WQ0001026_2023 Residual Annual Report_20240229 (2)

Initial Review
Reviewer
nathaniel.thorn burg
Is this submittal an application? (Excluding additional information.) *
Yes No
If not an application what is the submittal type?* Annual Report
Residual Annual Report
Additional Information
Other
Annual Report Year* 2023
Permit Number (IR) * WQ0001026
Applicant/Permittee City of Washington
Email Notifications
Does this need review by the hydrogeologist? * Yes U No
Regional Office Washington
CO Reviewer
Admin Reviewer Wanda Gerald

Submittal Form
Project Contact Information
Please provide information on the person to be contacted by NDB Staff regarding electronic submittal, confirmation of receipt, and other correspondence.
Name* Brent Collins
Email Address*
[e-mail]
Project Information
.........................
Application/Document Type*
New (Fee Required)
Modification - Major (Fee Required)
Renewal with Major Modification (Fee
Required)
Annual Report
Additional Information
Other
Phone Number*
3363993646
Modification - Minor
Renewal
GW-59, NDMR, NDMLR, NDAR-1,
N DAR-2
Residual Annual Report
Change of Ownership
We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form.
https://edoes.deq.nc.gov/Forms/NonDischarge_Monitoring_Report
Permit Type:* Wastewater Irrigation High -Rate Infiltration
Other Wastewater Reclaimed Water
Closed -Loop Recycle Residuals
Single -Family Residence Wastewater Other
Irrigation
Permit Number:* WQ0001026
Has Current Existing permit number
Applicant/Permittee Address* PO Box 1988, Washington, NC 27889
Facility Name* City of Washington Class B Residuals Program
Please provide comments/notes on your current submittal below.
At this time, paper copies are no longer required. If you have any questions about what is required, please contact Nathaniel Thornburg
at [e-mail].
Please attach all information required or requested for this submittal to be reviewed here.
(Application Form, Engineering Plans, Specifications, Calculations, Etc.)
2023 Washington Annual Report - WQ0001026.pdf 12.38MB
Upload only 1 PDF document (less than 250 MB). Multiple documents must be combined into one PDF file unless file is larger
than upload limit.
* By checking this box, I acknowledge that I understand the application will not be accepted for pre -review until the fee (if required) has
been received by the Non -Discharge Branch. Application fees must be submitted by check or money order and made payable to the
North Carolina Department of Environmental Quality (NCDEQ). I also confirm that the uploaded document is a single PDF with all parts
of the application in correct order (as specified by the application).
Mail payment to:
NCDEQ — Division of Water Resources
Attn: Non -Discharge Branch
1617 Mail Service Center
Raleigh, NC 27699-1617
Signature
Submission Date 2/29/2024

M
i— Resources, Inc.
City of Washington
2023 Annual Report
Residuals Land Application
Permit No. WQ0001026
Prepared By:
EMA Resources, Inc.
Phone 336*751.1441 — Fax 336*751.1442
755 Yadkinville Rd — Mocksville, NC 27028

February 27, 2024
DENR/Water Quality Section
Non -Discharge Compliance Unit
1617 Mail Service Center
Raleigh, NC 27699-1617
Re: 2023 Annual Report - Washington
Treatment and Land Application of Residuals
Permit No. WQ0001026
Dear Sir or Madam:
Enclosed is the 2023 Annual Report for the above referenced land application permit.
During 2023 EMA Resources, Inc. land applied 327.77 dry tons of wastewater residuals
to 111.9 acres of private farmland. Please contact Brent Collins - Director of Technical
Services if you have any further questions regarding this report.
Sincerely,
z� 4: �'
Brent Collins
Director of Technical Services
brent. collinsnemaresourcesinc. com
Phone 336*751.1441 — Fax 336*751.1442
755 Yadkinville Rd — Mocksville, NC 27028

ANNUAL LAND APPLICATION CERTIFICATION FORM
WQ Permit#: WQ0001026 County
Facility Name (as shown on permit):
Land Application Operator:
Beaufort County, NC Year:
City of Washington
EMA Resources Inc.
2023
Phone: [phone]
Land application of residuals as allowed by the permit occurred during the past calendar year?
0 Yes 0 No - If No, skip Part A, and Part B and proceed to Part C. Also, If residuals were
generated but not land applied, please attach an explanation on how the residuals were handled.
Part A - Residuals Application Summary:
Total number of application fields in thepermit:
54
Total number of fields utilized for land application during the year:
6
Total amount of dry tons applied during the year for all application sites:
327.77
Total number of acres utilizes for land application during the year:
111.9
Part B - Annual Compiance Statement:
Facility was compliant during calendar year 2023 with all conditions of the land application permit
(including but not limited to items 1-13 below) issued by the Division of Water Quality. 0 Yes 0 No
If no please, provide a written description why the facility was not compliant, the dates, and explain corrective action
taken.
1) Only residuals approved for this permit were applied to the permitted sites.
2) Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or
the limit specified in the permit.
3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies
of laboratory results are attached.
4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5) All other monitoring was performed in accordance with the permit and reported during the year as required and three (3)
copies of certified laboratory results are attached.
6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .1105(a) or the Pollutant
Loading Rates in 15A NCAC 02T .I 105(b) (applicable to 40 CFR Part 503 regulated facilities).
7) All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part
503 regulated facilities).
8) All monitoring and reporting requirements in 15A NCAC 02T .I I I I were complied with (applicable to 40 CFR Part
503 regulated facilities).
9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Quality.
10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
11) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as
specified in the permit.
12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13) All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C - Certification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate,
and complete. I am aware that there are significant penalties for submitting false information, including the
possibility of fines and imprisonment for knowing violations."
Hope Woolard - Public Works Director
Permittee Name and Title (type or print)
Lonnie Woolaw
Lonnie Woolard (Feb 6, 202414:28 EST)
02/06/24
Ifte Woo�yo( 02/07/24
Hope Woolard (Feb 7, 202415:34 EST)
Signature of Permittee
gad—,1
Date
4;510�,Z- 2/5/2024
Signature of Preparer* Date Signature of Land Applier Date
(if different from Permittee) (if different from Permittee and Preparer)
* Preparer is defined in 40 CFR Part 503.9 (r) and 15A NCAC 02T .1102 (26) DENR FORM ACF (12/2006)

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B
WQ Permit Number: WQ0001026 Laboratory: 1)
Facility Name: City of Washington 2)
Residual Source WQ # or NCO020648 3)
NPDES #: 4)
WWTP Name: Washington WWTP 5)
Residual Analysis Data
Waypoint Analytical
Parameter
(mg/kg)
Conc.
Limit
m /k a
Sample or Composite Date
4/20/23
4/25/23
Spring
Average
10/25/23
11/5/23
Fall
Average
Percent Solids (%)
NA
5.69
5.79
5.74
3.15
2.93
3.04
Arsenic
75
0.256
4.21
2.2
9.06
8.53
8.30
Cadmium
85
0.0214
0.432
0.2
1.61
1.71
1.66
Copper
4,300
9
151
80.0
294
305
299.50
Chromium
NA
0.567
10.9
5.7
21.6
21.8
21.70
Lead
840
0.756
13.8
7.3
23.6
30.2
26.90
Mercury
57
0.0308
0.511
0.3
1.08
0.706
0.89
Molybdenum
75
0.22
2.49
1.4
6.35
7.24
6.80
Nickel
420
0.462
9.4
4.9
16.4
16.3
16.35
Selenium
100
0.342
5.61
3.0
11.3
11.9
11.60
Zinc
7.500
24.5
421
222.8
810
843
826.50
Total Phosphorus
NA
1090
18200
9645
34800
36200
35500
TKN
NA
6570
87500
47035
47400
67900
57650
Ammonia -Nitrogen
NA
319
5890
3104.5
9520
9730
9625
Nitrate and Nitrite
NA
57.7
24
40.9
102
123
113
a For surface disposal facilities the ceiling concentration limits listed in this form are not applicable. Reference the individual permit for metals limits.
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant
penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
Lownie Woolai-d
Lonnie Woolard (Feb 6, 2024-8 EST)
Signature of Preparer
02/06/24
Date
*Preparer is defined in 40 CFR Part 5039(r) and 15A NCAC 2T .1102 (26)
DENR FORM RSSF (12/2006)

ANNUAL RESIDUAL SAMPLING SUMMARY FORM - B
Report all sampling analysis results for parameters not listed in FORM RSSF that are part of the WQ permit or were analyzed for over the past
calendar year. Use additional forms as needed.
WQ Permit Number:
1�.�L�IIIIIII[II►.T•'!
Facility Name: City of Washington
Residual Source
NPDES # or WQ#:
WWTP Name:
Residual Analysis Data
Laboratory: 1) Waypoint Analytical
2)
NCO020648 3)
4)
Washington WWTP 5)
Parameter
(mg/kg)
Sample or Composite Date
4/20/23
4/25/23
Spring
Average
10/25/23
11/5/23
Fall
Average
Aluminum
1050
38500
19775
40300
42700
41500
Calcium
5860
34200
20030
26700
28700
27700
Magnesium
3430
3580
3505
2350
2480
2415
pH
7.1
6.7
6.9
7.2
7.3
7.25
Potassium
98.7
3390
1744.35
2210
2350
2280
Sodium
103
3360
1731.5
3290
3450
3370
PAN
2092.5
27452
14772
16226
22439
19332.5
SAR
0.06
0.25
0.92
0.9
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
LOGy iie WOOINV(
Lonnie Woolard (Feb 6. N2414:2e EST)
Signature of Preparer
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
02/06/24
Date
DENR FORM RSSF - B (12/2006)

4/20/2023
mg/kg
mg/L
Equiv Weight Milli Equiv
Sodium
103
5.8607
23 0.254813
Calcium
5860
333.434
20 16.6717
Magnesium
3430
195.167
12 16.26392
Percent Solids
5.69
SAR
0.06
SAR =
Na+
z (Ci a2+ + Mg2+ )
0.25481
0.5( 16.672 2 + 16.26392 2 )

4/25/2023
mg/kg mg/L Equiv Weight Milli Equiv
Sodium 1770 102.483 23 4.455783
Calcium 110000 6369 20 318.45
Magnesium 63300 3665.07 12 305.4225
Percent Solids 5.79
SAR 0.25
SAR =
Na+
z (Ci a2+ + Mg2+ )
4.45578
0.5( 318.45 2 + 305.42250 2 )

10/25/2023
mg/kg
mg/L
Sodium
3290
103.635
Calcium
26700
841.05
Magnesium
2350
74.025
Percent Solids
3.15
SAR
0.92
SAR =
Na+
z (Ci a2+ + Mg2+ )
Equiv Weight Milli Equiv
23 4.50587
20 42.0525
12 6.16875
4.50587
0.5( 42.053 2 + 6.16875 2 )

11 /8/2023
mg/kg
mg/L
Sodium
3450
101.085
Calcium
28700
840.91
Magnesium
2480
72.664
Percent Solids
2.93
SAR
0.90
SAR =
Na+
z (Ci a2+ + Mg2+ )
Equiv Weight Milli Equiv
23 4.395
20 42.0455
12 6.055333
4.39500
0.5( 42.046 2 + 6.05533 2 )

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: City of Washington Total Dry Tons Applied (Annual):
Permit #: WQ0001026 Cation Exchange Capacity (non 503 only):
Operator: Hunter Roost Farms Owner: Hunter Roost Farms Predominant Soil Series:
Acres Used: 26.81 Acres Permitted: 26.81 Site #: BF210 Field #:
31.13
GoA
2
Residual Analysis Data (Heavy Metals and Total Phosphorus use mj!/kj!, % Solids use Raw Percent #):
Com-
posite
Date
Total
Phos-
phorus
Annual Heavy Metal Field Loadinjjs (Calculated in lbs/acre):
TotalMEB
D
Event
1 11
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 11
1 11
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 11
1 :.
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 :.
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
1 11
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 11
�
1 11
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 11
�
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
1 11
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 11
®
1 :
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 :
Total
'
`•
1 111
1 111
1111
1 111
1111
1 111
1111
1 111
1 111
1111
1 111M
"1 certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
2/5/2024
Signature of Land Applier
Date
DENR FORM MFLSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: City of Washington WQ Permit #: WQ0001026 Field #: 2 Acres Utilized: 26.81
Land Owner: Hunter Roost Farms Annual Dry Tons Applied: 31.13 Site #: BF210 Acres Permitted: 26.81
Operator: Hunter Roost Farms Predominant Soil Series: GoA Cation Exchange Capacity (non 503): 0
Crop 1 Name: Soybeans Crop 1 Max. PAN: 176 Crop 2 Name: Crop 2 Max. PAN:
O =
o
Volume applied
(enter one) Solids/
Liquid
Cu. Yds G8110nS
%
Solids
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
Soil
Cond.
(Dry,
Wet
Moist)
Precip.
Past 24
Hrs.
inches
a
4 '�
'a
a
o
� --
*
°�
4.
w -
co :L
* N
TKN
mg/kg
Z a
.; El
o El
a� o0
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
(lbs/acre)
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Crop 1
Crop 2
4/19
19500
5.74
0.174
Washington
D
<.5"
S
0.5
0.3
47035
3105
41
5.144
NA
Beans
4/20
110500
5.74
0.987
Washington
D
<.5"
S
0.5
0.3
47035
3105
41
29.147
NA
Beans
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0
0
0.000
Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp
to this form):
0.000
0.000
TOTALS:
01
130000
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn
P
34.291
0.000
Lime Applied
Annuallbs/acre
0.005
0.001
0.186
0.013
0.017
0.001
0.003
0.011
0.007
0.518
22.396
Date
lbs/ac
Prior Years Cumulative lbs/ac
0.05
0.007
1.736
0.193
0.174
0.009
0.044
0.121
0.048
4.592
Current Cumulative lbs/ac
0.055
1 0.008
1.922
0.206
0.191
0.010
0.047
0.132
0.055
5.110
Permitted C. P. L. R.****
36
34
1 1338
1
1 267
1 15
1
1 374
1 89
1 2498
Permit PAN Limit 1 st/2nd Crop
F 176
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
2/5/2024 **Volatilization Rate: Surface - 0.5, Injection/Incorporation -1.0
Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: City of Washington Total Dry Tons Applied (Annual):
Permit #: WQ0001026 Cation Exchange Capacity (non 503 only):
Operator: Hunter Roost Farms Owner: Hunter Roost Farms Predominant Soil Series:
Acres Used: 15.14 Acres Permitted: 15.14 Site #: BF210 Field #:
83.10
Le
6
Residual Analysis Data (Heavy Metals and Total Phosphorus use mj!/kj!, % Solids use Raw Percent #):
. •
•
posite
Date
Avg
©
©
m
Total
Phos-
phorus
Annual Heavy Metal Field Loadinjjs (Calculated in lbs/acre):
TotalMEB
•
D
-
••
Event
1 •
1 1
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
OEM
1 11
1 11
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 11
1 .
1�
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1 �
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1:
1 1••
1 1�
1 111
1111
1 111
1111
1 111
1111
1 111
1 111
1111
1 111
1 1
1 11
1 11
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 11�
1 1
1 1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
��
1 1�
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
OEM
1 1
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1� •
®
1:
�
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
••
Total
'
m
1
1 111
1111
1 111
1111
1 111
1111
1 111
1 111
1111
1 111
:•
"1 certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
2/5/2024
Signature of Land Applier
Date
DENR FORM MFLSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: City of Washington
WQ Permit #: WQ0001026 Field #:
6 Acres Utilized:
15.14
Land Owner: Hunter Roost Farms
Annual Dry Tons Applied: 83.10 Site #:
BF210 Acres Permitted:
15.14
Operator: Hunter Roost Farms
Predominant Soil Series: Le
Cation Exchange Capacity (non 503):
0
Crop 1 Name: Soybeans
Crop 1 Max. PAN: 146 Crop 2 Name:
Small Grain Crop 2 Max. PAN:
50
p
M
Volume applied
(enter one) Solids/
Liquid
Cu. Yds Gallons
"
�"
Solids
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
Soil
Cond.
(Dry,
e '
Moist)
Precip.
Past 24
Hrs.
inches
>
4 �
co
•*
a m
c
7y
?:
*
o'
0
0
* N
TKN
mg/kg
Z 1
o
as o
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
lbs/acre
( )
Name of Crop Type
ReceivingResidual
Application
Crop 1
Crop 2
Crop 1
Crop 2
4/18
208000
5.74
3.288
Washington
D
<.5"
S
0.5
0.3
47035
3105
41
97.156
NA
Beans
4/19
91000
5.74
1.439
Washington
D
<.5"
S
0.5
0.3
47035
3105
41
42.506
NA
Beans
10/30
65000
3.04
0.544
Washington
D
<.5"
S
0.5
0.3
57650
9625
113
Na
21.044
SG
10/31
26000
3.04
0.218
Washington
D
<.5"
S
0.5
0.3
57650
9625
113
Na
8.418
SG
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0
0
0.000
Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp
to this form):
0.000
0.000
TOTALS:
o
390000
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn P
139.662
r 29.461
Lime Applied
Annuallbs/acre
0.034
0.005
1.214
0.087
0.110
0.004
0.023
0.072
0.046
3.369 145.286
Date
lbs/ac
Prior Years Cumulative lbs/ac
0.205
0.044
8.276
0.908
0.844
0.044
0.159
0.507
0.212
19.7
Current Cumulative lbs/ac
0.239
1 0.049
9.490
0.995
0.954
0.048
0.182
0.579
0.258
23.069
Permitted C. P. L. R.****
1 36
34
1 1338
1
1 267
1 15
1
1 374
1 89
1 2498
Permit PAN Limit 1 st/2nd Crop
1
1 146
1 50
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
2/5/2024 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
City of Washington Total Dry Tons Applied (Annual):
WQ0001026 Cation Exchange Capacity (non 503 only):
Hunter Roost Farms Owner: Hunter Roost Farms Predominant Soil Series:
11.82 Acres Permitted: 11.82 Site #: BF210 Field #:
63.52
Le
7
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
kVWPT_"1
Com-
posite
Date
©
©
m
Total
Phos-
phorus
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
TotalE
D
-
••
Event
�•
1
1 1
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
OEM
1 11
1 11
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 11
��
1 � .1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1:•
1 1•
1 1�
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1:
1 11
1 11
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 11�
1 1
1 1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
��
1 1�
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
1 1
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1�
®��
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
Total
'
:::•`
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
•
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
2/5/2024
Signature of Land Applier
Date
DENR FORM MFLSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: City of Washington
WQ Permit #: WQ0001026 Field #:
7 Acres Utilized:
11.82
Land Owner: Hunter Roost Farms
Annual Dry Tons Applied: 63.52 Site #:
BF210 Acres Permitted:
11.82
Operator: Hunter Roost Farms
Predominant Soil Series: Le
Cation Exchange Capacity (non 503):
0
Crop 1 Name: Soybeans
Crop 1 Max. PAN: 146 Crop 2 Name:
Small Grain Crop 2 Max. PAN:
50
p
M
Volume applied
(enter one) Solids/
Liquid
Cu. Yds Gallons
"
�"
Solids
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
Soil
Cond.
(Dry,
e '
Moist)
Precip.
Past 24
Hrs.
inches
>
4 �
co
•*
a m
c
7y
?:
*
o'
0
0
* N
TKN
mg/kg
Z 1
o
as o
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
lbs/acre
( )
Name of Crop Type
ReceivingResidual
Application
Crop 11
Crop 2
Crop 1
Crop 2
4/17
175500
5.74
3.554
Washington
D
<.5"
S
0.5
0.3
47035
3105
41
105.00
NA
Beans
4/18
52000
5.74
1.053
Washington
D
<.5"
S
0.5
0.3
47035
3105
41
31.11
NA
Beans
10/31
71500
3.04
0.767
Washington
D
<.5"
S
0.5
0.3
57650
9625
113
Na29.650
SG
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0
0
0.000
Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp
to this form):
0.000
0.000
TOTALS:
0
299000
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn P
136.112
29.650
Lime Applied
Annuallbs/acre
0.033
0.005
1.197
0.086
0.108
0.004
0.023
0.071
0.045
3.323 143.326
Date
lbs/ac
Prior Years Cumulative lbs/ac
0.206
0.041
7.699
0.812
0.801
0.041
0.151
0.473
0.212
18.538
Current Cumulative lbs/ac
0.239
1 0.046
8.896
0.898
0.909
0.045
0.174
0.544
0.257
21.861
Permitted C. P. L. R.****
1 36
34
1 1338
1
1 267
1 15
1
1 374
1 89
1 2498
Permit PAN Limit 1 st/2nd Crop
1
1 146
1 50
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
2/5/2024 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
City of Washington Total Dry Tons Applied (Annual):
WQ0001026 Cation Exchange Capacity (non 503 only):
Hunter Roost Farms Owner: Hunter Roost Farms Predominant Soil Series:
19.21 Acres Permitted: 19.21 Site #: BF210 Field #:
83.29
Le
8
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
. •
•
posite
Date
Avg
©
©
m
Total
Phos-
phorus
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
D
-
••
Event
•
1
1 1 •
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1'
OEM
1 11
1 11
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 11�
1 1
1�.
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1�
1 1 �
1 111
1111
1 111
1111
1 111
1111
1 111
1 111
1111
1 111
1 1
1 1
1 1�
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1'
1 11
1 11
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 11
1 1 1
1 1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1 1
••
1 1
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1.1
OEM
1 1
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1'
®�®
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
: • •
Total
' •
•: 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
•
•
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
2/5/2024
Signature of Land Applier
Date
DENR FORM MFLSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: City of Washington
WQ Permit #: WQ0001026 Field #:
8 Acres Utilized:
19.21
Land Owner: Hunter Roost Farms
Annual Dry Tons Applied: 83.29 Site #:
BF210 Acres Permitted:
19.21
Operator: Hunter Roost Farms
Predominant Soil Series: Le
Cation Exchange Capacity (non 503):
0
Crop 1 Name: Soybeans
Crop 1 Max. PAN: 146 Crop 2 Name:
Small Grain Crop 2 Max. PAN:
50
p
M
Volume applied
(enter one) Solids/
Liquid
Cu. Yds Gallons
"
�"
Solids
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
Soil
Cond.
(Dry,
e '
Moist)
Precip.
Past 24
Hrs.
inches
>
4 �
co
•*
a m
c
7y
?:
*
o'
0
0
* N
TKN
mg/kg
Z 1
o
as o
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
lbs/acre
( )
Name of Crop Type
ReceivingResidual
Application
Crop 1
Crop 2
Crop 1
Crop 2
4/19
149500
5.74
1.863
Washington
D
<.5"
S
0.5
0.3
47035
3105
41
55.036
NA
Beans
4/20
136500
5.74
1.701
Washington
D
<.5"
S
0.5
0.3
47035
3105
41
50.250
NA
Beans
10/31
97500
3.04
0.643
Washington
D
<.5"
S
0.5
0.3
57650
9625
113
Na
24.878
SG
11/1
19500
3.04
0.129
Washington
D
<.5"
S
0.5
0.3
57650
9625
113
Na
4.976
SG
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0
0
0.000
Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp
to this form):
0.000
0.000
TOTALS:
0
40,00o
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn P
105.286
29.854
Lime Applied
Annuallbs/acre
0.029
0.004
1.033
0.074
0.093
0.003
0.020
0.060
0.039
2.866 123.562
Date
lbs/ac
Prior Years Cumulative lbs/ac
0.173
0.034
6.007
0.637
0.645
0.034
0.121
0.38
0.181
14.515
Current Cumulative lbs/ac
0.202
1 0.038
7.040
0.711
0.738
0.037
0.141
0.440
0.220
17.381
Permitted C. P. L. R.****
1 36
34
1 1338
1
1 267
1 15
1
1 374
1 89
1 2498
Permit PAN Limit 1 st/2nd Crop
1
1 146
1 50
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
2/5/2024 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
City of Washington Total Dry Tons Applied (Annual):
WQ0001026 Cation Exchange Capacity (non 503 only):
Hunter Roost Farms Owner: Hunter Roost Farms Predominant Soil Series:
13.48 Acres Permitted: 13.48 Site #: BF210 Field #:
21.42
Ly
15
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Com-
posite
Date
Total
Phos-
phorus
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
TotalBOB
D
Event
1 1 •
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1 •
1 11
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 11
1•
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1'
1 1•
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1••
1 1:
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1:
1 11
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 11
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
��
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
®
• :
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
• :
Total
'
•
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
'
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
2/5/2024
Signature of Land Applier
Date
DENR FORM MFLSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: City of Washington
Land Owner: Hunter Roost Farms
Operator: Hunter Roost Farms
Crop 1 Name: Small Grain
WQ Permit #: WQ0001026 Field #:
Annual Dry Tons Applied: 21.42 Site #:
Predominant Soil Series: Ly
Crop 1 Max. PAN: 97 Crop 2 Name:
15
Acres Utilized:
BF210 Acres Permitted:
Cation Exchange Capacity (non 503):
Crop 2 Max. PAN:
13.48
13.48
0
o
o
Volume applied
(enter one) Solids/
Liquid
Cu. Yds Gallons
%
Solids
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
Soil
Cond.
(Dry,
Wet
Moist)
Precip.
Past 24
Hrs.
inches
a
4
a
o
� --
°�
4.
w -
co :L
* N
TKN
mg/kg
Z a
El
o
M o0
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
(lbs/acre)
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Crop 1
Crop 2
11/3
169000
3.04
1.589
Washington
D
<.5"
S
0.5
0.3
57650
9625
113
61.452
NA
SG
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1 0.000
0.000
0.000
0.000
0
0
0.000
Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp
to this form):
0.000
0.000
TOTALS:
01
169000
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn
P
61.452
0.000
Lime Applied
Annuallbs/acre
0.026
0.005
0.953
0.069
0.085
0.003
0.022
0.052
0.037
2.628
112.819
Date
lbs/ac
Prior Years Cumulative lbs/ac
0.038
0.006
1.132
0.076
0.105
0.005
0.021
0.062
0.037
3.2
Current Cumulative lbs/ac
0.064
0.011
2.085
0.145
0.190
0.008
0.043
0.114
0.074
5.828
Permitted C. P. L. R.****
36
34
1 1338
1
1 267
1 15
1
1 374
1 89
1 2498
Permit PAN Limit 1 st/2nd Crop
97
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
2/5/2024 **Volatilization Rate: Surface - 0.5, Injection/Incorporation -1.0
Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
City of Washington Total Dry Tons Applied (Annual):
WQ0001026 Cation Exchange Capacity (non 503 only):
Hunter Roost Farms Owner: Hunter Roost Farms Predominant Soil Series:
25.44 Acres Permitted: 25.44 Site #: BF210 Field #:
45.31
CrA
16
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Com-
posite
Date
Total
Phos-
phorus
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
TotalMEB
D
-
••
Event
1 1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1 1
1 11•
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 11•
1••
1 111
1 111
1111
1 111
1111
1 111
1111
1 111
1 111
1111
1 111
1•'
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
1 1••
1 111
1 111
1111
1 111
1111
1 111
1111
1 111
1 111
1111
1 111
1 1'•
1 11
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 11
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1'
��
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
1 1'
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1'
®
'•
1 111
1 111
1111
1 111
1111
1 111
1111
1 111
1 111
1111
1 111
•'•
Total
' •
•'
1 111
1 111
1111
1 111
1111
1 111
1111
1 111
1 111
1111
1 111
•'
•
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
2/5/2024
Signature of Land Applier
Date
DENR FORM MFLSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: City of Washington WQ Permit #: WQ0001026 Field #: 16 Acres Utilized: 25.44
Land Owner: Hunter Roost Farms Annual Dry Tons Applied: 45.31 Site #: BF210 Acres Permitted: 25.44
Operator: Hunter Roost Farms Predominant Soil Series: CrA Cation Exchange Capacity (non 503): 0
Crop 1 Name: Small Grain Crop 1 Max. PAN: 95 Crop 2 Name: Crop 2 Max. PAN:
o
o
Volume applied
(enter one) Solids/
Liquid
Cu. Yds G8110nS
%
Solids
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
Soil
Cond.
(Dry,
Wet
Moist)
Precip.
Past 24
Hrs.
inches
a
a
o
� --
*
°�
4.
w -
co
* N
TKN
mg/kg
Z a
.; El
o
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
(lbs/acre)
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Crop 1
Crop 2
11/1
123500
3.04
0.615
Washington
D
<.5"
S
0.5
0.3
57650
9625
113
23.795
NA
SG
11/2
201500
3.04
1.004
Washington
D
<.5"
S
0.5
0.3
57650
9625
113
38.824
NA
SG
11/3
32500
3.04
0.162
Washington
D
<.5"
S
0.5
0.3
57650
9625
113
6.262
NA
SG
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0
0
0.000
Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp
to this form):
0.000
0.000
TOTALS:
01
357500
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn
P
68.8s1
0.000
Lime Applied
Annuallbs/acre
0.030
0.006
1.069
0.077
0.096
0.003
0.024
0.058
0.041
2.946
126.451
Date
lbs/ac
Prior Years Cumulative lbs/ac
0.238
0.043
8.432
0.886
0.848
0.044
0.166
0.505
0.25
20.635
Current Cumulative lbs/ac
0.268
0.049
9.501
0.963
0.944
0.047
0.190
0.563
0.291
23.581
Permitted C. P. L. R.****
36
34
1 1338
1
1 267
1 15
1
1 374
1 89
1 2498
Permit PAN Limit 1 st/2nd Crop
95
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
2/5/2024 **Volatilization Rate: Surface - 0.5, Injection/Incorporation -1.0
Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

Waypointo
ANALYTICAL
5/1 /2023
EMA Resources Inc
Mr. Brent Collins
755 Yadkinville Rd
Mocksville, NC, 27028
Ref: Analytical Testing
Lab Report Number: 23-111-0011
Client Project Description: Washington, NC
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 1 Fax [phone]
www.waypointanalytical.com
Dear Mr. Brent Collins:
Waypoint Analytical, LLC. received sample(s) on 4/21/2023 for the analyses presented in the following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Where the laboratory was not responsible for the sampling
stage (refer to the chain of custody) results apply to the sample as received.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2021) and NELAC unless otherwise indicated. Any parameter
for which the laboratory is not officially NELAP accredited is indicated by a'—' symbol. These are not included in
the scope because NELAP accreditation is either not available or has not been applied for. Additional
certifications may be held/are available for parameters, where NELAP accreditation is not required or applicable.
A full list of certifications is available upon request.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Connie Cook
Project Manager
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 1 of 8

Waypointo
ANALYTICAL
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 ° Fax [phone]
www.waypointanalytical.corn
Certification Summary
Laboratory ID: WP MTN: Waypoint Analytical, LLC., Memphis, TN
State
Program
Lab ID
Expiration Date
Alabama
State Program
40750
02/29/2024
Arkansas
State Program
88-0650
02/07/2024
California
State Program
2904
06/30/2023
Florida
State Program
- NELAP
E871157
06/30/2023
Georgia
State Program
C044
11/14/2025
Georgia
State Program
04015
06/30/2023
Illinois
State Program
- NELAP
200078
10/10/2023
Kentucky
State Program
80215
06/30/2023
Kentucky
State Program
KY90047
12/31/2023
Louisiana
State Program
- NELAP
LA037
12/31/2023
Louisiana
State Program
- NELAP
04015
06/30/2023
Mississippi
State Program
MS
11/14/2025
North Carolina
State Program
47701
07/31/2023
North Carolina
State Program
415
12/31/2023
Pennsylvania
State Program
- NELAP
68-03195
05/31/2024
South Carolina
State Program
84002
06/30/2023
Tennessee
State Program
02027
11/14/2025
Texas
State Program
- NELAP
T104704180
09/30/2023
Virginia
State Program
00106
06/30/2023
Virginia
State Program
- NELAP
460181
09/14/2023
Page 1 of 1 00001/23-111-0011
Page 2 of 8

waypoint 2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 Fax [phone]
ANALYTICAL www.waypointanalytical.com
Sample Summary Table
Report Number: 23-111-0011
Client Project Description: Washington, NC
Lab No Client Sample ID
99755 Washington
Matrix Date Collected
Solids 04/20/2023 08:00
Date Received
04/21/2023
Page 3 of 8

Waypointo
ANALYTICAL
Client: EMA Resources Inc
Project: Washington, NC
Lab Report Number: 23-111-0011
Date: 4/28/2023
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 1 Fax [phone]
www.waypointanalytical.com
CASE NARRATIVE
Metals Analysis Method 6010D
Sample 99755 (Washington)
Analyte: Calcium
QC Batch No: L678393/L677740
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 99755 (Washington)
Analyte: Potassium
QC Batch No: L678393/L677740
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Sample 99755 (Washington)
Analyte: Magnesium
QC Batch No: L678393/L677740
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Page 4 of 8

0
Waypoint, 2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 Fax [phone]
ANALYTICAL www.waypointanalytical.com
46245
EMA Resources Inc Project Washington, NC
Mr. Brent Collins Report Date : 05/01/2023
755 Yadkinville Rd Information : Received : 04/21/2023
Mocksville , NC 27028 n �
Connie Cook
Report Number : 23-111-0011
REPOR T OF A NA L YSIS
Project
Manager
Lab No : 99755
Matrix:
Solids
Sample ID : Washington
Sampled:
4/20/2023
8:00
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Method
Moisture
6.60
%
1
04/27/2317:15
JLS
SW-DRYWT
Ammonia Nitrogen
319
mg/Kg - dry
17.1
107
1
04/27/23 13:30
CLP
4500NH3C-2011
Nitrate+Nitrite-N
57.7
mg/Kg - dry
1.07
5.35
1
04/27/23 16:06
ZBD
4500NO3F-2016
Organic N
6255
mg/Kg - dry
17.13
107.1
1
04/27/23 12:30
CALCULATION
pH
7.1
s.u.
1
04/28/2316:00
CNB
9045D
Total Solids
5.69
%
0.010
0.010
1
04/27/23 16:15
JLS
2540G-2011
Total Volatile Solids
40.3
%
0.010
0.010
1
04/27/23 16:15
JLS
2540G-2011
Total Kjeldahl Nitrogen
6570
mg/Kg - dry
10.7
268
1
04/27/23 12:30
CLP ')M-4500-NH3C-TKP
Phosphorus
1090
mg/Kg - dry
2.96
5.35
1
04/25/23 18:13
TJS
6010D
Aluminum
1050
mg/Kg - dry
4.95
5.35
1
04/25/23 18:13
TJS
6010D
Arsenic
<0.256
mg/Kg - dry
0.256
0.535
1
04/25/23 18:13
TJS
6010D
Cadmium
<0.0214
mg/Kg - dry
0.0214
0.107
1
04/25/23 18:13
TJS
6010D
Calcium
5860
mg/Kg - dry
41.4
53.5
1
04/25/23 18:13
TJS
6010D
Chromium
0.567
mg/Kg - dry
0.252
0.267
1
04/25/23 18:13
TJS
6010D
Copper
9.00
mg/Kg - dry
0.332
0.535
1
04/25/23 18:13
TJS
6010D
Iron
486
mg/Kg - dry
9.12
10.7
1
04/25/23 18:13
TJS
6010D
Lead
0.756
mg/Kg - dry
0.192
0.321
1
04/25/23 18:13
TJS
6010D
Magnesium
3430
mg/Kg - dry
2.76
5.35
1
04/25/23 18:13
TJS
6010D
Manganese
16.8
mg/Kg - dry
0.347
0.535
1
04/25/23 18:13
TJS
6010D
Mercury
0.0308 J
mg/Kg - dry
0.0211
0.175
1
04/28/23 14:03
FDS
7471A
Molybdenum
0.220 J
mg/Kg - dry
0.144
0.267
1
04/25/23 18:13
TJS
6010D
Nickel
0.462
mg/Kg - dry
0.128
0.267
1
04/25/23 18:13
TJS
6010D
Potassium
98.7
mg/Kg - dry
6.62
10.7
1
04/25/23 18:13
TJS
6010D
Qualifiers/ DF
Dilution Factor
J
Estimated value
Definitions MQL
Method Quantitation Limit
Page 5 of 8

0
Waypoint,
2790 Whitten
Road, Memphis, TN 38133
Main 901.213.2400 0 Fax [phone]
ANALYTICAL
www.waypointanalytical.com
46245
EMA Resources Inc
Project
Washington, NC
Mr. Brent Collins
Report Date : 05/01/2023
755 Yadkinville Rd
Information :
Received : 04/21/2023
Mocksville , NC 27028
Connie Cook
Report Number : 23-111-0011
REPOR T OF A NA L YSIS
Project Manager
Lab No : 99755
Matrix: Solids
Sample ID : Washington
Sampled: 4/20/2023 8:00
Test
Results
Units
MDL
MQL DF Date / Time By Analytical
Analyzed Method
Selenium
<0.342
mg/Kg - dry
0.342
0.535 1 04/25/23 18:13 TJS 6010D
Sodium
103
mg/Kg - dry
13.9
26.8 1 04/25/23 18:13 TJS 6010D
Zinc
24.5
mg/Kg - dry
0.867
1.34 1 04/25/23 18:13 TJS 6010D
Sulfur
342
mg/Kg - dry
5.55
10.7 1 04/27/23 00:53 BKN 6010D
Sodium Absorption Ratio
0.25
Ratio
0.01
0.01 1 04/25/23 18:13 CALCULATION
Qualifiers/ DF Dilution Factor
Definitions
J Estimated value
Page 6 of 8

(2)
WayPAoint..
NALYTICAL
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 ° Fax [phone]
www.waypointanalytical.com
Shipment Receipt Form
Customer Number: 46245
Customer Name: EMA Resources Inc
Report Number: 23-111-0011
Shipping Method
Fed Ex 0 US Postal 0 Lab 0 Other:
0 UPS 0 Client 0 Courier Thermometer ID: T135
Shipping container/cooler uncompromised?
* Yes
0 No
Number of coolers/boxes received
F
Custody seals intact on shipping container/cooler?
0 Yes
0 No
Not Present
Custody seals intact on sample bottles?
0 Yes
0 No
Not Present
Chain of Custody (COC) present?
Yes
0 No
COC agrees with sample label(s)?
U Yes
0 No
COC properly completed
U Yes
0 No
Samples in proper containers?
U Yes
0 No
Sample containers intact?
Yes
0 No
Sufficient sample volume for indicated test(s)?
Yes
0 No
All samples received within holding time?
Yes
0 No
Cooler temperature in compliance?
Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
Yes
0 No
Water - Sample containers properly preserved
0 Yes
0 No
N/A
Water - VOA vials free of headspace
0 Yes
0 No
N/A
Trip Blanks received with VOAs
0 Yes
0 No
0 N/A
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
0 N/A
F_ High concentration container (48 hr) F Low concentration EnCore samplers (48 hr)
F_ High concentration pre -weighed (methanol -14 d) Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included?
0 Yes
0 No
Comments:
Signature: Emily M. Peterson Date & Time: 04/21/2023 09:28:43
Page 7 of 8

.0
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Page 8 of 8

Waypointo
ANALYTICAL
5/8/2023
EMA Resources Inc
Mr. Brent Collins
755 Yadkinville Rd
Mocksville, NC, 27028
Ref: Analytical Testing
Lab Report Number: 23-116-0077
Client Project Description: Washington, NC
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 1 Fax [phone]
www.waypointanalytical.com
Dear Mr. Brent Collins:
Waypoint Analytical, LLC. received sample(s) on 4/26/2023 for the analyses presented in the following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Where the laboratory was not responsible for the sampling
stage (refer to the chain of custody) results apply to the sample as received.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2021) and NELAC unless otherwise indicated. Any parameter
for which the laboratory is not officially NELAP accredited is indicated by a'—' symbol. These are not included in
the scope because NELAP accreditation is either not available or has not been applied for. Additional
certifications may be held/are available for parameters, where NELAP accreditation is not required or applicable.
A full list of certifications is available upon request.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Connie Cook
Project Manager
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 1 of 9

Waypointo
ANALYTICAL
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 ° Fax [phone]
www.waypointanalytical.corn
Certification Summary
Laboratory ID: WP MTN: Waypoint Analytical, LLC., Memphis, TN
State
Program
Lab ID
Expiration Date
Alabama
State Program
40750
02/29/2024
Arkansas
State Program
88-0650
02/07/2024
California
State Program
2904
06/30/2023
Florida
State Program
- NELAP
E871157
06/30/2023
Georgia
State Program
C044
11/14/2025
Georgia
State Program
04015
06/30/2023
Illinois
State Program
- NELAP
200078
10/10/2023
Kentucky
State Program
80215
06/30/2023
Kentucky
State Program
KY90047
12/31/2023
Louisiana
State Program
- NELAP
LA037
12/31/2023
Louisiana
State Program
- NELAP
04015
06/30/2023
Mississippi
State Program
MS
11/14/2025
North Carolina
State Program
47701
07/31/2023
North Carolina
State Program
415
12/31/2023
Pennsylvania
State Program
- NELAP
68-03195
05/31/2024
South Carolina
State Program
84002
06/30/2023
Tennessee
State Program
02027
11/14/2025
Texas
State Program
- NELAP
T104704180
09/30/2023
Virginia
State Program
00106
06/30/2023
Virginia
State Program
- NELAP
460181
09/14/2023
Page 1 of 1 00001/23-116-0077
Page 2 of 9

waypoint 2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 Fax [phone]
ANALYTICAL www.waypointanalytical.com
Sample Summary Table
Report Number: 23-116-0077
Client Project Description: Washington, NC
Lab No Client Sample ID
83191 Washington
Matrix Date Collected
Solids 04/25/2023 09:00
Date Received
04/26/2023
Page 3 of 9

Waypointo
ANALYTICAL
Client: EMA Resources Inc
Project: Washington, NC
Lab Report Number: 23-116-0077
Date: 5/8/2023
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 1 Fax [phone]
www.waypointanalytical.com
CASE NARRATIVE
Metals Analysis Method 6010D
Sample 62824 (Oil Water Separator)
Analyte: Aluminum
QC Batch No: 1-679192/1-678708
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 62824 (Oil Water Separator)
Analyte: Calcium
QC Batch No: 1-679352/1-678708
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 62824 (Oil Water Separator)
Analyte: Iron
QC Batch No: 1-679192/1-678708
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 62824 (Oil Water Separator)
Analyte: Potassium
QC Batch No: 1-679192/1-678708
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 62824 (Oil Water Separator)
Analyte: Magnesium
QC Batch No: 1-679192/1-678708
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 62824 (Oil Water Separator)
Analyte: Selenium
QC Batch No: 1-679192/1-678708
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Sample 62824 (Oil Water Separator)
Analyte: Selenium
QC Batch No: 1-679352/1-678708
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Sample 62824 (Oil Water Separator)
Analyte: Zinc
Page 4 of 9

Waypointo
ANALYTICAL
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 Fax [phone]
www.waypointanalytical.com
QC Batch No: 1-679192/1-678708
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Page 5 of 9

0
Waypoint, 2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 Fax [phone]
ANALYTICAL www.waypointanalytical.com
46245
EMA Resources Inc Project Washington, NC
Mr. Brent Collins Report Date : 05/08/2023
755 Yadkinville Rd Information : Received : 04/26/2023
Mocksville , NC 27028 n �
Connie Cook
Report Number : 23-116-0077
REPOR T OF A NA L YSIS
Project
Manager
Lab No : 83191
Matrix:
Solids
Sample ID : Washington
Sampled:
4/25/2023
9:00
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Method
Moisture
94.3
%
1
05/02/2314:00
JLS
SW-DRYWT
Ammonia Nitrogen
5890
mg/Kg - dry
281
1750
1
04/27/23 13:30
CLP
4500NH3C-2011
Nitrate+Nitrite-N
24.03
mg/Kg - dry
17.5
87.7
1
04/27/23 16:07
ZBD
4500NO3F-2016
Organic N
81650
mg/Kg - dry
280.7
1754
1
04/27/23 12:30
CALCULATION
pH
6.9
s.u.
1
05/03/2316:00
CNB
9045D
Total Solids
5.79
%
0.010
0.010
1
05/04/23 19:37
CJR
2540G-2011
Total Volatile Solids
56.5
%
0.010
0.010
1
05/04/23 19:37
CJR
2540G-2011
Total Kjeldahl Nitrogen
87500
mg/Kg - dry
175
4390
1
04/27/23 12:30
CLP ')M-4500-NH3C-TKP
Phosphorus
18200
mg/Kg - dry
48.4
87.7
1
04/28/23 23:50
JTR
6010D
Aluminum
17900
mg/Kg - dry
81.1
87.7
1
04/28/23 23:50
JTR
6010D
Arsenic
<4.21
mg/Kg - dry
4.21
8.77
1
04/28/23 23:50
JTR
6010D
Cadmium
0.4323
mg/Kg - dry
0.351
1.75
1
04/28/23 23:50
JTR
6010D
Calcium
110000
mg/Kg - dry
679
877
1
04/28/23 23:50
TJS
6010D
Chromium
10.9
mg/Kg - dry
4.14
4.39
1
04/28/23 23:50
JTR
6010D
Copper
151
mg/Kg - dry
5.44
8.77
1
04/28/23 23:50
JTR
6010D
Iron
8280
mg/Kg - dry
149
175
1
04/28/23 23:50
JTR
6010D
Lead
13.8
mg/Kg - dry
3.16
5.26
1
04/28/23 23:50
JTR
6010D
Magnesium
63300
mg/Kg - dry
45.3
87.7
1
04/28/23 23:50
JTR
6010D
Manganese
300
mg/Kg - dry
5.70
8.77
1
04/28/23 23:50
JTR
6010D
Mercury
0.511 J
mg/Kg - dry
0.358
2.96
1
05/03/23 13:32
FDS
7471A
Molybdenum
2.49 J
mg/Kg - dry
2.37
4.39
1
04/28/23 23:50
JTR
6010D
Nickel
9.40
mg/Kg - dry
2.11
4.39
1
04/28/23 23:50
JTR
6010D
Potassium
1610
mg/Kg - dry
108
175
1
04/28/23 23:50
JTR
6010D
Qualifiers/ DF
Dilution Factor
J
Estimated value
Definitions MQL
Method Quantitation Limit
Page 6 of 9

0
Waypoint,
2790 Whitten
Road, Memphis, TN 38133
Main 901.213.2400 0 Fax [phone]
ANALYTICAL
www.waypointanalytical.com
46245
EMA Resources Inc
Project
Washington, NC
Mr. Brent Collins
Report Date : 05/08/2023
755 Yadkinville Rd
Information :
Received : 04/26/2023
Mocksville , NC 27028
Connie Cook
Report Number : 23-116-0077
REPOR T OF A
NA L YSIS
Project Manager
Lab No : 83191
Matrix: Solids
Sample ID : Washington
Sampled: 4/25/2023 9:00
Test
Results
Units
MDL
MQL DF Date / Time By Analytical
Analyzed Method
Selenium
<5.61
mg/Kg - dry
5.61
8.77 1 04/28/23 23:50 TJS 6010D
Sodium
1770
mg/Kg - dry
228
439 1 04/28/23 23:50 JTR 6010D
Zinc
421
mg/Kg - dry
14.2
21.9 1 04/28/23 23:50 JTR 6010D
Sulfur
5740
mg/Kg - dry
90.9
175 1 04/28/23 23:50 JTR 6010D
Sodium Absorption Ratio
0.25
Ratio
0.01
0.01 1 04/28/23 23:50 CALCULATION
Qualifiers/ DF Dilution Factor
Definitions
J Estimated value
Page 7 of 9

(2)
WayPAoint..
NALYTICAL
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 ° Fax [phone]
www.waypointanalytical.com
Shipment Receipt Form
Customer Number: 46245
Customer Name: EMA Resources Inc
Report Number: 23-116-0077
Shipping Method
Fed Ex 0 US Postal 0 Lab 0 Other:
0 UPS 0 Client 0 Courier Thermometer ID: T136
Shipping container/cooler uncompromised?
* Yes
0 No
Number of coolers/boxes received
F
Custody seals intact on shipping container/cooler?
0 Yes
0 No
Not Present
Custody seals intact on sample bottles?
0 Yes
0 No
Not Present
Chain of Custody (COC) present?
Yes
0 No
COC agrees with sample label(s)?
U Yes
0 No
COC properly completed
U Yes
0 No
Samples in proper containers?
U Yes
0 No
Sample containers intact?
Yes
0 No
Sufficient sample volume for indicated test(s)?
Yes
0 No
All samples received within holding time?
Yes
0 No
Cooler temperature in compliance?
Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
Yes
0 No
Water - Sample containers properly preserved
0 Yes
0 No
N/A
Water - VOA vials free of headspace
0 Yes
0 No
N/A
Trip Blanks received with VOAs
0 Yes
0 No
0 N/A
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
0 N/A
F_ High concentration container (48 hr) F Low concentration EnCore samplers (48 hr)
F_ High concentration pre -weighed (methanol -14 d) Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included?
0 Yes
0 No
Comments:
Signature: Makayla Weaver Date & Time: 04/26/2023 11:30:45
Page 8 of 9

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Page 9 of 9

Waypointo
ANALYTICAL
11 /3/2023
EMA Resources Inc
Mr. Brent Collins
755 Yadkinville Rd
Mocksville, NC, 27028
Ref: Analytical Testing
Lab Report Number: 23-299-0005
Client Project Description: Washington
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 1 Fax [phone]
www.waypointanalytical.com
Dear Mr. Brent Collins:
Waypoint Analytical, LLC. received sample(s) on 10/26/2023 for the analyses presented in the following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Where the laboratory was not responsible for the sampling
stage (refer to the chain of custody) results apply to the sample as received.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2021) and NELAC unless otherwise indicated. Any parameter
for which the laboratory is not officially NELAP accredited is indicated by a'—' symbol. These are not included in
the scope because NELAP accreditation is either not available or has not been applied for. Additional
certifications may be held/are available for parameters, where NELAP accreditation is not required or applicable.
A full list of certifications is available upon request.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Connie Cook
Project Manager
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 1 of 9

Waypointo
ANALYTICAL
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 ° Fax [phone]
www.waypointanalytical.corn
Certification Summary
Laboratory ID: WP MTN: Waypoint Analytical, LLC., Memphis, TN
State
Program
Lab ID
Expiration Date
Alabama
State Program
40750
02/29/2024
Arkansas
State Program
88-0650
02/07/2024
California
State Program
2904
06/30/2024
Florida
State Program
- NELAP
E871157
06/30/2024
Georgia
State Program
C044
11/14/2025
Georgia
State Program
04015
06/30/2024
Illinois
State Program
- NELAP
200078
10/31/2024
Kentucky
State Program
80215
06/30/2024
Kentucky
State Program
KY90047
12/31/2023
Louisiana
State Program
- NELAP
LA037
12/31/2023
Louisiana
State Program
- NELAP
04015
06/30/2024
Mississippi
State Program
MS
11/14/2025
North Carolina
State Program
47701
07/31/2024
North Carolina
State Program
415
12/31/2023
Pennsylvania
State Program
- NELAP
68-03195
05/31/2024
South Carolina
State Program
84002
06/30/2024
Tennessee
State Program
02027
11/14/2025
Texas
State Program
- NELAP
T104704180
09/30/2024
Virginia
State Program
00106
06/30/2024
Virginia
State Program
- NELAP
460181
09/14/2024
Page 1 of 1 00001/23-299-0005
Page 2 of 9

waypoint 2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 Fax [phone]
ANALYTICAL www.waypointanalytical.com
Sample Summary Table
Report Number: 23-299-0005
Client Project Description: Washington
Lab No Client Sample ID Matrix Date Collected Date Received
92920 Washington Solids 10/25/2023 10:00 10/26/2023
Page 3 of 9

Waypointo
ANALYTICAL
Client: EMA Resources Inc
Project: Washington
Lab Report Number: 23-299-0005
Date: 11 /2/2023
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 1 Fax [phone]
www.waypointanalytical.com
CASE NARRATIVE
Metals Analysis Method 6010D
Sample 63789 (WWTP Cake)
Analyte: Aluminum
QC Batch No: 1-713991/1-713475
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 63789 (WWTP Cake)
Analyte: Calcium
QC Batch No: 1-714093/1-713475
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 63789 (WWTP Cake)
Analyte: Iron
QC Batch No: L713991/L713475
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 63789 (WWTP Cake)
Analyte: Potassium
QC Batch No: 1-713991/1-713475
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 63789 (WWTP Cake)
Analyte: Magnesium
QC Batch No: 1-713991/1-713475
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 63789 (WWTP Cake)
Analyte: Manganese
QC Batch No: 1-713991/1-713475
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 63789 (WWTP Cake)
Analyte: Phosphorus
QC Batch No: 1-713991/1-713475
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 63789 (WWTP Cake)
Analyte: Lead
Page 4 of 9

Waypointo
ANALYTICAL
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 1 Fax [phone]
www.waypointanalytical.com
QC Batch No: 1-713991/1-713475
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Sample 63789 (WWTP Cake)
Analyte: Sulfur
QC Batch No: 1-713991/1-713475
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 63789 (WWTP Cake)
Analyte: Zinc
QC Batch No: 1-713991/1-713475
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Solids Total Mercury Analysis - CVAA Method 7471A
Sample 63814 (23102407.01A)
Analyte: Mercury
QC Batch No: 1-713736/1-713529
The matrix spike, matrix spike duplicate and the post digestion spike were all outside of the quality control
acceptance ranges. Matrix interference is suspected.
Page 5 of 9

0
Waypoint, 2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 Fax [phone]
ANALYTICAL www.waypointanalytical.com
46245
EMA Resources Inc Project Washington
Mr. Brent Collins Report Date : 11/03/2023
755 Yadkinville Rd Information : Received : 10/26/2023
Mocksville , NC 27028 n �
Connie Cook
Report Number : 23-299-0005
REPOR T OF A NA L YSIS
Project
Manager
Lab No : 92920
Matrix:
Solids
Sample ID : Washington
Sampled:
10/25/2023
10:00
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Method
Moisture
96.9
%
1
10/26/23 16:12
CAH
SW-DRYWT
Ammonia Nitrogen
9520
mg/Kg - dry
516
3230
1
10/30/23 10:21
JPJ
4500NH3C-2011
Nitrate+Nitrite-N
102 )B
mg/Kg - dry
32.3
161
1
11/02/23 15:44
CLP
4500NO3F-2016
Organic N
37900
mg/Kg - dry
12030
1
10/30/23 10:21
DH
CALCULATION
pH
7.2
S.U.
1
10/26/2314:18
ANV
9045D
Total Solids
3.15
%
0.010
0.010
1
10/26/23 16:12
CAH
2540G-2011
Total Volatile Solids
61.3
%
0.010
0.010
1
10/26/23 16:12
CAH
2540G-2011
Total Kjeldahl Nitrogen
47400
mg/Kg - dry
12000
1
11/01/23 09:26
ANH 4500NORGD-2011
Phosphorus
34800
mg/Kg - dry
90.3
161
1
10/28/23 02:00
JTR
6010D
Aluminum
40300
mg/Kg - dry
150
161
1
10/28/23 02:00
JTR
6010D
Arsenic
<8.06
mg/Kg - dry
8.06
16.1
1
10/28/23 02:00
JTR
6010D
Cadmium
<1.61
mg/Kg - dry
1.61
3.23
1
10/28/23 02:00
JTR
6010D
Calcium
26700
mg/Kg - dry
1250
1610
1
10/30/23 14:40
TJS
6010D
Chromium
21.6
mg/Kg - dry
8.06
8.06
1
10/28/23 02:00
JTR
6010D
Copper
294
mg/Kg - dry
9.68
16.1
1
10/28/23 02:00
JTR
6010D
Iron
17100
mg/Kg - dry
276
323
1
10/28/23 02:00
JTR
6010D
Lead
23.6
mg/Kg - dry
6.45
9.68
1
10/28/23 02:00
JTR
6010D
Magnesium
2350
mg/Kg - dry
83.9
161
1
10/28/23 02:00
JTR
6010D
Manganese
697
mg/Kg - dry
11.3
16.1
1
10/28/23 02:00
JTR
6010D
Mercury
1.081
mg/Kg - dry
0.655
5.42
1
10/27/23 11:37
FDS
7471A
Molybdenum
6.351
mg/Kg - dry
4.84
8.06
1
10/28/23 02:00
JTR
6010D
Nickel
16.4
mg/Kg - dry
4.84
8.06
1
10/28/23 02:00
JTR
6010D
Potassium
2210
mg/Kg - dry
200
323
1
10/28/23 02:00
JTR
6010D
Qualifiers/ B
Analyte detected in blank
DF
Dilution Factor
Definitions J
Estimated value
MQL
Method Quantitation
Limit
Page 6 of 9

0
Waypoint,
2790 Whitten
Road, Memphis, TN 38133
Main 901.213.2400 0 Fax [phone]
ANALYTICAL
www.waypointanalytical.com
46245
EMA Resources Inc
Project
Washington
Mr. Brent Collins
Report Date : 11/03/2023
755 Yadkinville Rd
Information :
Received : 10/26/2023
Mocksville , NC 27028
Connie Cook
Report Number : 23-299-0005
REPOR T OF A NA L YSIS
Project Manager
Lab No : 92920
Matrix: Solids
Sample ID : Washington
Sampled: 10/25/2023 10:00
Test
Results
Units
MDL
MQL DF Date / Time By Analytical
Analyzed Method
Selenium
<11.3
mg/Kg - dry
11.3
16.1 1 10/28/23 02:00 JTR 6010D
Sodium
3290
mg/Kg - dry
419
806 1 10/28/23 02:00 JTR 6010D
Zinc
810
mg/Kg - dry
27.4
40.3 1 10/28/23 02:00 JTR 6010D
Sulfur
11200
mg/Kg - dry
168
323 1 10/28/23 02:00 JTR 6010D
Sodium Absorption Ratio
0.91
Ratio
0.01
0.01 1 10/28/23 02:00 CALCULATION
Qualifiers/ B Analyte detected in blank
Definitions
DF Dilution Factor
Page 7 of 9

(2)
WayPAoint..
NALYTICAL
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 ° Fax [phone]
www.waypointanalytical.com
Shipment Receipt Form
Customer Number: 46245
Customer Name: EMA Resources Inc
Report Number: 23-299-0005
Shipping Method
Fed Ex 0 US Postal 0 Lab 0 Other:
0 UPS 0 Client 0 Courier Thermometer ID: t100
Shipping container/cooler uncompromised?
* Yes
0 No
Number of coolers/boxes received
F
Custody seals intact on shipping container/cooler?
0 Yes
0 No
Not Present
Custody seals intact on sample bottles?
0 Yes
0 No
Not Present
Chain of Custody (COC) present?
Yes
0 No
COC agrees with sample label(s)?
U Yes
0 No
COC properly completed
U Yes
0 No
Samples in proper containers?
U Yes
0 No
Sample containers intact?
Yes
0 No
Sufficient sample volume for indicated test(s)?
Yes
0 No
All samples received within holding time?
Yes
0 No
Cooler temperature in compliance?
Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
Yes
0 No
Water - Sample containers properly preserved
0 Yes
0 No
0 N/A
Water - VOA vials free of headspace
0 Yes
0 No
N/A
Trip Blanks received with VOAs
0 Yes
0 No
0 N/A
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
0 N/A
F_ High concentration container (48 hr) F Low concentration EnCore samplers (48 hr)
F_ High concentration pre -weighed (methanol -14 d) Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included?
0 Yes
0 No
Comments:
Signature: mber Smith Date & Time: I10/26/2023 08:47:09
Page 8 of 9

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Page 9 of 9

Waypointo
ANALYTICAL
11 /17/2023
EMA Resources Inc
Mr. Brent Collins
755 Yadkinville Rd
Mocksville, NC, 27028
Ref: Analytical Testing
Lab Report Number: 23-313-0139
Client Project Description: Washington, NC
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 1 Fax [phone]
www.waypointanalytical.com
Dear Mr. Brent Collins:
Waypoint Analytical, LLC. received sample(s) on 11/9/2023 for the analyses presented in the following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Where the laboratory was not responsible for the sampling
stage (refer to the chain of custody) results apply to the sample as received.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2021) and NELAC unless otherwise indicated. Any parameter
for which the laboratory is not officially NELAP accredited is indicated by a'—' symbol. These are not included in
the scope because NELAP accreditation is either not available or has not been applied for. Additional
certifications may be held/are available for parameters, where NELAP accreditation is not required or applicable.
A full list of certifications is available upon request.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Connie Cook
Project Manager
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 1 of 8

Waypointo
ANALYTICAL
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 ° Fax [phone]
www.waypointanalytical.corn
Certification Summary
Laboratory ID: WP MTN: Waypoint Analytical, LLC., Memphis, TN
State
Program
Lab ID
Expiration Date
Alabama
State Program
40750
02/29/2024
Arkansas
State Program
88-0650
02/07/2024
California
State Program
2904
06/30/2024
Florida
State Program
- NELAP
E871157
06/30/2024
Georgia
State Program
C044
11/14/2025
Georgia
State Program
04015
06/30/2024
Illinois
State Program
- NELAP
200078
10/31/2024
Kentucky
State Program
80215
06/30/2024
Kentucky
State Program
KY90047
12/31/2023
Louisiana
State Program
- NELAP
LA037
12/31/2023
Louisiana
State Program
- NELAP
04015
06/30/2024
Mississippi
State Program
MS
11/14/2025
North Carolina
State Program
47701
07/31/2024
North Carolina
State Program
415
12/31/2023
Pennsylvania
State Program
- NELAP
68-03195
05/31/2024
South Carolina
State Program
84002
06/30/2024
Tennessee
State Program
02027
11/14/2025
Texas
State Program
- NELAP
T104704180
09/30/2024
Virginia
State Program
00106
06/30/2024
Virginia
State Program
- NELAP
460181
09/14/2024
Page 1 of 1 00001/23-313-0139
Page 2 of 8

waypoint 2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 Fax [phone]
ANALYTICAL www.waypointanalytical.com
Sample Summary Table
Report Number: 23-313-0139
Client Project Description: Washington, NC
Lab No Client Sample ID
89359 Washington
Matrix Date Collected
Solids 11/08/2023 08:00
Date Received
11/09/2023
Page 3 of 8

Waypointo
ANALYTICAL
Client: EMA Resources Inc
Project: Washington, NC
Lab Report Number: 23-313-0139
Date: 11 /17/2023
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 Fax [phone]
www.waypointanalytical.com
CASE NARRATIVE
Metals Analysis Method 6010D
Sample 63921 (4)
Analyte: Aluminum
QC Batch No: L717129/L716429
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 63921 (4)
Analyte: Manganese
QC Batch No: 1-717129/1-716429
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Page 4 of 8

0
Waypoint, 2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 Fax [phone]
ANALYTICAL www.waypointanalytical.com
46245
EMA Resources Inc Project Washington, NC
Mr. Brent Collins Report Date : 11/17/2023
755 Yadkinville Rd Information : Received : 11/09/2023
Mocksville , NC 27028 n �
Connie Cook
Report Number : 23-313-0139
REPOR T OF A NA L YSIS
Project
Manager
Lab No : 89359
Matrix:
Solids
Sample ID : Washington
Sampled:
11/8/2023
8:00
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Method
Moisture
97.07
%
0.010
0.010
1
11/10/23 16:14
CAH
SW-DRYWT
Ammonia Nitrogen
9730
mg/Kg - dry
546
3410
1
11/16/23 10:48
JPJ
4500NH3C-2011
Nitrate+Nitrite-N
123 3B
mg/Kg - dry
34.1
171
1
11/14/23 14:42
CLP
4500NO3F-2016
Organic N
58190
mg/Kg - dry
546.1
3413
1
11/16/23 06:46
DH
CALCULATION
pH
7.3
S.U.
1
11/16/2316:40
CNB
9045D
Total Solids
2.93
%
0.010
0.010
1
11/10/23 16:14
CAH
2540G-2011
Total Volatile Solids
60.3
%
0.010
0.010
1
11/10/23 16:14
CAH
2540G-2011
Total Kjeldahl Nitrogen
67900
mg/Kg - dry
341
8530
1
11/16/23 06:46
JPJ ')M-4500-NH3C-TKP
Phosphorus
36200
mg/Kg - dry
95.6
171
1
11/14/23 19:12
BKN
6010D
Aluminum
42700
mg/Kg - dry
159
171
1
11/14/23 19:12
BKN
6010D
Arsenic
<8.53
mg/Kg - dry
8.53
17.1
1
11/14/23 19:12
BKN
6010D
Cadmium
<1.71
mg/Kg - dry
1.71
3.41
1
11/14/23 19:12
BKN
6010D
Calcium
28700
mg/Kg - dry
1320
1710
1
11/14/23 19:12
BKN
6010D
Chromium
21.8
mg/Kg - dry
8.53
8.53
1
11/14/23 19:12
BKN
6010D
Copper
305
mg/Kg - dry
10.2
17.1
1
11/14/23 19:12
BKN
6010D
Iron
17200
mg/Kg - dry
292
341
1
11/14/23 19:12
BKN
6010D
Lead
30.2
mg/Kg - dry
6.83
10.2
1
11/14/23 19:12
BKN
6010D
Magnesium
2480
mg/Kg - dry
88.7
171
1
11/14/23 19:12
BKN
6010D
Manganese
727
mg/Kg - dry
11.9
17.1
1
11/14/23 19:12
BKN
6010D
Mercury
0.7061
mg/Kg - dry
0.693
5.73
1
11/13/23 11:16
FDS
7471A
Molybdenum
7.241
mg/Kg - dry
5.12
8.53
1
11/14/23 19:12
BKN
6010D
Nickel
16.3
mg/Kg - dry
5.12
8.53
1
11/14/23 19:12
BKN
6010D
Potassium
2350
mg/Kg - dry
212
341
1
11/14/23 19:12
BKN
6010D
Qualifiers/ B
Analyte detected in blank
DF
Dilution Factor
Definitions J
Estimated value
MQL
Method Quantitation
Limit
Page 5 of 8

0
Waypoint,
2790 Whitten
Road, Memphis, TN 38133
Main 901.213.2400 0 Fax [phone]
ANALYTICAL
www.waypointanalytical.com
46245
EMA Resources Inc
Project
Washington, NC
Mr. Brent Collins
Report Date : 11/17/2023
755 Yadkinville Rd
Information :
Received : 11/09/2023
Mocksville , NC 27028
Connie Cook
Report Number : 23-313-0139
REPOR T OF A
NA L YSIS
Project Manager
Lab No : 89359
Matrix: Solids
Sample ID : Washington
Sampled: 11/8/2023 8:00
Test
Results
Units
MDL
MQL DF Date / Time By Analytical
Analyzed Method
Selenium
<11.9
mg/Kg - dry
11.9
17.1 1 11/14/23 19:12 BKN 6010D
Sodium
3450
mg/Kg - dry
444
853 1 11/14/23 19:12 BKN 6010D
Zinc
843
mg/Kg - dry
29.0
42.7 1 11/14/23 19:12 BKN 6010D
Sulfur
12100
mg/Kg - dry
177
341 1 11/14/23 19:12 BKN 6010D
Sodium Absorption Ratio
0.89
Ratio
0.01
0.01 1 11/14/23 19:12 CALCULATION
Qualifiers/ B Analyte detected in blank
Definitions
DF Dilution Factor
Page 6 of 8

(2)
WayPAoint..
NALYTICAL
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 ° Fax [phone]
www.waypointanalytical.com
Shipment Receipt Form
Customer Number: 46245
Customer Name: EMA Resources Inc
Report Number: 23-313-0139
Shipping Method
Fed Ex 0 US Postal 0 Lab 0 Other:
0 UPS 0 Client 0 Courier Thermometer ID: T136
Shipping container/cooler uncompromised?
* Yes
0 No
Number of coolers/boxes received
F
Custody seals intact on shipping container/cooler?
0 Yes
0 No
Not Present
Custody seals intact on sample bottles?
0 Yes
0 No
Not Present
Chain of Custody (COC) present?
Yes
0 No
COC agrees with sample label(s)?
U Yes
0 No
COC properly completed
U Yes
0 No
Samples in proper containers?
U Yes
0 No
Sample containers intact?
Yes
0 No
Sufficient sample volume for indicated test(s)?
Yes
0 No
All samples received within holding time?
Yes
0 No
Cooler temperature in compliance?
Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
Yes
0 No
Water - Sample containers properly preserved
0 Yes
0 No
0 N/A
Water - VOA vials free of headspace
0 Yes
0 No
N/A
Trip Blanks received with VOAs
0 Yes
0 No
0 N/A
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
0 N/A
F_ High concentration container (48 hr) F Low concentration EnCore samplers (48 hr)
F_ High concentration pre -weighed (methanol -14 d) Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included?
0 Yes
0 No
Comments:
Signature: mber Smith Date & Time: 11/09/2023 16:38:15
Page 7 of 8

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Page 8 of 8

PaceAnalytical
ANALYTICAL REPORT
May 01, 2023
EMA Resources
Sample Delivery Group
Samples Received:
Project Number:
Description:
Report To:
L1608049
04/21/2023
Sludge
Mr. Brent Collins
755 Yadkinville Road
Mocksville, NC 27028
Entire Report Reviewed By
zezr�6""
Reagan Johnson
Project Manager
Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be
reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pace
Analytical National is performed per guidance provided in laboratory standard operating procedures ENV-SOP-MTJL-0067 and ,
ENV-SOP-MTJL-0068. Where sampling conducted by the customer, results relate to the accuracy of the information provided,
and as the samples are received.
I
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1608049 05/01/23 11:08 1 of 21

TABLE OF CONTENTS
Cp: Cover Page
Tc: Table of Contents
Ss: Sample Summary
Cn: Case Narrative
Sr: Sample Results
WASHINGTON L1608049-01
Qc: Quality Control Summary
Wet Chemistry by Method 9012 B
Wet Chemistry by Method 9034-9030B
Wet Chemistry by Method 9045D
Wet Chemistry by Method D93/1010A
Mercury by Method 7470A
Metals (ICP) by Method 6010D
Volatile Organic Compounds (GC/MS) by Method 8260D
Chlorinated Acid Herbicides (GC) by Method 8151A
Pesticides (GC) by Method 80818
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
GI: Glossary of Terms
Al: Accreditations & Locations
Sc: Sample Chain of Custody
1
2
3
4
5
5
7
7
8
9
10
11
12
13
15
16
17
19
20
21
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1608049 05/01/23 11:08 2 of 21

SAMPLE SUMMARY
Collected by
Collected
date/time
Received date/time
WASHINGTON L1608049-01 Waste
Brent Collins
04/20/2308:00
04/21/2309:15
Method
Batch
Dilution Preparation
Analysis
Analyst
Location
date/time
date/time
Preparation by Method 1311
WG2047246
1 04/24/23 08:44
04/24/23
08:44
WC
Mt.
Juliet, TN
Preparation by Method 1311
WG2047434
1 04/24/2314:46
04/24/2314:46
WC
Mt.
Juliet, TN
Wet Chemistry by Method 9012 B
WG2047833
1 04/25/2314:27
04/25/23
22:03
UNP
Mt.
Juliet, TN
Wet Chemistry by Method 9034-9030B
WG2047053
1 04/26/2319:26
04/27/2314:00
RLS
Mt.
Juliet, TN
Wet Chemistry by Method 9045D
WG2047035
1 04/26/2318:00
04/26/23
20:12
KAD
Mt.
Juliet, TN
Wet Chemistry by Method D93/1010A
WG2049464
1 04/27/23 02:49
04/27/23
02:49
CRB
Mt.
Juliet, TN
Mercury by Method 7470A
WG2049230
1 04/26/2315:44
04/27/23
21:02
NDL
Mt.
Juliet, TN
Metals (ICP) by Method 6010D
WG2048451
1 04/26/23 01:07
04/27/23
00:08
ABL
Mt.
Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260D
WG2048161
1 04/26/23 03:54
04/26/23
03:54
JAH
Mt.
Juliet, TN
Chlorinated Acid Herbicides (GC) by Method 8151A
WG2048803
1 04/26/2314:50
04/28/23
05:49
JMB
Mt.
Juliet, TN
Pesticides (GC) by Method 8081B
WG2049577
1 04/27/2316:27
04/28/23
00:04
HMH
Mt.
Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
WG2050468
1 04/28/2312:36
04/29/23
04:20
AGW
Mt.
Juliet, TN
ACCOUNT:
PROJECT:
SDG:
DATE/TIME:
PAGE:
EMA Resources
L1608049
05/01/23 11:08
3 of 21
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CASE NARRATIVE
All sample aliquots were received at the correct temperature, in the proper containers, with the FP1
appropriate preservatives, and within method specified holding times, unless qualified or notated within
the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples FTChave been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control
are within established criteria except where addressed in this case narrative, a non-conformance form
or properly qualified within the sample results. By my digital signature below, I affirm to the best of my FSS
knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the
quality of the data have been identified by the laboratory, and no information or data have been
knowingly withheld that would affect the quality of the data.
Fr]
.� FQc
�GI
Reagan Johnson rAl
Project Manager
LE
Project Narrative
All Reactive Cyanide results reported in the attached report were determined as totals using method 9012 B.
All Reactive Sulfide results reported in the attached report were determined as totals using method 9034-9030B.
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1608049 05/01/23 11:08 4 of 21

■
SAMPLE RESULTS - 01
L1608049
WASHINGTON
Collected date/time: 04/20/23 08:00
Preparation by Method 1311
Result
Analyte
TCLP Extraction
TCLP ZHE Extraction -
Fluid 1
Initial pH 7.04
Final pH 5.05
Wet Chemistry by Method 9012 B
Qualifier Prep Batch
date / time
4/24/2023 2:46:51 PM WG2047434
4/24/2023 8:44:48 AM WG2047246
4/24/2023 2:46:51 PM WG2047434
4/24/2023 2:46:51 PM WG2047434
4/24/2023 2:46:51 PM WG2047434
Result Qualifier
RDL
Analyte mg/kg
mg/kg
Reactive Cyanide ND
0.250
Wet Chemistry by Method 9034-9030B
Result Qualifier
RDL
Analyte mg/kg
mg/kg
Reactive Sulfide 87.5
75.0
Wet Chemistry by Method 9045D
Dilution Analysis Batch
date / time
1 04/25/2023 22:03 WG2047833
Dilution Analysis
date / time
1 04/27/202314:00
Result Qualifier
Dilution Analysis
Batch
Analyte su
date / time
Corrosivity by pH 6.99 T8
1 04/26/2023 20:12
WG2047035
Sample Narrative:
L1608049-01 WG2047035: 6.99 at 21.3C
Wet Chemistry by Method D93/1010A
Result Qualifier
Dilution Analysis
Batch
Analyte Deg. F
date / time
Ignitability DNI at 170
1 04/27/2023 02:49
WG2049464
Mercury by Method 7470A
Batch
WG2047053
Result Qualifier RDL Limit Dilution Analysis
Analyte mg/I mg/I mg/I date/time
Mercury ND 0.0100 0.20 1 04/27/2023 21:02
Metals (ICP) by Method 6010D
Result
Qualifier RDL
Limit
Analyte
mg/I
mg/I
mg/I
Arsenic
ND
0.100
5
Barium
ND
0.100
100
Cadmium
ND
0.100
1
Chromium
ND
0.100
5
Lead
ND
0.100
5
Selenium
ND
0.100
1
Silver
ND
0.100
5
Volatile Organic Compounds (GC/MS) by Method 8260D
Batch
WG2049230
Dilution Analysis
Batch
date / time
1 04/27/2023 00:08
WG2048451
1 04/27/2023 00:08
WG2048451
1 04/27/2023 00:08
WG2048451
1 04/27/2023 00:08
WG2048451
1 04/27/2023 00:08
WG2048451
1 04/27/2023 00:08
WG2048451
1 04/27/2023 00:08
WG2048451
Result
Qualifier RDL
Limit
Dilution Analysis
Batch
Analyte
mg/I
mg/I
mg/I
date/time
Benzene
ND
0.0500
0.50
1 04/26/2023 03:54
WG2048161
Carbon tetrachloride
ND
0.0500
0.50
1 04/26/2023 03:54
WG2048161
Chlorobenzene
0.756
0.0500
100
1 04/26/2023 03:54
WG2048161
Chloroform
ND
0.250
6
1 04/26/2023 03:54
WG2048161
ACCOUNT:
PROJECT:
SDG:
DATE/TIME: PAGE:
EMA Resources
L1608049
05/01/23 11:08 5 of 21
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WASHINGTON SAMPLE RESULTS - 01
Collected date/time: 04/20/23 08:00 L1608049
Volatile Organic Compounds (GC/MS) by Method 8260D
Result
Qualifier RDL
Limit
Dilution Analysis
Analyte
mg/I
mg/I
mg/I
date / time
1,2-Dichloroethane
ND
0.0500
0.50
1 04/26/2023 03:54
1,1-Dichloroethene
ND
0.0500
0.70
1 04/26/2023 03:54
2-Butanone (MEK)
ND
0.500
200
1 04/26/2023 03:54
Tetrachloroethene
ND
0.0500
0.70
1 04/26/2023 03:54
Trichloroethene
ND
0.0500
0.50
1 04/26/2023 03:54
Vinyl chloride
ND
0.0500
0.20
1 04/26/2023 03:54
(S) Toluene-d8
100
80.0-120
0412612023 03:54
(S) 4-Bromof/uorobenzene
94.6
77.0-126
0412612023 03:54
(S)1,2-Dichloroethane-d4
98.1
70.0-130
0412612023 03:54
Chlorinated Acid Herbicides (GC) by Method 8151A
Result Qualifier RDL
Analyte mg/I mg/I
2,4,5-TP (Silvex) ND 0.00200
2,4-D ND 0.00200
(S)2,4-Dichloropheny/Acetic Acid 92.6 14.0-158
Pesticides (GC) by Method 8081B
Batch
WG2048161
WG2048161
WG2048161
WG2048161
WG2048161
WG2048161
WG2048161
WG2048161
WG2048161
Limit Dilution Analysis Batch
mg/I date / time
1 1 04/28/2023 05:49 WG2048803
10 1 04/28/2023 05:49 WG2048803
041281202305.49 WG2048803
Result
Qualifier RDL
Limit
Dilution Analysis
Analyte
mg/I
mg/I
mg/I
date / time
Chlordane
ND
0.00500
0.03
1 04/28/2023 00:04
Endrin
ND
0.00500
0.02
1 04/28/2023 00:04
Heptachlor
ND
0.00500
0.0080
1 04/28/2023 00:04
Heptachlor epoxide
ND
0.00500
0.0080
1 04/28/2023 00:04
Lindane
ND
0.00500
0.40
1 04/28/2023 00:04
Methoxychlor
ND
0.00500
10
1 04/28/2023 00:04
Toxaphene
ND
0.0100
0.50
1 04/28/2023 00:04
(S) Decachlorobipheny/
86.2
10.0-128
0412812023 00:04
(S) Tetrach/oro-m-xylene
86.0
10.0-127
0412812023 00:04
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
Result Qualifier
Analyte mg/I
1,4-Dichlorobenzene
2,4-Dinitrotoluene
Hexachlorobenzene
Hexachloro-1,3-butadiene
Hexachloroethane
Nitrobenzene
Pyridine
3&4-Methyl Phenol
2-Methylphenol
Pentachlorophenol
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
(S) 2-Fluorophenol
(S) Phenol-d5
(S) Nitrobenzene-d5
(S) 2-F/uorobiphenyl
(S) 2,4,6-Tribromophenol
(S) p-Terphenyl-d14
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
26.2
18.8
71.6
56.9
58.5
70.3
RDL
mg/I
0.100
0.100
0.100
0.100
0.100
0.100
0.100
0.100
0.100
0.100
0.100
0.100
10.0-120
10.0-120
10.0-127
10.0-130
10.0-155
10.0-128
Limit
mg/I
7.50
0.13
0.13
0.50
3
2
5
400
200
100
400
2
Dilution Analysis
date / time
1 04/29/2023 04:20
1 04/29/2023 04:20
1 04/29/2023 04:20
1 04/29/2023 04:20
1 04/29/2023 04:20
1 04/29/2023 04:20
1 04/29/2023 04:20
1 04/29/2023 04:20
1 04/29/2023 04:20
1 04/29/2023 04:20
1 04/29/2023 04:20
1 04/29/2023 04:20
0412912023 04:20
0412912023 04:20
0412912023 04:20
0412912023 04:20
0412912023 04:20
0412912023 04:20
Batch
WG2049577
WG2049577
WG2049577
WG2049577
WG2049577
WG2049577
WG2049577
WG2049577
WG2049577
Batch
WG2050468
WG2050468
WG2050468
WG2050468
WG2050468
WG2050468
WG2050468
WG2050468
WG2050468
WG2050468
WG2050468
WG2050468
WG2050468
WG2050468
WG2050468
WG2050468
WG2050468
WG2050468
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ACCOUNT: PROJECT: SDG:
EMA Resources L1608049
DATE/TIME: PAGE:
05/01/23 11:08 6 of 21

WG2047833
Wet Chemistry by Method 9012 B
Method Blank (MB)
(MB) R3917494-1 04/25/23 21:39
MB Result
Analyte mg/kg
Reactive Cyanide U
MB Qualifier MB MDL MB RDL
mg/kg mg/kg
0.0390 0.250
Laboratory Control Sample (LCS)
QUALITY CONTROL SUMMARY
L1608049-01
(LCS) R3917494-2 04/25/23 21:40
Spike Amount LCS Result LCS Rec. Rec. Limits
Analyte mg/kg mg/kg % %
Reactive Cyanide 2.50 2.50 100 85.0-115
LCS Qualifier
— I
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ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1608049 05/01/23 11:08 7 of 21

WG2047053
Wet Chemistry by Method 9034-9030B
Method Blank (MB)
(MB) R3918211-1 04/27/2314:00
MB Result
Analyte mg/kg
Reactive Sulfide U
MB Qualifier MB MDL MB RDL
mg/kg mg/kg
30.0 75.0
Laboratory Control Sample (LCS)
QUALITY CONTROL SUMMARY
L1608049-01
(LCS) R3918211-2 04/27/2314:00
Spike Amount LCS Result LCS Rec. Rec. Limits
Analyte mg/kg mg/kg % %
Reactive Sulfide 100 76.1 76.1 53.8-124
LCS Qualifier
L1608O64-04 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1608064-04 04/27/2314:00 • (MS) R3918211-3 04/27/2314:00 • (MSD) R3918211-4 04/27/2314:00
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD
Analyte mg/kg mg/kg mg/kg mg/kg % % % %
Reactive Sulfide 100 ND ND ND 63.0 60.7 1 10.0-136 0.000
RPD Limits
20
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ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1608049 05/01/23 11:08 8 of 21

WG2047035 QUALITY CONTROL SUMMARY
Wet Chemistry by Method 9045D L1608049-01
Laboratory Control Sample (LCS)
(LCS) R3917784-1 04/26/23 20:12
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte su su % %
Corrosivity by pH 10.0 10.0 100 99.0-101
Sample Narrative:
LCS:10.01 at19AC
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1608049 05/01/23 11:08 9 of 21
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WG2049464 QUALITY CONTROL SUMMARY
Wet Chemistry by Method D93/1010A L1608049-01
L16O6891-03 Original Sample (OS) • Duplicate (DUP)
(OS) L1606891-03 04/27/23 02:49 • (DUP) R3917840-3 04/27/23 02:49
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte Deg. F Deg. F % %
Ignitability DNIat170 DNIat170 1 0.000 10
L1607975-08 Original Sample (OS) • Duplicate (DUP)
(OS) L1607975-08 04/27/23 02:49 • (DUP) R3917840-4 04/27/23 02:49
Original Result DUP Result Dilution DUP RPD
Analyte Deg. F Deg. F %
Ignitability DNIat170 DNIat170 1 0.000
DUP Qualifier DUP RPD
Limits
10
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3917840-1 04/27/23 02:49 • (LCSD) R3917840-2 04/27/23 02:49
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte Deg. F Deg. F Deg. F % % % % %
Ignitability 126 125 129 98.9 102 95.6-104 3.16 10
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1608049 05/01/23 11:08 10 of 21
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WG2049230
Mercury by Method 7470A
Method Blank (MB)
(MB) R3918458-1 04/27/23 20:21
MB Result
Analyte mg/1
Mercury U
MB Qualifier MB MDL MB RDL
mg/I mg/1
0.00333 0.0100
Laboratory Control Sample (LCS)
(LCS) R3918458-2 04/27/23 20:23
Spike Amount LCS Result LCS Rec.
Analyte mg/1 mg/1 %
Mercury 0.0300 0.0312 104
QUALITY CONTROL SUMMARY
L1608049-01
Rec. Limits LCS Qualifier
80.0-120
L1607975-06 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1607975-06 04/27/23 20:25 • (MS) R3918458-3 04/27/23 20:32 • (MSD) R3918458-4 04/27/23 20:34
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD
Analyte mg/1 mg/1 mg/I mg/1 % % % %
Mercury 0.0300 ND 0.0324 0.0305 108 102 1 75.0-125 5.74
RPD Limits
20
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ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1608049 05/01/23 11:08 11 of 21

WG2048451 QUALITY CONTROL SUMMARY
Metals (ICP) by Method 6010D L1608049-01
Method Blank (MB)
(MB) R3917857-1 04/26/23 23:16
MB Result
Analyte mg/I
MB Qualifier MB MDL
mg/I
MB RDL
mg/I
Arsenic 0.0518
J 0.0333
0.100
Barium U
0.0333
0.100
Cadmium U
0.0333
0.100
Chromium U
0.0333
0.100
Lead U
0.0333
0.100
Selenium U
0.0333
0.100
Silver U
0.0333
0.100
Laboratory Control Sample (LCS)
(LCS) R3917857-2 04/26/23 23:19
Spike Amount
LCS Result
LCS Rec.
Analyte mg/I
mg/I
%
Arsenic 10.0
10.2
102
Barium 10.0
10.2
102
Cadmium 10.0
10.2
102
Chromium 10.0
9.78
97.8
Lead 10.0
10.1
101
Selenium 10.0
10.8
108
Silver 2.00
2.02
101
Rec. Limits LCS Qualifier
°/
80.0-120
80.0-120
80.0-120
80.0-120
80.0-120
80.0-120
L1607968-02 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1607968-02 04/26/23 23:22 • (MS) R3917857-4 04/26/23 23:27 • (MSD) R3917857-5 04/26/23 23:30
Spike Amount
Original Result
MS Result
MSD Result
MS Rec.
MSD Rec.
Analyte
mg/I
mg/I
mg/I
mg/I
%
%
Arsenic
10.0
ND
10.3
10.4
103
104
Barium
10.0
0.171
10.5
10.6
103
104
Cadmium
10.0
ND
10.2
10.4
102
104
Chromium
10.0
ND
9.91
10.0
99.1
100
Lead
10.0
ND
10.3
10.4
102
103
Selenium
10.0
ND
11.0
10.9
110
109
Silver
2.00
ND
2.05
2.06
102
103
Dilution Rec. Limits
MS Qualifier MSD Qualifier RPD
1 75.0-125
1.67
1 75.0-125
1.03
1 75.0-125
1.36
1 75.0-125
1.28
1 75.0-125
1.08
1 75.0-125
0.222
1 75.0-125
0.736
RPD Limits
20
20
20
20
20
20
20
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ACCOUNT:
EMA Resources
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SDG: DATE/TIME:
L1608049 05/01/23 11:08
PAGE:
12 of 21

WG2048161
Volatile Organic Compounds (GC/MS) by Method 8260D
Method Blank (MB)
(MB) R3917909-2 04/25/23 20:56
MB Result MB Qualifier
A-hh- -,/I
Carbon tetrachloride
U
Chlorobenzene
U
Chloroform
0.216 J
1,2-Dichloroethane
U
1,1-Dichloroethene
U
2-Butanone (MEK)
0.425 J
Tetrachloroethene
U
Trichloroethene
U
Vinyl chloride
U
(S) Toluene-d8
104
(S) 4-Bromof/uorobenzene
102
(S)1,2-Dichloroethane-d4
95.5
Laboratory Control Sample (LCS)
(LCS) R3917909-1 04/25/23 19:19
Spike Amount
LCS Result
Analyte
mg/I
mg/I
Benzene
0.250
0.251
Carbon tetrachloride
0.250
0.202
Chlorobenzene
0.250
0.211
Chloroform
0.250
0.223
1,2-Dichloroethane
0.250
0.221
1,1-Dichloroethene
0.250
0.239
2-Butanone (MEK)
1.25
1.11
Tetrachloroethene
0.250
0.203
Trichloroethene
0.250
0.220
Vinyl chloride
0.250
0.221
(S) Toluene-d8
(S) 4-Bromofluorobenzene
(S)1,2-Dichloroethane-d4
MB MDL
mg/I
0.0167
0.0167
0.0167
0.0833
0.0167
0.0167
0.167
0.0167
0.0167
0.0167
LCS Rec.
100
80.8
84.4
89.2
88.4
95.6
88.8
81.2
88.0
88.4
100
102
97.6
QUALITY CONTROL SUMMARY
L1608049-01
MB RDL
mg/I
0.0500
0.0500
0.0500
0.250
0.0500
0.0500
0.500
0.0500
0.0500
0.0500
80.0-120
77.0-126
70.0-130
Rec. Limits LCS Qualifier
70.0-123
68.0-126
80.0-121
73.0-120
70.0-128
71.0-124
44.0-160
72.0-132
78.0-124
67.0-131
80.0-120
77.0-126
70.0-130
FP1
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ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1608049 05/01/23 11:08 13 of 21

WG2048161 QUALITY CONTROL SUMMARY
Volatile Organic Compounds (GC/MS) by Method 8260D L1608049-01
L16O7401-06 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1607401-06 04/25/23 22:41 • (MS) R3917909-3 04/26/23 05:19 • (MSD) R3917909-4 04/26/23 05:40
Spike Amount
Original Result
MS Result
MSD Result
MS Rec.
MSD Rec.
Analyte
mg/I
mg/I
mg/I
mg/I
%
%
Benzene
0.250
ND
0.259
0.263
104
105
Carbon tetrachloride
0.250
ND
0.235
0.239
94.0
95.6
Chlorobenzene
0.250
0.747
0.955
0.976
83.2
91.6
Chloroform
0.250
ND
ND
0.254
97.2
102
1,2-Dichloroethane
0.250
ND
0.229
0.226
91.6
90.4
1,1-Dichloroethene
0.250
ND
0.272
0.275
109
110
2-Butanone (MEK)
1.25
ND
1.13
1.07
90.4
85.6
Tetrachloroethene
0.250
ND
0.580
0.246
232
98.4
Trichloroethene
0.250
ND
0.258
0.245
103
98.0
Vinyl chloride
0.250
ND
0.265
0.260
106
104
(S Toluene-d8
102
99.2
(S) 4-Bromof/uorobenzene
102
99.7
(S)1,2-Dichloroethane-d4
94.6
99.6
Dilution Rec. Limits MS Qualifier
1 17.0-158
1 23.0-159
1 33.0-152
1 29.0-154
1 29.0-151
1 11.0-160
1 10.0-160
1 10.0-160
1 10.0-160
1 10.0-160
80.0-120
77.0-126
70.0-130
J5
MSD Qualifier RPD
RPD Limits
1.53
27
1.69
28
2.18
27
4.43
28
1.32
27
1.10
29
5.45
32
J3 80.9
27
5.17
25
1.90
27
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ACCOUNT: PROJECT:
EMA Resources
SDG:
L1608049
DATE/TIME:
05/01/23 11:08
PAGE:
14 of 21

WG2048803
Chlorinated Acid Herbicides (GC) by Method 8151A
Method Blank (MB)
(MB) R3918819-1 04/28/23 03:25
MB Result
Analyte mg/I
2,4,5-TP (Silvex) U
2,4-D U
(S)2,4-Dichloropheny/Acetic 70.4
Acid
MB Qualifier MB MDL
mg/I
0.000667
0.000667
Laboratory Control Sample (LCS)
QUALITY CONTROL SUMMARY
L1608049-01
MB RDL
Mg/1
0.00200
0.00200
14.0-158
(LCS) R3918819-2 04/28/23 03:36
Spike Amount
LCS Result
LCS Rec.
Rec. Limits LCS Qualifier
Analyte mg/1
mg/1
%
%
2,4,5-TP (Silvex) 0.0500
0.0361
72.2
50.0-125
2,4-D 0.0500
0.0365
73.0
50.0-120
(S) 2,4-Dich/oropheny/Acetic
88_8
14.0-158
Acid
L1607401-12 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1607401-12 04/28/23 04:20 • (MS) R3918819-3 04/28/23 04:31 • (MSD) R3918819-4 04/28/23 04:42
Spike Amount
Original Result
MS Result
MSD Result
MS Rec.
MSD Rec.
Analyte
mg/I
mg/1
mg/I
mg/1
%
2,4,5-TP (Silvex)
0.0500
ND
0.0425
0.0393
85.0
78.6
2,4-D
0.0500
ND
0.0422
0.0436
84.4
87.2
(S) 2,4-Dichloropheny/Acetic
91.2
95.2
Acid
Dilution Rec. Limits MS Qualifier MSD Qualifier RPD
1 50.0-125 7.82
1 50.0-120 3.26
14.0-158
RPD Limits
o�
20
20
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ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1608049 05/01/23 11:08 15 of 21

WG2049577
Pesticides (GC) by Method 8081B
Method Blank (MB)
(MB) R3918653-1 04/27/23 21:34
MB Result
Analyte
mg/1
Chlordane
U
Endrin
U
Heptachlor
U
Heptachlor epoxide
U
Gamma BHC
U
Methoxychlor
U
Toxaphene
U
(S) Decachlorobipheny/
73.6
(S) Tetrach/oro-m-xylene
68.6
MB Qualifier MB MDL MB RDL
mg/I mg/1
Laboratory Control Sample (LCS)
QUALITY CONTROL SUMMARY
L1608049-01
0.00167
0.00500
0.00167
0.00500
0.00167
0.00500
0.00167
0.00500
0.00167
0.00500
0.00167
0.00500
0.00333
0.0100
10.0-128
10.0-127
(LCS) R3918653-2 04/27/23 21:47
Spike Amount
Analyte mg/1
LCS Result
mg/1
LCS Rec.
%
Rec. Limits LCS Qualifier
%
Endrin
0.0100
0.00805
80.5
57.0-134
Heptachlor
0.0100
0.00873
87.3
27.0-132
Heptachlor epoxide
0.0100
0.00804
80.4
57.0-130
Gamma BHC
0.0100
0.00780
78.0
55.0-129
Methoxychlor
0.0100
0.00876
87.6
54.0-155
(S) Decachlorobipheny/
57.3
10.0-128
(S) Tetrach/oro-m-xylene
68.8
10.0-127
L1606997-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1606997-01 04/27/23 22:36 • (MS) R3918653-3 04/27/23 22:49 • (MSD) R3918653-4 04/27/23 23:01
Spike Amount
Original Result
MS Result
MSD Result
MS Rec.
MSD Rec.
Analyte
mg/1
mg/1
mg/I
mg/1
%
%
Endrin
0.0100
ND
0.00859
0.00792
85.9
79.2
Heptachlor
0.0100
ND
0.00846
0.00827
84.6
82.7
Heptachlor epoxide
0.0100
ND
0.00842
0.00793
84.2
79.3
Gamma BHC
0.0100
ND
0.00797
0.00742
79.7
74.2
Methoxychlor
0.0100
ND
0.0115
0.0104
115
104
(S) Decachlorobipheny/
41.1
40.9
(S) Tetrach/oro-m-xylene
674
62.7
Dilution Rec. Limits
MS Qualifier MSD Qualifier RPD
1 10.0-160
8.12
1 16.0-136
2.27
1 10.0-160
5.99
1 14.0-141
7.15
1 10.0-160
P P 10.0
10.0-128
10.0-127
RPD Limits
39
40
36
40
34
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ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1608049 05/01/23 11:08 16 of 21

WG2050468
Semi Volatile Organic Compounds
Method Blank (MB)
QUALITY CONTROL SUMMARY
(GC/MS) by Method 8270E L1608049-01
(MB) R3919094-2 04/28/23 23:41
MB Result
MB Qualifier
MB MDL
MB RDL
Analyte mg/I
mg/I
mg/I
1,4-Dichlorobenzene U
0.0333
0.100
2,4-Dinitrotoluene U
0.0333
0.100
Hexachlorobenzene U
0.0333
0.100
Hexachloro-1,3-butadiene U
0.0333
0.100
Hexachloroethane U
0.0333
0.100
Nitrobenzene U
0.0333
0.100
Pyridine U
0.0333
0.100
3&4-Methyl Phenol U
0.0333
0.100
2-Methylphenol U
0.0333
0.100
Pentachlorophenol U
0.0333
0.100
2,4,5-Trichlorophenol U
0.0333
0.100
2,4,6-Trichlorophenol U
0.0333
0.100
(S) 2-Fluorophenol 27.8
10.0-120
(S) Phenol-d5 19.1
10.0-120
(S) Nitrobenzene-d5 73.8
10.0-127
(S) 2-F/uorobipheny/ 54.2
10.0-130
(S) 2,4,6-Tribromophenol 63.5
10.0-155
(S) p-Terphenyl-d14 72.8
10.0-128
Laboratory Control Sample (LCS)
(LCS) R3919094-1 04/28/23 23:20
Spike Amount
LCS Result
LCS Rec.
Rec. Limits LCS Qualifier
Analyte mg/I
mg/I
%
%
1,4-Dichlorobenzene 0.500
0.369
73.8
18.0-120
2,4-Dinitrotoluene 0.500
0.559
112
49.0-124
Hexachlorobenzene 0.500
0.459
91.8
44.0-120
Hexachloro-1,3-butadiene 0.500
0.371
74.2
19.0-120
Hexachloroethane 0.500
0.398
79.6
15.0-120
Nitrobenzene 0.500
0.468
93.6
27.0-120
Pyridine 0.500
0.0959
19.2
10.0-120
3&4-Methyl Phenol 0.500
0.291
58.2
31.0-120
2-Methylphenol 0.500
0.287
57.4
28.0-120
Pentachlorophenol 0.500
0.459
91.8
23.0-120
2,4,5-Trichlorophenol 0.500
0.428
85.6
44.0-120
2,4,6-Trichlorophenol 0.500
0.394
78.8
42.0-120
(S) 2-F/uorophenol
33.6
10.0-120
(S) Phenol-d5
25.0
10.0-120
(S) Nitrobenzene-d5
90.0
10.0-127
ACCOUNT:
PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources
L1608049 05/01/23 11:08 17 of 21
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WG2050468 QUALITY CONTROL SUMMARY
Semi Volatile Organic Compounds (GC/MS) by Method 8270E L1608049-01
Laboratory Control Sample (LCS)
(LCS) R3919094-1 04/28/23 23:20
Spike Amount LCS Result
Analyte mg/I mg/I
(S) 2-F/uorobiphenyl
(S) 2,4,6-Tribromophenol
(S) p-Terphenyl-dM
LCS Rec.
Rec. Limits LCS Qualifier
77.6
10.0-130
90.0
10.0-155
100
10.0-128
L1607975-10 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1607975-10 04/29/23 01:07 • (MS) R3919094-3 04/29/23 01:29 • (MSD) R3919094-4 04/29/23 01:50
Spike Amount
Original Result
MS Result
MSD Result
MS Rec.
MSD Rec.
Dilution Rec. Limits
Analyte
mg/I
mg/I
mg/I
mg/I
%
%
%
1,4-Dichlorobenzene
0.500
ND
0.275
0.223
55.0
44.6
1 17.0-120
2,4-Dinitrotoluene
0.500
ND
0.384
0.381
76.8
76.2
1 39.0-125
Hexachlorobenzene
0.500
ND
0.349
0.332
69.8
66.4
1 35.0-122
Hexachloro-1,3-butadiene
0.500
ND
0.298
0.234
59.6
46.8
1 12.0-120
Hexachloroethane
0.500
ND
0.297
0.237
59.4
47.4
1 10.0-120
Nitrobenzene
0.500
ND
0.367
0.340
73.4
68.0
1 12.0-120
Pyridine
0.500
ND
ND
0.127
16.5
25.4
1 10.0-120
3&4-Methyl Phenol
0.500
ND
0.212
0.225
42.4
45.0
1 10.0-120
2-Methylphenol
0.500
ND
0.232
0.232
46.4
46.4
1 10.0-120
Pentachlorophenol
0.500
ND
0.322
0.339
64.4
67.8
1 10.0-128
2,4,5-Trichlorophenol
0.500
ND
0.330
0.342
66.0
68.4
1 33.0-120
2,4,6-Trichlorophenol
0.500
ND
0.307
0.309
61.4
61.8
1 26.0-120
(S)2-F/uorophenol
25.0
274
10.0-120
(S) Phenol-d5
18.2
19.4
10.0-120
(S) Nitrobenzene-d5
73.2
65.4
10.0-127
(S) 2-F/uorobipheny/
62.0
56.6
10.0-130
(S)2,4,6-Tribromophenol
69.5
68.0
10.0-155
(S) p-Terphenyl-d14
74.2
82.1
10.0-128
MS Qualifier MSD Qualifier RPD
J3
20.9
0.784
4.99
24.1
22.5
7.64
42.4
5.95
0.000
5.14
3.57
0.649
RPD Limits
40
25
24
34
40
30
37
36
30
37
31
31
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ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1608049 05/01/23 11:08 18 of 21

GLOSSARY OF TERMS
Guide to Reading and Understanding Your Laboratory Report
The information below is
designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not
u
intended as a comprehensive explanation, and if you have additional questions please contact your project representative.
Results Disclaimer - Information
that may be provided by the customer, and contained within this report, include Permit Limits, Project Name,
FTC
Sample ID, Sample Matrix,
Sample Preservation, Field Blanks, Field Spikes, Field Duplicates, On -Site Data, Sampling Collection Dates/Times, and
Sampling Location. Results relate to the accuracy of this information provided, and as the samples are received.
Abbreviations and Definitions
FSS
MDL
Method Detection Limit.
ND
Not detected at the Reporting Limit (or MDL where applicable).
rqn
RDL
Reported Detection Limit.
Rec.
Recovery.
Fr]
RPD
Relative Percent Difference.
SDG
Sample Delivery Group.
Surrogate (Surrogate Standard) - Analytes added to every blank, sample, Laboratory Control Sample/Duplicate and
e
QC
(S)
Matrix Spike/Duplicate; used to evaluate analytical efficiency by measuring recovery. Surrogates are not expected to be
detected in all environmental media.
U
Not detected at the Reporting Limit (or MDL where applicable).
Analyte
The name of the particular compound or analysis performed. Some Analyses and Methods will have multiple analytes
reported.
If the sample matrix contains an interfering material, the sample preparation volume or weight values differ from the
a
Dilution
standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the
laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the
result reported has already been corrected for this factor.
FSC
These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal
Limits
for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or
duplicated within these ranges.
Original Sample
The non -spiked sample in the prep batch used to determine the Relative Percent Difference (RPD) from a quality control
sample. The Original Sample may not be included within the reported SDG.
This column provides a letter and/or number designation that corresponds to additional information concerning the result
Qualifier
reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and
potentially a discussion of possible implications of the Qualifier in the Case Narrative if applicable.
The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. If there was
no measurable result returned for a specific analyte, the result in this column may state "ND" (Not Detected) or "BDL"
Result
(Below Detectable Levels). The information in the results column should always be accompanied by either an MDL
(Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect
or report for this analyte.
Uncertainty
(Radiochemistry)
Confidence level of 2 sigma.
A brief discussion about the included sample results, including a discussion of any non -conformances to protocol
Case Narrative (Cn)
observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will
be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report.
Quality Control
This section of the report includes the results of the laboratory quality control analyses required by procedure or
Summary (Qc)
analytical methods to assist in evaluating the validity of the results reported for your samples. These analyses are not
being performed on your samples typically, but on laboratory generated material.
This is the document created in the field when your samples were initially collected. This is used to verify the time and
Sample Chain of
date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This
Custody (Sc)
chain of custody also documents all persons (excluding commercial shippers) that have had control or possession of the
samples from the time of collection until delivery to the laboratory for analysis.
This section of your report will provide the results of all testing performed on your samples. These results are provided
Sample Results (Sr)
by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for
each sample will provide the name and method number for the analysis reported.
Sample Summary (Ss)
This section of the Analytical Report defines the specific analyses performed for each sample ID, including the dates and
times of preparation and/or analysis.
Qualifier
Description
J
The identification of the analyte is acceptable; the reported value is an estimate.
J3
The associated batch QC was outside the established quality control range for precision.
J5
The sample matrix interfered with the ability to make any accurate determination; spike value is high.
P
RPD between the primary and confirmatory analysis exceeded 40%.
T8
Sample(s) received past/too close to holding time expiration.
ACCOUNT:
PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources
L1608049 05/01/23 11:08 19 of 21

ACCREDITATIONS & LOCATIONS
Pace Analytical National 12065 Lebanon Rd Mount Juliet, TN 37122
Alabama
40660
Nebraska
NE-OS-15-05
Alaska
17-026
Nevada
TN000032021-1
Arizona
AZ0612
New Hampshire
2975
Arkansas
88-0469
New Jersey—NELAP
TN002
California
2932
New Mexico
TN00003
Colorado
TN00003
New York
11742
Connecticut
PH-0197
North Carolina
Env375
Florida
E87487
North Carolina'
DW21704
Georgia
NELAP
North Carolinas
41
Georgia'
923
North Dakota
R-140
Idaho
TN00003
Ohio—VAP
CL0069
Illinois
200008
Oklahoma
9915
Indiana
C-TN-01
Oregon
TN200002
Iowa
364
Pennsylvania
68-02979
Kansas
E-10277
Rhodelsland
LA000356
Kentucky16
KY90010
South Carolina
84004002
Kentucky 2
16
South Dakota
n/a
Louisiana
A130792
Tennessee' °
2006
Louisiana
LA018
Texas
T104704245-20-18
Maine
TN00003
Texas'
LAB0152
Maryland
324
Utah
TN000032021-11
Massachusetts
M-TN003
Vermont
VT2006
Michigan
9958
Virginia
110033
Minnesota
047-999-395
Washington
C847
Mississippi
TN00003
West Virginia
233
Missouri
340
Wisconsin
998093910
Montana
CERT0086
Wyoming
A21-A
A21-A — ISO 17025
1461.01
AIHA-LAP,LLC EMLAP
100789
A21-A — ISO 17025 s
1461.02
DOD
1461.01
Canada
1461.01
USDA
P330-15-00234
EPA—Crypto
TN00003
Drinking Water 2 Underground Storage Tanks 'Aquatic Toxicity ° Chemical/Microbiological 'Mold 6 Wastewater n/a Accreditation not applicable
Not all certifications held by the laboratory are applicable to the results reported in the attached report.
Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace Analytical.
FP1
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ACCOUNT: PROJECT: SDG: DATE/TIME:
EMA Resources L1608049 05/01/23 11:08
PAGE:
20 of 21

re
esurces
775M5YadkoinviolleRoad
Mocksville, NC 27028
Billing Information:
Mr. Brent Collins TChk
755 Yadkinville Road
Mocksville, NC 27028
AnalvSiq
/ (nntainar
/ PrPgart/ativP
Chain of Custody Page _ of _
- ace,
P.P E AnvANCiNG SCIENCE
MT JULIET, TN
12065 Lebanon Rd Mount Juliet TN 37122
Submitting a sample via this chain of custody
constitutes acknowledgment and acceptance of the
Pace terms and Conditions found as
nttp:://inl°.pacelab:.r°m/n,bf:/pas-teanaard-
terms.pol
t7
o
�
CL
z
•_
u
,J
-
ZI
Report to:
Mr. Brent Collins
Email To:
[e-mail];roy.whitak
Project Description:
Sludge
City/State
/, A
Collected: QSi1,� 'I'lTl//'
Please Circle:
PT MT CT ET
Phone: [phone]
Client Project #
Lab Project #
SDG #
E 173
Acctnum: EMARES
Template:T11413
Prelosin: P977658
P ns
2 - ea
Collected by (print):
�� �S
Site/Facility ID #
P.O. #
Collected by (signature):
Immediately /
Packed on Ice N Y V
Rush? (Lab MUST Be Notified) Quote #
Same Day Five Day
Next Day 5 Day (Rad Only) Date Results Needed
Two Day _ 10 Day (Rad Only) No.
_ Three Day
--TtH
Ship ed Via: edEX Ground
Depth
Date
Time
ntrs
>
W
cJa.
U
Sample ID
Comp/Grab
Matrix'
Remarks Sample d (lab only)
—
as "+ �� _
C
SS
'S�/1�o/L3
5L.-00
_
G
-
-f--
i
t
........
- ._.............. ............. ........... ............... ........... ............................... .
" Matrix:Remarks:
SS - Soil AIR - Air F- Filter
GW- Groundwater B- Bioassay
WW - WasteWater
DT- OthekingV�}ter
3�
OT-Other der—
pH Temp
Flow Other
_
Sample Recei heck ist
COC Seal Present/Intact: NP Y N
COC Signed/Accurate: N
Bottles arrive intact: ZW N
correct bottles used: N
Sufficient volume sent: �t _N
VOA Zero HeadspaceIf iicable Y N
Preservation Correct/checked: Y —N
RFD Screen <0.5 mR/hr: Y —N
`
Samples returned via:
UPS FedEx —Courier
„ �
Tracking# 7
Relinquished by : (Signature) Date:
Time:
Received by: (Signature)
Trip Blank Received: Yes /
HCL MeoH
TBR
Relinquished by : (Signature) Date:
Time:
Received by: (Signature)
Temp: °C Bottles Received:
If preservation required by Login: Date/Time
Relinquished by : (Signature) Date:
Time:
Received for lab by: (Signature)
D te: Time:
J � 1 ('
�a'J
Hold:
Conditio
NCF / OK

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Washington WQ Permit Number: WQ0001026
WWTP Name: Washington WWTP
Monitoring Period: From 4/10/2023 To
NPDES Number: NCO020648
4/10/2023
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. A (time/temp) ❑
Alt B (Alk Treatment) ❑
Alt. C (Prior Testing) 0
Alt.D (No Prior Test) ❑
1 Process to Further Reduce Pathogengs ❑
If applicable to alternative
performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost 0
Heat Drying ❑
Heat Treatment ❑
Thermophilic ❑
Beta Ray 0
Gamma Ray ❑
Pasteurization ❑
Class B:
JAIL (1) Fecal Density ®
Alt. (2) Process to Significantly Reduce Pathogens ❑
If applicable to alternative
performed (Class
B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization ❑
1 Air Drying ❑
Composting ❑
Aerobic Digestion ❑
Anaerobic Digestion ❑
If applicable to alternative performed (Class A or Ch 2021
Parameter
Allowable Level
in Sludge
Pathogen Density
g y
Number o
Excee-
dences
Frequency
of Analysis
Sample
Type
Analytical
Tech -pique
Minimum
Geo. Mean
Maximum
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
4500
11141
55000
MPN/g
0
Quarterly
G
SM92210E
CFu
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per 4 grams
total solid (dry
weight)
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed:
Alt.1 (VS reduction) ®
Alt. 2 (40-day bench) ❑
Alt. 3 (30-day bench) ❑
Alt. 4 (Spec. OZ uptake) ❑
Alt. 5 (14-Day Aerobic) ❑
Alt. 6 (Alk. Stabilization ❑
Alt 7 (Drying - Stable) ❑
Alt. 8 (Drying - Unstable) ❑
Alt. 9 (Injection) ❑
Alt. 10 (Incorporation) ❑
No vector attraction reduction alternatives were performed ❑
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if
you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Lonnie Woolard - NPDES ORC
Brent Collins; Director of Technical Services
Preparer Name and Title (type or print) Land Applier Name and Title (if applicable)(type or print)
Loiml� PyooG i 02/06/2z
Lonnie Woolard (Feb 6, 202414:28 EST) 4./�/J►��- 2/5/2024
Signature of Preparer* Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 02T (12/2006)

Date: 4/10/2023
Location #
1
2
3
4
5
6
7
Summary Sheet
Fecal Coliforms
Pathogen Reduction
MPN/g
5000
11250
55000
6000
4500
22667
11250
Log
3.6990
4.0512
4.7404
3.7782
3.6532
4.3554
4.0512
11141
Geometric Means/g
Total Dry Solids
r

M
Sampled By:
Received By: t1)-
Analyzed By:
Calculated By: t c
Checked By '
FECAL COLIFORM TEST
Standard Methods 9221 E-2014 (MPN) (Biosolids)
Permit #: WQ001026
DATE / TIME
4110)a-3 crx,-
�t 1► �:� .�-� iau �
Sample Location: Sludge #
Sample Type: Grab X Composite
Preservation: None Cooled to 40C
24 hr. Check Rill .o �3
48 hr. Check -A
72 hr. Check &J +-fti"AA131(SL�S
b PrPsumntive Test D
Top Shelf: • x °C
Bottom Shelf: °C
Water Bath: 9'-f.15 °C
19-M
mL Sampleh0.001
0.0001
0.00001
0.000001
0.0000001
0.00000001
24 hours
M
48 hours
--
�-
—
—
—
—
1 0 0 Fecal Coliform Test
mL Sample
0.001
0.0001
0.00001
0.000001
0.0000001
0.00000001
MPN
24 hours
a. O
yiio31�3
MPN Fecal Coliform/g = 10 x MPN index / 100 ml
largest volume X % dry solids tested
Sterility Control
Quality Control Tubes
10 mL
Double Strength (DS) Control:".
Single Strength (SS) Control
y\J<,
EC Broth Control
p't
Revised 5-23-16; 4/4l22
MPN/g = 1Ox 4. Q =
0 , oo I � +
0,oa�+
500 o m"N/'6

M
Sampled By:
Received By:
Analyzed By:
Calculated By: (�
Checked By:
FECAL COLIFORM TEST
Standard Methods 9221 E-2014 (MPN) (Biosolids)
Permit* WQ001026
DATE I TIME
�t I ��I2r3 11 l�
Sample Location: Sludge # l C� .4^hCrS- Top Shelf: °C
Sample Type: Grab X Composite Bottom Shelf: �,�j,c� °C
Preservation: None Cooled to 4°C Water Bath: Lj I f.5 °C
24 hr. Check I . ,,�,q ' '_�
48 hr. Check q>>2{}3 t.)a ='-, rZ. .`
72 hr. Check T,py�`� b
S P O PrP_gmmntivP_ Test O
tqcl k
mL Sample
0.001
01
0.00001
0.000001
0.0000001
0.00000001
MPN
24 hours
�'
t
Ei-
0
O D Fecal Coliform Test
mL Sample 0.001 0.0001 0.00001 0.000001 I 0.0000001 0.00000001 MPN
24 hours — 11411
MPN Fecal Coliformlg =
10 x MPN index / 100 ml
largest volume X % dry solids tested
Sterility Control
Quality Control Tubes
10 mL
Double Strength (DS) Control
kA4-
Single Strength (SS) Control
t,
EC Broth Control
li a'7t.
Revised 5-23-16; 4/4/22
MPNIg = 10x I ,' _ L
'-�5 a o >n P N`d�
0.00I 6,c)(3 -

Sampled By:
M
Received By:
Analyzed By:
By:
Calculated By:
-
Checked By
6`
5 v
FECAL COLIFORM TEST
Standard Methods 9221 E-2014 (MPN) (Biosolids)
Permit #: W0001026
DATE / TIME
�tl��la�3 1tI�
Sample Location: Sludge #
Sample Type: Grab X Composite
Preservation: None Cooled to 40C I-
24 hr. Check ►1�u133 1�3�{ �s�
48 hr. Check
72 hr. Check Lt 1 1,31 Z�,3 Hit. ?0 N"A
I Presumptive Test o
Top Shelf: "� �,g, °C
Bottom Shelf: �c.O °C
Water Bath: 9 Lf-'j °C
91
mL Sample
0.001
0.0001
0.00001
0.000001
0.0000001
0.00000001
MPN
24 hours
K--Ell
I
j
I
-
-
-
-
-
-
-
-
-48
hours
�'
,-
�"-
D G
v Fecal Coliform Test
mL Sample
0.001
0.0001
0.00001
0.000001
0.0000001
0.00000001
MPN
24 hours
.5
MPN Fecal Coliformlg =
10 x MPN index / 100 ml
largest volume X % dry solids tested
Sterility Control
Quality Control Tubes
10 mL
Double Strength (DS) Control
Single Strength (SS) Control
ti t,
EC Broth Control
Revised 5-23-16; 4/4/22
MPN/g = 10x
a-$0 p1 PA)14(,
0,00 l X 4p,ao4

M
Sampled By:
Received By:
Analyzed By:
Calculated By:
Checked By:
to r
FECAL COLIFORM TEST
Standard Methods 9221 E-2014 (MPN) (Biosolids)
Permit #: W0001026
DATE / TIME
4 1 1o)a-3 (off,
-4kular3 1110
Li IQ) a-% I , q
q 7::;L-,, 1 4�-n
Sample Location: Sludge #
Sample Type: Grab X Composite
Preservation: None Cooled to 40C I
24 hr. Check
48 hr. Checkl►
72 hr. Check -j j,3 j 23. gxg-.'R'/ '
9 D Pracsimntiva Tact I
Top Shelf: • , e °C
Bottom Shelf: - 5,0 °C
Water Bath: q Lf- j °C
916 4(oU
mL Sample
0.001
0.0001
0.00001
0.000001
0.0000001
0.00000001
MPN
24 hours
}
,�
—
—
—
—
48 hours
-F-
I
I
I
�
ate" �W1��
N `� Zl. 'D Fecal Coliform Test o
mL Sample
0.001
1 0.0001
1 0.00001 71
0.000001
1 0.0000001
1 0.00000001
PN
U.-A
24 hours
+
�-
—
t-
}
—
MPN Fecal Coliformlg =
10 x MPN index / 100 ml
largest volume X % dry solids tested
Sterility Control
Quality Control Tubes
10 mL
Double Strength (DS) Control
Single Strength (SS) Control
EC Broth Control
Revised 5-23-16; 4/4/22
MPNIg = 10x :r.a = a _-�, O
" 5-15�, Oef vn,Prv/y
o,UC) I g, 4 0,©c

f
Sampled By:
�K�M
Received By:
Analyzed By:
Calculated By:
Checked By
��.V..
L`I
FECAL COLIFORM TEST
Standard Methods 9221 E-2014 (MPN) (Biosolids)
Permit #: WQ001026
DATE / TIME
4j►oja-3 I Cf-')b
-+I101a3 hto
y1►u��.3.3 lacy
Sample Location: Sludge # +
Sample Type: Grab X Composite
Preservation: None Cooled to 4°C A
24 hr. Check
48 hr. Check
72 hr. Check �} i.3L�.3lyt g �3 IPA
Presumotive Test O
Top Shelf: °C
Bottom Shelf: ?6.0 °C
Water Bath: y Lf-'5 °C
al
mL Sample
0.001
0.0001
0.00001
0.000001
0.0000001
0.00000001
MPN
24 hours
48 hours
-f-
—
_
—
-�
—
fl 0 0 Fecal Coliform Test
mL Sample
0.001
0.0001
0.00001
0.000001
0.0000001
0.00000001
MPN
24 hours
I
I
I
I
I—
I
I
I
I
I
I
I
<I,B'
MPN Fecal Coliform/g =
10 x MPN index / 100 ml
largest volume X % dry solids tested
Sterilitv Control
Quality Control Tubes
10 mL
Double Strength (DS) Control
Single Strength (SS) Control
y` C
EC Broth Control
Revised 5-23-16; 4/4/22
MPN/g = 10x 1 , g = l � � �00 Yx�/�! `�
oc 1 X > 0, 003

FECAL COLIFORM TEST
Standard Methods 9221 E-2014 (MPN) (Biosolids)
Permit #: WQ001026
,ALAM
DATE / TIME
Sampled By:
,
41 `01a-' �
� 0S'-t
Sample Location: Sludge # ram" Top Shelf: -� A,f? °C
Received By:
t_t„�� ,r—
�i 1�=1 a 3
11'C
Sample Type: Grab X Composite Bottom Shelf: °C
Analyzed By:
Preservation: None Cooled to 40C Water Bath: Lf.5 °C
Calculated By:
5
Checked By:
w
j ��I
j 3t.�
24 hr. Check glu�23
48 hr. Check -4��v�{a3 i a33 fit/
72 hr. Check &k1i;3`�J-ilk,
ON " Presum tive Test `" `1 --'
nL Sample 0.001 0.0001 0.00001 0.000001 0.0000001 0.00000001 mph
24 hours-
48 hours
c c7 CP Fecal Coliform Test
mL Sample 0.001 0.0001 0.00001 0.000001 0.0000001 0.00000001 MPN
24 hours e-J.�r
MPN Fecal Coliform/g = 10 x MPN index / 100 ml
largest volume X % dry solids tested
Sterility Control
Quality Control Tubes
10 mL
Double Strength (DS) Control
V\RS, CjLcf-
Single Strength (SS) Control
EC Broth Control
tit
Revised 5-23-16; 4/4122
MPN/g = 10x ? g` _
0,00 t x if
1 ?, ;:7 45 aL)
0, CMG

—NAME
Sampled By:
Received By:
Analyzed By:��-w:
Calculated By:_�
Checked BX-,��n-�
FECAL COLIFORM TEST
Standard Methods 9221 E-2014 (MPN) (Biosolids)
Permit #: WQ001026
DATE I TIME
41 ")OI
Sample Location: Sludge # tp Top Shelf: °C
Sample Type: Grab X Composite Bottom Shelf: °C
Preservation: None Cooled to 40C 1 Water Bath: 'J't-5 °C
24 hr. Check
48 hr. Check
72 hr. Check
1 `1 i Presum tive Test a
mL Sample 0.001 0.0001 0.00001, 0.000001 0.0000001 0.00000001 MPN
24 hours
48 hours — I 1 14 — -k-
a- 1 J Fecal Coliform Test
mL Sample
0.001
0.0001
0.00001
0.000001
0.0000001
0.00000001
MPN
24 hours
I +
I—
—
-t-
(-, g'
MPN Fecal Coliform/g =
10 x MPN index / 100 ml
largest volume X % dry solids tested
Sterility Control
Quality Control Tubes
10 mL
Double Strength (DS) Control
Single Strength (SS) Control
yam' LO 1C
EC Broth Control
Revised 5-23-16; 4/4/22
MPN/g = 10x (P _
00
o, oaf a � � �

M Sampled By:
Received By: >�
Analyzed By:
Calculated By:
Checked By
S
FECAL COLIFORM TEST
Standard Methods 9221 E-2014 (MPN) (Biosolids)
Permit #: WQ001026
DATE/TIME
�t�►��a3 h03
Sample Location: Sludge # —]
Sample Type: Grab X Composite
Preservation: None Cooled to 4°C
24 hr. Check '1`u.`a3 1 -\347 , P5
48 hr. Check -A1%,*),3 ,7,31 , %Z-63/ wb
72 hr. Check `t 1 i_3�20'3 F1`I1L �713T/k,QA
�
1 11 Presumptive Test b
Top Shelf: l,� °C
Bottom Shelf: °C
Water Bath: °C
46
mL Sample
0.001
1
0.00001
0.000001
0.0000001
0.00000001
MPN
24 hours
Y
�'
h0.00
—
---
—
—
48 hours
—
—
—
—
.—
—
'1 0
0 Fecal Coliform Test
yS
mL Sample
0.001
0.0001
0.00001
1 0.000001
0.0000001
0.00000001 MPN
24 hours
—
1-t.5
MPN Fecal Coliform/g =
10 x MPN index / 100 ml
largest volume X % dry solids tested
Sterilitv Control
Quality Control Tubes
10 mL
Double Strength (DS) Control
�Q f
Single Strength (SS) Control
V� t
EC Broth Control
Revised 5-23-16; 4/4/22
MPN/g = 10x
0,001 -- 4f
1-1S = MAY
o,00 �

Sampled By: �� I
Received By:
Analyzed By: }1�� :1 l c
Calculated By: J 1-
Checked By, GrG�Qtj11,�
City of Washington
Sludge
Standard Methods 2540 G-2015 (Aqueous)
Permit #: W0001026
10 5u Time onyH/2O� bath
y j i o ja-3 l 1 Drying Oven Terrip (in)
4 - J I Time in Oven
Drying Oven Temp (out)
Time Out of Oven
Time Weighed
1st
2nd
r/
/C
c
(o
qua
lea
Sample
Blank
Sludge #
Duplicate
Evaporating Dish #
5 5
Wet Weight + Dish Weight
Dish Weight
a5 a
9 (� I p,
i b 0, 9
Wet Weight
�3 0 0 `
J3 0 ! '4
1 st Dry Weight + Dish Weight
Q ,
k a S v
2nd Dry Weight + Dish Weight
.� 5 a . 3
[� 5 ,, S
S 3
Difference
1 st & 2nd Dry Weight + Dish Weight
(2nd-1st)
O .
D , I
D
Dry Weight
(2nd Dry Wt + Dish Wt - Dish Wt)
O .
% Dry Solids [(Dry Wt/Wet Wt) x 100)]
3,
*Note -Differences should agree within 4% or 0.5 mg, which ever is less Revised: 9/26/19 JDW; 4/6/22 RWB

City of Washington
Sludge
Standard Methods 2540 G-2015 (Aqueous)
Permit #: WQ001026
Sampled By: /� ! 4 �-) l u a3 �; oL Time on H2O bath
Received By: yl aU4,_j_Q W i3-, j, u I.-*- 1 l 1 L Drying OvenTemp (in)
Analyzed By: .,<<�, '23 J; c qu c K j b o? - . / a `> Time in Oven
Calculated By: `._- - q - 0 -,_13 , 7 Olt Drying Oven Temp (out)
Checked By: t,47,�_ i 0,c I D-3 IG ;jo Time Out of Oven
Time Weighed
1st
2nd
c
0
e
a
-719
954
1Lo
nb�"I
3
Sample
Blank
Sludge #
Duplicate
Evaporating Dish #
13
I'Z
Wet Weight + Dish Weight
/ o / (D 4 5 T
Dish Weight
S- a Sa S
-7 d 9 5 S: S
Wet Weight
/3 a n 9 . 3
1st Dry Weight + Dish Weight
oZ S a , S
I t4 q , 3
2nd Dry Weight + Dish Weight
,P I
Difference
1 st & 2nd Dry Weight + Dish Weight
(2nd-1 st)
,
Dry Weight
(2nd Dry Wt + Dish Wt - Dish Wt)
O .
�! 1 $ 12", &
% Dry Solids [(Dry Wt/Wet Wt) x 100)]
�3, 9 S=
*Note -Differences should agree within 4% or 0.5 mg, which ever is less Revised: 9/26/19 JDW; 4/6/22 RWB

Sampled By:
Received By: 6�u"Wf�-•—f
Analyzed By:
Calculated By:
Checked By:�
City of Washington
Sludge
Standard Methods 2540 G-2015 (Aqueous)
Permit #: W0001026
Time on H2O bath
o 3 3 ►11 Drying Oven I e)mp (in)
y -I O 3 1 I q Time in Oven
Drying Oven Temp (out)
`f)26123 Time Out of Oven
Time Weighed
1 st
2nd
103`
lo;c
v
iii�
135�
Sample
Blank
Sludge # 3
Duplicate
Evaporating Dish #
3
Wet Weight + Dish Weight
1 ] 61, `-
Dish Weight
00 7 a 5" a, s
6) kj
Wet Weight
3 b 1. 3, 6
1 st Dry Weight + Dish Weight
8 5
- 4 3L
2nd Dry Weight + Dish Weight
g S , `
L7 _ a 5-
Difference
1 st & 2nd Dry Weight + Dish Weight
(2nd-1st)
©. y
.
Dry Weight
(2nd Dry Wt + Dish Wt - Dish Wt)
p
✓ 14 = f
% Dry Solids [(D Wt/Wet Wt) x 100)]
mot, y-1 _ �a
*Note -Differences should agree within 4% or 0.5 mg, which ever is less Revised: 9/26/19 JDW; 4/6/22 RWB

Sampled By:
"LIZ 4
Received By:
6 j1 � zQ W la-•—�
Analyzed By:
,,/ 3- (
Calculated By:
, .') LL" --
Checked By:
"jwn_;
City of Washington
Sludge
Standard Methods 2540 G-2015 (Aqueous)
Permit* WQ001026
(a3 10 5Cr Time on H2O bath
(.I/, �>
Drying Oven Temp (in)
Time in Oven
`f - I a 23, 1 4 Drying Oven Temp (out)
q I I a r o 93 Time Out of Oven
Time Weighed
1 st
2nd
13411
°1
S
N
Sample
Blank
Sludge # z4
Duplicate
Evaporating Dish #
/ (�
Wet Weight + Dish Weight
7" , 6—
Dish Weight
8 a 5;- , 57
O % 5 I , 3
Wet Weight
f_3 d o ,-1
1st Dry Weight + Dish Weight
S .a ; "7
q5 I S 1:7
2nd Dry Weight + Dish Weight
3
S 1 8 -
Difference
1st & 2nd Dry Weight + Dish Weight
(2nd-1st)
Dry Weight
(2nd Dry Wt + Dish Wt - Dish Wt)
% D Solids D Wt/Wet Wt) x 100))
3 , y 1 = ,
*Note -Differences should agree within 4% or 0.5 mg, which ever is less Revised: 9/26/19 JDW; 4/6/22 RWB

City of Washington
Sludge
Standard Methods 2540 G-2015 (Aqueous)
Q Permit #: WQ001026
Sampled By: 1p 5-q Time on H2O bath
• (am)
Received By: y 1 ) o ja-3 1110 Drying Oven Temp (in)
Analyzed By: ,,,rY, ;� ? � .� - %b / y C, (2) Time in Oven
Calculated By: ..,, _ ��ir j )a-, f Drying Oven Temp (out)
Checked By: Time Out of Over
Time Weighed
1st
2nd
/NIC
/C) 6
!C
2
%I!8
135�
Sample
Blank
Sludge #
Duplicate
Evaporating Dish #
1
G'P
l ° S 3,
Wet Weight + Dish Weight
Dish Weight
Wet Weight
1 st Dry Weight + Dish Weight
2nd Dry Weight + Dish Weight
�7 a 5
a : 1
Difference
1 st & 2nd Dry Weight + Dish Weight
(2nd-1st)
,
Dry Weight
J
(2nd Dry Wt + Dish Wt - Dish Wt)
G' . 1;11
1 I ' >< 2L - O
% Dry Solids D Wt/Wet Wt) x 100)]
J
, B U
*Note -Differences should agree within 4% or 0.5 mg, which ever is less Revised: 9/26/19 JDW; 4/6/22 RWB

Sampled By:
Received By: (Au4to W 11
Analyzed By:
Calculated By: ,, , c Ce
12 LI
Checked By: I At "-Q L00_1�_
City of Washington
Sludge
Standard Methods 2540 G-2015 (Aqueous)
Permit* W0001026
a3 1 ! o I Time on H2O bath
yllola-3 1110
`11��2-3 �a2-tP
Drying Oven Temp (in)
Time in Oven
Drying Oven Temp (out)
Time Out of Over
Time Weighec
1st
2nd
�a,r-
lo�°
l03`
Sample
Blank
Sludge # (�
Duplicate
Evaporating Dish #
l�
Wet Weight + Dish Weight
Dish Weight
g a sa
Wet Weight
3 CC) (e 1 . 3
1 st Dry Weight + Dish Weight
8 oZ S a 3
D ! S Ii
2nd Dry Weight + Dish Weight
�Sa • `�
- ! 06 S
Difference
1 st & 2nd Dry Weight + Dish Weight
(2nd-1st)
D 3
Dry Weight
(2nd Dry Wt + Dish Wt - Dish Wt)
! o 3 G,
% Dry Solids [(Dry Wt/Wet Wt) x 100),
*Note -Differences should agree within 4% or 0.5 mg, which ever is less Revised: 9/26/19 JDW; 4/6/22 RWB

Sampled By: plze_¢.�
Received By:
Analyzed By: ; . z , -c
Calculated By::
Checked By: '
City of Washington
Sludge
Standard Methods 2540 G-2015 (Aqueous)
Permit #: WQ001026
Time on H2O bath
yl,0ja-3 1110
�f-/a--a3 i05`i
Drying Oven Temp (in)
Time in Oven
Drying Oven Temp (out;
Time Out of Over
Time Weighec
Elst
2nd
1030
0�`
g,5(,
la y
ro3°
to '
ll/`d
135�
Sample
Blank
Sludge # -7
Duplicate
Evaporating Dish #
Wet Weight + Dish Weight
Dish Weight
-f :4 �—, 5�
D a . a
Wet Weight
3 C O 1-, p
1 st Dry Wei ht + Dish Weight
� �L 1, 9, T
2nd Dry Weight + Dish Weight
a Sa ,
��L(p�
Difference
1 st & 2nd Dry Weight + Dish Weight
(2nd-1 st)
0,4
0. 1
Dry Weight
(2nd Dry Wt + Dish Wt - Dish Wt)
0, a
Jr c q 3 ,
% Dry Solids [(Dry Wt/Wet Wt) x 100)]
*Note -Differences should agree within 40/6 or 0.5 mg, which ever is less Revised: 9/26/19 JDW; 4/6/22 RWB

January 2023 Average
AVG.
2023 Average
R.S. 1 & 2
R.S. 3
R.S. 4
76.50%
78.04%
1 75.91%
76.82%
4/20/23 Sample
VS in 0.7383
February 2023 Average
VS out 0.403
R.S. 1 & 21
R.S. 3
R.S. 4
VSFR= 76.07
75.89%
1 76.14%
1 76.49%
76.17%
4/25/23 Sample
March 2023 Average
VS in 0.7383
R.S. 1 & 21
R.S. 3
R.S. 4
VS out 0.565
76.07%
1 76.11%
1 75.08%
75.75%
VSFR= 53.96
10/25/23 Sample
April 2023 Average
R.S. 1 & 2
R.S. 3
R.S. 4
VS in 0.7383
75.07%
74.80%
1 74.31%
74.73%
VS out 0.613
VSFR= 43.85
May 2023 Average
R.S. 1 & 21
R.S. 3
R.S. 4
11/8/23 Sample
72.43%
1 76.69%
1 71.81%
73.64%
VS in 0.7383
VS out 0.603
June 2023 Average
VSFR= 46.16
R.S. 1 & 21
R.S. 3
R.S. 4
74.10%
1 75.41%
1 70.55%
73.35%
July 2023 Average
R.S. 1 & 21 R.S. 3 R.S. 4
73.00% 1 75.50% 1 68.49% 72.33%
August 2023 Average
R.S. 1 & 21 R.S. 3 R.S. 4
70.12% 1 74.08% 68.13% 70.78%
September 2023 Average
R.S. 1 & 2 R.S. 3 R.S. 4
70.44% 76.30% 1 66.87% 71.20%
October 2023 Average
R.S. 1 & 2 R.S. 3 R.S. 4
72.62% 71.92% 1 69.32% 71.29%
November 2023 Average
R.S. 1 & 2 R.S. 3 R.S. 4
73.53% 74.84% 1 70.81% 73.06%
December 2023 Average
R.S. 1 & 2 R.S. 3 R.S. 4
75.15% 80.94% 1 74.40% 76.83%
73.83%

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Washington WQ Permit Number: WQ0001026
WWTP Name: Washington WWTP
Monitoring Period: From 4/18/2023 To
NPDES Number: NCO020648
4/18/2023
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. A (time/temp) ❑
Alt B (Alk Treatment) ❑
Alt. C (Prior Testing) ❑
Alt.D (No Prior Test) ❑
1 Process to Further Reduce Pathogengs ❑
If applicable to alternative
performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost 0
Heat Drying 0
Heat Treatment 0
Thermophilic 0
Beta Ray 0
Gamma Ray 0
Pasteurization 0
Class B:
JAIL (1) Fecal Density ®
Alt. (2) Process to Significantly Reduce Pathogens ❑
If applicable to alternative
performed (Class
B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization ❑
1 Air Drying ❑
Composting ❑
Aerobic Digestion ❑
Anaerobic Digestion ❑
If applicable to alternative performed (Class A or Ch 2021
Parameter
Allowable Level
in Sludge
Pathogen Density
g y
Number o
Excee-
dences
Frequency
of Analysis
Sample
Type
Analytical
Tech -pique
Minimum
Geo. Mean
Maximum
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
3600
5276
15600
MPN/g
0
Quarterly
G
SM92210E
CFu
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per 4 grams
total solid (dry
weight)
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed:
Alt.1 (VS reduction) ®
Alt. 2 (40-day bench) 0
Alt. 3 (30-day bench) ❑
Alt. 4 (Spec. OZ uptake) ❑
Alt. 5 (14-Day Aerobic) ❑
Alt. 6 (Alk. Stabilization ❑
Alt 7 (Drying - Stable) ❑
Alt. 8 (Drying - Unstable) ❑
Alt. 9 (Injection) ❑
Alt. 10 (Incorporation) ❑
No vector attraction reduction alternatives were performed ❑
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if
you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Lonnie Woolard - NPDES ORC
Brent Collins; Director of Technical Services
Preparer Name and Title (type or print) Land Applier Name and Title (if applicable)(type or print)
Loiml� PyooG i 02/06/2z
Lonnie Woolard (Feb 6, 202414:28 EST) 4. --
/�/J►�
�- 2/5/2024
Signature of Preparer* Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 02T (12/2006)

Date: 4/18/2023
Location #
1
2
3
4
5
6
7
Summary Sheet
Fecal Coliforms
Pathogen Reduction
MPN/g
4000
15600
3600
4500
5000
5000
4500
Log
3.6021
4.1931
3.5563
3.6532
3.6990
3.6990
3.6532
5276
Geometric Means/g
Total Dry Solids
11J--
na ure

Sampled By:
NAME
Received By:t�6�-yam
Analyzed
Calculated By:
"
Checked By.!3�"b
5
FECAL COLIFORM TEST
Standard Methods 9221 E-2014 (MPN) (Biosolids)
Permit #: W0001026
DATE / TIME
31a)7
�-i-:,ib-a3. fog
Ala-i��
Sample Location: Sludge # 4 Top Shelf: . 8' °C
Sample Type: Grab X Composite Bottom Shelf: W.0 °C
Preservation: None Cooled to 40C Water Bath: t'I4-s °C
24 hr. Check 461,1\3 l3�tf� P.PiI 1G
48 hr. Check Ljj2ola-3
72 hr. Check , 13�j0 zmo
C; I Pracmimnflua Tncf D
35u
mL Sample
0.001
.0001
0.00001
0.000001
0.0000001
0.00000001
MPN
24 hours
�-
t
I
t48
El
hours;
( c--�, n Fecal Coliform Test
mL Sample
0.001
0.0001
0.00001
0.000001
0.0000001
0.00000001
24 hours
I -
I-
-I
-
I_
..
HN
MPN Fecal Coliform/g = 10 x MPN index / 100 ml
largest volume X % dry solids tested
Sterility Control
Quality Control Tubes
10 mL
Double Strength (DS) Control
Single Strength (SS) Control
kQS
EC Broth Control
Revised 5-23-16; 4l4/22
MPN/g = 10x ),t9
av
2f000 TTLPA.'

NAME
Sampled By: �a���L D"-;,-
Received By: ,� t1 U_)O-y_Z_
Analyzed By: &uW1"` �
Calculated By: o
Checked By:
a
FECAL COLIFORM TEST
Standard Methods 9221 E-2014 (MPN) (Biosolids)
Permit #: W0001026
DATE I TIME
Lk) 3�y�„ 3)yid
Sample Location: Sludge # ( cj u_j)'j C&b_ Top Shelf: 34 8' °C
Sample Type: Grab X Composite Bottom Shelf: 35.0 °C
Preservation: None Cooled to 40C Water Bath: t'Pq.E> °C
24 hr. Check ,3Lt6 _gAj I
48 hr. Check q Doi2$ (1
72 hr. Check %flnd;z r 1350 .K-/� f OD-j
(-D Prasmmr-tiva Tact 0
'%q
mL Sample
0.001
0.0001
0.00001
0.000001
0.0000001
0.00000001
MPN
24 hours
-
-
-
-
-
-
-
-
1-79
48 hours
--
-
_
-
1j._
_
_
_
t (D (D Fecal Coliform Test
mL Sample
0.001
0.0001
0.00001
0.000001
0.0000001
0.00000001
MPN
24 hours
-
-
-
t
I
I -
I -
.a
MPN Fecal Coliform/g =
10 x MPN index / 100 ml
largest volume X % dry solids tested
Sterility Control
Quality Control Tubes
10 mL
Double Strength (DS) Control
Single Strength (SS) Control
YUiS
EC Broth Control
Revised 5-23-16; 414/22
MPN/g = 10x a.
6.001 x; -
ao
0, 00 T

NAME
Sampled By:
Received By:,�
Analyzed
Calculated By: t
Checked By:)�
it
FECAL COLIFORM TEST
Standard Methods 9221 E-2014 (MPN) (Biosolids)
Permit #: WQ001026
DATE / TIME
41Xfsja-3 lll�
L r33yu `i-
�p-18�3
��� ..+�
-ass �3 -T1
Sample Location: Sludge # a
Sample Type: Grab X Composite
Preservation: None Cooled to 40C
24 hr. Check Ljjlg'gL3 3He �j ,,` 1 "
48 hr. Check %41 ap��3 )��jk , aAc pj�
72 hr. Check i 1.-�% l�-3 , 13S , OA,Lj'
q n Pracumntiva Tact 77)
Top Shelf: , 8' °C
Bottom Shelf: 35. C) °C
Water Bath: `-t' It> °C
) 3b
mL Sample
0.001
0.0001
0.00001
0.000001
0.0000001
6.00000001
MPN
24 hours
t
k
t
�
�
A
�
A
a
-
-
-
-
-
T
-
-
48 hours
-
-
-
-
-
-
_
_
13(�
r--, [-1) Fecal Coliform Test
mL Sample
0.001
0.0001
0.00001
0.000001
0.0000001
0.00000001
MPN
24 hours
-
k
}
-
-
-
-
MPN Fecal Coliform/g =
10 x MPN index / 100 ml
largest volume X % dry solids tested
Sterilitv Control
Quality Control Tubes
10 mL
Double Strength (DS) Control
Single Strength (SS) Control
wsij
EC Broth Control
Revised 5-23-16; 4/4/22
MPN/g = 10x -4. K _
0,oa 1 )< S—

NAME
Sampled By:lC�
Received By:
Analyzed By:.a.,l,;, f')
Calculated By:
Checked By
FECAL COLIFORM TEST
Standard Methods 9221 E-2014 (MPN) (Biosolids)
Permit #: WQ001026
DATE ! TIME
Sample Location: Sludge # ` j Top Shelf: 3-1. $ °C
Sample Type: Grab X Composite Bottom Shelf: 35.d °C
Preservation: None Cooled to 40C Water Bath: 14+6 °C
24 hr. Check �ltu�a3 11355s./
48 hr. Check
72 hr. Check 13S0
9 A I Presumptive Test O
af-
mL Sample
0.001
0.0001
0.00001
0.000001
0.0000001
0.00000001
MPN
24 hours
-
t
+
1
-
A
L-
-
-
1 -
-
-
-
-
-
-
48 hours
k
-
}
-
-
-
-
+
-
_
-
-
�40
VA,41l5l t�
C? D Fecal Coliform Test
mL Sample J
0.001
0.0001
0.00001
0.000001
0.0000001
0.00000001
MPN
24 hours
-
-
-
_-I.g
MPN Fecal Coliform/g =
10 x MPN index / 100 ml
largest volume X % dry solids tested
Sterilitv Control
Quality Control Tubes
10 mL
Double Strength (DS) Control
U�£.
Single Strength (SS) Control
}
EC Broth Control
-
Revised 5-23-16; 4/4122
MPN/g = 10x I , Y
0,001 x 5-
I
C,oo57-

NAME
Sampled By:1�
Received By: ,,£_ jLOD-„:�-
Analyzed By:,„1
Calculated By:
Checked By:
21
FECAL COLIFORM TEST
Standard Methods 9221 E-2014 (MPN) (Biosolids)
Permit #: WQ001026
DATE / TIME
Sample Location: Sludge # 9
Sample Type: Grab X Composite
Preservation: None Cooled to 4°C 'Q
24 hr. Check Allglz�L3
48 hr. Check yjZooja-3
72 hr. Check %t
!� C�nm�mn4ivn Tec4 7l
Top Shelf: . $ °C
Bottom Shelf: W- 0 °C
Water Bath: Ltq-S °C
/1 1
mL Sample
0.001
0.0001
0.00001
0.000001
0.0000001
0.00000001
MPN
24 hours
48 hours
1
-
-
_
_
-
-
_
_
-
_
-
-
-
-
_
_
_
V D a Fecal Coliform Test
mL Sample
0.001
0.0001
0.00001
0.000001
0.0000001
0.00000001
MPN
24 hours
-
-I
-
-
MPN Fecal Coliform/g = 10 x MPN index / 100 ml
largest volume X % dry solids tested
Sterilitv Control
Quality Control Tubes
10 mL
Double Strength (DS) Control
Single Strength (SS) Control
EC Broth Control
Revised 5-23-16; 4/4/22
MPN/g = 10x 11 g =
�Si7o rnN���
D.oal

NAME
Sampled By: 1,1�1C�.
Received By: t-t"ff
Analyzed
Calculated By:
Checked By: I,
I
FECAL COLIFORM TEST
Standard Methods 9221 E-2014 (MPN) (Biosolids)
Permit #: WQ001026
DATE / TIME
libala,3 t V3,1
�t-
�yw,t-,$�3
Sample Location: Sludge #j Top Shelf: $ °C
Sample Type: Grab X Composite Bottom Shelf: 35.0 °C
Preservation: None Cooled to 4°C V— Water Bath:gg.s °C
24 hr. Check
48 hr. Check yjaoja-3i
72 hr. Check 1-,-3 f (350 { Il( hv/
I Pracumntiva Tact r)
mL Sample
0.001
0.0001
0.00001
0.000001
0.0000001
0.00000001
11MPN
24 hours
48 hours
c7 Fecal Coliform Test
mL Sample 0.001 0.0001 0.00001 0.000001 0.0000001 0.00000001 MPN
24 hours I I— 0
MPN Fecal Coliform/g = 10 x MPN index / 100 ml
largest volume X % dry solids tested
Sterilitv Control
Quality Control Tubes
10 mL
Double Strength (DS) Control
Single Strength (SS) Control
}
EC Broth Control
.
Revised 5-23-16; 4/4122
MPN/g = 10x oZ . O =
0, ao 1 Y- A�
o`Z O
500O rn ? v je&-
o, 06f

Sampled
NAME
fall->_,�-
By:
Received By:
241t (l-a t�}61-yam
Analyzed By:,(
jl ;l
Calculated By:
Checked B .
i
FECAL COLIFORM TEST
Standard Methods 9221 E-2014 (MPN) (Biosolids)
Permit #: W0001026
DATE / TIME
2-6612,3 11 '�5
Sample Location: Sludge # to
Sample Type: Grab X Composite
Preservation: None Cooled to 4°C
24 hr. Check LAIjgjg 3 i35fS_ may/
48 hr. Check
72 hr. Check�3��y3
D h Promimnflua Tacf (7
Top Shelf: . g' °C
Bottom Shelf: 35.0 °C
Water Bath: L+q-S °C
as
mL Sample
0.001
0.0001
0.00001
0.000001
0.0000001
0.00000001
MPN
24 hours
A
-
>
y
-
-
-
-
-
-
-
-
_
_
48 hours
-
}
-
-
_
_
_
_
_
Id
I
I
I
I ,, T, Fecal Coliform Test
mL Sample
0.001
1 0.0001
1 0.00001
0.000001
0.0000001
0.00000001
MPN
24 hours
t
-I
-
-
I
I
I -
I
I
I
I
I
I
I
I
I
I
I
1C9.0
MPN Fecal Coliform/g =
10 x MPN index / 100 ml
largest volume X % dry solids tested
Sterility Control
Quality Control Tubes
10 mL
Double Strength (DS) Control
b VLi
Single Strength (SS) Control
EC Broth Controls
U�
Revised 5-23-16; 414122
MPN/g = 10x A, O
C,,Do1 x
5000 ra PN/a

FECAL COLIFORM TEST
Standard Methods 9221 E-2014 (MPN) (Biosolids)
Permit #: W0001026
NAME DATE I TIME
Sampled By: � !`�� P 41t&13,3 ( 1 �D Sample Location: Sludge # -7 Top Shelf: $' °C
Received By: ,� �tJ6Yy� Li 116 1.-)-3 11 `fi � Sample Type: Grab X Composite Bottom Shelf: '5.0 °C
Analyzed By: � � k � � 3 L441P,. ,,t-I$.13 [�i)"� Preservation: None Cooled to 40C � Water Bath: 14q• 5 °C
Calculated By:4
Checked By: ! c (tagf 3 [,)A 24 hr. Check ��1a1�3 1 35
48 hr. Check
72 hr. Check �rl►��.3 I `r > 1(,EJ�/Spv�
(7 Pracmn4ivn Toct (� '2?
mL Sample
0.001
0.0001
0,00001
0.000001
0.0000001
0.00000001
MPN
24 hours-
48 hours
a
.t-
-
k
LL
...i w�i1lL�3
n Fecal Coliform Test
mL Sample
0.001
0.0001
0.00001
0.000001
0.0000001
0.00000001
MPN
24 hours
MPN Fecal Coliform/g = 10 x MPN index / 100 ml
largest volume X % dry solids tested
Sterilitv Control
Quality Control Tubes
10 mL
Double Strength (DS) Control
KA-
Single Strength (SS) Controls
EC Broth Control
Revised 5-23-16; 4/4/22
MPN/g = 10x J , 1 _
D, oo I >,-, if
/ 1� q 5-b0 IMPAII
�

Sampled By: f&"-L � w
Received By: n-
Analyzed By:
Calculated By: ,In
Checked By:
City of Washington
Sludge
Standard Methods 2540 G-2015 (Aqueous)
Permit #: WQ001026
Time on H2O bath
Drying Oven Temp (in)
Time in Oven
Drying Oven Temp (out)
Time Out of Oven
�'f feig
Time Weighed
1st
2nd
4
C
e
^n
Sample
Blank
Sludge #
Duplicate
Evaporating Dish #
(J
Wet Weight + Dish Weight
Dish Weight
4
q O Co 9
Wet Weight
3 v
1 st Dry Weight + Dish Weight
$ a S 3,
' cc)
7 0 5-
2nd Dry Weight + Dish Weight
;
L 600 , 3
a 5 0 <6 .
Difference
1 st & 2nd Dry Weight + Dish Weight
(2nd-1st)
D, I
b. 3
0.1
Dry Weight
(2nd Dry Wt + Dish Wt - Dish Wt)
/;
/
14 l U
% Dry Solids [(Dry Wt/Wet Wt) x 100))
�{, t _ % -;
- 5 I
*Note -Differences should agree within 4% or 0.5 mg, which ever is less Revised: 9/26/19 JDW; 4/6/22 RWB

Sampled By: /� 1 �
Received By: a `
Analyzed By: '
Calculated By: ,
Checked By c \JLIIW ice_
City of Washington
Sludge
Standard Methods 2540 G-2015 (Aqueous)
Permit #: W0001026
Time on H2O bath
Drying Oven Temp (in)
3 ` Time in Oven
LI aO -.� 3, 13,1 1 Drying Oven Temp (out)
Time Out of Oven
(q/1))
Time Weighed
1st
2nd
01/
D .
D 9`
�s
Sample
Blank
Sludge # a
Duplicate
Evaporating Dish #
Wet Weight + Dish Weight
/ 0 0 13 r
Dish Weight
�� 3 • f
c — 6
Wet Weight
3 ©/
1 st Dry Weight + Dish Weight
2nd Dry Weight + Dish Weight
a2 S "
C
Difference
1 st & 2nd Dry Weight + Dish Weight
(2nd-1st)
i'
p
Dry Weight
(2nd Dry Wt + Dish Wt - Dish Wt)
- t'
% Dry Solids [(D Wt/Wet Wt) x 100)]
y , - !_
*Note -Differences should agree within 4% or 0.5 mg, which ever is less Revised: 9/26/19 JDW; 4/6/22 RWB

Sampled By: !-w
Received
Analyzed By: ��K,Jg, ,� J,,
Calculated By:C
Checked By
City of Washington
Sludge
Standard Methods 2540 G-2015 (Aqueous)
Permit #: W0001026
s hrl a3 I l
y-ao -_;3 . / I/3_
Time on H2O bath
Drying Oven Temp (in)
Time in Oven
Drying Oven Temp (out)
Time Out of Oven
Time Weighed
1 st
2nd
Ct�aD
e
G `f
3
10.14
l l s9
Sample
Blank
Sludge # 3
Duplicate
Evaporating Dish #
F?
3 t3
Wet Weight + Dish Weight
J /. - S o
Dish Weight
-
L+ S
Wet Weight
o 2 O 4,
1 st Dry Weight + Dish Weight
- 3 ,"
g O 7,
2nd Dry Weight + Dish Weight
g3, 4
g g p 7,
Difference
1 st & 2nd Dry Weight + Dish Weight
(2nd-1st)
0.
Dry Weight
(2nd Dry Wt + Dish Wt - Dish Wt)
3
'
% Dry Solids [(Dry Wt/Wet Wt) x 100
*Note -Differences should agree within 4% or 0.5 mg, which ever is less Revised: 9/26/19 JDW; 4/6/22 RWB

Sampled By: /•�
ReceivedAnalyzed By:
By: i
Calculated By: �; Y
Checked By:
City of Washington
Sludge
Standard Methods 2540 G-2015 (Aqueous)
Permit #: W0001026
24 Time on H2O bath
y I�srja3 1 1'1 3 Drying Oven Temp (in)
Time in Oven
-moo � _ / y 31 -1 Drying Oven Temp (out)
W:H\aa I'Mcl Time Out of Oven
Time Weighed
1st
2nd
D `
00-)
O"
I ' 1
(^�
Sample
Blank
Sludge # J4
Duplicate
Evaporating Dish #
J
Wet Weight + Dish Weight
Dish Weight
L, 9 I C'
Wet Weight
S Do a -a -
1st Dry Weight + Dish Weight
r, " a s' -
t) a-© Z.
2nd Dry Weight + Dish Weight
0 is D 3 , O
Difference
1 st & 2nd Dry Weight + Dish Weight
(2nd-1 st)
0.3
Dry Weight
(2nd Dry Wt + Dish Wt - Dish Wt)
/ ' ,
% Dry Solids [(Dry Wt/Wet Wt) x 100)]
3 _ -- '
*Note -Differences should agree within 4% or 0.5 mg, which ever is less Revised: 9/26/19 JDW; 4/6/22 RWB

Sampled By: �w
Received By:L L .1 UJa
Analyzed By:
Calculated By: „._ t,
Checked By:r ,L j kL C�1�
City of Washington
Sludge
Standard Methods 2540 G-2015 (Aqueous)
Permit* W0001026
,Alllk�a3 , 14 Time on H2O bath
((q1, ,,
y 11 Srj a3 i i '-1 3 Drying riven emp (in)
Time in Oven
2u I Drying Oven Temp (out)
{�yl 1Z3 I Time Out of Over
Time Weighed
1 st
2nd
1,/a
O
l03
e,?.`
0�
I IC) 3
Sample
Blank
Sludge # ty
Duplicate
Evaporating Dish #
0
Wet Weight + Dish Weight
Dish Weight
Wet Weight
a O $
1 st Dry Weight + Dish Weight
8 = 3
p -t I ,
2nd Dry Weight + Dish Weic ht
- 7
g Ll (,
Difference
1 st & 2nd Dry Weight + Dish Weight
(2nd-1 st)
r
p
Dry Weight
(2nd Dry Wt + Dish Wt - Dish Wt)
% Dry Solids ((Dry Wt/Wet Wt) x 100)
3, R
*Note -Differences should agree within 4% or 0.5 mg, which ever is less Revised: 9/26/19 JDW; 4/6/22 RWB

Sampled By:
Received By:6&r (}L,0YLy
Analyzed By:, _ . f
Calculated By:
Checked By:+_ -
City of Washington
Sludge
Standard Methods 2540 G-2015 (Aqueous)
Permit #: W0001026
Time on HH� bath
`r �1i31 3 i I `i 3 Drying Oven Temp (in)
Time in Oven
L1 -moo _ -� ; / y �- ( Drying Oven Temp (out)
1
LJ13t1a3 135 I Time Out of Over
Time Weighed
1 st
2nd
,, a
l03°
`bra°� 63"
�.
/ o _
°f �
/3
Sample
Blank
Sludge # (�
Duplicate
Evaporating Dish #
Wet Weight + Dish Weight
! o aJ4 O 2� C�
Dish Weight
Wet Weight
3 0 0 .�g c7 , S
1 st Dry Weight + Dish Weight
Q S . '7
3 S 7 3 ,
2nd Dry Weight + Dish Weight
7 a -3 .
73577 3 ,
Difference
1 st & 2nd Dry Weight + Dish Weight
(2nd-1st)
Dry Weight
(2nd Dry Wt + Dish Wt - Dish Wt)
3
i a `t 5 ��
% Dry Solids [(Dry Wt/Wet Wt) x 100)]
,71cy 50
*Note-Differences should agree within 4% or 0.5 mg, which ever is less Revised: 9/26/19 JDW; 4/6/22 RWB

Sampled By: /�-
Received
Analyzed By: -
Calculated By: ,,,.
Checked By: 1 " _�-
City of Washington
Sludge
Standard Methods 2540 G-2015 (Aqueous)
Permit #: WQ001026
-Al, gla3 Time on H2O bath
Drying D in i �aOven Temp p (in)
i l l 3
;,4 40 Time in Oven
y q ,' Drying Oven Temp (out)
yi�th3 135�— Time Out of Over
Time Weighed
1 st
2nd
4
�i.,o
iao3
q
io
V
-1
i3lo
vy4
I F
1i59
Sample
Blank
Sludge # -�
Duplicate
Evaporating Dish #
T_11
7
Wet Weight + Dish Weight
/ D j S - 9. 3
Dish Weight
S �- ° ,
Wet Weight
3 00 1` j. Q
1st Dry Weight + Dish Weight
S � 3 ,
2 - j
2nd Dry Weight + Dish Weight
$ S 3,
q
Difference
1 st & 2nd Dry Weight + Dish Weight
(2nd-1st)
Dry Weight
(2nd Dry Wt + Dish Wt - Dish Wt)
% Dry Solids [(Dry Wt/Wet Wt) x 100)]
*Note -Differences should agree within 4% or 0.5 mg, which ever is less Revised: 9/26/19 JDW; 4/6/22 RWB

January 2023 Average
AVG.
2023 Average
R.S. 1 & 2
R.S. 3
R.S. 4
76.50%
78.04%
1 75.91%
76.82%
4/20/23 Sample
VS in 0.7383
February 2023 Average
VS out 0.403
R.S. 1 & 21
R.S. 3
R.S. 4
VSFR= 76.07
75.89%
1 76.14%
1 76.49%
76.17%
4/25/23 Sample
March 2023 Average
VS in 0.7383
R.S. 1 & 21
R.S. 3
R.S. 4
VS out 0.565
76.07%
1 76.11%
1 75.08%
75.75%
VSFR= 53.96
10/25/23 Sample
April 2023 Average
R.S. 1 & 2
R.S. 3
R.S. 4
VS in 0.7383
75.07%
74.80%
1 74.31%
74.73%
VS out 0.613
VSFR= 43.85
May 2023 Average
R.S. 1 & 21
R.S. 3
R.S. 4
11/8/23 Sample
72.43%
1 76.69%
1 71.81%
73.64%
VS in 0.7383
VS out 0.603
June 2023 Average
VSFR= 46.16
R.S. 1 & 21
R.S. 3
R.S. 4
74.10%
1 75.41%
1 70.55%
73.35%
July 2023 Average
R.S. 1 & 21 R.S. 3 R.S. 4
73.00% 1 75.50% 1 68.49% 72.33%
August 2023 Average
R.S. 1 & 21 R.S. 3 R.S. 4
70.12% 1 74.08% 68.13% 70.78%
September 2023 Average
R.S. 1 & 2 R.S. 3 R.S. 4
70.44% 76.30% 1 66.87% 71.20%
October 2023 Average
R.S. 1 & 2 R.S. 3 R.S. 4
72.62% 71.92% 1 69.32% 71.29%
November 2023 Average
R.S. 1 & 2 R.S. 3 R.S. 4
73.53% 74.84% 1 70.81% 73.06%
December 2023 Average
R.S. 1 & 2 R.S. 3 R.S. 4
75.15% 80.94% 1 74.40% 76.83%
73.83%

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Washington WQ Permit Number: WQ0001026
WWTP Name: Washington WWTP
Monitoring Period: From 11/28/2023 To
NPDES Number: NCO020648
11/28/2023
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. A (time/temp) ❑
Alt B (Alk Treatment) ❑
Alt. C (Prior Testing) ❑
Alt.D (No Prior Test) ❑
1 Process to Further Reduce Pathogengs ❑
If applicable to alternative
performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost 0
Heat Drying 0
Heat Treatment 0
Thermophilic 0
Beta Ray 0
Gamma Ray 0
Pasteurization 0
Class B:
JAIL (1) Fecal Density ®
Alt. (2) Process to Significantly Reduce Pathogens ❑
If applicable to alternative
performed (Class
B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization ❑
1 Air Drying ❑
Composting ❑
Aerobic Digestion ❑
Anaerobic Digestion ❑
If applicable to alternative performed (Class A or Ch 2021
Parameter
Allowable Level
in Sludge
Pathogen Density
g y
Number o
Excee-
dences
Frequency
of Analysis
Sample
Type
Analytical
Tech -pique
Minimum
Geo. Mean
Maximum
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
3600
4515
9000
MPN/g
0
Quarterly
G
SM92210E
CFu
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per 4 grams
total solid (dry
weight)
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed:
Alt.1 (VS reduction) ®
Alt. 2 (40-day bench) 0
Alt. 3 (30-day bench) ❑
Alt. 4 (Spec. OZ uptake) ❑
Alt. 5 (14-Day Aerobic) ❑
Alt. 6 (Alk. Stabilization ❑
Alt 7 (Drying - Stable) ❑
Alt. 8 (Drying - Unstable) ❑
Alt. 9 (Injection) ❑
Alt. 10 (Incorporation) ❑
No vector attraction reduction alternatives were performed ❑
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if
you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Lonnie Woolard - NPDES ORC
Brent Collins; Director of Technical Services
Preparer Name and Title (type or print) Land Applier Name and Title (if applicable)(type or print)
Loiml� PyooG i 02/06/2z
Lonnie Woolard (Feb 6, 202414:28 EST) 4. --
/�/J►�
�- 2/5/2024
Signature of Preparer* Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 02T (12/2006)

Date: 11 /28/2023
Location #
1
2
3
4
5
6
7
Summary Sheet
Fecal Coliforms
Pathogen Reduction
MPN/g
9000
3600
3600
4500
3600
4500
4500
Log
3.9542
3.5563
3.5563
3.6532
3.5563
3.6532
3.6532
4515
Geometric Means/g
Total Dry Solids
Pykic
Sign ture

NAME
Sampled By:
Received By: uq, ' mryKy,Jp
Analyzed By: p9WAI-eQUK) A- ---
Calculated By:
Checked By:�
FECAL COLIFORM TEST
Standard Methods 9221 E-2014 (MPN) (Biosolids)
Permit #: W0001026
DATE I TIME
t0(Z3I��� ) oo 1
l0l2,�)l1b
l ola3 j �3 I I l�
Sample Location: Sludge # ` Top Shelf: ,� °C
Sample Type: Grab X Composite Bottom Shelf: 1�j,Q °C
Preservation: None Cooled to 40C Water Bath: 445 °C
24 hr. Check W 1 Z41)b
48 hr. Check
T2 hr. Check l011(p �J)D )I D5 ii?-3
Presum tive Test
mL Sample 0.001 El 0.0001 0.00001 0.000001 0.0000001 0.00000001 MPN
24 hours -+ — - — —
48 hours I + I I I jj� I J— I "-ct
Fecal Coliform Test
mL Sample
1 0.001
0.0001 0.00001
0.000001
0.0000001
0.00000001
MPN
24 hours
I -Ir
I —
_
,
MPN Fecal Coliformlg =
10 x MPN index 1100 ml
largest volume X % dry solids tested
5terility Control
Quality Control Tubes 10 mL
Double Strength DS Control Ne rt
Sin le Strength SS Control Ake q Q ` A
EC Broth Control '
Revised 5-23-16; 4l4J22
MPNIg = 10x L
b.00 1 X 5-"1.

NAME
Sampled By:
Received By: ' 'tom, ' M1Y1t7�e
Analyzed By: �j exuj P1-ti—
Calculated By:
Checked By. TLC,
FECAL COLIFORM TEST
Standard Methods 9221 E-2014 (MPN) (Biosolids)
Permit #: W0001026
DATE / TIME
io1Z31)z , )ouI
loixbllb 10�0
i 1-'4-a3 13 J::8L
Sample Location: Sludge # l Top Shelf: M,q °C
Sample Type: Grab X Composite Bottom Shelf: i�j,Q °C
Preservation: None Cooled to 40C Water Bath: 445 °C
24 hr. Check 10111ZJ of ,
48 hr. Check �0I z5i 111'
72 hr. Check�0
N
Presum tive Test
mL Sample 0.001 0.0001 0.00001 0.000001 0.0000001 0.00000001 MPN
24 hours + --t - - - I - - I - - -
48 hours - - -
t v Z' Fecal Coliform Test
mL Sample
0.001
0.0001
0.00001
0.000001
0.0000001
0.00000001
MPN
24 hours
-
i-
-
-
-
MPN Fecal Coliformlg =
10 x MPN index / 100 ml
largest volume X % dry solids tested
Sterilitv Control
Quality Control Tubes
10 mL
Double Strength DS Control
Single Strength SS Control
� a ` v�
EC Broth Control
' Ve
J
Revised 5-23-16; 4l4/22
MPN/g = 10x r) , 0 =
® .0 0
1 1 /

FECAL COLIFORM TEST
Standard Methods 9221 E-2014 (MPN) (Biosolids)
Permit #: WQ001026
NAME
DATE / TIME
Sampled By:
b07
Sample Location: Sludge # 01�
Top Shelf: ,q °C
Received By:
/1AU i MMOA
W i lb hb , 10�0
Sample Type: Grab X Composite
Bottom Shelf: 1�j ,Q °C
Analyzed By:
A ^-� Q W r� -L--
WA
1 D��.3 �a3 �I 13�
Preservation: None Cooled to 4°C x
Water Bath: 445 °C
Calculated By:
Checked By:
�y---
l���j��
24 hr. Check I 1 at
48 hr. Check IO l i5 i 1, o 4 a-
72 hr. Check 10 jJU J1,�jT rz.l3
S
a Presum
tive Test
3
mL Sample
0.001
0.0001
0.00001
0.000001
0.0000001
0.00000001
MPN
24 hours
-
-
-
-
-
- -- -
-
-
-
-
-
-
-
-
-
48 hours
--
-
-
-
Fecal Coliform Test
mL Sample
0.001
0.0001
0.00001
0.000001 0.0000001
0.00000001
MPN
24 hours
-
-
-
-
I
I-
I
I
I
I
I
I
I
I
z-1. f<
MPN Fecal Coliformlg = 10 x MPN index / 100 ml
largest volume X % dry solids tested
Sterility Control
Quality Control Tubes
10 mL
Double Strength DS Control
Single Strength SS Control
1,Ae g a ` , vw-
EC Broth Control
'
J
Revised 5-23-16; 414/22
MPN/g = 10x co Y,40
j/�
0 ,00 1 x © rC)©5

NAME
Sampled By: `
Received By:1v�., Irry10�o
Analyzed By: ptA.eQW 1�
Calculated By:
Checked By: ,
FECAL COLIFORM TEST
Standard Methods 9221 E-2014 (MPN) (Biosolids)
Permit #: WQ001026
DATE / TIME
10113112, ) WO
,o/11J—� 1135
i l-• I -.a 3 / 3 7,1
1314 2,-3 150
Sample Location: Sludge # I
';
Sample Type: Grab X Composite
Preservation: None Cooled to 4°C x
24 hr. Check 10 � I � I13 , ►'I aI £s
48 hr. Check 10 j Z5 j 1�
72 hr. Check 10 I� 11,�j 110�
I Presumptive Test
Top Shelf: ,q °C
Bottom Shelf: °C
Water Bath: 445 °C
q(6
mL Sample
0.001
0.0001
0.00001
0.000001
0.0000001
0.00000001
MPN
24 hours
-
-
—
—
-
, 1
48 hours
'E[
]—�—I--
r
-
-
r
v n Fecal Coliform Test
mL Sample
0.001
0.0001
0.00001
0.000001
0.0000001
0.00000001
MPN
24 hours
—
I
MPN Fecal Coliform/g =
10 x MPN index 1100 ml
largest volume X % dry solids tested
Sterility Control
Quality Control Tubes 10 mL
Double Strength DS Control f
Single Strength SS ` Control AAe a r�
EC Broth Control A%r n11`1 ,W
Revised 5-23-16; 4/4/22
MPN/g = 10x
oo mp���'

NAME
Sampled By: `
Received By: rwuA
Analyzed By: OLLAA.& W r)-'--
Calculated By: z. J
Checked By: L
C
FECAL COLIFORM TEST
Standard Methods 9221 E-2014 (MPN) (Biosolids)
Permit #: W0001026
DATE I TIME
IoIZ31iz� , t 01,;L-
tOlZ31lb , MO
l 0101T1 \ 5d
t"'�;L--5 l i
Sample Location: Sludge #
Sample Type: Grab X Composite
Preservation: None Cooled to 40C
24 hr. Check is 0 IL3 h `1 4?"3-
48 hr. Check
72 hr. Check l0 �� ��,�j ) l O-7 . ?-Z5
Top Shelf: � ,q °C
Bottom Shelf: i f j ,Q °C
Water Bath: q4 ,S °C
14
.0 Presum tive Test '
mL Sample 0.001 0.0001 0.00001 0.000001 0.0000001 0.00000001 []MPN
24 hours �' — — — — �^' — — — — — — — —
48 hours f' i- — — _1-1
J Fecal Coliform Test
mL Sample
0.001
0.0001
0.00001
0.000001
0.0000001
0.00000001
MPN
24 hours
—
—
—
1
1-1q-
MPN Fecal Coliform/g =
10 x MPN index / 100 ml
largest volume X % dry solids tested
Sterilitv Control
Quality Control Tubes
10 mL
Double Strength DS Control
.e
Single Strength SS Control
AAf a ' ►�
EC Broth Control
&tf ir Q_ ,
J
Revised 5-23-16: 4/4I22
MPN/g = 10x I, S = J � : t Soo rmPA)h
D.Oot X 4%, 0,00LL

FECAL COLIFORM TEST
Standard Methods 9221 E-2014 (MPN) (Biosolids)
Permit #: W0001026
NAME
DATE ! TIME
Sampled By:
/
kotnI1,-�
1 D15
Received By: r
V Q, ' tj\MUA p
W i 13 i1:b
io�o
Analyzed By:
pPtA.a_QW r1-,--
10��3��3r
I50
Calculated By: `
is - -As
13, $'
Checked By:
c
Sample Location: Sludge # 5
Sample Type: Grab X Composite
Preservation: None Cooled to 40C x
24hr.Check ioUlAbol`l` 'm
48 hr. Check 14 l LS 110k,
72 hr. Check
Top Shelf: °C
Bottom Shelf: 7j,Q °C
Water Bath: 445 J °C
2 Z,
-� d P sumptive Test " �J
mL Sample 0.001 0.0001 0.00001 0.000001 0.0000001 0.00000001 MPN
24 hours — — — — — — — — — — — — —
48 hours — — — — —
0 L--) 0 Fecal Coliform Test
mL Sample 0.001 0.0001 0.00001 0.000001 0.0000001
24 hours — 1
MPN Fecal Coliformlg = 10 x MPN index / 100 ml MPNIg = 10x ( , % _
largest volume X % dry solids tested
( X 5�a
Sterilitv Control
Quality Control Tubes 10 t
Double Strength DS Control x
Single Strength SS Control N-e a�
EC Broth Control a '
J
Revised 5-23-16; 4/4/22
0.00000001 MPN
6,005

NAME
Sampled By:
`
Received By:
Analyzed By:
pit Q W r-+
Calculated By:
Checked
r,
FECAL COLIFORM TEST
Standard Methods 9221 E-2014 (MPN) (Biosolids)
Permit #: W0001026
DATE / TIME
101Z'al1,� IOCXa
loltblib
INN L5i 1
-j b
Sample Location: Sludge # (,�,— Top Shelf: ,q °C
Sample Type: Grab X Composite Bottom Shelf: ij,Q °C
Preservation: None Cooled to 40C X Water Bath: °C
24hr.Check j0jj�jjbFlly`A,96
48 hr. Check W t Z5l �b 1 Iy . P-�%
72 hr. Check l0 IL(o I1,�j , 11 Off.
-n G
� ' - Presum tive Test " 1-1
mL Sample 0.001 0.0001 lI-0.[00001 0.000001 0.0000001 0.00000001 MPN
24 hours — — — — — -' — —
48 hours t- -— — — — - — / C
o O C Fecal Coliform Test
mL Sample 0.001
0.0001
0.00001 0.000001
0.0000001
0.00000001
MPN
24 hours
—
—
—
—
MPN Fecal Coliform/g = 10 x MPN index / 100 ml
largest volume X % dry solids tested
Sterility Control
Quality Control Tubes 10 mL
Double Strength DS Control -e �
;
Sin le Strength SS Control �f a ' ►�
EC Broth Control A)-r n2i;
Revised 5-23-16; 4/4/22
MPN/g = 10x
0,00 ( x 4 0,co,-

NAME
Sampled By:
`
Received By:
Analyzed By: �OJ,4A.
UW r- --
Calculated By:
Checked By: . Itfli
1,-�
FECAL COLIFORM TEST
Standard Methods 9221 E-2014 (MPN) (Biosolids)
Permit #: W0001026
DATE I TIME
OIt31j,-� I t>a3
toilbi b MO
►o�,� Ja3. I �.�i
ti�la�la 3 lei
Sample Location: Sludge # Top Shelf: ,q °C
Sample Type: Grab X Composite Bottom Shelf: i f j ,Q °C
Preservation: None Cooled to 4°C jL Water Bath: 445 °C
24 hr. Check i01 2 Ib I) N 14 ` ?-0)
48 hr. Check �0 Zia I , 11'�g i2�
72 hr. Check lO Il1,O JZ 109 ?t-3
2
-.D t - Presumptive Test J
mL Sample 0.001 0.0001 0.00001I+dI I
0.000001 0.0000001 0.00000001 MPN
24 hours T - - - - - - -I- - - - - 'I II -
48 hours - - - - -
4�1 C:D a Fecal Coliform Test
ml. Sample 0.001
0.0001
0.00001
0.000001
0.0000001
0.00000001 MPN
24 hours
-
-
I
G
MPN Fecal Coliformlg = 10 x MPN index / 100 ml
largest volume X % dry solids tested
Sterilitv Control
Quality Control Tubes
10 mL
Double Strength DS Control
f
Single Strength SS Control
Q ` ve-
EC Broth Control
A.4 aaJI've-
J
Revised 5-23-16; 4/4122
MPN1g = 10x
0,001 X

Sampled By: Zdk6y\4
Received By: mo)OVA
Analyzed By: �-Jtx�,
Calculated By: u m14mrnwA
Checked By:
City of Washington
Sludge
Standard Methods 2540 G-2015 (Aqueous)
Permit #: WQ001026
w I n I2 j 1001 Time on H2O bath
O INV) / o
Drying Oven Temp (in)
K*AVI5Iti3
Time in Oven
Drying Oven Temp (out;
Time Out of Over
Time Weighec
1 st
2nd
1 1 iV�
�o�
G
ii�OJ
i 10
lorbi
13►�1
�2bi
1�24
Sample
Blank
Sludge # 9
Duplicate
Evaporating Dish #
Wet Weight + Dish Weight
1
� q 1 '
Dish Weight
01 �7�'�`
�D�°�
U61 (Pgq'kP
Wet Weight
'
300 19
1stDry Weight + Dish Weight
2nd Dry Weight + Dish Weight
Difference
1 st & 2nd Dry Weight + Dish Weight
(2nd-1st)
`al - �• ..i (;0(3,�13
41
a,
-
Dry Weight
(2nd Dry Wt + Dish Wt - Dish Wt)
-V�J"l��p
% Dry Solids [(Dry Wt/Wet Wt) x 100
*Note -Differences should agree within 4% or 0.5 mg, which ever is less Revised: 9/26/19 JDW; 4/6/22 RWB

Sampled By: bc-Az
Received By: MMOVA
n*y;z te
Calculated By: Pt-dv_VjKt%- M wtiA
Checked By:
City of Washington
Sludge
Standard Methods 2540 G-2015 (Aqueous)
Permit #: WQ001026
1301 Time on H2O bath
i01�51L� iSol
3 7-1
Drying Oven Temp (in)
Time in Oven
Drying Oven Temp (out;
Time Out of Over
Time Weighec
1st
2nd
103
IUD
q3�
1aoc�
l04
1o51
�31�
Sample
Blank
Sludge #
Duplicate
Evaporating Dish #
b
Wet Weight + Dish Weight
t U`t:1
Dish Weight
3
�1 a5� a
1Aoa� .1
Wet Weight
1stDry Weight + Dish Weight
�1a5a.`b
15GJ�Pa,1
2nd Dry Weight + Dish Weight
�1 a 5 a • {
�5 `p ,
Difference
1st & 2nd Dry Weight + Dish Weight
2nd-1 st
Dry Weight
(2nd Dry Wt + Dish Wt - Dish Wt)
-
% Dry Solids D Wt/Wet Wt x 100
*Note -Differences should agree within 4% or 0.5 mg, which ever is less Revised: 9/26/19 JDW; 4/6/22 RWB

Sampled By:
Received By: "L MOOVA
Analyzed By: �mm "ffit�
Calculated By: VA6 ran61A
Checked By:
City of Washington
Sludge
Standard Methods 2540 G-2015 (Aqueous)
Permit #: WQ001026
l o i Q Time on H2O bath
I O Z M .
'((IJ
Drying Oven Temp (in)
Time in Oven
Drying Oven Temp (out)
Time Out of Ove
Time Weighed
1 st
2nd
�20
ion
l05
t 3�0
IZa�O
IZot
14'�
Sample
Blank
Sludge #
Duplicate
Evaporating Dish #
Wet Weight + Dish Weight
�� �� U •
Dish Weight
Wet Weight
;J�o1� •�
1 st Dry Weight + Dish Weight
U1 �`� �
b D� �� • Y�
2nd Dry Weight + Dish Weight,0
D o
Difference
1 st & 2nd Dry Weight + Dish Weight
(2nd-1 st)
".. q P�,oiau
> 0,
Dry Weight
(2nd Dry Wt + Dish Wt - Dish Wt)
- V ✓
1�0�4 •�
% Dry Solids [(Dry Wt/Wet Wt x 100)
"t0i L�)IL'b
*Note -Differences should agree within 4% or 0.5 mg, which ever is less dp .- �• ,
► 'J 10,1311b3
Revised: 9/26/19 JDW; 4/6/22 RWB

Sampled By:k,,,, J,, J w �
(- c.
� Received
BBy
Anv aly: _�ojto,r`►V�.�rAfr )ova
yzed By/
Calculated By:htXi►� MmOv�r
Checked By:
City of Washington
Sludge
Standard Methods 2540 G-2015 (Aqueous)
Permit* WQ001026
10174 Time on H2O bath
/0 31-9.3 Cali
Drying Oven Temp (in)
Time in Oven
Drying Oven Temp (out)
Time Out of Ove
Time Weighed
F11 st
2nd
at
lob
105
qb3 p
aup
104
i�L04
Sample
Blank
Sludge # 4
Duplicate
Evaporating Dish #
1)
U V
Wet Weight + Dish Weight
"l q cico
V1
Dish Weight
01 �l5
V b
Wet Weight
b00%4 • a
�1 p
��� Ao
1stDry Weight + Dish Weight
iGNI°W
2nd Dry Weight + Dish Weight
Difference
V )91,1 ta�ta �1>b
n
1 st & 2nd Dry Weight + Dish Weight
- 0 J
(2nd-1 st
Dry Weight
}, 0
(2nd Dry Wt + Dish Wt - Dish Wt)
J
% Dry Solids D Wt/Wet Wt) x 100
*Note -Differences should agree within 4% or 0.5 mg, which ever is less Revised: 9/26/19 JDW; 4/6/22 RWB

Sampled By: - i l.L-Lk
Received By: . M OVA
Analyzed By: fwf,hW,%. MM0430)
Calculated By:�12hh1Qi?fjld�mpUl�j�
Checked By:
City of Washington
Sludge
Standard Methods 2540 G-2015 (Aqueous)
r�
Permit #: WQ001026
j O Z i2 1015 Time on H2O bath
1011? III-) . I & ,.� n
IOi14I213, 115Z
wiz�,n r 95
10-31-a3, 1240
Drying Oven Temp (in)
Time in Oven
Drying Oven Temp (out
Time Out of Ove
Time Weighed
1 st
2nd
106
104
105
I05
110(^5�
IGLcv
1 G�'"I
114G
1h01
Sample
Blank
Sludge #
Duplicate
Evaporating Dish #
A
Wet Weight + Dish Weight
qq ryt D I.5
Dish Weight
0
u "I 15 a •�
Wet Weight
b0 � XO
1 st Dry Weight + Dish Weight
0 \0
105V •
2nd Dry Weight + Dish Weight
05#
��� • 'J
Difference
1 st & 2nd Dry Weight + Dish Weight
2nd-1 st)
G' I
0,
Dry Weight
(2nd Dry Wt +Dish Wt -Dish Wt)
V � %
% Dry Solids D Wt/Wet Wt x 100
4
*Note -Differences should agree within 4% or 0.5 mg, which ever is less Revised: 9/26/19 JDW; 4/6/22 RWB

Sampled By: w, -, i w`i� 7tic
Received By:
Analyzed By: V,p&ytQ,6111641 AIx)
Calculated By: ,M&hKI&lYllnlilVA
Checked By:A Y`r_�.—
City of Washington
Sludge
Standard Methods 2540 G-2015 (Aqueous)
Permit #: W0001026
l Z 12 l U Time on H2O bath
011? I t') , v
1612AIn: IC4�
10 Z5 IZ , 151A
fa°31-a3
Drying Oven Temp (in)
Time in Over
Drying Oven Temp (out;
Time Out of Over
Time Weighec
1 st
2nd
Baia
k1CA
LGI�10�0
CL5
Sample
Blank
Sludge # U
Duplicate
Evaporating Dish #
% " to -A
t
J
Ml© `
Wet Weight + Dish Weight
1 °
IV a I
Dish Weight
MOW 0
Wet Weight
°
1st Dry Weight+ Dish Weight
�
CI
2nd Dry Weight + Dish Weight
J� ��
Difference
1 st & 2nd Dry Weight + Dish Weight
`
0,0
2nd-1 st
Dry Weight
O
(2nd Dry Wt + Dish Wt - Dish Wt)
t
% Dry Solids D Wt/Wet Wt x
*Note -Differences should agree within 4% or 0.5 mg, which ever is less Revised: 9/26/19 JDW; 4/6/22 RWB

Sampled By: rjN U4,: }--_
Received By: (' m 0
Analyzed By:) �:(xt�YA 1ij'!Y'iCy16"A o
Calculated By: 1�Wyt &A1MQ9
Checked By:
City of Washington
Sludge
Standard Methods 2540 G-2015 (Aqueous)
Permit #: WQ001026
`(, � Time on H2O bath
10iZ�IZ� lOi�
Drying Oven Temp (in)
Time in Oven
Drying Oven Temp (out)
Time Out of Oven
Time Weighed
1 st
2nd
U "1
V7
q�i
i15h
G�
165
Zr7°i
`O��yt`P
Sample
Blank
Sludge #
Duplicate
Evaporating Dish #
Wet Weight + Dish Weight
"i q 1A.5
Dish Weight
o� J� `�
4 q 01LA 3
Wet Weight
1 st Dry Weight + Dish Weight
2nd Dry Weight + Dish Weight
4�5 • `i
1 Mike
Difference
1 st & 2nd Dry Weight + Dish Weight
2nd-1 st
Q
0,0
Dry Weight
(2nd Dry Wt + Dish Wt - Dish Wt)
`
% Dry Solids [(Dry Wt/Wet Wt x 100
�•��" 1'
*Note -Differences should agree within 4% or 0.5 mg, which ever is less Revised: 9/26/19 JDW; 4/6/22 RWB

January 2023 Average
AVG.
2023 Average
R.S. 1 & 2
R.S. 3
R.S. 4
76.50%
78.04%
1 75.91%
76.82%
4/20/23 Sample
VS in 0.7383
February 2023 Average
VS out 0.403
R.S. 1 & 21
R.S. 3
R.S. 4
VSFR= 76.07
75.89%
1 76.14%
1 76.49%
76.17%
4/25/23 Sample
March 2023 Average
VS in 0.7383
R.S. 1 & 21
R.S. 3
R.S. 4
VS out 0.565
76.07%
1 76.11%
1 75.08%
75.75%
VSFR= 53.96
10/25/23 Sample
April 2023 Average
R.S. 1 & 2
R.S. 3
R.S. 4
VS in 0.7383
75.07%
74.80%
1 74.31%
74.73%
VS out 0.613
VSFR= 43.85
May 2023 Average
R.S. 1 & 21
R.S. 3
R.S. 4
11/8/23 Sample
72.43%
1 76.69%
1 71.81%
73.64%
VS in 0.7383
VS out 0.603
June 2023 Average
VSFR= 46.16
R.S. 1 & 21
R.S. 3
R.S. 4
74.10%
1 75.41%
1 70.55%
73.35%
July 2023 Average
R.S. 1 & 21 R.S. 3 R.S. 4
73.00% 1 75.50% 1 68.49% 72.33%
August 2023 Average
R.S. 1 & 21 R.S. 3 R.S. 4
70.12% 1 74.08% 68.13% 70.78%
September 2023 Average
R.S. 1 & 2 R.S. 3 R.S. 4
70.44% 76.30% 1 66.87% 71.20%
October 2023 Average
R.S. 1 & 2 R.S. 3 R.S. 4
72.62% 71.92% 1 69.32% 71.29%
November 2023 Average
R.S. 1 & 2 R.S. 3 R.S. 4
73.53% 74.84% 1 70.81% 73.06%
December 2023 Average
R.S. 1 & 2 R.S. 3 R.S. 4
75.15% 80.94% 1 74.40% 76.83%
73.83%

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Washington WQ Permit Number: WQ0001026
WWTP Name: Washington WWTP
Monitoring Period: From 11/29/2023 To
NPDES Number: NCO020648
11/29/2023
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. A (time/temp) ❑
Alt B (Alk Treatment) ❑
Alt. C (Prior Testing) ❑
Alt.D (No Prior Test) ❑
1 Process to Further Reduce Pathogengs ❑
If applicable to alternative
performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost 0
Heat Drying 0
Heat Treatment 0
Thermophilic 0
Beta Ray 0
Gamma Ray 0
Pasteurization 0
Class B:
JAIL (1) Fecal Density ®
Alt. (2) Process to Significantly Reduce Pathogens ❑
If applicable to alternative
performed (Class
B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization ❑
1 Air Drying ❑
Composting ❑
Aerobic Digestion ❑
Anaerobic Digestion ❑
If applicable to alternative performed (Class A or Ch 2021
Parameter
Allowable Level
in Sludge
Pathogen Density
g y
Number o
Excee-
dences
Frequency
of Analysis
Sample
Type
Analytical
Tech -pique
Minimum
Geo. Mean
Maximum
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
3600
6728
19500
MPN/g
0
Quarterly
G
SM92210E
CFu
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per 4 grams
total solid (dry
weight)
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed:
Alt.1 (VS reduction) ®
Alt. 2 (40-day bench) 0
Alt. 3 (30-day bench) ❑
Alt. 4 (Spec. OZ uptake) ❑
Alt. 5 (14-Day Aerobic) ❑
Alt. 6 (Alk. Stabilization ❑
Alt 7 (Drying - Stable) ❑
Alt. 8 (Drying - Unstable) ❑
Alt. 9 (Injection) ❑
Alt. 10 (Incorporation) ❑
No vector attraction reduction alternatives were performed ❑
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if
you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Lonnie Woolard - NPDES ORC
Brent Collins; Director of Technical Services
Preparer Name and Title (type or print) Land Applier Name and Title (if applicable)(type or print)
Loiml� PyooG i 02/06/2z
Lonnie Woolard (Feb 6, 202414:28 EST) 4. --
/�/J►�
�- 2/5/2024
Signature of Preparer* Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 02T (12/2006)

Summary Sheet
Fecal Coliforms
Pathogen Reduction
Date: 11 /29/2023
Location #
MPN/g
1
3600
2
4500
3
19500
4
4500
5
19500
6
5000
7
4500
Log
3.5563
3.6532
4.2900
3.6532
4.2900
3.6990
3.6532
6728
Geometric Means/g
Total Dry Solids
n ture

NAME
Sampled By:
Received By: - MMO W%
Analyzed By: '�CaG'j U.)17. ---
Calculated By:
Checked By: tom..
5
FECAL COLIFORM TEST
Standard Methods 9221 E-2014 (MPN) (Biosolids)
Permit* W0001026
DATE / TIME
iol3i103 .CILAD
Sample Location: Sludge # 1 Top Shelf: 39. $' °C
Sample Type: Grab, X Composite Bottom Shelf: 3 °C
Preservation: None Cooled to 40C X Water Batr: .5 °C
24 hr. Check o ->1
48 hr. Check 1%�a1-:3
72 hr. Check 1 13j a3 , I K
Iv Dracumnfi is Tec4 O
mL Sample
0.001
0.0001
0.00001
0.000001 0.0000001
0.00000001
MPN
24 hours
-
—
—
—
—
48 hours
—
#►
_
r
_
?
4e'(ru
-& ,.isia3
_,­ .. • - c� Fecal Cofirorm rest t . s
mL Sample 0.001 0.0001 0.00001 = 0.000001 5.0000001 0.00000001
24 hours --
�l,
MPN Fecal Coliform/9 = 10 x MPN index / 100 ml
largest volume X % dry solids tested
Sterility Control
Control Tubes I 10 mL
Double Strength (DS) Control
Single Strength (SS) Control
EC Broth Control
Revised 5-23-16; 414122
MPN/g = 10x � , � _ � I C W -
1►•�`t`
0 0 0o

NAME
Sampled By:,
., k�L'' -
Received By:
Z�-) Mmo w%
Analyzed By:
at'd L)11 ,—
Calculated By:
9,ai.yl,. 17 G
Checked By:
FECAL COLIFORM TEST
Standard Methods 9221 E-2014 (MPN) (Biosolids)
Permit #: WQ001026
DATE / TIME
CJL}o
iol�il�3 � lbc� �
--
i
Sample Location: Sludge # I CI�,pI,Ca� Top Shelf: ,$' °C
Sample Type: Grab X Composite Bottom Shelf: 319 oC
Preservation: None Cooled to 40C ' Water Bath: `} y �� °C
24 hr. Check oli j'3 1'a\5 j
48 hr. Check Jz N
72 hr. Check
\ O Presumntive Test D
4- 8'
mL Sample
0.001
0.0001
0.00001
0.000001
0.0000001
0.00000001
MEN
24 hours
-�
.�
''�
_
;—
—
•'
_
r
--
—
—.
_
'_
48 hours
t_-;, f-1 r'7 Fecal Coliform Test
mL Sample
0.001
0.0001
0.00001
0.000001
0.0000001
0.00000001
24 hours
I
I—
G II I
MPN Fecal Coliform/g =
10 x MPN index / 100 ml
largest volume X % dry solids tested
Sterility Control
Quality Control Tubes
10 mL
Double Strength DS Control
itiCe :cLL-e—
Sin le Strength SS Control
OaLf-
EC Broth Control
\ Gt
Revised 5-23-16; 4/4/22
MPN/g = 10x 1, 9�
o .00 I x 5�
0 . C7OJ�

Sampled By:
Received By:
Analyzed By:
Calculated By:
Checked By:
NAME
c
FECAL COLIFORM TEST
Standard Methods 9221 E-2014 (MPN) (Biosolids)
Permit #: W0001026
DATE I TIME
iol3i103 , CJAJ6 Sample Location: Sludge #
101311 ,.),3 . l ao l Sample Type: Grab X Composite
j0�3i �a3 i l�� Preservation: None Cooled to 4°C 'X
11 24 hr. Check r���
48 hr. Check
72 hr. Check 1
Top Shelf: 3q. R, °C
Bottom Shelf: 3 °C
Water Batr: ,rj °C
O b Presum tive Test o C91-3
nL Sample 0.001 0.0001 0.00001 0.000001 0.0000001 0.00000001 MPS
24 hours -- - - -- - - - -
48 hours - - - - - - - -�
0 o d Fecal Coliform Test a i, &1
mL Sample
0.001
0.0001
0.00001
0.000001
0.0000001
0.00000001
MPN
24 hours
-I
-
MPN Fecal Coliformlg = 10 x MPN index / 100 ml
largest volume X % dry solids tested
Sterilitv Control
Quality Control Tubes
10 mL
Double Strength DS Control
w-e-
Single Strength SS Control
il�je
EC Broth Control
Revised 5-23-16; 414122
MPNIg = 10x I , �( _ , 12� _
0,00) ,l ! � 0 0 C� /
D `

NAME
Sampled By:
Received By:
Analyzed By:
Calculated By:
Checked By:
FECAL COLIFORM TEST
Standard Methods 9221 E-2014 (MPN) (Biosolids)
Permit #: W0001026
DATE I TIME
1013i1:)- . Cji�z/
ID131la3 , tUD1
10)311:113 1 1 l
Sample Location: Sludge # 3
Sample Type: Grab X Composite
Preservation: None Cooled to 40C
24 hr. Check
48 hr. Check i> >a J-,
72 hr. Check 1 A 1151
Top Shelf: 3q� W, °C
Bottom Shelf: 39.9 °C
Water Bath: Htl, 5 °C
7 ( ° Presum tive Test'D 35
mL Sample 0.001 0.0001 0.00001 0.000001 0.0000001 0.00000001 MPN
24 hours �j- -
48 hours - - - � -- - - - � �j 3
p 0 Fecal Coliform Test -71
mL Sample 0.001 1 0.0001 0.00001 0.000001 0.0000001 0.00000 001
24 hours - r ,
MPN Fecal Coliform/g = - _ 10 x MPN index / 100 ml
largest volume X % dry solids tested
Sterility Control
Quality Control Tubes
Double Strength DS Control
Single Strength SS Control
EC Broth Control
Revised 5-23-16; 4/4/22
10 mL
MPNIg = 10x 1.21 � - 7,� = J q7 �a O wtPNYa�
�,QO � � a Q,G?O�-

Sampled By:
Received By:
Analyzed By:
Calculated By:
Checked By:
NAME
FECAL COLIFORM TEST
Standard Methods 9221 E-2014 (MPN) (Biosolids)
Permit #: W0001026
DATE / TIME
Iol3iIQ3 a150
1013, luo l
I.1 _D.3 r 30
Sample Location: Sludge # 4 Top Shelf: 39-?, °C
Sample Type: Grab X Composite Bottom Shelf: 3 °C
Preservation: None Cooled to 40C X Water Bato: L i °C
24 hr. Check
48 hr. Check 1%
72 hr. Check 1 1 131wy (46 ,
Ll 1 o Prac,imn+iva Tac+ b
1'
mple
0.001
0.0001
0.00001
0.000001
0.0000001
0.00000001
MPN
ursurs
n
-(-
1
1
V O o Fecal Coliform Test C1.7
mL Sample 0.001 0.0001 0.00001 0.000001 0.0000001 0.00000001
24 hours — I I I I I I I I I I I_ r_
MPN Fecal Coliform/g = - 10 x MPN index / 100 ml
largest volume X % dry solids tested
Sterility Control
Quality Control Tubes 10 mL
Double Strength DS Control e
Single Strength SS ControllJ�
EC Broth Control
Revised 5-23-16; 414122
MPN/g = 10x _ % $� r 4500 m IolJ f �,
0,00l )< 0.Vo

NAME
Sampled By:
Received By:
Analyzed By:
Calculated By:
Checked By:
FECAL COLIFORM TEST
Standard Methods 9221 E-2014 (MPN) (Biosolids)
Permit #: WQ001026
DATE / TIME
i o l31 133 C6-02 Sample Location: Sludge_ #
10 13, 1�3 . )'mil Sample Type: Grab X Composite
ic0l b'3 )yA5 Preservation: None Cooled to 40C X
11\a$�2r3 1,55 24hr. Check `,'v3
48 hr. Check
72 hr. Check
0 Prpcumotiva Tact
Top Shelf: qq. T °C
Bottom Shelf: 3 °C
Water Batr: H 5 °C
mL Sample
0.001
0.0001
0.00001
0.000001
0.0000001
0.00000001
MPN
24 hours
I
•-
48 hours
-
_ ..
.-
-11 r7 Fecal Coliform Test 17 - Ir
mL Sample 0.001 0.0001 0.00001 5.000001 0.0000001 0.00000001
24 hours + t
MPN Fecal Coliformlg =
10 x MPN index / 100 ml
largest volume X % dry solids tested
Sterility Control
Quality Control Tubes
Double Strength DS Control
Single Strength SS Control
EC Broth Control
Revised 5-23-16; 414122
10 mL
MPN/g = 10x 4, 8'
0 , 0O I x Zi 0
`z�
l �',
O,Od`�

NAME
Sampled By:
Received By:
Analyzed By:
Calculated By:
Checked By:
FECAL COLIFORM TEST
Standard Methods 9221 E-2014 (MPN) (Biosolids)
Permit #: WQ001026
DATE / TIME
1013i'33
i0131la3 10�Ji
-'S kS15
Sample Location: Sludge # (.p Top Shelf: 39,r °C
Sample Type: Grab X Composite Bottom Shelf: 3� .9 °C
Preservation: None Cooled to 40C X Water Batr: t) Ll 5 °C
24 hr. Check 73 Ie,� 15�
48 hr. Check
72 hr. Check 111-61 '-5
:-1 DMnm�w•v�4:ve Te�� h
mL Sample
0.001
0.0001
0.00001
0.000001 0.0000001
0.00000001
MPN
24 hours
�'
Ell
�
�—
—
,r
48 hours
—
—
—
—
—
b 'D Fecal Coliform Test
mL Sample 0.001 0.0001 0.00001 1 0.000001 0.0000001 0.00000001
24 hours I A-
MPN Fecal Coliformlg =
10 x MPN index / 100 ml
largest volume X % dry solids tested
Sterility Control
Quality Control Tubes 10 mL
Double Strength DS Control 41,-
Sin le Stren th SS ControlLIQ%j�.
EC Broth Control N%S�-P" a—ktt_Je-
Revised 5-23-16; 4/4/22
MPN/g = 10x ,Z , 0
x 4 5a 0, o D 5o00 rw+Pl)1-&

Sampled By:
Received By:
Analyzed By:
Calculated By:
Checked By:
NAME
FECAL COLIFORM TEST
Standard Methods 9221 E-2014 (MPN) (Biosolids)
Permit #: W0001026
DATE ! TIME
i o I31 I:D3 . q5-�
101311a3.1'ZO1
�olg�
i►12�1a�3 j5��
Sample Location: Sludge # I
Sample Type: Grab X Composite
Preservation: None Cooled to 4°C X
24 hr. Check t N 1 i , 1 15
48 hr. Check %i },2o �3-,)g ,1Z!W3
72 hr. Check 1 A131a3,1140 ; VA
S3 CDO Procmmn+ivo Too+ C�'
Top Shelf: 3q,$' °C
Bottom Shelf: 3 °C
Water Bath: 4tL 5 °C
7e^i
mL Sample
0.001
0.0001
0.00001
0.000001
0.0000001
0.00000001
24 hours
—
--
—
—
—
—
—
—
—
"
48 hours
�� e7 e? Fecal Cnlifnrm TRct I.S?
mL Sample 0.001
0.0001
0.00001
0.000001
0.0000001
0.00000001 1 M
24 hours
G[,., i
MPN Fecal Coliform/g =
10 x MPN index / 100 ml
largest volume X % dry solids tested
Sterility Control
Quality Control Tubes 10 mL
Double Strength DS Control
Single Strength SS Controls
EC Broth Control
Revised 5-23-16; 4/4/22
MPN/g = 10x I, g = l 81 :-- 4 SOv fn ?All,
V , 001 x 2( 1% 0 .00-�

Sampled By:. 6
Received By: ;,
Analyzed By: itmwr ., InWOVA
Calculated By: Q,�haMWOK[
Checked By: ,
City of Washington
Sludge
Standard Methods 2540 G-2015 (Aqueous)
Permit #: W0001026
I 0 j 31 123 Time on H2O bath
to�311�3 IoS�
1tlZlZ'� �15�
Drying Oven Temp (in)
Time in Oven
Drying Oven Temp (out)
Time Out of Oven
Time Weighed
Sample
Blank
Sludge # 1
Duplicate
Evaporating Dish #
©1
Wet Weight + Dish Weight
091 • 0
101051.1'A
Dish Weight
a�4''J
U q 01 i .1
�09 5^1' )
Wet Weight
bboa5,J
/
V�O�✓. 1
1stDry Weight + Dish Weight
F,�a54.
1045q•9
"la4 �i,g
2nd Dry Weight + Dish Weight
S1 a5 410
o a. 4
Difference
1st & 2nd Dry Weight + Dish Weight
(2nd-1st)
010
_
Dry Weight
(2nd Dry Wt +Dish Wt -Dish Wt)
O,�
% Dry Solids D Wt/Wet Wt x 100
*Note -Differences should agree within 4% or 0.5 mg, which ever is less
'S•i•
ttt1113 Revised: 9/26/19 JDW; 4/6/22 RWB

Sampled By: ,
Received By: lu,hoi� no
Analyzed By:Y1�hwV2 bl fYiiYlOr
Calculated By: I�"�'l ✓�ilh11Y16SA1�
Checked By: n
Sam
City of Washington
Sludge
Standard Methods 2540 G-2015 (Aqueous)
((��
Permit #: W0001026
10� 31 in 145 Time on H2O batF
10 IN I o n J Drying Oven Temp (in
�0 �_) j Z I I I Time in Over
j jZ j Z� 1010 Drying Oven Temp (out
Time Out of Ovei
Time Weighe,
Blank
1 st
2nd
IIIS
10.1
05
q aI
Ll .
105
101
I V14L'�
Elcql
Sludge # '� I Duplicate
Evaporating Dish #
0
Wet Weight + Dish Weight
6%5 (P - o
Dish Weight
u� _' 54
uo D 5 'q
Wet Weight
0 01
1 st Dry Weight + Dish Weight
u �'` o
2nd Dry Weight + Dish Weight
U) S4 ` O
Ci
Difference
1st & 2nd Dry Weight + Dish Weight
2nd-1 st
0,0
0 ,%
Dry Weight
(2nd Dry Wt + Dish Wt - Dish Wt)
Y'
% Dry Solids RDry Wt/Wet Wt) x 100)]
*Note -Differences should agree within 4% or 0.5 mg, which ever is less Revised: 9/26/19 JDW; 4/6/22 RWB

Sampled By: ,
Received By: UIUA no,�- xmu�
Analyzed By:}�QhytQiryl(Y1U1ti1t�
Calculated By: otAid
Checked By: �V
City of Washington
Sludge
Standard Methods 2540 G-2015 (Aqueous)
Permit #: W0001026
10 `�j) In q ! D Time on H2O bats
101IN j23 it) rn ► Drying Oven Temp (ir
i p IN i I Time in Ovei
Drying Oven Temp (ou
C Time Out of Ove
Time Weighe
1 st
2nd
1 I0
Jos
qZ4
1�4�
> ias
104
io3a
1304
Sample Blank Sludge # Duplicate
Evaporating Dish # CJ A
Wet Weight + Dish Weight
q0I 1015 , q
Dish Weight
2
0 a 5 j J
u °I I s 4. a
Wet weight
b 0 0 41.i
1st Dry Weight + Dish Weight
g� a 54 .0
`i 035U ` 1
2nd Dry Weight + Dish Weight
�� a 54 . 0
lb S?% - 0
Difference
1 st & 2nd Dry Weight + Dish Weight
2nd-1 st
0,0
0,
Dry Weight
(2nd Dry Wt + Dish Wt - Dish Wt)
0,2)
Q
1 D
% Dry Solids i(Dry Wt/Wet Wt) x 100)1
-�
*Note -Differences should agree within 4% or 0.5 mg, which ever is less Revised: 9/26/19 JDW; 4/6/22 RWB

Sampled By: ,
Received By: a ,y) n0_�; ;mma,
Analyzed By: iC(ti1 i1.Q�y1YUL M" -
Calculated By: Lb ` IYIYYt
Checked By:.
City of Washington
Sludge
Standard Methods 2540 G-2015 (Aqueous)
Permit #: W0001026
i0I<�) In qG0 Time on H2O bath
IDIN 123 ifm i
10IN 123 IaS�b
Drying Oven Temp (in)
Time in Oven
lw%'Imf S
Drying Oven Temp (out;
Time Out of Over
Time Weighec
1 st
2nd
005
104
109
11
Ptn
I t Mp
105
1 t 04
1030
t 04
hi
1411
Sample
_T
Blank
Sludge # 9- Duplicate
Evaporating Dish #
1
Wet Wei ht+_Dish Weight
Dish Weight
Wet Weight
1st Dry Weight + Dish Weight
2nd Dry Weight + Dish Weight
. o
'I bb pvl. a
Difference
1st & 2nd Dry Weight + Dish Weight
2nd-1 st
010
0,
Dry Weight
(2nd Dry Wt +Dish Wt -Dish Wt)
0-j)
.
I ;bI d
Dry Solids [(Dry Wt/Wet Wt)
j •i4 ' 4 �'
*Note -Differences should agree within 4% or 0.5 mg, which ever is less Revised: 9/26/19 JDW; 4/6/22 RWB

Sampled By: ,
Received By:
Analyzed By: }CAKb Smm6LJ�
Calculated By:
Checked By:
City of Washington
Sludge
Standard Methods 2540 G-2015 (Aqueous)
Permit #: W0001026
jQ+�J) In 95a Time on H2O bath
1013i 123 It) n I
l6 N 12"� 1?)0w
it-114-a3 , / 732-
Drying Oven Temp (in)
Time in Oven
Drying Oven Temp (out)
Time Out of Oven
Time Weighed
1 st
2nd
No
101
105
q a,�
11 .
105
104
1030
1�04
11+1
14A
Sample
Blank
Sludge#
Duplicate
Evaporating Dish #
55
Wet Weight + Dish Weight
qq WSI ,s
Dish Weight
a 54. 3
U q � 13. 2)
Wet Weight
3u aI 1- 5
1st Dry Weight + Dish Weight
�i a54 •
'l d I,b(P
2nd Dry Weight + Dish Weight
Difference
1st & 2nd Dry Weight + Dish Weight
(2nd-1 stl
0,0
0.1
Dry Weight
(2nd Dry Wt + Dish Wt - Dish Wt)
+y � �
0
�1
•J
% Dry Solids [(Dry Wt/Wet Wt) x 100
2
*Note -Differences should agree within 4% or 0.5 mg, which ever is less Revised: 9/26/19 JDW; 4/6/22 RWB

Sampled By:. "
Received By: likoln
Analyzed By: Lq I�t'o,V1►tiL� , nnmwA
Calculated By: Vwt NW wt h-'Mlmx
Checked By:
City of Washington
Sludge
Standard Methods 2540 G-2015 (Aqueous)
Permit #: W0001026
11st
2nd
10 i %) Izb C 1) Time on H2O bath
q 11(P
ID f bt nj Drying Oven Temp (in)
o E
0 s
17-i(i
rlmle iny6
�i I I IL�j q=� � Time in ven
7i10 i i0�
13
�) Vb Drying Oven Temp (out)
104
� 05
Time Out of Oven
a a 1
i IOJO
Time Weighed
I � a D I
I�DlJ
Sample
Blank
Sludge # Cp Duplicate
Evaporating Dish #
'CJ
y
Wet Weight + Dish Weight
1 C11 1 0 -
Dish Weight
eI
o W `AS' Q
1-1 1550 • a
Wet Weight
3b I � 1 `
1 st D Weight + Dish Weight
�,
,� `p -b4 5 •
TT-5q , -I
2nd Dry Weight + Dish Weight
S
Difference
1st & 2nd Dry Weight+ Dish Weight
2nd-1 st
0.1
0. 4
Dry Weight
(2nd D Wt + Dish Wt - Dish Wt)
n
U�
` t '01
% Dry Solids I(Dry Wt/Wet Wt) x 100)]
3 •°i 6 / ' )
*Note -Differences should agree within 4% or 0.5 mg, which ever is less Revised: 9/26/19 JDW; 4/6/22 RWB

Sampled By: , ,
Received By: JAIU,� VI&- wmw,�
Analyzed By: VXW) . )tAVMK6
Calculated By: NW a cis M m&J%
Checked By: {
City of Washington
Sludge
Standard Methods 2540 G-2015 (Aqueous)
Permit#: W0001026
10 j �) I2 "(►54 Time on H2O bath
I0j31123 /t)n i
I�IIIZ� aA(P
I , l �5- _:34e
Drying Oven Temp (in]
Time in Over
Drying Oven Temp (out
Time Out of Over
Time Weigher
1 st
2nd
t 05
t 0�
i t 04
105
taa�
11,50
Sample
Blank
Sludge #
Duplicate
Evaporating Dish #
Wet Weight + Dish Weight
Dish Weight I0
`a' �`� o
`6 D .5
Wet Weight
30aICA. I
1 st Dry Weight + Dish Weight
✓ ' �' t
0 0 1 I � ,')`
2nd Dry Weight + Dish Weight
Difference
1st & 2nd Dry Weight + Dish Weight
2nd-1 st)
V j
Dry Weight
(2nd Dry Wt + Dish Wt - Dish Wt)
®I
1
% D Solids D Wt/Wet Wt x 100
4 I'
*Note -Differences should agree within 4% or 0.5 mg, which ever is less Revised: 9/26/19 JDW; 4/6/22 RWB

January 2023 Average
AVG.
2023 Average
R.S. 1 & 2
R.S. 3
R.S. 4
76.50%
78.04%
1 75.91%
76.82%
4/20/23 Sample
VS in 0.7383
February 2023 Average
VS out 0.403
R.S. 1 & 21
R.S. 3
R.S. 4
VSFR= 76.07
75.89%
1 76.14%
1 76.49%
76.17%
4/25/23 Sample
March 2023 Average
VS in 0.7383
R.S. 1 & 21
R.S. 3
R.S. 4
VS out 0.565
76.07%
1 76.11%
1 75.08%
75.75%
VSFR= 53.96
10/25/23 Sample
April 2023 Average
R.S. 1 & 2
R.S. 3
R.S. 4
VS in 0.7383
75.07%
74.80%
1 74.31%
74.73%
VS out 0.613
VSFR= 43.85
May 2023 Average
R.S. 1 & 21
R.S. 3
R.S. 4
11/8/23 Sample
72.43%
1 76.69%
1 71.81%
73.64%
VS in 0.7383
VS out 0.603
June 2023 Average
VSFR= 46.16
R.S. 1 & 21
R.S. 3
R.S. 4
74.10%
1 75.41%
1 70.55%
73.35%
July 2023 Average
R.S. 1 & 21 R.S. 3 R.S. 4
73.00% 1 75.50% 1 68.49% 72.33%
August 2023 Average
R.S. 1 & 21 R.S. 3 R.S. 4
70.12% 1 74.08% 68.13% 70.78%
September 2023 Average
R.S. 1 & 2 R.S. 3 R.S. 4
70.44% 76.30% 1 66.87% 71.20%
October 2023 Average
R.S. 1 & 2 R.S. 3 R.S. 4
72.62% 71.92% 1 69.32% 71.29%
November 2023 Average
R.S. 1 & 2 R.S. 3 R.S. 4
73.53% 74.84% 1 70.81% 73.06%
December 2023 Average
R.S. 1 & 2 R.S. 3 R.S. 4
75.15% 80.94% 1 74.40% 76.83%
73.83%

NCDA&CS Agronomic Division Phone: [phone]
Website: www.ncagr.gov/agronomi/
Report No. FY23-SL031750
Predictive
Client:
Harvey Williamson
Hunters Roost Farm Septic Service
Advisor: Brent Collins
EMA Resources Inc
£
Soil Report Mehlich-3 Extraction
5365 US Hwy 17 N
Washington, NC 27889
755 Yadkinville Rd
Mocksville, NC 27028
Links to Helpful Information
Sampled County : Beaufort
Client ID: 282102
Advisor ID: 405413
Sampled: Received: 05/04/2023 Completed: 05/15/2023
Farm: BF210
Sample ID: 00002
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P2O5
K2O
Mg S Mn Zn
Cu B
Information
Lime History:
1-Soybean 0.0
0 0
30
0 0 0 0
0 0
Note: 3
2 - 0.0
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class: Mineral
HM% W/V CEC BS% Ac pH P-1 K-1
Ca% Mg%
S-1
Mn-I
Mn-All Mn-Al2 Zn-I Zn-AI
Cu-I Na ESP SS-1 NO3-N
0.71 1.21 5.6 86 0.8 6.2 209 58
60 21
36
47
36 153 153
119 0.1 2
Sample ID: 00005
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P2O5
K2O
Mg S Mn Zn
Cu B
Information
Lime History:
1-Soybean 0.3
0 0
60
0 0 0 0
0 0
Note: 3
2 - 0.0
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class: Mineral -Organic
HM% W/V CEC BS% Ac pH P-1 K-1
Ca% Mg%
S-1
Mn-I
Mn-All Mn-AI2 Zn-I Zn-AI
Cu-I Na ESP SS-1 NO3-N
5.23 0.93 13.5 74 3.5 5.4 159 39
48 24
50
58
52 331 414
136 0.1 1
North Carolina
f. 1 ' >
IOdvuO iiu%t lLaW Ctwnawukm
Reprogramming of the laboratory -information -management system that makes this report possible is being funded
through a grant from the North Carolina Tobacco Trust Fund Commission.
Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
- Steve Troxler, Commissioner of Agriculture

NCDA&CS Agronomic Division Phone:
[phone]
Website: www.ncagr.gov/agronomi/
Report No.
FY23-SL031750
Harvey Williamson
Page 2 of 3
Sample ID: 00006
Recommendations:
Lime
Nutrients (lb/acre)
More
Crop
(tons/acre)
N P2O5
K2O
Mg
S
Mn
Zn
Cu
B
Information
Lime History:
1-Soybean
0.0
0 0
20
0
0
0
0
0
0
Note: 3
2 -
0.0
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class:
Mineral
HM% W/V CEC BS% Ac pH
P-1 K-I
Ca% Mg%
S-1
Mn-I
Mn-All
Mn-Al2
Zn-I
Zn-AI
Cu-I
Na ESP
SS -I NO3-N
1.80 1.14 10.6
88 1.3 6.2
209 67
61 24
42
33
27
232
232
179
0.1
1
Sample ID: 00007
Recommendations:
Lime
Nutrients (lb/acre)
More
Crop
(tons/acre)
N P2O5
K2O
Mg
S
Mn
Zn
Cu
B
Information
Lime History:
1-Soybean
0.5
0 0
10
0
0
0
0
0
0
Note: 3
2 -
0.0
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class:
Mineral
HM% W/V CEC BS% Ac pH
P-1 K-I
Ca% Mg%
S-1
Mn-I
Mn-All
Mn-AI2
Zn-I
Zn-AI
Cu-I
Na ESP
SS -I NO3-N
1.14 1.16 7.7
80 1.5 5.7
305 72
53 23
44
47
38
247
247
145
0.1
1
Sample ID: 00023
Recommendations:
Lime
Nutrients (lb/acre)
More
Crop
(tons/acre)
N P2O5
K2O
Mg
S
Mn
Zn
Cu
B
Information
Lime History:
1-Soybean
0.0
0 0
10
0
0
0
0
0
0
Note: 3
2 -
0.0
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class:
Mineral
HM% W/V CEC BS% Ac pH
P-1 K-I
Ca% Mg%
S-1
Mn-I
Mn-All
Mn-AI2
Zn-I
Zn-AI
Cu-I
Na ESP
SS-1 NO3-N
2.60 1.14 8.7
80 1.7 5.9
211 73
54 22
45
29
27
119
119
99
0.1
1

NCDA&CS Agronomic Division Phone: [phone]
Website: www.ncagr.gov/agronomi/
Report No. FY23-SL034816
Predictive
Client: Harvey Williamson
Hunters Roost Farm Septic Service
Advisor: Brent Collins
EMA Resources Inc
£
Soil Report Mehlich-3 Extraction
5365 US Hwy 17 N
Washington, NC 27889
755 Yadkinville Rd
Mocksville, NC 27028
Links to Helpful Information
Sampled County : Beaufort
Client ID: 282102
Advisor ID: 405413
Sampled:
Received: 06/26/2023 Completed: 07/05/2023
Farm: BF210
Sample ID: 00008
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P2O5
K2O Mg S Mn Zn
Cu B
Information
Lime History:
1-Soybean 0.9
0 0
30 0 0 0 0
0 0
Note: 3
2 - 0.0
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class: Mineral
HM% W/V
CEC BS% Ac pH P-1 K-1
Ca% Mg%
S-1 Mn-I Mn-All Mn-Al2 Zn-I Zn-AI
Cu-I Na ESP SS-1 NO3-N
2.84 1.14
6.9 73 1.9 5.5 177 59
55 14
40 30 28 177 177
112 0.1 1
North Carolina
lobitty lru%t FuivJ Ctwnauukm
Reprogramming of the laboratory -information -management system that makes this report possible is being funded
through a grant from the North Carolina Tobacco Trust Fund Commission.
Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
- Steve Troxler, Commissioner of Agriculture

NCDA&CS Agronomic Division Phone: [phone]
Website: www.ncagr.gov/agronomi/
Report No. FY24-SL013945
Predictive
Client: Harvey Williamson
Hunters Roost Farm Septic Service
Advisor: Brent Collins
EMA Resources Inc
£
Soil Report Mehlich-3 Extraction
5365 US Hwy 17 N
Washington, NC 27889
755 Yadkinville Rd
Mocksville, NC 27028
Links to Helpful Information
Sampled County : Beaufort
Client ID: 282102
Advisor ID: 405413
Sampled: Received: 11/09/2023 Completed: 12/05/2023
Farm: BF210
Sample ID: 00015
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P2O5
K2O Mg S Mn Zn
Cu B
Information
Lime History:
1 -Small Grain (SG) 0.0
80-100 0
40 0 0 pH$ 0
0 0
Note: 3 Note:
2 - 0.0
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class: Mineral
HM% W/V CEC BS% Ac pH P-1 K-1
Ca% Mg%
S-1
Mn-I Mn-All Mn-Al2 Zn-I Zn-AI
Cu-I Na ESP SS-1 NO3-N
1.19 1.05 11.1 93 0.8 6.6 314 51
67 23
37
63 39 293 293
240 0.1 1
Sample ID: 00016
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P2O5
K2O Mg S Mn Zn
Cu B
Information
Lime History:
1 -Small Grain (SG) 0.0
80-100 0
0 0 0 pH$ 0
0 0
Note: 3 Note:
2 - 0.0
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class: Mineral
HM% W/V CEC BS% Ac pH P-1 K-1
Ca% Mg%
S-1
Mn-I Mn-All Mn-AI2 Zn-I Zn-AI
Cu-I Na ESP SS-1 NO3-N
1.49 1.11 10.2 93 0.7 6.6 341 119
67 20
37
64 40 269 269
173 0.1 1
North Carolina
A� `� J
lobitt o iru%( FtavJ Cianauukm
Reprogramming of the laboratory -information -management system that makes this report possible is being funded
through a grant from the North Carolina Tobacco Trust Fund Commission.
Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
- Steve Troxler, Commissioner of Agriculture

Signature Pages
Final Audit Report
Created: 2024-02-06
By: Brent Collins([e-mail])
Status: Signed
Transaction ID: CBJCHBCAABAADV4Zthsr9alpxWEjSmNxWTX1GeaODRj8
"Signature Pages" History
Document created by Brent Collins([e-mail])
2024-02-06 - 4:25:56 PM GMT- IP address: 206.85.202.26
2024-02-06
w Document emailed to Lonnie Woolard ([e-mail]) for signature
2024-02-06 - 4:26:01 PM GMT
Email viewed by Lonnie Woolard ([e-mail])
2024-02-06 - 4:50:38 PM GMT- IP address: 18.210.6.165
r,�O, Document e-signed by Lonnie Woolard ([e-mail])
Signature Date: 2024-02-06 - 7:28:54 PM GMT - Time Source: server- IP address: 208.180.158.162
Agreement completed.
2024-02-06 - 7:28:54 PM GMT
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Washington Signature Pages
Final Audit Report 2024-02-07
Created: 2024-02-07
By: Brent Collins ([e-mail])
Status: Signed
Transaction ID: CBJCHBCAABAAluixBNrwj6A47ngo39WDaYL8tSBoEjDu
"Washington Signature Pages" History
Document created by Brent Collins ([e-mail])
2024-02-07 - 4:52:09 PM GMT- IP address: 206.85.202.26
Document emailed to Hope Woolard ([e-mail]) for signature
2024-02-07 - 4:52:15 PM GMT
Email viewed by Hope Woolard ([e-mail])
2024-02-07 - 8:33:37 PM GMT- IP address: 3.80.81.176
Document e-signed by Hope Woolard ([e-mail])
Signature Date: 2024-02-07 - 8:34:04 PM GMT - Time Source: server- IP address: 208.180.158.162
Agreement completed.
2024-02-07 - 8:34:04 PM GMT
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