/Permittee Triple S Farms and Cleaning, Inc.
Email Notifications
Does this need review by the hydrogeologist? * Yes U No
Regional Office Wilmington
CO Reviewer
Admin Reviewer Wanda Gerald

Submittal Form
Project Contact Information
Please provide information on the person to be contacted by NDB Staff regarding electronic submittal, confirmation of receipt, and other correspondence.
Name* Robert T. Branch
Email Address*
[e-mail]
Project Information
.........................
Application/Document Type*
New (Fee Required)
Modification - Major (Fee Required)
Renewal with Major Modification (Fee
Required)
Annual Report
Additional Information
Other
Phone Number*
3363129007
Modification - Minor
Renewal
GW-59, NDMR, NDMLR, NDAR-1,
N DAR-2
Residual Annual Report
Change of Ownership
We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form.
https://edoes.deq.nc.gov/Forms/NonDischarge_Monitoring_Report
Permit Type:*
Wastewater Irrigation
High -Rate Infiltration
Other Wastewater
Reclaimed Water
Closed -Loop Recycle
Residuals
Single -Family Residence Wastewater
Other
Irrigation
Permit Number:*
WQ0030998
Has Current Existing permit number
Applicant/Permittee Address*
PO Box 709 Beulaville NC 28518
Facility Name*
Triple S Farms and Cleaning Class B Residuals Program
Please provide comments/notes on your current submittal below.
At this time, paper copies are no longer required. If you have any questions about what is required, please contact Nathaniel Thornburg
at [e-mail].
Please attach all information required or requested for this submittal to be reviewed here.
(Application Form, Engineering Plans, Specifications, Calculations, Etc.)
2023 ANNUAL REPORT Triple S DEQ Final.pdf 16.24MB
Upload only 1 PDF document (less than 250 MB). Multiple documents must be combined into one PDF file unless file is larger
than upload limit.
* By checking this box, I acknowledge that I understand the application will not be accepted for pre -review until the fee (if required) has
been received by the Non -Discharge Branch. Application fees must be submitted by check or money order and made payable to the
North Carolina Department of Environmental Quality (NCDEQ). I also confirm that the uploaded document is a single PDF with all parts
of the application in correct order (as specified by the application).
Mail payment to:
NCDEQ — Division of Water Resources
Attn: Non -Discharge Branch
1617 Mail Service Center
Raleigh, NC 27699-1617
Signature
Submission Date 2/29/2024

2023 ANNUAL REPORT
TRIPLE S FARMS & CLEANING, INC.
LAND APPLICATION PROGRAM
PERMIT #WQ0030998
Prepared For:
Triple S Farms & Cleaning, Inc.
Post Office Box 709
Beulaville, NC 28518
Prepared By:
Branch Residuals & Soils, LLC
1735 Heckle Blvd. Suite 103-291
Rock Hill, SC 29732
February 2024

BRANCH RESIDUALS & SOILS, LLC
1735 Heckle Blvd, Suite 103-291, Rock Hill, SC 29732
PHONE [phone]
February 29, 2024
North Carolina Department of Environmental Quality
Division of Water Resources
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
Reference: 2023 LAND APPLICATION ANNUAL REPORT
Triple S Farms & Cleaning, Inc.
Permit No. WQ0030998
Branch Residuals & Soils Project No. 2007-70
Information Processing Unit:
Branch Residuals & Soils is submitting all monitoring and reporting information as required in the referenced
permit on behalf of the Triple S Farms & Cleaning, Inc. This data includes: 1) Certification Forms and Facility
Information, 2) Annual Residual Sampling Summary Forms, 3) Annual Metals Field Loading Summary Forms,
4) Annual land application Field Summary Forms, 5) Residual Analysis Lab Sheets, 6) TCLP Lab Sheets, 7)
Pathogen & Vector Attraction Forms, 8) Pathogen and Vector Attraction Reduction Documentation, 9) Soils
Lab Data 10) 2023 Application Summary Table, and 11) 2023 Application Condition Summaries.
A total of 8,357,358 gallons of Class B lime -stabilized biosolids
injected/incorporated/ SOUR tested biosolids were land applied to 270.32 acres i
applied as follows:
• 168,000 gallons (I I dry tons) from Beulaville WWTP,
• 4,179,320 gallons (459.39 dry tons) from Clayton Little Creek WRF,
• 60,000 gallons (3.25 dry tons) from Kenansville WWTP,
• No Applications were made the Town of Rose Hill,
0 914,000 gallons (50.69 dry tons) from Warsaw WWTP,
• 36,000 gallons (1.65 dry tons) from Southwest Plantation WWTP
• 54,000 gallons (1:1 dry tons) from the Town of Bridgeton,
• 96,000 gallons (1.96 dry tons), from the Town of Maysville,
0 384,476 gallons (12.12 dry tons), from the Summerhouse WWTP,
• 403,122 gallons (30.09 dry tons) from Swansboro WWTP, and
• 1,710,000 gallons (191.27 dry tons) from the Town of Wallace.
or Class B fecal and
n 2023. This material was
If any further information is required regarding this land application program, please do not hesitate to contact
me at [phone].
Sincerely,
t
Robert T. Branch, L.S.S.
Land Application/Residuals Operator # 15676
RTB
Enclosures
cc: Town of Beulaville Town of Kenansville ONWASA Northwest Regional WWTP
ONWASA Summerhouse WWTP Town of Warsaw Southwest Plantation
Town of Wallace Town of Clayton Town of Bridgeton
Town of Maysville ONWASA Swansboro WWTP

TABLE OF CONTENTS
SECTION NO. TITLE
I Certification Forms and Facility Information
II Annual Residual Sampling Summary Forms
III Annual Metals Field Loading Summary Forms
IV Annual Land Application Field Summary Forms
V Residual Analysis Lab Sheets
VI Toxicity Characteristics Leaching Procedure
(TCLP) Analysis Report
VII Pathogen and Vector Attraction Reduction
Forms
VIII Pathogen and Vector Attraction Reduction Documentation
IX Soil Analysis Reports
X 2023 Application Summary Table
XI 2023 Application Condition Summaries

CERTIFICATION FORMS AND FACILITY INFORMATION

ANNUAL LAND APPLICATION CERTIFICATION FORM
WQ Permit#: WQ0030998 County: Duplin Year: 2023
Facility Name (as shown on permit): Triple S Farms & Cleaning
Land Application Operator: Triple S Farms & Cleaning Phone: [phone]
Land application of residuals as allowed by the permit occurred during the past calendar year?
El Yes ❑ No - If No, skip Part A, and Part B and proceed to Part C. Also, If residuals were
generated but not land applied, please attach an explanation on how the residuals were handled.
Part A - Residuals Application_ ummary:
Total number of a lication fields in thepermit:
26
Total number of fields utilized for land ap lication during the year:
21
Total amount of dry tons aEplied during the year for all application sites:
717.25
Total number of acres utilizes for land application during the year:
270.32
Part B - Annual Comuiance Statement:
Facility was compliant during calendar year 2023 with all conditions of the land application permit
(including but not limited to items 1-13 below) issued by the Division of Water Quality. ❑ Yes El No
If no please, provide a written description why the facility was not compliant, the dates, and explain corrective action taken. The Town
of Maysville was noncompliant ( explanation follows). Other facildes and the land applier were compliant.
1) Only residuals approved for this permit were applied to the permitted sites.
2) Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or
the limit specified in the permit.
3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies
of laboratory results are attached.
4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5) All other monitoring was performed in accordance with the permit and reported during the year as required and three
(3) copies of certified laboratory results are attached.
6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .1105(a) or the Pollutant
Loading Rates in 15A NCAC 02T .I 105(b) (applicable to 40 CFR Part 503 regulated facilities).
7) All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part
503 regulated facilities).
8) All monitoring and reporting requirements in 15A NCAC 02T. I I I I were complied with (applicable to 40 CFR Part
503 regulated facilities).
9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Quality.
10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
11) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as
specified in the permit.
12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13) All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C - Certification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate.
and complete. I am aware that there are significant penalties for submitting false information, including the
possibility of fines and imprisonment for knowing violations."
Mr. Eric R. Smith, Owner
Permittee Name and Title (type or print)
Signature of Permittee Date
See Attached
Signature of Preparer* Date Signature of Land Applier Date
(if different from Permittee) (if different from Permittee and Preparer)

ANNUAL LAND APPLICATION CERTIFICATION FORM
TOWN OF BRIDGETON
Part B - Annual Compiance Statement:
Facility was compliant during calendar year 2023 with all conditions of the land application permit
(including but not limited to items 1-13 below) issued by the Division of Water Quality. El Yes p No
If no please, provide a written description why the facility was not compliant, the dates, and explain corrective
action taken.
I ) Only residuals approved for this permit were applied to the permitted sites.
2) Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or
the limit specified in the permit.
3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies
of laboratory results are attached.
4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5) All other monitoring was performed in accordance with the permit and reported during the year as required and three
(3) copies of certified laboratory results are attached.
6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .1105(a) or the Pollutant
Loading Rates in 15A NCAC 02T .1105(b) (applicable to 40 CFR Part 503 regulated facilities).
7) All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Pan
503 regulated facilities).
8) All monitoring and reporting requirements in 15A NCAC 02T .1111 were complied with (applicable to 40 CFR Part
503 regulated facilities).
9) All operations and maintenance requirements in the pennit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Quality.
10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
1 1) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as
specified in the permit.
12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13) All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C - Certification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate
and complete. I am aware that there are significant penalties for submitting false information, including the
possibility of fines and imprisonment for knowing violations."
Signature of Preparer* Date
(if different from Perriuttee)
* Preparer is defined in 40 CFR Part 503.9 (r) and 15A NCAC 02T. 1102 (26)

ANNUAL LAND APPLICATION CERTIFICATION FORM
TOWN OF BEULAVILLE
Part B - Annual Comniance Statement:
Facility was compliant during calendar year 2023 with all conditions of the land application permit
(including but not limited to items 1-13 below) issued by the Division of Water Quality. El Yes p No
If no please, provide a written description why the facility was not compliant, the dates, and explain corrective
action taken.
1) Only residuals approved for this permit were applied to the permitted sites.
2) Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or
the limit specified in the permit.
3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies
of laboratory results are attached.
4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5) All other monitoring was performed in accordance with the permit and reported during the year as required and three
(3) copies of certified laboratory results are attached.
6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .1105(a) or the Pollutant
Loading Rates in 15A NCAC 02T .1105(b) (applicable to 40 CFR Part 503 regulated facilities).
7) All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part
503 regulated facilities).
8) All monitoring and reporting requirements in 15A NCAC 02T .1111 were complied with (applicable to 40 CFR Part
503 regulated facilities).
9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Quality.
10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
11) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as
specified in the permit.
12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13) All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C - Certification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate
and complete. I am aware that there are significant penalties for submitting false information, including the
possibility of fines and imprisonment for knowing violations."
Signature o re rer* Date
(if different from Permittee)
* Preparer is defined in 40 CFR Part 503.9 (r) and 15A NCAC 02T .1102 (26)

ANNUAL LAND APPLICATION CERTIFICATION FORTNII
TOWN OF CLAYTON
Part B - Annual Compiance Statement:
Facility was compliant during calendar year 2023 with all conditions of the land application permit
(including but not limited to items 1-13 below) issued by the Division of Water Quality. CJ Yes ❑ No
If no please, provide a written description why the facility was not compliant, the dates, and explain corrective
action taken.
I ) Only residuals approved for this permit were applied to the pernutted sites.
2) Soil pH was adjusted as specified in the pernut and lime was applied (if needed) to achieve a soil pII of at least 6.0 or
the limit specified in the pennit.
3) Annual soils analysis were perforned on each site receiving residuals during the past calendar year and three (3) copies
of laboratory results are attached.
4) Annual TCLP analysis (if required) was perfonmed and three (3) copies of certified laboratory results are attached.
5) All other monitoring was perfonmed in accordance with the pennit and reported during the year as required and three
(3) copies of certified laboratory results are attached.
6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .1 105(a) or the Pollutant
Loading Rates in 15A NCAC 02T .l 105(b) (applicable to 40 CFR Pan 503 regulated facilities).
7) All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part
503 regulated facilities).
8) All monitoring and reporting requirements in 15A NCAC 02T .I 11 l were complied with (applicable to 40 CFR
Part 503 regulated facilities).
9) All operations and maintenance requirements in the pennit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Quality.
10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
1 1) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as
specified in the permit.
12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13) All buffer requirements as specified on the pennit were maintained during each application of residuals.
Part C - Certification:
"1 certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate
and complete. I am aware that there are significant penalties for submitting false information, including the
possibility of fines and imprisonment for kning violations."
Signature of Preparer* 1./� /' ate
(if different from Permittee)
* Preparer is defined in 40 CFR Part 503.9 (r) and 15A NCAC 02T .1 102 (26)

ANNUAL LAND APPLICATION CERTIFICATION FORM
TOWN OF KENANSVILLE
Part B - Annual Comaiance Statement:
Facility was compliant during calendar year 2023 with all conditions of the land application permit
(including but not limited to items 1-13 below) issued by the Division of Water Quality. El Yes ❑ No
If no please, provide a written description why the facility was not compliant, the dates, and explain corrective
action taken.
1) Only residuals approved for this permit were applied to the permitted sites.
2) Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or
the limit specified in the permit.
3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies
of laboratory results are attached.
4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5) All other monitoring was performed in accordance with the pen -nit and reported during the year as required and three
(3) copies of certified laboratory results are attached.
6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .1105(a) or the Pollutant
Loading Rates in 15A NCAC 02T .1105(b) (applicable to 40 CFR Part 503 regulated facilities).
7) All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part
503 regulated facilities).
8) All monitoring and reporting requirements in 15A NCAC 02T. I I I I were complied with (applicable to 40 CFR Part
503 regulated facilities).
9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Quality.
10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
11) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as
specified in the permit.
12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13) All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C - Certification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate
and complete. I am aware that there are significant penalties for submitting false information, including the
possibility of fines and imprisonment for knowing violations."
Signature ottreparer* Date
(if different from Permittee)
* Preparer is defined in 40 CFR Part 503.9 (r) and 15A NCAC 02T .1102 (26)

ANNUAL LAND APPLICATION CERTIFICATION FORM
TOWN OF MAYSVILLE
Part B - Annual Compiance Statement:
Facility was compliant during calendar year 2023 with all conditions of the land application permit
(including but not limited to items 1-13 below) issued by the Division of Water Quality. ❑ Yes 0 No
If no please, provide a written description why the facility was not compliant, the dates, and explain corrective
action taken.
1) Only residuals approved for this permit were applied to the permitted sites.
2) Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or
the limit specified in the permit.
3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies
of laboratory results are attached.
4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5) All other monitoring was performed in accordance with the permit and reported during the year as required and three
(3) copies of certified laboratory results are attached.
6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .1105(a) or the Pollutant
Loading Rates in 15A NCAC 02T. I 105(b) (applicable to 40 CFR Part 503 regulated facilities).
7) All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part
503 regulated facilities).
8) All monitoring and reporting requirements in 15A NCAC 02T .1111 were complied with (applicable to 40 CFR
Part 503 regulated facilities).
9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Quality.
10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
11) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as
specified in the permit.
12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13) All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C - Certification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate
and complete. I am aware that there are significant penalties for submitting false information, including the
possibility of fines 9d imprisonment for knowing violations."
of Preparer*
Date
(if different from Permittee)
* Preparer is defined in 40 CFR Part 503.9 (r) and 15A NCAC 02T .1102 (26)

ANNUAL LAND APPLICATION CERTIFICATION FORM
NORTHWEST REGIONAL WWTP
Part B - Annual Compiance Statement:
Facility was compliant during calendar year 2023 with all conditions of the land application permit
(including but not limited to items 1-13 below) issued by the Division of Water Quality. El Yes ❑ No
If no please, provide a written description why the facility was not compliant, the dates, and explain corrective
action taken.
1) Only residuals approved for this permit were applied to the permitted sites.
2) Soil pH was adjusted as specified in the permit and time was applied (if needed) to achieve a soil pH of at least 6.0 or
the limit specified in the permit.
3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies
of laboratory results are attached.
4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5) All other monitoring was performed in accordance with the permit and reported during the year as required and three
(3) copies of certified laboratory results are attached.
6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .1105(a) or the Pollutant
Loading Rates in 15A NCAC 02T .1105(b) (applicable to 40 CFR Part 503 regulated facilities).
7) All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part
503 regulated facilities).
8) All monitoring and reporting requirements in 15A NCAC 02T .1111 were complied with (applicable to 40 CFR Part
503 regulated facilities).
9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Quality.
10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
11) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as
specified in the permit.
12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13) All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C - Certification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate,
and complete. I am aware that there are significant penalties for submitting false information, including the
possibility of fines and imprisonment for knowing violations."
Signature of Preparer* (/ Date
(if different from Pertnittee)
* Preparer is defined in 40 CFR Part 503.9 (r) and 15A NCAC 02T .1102 (26)

ANNUAL LAND APPLICATION CERTIFICATION FORM
SOUTIIW LS'l I'LANTATI ON
Part B - Annual Compiance Statement:
Facifit- was compliant during calendar year 2023 with all conditions of the land application permit
(including but not limieed to items 1-13 heloa) issued by the Division of Water Quality. 1] Yes Cl No
If no please, provide a written description Nvhy the facility was not compliant, the date%, and explain corrective
action taken.
1) Unly residuals approved for this permit were applied to the pvrinitted sites.
2) Soil pl-i was adjusted as specified in the pennit and litne was applied (if needed) to achieve a soil pH of at least 6.0 or
the limit specified in the permit.
3) Annual soils analysis were performed un each site receiving residuals during the past calendar yeai and three (3) copies
of laboratury results are attached-
4 *1 Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratun- results arc attachcd.
5) All other monitoring was performed in accordance: with the permit and reported during the � ear as required and three
(3) copies of'certifted laboratory results are attached.
6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 021' .1 105(a) or the Pollutant
Loading Rates in 15A NCAC 02T .1 105(b) (applicable to 40 CFR Pan 503 regulated facilities).
7) All general requirements in as specified in the Land Application Permit were complied with tupplicable to 40 CFR Part
503 regulated facilities).
8) All monitoring and reporting recluirennents in 15A NCAC 02T .I 1 I 1 were complied with (applicable to 40 CFR Part
501 regulated facilities).
9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Quality.
10) No, contravention of Ground \loa(er Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and rennediations.
1 1) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as
specified in the permit.
12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13) All buffer requirements as specified an the permit were maintained during each application of residuals.
Part C - Certification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate
and complete. I a�Ttsre that there are significant penalties for submitting false information, including the
possibility of tin and imprisonment for knowing violations,"
Signature erg Hate
(if diff ent rum Permittre)
y
* Pre arur defined in 40 CFR Part 503.9 (r) and 15A NCAC 02T .1102 (26)

ANNUAL. LAND APPLICATION CERTIFICATION FORM
SUMMERHOUSE WRF
Part B - Annual Compiance Statement:
Facility was compliant during calendar year 2023 with all conditions of the land application permit
(including but not limited to items 1-13 below) issued by the Division of Water Quality. El Yes ❑ No
If no please, provide a written description why the facility was not compliant, the dates, and explain corrective
action taken.
1) Only residuals approved for this permit were applied to the permitted sites.
2) SoiI pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or
the limit specified in the permit.
3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies
of laboratory results are attached.
4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5) All other monitoring was performed in accordance with the permit and reported during the year as required and three
(3) copies of certified laboratory results are attached.
6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .1105(a) or the Pollutant
Loading Rates in 15A NCAC 02T .1105(b) (applicable to 40 CFR Part 503 regulated facilities).
7) All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part
503 regulated facilities).
9) All monitoring and reporting requirements in 15A NCAC 02T .1111 were complied with (applicable to 40 CFR Part
503 regulated facilities).
9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Quality.
10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
11) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as
specified in the permit.
12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13) All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C - Certification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate
and complete. I am aware that tl lre are significant penalties for submitting false information, including the
possibility of fines and impriso ment for knowing violations."
2/2
Zf
Signature of P _ aret!/' / Dati
(if differe _ em Per-ruttee)
* Prepares defined in 40 CFR Part 503.9 (r) and 15A NCAC 02T .l 102 (26)

ANNUAL LAND APPLICATION CERTIFICATION FORM
SWANSBORO WWTP
Part B - Annual Comaiance Statement:
Facility was compliant during calendar year 2023 with all conditions of the land application permit
(including but not limited to items 1-13 below) issued by the Division of Water Quality. El Yes ❑ No
If no please, provide a written description why the facility was not compliant, the dates, and explain corrective
action taken.
1) Only residuals approved for this permit were applied to the permitted sites.
2) Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or
the limit specified in the permit.
3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies
of laboratory results are attached.
4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5) All other monitoring was performed in accordance with the permit and reported during the year as required and three
(3) copies of certified laboratory results are attached.
6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .1105(a) or the Pollutant
Loading Rates in 15A NCAC 02T .1105(b) (applicable to 40 CFR Part 503 regulated facilities).
7) All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part
503 regulated facilities).
8) All monitoring and reporting requirements in 15A NCAC 02T .1111 were complied with (applicable to 40 CFR Part
503 regulated facilities).
9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Quality.
10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
11) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as
specified in the permit.
12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13) All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C - Certification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate,
and complete. I am aware that there are significant penalties for submitting false information, including the
possibility of fines and imprisonment for knowing violations."
Signature of Preparerv*,-/ U Date
(if different from Permittee)
* Preparer is defined in 40 CFR Part 503.9 (r) and 15A NCAC 02T .1102 (26)

ANNUAL LAND APPLICATION CERTIFICATION FORM
TOWN OF WALLACE
Part B - Annual Comniance Statement:
Facility was compliant during calendar year 2023 with all conditions of the land application permit
(including but not limited to items 1-13 below) issued by the Division of Water Quality. El Yes El No
If no please, provide a written description why the facility was not compliant, the dates, and explain corrective
action taken.
1) Only residuals approved for this permit were applied to the permitted sites.
2) Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or
the limit specified in the permit.
3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies
of laboratory results are attached.
4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5) All other monitoring was performed in accordance with the permit and reported during the year as required and three
(3) copies of certified laboratory results are attached.
6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .1105(a) or the Pollutant
Loading Rates in 15A NCAC 02T. 1105(b) (applicable to 40 CFR Part 503 regulated facilities).
7) All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part
503 regulated facilities).
8) All monitoring and reporting requirements in 15A NCAC 02T .I I I I were complied with (applicable to 40 CFR Part
503 regulated facilities).
9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Quality.
10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
11) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as
specified in the permit.
12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13) All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C - Certification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate,
and complete. I am aware that there are significant penalties for submitting false Information, including the
possibility of fines and imprisonment for knowing violations."
ncj -�-044 . 2
Signature of Preparer* Date
(if different from Permittee)
* Preparer is defined in 40 CFR Part 503.9 (r) and 15A NCAC 02T .1102 (26)

ANNUAL LAND APPLICATION CERTIFICATION FORM
TOWN OF WARSAW
Part B - Annual Compiance Statement:
Facility was compliant during calendar year 2023 with all conditions of the land application permit
(including but not limited to items 1-13 below) issued by the Division of Water Quality. O Yes ❑ No
If no please, provide a written description why the facility was not compliant, the dates, and explain corrective
action taken.
1) Only residuals approved for this permit were applied to the permitted sites.
2) Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or
the limit specified in the permit.
3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies
of laboratory results are attached.
4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5) All other monitoring was performed in accordance with the permit and reported during the year as required and three
(3) copies of certified laboratory results are attached.
6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .1105(a) or the Pollutant
Loading Rates in 15A NCAC 02T .1105(b) (applicable to 40 CFR Part 503 regulated facilities).
7) All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part
503 regulated facilities).
8) All monitoring and reporting requirements in 15A NCAC 02T .1111 were complied with (applicable to 40 CFR Part
503 regulated facilities).
9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Quality.
10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
11) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as
specified in the permit.
12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13) All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C - Certification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate
and complete. I am awarg that there are significant penalties for submitting false information, including the
possibility of fines and imprisonment for knowing violations."
Pam^ J 7L
Signature of Preparer* Date
(if different from Permittee)
* Preparer is defined in 40 CFR Part 503.9 (r) and 15A NCAC 02T .1102 (26)
2-26-24

ANNUAL RESIDUAL SAMPLING SUMMARY FORMS

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ANNUAL METALS FIELD LOADING SUMMARY FORMS

ANNUAL METALS FIELD LOADING SUMMARY FORM
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Triple S Farms Total Dry Tons Applied (Annual): 199.95
Permit #: WQ0030998 Cation Exchange Capacity (non 503 only): n/a
Operator: Eric Smith Owner: Eric Smith Predominant Soil Series NoA
Acres Used: 36 Acres Permitted: 36 Site #: l Field #: I
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
wL iowi.nnsda rt.ini_nni r i-,n_ini_i wci ,m,_ r, n_,cc an .IdnA r, „ uc nr un , ,n„ n, „ ,
Sample
orCom-
posite
Date
1/10/23
4/10/23
4/1023
6/21/23
9/12123
3/20/23
9/12/23
7/11/23
12/19/23
12/22123
10/3123
12/22/23
% Solids
2.97
2.78
2.78
1.13
2.69
0.49
2.69
2.41
2.44
2.57
2.40
1.78
Arsenic
20.70
17.90
17.90
41.20
18.50
2.50
18.50
19.10
20.80
19.20
19.80
12.90
Cadmium
15.98
3.57
3.57
41.20
3.70
2.00
3.70
38.30
4.17
3.75
19.80
12.90
Chromium
28.20
17.20
17.20
41.20
24.80
20.00
24.80
38.30
19.00
16.60
23.40
15.70
Copper
790.00
138.00
138.00
395.00
156.00
463.00
156.00
755.00
135.00
127.00
579.00
83.10
Lead
35.90
10.70
10.70
51.20
11.10
18.00
11.10
38.30
12.50
11.50
26.00
12.90
Mercury
0.92
6.39
6.39
1.69
6.19
0.26
6.19
0.72
7.50
6.62
0.76
0.89
Molyb-
denum
15.98
8.93
8.93
41.20
9.26
7.10
9.26
38.30
10.40
9.62
19.80
12.90
Nickel
20.00
17.40
17.40
41.20
15.70
17.00
15.70
38.30
15.00
15.10
19.80
12.90
15.98
27.90
27.90
41.20
18.50
5.00
18.50
38.30
20.80
19.20
19.80
12.90
1390.00
664.00
664.00
784.00
800.00
2989.00
800.00
1340.00
571.00
546.00
1010.00
370.00
Lh
19,500
31,600
31,600
27,100
34,300
16,160
34,300
18,200
28,800
26,200
14,900
1,800
Annuat heavy metal meld Loadings
(Ualculated in lbs/acre):
H
rnari
00.64
0.43
0.15
0.25
0.15
0.02
0.90
0.57
1.65
0.32
0.38
0.10
e
3 �
Arsenic
0.03
0.02
1 0.01
0.02
1 0.01
0.00
0.03
0.02
0.07
0.01
0.02
0.00
0.2.
Cadmium
0.02
0.00
0.00
0.02
0.00
0.00
0.01
0.04
0.01
0.00
0.02
0.00
0. F
�harworniUmiji
0.04
0.01
0.01
0.02
0.01
0.00
0.04
0.04
0.06
0.01
0.02
0.00
0.2'
Copper
1.01
0.12
0.04
0.20
0.05
0.02
0.28
0.86
0.44
0.08
0.44
0.02
3.51
Lead
0.05
0.01
0.00
0.03
0.00
0.00
0.02
0.04
0.04
0.01
0.02
0.00
0.2:
Mercury
0.00
0.01
0.00
0.00
0.00
0.00
0.01
0.00
0.02
0.00
0.00
0.00
0.0:
Molyb-
denum
0.02
0.01
0.00
0.02
0.00
0.00
0.02
0.04
0.03
0.01
0.02
0.00
0.1'
Nickel
0.03
0.01
0.01
0.02
0.00
0.00
0.03
0.04
0.05
0.01
0.02
0.00
0.2:
Selenium
0.02
0.02
0.01
0.02
0.01
0.00
0.03
0.04
0.07
0.01
0.02
0.00
0.2:
Zinc
1.78
0.56
0.21
0.39
0.24
0.12
1.44
1.53
1.88
0.35
0.77
0.07
9.3-
Total
1
Phos-
24.92
26.86
9.77
13.48
10.26
0.66
61.60
20.73
94.77
16.85
11.43
1 0.36
29 Li
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
sig cant penald s for bmitting false information, including the possibilityof fi/nes and imprisonment for knowing violations"
Signature of Land Applter Date

ANNUAL METALS FIELD LOADING SUMMARY FORM
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Triple S Farms Total Dry Tons Applied (Annual): 70.92
Permit #: WQ0030998 Cation Exchange Capacity (non 503 only): nia
Operator: Eric Smith Owner: Eric Smith Predominant Soil Series FoA
Acres Used: 12.6 Acres Permitted: 12.6 Site #: 1 Field #: 2
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
r 1.71.in1.nn1 7nvt_n2AAn t un i in,,
Sample
orCom-
posite
Date
4/10/23
5/2/23
9112t23
7/11/23
12/22/23
3/20/23
% Solids
2.78
2.80
2.69
2.41
2.57
0.49
Arsenic
17.90
35.00
18.50
19.10
19.20
2.50
Cadmium
3.57
35.00
3.70
38.30
3.75
2.00
Chromium
17.20
35.00
24.80
38.30
16.60
20.00
-Copper
138.00
718.00
156.00
755.00
1 127.00
463.00
Lead
10.70
36.80
11.10
38.30
11.50
18.00
Mercury
6.39
0.64
6.I9
0.72
6.62
0.26
Molyb-
denum
8.93
35.00
9.26
38.30
9.62
7.10
Nickel
17.40
35.00
15.70
38.30
15.10
17.00
Selenium
27.90
35.00
18.50
38.30
19.20
5.00
Zinc
664.00
1140.00
800.00
1340.00
546.00
2989.00
Total
Phos-
horus
31,600
819
34,300
18,200
26,200
16,160
r►u.aun, raCavy iraC181 VIM i.oaamgs
(c;alculated
in Ibs/acre):
* -i
`> 0
o+
$ 0
1.49
1.28
0.43
1.39
1.02
0.03
.4
a- n
Arsenic
0.05
0.09
0.02
0.05
1 0.04
0.00
1
0.2.
Cadmium
0.01
0.09
0.00
0.11-1
0.01
0.00
0 2:
Chromium
0.05
0.09
0.02
0.11
0.03
0.00
0.31
Copper
0.41
1.84
0.13
2.10
0.26
0.03
4.71
Lead
0.03
0.09
0.01
0.11
0.02
0.00
0 2'
Mercury
0.02
0.00
0.01
0.00
0.01
0.00
1
0.01
Molyb-
denum
0.03
0.09
0.01
0.11
0.02
0.00
0.2:
Nickel
0.05
0.09
0.01
0.11
0.03
0.00
0 2,
Selenium 1
0.08
0.09
0.02
0.11
0.04
0.00
0.3:
Zinc
1.98
2.92
0.68
3.72
1.11
0.17
10.5
Total
Phos-
94.20
2.09 1
29.30
50.52
53.20
0.94
230.:
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. 1 am aware that there are
significant penalties for subjnItting false information, including the possibility f fines and Imprisonment for knowing violations"
7A W. - . - .-. 41-111all
Signature of Land Applier Date

ANNUAL METALS FIELD LOADING SUMMARY FORM
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Reporl
Facility Name: Triple S Farms Total Dry Tons Applied (Annual):
Permit #: WQ0030998 Cation Exchange Capacity (non 503 only): n,a
Operator: Eric Smith Owner: Eric Smith Predominant Soil Series FoA
Acres Used: 14 Acres Permitted: 14 Site #: I Field #:
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
r i.7i.Inldlni7Mi.nuni1t uv7mi_mcurojmi,un i_imi_un a_Im,
an Qr.
Sample
orCom-
posite
Date
4/10/23
2/28/23
2/14/23
9/28/23
1/10/23
10/3,23
% Solids
2.78
0.76
1 0.49
1.10
2.97
2.40
Arsenic
17.90
25.30
43.10
43.60
20.70
19.80
Cadmium
3.57
25.30
43.10
43.70
15.98
19.80
Chromium
17.20
25.30
43.10
43.70
28.20
23.40
Copper
138.00
114.00
496.00
214.00
790.00
579.00
Lead
10.70
25.30
43.10
43.70
35.90
26.00
Mercury
6.39
2.32
3.51
1.40
0.92
0.76
Molyb-
denum
8.93
25.30
43.10
43.70
15.98
19.80
Nickel
17.40
25.30
43.10
43.70
20.00
19.80
Selenium
27.90
25.30
43.10
43.70
15.98
19.80
Zinc
664.00
2210.00
784.00
1370.00
1390.001010.00
Total
Phos-
horus
31,600
25,800
21,400
12,500
19,500
14,900
Annuali
heavy Metal Yield Loadings
(Calculated
in Ibs/acre):
-t
Z. a
.0
2.09
0.14
0.06
0.04
0.27
0.26
y
2
0>
3. C
..
Arsenic
0.07
0.01
1 0.01
0.00
0.01
1 0.01
1
0.11
Cadmium
0.01
0.01
0.01
0.00
0.01
0.01
0.0!
Chromium
0.07
0.01
0.01
0.00
0.01
0.01
0.11
Copper
0.58
0.03
0.06
0.02
0.42
0.30
1.4(
Lead
0.04
0.01
0.01
0.00
0.02
0.01
0.05
Mercury
0.03
0.00
0.00
0.00
0.00
0.00
0,02.
Molyb-
denum
0.04
0.01
0.01
0.00
0.01
0.01
0.0;
Nickel
0.07
0.01
0.01
0.00
0.01
0.01
0.11
Selenium
0.12
0.01
0.01
0.00
0.01
0.01
0.1!
Zinc
2.77
0.60
0.10
0.11
0.74
1 0.52
4,8?
Total
Phos-
131.95
7.02
2.62
0.98
10.34
1 7.67
160.!
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for s mitting false information, including the possibility of fines and imprisonment for knowing violations"
a71,3 laq
Signature of Land Applier Date:

ANNUAL METALS FIELD LOADING SUMMARY FORM
Attach this form to the corresponding Field Loading Summary Form to be submitted In Annual Report
Facility Name: Triple S Farms Total Dry Tons Applied (Annual): 80.77
Permit #: WQ0030998 Cation Exchange Capacity (non 503 only): n1a
Operator: Eric Smith Owner: Eric Smith Predominant Soil Series FoA
Acres Used: 19.6 Acres Permitted: 19.6 Site #: I Field #: 345
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
C 1-23-101-Oni 23-101_Ml WL.I_?n23.lyd_39.961.W1.d.]n?v
Sample
or Com-
posite
Date
4/10/23
4/10/23
1/10/23
12/22/23
105 23
% Solids
2.78
2.78
2.97
2.57
2.40
Arsenic
17.90
17.90
20.70
19.20
19.80
Cadmium
3.57
3.57
15.98
3.75
19.80
Chromium
17.20
17.20
28.20
16.60
23.40
Copper
138.00
138.00
790.00
127.00
579.00
Lead
10.70
10.70
35.90
11.50
26.00
Mercury
6.39
6.39
0.92
6.62
0.76
Molyb-
denum
8.93
8.93
15.98
9.62
19.80
Nickel
17.40
17.40
20.00
15.10
19.80
Selenium
27.90
27.90
15.98
19.20
19.80
Zinc
664.00
664.00
1390.00
546.00
1010.00
Total
Phos-
horu5
31,600
31.600
19,500
26,200
14,900
Annual
Heavy Metal Field Loadings
(Calculated
in Ibs/acre):
o
mag,
o
0
0.28
0.92
1.10
1.05
0.77
7 �
Arsenic
0.01
0.03
0.05
0.04
0.03
1
1
1
0.1
Cadmium
0.00
0.01
0.04
0.01
0.03
0.0
Chromium
0.01
0.03
0.06
0.03
0.04
0.1
Copper
0.08
0.25
1.73
0.27
0.89
3.2
Lead
0.01
0.02
0.08
0.02
0.04
0.1
Mercury
0.00
0.01
0.00
0.01
0.00
0.0
Molyb-
denum
0.01
0.02
0.04
0.02
0.03
0.1
Nickel
0.01
0.03
0.04
0.03
0.03
0.1
Selenium
0.02
0.05
0.04
0.04
0.03
0.1
Zinc
0.38
1.23
3.05
1.15
1.55
7.3
Total
Phos-
17.95
58.32
42.82
55.05
22.82
196,
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there an
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations"
ILI �1D.0
Signature of Land Applier Date

ANNUAL METALS FIELD LOADING SUMMARY FORM
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Triple S Farms Total Dry Tons Applied (Annual): 106.54
Permit #: WQ0030998 Cation Exchange Capacity (non 503 only): n/a
Operator: Eric Smith Owner: Eric Smith Predominant Soil Series GoA
Acres Used: 17.3 Acres Permitted: 17.3 Site #: I Field #: 6
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
r i.7;.Inl.nnl ,)mnt.nnt wri mrui r7_7um&wr 7_7n7i. \VC770)7Ir 7_7t_i51_OI \VI 3_7tl77_r i77_761_O
Sample
or Com-
posite
Date
4/10/23
4/10123
6/210
9/12/23
5/2/23
12/22/23
12/19/23
7/11/23
12/22/23
% Solids
2.78
2.78
1.13
2.69
2.80
1.78
2.44
2.41
2.57
Arsenic
17.90
17.90
41.20
18.50
35.00
12.90
20.80
19.10
19.20
Cadmium
3.57
3.57
41.20
3.70
35.00
12.90
4.17
38.30
3.75
Chromium
17.20
17.20
41.20
24.80
35.00
15.70
19.00
38.30
16.60
Copper
138.00
138.00
395.00
156.00
718.00
83.10
135.00
755.00
127.00
Lead
10.70
10.70
51.20
11.10
36.80
12.90
12.50
38.30
11.50
Mercury
6.39
6.39
1.69
6.19
0.64
0.89
7.50
0.72
6.62
Molyb-
denum
8.93
8.93
41.20
9.26
35.00
12.90
10.40
38.30
9.62
Nickel
17.40
17.40
41.20
15.70
35.00
12.90
15.00
38.30
15.10
Selenium
27.90
27.90
41.20
18.50
35.00
12.90
20.80
38.30
19.20
Zinc
664.00
664.00
784.00
800.00
1140.00
370.00
571.00
1340.00
546.00
Total
Phos-
horus
31,600
31,600
27,100
34,300
819
1,800
28,800
18,200
26,200
Annual
Heavy Metal Field Loadings
(Calculated
in Ibs/acre):
n,ad
0
0.24
0.64
0.25
1.95
0.53
0.56
1.06
0.17
0.76
e
9
o, n
3
..
Arsenic
0.01
0.02
1 0.02
0.07 1
0.04
0.01
0.04 1
0.01
0.03 1
1
0.:
Cadmium
0.00
0.00
0.02
0.01
0.04
0.01
0.01
0.01
0.01
0.)
Chromium
0.01
0.02
0.02
0.10
0.04
0.02
0.04
0.01
0.03
0.1
Copper
0.07
0.18
0.19
0.61
0.76
0.09
0.29
0.26
0.19
2d
Lead
0.01
0.01
0.03
0.04
0.04
0.01
0.03
0.01
0.02
0.,
Mercury
0.00
0.01
0.00
0.02
0.00
0.00
0.02
0.00
0.01
0.(
Molyb-
0.00
0.01
0.02
0.04
0.04
0.01
0.02
0.01
0.01
0.
denum
Nickel
0.01
0.02
0.02
0.06
0.04
0.01
0.03
0.01
0.02
0.:
Selenium
0.01
0.04
0.02
0.07
0.04
0.01
0.04
0.01
0.03
0.:
Zinc
0.32
0.85
0.38
3.11
1.20
0.42
1.21
0.47
0.83
8.1
Total
Phos-
15.25
40.66
13.29
133.45
0.86
2.02
61.01
6.34
39.90
312
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there at
significant penalties rAsuitting false information, including the possibility of fines and imprisonment for knowing violations"
bsj
Signature of Land Applier Date

ANNUAL METALS FIELD LOADING SUMMARY FORM
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Triple S Farms Total Dry Tons Applied (Annual): 46.76
Permit #: WQ0030998 Cation Exchange Capacity (non 503 only): Wa
Operator: Eric Smith Owner: Eric Smith Predominant Soil Series FoA
Acres Used: 11.5 Acres Permitted: 11.5 Site #: 1 Field #: 7
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
r
Sample
or Com-
posite
Date
4/10/23
5/2/23
12/22i23
%Solids
2.78
2.80
2.57
Arsenic
17.90
35.00
19.20
Cadmium
3.57
35.00
3.75
Chromium
17.20
35.00
16.60
Copper
138.00
718.00
127.00
Lead
1 10.70
36.80
1 11.50
Mercury
6.39
0.64
6.62
Molyb-
denum
8.93
35.00
9.62
Nickel
17.40
35.00
15.10
27.90
35.00
19.20
664.00
1140.00
546.00
L
31.600
819
26,200
Annual
Heavy Metal Field Loadings
(Calculated
In Ibs/acre):
m > P-
n d
1.03
1.58
1.45
m
o• n
Arsenic
0.04
0.11
0.06
0.2
Cadmium
0.01
0.11
0.01
0.1
Chromium
0.04
0.11
0.05
0.1
Copper
0.28
2.27
0.37
2.9
Lead
0.02
0.12
0.03
0.1
Mercury
0.01
0.00
0.02
0.0
Molyb-
denum
0.02
0.11
0.03
0.1
Nickel
0.04
0.11
0.04
0.1
Seleniuml
0.06
0.I1
0.06
0.2
Zinc
1.37
3.61
1.59
6.5
Total
1
Phos-
64.98
2.59
76.18
143
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there ar
significant penalties for stihotting false information, including the possibilitykiffines and imprisonment for knowing violations"
`/
Signature of Land Applier Date

:ANNUAL. METALS FIELD LOADING SUMMARY FORM
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility ,'dame:
Permit P#:
Operator:
Acres Used:
NVQ0030998
Eric Smith
Triple S Farms Total Dry Tons Applied (Annual):
Cation Exchange Capacity (non 503 only):
Owner: Eric Smith Predominant Soil Series
16.1 Acres Permitted: 16.1 Site #: t Field 4:
n/a
GoA
Residual Analysis Data (Reavy Metals and 'l'otal Phosphorus use mg/kg, % Solids use Ra`v Percent #):
C 2-2_-256.003 23.256.003 W"t-2-2023-i C+4.23.361
73.73
Sample
or Cornr-
9.-12i23
9/12/23
5023
1"-22r;23
posite
Mule
'
% Solids
2.69
2.69
2.80
2.57
Arsenic
18.50
18.50
35.00
19.20
Cadmium
3.70
3.70
35.00
3,75
Chromium
24.80
24.80
35.00
16.60
T
Copper
156,00
156.00
718.00
127,00
_
:_cad
11.10
11.10
36.80
11.50
Alercwv
0.19
6.19
0.64
6.62
Molyh-
9.26
9.26
35.00
9.62
denurn
Nickel
15.70
15.70
35.00
15.10
Seleniuml
18.50
18.50
35.00
19.20
Zinc
800.00
800.00
1140.00
546.00
Total
Phos-
34,300
34,300
819
26,200
horus
Annual Heavy Metal field Loadings (Calculated in lbs/acre):
�r
1.63
1,46
0.57
0.92
a
.0
n'
�n
Arsenic.
0.06
0.05
0.04
0.04
1
1
1
0.19
Cadmium
0.01
0.01
0.04
0.01
0.07
C hromiLlUl
0,08
0.07
0.04
0.03
0.22
Copper
0.51
0.46
0.81
0.23
2.01
Lead
0.04
0.03
0.04
0.02
0,13
Mercury
0.02
0.02
0.00
0.01
0.05
t�lolyh
0.03
0.03
0.04
0.02
0.11
denurn
Nicks l
0.05
0.05
0.04
0.03
_
0.16
Selenium
0.06
0.05
0.04
0.04
0.19
Zinc
2.61
2.34
1.29
1.00
7.24
Total
Phos-
111.84
100.37
0.93
4 8.2 1
261.35
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
sii = ii'tir_ant penalties for su rtting false information, including the possibili y off es and imprisonment for knowing violations"
1--
7, .
--
Signature of Land Applier Date
Author Daryl D. Merritt DENR FORM MFLSF (7!2002)

ANINUAL N4IETALS FIELD LOADINGSUNIMARY FORM
Attach this farm to the corresponding Field Loading Sumntary Form to be subntitted in Annual Report
Facility Natne:
Permit fl:
Operator:
Acres Used:
Triple S Farms 'Total Dry Tons Applied (.Annual)
WQ0030998 Cation Exchange Capacity (non 503 only): _
Fric Smith Owner: Eric Smith Predominant Soil Series
12.8 Acres Permitted: 12.8 Site #
40.41
n/a
NoA
Field #: 10
Residual Analysis Data (IIeavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Wi.. 1 -2023-00643 2.3-101.0401 KV 7023-18 WS2 2023-1'
Sample
or Coin
posite
Datc
1I10."_?
All O!''3
81I b'23
12/22123
5o Solids
2.97
2.78
1.30
1.78
Arsenic
20.70
17.90
32.40
12.90
Cadmium
15.98
3.57
32.40
12.90
C"hromiurn
28.20
17.20
32.40
15.70
Copper
790.00
13,8.00
511.00
83.10
Lead
35.90
10.70
32.40
12.90
_
1N1ercury
0,92
6.39
1.32
0.89
Molyh
denunn
15.98
8,93
32.40
12.90
Nickel
20.00
17.40
32.40
12.90
Selenium
15.98
21.90
32.40
12.90
Zinc
1390.00
664.00
762.00
370.00
Total
Phos-
phorus
10,500
31,600
5,520
1;800
Annual Heavy Metal field Loadings (Calculated in ibs/acre):
0
1.33
0.98
0,25
0.59
d
;>
_ n
Arsenic
0.06
0.04
0.02
0.02
0.12
Cadmium
0.04
0.01
0.02
0.02
0.08
Chromium
0.08
0.03
0.02
0.02
0.14
Copper
I11
0.217
0.26
0.10
2.73
Lead
0.10
0.02
0.02
0.02
0.15
Mercury
0.00
0.01
0.00
0.00
0.02
Molyb-
0.04
0.02
0.02
0.02
0.09
denum
Nickel
0.05
0.03
0.02
0.02
0.12
Selenium
0.04
0.05
0.02
0.02
0.13
Zinc
3.71
1.30
0.39
0.44
5.83
Total
P1105-
52.00
61.83
2.81
2.13
118.76
phorus
"I certify, under penalty of Jaw, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
si * scant penalties for ubmitting false information, including the possibili , of fines and imprisonment for knowing violations"
Signature of Land rAppiier Date
Author Daryl D. Merritt DENR FORM MFLSF (7/2002)

ANNUAL METALS FIELD LOADING SUMMARY FORM
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Triple S Farms Total Dry Tons Applied (Annual): 38.55
Permit #: WQ0030998 Cation Exchange Capacity (non 503 only): n/a
Operator: Scott Thigpen Owner: ScottThigpen Predominant Soil Series FoA
Acres Used: 14.05 Acres Permitted: 14.05 Site #: ST Field #: 1
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
MV 202MI127 mli.1 mA r e_7z_tR 1 cum mm. cum gym:_ 1vc imi_
Sample
orCom-
posite
Date
2/14/23
6/27/23
12/22/23
1/24/24
9/28/23
6/21/23
% Solids
0.49
1.57
2.57
1.79
1.10
1.13
Arsenic
43.10
20.90
19.20
0.00
43.60
41.20
Cadmium
43.10
20.90
3.75
9.27
43.70
41.20
Chromium
43.10
20.90
16.60
19.70
43.70
41.20
Copper
496.00
513.00
127.00
420.00
214.00
395.00
Lead
43.10
29.40
11.50
10.60
43.70
51.20
Mercury
3.51
1.50
6.62
1.12
1.40
1.69
Molyb-
d num
43.10
20.90
9.62
9.27
43.70
41.20
Nickel
43.10
20.90
15.10
13.20
43.70
41.20
Selenium
43.10
20.90
19.20
9.27
43.70
41.20
Zinc
784.00
1230.00
546.00
3980.00
1370.00
784.00
Total
Phos-
horus
21,400
16,200
26,200
12,000
12,500
27,100
Annual Heavy Metal Field Loadings
(Calculated
in Ibs/acre):
M =
v
0.04
0.37
1.42
0.73
0.04
0.14
a
Arsenic
0.00
0.02
1 0.05
0.00
1 0.00
0.01
1
0.01
Cadmium
0.00
0.02
0.01
0.01
0.00
0.OI
0.01
Chromium
0.00
0.02
0.05
0.03
0.00
0.01
0.1
Copper
0.04
0.38
0.36
0.62
0.02
0.11
1.5:
Lead
0.00
0.02
0.03
0.02
0.00
0.01
1
0.0!
Mercury
0.00
0.00
0.02
0.00
0.00
0.00
0.0:
Molyb-
denum
0.00
0.02
0.03
0.01
0.00
0.01
0.0'
Nickel
0.00
0.02
0.04
0.02
0.00
0.01
0.11
Selenium
0.00
0.02
0.05
0.01
0.00
0.01
0.11
Zinc
0.06
0.92
1.55
5.84
0.11
0.22
T 8.61
Total
Phos-
1.68
12.08
74.34
17.60
0.98
7.63
1
1114.
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there art
Sigant penalties for sybmitting false information, including the possibililp of f es �and imprisonment for knowing violations"
� ' � _. � ' �a `t%
Signature of Land Applier Date

ANNUAL METALS FIELD LOADING SUMMARY FORM
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Triple S Farms Total Dry Tons Applied (Annual): 12.58
Permit #: WQ0030998 Cation Exchange Capacity (non 503 only): n/a
Operator: Scott Thigpen Owner: ScottThigpen Predominant Soil Series NbB
Acres Used: 20.3 Acres Permitted: 20.3 Site #: ST Field #: 2
Residual Analysis Data (Heavy Metals and Total Phosphorus use mgtkg, % Solids use Raw Percent #):
CtA41 Fim1_nan�7 )n7iJldnl l cum 7m1_,) umi 7m2_
ample
or Com-
posite
Date
2/28/23
2/28/23
9/28/23
6/21/23
% Solids
0.76
0.76
1.10
1.13
Arsenic
25.30
25.30
43.60
41.20
Cadmium
25.30
25.30
43.70
41.20
Chromium
25.30
25.30
43.70
41.20
Copper
114.00
114.00
214.00
395.00
Lead
25.30
25.30
43.70
51.20
Mercury
2.32
2.32
1.40
1.69
Molyb-
denu
25.30
25.30
43.70
41.20
Nickel
25.30
25.30
43.70
41.20
25.30
25.30
43.70
41.20
2210.00
2210.00
1370.00
784.00
L
25,800
25,800
12,500
27,100
Annual Heavy Metal Field Loadings (Calculated in
�a
n t7 0.12 0.11 0.03 0.36
it y
Arsenic
0.01
0.01
1 0.00
0.03
0.0e
Cadmium
0.01
0.01
0.00
0.03
0.0e
Chromium
0.01
0.01
0.00
0.03
0.0'
Copper
0.03
0.03
0.01
0.28
0.3:
Lead
0.01
0.01
0.00
0.04
0.0:
Mercury
0.00
0.00
0.00
0.00
00
Molyb-
denum
0.01
0.01
0.00
0.03
0.0,
Nickel
0.01
0.01
0.00
0.03
0.0,
Selenium
0.01
0.01
0.00
0.03
0.0,
Zinc
0.54
0.49
0.07
0.56
1.6'
Total
Phos-
6.25
5.77
0.68
19.50
32.1
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
cant Pena ies io supmitting false information, including the possibili of fi es and imprisonment for knowing violations"
Signature of Land Applier Date

ANNUAL METALS FIELD LOADING SUMMARY FORM
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Triple S Farms Total Dry Tons Applied (Annual): 8.41
Permit #: WQ0030998 Cation Exchange Capacity (non 503 only): n/a
Operator: Jonathan Smith Owner: Jonathan Smith Predominant Soil Series WoA
Acres Used: 5.03 Acres Permitted: 5.03 Site #: JS Field #: 2
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
C4-23-361-00092023.04013 WS12023-1.
Sample
or Com-
posite
Date
12/22/23
2/28/23
6/211/23
% Solids
2.57
0.76
1.13
Arsenic
19.20
25.30
41.20
Cadmium
3.75
25.30
41.20
Chromium
16.60
25.30
41.20
Copper
127.00
114.00
395.00
Lead
11.50
25.30
51.20
Mercury
6.62
2.32
1.69
Molyb-
denum
9.62
25.30
41.20
N ickel
15.10
25.30
41.20
Selenium
19.20
25.30
41.20
Zinc
546.00
2210.00
784.00
Total
Phos-
horu5
26,200
25,800
27,100
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
•�
1!
t t
t t
��_��_����
t t'
1 t ONE
# t
i l:
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties fors bmittie information, including the possibility of tines and imprisonment for tatotiving violations,
Signature of Land Appller Date
Atithnr r)wwi n Merritt nF=NR MRM MR SF (7l7()09)

ANNUAL METALS FIELD LOADING SUMMARY FORM
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Triple S Farms Total Dry Tons Applied (Annual): 6.79
Permit #: WQ0030998 Cation Exchange Capacity (non 503 only): n/a
Operator: Jonathan Smith Owner: Jonathan Smith Predominant Soil Series LnA
Acres Used: 7.27 Acres Permitted: 7.27 Site #: JS Field #: 3
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
qmu Fin?i-ndnl i 7mi_i »Rn
.=
rauuuul
rauuuul
heavy ivietai riesa iLoaamgs
tc;aicuiaten in ills/acre):
o
v
0.31
0.62
Arsenic
0.02
0.05
0.0'
Cadmium
0.02
0.05
0.01
Chromium
0.02
0.05
0.0'
Copper
0.07
0.49
0.51
Lead
0.02
0.06
0.01
Mercury
0.00
0.00
0.01
Molyb-
0.02
0.05
denum
0.0'
Nickel
0.02
0.05
0.01
Selenium
0.02
0.05
0.0'
Zinc 1
1.38
0.98
2.31
Total
Phos- 16.10 1 33.72 49.8
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penal 'es for bmitting false information, including the possibility f fines and imprisonment for knowing violations"
y
Signature of Land Applier Date

ANNUAL METALS FIELD LOADING SUMMARY FORM
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Triple S Farms Total Dry Tons Applied (Annual): 14.34
Permit #: WQ0030998 Cation Exchange Capacity (non 503 only): n a
Operator: Jonathan Smith Owner: Jonathan Smith Predominant Soil Series WoA
Acres Used: 8.66 Acres Permitted: 866 Site #: JS Field #: 4
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
C 4-23-361-0009 2023-04013 WS1 2023-1
Sample
or Com-
posite
Date
12/22/23
2128/23
6'21123
% Solids
2.57
0.76
1.13
Arsenic
19.20
25.30
41.20
Cadmium
3.75
25.30
41.20
Chromium
16.60
25.30
41.20
Copper
127.00
114.00
395.00
Lead
11.50
25.30
51.20
Mercury
6.62
2.32
1.69
Molyb-
denum
9.62
25.30
41.20
Nickel
15.10
25.30
41.20
Selenium
19.20
25.30
41.20
Zinc
546.00
2210.00
784.00
Total
Phos-
horus
26,200
25,800
27,100
Annual Heavy Metal Field Loadings (Calculated in ibs/acre):
/
1
t
•
1 1
1!
1 1'
__________
t t
•
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penaltites for, ubmitdng false information, including the possibility f fine and imprisonment for knowing violations"
Signature of Land Applier Date
Author f3arvl f7 Merritt DENR FORM MFLSF (7/2002)

ANNUAL METALS FIELD LOADING SUMMARY FORM
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Triple S Farms Total Dry Tons Applied (Annual): 17.73
Permit #: WQ0030998 Cation Exchange Capacity (non 503 only): n/a
Operator: Mike Williams Owner: Mike Williams Predominant Soil Series FoA
Acres Used: 10.88 Acres Permitted: 10.88 Site #: MW Field #: 1
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
al m7i-ti7ia m77.ndMl uv 7(Yfi_ni cum cwm.
Sample
or Com-
polite
Date
6/27123
2/28/23
2/14/23
IJ24/24
% Solids
1.57
0.76
0.49
1.79
Arsenic
20.90
25.30
43.10
0.00
Cadmium
20.90
25.30
43.10
9.27
Chromium
20.90
25.30
43.10
19.70
Copper
513.00
114.00
496.00
420.00
Lead
29.40
25.30
43.10
10.60
Mercury
1.50
2.32
3.51
1.12
Moiyb-
denum
20.90
25.30
43.10
9.27
Nickel 1
20.90
25.30
43.10
13.20
Selenium
20.90
25.30
43.10
9.27
Zinc
1230.00
2210.00
784.00
3980.00
Total
Phos-
horus
16,200
25,800
21,400
12,000
Annual Heavy Metal Field Loadings
(Calculated
in Ibs/acre):
;a
3 0
0.53
0.23
0.05
0.82
0
Arsenic
1 0.02
0.01
1 0.00
0.00
1
0.0,
Cadmiuml
0.02
0.01
0.00
0.02
0.0:
Chromium
0.02
0.01
0.00
0.03
0.0'
Copper
0.54
0.05
0.05
0.69
1.3,
Lead
0.03
0.01
0.00
0.02
0.0(
Mercury
0.00
0.00
0.00
0.00
0.01
Molyb-
denum
0.02
0.01
0.00
0.02
0.01
Nickel
0.02
0.01
0.00
0.02
0.01
Selenium
0.02
0.01
0.00
0.02
0.0:
Zinc
1.30
1.00
0.08
6.55
8.9:
Total
Phos-
17.16
11.66
2.17
19.76
50.7
"I certify, under penalty of law, that this document was prepared under my direction or supervision In accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibili of fins and imprisonment for knowing violations"
2.
Signature of Land Applier Dat

ANNUAL METALS FIELD LOADING SUMMARY FORM
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Triple S Farms Total Dry Tons Applied (Annual): 8.50
Permit #: W00030996 Cation Exchange Capacity (non 503 only): nla
Operator: Mike Williams Owner: Mike Williams Predominant Soil Series AuB
Acres Used: 6.21 Acres Permitted: 6.21 Site #: MW Field #: 6
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
?JR 7077.10142 Tfl]d_07MO
ST
' •
11
111
Annual Heavy Metal Field Loadings
(Calculated
in lbs/acre):
3 0
0.49
0.88
m
a
W`
H
..
Arsenic
0.01
0.00
1
0.0
Cadmium
0.01
0.02
0.0:
hromiu
0.02
0.03
0.0'
Copper
0.25
0.74
0.91
Lead
0.01
0.02
0.0:
Mercury
0.00
0.00
0.0(
Molyb-
0.01
0.02
0.0:
denum
Nickel
0.01
0.02
0.0:
Selenium
0.01
0.02
0.0:
Zinc
0.95
7.00
7.9,
Total
Phos-
26.53
21.09
47.6
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. i am aware that there are
significant penalties for s mitAing false information, including the possibili of fine and
%imprisonment for knowing violations"
Signature of Land Appl er Date

ANNUAL METALS FIELD LOADING SUMMARY FORM
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Triple S Farms Total Dry Tons Applied (Annual): 10.28
Permit #: W00030998 Cation Exchange Capacity (non 503 only): Na
Operator: Mike Williams Owner: Mike Williams Predominant Soil Series AuB
Acres Used: 10 Acres Permitted: 10 Site #: MW Field #: 9
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg ft, % Solids use Raw Percent #):
MR 2021-291iR 7w&wma
• •
®®
Will",
Annual Heavy Metal !Wield Loadings
(Calculated
in lbslacre):
o
st
y
0
0.49
0.54
_. n
..
Arsenic
0.01
0.00
0.0
Cadmium
0.01
0.01
0.0:
Chromium
0.02
0.02
0.0,
Copper
0.25
0.45
0.7(
Lead
0.01
0.01
0.0:
Mercury
0.00
0.00
00
Molyb-
denum
0.01
0.01
0.0:
Nickel
0.01
0.01
0.0.
Selenium
0.01
0.01
0.0:
Zinc
0.95
4.28
5.2:
Total
Phos-
26.57
12.90
39.4
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
]cant penalties or submitting false information, including the possibility, of fines and imprisonment for knowing violations"
!71
�
Signature of Land Applier Date

ANNUAL METALS FIELD LOADING SUMMARY FORM
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Triple S Farms Total Dry Tons Applied (Annual): 30.80
Permit #: WQ0030998 Cation Exchange Capacity (non 503 only): n/a
Operator: Lonnie Thigpen Owner: Lonnie Thigpen Predominant Sall Series NbB
Acres Used: 21.58 Acres Permitted: 21.58 Site #: LT Field #: 1
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
MR 2021.2915R 3.35d.nnm CWR FWA
Sample
or Com-
posite
Date
12/13/23
12/19/23
1/24/24
% Solids
1.62
2.44
1.79
Arsenic
11.40
20.80
0.00
Cadmium
11.40
4.17
9.27
Chromium
19.80
19.00
19.70
Copper
251.00
135.00
420.00
Lead
11.60
12.50
10.60
Mercury
1.04
7.50
1.12
Molyb-
enum
11.40
10.40
9.27
Nickel
11.40
15.00
13.20
Selenium
11.40
20.80
9.27
Zinc
969.00
571.00
3980.00
Total
Phos-
horus
27,100
28,800
12,000
Annual
Heavy Metal Field Loadings
(Calculated
in lbs/acre):
o
mag:
e
0
0.41
0.85
0.17
&`
..
Arsenic
0.01
0.04
0.00
0.0,
Cadmium
0.01
0.01
0.00
0.0:
Chromium
0.02
0.03
0.01
Q.01
Copper
0.21
0.23
0.14
0.51
Lead
0.01
0.02
0.00
0.0:
Mercury
0.00
0.01
0.00
0.0
Molyb-
0.01
0.02
0.00
0.0:
denum
Nickel
0.01
0.03
0.00
0.0-
Selenium
0.01
0.04
0.00
0.0:
Zinc
0.80
0.97
1.32
3.0!
Total
Phos-
22.35
48.88
3.98
75.2
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
7M7�z:=
ncluding the possibili of fiin s and imprisonment for knowing violations"
1 Signature of Land Applier Dat

ANNUAL NIETALS FIELD LOADING SUMMARY FORM
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name; ^ _ 1'npic S tarnu TotalE)ryT'ons Applied (Annual): 0.93
Permit #: WQ0030998 _ Cation Exchange Capacity (non -5Q3 only): n a
Operator: Mike Williams Owner: Mike Williams Predominant Soil Series G.)A
Acres Used: 1.9 Acrec Permitted: 1.9 Site #: MW Field #: 5
Residual Analysis Data (Heavy Metals and 'Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample
or Cool-
posite
Date
12'I3;23
% Solids
1.62
Arsenic
11.40
Cadmiuni
11.40
Chromium
19.80
('upper
255 1.00
Lead
11.60
Mercury
1.04
Molvb-
denuin
`11.40
Nickel
11.40
Selenium
I L40
Lira
969.00
Total
p1los-
liorus
27,100
Annnal t1+-avv (Metal field l.nadinas Walculated in Ilm/acre):
>
7 Z�
0.49
VI
AI';eni
0.01
0.01
C "Idmiunt
0.01
0.01
hwiniun
0.02
0.02
Copper
0.25
0.25
Lead
0.01
0.01
Mercury
0.00
0.00
Molyti-
r).t)1
o.a t
denurn
Nickel
_
0.01
0.01
Selenium
0.01
0.01
Z,nc
0.95
0.95
Total
I'hos-
26.50
26.50
:hones
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assnrc that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties f+>r submitting; false information, including: the possibi ' y of flnes and imprisonment for knowing violations"
Signature of f.and Applier Date
Author Daryl D Merritt DENR FORM MFLSF (7/2002)

ANNUAL NIETALS FIELD LOADING SUMMARY FORN-1
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Triple S Fanns 'Total Dry-T-ons Applied (Annual): 2.63 _
Permit is WQ0030998 Cation Exchange Capacity (non .503 only): n a
Operator: Mike Williams _Owner: ,Mike Williams Predominant Soil Series NbB
Acres Used: 5.36 Acres Permitted: _ 5 36 Site #: MW Field #: 7
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
NR 2023-�9358
Sample
or Cant-
posits
Date
12113i23
9% Solids
1.62
Arsenic
11,40
CIdniiUnl
11.40
Chromium
19.80
Copper
251.00
Lead
�11.60
Mercury
1.04
Molyb-
denun.
11,40
Nickci
11.40
_
Selenium
11.40
Zinc
969.00
TCunl
I'hos-
phorus
27.100
1
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
.. D
.ram'
Arsenic
0.01
0.l)1
01(1nli 1111
0.01
0.01
C'hroiniuir
0.02
0.02
Copper
0.25
0.25
I -cad
0.01
0.01
Mercury
0.00
0.00
Molyb-
1U 1
0.01
denum
Nickel
0.01
0.01
Selenium
0.01
UI_
Zinc
0.95
0.9.
'tonal
Phos•
I 6.64
26.64
?lu�rus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
s ficant penalties for b►nitting false information, including the possibility of fines and imprisonment for knowing violations"
J I i r r t{
Signature or Land Applier Date
Author Daryl D. Merritt DENR FORM MFLSF (7/'2002)

ANNUAL, METALS FIELD LOADING SUMMARY FORM
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
Triple S Farms 'Dotal Dry Tons Applied (Annual):
WQ0030998 Cation Exchange Capacity (non 503 only):
Mike Williams Owner: Mike Williams Predominant Soil Series
4.72
Acres Permitted: 4,72 Site #: MW Field It
2,30
n/a
GuA
R
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Rays Percent #):
,'U ,pia 'If, I CC
Sample
or Corn-12(l3%?.3
polite
Date
7 solids
1,62
Arsenic
11.40
Cadmium
11.40
i
Chromium
19.80
Copper
25 L00
Lead
11.60
Mercury
1.04
Molyh
I I A0
denum
Nickel
11,40
Seleniuol
I I A0
Zinc
969.00
Total
Phos-
27,100
liorus
Annual Heavv Metal Field Loadinim (Calculated in lbs/acre):
'-1
ram`
o'
n ?
0,41)
r;
r.
o �
Arsenic
0.01
0.01
Cadmium
0.01
0.01
chrrnniun
0.02
v
0.02
Copper
0,24
0.24
Lead
0.01
0.01
Mercury
0.00
0.00
hlolyb-
0.01
0,01
denunl
Nickel
0.01
0.01
Selenium
0.01
0.01
Zinc
0.94
0.94
Tntal
Phos
2 6.37
26.37
horns
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibi 'ry of fines and imprisonment for knowing violations"
Signature of Ladd Applier t}ate
Author Daryl D Merritt DENR FORM Ml- LSF (7/2002)

ANNUAL METALS FIELD LOADING SUNIMARY FORM
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
WQ0030998
Mike Williams
14.46
Triple S Farms Total Dry Tons Applied (Annual): 10.01
Cation Exchange Capacity (non 503 only): n•a
Owner: Mike Williams Predominant Soil Series FoA
Acres Permitted: 14.46 Site #: MW Field #: 2B
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
hk 2023-'93�8
Sample
or Com-
polite
Date
12! 13f21 3
% Solids
LK
Arsenic
11.40
Cadmium
11.40
Chromium
19.80
Copper
251.00
[-eacl
1 1.60
Mercury
1.04
Mulyb-
denun1
11.40
Nickel
11,40
Selenium
I L40
zinc
969.00
'i'atal
Phos-
bolus
2 7' 100
Annual 11-Icavy ;Metal Field Loadings (Calculated in lbs/acre):
C•
> =
o
a
0.69
w
>
Arsenic
0.02
0•02
Cadmium
0.02
0.02
Chromiuir
0.03
0.03
Copper
0.35
0.35
Lead
0.02
0.02
MCVCUPY
0.00
0.00
Molyb-
0.111-1
0.02
clenum
Nickel
0.02
0.02
Selenium
0.02
0.02
Zinc
1.3It
1.34
fatal
Kos-
37.51
Lj
nhorus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with it system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
, jWdficant penalties f f submitting false information, including the possibi 'UDa
and imprisonment for knowing violations"
Sienature of Land .Applicr
Author Daryl D. Merritt DENR FORM MFLSF (712002)

ANNUAL LAND APPLICATION FIELD SUMMARY FORMS

ANNUAL LAND APPLICATION FIELD SUMMARY FORMS LEGEND
All nutrients and metals concentrations listed on the following annual land application field
summary forms are on a pound per acre basis.
The following is a list of symbols and abbreviations used on the field loading rate report:
%TS — Percent Solids
DT/ACRE — Dry Tons Applied per Acre
lb/ac — Pounds per Acre
Metals (lbs/ac
As —
Arsenic
Cd
— Cadmium
Cr —
Chromium
Cu
— Copper
Pb —
Lead
Hg
— Mercury
Mo
— Molybdenum
Ni —
Nickel
Se —
Selenium
Zn —
Zinc
Nutrients lbs/ac)
PAN — Plant Available Nitrogen
P — Phosphorus
K — Potassium
Annual Totals — lbs/ac applied during the calendar year.
Cumulative Totals — lbs/ac applied during the lifetime of field use.

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RESIDUAL ANALYSIS LAB SHEETS

Facility:
Source:
Location:
Contractor:
Type of Analysis:
Report No:
Date Sampled:
Date Reported:
Reporting Period:
Town of Beulaville
Beulaville WWTP
Beulaville, North Carolina
Triple S Farms & Cleaning, Inc
Wastewater Treatment Plant
BL 2023-13234
6/27/2023
8/18/2023
Annual 2023
Parameter
%
PPM
Dry Weight
EPA
Monthly Limits
Solids
1.570
Nitrogen (TKN)
4.750
47,500.000
Phosphorus
1.620
16,200.000
Potassium
0.483
4,830.000
Sulfur
0.000
Calcium
2.150
21,500.000
Magnesium
0.213
2,130.000
Sodium
0.669
6,690.000
Iron
---
Aluminum
---
4,030.000
Manganese
---
Copper
---
513.000
1,500
Zinc
---
1,230.000
2,800
Ammonia Nitrogen
0.292
2,920.000
Nitrate N / Nitrite N
---
15,000.000
Cadmium
---
20.900
85
Chromium
---
20.900
1,200
Nickel
---
20.900
420
Lead
---
29.400
300
Arsenic
---
20.900
75
Mercury
---
1.500
17
Selenium
---
20.900
100
pH
3.900
Calcium Carbonate Eq. (est)
0.000
Organic Nitrogen
4.458
Molybdenum
---
20.900
75
Chloride
---
Boron
Available P2O5
Specific Gravity
8.340

Wastewater Treatment Plant
Beulaville WWTP
Beulaville, North Carolina
Triple S Farms & Cleaning, Inc
Annual 2023
Date Reported: 8/18/2023 Report No: BL 2023-13234
Note All Units in Pounds Per Dry Ton
Macro Nutrients Physical Characteristics
PAN Surf.
59.668
PAN Inj.
62.588
P
32.400
K
9.660
Lime (estimated)
0.000
Secondary Nutrients
Calcium
43.000
Magnesium
4.260
Sodium
13.380
SAR
1.456
Chloride
0.000
Iron
0.000
Alumium
8.060
Manganese
0.000
Boron
0.000
Sulfur
0.000
% Solids
1.57
pH
3.900
Min Rate
0.300
Metals
Arsenic
0.042
Cadmium
0.042
Chromium
0.042
Copper
1.026
Lead
0.059
Mercury
0.003
Molybdenum
0.042
Nickel
0.042
Seleniun
0.042
Zinc
2.460

envirochem
ANALYTICAL $ CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
[e-mail]
Town of Beulaville
Date of Report: Aug 18, 2023
PO Box 130
Customer PO #:
Beulaville NC
28518
Customer ID: 08100015
Attention:
Report #: 2023-13234
Project ID: Sludge
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
23-32951 Site: Sludge
6/27/2023
9:30 AM Solid/Sludge Client
Test
Method
Results
Date Analyzed
Sludge Residuals
Aluminum
EPA 200.7, Rev. 4.4,1994
4030 mg/kg
06/28/2023
Arsenic
EPA 200.7, Rev. 4.4,1994
<20.9 mg/kg
06/28/2023
Cadmium
EPA 200.7, Rev. 4.4, 1994
<20.9 mg/kg
06/28/2023
Calcium
EPA 200.7, Rev. 4.4,1994
21500 mg/kg
06/28/2023
Chromium
EPA 200.7, Rev. 4.4,1994
<20.9 mg/kg
06/28/2023
Copper
EPA 200.7. Rev. 4.4, 1994
513 mg/kg
06/28/2023
Lead
EPA 200.7, Rev, 4.4, 1994
29.4 mg/kg
06/28/2023
Magnesium
EPA 200.7, Rev. 4.4,1994
2130 mg/kg
06/28/2023
Molybdenum
EPA 200.7, Rev. 4.4,1994
<20.9 mg/kg
06/28/2023
Nickel
EPA 200.7, Rev. 4.4,1994
<20.9 mg/kg
06/28/2023
Potassium
EPA 200.7, Rev. 4.4,1994
4830 mg/kg
06/28/2023
Selenium
EPA 200.7, Rev. 4.4, 1994
<20.9 mg/kg
06/28/2023
Sodium
EPA 200.7, Rev. 4.4,1994
6690 mg/kg
06/28/2023
Zinc
EPA 200.7, Rev. 4.4,1994
1230 mg/kg
06/28/2023
Nitrate+Nitrite-Nitrogen
EPA353.2
15000mg/kg
06/28/2023
Total Solids (%)
SM 2540 a
1.57 %
06/30/2023
Ammonia Nitrogen
SM 4500 NH3 C-2011
2920 mg/kg
07/03/2023
Total Kjeldahl Nitrogen (TKN)
SM 4500 Norg &2011
47500 mg/kg
06/28/2023
Total Phosphorus
SM 4500 P (F-H)-2011
16200 mg/kg
07/04/2023
pH
SW 846 Method 9045D
3.90 units
07/21 /2023
Analyzed outside of 15 minute hold time. Estimate: result is outside calibration
range.
Mercury SW-a48 7471 a 1.50 mg/kg 06/29/2023
Comment: Results, except pH, reported on a dry weight basis. pH reported on an as received basis.
Reviewed by:
Report#:: 2023-13234 Page 1 of 1

tnvironmental Chemist, Inc., Wilmington, NC Lab #94
Sample Receipt Checklist
Client: �� L-U—Y y l vl� i T Date:
6602 Windmill Wa
Wilmington, NC 2840t
910.392.022:
Number: _ 2023- V �a' -
P,eceipt of sample:
❑ YES ❑
ECHEP0 Pickup Client Dehvert,, ❑ UPS ❑ =_dux ❑ t lJ
❑
NO
® N/A
/ 1. Were custody seals present on the cooler?
YES
Original temperature
D NO
upon
N/A 2. If custody seals were present, were they intact/unbroken?
receipt o� °C
t Corrected temperature upon receipt . _
How temperature taken: D Temperature Blank ® Against Bottles
IR Gun ID: Thomas Traceable SIN 210886869 IR Gun Correction Factor'C: 0.0
YES
YES
❑ NO
3. If temperature of cooler exceeded 6°C, was Project Mgr./QA notified?
Cat
❑ NO
4. Were proper custody procedures (relinquished/received) followed?
YES
❑ NO
S. Were sample ID's listed on the COC?
YES
❑ NO
6. Were samples ID's listed on sample containers?
YES
❑ NO
7. Were collection date and time listed on the COC?
YES
�l
❑ NO
8. Were tests to be performed listed on the COC?
YES
YES
❑ NO
9. Did samples arrive in proper containers for each test?
0. YES
❑ NO
10. Did samples arrive in good condition for each test?
❑ NO
11. Was adequate sample volume available?'
YES
❑
❑ NO
12. Were samples received within proper holding time for requested tests?
YES
❑
❑ NO
13. Were acid preserved samples received at a pH of <2?
YES
❑ NO
14. Were cyanide samples received at a pH >12?
❑ YES
❑ NO
15. Were sulfide samples received at a pH >9?
❑ YES
❑
❑ NO
16. Were NH3/TKN/Phenol received at a chlorine residual of <0.5 m/L? *"
YES
❑ YES
❑ NO
❑
17. Were Sulfide/Cyanide received at a chlorine residual of <0.5 m/L?
NO
18. Were orthophosphate samples filtered in the field within 15 minutes?
* TOC/Volatiles are pH checked at time of analysis and recorded on the benchsheet
** Bacteria samples are checked for Chlorine at time of analysis and recorded on the benchsheet.
Sample Preservation: (Must be completed for any sample(s) incorrectly preserved or with headspace)
Sample(s) were received incorrect)
by adding (circle one): H2SO4 HNO3 HCI NaOH
eserved and were adjusted accordingly
Time of preservation: If more than one preservative is needed, notate in comments below
Note Notify custome- se-v'ce immediately for incorrectly preserved samples. Oota n a new sample or
notify the state lab if directed to analyzed by the customer. Who was notified, date and time: _
Volatiles Sample(s) were received with headspace
COMMENTS:
DOC. QA.002 Rev 1
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Facility:
Source:
Location:
Contractor:
Type of Analysis:
Report No:
Date Sampled:
Date Reported:
Reporting Period:
Town of Bridgeton
Bridgeton WWTP
Havelock, North Carolina
Triple S Farms and Cleaning, Inc.
Wastewater Treatment Plant
BG-440A
3/20/2023 Type of Stabilization: Lime
4/24/2023
Annual 2023
Parameter
%
PPM
Dry Weight
EPA
Monthly Limits
Solids*
0.490
Nitrogen (TKN)*
5.327
53,270.00
Phosphorus
1.616
16,160.00
Potassium
0.454
4,537.00
Sulfur
Calcium
3.180
31,795.00
Magnesium
0.344
3,438.00
Sodium
1.448
14,476.00
Iron
---
Aluminum
---
3875.00
Manganese
---
Copper
---
463.00
1,500
Zinc
---
2989.00
7,500
Ammonia Nitrogen*
0.030
296.20
Nitrate N / Nitrite N*
---
3.99
Cadmium
---
2.00
39
Chromium
---
20.00
1,200
Nickel
---
17.00
420
Lead
---
18.00
300
Arsenic
---
2.50
41
Mercury
---
0.26
17
Selenium
---
5.00
100
pH
6.900
Calcium Carbonate Eq. (es
t)
0.00
Organic Nitrogen
5.297
52,973.80
Molybdenum
---
7.10
75
Chloride
---
Boron
Available P2O5
Specific Gravity
8.340

Wastewater Treatment Plant
Bridgeton WWTP
Havelock, North Carolina
Triple S Farms and Cleaning, Inc.
Annual 2023
Date Reported: 4/24/2023 Report No: BG-440A
Note All Units in Pounds Per Dry Ton
Macro Nutrients Physical Characteristics
PAN Surf.
32.088
PAN Inj.
32.385
P
32.320
K
9.074
Lime (estimated)
0.000
Secondary Nutrients
Calcium
63.590
Magnesium
6.876
Sodium
28.952
SAR
1.438
Chloride
0.000
Iron
0.000
Alumium
7.750
Manganese
0.000
Boron
0.000
Sulfur
0.000
% Solids
0.49
pH
6.900
Min Rate
0.300
Metals
Arsenic
0.005
Cadmium
0.004
Chromium
0.040
Copper
0.926
Lead
0.036
Mercury
0.001
Molybdenum
0.014
Nickel
0.034
Seleniun
0.010
Zinc
5.978

1
f
Way P aa� H
ANALYTICAL
114 OAKMONT DRIVE
GREENVILLE, NC 27858
TOWN OF BRIDGETON
HYDRO SERVICES & CONSULTING
MR. KEVIN MULLINEAUX
P.O. BOX 317
HAVELOCK, NC 28532
PARAMETERS
PH (not to be used for reporting)
Ahnginum, (dry wt. basis), mg/kg
Arsenic (dry wt. basis), mg/kg
Calcium (dry wt. basis), mg/kg
Cadmium (dry wt. basis), mg/kg
Copper (dry wt. basis), mg/kg
Chromium, T.(dry wt. basis),mg/kg
Lead (dry weight basis), mg/kg
Magnesium (dry wt. basis), mg/kg
14ercury (dry wt. basis), mg/kg
Nickel (dry wt. basis), mg/kg
Potassium (dry wt. basis), mg/kg
Selenium (dry wt. basis), mg/kg
Sodium (dry wt. basis), mg/Icg
Zinc (dry wt. basis), mg/Icg
Sodium Adsorption Ratio (talc)
Total Solids, %
TKN (dry wt.), mg/kg
Ammonia Nitrogen (dry wt.),mg/lig
Phosphorus, T. (dry wt.), mg/kg
Nitrate+Nitrite (dry wt.), mg/kg
Molybdenum (dry wt. basis), ►ng/kg
Sludge
Analysis
Method
Sample
Date Analyst
Code
6.9
03/20/23
BLV
4500HB-11
3875
04/17/23
MTM
EPA200.7
<2.5
04/18/23
DRC
3113B-04
31795
04/18/23
D,1TN1
EPA200.7
2.0
04/17/23
DRC
3113B-04
463
04/18/23
MTM
EPA200.7
20
04/17/23
MTM
EPA200.7
18
04/18/23
DRC
3113B-04
3438
04/18/23
MTM
EPA200.7
0.26
04/14/23
DRC
EPA7471B
17
04/18/23
INTi41
EPA200.7
4537
04/18/23
MT11
EPA200.7
<5.0
04/18/23
DRC
3113B-04
14476
04/18/23
MTNI
EPA200.7
2989
04/18/23
MTM
EPA200.7
20.6
0.49
03/21/23
BLV
2540G-15
c 53270
03/30/23
TRJ
351.2 R2-93
c 296.2
03/31/23
AMC
350.1 R2-93
c 16160
03/30/23
BMD
365.4-74
c 3.99
03/30/23
AMC
353.2 R2-93
7.1
04/18/23
MTM
EPA200.7
Drinking Water ID: 37715
Wastewater ID: 10
PHONE [phone]
FAX [phone]
ID#: 440 A
DATE COLLECTED: 03/20/23
DATE REPORTED : 04/24/23
N
REVIEWED BY: 1, ticJt l
c Uncertified data. DWR does not offer non -aqueous certification for this analytical procedure.

Facility:
Source:
Location:
Contractor:
Type of Analysis:
Report No:
Date Sampled:
Date Reported:
Reporting Period:
Triple S Farms
Little Creek WWTP
Clayton, North Carolina
Triple S Farms
Clayton WWTP
C 1-23-101-001
4/10/2023 Type of Stabilization: Lime
4/20/2023
1st Quarter 2023
Parameter
%
PPM
Dry Weight
EPA
Monthly Limits
Solids*
2.78
Nitrogen (TKN)*
9.250
92,500.000
Phosphorus
3.160
31,600.000
Potassium
0.889
8,890.000
Sulfur
0.000
Calcium
2.010
20,100.000
Magnesium
0.525
5,250.000
Sodium
0.290
2,900.000
Iron
---
Aluminum
---
10,300.000
Manganese
---
Copper
---
138.000
1,500
Zinc
---
664.000
2,800
Ammonia Nitrogen*
1.110
11,100.000
Nitrate N / Nitrite N*
---
179.000
Cadmium
---
3.570
39
Chromium
---
17.200
1,200
Nickel
---
17.400
420
Lead
---
10.700
300
Arsenic
---
17.900
41
Mercury
---
6.390
17
Selenium
---
27.900
100
pH
7.300
Calcium Carbonate Eq. (est)
0.000
Organic Nitrogen
8.140
Molybdenum
---
8.930
75
Chloride
---
Boron
Available P2O5
Specific Gravity
8.340

Clayton WWTP
Little Creek WWTP
Clayton, North Carolina
Triple S Farms
1st Quarter 2023
Date Reported: 4/20/2023 Report No: C 1-23-101-001
Note All Units in Pounds Per Dry Ton
Macro Nutrients Physical Characteristics
PAN Surf.
60.298
PAN Inj.
71.398
P
63.200
K
17.780
Lime (estimated)
0.000
Secondary Nutrients
Calcium
40.200
Magnesium
10.500
Sodium
5.800
SAR
0.783
Chloride
0.000
Iron
0.000
Alumium
20.600
Manganese
0.000
Boron
0.000
Sulfur
0.000
% Solids
2.78
pH
7.300
Min Rate
0.300
Metals
Arsenic
0.036
Cadmium
0.007
Chromium
0.034
Copper
0.276
Lead
0.021
Mercury
0.013
Molybdenum
0.018
Nickel
0.035
Seleniun
0.056
Zinc
1.328

Waypointo
ANALYTICAL
4/20/2023
Town Of Clayton
Salvador Valdiviezo
POB 879
Clayton, NC, 27528
Ref: Analytical Testing
Report Number: 23-101-0010
Project Description: Sludge Disposal
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Dear Salvador Valdiviezo:
Waypoint Analytical Virginia, Inc. received sample(s) on 4/11/2023 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Brandi Watson
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.

(2)
Waypoint.7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
ANALYTICAL www.waypointanalytical.com
Sample Summary Table
Report Number: 23-101-0010
Client Project Description: Sludge Disposal
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
61703
Holding
Tank
#1
Solids
04/10/2023
10:58
04/11/2023
SM-4500-NH3C
WP
MTN
61703
Holding
Tank
#1
Solids
04/10/2023
10:58
04/11/2023
SM-4500-NH3C-TKN
WP
MTN
61703
Holding
Tank
#1
Solids
04/10/2023
10:58
04/11/2023
4500NO3F-2011
WP
MTN
61703
Holding
Tank
#1
Solids
04/10/2023
10:58
04/11/2023
6010D
WP
MTN
61703
Holding
Tank
#1
Solids
04/10/2023
10:58
04/11/2023
SW-7471B
WP
MTN
61703
Holding
Tank
#1
Solids
04/10/2023
10:58
04/11/2023
9045D
WP
MTN
61703
Holding
Tank
#1
Solids
04/10/2023
10:58
04/11/2023
SM-2540G
WP
MTN
WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN

WavDo i nt .
ANALYTICAL
46546
Town Of Clayton
Salvador Valdiviezo
POB 879
Clayton , NC 27528
Report Number : 23-101-0010
Lab No : 61703
Sample ID : Holding Tank #i
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Project Sludge Disposal
Information :
REPORT OFANAL YSIS
Report Date : 04/20/2023
Received : 04/11/2023
Brandi Watson
Matrix: Solids
Sampled: 4/ 10/ 2023 10:58
Test
Results
Units
MQL
DF
Date / Time
Analyzed
By
Analytical
Method
Moisture
97.2
%
0.010
1
04/14/2315:05
JLS
SM-2540G
Total Kjeldahl Nitrogen
92500
mg/Kg - dry
8930
1
04/18/23 14:00
JPJ ;M-4500-NH3C-TKP
Potassium
8890
mg/Kg - dry
357
1
04/15/23 02:56
BKN
6010D
Calcium
20100
mg/Kg - dry
1790
1
04/15/23 02:56
BKN
6010D
Aluminum
10300
mg/Kg - dry
179
1
04/15/23 02:56
BKN
6010D
Copper
138
mg/Kg - dry
17.9
1
04/15/23 02:56
BKN
6010D
Zinc
664
mg/Kg - dry
44.6
1
04/15/23 02:56
BKN
6010D
Nickel
17.4
mg/Kg - dry
8.93
1
04/15/23 02:56
BKN
6010D
Arsenic
<17.9
mg/Kg - dry
17.9
1
04/15/23 02:56
BKN
6010D
Silver
<8.93
mg/Kg - dry
8.93
1
04/15/23 02:56
BKN
6010D
Test
Results
Units
MQL
DF
Date / Time
By
Analytical
Analyzed
Method
pH
7.3
S.U.
1
04/17/2317:03
CNB
9045D
Lead
<10.7
mg/Kg - dry
10.7
1
04/15/23 02:56
BKN
6010D
Magnesium
5250
mg/Kg - dry
179
1
04/15/23 02:56
BKN
6010D
Selenium
27.9
mg/Kg - dry
17.9
1
04/15/23 02:56
BKN
6010D
Qualifiers/ DF Dilution Factor MQL Method Quantitation Limit
Definitions

W���`0 7621 Whitepine Road, Richmond, VA 23237
ypoi Main 804-743-9401 ° Fax [phone]
ANALYTICAL www.waypointanalytical.com
46546
Town Of Clayton Project Sludge Disposal
Salvador Valdiviezo Report Date : 04/20/2023
POB 879 Information : Received : 04/11/2023
Clayton , NC 27528
Brand! Watson
Report Number: 23-101-0010 REPORT OFANAL YSIS
Lab No : 61703
Sample ID : Holding Tank #1
Matrix: Solids
Sampled: 4/10/2023 10:58
Total Solids
2.78
%
0.010
1
04/14/23 15:05
JLS
SM-254OG
Phosphorus
31600
mg/Kg - dry
179
1
04/15/23 02:56
BKN
6010D
Sodium
2900
mg/Kg - dry
893
1
04/15/23 02:56
BKN
6010D
Ammonia Nitrogen
11100
mg/Kg - dry
3570
1
04/19/23 13:45
JPJ
SM-4500-NH3C
Nitrate+Nitrite-N
<179
mg/Kg - dry
179
1
04/18/23 13:27
ZBD
4500NO3F-2011
Cadmium
<3.57
mg/Kg - dry
3.57
1
04/15/23 02:56
BKN
6010D
Chromium
17.2
mg/Kg - dry
8.93
1
04/15/23 02:56
BKN
6010D
Mercury
<6.39
mg/Kg - dry
6.39
1
04/14/23 11:49
FDS
SW-7471B
Molybdenum
<8.93
mg/Kg - dry
8.93
1
04/15/23 02:56
BKN
6010D
Qualifiers/ DF Dilution Factor MQL Method Quantitation Limit
Definitions

Waypo'16 t
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Client: Town Of Clayton CASE NARRATIVE
Project: Sludge Disposal
Lab Report Number: 23-101-0010
Date: 4/20/2023
Solids Total Mercury Analysis - CVAA Method 7471A
Sample 95708
Analyte: Mercury
QC Batch No: 1-676255/1-676023
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.

WayPA�int s
NALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
www.waypointanalytical.com
Shipment Receipt Form
Customer Number: 46546
Customer Name: Town Of Clayton
Report Number: 23-101-0010
Shipping Method
0 Fed Ex 0 US Postal 0 Lab
UPS 0 Client 0 Courier
Other
Thermometer ID:
Shipping container/cooler uncompromised?
Yes
0 No
Number of coolers/boxes received
1
Custody seals intact on shipping container/cooler?
0 Yes
0 No
Not Present
Custody seals intact on sample bottles?
0 Yes
0 No
0 Not Present
Chain of Custody (COC) present?
Yes
0 No
COC agrees with sample label(s)?
0 Yes
0 No
COC properly completed
Yes
0 No
Samples in proper containers?
0 Yes
0 No
Sample containers intact?
Yes
0 No
Sufficient sample volume for indicated test(s)?
0 Yes
0 No
All samples received within holding time?
Yes
0 No
Cooler temperature in compliance?
0 Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
0 Yes
0 No
Water - Sample containers properly preserved
0 Yes
0 No
0 N/A
Water - VOA vials free of headspace
0 Yes
0 No
0 N/A
Trip Blanks received with VOAs
0 Yes
0 No
0 N/A
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
N/A
High concentration container (48 hr) F_ Low concentration EnCore samplers (48 hr)
High concentration pre -weighed (methanol -14 d) F_ Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included? 0 Yes t• No
Comments:
Signature: Brandi Watson Date & Time: 04/11/2023 16:05:42

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Facility:
Source:
Location:
Contractor:
Type of Analysis:
Report No:
Date Sampled:
Date Reported:
Reporting Period:
Triple S Farms
Little Creek WWTP
Clayton, North Carolina
Triple S Farms
Clayton WWTP
C 2-23-256-003
9/12/2023 Type of Stabilization: Lime
9/25/2023
2nd Quarter 2023
Parameter
%
PPM
Dry Weight
EPA
Monthly Limits
Solids*
2.69
Nitrogen (TKN)*
6.700
67,000.000
Phosphorus
3.430
34,300.000
Potassium
0.944
9,440.000
Sulfur
0.000
Calcium
11.900
119,000.000
Magnesium
0.715
7,150.000
Sodium
1.170
11,700.000
Iron
---
Aluminum
---
12,700.000
Manganese
---
Copper
---
156.000
1,500
Zinc
---
800.000
2,800
Ammonia Nitrogen*
1.490
14,900.000
Nitrate N / Nitrite N*
---
185.000
Cadmium
---
3.700
39
Chromium
---
24.800
1,200
Nickel
---
15.700
420
Lead
---
11.100
300
Arsenic
---
18.500
41
Mercury
---
6.190
17
Selenium
---
18.500
100
pH
7.700
Calcium Carbonate Eq. (est)
0.000
Organic Nitrogen
5.210
Molybdenum
---
9.260
75
Chloride
---
Boron
Available P2O5
Specific Gravity
8.340

Clayton WWTP
Little Creek WWTP
Clayton, North Carolina
Triple S Farms
2nd Quarter 2023
Date Reported: 9/25/2023 Report No: C 2-23-256-003
Note All Units in Pounds Per Dry Ton
Macro Nutrients Physical Characteristics
PAN Surf.
46.530
PAN Inj.
61.430
P
68.600
K
18.880
Lime (estimated)
0.000
Secondary Nutrients
Calcium
238.000
Magnesium
14.300
Sodium
23.400
SAR
1.458
Chloride
0.000
Iron
0.000
Alumium
25.400
Manganese
0.000
Boron
0.000
Sulfur
0.000
% Solids
2.69
pH
7.700
Min Rate
0.300
Metals
Arsenic
0.037
Cadmium
0.007
Chromium
0.050
Copper
0.312
Lead
0.022
Mercury
0.012
Molybdenum
0.019
Nickel
0.031
Seleniun
0.037
Zinc
1.600

Waypoint
ANALYTICAL
9/25/2023
Town Of Clayton
Salvador Valdiviezo
POB 879
Clayton, NC, 27528
Ref: Analytical Testing
Report Number: 23-256-0003
Project Description: Sludge Disposal
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Dear Salvador Valdiviezo:
Waypoint Analytical Virginia, Inc. received sample(s) on 9/13/2023 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Brandi Watson
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.

(2)
Waypoint. 7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
ANALYTICAL www.waypointanalytical.com
Sample Summary Table
Report Number: 23-256-0003
Client Project Description: Sludge Disposal
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
63347
Holding
Tank
Solids
09/12/2023
12:00
09/13/2023
63347
Holding
Tank
Solids
09/12/2023
12:00
09/13/2023
63347
Holding
Tank
Solids
09/12/2023
12:00
09/13/2023
63347
Holding
Tank
Solids
09/12/2023
12:00
09/13/2023
63347
Holding
Tank
Solids
09/12/2023
12:00
09/13/2023
63347
Holding
Tank
Solids
09/12/2023
12:00
09/13/2023
63347
Holding
Tank
Solids
09/12/2023
12:00
09/13/2023
63347
Holding
Tank
Solids
09/12/2023
12:00
09/13/2023
SM-4500-NH3C
WP MTN
9045D
WP MTN
4500NO3F-2016
WP MTN
6010D
WP MTN
SW-7471B
WP MTN
SM-4500-NH3C-TKN
WP MTN
SM-2540G
WP MTN
WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN

WavDointo
ANALYTICAL
46546
Town Of Clayton
Salvador Valdiviezo
POB 879
Clayton , NC 27528
Report Number: 23-256-0003
Lab No : 63347
Sample ID : Holding Tank
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Project Sludge Disposal
Information :
REPORT OFANAL YSIS
Report Date : 09/25/2023
Received : 09/13/2023
Brandi Watson
Matrix: Solids
Sampled: 9/ 12/ 2023 12:00
Test
Results
Units
MQL
DF
Date / Time
By
Analytical
Analyzed
Method
Moisture
97.3
%
0.010
1
09/15/2315:27
CAH
SM-254OG
Total Kjeldahl Nitrogen
67000
mg/Kg - dry
9260
1
09/22/23 10:00
JPJ iM-4500-NH3C-TKP
Potassium
9440
mg/Kg - dry
370
1
09/21/23 14:10
6010D
Calcium
119000
mg/Kg - dry
1850
1
09/19/23 23:00
BKN
6010D
Aluminum
12700
mg/Kg - dry
185
1
09/19/23 00:49
BKN
6010D
Copper
156
mg/Kg - dry
18.5
1
09/19/23 00:49
BKN
6010D
Zinc
g00
mg/Kg - dry
46.3
1
09/19/23 00:49
BKN
6010D
Nickel
15.7
mg/Kg - dry
9.26
1
09/19/23 00:49
BKN
6010D
Arsenic
<18.5
mg/Kg - dry
18.5
1
09/19/23 00:49
BKN
6010D
Silver
<9.26
mg/Kg - dry
9.26
1
09/19/23 00:49
BKN
6010D
Test
Results
Units
MQL
DF
Date / Time
By
Analytical
Analyzed
Method
Sodium Absorption Ratio
54.1
mg/Kg - dry
37.0
1
09/19/23 00:49
CALCULATION
pH
7.7
S.U.
1
09/15/2314:49
CNB
9045D
Lead
<11.1
mg/Kg - dry
11.1
1
09/19/23 00:49
BKN
6010D
Magnesium
7150
mg/Kg - dry
185
1
09/19/23 00:49
BKN
6010D
Selenium
<18.5
mg/Kg - dry
18.5
1
09/19/23 00:49
BKN
6010D
Qualifiers/ DF
Dilution Factor
MQL Method Quantitation Limit
Definitions

Wao' nt 7621 Whitepine Road, Richmond, VA 23237
y� Main 804-743-9401 ° Fax [phone]
ANALYTICAL www.waypointanalytical.com
46546
Town Of Clayton Project Sludge Disposal
Salvador Valdiviezo Report Date : 09/25/2023
POB 879 Information : Received : 09/13/2023
Clayton , NC 27528
Report Number : 23-256-0003
REPORT OPANAL YSIS
Brandi Watson
Lab No : 63347
Sample ID : Holding Tank
Matrix: Solids
Sampled: 9/12/2023 12:00
Total Solids
2.69
%
0.010
1
09/15/23 15:27
CAH
SM-254OG
Phosphorus
34300
mg/Kg - dry
185
1
09/19/23 00:49
BKN
6010D
Sodium
11700
mg/Kg - dry
926
1
09/19/23 00:49
BKN
6010D
Ammonia Nitrogen
14900
mg/Kg - dry
3700
1
09/22/23 12:40
JPJ
SM-4500-NH3C
Nitrate+Nitrite-N
<185
mg/Kg - dry
185
1
09/19/23 10:37
CLP
4500NO3F-2016
Cadmium
<3.70
mg/Kg - dry
3.70
1
09/19/23 00:49
BKN
6010D
Chromium
24,8
mg/Kg - dry
9.26
1
09/19/23 00:49
BKN
6010D
Mercury
<6.19
mg/Kg - dry
6.19
1
09/18/23 11:32
MRE
SW-7471B
Molybdenum
<9.26
mg/Kg - dry
9.26
1
09/19/23 00:49
BKN
6010D
Qualifiers/ DF Dilution Factor MQL Method Quantitation Limit
Definitions

Waypoint
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Client: Town Of Clayton CASE NARRATIVE
Project: Sludge Disposal
Lab Report Number: 23-256-0003
Date: 9/25/2023
Metals Analysis Method 6010D
Sample 90486 (Salt)
Analyte: Calcium
QC Batch No: 1-705560/1-704630
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 90486 (Salt)
Analyte: Potassium
QC Batch No: 1-705560/1-704630
The matrix spike, matrix spike duplicate and the post digestion spike were all outside of the quality control
acceptance ranges. Matrix interference is suspected
Sample 90486 (Salt)
Analyte: Sodium
QC Batch No: 1-705246/1-704630
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Sample 90486 (Salt)
Analyte: Sodium
QC Batch No: 1-705560/1-704630
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 90486 (Salt)
Analyte: Sodium
QC Batch No: L705560/L704630
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Sample 63436 (A-6)
Analyte: Aluminum
QC Batch No: 1-705958/1-705683
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 63436 (A-6)
Analyte: Arsenic
QC Batch No: 1-705958/1-705683
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Sample 63436 (A-6)
Analyte: Potassium
QC Batch No: 1-705958/1-705683

Waypo'16 t
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Sample 63436 (A-6)
Analyte: Magnesium
QC Batch No: 1-705958/1-705683
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 63436 (A-6)
Analyte: Molybdenum
QC Batch No: 1-705958/1-705683
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Sample 63436 (A-6)
Analyte: Selenium
QC Batch No: 1-705958/1-705683
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Solids Total Mercury Analysis - CVAA Method 7471A
Sample 89923 (4 Day Composite)
Analyte: Mercury
QC Batch No: 1-705009/1-704730
The matrix spike, matrix spike duplicate and the post digestion spike were all outside of the quality control
acceptance ranges. Matrix interference is suspected

IIE&II-4
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Shipment Receipt Form
Customer Number: 46546
Customer Name: Town Of Clayton
Report Number: 23-256-0003
Shipping Method
0 Fed Ex 0 US Postal 0 Lab
UPS 0 Client 0 Courier
0 Other:
Thermometer ID:
Shipping container/cooler uncompromised?
0 Yes
0 No
Number of coolers/boxes received
F 1
Custody seals intact on shipping container/cooler?
0 Yes
0 No
Not Present
Custody seals intact on sample bottles?
0 Yes
0 No
Not Present
Chain of Custody (COC) present?
* Yes
0 No
COC agrees with sample label(s)?
# Yes
0 No
COC properly completed
Yes
0 No
Samples in proper containers?
# Yes
0 No
Sample containers intact?
# Yes
0 No
Sufficient sample volume for indicated test(s)?
# Yes
0 No
All samples received within holding time?
Yes
0 No
Cooler temperature in compliance?
0 Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
0 Yes
0 No
Water - Sample containers properly preserved
# Yes
0 No
0 N/A
Water - VOA vials free of headspace
0 Yes
0 No
N/A
Trip Blanks received with VOAs
0 Yes
0 No
N/A
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
N/A
High concentration container (48 hr) F_ Low concentration EnCore samplers (48 hr)
High concentration pre -weighed (methanol -14 d) F_ Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included? 0 Yes G No
Comments:
Signature: David Lennon Date & Time: 9/13/2023 08:52:40

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Bob Branch
Subject: FW: [EXTERNAL] RE: Holding Tank 1 Sludge Disposal Sample
From: David Lennon <[e-mail]>
Sent: Tuesday, April 4, 2023 11:21 AM
To: [e-mail]; William Simpson <[e-mail]>
Cc: Bob Branch <[e-mail]>; Brandi Watson <[e-mail]>
Subject: [EXTERNAL) RE: Holding Tank 1 Sludge Disposal Sample
Since around 2020 we send all samples needing validation to our Memphis lab to be tested. This sample was send out on
Thursday to Memphis but did not arrive on Friday as it should so it sat over the weekend until Monday. The address of
the Memphis lab is 2790 Whitten Road Memphis Tn 38133.
>>> William Simpson <[e-mail]> 4/4/2023 9:20 AM >>>
David, can you give me the lab address that our samples need to be sent to. We have always sent them to VA for testing,
if we need to start sending them somewhere else we can. I believe this is the second time in my 2 years this has
happened. I know we grabbed the samples late in the quarter, but this now put us out of compliance for our sludge
sampling on a shipping mistake.
Please return the Cooler and sample bottles and we will take care of the resample ASAP.
Thanks,
William Simpson
From: Bob Branch <[e-mail]>
Sent: Tuesday, April 4, 2023 10:06 AM
To: David Lennon <[e-mail]>; [e-mail]; William Simpson
<[e-mail]>
Cc: Brandi Watson <[e-mail]>
Subject: Re: Holding Tank 1 Sludge Disposal Sample
Be Advised: This email originated from outside of the Town of Clayton's network. Do not click links or open attachments unless
you recognize the sender and know the content is safe.
No. Resample. The results will be invalid.
From: David Lennon <[e-mail]>
Sent: Tuesday, April 4, 2023 9:31:37 AM
To: [e-mail] <[e-mail]>; [e-mail]
<[e-mail]>; [e-mail] <[e-mail]>
Cc: Brandi Watson<[e-mail]>
Subject: Holding Tank 1 Sludge Disposal Sample
Hello,

I was just informed by our Memphis lab whom we sent the sample for Holding Tank 1 Sludge Disposal for testing that
the cooler arrived late from UPS and was therefore out of temperature. Would you like to have us continue with the
testing for this sample or have it re -sampled?
Thanks David Lennon

Facility:
Source:
Location:
Contractor:
Type of Analysis:
Report No:
Date Sampled:
Date Reported:
Reporting Period:
Triple S Farms
Little Creek WWTP
Clayton, North Carolina
Triple S Farms
Clayton WWTP
C 3-23-354-0003
12/19/2023
1/12/2024
3rd Quarter 2023
Type of Stabilization: Lime
Parameter
%
PPM
Dry Weight
EPA
Monthly Limits
Solids*
2.44
Nitrogen (TKN)*
6.290
62,900.000
Phosphorus
2.880
28,800.000
Potassium
0.950
9,500.000
Sulfur
0.000
Calcium
13.600
136,000.000
Magnesium
0.771
7,710.000
Sodium
0.617
6,170.000
Iron
---
Aluminum
---
8,710.000
Manganese
---
Copper
---
135.000
1,500
Zinc
---
571.000
2,800
Ammonia Nitrogen*
0.879
8,790.000
Nitrate N / Nitrite N*
---
208.000
Cadmium
---
4.170
39
Chromium
---
19.000
1,200
Nickel
---
15.000
420
Lead
---
12.500
300
Arsenic
---
20.800
41
Mercury
---
7.500
17
Selenium
---
20.800
100
pH
11.800
Calcium Carbonate Eq. (est)
0.000
Organic Nitrogen
5.411
Molybdenum
---
10.400
75
Chloride
---
Boron
Available P2O5
Specific Gravity
8.340

Clayton WWTP
Little Creek WWTP
Clayton, North Carolina
Triple S Farms
3rd Quarter 2023
Date Reported: 1/12/2024 Report No: C 3-23-354-0003
Note All Units in Pounds Per Dry Ton
Macro Nutrients Physical Characteristics
PAN Surf.
41.672
PAN Inj.
50.462
P
57.600
K
19.000
Lime (estimated)
t 0.000
Secondary Nutrients
Calcium
272.000
Magnesium
15.420
Sodium
12.340
SAR
0.687
Chloride
0.000
Iron
0.000
Alumium
17.420
Manganese
0.000
Boron
0.000
Sulfur
0.000
% Solids
2.44
pH
11.800
Min Rate
0.300
Metals
Arsenic
0.042
Cadmium
0.008
Chromium
0.038
Copper
0.270
Lead
0.025
Mercury
0.015
Molybdenum
0.021
Nickel
0.030
Seleniun
0.042
Zinc
1.142

Waypointo
ANALYTICAL
1 /12/2024
Town Of Clayton
Salvador Valdiviezo
POB 879
Clayton, NC, 27528
Ref: Analytical Testing
Report Number: 23-354-0003
Project Description: Sludge Disposal
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Dear Salvador Valdiviezo:
Waypoint Analytical Virginia, Inc. received sample(s) on 12/20/2023 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Brandi Watson
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.

(2)
Waypoint 7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
ANALYTICAL www.waypointanalocal.com
Sample Summary Table
Report Number: 23-354-0003
Client Project Description: Sludge Disposal
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
64228
Holding Tank
Solids
12/19/2023 09:00
12/20/2023
64228
Holding Tank
Solids
12/19/2023 09:00
12/20/2023
SM-4500-NH3C
WP MTN
64228
Holding Tank
Solids
12/19/2023 09:00
12/20/2023
9045D
WP MTN
64228
Holding Tank
Solids
12/19/2023 09:00
12/20/2023
4500NO3F-2016
WP MTN
64228
Holding Tank
Solids
12/19/2023 09:00
12/20/2023
6010D
WP MTN
64228
Holding Tank
Solids
12/19/2023 09:00
12/20/2023
SW-7471B
WP MTN
64228
Holding Tank
Solids
12/19/2023 09:00
12/20/2023
SM-4500-NH3C-TKN
WP MTN
64228
Holding Tank
Solids
12/19/2023 09:00
12/20/2023
SM-2540G
WP MTN
WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN

•
•
Waypoint,
7621 Whitepine
Road, Richmond,
VA 23237
Main 804-743-9401 ° Fax
804-271-6446
ANALYTICAL
www.waypointanalytical.com
46546
Town Of Clayton
Project
Sludge Disposal
Salvador Valdiviezo
Report Date : 01/12/2024
POB 879
Information :
Received : 12/20/2023
Clayton , NC 27528
�J//zrrvG �.E�t✓i
Brandi Watson
Report Number: 23-354-0003
REPOR TOF A NA L YSIS
Lab No : 64228
Matrix: Solids
Sample ID : Holding Tank
Sampled: 12/19/2023 9:00
Test
Results
Units
MQL
DF
Date / Time
By
Analytical
Analyzed
Method
Moisture
97.6 H
%
0.010
1
12/29/23 17:24
CJR
SM-254OG
Potassium
9500
mg/Kg - dry
417
1
01/02/24 19:11
SML
6010D
Sulfur
10400
mg/Kg - dry
417
1
01/02/24 19:11
TJS
6010D
Calcium 136000
mg/Kg - dry
2080
1
01/02/24 19:11
TJS
6010D
Aluminum
8710
mg/Kg - dry
206
1
01/02/24 19:11
TJS
6010D
Manganese
135
mg/Kg - dry
20.8
1
01/02/24 19:11
TJS
6010D
Copper
135
mg/Kg - dry
20.8
1
01/02/24 19:11
TJS
6010D
Nickel
15.0
mg/Kg - dry
10.4
1
01/02/24 19:11
TJS
6010D
Lead
<12.5
mg/Kg - dry
12.5
1
01/02/24 19:11
TJS
6010D
Arsenic
<20.8
mg/Kg - dry
20.8
1
01/02/24 19:11
TJS
6010D
Silver
<10.4
mg/Kg - dry
10.4
1
01/02/24 19:11
TJS
6010D
Test
Results
Units
MQL
DF
Date / Time
By
Analytical
Analyzed
Method
Sodium Absorption Ratio
<41.7
mg/Kg - dry
41.7
1
01/02/24 19:11
CALCULATION
pH
11.8
S.U.
1
12/28/2316:45
CNB
9045D
Total Solids
2.44 H
%
0.010
1
12/29/23 17:24
CIR
SM-2540G
Selenium
<20.8
mg/Kg - dry
20.8
1
01/02/24 19:11
TJS
6010D
Sodium
6170
mg/Kg - dry
1040
1
01/02/24 19:11
TJS
6010D
Qualifiers/ DF Dilution Factor
H Beyond holding time
Definitions MQL Method Quantitation Limit

•
Waypoin't
7621 Whitepine
Road, Richmond,
VA 23237
Main 804-743.9401 ° Fax
804-271-6446
ANALYTICAL
www.waypointanalytical.com
46546
Town Of Clayton
Project
Sludge Disposal
Salvador Valdiviezo
Report Date : 01/12/2024
POB 879
Information :
Received : 12/20/2023
Clayton , NC 27528
�ntYYJ�L Ei,F�t;y
Brandi Watson
Report Number: 23-354-0003
REPORT OFANALYSIS
Lab No : 64228
Matrix: Solids
Sample ID : Holding Tank
Sampled: 12/19/2023 9:00
Test
Results
Units
MQL
DF
Date / Time
By Analytical
Analyzed
Method
Total Kjeldahl Nitrogen
62900
mg/Kg - dry
10400
1
01/08/24 09:28
JPJ ;M-4500-NH3C-TKP
Phosphorus
28800
mg/Kg - dry
208
1
01/02/24 19:11
TJS 6010D
Magnesium
7710
mg/Kg - dry
208
1
01/02/24 19:11
TJS 6010D
Iron
8080
mg/Kg - dry
417
1
01/02/24 19:11
TJS 6010D
Zinc
571
mg/Kg - dry
52.1
1
01/02/24 19:11
TJS 6010D
Ammonia Nitrogen
8790
mg/Kg - dry
4170
1
01/08/24 09:27
JPJ SM-4500-NH3C
Nitrate+Nitrite-N
<208
mg/Kg - dry
208
1
12/29/23 15:41
CLP 4500NO317-2016
Cadmium
<4.17
mg/Kg - dry
4.17
1
01/02/24 19:11
TJS 6010D
Chromium
19.0
mg/Kg - dry
10.4
1
01/02/24 19:11
TJS 6010D
Mercury
<7.50
mg/Kg - dry
7.50
1
12/28/23 11:32
FDS SW-7471B
Molybdenum
<10.4
mg/Kg - dry
10.4
1
01/02/24 19:11
TJS 6010D
Qualifiers/ DF Dilution Factor H Beyond holding time
Definitions

Waypai nto
ANALYTICAL
Client: Town Of Clayton
Project: Sludge Disposal
Lab Report Number: 23-354-0003
Date: 1 /11 /2024
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
CASE NARRATIVE
Metals Analysis Method 6010D
Sample 83189 (South)
Analyte: Potassium
QC Batch No: 1-725735/1-725116
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Sample 83189 (South)
Analyte: Potassium
QC Batch No: 1-725891/1-725116
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 83189 (South)
Analyte: Sodium
QC Batch No: 1-725735/1-725116
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 83189 (South)
Analyte: Sulfur
QC Batch No: 1-725735/1-725116
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Solids Total Mercury Analysis - CVAA Method 7471A
Sample 64228 (Holding Tank)
Analyte: Mercury
QC Batch No: 1-725028/1-724733
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.

(2)WayPnt 7621 ain 80 -7 Road, Richmond, 27 -6446
Main 804-743-9401 0Fax [phone]
ANALYTICAL www.waypointanalytical.com
Shipment Receipt Form
Customer Number: 46546
Customer Name: Town Of Clayton
Report Number: 23-354-0003
Shipping Method
0 Fed Ex 0 US Postal 0 Lab 0 Other:
0 UPS 0 Client 0 Courier Thermometer ID:
F
Shipping container/cooler uncompromised?
# Yes
0 No
Number of coolers/boxes received
F 1
Custody seals intact on shipping container/cooler?
0 Yes
0 No
Q Not Present
Custody seals intact on sample bottles?
0 Yes
0 No
0 Not Present
Chain of Custody (COC) present?
# Yes
0 No
COC agrees with sample label(s)?
0 Yes
0 No
COC properly completed
0 Yes
0 No
Samples in proper containers?
0 Yes
0 No
Sample containers intact?
0 Yes
0 No
Sufficient sample volume for indicated test(s)?
0 Yes
0 No
All samples received within holding time?
0 Yes
0 No
Cooler temperature in compliance?
# Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
0 Yes
0 No
Water - Sample containers properly preserved
0 Yes
0 No
# N/A
Water - VOA vials free of headspace
0 Yes
0 No
# N/A
Trip Blanks received with VOAs
P Yes
0 No
# N/A
Soil VOA method 5035 — compliance criteria met
Yes
No
0 N/A
High concentration container (48 hr) Low concentration EnCore samplers (48 hr)
High concentration pre -weighed (methanol -14 d) Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included?
Yes
• No
Comments:
Signature: Oavid Lennon Date & Time: 12/20/2023 12:59.26

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Facility:
Source:
Location:
Contractor:
Type of Analysis:
Report No:
Date Sampled:
Date Reported:
Reporting Period:
Triple S Farms
Little Creek WWTP
Clayton, North Carolina
Triple S Farms
Clayton WWTP
C 4-23-361-0009 _
12/22/2023 Type of Stabilization: Lime
1/15/2024
4th Quarter 2023
Parameter
%
PPM
Dry Weight
EPA
Monthly Limits
Solids*
2.57
Nitrogen (TKN)*
5.620
56,200.000
Phosphorus
2.620
26,200.000
Potassium
0.827
8,270.000
Sulfur
0.000
Calcium
12.700
127,000.000
Magnesium
0.704
7,040.000
Sodium
0.535
5,350.000
Iron
---
Aluminum
---
8,150.000
Manganese
---
Copper
---
127.000
1,500
Zinc
---
546.000
2,800
Ammonia Nitrogen*
2.070
20,700.000
Nitrate N / Nitrite N*
---
2,120.000
Cadmium
---
3.750
39
Chromium
---
16.600
1,200
Nickel
---
15.100
420
Lead
---
11.500
300
Arsenic
---
19.200
41
Mercury
---
6.620
17
Selenium
---
19.200
100
pH
11.600
Calcium Carbonate Eq. (est)
0.000
Organic Nitrogen
3.550
Molybdenum
---
9.620
75
Chloride
---
Boron
Available P2O5
Specific Gravity
8.340

Clayton WWTP
Little Creek WWTP
Clayton, North Carolina
Triple S Farms
4th Quarter 2023
Date Reported: 1/15/2024 Report No: C 4-23-361-0009
Note All Units in Pounds Per Dry Ton
Macro Nutrients Physical Characteristics
PAN Surf.
46.240
PAN Inj.
66.940
P
52.400
K
16.540
Lime (estimated)
0.000
Secondary Nutrients
Calcium
254.000
Magnesium
14.080
Sodium
10.700
SAR
0.633
Chloride
0.000
Iron
0.000
Alumium
16.300
Manganese
0.000
Boron
0.000
Sulfur
0.000
% Solids
2.57
pH
11.600
Min Rate
0.300
Metals
Arsenic
0.038
Cadmium
0.008
Chromium
0.033
Copper
0.254
Lead
0.023
Mercury
0.013
Molybdenum
0.019
Nickel
0.030
Seleniun
0.038
Zinc
1.092

Waypointo
ANALYTICAL
1 /15/2024
Town Of Clayton
Salvador Valdiviezo
POB 879
Clayton, NC, 27528
Ref: Analytical Testing
Report Number: 23-361-0009
Project Description: Sludge Disposal
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-94010Fax [phone]
www.waypointanalytical.com
Dear Salvador Valdiviezo:
Waypoint Analytical Virginia, Inc. received sample(s) on 12/27/2023 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Brandi Watson
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.

(2)
Waypoint. 7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
ANALYTICAL www.waypointanalytical.com
Sample Summary Table
Report Number: 23-361-0009
Client Project Description: Sludge Disposal
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
64312
Holding
Tank
Solids
12/26/2023
11:00
12/27/2023
64312
Holding
Tank
Solids
12/26/2023
11:00
12/27/2023
64312
Holding
Tank
Solids
12/26/2023
11:00
12/27/2023
64312
Holding
Tank
Solids
12/26/2023
11:00
12/27/2023
64312
Holding
Tank
Solids
12/26/2023
11:00
12/27/2023
64312
Holding
Tank
Solids
12/26/2023
11:00
12/27/2023
64312
Holding
Tank
Solids
12/26/2023
11:00
12/27/2023
64312
Holding
Tank
Solids
12/26/2023
11:00
12/27/2023
SM-4500-NH3C
WP MTN
9045D
WP MTN
4500NO3F-2016
WP MTN
6010D
WP MTN
SW-7471B
WP MTN
SM-4500-NH3C-TKN
WP MTN
SM-2540G
WP MTN
WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN

0
Waypoint,
7621 Whitepine Road, Richmond, VA 23237
Main 804-743.9401 ° Fax [phone]
ANALYTICAL
www.waypointanalytical.com
46546
Town Of Clayton
Project
Sludge Disposal
Salvador Valdiviezo
Report Date : 01/15/2024
POB 879
Information :
Received : 12/27/2023
Clayton , NC 27528
�/�L lL�ity
Brandi Watson
Report Number: 23-361-0009
REPORTOFANALYSIS
Lab No : 64312
Matrix:
Solids
Sample ID : Holding Tank
Sampled: 12/26/2023 11:00
Test
Results
Units
MOL
DF
Date / Time
By
Analytical
Analyzed
Method
Moisture
97.4
%
0.010
1
12/29/2317:24
CJR
SM-254OG
Potassium
8270
mg/Kg - dry
385
1
01/02/24 23:02
TJS
6010D
Sulfur
9380
mg/Kg - dry
385
1
01/02/24 23:02
TJS
6010D
Calcium 127000
mg/Kg - dry
1920
1
01/02/24 23:02
TJS
6010D
Aluminum
8150
mg/Kg - dry
192
1
01/02/24 23:02
TJS
6010D
Manganese
123
mg/Kg - dry
19.2
1
01/02/24 23:02
TJS
6010D
Copper
127
mg/Kg - dry
19.2
1
01/02/24 23:02
TJS
6010D
Nickel
15.1
mg/Kg - dry
9.62
1
01/02/24 23:02
TJS
6010D
Lead
<11.5
mg/Kg - dry
11.5
1
01/02/24 23:02
TJS
6010D
Arsenic
<19.2
mg/Kg - dry
19.2
1
01/02/24 23:02
TJS
6010D
Silver
<9.62
mg/Kg - dry
9.62
1
01/02/24 23:02
TJS
6010D
Test
Results
Units
MQL
DF
Date / Time
By
Analytical
Analyzed
Method
Sodium Absorption Ratio
<38.5
mg/Kg - dry
38.5
1
01/02/24 23:02
CALCULATION
pH
11.6
S.U.
1
12/29/2315:30
CNB
9045D
Total Solids
2.57
%
0.010
1
12/29/23 17:24
CJR
SM-2540G
Selenium
<19.2
mg/Kg - dry
19.2
1
01/02/24 23:02
TJS
6010D
Sodium
5350
mg/Kg - dry
962
1
01/02/24 23:02
TJS
6010D
Qualifiers/ DF Dilution Factor
MQL Method
Quantitation Limit
Definitions

WavDointo
ANALYTICAL
46546
Town Of Clayton
Salvador Valdiviezo
POB 879
Clayton , NC 27528
Report Number:23-361-0009
Lab No : 64312
Sample ID : Holding Tank
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Project Sludge Disposal
Information :
REPORT OFANAL YSIS
Report Date : 01/15/2024
Received : 12/27/2023
Brandi Watson
Matrix: Solids
Sampled: 12/ 26/ 2023 11:00
Test
Results
Units
MQL
DF
Date / Time
Analyzed
By
Analytical
Method
Total Kjeldahl Nitrogen
S6200
mg/Kg - dry
9620
1
01/11/24 06:47
JPJ ;M-4500-NH3C-TKP
Phosphorus
26200
mg/Kg - dry
192
1
01/02/24 23:02
TJS
6010D
Magnesium
7040
mg/Kg - dry
192
1
01/02/24 23:02
TJS
6010D
Iron
7620
mg/Kg - dry
385
1
01/02/24 23:02
TJS
6010D
Zinc
S46
mg/Kg - dry
48.1
1
01/02/24 23:02
TJS
6010D
Ammonia Nitrogen
20700
mg/Kg - dry
3850
1
01/11/24 06:45
JPJ
SM-4500-NH3C
Nitrate+Nitrite-N
2120
mg/Kg - dry
192
1
01/04/24 14:52
CLP
4500NO3F-2016
Cadmium
<3.85
mg/Kg - dry
3.85
1
01/02/24 23:02
TJS
6010D
Chromium
16.6
mg/Kg - dry
9.62
1
01/02/24 23:02
BKN
6010D
Mercury
<6.62
mg/Kg - dry
6.62
1
12/29/23 12:06
MRE
SW-7471B
Molybdenum
<9.62
mg/Kg - dry
9.62
1
01/02/24 23:02
TJS
6010D
Qualifiers/ DF Dilution Factor MQL Method Quantitation Limit
Definitions

WaypointoYTI ANAL AL C
Client: Town Of Clayton
Project: Sludge Disposal
Lab Report Number: 23-361-0009
Date: 1 /12/2024
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
CASE NARRATIVE
Nitrate + Nitrite Nitrogen Method 4500NO3F-2016
Analyte: Nitrate+Nitrite N
QC Batch No: L726132
Target analyte(s) was identified in the method blank associated with this project, below the Method Quantitation
Limit. Per laboratory protocol any associated affected sample result is flagged "B" to indicate that it was detected
in the method blank.

0
Waypoint.
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Shipment Receipt Form
Customer Number: 46546
Customer Name: Town Of Clayton
Report Number: 23-361-0009
Shipping Method
0 Fed Ex 0 US Postal 0 Lab
0 UPS 0 Client 0 Courier
Other :
Thermometer ID:
f
Shipping container/cooler uncompromised?
0 Yes
0 No
Number of coolers/boxes received
F 1
Custody seals intact on shipping container/cooler?
0 Yes
0 No
# Not Present
Custody seals intact on sample bottles?
0 Yes
0 No
# Not Present
Chain of Custody (COC) present?
0 Yes
0 No
COC agrees with sample label(s)?
0 Yes
0 No
COC properly completed
Yes
0 No
Samples in proper containers?
Yes
0 No
Sample containers intact?
Yes
0 No
Sufficient sample volume for indicated test(s)?
0 Yes
0 No
All samples received within holding time?
# Yes
0 No
Cooler temperature in compliance?
# Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
Yes
0 No
Water - Sample containers properly preserved
Yes
0 No
# N/A
Water - VOA vials free of headspace
Yes
0 No
# N/A
Trip Blanks received with VOAs
Yes
0 No
# N/A
Soil VOA method 5035 — compliance criteria met
Yes
0 No
0 N/A
High concentration container (48 hr) Low concentration EnCore samplers (48 hr)
High concentration pre -weighed (methanol -14 d) Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included?
Yes
# No
Comments:
Signature: jDavid Lennon Date & Time: 12/27/2023 12:31:44

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Facility:
Source:
Location:
Contractor:
Type of Analysis:
Report No:
Date Sampled:
Date Reported:
Reporting Period:
Town of Kenansville
Kenansville WWTP
Kenansville, North Carolina
Triple S Farms & Cleaning, Inc
Wastewater Treatment Plant
KV 2023-18528
8/16/2023
10/3/2023
Annual 2023
Parameter
%
PPM
Dry Weight
EPA
Monthly Limits
Solids*
1.300
Nitrogen (TKN)
2.390
23,900.000
Phosphorus
0.552
5,520.000
Potassium
0.325
3,250.000
Sulfur
0.000
Calcium
1.490
14,900.000
Magnesium
0.171
1,710.000
Sodium
0.869
8,690.000
Iron
---
Aluminum
---
4,000.000
Manganese
---
Copper
---
511.000
1,500
Zinc
---
762.000
2,800
Ammonia Nitrogen
0.291
2,910.000
Nitrate N / Nitrite N
---
18.500
Cadmium
---
32.400
85
Chromium
---
32.400
1,200
Nickel
---
32.400
420
Lead
---
32.400
300
Arsenic
---
32.400
75
Mercury
---
1:320
17
Selenium
---
32.400
100
pH
7.420
Calcium Carbonate Eq. (est)
0.000
Organic Nitrogen
2.099
Molybdenum
---
32.400
75
Chloride
---
Boron
Available P205
Specific Gravity
8.340

Wastewater Treatment Plant
Kenansville WWTP
Kenansville, North Carolina
Triple S Farms & Cleaning, Inc
Annual 2023
Date Reported: 10/3/2023 Report No: KV 2023-18528
Note All Units in Pounds Per Dry Ton
Macro Nutrients Physical Characteristics
PAN Surf.
15.541
PAN Inj.
18.451
P
11.040
K
6.500
Lime (estimated)
0.000
Secondary Nutrients
Calcium
29.800
Magnesium
3.420
Sodium
17.380
SAR
2.045
Chloride
0.000
Iron
0.000
Alumium
8.000
Manganese
0.000
Boron
0.000
Sulfur
0.000
% Solids
1.30
pH
7.420
Min Rate
0.300
Metals
Arsenic
0.065
Cadmium
0.065
Chromium
0.065
Copper
1.022
Lead
0.065
Mercury
0.003
Molybdenum
0.065
Nickel
0.065
Seleniun
0.065
Zinc
1.524

Environmental Chemists, Inc.
envirochem 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910,392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilrnington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS info�ayenvironmentalchemistscom
Town of Kenansville Date of Report: Oct 03, 2023
PO Box 370 Customer PO #:
Kenansville NC 28349 Customer ID: 09020018
Attention: Report #: 2023-18528
Project ID: Sludge
Lab ID Sample ID: Collect Date/Tlme Matrix Sampled by
23-45434 Site: sludge 8/16/2023 10:30 AM Solid/Sludge Client
Test Method Results Date Analyzed
Chlordane (TCLP)
Sw.8406081 B
<0.02 mg/L
08/28/2023
Endrin (TCLP)
$W-e46 80818
<0.0005 mg/L
08/28/2023
Heptachlor (TCLP)
Sw-8460081 B
<0.0005 mg/L
08/28/2023
Heptachlor epoxide (TCLP)
SW-846 80818
<0.0005 mg/L
08/28/2023
Lindane (TCLP)
SW-8488081 B
<0.0005mg/L
08/28/2023
Methoxychlor (TCLP)
SW-e46 80818
<0.0005 mg/L
08/28/2023
Toxaphene (TCLP)
SW-848 8081 B
<0.05 mg/L
08/28/2023
2,4,5-TP (TCLP)
SW-846 8161 A
<0.003 mg/L
08/24/2023
2,4-D (TCLP)
SW-846 6151 A
<0.003 mg/L
08/24/2023
1,4-Dlchlorobenzene (TCLP)
SW-846 8270 E
<0.050 mg/L
08/28/2023
2,4,5-Trichlorophenol (TCLP)
SW-840 6270 E
<0.050 mg/L
08/28/2023
2,4,6-Trichlorophenol (TCLP)
SW-846 8270 E
<0.050 mg/L
08/28/2023
2,4-Dinitrotoluene (TCLP)
SW-846 6270 E
<0.050 mg/L
08/28/2023
Cresol (TCLP)
SW-846 8270 E
<0.050 mg/L
08/28/2023
Hexachioro-1,3-butadiene (TCLP)
SW-846 8270 E
<0.050 mg/L
08/28/2023
Hexachlorobenzene (TCLP)
SW 846 8270 E
<0.050 mg/L
08/28/2023
Hexachloroethane (TCLP)
SW-848 8270 E
<0.050 mg/L
08/28/2023
m + p-Cresol (TCLP)
SW 846 8270 E
<0.050 mg/L
08/28/2023
Nitrobenzene (TCLP)
SW 846 0270 E
<0.050 mg/L
08/28/2023
o-Cresol (TCLP)
SW-846 8270 E
<0.050 mg/L
08/28/2023
Pentachlorophenol (TCLP)
SW-646 0270 E
<0.250 mg/L
08/28/2023
Pyridine (TCLP)
SW-846 8270 E
<0.050 mg/L
08/28/2023
1,1-Dichloroethylene (TCLP)
SW-846Method 8260D
<0.01 mg/L
09/07/2023
1,2-Dichloroethane (TCLP)
Sw-e46Method 8260D
<0.01 mg/L
09/07/2023
Benzene (TCLP)
SW-848 Method 8260D
<0.01 mg/L
09/07/2023
Carbon Tetrachloride (TCLP)
SW-e40 Method 62600
<0.01 mg/L
09/07/2023
Report #:: 2023.10528 Page 1 of 3

envirochem
ANALYTICAL & CONSULTING CHEMISTS
Town of Kenansviile
PO Box 370
Kenansville NC 28349
Attention:
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392,4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
infoq%environmentalchemismcom
Date of Report: Oct 03, 2023
Customer PO #:
Customer ID: 09020018
Report #: 2023-18528
Project ID: Sludge
Chlorobenzene (TCLP)
SW-846 Method 82600
<0.01 mg/L
09/07/2023
Chloroform (TCLP)
SW-846 Method 8280D
<0.01 mg/L
09/07/2023
Methyl ethyl ketone (TCLP)
SW-846 Method 8260D
0.05 mg/L
09/07/2023
Tetrachloroethylene (TCLP)
SW-846 Method 8260D
<0.01 mg/L
09/07/2023
Trichloroethylene (TCLP)
SW-846 Method 8260D
<0,01 mglL
09/07/2023
Vinyl Chloride (TCLP)
SW-846 Method 8280D
<0.01 mg/L
09/07/2023
RCI
Cyanide SM 4500 CN 0-2016
1.55 mg/kg
09/06/2023
Sulfide SM 4500 S D-2011
0.12 mg/kg
09/11/2023
Ignitability SW 846 method 1010
>158 °F
09/12/2023
pH SW 846 Method 9045D
7.42 units
08/23/2023
Result estimated. Analyzed out of 15 minutes hold time.
Sludge Residuals
Aluminum
EPA 200.7. Rev. 4.4. '1994
4000mg/kg
09/01/2023
Arsenic
EPA 200.7, Rev. 4.4.1904
<32.4 mg/kg
09/01/2023
Cadmium
EPA 200.7, Rev. 4.4, 1994
<32.4 mg/kg
09/01/2023
Calcium
EPA 200.7, Rev. 4.4.1004
14900 mg/kg
09/01/2023
Chromium
EPA 200.7. Rev. 4.4.1094
<32.4 mg/kg
09/01/2023
Copper
EPA 200.7, Rev. 4.4, 1094
511 mg/kg
09/01/2023
Lead
EPA 200.7, Rev. 4.4,1994
<32.4 mg/kg
09/01/2023
Magnesium
EPA 200.7, Rev. 4.4,1994
1710 mg/kg
09/01/2023
Molybdenum
EPA 200.7, Rev. 4.4,1994
<32.4 mg/kg
09/01/2023
Nickel
EPA 200.7, Rev. 4.4.1994
<32.4 mg/kg
09/01/2023
Potassium
EPA 200.7. Rev. 4.4.1904
3250 mg/kg
09/12/2023
Selenium
EPA 200.7, Rev. 4.4,1994
<32.4 mg/kg
09/01/2023
Sodium
EPA 200.7, Rev, 4.4,1994
8690 mg/kg
09/01/2023
Zinc
EPA 200,7, Rev. 4.4,1994
762 mg/kg
09/01/2023
Nitrate+Nitrite-Nitrogen
EPA 353.2
18.5 mg/kg
08/24/2023
Total Solids N
SM 2540 a
1.30 %
08/16/2023
Ammonia Nitrogen
SM 4500 NH3 C-2011
2910 mg/kg
08/21/2023
Report #:: 2023.18628 Page 2 of 3

:envirochem
ANALYTICAL & CONSULTING CHEMISTS
Town of Kenansville
PO Box 370
Kenansviile NC 28349
Attention:
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 a 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28W • 910.347.5843 Lab/Fax
[e-mail]
Date of Report: Oct 03, 2023
Customer PO M
Customer ID: 09020018
Report M 2023-18528
Project ID: Sludge
Total Kjeldahl Nitrogen (TKN) SM 4500 Norg B-2011 23900 mg/kg 08/22/2023
Total Phosphorus SM 4500 P (F-H)-2011 5520 mg/kg 08/30/2023
Mercury SW-Ue 74718 <1.32 mg/kg 08/22/2023
TCLP Metals
Arsenic (TCLP)
EPA 200.7, Rev. 4.4, 1994
<1.0 mg/L
09/02/2023
Barium (TCLP)
EPA 200.7, Rev. 4.4,1994
<1.0 mg/L
09/02/2023
Cadmium (TCLP)
EPA 200.7, Rev. 4.4.1094
<1.0 mg/L
09/02/2023
Chromium (TCLP)
EPA 200.7. Rev. 4.4. 1094
<1.0 mg/L
09/02/2023
Lead (TCLP)
EPA 200.7, Rev. 4.4, 1994
0.0 mg/L
09/02/2023
Selenium (TCLP)
EPA 200.7, Rev. 4.4,1994
<1.0 mg/L
09/02/2023
Silver (TCLP)
EPA 200.7. Rev. 4.4,1994
0.0 mg/L
09/02/2023
Mercury (TCLP)
EPA 245.1
<0.0002 mg/L
09/13/2023
Comment. Sludge residuals reported on a dry weight basis,
Reviewed by: ^_
Report #:: 2023.18628 Page 3 of 3

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Facility:
Source:
Location:
Contractor:
Type of Analysis:
Report No:
Date Sampled:
Date Reported:
Reporting Period:
Town of Maysville
Maysville WWTP
Maysville, North Carolina
Triple S Farms & Cleaning, Inc
Wastewater Treatment Plant
MV 2023-03127
2/14/2023
3/3/2023
Annual 2023
Parameter
%
PPM
Dry Weight
EPA
Monthly Limits
Solids
0.490
Nitrogen (TKN)
10.200
102,000.000
Phosphorus
2.140
21,400.000
Potassium
0.704
7,040.000
Sulfur
0.000
Calcium
5.430
54,300.000
Magnesium
0.347
3,470.000
Sodium
0.663
6,630.000
Iron
---
Aluminum
---
5,330.000
Manganese
---
Copper
---
496.000
1,500
Zinc
---
784.000
2,800
Ammonia Nitrogen
0.724
7,240.000
Nitrate N / Nitrite N
---
204.000
Cadmium
---
43.100
85
Chromium
---
43.100
1,200
Nickel
---
43.100
420
Lead
---
43.100
300
Arsenic
---
43.100
75
Mercury
---
3.510
17
Selenium
---
43.100
100
pH
Calcium Carbonate Eq. (est)
0.000
Organic Nitrogen
9.476
Molybdenum
---
43.100
75
Chloride
---
Boron
Available P2O5
Specific Gravity
8.340

Wastewater Treatment Plant
Maysville WWTP
Maysville, North Carolina
Triple S Farms & Cleaning, Inc
Annual 2023
Date Reported: 3/3/2023 Report No: MV 2023-03127
Note All Units in Pounds Per Dry Ton
Macro Nutrients Physical Characteristics
PAN Surf.
64.504
PAN Inj.
71.744
P
42.800
K
14.080
Lime (estimated)
0.000
Secondary Nutrients
Calcium
108.600
Magnesium
6.940
Sodium
13.260
SAR
0.521
Chloride
0.000
Iron
0.000
Alumium
10.660
Manganese
0.000
Boron
0.000
Sulfur
0.000
% Solids
0.49
pH
0.000
Min Rate
0.300
Metals
Arsenic
0.086
Cadmium
0.086
Chromium
0.086
Copper
0.992
Lead
0.086
Mercury
0.007
Molybdenum
0.086
Nickel
0.086
Seleniun
0.086
Zinc
1.568

r7Environmental Chemists, Inc.
envirochem 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab - 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
5M 255-A Wilmington Highway, Jacksonville, NC 28540 4 91.0.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS [e-mail]
Town of Maysville Date of Report: Mar 03 2023
Post Office Box 265 Customer PO #:
Maysville NC 28555 Report #: 2023-03127
Attention: Customer ID: 17020023
Project ID: Sludge
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
23-07736 Site: Sludge 2/14/2023 Solid/Sludge Client
Test
Method
Results
Date Analyzed
Sludge Residuals
Aluminum
EPA 200.7, Rev. 4.4, 1994
5330 mg/kg
02/20/2023
Calcium
EPA 200.7, Rev. 4 4, 1994
54300 mg/kg
02/20/2023
Copper
EPA 2D0.7, Rev 4.4, 1994
496 mg/kg
02/20/2023
Potassium
EPA 200.7, Rev 4 4, 1994
7040 mg/kg
02/20/2023
Sodium
EPA 200.7. Rev 4 4, 1994
6630 mg/kg
02/20/2023
Zinc
EPA 200.7, Rev 4 4, 1994
784 mg/kg
02/20/2023
Nitrate+Nitrite-Nitrogen
EPA3532
204 mg/kg
02/21/2023
Total Solids (%)
SM 2540 s
0.49 %
02/16/2023
Ammonia Nitrogen
SM 4500 NH3 C-2011
7240 mg/kg
02/17/2023
Total Kjeldahl Nitrogen (TKN)
SM 4500 Norg B-2011
102000 mg/kg
02/18/2023
Total Phosphorus
SM 4500 P (F-H)-2011
21400 mg/kg
02/23/2023
Lab ID Sample ID:
Collect Date/Time
Matrix Sampled by
23-07736A Site: Sludge
2/14/2023
Solid/Sludge Client
Test
Method
Results
Date Analyzed
Arsenic
EPA 200.7, Rev. 4 4, 1994
<43.1
mg/kg
03/01 /2023
Cadmium
EPA 200.7. Rev. 4 4, 1994
<43.1
mg/kg
03/01 /2023
Chromium
EPA 200.7, Rev 4 4, 1994
<43.1
mg/kg
03/01 /2023
Lead
EPA 200.7. Rev 4.4, 1994
<43.1
mg/kg
03/01 /2023
Magnesium
EPA 200.7, Rev 4.4,1994
3470
mg/kg
03/01/2023
Molybdenum
EPA 200.7. Rev 4 4, 1994
<43.1
mg/kg
03/01/2023
Nickel
EPA 200 7, Rev 44 1994
<43.1
mg/kg
03/01 /2023
Selenium
EPA 200 7, Rev 44 1994
<43.1
mg/kg
03/01 /2023
Mercury
SW-945 74716
<3.51
mg/kg
03/03/2023
Comment: Reported on a dry weight basis
Aeviewed by: i1' 0�'1V .im
Renort # 2023-03127 Pana 1 of i

Environmental Chemist, Inc., Wilmington, NC Lab #94
Sample Receipt Checklist
6602 Windmill Way
Wilmington, NC 28405
910.392.0223
Client: l (LLe } Datea�o _ Report Number: _ 2023- 03/R
Receipt of sample: ECHEM Pickup Client Delivery ❑
UPS ❑ FedEx ❑ Other ❑
❑ YES
❑ NO
1R N/A
us
1. Were ctody seals present on the cooler?
❑ YES
10NO
N/A
12. If custody seals were present, were they intact/unbroken?
Original temperature upon receipt °C Corrected temperature upon receipt °C
How temperature taken: ❑ Temperature Blank Against Bottles
IR Gun ID: Thomas Traceable S/N 210886869 IR Gun Correction Factor °C: 0.0
YES
¢rt] YES
>ei YES
I1 YES
❑ NO
❑ NO
❑ NO
❑ NO
3. If temperature of cooler exceeded 6°C, was Project Mgr./QA notified?
4. Were proper custody procedures (relinquished/received) followed?
5. Were sample ID's listed on the COC?
6. Were samples ID's listed on sample containers?
W YES
❑ NO
7. Were collection date and time listed on the COC?
IN YES
❑ NO
8. Were tests to be performed listed on the COC?
C41 YES
❑ NO
9. Did samples arrive in proper containers for each test?
I$d YES
❑ NO
10. Did samples arrive in good condition for each test?
YES
❑ NO
11, Was adequate sample volume available?'
YES
❑ NO
12. Were samples received within proper holding time for requested tests?
❑ YES
❑ NO
13. Were acid preserved samples received at a pH of <2? *
❑ YES
❑ NO
14. Were cyanide samples received at a pH >12?
❑ YES
❑ NO
15. Were sulfide samples received at a pH >9?
❑ YES
❑ YES
❑ YES
❑ NO
❑ NO
❑ NO 118.
16, Were NH3/TKN/Phenol received at a chlorine residual of <0.5 m/L? **
17. Were Sulfide/Cyanide received at a chlorine residual of <0.5 m/L?
Were orthophosphate samples filtered in the field within 15 minutes?
* TOC/Volatiles are pH checked at time of analysis and recorded on the benchsheet.
** Bacteria samples are checked for Chlorine at time of analysis and recorded on the benchsheet.
Sample Preservation: (Must be completed for any sample(s) incorrectly preserved or with headspace)
Sample(s) were received incorrectly preserved and were adjusted accordingly
by adding (circle one): H2SO4 HNO3 HCI NaOH
Time of preservation: If more than one preservative is needed, notate in comments below
Note: Notify customer service immediately for incorrectly preserved samples. Obtain a new sample or
notify the state lab if directed to analyzed by the customer. Who was notified, date and time:
Volatiles Sample(s) were received with headspace
COMMENTS:
DOC. QA.002 Rev 1

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Facility:
Source:
Location:
Contractor:
Type of Analysis:
Report No:
Date Sampled:
Date Reported:
Reporting Period:
Northwest Regional WRIT
Northwest Regional WRIT
Richlands, North Carolina
Triple S Farms & Cleaning, Inc
Water Reclamation Facility
NR 2023-29358
12/13/2023
1/15/2024
Annual 2023
Parameter
%
PPM
Dry Weight
EPA
Monthly Limits
Solids
1.620
Nitrogen (TKN)
1.550
15,500.000
Phosphorus
2.710
27,100.000
Potassium
0.378
3,780.000
Sulfur
0.000
Calcium
1.630
16,300.000
Magnesium
0.204
2,040.000
Sodium
1.010
10,100.000
Iron
---
Aluminum
---
22,700.000
Manganese
---
Copper
---
251.000
1,500
Zinc
---
969.000
2,800
Ammonia Nitrogen
0.172
1,720.000
Nitrate N / Nitrite N
---
5,990.000
Cadmium
---
11.400
85
Chromium
---
19.800
1,200
Nickel
---
11.400
420
Lead
---
11.600
300
Arsenic
---
11.400
75
Mercury
---
1.040
17
Selenium
---
11.400
100
pH
6.590
Calcium Carbonate Eq. (est)
0.000
Organic Nitrogen
1.378
Molybdenum
---
11.400
75
Chloride
---
Boron
Available P2O5
Specific Gravity
8.340

Water Reclamation Facility
Northwest Regional WRF
Richlands, North Carolina
Triple S Farms & Cleaning, Inc
Annual 2023
Date Reported: 1/15/2024 Report No: NR 2023-29358
Note All Units in Pounds Per Dry Ton
Macro Nutrients Physical Characteristics
PAN Surf.
21.968
PAN Inj.
23.688
P
54.200
K
7.560
Lime (estimated)
0.000
Secondary Nutrients
Calcium
32.600
Magnesium
4.080
Sodium
20.200
SAR
2.519
Chloride
0.000
Iron
0.000
Alumium
45.400
Manganese
0.000
Boron
0.000
Sulfur
0.000
% Solids
1.62
pH
6.590
Min Rate
0.300
Metals
Arsenic
0.023
Cadmium
0.023
Chromium
0.040
Copper
0.502
Lead
0.023
Mercury
0.002
Molybdenum
0.023
Nickel
0.023
Seleniun
0.023
Zinc
1.938

row,"—. -Mqql Environmental Chemists, Inc.
envirochem 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910 392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/ Fax
` 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/ Fax
ANALYTICAL & CONSULTING CHEMISTS [e-mail]
Onslow Water & Sewer Authority
Date of Report: Jan 15, 2024
228 Georgetown Road
Customer PO #:
Jacksonville NC 28540
Customer ID: 08100092
Attention:
Report #: 2023-29358
Project ID: Northwest RWRF Digester
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
23-71078 Site: Digester #1
12/13/2023
10:20 AM Solid/Sludge Jerry Parker
Test
Method
Results Date Analyzed
Chlordane (TCLP)
SW-846 8081 B
<0.02 mg/L
12/19/2023
Endrin (TCLP)
SW-846 60818
<0.0005 mg/L
12/19/2023
Heptachlor (TCLP)
SW-846 8081 B
<0.0005 mg/L
12/19/2023
Heptachlor epoxide (TCLP)
SW-846 8081 B
<0.0005 mg/L
12/19/2023
Lindane (TCLP)
SW-846 80816
<0.0005 mg/L
12/19/2023
Methoxychlor (TCLP)
SW-846 8081 B
<0.0005 mg/L
12/19/2023
Toxaphene (TCLP)
SW-846 8081 B
<0.05 mg/L
12/19/2023
2,4,5-TP (TCLP)
Sw-8468151 A
<0.003 mg/L
12/19/2023
2,4-D (TCLP)
SW-646 8151 A
<0.003 mg/L
12/19/2023
1,4-Dichlorobenzene (TCLP)
SW 8458270 E
<0.050 mg/L
12/20/2023
2,4,5-Trichlorophenol (TCLP)
SW-846 8270 E
<0.050 mg/L
12/20/2023
2,4,6-Trichlorophenol (TCLP)
SW-846 8270 E
<0.050 mg/L
12/20/2023
2,4-Dinitrotoluene (TCLP)
SW-848 8270 E
<0.050 mg/L
12/20/2023
Cresol (TCLP)
SW-846 8270 E
<0.050 mg/L
12/20/2023
Hexachloro-1,3-butadiene (TCLP)
SW-846 8270 E
<0.050 mg/L
12/20/2023
Hexachlorobenzene (TCLP)
SW-846 8270 E
<0.050 mg/L
12/20/2023
Hexachloroethane (TCLP)
SW-846 8270 E
<0.050 mg/L
12/20/2023
m + p-Cresol (TCLP)
SW-846 8270 E
<0.050 mg/L
12/20/2023
Nitrobenzene (TCLP)
SW-046 8270 E
<0.050 mg/L
12/20/2023
o-Cresol (TCLP)
SW-846 8270 E
<0.050 mg/L
12/20/2023
Pentachlorophenol (TCLP)
SW-846 8270 E
<0.250 mg/L
12/20/2023
Pyridine (TCLP)
SW-846 8270 E
<0.050 mg/L
12/20/2023
1,1-Dichloroethyiene (TCLP)
SW-846 Method 8260D
< 0.01 mg/L
12/21/2023
1,2-Dichloroethane (TCLP)
SW-846 Method 8260D
< 0.01 mg/L
12/21/2023
Benzene (TCLP)
SW-846 Method 8260D
< 0.01 mg/L
12/21/2023
Carbon Tetrachloride (TCLP)
SW-846 Method 8260D
< 0.01 mg/L
12/21/2023
Report 9 2023-29358
Page 1 of 3

Environmental Chemists, Inc.
envirochem 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab!Fax
�' 255 A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS infoirr-environmentalchemists.com
Onslow Water & Sewer Authority
Date of Report: Jan 15, 2024
228 Georgetown Road
Customer PO #:
Jacksonville NC 28540
Customer ID: 08100092
Attention:
Report #: 2023-29358
Project ID: Northwest RWRF Digester
Chlorobenzene (TCLP)
SW-846 Method 8260D
< 0.01 mg/L
12/21/2023
Chloroform (TCLP)
SW-848 Method 8260D
< 0.01 mg/L
12/21/2023
Methyl ethyl ketone (TCLP)
SW -US Method 8260D
< 0.05 mg/L
12/21/2023
Tetrachloroethylene (TCLP)
SW-846 Method 8260D
< 0.01 mg/L
12/21/2023
Trichloroethylene (TCLP)
SW-846 Method 8260D
< 0.01 mg/L
12/21/2023
Vinyl Chloride (TCLP)
SW-846 Method 0260D
< 0.01 mg/L
12/21/2023
RCI
Cyanide
SM 4500 CN D-2016
<1 mg/kg
12/27/2023
Sulfide
SM 4500 S 0-2011
0.18 mg/kg
01/02/2024
Ignitability
SW 846 method 1010
>157 OF
12/15/2023
Sludge Residuals
Aluminum
EPA 200.7, Rev. 4 4,1994
22700 mg/kg
01/02/2024
Arsenic
EPA 200.7, Rev. 4.4, 1994
<11.4 mg/kg
12/29/2023
Cadmium
EPA 200.7, Rev. 4.4,1994
<11.4 mg/kg
12/29/2023
Calcium
EPA 200.7, Rev 4.4,1994
16300 mg/kg
12/29/2023
Chromium
EPA 200.7, Rev 4.4,1994
19.8 mg/kg
12/29/2023
Copper
EPA 200.7, Rev. 4.4, 1994
251 mg/kg
12/29/2023
Lead
EPA 200.7, Rev 4.4,1994
11.6 mg/kg
12/29/2023
Magnesium
EPA 200.7, Rev 4A, 1994
2040 mg/kg
12/29/2023
Molybdenum
EPA 200.7, Rev 4.4, 1994
<11.4 mg/kg
12/29/2023
Nickel
EPA 200.7, Rev 4.4,1994
<11.4 mg/kg
12/29/2023
Potassium
EPA 200.7, Rev 4.4,1994
3780 mg/kg
01/02/2024
Selenium
EPA 200.7, Rev 4.4,1994
<11.4 mg/kg
12/29/2023
Sodium
EPA 200.7, Rev 4.4,1994
10100 mg/kg
01/02/2024
Zinc
EPA 200.7. Rev 4.4 1994
969 mg/kg
12/29/2023
Nitrate+Nitrite-Nitrogen
EPA 353.2
5990 mg/kg
12/18/2023
Total Solids (%)
SM 2540 6
1.62 %
12/18/2023
Ammonia Nitrogen
SM 4500 NIi3 C-2011
1720 mg/kg
12/17/2023
Total Kjeldahl Nitrogen (TKN)
SM 4500 Norg B-2011
15500 mg/kg
12/17/2023
Total Phosphorus
SM 4600 P (F-H}2011
27100 mg/kg
12/20/2023
Report 0: 2023-29358
Page 2 of 3

[envirroche]m
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab Fax
255-A Wilmington Highway, Jacksonville, NC 28540 ' 910.347.5843 Lab! Fax
inro(a environmentalchemists.com
Onslow Water & Sewer Authority Date of Report: Jan 15, 2024
228 Georgetown Road Customer PO #:
Jacksonville NC 28540 Customer ID: 08100092
Attention: Report #: 2023-29358
Project ID: Northwest RWRF Digester
pH SW 846 Method 9045D 6.59 units 12/22/2023
Result estimated. Analyzed out of 15 minutes hold time.
Mercury SW-846 7471 s <1.04 mg/kg 12/15/2023
TCLP Metals
Arsenic (TCLP)
EPA 200.7. Rev. 4.4,1994
<1.0 mg/L
12/27/2023
Barium (TCLP)
EPA 200.7. Rev. 4.4,1994
<1.0 mg/L
12/27/2023
Cadmium (TCLP)
EPA 200.7, Rev. 4.4, 1994
<1.0 mg/L
12/27/2023
Chromium (TCLP)
EPA 200.7, Rev. 4.4, 1094
<1.0 mg/L
12/27/2023
Lead (TCLP)
EPA 200.7, Rev. 4.4,1994
<1.0 mg/L
12/27/2023
Selenium (TCLP)
EPA 200.7, Rev. 4.4,1994
<1.0 mg/L
12/27/2023
Silver (TCLP)
EPA 2ca.7. Rev 4.4,1994
<1.0 mg/L
12/27/2023
Mercury (TCLP)
EPA 245.1
<0.0002 mg/L
12/27/2023
Comment: Sludge residuals, except pH, reported on a dry weight basis. pH reported on an as received basis.
Reviewed by: , �.'j���P�
Report V:: 2023-29358 Page 3 of 3

Environmental Chemist, Inc., Wilmington, NC Lab #94
6602 Windmill Way
Wilmington, NC 28405
910.392,0223
Sample Receipt Checklist
Client: A Date: A14 0- Report Number: 2023-
Receipt of sample:
ECHEM Pickup Client Delivery ❑ JUPS ❑ Fed Ex ❑ Other ❑
❑ YES 10 NO
DD N/A II. Were custody seals present on the cooler?
❑ YES 10 NO
I Cl N/A If custody seals were present, were they intact/unbroken?
112.
Original temperature upon receipt "C Corrected temperature upon receipt oC
How temperature taken:
_ _
El Terfiperature Blank O Against Bottles
IR Gun ID: Thomas Traceable S/N 210886869 IR Gun Correction Factor °C: 0.0
19 YES ❑ NO
3. If temperature of cooler exceeded 6°C, was Project Mgr./QA notified?
19 YES ❑ NO
4. Were proper custody procedures (relinquished/received) followed?
0 YES ❑ NO
5. Were sample ID's listed on the COO
© YES O
6. Were samples ID's listed on sample containers?
O YES O
7. Were collection date and time listed on the COC?
0 YES O
kCO3N
8. Were tests to be performed listed on the COC?
0 YES O
9. Did samples arrive in proper containers for each test?
O YES O
10. Did samples arrive in good condition for each test?
O YES O
11. Was adequate sample volume availableT
O YES 13 NO
12. Were samples received within proper holding time for requested tests?
❑ YES ❑ NO
13. Were acid preserved samples received at a pH of <27
C] YES ❑ NO
14. Were cyanide samples received at a pH >12?
ElYES ❑ NO
15. Were sulfide samples received at a pH >9?
❑ YES ❑ NO
16. Were NH3/TKN/Phenol received at a chlorine residual of <0.5 m/L? **
❑ YES ❑ NO
17. Were Sulfide/Cyanide received at a chlorine residual of <0.5 m/L?
0 YES 13 NO
18. Were orthophosphate samples filtered in the field within 15 minutes?
* TOC/Volatiles are pH checked at time of analysis and recorded on the benchsheet.
** Bacteria samples are checked for Chlorine at time of analysis and recorded on the benchsheet.
Sample Preservation:
(Must be completed for any sample(s) incorrectly preserved or with headspace)
Sample(s) _
were received incorrectly preserved and were adjusted accordingly
by adding (circle one):
H2SO4 HNO3 HCl NaOH
Time of preservation:
If more than one preservative is needed, notate in comments below
Note: Notify customer service immediately
for incorrectly preserved samples. Obtain a new sample or
notify the state lab if directed to analyzed by the customer. Who was notified, date and time:
Volatiles Sample(s)
were received with Mricnnro
COMMENTS:
DOC. QA.002 Rev 1

V
Z
C
2
W
V
J
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Facility:
Source:
Location:
Contractor:
Type of Analysis:
Report No:
Date Sampled:
Date Reported:
Reporting Period:
Triple S Farms
Southwest Plantation
Jacksonville, North Carolina
Triple S Farms
Jacksonville WWTP
SWP 2023-22677
9/28/2023
10/24/2023
Annual 2023
Parameter
%
PPM
Dry Weight
EPA
Monthly Limits
Solids
1.100
Nitrogen (TKN)
6.570
65,700.000
Phosphorus
1.250
12,500.000
Potassium
0.512
5,120.000
Sulfur
0.000
Calcium
1.690
16,900.000
Magnesium
0.346
3,460.000
Sodium
2.180
21,800.000
Iron
---
Aluminum
---
3,140.000
Manganese
---
Copper
---
214.000
1,500
Zinc
---
1,370.000
2,800
Ammonia Nitrogen
0.574
5,740.000
Nitrate N / Nitrite N
---
88.000
Cadmium
---
43.700
39
Chromium
---
43.700
1,200
Nickel
---
43.700
420
Lead
---
43.700
300
Arsenic
---
43.600
41
Mercury
---
1.400
17
Selenium
---
43.700
100
pH
7.480
Calcium Carbonate Eq. (est)
0.000
Organic Nitrogen
5.996
Molybdenum
---
43.700
75
Chloride
---
Boron
Available P2O5
Specific Gravity
8.340

Jacksonville WWTP
Southwest Plantation
Jacksonville, North Carolina
Triple S Farms
Annual 2023
Date Reported: 10/24/2023 Report No: SWP 2023-2267'
Note All Units in Pounds Per Dry Ton
Macro Nutrients Physical Characteristics
PAN Surf.
41.892
PAN Inj.
47.632
P
25.000
K
10.240
Lime (estimated)
0.000
Secondary Nutrients
Calcium
33.800
Magnesium
6.920
Sodium
43.600
SAR
4.176
Chloride
0.000
Iron
0.000
Alumium
6.280
Manganese
0.000
Boron
0.000
Sulfur
0.000
% Solids
1.10
pH
7.480
Min Rate
0.300
Metals
Arsenic
0.082
Cadmium
0.087
Chromium
0.087
Copper
0.428
Lead
0.087
Mercury
0.003
Molybdenum
0.087
Nickel
0.087
Seleniun
0.087
Zinc
2.740

envirochem
ANALYTICAL S CONSULTING CHEMISTS
Environmental Services
PO Box 1054
Jacksonville NC
Attention: Sonny Scozzari
Lab ID Sample ID:
23-55279 Site: Sludge
Test
Sludge Residuals
Aluminum
Arsenic
Cadmium
Calcium
Chromium
Copper
Lead
Magnesium
Molybdenum
Nickel
Potassium
Selenium
Sodium
Zinc
Nitrate+Nitrite-Nitrogen
Total Solids (%)
Ammonia Nitrogen
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 . 910.392.0223 Lab . 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 . 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 . 910.347.5843 Lab/Fax
[e-mail]
Date of Report: Oct 24, 2023
Customer PO #:
28541 Customer ID: 14110017
Report #: 2023-22677
Project ID: Bear Trail Golf Course
Collect Date/Time Matrix Sampled by
9/28/2023 5:15 PM Solid/Sludge Sonny Scozzari
Method
EPA 200 7 Rev 4 4, 1994
EPA 200 7 Rev 44 1994
EPA 200 7 Rev 44.1994
EPA 200 7 Rev 4 4, 1994
EPA 200 7 Rev 4 4, 1994
EPA 200 7 Rev 44, 1994
EPA 200 7 Rev 44, 1994
EPA 200 7 Rev 4 4, 1994
EPA 200 7 Rev 44 1994
EPA 200 7 Rev 44 1994
EPA 200 7 Rev 44 1994
EPA 200 7 Rev 44 1994
EPA 200 7 Rev 44 1994
EPA 200 7 Rev 44 1994
EPA 353 2
SM 2540 B
SM 4500 NH3 C-2011
Total Kjeldahl Nitrogen (TKN) SM 4500 Norg B-2011
Total Phosphorus SM 4500 P (F H;-2011
pH SW 846 Method 90450
Result estimated Analyzed out of 15 minutes hold time
Results
3140 mg/kg
<43.6 mglkg
<43.7 mg/kg
16900 mg/kg
<43.7 mg/kg
214 mg/kg
<43.7 mg/kg
3460 mg/kg
<43.7 mg/kg
<43.7 mg/kg
5120 mg/kg
<43.7 mg/kg
21800 mg/kg
1370 mg/kg
88.0 mg/kg
1.10%
5740 mg/kg
65700 mg/kg
12500 mg/kg
7.48 units
Date Analyzed
10/18/2023
10/18/2023
10/09/2023
10/09/2023
10/09/2023
10/09/2023
10/09/2023
10/09/2023
10/09/2023
10/09/2023
10/09/2023
10/09/2023
10/09/2023
10/09/2023
10/03/2023
10/03/2023
10/02/2023
10/02/2023
10/09/2023
10/09/2023
Mercury SW-846 7471 B <1.40 mg/kg 10/11 /2023
Comment, Results, except pH, reported on a dry weight basis. pH reported on an as received basis.
Reviewed by: }
Report S 2023-22677 Page 1 of 1

, --I ISLVII, ,vt— Lao;:y4
6602 Windmill Wal
Wilmington, NC 28405
910
Sample Receipt Checklist .392.0223
Client: R(�r�(' Date Z2.lo7-7
Report
Number;
FCH_Efo PI ❑ r -- - ---_- --- - —
_
❑ YES ❑
70
NO
id/A- 1. Were custody seals present on the cooler?
Original temperature
upon
N/A 2. If custody seals were present, were the unbr ?
receipt y intact / oken . '--
---�� C Corrected temperature upon receipt
!Hove temperature taken: O Temperature Sian; --
tigainst Bottles
iFZ Gun ID, Thomas Traceable 5/N 210886869 IR Gun Correction Factor "C: O.p
YES ©
YES ❑
NO
NO
3. If temperature of cooler exceeded 6'C, eras Project Mgr./QA notified?
YES ❑
NO
4. Were proper custody procedures (relinquished/received) followed?
YES
S. Were sample ID's listed on the COO
❑
YES ❑
NO
6. Were samples ID's listed on sample containers?
YES ❑
NO
7. Were collection date and time listed on the COC?
YLS ❑
NO
8. Were tests to be performed fisted on the COC?
YES ❑
NO
9. Did samples arrive in proper containers for each test?
YES ❑
NO
10. Did samples arrive in good condition for each test?
NO
11. Was adequate sample volume available?
YES ❑
O YES ❑
NO
NO
12. Were samples received within proper holding time for requested tests?
❑ YES ❑
NO
13. Were acid preserved samples received at a pH of <2?
❑ YES ❑
14. Were cyanide samples received at a pH >12?
YES ❑
NO
15. Were sulfide samples received at a pH >9?
15 YES ❑
NO
NO
16. Were NH3/TKN/Phenol received at a chlorine residual of <0.5 m/L?
❑ YES ❑
NO
17. Were Sulfide/Cyanide received at a chlorine residual of <0.5 m/L7
18. Were orthoohosnhata c2., ni— 0,7... A :- —
* TOC/Volatiles are pH checked at time of analysis and recorded on the benchsheet.
** Bacteria samples are checked for Chlorine at time of analysis and recorded on the benchshL.et.
Sample Preservation: (Must be completed for any Sample(s) incorrectly preserved or with
Sample(s)
headspace)
by adding (circle one): were received incorrectly preserved and were adjusted accordingly
HzSO4 HNOa HCl NaOH
INola
ime of preservation; If more than one preservative is needed, notate in comments below
ate: Notiry custome- service immediately for incorrectly preserved samples. Obtain a new sample or
otify the state lab if directed to analyzed by the customer. Who was notified, date and time:
vles Samples) were received with headspace
COMMENTS:
DOC. CtA.002 Rev 1

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Facility:
Source:
Location:
Contractor:
Type of Analysis:
Report No:
Date Sampled:
Date Reported:
Reporting Period:
Summerhouse WRF
Summerhouse WRF
Holly Ridge, NC
Triple S Farms
Water Reclamation Facility
SMH E2023-04013
2/28/2023 Type of Stabilization: Fecal/SOUR
3/10/2023
Annual 2023
Parameter
%
PPM
Dry Weight
EPA
Monthly Limits
Solids
0.756
Nitrogen (TKN)
2.570
25,700.000
Phosphorus
2.580
25,800.000
Potassium
0.479
4,790.000
Sulfur
0.000
Calcium
3.710
37,100.000
Magnesium
0.299
2,990.000
Sodium
2.760
27,600.000
Iron
---
Aluminum
---
1,460.000
Manganese
---
Copper
---
114.000
1,500
Zinc
---
2,210.000
2,800
Ammonia Nitrogen
0.264
2,640.000
Nitrate N / Nitrite N
---
19,000.000
Cadmium
---
25.300
85
Chromium
---
25.300
1,200
Nickel
---
25.300
420
Lead
---
25.300
300
Arsenic
---
25.300
75
Mercury
---
2.320
17
Selenium
---
25.300
100
pH
4.790
Calcium Carbonate Eq. (est)
0.000
Organic Nitrogen
2.306
Molybdenum
---
25.300
75
Chloride
---
Boron
Available P2O5
Specific Gravity
8.340

Water Reclamation Facility
Summerhouse WRF
Holly Ridge, NC
Triple S Farms
Annual 2023
Date Reported: 3/10/2023 Report No: SMH E2023-040
Note All Units in Pounds Per Dry Ton
Macro Nutrients Physical Characteristics
PAN Surf.
54.476
PAN Inj.
57.116
P
51.600
K
9.580
Lime (estimated)
0.000
Secondary Nutrients
Calcium
74.200
Magnesium
5.980
Sodium
55.200
SAR
3.216
Chloride
0.000
Iron
0.000
Alumium
2.920
Manganese
0.000
Boron
0.000
Sulfur
0.000
% Solids
0.76
pH
4.790
Min Rate
0.300
Metals
Arsenic
0.051
Cadmium
0.051
Chromium
0.051
Copper
0.228
Lead
0.051
Mercury
0.005
Molybdenum
0.051
Nickel
0.051
Seleniun
0.051
Zinc
4.420

ONWASA
March 24, 2023
Kary Herndon
Summer House WRF
Twining Rose Lane
Holly Ridge, NC 28445
RE: Summer House Sludge
ONWASA Laboratory
228 Georgetown Road
Jacksonville NC 28540
[phone]
Enclosed are the results of analyses for samples received by our laboratory on 2/27/2023. If you
have any questions concerning this report, please feel free to contact me.
Sincerely,
7 CNO"'--z .�
Todd A. Roberts For Kary Herndon
ORC

ONWASA
Summer House WRF Project: Summer House Sludge
Twining Rose Lane Project Number: Reported:
Holly Ridge, NC 28445 Project Manager: Katy Herndon 03/24/2023 15:06
Sample Results
Data Analyzed by: Environmental Chemists, Inc.
Sample: SH Digestor Q230904-01 (SL) 02/28/2023 07:04
Reporting Date Analyst
Analyse Result Qua[ Limit Units Analyzed Initials Method
Aluminum
1460
mg/Kg
03/01/2023
EPA 200.7
Ammonia-N
2640
mg/Kg
03/01/2023
SM 4500 NH3 C
Arsenic
< 25.3
mg/Kg
03/01/2023
EPA 200.7
Calcium
37100
mg/Kg
03/01/2023
EPA 200.7
Cadmium
< 25.3
mg/Kg
03/01/2023
EPA 200.7
Chromium
< 25.3
mg/Kg
03/01/2023
EPA 200.7
Copper
114
mg/Kg
03/01/2023
EPA 200.7
Mercury
< 2.32
mg/Kg
03/03/2023
SW846 7471E
Potassium
4790
mg/Kg
03/01/2023
EPA 200.7
Magnesium
2990
mg/Kg
03/01/2023
EPA 200.7
Molybdenum
< 25.3
mg/Kg
03/01/2023
EPA 200.7
Sodium
27600
mg/Kg
03/03/2023
EPA 200.7
Nickel
< 25.3
mg/Kg
03/01/2023
EPA 200.7
Nitrate+ Nitrate -Nitrogen
19000
mg/Kg
03/02/2023
EPA 353.2
Lead
< 25.3
mg/Kg
03/01/2023
EPA 200.7
PH
4.79
pH Units
03/01/2023
SM 4500 H B
Selenium
< 25.3
mg/Kg
03/01/2023
EPA 200.7
Total Kjeldahl Nitrogen
25700
mg/Kg
03/01/2023
EPA 351.2
Phosphorus, total Sludge
25800
mg/Kg
03/08/2023
SM 4500 P E
Total Solids (%)
0.72
%
03/01/2023
SM 2540 G
Zinc
2210
mg/Kg
03/01/2023
EPA 200.7
Sample: SH Fecal # 1 Q230904-02 (SL) 02/28/2023 07:13
Reporting Date Analyst
Analyse Result Qual Limit Units Analyzed Initials Method
Fecal Density < 291 MPN/g 02/28/2023 SM 9221C E MPN
24hr 503
Total Solids (%) 0.62 % 03/O1/2023 SM 2540 G
Sample: SH Fecal # 2 Q230904-03 (SL) 02/28/2023 07:15
Reporting Date Analyst
Analyse Result Qual Limit Units Analyzed Initials Method
Fecal Density < 240 MPN/g 02/28/2023 SM 9221C E MPN
24hr 503
Total Solids (%) 0.75 % 03/01/2023 SM 2540 G
The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document
No duplication of this report is allowed, except in its entirety. Page 2 of 6

6
ONWASA
Summer House WRF Project: Summer House Sludge
Twining Rose Lane Project Number: Reported:
Holly Ridge, NC 28445 Project Manager: Kary Herndon 03/24/2023 15:06
Sample Results
(Continued)
Data Analyzed by: Environmental Chemists, Inc.
Sample: SH Fecal # 3 Q230904-04 (SQ 02/28/2023 07:17
Reporting Date Analyst
Analyte Result Qual Limit Units Analyzed Initials Method
Fecal Density < 228 MPN/g 02/28/2023 SM 9221C E MPN
24hr 503
Total Solids (%) 0.79 % 03/O1/2023 SM 2540 G
Sample: SH Fecal # 4 Q230904-05 (SQ 02/28/2023 07:20
Reporting Date Analyst
Analyte Result Qual Limit Units Analyzed Initials Method
Fecal Density < 196 MPN/g 02/28/2023 SM 9221C E MPN
24hr 503
Total Solids (%) 0.92 % 03/01/2023 SM 2540 G
Sample: SH Fecal # 5 Q230904-06 (SQ 02/28/2023 07:22
Reporting Date Analyst
Analyte Result Qual Limit Units Analyzed Initials Method
Fecal Density < 254 MPN/g 02/28/2023 SM 9221C E MPN
24hr 503
Total Solids (%) 0.71 % 03/01/2023 SM 2540 G
Sample: SH Fecal # 6 Q230904-07 (SQ 02/28/2023 07:25
Reporting Date Analyst
Analyte Result Qual Limit Units Analyzed Initials Method
Fecal Density < 234 MPN/g 02/28/2023 SM 9221C E MPN
24hr 503
Total Solids (%) 0.77 % 03/01/2023 SM 2540 G
Sample: SH Fecal # 7 Q230904-08 (SQ 02/28/2023 07:27
Reporting Date Analyst
Analyte Result Qual Limit Units Analyzed Initials Method
Fecal Density < 247
Total Solids (%) 0.73
The contenes of this report apply to the sample(s) analyzed in accordance with the chain of custody document.
No duplication of this report is allowed, except in its entirety.
MPN/g 02/28/2023 SM 9221C E MPN
24hr 503
% 03/01/2023 SM 2540 G
Page 3 of 6

4
0NWASA
Summer House WRF Project: Summer House Sludge
Twining Rose Lane Project Number: Reported:
Holly Ridge, NC 28445 Project Manager: Kary Herndon 03/24/2023 15:06
Notes and Definitions
Item Definition
Dry Sample results reported on a dry weight basis.
ND Analyte NOT DETECTED at or above the reporting limit.
The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document.
No duplication of this report is allowed, except in its entirety. Page 4 of 6

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envirochem
ANALYTICAL & CONSULTING CHEMISTS
F"07 —Iqqql
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28W • 910.347.5843 Lab/Fax
[e-mail]
Onslow Water & Sewer Authority
Date of Report: Mar 10, 2023
228 Georgetown Road
Customer PO #:
Jacksonville NC 28540
Customer ID: 08100092
Attention: Todd Roberts
Report #: 2023-04013
Project ID: Summerhouse
Lab ID Sample ID:
Collect DatelTime Matrix Sampled by
23-09939 Site: Digester
2/28/2023
7:04 AM Solid/Sludge Kary Herndon
Test
Method
Results Date Analyzed
Sludge Residuals
Aluminum
EPA 200.7, Rev. 4.4, 1994
1460 mg/kg
03/01 /2023
Arsenic
EPA 200.7, Rev. 4.4. 1994
<25.3 mg/kg
03/01/2023
Cadmium
EPA 200.7, Rev. 4.4, 1994
<25.3 mg/kg
03/01/2023
Calcium
EPA 200.7, Rev. 4.4,1994
37100 mg/kg
03/01/2023
Chromium
EPA 200.7, Rev. 4A.1994
<25.3 mg/kg
03/01/2023
Copper
EPA 200.7, Rev. 4.4. 1994
114 mg/kg
03/01/2023
Lead
EPA 200.7, Rev. 4.4, 1994
<25.3 mg/kg
03/01/2023
Magnesium
EPA 200.7, Rev. 4.4.1994
2990 mg/kg
03/01/2023
Molybdenum
EPA 200.7, Rev. 4.4. 1994
<25.3mg/kg
03/01/2023
Nickel
EPA 200 7, Rev. 4.4. 1994
<25.3 mg/kg
03/01/2023
Potassium
EPA 200 7, Rev. 4.4. 1994
4790 mg/kg
03/01/2023
Selenium
EPA 200.7, Rev. 4.4. 1994
<25.3 mg/kg
03/01/2023
Sodium
EPA 200.7, Rev. 4.4.1994
27600 mg/kg
03/03/2023
Zinc
EPA 200.7, Rev. 4.4,1994
2210 mg/kg
03/01/2023
Nitrate+Nitrite-Nitrogen
EPA 353.2
19000 mg/kg
03/02/2023
Total Solids (%)
SM 2540 s
0.72 %
03/01/2023
Ammonia Nitrogen
SM 4500 NH3 C-2011
2640 mg/kg
03/01/2023
Total Kjeldahi Nitrogen (TKN)
SM 4500 Norg B-2011
25700 mg/kg
03/01/2023
Total Phosphorus
SM 4500 P (F-H)-2011
25800 mg/kg
03/08/2023
pH
SW e4e Method 9045D
4.79 units
03/01/2023
Result estimated. Analyzed out of 15 minutes hold time.
Mercury SW-e4e 7471 s <2.32 mg/kg 03/03/2023
Report t 2023 04013 Page 1 of 3

:envirochem'-
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 - 910392.0223 Lab - 910392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 - 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 - 910.347.5843 Lab/Fax
infotrcenvironmentalchemists.com
Onslow Water & Sewer Authority Date of Report: Mar 10, 2023
228 Georgetown Road Customer PO #:
Jacksonville NC 28540 Customer ID: 08100092
Attention: Todd Roberts Report #: 2023-04013
Project ID: Summerhouse
Lab ID Sample ID: Collect DatelTime Matrix Sampled by
23-09940 Site: #1 2/28/2023 7:13 AM Solid/Sludge Kary Herndon
Test Method Results Date Analyzed
Total Solids (%)
Fecal Density
Lab ID Sample ID:
23-09941 Site: #2
SM 2540 B
SM 9221C E-2014
0.62 %
<291 MPN/g
Collect Date/Time Matrix Sampled by
2/28/2023 7:15 AM Solid/Sludge Kary Herndon
03/01 /2023
02/28/2023
Test Method Results Date Analyzed
Total Solids (%)
SM 2540 B
0.75 % 03/01/2023
Fecal Density SM 9221C E-2014 <240 MPN/g 02/28/2023
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
23-09942 Site: #3 2/2812023 7:17 AM Solid/Sludge Kary Herndon
Test Method Results Date Analyzed
Total Solids (%) SM 2540 B 0.79 % 03/01 /2023
Fecal Density SM 9221C E-2014 <228 MPN/g 02/28/2023
Lab ID Sample ID: Collect DatelTime Matrix Sampled by
23-09943 Site: #4 2/28/2023 7:20 AM Solid/Sludge Kary Herndon
Test Method Results Date Analyzed
Total Solids (%) SM 2540 B 0.92 % 03/01/2023
Fecal Density SM 9221C E-2014 <196 MPN/g 02/28/2023
Lab ID Sample ID: Collect Daterrime Matrix Sampled by
23-09944 Site: #5 2/28/2023 7:22 AM Solid/Sludge Kary Herndon
Test Method Results Date Analyzed
Total Solids (%)
Fecal Density
SM 2540 B
SM 9221C E-2014
0.71 %
<254 MPN/g
03/01 /2023
02/28/2023
Reports - 2023-04013 Page 2 of 3

Environmental Chemists, Inc.
• 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab - 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.3475843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS info(a environmentalchemismcom
Onslow Water & Sewer Authority
228 Georgetown Road
Jacksonville NC 28540
Attention: Todd Roberts
Lab ID Sample ID:
23-09945 Site: #6
Date of Report: Mar 10, 2023
Customer PO #:
Customer ID: 08100092
Report #: 2023-04013
Project ID: Summerhouse
Collect Date/Time Matrix Sampled by
2/28/2023 7.25 AM Solid/Sludge Kary Hemdon
Test Method Results Date Analyzed
Total Solids (%)
Fecal Density
Lab ID Sample ID:
23-09946 Site: #7
SM 2540 B
SM 9221C E•2014
0.77 % 03/01 /2023
<234 MPN/g 02/28/2023
Collect Date/Time Matrix Sampled by
2/28/2023 7:27 AM Solid/Sludge Kary Herndon
Test Method Results Date Analyzed
Total Solids (%)
Fecal Density
SM 2540 B
SM 9221 C E-2014
0.73 % 03/01 /2023
<247 MPN/g 02/28/2023
Comment: Results, except pH, reported on a dry weight basis. pH reported on an as received basis.
Reviewed by:
Report # . 2023-04013 Page 3 or 3

Environmental Chemist, Inc., Wilmington, NC Lab #94
6602 Windmill Way
Wilmington, NC 28405
Sample Receipt Checklist 910.392.0223
Client: — Date: Report Number. 29 L 40 3
Receipt of sample:
❑ YES ❑ NO
HEM Pickup Client Delivery ❑ UPS ❑ FeclEx ❑ Other ❑
N/A
❑ YES
0—NO
1. Were custody seals present on the cooler?
N/A
Original temperature upon
2. If custody seals were present, were they intact/unbroken?
receipt °C
_ Corrected temperature upon receipt aC
How temperature taken: ❑ Temperature Blank
es
IR Gun 1D: Thomas Traceable S/N 210886869 IR Gun Correction Factor Ct10 0
YES ❑ NO
YES ❑ NO
3. If temperature of cooler exceeded 6'C, was Project Mgr./QA notified?
YES ❑
4. Were proper custody procedures (relinquished/received) followed?
NO
5. Were sample ID's listed on the COC?
YES ❑ NO
6. Were samples iD's listed on sample containers?
YES ❑ NO
7. Were collection date and time listed on the COC?
YES ❑ NO
8. Were tests to be performed listed on the COC?
YES ❑ NO
YES ❑
9. Did samples arrive in proper containers for each test?
NO
10. Did samples arrive in good condition for each test?
YES ❑ NO
11. Was adequate sample volume availabie?'
YES ❑ NO
❑ YES ❑ NO
12. Were samples received within proper holding time for requested tests?
❑ YES ❑
13. Were acid preserved samples received at a pH of <2?
NO
❑
14. Were cyanide samples received at a pH >12?
YES ❑ NO
❑
15. Were sulfide samples received at a pH >9?
YES ❑ NO
❑ YES ❑
16. Were NH3/TKN/Phenol received at a chlorine residual of <0.5 m/L? "
NO
❑ YES ❑
17. Were Sulfide/Cyanide received at a chlorine residual of <0.5 m/L?
NO
18. Were orthophosphate samples filtered in the field within 15 minutes?
* TOC/Volatiles are pH checked at time of analysis and recorded on the benchsheet.
*# Bacteria samples are checked for Chlorine at time of analysis and recorded on the benchsheet.
Sample Preservation: (Must be completed for any sample(s) incorrectly preserved or with headspace)
Sample(s) were received incorrectly preserved and were adjusted accordingly
by adding (circle one): H2SO4 HNO3 HCi NaOH
Time of preservation: If more than one preservative is needed, notate in comments below
Note: Notify customer service immediately for incorrectly preserved samples. Obtain anew sample or
notify the state lab if directed to analyzed by the customer. Who was notified, date and time:
Volatiles Sample(s) were received with headspace
COMMENTS:
Y
DOC. QA.002 Rev 1

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Facility:
Source:
Location:
Contractor:
Type of Analysis:
Report No:
Date Sampled:
Date Reported:
Reporting Period
Swansboro WWTP
Swansboro WWTP
Swansboro, NC
Triple S Farms
WWTP
SWB E2024-02029
1/24/2024 Type of Stabilization: Fecal/SOUR
2/14/2024
Annual 2023
Parameter
%
PPM
Dry Weight
EPA
Monthly Limits
Solids
1.790
Nitrogen (TKN)
4.790
47,900.000
Phosphorus
1.200
12,000.000
Potassium
0.363
3,630.000
Sulfur
0.000
Calcium
3.060
30,600.000
Magnesium
0.227
2,270.000
Sodium
0.603
6,030.000
Iron
---
Aluminum
---
2,920.000
Manganese
---
Copper
---
420.000
1,500
Zinc
---
3,980.000
7,500
Ammonia Nitrogen
0.157
1,570.000
Nitrate N / Nitrite N
---
106.000
Cadmium
---
9.270
85
Chromium
---
19.700
1,200
Nickel
---
13.200
420
Lead
---
10.600
300
Arsenic
---
9.270
75
Mercury
---
1.120
17
Selenium
---
9.270
100
pH
7.100
Calcium Carbonate Eq. (est)
0.000
Organic Nitrogen
4.633
Molybdenum
---
9.270
75
Chloride
---
Boron
Available P2O5
Specific Gravity
8.340

WWTP
Swansboro WWTP
Swansboro, NC
Triple S Farms
Annual 2023
Date Reported: 2/14/2024 Report No: SWB E2024-020
Note All Units in Pounds Per Dry Ton
Macro Nutrients Physical Characteristics
PAN Surf.
29.580
PAN Inj.
31.150
P
24.000
K
7.260
Lime (estimated)
0.000
Secondary Nutrients
Calcium
61.200
Magnesium
4.540
Sodium
12.060
SAR
1.196
Chloride
0.000
Iron
0.000
Alumium
5.840
Manganese
0.000
Boron
0.000
Sulfur
0.000
% Solids
1.79
pH
7.100
Min Rate
0.300
Metals
Arsenic
0.019
Cadmium
0.019
Chromium
0.039
Copper
0.840
Lead
0.021
Mercury
0.002
Molybdenum
0.019
Nickel
0.026
Seleniun
0.019
Zinc
7.960

Environmental Chemists, Inc.
envirochem 6602 Windmill Way, Wilmington, NC 28405 ' 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab,./Fax
ANALYTICAL & CONSULTING CHEMISTS info'menvironmentalchemists.com
Onslow Water & Sewer Authority
Date of Report: Feb 14, 2024
228 Georgetown Road
Customer PO #:
Jacksonville NC 28540
Customer ID: 08100092
Attention:
Report #: 2024-02029
Project ID: Swansboro
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
24-04808 Site: Sludge
1/24/2024
8:45 AM Solid/Sludge Samantha Howard
Test
Method
Results Date Analyzed
Sludge Residuals
Aluminum
EPA 200 7, Rev 4 4, 1994
2920 mg/kg
02/09/2024
Arsenic
EPA 200 7, Rev 4 4, 1994
20.1 mg/kg
02/09/2024
Cadmium
EPA 200 7, Rev 4 4 1994
<9.27 mg/kg
02/08/2024
Calcium
EPA 200 7, Rev 4 4 1994
30600 mg/kg
02/08/2024
Chromium
EPA 200.7. Rev 4 4. 1994
19.7 mg/kg
02/08/2024
Copper
EPA 200 7. Rev 4 4, 1994
420 mpg
02/08/2024
Lead
EPA 200.7, Rev 4 4. 1994
10.6 mg/kg
02/08/2024
Magnesium
EPA 200.7, Rev 4 4 1994
2270 mg/kg
02/08/2024
Molybdenum
EPA 200.7, Rev 4 4, 1994
<9.27 mg/kg
02/08/2024
Nickel
EPA 200.7, Rev 4 4, 1994
13.2 mg/kg
02/08/2024
Potassium
EPA 200.7, Rev 4 4,1994
3630 mg/kg
02/08/2024
Selenium
EPA 200.7, Rev 44. 1994
<9.27 mg/kg
02/08/2024
Sodium
EPA 200.7, Rev 4 4, 1994
6030 mg/kg
02/08/2024
Zinc
EPA 200.7, Rev 4 4, 1994
3980 mg/kg
02/08/2024
Nitrate+Nitrite-Nitrogen
EPA353.2
106mg/kg
01/25/2024
Total Solids (%)
SM 2540 8
1.79 %
01/25/2024
Ammonia Nitrogen
SM 4500 NH3 C-2011
1570 mg/kg
01/25/2024
Total KJeldahl Nitrogen (TKN)
SM 4500 Norg 8-2011
47900 mg/kg
01/25/2024
Total Phosphorus
SM 4500 P (F-H)-2011
12000 mg/kg
02/05/2024
pH
SW 846 Method 9045D
7.10 units
01/25/2024
Result estimated. Analyzed out of 15 minutes hold time
Mercury SW-846 7471 B <1.12 mg/kg 02/01/2024
Comment -
Reviewed by:
Report # 2024.02029 Page 1 of 1

Environmental Chemist, Inc., Wilmington, NC Lab #94
6602 Windmill Way
Wilmington, NC 28405
910.392.0223
Sample Receipt Checklist
Client: WN R Date: L Report Number: _ 2024-
Receipt of sample: ECHEM Pickup R Client Delivery ❑
UPS ❑ FedEx ❑ Other ❑
❑ YES
113 NO
Cl N/A
1. Were custody seals present on the cooler?
❑ YES
113 NO
0 N/A 12.
If custody seals were present, were they intact/unbroken?
Original temperature upon receipt °C Corrected temperature upon receipt °C
How temperature taken: ❑ Temperature Blank © Against Bottles
IR Gun ID: Thomas Traceable S/N 210886869 IR Gun Correction Factor °C: 0.0
© YES
❑ NO
3. If temperature of cooler exceeded 6°C, was Project Mgr./QA notified?
IN YES
❑ NO
4. Were proper custody procedures (relinquished/received) followed?
© YES
❑ NO
S. Were sample ID's listed on the COC?
© YES
❑ NO
6. Were samples ID's listed on sample containers?
© YES
❑ NO
7. Were collection date and time listed on the COC?
® YES
❑ NO
8. Were tests to be performed listed on the COC?
0 YES
❑ NO
9. Did samples arrive in proper containers for each test?
® YES
❑ NO
10. Did samples arrive in good condition for each test?
© YES
❑ NO
11. Was adequate sample volume available?'
® YES
❑ NO
12. Were samples received within proper holding time for requested tests?
❑ YES
❑ YES
❑ NO
❑ NO
13. Were acid preserved samples received at a pH of <2?
14. Were cyanide samples received at a pH >12?
❑ YES
❑ NO
15. Were sulfide samples received at a pH >9?
❑ YES
❑ NO
16. Were NH3/TKN/Phenol received at a chlorine residual of <0.5 m/L? **
❑ YES
❑ NO
17. Were Sulfide/Cyanide received at a chlorine residual of <0.5 m/L?
❑ YES
❑ NO
18. Were orthophosphate samples filtered in the field within 15 minutes?
* TOC/Volatiles are pH checked at time of analysis and recorded on the benchsheet.
** Bacteria samples are checked for Chlorine at time of analysis and recorded on the benchsheet.
Sample Preservation: (Must be completed for any sample(s) incorrectly preserved or with headspace)
Sample(s) were received incorrectly preserved and were adjusted accordingly
by adding (circle one): H2SO4 HNO3 HCI NaOH
Time of preservation: If more than one preservative is needed, notate in comments below
Note: Notify customer service immediately for incorrectly preserved samples. Obtain a new sample or
notify the state lab if directed to analyzed by the customer. Who was notified, date and time:
Volatiles Sample(s) were received with headspace
COMMENTS:
DOC. QA.002 Rev 1

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Facility:
Triple S Farms
Source:
Wallace WWTP
Location:
Wallace, North Carolina
Contractor:
Triple S Farms
Type of Analysis:
Wallace WWTP
Report No:
WL 1-2023-00643
Date Sampled:
1/10/2023 Type of Stabilization: Lime
Date Reported:
2/1/2023
Reporting Period:
1st Quarter 2023
Parameter
% PPM EPA
Dry Weight Monthly Limits
Solids*
2.97
Nitrogen (TKN)
4.700
47,000.000
Phosphorus
1.950
19,500.000
Potassium
0.506
5,060.000
Sulfur
0.000
Calcium
2.740
27,400.000
Magnesium
0.458
4,580.000
Sodium
0.550
5,500.000
rm"
---
Copper
---
790.000
1,500
Zinc
---
1,390.000
2,800
Ammonia Nitrogen
0.086
858.000
Nitrate N / Nitrite N
---
2,440.000
Cadmium
---
15.978
39
Chromium
---
28.200
1,200
Nickel
---
20.000
420
Lead
---
35.900
300
Arsenic
---
20.700
41
Mercury
---
0.915
17
Selenium
---
15.978
100
pH**
5.280
Calcium Carbonate Eq. (est)
0.000
Organic Nitrogen
4.614
Molybdenum
---
15.978
75
Chloride
---
Boron
Available P2O5
Specific Gravity
8.340
I*Percent Solids listed are an average from Fecal Density Analyses.
**pH result listed was pulled from lime stabilzation.

Wallace WWTP
Wallace WWTP
Wallace, North Carolina
Triple S Farms
1st Quarter 2023
Date Reported: 2/l/2023 Report No: WL 1-2023-0064
Note All Units in Pounds Per Dry Ton
Macro Nutrients Physical Characteristics
PAN Surf.
33.423
PAN Inj.
34.281
P
39.000
K
10.120
Lime (estimated)
0.000
Secondary Nutrients
Calcium
54.800
Magnesium
9.160
Sodium
11.000
SAR
1.392
Chloride
0.000
Iron
0.000
Alumium
17.200
Manganese
0.000
Boron
0.000
Sulfur
0.000
% Solids
2.97
pH
5.280
Min Rate
0.300
Metals
Arsenic
0.041
Cadmium
0.032
Chromium
0.056
Copper
1.580
Lead
0.072
Mercury
0.002
Molybdenum
0.032
Nickel
0.040
Seleniun
0.032
Zinc
2.780

F""M' _- _71 Environmental Chemists, Inc.
1 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
sM 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS [e-mail]
Branch Residuals/Bob Branch
Date of Report: Feb 01, 2023
1735 Heckle Blvd Suite 103-291
Customer PO #:
Rock Hill SC 29732
Customer ID: 15060009
Attention:
Report #: 2023-00643
Project ID: Sludge -Wallace WWTP
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
23-01571 Site: Sludge
1/10/2023
11:25 AM Solid/Sludge
Test
Method
Results
Date Analyzed
Zinc
EPA 200 7, Rev. 4.4, 1994
1390 mg/kg
01/16/2023
Chlordane (TCLP)
SW-846 8081 B
<0.02 mg/L
01/16/2023
Endrin (TCLP)
SW-846 8081 B
<0.0005 mg/L
01/16/2023
Heptachlor (TCLP)
SW-8468081 B
<0.0005mg/L
01/16/2023
Heptachlor epoxide (TCLP)
SW-846 8081 B
<0.0005 mg/L
01/16/2023
Lindane (TCLP)
SW-846 8081 B
<0.0005 mg/L
01/16/2023
Methoxychlor (TCLP)
SW-8468081 B
<0.0005 mg/L
01/16/2023
Toxaphene (TCLP)
SW-846 8081 B
<0.05 mg/L
01/16/2023
2,4,5-TP (TCLP)
SW-846 8151 A
<0.003 mg/L
01/16/2023
2,4-D (TCLP)
SW-8468151 A
<0.003mg/L
01/16/2023
1,4-Dichlorobenzene (TCLP)
SW-846 8270 E
<0.050 mg/L
01/13/2023
2,4,5-Trichlorophenol (TCLP)
SW-8468270E
<0.050mg/L
01/13/2023
2,4,6-Trichlorophenol (TCLP)
SW-846 8270 E
<0.050 mg/L
01/13/2023
2,4-Dinitrotoluene (TCLP)
SW-8468270 E
<0.050 mg/L
01/13/2023
Cresol (TCLP)
SW-8468270E
<0.050mg/L
01/13/2023
Hexachloro-1,3-butadiene (TCLP)
SW-846 8270 E
<0.050 mg/L
01/13/2023
Hexachlorobenzene (TCLP)
SW-846 8270 E
<0.050 mg/L
01/13/2023
Hexachloroethane (TCLP)
SW-8468270E
<0.050mg/L
01/13/2023
m + p-Cresol (TCLP)
SW-846 8270 E
<0.050 mg/L
01/13/2023
Nitrobenzene (TCLP)
SW-846 8270 E
<0.050 mg/L
01/13/2023
o-Cresol (TCLP)
SW-846 8270 E
<0.050 mg/L
01/13/2023
Pentachlorophenol (TCLP)
SW-8468270E
<0.250mg/L
01/13/2023
Pyridine (TCLP)
SW-846 8270 E
<0.050 mg/L
01/13/2023
1,1-Dichloroethylene (TCLP)
SW-846 Method8260D
<0.01 mg1L
01/24/2023
1,2-Dichloroethane (TCLP)
SW-846 Method8260D
<0.01 mg/L
01/24/2023
Benzene (TCLP)
SW-846 Method 8260D
<0.01 mg/L
01/24/2023
Report #. 2023-00643
0- 1 ..a A

F 7"", 7 _1"_' q _7 I Environmental Chemists, Inc.
envirochem6602 Windmill Way, Wilmington, NC 28405 * 910.392.0223 Lab a 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
sM 255-A Wilmington Highway, Jacksonville, NC 28540 a 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS [e-mail]
Branch Residuals/Bob Branch
Date of Report: Feb 01, 2023
1735 Heckle Blvd Suite 103-291
Customer PO #:
Rock Hill SC 29732
Customer ID: 15060009
Attention:
Report #: 2023-00643
Project ID: Sludge -Wallace WWTP
Carbon Tetrachloride (TCLP)
SW-846 Method 8260D
<0.01 mg/L
01/24/2023
Chlorobenzene (TCLP)
SW-846 Method 8260D
<0.01 mg/L
01/24/2023
Chloroform (TCLP)
SW-846 Method 8260D
<0.01 mg/L
01/24/2023
Methyl ethyl ketone (TCLP)
SW-646 Method 8260D
<0.05 mg/L
01/24/2023
Tetrachloroethylene (TCLP)
SW-846 Method 8260D
<0.01 mg/L
01/24/2023
Trichloroethylene (TCLP)
SW-846 Method 8260D
<0.01 mg/L
01/24/2023
Vinyl Chloride (TCLP)
SW-846 Method 8260D
<0.01 mg/L
01/24/2023
RCI
Cyanide
SM 4500 CN D-2016
<1 mg/kg
01/12/2023
Sulfide
SM 4500 S D
<0.05 mg/kg
01 /19/2023
Analyzed outside of hold time.
Ignitability
SW 846 method 1010
>158 °F
01/17/2023
Sludge Residuals
Aluminum
EPA 200.7, Rev. 4.4, 1994
8600 mg/kg
01/16/2023
Arsenic
EPA 200.7, Rev. 4.4, 1994
20.7 mg/kg
01/16/2023
Cadmium
EPA 200.7, Rev. 4.4. 1994
<15.978 mg/kg
01/16/2023
Calcium
EPA 2D0.7, Rev. 4.4, 1994
27400 mg/kg
01/16/2023
Chromium
EPA 200.7, Rev. 4.4,1994
28.2 mg/kg
01/16/2023
Copper
EPA 200.7, Rev. 4.4, 1994
790 mg/kg
01/16/2023
Lead
EPA 200.7, Rev. 4.4, 1994
35.9 mg/kg
01/16/2023
Magnesium
EPA 200.7. Rev. 4.4, 1994
4580 mg/kg
01/16/2023
Molybdenum
EPA 200.7, Rev. 4.4. 1994
<15.978 mg/kg
01/17/2023
Nickel
EPA 200.7, Rev. 4.4, 1994
20.0 mg/kg
01/16/2023
Potassium
EPA 200.7. Rev. 4.4, 1994
5060 mg/kg
01/16/2023
Selenium
EPA 200.7, Rev. 4.4, 1994
<15.978 mg/kg
01/16/2023
Sodium
EPA 200.7, Rev. 4.4, 1994
5500 mg/kg
01/16/2023
Nitrate+Nitrite-Nitrogen
EPA 353.2
2440 mg/kg
01/12/2023
Total Solids (%)
SM 2540 8
2,71 %
01/11 /2023
Ammonia Nitrogen
SM 4500 NH3 C-2011
858 mg/kg
01/10/2023
Total Kjeldahl Nitrogen (TKN)
SM 4500 Norg B-2011
47000 mg/kg
01/11/2023
Report #:: 2023-00643
0- 1 '1 n

:enviroe-hhem
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 - 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.584-3 Lab/Fax
[e-mail]
Branch Residuals/Bob Branch Date of Report: Feb 01, 2023
1735 Heckle Blvd Suite 103-291 Customer PO #:
Rock Hill SC 29732 Customer ID: 15060009
Attention: Report #: 2023-00643
Project ID: Sludge -Wallace WWTP
Total Phosphorus SM 4500 P (F-H)-2011 19500 mg/kg 01/17/2023
pH SW B46 Method 9045D 6.35 units 01/20/2023
Result estimated. Analyzed out of 15 minutes hold time.
Mercury
SW-8467471B
0.915mg/kg
01/13/2023
TCLP Metals
Arsenic (TCLP)
EPA 2007, Rev 44, 1994
<1.0mg/L
01/17/2023
Barium (TCLP)
EPA 2007,Rev 44.1994
<1.0mg/L
01/17/2023
Cadmium (TCLP)
EPA 200 7, Rev 4 4, 1994
<1.0 mg/L
01/17/2023
Chromium (TCLP)
EPA 2007,Rev 44, 1994
<1.0mg/L
01/17/2023
Lead (TCLP)
EPA 200.7, Rev 4 4, 1994
<1.O mg/L
01/17/2023
Selenium (TCLP)
EPA 200.7, Rev. 4 4. 1994
<1.Omg/L
01/17/2023
Silver (TCLP)
EPA 200.7, Rev 4 4, 1994
<1.0 mg/L
01/17/2023
Mercury (TCLP)
EPA245.1
<0.0002 mg/L
01/27/2023
Lab ID Sample ID:
Collect Date/Time
Matrix Sampled by
23-01572 Site: Sludge 1
1/10/2023 11:25 AM
Solid/Sludge
Test
Method
Results
Date Analyzed
Total Solids (%) SM 2540 B 2.97 % 01 /11 /2023
Fecal Density SM 9221C E-2014 1112 MPN/g 01/10/2023
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
23-01573 Site: Sludge 2 1/10/2023 11:25 AM Solid/Sludge
Test Method Results Date Analyzed
Total Solids (%) SM 2540 B 2.85 % 01/11/2023
Fecal Density SM 9221C E-2014 1193 MPN/g 01/10/2023
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
23-01574 Site: Sludge 3 1/10/2023 11:25 AM Solid/Sludge
Test Method Results Date Analyzed
Total Solids (%) SM 2540 a 2.84 % 01 /11 /2023
Fecal Density SM 9221C E-2014 1726 MPN/g 01/10/2023
Report #:: 2023-00643 P- 1 of d

:enviroehemt]i
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab ° 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 ' 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 ` 910.347.5843 Lab/Fax
[e-mail]
Branch Residuals/Bob Branch Date of Report: Feb 01, 2023
1735 Heckle Blvd Suite 103-291 Customer PO #:
Rock Hill SC 29732 Customer ID: 15060009
Attention: Report #: 2023-00643
Project ID: Sludge -Wallace WWTP
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
23-01575 Site: Sludge 4 1/10/2023 11:25 AM Solid/Sludge
Test Method Results Date Analyzed
Total Solids (%) SM 2540 B 3.09 % 01/11/2023
Fecal Density SM 9221C E-2014 1068 MPN/g 01/10/2023
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
23-01576 Site: Sludge 5 1/10/2023 11:25 AM Solid/Sludge
Test Method Results Date Analyzed
Total Solids (%) SM 2540 B 2.94 % 01/11/2023
Fecal Density SM 9221C E-2014 375MPN/g 01/10/2023
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
23-01577 Site: Sludge 6 1/10/2023 11:25 AM Solid/Sludge
Test Method Results Date Analyzed
Total Solids (%) SM 2540 B 3.07 % 01/11/2023
Fecal Density SM 9221C E-2014 750 MPN/g 01/10/2023
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
23-01578 Site: Sludge 7 1/10/2023 11:25 AM Solid/Sludge
Test Method Results Date Analyzed
Total Solids (%) SM 2540 B 3.00 % 01/11/2023
Fecal Density SM 9221C E-2014 1134 MPN/g 01/10/2023
Comment: Surrogate DBA on column 2 Method 8081 manually integrated due to sample matrix." Sludge
residual r sults, except pH, reported on a dry weight basis. pH reported on an as received basis.
r
Reviewed by: - t lei
Report # 2023.00643 ❑, .,., A -r A

Environmental Chemist, Inc., Wilmington, NC Lab ##94
6602 Windmill Way
Wilmington, NC 284D5
910.392.D223
Sample Receipt Checklist
Client( -,a J�� ►..Lx L
---- - -- iu�s Date: � O
-.. a Report Numb:;, 2023 00lo�—
lit of s�,nlple:
FoYES -Tp
ECHEM Pickirpl Client Delivr: p,, ❑ OJT [�_ hecil_k ❑ i
--
❑ ''r`ES
Nr�
_
Cl
—_l_ _ ler ❑
f 1/<+. 1. 4"lore custody seals present on the cooler?-- -- --
Original temperature
NO
upon
ere N/A 1_. If custody Se315 :: present, � -- �— --
, were they intact/unbroken?
receipt "C —
`
How temperature taken: ❑ Temperature — Corrected temperature upon, receipt - — ,c
-. __---. Blank Against Mottles --�--- -
IR Gun ID.
Thornas Traceable
S/N 210886869 —-------
---clot
IR Gun Correction Fa °C: 0 p
YES
YES
❑ NO
❑ NO
3.-If temperature of cooler exceeded VC, was Project N119r./QA notified?
YES
❑ NO
( 4. Were proper custody procedures (relinquished/received) follc ed?
5.
Were sample ID's listed on the COC? ----`�
YES
❑ NO
—
6. Were samples ID's listed on sample containers?
YES
❑ NO
_
7. Were collection date and time listed on the COC?
YES
❑ NO
8. Were tests to be performed listed on the COC?
YES
❑ NO
9. Did samples arrive in proper rontainers for earh test?
YES
�( YES
❑ NO
10. Did samples arrive in good condition for each test? — —
❑ NU
11. Was adequate sample volume available'?' -`-- _--
YES
❑
❑ NO
12, Were samples received within proper holding time for requested tests?
YES
❑ NO
13. Were acid preserved samples received at a off of <2?
❑ _ YES _
D
❑ NO
i
14. Were cyanide samples received at a pH>12?
YES
D NO
15. Were sulfide samples received at a pi-1 >95—
❑ YES
❑
❑ NO
16, Were NH3 TKN Phi -�
/ / nol received at a chlorine residual of <0.S rr?/L?
YES
❑ YES
❑ NO
❑
17. Were Sulfide/Cyanide received at a chi lorine residual of <0-
_
NO
18. Were orthophosphate samples filtered in the field within 15 minutes?
r OC/Volailles uirp
_ pii chr'cked ai timenf analysis and recorded an the benchshnet
Bacteria samples ire F checked for Chlorine at time of analysis and recorded on the benchsheet
Sample Preservation: (Must be completed for any sample(s) incorrectly
Sarr,p)e(s) - y preserved or with headspace)
were received incorrectly preserved and were adjusted accordingly
by adding (circle one): H,SO� HNO3 HCI NaOH
rime of preservation: __— If rnore than one preservative is needed notate 1 .::,, e In Con?menCS below Note: ! i�. cUst'omer Ser.'ir- In'niedotel f-.r inCorre tl' r--. ----
es. Obtain
P y ".rid sa(nl;i Y a
nDatj' the sidt? fats Ir dlre_t?l ;o a,t%iyZed by the custufiler. Vdi10 :?s nOtiii>r I '
J, Gate are , ,Irr,:? _
Velatiles Sample(s) — were received with headspace
COMMENTS:
DOC, QA.002 Rev 1

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Facility:
Triple S Farms
Source:
Wallace WWTP
Location:
Wallace, North Carolina
Contractor:
Triple S Farms
Type of Analysis:
Wallace WWTP
Report No:
WL 2-2023-08640
Date Sampled:
5/2/2023 Type of Stabilization: Lime
Date Reported:
6/1/2023
Reporting Period:
2nd Quarter 2023
Parameter
%
PPM
Dry Weight
EPA
Monthly Limits
Solids*
2.80
Nitrogen (TKN)*
5.310
53,100.000
Phosphorus
0.082
819.000
Potassium
0.389
3,890.000
Sulfur
0.000
Calcium
3.470
34,700.000
Magnesium
0.349
3,490.000
Sodium
0.504
5,040.000
Iron
---
Aluminum
---
7,500.000
Manganese
---
Copper
---
718.000
1,500
Zinc
---
1,140.000
2,800
Ammonia Nitrogen*
0.157
1,570.000
Nitrate N / Nitrite N*
---
36.400
Cadmium
---
35.000
39
Chromium
---
35.000
1,200
Nickel
---
35.000
420
Lead
---
36.800
300
Arsenic
---
35.000
41
Mercury
---
0.636
17
Selenium
---
35.000
100
pH
7.860
Calcium Carbonate Eq. (est)
0.000
Organic Nitrogen
5.153
Molybdenum
---
35.000
75
Chloride
---
Boron
Available P2O5
Specific Gravity
8.340

Wallace WWTP
Wallace WWTP
Wallace, North Carolina
Triple S Farms
2nd Quarter 2023
Date Reported: 6/1/2023
Report No: WL 2-2023-08640
Note All Units in Pounds Per Dry Ton
Macro Nutrients
PAN Surf.
32.561
PAN Inj.
34.131
P
1.638
K
7.780
Lime (estimated)
t 0.000
Secondary Nutrients
Calcium
69.400
Magnesium
6.980
Sodium
10.080
SAR
1.152
Chloride
0.000
Iron
0.000
Alumium
15.000
Manganese
0.000
Boron
0.000
Sulfur
0.000
Physical Characteristics
% Solids
2.80
pH
7.860
Min Rate
0.300
Metals
Arsenic
0.070
Cadmium
0.070
Chromium
0.070
Copper
1.436
Lead
0.074
Mercury
0.001
Molybdenum
0.070
Nickel
0.070
Seleniun
0.070
Zinc
2.280

r: - -. -owl
nvirochem
�5lf•
ANALYTICAL $ CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 + 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
infoiu environmentalchemists.com
Branch Residuals/Bob Branch
Date of Report: Jun 01, 2023
1735 Heckle Blvd -Suite 103-291
Customer PO #:
Rock Hill SC 29732
Customer ID: 15060009
Attention:
Report #: 2023-08640
Project ID: Sludge -Wallace WWTP
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
23-21730 Site: Sludge
5/2/2023
Solid/Sludge Sean Pistorino
Test
Method
Results
Date Analyzed
Sludge Residuals
Aluminum
EPA 200.7, Rev. 4.4, 1994
7500 mg/kg
05/24/2023
Arsenic
EPA 200.7, Rev. 4.4, 1994
<35.0 mg/kg
05/24/2023
Cadmium
EPA 200.7. Rev. 4 4, 1994
<35.0 mg/kg
05/24/2023
Calcium
EPA 2001, Rev. 4.4. 1994
34700 mg/kg
05/24/2023
Chromium
EPA 200.7, Rev 4.4, 1994
<35.0mglkg
05/24/2023
Copper
EPA 200.7. Rev 4.4, 1994
718 mg/kg
05/24/2023
Lead
EPA 200 7, Rev 4 4, 1994
36.8 mg/kg
05/24/2023
Magnesium
EPA 200.7. Rev 4 4, 1994
3490 mg/kg
05/24/2023
Molybdenum
EPA 200.7. Rev 4 4 1994
<35.0 mg/kg
05/24/2023
Nickel
EPA 200.7. Rev 4 4 1994
<35.0 mg/kg
05/24/2023
Potassium
EPA 2C0.7, Rev 4 4 1994
3890 mg/kg
05/24/2023
Selenium
EPA 200.7. Rev 4 4. 1994
<35.0 mg/kg
05/24/2023
Sodium
EPA 200.7, Rev 4 4. 1994
5040 mg/kg
05/24/2023
Zinc
EPA 200.7, Rev 4.4, 1994
1140 mg/kg
05/24/2023
Nitrate+Nitrite-Nitrogen
EPA353.2
36.4mg/kg
05/03/2023
Total Solids (%)
SM 2540 B
2.80 %
05/03/2023
Ammonia Nitrogen
SM 4500 NH3 C-2011
1570 mg/kg
05/03/2023
Total Kjeldahl Nitrogen (TKN)
SM 4500 Norg B-2011
53100 mg/kg
05/03/2023
Total Phosphorus
SM 4500 P (F-H)-2011
819 mg/kg
05/11 /2023
pH SW 846 Method 9045D
Result estimated. Analyzed out of 15 minutes hold time.
7.86 units
05/08/2023
Mercury SW-8467471 B 0.636mg/kg 05/19/2023
Comment: Results, except pH, reported on a dry weight basis. pH reported on an as received basis.
Reviewed by:� `
Report #:. 2023.08e40
Pape 1 of 1

Environmental Chemist, Inc., Wilmington, NC Lab #94
Sample Receipt Checklist
6602 Windmill Way
Wilmington, NC 28405
910.392.0223
Client: f C'n e ks'IAL.&Date: 5 Z Report Number: - O64
Receipt of sample: Echem Pick up PIL Client Delivery ❑ UPS ❑ FeclEx ❑ Other ❑
❑ YES
10 NO
N/A
1. Were custody seals present on the cooler?
❑ YES
❑ NO
N/A
2. If custody seals were present, were they intact/unbroken?
Original temperature upon re P.n °C Corrected temperature upon receipt °C
How temperature taken: ❑ Temperature Blank N Against Bottles
IR Gun ID: Thomas Traceable S/N 192511657 IR Gun Correction Factor °C: 0.0
❑ YES
❑ NO
3. If temperature of cooler exceeded 6°C, was Project Mgr./QA notified?
YES
❑ NO
4. Were proper custody procedures (relinquished/received) followed?
YES
❑ NO
S. Were sample ID's listed on the COC?
YES
❑ NO
6. Were samples ID's listed on sample containers?
HL YES
❑ NO
7. Were collection date and time listed on the COC?
YES
❑ NO
8. Were tests to be performed listed on the COC?
YES
❑ NO
9. Did samples arrive in proper containers for each test?
YES
❑ NO
10. Did samples arrive in good condition for each test?
bk YES
❑ NO
11. Was adequate sample volume available?'
YES
❑ NO
12. Were samples received within proper holding time for requested tests?
❑ YES
❑ NO
13. Were acid preserved samples received at a pH of <2?
❑ YES 113
NO
14. Were cyanide samples received at a pH >12?
❑ YES
❑ NO
15. Were sulfide samples received at a pH >9?
❑ YES
❑ NO
16. Were NH3/TKN/Phenol received at a chlorine residual of <0.5 m/L? **
❑ YES
❑ NO
17. Were Sulfide/Cyanide received at a chlorine residual of <0.5 m/L?
❑ YES
❑ NO 1
18. Were orthophosphate samples filtered in field within 15 minutes?
* TOC/Volatiles are pH checked at time of analysis and recorded on the benchsheet.
** Bacteria samples are checked for Chlorine at time of analysis and recorded on the benchsheet.
Sample Preservation (Must be completed for any sample(s) incorrectly preserved or with headspace)
Sample(s) were received incorrectly preserved and were adjusted accordingly
by adding (circle one): H2SO4 HNO3 HCl NaOH
Time of preservation: If more than one preservative is needed, notate in comments below
Note: Notify customer service immediately for incorrectly preserved samples Obtain a new sample or
notify the state lab if directed to analyzed by the customer. Who was notified, date and time: _
Volatiles Sample(s) were received with headspace
COMMENTS:
DOC.OA.002 Rev 1

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Facility:
Source:
Location:
Contractor:
Type of Analysis:
Report No:
Date Sampled:
Date Reported:
Reporting Period
Triple S Farms
Wallace WWTP
Wallace, North Carolina
Triple S Farms
Wallace WWTP
WL 3-2023-14447
7/11/2023 Type of Stabilization: Non
10/10/2023
3rd Quarter 2023
Parameter
%
PPM
Dry Weight
EPA
Monthly Limits
Solids*
2.41
Nitrogen (TKN)*
6.050
60,500.000
Phosphorus
1.820
18,200.000
Potassium
0.302
3,020.000
Sulfur
0.000
Calcium
2.700
27,000.000
Magnesium
0.318
3,180.000
Sodium
0.531
5,310.000
Iron
---
Aluminum
---
8,460.000
Manganese
---
Copper
---
755.000
1,500
Zinc
---
1,340.000
2,800
Ammonia Nitrogen*
0.000
4.150
Nitrate N / Nitrite N*
---
15.900
Cadmium
---
38.300
39
Chromium
---
38.300
1,200
Nickel
---
38.300
420
Lead
---
38.300
300
Arsenic
---
19.100
41
Mercury
---
0.718
17
Selenium
---
38.300
100
pH
7.540
Calcium Carbonate Eq. (est)
0.000
Organic Nitrogen
6.050
Molybdenum
---
38.300
75
Chloride
---
Boron
Available P2O5
Specific Gravity
8.340

Wallace WWTP
Wallace WWTP
Wallace, North Carolina
Triple S Farms
3rd Quarter 2023
Date Reported: 10/10/2023 Report No: WL 3-2023-14447
Note All Units in Pounds Per Dry Ton
Macro Nutrients Physical Characteristics
PAN Surf.
36.333
PAN Inj.
36.338
P
36.400
K
6.040
Lime (estimated)
0.000
Secondary Nutrients
Calcium
54.000
Magnesium
6.360
Sodium
10.620
SAR
1.261
Chloride
0.000
Iron
0.000
Alumium
16.920
Manganese
0.000
Boron
0.000
Sulfur
0.000
% Solids
2.41
pH
7.540
Min Rate
0.300
Metals
Arsenic
0.038
Cadmium
0.077
Chromium
0.077
Copper
1.510
Lead
0.077
Mercury
0.001
Molybdenum
0.077
Nickel
0.077
Selemun
0.077
Zinc
2.680

rp"o-7 7:,0"7 Environmental Chemists, Inc.
envirochem 16602 Windmill Way, Wilmington, NC 28405 ' 910392.0223 Lab ' 910392.4424 Fax
® 710 Bowsertown Road, Manteo, NC 27954 ' 252.4735702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 ' 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS [e-mail]
Branch Residuals/Bob Branch
Date of Report: Oct 10, 2023
1735 Heckle Blvd Suite 103-291
Customer PO M
Rock Hill SC 29732
Customer ID: 15060009
Attention:
Report M 2023-14447
Project ID: Sludge -Wallace WWTP
Lab ID Sample ID:
Collect DatelTime Matrix Sampled by
23-35949 Site: Sludge
7/11/2023
9:35 AM Solid/Sludge Sean Pistorino
Test
Method
Results Date Analyzed
Sludge Residuals
Aluminum
EPA 200.7, Rev. 4.4. 1994
8460 mg/kg
08/01/2023
Cadmium
EPA 200.7, Rev. 4.4, 1994
<38.3 mg/kg
08/01/2023
Calcium
EPA 200.7. Rev. 4.4, 1994
27000 mg/kg
08/01/2023
Chromium
EPA 200.7. Rev. 4.4.1994
<38.3 mg/kg
08/01/2023
Copper
EPA 200.7. Rev. 4.4, 1994
755 mg/kg
08101 /2023
Lead
EPA 200.7, Rev. 4.4, 1994
<38.3 mg/kg
08/01/2023
Magnesium
EPA 200 7, Rev 4 4, 1994
3180 mg/kg
08/01/2023
Molybdenum
EPA 200.7, Rev 4 4, 1994
<38.3 mg/kg
08/01/2023
Nickel
EPA 200.7, Rev 4 4, 1904
<38.3 mg/kg
08/01/2023
Potassium
EPA 200.7, Rev, 4A, 1994
3020 mg/kg
08/01/2023
Selenium
EPA 200.7, Rev.4.4, 1994
<38.3 mg/kg
08/01/2023
Sodium
EPA 200.7. Rev. 4.4,1994
5310 mg/kg
08/16/2023
Zinc
EPA 200.7, Rev. 4.4, 1994
1340 mg/kg
08/01/2023
Nitrate+Nitrite-Nitrogen
EPA353.2
15.9mg/kg
07/18/2023
Total Solids (%)
SM 2540 8
2.41 %
07/14/2023
Ammonia Nitrogen
SM 4500 NH3 C-2011
<4.15 mg/kg
07/18/2023
Total Kjeldahl Nitrogen (TKN)
SM 4500 Norg &2011
60500 mg/kg
07/19/2023
Total Phosphorus
SM 4500 P (F-H)•2011
18200 mg/kg
07/25/2023
pH
SW 846 Method 90450
7.54 units
07/21/2023
Result estimated Analyzed out of 15 minutes hold time
Mercury SW-846 7471 a <0.718 mg/kg 07/31 /2023
Lab ID Sample ID:
23-35949A Site: Sludge
Collect Date/Time Matrix Sampled by
7/11/2023 9.35 AM Solid/Sludge Sean Pistodno
Test Method Results Date Analyzed
Arsenic
EPA 200.7, Rev. 4 4, 1994
<19.1 mg/kg 09/28/2023
Report #:: 2023-14447 Page 1 of 2

,:nviroehem
ANALYTICAL & CONSULTING CHEMISTS
Branch Residuals/Bob Branch
1735 Heckle Blvd Suite 103-291
Rock Hill SC 29732
Attention:
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 ' 910.392.0223 Lab ' 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 ' 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 ' 910.347.5843 Lab/Fax
[e-mail]
Date of Report: Oct 10, 2023
Customer PO M
Customer ID: 15060009
Report M 2023-14447
Project ID: Sludge -Wallace WWTP
Comment: Sludge residuals, except pH, reported on a dry weight basis. pH reported on an as received basis.
Reviewed by:9.J�CtL11
ReportA . 2023-14447 Page 2 of 2

Environmental Chemist, Inc., Wilmington, NC Lab #94
Sample Receipt Checklist
6602 Windmill Way
Wilmington, NC 28405
910.392.0223
Client: CA4 2 E;S Date � I � Report Number: _ 2023- ) 44n
Receipt of sample: ECHEM Pickup Client Delivery ❑
JUPS ❑ FedEx ❑ Other ❑
❑ YES
113 NO IN
N/A
1. Were custody seals present on the cooler?
❑ YES
1113 NO 119
N/A
2. If custody seals were present, were they intact/unbroken?
Original temperature upon receipt
°C Corrected temperature upon receipt °C
How temperature taken: ❑ Temperature Blank 9 Against Bottles
IR Gun ID: Thomas Traceable S/N 210886869 IR Gun Correction Factor °C: 0.0
© YES
❑ NO
3. If temperature of cooler exceeded 6°C, was Project Mgr./QA notified?
® YES
❑ NO
4. Were proper custody procedures (relinquished/received) followed?
® YES
❑ NO
5. Were sample ID's listed on the COC?
19 YES
❑ NO
6. Were samples ID's listed on sample containers?
® YES
113 NO
7. Were collection date and time listed on the COC?
® YES
113 NO
8. Were tests to be performed listed on the COC?
® YES
113 NO
9. Did samples arrive in proper containers for each test?
® YES
113 NO
10. Did samples arrive in good condition for each test?
® YES
❑ NO
11. Was adequate sample volume available?'
® YES
C] NO
12. Were samples received within proper holding time for requested tests?
❑ YES
❑ NO
13. Were acid preserved samples received at a pH of <2?
❑ YES
❑ NO
14. Were cyanide samples received at a pH >12?
❑ YES
❑ NO
15. Were sulfide samples received at a pH >9?
❑ YES
❑ NO
16. Were NH3/TKN/Phenol received at a chlorine residual of <0.5 m/L? **
❑ YES
❑ NO
17. Were Sulfide/Cyanide received at a chlorine residual of <0.5 m/L?
❑ YES
❑ NO
18. Were orthophosphate samples filtered in the field within 15 minutes?
* TOC/Volatiles are pH checked at time of analysis and recorded on the benchsheet.
** Bacteria samples are checked for Chlorine at time of analysis and recorded on the benchsheet.
Sample Preservation: (Must be completed for any sample(s) incorrectly preserved or with headspace)
Sample(s) were received incorrectly preserved and were adjusted accordingly
by adding (circle one): H2SO4 HNO3 HCI NaOH
Time of preservation: If more than one preservative is needed, notate in comments below
Note: Notify customer service immediately for incorrectly preserved samples. Obtain a new sample or
notify the state lab if directed to analyzed by the customer. Who was notified, date and time:
Volatiles Sample(s) were received with headspace
COMMENTS:
DOC. QA.002 Rev 1

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Facility:
Triple S Farms
Source:
Wallace WWTP
Location:
Wallace, North Carolina
Contractor:
Triple S Farms
Type of Analysis:
Wallace WWTP
Report No:
WL 4-2023-22878
Date Sampled:
10/3/2023 Type of Stabilization: Lime
Date Reported:
10/24/2023
Reporting Period:
4th Quarter 2023
Parameter
%
PPM
Dry Weight
EPA
Monthly Limits
Solids
2.40
Nitrogen (TKN)
3.740
37,400.000
Phosphorus
1.490
14,900.000
Potassium
0.254
2,540.000
Sulfur
0.000
Calcium
11.800
118,000.000
Magnesium
0.318
3,180.000
Sodium
0.446
4,460.000
Iron
---
Aluminum
---
6,420.000
Manganese
---
Copper
---
579.000
1,500
Zinc
---
1,010.000
2,800
Ammonia Nitrogen
0.463
4,630.000
Nitrate N / Nitrite N
---
264.000
Cadmium
---
19.800
39
Chromium
---
23.400
1,200
Nickel
---
19.800
420
Lead
---
26.000
300
Arsenic
---
19.800
41
Mercury
---
0.763
17
Selenium
---
19.800
100
pH*
11.370
Calcium Carbonate Eq. (est)
0.000
Organic Nitrogen
3.277
Molybdenum
---
19.800
75
Chloride
---
Boron
Available P2O5
Specific Gravity
8.340

Wallace WWTP
Wallace WWTP
Wallace, North Carolina
Triple S Farms
4th Quarter 2023
Date Reported: 10/24/2023
Report No: WL 4-2023-22878
Note All Units in Pounds Per Dry Ton
Macro Nutrients
PAN Surf.
24.820
PAN Inj.
29.450
P
29.800
K
5.080
Lime (estimated)
0.000
Secondary Nutrients
Calcium
236.000
Magnesium
6.360
Sodium
8.920
SAR
0.541
Chloride
0.000
Iron
0.000
Alumium
12.840
Manganese
0.000
Boron
0.000
Sulfur
0.000
Physical Characteristics
% Solids
2.40
pH
11.370
Min Rate
0.300
Metals
Arsenic
0.040
Cadmium
0.040
Chromium
0.047
Copper
1.158
Lead
0.052
Mercury
0.002
Molybdenum
0.040
Nickel
0.040
Seleniun
0.040
Zinc
2.020

r"100-- - _. _0q7 Environmental Chemists, Inc.
• 6602 Windmill Way, Wilmington, NC 28405 . 910.392.0223 Lab . 910.392.4424 Fax
LhL
® 710 Bowsertown Road, Manteo, NC 27954 . 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 . 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS [e-mail]
Town of Wallace
Date of Report: Oct 24, 2023
316 E Murray Street
Customer PO #:
Wallace NC 28466
Customer ID: 09010063
Attention:
Report #: 2023-22878
Project ID: WWTP Sludge
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
23-55815 Site: Sludge
10/3/2023
9:40 AM Solid/Sludge Sean Pistorino
Test
Method
Results Date Analyzed
Sludge Residuals
Aluminum
EPA 200 7 Rev 4 4 1994
6420 mg/kg
10/18/2023
Arsenic
EPA 200 7 Rev 4 4 1994
<19.8 mg/kg
10/18/2023
Cadmium
EPA 200 7. Rev 4 4 1994
<19.8 mg/kg
10/09/2023
Calcium
EPA 200 7 Rev 4 4 1994
118000 mg/kg
10/18/2023
Chromium
EPA 200 7 Rev 4 4 1994
23.4 mg/kg
10/09/2023
Copper
EPA 200 7 Rev 4 4 1994
579 mg/kg
10/09/2023
Lead
EPA 200 7. Rev 4 4 1994
26.0 mg/kg
10/09/2023
Magnesium
EPA 200 7 Rev 4 4 1994
3180 mg/kg
10/09/2023
Molybdenum
EPA 200 7 Rev 4 4 1994
<19.8 mg/kg
10/09/2023
Nickel
EPA 200 7 Rev 4 4 1994
<19.8 mg/kg
10/09/2023
Potassium
EPA 200 7 Rev 4 4 1994
2540 mg/kg
10/09/2023
Selenium
EPA 200 7 Rev 44 1994
<19.8 mg/kg
10/09/2023
Sodium
EPA 200 7 Rev 4 4 1994
4460 mg/kg
10/09/2023
Zinc
EPA 200 7 Rev 4 4 1994
1010 mg/kg
10/09/2023
Nitrate+Nitrite-Nitrogen
EPA 353 2
264 mg/kg
10/09/2023
Total Solids (ova)
SM 2540 B
2.40 %
10/09/2023
Ammonia Nitrogen
SM 4500 NH3 C-2011
4630 mg/kg
10/09/2023
Total Keldahl Nitrogen (TKN)
SM 4500 Norg B-2011
37400 mg/kg
10/09/2023
Total Phosphorus
SM 4500 P (F-H).2011
14900 mg/kg
10/10/2023
pH
SW 846 Method 9045D
11.37 units
10/09/2023
Result estimated. Analyzed out of 15 minutes hold time
Mercury SW 846 7471 B <0.763 mg/kg 10/11 /2023
Comment: Results, except pH, reported on a dry weight basis. pH reported on an as received basis.
Reviewed by: _
U
Report 9- 2023-22878 Page 1 of 1

Environmental Chemist, Inc., Wilmington, NC Lab #94
Sample Receipt Checklist
6602 Windmill Way
Wilmington, NC 28405
910.392.0223
Client:_ JQ W I 1 Of WQAgCjPJ Date: Report Number: _ 2023-
Receipt of sample:
ECHEM Pickup Client Delivery ❑ IUPS ❑ FeclEx ❑ Other ❑
❑ YES
❑ NO
❑O N/A
Were custody seals present on the cooler?
❑ YES
113 NO
© N/A
2. If custody seals were present, were they intact/unbroken?
Original temperature upon receipt . I 'C Corrected temperature upon receipt °C
How temperature taken:
❑ Temperature Blank ❑O Against Bottles
IR Gun ID: Thomas Traceable S/N 210886869 IR Gun Correction Factor `C: 0.0
❑O YES
❑ NO
3. If temperature of cooler exceeded FC, was Project Mgr./CIA notified?
© YES
❑ NO
4. Were proper custody procedures (relinquished/received) followed?
© YES
❑ NO
5. Were sample ID's listed on the COC?
❑O YES
❑ NO
6. Were samples ID's listed on sample containers?
O YES
❑ NO
7. Were collection date and time listed on the COC?
❑x YES
O NO
8. Were tests to be performed listed on the COC?
0 YES
❑ NO
9. Did samples arrive in proper containers for each test?
© YES
❑ NO
10. Did samples arrive in good condition for each test?
® YES
❑ NO
11. Was adequate sample volume available?'
® YES
❑ NO
12. Were samples received within proper holding time for requested tests?
❑ YES
❑ NO
13. Were acid preserved samples received at a pH of <2?
❑ YES
❑ NO
14. Were cyanide samples received at a pH >12?
❑ YES ❑ NO
15. Were sulfide samples received at a pH >9?
❑ YES ❑ NO
16. Were NH3/TKN/Phenol received at a chlorine residual of <0.5 m/L? **
❑ YES ❑ NO
17. Were Sulfide/Cyanide received at a chlorine residual of <0.5 m/L?
❑ YES 113 NO
18. Were orthophosphate samples filtered in the field within 15 minutes?
* TOC/Volatiles are pH checked at time of analysis and recorded on the benchsheet.
** Bacteria samples are checked
for Chlorine at time of analysis and recorded on the benchsheet.
Sample Preservation:
(Must be completed for any sample(s) incorrectly preserved or with headspace)
Sample(s)
were received incorrectly preserved and were adjusted accordingly
by adding (circle one):
1-12SO4 HNO3 HCI NaOH
Time of preservation:
If more than one preservative is needed, notate in comments below
Note: Notify customer service immediately for incorrectly preserved samples. obtain a new sample or
notify the state lab if directed to analyzed by the customer. Who was notified, date and time:
Volatiles Sample(s)
were received with headspace
COMMENTS:
DOC. CIA.002 Rev 1

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Facility:
Source:
Location:
Contractor:
Type of Analysis:
Report No:
Date Sampled:
Date Reported:
Reporting Period:
Town of Warsaw
Warsaw WWTP
Warsaw, North Carolina
Triple S Farms & Cleaning, Inc
Wastewater Treatment Plant
WS1 2023-12762
6/21/2023
7/24/2023
Normal Annual 2023
Parameter
%
PPM
Dry Weight
EPA
Monthly Limits
Solids
1.130
Nitrogen (TKN)
6.720
67,200.000
Phosphorus
2.710
27,100.000
Potassium
0.622
6,220.000
Sulfur
0.000
Calcium
3.580
35,800.000
Magnesium
0.244
2,440.000
Sodium
5.100
51,000.000
Iron
---
Aluminum
---
6,640.000
Manganese
---
Copper
---
395.000
1,500
Zinc
---
784.000
2,800
Ammonia Nitrogen
0.127
1,270.000
Nitrate N / Nitrite N
---
15,000.000
Cadmium
---
41.200
85
Chromium
---
41.200
1,200
Nickel
---
41.200
420
Lead
---
51.200
300
Arsenic
---
41.200
75
Mercury
---
1.690
17
Selenium
---
41.200
100
pH
7.210
Calcium Carbonate Eq. (est)
0.000
Organic Nitrogen
6.593
Molybdenum
---
41.200
75
Chloride
---
Boron
Available P2O5
Specific Gravity
8.340

Wastewater Treatment Plant
Warsaw WWTP
Warsaw, North Carolina
Triple S Farms & Cleaning, Inc
Normal Annual 2023
Date Reported: 7/24/2023 Report No: WS1 2023-1276,'
Note All Units in Pounds Per Dry Ton
Macro Nutrients Physical Characteristics
PAN Surf.
70.828
PAN Inj.
72.098
P
54.200
K
12.440
Lime (estimated)
0.000
Secondary Nutrients
Calcium
71.600
Magnesium
4.880
Sodium
102.000
SAR
7.466
Chloride
0.000
Iron
0.000
Alumium
13.280
Manganese
0.000
Boron
0.000
Sulfur
0.000
% Solids
1.13
pH
7.210
Min Rate
0.300
Metals
Arsenic
0.082
Cadmium
0.082
Chromium
0.082
Copper
0.790
Lead
0.102
Mercury
0.003
Molybdenum
0.082
Nickel
0.082
Seleniun
0.082
Zinc
1.568

r,pm,-. qqql
Environmental Chemists,
Inc.
envirochem
6602 Windmill Way,
Wilmington, NC 28405 • 910.392.0223 Lab - 910.392.4424 Fax
i3w
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 -h 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS
[e-mail]
Town of Warsaw
Date of Report: Jul 24, 2023
PO Box 464
Customer PO #:
Warsaw NC 28398
Customer ID: 09070029
Attention:
Report #: 2023-12762
Project ID: Sludge
Lab ID Sample ID:
Collect DatelTime Matrix Sampled by
23-31855 Site: Sludge
6/21/2023
9:10 AM Solid/Sludge Greg Hughes
Test
Method
Results Date Analyzed
Chlordane (TCLP)
SW-848 8081 a
<0.02 mg/L
06/30/2023
Endrin (TCLP)
SW-84680818
<0.0005mg/L
06/30/2023
Heptachlor (TCLP)
SW-846 8081 B
<0.0005 mg/L
06/30/2023
Heptachlor epoxide (TCLP)
SW-846 80818
<0.0005 mg/L
06/30/2023
Lindane (TCLP)
SW-846 80818
<0.0005 mg/L
06/30/2023
Methoxychlor (TCLP)
SW-646 8081 B
<0.0005 mg/L
06/30/2023
Toxaphene (TCLP)
SW-846 8081 B
<0.05 mg/L
06/30/2023
2,4, 5-TP (TCLP)
SW-848 8151 A
<0.003 mg/L
07/03/2023
2,4-D (TCLP)
SW-848 8151 A
<0.003 mg/L
07/03/2023
1,4-Dichiorobenzene(TCLP)
SW-8488270E
<0.050mg/L
07/03/2023
2,4,5-Trichlorophenol (TCLP)
SW-8468270E
<0.050mg/L
07/03/2023
2,4,6-Trichlorophenol (TCLP)
SW-846 8270 E
<0.050 mg/L
07/03/2023
2,4-Dinitrotoluene (TCLP)
SW-846 8270 E
<0.050 mg/L
07/03/2023
Cresol (TCLP)
SW-848 8270 E
<0.050 mg/L
07/03/2023
Hexachloro-1,3-butadiene (TCLP)
SW-846 8270 E
<0.050 mg/L
07/03/2023
Hexachlorobenzene (TCLP)
SW-846 8270 E
<0.050 mg/L
07/03/2023
Hexachloroethane (TCLP)
SW-846 8270 E
<0.050 mg/L
07/03/2023
m + p-Cresol (TCLP)
SW-846 8270 E
<0.050 mg/L
07/03/2023
Nitrobenzene (TCLP)
SW-846 8270 E
<0.050 mg/L
07/03/2023
o-Cresol (TCLP)
SW-846 8270 E
<0.050 mg/L
07/03/2023
Pentachlorophenol (TCLP)
SW-846 8270 E
<0.250 mg/L
07/03/2023
Pyridine (TCLP)
SW-846 8270 E
<0.050 mg/L
07/03/2023
1,1-Dichloroethylene (TCLP)
SW-846 Method 8260D
<0.01 mg/L
07/07/2023
1,2-Dichloroethane (TCLP)
Sw 846 Method 8260D
<0.01 mg/L
07/07/2023
Benzene (TCLP)
SW-845 Method 82e0D
<0.01 mg/L
07/07/2023
Carbon Tetrachloride (TCLP)
SW-846 Method 8260D
<0.01 mg/L
07/07/2023
Report L:: 2023-12702
Page 1 of 3

Environmental Chemists, Inc.
enviroehem
ANALYTICAL & CONSULTING CHEMISTS
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5943 Lab/Fax
infoaienvironmentalchemists.com
Town of Warsaw
Date of Report: Jul 24, 2023
PO Box 464
Customer PO #:
Warsaw NC
28398
Customer ID: 09070029
Attention:
Report #: 2023-12762
Project ID: Sludge
Chlorobenzene (TCLP)
SW-846 Method 8260D
<0.01 mg/L
07/07/2023
Chloroform (TCLP)
SW-846 Method 8260D
<0.01 mg/L
07/07/2023
Methyl ethyl ketone (TCLP)
SW-845 Method 8280D
0.17 mg/L
07/07/2023
Tetrachloroethylene (TCLP)
SW-846 Method 8260D
<0.01 mg/L
07/07/2023
Trichloroethylene (TCLP)
SW-846 Method 8260D
<0.01 mg/L
07/07/2023
Vinyl Chloride (TCLP)
SW-846 Method 8260D
<0.01 mglL
07/07/2023
RCI
Cyanide
SM 4500 CN D-2016
<1 mg/kg
07/03/2023
Sulfide
SM 4500 S D
<0.05 mg/kg
07/03/2023
Ignitability
SW 048 method 1010
>158 °F
07/20/2023
Sludge Residuals
Aluminum
EPA 200.7, Rev. 4.4,1994
6640 mg/kg
06/28/2023
Arsenic
EPA 200.7. Rev 4.4.1994
<41.2 mg/kg
06/28/2023
Cadmium
EPA 200.7, Rev. 4.4,1994
<41.2 mg/kg
06/28/2023
Calcium
EPA 200.7, Rev. 4.4, 1994
35800 mg/kg
06/28/2023
Chromium
EPA 200.7, Rev. 4.4.1994
<41.2 mg/kg
06/28/2023
Copper
EPA 200.7, Rev. 4.4, 1094
395 mg/kg
06/28/2023
Lead
EPA 200.7, Rev. 4 4, 1994
51.2 mg/kg
06/28/2023
Magnesium
EPA 200.7, Rev 4.4,1994
2440 mg/kg
06/28/2023
Molybdenum
EPA 200.7, Rev. 4.4, 1994
<41.2 mg/kg
06/28/2023
Nickel
EPA 200.7, Rev. 4.4, 1994
<41.2 mg/kg
06/28/2023
Potassium
EPA 200.7, Rev. 4.4, 1994
6220 mg/kg
06/28/2023
Selenium
EPA 200.7, Rev. 4.4, 1994
<41.2 mg/kg
06/28/2023
Sodium
EPA 200 7, Rev. 4.4, 1994
51000 mg/kg
06/28/2023
Zinc
EPA 200.7. Rev. 4.4. 1994
784 mg/kg
06/28/2023
Nitrate+Nitrite-Nitrogen
EPA 353.2
15000 mg/kg
06/22/2023
Total Solids (%)
SM 2540 a
1.13 %
06/23/2023
Ammonia Nitrogen
SM 4500 NH3 C-2011
1270 mg/kg
06/26/2023
Total Kjeldahl Nitrogen (TKN)
SM 4500 Norg 8-2011
67200 mg/kg
06/28/2023
Report 0: 2023-12762 Page 2 of 3

Town of Warsaw
PO Box 464
Warsaw
Attention:
Date of Report: Jul 24, 2023
Customer PO #:
NC 28398 Customer ID: 09070029
Report #: 2023-12762
Project ID: Sludge
Total Phosphorus SM 4500 P (F-H)-2011
pH SW 848 Method 9045D
Analyzed outside of 15 minute hold time.
Mercury
TCLP Metals
Arsenic (TCLP)
Barium (TCLP)
Cadmium (TCLP)
Chromium (TCLP)
Lead (TCLP)
Selenium (TCLP)
Silver (TCLP)
Mercury (TCLP)
SW-846 74718
EPA 200 7, Rev. 4.4. 1994
EPA 200.7. Rev. 4.4. 1994
EPA 2007, Rev. 4.4, 1994
EPA 200 7. Rev 4.4. 1994
EPA 200 7, Rev, 4.4,1994
EPA 200.7. Rev. 4.4,1994
EPA 200.7. Rev. 4.4.1994
EPA 245.1
27100 mg/kg
7.21 units
<1.69 mg/kg
<1.0 mg/L
<1.O mg/L
<1.0 mg/L
<1.0 mg/L
<1.0 mg/L
<1.0 mg/L
<1.0 mg/L
<0.0002 mg/L
Comment: Results, except pH, rep rted on a dry weight basis. pH reported on an as received basis.
Reviewed by: _ --ic
06/29/2023
07/21 /2023
06/29/2023
07/06/2023
07/06/2023
07/06/2023
07/06/2023
07/06/2023
07/06/2023
07/06/2023
06/30/2023
Report M. 2023-12782 Page 3 of 3

Environmental Chemist, Inc., Wilmington, NC Lab #94 6602 Windmill Way
Wilmington, NC 28405
910.392.0223
Sample Receipt Checklist
Client: • V v i i�� �( Date: LC 12J 123 Report Number: _ L)— I 1 �0 2-
Receipt of sample:
ECHEM Pickup K Client Delivery 13 1 UPS ❑ FedEx ❑ Other ❑
❑
YES
10
NO
N/A
Were custody seals present on the cooler?
❑
YES
C]
NO
N/A
L22.'
If custody seals were present, were they intact/unbroken?
Original temperature upon receipt "C Corrected temperature upon receipt
How temperature taken:
❑ Temperature Blank Against Bottles
IR Gun ID: Thomas Traceable S/N 210886869 IR Gun Correction Factor °C: 0.0
YES
❑
NO
3. If temperature of cooler exceeded 6°C, was Project Mgr./QA notified?
YES
❑
NO
4. Were proper custody procedures (relinquished/received) followed?
YES
❑
NO
S. Were sample ID's listed on the COC?
YES
❑
NO
6. Were samples ID's listed on sample containers?
A
YES
❑
NO
7. Were collection date and time listed on the COC?
YES
❑
NO
8. Were tests to be performed listed on the COC?
YES
❑
NO
9. Did samples arrive in proper containers for each test?
YES
❑
NO
10. Did samples arrive in good condition for each test?
YES
CI
NO
11. Was adequate sample volume available?'
YES
❑
NO
12. Were samples received within proper holding time for requested tests?
❑
YES
❑
NO
13. Were acid preserved samples received at a pH of <2?
❑
YES
❑
NO
14. Were cyanide samples received at a pH >12?
❑
YES
O
NO
15. Were sulfide samples received at a pH >9?'
❑
YES
❑
NO
16. Were NH3/TKN/Phenol received at a chlorine residual of <0.5 m/L? **
❑
YES
113
NO
17. Were Sulfide/Cyanide received at a chlorine residual of <0.5 m/L?
❑
YES
113
NO
18. Were orthophosphate samples filtered in the field within 15 minutes?
* TOC/Volatiles are pH checked at time of analysis and recorded on the benchsheet.
** Bacteria samples are checked for Chlorine at time of analysis and recorded on the benchsheet.
Sample Preservation: (Must be completed for any sample(s) incorrectly preserved or with headspace)
Sample(s) were received incorrectly preserved and were adjusted accordingly
by adding (circle one): H2SO4 HNO3 HCI NaOH
Time of preservation: If more than one preservative is needed, notate in comments below
Vote: Notify customer service immediately for incorrectly preserved samples. Obtain a new sample or
iotify the state lab if directed to analyzed by the customer. Who was notified, date and time:
Volatiles Sample(s) were received with heacisnarp
COMMENTS:
DOC. QA.002 Rev 1
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Facility:
Source:
Location:
Contractor:
Type of Analysis:
Report No:
Date Sampled:
Date Reported:
Reporting Period:
Town of Warsaw
Warsaw WWTP
Warsaw, North Carolina
Triple S Farms & Cleaning, Inc
Wastewater Treatment Plant
WS2 2023-29979
12/22/2023
1/15/2024
Annual 2 2023
Parameter
%
PPM
Dry Weight
EPA
Monthly Limits
Solids
1.780
Nitrogen (TKN)
0.783
7,830.000
Phosphorus
0.180
1,800.000
Potassium
0.240
2,400.000
Sulfur
0.000
Calcium
1.020
10,200.000
Magnesium
0.083
826.000
Sodium
2.120
21,200.000
Iron
---
Aluminum
---
3,940.000
Manganese
---
Copper
---
83.100
1,500
Zinc
---
370.000
2,800
Ammonia Nitrogen
0.275
2,750.000
Nitrate N / Nitrite N
---
24.400
Cadmium
---
12.900
85
Chromium
---
15.700
1,200
Nickel
---
12.900
420
Lead
---
12.900
300
Arsenic
---
12.900
75
Mercury
---
0.893
17
Selenium
---
12.900
100
pH
7.140
Calcium Carbonate Eq. (est)
0.000
Organic Nitrogen
0.508
Molybdenum
---
12.900
75
Chloride
---
Boron
Available P2O5
Specific Gravity
8.340

Wastewater Treatment Plant
Warsaw WWTP
Warsaw, North Carolina
Triple S Farms & Cleaning, Inc
Annual 2 2023
Date Reported: 1/15/2024 Report No: WS2 2023-2997�
Note All Units in Pounds Per Dry Ton
Macro Nutrients Physical Characteristics
PAN Surf.
5.847
PAN Inj.
8.597
P
3.600
K
4.800
Lime (estimated)
0.000
Secondary Nutrients
Calcium
20.400
Magnesium
1.652
Sodium
42.400
SAR
7.229
Chloride
0.000
Iron
0.000
Alumium
7.880
Manganese
0.000
Boron
0.000
Sulfur
0.000
% Solids
1.78
pH
7.140
Min Rate
0.300
Metals
Arsenic
0.026
Cadmium
0.026
Chromium
0.031
Copper
0.166
Lead
0.026
Mercury
0.002
Molybdenum
0.026
Nickel
0.026
Seleniun
0.026
Zinc
0.740

Environmental Chemists, Inc.
envirochem 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
" 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/ Fax
ANALYTICAL & CONSULTING CHEMISTS infota environmentalchemists.com
Town of Warsaw
Date of Report: Jan 29, 2024
PO Box 464
Customer PO #:
Warsaw NC 28398
Customer ID: 09070029
Attention:
Report #: 2023-29979
Project ID: Wastewater
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
23-72662 Site: Influent
12/22/2023
8:30 AM Solid/Sludge Greg Hughes
Test
Method
Results Date Analyzed
Chlordane (TCLP)
SW-846 8081 B
<0.02 mg/L
12/27/2023
Endrin (TCLP)
SW-848 8081 B
<0.0005 mg/L
12/27/2023
Heptachlor (TCLP)
SW-848 8081 B
<0.0005 mg/L
12/27/2023
Heptachlor epoxide (TCLP)
SW-846 8081 B
<0.0005 mg/L
12/27/2023
Lindane (TCLP)
SW-846 8081 B
<0.0005 mg/L
12/27/2023
Methoxychlor (TCLP)
SW-846 80818
<0.0005 mg/L
12/27/2023
Toxaphene (TCLP)
SW-846 8081 B
<0.05 mg/L
12/27/2023
2,4,5-TP (TCLP)
SW-846 8151 A
<0.003 mg/L
01/02/2024
2,4-D (TCLP)
SW-846 8151 A
<0.003 mg/L
01/02/2024
1,4-Dichlorobenzene (TCLP)
SW-8468270E
<0.050mg/L
01/03/2024
2,4,5-Thchlorophenol (TCLP)
SW-846 $270 E
<0.050 mg/L
01/03/2024
2,4,6-Trichlorophenol (TCLP)
SW-8468270E
<0.050mg/L
01/03/2024
2,4-Dinitrotoluene (TCLP)
SW-846 8270 E
<0.050 mg/L
01/03/2024
Cresol (TCLP)
SW-646 8270 E
<0.050 mg/L
01/03/2024
Hexachloro-1,3-butadiene(TCLP)
SW 8468270E
<0.050mg/L
01/03/2024
Hexachlorobenzene(TCLP)
SW 8468270E
<0.050mg/L
01/03/2024
Hexachloroethane (TCLP)
SW 846 8270 E
<0.050 mg/L
01/03/2024
m + p-Cresol (TCLP)
SW 846 8270 E
<0.050 mg/L
01/03/2024
Nitrobenzene (TCLP)
SW-8468270E
<0.050mg/L
01/03/2024
o-Cresol (TCLP)
SW-846 8270 E
<0.050 mg/L
01/03/2024
Pentachlorophenol (TCLP)
SW-8468270E
<0.250mg/L
01/03/2024
Pyridine (TCLP)
SW-8468270E
<0.050mg/L
01/03/2024
1,1-Dtchloroethylene (TCLP)
SW-846 Method 8260D
< 0.01 mg/L
12/29/2023
1,2-Dichloroethane (TCLP)
SW-846 Method 8260D
< 0.01 mg/L
12/29/2023
Benzene (TCLP)
SW-846 Method 8260D
< 0.01 mg/L
12/29/2023
Carbon Tetrachloride (TCLP)
SW-846 Method 8260D
< 0.01 mg/L
12/29/2023
ReportA 2023.29979
Pagel of 3

Environmental Chemists,
Inc.
' 1
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/
Fax
5M
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/ Fax
ANALYTICAL & CONSULTING CHEMISTS
info.u.enviromnentalcliemists.com
Town of Warsaw
Date of Report: Jan 29, 2024
PO Box 464
Customer PO #:
Warsaw NC 28398
Customer ID: 09070029
Attention:
Report #: 2023-29979
Project ID: Wastewater
Chlorobenzene (TCLP)
SW-846 Method 82WD < 0.01 mg/L
12/29/2023
Chloroform (TCLP)
SW-846 Method 8260D < 0.01 mg/L
12/29/2023
Methyl ethyl ketone (TCLP)
SW-846 Method 8260D < 0.05 mg/L
12/29/2023
Tetrachloroethylene (TCLP)
SW-846 Method 8260D < 0.01 mg/L
12/29/2023
Trichloroethylene (TCLP)
SW-846 Method 8260D < 0.01 mg/L
12/29/2023
Vinyl Chloride (TCLP)
SW-846 Method 8260D < 0.01 mg/L
12/29/2023
liTei
Cyanide
SM 4500 CN D-2016
2.05 mg/kg
12/29/2023
Sulfide
SM 4500 S D-2011
17.6 mg/kg
01/02/2024
Ignitability
SW 846 method 101a
>157 °F
01/05/2024
pH
SW 646 Method 9045D
7.14 units
01/16/2024
Result estimated Analyzed out of 15 minutes hold time
Sludge Residuals
Aluminum
CPA 200.7, Rev 4.4 1994
3940 mg/kg
01/02/2024
Arsenic
FPA 200.7, Rev 4.4, 1994
<12.9 mg/kg
12/29/2023
Cadmium
FPA 200.7, Rev. 4.4, 1994
<12.9 mg/kg
12/29/2023
Calcium
EPA 200.7. Rev. 4.4, 1994
10200 mg/kg
12/29/2023
Chromium
EPA 200.7, Rev. 4 4, 1994
15.7 mg/kg
12/29/2023
Copper
EPA 200.7, Rev. 4.4,1994
83.1 mg/kg
12/29/2023
Lead
EPA 200.7, Rev. 4.4, 1994
<12.9 mg/kg
12/29/2023
Magnesium
EPA 200.7, Rev. 4.4, 1994
826 mg/kg
12/29/2023
Molybdenum
EPA 200.7. Rev. 4 4,1994
<12.9 mg/kg
12/29/2023
Nickel
EPA 200.7, Rev. 4.4, 1994
<12.9 mg/kg
12/29/2023
Potassium
EPA 200.7, Rev. 4 4,1994
2400 mg/kg
01/02/2024
Selenium
EPA 200.7, Rev 4 4, 1994
<12.9 mg/kg
12/29/2023
Sodium
EPA 200.7, Rev 4 4, 1994
21200 mg/kg
01/03/2024
Zinc
EPA 200.7, Rev 4.4 1994
370 mg/kg
12/29/2023
Nitrate+Nitrite-Nitrogen
EPA 353.2
24.4 mg/kg
12/26/2023
Total Solids (%)
SM 2540 8
1.78 %
12/27/2023
Ammonia Nitrogen
SM 46CO NH3 C 2C11
2750 mg/kg
12/28/2023
Report 0:: 2023-29979 Page 2 of 3

Environmental Chemists, Inc.
envirochem 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab," Fax
A 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Labl Fax
ANALYTICAL & CONSULTING CHEMISTS infoia environmentalchemists.com
Town of Warsaw Date of Report: Jan 29, 2024
PO Box 464 Customer PO #:
Warsaw NC 28398 Customer ID: 09070029
Attention: Report #: 2023-29979
Project ID: Wastewater
Total Kjeldahl Nitrogen (TKN) SM 4500 Norg B-2011 7830 mg/kg 12/27/2023
Total Phosphorus SM 4500 P (F-H)-2011 1800 mg/kg 01/03/2024
Mercury SW-846 7471 B <0.893 mg/kg 12/29/2023
TCLP Metals
Arsenic (TCLP)
EPA 200 7 Rev 4 4, 1994
0.0 mg/L
12/29/2023
Barium (TCLP)
EPA 200 7 Rev 4 4. 1994
0.0 mg/L
12/29/2023
Cadmium (TCLP)
EPA 200 7 Rev 4 4. 1994
<1.0 mg/L
12/29/2023
Chromium (TCLP)
EPA 200 7 Rev 4 4. 1994
<1.0 mg/L
12/29/2023
Lead (TCLP)
EPA 200 7 Rev 4 4.1994
<1.0 mg/L
12/29/2023
Selenium (TCLP)
EPA 200 7 Rev 4 4.1994
<1.0 mg/L
12/29/2023
Silver (TCLP)
EPA zoo 7 Rev 4 4, 1994
0.0 mg/L
01/02/2024
Mercury (TCLP)
EPA 245 1
<0.0002 mg/L
12/28/2023
Comment: Sludge residuals reported on at dry weight basis. Revised to add pH result.
Reviewed by:V-, I (L �ao r-,
Report 8:: 2023-29979 Page 3 of 3

TOXICITY CHARACTERISTICS LEACHING PROCEDURE
(TCLP) ANALYSIS REPORTS

A TCLP ANALYSIS IS REQUIRED FOR THE FOLLOWING FACILITIES:
TOWN OF WALLACE
TOWN OF CLAYTON
ONWASA NORTHWEST REGIONAL
TCLP DATA IS REQUIRED ONCE PER PERNHT CYCLE
FOR THE OTHER FACILITIES

Waypointo.
ANALYTICAL
2/28/2023
Town Of Clayton
Salvador Valdiviezo
POB 879
Clayton, NC, 27528
Ref: Analytical Testing
Report Number: 23-039-0005
Project Description: Holding Tank 1
7621 whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Dear Salvador Valdiviezo:
Waypoint Analytical Virginia, Inc. received sample(s) on 2/8/2023 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Brandi Watson
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 1 of 10

Waypoint. 7621 0 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
ANALYTICAL www.waypointanalytical.com
Sample Summary Table
Report Number: 23-039-000S
Client Project Description: Holding Tank 1
Lab No
Client Sample ID
Matrix
Date Collected
Date Received
Method
Lab ID
60712
Holding Tank 1
TCLP
02/07/2023
02/08/2023
SW-1311
WP MTN
60712
Holding Tank 1
TCLP
02/07/2023
02/08/2023
8081A
WP MTN
60712
Holding Tank 1
TCLP
02/07/2023
02/08/2023
SW-1311 (ZHE)
WP MTN
60712
Holding Tank 1
TCLP
02/07/2023
02/08/2023
8151A
WP MTN
60712
Holding Tank 1
TCLP
02/07/2023
02/08/2023
6010D
WP MTN
60712
Holding Tank 1
TCLP
02/07/2023
02/08/2023
8260E
WP MTN
60712
Holding Tank 1
TCLP
02/07/2023
02/08/2023
8270C
WP MTN
60712
Holding Tank 1
TCLP
02/07/2023
02/08/2023
7470A
WP MTN
60713
Holding Tank 1
Solids
02/07/2023
02/08/2023
SW-9045C
WP MTN
60713
Holding Tank 1
Solids
02/07/2023
02/08/2023
SW-7.3.4
WP MTN
60713
Holding Tank 1
Solids
02/07/2023
02/08/2023
SW-7.3.3
WP MTN
60713
Holding Tank 1
Solids
02/07/2023
02/08/2023
ASTM D93-80
WP MTN
WP MTN - Memphis, TN: Waypoint Analytical -TN, Memphis, TN
Page 2 of 10

Waypointo
ANALYTICAL
46546
Town Of Clayton
Salvador Valdiviezo
POB 879
Clayton , NC 27528
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Project Holding Tank 1
Information :
Report Number: 23-039-0005 REPORT OFANAL YSIS
Report Date : 02/28/2023
Received : 02/08/2023
Brandi Watson
Lab No : 60712
Matrix: TCLP
Sample ID : Holding Tank 1
Sampled:
2/7/2023 0:00
Test
Results
Units
MOL
DF
Date / Time
By
Analytical
Analyzed
Method
TCLP Herbicide Extraction
Combined
1
02/21/23 15:00
HAW
SW-1311
TCLP Metals Extraction
Combined
1
02/21/23 15:00
HAW
SW-1311
TCLP Pesticide Extraction
Combined
1
02/21/23 15:00
HAW
SW-1311
TCLP SVOC Extraction
Combined
1
02/21/23 15:00
HAW
SW-1311
TCLP VOC ZHE Extraction
Combined
1
02/21/23 15:00
HAW
SW-1311 (ZHE)
Analytical Method: 6010D
Prep Batch(es):
L665549
02/22/23 12:55
Prep Method: 3015A
Test
Results
Units
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
TCLP Arsenic
<0.250
mg/L
0.250
1
02/22/23 21:48
BKN
L665772
TCLP Barium
<0.250
mg/L
0.250
1
02/22/23 21:48
BKN
L665772
TCLP Cadmium
<0.0500
mg/L
0.0500
1
02/22/23 21:48
BKN
L665772
TCLP Chromium
<0.100
mg/L
0.100
1
02/22/23 21:48
BKN
L665772
TCLP Lead
<0.100
mg/L
0.100
1
02/22/23 21:48
BKN
L665772
TCLP Selenium
<0.500
mg/L
0.500
1
02/22/23 21:48
BKN
L665772
TCLP Silver
<0.0500
mg/L
0.0500
1
02/22/23 21:48
BKN
L665772
Qualifiers/ DF Dilution Factor MQL Method Quantitation Limit
Definitions Q RPD >40% dual column results
Page 3 of 10

0
Waypoint.
7621 VJhitepine
Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
ANALYTICAL
www.waypointanalytical.com
46546
Town Of Clayton
Project Holding Tank 1
Salvador Valdiviezo
Report Date : 02/28/2023
POB 879
Information :
Received : 02/08/2023
Clayton , NC 27528
Brandi Watson
Report Number: 23-039-0005
REPORT OFANALYSIS
Lab No : 60712
Matrix: TCLP
Sample ID : Holding Tank 1
Sampled: 2/7/2023 0:00
Analytical Method: 7470A
Prep Batch(es):
L665719
02/23/23 08:12
Prep Method: 7470A
Test
Results
Units
MOL
DF Date / Time By
Analytical
Analyzed
Batch
TCLP Mercury
<0.0200
mg/L
0.0200
1 02/23/23 12:47 FDS
L665894
Analytical Method: 8081A
Prep Batch(es):
L66SS98
02/22/23 14:30
Prep Method: 3510C
Test
Results
Units
MOL
DF Date / Time By
Analytical
Analyzed
Batch
TCLP Endrin
<0.004000
mg/L
0.004000
10 02/24/23 07:20 VIC
L666158
TCLP gamma-BHC
<0.004000
mg/L
0.004000
10 02/24/23 07:20 VIC
L666158
TCLP Methoxychlor
<0.004000
mg/L
0.004000
10 02/24/23 07:20 VIC
L666158
TCLP Toxaphene
<0.03000
mg/L
0.03000
10 02/24/23 07:20 VIC
L666158
TCLP Chlordane
<0.02000
mg/L
0.02000
10 02/24/23 07:20 VIC
L666158
TCLP Heptachlor Epoxide
<0.004000
mg/L
0.004000
10 02/24/23 07:20 VIC
L666158
TCLP Heptachlor
<0.004000
mg/L
0.004000
10 02/24/23 07:20 VIC
L666158
Surrogate: Decachlorobiphenyl
57.33
Limits: 34-116% 10 02/24/23 07:20 VIC
L666158
Surrogate: Tetrachloro-m-xylene
47.90
Limits: 25-123% 10 02/24/23 07:20 VIC
L666158
Analytical Method: 8151A
Prep Batch(es):
L665659
02/22/23 17:30
Prep Method: 8151A
Test
Results
Units
MOL
DF Date / Time By
Analytical
Analyzed
Batch
TCLP 2,4-D
<0.0200
mg/L
0.0200
1 02/25/23 04:47 VIC
L666406
TCLP 2,4,5-TP (Silvex)
<0.0020
mg/L
0.0020
1 02/25/23 04:47 VIC
L666406
Surrogate: DCAA
80.80
Limits: 20-120% 1 02/25/23 04:47 VIC
L666406
Qualifiers/ OF Dilution Factor
MQL Method Quantitation Limit
Definitions Q RPD >40% dual column results
Page 4 of 10

a
Waypoint.
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
ANALYTICAL
www.waypointanalytical.com
46546
Town Of Clayton
Project
Holding Tank 1
Salvador Valdiviezo
Report Date : 02/28/2023
POB 879
Information :
Received
: 02/08/2023
Clayton , NC 27528
pp
d7/�zrL k�C1
Brandi Watson
Report Number: 23-039-0005
REPORT OFANAL YSIS
Lab No : 60712
Matrix: TCLP
Sample ID: Holding Tank 1
Sampled: 2/7/2023 0:00
Analytical Method: 8260B
Prep Batch(es):
L665734 02/22/23 11:23
Prep Method: 5030B
Test
Results
Units
MOL
DF Date / Time By
Analytical
Analyzed
Batch
TCLP Benzene
<0.100
mg/L
0.100
10 02/22/23 16:37 ELM
L665735
TCLP Carbon Tetrachloride
<0.100
mg/L
0.100
10 02/22/23 16:37 ELM
L665735
TCLP Chlorobenzene
<0.100
mg/L
0.100
10 02/22/23 16:37 ELM
L665735
TCLP Chloroform
<0.100
mg/L
0.100
10 02/22/23 16:37 ELM
L665735
TCLP 1,4-Dichlorobenzene
<0.100
mg/L
0.100
10 02/22/23 16:37 ELM
L665735
TCLP 1,2-Dichloroethane
<0.100
mg/L
0.100
10 02/22/23 16:37 ELM
L665735
TCLP 1,1-Dichloroethene
<0.100
mg/L
0.100
10 02/22/23 16:37 ELM
L665735
TCLP Methyl Ethyl Ketone (MEK)
<2.00
mg/L
2.00
10 02/22/23 16:37 ELM
L665735
TCLP Tetrachloroethene
<0.100
mg/L
0.100
10 02/22/23 16:37 ELM
L665735
TCLP Trichloroethene
<0.100
mg/L
0.100
10 02/22/23 16:37 ELM
L665735
TCLP Vinyl Chloride
<0.100
mg/L
0.100
10 02/22/23 16:37 ELM
L665735
Surrogate:4-Bromofluorobenzene
128
Limits: 71-137%
10 02/22/23 16:37 ELM
L665735
Surrogate: Dibromofluoromethane
87.0
Limits: 70-128%
10 02/22/23 16:37 ELM
L665735
Surrogate: 1,2-Dichloroethane - d4
106
Limits: 63-136%
10 02/22/23 16:37 ELM
L665735
Surrogate: Toluene-d8
113
Limits: 70-130%
10 02/22/23 16:37 ELM
L665735
Analytical Method: 8270C
Prep Batch(es):
L665795 02/23/23 10:30
Prep Method: 3510C
Test
Results
Units
MQL
DF Date / Time By
Analytical
Analyzed
Batch
TCLP 2-Methylphenol
<0.0620
mg/L
0.0620
5 02/23/23 23:22 VBW
L665944
TCLP 3&4 Methylphenol
0.0800
mg/L
0.0620
5 02/23/23 23:22 VBW
L665944
TCLP 2,4-Dinitrotoluene
<0.0620
mg/L
0.0620
5 02/23/23 23:22 VBW
L665944
Qualifiers/ DF Dilution Factor
MQL
Method Quantitation Limit
Definitions Q RPD >40% dual column results
Page 5 of 10

Waypoint.0
ANALYTICAL
46546
Town Of Clayton
Salvador Valdiviezo
POB 879
Clayton , NC 27528
Report Number:23-039-0005
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Project Holding Tank 1
Information :
REPORT OPANAL YSIS
Report Date: 02/28/2023
Received : 02/08/2023
Brandi Watson
Lab No : 60712
Sample ID : Holding Tank 1
Matrix: TCLP
Sampled: 2/7/2023 0:00
Analytical Method: 8270C
Prep Batch(es):
L665795 02/23/23 10:30
Prep Method: 3510C
Test
Results
Units
MOL
DF
Date / Time By
Analytical
Analyzed
Batch
TCLP Hexachlorobenzene
<0.0620
mg/L
0.0620
5
02/23/23 23:22 VBW
L665944
TCLP Hexachlorobutadiene
<0.0620
mg/L
0.0620
5
02/23/23 23:22 VBW
L665944
TCLP Hexachloroethane
<0.0620
mg/L
0.0620
5
02/23/23 23:22 VBW
L665944
TCLP Nitrobenzene
<0.0620
mg/L
0.0620
5
02/23/23 23:22 VBW
L665944
TCLP Pentachlorophenol
<0.125
mg/L
0.125
5
02/23/23 23:22 VBW
L665944
TCLP Pyridine
<0.125
mg/L
0.125
5
02/23/23 23:22 VBW
L665944
TCLP 2,4,5-Trichlorophenol
<0.0620
mg/L
0.0620
5
02/23/23 23:22 VBW
L665944
TCLP 2,4,6-Trichlorophenol
<0.0620
mg/L
0.0620
5
02/23/23 23:22 VBW
L665944
Surrogate: TCLP 2,4,6-Tribromophenol
53.5
Limits: 42-102%
5 02/23/23 23:22 VBW
L665944
Surrogate: TCLP 2-Fluorobiphenyl
49.1
Limits: 24-86%
5 02/23/23 23:22 VBW
L665944
Surrogate: TCLP 2-Fluorophenol
17.9
Limits: 13-37%
5 02/23/23 23:22 VBW
L665944
Surrogate: TCLP 4 Terphenyl-d14
62.5
Limits: 30-122%
5 02/23/23 23:22 VBW
L665944
Surrogate: TCLP Nitrobenzene-d5
48.4
Limits: 25-78%
5 02/23/23 23:22 VBW
L665944
Surrogate: TCLP Phenol-d6
13.5
Limits: 9-27%
5 02/23/23 23:22 VBW
L665944
Qualifiers/ DF
Definitions Q
Dilution Factor
RPD >40% dual column results
MQL Method Quantitation Limit
Page 6 of 10

0
Waypoint
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
ANALYTICAL
www.waypointanalytical.com
46546
Town Of Clayton
Project
Holding Tank 1
Salvador Valdiviezo
Report Date : 02/28/2023
POB 879
Information :
Received : 02/08/2023
Clayton , NC 27528
Brandi Watson
Report Number: 23-039-0005
REPORTOFANALYSIS
Lab No : 60713
Matrix: Solids
Sample ID : Holding Tank 1
Sampled: 2/7/2023 0:00
Test
Results
Units
MQL DF Date / Time By Analytical
Analyzed Method
Sulfide (Reactivity)
<25.0
mg/Kg
25.0 1 02/20/23 11:09 FMM SW-7.3.4
Cyanide (Reactivity)
<0.125
mg/Kg
0.125 1 02/17/23 10:55 FMM SW-7.3.3
Ignitability
>96
degrees C
1 02/24/23 09:30 CNB ASTM D93-80
pH
9.5
s.u.
1 02/20/2315:00 SAR SW-9045C
Qualifiers/ DF Dilution Factor
Definitions Q RPD >40% dual column results
MQL Method Quantitation Limit
Page 7 of 16

Waypoint .
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Client: Town Of Clayton CASE NARRATIVE
Project: Holding Tank 1
Lab Report Number: 23-039-0005
Date: 2/27/2023
Separatory Funnel Extraction 8081 Method 3510C
Sample 60712 (Holding Tank 1)
QC Batch No: 1-665598/1-665598
The weight/volume extracted was reduced during the extraction procedure due to the nature of the sample.
Reporting limits are factored for the sample size reduction.
Separatory Funnel Extraction 8270 Method 3510C
Sample 60712 (Holding Tank 1)
QC Batch No: 1-665795/1-665795
The weight/volume extracted was reduced during the extraction procedure due to the nature of the sample.
Reporting limits are factored for the sample size reduction.
Volatile Organic Compounds - GC/MS (TCLP) Method 8260E
Sample 60712 (Holding Tank 1)
QC Batch No: 1-665735/1-665734
The sample was analyzed at a dilution due to the foamy nature of the matrix. Reporting limits have been adjusted
accordingly.
Semivolatile Organic Compounds - GC/MS (TCLP) Method 8270D
Sample 60712 (Holding Tank 1)
QC Batch No: 1-665944/1-665795
The sample was diluted due to the nature of the sample matrix. Reporting limits have been adjusted accordingly.
Page 8 of 10

0 (D
Waypoint
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
www.waypointanalytical.com
Shipment Receipt Form
Customer Number: 46546
Customer Name: Town Of Clayton
Report Number: 23-039-0005
Shipping Method
0 Fed Ex 0 US Postal 0 Lab
* UPS 0 Client 0 Courier
Other
Thermometer ID:
Shipping container/cooler uncompromised?
* Yes
0 No
Number of coolers/boxes received
F 1
Custody seals intact on shipping container/cooler?
0 Yes
0 No
Not Present
Custody seals intact on sample bottles?
0 Yes
0 No
0 Not Present
Chain of Custody (COC) present?
Yes
0 No
COC agrees with sample label(s)?
Yes
0 No
COC properly completed
Yes
0 No
Samples in proper containers?
Yes
0 No
Sample containers intact?
Yes
0 No
Sufficient sample volume for indicated test(s)?
0 Yes
0 No
All samples received within holding time?
Yes
0 No
Cooler temperature in compliance?
Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
Yes
0 No
Water - Sample containers properly preserved
0 Yes
0 No
N/A
Water - VOA vials free of headspace
0 Yes
0 No
0 N/A
Trip Blanks received with VOAs
0 Yes
0 No
N/A
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
N/A
High concentration container (48 hr) [_ Low concentration EnCore samplers (48 hr)
High concentration pre -weighed (methanol -14 d) F_ Low cone pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included?
Comments:
0 Yes * No
Signature: jBrandi Watson Date & Time: 2/08/2023 10:25:39
Page 9 of 10

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Page 10 of 10

row,"—. -Mqql Environmental Chemists, Inc.
envirochem 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910 392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/ Fax
` 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/ Fax
ANALYTICAL & CONSULTING CHEMISTS [e-mail]
Onslow Water & Sewer Authority
Date of Report: Jan 15, 2024
228 Georgetown Road
Customer PO #:
Jacksonville NC 28540
Customer ID: 08100092
Attention:
Report #: 2023-29358
Project ID: Northwest RWRF Digester
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
23-71078 Site: Digester #1
12/13/2023
10:20 AM Solid/Sludge Jerry Parker
Test
Method
Results Date Analyzed
Chlordane (TCLP)
SW-846 8081 B
<0.02 mg/L
12/19/2023
Endrin (TCLP)
SW-846 60818
<0.0005 mg/L
12/19/2023
Heptachlor (TCLP)
SW-846 8081 B
<0.0005 mg/L
12/19/2023
Heptachlor epoxide (TCLP)
SW-846 8081 B
<0.0005 mg/L
12/19/2023
Lindane (TCLP)
SW-846 80816
<0.0005 mg/L
12/19/2023
Methoxychlor (TCLP)
SW-846 8081 B
<0.0005 mg/L
12/19/2023
Toxaphene (TCLP)
SW-846 8081 B
<0.05 mg/L
12/19/2023
2,4,5-TP (TCLP)
Sw-8468151 A
<0.003 mg/L
12/19/2023
2,4-D (TCLP)
SW-646 8151 A
<0.003 mg/L
12/19/2023
1,4-Dichlorobenzene (TCLP)
SW 8458270 E
<0.050 mg/L
12/20/2023
2,4,5-Trichlorophenol (TCLP)
SW-846 8270 E
<0.050 mg/L
12/20/2023
2,4,6-Trichlorophenol (TCLP)
SW-846 8270 E
<0.050 mg/L
12/20/2023
2,4-Dinitrotoluene (TCLP)
SW-848 8270 E
<0.050 mg/L
12/20/2023
Cresol (TCLP)
SW-846 8270 E
<0.050 mg/L
12/20/2023
Hexachloro-1,3-butadiene (TCLP)
SW-846 8270 E
<0.050 mg/L
12/20/2023
Hexachlorobenzene (TCLP)
SW-846 8270 E
<0.050 mg/L
12/20/2023
Hexachloroethane (TCLP)
SW-846 8270 E
<0.050 mg/L
12/20/2023
m + p-Cresol (TCLP)
SW-846 8270 E
<0.050 mg/L
12/20/2023
Nitrobenzene (TCLP)
SW-046 8270 E
<0.050 mg/L
12/20/2023
o-Cresol (TCLP)
SW-846 8270 E
<0.050 mg/L
12/20/2023
Pentachlorophenol (TCLP)
SW-846 8270 E
<0.250 mg/L
12/20/2023
Pyridine (TCLP)
SW-846 8270 E
<0.050 mg/L
12/20/2023
1,1-Dichloroethyiene (TCLP)
SW-846 Method 8260D
< 0.01 mg/L
12/21/2023
1,2-Dichloroethane (TCLP)
SW-846 Method 8260D
< 0.01 mg/L
12/21/2023
Benzene (TCLP)
SW-846 Method 8260D
< 0.01 mg/L
12/21/2023
Carbon Tetrachloride (TCLP)
SW-846 Method 8260D
< 0.01 mg/L
12/21/2023
Report 9 2023-29358
Page 1 of 3

Environmental Chemists, Inc.
envirochem 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab!Fax
�' 255 A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS infoirr-environmentalchemists.com
Onslow Water & Sewer Authority
Date of Report: Jan 15, 2024
228 Georgetown Road
Customer PO #:
Jacksonville NC 28540
Customer ID: 08100092
Attention:
Report #: 2023-29358
Project ID: Northwest RWRF Digester
Chlorobenzene (TCLP)
SW-846 Method 8260D
< 0.01 mg/L
12/21/2023
Chloroform (TCLP)
SW-848 Method 8260D
< 0.01 mg/L
12/21/2023
Methyl ethyl ketone (TCLP)
SW -US Method 8260D
< 0.05 mg/L
12/21/2023
Tetrachloroethylene (TCLP)
SW-846 Method 8260D
< 0.01 mg/L
12/21/2023
Trichloroethylene (TCLP)
SW-846 Method 8260D
< 0.01 mg/L
12/21/2023
Vinyl Chloride (TCLP)
SW-846 Method 0260D
< 0.01 mg/L
12/21/2023
RCI
Cyanide
SM 4500 CN D-2016
<1 mg/kg
12/27/2023
Sulfide
SM 4500 S 0-2011
0.18 mg/kg
01/02/2024
Ignitability
SW 846 method 1010
>157 OF
12/15/2023
Sludge Residuals
Aluminum
EPA 200.7, Rev. 4 4,1994
22700 mg/kg
01/02/2024
Arsenic
EPA 200.7, Rev. 4.4, 1994
<11.4 mg/kg
12/29/2023
Cadmium
EPA 200.7, Rev. 4.4,1994
<11.4 mg/kg
12/29/2023
Calcium
EPA 200.7, Rev 4.4,1994
16300 mg/kg
12/29/2023
Chromium
EPA 200.7, Rev 4.4,1994
19.8 mg/kg
12/29/2023
Copper
EPA 200.7, Rev. 4.4, 1994
251 mg/kg
12/29/2023
Lead
EPA 200.7, Rev 4.4,1994
11.6 mg/kg
12/29/2023
Magnesium
EPA 200.7, Rev 4A, 1994
2040 mg/kg
12/29/2023
Molybdenum
EPA 200.7, Rev 4.4, 1994
<11.4 mg/kg
12/29/2023
Nickel
EPA 200.7, Rev 4.4,1994
<11.4 mg/kg
12/29/2023
Potassium
EPA 200.7, Rev 4.4,1994
3780 mg/kg
01/02/2024
Selenium
EPA 200.7, Rev 4.4,1994
<11.4 mg/kg
12/29/2023
Sodium
EPA 200.7, Rev 4.4,1994
10100 mg/kg
01/02/2024
Zinc
EPA 200.7. Rev 4.4 1994
969 mg/kg
12/29/2023
Nitrate+Nitrite-Nitrogen
EPA 353.2
5990 mg/kg
12/18/2023
Total Solids (%)
SM 2540 6
1.62 %
12/18/2023
Ammonia Nitrogen
SM 4500 NIi3 C-2011
1720 mg/kg
12/17/2023
Total Kjeldahl Nitrogen (TKN)
SM 4500 Norg B-2011
15500 mg/kg
12/17/2023
Total Phosphorus
SM 4600 P (F-H}2011
27100 mg/kg
12/20/2023
Report 0: 2023-29358
Page 2 of 3

[envirroche]m
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab Fax
255-A Wilmington Highway, Jacksonville, NC 28540 ' 910.347.5843 Lab! Fax
inro(a environmentalchemists.com
Onslow Water & Sewer Authority Date of Report: Jan 15, 2024
228 Georgetown Road Customer PO #:
Jacksonville NC 28540 Customer ID: 08100092
Attention: Report #: 2023-29358
Project ID: Northwest RWRF Digester
pH SW 846 Method 9045D 6.59 units 12/22/2023
Result estimated. Analyzed out of 15 minutes hold time.
Mercury SW-846 7471 s <1.04 mg/kg 12/15/2023
TCLP Metals
Arsenic (TCLP)
EPA 200.7. Rev. 4.4,1994
<1.0 mg/L
12/27/2023
Barium (TCLP)
EPA 200.7. Rev. 4.4,1994
<1.0 mg/L
12/27/2023
Cadmium (TCLP)
EPA 200.7, Rev. 4.4, 1994
<1.0 mg/L
12/27/2023
Chromium (TCLP)
EPA 200.7, Rev. 4.4, 1094
<1.0 mg/L
12/27/2023
Lead (TCLP)
EPA 200.7, Rev. 4.4,1994
<1.0 mg/L
12/27/2023
Selenium (TCLP)
EPA 200.7, Rev. 4.4,1994
<1.0 mg/L
12/27/2023
Silver (TCLP)
EPA 2ca.7. Rev 4.4,1994
<1.0 mg/L
12/27/2023
Mercury (TCLP)
EPA 245.1
<0.0002 mg/L
12/27/2023
Comment: Sludge residuals, except pH, reported on a dry weight basis. pH reported on an as received basis.
Reviewed by: , �.'j���P�
Report V:: 2023-29358 Page 3 of 3

Environmental Chemist, Inc., Wilmington, NC Lab #94
6602 Windmill Way
Wilmington, NC 28405
910.392,0223
Sample Receipt Checklist
Client: A Date: A14 0- Report Number: 2023-
Receipt of sample:
ECHEM Pickup Client Delivery ❑ JUPS ❑ Fed Ex ❑ Other ❑
❑ YES 10 NO
DD N/A II. Were custody seals present on the cooler?
❑ YES 10 NO
I Cl N/A If custody seals were present, were they intact/unbroken?
112.
Original temperature upon receipt "C Corrected temperature upon receipt oC
How temperature taken:
_ _
El Terfiperature Blank O Against Bottles
IR Gun ID: Thomas Traceable S/N 210886869 IR Gun Correction Factor °C: 0.0
19 YES ❑ NO
3. If temperature of cooler exceeded 6°C, was Project Mgr./QA notified?
19 YES ❑ NO
4. Were proper custody procedures (relinquished/received) followed?
0 YES ❑ NO
5. Were sample ID's listed on the COO
© YES O
6. Were samples ID's listed on sample containers?
O YES O
7. Were collection date and time listed on the COC?
0 YES O
kCO3N
8. Were tests to be performed listed on the COC?
0 YES O
9. Did samples arrive in proper containers for each test?
O YES O
10. Did samples arrive in good condition for each test?
O YES O
11. Was adequate sample volume availableT
O YES 13 NO
12. Were samples received within proper holding time for requested tests?
❑ YES ❑ NO
13. Were acid preserved samples received at a pH of <27
C] YES ❑ NO
14. Were cyanide samples received at a pH >12?
ElYES ❑ NO
15. Were sulfide samples received at a pH >9?
❑ YES ❑ NO
16. Were NH3/TKN/Phenol received at a chlorine residual of <0.5 m/L? **
❑ YES ❑ NO
17. Were Sulfide/Cyanide received at a chlorine residual of <0.5 m/L?
0 YES 13 NO
18. Were orthophosphate samples filtered in the field within 15 minutes?
* TOC/Volatiles are pH checked at time of analysis and recorded on the benchsheet.
** Bacteria samples are checked for Chlorine at time of analysis and recorded on the benchsheet.
Sample Preservation:
(Must be completed for any sample(s) incorrectly preserved or with headspace)
Sample(s) _
were received incorrectly preserved and were adjusted accordingly
by adding (circle one):
H2SO4 HNO3 HCl NaOH
Time of preservation:
If more than one preservative is needed, notate in comments below
Note: Notify customer service immediately
for incorrectly preserved samples. Obtain a new sample or
notify the state lab if directed to analyzed by the customer. Who was notified, date and time:
Volatiles Sample(s)
were received with Mricnnro
COMMENTS:
DOC. QA.002 Rev 1

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Eenvi.r(owhem
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
[e-mail]
Branch Residuals/Bob Branch Date of Report: Feb 01, 2023
1735 Heckle Blvd Suite 103-291 Customer PO #:
Rock Hill SC 29732 Customer ID: 15060009
Attention: Report #: 2023-00643
Project ID: Sludge -Wallace WWTP
Lab ID Sample ID: Collect DatefTime Matrix Sampled by
23-01571 Site: Sludge 1/10/2023 11:25 AM Solid/Sludge
Test Method Results Date Analyzed
Zinc
EPA 200 7, Rev 4.4,1994
1390 mg/kg
01/16/2023
Chlordane (TCLP)
SW-8468081 B
<0.02 mg/L
01/16/2023
Endrin (TCLP)
SW-846 8081 B
<0.0005 mg/L
01/16/2023
Heptachlor (TCLP)
SW-8468081 B
<0.0005mg/L
01/16/2023
Heptachlor epoxide (TCLP)
SW-846 8081 B
<0.0005 mg/L
01/16/2023
Lindane (TCLP)
SW-846 8081 B
<0.0005 mg/L
01/16/2023
Methoxychlor (TCLP)
SW-8468081 B
<0.0005 mg/L
01/16/2023
Toxaphene (TCLP)
SW-846 8081 B
<0.05 mg/L
01/16/2023
2,4,5-TP (TCLP)
SW 846 8151 A
<0.003 mg/L
01/16/2023
2,4-D (TCLP)
SW-846 e151 A
<0.003 mg/L
01/16/2023
1,4-Dichlorobenzene (TCLP)
SW-848 8270 E
<0.050 mg/L
01/13/2023
2,4,5-Trichlorophenol (TCLP)
SW-8468270E
<0.050mg/L
01/13/2023
2,4,6-Trichlorophenol (TCLP)
SW-846 8270 E
<0.050 mg/L
01/13/2023
2,4-Dinitrotoluene (TCLP)
SW-846 8270 E
<0.050 mg/L
01/13/2023
Cresol (TCLP)
SW-8468270E
<0.050mg/L
01/13/2023
Hexachloro-1,3-butadiene (TCLP)
SW-846 8270 E
<0.050 mg/L
01/13/2023
Hexachlorobenzene (TCLP)
SW-846 8270 E
<0.050 mg/L
01/13/2023
Hexachloroethane(TCLP)
SW-8468270E
<0.050mg/L
01/13/2023
m + p-Cresol (TCLP)
SW-846 8270 E
<0.050 mg/L
01/13/2023
Nitrobenzene (TCLP)
SW-846 8270 E
<0.050 mg/L
01/13/2023
o-Cresol (TCLP)
SW-846 8270 E
<0.050 mg/L
01/13/2023
Pentachlorophenol (TCLP)
SW-8468270E
<0.250mg/L
01/13/2023
Pyridine (TCLP)
SW-846 8270 E
<0.050 mg/L
01/13/2023
1, 1 -Dichloroethylene (TCLP)
SW-846 Method8260D
<0.01 mg/L
01/24/2023
1,2-Dichloroethane (TCLP)
SW-846 Method8260D
<0.01 mg/L
01/24/2023
Benzene (TCLP)
SW-846 Method 8260D
<0.01 mg/L
01/24/2023
Report #. 2023-00643
0 4 -9 A

F"007
enviroche
A
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab a 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 e 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 a 910.347.5843 Lab/Fax
[e-mail]
Branch Residuals/Bob Branch
Date of Report: Feb 01, 2023
1735 Heckle Blvd Suite 103-291
Customer PO #:
Rock Hill SC 29732
Customer ID: 15060009
Attention:
Report #: 2023-00643
Project ID: Sludge -Wallace WWTP
Carbon Tetrachloride (TCLP)
sw-a46 Method 82600
<0.01 mg/L
01/24/2023
Chlorobenzene (TCLP)
SW-846 Method82600
<0.01 mg/L
01/24/2023
Chloroform (TCLP)
SW-846 Method 8260D
<0.01 mg/L
01/24/2023
Methyl ethyl ketone (TCLP)
SW-846 Method 8260D
<0.05 mg/L
01/24/2023
Tetrachloroethylene (TCLP)
SW-846 Method 8260D
<0.01 mg/L
01/24/2023
Trichloroethylene (TCLP)
SW-846 Method 8260D
<0.01 mg/L
01/24/2023
Vinyl Chloride (TCLP)
SW-846 Method 8260D
<0.01 mg/L
01/24/2023
RCI
Cyanide
SM 4500 CN D-2016
<1 mg/kg
01/12/2023
Sulfide
SM 4500 S D
<0.05 mg/kg
01/19/2023
Analyzed outside of hold time.
Ignitability
SW 846 method 1010
>158 aF
01/17/2023
Sludge Residuals
Aluminum
EPA 200.7, Rev. 4.4, 1994
8600 mg/kg
01/16/2023
Arsenic
EPA 200.7, Rev. 4.4, 1994
203 mg/kg
01/16/2023
Cadmium
EPA 200.7, Rev. 4.4. 1994
<15.978 mg/kg
01/16/2023
Calcium
EPA 200.7, Rev. 4.4, 1994
27400 mg/kg
01/16/2023
Chromium
EPA 200.7. Rev. 4.4, 1994
28.2 mg/kg
01/16/2023
Copper
EPA 200.7, Rev. 4.4,1994
790 mg/kg
01/16/2023
Lead
EPA 200.7, Rev. 4.4, 1994
35.9 mg/kg
01/16/2023
Magnesium
EPA 200.7, Rev. 4.4, 1994
4580 mg/kg
01/16/2023
Molybdenum
EPA 200.7, Rev. 4.4, 1994
<15.978 mg/kg
01/17/2023
Nickel
EPA 200.7, Rev. 4.4, 1994
20.0 mg/kg
01/16/2023
Potassium
EPA 200.7, Rev. 4.4,1994
5060mg/kg
01/16/2023
Selenium
EPA 200.7, Rev. 4.4, 1994
<15.978 mg/kg
01/16/2023
Sodium
EPA 200.7, Rev. 4.4, 1994
5500 mg/kg
01/16/2023
Nitrate+Nitrite-Nitrogen
EPA353.2
2440mg/kg
01/12/2023
Total Solids (%)
SM 2540 B
2.71 %
01/11 /2023
Ammonia Nitrogen
SM 4500 NH3 C-2011
858 mg/kg
01/10/2023
Total Kjeldahl Nitrogen (TKN)
SM 4500 Norg B-2011
47000 mg/kg
01 /11/2023
Report #': 2023-00843
0- o ..r

r 47
Si+
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910-347.584-3 Lab/Fax
[e-mail]
Branch Residuals/Bob Branch Date of Report: Feb 01, 2023
1735 Heckle Blvd Suite 103-291 Customer PO #:
Rock Hill SC 29732 Customer ID: 15060009
Attention: Report #: 2023-00643
Project ID: Sludge -Wallace WWTP
Total Phosphorus SM 4500 P (F-H)-2011 19500 mg/kg 01/17/2023
pH SW 846 Method 9045D 6.35 units 01 /20/2023
Result estimated. Analyzed out of 15 minutes hold time.
Mercury
SW-846 7471 B
0.915 mg/kg
01/13/2023
TCLP Metals
Arsenic (TCLP)
EPA 2007, Rev 44,1994
<1.0mg/L
01/17/2023
Barium (TCLP)
EPA 200 7, Rev 44, 1994
<1.0mg/L
01/17/2023
Cadmium (TCLP)
EPA 2007.Rev 4 4. 1994
<1.Omg/L
01/17/2023
Chromium (TCLP)
EPA 2007,Rev 44,1994
<1.0mg/L
01/17/2023
Lead (TCLP)
EPA 200.7, Rev 44, 1994
<1.0 mg/L
01/17/2023
Selenium (TCLP)
EPA 200.7, Rev. 4 4, 1994
<1.0mg/L
01/17/2023
Silver (TCLP)
EPA 200.7, Rev 4 4, 1994
<1.0 mg/L
01/17/2023
Mercury (TCLP)
EPA 245.1
<0.0002 mg/L
01/27/2023
Lab ID Sample ID:
Collect Date/Time
Matrix Sampled by
23-01572 Site: Sludge 1
1/10/2023 11:25 AM
Solid/Sludge
Test
Method
Results
Date Analyzed
Total Solids (%)
SM2540B
2.97% 01/11/2023
Fecal Density
SM 9221C E-2014
1112 MPN/g 01/10/2023
Lab ID Sample ID:
Collect Date/Time
Matrix Sampled by
23-01573 Site: Sludge 2
1/10/2023 11:25 AM
Solid/Sludge
Test
Method
Results Date Analyzed
Total Solids (%)
SM2540B
2.85% 01/11/2023
Fecal Density
SM 9221C E-2014
1193 MPN/g 01/10/2023
Lab ID Sample ID:
Collect Date/Time
Matrix Sampled by
23-01574 Site: Sludge 3
1/10/2023 11:25 AM
Solid/Sludge
Test
Method
Results Date Analyzed
Total Solids (%)
SM 2540 8
2.84 % 01/11/2023
Fecal Density
SM 9221C E-2014
1726 MPN/g 01/10/2023
Report #:: 2023-00643
P— a , f d

,:n:v:7irocohem
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab ° 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 ' 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 ' 910.347.5843 Lab/Fax
info@ environmentalchenlists.com
Branch Residuals/Bob Branch Date of Report: Feb 01, 2023
1735 Heckle Blvd Suite 103-291 Customer PO #:
Rock Hill SC 29732 Customer ID: 15060009
Attention: Report #: 2023-00643
Project ID: Sludge -Wallace WWTP
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
23-01575 Site: Sludge 4 1/10/2023 11:25 AM Solid/Sludge
Test Method Results Date Analyzed
Total Solids (%) SM 2540 B 3.09 % 01/11 /2023
Fecal Density SM 9221C E-2014 1068 MPN/g 01/10/2023
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
23-01576 Site: Sludge 5 1/10/2023 11:25 AM Solid/Sludge
Test Method Results Date Analyzed
Total Solids (%) SM 2540 B 2.94 % 01 /11 /2023
Fecal Density SM 9221C E-2014 375 MPN/g 01/10/2023
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
23-01577 Site: Sludge 6 1/10/2023 11:25 AM Solid/Sludge
Test Method Results Date Analyzed
Total Solids (%) SM 2540 B 3.07 % 01111 /2023
Fecal Density SM 9221C E-2014 750 MPN/g 01/10/2023
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
23-01578 Site: Sludge 7 1/10/2023 11:25 AM Solid/Sludge
Test Method Results Date Analyzed
Total Solids (%) SM 2540 B 3.00 % 01/11/2023
Fecal Density SM 9221C E•2014 1134 MPN/g 01/10/2023
Comment: Surrogate DBA on column 2 Method 8081 manually integrated due to sample matrix." Sludge
residual r sults, except pH, reported on a dry weight basis. pH reported on an as received basis.
Reviewed by: t
Report # 2023-00643 0,, A �f A

Environmental Chemist, Inc., Wilmington, NC Lab #94
6602 Windmill Way
Wilmington, NC 28405
01n -in-i
Sample Receipt Checklist
Date: O�3 Reportrqlumb— 2Q23--00(oq'--),
ecP6)t
ECHETA Flicklif
i e r 'n
ient Delivef " 0 UPS 0
PDP,2�-f-YES D NO N A I. Y/ere custody seals present on 'the cooler?
0 E S CJ NO N/A 2. lfcustod
Original temperature upon receipt 'C —y seals v.,ere present, were they int-act/unbrolken?
--- Corrected temperature upon receipt nc
How temperature taken: Temperature Blank Against Bottles
-hornas Traceable S/N 210886869 1 R Gun Correction T� Gun I D.- —I Ltles
ction Factor 'C: 0.()
YES C3 NO 3.— If temperature of cooler exceeded 6°C,
YES Ej- NO 11 1A C, was Project Nlgf./QA notified?:
Were proper custody procedures (relin--­ : _
quished/received) followed',
YES 0 NO 5. Were sample ID listed on the �COC?
YES 0 NO 6. Were samples
Ples ID's listed on sample containe-15?--
YES 7. Were collection date and time listed on the
YES D NO 8. Were tests to be performed listed on the CoC?
YES E3 NO 9. Did samples arrive in Proper containers for each test?
YES 0 N 0 10. Did samples arrive in good condition for eacl—i--�
test?
CK YES 0 NO 11, Was adequate sample Volume available?'
YES E3 NO 12. Were samples -- I received within proper holding t
E3 YES 0 NO 1 time for requested tests?
— 3. Were acid preserved samples❑ es received at a PH of <2 ?
---- 0 NO 14..Were cyanide samples received at a PH >12a
El YES 0 NO 15. Were sulfide —samples received at a pH >9?
0 YES El NO 1-6. Were W-13/1'KN/Phenol received at a chlorine residual
11 YES 0 NO i(FLIal of �<01 rl�,//L?
17. Were Sulfide/Cyanide —received it'a
chlorine residual of <0 nj /I
0 YES 0 NO 18. Were orthophosphate samples filtered in the field within 15
TOC/VoI�11ij(_,sare pil clipckocl, - I — — minutes?
,)t time Of analysis and recorded On the benchsh-,(2t
Bacteria samples Zlrc-. checked for Chlorine at time of analysis and recorded on the benchsheet
Sample Preservation: (Must be completed for any sample(s) incorrectly preserved or with headspace)
Sarriple(s) were received incorrectl
by adding (circle one - y preserved and were adjusted accordingly
)HNO3
Time of'preservation: IF HCI WOH
Note: N�,tifll Ctlstomerservice imri-�d:atel�, rnnrca than one preservative is needed, riotate in comments belotiv
rl'),ily the 5,eite lab if direr-tz',' lto anaiyzed by the cust�jl"E,", Clate arl", Virl-P
Volatiles Sample(s)
were received with headspace
COMMENTS:
DOC. QA.002 Rev 1

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PATHOGEN AND VECTOR
ATTRACTION REDUCTION FORMS

PATHOGEN REDUCTION AND VECTOR ATTRACTION REDUCTION
The Town of Beulaville, Town of Kenansville, Town of Warsaw, Town of Bridgeton, Town of
Maysville, Southwest Plantation, Town of Clayton (all except for part of the second quarter) and the
Town of Wallace meet pathogen reduction and vector attraction reduction requirements through
lime stabilization. The Town of Clayton (part of the second quarter) met pathogen reduction
through fecal density and vector attraction reduction through injection or incorporation. ONWASA
facilities Northwest Regional, Summerhouse and Swansboro met pathogen reduction and vector
attraction reduction through fecal density and SOUR testing.
The forms for these facilities are marked appropriately.

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Triple S Farms & Cleaning
WWTP Name: Town of Bridgeton WWTP
Monitoring Period: From 1 1 2023 To
WQ Permit Number: WQ0030998
NPDES Number: NCO074837
12/31 /2023
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. A (time/temp) ❑
Alt B (Alk Treatment) ❑
Alt. C (Prior Testing) ❑
A1t.D (No Prior Test) .J
Process to Further Reduce Patho ens ❑ ,d
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
ying❑ Heat Treatment_ ❑ Thenno hilic ❑
Compost ❑ Heat Dr
Beta Ray 01
Gamma Ray ❑
Pasteurization ❑
Class B:
jAlt. (1) Fecal Density ❑
Alt. (2) Process to Significantly Reduce Pathogens El
If applicable to alternative peiformed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization El
Air Drying ❑
Composting ❑
Aerobic Digestion ❑
Anaerobic Di estion ❑
If applicable to alternative performed (Class A or Class B) complete the following
monitoring data:
Parameter
Allowable Level
in Sludge
Pathogen Density
NUMbEroilFrequency
Excee-
of Anal sis
Y
Sample
Type
Analytical
Tech -
MinimumGco.
Mean
aximu
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
CFU
_
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per 4 grams
total solid (dry
weight)
Vector Attraction Reduction (15A NCAC 02'r .1107) - Please indicate alternative performed:
Alt.1 (VS reduction) ❑
Alt. 2 (40-day bench) ❑
Alt. 3 (30-day bench) ❑
Alt. 4 (Spec. O, uptake) lJ
Alt. 5 (14-Day Aerobic) ❑
Alt. 6 (Alk. Stabilization8
Alt 7 (Drying - Stable) ❑
jAlt. 8 (Drying - Unstable) ❑
Alt. 9 (Injection) ❑
Alt. 10 (Incorporation) ❑
No vector attraction reduction alternatives were performed ❑
CERTIFICATION STATEMENT (please check the appropriate statement)
El "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
Cl vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note
if you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Mr. Eric R. Smith
Preparer Name and Title (type or print)
Signature of Preparer* Date
1` C t Poe
Land Applier Name agd Title (if Applicable) (type or print)
Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Triple S Farms & Cleaning WQ Permit Number: WQ0030998
WWTP Name: Town of Beulaville WWTP NPDES Number- NCO026018
Monitoring Period: From 1/1/2023 To 12/31/2023
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. A (time/tem) ❑
Alt B (Alk Treatment) ❑
1 Alt. C (Prior Testing) ❑
A1t.D (No Prior Test) ❑
Process to Further Reduce Patho ens ❑
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost ❑
Heat D ' t ❑
Heat Treatment ❑
Thermo hilic ❑
Beta Ray ❑
Gamma Ray ❑
Pasteurization ❑
Class B:
Alt. (I) Fecal Density ❑
Alt. (2) Process to SignificantiX Reduce Pathogens Q
!LIpplicable to alternative performed Class B only) indicate `Process to Sipfficantly Reduce Path ens":
Lime Stabilization Cl
Air Drying ❑
composting ❑
Aerobic Digestion ❑
Anaerobic Digestion ❑
If a licable to alternative erformed (Class A or Class B complete the followingmonitoringdata:
Parameter
Allowable Level
in Sludge
Pathogen Density
NO = or
Excee-
denrer
Frequency
of Analysis
Sample
Type
na ica
Tech-
Minimum
Geo. Mean
Maximum.Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
CFU
1000 mpn per gram
of total solid (dry
wei ht
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per 4 grams
total solid (dry
I weight)
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative
performed:
Alt.1 (VS reduction) ❑
Alt. 2 (40-day bench) ❑
Alt. 3 (30-day bench) ❑
jAlt. 4 (Spec. OZ uptake) ❑
Alt. 5 (14-Day Aerobic) ❑
Alt. 6 (Alk. StabilizationEl
Alt 7 (Drying -Stable)' ❑
1 Alt. 8 (Drying -Unstable) 0
Alt. 9 (Injection) El
Alt. 10 (Incorporation) ❑
No vector attraction reduction alternatives were performed ❑
t;EKi1riuATION ST TEMENT (please check the appropriate statement)
t] "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
❑ vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note
if you check this statement attach an explanation why you have not met one or both of the
11113 uMcrmmauon nas peen maae unaer my aireenon ana supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Mr. Stanley Miller, WWTP ORC f
Preparer Name and Title (type or print) Land Applier Name an itle (if applicable)(type or print
—Al 2�& 9;11e1--1f-WA--1--- - — A,56
Signature reparer* Date Signature of Land Ap lier (if applicable) Date
r rr )
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Triple S Farms & Cleaning WQ Permit Number: WQ0030998
WWTP Name: Town of Clayton Little Creek WRF NPDES Number: NCO025453
Monitoring Period: From 1 1 2023 To 3/31/2023
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. A (time/tern) ❑
Alt B (Alk Treatment) ❑
Alt. C (Prior Testing) ❑
Alt.D (No Prior Test) ❑
Process to Further Reduce Pathogens ❑
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost ❑
Heat Drying ❑
Heat Treatment ❑
Thermo hilic ❑
Beta Ray ❑
Gamnta Ray ❑
Pasteurization ❑
Class B:
Alt. (1) Fecal Density ❑
I Alt. (2) Process to Significantly Reduce Pathogens E
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization El
Air Drying ❑
Coniposting ❑
jAerobic Digestion ❑
Anaerobic Digestion ❑
If applicable to alternative performed (Class A or Class B) complete the following
monitoring data:
Parameter
Allowable Level
in Sludge
Pathogen Density
Numt5er ot
Excee-
Frequency
of Analysis
Sample
Type
Analytical
Tech -
ninue
inimu
Geo. Mean
aximu
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
CFU
1000 mpn per gram
of total solid (dry
weight),
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per 4 grams
total solid (dry
weigh
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed:
Alt.1 (VS reduction) ❑
Alt. 2 (40-day bench) ❑
Alt. 3 (30-day bench) ❑
JAIt. 4 (Spec. O, uptake) ❑
Alt. 5 (14-Day Aerobic) ❑
Alt. 6 (Alk. Stabilization El
Alt 7 (Drying - Stable) ❑
jAlt. 8 (Drying - Unstable) L t
Alt. 9 (Injection) 1-1
Alt. 10 (Incorporation) ❑
No vector attraction reduction alternatives were performed ❑
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note
if you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Mr. Salvador Valdiviezo, Jr., WWTP ORC
Prepare Name an Tait (type or p int)
Signature of Preparer
Land Applier Name and Title (if appl icab le) (type or print)
�/, U V
Date Signature of Land Applier (if applicable)
Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Triple S Farms & Cleaning WQ Permit Number: WQ0030998
WWTP Name: Town of Clayton Little Creek WRF NPDES Number: NCO025453
Monitoring Period: From 4/1/2023 To 6/30/2023
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative nerformed:
Class A: Alt. A time/tern) ❑
1 Alt B (Alk Treahnent) ❑
1 Alt. C(Prior Testing) ❑
A1t.D (No Prior Test) ❑
Process to Further Reduce PathogenPaihogenp ❑
If applicable to alternative performed (Class A only) Indicate "Process to Fuitber Reduce Pathogens":
Compost ❑
Heat Drying ❑
Heat Treatment ❑
Themin hilic ❑
Beta Ra ❑
Gamma Ray ❑
Pasteurization ❑
Class B:
Alt. (1) Fecal Density El
Alt. (2) Process to —Significantly Reduce Pathogens E)
Uapplicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Patho ens":
Lime Stabilization C1
Air in ❑
Com ostin ❑
Aerobic Digestion U
Anaerobic Digestion ❑
If applicable to alternative performed Class A or Class B) complete the followingmonitorin data:
Parameter
Allowable Level
in Sludge
Pathogen Density
um r o
Excee-
FrequencySam
of Analysis
P le
Type
na ica
Tech-
inimu
Geo. Mean
Maximum
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
54
57
63
MPN/
Gram
0
Quarterly
Grab
SMIS
9221 E
CFU
10 0 mpn per gram
of total solid (dry
Wei ht
Salmonella bacteria
(in lieu of Fecal
coliform) I
3 MPN per grams
total solid (dry
weight)
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate
alternative pe ormed:
Alt. t (VS reduction) ❑
Alt. 2 (40-day bench) Ll
Alt. 3 (30-day bench) ❑
JAIL 4 (Spec. O., uptake) ❑
Alt. 5 (14-Day Aerobic) ❑
]Alt.
Alt. 6 (Alk. Stabilization El
Alt 7 (Drying- Stable) ❑
JAII. 8 (Drying- Unstable) ❑
Alt. 9 (Injection) ❑
10 (Incorporation) ❑
No vector attraction reduction alternatives were performed ❑
%-r,ec i W 1%. A 11Uty bT a► EMEW (please check the appropriate statement)
❑ "1 certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T 1107 have been met."
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if
you check this statement attach an explanation why you have not met one or both of the
under my
system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. 1 am aware that there are
significant penalties for false certification including fine and imprisonment."
Mr. Salvador Valdiviezo, Jr., WWTP ORC Mr. Eric Smith, Land Applier
Preparer Name and T' le a or print) Land Applier Name and Ti (it applicable)(type or print)
Aj
Ile L_Z71ZE-1
Signature of Preparer Date Signature of Land Applier (if applicable) Date
•Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Triple S Farms & Cleaning WQ Permit Number: WQ0030998
WWTP Name: Town of Clayton Little Creek WRF NPDES Number: NCO025453
Monitoring Period: From 7 1 2023 To 9 30 2023
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. A (time/temp) ❑
Alt B (Alk Treatment) U
All. C (Prior Testing) LJ
A1t.D (No Prior Test) ❑
Process to Further Reduce Pathogengs J
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost ❑
Heat Drying 01
Heat Treatment ❑
Thermo hilic -J
Beta Ray ❑
Gamma Ray 01
Pasteurization ❑
Class B:
jAlt. (1) Fecal Density CI
I Alt. (2) Process to Significantly Reduce Patho ensEl
If applicable to alternative peiformed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization p
Air Drying ❑
I Composting ❑ jAerobic
Digestion ❑
Anaerobic Digestion ❑
If applicable to alternative performed (Class A or Class B) complete the following
monitoring data:
Parameter
Allowable Level
in Sludge
Pathogen Density
Number or
Excee-
Frequency
of Analysis
Sample
Type
Analytical
Tech -
ninue
Minimum
Geo. Mean
aximu
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
CFU
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per 4 grams
total solid (dry
weight)
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed:
Alt.1 (VS reduction) ❑
Alt. 2 (40-day bench) ❑
Alt. 3 (30-day bench) ❑
Alt. 4 (Spec. O, uptake) ❑
Alt. 5 (14-Day Aerobic) ❑
Alt. 6 (Alk. StabilizationEl
Alt 7 (Drying - Stable) J
Alt. 8 (Drying - Unstable) U
Alt. 9 (Injection) ❑
Alt. 10 (Incorporation) ❑
No vector attraction reduction alternatives were performed Ll
CERTIFICATION STATEMENT (please check the appropriate statement)
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
❑ vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note
if you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Mr. Salvador Valdiviezo, Jr., WWTP ORC
Prep r Name itle (type or print) Land Applier Name and Title (if app I icable) (type or print)
Signature of Prep r* Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Triple S Farms & Cleaning
WNVTP Name: Town of Clayton Little Creek WRF
Monitoring Period: From 10/1/2023 To
WQ Permit Number:
NPDES Number:
12,'31/2023
WQ0030998
NCO025453
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. A (time/tern) 7-Alt
B (Alk Treatment) ❑
Alt. C (Prior Testing) U
Alt.D (No Prior Test) ❑
Process to Further Reduce Pathogen Ss ❑
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost 0
Heat Drying ElHeat
Treatment ❑
Themio Itilic U
Beta Ray❑
Gamma Ray ❑
Pasteurization ❑
Class B:
JAIL (1) Fecal Density 11
1 Alt. (2) Process to Significantly Reduce Pathogens 2
If a plicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization El
Air Dlying ❑
Composting ❑
jAerobic Digestion U
Anaerobic Digestion ❑
If applicable to alternaitive performed (Class A or Class B) complete the followingmonitorin
dtlta:
Parameter
Allowable Level
in Sludge
Pathogen Density
Number Of
Escee-
Frequency
of Analysis
Sample
Type
Analytical
Tech -
inimun
Geo. Mean
Maximum
Unitsenreq
Fecal Coliform
2 x 10 to the
6th poker
per glum of
total solids
MPN
CFU
1000 mpn per graiu
of total solid (dry
Weieltt)
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per 4 grams
total solid (dry
Aveialu)
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed:
Alt.1 (VS reduction) ❑
Alt. 2 (40-day bench) ❑
Alt. 3 (30-day bench) ❑
JAIL 4 (Spec. O, uptake) U
Alt. 5 (14-Day Aerobic) ❑
Alt. 6 (Alk. StabilizationEl
Alt 7 (Drying- Stable) ❑
Alt. 8 (Drying -Unstable) ❑
Alt. 9 (Injection) ❑
Alt. 10 (Incorporation) ❑
No vector attraction reduction alternatives were performed ❑
CERTIFICATION STATEMENT (please check the appropriate statement)
El "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if
you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Mr. Salvador Valdiviezo, Jr., WWTP ORC
Prepa er Name an Title (type or print)
Q
Signature of Prepa
Land Applier Name and Title (if applicable)(type or print)
a, //1 L45IK
Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Triple S Farms & Cleaning WQ Permit Number: WQ0030998
WWTP Name: Town of Kenansville WWTP NPDES Number: NCO036668
Monitoring Period: From 1/l/2023 To 12/31/2023
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. A (time/temp) E17F7Alt
B (Allc Treatment) ❑
F Alt. C (Prior Testing) ❑
Alt.D (No Prior Test) ❑
Process to Further Reduce Pathogengs ❑
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost ❑
I Heat Drying ❑
Heat Treatment ❑
Thermophilic ❑
Beta Ray 01
Gamma Ray ❑
Pasteurization ❑
Class B:
Alt. (1) Fecal Density ❑
I Alt. (2) Process to Significantly Reduce Pathogens E7
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization El
I Air Drying ❑
Composting ❑
jAcrobic Digestion p
Anaerobic Digestion ❑
If a plicable to alternative performed (Class A or Class B) complete the following
monitoring data:
Parameter
Allowable Level
in Sludge
Pathogen Density
NUMUCrOt
Excee-
Frequency
of Analysis
Sample
Type
Analytical
Tech -
Minimum
Geo. Mean
Maximum
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
CFU
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per 4 grains
total solid (dry
weight)
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed:
Alt. I (VS reduction) ❑
Alt. 2 (40-day bench) ❑
Alt. 3 (30-clay bench) ❑
I Alt. 4 (Spec. 02 uptake) ❑
Alt. 5 (14-Day Aerobic) ❑
Alt. 6 (Alk. Stabilization El
Alt 7 (Drying- Stable) ❑
Alt. 8 (Drying - Unstable) ❑
Alt. 9 (Injection) ❑
Alt. 10 (Incorporation) ❑
No vector attraction reduction alternatives were performed ❑
CERTIFICATION STATEMENT (please check the appropriate statement)
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
❑ vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note
if you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Mr. Garay Benson, WWTP ORC
Preparer Name and Title (type or print)
A�I m n l l 19 nl")r",
Signature 6 Prf eparer*
Land Applier Name and Title (if applicable)(type or print)
Date Signature of Land Applier (if applicable) Date
*Prepares is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 02T (12/2006)

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Triple S Farms & Cleaning
WWTP Name: Town of Maysville WWTP
Monitoring Period: From 1/l/2023 To
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
WQ Permit Number: WQ0030998
NPDFS Number: NCO021482
12/31 /2023
Class A:
Alt. A (time/temp) ❑
Alt B (Alk Treatment) ❑
I Alt. C (Prior Testing) ❑
A1t.D (No Prior Test) ❑ Process to Further Reduce Patho enas U
If applicable to alternative petforined (Class A only) indicate "Process to Further Reduce Pathogens":
Compost ❑ Heat D in ❑ Heat Treatment ❑ Thenno hilic ❑
Beta Ray ❑
Gatnnia Ray ❑
Pasteurization ❑
Class B:
JAIL (1) Fecal Density ❑
Alt. (2) Process to Significantly Reduce Pathogens p
If applicable to alternative performed Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization EJ Air Drying ❑ C01112osting ❑
Aerobic Digestion ❑
Anaerobic Digestion ❑
If applicable to alternative performed (Class A or Class B) corn lete the followin
monitorin data:
-Analytical
Parameter
Allowable Level
in Sludge
Pathogen Density
NOW o
Excee-
Frequency
of Analysis
Sample
Type
Tech-
inimu
Geo. Mean
axituu
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
CFU
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per 4 grams
total solid (dry
weight
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative
performed:
Alt.1 (VS reduction) ❑
Alt. 2 (40-day bench) ❑
Alt. 3 (30-day bench) ❑ jAlt.
4 (Spec. 03 uptake)
Alt. 5 (14-Day Aerobic) ❑
Alt. 6 (Alk. Stabilization!]
Alt 7 (Drying - Stable) ❑
Alt. 8 (Drying - Unstable) ❑
Alt. 9(Injection) ❑
Alt. 10 (Incorporation) ❑
No vector attraction reduction alternatives were perfonned ❑
CERTIFICATION STATEMENT (please check the appropriate statement)
El " I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
❑ vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note
If you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Jason Baker WWTP ORC
;Prep ame and Titl a or print)
'gn of Prepares•* Date
Land Applier Name and Title (if applicable)(type or print)
Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 02T (12/2006)

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Triple S Farms & Cleaning WQ Permit Number: WQ0030998
WWTP Name: ONWASA Northwest Regional WWTP NPDES Number: WQ0034367
Monitoring Period: From l/l/2023 To 12 31/2023
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. A (time/temp) ❑
Alt B (Alk Treatment) ❑
1 Alt. C (Prior Testing) L1
A1t.D (No Prior Test) ❑
Process to Further Reduce Pathogen s Ll
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost ❑
Heat Drying ❑
Heat Treatment ❑
Thermophilic ❑
Beta Ray ❑
Gamma Ray ❑
Pasteurization ❑
Class B:
Alt. (1) Fecal Density 0
Alt. (2) Process to Significantly Reduce Pathogens ❑
If applicable to alternative performed (C:loss B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization ❑
Air Drying ❑
Composting ❑
Aerobic Digestion ❑
Anaerobic Digestion ❑
If applicable to alternative performed (Class A or Class B) complete the following monitoring data:
Parameter
Allowable Level
in Sludge
Pathogen Density
Number
Excee-
den er
Frequency
of Analysis
Sample
Type
Analytical
Tech -
Minimum
Geo. Mean
Maximu
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
1,480
3,514
9,959
MPN/
Gram
0
Quarterly
Grab
SM 9221 C
E
CFU
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per 4 grams
total solid (dry
I weight)
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed:
Alt.l (VS reduction) O
Alt. 2 (40-day bench) ❑
Alt. 3 (30-day bench) ❑
lAlt. 4 (Spec. 0, uptake) ❑
Alt. 5 (14-Day Aerobic) ❑
Alt. 6 (Alk. StabilizationEl
Alt 7 (Drying - Stable) ❑
JAIt. 8 (Drying - Unstable)
Alt. 9 (Injection) ❑
Alt. 10 (Incorporation) ❑
No vector attraction reduction alternatives were performed
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note
if you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Mr. Mark Young, WWTP ORC
Preparer Name and Title (type or print)
2/29/24
Signature of Preparer* Date
Land Applier Name and Title (if applicable)(type or print)
Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 02T (12/2006)

ANNUAL., PATROGEN AND VECTOR ATCRACTION REDUCTION FORM (02T Rules)
Facility Name: Triple S farms & Cleaning
1VWTP Name: Southwest Plantation WWT.P
Monitoring Period: From 112022 To
WQ Permit Number: WQ0030998
NI'DES Number: WQ0029601
12131 /2022
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A:
It. A (timeltelllp) ❑ Alt A (Alk Treattnent) ❑
Alt. C (Prior Testing) ❑
Alt.D (No Prior Test) J f Process to Furthet Reduce Patho'e1lgs
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
('Elul . ost U ficat Di-vitig t--1 Heat 1)enttncnt ❑ Thermo lhllic ❑
Beta Ray ❑
Gamma Rav L7
Pasteurization ❑
Class B:
Alt. (1) Fecal Density ❑
I Alt. (2) Ptoce55 to Significantly Reduce Pathogens El
If applicable to alternative performed (CIass B only) indicate "Process to Siguificantl' Reduce Pathogens":
Lime Stabilization O Air Drying C1 Composting ❑
jAerobic Di cstion ❑
Anaerobic Digestion
If applicable to alternative perfocmed (Class A or Chess B) complete the following monitoringdata:
Parameter
Allowable I el'el
Pat ltocen 13entiit��
un�r o
FFxcce-
FrequFrequencysample
na
yt)ca
rech-
lillttlltill
(iCo. Mean
h'IaXi111tt11
11nits
in S1litlgC
of Atl:11Yi1S
Type
ninue
2 x 10 to Elie
N1PN
6th power
per gram of
Fecal Colifor-nl
total solids
Ct U
1000 mpn per gram
of total solid (dry
Werehtl
Salmonella bactena
3 NIPN per 4 ¢rm1s
(III lieu of renal
total solid ((113'
CohtC)1'111
Wel@ht)
Vector Attraction Reduction (15A NCAC 02T .I107) - Please indicate :alternative performed:
Alt.I (VS reduction) Cl
Alt. 2 (40-day bench) ❑
Alt. 3 (30-day bench) Cl
Alt 4 (Spec. O, uptake) ❑
Alt. 5 (14-Day Aerobic) ❑
Alt. 6 (Alk. Stabilization El
Alt 7 (Drying- Stable) ❑ JAIt.
8 (Drying; - Unstable) ❑
Alt. 9 (Injection) ❑
Alt. 10 (Incorporation) 0
No vector attraction reduction alternatives were performed ❑
CERTIFICATION STATEMENT (please check the appropriate statement)
"1 certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in ISA NCAC 02T .11.07 have been met."
❑ "I certify, under penalty, of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 021' .1107 have not been met." (Please note
if you check this statement attach an explanation why you have not uret one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penaltiesAr false certification including fine and imprisonment."
Mr. SonnN
Preparer Narge
S
W WTP ORC
itle (type or print)
1-and Applier Name and "Title (if applicable)(type or print)
Date Signature of I and Applier (if applicable) Date
*Prel(are/ is delined in 410 CFR Part 503M,r) and 15A NCAC; 2T .1 102 (26)
DENR t-0fW PVRF 02T (12/2006)

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Triple S Farms & Cleaning WQ Permit Number: WQ0030998
WWTP Name: ONWASA Summerhouse WRF WWTP NPDES Number: NCO029945
Monitoring Period: From 1/l/2022 To 12131/2022
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate Lvel achieved and alternative performed:
Class A: It. A (time/temp) ❑
Alt B (Alk Treatment) ❑ 1
Alt. C (Prior Testing) ❑
AIt.D (No Prior Test) ❑ Process to Further Reduce Patio-enas ❑
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost ❑
Heat Drying ❑
Heat Treatment ❑ Thenno hilic ❑
Beta Ray❑
Gamma Ray❑
Pasteurization ❑
Class B:
jAlt. (1) Fecal Density El
I AIt. (2) Process to Significantly Reduce Pathogens ❑
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization ❑ Air Drying ❑
Composting ❑
Aerobic Digestion ❑
Anaerobic Digestion ❑
If applicable to alternative pe med (Class A or Class B) complete the following
monitoring data:
Parameter
Allowable Level
in
in Sludge
Pathogen Density
Numoer of
Excee-
Frequency
of Anal sis
Y
Sample
Type
na ynca
Tech -
inimu
Geo. Mean
aximu
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
462
1,079
1,475
MPN/
Gram
0
Quarterly
Grab
SM 9221
C E
CFU
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per 4 grams
total solid (dry
weight)
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed:
Alt.l (VS reduction) CI
Alt. 2 (40-day bench) ❑
Alt. 3 (30-day bench) ❑
Alt. 4 (Spec. O, uptake) S
Alt. 5 (14-Day Aerobic) ❑
Alt. 6 (Alk Stabilization❑
Alt 7 (Drying - Stable) ❑
I.Alt. 8 (Drying -Unstable) ❑
Alt. 9 (Injection) ❑
Alt. 10 (Incorporation) ❑
No vector attraction reduction alternatives were performed ❑
CERTIFICATION STATEMENT (please check the appropriate statement)
F-11 "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
❑ vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note
if you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Mr. Kary Hemdon `TP ORC
Preparer Names' d Title ` e or print) Land Applier Name and Title (if applicable)(type or print)
' I DIte Signature of Land Applier (if applicable) Date
defined inJJ40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 02T (1212006)

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Triple S Farms & Cleaning
WWTP Name: ONWASA Swansboro WWTP
Monitoring Period: From 1/1/2023 To
WQ Permit Number: WQ0030998
NPDES Number: NCO023261
12/31/2023
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. A (time/temp) ❑
Alt B (Alk Treatment) ❑
r Alt. C (Prior Testing) ❑
A1t.D (No Prior Test) ❑
Process to Further Reduce Patho en s Ll
If applicable to alternative performed (Class A only) indicate "Pibcess to Further Reduce Pathogens":
compost Cl Heat Drying ❑ Heat Treatment ❑ Thernio hilic 1
Beta Ray ❑
Gamma Ray ❑
Pasteurization ❑ d
Class B:
Alt. (1) Fecal Density El
Alt. (2) Process to Significantly Reduce Pathogens ❑
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization ❑
Air Drying ❑
Composting ❑
jAerobic Digestion ❑
Anaerobic Digestion ❑
......
If applicable to alternative perfo,rmed (Class A or Class B) complete the following
monitoring data:
Parameter
Allowable Level
in Sludge
Pathogen Density
um er o
Excee-
Frequency
of Analysis
Sample
Type
Ana ica
Tech -
Minimum
Geo. Mean
MaximuH
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
244
539
1,227
MPN/
Gram
0
Annually
Grab
SM 9221
C E
CFU
1000 mpn per gram
of total solid (dry
wei ht
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per 4 grams
total solid (dry
I weight)
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed:
Alt.1 (VS reduction) ❑
Alt. 2 (40-day bench) ❑
Alt. 3 (30-day bench) ❑
JAR. 4 (Spec. OZ uptake) El
Alt. 5 (14-Day Aerobic) ❑
Alt. 6 (Alk. Stabilization[]
Alt 7 (Drying - Stable) ❑
JAR. 8 (Drying - Unstable) ❑
Alt. 9 (Injection) ❑
Alt. 10 (Incorporation) ❑
No vector attraction reduction alternatives were performed ❑
CERTIFICATION STATEMENT (please check the appropriate statement)
El "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
❑ vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note
if you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Mr. Mark Young WWTP ORC
Preparer Name and Title (type or print)
(� Y&U�Ze 2/26/24
Signature of Prep * V Date
Land Applier Name and Title (if applicable)(type or print)
Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 02T (12/2006)

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Triple S Farms & CIeaning WQ Permit Number: WQ0030998
WWTP Name: Town of Wallace Regional WWTP NPDES Number: NC0003450
Monitoring Period: From 1/l/2023 To 3/31/2023
Patho en Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
g
Class A:
Alt, A (time/tens) ❑
Alt B (Alk Treatment) ❑ I
Alt. C (Prior Testin) ❑
A1t.D (No Prior Test)
Process to Further Reduce Patho en s 0
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost ❑
Heat D in ❑
Heat Treattnen l ❑
Thermo hilic O
Beta Ray ❑
Gamina Ray ❑
Pasteurization ❑
Class B:
JAIL (1) Fecal Density ❑
Alt. (2) Process to Significantly Reduce Pathogens M
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization El
Air Drying ❑
Coniposting ❑ jAerobic
Digestion CI
Anaerobic Digestion ❑
If applicable to alternative performed (Class A or Class B) complete the following monitoring data:
Parameter
Allowable Level
in Sludge
Pathogen Density
INUMOCT 01
Excee-
Frequency
of Analysis
Sample
Yp
Type
na ica
Tech -
inimu
Geo. Mean
aximu
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
CFU
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per 4 grams
total solid (dry
I weight)
venfnr Affrarfinn 1RPdnrtinn f1SA NCAI; 62"1" .11071 - Nease malcate alternative periunueu:
Alt.l (VS reduction) ❑
Alt. 2 (40-day bench) ❑
Alt. 3 (30-day bench) ❑
JAR. 4 (Spec. OZ uptake) ❑
Alt. 5 (14-Day Aerobic) ❑
Alt. 6 (Alk. StabilizationEl
Alt 7 (Drying - Stable) ❑
1 Alt. 8 (Drying - Unstabl T ❑
Alt. 9 (Injection) ❑
Alt. 10 (Incorporation) ❑
No vector attraction reduction alternatives were performed ❑
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
"1 certify, under penalty of law, that the pathogen requirements In 15A NCAC 02T .1106 and the
❑ vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note
if you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision In accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Ms. Lisa Cottle, WWTP ORC
Prep er Name and Title (type or print)
—na &4u 2�lZ-z
Signature of Preparer* Date
Land Applier Name and Title (if applicable)(type or print)
Signature of Land Applier (if applicable)
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
Date
DENR FORM PVRF 02T (12/2006)

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Triple S Farms & Cleaning
WWTP Name: Town of Wallace Regional WWTP
Monitoring Period: From 4/1/2023 To
Pafhnapn Reduction (I SA NCAC 02T .11061- Please indicate level achieved and alternative performed:
WQ Permit Number: WQ0030998
NPDES Number: NC0003450
6/30/2023
Class A:
Alt. A (tineItem) ❑
Alt B (Alk Treattnent) ❑
Alt. C (Prior Testin ❑
Alt.D (No Prior Test) ❑
Process to Further Reduce Patho ens ❑
A indicate "Process to Further Reduce Pathogens":
If applicable to alternative performed (Class only)
Compost ❑
Heat Drying ❑
Heat Treattnent ❑
Thenno hilic ❑
Beta Ra ❑
Gainina Ray ❑
Pasteurization ❑
Class B:
Alt. (1) Fecal Density❑
Alt. (2) Process to SignificantlyReduce Pathogens El
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization O
Air Drying ❑
Com ostin ❑
Aerobic Digestion ❑
Anaerobic Digestion ❑
If applicable to alternative performed (Class A or Class B) complete the following monitoring
data:
Allowable Level
Pathogen Density
um er o
Excee-
Frequency
Sample
na ica
Tech -
Parameter
in Sludge
MinimumGeo.
Mean
Maximum
Unitse.
of Analysis
Y
T e
Type
2 x 10 to the
MPN
6th power
per gram of
Fecal Coliform
total solids
CFU
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
3 MPN per 4 grams
(in lieu of fecal
total solid (dry
colifonn
weight)
Vantnr Affrnrtinn Redurtion (15A 14 HE I 16-7 1 - Please indicate arternadve perrurmeu:
Alt.I (VS reduction) ❑
Alt. 2 (40-day bench) ❑
Alt. 3 (30-day bench) ❑
Alt. 4 (Spec. 0, uptake) ❑
Alt. 5 (14-Day Aerobic) ❑
Alt. 6 (Alk. Stabilization El
Alt 7 (Drying - Stable) ❑
JAIt. 8 (Drying - Unstable) ❑
Alt. 9 (Injection) ❑
Alt. 10 (Incorporation) ❑
No vector attraction reduction alternatives were performed ❑
CERTIFICATION STATEMENT (please check the appropriate statement)
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
❑ vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met" (Please note if
you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Ms. Lisa Cottle, WWTP ORC
Prepa r Name and Title (type or print)
2-IZ-2
Signature of Preparer* Date
Land Applier Name and Title (if applicable)(type or print)
Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 02T (12/2006)

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Triple S Farms & Cleaning WQ Permit Number: WQ0030998
WWTP Name: Town of Wallace Regional WWTP NPDES Number: NCO003450
Monitoring Period: From 7/1/2023 To 9/30/2023
Pa+16neron 12nrinrtinn nsA WAC 02T A 106) - Please indicate level achieved and alternative performed:
Class A:
Alt. A (time/tem) ❑
Alt B (Alk Treatment) ❑ 1
Alt. C (Prior Testing) ❑
Alt.D (No Prior Test) ❑
Process to Further Reduce Patho ens ❑
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost ❑
Heat Drying ❑
Beat Treatment ❑
Thermo ltilic ❑
Beta Ray ❑
Gatnnia Ray ❑
Pasteurization ❑
Class B:
Alt. (I) Fecal Density ❑
Alt. (2) Process to Signi-ficandy Reduce Patho enO
if —applicable to alternative performed (Class B only) indicate "Process to Si nificantky Reduce Pathogens":
Lime Stabilization El
Air Drying ❑
Composting ❑ jAerobic
Digestion ❑
Anaerobic Digestion ❑
If applicable to alternative performed (Class A or Class B) complete the following
monitoring data:
Allowable Level
Pathogen Density
Number o
Excee-
Frequency
Sample
Analytical
Tech -
Parameter
in Sludge
inimu
Geo. Mean
aximu
Units
of Analysis
Y
T enintic
Type
2 x 10 to the
MPN
6th power
CFU
per gram of
Fecal Coliform
total solids
1000 mpn per gram
of total solid (dry
wei ht
Salmonella bacteria
3 MPN per 4 grams
(in lieu of fecal
total solid (dry
f
coliform)
weight)
Vector Attraction Reduction (1AA NCAC vi r .110-/1 - riease inuicare a[aeriiaLivc PCriw iuou:
Alt.1 (VS reduction) ❑
Alt. 2 (40-day bench) ❑
Alt. 3 (30-day bench) ❑
Alt. 4 (Spec. 02 uptake) ❑
Alt. 5 (14-Day Aerobic) ❑
Alt. 6 (Alk. StabilizationEl
Alt 7 (Drying - Stable) ❑ Alt. 8 (Drying - Unstable) ❑
Alt. 9 (Injection) ❑
Alt. 10 (Incorporation) ❑
No vector attraction reduction alternatives were performed ❑
CERTIFICATION STATEMENT (please check the appropriate statement)
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
❑ vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note
if you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Ms. Lisa Cottle, WWTP ORC
Preparer Name and Title (type or print)
�PW k-
Signature of Preparer* Date
Land Applier Name and Title (if applicable)(type or print)
Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 02T (12/2006)

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Triple S Farms & Cleaning WQ Permit Number: WQ0030998
WWTP Name: Town of Wallace Regional WWTP NPDES Number: NCO003450
Monitoring Period: From 10/1/2023 To 12/31/2023
Pathogen Reduction (15A NCAC 02T .1106) -Please indicate level achieved and alternative performed:
Class A:
Alt. A time/tens 01
Alt B (Alk Treatment) T77771C.
C (Prior Testing) ❑
A1t.D (No Prior Test) ❑
Process to Further Reduce Pathogen gs ❑
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost ❑
1 Heat Drying ❑
Heat Treatment ❑
Thermo lulic ❑
Beta Ray ❑
GainniaRay, O
1 Pasteurization ❑
Class B:
jAlt. (1) Fecal Density❑I
Alt. (2) Process to Significantly Reduce Pathogen
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization B
Air Drying ❑
1 Composting ❑
jAerobic Digestion D
Anaerobic Digestion O
............
If applicable to alternative performed (Class A or Class B) complete the followingmonitorin
data:
Parameter
AlloAt�able Level
in Sludge
Pathogen Density
um er o
Excee-
Frequency
of Analenreqysis
Sample
Type
na rca
Tech -
ninne
inimun
Geo. Mean
Maximum
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
WN
CFU
1000 mpn per gram
of total solid (dry
Weisht
Salmonella bacteria
(in lieu of fecal
coliform) I
3 MPNper 4 grams
total solid (dry
iveiaht
Vector Attraction Reduction (15A NCAC 02T .11W) - Please indicate alternative performed:
Alt.1 (VS reduction) ❑
Alt. 2 (40-day bench) ❑
Alt. 3 (30-day bench) ❑
Alt. 4 (Spec. O, uptake) U
Alt. 5 (14-Day Aerobic) ❑
Alt. 6 (Alk. StabilizationCl
Alt 7 (Drying - Stable) ❑
jAlt. 8 (Drying - Unstable) ❑
Alt. 9 (Injection) ❑
Alt. 10 (Incorporation) ❑
No vector attraction reduction alternatives were performed ❑
CERTIFICATION STATEMENT (please check the appropriate statement)
El "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met" (Please note if
you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Ms. Lisa Cottle, WWTP ORC
Prep r
Sier Name and Title (type or print) Land Applier Name and Title (if applicable)(type or print)
oo � AU_ 2A
ature of Preparer* Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 02T (12/2006)

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Triple S Farms & Cleaning WQ Permit Number: WQ0030998
WWTP Name: Town of Warsaw WWTP NPDES Number: WQ0021903
Monitoring Period: From 1/l/2022 To 12/31/2022
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. A (time/temp) ❑
Alt B (Alk Treatment) ❑
Alt. C (Prior Testing) ❑
A1t.D (No Prior Test) ❑
Process to Further Reduce Patho ens ❑
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost 01
Beta Ray ❑
Heat Drying ❑
Heat Treatment ❑
Thenno hilic ❑
Gamma Ra ❑
Pasteurization ❑
Class B:
Alt. (1) Fecal Density ❑
It. (2) Process to Significantly Reduce Pathogens �.
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
•❑
Lime Stabilization 0
Air Drying
Composting ❑
Aerobic Digestion ❑
Anaerobic Digestion ❑
............
If applicable to alternative performed (Class A or Class B) complete the following
monitoring data:
Parameter
Allowable Level
in Sludge
Pathogen Density
Num er o
Excee-
Frequency
Analysis
Sample
Type
Analytical
Tech -
Minimum
Geo. Mean
Maximu
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
_denreqof
CFU
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
(in lieu of fecal
coliform
3 MPN per 4 grams
total solid (dry
weight)
Vector Attraction Reduction (15A NCAC 02T .1107) -Please indicate
alternative
performed:
Alt.l (VS reduction) ❑
Alt. 2 (40-day bench) ❑
Alt. 3 (30-day bench) ❑
1 Alt. 4 (Spec. O, uptake) ❑
Alt. 5 (14-Day Aerobic) ❑
Alt. 6 (Alk. StabilizationEl
Alt 7 (Drying - Stable) ❑
jAlt. 8 (Drying - Unstable) ❑
Alt. 9 (Injection) ❑
Alt. 10 (Incorporation) ❑
No vector attraction reduction alternatives
were performed ❑
CERTIFICATION STATEMENT (please check the appropriate statement)
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note
if you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Mr. Greg Hughes, WWTP ORC
Prepa er Name an Tit (type or print)
Signature o Prepare
Land Applier Name and Title (if applicable)(type or print)
ala-7-la4
Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 02T (12/2006)

PATHOGEN AND VECTOR
ATTRACTION REDUCTION DOCUMENTATION

PATHOGEN REDUCTION AND VECTOR
ATTRACTION REDUCTION DOCUMENTATION
The Town of Beulaville, Town of Kenansville, Town of Warsaw, Town of Bridgeton, Town of
Maysville, Southwest Plantation, Town of Clayton (all except for part of the second quarter) and the
Town of Wallace meet pathogen reduction and vector attraction reduction requirements through
lime stabilization. The Town of Clayton (part of the second quarter) met pathogen reduction
through fecal density and vector attraction reduction through injection or incorporation. ONWASA
facilities Northwest Regional, Summerhouse and Swansboro met pathogen reduction and vector
attraction reduction through fecal density and SOUR testing.
Documentation of these activities are found in the following section.

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Town of Clayton
Little Creek Water Reclamation Facility
W Q0023178
Apr-23
Waypoint Analytical
b #..:.
Date Analyzed
k'eeal'Col orm
per.g; rats
....
:.:.:.:.:.:
......:::::::::::::.::..
HT-1
4/18/23
59
1.771
HT-2
4/18/23
56
1.748
HT-3
4/18/23
54
1.732
HT-4
4/18/23
55
1.740
HT-5
4/18/23
54
1.732
HT-6
4/18/23
63
1.799
HT-7
4/18/23
58
1.763
Total ` X87
Average . . 1 `..... ; '
Most Probable Number / Gram ...... S7`:=:=:: .... Fecal Coliform/gram
Fecal Coliform values are less than 2,000,000 and meets the Class B pathogen reduction
requirement
Data provided in this summary have been used for the values and geometric means
reported on the Annual Pathogen and Vector Attraction Reduction Form for this land
application event.

a
Waypoinumw
J ANALYTICAL
``
114 OAKMONT DRIVE
GREENVILLE, N.C. 27858
TOWN OF CLAYTON
MR. BILL SIMPSON
P.O. BOX 879
CLAYTON, NC 27528
Drinking Water ID: 37715
IDFV IV
PHONE [phone]
FAX [phone]
ID#: 890 I
DATE COLLECTED: 04/18/23
DATE REPORTED : 04/25/23
REVIEWED BY:
Sample Sample Sample Sample Sample Analysis 1%lethod
PARAMETERS #1 #2 #3 #4 #5 Date Analyst Code
Total Residue, mg/l 34100 31967 33567 33033 33133 04/19/23 JDJ 254OB-15
Fecal Coliform (1NIPN), /gram Solids 59 <56 <54 <55 54 04/18/23 BNC 9221E-14

f
WaypA nt
ANALYTICAL
114 OAKMONT DRIVE
GREENVILLE, N.C. 27858
TOWN OF CLAYTON
MR. BILL SIMPSON
P.O. BOX 879
CLAYTON, NC 27528
PARAIME, TERS
Total Residue, mg/I
Fecal Coliform (NIPN), /gram Solids
Drinking Water ID: 37715
PHONE [phone]
FAX [phone]
ID#: 890 I
DATE COLLECTED: 04/18/23
DATE REPORTED : 04/25/23
REVIEWED BY:
Sample Sample Analysis iblethod
#6 N7 Date Analyst Code
31900 32767 04/19/23 JDJ 2540B-15
63 <58 04/18/23 BNC 9221E-14

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Rey 4 21 20"
ti;hmke Stabilization Record
Tov.n of Clayton
S:am's Branch Water Reclamation Facilit% Nrmit: NO)O2
t-olunie Treated:
IRali Used: CA CO 3
V olume C+e(l:
Time Foate
Initial
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afterAddition
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Preparer:
Correction Final Temp
I'1Ct)r __p.fi CC)
p,� t2.5�d tS
— 0.�I RA IT. c
f1�te Time
Puffer
-- Readit}u_
Temp (=C-�
NIA --
---
oc�
I-.yc.'
tv
BA
lilt:
slope: -5' "o
Fff:
Date -rime Buffer
�—I. ex,
Reading -- Temp ('C) M` --
_� •yam l���y� �ti•j ..�L�
[nt: Slope: " 7. �� _ �,, Lff: li '7

key 4 WHO
_'H ti
loon ! i ( t- l p u rn
%.iiti iiiam
A %Awr Nee I. mito"i {'.iitl
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,( tit;2415Zm
� 1
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t
!into Dare InNi.,l
i nvr1,� ctioIi
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l::m{!
1.53
z1 3
�Irt.'i' .1(ItllftU[t
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i2_L..
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c:,rr�tiiionl-- -U
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•
1 :17 A/9101 Z'33
- p. o (�
12.32.
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—.
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-
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i-t.tro J irne Bul'icr
To,

Rev 4/21/2022
Sludge Stabilization Record
Town of Clayton
Sam's Branch Water Reclamation Facility Permit: NC0025453
Date:
Location:
Volume Treated: ?Z90 r 000
Alkali Used:
Volume Used: 'Z CCJ G (c'
Time / Date
Initial
Correction
Final
Temp
H
Factor
PH
°C)
Initial
i i
q 7
After Addition
(>= 12.00 after temp.
)2. 2--L
r l . 3 -7
Zl
correction)
Two IIrs. After Addition
4
I�c,v� 1/l6(L
21
1- 15
(Z 34"
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correction)
24 Hrs. after Addition
j Z l
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� '07-71L7/,t
i Z. IZ
� Oq
T.7.
correction)
Preparer: Ll"4✓
Date / Time
Buffer
Reading
Temp (IC)
My
7vo/2L
0
22, '7
/Ga• 6
o v
Z2,
y'
�o.uv
22,
�16./
2.2.
320.g
Int• A,- Slope: - 3 %, 9 2 % Eff: 9(
Date / Time
Buffer
Reading
Temp (°C)
My
. CsC>
7 Oclt°
S
L;
Int: C-- " Slope: --S (, I kV % Eff:

Rev 4 M2022
hmi ;e Stabilization Record
Town or mysm
`'ianCs i;ruch Wtvr kecNnuItion. I&cilhy 1"2 cKh 'r'C'i_i(1'A_N
A
Volu1110 Treated: 30 Oav I, AIkaIi Us
Volume Usi•,r: 6 .S'Soo��.
-Iiti1C f7;ife
fnitlal
i_.01't'CCrUJt!
r'inal—T.til(�---•
p1l
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-92• -� •�
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—
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i
1 �G
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9�Z3
110 after tend).
�,cyvv�
�J
[r 1
Pr'eparer:
i Dati I'If'tit faUtr':1'
-- -- — ------
Rea!i11111.E
1.
-=---
41
._._—
lut: Agallv Slope:
_�G,Z3_
t;;� Err:
Date_` finie LBufFeI-
Ite ldin;; ;Tem'C')
—fly/Z_S b � . a V ---- a s —'Z p ((
�� ---
-174,7
----------_----- fnr; �v_3 �t� Mope:

Rec -t 't:-.,ON
�Ill,i ;e itabili.catiurl I ecol"ll
Fo" n of C by toil
'Yaws 1-ho ch WaUr Reclamation VANQ Permit: V:002541;
t)iliiil: Treated: h �lL\.11�(.�L�, AM �.:;i tt�—
�f l t�iL,(1: _95 �l1 1!✓�
--_—lime Bate —Initial
(7orrec:tit.)n
i'inal Terlp--
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pH
AM AddMun
t = 1210 after temp.
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i i FlAn .fitter A.{idMon
W 12MO lifter temp. '
lv � f3</2_3_�•_�.� �� �C�'.---�2:.37
7
_-�.orrection) ---�.�
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4 C05 C)C(
/Z Z 1
1
- --_z:L
---
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co
tul
��.C,
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['em � ('C')
11c
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�., Eff: 4_� _

I'll e \ 4 .1. 1 - 19 i.'_
Iv"n of C L"no
ti im', Wanch %tor RvehinIAMIl Ohn Arnlin V MAE'
qtA5-213
4
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)a � c 1114 i A f orre.thn Finvil Tenip
-- - . [?I[ - -- - - p1l, L---_-
1 2MO after IvIllp. Ll Lj Z(p D
I o IN, After Addiriufl
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12.31 12.3? .5'
2 1 Hr; setterAddition
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hit:

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-
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t_•ort-ocrioll Final F'elup
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_
date :' "I ifne
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Per 4 ? 42022
Aid: e Stabifi.cM)n Recorii
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SaWs Munch tt'.it.r Rodaril,Kon Faci(ftt Pa nit: NC:t 02541;
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Sludge Stabilization tlecord
Co" n of Clay Mn
SanCs 1i11 nch Water Reclamation f:acilit't Permit: ,Nt-I}02 ,5_}
61-2 --
Location: Lh
Vohim-- Treated: �'j (-?-C''
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Northwest Regional WWTP
Northwest Regional WWTP
WQ0034367
May-23
Environmental Chemists, Inc.
......... I ................
..... ........
...................
...........
...............
.. ......................
. .......
..................
... .... ...
.. ............................. ...
.............
...............
........................................................
.............
.
. ......................
.......
....................
.........................
...................... ......
..................................
..................... .
.......................
...................... ...........
...............
.............................................
.............. ..............
...............
.............................
............................. .............................
23-26433
5/25/23
2,208
3.344
23-26434
5/25/23
3,543
3,549
23-26435
5/25/23
3,435
3.536
23-26436
5/25/23
1,480
3.170
23-26437
5/25/23
9,959
3.998
23-26438
5/25/23
5,653
3.752
23-26439
5/25/23
1,954
3.470
TotaIL",
.... .........
..........
Average
Most Probable Number / Gram :
..7 37514; ]Fecal Coliferm
Fecal Coliform values are less than 2,000,000 and meets the Class B pathogen reduction
requirement
Data provided in this summary have been used for the values and geometric means
reported on the Annual Pathogen and Vector Attraction Reduction Form for this land
application event.

ANALYTICAL & CONSULTING CHEMISTS
Onslow Water & Sewer Authority
228 Georgetown Road
Jacksonville NC 28540
Attention
Lab ID Sample ID:
23-26433 Site: Digester #1
Test
Total Solids (%)
Fecal Density
Lab ID
Sample ID:
23-26434
Site: Digester #2
Test
Total Solids (%)
Fecal Density
Lab ID
Sample ID:
23-26435
Site: Digester #3
Test
Total Solids (%)
Fecal Density
Lab ID
Sample ID:
23-26436
Site: Digester #4
Test
Total Solids (%
Fecal Density
Lab ID Sample ID:
3-26437 Site: Digester #5
Test
Total Solids (%)
Fecal Density
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
infoott.environmentalchemists.com
Date of Report: May 31, 2023
Customer PO #:
Customer ID: 08100092
Report #: 2023-10521
Project ID: Northwest RWRF Digester
Collect Date/Time Matrix Sampled by
5/24/2023 9:34 AM Solid/Sludge Mark Young
Method Results Date Analyzed
SM 2540 8
SM 9221C E-2014
Collect Date/Time
5/24/2023 9:38 AM
Method
SM 2540 B
SM 9221C E-2014
Collect Date/Time
5/24/2023 9:40 AM
Method
2.22 % 05/25/2023
2208 MPN/g 05/24/2023
Matrix Sampled by
Solid/Sludge Mark Young
Results Date Analyzed
2.23 % 05/25/2023
3543MPN/g 05/24/2023
Matrix Sampled by
Solid/Sludge Mark Young
Results Date Analyzed
SM 2540 B
2.30 %
05/25/2023
SM 9221C E-2014
3435 MPN/g
05/24/2023
Collect Date/Time
Matrix Sampled by
5/24/2023 9:42 AM
Solid/Sludge Mark Young
Method
Results Date Analyzed
SM 2540 B
2.23 %
05/25/2023
SM 9221C E 2014
1480 MPN/g
05/24/2023
Collect Date/Time
Matrix Sampled by
5/24/2023 9:44 AM
Solid/Sludge Mark Young
Method
Results Date Analyzed
SM 2540 B
2.41 %
05/25/2023
SM 9221C E-2014
9959 MPN/g
05/24/2023
Report 9: 2023-10521 Page 1 of 2

k L envirochem A
;u
ANALYTICAL 8 CONSULTING CHEMISTS
77
Onslow Water & Sewer Authority
228 Georgetown Road
Jacksonville NC 28540
Attention
Lab ID R Sample ID:
23-26438 Site: Digester #6
Test
Total Solids (%)
Fecal Density
Lab ID Sample ID:
23-26439 Site: Digester #7
Test
Total Solids (%)
Fecal Density
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab * 910.392.4424 Fax
710 Sowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
infoCenvironmentalchem ists.com
Date of Report: May 31, 2023
Customer PO M
Customer ID: 08100092
Report M 2023-10521
Project ID: Northwest RWRF Digester
Collect Date/Time Matrix Sampled by
5/24/2023 9:45 AM Solid/Sludge Mark Young
Method
SM 2540 B
SM 9221C E-2014
Results Date Analyzed
2.30 %
5653 MPN/g
05/25/2023
05/24/2023
Collect Date/Time Matrix Sampled by
5/2412023 9:48 AM Solid/Sludge Mark Young
Method Results Date Analyzed
SM 2540 B
SM 9221 C E-2014
Comment: Results reported on a dry weight basis
Reviewed by:
r�
2.37 % 05/25/2023
2954 MPN/g 05/24/2023
Report # 2023.10621 Page 2 of 2

Environmental Chemist, Inc., Wilmington, NC Lab #94
Sample Receipt Checklist
6602 Windmill Way
Wilmington, NC 28405
910.392.0223
Client:iuw"A� Date:/Q`( Number: _ 2023- O
Receipt of sample: ECHEM Pickup Client De 'very ❑
UPS ❑ FedEx ❑ Other ❑
❑ YES
❑ NO
d N/A I. Were custody seals present on the cooler?
❑ YES
❑ NO
N/A 2. If custody seals were present, were they intact/unbroken?
Original temperature upon receipt °C Corrected temperature upon receipt _ °C
How temperature taken: ❑ Temperature Blank ® Against Bottles
IR Gun ID: Thomas Traceable S/N 210886869 IR Gun Correction Factor °C: 0.0
YES
❑ NO
3. If temperature of cooler exceeded 6°C, was Project Mgr./QA notified?
rA YES
❑ NO
4. Were proper custody procedures (relinquished/received) followed?
l YES
❑ NO
5. Were sample ID's listed on the COC?
YES
❑ NO
6. Were samples ID's listed on sample containers?
YES
❑ NO
7. Were collection date and time listed on the COC?
YES
❑ NO
8. Were tests to be performed listed on the COC?
10 YES
❑ NO
9. Did samples arrive in proper containers for each test?
R YES
❑ NO
10. Did samples arrive in good condition for each test?
M YES
❑ NO
11. Was adequate sample volume available?'
4a YES
❑ NO
12. Were samples received within proper holding time for requested tests?
❑ YES
❑ NO
13. Were acid preserved samples received at a pH of <2?
❑ YES
❑ NO
14. Were cyanide samples received at a pH >12?
❑ YES
❑ NO i15.
Were sulfide samples received at a pH >9?
❑ YES
❑ NO
16. Were NH3/TKN/Phenol received at a chlorine residual of <0.5 m/L? **
❑ YES
❑ NO
17. Were Sulfide/Cyanide received at a chlorine residual of <0.5 m/L?
❑ YES
❑ NO
18. Were orthophosphate samples filtered in the field within 15 minutes?
* TOC/Volatiles are pH checked at time of analysis and recorded on the benchsheet.
** Bacteria samples are checked for Chlorine at time of analysis and recorded on the benchsheel.
Sample Preservation: (Must be competed for any sample(s) incorrectly preserved or with headspace)
Sample(s) were received incorrectly preserved and were adjusted accordingly
by adding (circle one): H2SO4 HNO3 HCl NaOH
Time of preservation: If more than one preservative is needed, notate in comments below
Note: Notify customer serv'ce immed ate;y for ncorrectly preserved samples. Obtain a new sample or
notify the state lab if directed to analyzed by the customer. Who wa, notified, date and time
Volatiles Sample(s) were received with headspace
COMMENTS:
DOC. OA.002 Rev 1

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d
W
C
LL
F
a
CD
E
N
N
N
m
aNi
w
N
_
0
0
ol
_
0
_
0
_
0
rr
CV

Northwest Regional WWTP
Northwest Regional WWTP
WQ0034367
Annual 2023
:::: ,�:::.:r
6/20/2023
0.34
11 / 16/2023
0.05
11 /20/2023
0.11
11 /21 /2023
0.08
11 /22/2023
0.06
11/23/2023
0.10
11/24/2023
0.16
11 /25/2023
0.16
11 /26/2023
0.07
11 /29/2023
0.09
12/2/2023
0.02
12/4/2023
0.15
12/7/2023
0.21
12/8/2023
0.19
12/ 11 /2023
0.30
12/12/2023
0.33
12/13/2023
0.22
12/ 14/2023
0.26
12/15/2023
0.54
12/16/2023
0.38
12/17/2023
0.15
12/21 /2023
0.25
12/22/2023
0.59
12/23/2023
0.18
12/24/2023
0.36
12/28/2023
0.26
* SOUR = Specific Oxygen Uptake Rate
Average : >::' 0 26
SOUR values are less than 1.5 mg oxygen/graWhour and meets the 40 CFR Part
503.33 Option 4 for Vector Attraction Reduction.
SOUR values provided by Northwest Regional WWTP

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name: Nc
Biosolids Permit Number: NC
Date:
Digester Temperature:
Sampling Date/Time: 6/.'
Sampled By: M.
Analysis Date/Time:
Analyzed By: M.
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
6.62
6.48
6.33
6.14
5.99
5.87
5.74
5.66
5.9
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
RWRF
3 - 1100
l9 % Dry Solids
3 degrees Celsius
1 degrees Celsius
0.14
6.7
1.00
8.55 mg Oxygen/hr
0.43 mg Oxygen/hr/g
25 degrees Celsius
0.78
Temperature Corrected Specific Oxygen Uptake Rate:1 mg Oxygen/hr/g
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.
Updated 10/23/2013

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name: NW
Biosolids Permit Number: NCL110149
Date: 11/11
Digester Temperature:
Sampling Date/Time.
Sampled By: RR/PJP
Analysis Date/Time: 11/1
Analyzed By:
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
7.23
7.23
7.21
7.19
7.18
7.16
7.15
7.13
7.12
7.09
0
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
1
0.02
7.3
0.98
Dry Solids
grees Celsius
grees Celsius
1.00 mg Oxygen/hr
0.05 mg Oxygen/hr/g
19 degrees Celsius
1.07
Temperature Corrected Specific Oxygen Uptake Rate:1 0.05 mg Oxygen/hr/g
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.
Updated 10/23/2013

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
7.51
7.43
7.37
7.31
7.23
7.17
7.15
7.14
7.13
7.09
7.07
7.05
7.01
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
18.
Dry Solids
agrees Celsius
agrees Celsius
0.03
7.4
0.97
2.06 mg Oxygen/hr
0.10 mg Oxygen/hr/g
19 degrees Celsius
1.07
Temperature Corrected Specific Oxygen Uptake Rate: mg Oxygen/hr/g
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.
Updated 10/23/2013

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name
Biosolids Permit Number
Date
Digester Temperature
Sampling Date/Time
Sampled By
Analysis Date/Time
Analyzed By
Total Solids
Beginning Temperature
End Temperature
Dissolved Oxygen Level
7.34
7.3
7.27
7.24
7.21
7.19
7.17
7.15
7.12
7.11
7.09
7.07
7.03
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
PNC
rthwest RWRF
L110149
11 /21 /2023
18.7
11 /21 /2023 12:16
R. Riggs
11 /21 /2023 12:27
R. Riggs
2
18.7
18.9
0.02
7.4
0.99
Yo Dry Solids
legrees Celsius
legrees Celsius
1.47 mg Oxygen/hr
0.07 mg Oxygen/hr/g
19 degrees Celsius
1.07
Temperature Corrected Specific Oxygen Uptake Rate:1 0.08 mg Oxygen/hr/g
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.
Updated 10/23/2013

Time
(minutes)
0
1
2
3
4
5
6
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name: NWRWWTP
Biosolids Permit Number:
Date
Digester Temperature
Sampling Date/Time
Sampled By
Analysis Date/Time
Analyzed By
Total Solids
Beginning Temperature
End Temperature
Dissolved Oxygen Level
N.
R
6.53
6.51
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
11 /22/2023 11:50
Riggs
11 /22/2023 12:00
Riggs
2 % Dry Solids
19.2 degrees Celsius
19.6 deorees Celsius
0.02
6.6
0.99
1.03 mg Oxygen/hr
0.05 mg Oxygen/hr/g
19 degrees Celsius
1.07
Temperature Corrected Specific Oxygen Uptake Ratel 0.06 mg Oxygen/hr/g
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.
Updated 10/23/2013

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name: N'
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By: R
Analysis Date/Time:
Analyzed By: R
Total Solids:
Beginning Tern
End Tern
Dissolved Oxygen Level
7.04
7.03
7.01
6.97
6.94
6.9
6.87
6.83
6.8
6.77
6.73
6.71
6.69
6.66
6.63
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
23-Nov-23
19.5
11/23/2023
1
1
0.03
7.1
1.00
Dry Solids
grees Celsius
arees Celsius
1.84 mg Oxygen/hr
0.09 mg Oxygen/hr/g
19 degrees Celsius
1.07
Temperature Corrected Specific Oxygen Uptake Rate:1 mg Oxygen/hr/g
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.
Updated 10/23/2013

Time
(minutes)
0
1
2
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time.-
Sampled By:
Analysis Date/Time:
Analyzed By:
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
7,
7,
7.2
71
7.1
71
7a
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
NWRWWTP
24-Nov-23
18.9
11 /24/2023
R Riggs
11 /24/2023
2 % Dry Solids
18.9 degrees Celsius
18.7 degrees Celsius
0.05
7.5
0.91
3.04 mg Oxygen/hr
0.15 mg Oxygen/hr/g
19 degrees Celsius
1.07
Temperature Corrected Specific Oxygen Uptake Rate:1 0.16 mg Oxygen/hr/g
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.
Updated 10/23/2013

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name: NWRWWTP
Biosolids Permit Number:
Date: 25-Nov-23
Digester Temperature: 19
Sampling Date/Time: 11/25/2023
Sampled By: R Riggs
Analysis Date/Time: 11/25/2023
Analyzed By: R Riggs
Total Solids: 2 % Dry Solids
Beginning Temperature: 19 degrees Celsius
End Temperature: 19 degrees Celsius
Dissolved Oxygen Level
7.66
7.48
7.25
7.19
7.17
7.13
7.1
7.05
7.01
6.96
6.93
6.9
6.85
q
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
0.05
7.4
0.94
2.90 mg Oxygen/hr
0.15 mg Oxygen/hr/g
19 degrees Celsius
1.07
Temperature Corrected Specific Oxygen Uptake Rate:1 0.16 mg Oxygen/hr/g
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.
Updated 10/23/2013

Time
(minutes)
0
1
2
3
4
5
6
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
7.6
7.6
76
7.6
76
7.6
76
7.5
75
77
77
77
77
773
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
11
18
2 % Dry Solids
88.2 degrees Celsius
18.3 deorees Celsius
0.02
7.7
0.96
1.30 mg Oxygen/hr
0.06 mg Oxygen/hr/g
18 degrees Celsius
1.14
Temperature Corrected Specific Oxygen Uptake Rate:1 0.07 mg Oxygen/hr/g
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.
Updated 10/23/2013

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
1 11 /29/20231
6.84
6.84
6.8
6.79
6.76
6.73
6.69
6.66
6.64
6.61
6.59
6.56
6.54
6.51
6.48
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
11
42 % Dry Solids
17.6 degrees Celsius
17.8 degrees Celsius
0.03
6.9
0.99
1.55 mg Oxygen/hr
0.08 mg Oxygen/hr/g
18 degrees Celsius
1.14
Temperature Corrected Specific Oxygen Uptake Rate:1 0.09 mg Oxygen/hr/g
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.
Updated 10/23/2013

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name: NW
Biosolids Permit Number: NCL110149
Date: 12/2/2023
Digester Temperature:
Sampling Date/Time: 13:12 PM
Sampled By: EJC
Analysis Date/Time: 12/2/23/13
Analyzed By: EJC
Total Solids.
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
7.26
7.28
7.29
7.3
7.3
7.3
7.29
7.29
6.71
7.28
7.27
7.26
7.25
7.23
7.22
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
1
0.01
7.3
0.19
Dry Solids
grees Celsius
arees Celsius
0.34 mg Oxygen/hr
0.02 mg Oxygen/hr/g
18 degrees Celsius
1.14
Temperature Corrected Specific Oxygen Uptake Rate:1 mg Oxygen/hr/g
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.
Updated 10/23/2013

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name:
NWRWWTP
Biosolids Permit Number:
Date:
4-Dec-23
Digester Temperature:
17.7
Sampling Date/Time.
12/4/2023
Sampled By:
R Riggs
Analysis Date/Time:
12/04/23
0952
Analyzed By:
R Riggs
Total Solids:
2
% Dry Solids
Beginning Temperature:
17.7
degrees Celsius
End Temperature:
17.8
degrees Celsius
Dissolved Oxygen Level
7.85
7.62
7.52
7.49
7.44
7.41
7.38
7.35
7.33
7.31
7.28
7.26
d7.24
7.22
7.2
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
0.05
7.8
0.88
2.70 mg Oxygen/hr
0.14 mg Oxygen/hr/g
18 degrees Celsius
1.14
Temperature Corrected Specific Oxygen Uptake Rate:1 mg Oxygen/hr/g
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.
Updated 10/23/2013

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name: N
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time: 1:
Sampled By: R
Analysis Date/Time: 1:
Analyzed By: R
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
6.71
5.98
5.97
5.96
5.91
5.87
5.83
5.78
5.76
5.72
5.69
5.66
5.63
q5.6
5.57
5.52
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
17.1
1.75 % Dry Solids
17.1 degrees Celsius
17.2 degrees Celsius
0.05
6.2
0.83
2.93 mg Oxygen/hr
0.17 mg Oxygen/hr/g
17 degrees Celsius
1.23
Temperature Corrected Specific Oxygen Uptake Rate:1 0.21 mg Oxygen/hr/g
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.
Updated 10/23/2013

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name: N'
Biosolids Permit Number:
Date: Oi
Digester Temperature:
Sampling Date/Time: 1:
Sampled By: R
Analysis Date/Time: 1:
Analyzed By: R
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
6.71
6.54
6.45
6.38
6.32
6.27
6.23
6.19
6.15
6.12
6.08
6.05
6.02
5.99
5.97
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
17
1.8 % Dry Solids
17.5 degrees Celsius
17.2 degrees Celsius
0.05
6.6
0.97
2.73 mg Oxygen/hr
0.15 mg Oxygen/hr/g
17 degrees Celsius
1.23
Temperature Corrected Specific Oxygen Uptake Rate:1 mg Oxygen/hr/g
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.
Updated 10/23/2013

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name: NWRWW'
Biosolids Permit Number:
Date: 11
Digester Temperature:
Sampling Date/Time: 12/11/23
Sampled By: R Rig
Analysis Date/Time: 12/11
Analyzed By: R Rig
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
7.47
7.39
7.35
7.29
7.23
7.21
7.16
7.1
7.08
7.06
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
16
1248
1253
1.08 % Dry Solids
16 degrees Celsius
17.5 degrees Celsius
0.04
7.5
0.98
2.61 mg Oxygen/hr
0.24 mg Oxygen/hr/g
17 degrees Celsius
1.23
Temperature Corrected Specific Oxygen Uptake Rate:1 mg Oxygen/hr/g
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.
Updated 10/23/2013

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name: NWRWWTP
Biosolids Permit Number:
Date:MRiggs
2
Digester Temperature:.
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:Total
Solids:1Beginning
Temperature:.End
Temperature:.
Dissolved Oxygen Level
6.31
6.2
6.09
6
5.96
5.91
5.87
5.84
5.8
5.75
5.72
5.69
d
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
0.05
6.3
0.97
Dry Solids
grees Celsius
arees Celsius
3.00 mg Oxygen/hr
0.27 mg Oxygen/hr/g
17 degrees Celsius
1.23
Temperature Corrected Specific Oxygen Uptake Rate: 0.33 mg Oxygen/hr/g
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.
Updated 10/23/2013

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name
Biosolids Permit Number
Date:VRiggs
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
5.89
5.85
5.83
5.81
5.78
5.76
5.74
5.69
5.65
5.63
5.58
5.56
5.53
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
1020
1025
1.08 % Dry Solids
16.5 degrees Celsius
17.31degrees Celsius
0.03
5.9
0.99
1.90 mg Oxygen/hr
0.18 mg Oxygen/hr/g
17 degrees Celsius
1.23
Temperature Corrected Specific Oxygen Uptake Rate:1 mg Oxygen/hr/g
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.
Updated 10/23/2013

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name: NWRWWTP
Biosolids Permit Number:
Date: 14-Dec-23
Digester Temperature: 16
Sampling Date/Time: 12/14/23 1224
Sampled By: R Riggs
Analysis Date/Time: 12/14/23 1228
Analyzed By: R Riggs
Total Solids: 1.08 % Dry Solids
Beginning Temperature: 16 degrees Celsius
End Temperature: 16.1 degrees Celsius
Dissolved Oxygen Level
6.39
6.34
6.29
6.25
6.22
6.19
6.16
6.14
6.11
6.08
6.06
6.03
6.02
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
0.04
6.4
0.92
2.12 mg Oxygen/hr
0.20 mg Oxygen/hr/g
16 degrees Celsius
1.31
Temperature Corrected Specific Oxygen Uptake Rate:1 mg Oxygen/hr/g
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.
Updated 10/23/2013

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name: NWRWWTP
Biosolids Permit Number:
Date: 15-Dec-2
Digester Temperature: 16.
Sampling Date/Time: 12/15/23 1212
Sampled By: R R
Analysis Date/Time: 12/1
Analyzed By: R R
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
7.1
9M
4
1.1
6.1
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
1217
1
0.08
7.1
0.92
Dry Solids
grees Celsius
❑rees Celsius
4.69 mg Oxygen/hr
0.41 mg Oxygen/hr/g
16 degrees Celsius
1.31
Temperature Corrected Specific Oxygen Uptake Rate:1 0.54 mg Oxygen/hr/g
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.
Updated 10/23/2013

Time
(minutes)
0
1
2
4
5
6
7
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name: NW
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time: 12/
Sampled By: R R
Analysis Date/Time: 12/
Analyzed By: R R
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
6.2
720
61
6.1
6C
6C
5!
5E
5�
5.E
5f
5f
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
Dry Solids
egrees Celsius
egrees Celsius
0.05
6.5
0.95
3.12 mg Oxygen/hr
0.29 mg Oxygen/hr/g
16 degrees Celsius
1.31
Temperature Corrected Specific Oxygen Uptake Rate: 0.38 mg Oxygen/hr/g
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.
Updated 10/23/2013

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name: NWRWWTP
Biosolids Permit Number:
Date: 17-Dec-:
Digester Temperature: 14
Sampling Date/Time: 12/17/23 1255
Sampled By: E. Collins
Analysis Date/Time: 12/17/23 1300
Analyzed By: E. Collins
Total Solids: 1
Beginning Temperature: 14
End Temperature:
Dissolved Oxygen Level
6.51
6.45
6.41
6.38
6.34
6.31
6.27
6.25
6.22
6.19
6.16
6.14
6.13
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
0.03
6.5
0.99
Dry Solids
grees Celsius
arees Celsius
1.91 mg Oxygen/hr
0.13 mg Oxygen/hr/g
15 degrees Celsius
1.40
Temperature Corrected Specific Oxygen Uptake Rate:1 0.18 mg Oxygen/hr/g
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.
Updated 10/23/2013

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name: NWRWWTP
Biosolids Permit Number:
Date: 21-Dec-2
Digester Temperature: 13.
Sampling Date/Time: 12/21/23 0902
Sampled By: R Rig
Analysis Date/Time: 12/21
Analyzed By: R Rig
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
6.19
6.17
6.13
6.1
6.06
6.02
5
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
1
0.03
6.2
0.99
Dry Solids
grees Celsius
arees Celsius
1.82 mg Oxygen/hr
0.17 mg Oxygen/hr/g
14 degrees Celsius
1.50
Temperature Corrected Specific Oxygen Uptake Rate:1 mg Oxygen/hr/g
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.
Updated 10/23/2013

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
6.42
6.3
6.2
6.11
6.04
5.97
5.93
5.87
5.84
5.79
5.75
5.72
5.69
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
R
R
1
1.08 % Dry Solids
14 degrees Celsius
14.3 degrees Celsius
0.07
6.6
0.94
4.22 mg Oxygen/hr
0.39 mg Oxygen/hr/g
14 degrees Celsius
1.50
Temperature Corrected Specific Oxygen Uptake Rate: 0.59 mg Oxygen/hr/g
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.
Updated 10/23/2013

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
15.7
12/22/23 1055
E.Collins
12/22/23 1100
1E.Collins
7.27
7.18
7.11
7.06
7.02
6.97
6.93
6.9
6.87
6.83
6.8
6.77
6.74
6.72
6.68
6.65
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
1.7 % Dry Solids
15.7 degrees Celsius
15.9 degrees Celsius
0.04
7.2
0.99
2.29 mg Oxygen/hr
0.13 mg Oxygen/hr/g
16 degrees Celsius
1.31
Temperature Corrected Specific Oxygen Uptake Rate:1 0.18 mg Oxygen/hr/g
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.
Updated 10/23/2013

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name: NWRWWTP
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time: 1:
Sampled By: R
Analysis Date/Time: 1:
Analyzed By: R
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
7
6.8
6.7
6. 55
6.58
C:1�y
14.8
1.14 % Dry Solids
14.8 degrees Celsius
15.2 degrees Celsius
Slope: 0.05
Intercept: 6.9
Correlation Coefficient: 0.97
Oxygen Uptake Rate: 2.94 mg Oxygen/hr
Ambient Specific Oxygen Uptake Rate: 0.26 mg Oxygen/hr/g
Average Temperature: 15 degrees Celsius
Temperature Correction Factor: 1.40
Temperature Corrected Specific Oxygen Uptake Rate:1 mg Oxygen/hr/g
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.
Updated 10/23/2013

Time
(minutes)
0
1
2
3
4
5
6
8
0
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time.
Sampled By:
Analysis Date/Time:
Analyzed By:
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
6.3
6.3
6.2
20
6.1
1
1
0M
6.0
6.0
90
5.9
5.9
[EE.Collins
WRWWTP
28-Dec-23
14
12/28/2023
12/28/2023
Collins
1.5
14
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
0.04
6.5
0.98
Dry Solids
grees Celsius
orees Celsius
2.58 mg Oxygen/hr
0.17 mg Oxygen/hr/g
14 degrees Celsius
1.50
Temperature Corrected Specific Oxygen Uptake Rate:1 mg Oxygen/hr/g
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.
Updated 10/23/2013

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Summerhouse WWTP
Summerhouse WWTP
WQ0029945
May-23
Environmental Chemists, Inc.
Laib #
...................................
Date Anal ed;
........
Most Probable Number
per gram
Log
23-20297
4/26/23
798
2.902
23-20298
4/26/23
462
2.665
23-20299
4/26/23
1,475
3.169
23-20300
4/26/23
1,346
3.129
23-20301
4/26/23
1,465
3.166
23-20302
4/26/23
1,217
3.085
23-20303
4/26/23
1,307
3.116
Total1:23Z
Average 3.033
Most Probable Number 1 Gram 079` ]Fecal Coliform
Fecal Coliform values are less than 2,000,000 and meets the Class B pathogen reduction
requirement
Data provided in this summary have been used for the values and geometric means
reported on the Annual Pathogen and Vector Attraction Reduction Form for this land
application event.

envirochem
..
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
[e-mail]
Onslow Water & Sewer Authority Date of Report: May 11, 2023
228 Georgetown Road Customer PO M
Jacksonville NC 28540 Customer ID: 08100092
Attention: Report #: 2023-08017
Project ID: Summerhouse
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
23-20297 Site: 1 4/25/2023 7:36 AM Solid/Sludge Kay Herndon
Test
Method
Results Date Analyzed
Total Solids (%)
SM 2540 B
1.63 % 04/26/2023
Fecal Density
SM 0221C E-2014
798 MPN/g 04/25/2023
Lab ID Sample ID:
Collect Date/Time
Matrix Sampled by
23-20298 Site: 2
4/25/2023 7:38 AM
Solid/Sludge Kay Herndon
Test
Method
Results Date Analyzed
Total Solids (%)
SM 2540 B
1.69 % 04/26/2023
Fecal Density
SM 9221C E-2014
462 MPN/g 04/25/2023
Lab ID Sample ID:
Collect Date/Time
Matrix Sampled by
23-20299 Site: 3
4/25/2023 7:40 AM
Solid/Sludge Kay Herndon
Test
Method
Results Date Analyzed
Total Solids (%)
SM 2540 B
1.56 % 04/26/2023
Fecal Density
SM 9221C E-2014
1475 MPN/g 04/25/2023
Lab ID Sample ID:
Collect Date/Time
Matrix Sampled by
23-20300 Site: 4
4/25/2023 7:42 AM
Solid/Sludge Kay Herndon
Test
Method
Results Date Analyzed
Total Solids (%) SM 2540 8 1.71 % 04/26/2023
Fecal Density SM 9221C E-2014 1346 MPN/g 04/25/2023
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
23-20301 Site: 5 4/25/2023 7:44 AM Solid/Sludge Kay Herndon
Test Method Results Date Analyzed
Total Solids (%) SM 2540 8 1.57 % 04/26/2023
Fecal Density SM=10E•2014 1465MPN/g 04/25/2023
Report # 2023 08017 Page 2 of 3

row"—. 771 Environmental Chemists, Inc.
envirochem6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/ Fax
'M 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS info(iz'cnvironmentalchemists com
Onslow Water & Sewer Authority Date of Report: May 11, 2023
228 Georgetown Road Customer PO #:
Jacksonville NC 28540 Customer ID: 08100092
Attention: Report #: 2023-08017
Project ID: Summerhouse
Lab ID Sample ID: Collect DatelTime .Matrix Sampled by
23-20302 Site: 6 4/25/2023 7:46 AM Solid/Sludge Kay Herndon
Test Method Results Date Analyzed
Total Solids (%)
Fecal Density
SM 2540 B
SM 9221C E-2014
1.89 %
1217 MPN/g
Lab ID Sample ID: Collect DatelTime Matrix Sampled by
23-20303 Site: 7 4/25/2023 7:45 AM Solid/Sludge Kay Herndon
04/26/2023
04/25/2023
Test Method Results Date Analyzed
Total Solids (%)
Fecal Density
SM 2540 B
SM 9221C E-2o14
Comment: Results reported on a dry weight basis.
Reviewed by:
1.76 %
1307 MPN/g
04/26/2023
04/25/2023
Report tt-: 2023.08017 _ Page 3 of 3

Environmental Chemist, Inc., Wilmington, NC Lab #94
6602 Windmill Way
Wilmington, NC 28405
Sample Receipt Checklist 910.392.0223
L i l�'1 JI"f�yT Date: q��Z� Repor' Number.
Receipt of sample:
❑ YES ❑
ECHEM Pickup Client Delivery ❑
UPS ❑ FedEx ❑ Other ❑
NO
N/A
1. Were custody seals present on the cooler?
❑ YES
❑
NO
N/A
2. If custody seals were present, were they intact/unbroken?
Original temperature upon receipt °C Corrected temperature upon receipt
How temperature taken:
❑ Temperature Blank Against Bottles
IR Gun ID: Thomas Traceable S/N 210886869 IR Gun Correction Factor °C: 0.0
YES
❑
NO
3. If temperature of cooler exceeded 6°C, was Project Mgr./qA notified?
YES
❑
NO
4. Were proper custody procedures (relinquished/received) followed?
YES
❑
NO
5. Were sample ID's listed on the COV
YES
❑
NO
6. Were samples ID's listed on sample containers?
YES
❑
NO
7. Were collection date and time listed on the COV
YES
❑
NO
8. Were tests to be performed listed on the COC?
YES
❑
NO
9. Did samples arrive in proper containers for each test?
YES
11
NO
10. Did samples arrive in good condition for each test?
YES
❑
NO
11. Was adequate sample volume available?'
YES
❑
NO
12. Were samples received within proper holding time for requested tests?
13. Were acid preserved samples received at a pH of <2?
11YES
❑
NO
14. Were cyanide samples received at a pH >12?
❑ YES
❑
NO
15. Were sulfide samples received at a pH >9?
❑ YES
❑
❑
NO
16. Were NH3/TKN/Phenol received at a chlorine residual of <0.5 m/L? **
YES
❑
❑
NO
17. Were Sulfide/Cyanide received at a chlorine residual of <0.5 m/L?
YES
❑
NO
18. Were orthophosphate samples filtered in the field within 15 minutes?
* TOC/Volatiles are pH checked at time of analysis and recorded on the benchsheet.
** Bacteria samples are checked for Chlorine at time of ana?ysis and recorded on the benchsheet.
Sample Preservation: (Must be completed for any sample(s) incorrectly preserved or with headspace)
Sample(s) were received incorrectly preserved and were adjusted accordingly
by adding (circle one): HZSO4 HNO3 HCI NaOH
Time of preservation: If more than one preservative is needed, notate in comments below
Note: Notfy custome, service Immediately for incorrectly preserved samples. Obtain a new sample or
notify the state lab if directed to analyzed by the customer. Who was notified, date and time:
Volatiles Sample(s) were received with headspace
COMMENTS:
DOC. QA.002 Rev 1

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Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Total Solids:
Beginning Temperature:
End Temperature:
Time Dissolved Oxygen Level
(minutes)
m /I
0
6.23
1
6.19
2
6.09
3
5.99
4
5.93
5
5.85
6
5.82
7
5.81
8
5.78
9
5.7
10
5.67
11
5.65
12
5.58
13
5.57
14
5.22
15
5.19
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
umm
1515
1
0.06
6.2
0.96
Dry Solids
agrees Celsius
agrees Celsius
3.61 mg Oxygen/hr
0.20 mg Oxygen/hr/g
30 degrees Celsius
0.61
Temperature Corrected Specific Oxygen Uptake Rate: I0.13 mg Oxygen/hr/g
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.
Updated 10/23/2013

Summerhouse WRF
Summerhouse WRF
WQ0029945
Apr-23
Date:=
SOUR*
M oxygen/g/hr
4/25/2023
0.54
4/27/2023
0.53
4/29/2023
0.57
5/3/2023
0.73
5/8/2023
0.61
5/9/2023
0.44
5/10/2023
0.45
8/2/2023
0.18
8/6/2023
0.17
8/ 14/2023
0.19
8/17/2023
0.19
8/ 11 /2023
0.24
8/24/2023
0.14
* SOUR = Specific Oxygen Uptake Rate
Total4:980
........ ....
Average 0383
SOUR values are less than 1.5 mg oxygen/gram/hour and meets the 40 CFR Part
503.33 Option 4 for Vector Attraction Reduction.
SOUR values provided by Summerhouse WRF

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name: Summerhouse
Biosolids Permit Number: ') f
Date: 4/25/2023 yJ Z� 23
Digester Temperature: 23.7 /
Sampling Date/Time: 4/25/23 0736
Sampled By: K Herndon
Analysis Date/Time: 4/25/2023
Analyzed By: K Herndon
Total Solids: 1.63 Dry Solids
Beginning Temperature: 21.9 degrees Celsius
End Temperature: 22.1 degrees Celsius
Dissolved Oxygen Level
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
0.16
6.9
0.99
9.78 mg Oxygen/hr
0.60 mg Oxygen/hr/g
22 degrees Celsius
0.91
Temperature Corrected Specific Oxygen Uptake Rate. -I 0.54 mg Oxygen/hr/g
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.
Updated 10/23/2013

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
41z -4-1Z -,--
)ry Solids
rees Celsius
rees Celsius
0.16
7.0
0.97
9.83 mg Oxygen/hr
0.58 mg Oxygen/hr/g
22 degrees Celsius
0.91
Temperature Corrected Specific Oxygen Uptake Rate: a 0.53 mg Oxygen/hr/g
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.
Updated 10/23/2013

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name: Sum
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time: 4/25,
Sampled By: K He
Analysis Date/Time:
Analyzed By: K He
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
40
23.
0.17
7.3
0.99
1109)Z-5
o Dry Solids
egrees Celsius
egrees Celsius
10.26 mg Oxygen/hr
0.66 mg Oxygen/hr/g
23 degrees Celsius
0.86
Temperature Corrected Specific Oxygen Uptake Rate:1 0.57 mg Oxygen/hr/g
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.
Updated 10/23/2013

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name: Sum
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time: 4/25,
Sampled By: K He
Analysis Date/Time:
Analyzed By: K He
Total Solids.
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
7.31
7.21
6.95
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
Z3. /
nn S13
1.71 % Dry Solids
22.8 degrees Celsius
22.6 degrees Celsius
0.24
7.4
0.96
14.40 mg Oxygen/hr
0.84 mg Oxygen/hr/g
23 degrees Celsius
0.86
Temperature Corrected Specific Oxygen Uptake Rate:1 0.73 mg Oxygen/hr/g
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.
Updated 10/23/2013

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name: Sum
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time: 4/25,
Sampled By: K He
Analysis Date/Time:
Analyzed By: K He
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
5.
5
5
5
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
se
�5`114,3
Dry Solids
grees Celsius
grees Celsius
0.19
7.7
0.96
11.11 mg Oxygen/hr
0.71 mg Oxygen/hr/g
23 degrees Celsius
0.86
Temperature Corrected Specific Oxygen Uptake Rate: 0.61 mg Oxygen/hr/g
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.
Updated 10/23/2013

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
5.
11
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
olids
Celsius
Celsius
0.16
7.5
0.98
9.74 mg Oxygen/hr
0.52 mg Oxygen/hr/g
23 degrees Celsius
0.86
Temperature Corrected Specific Oxygen Uptake Rater 0.44 mg Oxygen/hr/g
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.
Updated 10/23/2013

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name
Biosolids Permit Number
Date
Digester Temperature
Sampling Date/Time
Sampled By
Analysis Date/Time
Analyzed By
Total Solids
Beginning Temperature
End Temperature
Dissolved Oxygen Level
7.3
69
6.7
6.6
6.4
63
6.1
6.0
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
m
+icaicuco
23.7
0745 S /'D 23
A
1.76 % Dry Solids
23.6 degrees Celsius
22.7 degrees Celsius
0.15
7.1
1.00
9.19 mg Oxygen/hr
0.52 mg Oxygen/hr/g
23 degrees Celsius
0.86
Temperature Corrected Specific Oxygen Uptake Rate:1 0.45 mg Oxygen/hr/g
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.
Updated 10/23/2013

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name
Biosolids Permit Number
Date
Digester Temperature
Sampling Date/Time
Sampled By
Analysis Date/Time
Analyzed By
Total Solids
Beginning Temperature
End Temperature
Dissolved Oxygen Level
5.83
5.78
5.57
5.38
5.34
5.33
5.26
5.12
5.09
5.03
5.01
4.89
4.79
4.72
4.63
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
5ummernouse
8/2/2023
30
8/2/23 0630
K Herndon
8/2/23 1000
K Herndon
% Dry Solids
degrees Celsius
degrees Celsius
0.08
5.7
0.99
4.83 mg Oxygen/hr
0.30 mg Oxygen/hr/g
30 degrees Celsius
0.61
Temperature Corrected Specific Oxygen Uptake Rate:1 0.18 mg Oxygen/hr/g
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.
Updated 10/23/2013

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
m /I
4.2
4.13
4.06
3.98
3.9
3.82
3.78
3.67
3.58
3.54
3.49
3.42
3.33
3.25
3.17
3.08
Summerhouse
8/6/2023
28.7
8/9/23 1330
K Herndon
8/9/23 1330
K Herndon
1.69 %
28.7 dE
28.7 1dE
Slope: 0.07
Intercept: 4.2
Correlation Coefficient: 1.00
Dry Solids
:grees Celsius
:grees Celsius
Oxygen Uptake Rate: 4.40 mg Oxygen/hr
Ambient Specific Oxygen Uptake Rate: 0.26 mg Oxygen/hr/g
Average Temperature: 29 degrees Celsius
Temperature Correction Factor: 0.64
Temperature Corrected Specific Oxygen Uptake Rate:1 0.17 mg Oxygen/hr/g
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.
Updated 10/23/2013

Specific Oxygen Uptake Rate
SOUR
Facility Name: Summ
Biosolids Permit Number:
Digester Temperature: 29.6
Sampling Date/Time: 8/14/23 1400
Sampled By: K Herndon
Analysis Date/Time: 8/14/23 1400
Analyzed By: K Herndon
Total Solids: 1.56 % Dry Solids
Beginning Temperature: 29.6 degrees Celsius
End Temperature: 29.5 degrees Celsius
Time Dissolved Oxygen Level
(minutes)
m /1)
0
5.36
1
5.29
2
4.89
3
4.75
4
4.56
5
4.49
6
4.37
7
4.32
8
4.28
9
4.25
10
4.24
11
4.21
12
4.19
13
4.12
14
4.08
15
4.01
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature
Correction Factor:
0.08
5.1
0.91
4.73 mg Oxygen/hr
0.30 mg Oxygen/hr/g
30 degrees Celsius
0.61
Temperature Corrected Specific Oxygen Uptake Rate: 0.19 mg Oxygen/hr/g
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.
Updated 10/23/2013

Specific Oxygen Uptake Rate
SOUR
Facility Name
Biosolids Permit Number
Date
Digester Temperature
Sampling Date/Time
Sampled By
Analysis Date/Time
Analyzed By
Total Solids
Beginning Temperature
End Temperature
Time Dissolved Oxygen Level
(minutes)
m /I
0
5.82
1
5.78
2
5.52
3
5.19
4
5.09
5
4.98
6
4.97
7
4.96
8
4.94
9
4.92
10
4.87
11
4.75
12
4.55
13
4.43
14
4.42
15
4.4
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
5ummernouse
8/17/2023
29.7
8/17/23 0900
K Herndon
8/17/23 0900
K Herndon
1.71
29.7
29.5
0.09
5.6
0.95
Dry Solids
egrees Celsius
egrees Celsius
5.28 mg Oxygen/hr
0.31 mg Oxygen/hr/g
30 degrees Celsius
0.61
Temperature Corrected Specific Oxygen Uptake Rate:1 mg Oxygen/hr/g
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.
Updated 10/23/2013

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name: Summerhouse
Biosolids Permit Number:
Date: 8/11 /2
Digester Temperature:
Sampling Date/Time: 8/22/23 1100
Sampled By: K Herndon
Analysis Date/Time: 8/22/23 1100
Analyzed By: K Herndon
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
5.92
5.77
5.7
5.57
5.44
5.41
5.19
5.17
5.14
5.05
4.85
4.73
4.56
4.53
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
57 % Dry Solids
30 degrees Celsius
).8 degrees Celsius
0.10
5.9
1.00
6.21 mg Oxygen/hr
0.40 mg Oxygen/hr/g
30 degrees Celsius
0.61
Temperature Corrected Specific Oxygen Uptake Rate:1 mg Oxygen/hr/g
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.
Updated 10/23/2013

Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Total Solids:
Beginning Temperature:
End Temperature:
Time Dissolved Oxygen Level
(Summerhouse 1
(minutes)
0
6.09
1
6.05
2
6
3
5.99
4
5.94
5
5.91
6
5.9
7
5.81
8
5.75
9
5.54
10
5.52
11
5.42
12
5.28
13
5.17
14
5.16
15
5.12
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
8/24/23 1330
K Herndon
ern
1.89 %Dry Solids
30 degrees Celsius
30 degrees Celsius
0.07
6.2
0.98
4.27 mg Oxygen/hr
0.23 mg Oxygen/hr/g
30 degrees Celsius
0.61
Temperature Corrected Specific Oxygen Uptake Rate:1 0.14 mg Oxygen/hr/g
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.
Updated 10/23/2013

Swansboro WWTP
Swansboro WWTP
WQ0023261
Annual 2023
iafe
.............. ...
$OUR*
mg oxygen/g/hr
8/22/2023
0.23
9/4/2023
0.61
9/28/2023
0.23
9/29/2023
0.27
10/2/2023
0.25
10/4/2023
0.24
10/9/2023
0.32
10/12/2023
0.32
10/16/2023
0.21
10/ 17/2023
0.17
10/ 19/2023
0.42
10/23/2023
0.43
10/24/2023
0.38
10/25/2023
0.36
11/28/2023
0.15
* SOUR = Specific Oxygen Uptake Rate
Total4:59Q
Average 0.3f
SOUR values are less than 1.5 mg oxygen/gram/hour and meets the 40 CFR Part
503.33 Option 4 for Vector Attraction Reduction.
SOUR values provided by Northwest Regional WWTP

Time
(minutes)
0
1
3
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name
Biosolids Permit Number
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
7.7
7.7
7.
7.6
76
7.6
75
74
7.3
72
70
69
6.7
6.6
6.4
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
5wansooro
8/22/2023
23.2
22-Aug
S Howard
7:15
2 % Dry Solids
23.2 degrees Celsius
22.9 degrees Celsius
0.09
8.0
0.95
5.24 mg Oxygen/hr
0.26 mg Oxygen/hr/g
23 degrees Celsius
0.86
Temperature Corrected Specific Oxygen Uptake Rate:1 mg Oxygen/hr/g
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.
Updated 10/23/2013

Time
(minutes)
0
2
4
5
6
7
8
0
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name:pHoward
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:Analysis Date/Time:
Analyzed By:
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
6.5
6.1
77
740
51
4a
4E
42
4C
70
72
3.1
7
2E
2E
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
2 % Dry Solids
25.4 degrees Celsius
25.7 degrees Celsius
0.27
6.3
0.99
16.44 mg Oxygen/hr
0.82 mg Oxygen/hr/g
26 degrees Celsius
0.75
Temperature Corrected Specific Oxygen Uptake Rate:1 0.61 mg Oxygen/hr/g
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.
Updated 10/23/2013

Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Total Solids:
Beginning Temperature:
End Temperature:
Time Dissolved Oxygen Level
(minutes)
(m /I
0
8.25
1
8.09
2
7.99
3
7.9
4
7.81
5
7.72
6
7.64
7
7.55
8
7.48
9
7.4
10
7.33
11
7.25
12
7.17
13
7.1
14
7.03
15
6.94
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature
Correction Factor:
Swansboro
9/28/2023
21.9
28-Sep
S Howard
8:10
2 % Dry Solids
21.9 degrees Celsius
21.9 degrees Celsius
0.08
8.2
1.00
4.98 mg Oxygen/hr
0.25 mg Oxygen/hr/g
22 degrees Celsius
0.91
Temperature Corrected Specific Oxygen Uptake Rate:1 0.23 mg Oxygen/hr/g
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.
Updated 10/23/2013

Time
(minutes)
0
2
4
5
6
7
8
0
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name
Biosolids Permit Number
Date
Digester Temperature
Sampling Date/Time
Sampled By
Analysis Date/Time
Analyzed By
Total Solids
Beginning Temperature
End Temperature
Dissolved Oxygen Level
7.2
7.0
69
78M
770
760
50
6.4
63
6.2
61
6.0
5.9
8M
Slope:
Intercept:
Correlation Coefficient:
IS Howard 1
IS. Howard 1
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
22
0.10
7.2
1.00
o Dry Solids
egrees Celsius
eorees Celsius
5.95 mg Oxygen/hr
0.30 mg Oxygen/hr/g
22 degrees Celsius
0.91
Temperature Corrected Specific Oxygen Uptake Rate:1 0.27 mg Oxygen/hr/g
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.
Updated 10/23/2013

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
6.11
6
5.88
5.77
5.65
5.55
5.44
5.34
5.23
5.14
5.04
4.94
4.8
4.74
4.63
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
1
1
24.
0.11
6.2
1.00
Dry Solids
grees Celsius
❑rees Celsius
6.48 mg Oxygen/hr
0.32 mg Oxygen/hr/g
25 degrees Celsius
0.78
Temperature Corrected Specific Oxygen Uptake Rate:1 mg Oxygen/hr/g
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.
Updated 10/23/2013

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
7.2
71
70
6.
6.
6.
6.
6.5
6.4
6.3
6.2
6.1
6.0
60
5.9
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
)ry Solids
rees Celsius
rees Celsius
0.10
7.3
0.99
5.90 mg Oxygen/hr
0.30 mg Oxygen/hr/g
24 degrees Celsius
0.82
Temperature Corrected Specific Oxygen Uptake Rate:1 mg Oxygen/hr/g
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.
Updated 10/23/2013

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
1
(Frank G. 1
(Frank G. 1
6.19
6.08
5.92
5.79
5.64
5.53
5.4
5.28
5.15
5.03
4.9
4.79
4.67
4.55
4.44
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
Dry Solids
egrees Celsius
egrees Celsius
0.12
6.2
1.00
7.47 mg Oxygen/hr
0.37 mg Oxygen/hr/g
23 degrees Celsius
0.86
Temperature Corrected Specific Oxygen Uptake Rate:1 mg Oxygen/hr/g
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.
Updated 10/23/2013

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Digester Temperature
Sampling Date/Time
Sampled By
Analysis Date/Time
Analyzed By
Total Solids
Beginning Temperature
End Temperature
Dissolved Oxygen Level
(mg/1)
21
(Frank G. 1
(Frank G. 1
6.29
6.1
5.99
5.86
5.73
5.
70M
U.
4
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
2 % Dry Solids
20.8 degrees Celsius
21.2 degrees Celsius
0.11
6.2
1.00
6.73 mg Oxygen/hr
0.34 mg Oxygen/hr/g
21 degrees Celsius
0.95
Temperature Corrected Specific Oxygen Uptake Rate: 0.32 mg Oxygen/hr/g
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.
Updated 10/23/2013

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name:pFrankG.
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
6.95
6.85
6.75
6.67
6.59
6.51
6.43
6.36
6.29
6.22
6.15
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
16-Oct
14:55
2 % Dry Solids
21.9 degrees Celsius
22.2 degrees Celsius
0.08
7.0
0.99
4.67 mg Oxygen/hr
0.23 mg Oxygen/hr/g
22 degrees Celsius
0.91
Temperature Corrected Specific Oxygen Uptake Rate:1 0.21 mg Oxygen/hr/g
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.
Updated 10/23/2013

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
7.61
7.54
7.48
7.43
7.35
7.31
7.25
7.19
7.12
7.04
7
6.92
6.86
6.8
6.74
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
10/17/2023
21.7
17-Oct
G.
9:21
G.
2 % Dry Solids
21.7 degrees Celsius
21.7 degrees Celsius
0.06
7.6
1.00
3.74 mg Oxygen/hr
0.19 mg Oxygen/hr/g
22 degrees Celsius
0.91
Temperature Corrected Specific Oxygen Uptake Rate: 0.17 mg Oxygen/hr/g
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.
Updated 10/23/2013

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
y�
4.
3
3
.01
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
20.6
19-Oct
Frank G.
13:55
Frank G.
2 % Dry Solids
20.6 degrees Celsius
20.7 degrees Celsius
0.15
5.2
0.99
8.85 mg Oxygen/hr
0.44 mg Oxygen/hr/g
21 degrees Celsius
0.95
Temperature Corrected Specific Oxygen Uptake Rate:1 mg Oxygen/hr/g
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.
Updated 10/23/2013

Time
(minutes)
0
1
2
3
4
5
6
7
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
5.8
5.6
73
50
9M
48
4.7
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
olids
Celsius
Celsius
0.15
6.5
0.99
9.13 mg Oxygen/hr
0.46 mg Oxygen/hr/g
21 degrees Celsius
0.95
Temperature Corrected Specific Oxygen Uptake Rate:1 mg Oxygen/hr/g
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.
Updated 10/23/2013

Time
(minutes)
0
1
2
3
4
6
7
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
6.5
6.3
61
6.0
58
5.7
55
54
730
51
5C
47
4.7
77
4E
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
Swansboro
10/24/2023
21.3
24-Oct
F. Grosiak
11:35
F. Grosiak
2 % Dry Solids
21.3 degrees Celsius
21.8 deorees Celsius
0.14
6.5
1.00
8.44 mg Oxygen/hr
0.42 mg Oxygen/hr/g
22 degrees Celsius
0.91
Temperature Corrected Specific Oxygen Uptake Rate:1 mg Oxygen/hr/g
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.
Updated 10/23/2013

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
6.12
5.93
5.78
5.6
5.43
5.31
5.13
4.98
4.83
4.72
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
owa
15:1
23
0.15
6.2
1.00
Dry Solids
egrees Celsius
egrees Celsius
8.87 mg Oxygen/hr
0.44 mg Oxygen/hr/g
24 degrees Celsius
0.82
Temperature Corrected Specific Oxygen Uptake Rate:1 mg Oxygen/hr/g
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.
Updated 10/23/2013

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name
Biosolids Permit Number
Date
Digester Temperature
Sampling Date/Time
Sampled By
Analysis Date/Time
Analyzed By
Total Solids
Beginning Temperature
End Temperature
Dissolved Oxygen Level
U.
Fj
8
1.1
8.31
25.5
28-Nov
F.Grosiak
11 /28/2023 11:00
IF.Grosiak
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
2 % Dry Solids
17.6 degrees Celsius
18.1 degrees Celsius
0.04
8.9
0.95
2.67 mg Oxygen/hr
0.13 mg Oxygen/hr/g
18 degrees Celsius
1.14
Temperature Corrected Specific Oxygen Uptake Rate:1 0.15 mg Oxygen/hr/g
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.
Updated 10/23/2013

Onslow Water and Sewer Authority
Swansboro WRF
Permit # WQ0023261
Oct-23
Environmental Chemists, Inc.
Lab #
Date Analyzed
Most Probable Number
per gram
Log
1
10/02/2023
1,227
3.089
2
10/02/2023
463
2.666
3
10/02/2023
1,100
3.041
4
10/02/2023
244
2.387
5
10/02/2023
264
2.422
6
10/02/2023
834
2.921
7
10/02/2023
395
2.597
Totall 19.123
Averagel 2.732
Most Probable Number / Gram 539 Fecal Coliform/gram
Fecal Coliform values are less than 2,000,000 and meets the Class B pathogen reduction
requirement
Data provided in this summary have been used for the values and geometric means
reported on the Annual Pathogen and Vector Attraction Reduction Form for this land
application event.

O N ASA
October 02, 2023
Mark Young
Swansboro WRF
199 Williams Road
Swansboro, NC 28584
RE: Swan Solids
ONWASA Laboratory
228 Georgetown Road
Jacksonville NC 28540
[phone]
Enclosed are the results of analyses for samples received by our laboratory on 8/23/2023. If you
have any questions concerning this report, please feel free to contact me.
Sincerely,
r
Todd A. Roberts For Mark Young
Northwest ORC

ONWASA
Swansboro WRF Project: Swan Solids
199 Williams Road Project Number: Reported:
Swansboro, NC 28584 Project Manager: Mark Young 10/02/2023 14:41
Sample Results
Data Analyzed by: Environmental Chemists, Inc.
Sample: Swan Fecal #1 S233409-01 (WW)
Reporting Date Analyst
Analyte Result Qua[ Limit Units Analyzed Initials Method
Fecal Density 1227 MPN/g 08/23/2023 SM 9221C E MPN
24hr 503
Total Solids (%) 2.69 % 08/25/2023 SM 2540 G
Sample Results
Data Analyzed by: Environmental Chemists, Inc.
Sample: Swan Fecal #2 S233409-02 (WW)
Reporting Date Analyst
Analyte Result Qual Limit Units Analyzed Initials Method
Fecal Density 463 MPN/g 08/23/2023 SM 9221C E MPN
24hr 503
Total Solids (%) 2.81 % 08/25/2023 SM 2540 G
Sample Results
Data Analyzed by: Environmental Chemists, Inc.
Sample: Swan Fecal #3 S233409-03 (WW)
Reporting Date Analyst
Analyte Result Qual Limit Units Analyzed Initials Method
Fecal Density 1100 MPN/g 08/23/2023 SM 9221C E MPN
24hr 503
Total Solids (%) 2.82 % 08/25/2023 SM 2540 G
Sample Results
Data Analyzed by: Environmental Chemists, Inc.
Sample: Swan Fecal #4 S233409-04 (WW)
Reporting Date Analyst
Analyte Result Qual Limit Units Analyzed Initials Method
The contents of this report apply to the samples) analyzed in accordance with the chain of custody document.
No duplication of this report is allowed, except in its entirety. Page 2 of 5

ONWASA
Swansboro WRF Project: Swan Solids
199 Williams Road Project Number: Reported:
Swansboro, NC 28584 Project Manager: Mark Young 10/02/2023 14:41
Sample Results
(Continued)
Data Analyzed by: Environmental Chemists, Inc.
Sample: Swan Fecal #4 (Continued) S233409-04 (WW)
Reporting Date Analyst
Analyte Result Qual Limit Units Analyzed Initials Method
Fecal Density 244 MPN/g 08/23/2023 SM 9221C E MPN
24hr 503
Total Solids (%) 2.79 % 08/25/2023 SM 2540 G
Sample Results
Data Analyzed by: Environmental Chemists, Inc.
Sample: Swan Fecal #5 S233409-05 (WW)
Reporting Date Analyst
Analyse Result Qual Limit Units Analyzed Initials Method
Fecal Density 264 MPN/g 08/23/2023 SM 9221C E MPN
24hr 503
Total Solids (%) 2.96 % 08/25/2023 SM 2540 G
Sample Results
Data Analyzed by: Environmental Chemists, Inc.
Sample: Swan Fecal #6 S233409-06 (WW)
Reporting Date Analyst
Analyte Result Qual Limit Units Analyzed Initials Method
Fecal Density 834 MPN/g 08/23/2023 SM 9221C E MPN
24hr 503
Total Solids (%) 2.76 % 08/25/2023 SM 2540 G
Sample Results
Data Analyzed by: Environmental Chemists, Inc.
Sample: Swan Fecal #7 S233409-07 (WW)
Reporting Date Analyst
Analyte Result Qua] Limit Units Analyzed Initials Method
The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document.
No duplication of this report is allowed, except in its entirety. Page 3 of 5

Wallace Regional Wastewater Treatment Plant
NC0003450 Lab Cert #5352
VAR :option 6
Basin ID SHT#2 date time
pH initial, S.0 5.28
1/24/2023 9:35 AM
pH after addition of lime, S 12.42
1/24/2023 10:25 AM
pH after 2 hours,S.0 12.26
1/24/2023 12:25 PM
pH after 24 hours,S.U. 12.33
1/25/2023 10:53 AM
*** Post analysis QC pH 10 did not meet requirement of ±0.1 S.U.
QC pH 10 read 10.3 S.U.
All pH values have had the correction factor applied for temperature.
report reviewed by: J&, " 4t f , J /,,
Lisa Cottle , Lab supervisor

Wallace Regional Wastewater Treatment Plant
VAR :option 6
Basin ID
NC0003450 Lab Cert #5352
SHT#1 date time
pH initial, S.0 6.63 3/14/2023 8:18 AM
pH after addition of lime, S.0 12.53 3/14/2023 10:20 AM
pH after 2 hours,S.0 12.44 3/14/2023 12:20 PM
pH after 24 hours,S.U. 12.06 3/15/2023 10:53 AM
All pH values have had the correction factor applied for temperature.
UbI
report reviewed b : 2q �P3
p v
Lisa Cottle , Lab supervisor

Wallace Regional Wastewater Treatment Plant
NC0003450
VAR :option 6
Basin ID
SHT#2
Lab Cert #5352
date time
pH initial, S.0
7.62
5/17/2023
7:59 AM
pH after addition of lime, S.0
12.64
5/17/2023
10:16 AM
pH after 2 hours,S.0
12.4
5/17/2023
12:47 PM
pH after 24 hours,S.U.
12.57
5/18/2023
10:30 AM
All pH values have had the correction factor applied for temperature.
report reviewed by: ` 0 �OOp
Lisa Cottle , Lab supervisor

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SOIL ANALYSIS REPORTS

SOIL SAMPLE ANALYSES
The Town of Beulaville, the Town of Warsaw, the Town of Clayton, the Town of Kenansville the
Town of Bridgeton, the Town of Maysville, the Town of Wallace, and Southwest Plantation met
pathogen reduction and vector attraction reduction requirements through lime stabilization. The soil
pH will continue to be raised through the continued application of lime stabilized biosolids to these
application fields.

2023 APPLICATION SUMMARY TABLE

TRIPLE S FARMS
LAND APPLICATION PROGRAM
PERMIT NO. WQ0030998
2023 APPLICATION SUMMARY
.Farmer
/Site:
........
:Field .........
. ..
:Acres :::Spre6d::::::Gatlotii*::'
....
n...................................
.o...
:: /Aore::
.............
::::::::::::::
.............
:::Dry:Ttitts:::::::::::::::
.....:::::::::: .:.. .
......... ...... ...
Cirop:::::::
....... ..
:Tract
.
:::. Source
PAN
�Ibs/act
Eric Smith
1
1
36.00
Apr-23
48,000.00
0.15
5.38
Bermudagrass
Little Creek WWTP
250.92
May-23
288,170.00
0.90
32.32
Bermudagrass
Little Creek WWTP
Aug-23
582,160.00
1.65
59.23
Bermudagrass
Little Creek WWTP
Oct-23
108,030.00
0.32
11.58
Bermudagrass
Little Creek WWTP
Feb-23
186,000.00
0.64
23.00
Oats
Wallace WWTP
Feb-23
132,000.00
0.43
15.30
Oats
Little Creek WWTP
Mar-23
48,000.00
0.15
5.56
Bermudagrass
Little Creek WWTP
190,000.00
0.25
8.95
Bermudagrass
Warsaw WWTP
May-23
36,000.00
0.02
0.74
Bermudagrass
Bridgeton WWTP
Jul-23
204,000.00
0.57
20.50
Bermudagrass
Wallace WWTP
Oct-23
138,000.00
0.38
13.81
Bermudagrass
Wallace WWTP
Dec-23
48,000.00
0.10
3.56
Oats
Warsaw WWTP
2
12.60
Jun-23
47,970.00
0.43
5.38
Bermudagrass
Little Creek WWTP
256.05
Oct-23
119,370.00
1.02
12.79
Oats
Little Creek WWTP
Mar-23
162,000.00
1.49
18.78
Bermudagrass
Little Creek WWTP
Apr-23
138,000.00
1.28
16.11
Bermudagrass
Wallace WWTP
Jul-23
174,000.00
1.39
17.49
Bermudagrass
Wallace WWTP
Nov-23
18,000.00
0.03
0.37
Oats
Bridgeton WWTP
6
17.30
Feb-23
36,000.00
0.24
4.17
Oats
Little Creek WWTP
296.31
Mar-23
96,000.00
0.64
11.13
Bermudagrass
Little Creek WWTP
May-23
300,020.00
1.95
33.65
Bermudagrass
Little Creek WWTP
Sep-23
131,000.00
0.56
9.72
Bermudagrass
Warsaw WWTP
Sep-23
180,080.00
1.06
18.32
Bermudagrass
Little Creek WWTP
Sep-23
30,000.00
0.17
3.01
Bermudagrass
Wallace WWTP
Oct-23
122,930.00
0.76
13.17
Oats
Little Creek WWTP
Mar-23
90,000.00
0.25
4.24
Bermudagrass
Warsaw WWTP
May-23
78,000.00
0.53
9.11
Bermudagrass
Wallace WWTP
7
11.50
Jan-23
102,000.00
1.03
11.82
Fescue
Little Creek WWTP
180.80
Nov-23
156,010.00
1.45
16.72
Fescue
Little Creek WWTP
May-23
156,000.00
1.58
18.21
Fescue
Wallace WWTP
9
16.10
Apr-23
234,000.00
1.63
26.25
Bermudagrass
Little Creek WWTP
226.70
Jun-23
78,000.00
0.57
9.11
Bermudagrass
Wallace WWTP
210,000.00
1.46
23.56
Bermudagrass
Little Creek WWTP
Nov-23
138,230.00
0.92
14.81
Oats
Little Creek WWTP
10
12.80
Feb-23
108,020.00
0.98
12.52
Oats
Little Creek WWTP
110.96
Feb-23
138,000.00
1.33
17.07
Oats
Wallace WWTP
Dec-23
60,000.00
0.25
3.25
Oats
Kenansville WWTP
Dec-23
1 102,000.00
0.59
7.57
Oats
Warsaw WWTP
345
19.60
Feb-23
48,010.00
0.28
5.57
Fescue
Little Creek WWTP
177.05
Mar-23
156,010.00
0.92
18.09
Fescue
Little Creek WWTP
Oct-23
150,000.00
0.77
15.01
Fescue
Wallace WWTP
192,150.00
1.05
20.59
Fescue
Little Creek WWTP
Mar-23
174,000.00
1.10
21.52
Fescue
Wallace WWTP
3A
14.00
Jan-23
252,130.00
2.09
29.23
Fescue
Little Creek WWTP
154.15
Jan-23
60,476.00
0.14
1.91
Fescue
Summerhouse WRF
Jan-23
42,000.00
0.06
0.86
Fescue
Maysville WWTP
Jan-23
12,000.00
0.04
0.55
Fescue
Southwest Plantation
Mar-23
30,000.00
0.27
3.71
Fescue
Wallace WWTP
Oct-23
1 36,000.00
0.26
3.60
Fescue
Wallace WWTP
Scott Thigpen
ST
1
14.05
Oct-23
186,000.00
1.42
19.93
Fescue
Little Creek WWTP
123.68
Nov-23
138,000.00
0.73
10.30
Fescue
Swansboro WWTP
Apr-23
27,000.00
0.04
0.55
Fescue
Maysville WWTP
Oct-23
80,000.00
0.37
5.24
Fescue
Beulaville WWTP
Dec-23
12,000.00
0.04
0.55
Fescue
Southwest Plantation
Dec-23
42,000.00
0.14
1.98
Fescue
Warsaw WWTP
2
20.30
Apr-23
78,000.00
0.12
2.46
Bermudagrass
Summerhouse WRF
39.30
Sep-23
72,000.00
0.11
2.27
Bermudagrass
Summerhouse WRF
Sep-23
12,000.00
0.03
0.55
Bermudagrass
Southwest Plantation
Oct-23
155,000.00
0.36
7.30
Bermudagrass
Warsaw WWTP
Mike Williams
MW
1
10.88
Aug-2 3
120,000.00
0.82
8.96
Bermudagrass
Swansboro WWTP
71.53
May-23
88,000.00
0.53
5.76
Bermudagrass
Beulaville WWTP
May-23
78,000.00
0.23
2.46
Bermudagrass
Summerhouse WRF
Aug-23
27,000.00
0.05
0.55
Bermudagrass
Maysville WWTP
5
1.90
Jun-23
13,750.00
0.49
0.93
Bermudagrass
Northwest Regional WRF
10.74
6
6.21
Sep-23
73,122.00
0.88
5.46
Bermudagrass
Swansboro WWTP
36.75
Jun-23
45,000.00
0.49
3.04
Bermudagrass
Northwest Regional WRF
7
5.36
Jun-23
39,000.00
0.49
2.63
Bermudagrass
Northwest Regional WRF
10.80
8
4.72
Jun-23
34,000.00
0.49
2.30
Bermudagrass
Northwest Regional WRF
37.36
9
10.00
Sep-23
72,000.00
0.54
5.37
Bermudagrass
Swansboro WWTP
26.67
Jun-23
72,565.00
0.49
4.90
Bermudagrass
Northwest Regional WRF
2B
14.46
Jul-23
148,125.39
0.69
10.01
Bermudagrass
Northwest Regional WRF
15.20
Jonathan Smith
JS
2
5.03
Oct-23
45,010.00
0.96
1 4.82
Oats
Little Creek WWTP
92.35
Oct-23
24,000.00
0.15
0.76
Oats
Summerhouse WRF
Nov-23
60,000.00
0.56
2.83
Oats
Warsaw WWTP
3
7.27
Nov-23
72,000.00
0.31
2.27
Oats
Summerhouse WRF
61.07
Dec-23
96,000.00
0.62
4.52
Oats
Warsaw WWTP
4
8.66
Oct-23
81,020.00
1.00
8.68
Oats
Little Creek WWTP
90.50
Nov-23
36,000.00
0.13
1.13
Oats
Summerhouse WRF
Dec-23
96,000.00
0.52
4.52
Oats
Warsaw WWTP
Lonnie Thigpen
LT
1
21.58
Jul-23
180,000.00
0.85
18.31
Bermudagrass
Little Creek WWTP
49.34
Dec-23
48,000.00
0.17
3.58
Ryegrass
Swansboro WWTP
Jul-23
131,726.28
0.41
8.90
Bermudagrass
Northwest Regional WRF
Totals 21 270.32
Town of Beulaville
Town of Clayton Little Creek WRF
Town of Kenansville
Southwest Plantation
Town of Wallace
Town of Warsaw
Town of Bridgeton
Town of Maysville
Summerhouse WWTP
Northwest Regional WWTP
Swansboro WWTP
Gallons Dry Tons Dry Metric Tons Permit Limit
168,000.00
11.00
10.00
30
4,179,320.00
459.39
417.63
300
60,000.00
3.25
2.96
10
36,000.00
1.65
1.50
5
11710,000.00
191.27
173.88
330
914,000.00
50.69
46.08
75
54,000.00
1.10
1.00
5
96,000.00
1.96
1.78
15
384,476.00
12.12
11.01
35
352,440.39
23.81
21.64
50
403,122.00
30.09
27.35
110
Totalsi 8,357,358 1 717.25 1 652.04
Branch Residuals Soils, LLC Confidential 2/28/2024 Page I

2023 APPLICATION CONDITION SUMMARIES

Town of Beulaville
Beulaville, North Carolina
Triple S Farms & Cleaning, Inc
WQ0030998
Annual 2023
Beulaville WWTP
Farmer: Mike Williams
Acres: 10.88
Site/Tract: MW
Application Method: Surface
Field: 1
Percent Solids: 1.57
Residual Report No.: BL 2023-13234
Crop: Bermudagrass
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
5/l/23
1
88,000.0
Dry
Cool
0.00
Total Gallons
68$,000.0

Town of Beulaville
Beulaville, North Carolina
Triple S Farms & Cleaning, Inc
WQ0030998
Annual 2023
Beulaville WWTP
Farmer: Scott Thigpen
Acres: 14.05
Site/Tract: ST
Application Method: Surface
Field: 1
Percent Solids: 1.57
Residual Report No.: BL 2023-13234
Crop: Fescue
......................
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
10/23/23
1
80,000.0
Dry
Cool
0.00
Total Gallons
80,000.0

Town of Bridgeton
Havelock, North Carolina
Triple S Farms and Cleaning, Inc.
WQ0030998
Annual 2023
Bridgeton WWTP
Stabilization Method Lime
Farmer: Eric Smith
Acres: 36
Site/Tract: 1
Application Method: Surface
Field: 1
Percent Solids: 0.49
Residual Report No.: BG-440A
Crop: Bermudagrass
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
5/1/23
1
18,000.0
Dry
Cool
0.00
7/12/23
1
18,000.0
Dry
warm
0.10
Total Gallons
36,000.0

Town of Bridgeton
Havelock, North Carolina
Triple S Farms and Cleaning, Inc.
WQ0030998
Annual 2023
Bridgeton WWTP
Stabilization Method Lime
Farmer: Eric Smith
Acres: 12.6
Site/Tract: 1
Application Method: Surface
Field: 2
Percent Solids: 0.49
Residual Report No.: BG-440A
Crop: Oats
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
1116/23
2
18,000.0
Dry
Cool
0.00
Total Gallons
1$,DOA

Triple S Farms
Clayton, North Carolina
Triple S Farms
WQ0030998
1st Quarter 2023
Little Creek WWTP
Stabilization Method: Lime
Farmer: Eric Smith
Acres: 36.00
Site/Tract: 1
Application Method: Surface
Field: 1
Percent Solids: 2.78
Residual Report No.: C 1-23-101-001
Crop: oats
........................................................................................... ............... ...........
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
2/21/23
1
48,000.0
Dry
coot
0.10
2/22/23
1
48,000.0
Dry
Cool
0.04
2/23/23
1
36,000.0
Dry
warm
0.00
Total Gallons
132,00.0.0

Triple S Farms
Clayton, North Carolina
Triple S Farms
WQ0030998
1st Quarter 2023
Little Creek WWTP
Stabilization Method: Lime
Farmer: Eric Smith
Acres: 36.00
Site/Tract: 1
Application Method: Surface
Field: 1
Percent Solids: 2.78
Residual Report No.: C 1-23-101-001
Crop: Bermudagrass
...................... ....... ....................
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
3/6/23
1
36,000.0
Dry
cool
0.00
3/7/23
1
12,000.0
Dry
cool
0.00
Total Gallons
48,000.0

Triple S Farms
Clayton, North Carolina
Triple S Farms
WQ0030998
1st Quarter 2023
Little Creek WWTP
Stabilization Method: Lime
Farmer: Eric Smith
Acres: 12.60
Site/Tract: 1
Application Method: Surface
Field: 2
Percent Solids: 2.78
Residual Report No.: C 1-23-101-001
Crop: Bermudagrass
......................... ..................
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
3/9/23
2
66,060.0
Dry
Cool
0.00
3/10/23
2
41,810.0
Dry
Cool
0.35
3/15/23
2
54,130.0
Dry
Cool
0.00
Total Gallons
162;00.0.0

Triple S Farms
Clayton, North Carolina
Triple S Farms
WQ0030998
1st Quarter 2023
Little Creek WWTP
Stabilization Method: Lime
Farmer: Eric Smith
Acres: 17.30
Site/Tract: 1
Application Method: Surface
Field: 6
Percent Solids: 2.78
Residual Report No.: C 1-23-101-001
Crop: oats
........................ ..
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
2/24/23
6
36,000.0
Dry
Cool
0.10
Total Gallons
36;00:0.0

Triple S Farms
Clayton, North Carolina
Triple S Farms
WQ0030998
1st Quarter 2023
Little Creek WWTP
Stabilization Method: Lime
Farmer: Eric Smith
Acres: 17.30
Site/Tract: 1
Application Method: Surface
Field: 6
Percent Solids: 2.78
Residual Report No.: C 1-23-101-001
Crop: Bermudagrass
............... .............. .......... .............. ... ...........
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
3/7/23
6
42,000.0
Dry
Cool
0.00
3/8/23
6
54,000.0
Dry
Cool
0.00
Total Gallons
961000.0

Triple S Farms
Clayton, North Carolina
Triple S Farms
WQ0030998
1st Quarter 2023
Little Creek WWTP
Stabilization Method: Lime
Farmer: Eric Smith
Acres: 11.50
Site/Tract: 1
Application Method: Surface
Field: 7
Percent Solids: 2.78
Residual Report No.: C 1-23-101-001
Crop: Fescue
.......... .................
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
1/25/23
7
29,990.0
Dry
Cool
0.45
1/26/23
7
18,000.0
Dry
Cool
0.00
1/30/23
7
30,000.0
Dry
Cool
0.23
1 /31 /23
7
18,010.0
Dry
Cool
0.00
2/8/23
7
6,000.0
Dry
Cool
0.00
Total Gallons
102,000.0

Triple S Farms
Clayton, North Carolina
Triple S Farms
WQ0030998
1st Quarter 2023
Little Creek WWTP
Stabilization Method: Lime
Farmer: Eric Smith
Acres: 19.60
Site/Tract: 1
Application Method: Surface
Field: 345
Percent Solids: 2.78
Residual Report No.: C 1-23-101-001
Crop: Fescue
....................... .....
............... ..................
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
2/9/23
345
36,010.0
Dry
cool
0.00
2/10/23
345
12,000.0
Dry
Cool
0.01
Total Gallons
48;010.0

Triple S Farms
Clayton, North Carolina
Triple S Farms
WQ0030998
1st Quarter 2023
Little Creek WWTP
Stabilization Method: Lime
Farmer: Eric Smith
Acres: 12.80
Site/Tract: 1
Application Method: Surface
Field: 10
Percent Solids: 2.78
Residual Report No.: C 1-23-101-001
Crop: oats
..................... ... .......................... ...................
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
2/16/23
10
36,020.0
Dry
cool
0.00
2/17/23
10
36,000.0
Dry
cool
0.10
2/20/23
10
36,000.0
Dry
Cool
0.00
Total Gallons
108,020.0

Triple S Farms
Clayton, North Carolina
Triple S Farms
WQ0030998
1st Quarter 2023
Little Creek WWTP
Stabilization Method: Lime
Farmer: Eric Smith
Acres: 19.60
Site/Tract: 1
Application Method: Surface
Field: 345
Percent Solids: 2.78
Residual Report No.: C 1-23-101-001
Crop: Fescue
.
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
3/20/23
345
42,010.0
Dry
Cool
0.00
3/21 /23
345
42,000.0
Dry
cool
0.00
3/22/23
345
36,000.0
Dry
cool
0.03
3/23/23
345
36,000.0
Dry
cool
0.00
Total Gallons
156,01-0.0

Triple S Farms
Clayton, North Carolina
Triple S Farms
WQ0030998
1st Quarter 2023
Little Creek WWTP
Stabilization Method: Lime
Farmer: Eric Smith
Acres: 14.00
Site/Tract: 1
Application Method: Surface
Field: 3A
Percent Solids: 2.78
Residual Report No.: C 1-23-101-001
Crop: Fescue
.. ........ . ....... .........
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
1/17/23
3A
18,060.0
Dry
Cool
0.10
1/18/23
3A
18,020.0
Dry
Cool
0.00
1/19/23
3A
18,030.0
Dry
Cool
0.00
1/20/23
3A
36,000.0
Dry
cool
0.00
1/23/23
3A
24,010.0
Moist
Cool
0.02
3/24/23
3A
18,010.0
Dry
warm
0.00
3/28/23
3A
36,000.0
Moist
Cool
0.21
3/29/23
3A
48,000.0
Dry
Cool
0.04
3/30/23
3A
36,000.0
Dry
Cool
0.00
Total Gallons .
.. .
252113U

Triple S Farms
Clayton, North Carolina
Triple S Farms
WQ0030998
2nd Quarter 2023
Little Creek WWTP
Stabilization Method: Lime
Farmer: Eric Smith
Acres: 36.00
Site/Tract: 1
Application Method: Surface
Field: 1
Percent Solids: 2.69
Residual Report No.: C 2-23-256-003
Crop: Bermudagrass
...................... .
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
4/26/23
1
36,000.0
Dry
Cool
0.28
4/27/23
1
12,000.0
Dry
Cool
0.13
Total Gallons
1 48,000.0

Triple S Farms
Clayton, North Carolina
Triple S Farms
WQ0030998
2nd Quarter 2023
Little Creek WWTP
Stabilization Method: Lime
Farmer: Eric Smith
Acres: 16.10
Site/Tract: 1
Application Method: Surface
Field: 9
Percent Solids: 2.69
Residual Report No.: C 2-23-256-003
Crop: Bermudagrass
. . . . . ......
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
4/17/23
9
36,000.0
Dry
Cool
0.00
4/18/23
9
36,000.0
Dry
Cool
0.00
4/19/23
9
36,000.0
Dry
Cool
0.00
4/20/23
9
36,000.0
Dry
warm
0.00
4/21/23
9
18,000.0
Dry
warm
0.00
4/24/23
9
36,000.0
Dry
Coot
0.00
4/25/23
9
36,000.0
Dry
Cool
0.00
Total Gallons
234,000.0

Triple S Farms
Clayton, North Carolina
Triple S Farms
WQ0030998
2nd Quarter 2023
Little Creek WWTP
Stabilization Method: Lime
Farmer: Eric Smith
Acres: 17.30
Site/Tract: 1
Application Method: Inject
Field: 6
Percent Solids: 2.69
Residual Report No.: C 2-23-256-003
Crop: Bermudagrass
.......................................... .
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
5/15/23
6
48,000.0
Dry
cool
0.00
5/16/23
6
48,020.0
Dry
warm
0.00
5/17/23
6
48,000.0
Dry
warm
0.08
5/18/23
6
17,990.0
Dry
warm
0.02
5/19/23
6
6,000.0
Dry
cool
0.14
5/22/23
6
36,010.0
Dry
Cool
0.00
5/23/23
6
48,000.0
Dry
Cool
0.00
5/24/23
6
30,000.0
Dry
cool
0.00
5/25/23
6
18,000.0
Dry
warm
0.00
Total Gallons
300,02.0.9

Triple S Farms
Clayton, North Carolina
Triple S Farms
WQ0030998
2nd Quarter 2023
Little Creek WWTP
Stabilization Method: Lime
Farmer: Eric Smith
Acres: 12.60
Site/Tract: 1
Application Method: Inject
Field: 2
Percent Solids: 2.69
Residual Report No.: C 2-23-256-003
Crop: Bermudagrass
. .. ... ...
.............................
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
6/1/23
2
17,990.0
Dry
warm
0.00
6/2/23
2
11,980.0
Dry
wart„
0.00
6/5/23
2
18,000.0
Dry
cool
0.00
Total Gallons
47,970;0

Triple S Farms
Clayton, North Carolina
Triple S Farms
WQ0030998
2nd Quarter 2023
Little Creek WWTP
Stabilization Method: Lime
Farmer: Eric Smith
Acres: 16.10
Site/Tract: 1
Application Method: Inject
Field: 9
Percent Solids: 2.69
Residual Report No.: C 2-23-256-003
Crop: Bermudagrass
................ .. .. ....................... ..
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
6/6/23
9
18,000.0
Dry
warm
0.00
6/7/23
9
30,000.0
Dry
warm
0.22
6/8/23
9
48,000.0
Dry
warm
0.00
6/9/23
9
30,000.0
Dry
cool
0.00
6/12/23
9
30,000.0
Moist
warm
0.12
6/13/23
9
18,000.0
Dry
warm
0.00
6/14/23
9
18,000.0
Dry
warm
0.00
6/15/23
9
18,000.0
Dry
warm
0.10
Total Gallons
210;00.0

Triple S Farms
Clayton, North Carolina
Triple S Farms
WQ0030998
2nd Quarter 2023
Little Creek WWTP
Stabilization Method: Lime
Farmer: Eric Smith
Acres: 36.00
Site/Tract: 1
Application Method: Inject
Field: 1
Percent Solids: 2.69
Residual Report No.: C 2-23-256-003
Crop: Bermudagrass
....................... ....... .....................
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
5/3/23
1
30,030.0
Dry
Cool
0.00
5/4/23
1
30,030.0
Dry
Cool
0.00
5/5/23
1
30,030.0
Dry
Cool
0.00
5/8/23
1
30,000.0
Dry
warm
0.00
5/9/23
1
42,010.0
Dry
warm
0.00
5/ 10/23
1
48,020.0
Dry
Cool
0.00
5/11/23
1
48,050.0
Dry
Cool
0.00
5/12/23
1
30,000.0
Dry
warm
0.00
Total Gallons
288,17.Q:0

Triple S Farms
Clayton, North Carolina
Triple S Farms
WQ0030998
3rd Quarter 2023
Little Creek WWTP
Stabilization Method: Lime
Farmer: Eric Smith
Acres: 36.00
Site/Tract: 1
Application Method: Surface
Field: 1
Percent Solids: 2.44
Residual Report No.: C 3-23-354-0003
Crop: Bermudagrass
. ............. ..... .
.. . .............. .
......... .......
. ..
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
8/3/23
1
24,000.0
Dry
warn
0.00
8/4/23
1
18,000.0
Dry
warn
0.30
8/7/23
1
24,010.0
Dry
Warr
0.25
8/8/23
1
36,000.0
Dry
Warm
0.00
8/9/23
1
36,020.0
Dry
Warm
0.00
8/10/23
1
35,990.0
Dry
Warm
0.12
8/11/23
1
18,020.0
Dry
Warr
0.00
8/14/23
1
48,030.0
Dry
Warm
0.35
8/15/23
1
48,000.0
Dry
Warm
0.00
8/16/23
1
42,000.0
Dry
Warr
0.00
8/17/23
1
48,000.0
Dry
Warr
0.00
9/7/23
1
48,020.0
Dry
warm
0.00
9/8/23
1
24,030.0
Dry
warm
0.01
9/11/23
1
30,010.0
Dry
Warr
0.00
9/12/23
1
30,000.0
Dry
Warm
0.02
9/13/23
1
30,000.0
Dry
Warr
0.04
9/14/23
1
30,000.0
Dry
Warm
0.00
9/29/23
1
12,030.0
Dry
Cool
0.00
Total Gallons
582,160.0

Triple S Farms
Clayton, North Carolina
Triple S Farms
WQ0030998
3rd Quarter 2023
Little Creek WWTP
Stabilization Method: Lime
Farmer: Eric Smith
Acres: 17.30
Site/Tract: 1
Application Method: Surface
Field: 6
Percent Solids: 2.44
Residual Report No.: C 3-23-354-0003
Crop: Bermudagrass
................ ...... .......... .
.................. . ................... ....................... . .
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
9/15/23
6
30,000.0
Dry
warm
0.00
9/18/23
6
18,000.0
Moist
warm
0.10
9/19/23
6
30,020.0
Dry
warm
0.00
9/20/23
6
30,000.0
Dry
warm
0.00
9/21/23
6
30,020.0
Dry
warm
0.00
9/22/23
6
24,010.0
Dry
Cool
0.47
9/28/23
6
18,030.0
Dry
Cool
0.00
Total Gallons
180,080.0

Triple S Farms
Clayton, North Carolina
Triple S Farms
WQ0030998
3rd Quarter 2023
Little Creek WWTP
Stabilization Method: Lime
Farmer: Lonnie Thigpen
Acres: 21.58
Site/Tract: LT
Application Method: Surface
Field: 1
Percent Solids: 2.44
Residual Report No.: C 3-23-354-0003
Crop: Bennudagrass
.................................
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
7/31/23
1
48,000.0
Dry
warn
0.10
8/1/23
1
54,000.0
Dry
warn
0.00
8/2/23
1
42,000.0
Dry
warn
0.00
8/3/23
1
36,000.0
Dry
warm
0.00
Total Gallons
1804000.0

Triple S Farms
Clayton, North Carolina
Triple S Farms
WQ0030998
4th Quarter 2023
Little Creek WWTP
Stabilization Method: Lime
Farmer: Eric Smith
Acres: 36.00
Site/Tract: 1
Application Method: Surface
Field: 1
Percent Solids: 2.57
Residual Report No.: C 4-23-361-0009
Crop: Bermudagrass
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
10/2/23
1
42,010.0
Dry
warm
0.00
10/3/23
1
36,020.0
Dry
warm
0.00
10/4/23
1
30,000.0
Dry
warm
0.00
Total Gallons
108;030.0

Triple S Farms
Clayton, North Carolina
Triple S Farms
WQ0030998
4th Quarter 2023
Little Creek WWTP
Stabilization Method: Lime
Farmer: Eric Smith
Acres: 12.60
Site/Tract: 1
Application Method: Surface
Field: 2
Percent Solids: 2.57
Residual Report No.: C 4-23-361-0009
Crop: oats
.......................
Date
•
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
.
Rainfall
10/23/23
2
35,120.0
Dry
Cool
0.00
10/24/23
2
18,000.0
Dry
Cool
0.00
10/25/23
2
12,000.0
Dry
Cool
0.00
11/1/23
2
18,040.0
Dry
Cool
0.00
11/2/23
2
18,050.0
Dry
cool
0.00
11/3/23
2
18,160.0
Dry
cool
0.00
Total Gallons
11%370:0

Triple S Farms
Clayton, North Carolina
Triple S Farms
WQ0030998
4th Quarter 2023
Little Creek WWTP
Stabilization Method: Lime
Farmer: Eric Smith
Acres: 17.30
Site/Tract: 1
Application Method: Surface
Field: 6
Percent Solids: 2.57
Residual Report No.: C 4-23-361-0009
Crop: oats
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
10/19/23
6
18,000.0
Dry
cool
0.00
10/20/23
6
6,010.0
Dry
cool
0.41
11/13/23
6
29,980.0
Dry
cool
0.00
11/14/23
6
38,940.0
Dry
cool
0.00
11/29/23
6
12,000.0
Dry
cold
0.00
11/30/23
6
18,000.0
Dry
Cool
0.00
Total Gallons
1221930.0

Triple S Farms
Clayton, North Carolina
Triple S Farms
WQ0030998
4th Quarter 2023
Little Creek WWTP
Stabilization Method: Lime
Farmer: Eric Smith
Acres: 11.50
Site/Tract: 1
Application Method: Surface
Field: 7
Percent Solids: 2.57
Residual Report No.: C 4-23-361-0009
Crop: Fescue
....................
.. ..................
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
11/6/23
7
35,990.0
Dry
Cool
0.00
11/7/23
7
36,000.0
Dry
Cool
0.00
11/8/23
7
29,990.0
Dry
Cool
0.00
11/9/23
7
42,030.0
Dry
Cool
0.00
11/10/23
7
12,000.0
Dry
Cool
0.01
Total Gallons
: 1*010.0

Triple S Farms
Clayton, North Carolina
Triple S Farms
WQ0030998
4th Quarter 2023
Little Creek WWTP
Stabilization Method: Lime
Farmer: Eric Smith
Acres: 16.10
Site/Tract: 1
Application Method: Surface
Field: 9
Percent Solids: 2.57
Residual Report No.: C 4-23-361-0009
Crop: oats
.................... .................. .
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
11/30/23
9
18,020.0
Dry
coot
0.00
12/1/23
9
18,200.0
Dry
cool
0.00
12/4/23
9
36,010.0
Dry
cool
0.00
12/5/23
9
42,000.0
Dry
cool
0.00
12/6/23
9
18,000.0
Dry
cool
0.00
12/7/23
9
6,000.0
Dry
Cool
0.00
Total Gallons
-138,23Q.0

Triple S Farms
Clayton, North Carolina
Triple S Farms
WQ0030998
4th Quarter 2023
Little Creek WWTP
Stabilization Method: Lime
Farmer: Eric Smith
Acres: 19.60
Site/Tract: I
Application Method: Surface
Field: 345
Percent Solids: 2.57
Residual Report No.: C 4-23-361-0009
Crop: Fescue
............
............
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
10/4/23
345
18,000.0
Dry
Warm
0.00
10/5/23
345
30,100.0
Dry
Warm
0.00
10/6/23
345
12,010.0
Dry
Warm
0.00
10/9/23
345
36,000.0
Dry
Cool
0.00
10/10/23
345
35,990.0
Dry
Cool
0.00
10/11/23
345
24,010.0
Dry
Cool
0.00
10/12/23
345
24,030.0
Dry
Cool
0.33
10/13/23
345
12,0100
Dry
Cool
0.00
....... . .... .......
.............
.'
.. 5.00I

Triple S Farms
Clayton, North Carolina
Triple S Farms
WQ0030998
4th Quarter 2023
Little Creek WWTP
Stabilization Method: Lime
Farmer: Jonathan Smith
Acres: 5.03
Site/Tract: JS
Application Method: Surface
Field: 2
Percent Solids: 2.57
Residual Report No.: C 4-23-361-0009
Crop: oats
......................................... ............ ........ . ......... .
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
10/18/23
2
30,010.0
Dry
Cool
0.00
11/9/23
2
12,000.0
Dry
cool
0.00
11/13/23
2
3,000.0
Dry
Cool
0.00
Total Gallons
45;010;0

Triple S Farms
Clayton, North Carolina
Triple S Farms
WQ0030998
4th Quarter 2023
Little Creek WWTP
Stabilization Method: Lime
Farmer: Jonathan Smith
Acres: 8.66
Site/Tract: JS
Application Method: Surface
Field: 4
Percent Solids: 2.57
Residual Report No.: C 4-23-361-0009
Crop: oats
..
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
:..........
Prev. 24 Hour
Rainfall
10/16/23
4
30,010.0
Dry
Coot
0.00
10/17/23
4
36,010.0
Dry
coot
0.00
11/10/23
4
12,000.0
Dry
coot
0.01
11/13/23
4
3,000.0
Dry
coot
0.00
Total Gallons
81,029.9

Triple S Farms
Clayton, North Carolina
Triple S Farms
WQ0030998
4th Quarter 2023
Little Creek WWTP
Stabilization Method: Lime
Farmer: Scott Thigpen
Acres: 14.05
Site/Tract: ST
Application Method: Surface
Field: 1
Percent Solids: 2.57
Residual Report No.: C 4-23-361-0009
Crop: Fescue
.................. ..... .. ..... ..................
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
10/26/23
1
18,000.0
Dry
Cool
0.00
10/27/23
1
18,000.0
Dry
cool
0.00
10/30/23
1
36,000.0
Dry
warm
0.00
12/12/23
1
48,000.0
Dry
cool
0.00
12/13/23
1
66,000.0
Dry
Cool
0.00
Total Gallons
186,000.0

Town of Bridgeton
Havelock, North Carolina
Triple S Farms and Cleaning, Inc.
WQ0030998
Annual 2023
Bridgeton WWTP
Stabilization Method Lime
Farmer: Eric Smith
Acres: 36
Site/Tract: 1
Application Method: Surface
Field: 1
Percent Solids: 0.49
Residual Report No.: BG-440A
Crop: Bermudagrass
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
5/1/23
1
18,000.0
Dry
Cool
0.00
7/12/23
1
18,000.0
Dry
warm
0.10
Total Gallons
36,000.0

Town of Kenansville
Kenansville, North Carolina
Triple S Farms & Cleaning, Inc
WQ0030998
Annual 2023
Kenansville WWTP
Farmer: Eric Smith Acres: 12.8
Site/Tract: I Application Method: Surface
Field: 10 Percent Solids: 1.30
Residual Report No.: KV 2023-18528 Crop: Oats
Soil Weather Prev. 24 Hour
Date Field No. Subfield Gallons Conditions Conditions Rainfall
12/13/23 10 6,000.0 Dry Cool 0.00
12/14/23 10 54,000.0 Dry Cool 0.00
........................... .......... 60 ..0......00.0.
::

Town of Maysville
Maysville, North Carolina
Triple S Farms & Cleaning, Inc
WQ0030998
Annual 2023
Maysville WWTP
Farmer: Eric Smith
Acres: 14
Site/Tract: 1
Application Method: Surface
Field: 3A
Percent Solids: 0.49
Residual Report No.: MV 2023-03127
Crop: Fescue
. .......... ......
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
1/19/23
3A
6,000.00
Dry
Cool
0.00
1/20/23
3A
24,000.00
Dry
Cool
0.00
1/23/23
3A
12,000.00
Moist
Cool
0.02
Total Gallons
42,000.06

Town of Maysville
Maysville, North Carolina
Triple S Farms & Cleaning, Inc
WQ0030998
Annual 2023
Maysville WWTP
Farmer: Mike Williams
Acres: 10.88
Site/Tract: MW
Application Method: Surface
Field: 1
Percent Solids: 0.49
Residual Report No.: MV 2023-03127
Crop: Bermudagrass
............. .............. ..
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
8/23;23
1
27,000.00
Dry
warm
0.10
Total Gallons
27,004 00

Town of Maysville
Maysville, North Carolina
Triple S Farms & Cleaning, Inc
WQ0030998
Annual 2023
Maysville WWTP
Farmer: Scott Thigpen
Acres: 14.05
Site/Tract: ST
Application Method: Surface
Field: 1
Percent Solids: 0.49
Residual Report No.: MV 2023-03127
Crop: Fescue
.. ... . ..... ........... ...
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
4/21/23
1
12,000.00
Dry
warm
0.00
4/24/23
1
15,000.00
Dry
coot
0.00
127,000.001
Total Gallons

Northwest Regional WRF
Richlands, North Carolina
Triple S Farms & Cleaning, Inc
WQ0030998
Annual 2023
Northwest Regional WRF
Farmer: Lonnie Thigpen
Acres: 21.58
Site/Tract: LT
Application Method: Surface
Field: 1
Percent Solids: 1.62
Residual Report No.: NR 2023-29358
Crop: Bermudagrass
...........
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
7/17/23
1
131,726.3
Dry
Warm
0.00
Total Gallons131;726:3

Northwest Regional WRF
Richlands, North Carolina
Triple S Farms & Cleaning, Inc
WQ0030998
Annual 2023
Northwest Regional WRF
Farmer: Mike Williams
Acres: 14.46
Site/Tract: MW
Application Method: Surface
Field: 2B
Percent Solids: 1.62
Residual Report No.: NR 2023-29358
Crop: Bermudagrass
. ........... .................
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
7/ 18/23
2B
124,132.4
Dry
warm
0.00
7/ 19/23
2B
23,993.0
Dry
warm
0.10
Total Gallons
148;125.4

Northwest Regional WRF
Richlands, North Carolina
Triple S Farms & Cleaning, Inc
WQ0030998
Annual 2023
Northwest Regional WRF
Farmer: Mike Williams
Acres: 1.9
Site/Tract: MW
Application Method: Surface
Field: 5
Percent Solids: 1.62
Residual Report No.: NR 2023-29358
Crop: Bermudagrass
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
6/29/23
5
13,750.0
Dry
Warm
0.00
Total Gallons
131.750.0

Northwest Regional WRF
Richlands, North Carolina
Triple S Farms & Cleaning, Inc
WQ0030998
Annual 2023
Northwest Regional WRF
Farmer: Mike Williams
Acres: 6.21
Site/Tract: MW
Application Method: Surface
Field: 6
Percent Solids: 1.62
Residual Report No.: NR 2023-29358
Crop: Bermudagrass
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
6/29/23
6
45,000.0
Dry
warm
0.00
Total Gallons
45,000.0

Northwest Regional WRF
Richlands, North Carolina
Triple S Farms & Cleaning, Inc
WQ0030998
Annual 2023
Northwest Regional WRF
Farmer: Mike Williams
Acres: 5.36
Site/Tract: MW
Application Method: Surface
Field: 7
Percent Solids: 1.62
Residual Report No.: NR 2023-29358
Crop: Bermudagrass
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
6 29 23
7
39,000.0
Dry
warm
0.00
Total. Gallons
39,000.0

Northwest Regional WRF
Richlands, North Carolina
Triple S Farms & Cleaning, Inc
WQ0030998
Annual 2023
Northwest Regional WRF
Farmer: Mike Williams
Acres: 4.72
Site/Tract: MW
Application Method: Surface
Field: 8
Percent Solids: 1.62
Residual Report No.: NR 2023-29358
Crop: Bermudagrass
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
6/29/23
8
34,000.0
Dry
Warm
0.00
Total Gallons
34,000.0

Northwest Regional WRF
Richlands, North Carolina
Triple S Farms & Cleaning, Inc
WQ0030998
Annual 2023
Northwest Regional WRF
Farmer: Mike Williams
Acres: 10
Site/Tract: MW
Application Method: Surface
Field: 9
Percent Solids: 1.62
Residual Report No.: NR 2023-29358
Crop: Bermudagrass
Date
Field No.
Suhfeld
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
6/29/23
9
12,565.0
Dry
Warm
0.00
6/30/23
9
60,000.0
Dry
Warm
0.28
TQ�a1 Gallons
725650

Triple S Farms
Jacksonville, North Carolina
Triple S Farms
WQ00030998
Annual 2023
Southwest Plantation
Farmer: Eric Smith
Acres: 14
Site/Tract: 1
Application Method: Surface
Field: 3A
Percent Solids: 1.10
Residual Report No.: SWP 2023-22677
Crop: Fescue
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
1/24/23
3A
12,000.0
Dry
coot
0.00
Teal Gallons
12,000.0

Triple S Farms
Jacksonville, North Carolina
Triple S Farms
WQ00030998
Annual 2023
Southwest Plantation
Farmer: Scott Thigpen
Acres: 20.3
Site/Tract: ST
Application Method: Surface
Field: 2
Percent Solids: 1.10
Residual Report No.: SWP 2023-22677
Crop: Bermudagrass
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
9/11/23
2
12,000.0
Dry
warm
0.00
Total Gallons
12,000.0

Triple S Farms
Jacksonville, North Carolina
Triple S Farms
WQ00030998
Annual 2023
Southwest Plantation
Farmer: Scott Thigpen
Acres: 14.05
Site/Tract: ST
Application Method: Surface
Field: 1
Percent Solids: 1.10
Residual Report No.: SWP 2023-22677
Crop: Fescue
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
12/4/23
1
12,000.0
Dry
Cool
0.00
Total Gallons
12,000.0

Summerhouse WRF
Holly Ridge, NC
Triple S Farms
WQ0030998
Annual 2023
Summerhouse WRF
Farmer: Eric Smith
Acres: 14
Site/Tract: 1
Application Method: Surface
Field: 3A
Percent Solids: 0.76
Residual Report No.: SMH E2023-04013
Crop: Fescue
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
1/17/23
3A
24,000.0
Dry
coot
0.10
1/18/23
3A
30,000.0
Dry
cool
0.00
1/19/23
3A
6,476.0
Dry
cool
0.00
Total _Gallons
601.476.0

Summerhouse WRF
Holly Ridge, NC
Triple S Farms
WQ0030998
Annual 2023
Summerhouse WRF
Farmer: Scott Thigpen
Acres: 20.3
Site/Tract: ST
Application Method: Surface
Field: 2
Percent Solids: 0.76
Residual Report No.: SMH E2023-04013
Crop: Bermudagrass
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
4/ 12/23
2
42,000.0
Dry
Cool
0.00
4/13/23
2
36,000.0
Dry
Cool
0.00
Total Gallons
78,000.0

Summerhouse WRF
Holly Ridge, NC
Triple S Farms
WQ0030998
Annual 2023
Summerhouse WRF
Farmer: Mike Williams
Acres: 10.88
Site/Tract: MW
Application Method: Surface
Field: 1
Percent Solids: 0.76
Residual Report No.: SMH E2023-04013
Crop: Bermudagrass
.... . .......... ...
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
5/ 18/23
1
66,000.0
Dry
Warm
0.02
5/22/23
1
12,000.0
Dry
Cool
0.00
Total Gallons
78,000.0

Summerhouse WRF
Holly Ridge, NC
Triple S Farms
WQ0030998
Annual 2023
Summerhouse WRF
Farmer: Scott Thigpen
Acres: 20.3
Site/Tract: ST
Application Method: Surface
Field: 2
Percent Solids: 0.76
Residual Report No.: SMH E2023-04013
Crop: Bermudagrass
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
9/9/23
2
30,000.0
Dry
Warm
0.47
9/ 10/23
2
42,000.0
Moist
warm
0.10
Total Gallons
72,000.0

Summerhouse WRF
Holly Ridge, NC
Triple S Farms
WQ0030998
Annual 2023
Summerhouse WRF
Farmer: Jonathan Smith
Acres: 5.03
Site/Tract: JS
Application Method: Surface
Field: 2
Percent Solids: 0.76
Residual Report No.: SMH E2023-04013
Crop: Oats
.....................................................................................................................
..........................................................
.........................................................
..........................................................
..........................................................
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
10/31/23
2
6,000.0
Dry
Cool
0.00
11/1/23
2
18,000.0
Dry
Cool
0.00
Taal Galioris
24;000 0

Summerhouse WRF
Holly Ridge, NC
Triple S Farms
WQ0030998
Annual 2023
Summerhouse WRF
Farmer: Jonathan Smith
Acres: 8.66
Site/Tract: JS
Application Method: Surface
Field: 4
Percent Solids: 0.76
Residual Report No.: SMH E2023-04013
Crop: oats
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
11/2/23
4
12,000.0
Dry
Cool
0.00
11/6/23
4
24,000.0
Dry
Cool
0.00
Total Gallons
36,000.0

Summerhouse WRF
Holly Ridge, NC
Triple S Farms
WQ0030998
Annual 2023
Summerhouse WRF
Farmer: Jonathan Smith
Acres: 7.27
Site/Tract: JS
Application Method: Surface
Field: 3
Percent Solids: 0.76
Residual Report No.: SMH E2023-04013
Crop: Oats
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
11/7/23
3
48,000.0
Dry
Cool
0.00
11/8/23
3
24,000.0
Dry
Cool
0.00
Total Gallons
72,000.0

Swansboro WWTP
Swansboro, NC
Triple S Farms
WQ0030998
Annual 2023
Swansboro WWTP
Farmer: Mike Williams
Acres: 10.88
Site/Tract: MW
Application Method: Surface
Field: 1
Percent Solids: 1.79
Residual Report No.: SWB E2024-02029
Crop: Bermudagrass
................ ...... ..........
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
8/23/23
1
6,000.0
Dry
Warm
0.10
8/24/23
1
66,000.0
Dry
warm
0.00
8/25/23
1
48,000.0
Dry
Warm
0.00
Total Gallons
120;000.0

Swansboro WWTP
Swansboro, NC
Triple S Farms
WQ0030998
Annual 2023
Swansboro WWTP
Farmer: Mike Williams
Acres: 10
Site/Tract: MW
Application Method: Surface
Field: 9
Percent Solids: 1.79
Residual Report No.: SWB E2024-02029
Crop: Bermudagrass
............................. ........... ..............
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
9/5/23
9
72,000.0
Dry
warm
0.00
Total Gallons
72;000.0

Swansboro WWTP
Swansboro, NC
Triple S Farms
WQ0030998
Annual 2023
Swansboro WWTP
Farmer: Mike Williams
Acres: 6.21
Site/Tract: MW
Application Method: Surface
Field: 6
Percent Solids: 1.79
Residual Report No.: SWB E2024-02029
Crop: Bermudagrass
........ ...
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
9/6/23
6
73,122.0
Dry
Warm
0.00
Total Gallons
73,122.0

Swansboro WWTP
Swansboro, NC
Triple S Farms
WQ0030998
Annual 2023
Swansboro WWTP
Farmer: Scott Thigpen
Acres: 14.05
Site/Tract: ST
Application Method: Surface
Field: 1
Percent Solids: 1.79
Residual Report No.: SWB E2024-02029
Crop: Fescue
.... _. _.._ _ ...... ................. _.............
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
11/29/23
1
72,000.0
Dry
Cold
0.00
11/30/23
1
42,000.0
Dry
cool
0.00
12/4/23
1
24,000.0
Dry
Cool
0.00
Total Gallons
138 (lO110

Swansboro WWTP
Swansboro, NC
Triple S Farms
WQ0030998
Annual 2023
Swansboro WWTP
Farmer: Lonnie Thigpen
Acres: 21.58
Site/Tract: LT
Application Method: Surface
Field: 1
Percent Solids: 1.79
Residual Report No.: SWB E2024-02029
Crop: Ryegrass
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
12/6/23
1
36,000.0
Dry
Cool
0.00
12/7/23
1
12,000.0
Dry
Cool
0.00
Total Gallons
48,000.0

Triple S Farms
Wallace, North Carolina
Triple S Farms
WQ0030998
1st Quarter 2023
Wallace WWTP
Stabilization Method: Lime
Farmer: Eric Smith
Acres: 36.00
Site/Tract: 1
Application Method: Surface
Field: 1
Percent Solids: 2.97
Residual Report No.: WL 1-2023-00643
Crop: oats
........ ....... ....
..........................
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
2/20/23
1
6,000.0
Dry
Cool
0.00
2/21/23
1
12,000.0
Dry
Cool
0.10
2/22/23
1
42,000.0
Dry
cool
0.04
2/23/23
1
6,000.0
Dry
warts
0.00
2/28/23
1
48,000.0
Dry
cool
0.00
3/1/23
1
48,000.0
Dry
cool
0.00
3/2/23
1
24,000.0
Dry
cool
0.08
==J
Total Gallons
186;000.0

Triple S Farms
Wallace, North Carolina
Triple S Farms
WQ0030998
1st Quarter 2023
Wallace WWTP
Stabilization Method: Lime
Farmer: Eric Smith
Acres: 12.80
Site/Tract: 1
Application Method: Surface
Field: 10
Percent Solids: 2.97
Residual Report No.: WL 1-2023-00643
Crop: oats
..........
........................ .....................
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
2/8/23
10
12,000.0
Dry
cool
0.00
2/9/23
10
78,000.0
Dry
cool
0.00
2/16/23
10
48,000.0
Dry
Cool
0.00
Total Gallons
138;000.0

Triple S Farms
Wallace, North Carolina
Triple S Farms
WQ0030998
1st Quarter 2023
Wallace WWTP
Stabilization Method: Lime
Farmer: Eric Smith
Acres: 19.60
Site/Tract: 1
Application Method: Surface
Field: 345
Percent Solids: 2.97
Residual Report No.: WL 1-2023-00643
Crop: Fescue
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
3/20/23
345
42,000.0
Dry
Cool
0.00
3/21/23
345
24,000.0
Dry
Cool
0.00
3/22/23
345
30,000.0
Dry
Cool
0.03
3/23/23
345
78,000.0
Dry
cool
0.00
Total Gallons
174,000.0

Triple S Farms
Wallace, North Carolina
Triple S Farms
WQ0030998
1st Quarter 2023
Wallace WWTP
Stabilization Method: Lime
Farmer: Eric Smith
Acres: 14.00
Site/Tract: 1
Application Method: Surface
Field: 3A
Percent Solids: 2.97
Residual Report No.: WL 1-2023-00643
Crop: Fescue
................. ............... ................. .................
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
3/24/23
3A
30,000.0
Dry
warm
0.00
Total Gallons
30,000.0

Triple S Farms
Wallace, North Carolina
Triple S Farms
WQ0030998
2nd Quarter 2023
Wallace WWTP
Stabilization Method Lime
Farmer: Eric Smith
Acres: 12.60
Site/Tract: 1
Application Method: Surface
Field: 2
Percent Solids: 2.80
Residual Report No.: WL 2-2023-08640
Crop: Bermudagrass
.................... ...... .... .. .
.................................................................... ...................;
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
4/3/23
2
48,000.0
Dry
Cool
0.10
4/4/23
2
42,000.0
Dry
warm
0.01
4/5/23
2
48,000.0
Dry
warm
0.00
Total Gallons
138,000.0

Triple S Farms
Wallace, North Carolina
Triple S Farms
WQ0030998
2nd Quarter 2023
Wallace WWTP
Stabilization Method Lime
Farmer: Eric Smith
Acres: 17.30
Site/Tract: 1
Application Method: Surface
Field: 6
Percent Solids: 2.80
Residual Report No.: WL 2-2023-08640
Crop: Bermudagrass
................................. . ...
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
5/24/23
6
48,000.0
Dry
Cool
0.00
5/25/23
6
3%000.0
Dry
warm
0.00
Total Gallons
78,000.0

Triple S Farms
Wallace, North Carolina
Triple S Farms
WQ0030998
2nd Quarter 2023
Wallace WWTP
Stabilization Method Lime
Farmer: Eric Smith
Acres: 11.50
Site/Tract: 1
Application Method: Surface
Field: 7
Percent Solids: 2.80
Residual Report No.: WL 2-2023-08640
Crop: Fescue
................... .................. .
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
5/26/23
7
36,000.0
Dry
cool
0.00
5/31/23
7
36,000.0
Dry
warm
0.00
6/1/23
7
6,000.0
Dry
warm
0.00
6/2/23
7
30,000.0
Dry
warm
0.00
6/5/23
7
48,000.0
Dry
Coot
0.00
Total Gallons
156;000A

Triple S Farms
Wallace, North Carolina
Triple S Farms
WQ0030998
2nd Quarter 2023
Wallace WWTP
Stabilization Method Lime
Farmer: Eric Smith
Acres: 16.10
Site/Tract: 1
Application Method: Surface
Field: 9
Percent Solids: 2.80
Residual Report No.: WL 2-2023-08640
Crop: Bermudagrass
.............................. ...............
............................
.............................
...........................
.............................
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
6/6/23
9
36,000.0
Dry
warm
0.00
6/7/23
9
42,000.0
Dry
warm
0.22
Total Gallons
78,000.0

Triple S Farms
Wallace, North Carolina
Triple S Farms
WQ0030998
3rd Quarter 2023
Wallace WWTP
Stabilization Method: Lime
Farmer: Eric Smith
Acres: 36.00
Site/Tract: 1
Application Method: Surface
Field: 1
Percent Solids: 2.41
Residual Report No.: WL 3-2023-14447
Crop: Bermudagrass
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
7/25/23
1
24,000.0
Dry
warm
0.00
7/26/23
1
108,000.0
Dry
warm
0.14
9/28/23
1
30,000.0
Dry
cool
0.00
9/29/23
1
42,000.0
Dry
cool
0.00
Total Gallons
2041000.0

Triple S Farms
Wallace, North Carolina
Triple S Farms
WQ0030998
3rd Quarter 2023
Wallace WWTP
Stabilization Method: Lime
Farmer: Eric Smith
Acres: 12.60
Site/Tract: 1
Application Method: Surface
Field: 2
Percent Solids: 2.41
Residual Report No.: WL 3-2023-14447
Crop: Bermudagrass
................. .......... ....... .. ......... ..........
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
7/24/23
2
72,000.0
Moist
warm
0.40
7/25/23
2
102,000.0
Dry
warm
0.00
Total. Gallons
174,000.0

Triple S Farms
Wallace, North Carolina
Triple S Farms
WQ0030998
3rd Quarter 2023
Wallace WWTP
Stabilization Method: Lime
Farmer: Eric Smith
Acres: 17.30
Site/Tract: 1
Application Method: Surface
Field: 6
Percent Solids: 2.41
Residual Report No.: WL 3-2023-14447
Crop: Bermudagrass
. ..... .....
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
9/ 19/23
6
12,000.0
Dry
warm
0.00
9/28/23
6
18,000.0
Dry
Cool
0.00
Total Gallons
3%000.0

Triple S Farms
Wallace, North Carolina
Triple S Farms
WQ0030998
4th Quarter 2023
Wallace WWTP
Stabilization Method: Lime
Farmer: Eric Smith
Acres: 36.00
Site/Tract: 1
Application Method: Surface
Field: 1
Percent Solids: 2.40
Residual Report No.: WL 4-2023-22878
Crop: Bermudagrass
............. ............
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
10/2/23
1
72,000.0
Dry
warm
0.00
10/2/23
1
369000.0
Dry
warm
0.00
10/3/23
1
6,000.0
Dry
warm
0.00
10/4/23
1
24,000.0
Dry
warm
0.00
Total Gallons
138,000.0

Triple S Farms
Wallace, North Carolina
Triple S Farms
WQ0030998
4th Quarter 2023
Wallace WWTP
Stabilization Method: Lime
Farmer: Eric Smith
Acres: 19.60
Site/Tract: 1
Application Method: Surface
Field: 345
Percent Solids: 2.40
Residual Report No.: WL 4-2023-22878
Crop: Fescue
............... .... .. ...........
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
10/4/23
345
30,000.0
Dry
warm
0.00
10/5/23
345
48,000.0
Dry
warm
0.00
10/6/23
345
72,000.0
Dry
warm
0.00
Total Gallons
150,000.0

Triple S Farms
Wallace, North Carolina
Triple S Farms
WQ0030998
4th Quarter 2023
Wallace WWTP
Stabilization Method: Lime
Farmer: Eric Smith
Acres: 14.00
Site/Tract: 1
Application Method: Surface
Field: 3A
Percent Solids: 2.40
Residual Report No.: WL 4-2023-22878
Crop: Fescue
........................ . .........
.............
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
10/11/23
3A
6,000.0
Dry
Cool
0.00
10/19/23
3A
24,000.0
Dry
Cool
0.00
10/20/23
3A
6,000.0
Dry
Cool
0.41
Total Gallons
36,000.0

Town of Warsaw
Warsaw, North Carolina
Triple S Farms & Cleaning, Inc
WQ0030998
Normal Annual 2023
Warsaw WWTP
Farmer: Eric Smith
Acres: 36
Site/Tract: 1
Application Method: Surface
Field: 1
Percent Solids: 1.13
Residual Report No.: WS1 2023-12762
Crop: Bermudagrass
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
3/6/23
1
42,000.0
Dry
Cool
0.00
5/l/23
1
48,000.0
Dry
Cool
0.00
5/2/23
1
100,000.0
Dry
Cool
0.02
Total Gallons
1190;000:0

Town of Warsaw
Warsaw, North Carolina
Triple S Farms & Cleaning, Inc
WQ0030998
Normal Annual 2023
Warsaw WWTP
Farmer: Eric Smith
Acres: 17.3
Site/Tract: 1
Application Method: Surface
Field: 6
Percent Solids: 1.13
Residual Report No.: WS1 2023-12762
Crop: Bermudagrass
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
3/7/23
6
54,000.0
Dry
Cool
0.00
3/8/23
6
36,000.0
Dry
Cool
0.00
Total Gallons
90,000.0

Town of Warsaw
Warsaw, North Carolina
Triple S Farms & Cleaning, Inc
WQ0030998
Normal Annual 2023
Warsaw WWTP
Farmer: Jonathan Smith
Acres: 5.03
Site/Tract: JS
Application Method: Surface
Field: 2
Percent Solids: 1.13
Residual Report No.: WS1 2023-12762
Crop: oats
.. ............ ...................... .. .. .... ........ . ...
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
11/30/23
2
18,000.0
Dry
Cool
0.00
12/7/23
2
42,000.0
Dry
Cool
0.00
Total Gallons
60,000.0

Town of Warsaw
Warsaw, North Carolina
Triple S Farms & Cleaning, Inc
WQ0030998
Normal Annual 2023
Warsaw WWTP
Farmer: Jonathan Smith
Acres: 7.27
Site/Tract: JS
Application Method: Surface
Field: 3
Percent Solids: 1.13
Residual Report No.: WS1 2023-12762
Crop: oats
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
12/4/23
3
24,000.0
Dry
Cool
0.00
12/7/23
3
72,000.0
Dry
Cool
0.00
Total Gallons
96090.0

Town of Warsaw
Warsaw, North Carolina
Triple S Farms & Cleaning, Inc
WQ0030998
Normal Annual 2023
Warsaw WWTP
Farmer: Jonathan Smith
Acres: 8.66
Site/Tract: JS
Application Method: Surface
Field: 4
Percent Solids: 1.13
Residual Report No.: WS1 2023-12762
Crop: oats
.. .. .................. ....
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
12/1/23
4
96,000.0
Dry
Cool
0.00
Total Gallons
96,000.0

Town of Warsaw
Warsaw, North Carolina
Triple S Farms & Cleaning, Inc
WQ0030998
Normal Annual 2023
Warsaw WWTP
Farmer: Scott Thigpen
Acres: 14.05
Site/Tract: ST
Application Method: Surface
Field: 1
Percent Solids: 1.13
Residual Report No.: WS1 2023-12762
Crop: Fescue
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
12/8/23
1
42,000.0
Dry
Cool
0.00
Total Gallons
42,000.0

Town of Warsaw
Warsaw, North Carolina
Triple S Farms & Cleaning, Inc
WQ0030998
Normal Annual 2023
Warsaw WWTP
Farmer: Scott Thigpen
Acres: 20.3
Site/Tract: ST
Application Method: Surface
Field: 2
Percent Solids: 1.13
Residual Report No.: WS1 2023-12762
Crop: Bermudagrass
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
10/16/23
2
72,000.0
Dry
Cool
0.00
10/17/23
2
83,000.0
Dry
Cool
0.00
Total Gallons
1155,000.0

Town of Warsaw
Warsaw, North Carolina
Triple S Farms & Cleaning, Inc
WQ0030998
Annual 2 2023
Warsaw WWTP
Farmer: Eric Smith
Acres: 17.3
Site/Tract: 1
Application Method: Surface
Field: 6
Percent Solids: 1.78
Residual Report No.: WS2 2023-29979
Crop: Bermudagrass
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
9/12/23
6
24,000.0
Dry
Warm
0.02
9/14/23
6
18,000.0
Dry
Warm
0.00
9/18/23
6
60,000.0
Moist
Warm
0.10
9/19/23
6
29,000.0
Dry
Warm
0.00
Total Gallons
13I,000.0

Town of Warsaw
Warsaw, North Carolina
Triple S Farms & Cleaning, Inc
WQ0030998
Annual 2 2023
Warsaw WWTP
Farmer: Eric Smith
Acres: 36
Site/Tract: 1
Application Method: Surface
Field: 1
Percent Solids: 1.78
Residual Report No.: WS2 2023-29979
Crop: oats
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
12/14/23
1
48,000.0
Dry
Cool
0.00
Total Gallons
48,000.0

Town of Warsaw
Warsaw, North Carolina
Triple S Farms & Cleaning, Inc
WQ0030998
Annual 2 2023
Warsaw WWTP
Farmer: Eric Smith
Acres: 12.8
Site/Tract: 1
Application Method: Surface
Field: 10
Percent Solids: 1.78
Residual Report No.: WS2 2023-29979
Crop: oats
.......... ... . .........
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
12/14/23
10
102,000.0
Dry
Cool
0.00
Total Gallons
102,000.0