WQ0002376_2023 Residual Annual Report_20240229 (2)

Initial Review
Reviewer
nathaniel.thorn burg
Is this submittal an application? (Excluding additional information.) *
Yes No
If not an application what is the submittal type?* Annual Report
Residual Annual Report
Additional Information
Other
Annual Report Year* 2023
Permit Number (IR) * WQ0002376
Applicant/Permittee City of Reidsville
Email Notifications
Does this need review by the hydrogeologist? * Yes U No
Regional Office Winston-Salem
CO Reviewer
Admin Reviewer Wanda Gerald

Submittal Form
Project Contact Information
Please provide information on the person to be contacted by NDB Staff regarding electronic submittal, confirmation of receipt, and other correspondence.
Name* Brent Collins
Email Address*
[e-mail]
Project Information
.........................
Application/Document Type*
New (Fee Required)
Modification - Major (Fee Required)
Renewal with Major Modification (Fee
Required)
Annual Report
Additional Information
Other
Phone Number*
3363993646
Modification - Minor
Renewal
GW-59, NDMR, NDMLR, NDAR-1,
N DAR-2
Residual Annual Report
Change of Ownership
We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form.
https://edoes.deq.nc.gov/Forms/NonDischarge_Monitoring_Report
Permit Type:*
Wastewater Irrigation
High -Rate Infiltration
Other Wastewater
Reclaimed Water
Closed -Loop Recycle
Residuals
Single -Family Residence Wastewater
Other
Irrigation
Permit Number:*
WQ0002376
Has Current Existing permit number
Applicant/Permittee Address*
1100 Vance St, Reidsville, NC 27320
Facility Name*
City of Reidsville Class B Residuals Program
Please provide comments/notes on your current submittal below.
At this time, paper copies are no longer required. If you have any questions about what is required, please contact Nathaniel Thornburg
at [e-mail].
Please attach all information required or requested for this submittal to be reviewed here.
(Application Form, Engineering Plans, Specifications, Calculations, Etc.)
2023 Reidsville Annual Report - WQ0002376.pdf 14.05MB
Upload only 1 PDF document (less than 250 MB). Multiple documents must be combined into one PDF file unless file is larger
than upload limit.
* By checking this box, I acknowledge that I understand the application will not be accepted for pre -review until the fee (if required) has
been received by the Non -Discharge Branch. Application fees must be submitted by check or money order and made payable to the
North Carolina Department of Environmental Quality (NCDEQ). I also confirm that the uploaded document is a single PDF with all parts
of the application in correct order (as specified by the application).
Mail payment to:
NCDEQ — Division of Water Resources
Attn: Non -Discharge Branch
1617 Mail Service Center
Raleigh, NC 27699-1617
Signature
Submission Date 2/29/2024

City of Reidsville
2023 Annual Report
Residuals Land Application
Permit No. WQ0002376
Prepared By:
EMA Resources, Inc.
Phone 336*751.1441 — Fax 336*751.1442
755 Yadkinville Rd — Mocksville, NC 27028

February 27, 2024
DENR/Water Quality Section
Non -Discharge Compliance Unit
1617 Mail Service Center
Raleigh, NC 27699-1617
Re: 2023 Annual Report - Reidsville
Treatment and Land Application of Residuals
Permit No. WQ0002376
Dear Sir or Madam:
Enclosed is the 2023 Annual Report for the above referenced land application permit.
During 2023 EMA Resources, Inc. land applied 309.34 dry tons of wastewater residuals
to 194.64 acres of private farmland. Please contact Brent Collins - Director of Technical
Services if you have any further questions regarding this report.
Sincerely,
z� 4: �'
Brent Collins
Director of Technical Services
brent. collinsnemaresourcesinc. com
Phone 336*751.1441 — Fax 336*751.1442
755 Yadkinville Rd — Mocksville, NC 27028

ANNUAL LAND APPLICATION CERTIFICATION FORM
WQ Permit#: WQ0002376 County
Facility Name (as shown on permit):
Land Application Operator:
Rockingham County Year:
City of Reidsville
EMA Resources Inc.
2023
Phone: [phone]
Land application of residuals as allowed by the permit occurred during the past calendar year?
© Yes 0 No - If No, skip Part A, and Part B and proceed to Part C. Also, If residuals were
generated but not land applied, please attach an explanation on how the residuals were handled.
Part A - Residuals Application Summary:
Total number of application fields in thepermit:
56
Total number of fields utilized for land application during the year:
12
Total amount of dry tons applied during the year for all application sites:
309.34
Total number of acres utilizes for land application during the year:
194.64
Part B - Annual Compiance Statement:
Facility was compliant during calendar year 2023 with all conditions of the land application permit
(including but not limited to items 1-13 below) issued by the Division of Water Quality. © Yes 0 No
If no please, provide a written description why the facility was not compliant, the dates, and explain corrective action
taken.
1) Only residuals approved for this permit were applied to the permitted sites.
2) Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or
the limit specified in the permit.
3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies
of laboratory results are attached.
4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5) All other monitoring was performed in accordance with the permit and reported during the year as required and three (3)
copies of certified laboratory results are attached.
6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .1105(a) or the Pollutant
Loading Rates in 15A NCAC 02T .I 105(b) (applicable to 40 CFR Part 503 regulated facilities).
7) All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part
503 regulated facilities).
8) All monitoring and reporting requirements in 15A NCAC 02T .I I 1 I were complied with (applicable to 40 CFR Part
503 regulated facilities).
9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Quality.
10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
11) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as
specified in the permit.
12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13) All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C - Certification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate,
and complete. I am aware that there are significant penalties for submitting false information, including the
possibility of fines and imprisonment for knowing violations."
,7o,fhm neck 02/13/24
Josh Beck - Public Works Director Joshua Beck (Feb 13, 202407:05 EST)
Permittee Name and Title (type or print) Signature of Permittee Date
lyow GG &-Othel%I 02/09/24
Mourice Brothers (Feb 9, 202410:40 EST) Z�fz 4" - 2/1 /2024
Signature of Preparer* Date Signature of Land Applier Date
(if different from Permittee) (if different from Permittee and Preparer)
* Preparer is defined in 40 CFR Part 503.9 (r) and 15A NCAC 02T .1102 (26) DENR FORM ACF (12/2006)

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B
WQ Permit Number:
Facility Name:
Residual Source WQ # or
NPDES #:
WWTP Name:
Residual Analysis Data
WQ0002376
City of Reidsville
NCO024881
Reidsville WWTP
Laboratory:
1)
2)
3)
4)
5)
Waypoint Analytical
Parameter
(mg/kg)
Conc.
Limit
m /k a
Sample or Composite Date
1/5/23
4/5/23
7/6/23
10/3/23
Percent Solids (%)
NA
1.13
1.56
2.24
0.951
Arsenic
75
21.8
26.3
11.4
26.3
Cadmium
85
1.82
5.26
2.27
5.26
Copper
4,300
398
222
228
377
Chromium
NA
58.5
42.7
45.5
58.1
Lead
840
94.5
63.7
60
79
Mercury
57
0.563
1.21
0.977
2.39
Molybdenum
75
14.2
7.11
8.86
15.8
Nickel
420
26.3
19.5
23.7
34.4
Selenium
100
29.1
26.3
15.9
36.8
Zinc
7,500
1420
847
841
1540
Total Phosphorus
NA
33200
24700
29400
43200
TKN
NA
70700
77900
65000
110000
Ammonia -Nitrogen
NA
21200
14400
17700
19300
Nitrate and Nitrite
NA
442
72.6
45.5
204
a For surface disposal facilities the ceiling concentration limits listed in this form are not applicable. Reference the individual permit for metals limits.
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant
penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
IV010- GB 6-1-0 lhsf-r
M.uftc Brothers( Feb 9.202410.0 EST)
Signature of Preparer
02/09/24
Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM RSSF (12/2006)

ANNUAL RESIDUAL SAMPLING SUMMARY FORM - B
Report all sampling analysis results for parameters not listed in FORM RSSF that are part of the WQ permit or were analyzed for over the past
calendar year. Use additional forms as needed.
WQ Permit Number:
WQ0002376
Facility Name: City of Reidsville
Residual Source
NPDES # or WQ#:
WWTP Name:
Residual Analysis Data
Laboratory: 1) Waypoint Analytical
2)
NCO024881 3)
4)
Reidsville WWTP 5)
Parameter
Sample or • .. - Date
11
11
•11
'11
--------
•
------------
------------
------------
------------
------------
------------
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
Moukic2 B-I-Other
M...... Eoth(Feb 9,-1— EST)
Signature of Preparer
*Preparer is defined in 40 CFR Part 5039(r) and 15A NCAC 2T .1102 (26)
02/09/24
Date
DENR FORM RSSF - B (12/2006)

1 /5/2023
mg/kg mg/L Equiv Weight Milli Equiv
Sodium 7520 84.976 23 3.694609
Calcium 19500 220.35 20 11.0175
Magnesium 5500 62.15 12 5.179167
Percent Solids 1.13
SAR
1.30
SAR = Na+
z (Ci a2+ + Mg2+ )
3.69461
0.5( 11.0182 + 5.179172 )

4/5/2023
mg/kg mg/L
Sodium 5320 82.992
Calcium 12600 196.56
Magnesium 4680 73.008
Percent Solids 1.56
SAR 1.28
SAR =
Na+
z (Ci a2+ + Mg2+ )
Equiv Weight Milli Equiv
23 3.608348
20 9.828
12 6.084
3.60835
0.5( 9.828 2 + 6.08400 2 )

7/6/2023
mg/kg
mg/L
Equiv Weight Milli Equiv
Sodium
6410
143.584
23 6.242783
Calcium
13700
306.88
20 15.344
Magnesium
5680
127.232
12 10.60267
Percent Solids
2.24
SAR
1.73
SAR =
Na+
z (Ci a2+ + Mg2+ )
6.24278
0.5( 15.344 2 + 10.60267 2 )

Sodium
Calcium
Magnesium
Percent Solids
SAR
SAR =
10/3/2023
mg/kg mg/L Equiv Weight Milli Equiv
17100 162.621 23 7.070478
23000 218.73 20 10.9365
8010 76.1751
0.951
2.41
Na+
z (Ci a2+ + Mg2+ )
12 6.347925
7.07048
0.5( 10.937 2 + 6.34793 2 )

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: City of Reidsville Total Dry Tons Applied (Annual):
Permit #: WQ0002376 Cation Exchange Capacity (non 503 only):
Operator: Harry Sharpe Owner: Daisy Purgason Predominant Soil Series:
Acres Used: 20.67 Acres Permitted: 20.67 Site #: RC011 Field #:
21.99
NaB
1
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Com-
posite
Date
Total
Phos-
phorus
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
•
D
-
Event
1•
1 1 •
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1 •
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
1�
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1•
1 •
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 •
1 11
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 11
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
��
1 1�
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1�
1 1 •
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1 •
®
:1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
:1
Total
'
•
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
1/25/2024
Signature of Land Applier
Date
DENR FORM MFLSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: City of Reidsville WQ Permit #: WQ0002376 Field #: 1 Acres Utilized: 20.67
Land Owner: Daisy Purgason Annual Dry Tons Applied: 21.99 Site #: RC011 Acres Permitted: 20.67
Operator: Harry Sharpe Predominant Soil Series: NaB Cation Exchange Capacity (non 503): 0
Crop 1 Name: Fescue -Hay Crop 1 Max. PAN: 178 Crop 2 Name: Crop 2 Max. PAN:
p
M
Volume applied
(enter one) Solids/
Liquid
Cu. Yds Gallons
"
�"
Solids
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
Soil
Cond.
(Dry,
e '
Moist)
Precip.
Past 24
Hrs.
inches
y
co
•*
a m
c
7y
?:
*
o'
0
* N•
TKN
mg/kg
Z
e 1
o
as o
CD Z.
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
lbs/acre
( )
Name of Crop Type
Receiving Residual
g
Application
Crop 1
Crop 2
Crop 1
Crop 2
6/1
58500
1.56
0.184
Reidsville WWTP
Dry
<.5"
S
0.5
0.3
77900
14400
72.6
9.692
NA
Fescue
6/2
143000
1.56
0.450
Reidsville WWTP
Dry
<.5"
S
0.5
0.3
77900
14400
72.6
23.693
NA
Fescue
6/5
136500
1.56
0.430
Reidsville WWTP
Dry
<.5"
S
0.5
0.3
77900
14400
72.6
22.616
NA
Fescue
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp
to this form):
TOTALS:
01
338000
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn P
56.001
0.00o
Lime Applied
Annuallbs/acre
0.056
0.011
0.472
0.091
0.136
0.003
0.015
0.041
0.056
1.802 52.562
Date
lbs/ac
Prior Years Cumulative lbs/ac
0.372
0.058
4.979
1.163
1.087
0.019
0.228
0.592
0.452
14.628
Current Cumulative lbs/ac
0.428
0.069
5.451
1.254
1.223
0.022
0.243
0.633
0.508
16.430
Permitted C. P. L. R.****
36
34
1 1338
1
267
1 15
374
1 89
1 2498
Permit PAN Limit 1 st/2nd Crop
r 178
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
1/25/2024 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: City of Reidsville Total Dry Tons Applied (Annual):
Permit #: WQ0002376 Cation Exchange Capacity (non 503 only):
Operator: Harry Sharpe Owner: Lawrence McCollum Predominant Soil Series:
Acres Used: 8.95 Acres Permitted: 8.95 Site #: RC012 Field #:
9.73
CgB2
1
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Com-
posite
Date
Total
Phos-
phorus
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
TotalNEBD
Event
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
1�:
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1•
1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1
1 11
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 11
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
��
1 1�
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1�
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
®
:�
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
:�
Total
'
• `:
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
`:
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
1/25/2024
Signature of Land Applier
Date
DENR FORM MFLSF (12/2006)

Facility Name:
Land Owner:
Operator:
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
City of Reidsville
Lawrence McCollum
Harry Sharpe
Crop 1 Name: Fescue -Hay
WQ Permit #: WQ0002376 Field #:
Annual Dry Tons Applied: 9.73 Site #:
Predominant Soil Series: Cg132
Crop 1 Max. PAN:
209 Crop 2 Name:
Acres Utilized:
RC012 Acres Permitted:
Cation Exchange Capacity (non 503):
Crop 2 Max. PAN:
8.95
8.95
0
�
p
Q
Volume applied
(enter one) Solids/
Liquid
Cu. Yds Gallons
"
�"
Solids
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
SoilPrecip.
Cond.
(Dry,
e '
Moist)
Past 24
Hrs.
inches
y
co
•*
a m
c
7y
,
*
o'
�
* N
TKN
mg/kg
Z �
1
o
as o
CD w
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
lbs/acre
( )
Name of Crop Type
ReceivingResidual
Application
Crop 1
Crop 2
Crop 1
Crop 2
6/1
149500
1.56
1.087
Reidsville WWTP
Dry
<.5"
S
0.5
0.3
77900
14400
72.6
57.205
NA
Fescue
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp
to this form):
TOTALS:
01
149500
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn P
57.205
o.000
Lime Applied
Annuallbs/acre
0.057
0.011
0.483
0.093
0.138
0.003
0.015
0.042
0.057
1.841 53.698
1
Date
lbs/ac
Prior Years Cumulative lbs/ac
0.422
0.063
5.102
1.199
1.145
0.023
0.27
0.629
0.545
15.724
Current Cumulative lbs/ac
0.479
0.074
5.585
1.292
1.283
0.026
0.285
0.671
0.602
17.565
Permitted C. P. L. R.****
36
1 34
1 1338
1
1 267
1 15
1
1 374
89
1 2498
Permit PAN Limit 1 st/2nd Crop
209
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
1/25/2024 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: City of Reidsville Total Dry Tons Applied (Annual):
Permit #: WQ0002376 Cation Exchange Capacity (non 503 only):
Operator: Harry Sharpe Owner: Lawrence McCollum Predominant Soil Series:
Acres Used: 3.52 Acres Permitted: 3.52 Site #: RC012 Field #:
2.96
RnB
2A
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Com-
posite
Date
Total
Phos-
phorus
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
TotalMED
Event
1 1� �
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1••
1 11
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 11•
��
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
1 11
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 11
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
��
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
1 1� �
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1••
®�
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
Total
'
1111
1111
1111
1111
1111
1111
1111
1111
1111
1111
1111
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
1/25/2024
Signature of Land Applier
Date
DENR FORM MFLSF (12/2006)

Facility Name:
Land Owner:
Operator:
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
City of Reidsville
Lawrence McCollum
Harry Sharpe
WQ Permit #: WQ0002376 Field #:
Annual Dry Tons Applied: 2.96 Site #:
Predominant Soil Series: RnB
Crop 1 Name: Fescue -Hay Crop 1 Max. PAN:
167 Crop 2 Name:
2A
Acres Utilized:
RC012 Acres Permitted:
Cation Exchange Capacity (non 503):
Crop 2 Max. PAN:
3.52
3.52
0
p
0
M
Volume applied
(enter one) Solids/
Liquid
Cu. Yds Gallons
"
�"
Solids
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
Soil
Cond.
(Dry,
e '
Moist)
Precip.
Past 24
Hrs.
inches
y
co
•*
a m
c
Pd
?:
*
o'
* N•
TKN
mg/kg
Z
Pt
o
aq o
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
lbs/acre
( )
Name of Crop Type
Receiving Residual
g
Application
Crop 1
Crop 2
Crop 1
Crop 2
514
45500
1.56
0.841
Reidsville WWTP
Dry
<.5"
S
0.5
0.3
77900
14400
72.6
44.268
NA
Fescue
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp
to this form):
TOTALS:
0
45500
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn P
44.268
1 0.000
Lime Applied
Annuallbs/acre
0.044
0.009
0.373
0.072
0.107
0.002
0.012
0.033
0.044
1.425 41.545
Date
lbs/ac
Prior Years Cumulative lbs/ac
0.128
0.024
1.049
0.189
0.26
0.002
0.065
0.079
0.132
3.374
Current Cumulative lbs/ac
0.172
0.033
1.422
0.261
0.367
0.004
0.077
0.112
0.176
4.799
Permitted C. P. L. R.****
36
34
1338
267
15
374
89
2498
Permit PAN Limit 1 st/2nd Crop
167
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
1/25/2024 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: City of Reidsville Total Dry Tons Applied (Annual):
Permit #: WQ0002376 Cation Exchange Capacity (non 503 only):
Operator: Harry Sharpe Owner: Lawrence McCollum Predominant Soil Series:
Acres Used: 10.94 Acres Permitted: 10.94 Site #: RC012 Field #:
12.26
CgB2
213
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Com-
posite
Date
Total
Phos-
phorus
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
TotalBOB
D
Event
1 1 •
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1'
OEM
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
1. •:
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 �':
1 1 •
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1••
1�
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1
1 11
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 11
1 1 •
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1 •
��
1 1� �
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1..
1 1 •
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1'
®
:
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
:••
Total
'
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
1/25/2024
Signature of Land Applier
Date
DENR FORM MFLSF (12/2006)

Facility Name:
Land Owner:
Operator:
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
City of Reidsville
Lawrence McCollum
Harry Sharpe
Crop 1 Name: Fescue -Hay
WQ Permit #: WQ0002376 Field #:
Annual Dry Tons Applied: 12.26 Site #:
Predominant Soil Series: Cg132
Crop 1 Max. PAN:
209 Crop 2 Name:
213
Acres Utilized:
RC012 Acres Permitted:
Cation Exchange Capacity (non 503):
Crop 2 Max. PAN:
10.94
10.94
0
p
M
Volume applied
(enter one) Solids/
Liquid
Cu. Yds Gallons
"
�"
Solids
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
Soil
Cond.
(Dry,
e '
Moist)
Precip.
Past 24
Hrs.
inches
y
co
•*
a m
c
7y
?:
*
o'
0
* N•
TKN
mg/kg
Z
e 1
o
as o
CD Z.
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
lbs/acre
( )
Name of Crop Type
Receiving Residual
g
Application
Crop 1
Crop 2
Crop 1
Crop 2
6/6
143000
1.56
0.850
Reidsville WWTP
Dry
<.5"
S
0.5
0.3
77900
14400
72.6
44.765
NA
Fescue
6/7
32500
1.56
0.193
Reidsville WWTP
Dry
<.5"
S
0.5
0.3
77900
14400
72.6
10.174
NA
Fescue
6/9
13000
1.56
0.077
Reidsville WWTP
Dry
<.5"
S
0.5
0.3
77900
14400
72.6
4.070
NA
Fescue
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp
to this form):
TOTALS:
01
1885001
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn P
59.008
0.000
Lime Applied
Annuallbs/acre
0.059
0.012
0.498
0.096
0.143
0.003
0.016
0.044
0.059
1.899 55.377
Date
lbs/ac
Prior Years Cumulative lbs/ac
0.115
0.019
1.088
0.204
0.271
0.003
0.06
0.083
0.127
3.63
Current Cumulative lbs/ac
0.174
0.031
1.586
0.300
0.414
0.006
0.076
0.127
0.186
5.529
Permitted C. P. L. R.****
36
34
1 1338
1
267
1 15
374
1 89
1 2498
Permit PAN Limit 1 st/2nd Crop
r 209
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
1/25/2024 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
City of Reidsville Total Dry Tons Applied (Annual):
WQ0002376 Cation Exchange Capacity (non 503 only):
Ronnie Marshall Owner: Bennett Farms LLC Predominant Soil Series:
57.22 Acres Permitted: 57.22 Site #: RC015 Field #:
77.42
FrD2
1
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample or
Com-
posite
Date
1 1
1 /5/23
2
4/5/23
3
10/3/23
41
1 51
6
L7 1
81
L 9
—1ol
Li 11
12
% Solids
1.13
1.56
0.951
Arsenic
21.8
26.3
26.3
Cadmium
1.82
5.26
5.26
Copper
398
222
377
Chromium
58.5
42.7
58.1
Lead
94.5
63.7
79
Mercury
0.563
1.21
2.39
Molyb-
denum
14.2
7.11
15.8
Nickel
26.3
19.5
1 34.4
Selenium
29.1
26.3
36.8
Zinc
1420
847
1540
Total
Phos-
horus
33200
24700
43200
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
TotalMEMD
Event
1 •
1
1 1
1 1
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1•
OEM
1 11
1 11
1 11
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
1 •
1 `1
1 .
1111
1 111
1111
1 111
1111
1 111
1 111
1111
1 111
1'1:
1 1 :
1 1
1 1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 ..
1 1•
1 1
1 1•:
1111
1 111
1111
1 111
1111
1 111
1 111
1111
1 111
1 •
1 11
1 11
1 11
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 11�
1 1 �
1 11
1 1 �
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
��
1 1 •
1 1
1 1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
1 1 •
1 1
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1:
®®�®
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
Total
'
••`
•
1111
1 111
1111
1 111
1111
1 111
1 111
1111
1 111
• :•
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
1/25/2024
Signature of Land Applier
Date
DENR FORM MFLSF (12/2006)

Facility Name:
Land Owner:
Operator:
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
City of Reidsville
Bennett Farms LLC
Ronnie Marshall
Crop 1 Name: Fescue -Hay
WQ Permit #: WQ0002376 Field #:
Annual Dry Tons Applied: 77.42 Site #:
Predominant Soil Series: FrD2
Crop 1 Max. PAN:
154
Crop 2 Name:
Acres Utilized:
RC015 Acres Permitted:
Cation Exchange Capacity (non 503):
Crop 2 Max. PAN:
57.22
57.22
0
p
M 0
Volume applied
(enter one) Solids/
Liquid
Cu. Yds Gallons
"
�"
Solids
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
Soil
Cond.
(Dry,
e '
Moist)
Precip.
Past 24
Hrs.
inches
y
co
•*
a m
c
7y
?:
*
o'
�
* N•
TKN
mg/kg
Z
1
o
aq o
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
lbs/acre
( )
Name of Crop Type
Receiving Residual
g
Application
Crop 1
Crop 2
Crop 1
Crop 2
2/23
39000
1.13
0.032
Reidsville WWTP
Dry
<.5"
S
0.5
0.3
70700
21200
442
1.663
NA
Fescue
2/24
78000
1.13
0.064
Reidsville WWTP
Dry
<.5"
S
0.5
0.3
70700
21200
442
3.326
NA
Fescue
2/27
104000
1.13
0.086
Reidsville WWTP
Dry
<.5"
S
0.5
0.3
70700
21200
442
4.435
NA
Fescue
2/28
84500
1.13
0.070
Reidsville WWTP
Dry
<.5"
S
0.5
0.3
70700
21200
442
3.603
NA
Fescue
3/1
84500
1.13
0.070
Reidsville WWTP
Dry
<.5"
S
0.5
0.3
70700
21200
442
3.603
NA
Fescue
3/7
136500
1.13
0.112
Reidsville WWTP
Dry
<.5"
S
0.5
0.3
70700
21200
442
5.821
NA
Fescue
3/8
71500
1.13
0.059
Reidsville WWTP
Dry
<.5"
S
0.5
0.3
70700
21200
442
3.049
NA
Fescue
6/9
58500
1.56
0.067
Reidsville WWTP
Dry
<.5"
S
0.5
0.3
77900
14400
72.6
3.501
NA
Fescue
6/13
78000
1.56
0.089
Reidsville WWTP
Dry
<.5"
S
0.5
0.3
77900
14400
72.6
4.668
NA
Fescue
6/14
97500
1.56
0.111
Reidsville WWTP
Dry
<.5"
S
0.5
0.3
77900
14400
72.6
5.835
NA
Fescue
6/15
84500
1.56
0.096
Reidsville WWTP
Dry
<.5"
S
0.5
0.3
77900
14400
72.6
5.057
NA
Fescue
6/16
58500
1.56
0.067
Reidsville WWTP
Dry
<.5"
S
0.5
0.3
77900
14400
72.6
3.501
NA
Fescue
0
624000
0.432
Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp
to this form):
32.058
0.000
TOTALS:
01
1599000
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn P
80.123
0.000
Lime Applied
Annuallbs/acre
0.067
0.011
0.908
0.144
0.216
0.004
0.034
0.072
0.083
3.455 91.186
Date
lbs/ac
Prior Years Cumulative lbs/ac
0.368
0.06
4.3
1.085
0.998
0.023
0.238
0.58
0.47
13.005
Current Cumulative lbs/ac
0.435
0.071
5.208
1.229
1.214
0.027
0.272
0.652
0.553
16.460
Permitted C. P. L. R.****
36
34
1 1338
1
1 267
15
374
89
1 2498
Permit PAN Limit 1 st/2nd Crop
1
154
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
1/25/2024 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
Supplemental Information
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: City of Reidsville WQ Permit #: WQ0002376 Field #: 1 Acres Utilized: 57.22
Land Owner: Bennett Farms LLC Annual Dry Tons Applied: 77.41866 Site #: RC015 Acres Permitted: 57.22
Operator: Ronnie Marshall Predominant Soil Series: FrD2 Cation Exchange Capacity (non 503):
Crop 1 Name: Fescue -Hay Crop 1 Max. PAN: 154 Crop 2 Name: Crop 2 Max PAN:
o
QSolids
Volume applied (enter
one)(Dry,Y
Cu. Yds Gallons
%
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
Soil
Cond.
Moist)
Precip.
Past 24
Hrs.
inches
y
2 �
°o o
o
� �
;
*
°�
5'
� �
7 m
o•
TKN
mg/kg
Z
o
R.
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
(lbs/acre)
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Crop 1
Crop 2
11/8
84500
0.951
0.059
Reidsville WWTP
Dry
<.5"
S
0.5
0.3
110000
19300
204
4.341
NA
Fescue
11/9
104000
0.951
0.072
Reidsville WWTP
Dry
<.5"
S
0.5
0.3
110000
19300
204
5.343
NA
Fescue
11/10
58500
0.951
0.041
Reidsville WWTP
Dry
<.5"
S
0.5
0.3
110000
19300
204
3.005
NA
Fescue
11/13
104000
0.951
1 0.072
Reidsville WWTP
Dry
<.5"
S
0.5
0.3
110000
19300
204
5.343
NA
Fescue
11/14
130000
0.951
0.090
Reidsville WWTP
Dry
<.5"
S
0.5
0.3
110000
19300
204
6.679
NA
Fescue
11115
104000
0.951
0.072
Reidsville WWTP
Dry
<.5"
S
1 0.5
0.3
110000
19300
204
1 5.343
NA
Fescue
11/16
39000
0.951
0.027
Reidsville WWTP
Dry
<.5"
S
0.5
0.3
110000
19300
204
2.004
NA
Fescue
0.000
1
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
TOTALS:
0
624000
0.000
0.432l
0.000
32.058
0.000
0.000
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
1/25/2024 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier Date ***C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (SUPP) (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
City of Reidsville Total Dry Tons Applied (Annual):
WQ0002376 Cation Exchange Capacity (non 503 only):
Donald Lovelace Owner: Lofton Lovelace Predominant Soil Series:
11.09 Acres Permitted: 11.09 Site #: RC041 Field #:
17.02
CdB2
1
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
kVWPT_"1
Com-
posite
Date
©
©
m
Total
Phos-
phorus
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
TotalE
D
-
••
Event
1
1 1 1
1 1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1' 1
1 11
1 11
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 11
1 •
1 "
1111
1111
1111
1111
1111
1111
1111
1111
1111
1111
1 1 •
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1
1 1'
1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1••
1 111
1 11
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 11
1 11 •
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1 1
��
1 1
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
1 1
1 1'
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
®
1 • :
�
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
: :
Total
' •
•
•
1111
1111
1111
1111
1111
1111
1111
1111
1111
1111
' '
•
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
1/25/2024
Signature of Land Applier
Date
DENR FORM MFLSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: City of Reidsville WQ Permit #: WQ0002376 Field #: 1 Acres Utilized: 11.09
Land Owner: Lofton Lovelace Annual Dry Tons Applied: 17.02 Site #: RC041 Acres Permitted: 11.09
Operator: Donald Lovelace Predominant Soil Series: CdB2 Cation Exchange Capacity (non 503): 0
Crop 1 Name: Fescue -Pasture Crop 1 Max. PAN: 156 Crop 2 Name: Crop 2 Max. PAN:
p
0
M
Volume applied
(enter one) Solids/
Liquid
Cu. Yds Gallons
"
�"
Solids
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
Soil
Cond.
(Dry,
e '
Moist)
Precip.
Past 24
Hrs.
inches
y
co
•*
a m
c
7y
?:
*
o'
* N•
TKN
mg/kg
Z
1
o
aq o
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
lbs/acre
( )
Name of Crop Type
Receiving Residual
g
Application
Crop 1
Crop 2
Crop 1
Crop 2
2/7
52000
1.13
0.221
Reidsville WWTP
Dry
<.5"
S
0.5
0.3
70700
21200
442
11.441
NA
Fescue
8/2
156000
2.24
1.314
Reidsville WWTP
Dry
<.5"
S
0.5
0.3
65000
17700
45.5
60.666
NA
Fescue
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp
to this form):
TOTALS:
01
208000
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn P
72,1087
0.000
Lime Applied
Annuallbs/acre
0.040
0.007
0.775
0.145
0.199
0.003
0.030
0.074
0.055
2.838 91.938
Date
lbs/ac
Prior Years Cumulative lbs/ac
0.474
0.272
12.748
1.833
2.899
0.061
0.616
1.701
0.631
27.802
Current Cumulative lbs/ac
0.514
0.279
13.523
1.978
3.098
0.064
0.646
1.775
0.686
30.640
Permitted C. P. L. R.****
36
34
1338
267
15
374
89
2498
Permit PAN Limit 1 st/2nd Crop
F 1-56
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
1/25/2024 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
City of Reidsville Total Dry Tons Applied (Annual):
WQ0002376 Cation Exchange Capacity (non 503 only):
Donald Lovelace Owner: Lofton Lovelace Predominant Soil Series:
8.81 Acres Permitted: 8.81 Site #: RC041 Field #:
18.88
CdB2
2
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
kVWPT_"1
Com-
posite
Date
©
©
m
Total
Phos-
phorus
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
TotalMEBD
••Event
1 1
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1•
1 11
1 11
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 11•
1 .1 •
1.
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1 1�
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1
1•
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
1 11
1 11
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 11�
1 1
1 1 �
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1� •
��
1 1� 1
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1•
1 1'
1 1"
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1::
®®
:
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
.. • 1
Total
'
1 ••
1 •
1 111
1111
1 111
1111
1 111
1111
1 111
1 111
1111
1 111
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
1/25/2024
Signature of Land Applier
Date
DENR FORM MFLSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: City of Reidsville WQ Permit #: WQ0002376 Field #: 2 Acres Utilized: 8.81
Land Owner: Lofton Lovelace Annual Dry Tons Applied: 18.88 Site #: RC041 Acres Permitted: 8.81
Operator: Donald Lovelace Predominant Soil Series: CdB2 Cation Exchange Capacity (non 503): 0
Crop 1 Name: Fescue -Pasture Crop 1 Max. PAN: 156 Crop 2 Name: Crop 2 Max. PAN:
p
M 0
Volume applied
(enter one) Solids/
Liquid
Cu. Yds Gallons
"
�"
Solids
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
Soil
Cond.
(Dry,
e '
Moist)
Precip.
Past 24
Hrs.
inches
y
co
•*
a m
c
7y
?:
*
o'
�
* N•
TKN
mg/kg
Z
Pt
o
aq o
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
lbs/acre
( )
Name of Crop Type
Receiving Residual
g
Application
Crop 1
Crop 2
Crop 1
Crop 2
1/12
58500
1.13
0.313
Reidsville WWTP
Dry
<.5"
S
0.5
0.3
70700
21200
442
16.203
NA
Fescue
2/9
84500
1.13
0.452
Reidsville WWTP
Dry
<.5"
S
0.5
0.3
70700
21200
442
23.404
NA
Fescue
8/8
71500
2.24
0.758
Reidsville WWTP
Dry
<.5"
S
0.5
0.3
65000
17700
45.5
35.001
NA
Fescue
8/9
58500
2.24
0.620
Reidsville WWTP
Dry
<.5"
S
0.5
0.3
65000
17700
45.5
28.637
NA
Fescue
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp
to this form):
TOTALS:
01
273000
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn P
103.2451
0.000
Lime Applied
Annuallbs/acre
0.065
0.009
1.237
0.215
0.310
0.004
0.046
0.106
0.088
4.490 131.822
Date
lbs/ac
Prior Years Cumulative lbs/ac
0.332
0.261
9.327
0.992
2.118
0.042
0.451
1.247
0.42
19.991
Current Cumulative lbs/ac
0.397
0.270
10.564
1.207
2.428
0.046
0.497
1.353
0.508
24.481
Permitted C. P. L. R.****
36
34
1 1338
1
1 267
15
374
89
1 2498
Permit PAN Limit 1 st/2nd Crop
156
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
1/25/2024 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
City of Reidsville Total Dry Tons Applied (Annual):
WQ0002376 Cation Exchange Capacity (non 503 only):
Donald Lovelace Owner: Lofton Lovelace Predominant Soil Series:
1.99 Acres Permitted: 1.99 Site #: RC041 Field #:
3.68
CdB2
3
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Com-
posite
Date
Total
Phos-
phorus
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
TotalNEB
•
D
-
••
Event
1 1:
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1:
1 11
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 11
' 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
� 1
1 •
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 •
1 . •
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 . •
1 11
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 11
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
��
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1•
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
®�
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
Total
' •m
1 111
1 111
1111
1 111
1111
1 111
1111
1 111
1 111
1111
1 111
•�
•
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
1/25/2024
Signature of Land Applier
Date
DENR FORM MFLSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: City of Reidsville WQ Permit #: WQ0002376 Field #: 3 Acres Utilized: 1.99
Land Owner: Lofton Lovelace Annual Dry Tons Applied: 3.68 Site #: RC041 Acres Permitted: 1.99
Operator: Donald Lovelace Predominant Soil Series: CdB2 Cation Exchange Capacity (non 503): 0
Crop 1 Name: Fescue -Hay Crop 1 Max. PAN: 209 Crop 2 Name: Crop 2 Max. PAN:
p
M
Volume applied
(enter one) Solids/
Liquid
Cu. Yds Gallons
"
�"
Solids
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
Soil
Cond.
(Dry,
e '
Moist)
Precip.
Past 24
Hrs.
inches
y
co
•*
a m
c
7y
?:
*
o'
0
* N•
TKN
mg/kg
Z
e 1
o
as o
CD Z.
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
lbs/acre
( )
Name of Crop Type
Receiving Residual
g
Application
Crop 1
Crop 2
Crop 1
Crop 2
1/12
39000
1.13
0.923
Reidsville WWTP
Dry
<.5"
S
0.5
0.3
70700
21200
442
47.821
NA
Fescue
2/8
6500
1.13
0.154
Reidsville WWTP
Dry
<.5"
S
0.5
0.3
70700
21200
442
7.970
NA
Fescue
2/9
32500
1.13
0.770
Reidsville WWTP
Dry
<.5"
S
0.5
0.3
70700
21200
442
39.851
NA
Fescue
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp
to this form):
TOTALS:
OY
78000
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn P
95.643
0.000
Lime A lied
Annuallbs/acre
0.081
0.007
1.470
0.216
0.349
0.002
0.052
0.097
0.107
5.245 122.641
Date
lbs/ac
Prior Years Cumulative lbs/ac
0.435
0.311
10.292
0.938
1.958
0.135
0.473
1.269
0.511
19.542
Current Cumulative lbs/ac
0.516
0.318
11.762
1.154
2.307
0.137
0.525
1.366
0.618
24.787
Permitted C. P. L. R.****
36
34
1 1338
267
15
374
89
2498
Permit PAN Limit 1 st/2nd Crop
F 2-09
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
1/25/2024 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
City of Reidsville Total Dry Tons Applied (Annual):
WQ0002376 Cation Exchange Capacity (non 503 only):
Donald Lovelace Owner: Lofton Lovelace Predominant Soil Series:
17.2 Acres Permitted: 17.2 Site #: RC041 Field #:
38.73
CdB2
4
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
kVWPT_"1
Com-
posite
Date
©
©
m
Total
Phos-
phorus
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
TotalBOB
D
-
••
Event
1 1'•
1 1 •
1 111
1111
1 111
1111
1 111
1111
1 111
1 111
1111
1 111
1 1
1 11�
1 11
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 11
1 :•
�
1 111
1111
1 111
1111
1 111
1111
1 111
1 111
1111
1 111
'1:
��
IZfii'ii}iiiiii'�
1 1
1 111
1111
1 111
1111
1 111
1111
1 111
1 111
1111
1 111
1
��
1 •
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1'
1 11
1 11
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 11
1 1
1 1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
��
1 1
1 1 �
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1•
1 1 •
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
®
: •
• 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1:
Total
'
1
M
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
'1''
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
1/25/2024
Signature of Land Applier
Date
DENR FORM MFLSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: City of Reidsville WQ Permit #: WQ0002376 Field #: 4 Acres Utilized: 17.2
Land Owner: Lofton Lovelace Annual Dry Tons Applied: 38.73 Site #: RC041 Acres Permitted: 17.2
Operator: Donald Lovelace Predominant Soil Series: CdB2 Cation Exchange Capacity (non 503): 0
Crop 1 Name: Fescue -Pasture Crop 1 Max. PAN: 156 Crop 2 Name: Crop 2 Max. PAN:
p
M 0
Volume applied
(enter one) Solids/
Liquid
Cu. Yds Gallons
"
�"
Solids
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
Soil
Cond.
(Dry,
e '
Moist)
Precip.
Past 24
Hrs.
inches
y
co
•*
a m
c
7y
?:
*
o'
�
* N•
TKN
mg/kg
Z
1
o
aq o
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
lbs/acre
( )
Name of Crop Type
Receiving Residual
g
Application
Crop 1
Crop 2
Crop 1
Crop 2
1/11
149500
1.13
0.410
Reidsville WWTP
Dry
<.5"
S
0.5
0.3
70700
21200
442
21.209
NA
Fescue
1/12
78000
1.13
0.214
Reidsville WWTP
Dry
<.5"
S
0.5
0.3
70700
21200
442
11.066
NA
Fescue
2/7
71500
1.13
0.196
Reidsville WWTP
Dry
<.5"
S
0.5
0.3
70700
21200
442
10.143
NA
Fescue
2/8
110500
1.13
0.303
Reidsville WWTP
Dry
<.5"
S
0.5
0.3
70700
21200
442
15.676
NA
Fescue
8/3
71500
2.24
0.388
Reidsville WWTP
Dry
<.5"
S
0.5
0.3
65000
17700
45.5
17.928
NA
Fescue
8/8
136500
2.24
0.741
Reidsville WWTP
Dry
<.5"
S
0.5
0.3
65000
17700
45.5
34.226
NA
Fescue
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp
to this form):
TOTALS:
01
617500
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn I P
1 110.2491
o.000
Lime Applied
Annuallbs/acre
0.075
0.009
1.408
0.234
0.348
0.003
0.052
0.113
0.101
5.087 1140.9451
Date
lbs/ac
Prior Years Cumulative lbs/ac
0.577
0.304
14.27
2.779
3.192
0.068
0.675
1.83
0.73
33.058
Current Cumulative lbs/ac
0.652
0.313
15.678
3.013
3.540
0.071
0.727
1.943
0.831
38.145
Permitted C. P. L. R.****
36
34
1338
267
15
374
89
2498
Permit PAN Limit 1 st/2nd Crop
1
1 156
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
1/25/2024 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: City of Reidsville Total Dry Tons Applied (Annual):
Permit #: WQ0002376 Cation Exchange Capacity (non 503 only):
Operator: Johnie Carty Owner: Johnie Carty Predominant Soil Series:
Acres Used: 5.2 Acres Permitted: 5.2 Site #: RC118 Field #:
4.29
CcB
2
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
kVWPT_"1
Com-
posite
Date
©
©
m
Total
Phos-
phorus
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
TotalMEB
D
••Event
1 1 •
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1 •
1 11
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 11
1•
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1•
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1•
1 •
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 •
1 11
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 11
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
••
1 1�
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1�
1 1�:
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1�:
®�
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
Total
' •m
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
:1
•
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
1/25/2024
Signature of Land Applier
Date
DENR FORM MFLSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: City of Reidsville WQ Permit #: WQ0002376 Field #: 2 Acres Utilized: 5.2
Land Owner: Johnie Carty Annual Dry Tons Applied: 4.29 Site #: RC118 Acres Permitted: 5.2
Operator: Johnie Carty Predominant Soil Series: CcB Cation Exchange Capacity (non 503): 0
Crop 1 Name: Fescue -Hay Crop 1 Max. PAN: 220 Crop 2 Name: Crop 2 Max. PAN:
o
o
Volume applied
(enter one) Solids/
Liquid
Cu. Yds Gallons
%
Solids
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
Soil
Cond.
(Dry,
Wet
Moist)
Precip.
Past 24
Hrs.
inches
a
a
o
� --
°�
4.
w -
co
* N
TKN
mg/kg
Z a
.; El
o
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
(lbs/acre)
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Crop 1
Crop 2
2/23
91000
1.13
0.825
Reidsville WWTP
Dry
<.5"
S
0.5
0.3
70700
21200
442
42.702
NA
Fescue
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp
to this form):
TOTALS:
01
91000
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn
P
42.702
1 0.000
Lime Applied
Annuallbs/acre
0.036
0.003
0.657
0.097
0.156
0.001
0.023
0.043
0.048
2.343
54.780
Date
lbs/ac
Prior Years Cumulative lbs/ac
0.604
0.482
40.446
1.447
7.683
0.181
1.284
5.568
0.773
65.152
Current Cumulative lbs/ac
0.640
1 0.485
41.103
1.544
7.839
0.182
1.307
5.611
0.821
67.495
Permitted C. P. L. R.****
36
34
1 1338
1
1 267
1 15
1
1 374
1 89
1 2498
Permit PAN Limit I st/2nd Crop
220
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
1/25/2024 **Volatilization Rate: Surface - 0.5, Injection/Incorporation -1.0
Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
City of Reidsville Total Dry Tons Applied (Annual):
WQ0002376 Cation Exchange Capacity (non 503 only):
Thomas Carter Owner: Thomas Carter Predominant Soil Series:
9.81 Acres Permitted: 9.81 Site #: RC119 Field #:
26.37
CdB2
9
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
kVWPT_"1
Com-
posite
Date
©
©
m
Total
Phos-
phorus
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
TotalMEBD
••Event
1 1
1 1� `
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
OEM
1 11
1 1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
1' •
1 `::
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
'1
1 1•
1•
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 :
1 1••
1 •1
1 111
1111
1 111
1111
1 111
1111
1 111
1 111
1111
1 111
1 '
1 11
1 11�
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 11
1 1
1 1 :
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
��
1 1
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
1 1 1
1 1•`
1 111
1111
1 111
1111
1 111
1111
1 111
1 111
1111
1 111
1 1••
®
' :
�
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
Total
' •m
•
1 111
1111
1 111
1111
1 111
1111
1 111
1 111
1111
1 111
• 1
•
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
1/25/2024
Signature of Land Applier
Date
DENR FORM MFLSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: City of Reidsville WQ Permit #: WQ0002376 Field #: 9 Acres Utilized: 9.81
Land Owner: Thomas Carter Annual Dry Tons Applied: 26.37 Site #: RC119 Acres Permitted: 9.81
Operator: Thomas Carter Predominant Soil Series: Cd132 Cation Exchange Capacity (non 503): 0
Crop 1 Name: Fescue -Pasture Crop 1 Max. PAN: 156 Crop 2 Name: Crop 2 Max. PAN:
o
o
Volume applied
(enter one) Solids/
Liquid
Cu. Yds Gallons
o
/o
Solids
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#
Fert., Animal
Waste, etc)
Soil
Cond.
(Dry,
Wet
Moist)
Precip.
Hrs.
inches
a
a
o
� --
*
°�
4.
=
-
co
* N
TKN
mg/kg
Z a
.; El
o
�.
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
(lbs/acre)
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Crop 1
Crop 2
2/21
104000
1.18
0.522
Reidsville WWTP
Dry
<.5"
S
0.5
0.3
70700
21200
442
27.013
NA
Fescue
8/9
162500
2.24
1.547
Reidsville WWTP
Dry
<.5"
S
0.5
0.3
65000
17700
45.5
71.439
NA
Fescue
8/10
65000
2.24
0.619
Reidsville WWTP
Dry
<.5"
S
0.5
0.3
65000
17700
45.5
28.576
NA
Fescue
0.000
0.000
0.000
0.000
1
1
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp
to this form):
TOTALS:
01
331500
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn
P
127.028
0.000
Lime Applied
Annuallbs/acre
0.072
0.012
1.403
0.258
0.359
0.005
0.053
0.130
0.099
5.126
162.022
Date
lbs/ac
Prior Years Cumulative lbs/ac
0.332
0.1
7.42
1.696
1.405
0.04
0.304
0.934
0.42
18.417
Current Cumulative lbs/ac
0.404
0.112
1 8.823
1.954
1.764
0.045
0.357
1.064
0.519
23.543
Permitted C. P. L. R.****
36
34
1338
267
15
374
89
2498
Permit PAN Limit 1 st/2nd Crop
156
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
1/25/2024 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
City of Reidsville Total Dry Tons Applied (Annual):
WQ0002376 Cation Exchange Capacity (non 503 only):
Ken Martin Owner: Ken Martin Predominant Soil Series:
39.24 Acres Permitted: 39.24 Site #: RC130 Field #:
76.01
CmB
1
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
kVWPT_"1
Com-
posite
Date
©
©
m
Total
Phos-
phorus
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
TotalMEBD
••Event
•
1 1
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
1 11
1 11
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 11•
1 ':
1
1 111
1111
1 111
1111
1 111
1111
1 111
1 111
1111
1 111
1':'
1 1
1�:
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 :�
11 •
1 `
1111
1111
1111
1111
1111
1111
1111
1111
1111
1111
1 '
1 111
1 11
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 11�
1 11
1 1 •
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1 :
•�
1 1 •
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1•
1 1
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1 1
®
1 ::•
®
1 111
1111
1 111
1111
1 111
1111
1 111
1 111
1111
1 111
• •
Total
'
1
` 1
1111
1111
1111
1111
1111
1111
1111
1111
1111
1111
• •
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
1/25/2024
Signature of Land Applier
Date
DENR FORM MFLSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: City of Reidsville WQ Permit #: WQ0002376 Field #: 1 Acres Utilized: 39.24
Land Owner: Ken Martin Annual Dry Tons Applied: 76.01 Site #: RC130 Acres Permitted: 39.24
Operator: Ken Martin Predominant Soil Series: CmB Cation Exchange Capacity (non 503): 0
Crop 1 Name: Fescue -Hay Crop 1 Max. PAN: 146 Crop 2 Name: Crop 2 Max. PAN:
p
M
Volume applied
(enter one) Solids/
Liquid
Cu. Yds Gallons
"
�"
Solids
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
Soil
Cond.
(Dry,
e '
Moist)
Precip.
Past 24
Hrs.
inches
y
co
•*
a m
c
7y
?:
*
o'
0
* N•
TKN
mg/kg
Z
e 1
o
as o
CD Z.
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
lbs/acre
( )
Name of Crop Type
Receiving Residual
g
Application
Crop 1
Crop 2
Crop 1
Crop 2
2/16
130000
1.13
0.156
Reidsville WWTP
Dry
<.5"
S
0.5
0.3
70700
21200
442
8.084
NA
Fescue
2/20
130000
1.13
0.156
Reidsville WWTP
Dry
<.5"
S
0.5
0.3
70700
21200
442
8.084
NA
Fescue
9/12
84500
2.24
0.201
Reidsville WWTP
Dry
<.5"
S
0.5
0.3
65000
17700
45.5
9.287
NA
Fescue
9/13
136500
2.24
0.325
Reidsville WWTP
Dry
<.5"
S
0.5
0.3
65000
17700
45.5
15.002
NA
Fescue
9/14
149500
2.24
0.356
Reidsville WWTP
Dry
<.5"
S
0.5
0.3
65000
17700
45.5
16.431
NA
Fescue
9/15
110500
2.24
0.263
Reidsville WWTP
Dry
<.5"
S
0.5
0.3
65000
17700
45.5
12.145
NA
Fescue
9/19
104000
2.24
0.248
Reidsville WWTP
Dry
<.5"
S
0.5
0.3
65000
17700
45.5
11.430
NA
Fescue
9/20
97500
2.24
0.232
Reidsville WWTP
Dry
<.5"
S
0.5
0.3
65000
17700
45.5
10.716
NA
Fescue
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.0001
1
10.000
0.000
Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp
to this form):
TOTALS:
01
942500
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn P
91.179
o.000
Lime Applied
Annuallbs/acre
0.051
0.009
0.989
0.184
0.254
0.004
0.038
0.093
0.070
3.619 116.267
Date
lbs/ac
Prior Years Cumulative lbs/ac
0.314
0.084
6.666
1.821
1.365
0.036
0.296
0.955
0.395
17.689
Current Cumulative lbs/ac
0.365
0.093
7.655
2.005
1.619
0.040
0.334
1.048
0.465
21.308
Permitted C. P. L. R.****
36
34
1338
267
15
374
89
1 2498
Permit PAN Limit 1 st/2nd Crop
1
1 146
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
1/25/2024 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

Waypointo
ANALYTICAL
1 /16/2023
EMA Resources Inc
Brent Collins
755 Yadkinville Rd
Mocksville, NC, 27028
Ref: Analytical Testing
Lab Report Number: 23-006-0003
Client Project Description: Reidsville, NC
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 1 Fax [phone]
www.waypointanalytical.com
Dear Brent Collins:
Waypoint Analytical, LLC. received sample(s) on 1/6/2023 for the analyses presented in the following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Where the laboratory was not responsible for the sampling
stage (refer to the chain of custody) results apply to the sample as received.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2021) and NELAC unless otherwise indicated. Any parameter
for which the laboratory is not officially NELAP accredited is indicated by a'—' symbol. These are not included in
the scope because NELAP accreditation is either not available or has not been applied for. Additional
certifications may be held/are available for parameters, where NELAP accreditation is not required or applicable.
A full list of certifications is available upon request.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Connie Cook
Project Manager
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 1 of 8

Waypointo
ANALYTICAL
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 ° Fax [phone]
www.waypointanalytical.corn
Certification Summary
Laboratory ID: WP MTN: Waypoint Analytical, LLC., Memphis, TN
State
Program
Lab ID
Expiration Date
Alabama
State Program
40750
02/28/2023
Arkansas
State Program
88-0650
02/07/2023
California
State Program
2904
06/30/2023
Florida
State Program
- NELAP
E871157
06/30/2023
Georgia
State Program
C044
02/18/2023
Georgia
State Program
04015
06/30/2023
Illinois
State Program
- NELAP
200078
10/10/2023
Kentucky
State Program
80215
06/30/2023
Kentucky
State Program
KY90047
12/31/2023
Louisiana
State Program
- NELAP
LA037
12/31/2023
Louisiana
State Program
- NELAP
04015
06/30/2023
Mississippi
State Program
MS
02/11/2023
North Carolina
State Program
47701
07/31/2023
North Carolina
State Program
415
12/31/2023
Pennsylvania
State Program
- NELAP
68-03195
05/31/2023
South Carolina
State Program
84002
06/30/2023
Tennessee
State Program
02027
02/11/2023
Texas
State Program
- NELAP
T104704180
09/30/2023
Virginia
State Program
00106
06/30/2023
Virginia
State Program
- NELAP
460181
09/14/2023
Page 1 of 1 00001/23-006-0003
Page 2 of 8

waypoint 2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 Fax [phone]
ANALYTICAL www.waypointanalytical.com
Sample Summary Table
Report Number: 23-006-0003
Client Project Description: Reidsville, NC
Lab No Client Sample ID
90141 Reidsville
Matrix Date Collected
Solids 01/05/202311:15
Date Received
01/06/2023
Page 3 of 8

Waypointo
ANALYTICAL
Client: EMA Resources Inc
Project: Reidsville, NC
Lab Report Number: 23-006-0003
Date: 1 /16/2023
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 1 Fax [phone]
www.waypointanalytical.com
CASE NARRATIVE
Metals Analysis Method 6010D
Sample 99364
Analyte: Aluminum
QC Batch No: 1-657906/1-657395
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 99364
Analyte: Calcium
QC Batch No: 1-657906/1-657395
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 99364
Analyte: Iron
QC Batch No: 1-657906/1-657395
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 99364
Analyte: Potassium
QC Batch No: 1-657906/1-657395
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 99364
Analyte: Manganese
QC Batch No: 1-657730/1-657395
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 99364
Analyte: Lead
QC Batch No: 1-657730/1-657395
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Page 4 of 8

0
Waypoint, 2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 Fax [phone]
ANALYTICAL www.waypointanalytical.com
46245
EMA Resources Inc Project Reidsville, NC
Brent Collins Report Date : 01/16/2023
755 Yadkinville Rd Information : Received : 01/06/2023
Mocksville , NC 27028 n �
Connie Cook
Report Number : 23-006-0003
REPOR T OF A NA L YSIS
Project
Manager
Lab No : 90141
Matrix:
Solids
Sample ID : Reidsville
Sampled:
1/5/2023 11:15
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Method
Moisture
98.9
%
1
01/09/23 15:55
FMM
SW-DRYWT
Ammonia Nitrogen
21200
mg/Kg - dry
1450
9090
1
01/16/23 14:00
JPJ
4500NH3C-2011
Nitrate+Nitrite-N
<442
mg/Kg - dry
442
442
1
01/09/23 14:25
ZBD
4500NO3F-2016
Organic N
49550
mg/Kg - dry
1455
9091
1
01/16/23 10:30
CALCULATION
pH
7.3
S.U.
1
01/13/2313:23
SAR
9045D
Total Solids
1.13
%
0.010
0.010
1
01/09/23 15:55
FMM
2540G-2011
Total Volatile Solids
72.2
%
0.010
0.010
1
01/09/23 15:55
FMM
2540G-2011
Total Kjeldahl Nitrogen
70700
mg/Kg - dry
909
22700
1
01/16/23 10:30
JPJ ')M-4500-NH3C-TKP
Phosphorus
33200
mg/Kg - dry
251
455
1
01/09/23 20:23
TJS
6010D
Aluminum
24500
mg/Kg - dry
420
455
1
01/09/23 20:23
TJS
6010D
Arsenic
<21.8
mg/Kg - dry
21.8
45.5
1
01/09/23 20:23
TJS
6010D
Cadmium
<1.82
mg/Kg - dry
1.82
9.09
1
01/09/23 20:23
TJS
6010D
Calcium
19500
mg/Kg - dry
3520
4550
1
01/09/23 20:23
TJS
6010D
Chromium
58.5
mg/Kg - dry
21.5
22.7
1
01/09/23 20:23
TJS
6010D
Copper
398
mg/Kg - dry
28.2
45.5
1
01/09/23 20:23
TJS
6010D
Iron
23500
mg/Kg - dry
775
909
1
01/09/23 20:23
TJS
6010D
Lead
94.5
mg/Kg - dry
16.4
27.3
1
01/09/23 20:23
TJS
6010D
Magnesium
5500
mg/Kg - dry
235
455
1
01/09/23 20:23
TJS
6010D
Manganese
842
mg/Kg - dry
29.5
45.5
1
01/09/23 20:23
TJS
6010D
Mercury
<0.563
mg/Kg - dry
0.563
12.9
1
01/11/23 13:55
JTR
7471A
Molybdenum
14.21
mg/Kg - dry
12.3
22.7
1
01/09/23 20:23
TJS
6010D
Nickel
26.3
mg/Kg - dry
10.9
22.7
1
01/09/23 20:23
TJS
6010D
Potassium
6030
mg/Kg - dry
562
909
1
01/09/23 20:23
TJS
6010D
Qualifiers/ DF
Dilution Factor
J
Estimated value
Definitions MQL
Method Quantitation Limit
Page 5 of 8

0
Waypoint,
2790 Whitten
Road, Memphis, TN 38133
Main 901.213.2400 0 Fax [phone]
ANALYTICAL
www.waypointanalytical.com
46245
EMA Resources Inc
Project
Reidsville,
NC
Brent Collins
Report Date : 01/16/2023
755 Yadkinville Rd
Information :
Received : 01/06/2023
Mocksville , NC 27028
Connie Cook
Report Number : 23-006-0003
REPOR T OF A
NA L YSIS
Project Manager
Lab No : 90141
Matrix: Solids
Sample ID : Reidsville
Sampled: 1/5/2023 11:15
Test
Results
Units
MDL
MQL DF Date / Time By Analytical
Analyzed Method
Selenium
<29.1
mg/Kg - dry
29.1
45.5 1 01/09/23 20:23 TJS 6010D
Sodium
7520
mg/Kg - dry
1180
2270 1 01/09/23 20:23 TJS 6010D
Zinc
1420
mg/Kg - dry
73.6
114 1 01/09/23 20:23 TJS 6010D
Sulfur
17100
mg/Kg - dry
471
909 1 01/09/23 20:23 TJS 6010D
Sodium Absorption Ratio
1.28
Ratio
0.01
0.01 1 01/09/23 20:23 CALCULATION
Qualifiers/ DF Dilution Factor
Definitions
J Estimated value
Page 6 of 8

(2)
WayPAoint..
NALYTICAL
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 ° Fax [phone]
www.waypointanalytical.com
Shipment Receipt Form
Customer Number: 46245
Customer Name: EMA Resources Inc
Report Number: 23-006-0003
Shipping Method
Fed Ex 0 US Postal 0 Lab 0 Other:
0 UPS 0 Client 0 Courier Thermometer ID: N/A
Shipping container/cooler uncompromised?
* Yes
0 No
Number of coolers/boxes received
F
Custody seals intact on shipping container/cooler?
0 Yes
0 No
Not Present
Custody seals intact on sample bottles?
0 Yes
0 No
Not Present
Chain of Custody (COC) present?
Yes
0 No
COC agrees with sample label(s)?
U Yes
0 No
COC properly completed
U Yes
0 No
Samples in proper containers?
U Yes
0 No
Sample containers intact?
Yes
0 No
Sufficient sample volume for indicated test(s)?
Yes
0 No
All samples received within holding time?
Yes
0 No
Cooler temperature in compliance?
Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
Yes
0 No
Water - Sample containers properly preserved
0 Yes
0 No
N/A
Water - VOA vials free of headspace
0 Yes
0 No
N/A
Trip Blanks received with VOAs
0 Yes
0 No
0 N/A
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
0 N/A
F_ High concentration container (48 hr) F Low concentration EnCore samplers (48 hr)
F_ High concentration pre -weighed (methanol -14 d) Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included?
0 Yes
0 No
Comments:
Signature: Makayla Weaver Date & Time: 01/06/2023 10:56:01
Page 7 of 8

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Page 8 of 8

Waypointo
ANALYTICAL
4/13/2023
EMA Resources Inc
Brent Collins
755 Yadkinville Rd
Mocksville, NC, 27028
Ref: Analytical Testing
Lab Report Number: 23-096-0014
Client Project Description: Reidsville, NC
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 1 Fax [phone]
www.waypointanalytical.com
Dear Brent Collins:
Waypoint Analytical, LLC. received sample(s) on 4/6/2023 for the analyses presented in the following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Where the laboratory was not responsible for the sampling
stage (refer to the chain of custody) results apply to the sample as received.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2021) and NELAC unless otherwise indicated. Any parameter
for which the laboratory is not officially NELAP accredited is indicated by a'—' symbol. These are not included in
the scope because NELAP accreditation is either not available or has not been applied for. Additional
certifications may be held/are available for parameters, where NELAP accreditation is not required or applicable.
A full list of certifications is available upon request.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Connie Cook
Project Manager
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 1 of 8

Waypointo
ANALYTICAL
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 ° Fax [phone]
www.waypointanalytical.corn
Certification Summary
Laboratory ID: WP MTN: Waypoint Analytical, LLC., Memphis, TN
State
Program
Lab ID
Expiration Date
Alabama
State Program
40750
02/29/2024
Arkansas
State Program
88-0650
02/07/2024
California
State Program
2904
06/30/2023
Florida
State Program
- NELAP
E871157
06/30/2023
Georgia
State Program
C044
11/14/2025
Georgia
State Program
04015
06/30/2023
Illinois
State Program
- NELAP
200078
10/10/2023
Kentucky
State Program
80215
06/30/2023
Kentucky
State Program
KY90047
12/31/2023
Louisiana
State Program
- NELAP
LA037
12/31/2023
Louisiana
State Program
- NELAP
04015
06/30/2023
Mississippi
State Program
MS
11/14/2025
North Carolina
State Program
47701
07/31/2023
North Carolina
State Program
415
12/31/2023
Pennsylvania
State Program
- NELAP
68-03195
05/31/2024
South Carolina
State Program
84002
06/30/2023
Tennessee
State Program
02027
11/14/2025
Texas
State Program
- NELAP
T104704180
09/30/2023
Virginia
State Program
00106
06/30/2023
Virginia
State Program
- NELAP
460181
09/14/2023
Page 1 of 1 00001/23-096-0014
Page 2 of 8

waypoint 2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 Fax [phone]
ANALYTICAL www.waypointanalytical.com
Sample Summary Table
Report Number: 23-096-0014
Client Project Description: Reidsville, NC
Lab No Client Sample ID
93338 Reidsville
Matrix Date Collected
Solids 04/05/2023
Date Received
04/06/2023
Page 3 of 8

Waypointo
ANALYTICAL
Client: EMA Resources Inc
Project: Reidsville, NC
Lab Report Number: 23-096-0014
Date: 4/13/2023
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 1 Fax [phone]
www.waypointanalytical.com
CASE NARRATIVE
Metals Analysis Method 6010D
Sample 93829 (#2)
Analyte: Aluminum
QC Batch No: 1-675666/1-674801
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 93829 (#2)
Analyte: Calcium
QC Batch No: 1-675666/1-674801
The matrix spike, matrix spike duplicate and the dilution test were all outside of the quality control acceptance
ranges. Matrix interference is suspected.
Sample 93829 (#2)
Analyte: Iron
QC Batch No: 1-675666/1-674801
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 93829 (#2)
Analyte: Potassium
QC Batch No: 1-675666/1-674801
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 93829 (#2)
Analyte: Magnesium
QC Batch No: 1-675666/1-674801
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 93829 (#2)
Analyte: Sulfur
QC Batch No: 1-675666/1-674801
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Solids Total Mercury Analysis - CVAA Method 7471A
Sample 93833 (San Elijo)
Analyte: Mercury
QC Batch No: 1-675254/1-674948
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Page 4 of 8

0
Waypoint, 2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 Fax [phone]
ANALYTICAL www.waypointanalytical.com
46245
EMA Resources Inc Project Reidsville, NC
Brent Collins Report Date : 04/13/2023
755 Yadkinville Rd Information : Received : 04/06/2023
Mocksville , NC 27028 n �
Connie Cook
Report Number : 23-096-0014
REPOR T OF A NA L YSIS
Project
Manager
Lab No : 93338
Matrix:
Solids
Sample ID : Reidsville
Sampled:
4/5/2023 0:00
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Method
Moisture
98.1
%
1
04/11/2313:02
JLS
SW-DRYWT
Ammonia Nitrogen
14400
mg/Kg - dry
842
5260
1
04/13/23 13:30
JPJ
4500NH3C-2011
Nitrate+Nitrite-N
72.63
mg/Kg - dry
52.6
263
1
04/11/23 12:54
ZBD
4500NO3F-2016
Organic N
63470
mg/Kg - dry
842.1
5263
1
04/13/23 08:00
CALCULATION
pH
7.3
S.U.
1
04/11/2311:25
HBT
9045D
Total Solids
1.56
%
0.010
0.010
1
04/10/23 14:09
JLS
2540G-2011
Total Volatile Solids
90.8
%
0.010
0.010
1
04/10/23 14:09
JLS
2540G-2011
Total Kjeldahl Nitrogen
77900
mg/Kg - dry
526
13200
1
04/13/23 08:00
JPJ ')M-4500-NH3C-TKP
Phosphorus
24700
mg/Kg - dry
145
263
1
04/11/23 04:31
JTR
6010D
Aluminum
15300
mg/Kg - dry
243
263
1
04/11/23 04:31
JTR
6010D
Arsenic
<26.3
mg/Kg - dry
12.6
26.3
1
04/11/23 04:31
JTR
6010D
Cadmium
<5.26
mg/Kg - dry
1.05
5.26
1
04/11/23 04:31
JTR
6010D
Calcium
12600
mg/Kg - dry
2040
2630
1
04/11/23 04:31
JTR
6010D
Chromium
42.7
mg/Kg - dry
12.4
13.2
1
04/11/23 22:55
JTR
6010D
Copper
222
mg/Kg - dry
16.3
26.3
1
04/11/23 04:31
JTR
6010D
Iron
13200
mg/Kg - dry
448
526
1
04/11/23 04:31
JTR
6010D
Lead
63.7
mg/Kg - dry
9.47
15.8
1
04/11/23 04:31
JTR
6010D
Magnesium
4680
mg/Kg - dry
136
263
1
04/11/23 04:31
JTR
6010D
Manganese
537
mg/Kg - dry
17.1
26.3
1
04/11/23 04:31
JTR
6010D
Mercury
<1.21
mg/Kg - dry
1.21
10.0
1
04/10/23 14:12
FDS
7471A
Molybdenum
<7.11
mg/Kg - dry
7.11
13.2
1
04/11/23 04:31
JTR
6010D
Nickel
19.5
mg/Kg - dry
6.32
13.2
1
04/11/23 04:31
JTR
6010D
Potassium
6470
mg/Kg - dry
325
526
1
04/11/23 04:31
JTR
6010D
Qualifiers/ DF
Dilution Factor
J
Estimated value
Definitions MQL
Method Quantitation Limit
Page 5 of 8

0
Waypoint,
2790 Whitten
Road, Memphis, TN 38133
Main 901.213.2400 0 Fax [phone]
ANALYTICAL
www.waypointanalytical.com
46245
EMA Resources Inc
Project
Reidsville,
NC
Brent Collins
Report Date : 04/13/2023
755 Yadkinville Rd
Information :
Received : 04/06/2023
Mocksville , NC 27028
Connie Cook
Report Number : 23-096-0014
REPOR T OF A
NA L YSIS
Project Manager
Lab No : 93338
Matrix: Solids
Sample ID : Reidsville
Sampled: 4/5/2023 0:00
Test
Results
Units
MDL
MQL DF Date / Time By Analytical
Analyzed Method
Selenium
<26.3
mg/Kg - dry
16.8
26.3 1 04/11/23 04:31 JTR 6010D
Sodium
5320
mg/Kg - dry
684
1320 1 04/11/23 04:31 JTR 6010D
Zinc
847
mg/Kg - dry
42.6
65.8 1 04/11/23 04:31 JTR 6010D
Sulfur
11700
mg/Kg - dry
273
526 1 04/11/23 04:31 JTR 6010D
Sodium Absorption Ratio
1.41
Ratio
0.01
0.01 1 04/11/23 04:31 CALCULATION
Qualifiers/ DF Dilution Factor
Definitions
J Estimated value
Page 6 of 8

(2)
WayPAoint..
NALYTICAL
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 ° Fax [phone]
www.waypointanalytical.com
Shipment Receipt Form
Customer Number: 46245
Customer Name: EMA Resources Inc
Report Number: 23-096-0014
Shipping Method
Fed Ex 0 US Postal 0 Lab 0 Other:
0 UPS 0 Client 0 Courier Thermometer ID: T135
Shipping container/cooler uncompromised?
* Yes
0 No
Number of coolers/boxes received
F
Custody seals intact on shipping container/cooler?
0 Yes
0 No
Not Present
Custody seals intact on sample bottles?
0 Yes
0 No
Not Present
Chain of Custody (COC) present?
Yes
0 No
COC agrees with sample label(s)?
U Yes
0 No
COC properly completed
U Yes
0 No
Samples in proper containers?
U Yes
0 No
Sample containers intact?
Yes
0 No
Sufficient sample volume for indicated test(s)?
Yes
0 No
All samples received within holding time?
Yes
0 No
Cooler temperature in compliance?
Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
Yes
0 No
Water - Sample containers properly preserved
0 Yes
0 No
0 N/A
Water - VOA vials free of headspace
0 Yes
0 No
N/A
Trip Blanks received with VOAs
0 Yes
0 No
0 N/A
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
0 N/A
F_ High concentration container (48 hr) F Low concentration EnCore samplers (48 hr)
F_ High concentration pre -weighed (methanol -14 d) Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included?
0 Yes
0 No
Comments:
Signature: Emily M. Peterson Date & Time: 04/06/2023 09:28:05
Page 7 of 8

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Page 8 of 8

Waypointo
ANALYTICAL
7/17/2023
EMA Resources Inc
Brent Collins
755 Yadkinville Rd
Mocksville, NC, 27028
Ref: Analytical Testing
Lab Report Number: 23-188-0007
Client Project Description: Reidsville, NC
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 1 Fax [phone]
www.waypointanalytical.com
Dear Brent Collins:
Waypoint Analytical, LLC. received sample(s) on 7/7/2023 for the analyses presented in the following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Where the laboratory was not responsible for the sampling
stage (refer to the chain of custody) results apply to the sample as received.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2021) and NELAC unless otherwise indicated. Any parameter
for which the laboratory is not officially NELAP accredited is indicated by a'—' symbol. These are not included in
the scope because NELAP accreditation is either not available or has not been applied for. Additional
certifications may be held/are available for parameters, where NELAP accreditation is not required or applicable.
A full list of certifications is available upon request.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Connie Cook
Project Manager
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 1 of 9

Waypointo
ANALYTICAL
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 ° Fax [phone]
www.waypointanalytical.corn
Certification Summary
Laboratory ID: WP MTN: Waypoint Analytical, LLC., Memphis, TN
State
Program
Lab ID
Expiration Date
Alabama
State Program
40750
02/29/2024
Arkansas
State Program
88-0650
02/07/2024
California
State Program
2904
06/30/2023
Florida
State Program
- NELAP
E871157
06/30/2024
Georgia
State Program
C044
11/14/2025
Georgia
State Program
04015
06/30/2024
Illinois
State Program
- NELAP
200078
10/10/2023
Kentucky
State Program
80215
06/30/2024
Kentucky
State Program
KY90047
12/31/2023
Louisiana
State Program
- NELAP
LA037
12/31/2023
Louisiana
State Program
- NELAP
04015
06/30/2024
Mississippi
State Program
MS
11/14/2025
North Carolina
State Program
47701
07/31/2023
North Carolina
State Program
415
12/31/2023
Pennsylvania
State Program
- NELAP
68-03195
05/31/2024
South Carolina
State Program
84002
06/30/2023
Tennessee
State Program
02027
11/14/2025
Texas
State Program
- NELAP
T104704180
09/30/2023
Virginia
State Program
00106
06/30/2024
Virginia
State Program
- NELAP
460181
09/14/2023
Page 1 of 1 00001/23-188-0007
Page 2 of 9

waypoint 2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 Fax [phone]
ANALYTICAL www.waypointanalytical.com
Sample Summary Table
Report Number: 23-188-0007
Client Project Description: Reidsville, NC
Lab No Client Sample ID
96684 Reidsville
Matrix Date Collected
Solids 07/06/202310:50
Date Received
07/07/2023
Page 3 of 9

Waypointo
ANALYTICAL
Client: EMA Resources Inc
Project: Reidsville, NC
Lab Report Number: 23-188-0007
Date: 7/17/2023
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 1 Fax [phone]
www.waypointanalytical.com
CASE NARRATIVE
Metals Analysis Method 6010D
Sample 96847 (NE Cake)
Analyte: Aluminum
QC Batch No: 1-692080/1-691569
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 96847 (NE Cake)
Analyte: Calcium
QC Batch No: 1-692080/1-691569
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 96847 (NE Cake)
Analyte: Iron
QC Batch No: 1-692095/1-691569
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 96847 (NE Cake)
Analyte: Potassium
QC Batch No: 1-692080/1-691569
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 96847 (NE Cake)
Analyte: Manganese
QC Batch No: 1-692080/1-691569
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 96847 (NE Cake)
Analyte: Phosphorus
QC Batch No: 1-692080/1-691569
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 96847 (NE Cake)
Analyte: Lead
QC Batch No: 1-692080/1-691569
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 96847 (NE Cake)
Analyte: Sulfur
Page 4 of 9

Waypointo
ANALYTICAL
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 Fax [phone]
www.waypointanalytical.com
QC Batch No: 1-692080/1-691569
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 96847 (NE Cake)
Analyte: Zinc
QC Batch No: 1-692080/1-691569
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Page 5 of 9

0
Waypoint, 2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 Fax [phone]
ANALYTICAL www.waypointanalytical.com
46245
EMA Resources Inc Project Reidsville, NC
Brent Collins Report Date : 07/17/2023
755 Yadkinville Rd Information : Received : 07/07/2023
Mocksville , NC 27028 n �
Connie Cook
Report Number : 23-188-0007
REPOR T OF A NA L YSIS
Project
Manager
Lab No : 96684
Matrix:
Solids
Sample ID : Reidsville
Sampled:
7/6/2023 10:50
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Method
Moisture
97.8
%
1
07/13/23 17:08
KDO
SW-DRYWT
Ammonia Nitrogen
17700
mg/Kg - dry
727
4550
1
07/15/23 12:00
JPJ
4500NH3C-2011
Nitrate+Nitrite-N
<45.5
mg/Kg - dry
45.5
227
1
07/11/23 15:09
CLP
4500NO3F-2016
Organic N
47270
mg/Kg - dry
727.3
4545
1
07/14/23 12:45
CALCULATION
pH
7.3
S.U.
1
07/11/2316:40
CNB
9045D
Total Solids
2.24
%
0.010
0.010
1
07/13/23 17:08
KDO
2540G-2011
Total Volatile Solids
77.5
%
0.010
0.010
1
07/13/23 17:08
KDO
2540G-2011
Total Kjeldahl Nitrogen
65000
mg/Kg - dry
455
11400
1
07/14/23 12:45
JPJ ')M-4500-NH3C-TKP
Phosphorus
29400
mg/Kg - dry
127
227
1
07/10/23 23:09
BKN
6010D
Aluminum
15900
mg/Kg - dry
211
227
1
07/10/23 23:09
BKN
6010D
Arsenic
<11.4
mg/Kg - dry
11.4
22.7
1
07/10/23 23:09
BKN
6010D
Cadmium
<2.27
mg/Kg - dry
2.27
4.55
1
07/10/23 23:09
BKN
6010D
Calcium
13700
mg/Kg - dry
1760
2270
1
07/10/23 23:09
BKN
6010D
Chromium
45.5
mg/Kg - dry
11.4
11.4
1
07/10/23 23:09
BKN
6010D
Copper
228
mg/Kg - dry
13.6
22.7
1
07/10/23 23:09
BKN
6010D
Iron
14200
mg/Kg - dry
389
455
1
07/10/23 23:09
BKN
6010D
Lead
60.0
mg/Kg - dry
9.09
13.6
1
07/10/23 23:09
BKN
6010D
Magnesium
5680
mg/Kg - dry
118
227
1
07/10/23 23:09
BKN
6010D
Manganese
586
mg/Kg - dry
15.9
22.7
1
07/10/23 23:09
BKN
6010D
Mercury
<0.977
mg/Kg - dry
0.977
8.09
1
07/10/23 11:54
MRE
7471A
Molybdenum
8.861
mg/Kg - dry
6.82
11.4
1
07/10/23 23:09
BKN
6010D
Nickel
23.7
mg/Kg - dry
6.82
11.4
1
07/10/23 23:09
BKN
6010D
Potassium
8450
mg/Kg - dry
282
455
1
07/10/23 23:09
BKN
6010D
Qualifiers/ DF
Dilution Factor
J
Estimated value
Definitions MQL
Method Quantitation Limit
Page 6 of 9

0
Waypoint,
2790 Whitten
Road, Memphis, TN 38133
Main 901.213.2400 0 Fax [phone]
ANALYTICAL
www.waypointanalytical.com
46245
EMA Resources Inc
Project
Reidsville,
NC
Brent Collins
Report Date : 07/17/2023
755 Yadkinville Rd
Information :
Received : 07/07/2023
Mocksville , NC 27028
Connie Cook
Report Number : 23-188-0007
REPOR T OF A
NA L YSIS
Project Manager
Lab No : 96684
Matrix: Solids
Sample ID : Reidsville
Sampled: 7/6/2023 10:50
Test
Results
Units
MDL
MQL DF Date / Time By Analytical
Analyzed Method
Selenium
<15.9
mg/Kg - dry
15.9
22.7 1 07/10/23 23:09 BKN 6010D
Sodium
6410
mg/Kg - dry
591
1140 1 07/10/23 23:09 BKN 6010D
Zinc
841
mg/Kg - dry
38.6
56.8 1 07/10/23 23:09 BKN 6010D
Sulfur
13500
mg/Kg - dry
236
455 1 07/10/23 23:09 BKN 6010D
Sodium Absorption Ratio
1.72
Ratio
0.01
0.01 1 07/10/23 23:09 CALCULATION
Qualifiers/ DF Dilution Factor
Definitions
3 Estimated value
Page 7 of 9

(2)
WayPAoint..
NALYTICAL
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 ° Fax [phone]
www.waypointanalytical.com
Shipment Receipt Form
Customer Number: 46245
Customer Name: EMA Resources Inc
Report Number: 23-188-0007
Shipping Method
Fed Ex 0 US Postal 0 Lab 0 Other:
0 UPS 0 Client 0 Courier Thermometer ID: T136
Shipping container/cooler uncompromised?
* Yes
0 No
Number of coolers/boxes received
F
Custody seals intact on shipping container/cooler?
0 Yes
0 No
Not Present
Custody seals intact on sample bottles?
0 Yes
0 No
Not Present
Chain of Custody (COC) present?
Yes
0 No
COC agrees with sample label(s)?
U Yes
0 No
COC properly completed
U Yes
0 No
Samples in proper containers?
U Yes
0 No
Sample containers intact?
Yes
0 No
Sufficient sample volume for indicated test(s)?
Yes
0 No
All samples received within holding time?
Yes
0 No
Cooler temperature in compliance?
Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
Yes
0 No
Water - Sample containers properly preserved
0 Yes
0 No
N/A
Water - VOA vials free of headspace
0 Yes
0 No
N/A
Trip Blanks received with VOAs
0 Yes
0 No
0 N/A
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
0 N/A
F_ High concentration container (48 hr) F Low concentration EnCore samplers (48 hr)
F_ High concentration pre -weighed (methanol -14 d) Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included?
0 Yes
0 No
Comments:
Signature: Makayla Weaver Date & Time: 07/07/2023 09:52:33
Page 8 of 9

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Page 9 of 9

Waypointo
ANALYTICAL
10/18/2023
EMA Resources Inc
Brent Collins
755 Yadkinville Rd
Mocksville, NC, 27028
Ref: Analytical Testing
Lab Report Number: 23-277-0012
Client Project Description: Reidsville, NC
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 1 Fax [phone]
www.waypointanalytical.com
Dear Brent Collins:
Waypoint Analytical, LLC. received sample(s) on 10/4/2023 for the analyses presented in the following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Where the laboratory was not responsible for the sampling
stage (refer to the chain of custody) results apply to the sample as received.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2021) and NELAC unless otherwise indicated. Any parameter
for which the laboratory is not officially NELAP accredited is indicated by a'—' symbol. These are not included in
the scope because NELAP accreditation is either not available or has not been applied for. Additional
certifications may be held/are available for parameters, where NELAP accreditation is not required or applicable.
A full list of certifications is available upon request.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Connie Cook
Project Manager
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 1 of 9

Waypointo
ANALYTICAL
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 ° Fax [phone]
www.waypointanalytical.corn
Certification Summary
Laboratory ID: WP MTN: Waypoint Analytical, LLC., Memphis, TN
State
Program
Lab ID
Expiration Date
Alabama
State Program
40750
02/29/2024
Arkansas
State Program
88-0650
02/07/2024
California
State Program
2904
06/30/2024
Florida
State Program
- NELAP
E871157
06/30/2024
Georgia
State Program
C044
11/14/2025
Georgia
State Program
04015
06/30/2024
Illinois
State Program
- NELAP
200078
10/31/2024
Kentucky
State Program
80215
06/30/2024
Kentucky
State Program
KY90047
12/31/2023
Louisiana
State Program
- NELAP
LA037
12/31/2023
Louisiana
State Program
- NELAP
04015
06/30/2024
Mississippi
State Program
MS
11/14/2025
North Carolina
State Program
47701
07/31/2024
North Carolina
State Program
415
12/31/2023
Pennsylvania
State Program
- NELAP
68-03195
05/31/2024
South Carolina
State Program
84002
06/30/2024
Tennessee
State Program
02027
11/14/2025
Texas
State Program
- NELAP
T104704180
09/30/2024
Virginia
State Program
00106
06/30/2024
Virginia
State Program
- NELAP
460181
09/14/2024
Page 1 of 1 00001/23-277-0012
Page 2 of 9

waypoint 2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 Fax [phone]
ANALYTICAL www.waypointanalytical.com
Sample Summary Table
Report Number: 23-277-0012
Client Project Description: Reidsville, NC
Lab No Client Sample ID
98032 Reidsville
Matrix Date Collected
Solids 10/03/202312:15
Date Received
10/04/2023
Page 3 of 9

Waypointo
ANALYTICAL
Client: EMA Resources Inc
Project: Reidsville, NC
Lab Report Number: 23-277-0012
Date: 10/18/2023
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 Fax [phone]
www.waypointanalytical.com
CASE NARRATIVE
Metals Analysis Method 6010D
Sample 98565
Analyte: Aluminum
QC Batch No: L709473/L708892
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 98565
Analyte: Calcium
QC Batch No: L709473/L708892
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 98565
Analyte: Potassium
QC Batch No: L709473/L708892
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Sample 98565
Analyte: Potassium
QC Batch No: L710024/L708892
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 98565
Analyte: Magnesium
QC Batch No: L709473/L708892
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 98565
Analyte: Manganese
QC Batch No: L709473/L708892
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 98565
Analyte: Sodium
QC Batch No: L709473/L708892
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 98565
Analyte: Phosphorus
QC Batch No: L709731/L708892
Page 4 of 9

Waypointo
ANALYTICAL
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 Fax [phone]
www.waypointanalytical.com
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 98565
Analyte: Sulfur
QC Batch No: 1-709473/1-708892
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Solids Total Mercury Analysis - CVAA Method 7471A
Sample 97716 (Annual Sludge)
Analyte: Mercury
QC Batch No: 1-709569/1-709290
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Page 5 of 9

0
Waypoint, 2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 Fax [phone]
ANALYTICAL www.waypointanalytical.com
46245
EMA Resources Inc Project Reidsville, NC
Brent Collins Report Date : 10/18/2023
755 Yadkinville Rd Information : Received : 10/04/2023
Mocksville , NC 27028 n �
Connie Cook
Report Number : 23-277-0012
REPOR T OF A NA L YSIS
Project
Manager
Lab No : 98032
Matrix:
Solids
Sample ID : Reidsville
Sampled:
10/3/2023
12:15
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Method
Moisture
99.049
%
0.010
0.010
1
10/05/23 16:10
CAH
SW-DRYWT
Ammonia Nitrogen
19300
mg/Kg - dry
1680
10500
1
10/18/23 14:37
JPJ
4500NH3C-2011
Nitrate+Nitrite-N
2043
mg/Kg - dry
105
526
1
10/11/23 15:29
CLP
4500NO3F-2016
Organic N
91060
mg/Kg - dry
1682
10520
1
10/18/23 10:30
CALCULATION
pH
7.4
S.U.
1
10/06/2316:07
CNB
9045D
Total Solids
0.951
%
0.010
0.010
1
10/05/23 16:10
CAH
2540G-2011
Total Volatile Solids
59.7
%
0.010
0.010
1
10/05/23 16:10
CAH
2540G-2011
Total Kjeldahl Nitrogen
110000
mg/Kg - dry
1050
26300
1
10/18/23 10:30
JPJ ')M-4500-NH3C-TKP
Phosphorus
43200
mg/Kg - dry
294
526
1
10/06/23 23:35
TJS
6010D
Aluminum
21900
mg/Kg - dry
489
526
1
10/06/23 23:35
BKN
6010D
Arsenic
<26.3
mg/Kg - dry
26.3
52.6
1
10/06/23 23:35
BKN
6010D
Cadmium
<5.26
mg/Kg - dry
5.26
10.5
1
10/06/23 23:35
BKN
6010D
Calcium
23000
mg/Kg - dry
4070
5260
1
10/06/23 23:35
BKN
6010D
Chromium
58.1
mg/Kg - dry
26.3
26.3
1
10/06/23 23:35
BKN
6010D
Copper
377
mg/Kg - dry
31.5
52.6
1
10/06/23 23:35
BKN
6010D
Iron
22500
mg/Kg - dry
899
1050
1
10/06/23 23:35
BKN
6010D
Lead
79.0
mg/Kg - dry
21.0
31.5
1
10/06/23 23:35
BKN
6010D
Magnesium
8010
mg/Kg - dry
273
526
1
10/06/23 23:35
BKN
6010D
Manganese
944
mg/Kg - dry
36.8
52.6
1
10/06/23 23:35
BKN
6010D
Mercury
<2.39
mg/Kg - dry
2.39
19.8
1
10/09/23 11:47
MRE
7471A
Molybdenum
<15.8
mg/Kg - dry
15.8
26.3
1
10/06/23 23:35
BKN
6010D
Nickel
34.4
mg/Kg - dry
15.8
26.3
1
10/06/23 23:35
BKN
6010D
Potassium
11100
mg/Kg - dry
652
1050
1
10/06/23 23:35
BKN
6010D
Qualifiers/ DF
Dilution Factor
J
Estimated value
Definitions MQL
Method Quantitation Limit
Page 6 of 9

0
Waypoint,
2790 Whitten
Road, Memphis, TN 38133
Main 901.213.2400 0 Fax [phone]
ANALYTICAL
www.waypointanalytical.com
46245
EMA Resources Inc
Project
Reidsville,
NC
Brent Collins
Report Date : 10/18/2023
755 Yadkinville Rd
Information :
Received : 10/04/2023
Mocksville , NC 27028
Connie Cook
Report Number : 23-277-0012
REPOR T OF A
NA L YSIS
Project Manager
Lab No : 98032
Matrix: Solids
Sample ID : Reidsville
Sampled: 10/3/2023 12:15
Test
Results
Units
MDL
MQL DF Date / Time By Analytical
Analyzed Method
Selenium
<36.8
mg/Kg - dry
36.8
52.6 1 10/06/23 23:35 BKN 6010D
Sodium
17100
mg/Kg - dry
1370
2630 1 10/06/23 23:35 BKN 6010D
Zinc
1540
mg/Kg - dry
89.4
131 1 10/06/23 23:35 BKN 6010D
Sulfur
18900
mg/Kg - dry
547
1050 1 10/06/23 23:35 BKN 6010D
Sodium Absorption Ratio
2.41
Ratio
0.01
0.01 1 10/06/23 23:35 CALCULATION
Qualifiers/ DF Dilution Factor
Definitions
3 Estimated value
Page 7 of 9

(2)
WayPAoint..
NALYTICAL
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 ° Fax [phone]
www.waypointanalytical.com
Shipment Receipt Form
Customer Number: 46245
Customer Name: EMA Resources Inc
Report Number: 23-277-0012
Shipping Method
Fed Ex 0 US Postal 0 Lab 0 Other:
0 UPS 0 Client 0 Courier Thermometer ID: T99
Shipping container/cooler uncompromised?
* Yes
0 No
Number of coolers/boxes received
F
Custody seals intact on shipping container/cooler?
0 Yes
0 No
Not Present
Custody seals intact on sample bottles?
0 Yes
0 No
Not Present
Chain of Custody (COC) present?
Yes
0 No
COC agrees with sample label(s)?
U Yes
0 No
COC properly completed
U Yes
0 No
Samples in proper containers?
U Yes
0 No
Sample containers intact?
Yes
0 No
Sufficient sample volume for indicated test(s)?
Yes
0 No
All samples received within holding time?
Yes
0 No
Cooler temperature in compliance?
Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
Yes
0 No
Water - Sample containers properly preserved
0 Yes
0 No
N/A
Water - VOA vials free of headspace
0 Yes
0 No
N/A
Trip Blanks received with VOAs
0 Yes
0 No
0 N/A
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
0 N/A
F_ High concentration container (48 hr) F Low concentration EnCore samplers (48 hr)
F_ High concentration pre -weighed (methanol -14 d) Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included?
0 Yes
0 No
Comments:
Signature: Makayla Weaver Date & Time: 10/04/2023 09:57:11
Page 8 of 9

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Page 9 of 9

PaceAnalytical
ANALYTICAL REPORT
January 16, 2023
F � e0000-
EMA Resources
Sample Delivery Group: L1573606
Samples Received: 01/06/2023
Project Number:
Description: Sludge
Report To: Mr. Brent Collins
755 Yadkinville Road
Mocksville, NC 27028
Entire Report Reviewed By
Z'Ie4-�7� V�
Reagan Johnson
Project Manager
Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be
reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pace
Analytical National is performed per guidance provided in laboratory standard operating procedures ENV-SOP-MTJL-0067 and ,
ENV-SOP-MTJL-0068. Where sampling conducted by the customer, results relate to the accuracy of the information provided,
and as the samples are received.
r
i
I
M
FSS
Rn
Rr
FQc
E7GI
rAl
FSC
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1573606 01/16/2311:52 1 of 22

TABLE OF CONTENTS
Cp: Cover Page
1
FP1
Tc: Table of Contents
2
Ss: Sample Summary
3
Cn: Case Narrative
4
Sr: Sample Results
5
FSS
REIDSVILLE L1573606-01
5
rqn
Qc: Quality Control Summary
7
Wet Chemistry by Method 9012 B
7
Fr]
Wet Chemistry by Method 9034-9030B
8
Wet Chemistry by Method 9045D
9
FQ Cl
Wet Chemistry by Method D93/1010A
10
GI
Mercury by Method 7470A
11
Metals (ICP) by Method 6010D
12
rAl
Volatile Organic Compounds (GC/MS) by Method 8260D
13
Chlorinated Acid Herbicides (GC) by Method 8151A
15
FC
Pesticides (GC) by Method 80818
16
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
17
GI: Glossary of Terms
19
Al: Accreditations & Locations
20
Sc: Sample Chain of Custody
21
ACCOUNT: PROJECT: SDG:
DATE/TIME:
PAGE:
EMA Resources L1573606
01/16/23 11:52
2 of 22

SAMPLE SUMMARY
REIDSVILLE L1573606-01 Waste
Collected by
Brent Collins
Collected date/time
01/05/2311:15
Received date/time
01/06/2309:00
Method
Batch
Dilution Preparation
Analysis
Analyst
Location
date/time
date/time
Preparation by Method 1311
WG1984764
1 01/07/2313:16
01/07/2313:16
BTP
Mt. Juliet, TN
Preparation by Method 1311
WG1984782
1 01/07/2315:30
01/07/2315:30
BTP
Mt. Juliet, TN
Wet Chemistry by Method 9012 B
WG1983961
1 01/09/2317:11
01/10/2314:38
CAT
Mt. Juliet, TN
Wet Chemistry by Method 9034-9030B
WG1983808
1 01/10/2315:00
01/11/2319:30
AW
Mt. Juliet, TN
Wet Chemistry by Method 9045D
WG1985927
1 01/10/2310:20
01/10/2312:00
SIDE
Mt. Juliet, TN
Wet Chemistry by Method D93/1010A
WG1987120
1 01/12/23 02:25
01/12/23 02:25
TOP
Mt. Juliet, TN
Mercury by Method 7470A
WG1985081
1 01/08/2317:19
01/09/2311:21
SRT
Mt. Juliet, TN
Metals (ICP) by Method 6010D
WG1985255
1 01/09/23 09:48
01/09/2315:08
ZSA
Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260D
WG1985098
1 01/09/2316:32
01/09/2316:32
ACG
Mt. Juliet, TN
Chlorinated Acid Herbicides (GC) by Method 8151A
WG1985228
1 01/12/23 08:21
01/13/2319:18
JMB
Mt. Juliet, TN
Pesticides (GC) by Method 8081B
WG1985657
1 01/11/2310:45
01/12/2315:39
RDH
Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
WG1985658
1 01/13/23 05:38
01/13/2313:59
JRM
Mt. Juliet, TN
FP1
FTC
M
rqn
Fr]
PC]
I qI
FAI
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ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1573606 01/16/23 11:52 3 of 22

CASE NARRATIVE
All sample aliquots were received at the correct temperature, in the proper containers, with the FP1
appropriate preservatives, and within method specified holding times, unless qualified or notated within
the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples FTChave been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control
are within established criteria except where addressed in this case narrative, a non-conformance form
or properly qualified within the sample results. By my digital signature below, I affirm to the best of my FSS
knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the
quality of the data have been identified by the laboratory, and no information or data have been
knowingly withheld that would affect the quality of the data.
Fr]
.� FQc
�GI
Reagan Johnson rAl
Project Manager
LE
Project Narrative
All Reactive Cyanide results reported in the attached report were determined as totals using method 9012 B.
All Reactive Sulfide results reported in the attached report were determined as totals using method 9034-9030B.
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1573606 01/16/23 11:52 4 of 22

SAMPLE RESULTS - 01
L1573606
REIDSVILLE
Collected date/time: 01/05/23 11:15
Preparation by Method 1311
Result
Analyte
TCLP Extraction
TCLP ZHE Extraction -
Fluid 1
Initial pH 7.16
Final pH 4.77
Wet Chemistry by Method 9012 B
Qualifier Prep Batch
date / time
1/7/2023 3:30:14 PM WG1984782
1/7/20231:16:01 PM WG1984764
1/7/2023 3:30:14 PM WG1984782
1/7/2023 3:30:14 PM WG1984782
1/7/2023 3:30:14 PM WG1984782
Result Qualifier
RDL
Analyte mg/kg
mg/kg
Reactive Cyanide ND
0.250
Wet Chemistry by Method 9034-9030B
Result Qualifier
RDL
Analyte mg/kg
mg/kg
Reactive Sulfide ND
75.0
Wet Chemistry by Method 9045D
Dilution Analysis Batch
date / time
1 01/10/202314:38 WG1983961
Dilution Analysis Batch
date / time
1 01/11/202319:30 WG1983808
Result Qualifier Dilution Analysis Batch
Analyte su date / time
Corrosivity by pH 7.46 T8 1 01/10/202312:00 WG1985927
Sample Narrative:
L1573606-01 WG1985927: 7.46 at 20AC
Wet Chemistry by Method D93/1010A
Result Qualifier Dilution Analysis
Analyte Deg. F date / time
Batch
Ignitability DNI at 170 1 01/12/2023 02:25 WG1987120
Mercury by Method 7470A
Result
Analyte mg/I
Mercury ND
Metals (ICP) by Method 6010D
Qualifier RDL Limit
mg/I mg/I
0.0100 0.20
Result
Qualifier RDL
Limit
Analyte
mg/I
mg/I
mg/I
Arsenic
ND
0.100
5
Barium
ND
0.100
100
Cadmium
ND
0.100
1
Chromium
ND
0.100
5
Lead
ND
0.100
5
Selenium
ND
0.100
1
Silver
ND
0.100
5
Volatile Organic Compounds (GC/MS) by Method 8260D
Analyte
Benzene
Carbon tetrachloride
Chlorobenzene
Result
Qualifier RDL
Limit
mg/I
mg/I
mg/I
ND
0.0500
0.50
ND
0.0500
0.50
ND
0.0500
100
ND
0.250
6
ACCOUNT: PROJECT
EMA Resources
Dilution Analysis Batch
date / time
1 01/09/202311:21 WG1985081
Dilution Analysis Batch
date / time
1 01/09/202315:08
WG1985255
1 01/09/202315:08
WG1985255
1 01/09/202315:08
WG1985255
1 01/09/202315:08
WG1985255
1 01/09/202315:08
WG1985255
1 01/09/202315:08
WG1985255
1 01/09/202315:08
WG1985255
FP1
FTc
FSS
rqn
FC]
I ql
FAI
FSC
Dilution Analysis
Batch
date / time
1 01/09/202316:32
WG1985098
1 01/09/202316:32
WG1985098
1 01/09/202316:32
WG1985098
1 01/09/202316:32
WG1985098
SDG:
DATE/TIME: PAGE:
L1573606
01/16/23 11:52 5 of 22

REIDSVILLE SAMPLE RESULTS - 01
Collected date/time: 01/05/23 11:15 L1573606
Volatile Organic Compounds (GC/MS) by Method 8260D
Result Qualifier
RDL
Limit
Dilution Analysis
Batch
Analyte
mg/I
mg/I
mg/I
date/time
1,2-Dichloroethane
ND
0.0500
0.50
1 01/09/202316:32
WG1985098
1,1-Dichloroethene
ND
0.0500
0.70
1 01/09/202316:32
WG1985098
2-Butanone (MEK)
ND
0.500
200
1 01/09/202316:32
WG1985098
Tetrachloroethene
ND
0.0500
0.70
1 01/09/202316:32
WG1985098
Trichloroethene
ND
0.0500
0.50
1 01/09/202316:32
WG1985098
Vinyl chloride
ND
0.0500
0.20
1 01/09/202316:32
WG1985098
(S) Toluene-d8
107
80.0-120
01/09/20231632
WG1985098
(S) 4-Bromof/uorobenzene
102
77.0-126
01/09/202316:32
WG1985098
(S)1,2-Dichloroethane-d4
89.5
70.0-130
01/09/202316:32
WG1985098
Chlorinated Acid Herbicides (GC) by Method
8151A
Result Qualifier
RDL
Limit
Dilution Analysis
Batch
Analyte
mg/I
mg/I
mg/I
date/time
2,4,5-TP (Silvex)
ND
0.00200
1
1 01/13/202319:18
WG1985228
2,4-D
ND
0.00200
10
1 01/13/202319:18
WG1985228
(S)2,4-Dichloropheny/Acetic Acid
93.6
14.0-158
011131202319:18
WG1985228
Pesticides (GC) by Method
8081B
Result
Qualifier RDL
Limit
Dilution Analysis
Batch
Analyte
mg/I
mg/I
mg/I
date / time
Chlordane
ND
0.00500
0.03
1 01/12/202315:39
WG1985657
Endrin
ND
0.00500
0.02
1 01/12/202315:39
WG1985657
Heptachlor
ND
0.00500
0.0080
1 01/12/202315:39
WG1985657
Heptachlor epoxide
ND
0.00500
0.0080
1 01/12/202315:39
WG1985657
Lindane
ND
0.00500
0.40
1 01/12/202315:39
WG1985657
Methoxychlor
ND
0.00500
10
1 01/12/202315:39
WG1985657
Toxaphene
ND
0.0100
0.50
1 01/12/202315:39
WG1985657
(S) Decachlorobipheny/
58.0
10.0-128
01/12/202315:39
WG1985657
(S) Tetrach/oro-m-xylene
45.6
10.0-127
01/12/202315:39
WG1985657
Semi Volatile Organic Compounds
(GC/MS) by Method 8270E
Result
Analyte mg/I
1,4-Dichlorobenzene
2,4-Dinitrotoluene
Hexachlorobenzene
Hexachloro-1,3-butadiene
Hexachloroethane
Nitrobenzene
Pyridine
3&4-Methyl Phenol
2-Methylphenol
Pentachlorophenol
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
(S) 2-Fluorophenol
(S) Phenol-d5
(S) Nitrobenzene-d5
(S) 2-F/uorobiphenyl
(S) 2,4,6-Tribromophenol
(S) p-Terphenyl-d14
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
31.3
18.6
56.3
60.0
71.5
80.6
Qualifier RDL
mg/I
0.100
0.100
0.100
0.100
0.100
0.100
0.100
0.100
0.100
0.100
0.100
0.100
10.0-120
10.0-120
10.0-127
10.0-130
10.0-155
10.0-128
Limit
mg/I
7.50
0.13
0.13
0.50
3
2
5
400
200
100
400
2
Dilution Analysis Batch
date / time
01/13/202313:59
01/13/202313:59
01/13/202313:59
01/13/202313:59
01/13/202313:59
01/13/202313:59
01/13/202313:59
01/13/202313:59
01/13/202313:59
01/13/202313:59
01/13/202313:59
01/13/202313:59
011131202313:59
011131202313:59
011131202313:59
011131202313:59
011131202313:59
011131202313:59
WG1985658
WG1985658
WG1985658
WG1985658
WG1985658
WG1985658
WG1985658
WG1985658
WG1985658
WG1985658
WG1985658
WG1985658
WG1985658
WG1985658
WG1985658
WG1985658
WG1985658
WG1985658
FP1
FTc
FSS
Fqn
FC]
I ql
FAI
FSC
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1573606 01/16/23 11:52 6 of 22

WG1983961 QUALITY CONTROL SUMMARY
Wet Chemistry by Method 9012 B L1573606-01
Method Blank (MB)
(MB) R3879579-1 01/10/2314:17
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Reactive Cyanide U 0.0390 0.250
L1572587-01 Original Sample (OS) • Duplicate (DUP)
(OS) L1572587-01 01/10/2314:22 • (DUP) R3879579-3 01/10/2314:23
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte mg/kg mg/kg % %
Reactive Cyanide ND ND 1 0.000 20
L1573606-01 Original Sample (OS) • Duplicate (DUP)
(OS) L1573606-01 01/10/2314:38 • (DUP) R3879579-6 01/10/2314:39
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte mg/kg mg/kg % %
Reactive Cyanide ND ND 1 0.000 20
Laboratory Control Sample (LCS)
(LCS) R3879579-2 01/10/2314:18
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg % %
Reactive Cyanide 2.50 2.34 93.7 85.0-115
L1572730-04 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1572730-04 01/10/2315:05 • (MS) R3879579-4 01/10/2314:26 • (MSD) R3879579-5 01/10/2314:29
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD
Analyte mg/kg mg/kg mg/kg mg/kg % % % %
Reactive Cyanide 1.67 0.930 1.97 2.17 62.6 74.2 1 75.0-125 9.32
Sample Narrative:
MS: Matrix spike failure due to matrix.
MSD: Matrix spike failure due to matrix.
RPD Limits
20
— I
Cp
FTc
FSS
rqn
FSr
_ �GI
FAI
FSC
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1573606 01/16/2311:52 7 of 22

WG1983808 QUALITY CONTROL SUMMARY
Wet Chemistry by Method 9034-9030B L1573606-01
Method Blank (MB)
(MB) R3880472-1 01/11/2319:30
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Reactive Sulfide U 30.0 75.0
Laboratory Control Sample (LCS)
(LCS) R3880472-2 01/11/23 19:30
Spike Amount LCS Result LCS Rec.
Analyte mg/kg mg/kg %
Reactive Sulfide 100 80.2 80.2
Rec. Limits LCS Qualifier
53.8-124
L1573683-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1573683-01 01/11/2319:30 • (MS) R3880472-3 01/11/2319:30 • (MSD) R3880472-4 01/11/2319:30
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD
Analyte mg/kg mg/kg mg/kg mg/kg % % % %
Reactive Sulfide 100 ND ND ND 39.5 35.4 1 10.0-136 0.000
RPD Limits
20
— I
Cp
FTc
FSS
rqn
FSr
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_ $AI
FSC
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1573606 01/16/2311:52 8 of 22

WG1985927 QUALITY CONTROL SUMMARY
Wet Chemistry by Method 9045D L1573606-01
L1573606-01 Original Sample (OS) • Duplicate (DUP)
(OS) L1573606-01 01/10/2312:00 • (DUP) R3879476-2 01/10/2312:00
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte su su % %
Corrosivity by pH 7.46 7.45 1 0.134 1
Sample Narrative:
OS: 7.46 at 20.4C
DUP: 7.45 at 20.5C
Laboratory Control Sample (LCS)
(LCS) R3879476-1 01/10/2312:00
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte su su % %
Corrosivity by pH 10.0 9.98 99.8 99.0-101
Sample Narrative:
LCS: 9.98 at 19.4C
FP1
FTc
FSS
LEI
FSr
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FAI
FSC
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1573606 01/16/2311:52 9 of 22

WG1987120 QUALITY CONTROL SUMMARY
Wet Chemistry by Method D93/1010A L1573606-01
L1573591-01 Original Sample (OS) • Duplicate (DUP)
(OS) L1573591-01 01/12/23 02:25 • (DUP) R3880201-3 01/12/23 02:25
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte Deg. F Deg. F % %
Ignitability 97.0 93.0 1 4.21 10
L1573699-06 Original Sample (OS) • Duplicate (DUP)
(OS) L1573699-06 01/12/23 02:25 • (DUP) R3880201-4 01/12/23 02:25
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte Deg. F Deg. F % %
Ignitability 83.0 83.0 1 0.000 10
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3880201-1 01/12/23 02:25 • (LCSD) R3880201-2 01/12/23 02:25
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte Deg. F Deg. F Deg. F % % % % %
Ignitability 126 131 129 104 102 95.6-104 1.54 10
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1573606 01/16/2311:52 10 of 22
FP1
FTc
FSS
rqn
FSr
�GI
FAI
FSC

WG1985081
Mercury by Method 7470A
Method Blank (MB)
(MB) R3879204-1 01/09/2310:44
MB Result
Analyte mg/1
Mercury U
MB Qualifier MB MDL MB RDL
mg/I mg/1
0.00330 0.0100
Laboratory Control Sample (LCS)
(LCS) R3879204-2 01/09/2310:46
Spike Amount LCS Result LCS Rec.
Analyte mg/1 mg/1 %
Mercury 0.0300 0.0296 98.7
QUALITY CONTROL SUMMARY
L1573606-01
Rec. Limits LCS Qualifier
80.0-120
L1572863-02 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1572863-02 01/09/2310:48 • (MS) R3879204-3 01/09/2310:50 • (MSD) R3879204-4 01/09/2310:52
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD
Analyte mg/1 mg/1 mg/I mg/1 % % % %
Mercury 0.0300 ND 0.0295 0.0297 98.5 99.1 1 75.0-125 0.594
RPD Limits
20
— I
Cp
FTc
FSS
rqn
FSr
�GI
_ $AI
FSC
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1573606 01/16/2311:52 11 of 22

WG1985255
Metals (ICP) by Method 6010D
Method Blank (MB)
(MB) R3879324-1 01/09/2314:17
MB Result
Analyte mg/I
Arsenic
Barium
Cadmium
Chromium
Lead
Selenium
Silver
U
U
U
U
U
0.0829
U
MB Qualifier MB MDL
mg/I
0.0333
0.0333
0.0333
0.0333
0.0333
J 0.0333
0.0333
Laboratory Control Sample (LCS)
MB RDL
mg/I
0.100
0.100
0.100
0.100
0.100
0.100
0.100
QUALITY CONTROL SUMMARY
L1573606-01
(LCS) R3879324-2 01/09/2314:20
Spike Amount
LCS Result
LCS Rec.
Rec. Limits LCS Qualifier
Analyte mg/I
mg/I
%
%
Arsenic 10.0
9.37
93.7
80.0-120
Barium 10.0
9.87
98.7
80.0-120
Cadmium 10.0
9.48
94.8
80.0-120
Chromium 10.0
9.54
95.4
80.0-120
Lead 10.0
9.50
95.0
80.0-120
Selenium 10.0
9.51
95.1
80.0-120
Silver 2.00
1.74
86.9
80.0-120
L1572846-02 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1572846-02 01/09/2314:22 • (MS) R3879324-4 01/09/2314:28 • (MSD) R3879324-5 01/09/2314:31
Spike Amount
Original Result
MS Result
MSD Result
MS Rec.
MSD Rec.
Analyte
mg/I
mg/I
mg/I
mg/I
%
%
Arsenic
10.0
ND
9.48
9.38
94.1
93.1
Barium
10.0
ND
9.99
9.88
99.9
98.8
Cadmium
10.0
ND
9.48
9.38
94.8
93.8
Chromium
10.0
ND
9.52
9.69
95.2
96.9
Lead
10.0
ND
9.67
9.56
96.7
95.6
Selenium
10.0
ND
9.71
9.59
97.1
95.9
Silver
2.00
ND
1.71
1.75
85.4
87.5
Dilution Rec. Limits
MS Qualifier MSD Qualifier RPD
1 75.0-125
1.06
1 75.0-125
1.15
1 75.0-125
1.10
1 75.0-125
1.82
1 75.0-125
1.23
1 75.0-125
1.28
1 75.0-125
2.46
RPD Limits
20
20
20
20
20
20
20
FP1
FTC
FSS
rqn
FSr
�GI
FAI
FSC
ACCOUNT:
EMA Resources
PROJECT:
SDG: DATE/TIME:
L1573606 01/16/2311:52
PAGE:
12 of 22

WG1985098 QUALITY CONTROL SUMMARY
Volatile Organic Compounds (GC/MS) by Method 8260D L1573606-01
Method Blank (MB)
(MB) R3879887-3 01/09/2314:30
MB Result MB Qualifier
Analyte
mg/I
Benzene
U
Carbon tetrachloride
U
Chlorobenzene
U
Chloroform
U
1,2-Dichloroethane
U
1,1-Dichloroethene
U
2-Butanone (MEK)
U
Tetrachloroethene
U
Trichloroethene
U
Vinyl chloride
U
(S) Toluene-d8
108
(S) 4-Bromof/uorobenzene 105
(S)1,2-Dichloroethane-d4 89.2
Laboratory Control Sample (LCS)
(LCS) R3879887-1 01/09/2312:49
Spike Amount
LCS Result
Analyte
mg/I
mg/I
Benzene
0.250
0.225
Carbon tetrachloride
0.250
0.224
Chlorobenzene
0.250
0.252
Chloroform
0.250
0.220
1,2-Dichloroethane
0.250
0.219
1,1-Dichloroethene
0.250
0.221
2-Butanone (MEK)
1.25
1.15
Tetrachloroethene
0.250
0.259
Trichloroethene
0.250
0.241
Vinyl chloride
0.250
0.203
(S) Toluene-d8
(S) 4-Bromofluorobenzene
(S)1,2-Dichloroethane-d4
MB MDL
mg/I
0.0167
0.0167
0.0167
0.0833
0.0167
0.0167
0.167
0.0167
0.0167
0.0167
LCS Rec.
90.0
89.6
101
88.0
87.6
88.4
92.0
104
96.4
81.2
105
102
89.6
MB RDL
mg/I
0.0500
0.0500
0.0500
0.250
0.0500
0.0500
0.500
0.0500
0.0500
0.0500
80.0-120
77.0-126
70.0-130
Rec. Limits LCS Qualifier
70.0-123
68.0-126
80.0-121
73.0-120
70.0-128
71.0-124
44.0-160
72.0-132
78.0-124
67.0-131
80.0-120
77.0-126
70.0-130
FP1
FTC
FSS
rqn
FSr
�GI
FAI
FSC
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1573606 01/16/2311:52 13 of 22

WG1985098 QUALITY CONTROL SUMMARY
Volatile Organic Compounds (GC/MS) by Method 8260D L1573606-01
L1573727-03 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1573727-03 01/09/2318:35 • (MS) R3879887-4 01/09/2319:36 • (MSD) R3879887-5 01/09/2319:56
Spike Amount
Original Result
MS Result
MSD Result
MS Rec.
MSD Rec.
Analyte
mg/I
mg/I
mg/I
mg/I
%
%
Benzene
0.250
0.162
0.365
0.384
81.2
88.8
Carbon tetrachloride
0.250
ND
0.248
0.255
99.2
102
Chlorobenzene
0.250
ND
0.245
0.265
98.0
106
Chloroform
0.250
ND
ND
ND
88.0
92.8
1,2-Dichloroethane
0.250
ND
0.211
0.219
84.4
87.6
1,1-Dichloroethene
0.250
ND
0.230
0.235
92.0
94.0
2-Butanone (MEK)
1.25
ND
1.01
1.06
80.8
84.8
Tetrachloroethene
0.250
ND
0.253
0.268
101
107
Trichloroethene
0.250
ND
0.242
0.248
96.8
99.2
Vinyl chloride
0.250
ND
0.220
0.228
88.0
91.2
(S) Toluene-d8
106
106
(S) 4-Bromof/uorobenzene
103
102
(S)1,2-Dichloroethane-d4
91.6
90.9
Dilution Rec. Limits MS Qualifier
ii.v-lots
23.0-159
33.0-152
29.0-154
29.0-151
11.0-160
10.0-160
10.0-160
10.0-160
10.0-160
80.0-120
77.0-126
70.0-130
MSD Qualifier RPD
5.07
2.78
7.84
5.31
3.72
2.15
4.83
5.76
2.45
3.57
RPD Limits
27
28
27
28
27
29
32
27
25
27
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SDG:
L1573606
DATE/TIME:
01/16/2311:52
PAGE:
14of22

WG1985228
Chlorinated Acid Herbicides (GC) by Method 8151A
Method Blank (MB)
(MB) R3880854-1 01/13/2313:42
MB Result
Analyte mg/I
2,4,5-TP (Silvex) U
2,4-D U
(S)2,4-Dichloropheny/Acetic 874
Acid
MB Qualifier MB MDL
mg/I
0.000667
0.000667
Laboratory Control Sample (LCS)
QUALITY CONTROL SUMMARY
L1573606-01
MB RDL
Mg/1
0.00200
0.00200
14.0-158
(LCS) R3880854-2 01/13/2313:52
Spike Amount
LCS Result
LCS Rec.
Rec. Limits LCS Qualifier
Analyte mg/1
mg/1
%
%
2,4,5-TP (Silvex) 0.0500
0.0467
93.4
50.0-125
2,4-D 0.0500
0.0589
118
50.0-120 E
(S) 2,4-Dich/oropheny/Acetic
108
14.0-158
Acid
L1572770-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1572770-01 01/13/2316:44 • (MS) R3880854-3 01/13/2316:55 • (MSD) R3880854-4 01/13/2317:06
Spike Amount
Original Result
MS Result
MSD Result
MS Rec.
MSD Rec.
Analyte
mg/I
mg/1
mg/I
mg/I
%
%
2,4,5-TP (Silvex)
0.0500
ND
0.0423
0.0517
84.6
103
2,4-D
0.0500
ND
0.0513
0.0567
103
113
(S) 2,4-Dichloropheny/Acetic
95.2
96.4
Acid
Dilution Rec. Limits MS Qualifier MSD Qualifier RPD
1 50.0-125 E 20.0
1 50.0-120 E E 10.0
14.0-158
RPD Limits
o�
20
20
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ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1573606 01/16/2311:52 15 of 22

WG1985657
Pesticides (GC) by Method 8081B
Method Blank (MB)
(MB) R3880772-1 01/12/2315:21
MB Result
Analyte
mg/1
Chlordane
U
Endrin
U
Heptachlor
U
Heptachlor epoxide
U
Gamma BHC
U
Methoxychlor
U
Toxaphene
U
(S) Decachlorobipheny/
59.8
(S) Tetrach/oro-m-xylene
33.8
MB Qualifier MB MDL MB RDL
mg/I mg/1
Laboratory Control Sample (LCS)
QUALITY CONTROL SUMMARY
L1573606-01
0.00167
0.00500
0.00167
0.00500
0.00167
0.00500
0.00167
0.00500
0.00167
0.00500
0.00167
0.00500
0.00333
0.0100
10.0-128
10.0-127
(LCS) R3880772-2 01/12/2315:30
Spike Amount
Analyte mg/1
LCS Result
mg/1
LCS Rec.
%
Endrin
0.0100
0.0103
103
Heptachlor
0.0100
0.00758
75.8
Heptachlor epoxide
0.0100
0.0100
100
Gamma BHC
0.0100
0.00783
78.3
Methoxychlor
0.0100
0.0104
104
(S) Decachlorobipheny/
59.0
(S) Tetrach/oro-m-xylene
38.4
Rec. Limits LCS Qualifier
27.0-132
57.0-130
55.0-129
54.0-155
10.0-128
10.0-127
L1573606-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1573606-01 01/12/2315:39 • (MS) R3880772-3 01/12/2315:49 • (MSD) R3880772-4 01/12/2315:58
Spike Amount
Original Result
MS Result
MSD Result
MS Rec.
MSD Rec.
Analyte
mg/1
mg/1
mg/I
mg/1
%
%
Endrin
0.0100
ND
0.00835
0.0111
83.5
ill
Heptachlor
0.0100
ND
0.00655
0.00859
65.5
85.9
Heptachlor epoxide
0.0100
ND
0.00796
0.0106
79.6
106
Gamma BHC
0.0100
ND
0.00685
0.00899
68.5
89.9
Methoxychlor
0.0100
ND
0.00804
0.0108
80.4
108
(S) Decachlorobipheny/
51.3
69.6
(S) Tetrach/oro-m-xylene
31.1
39.9
Dilution Rec. Limits
MS Qualifier MSD Qualifier RPD
1 10.0-160
28.3
1 16.0-136
26.9
1 10.0-160
28.4
1 14.0-141
27.0
1 10.0-160
29.3
10.0-128
10.0-127
RPD Limits
39
40
36
40
34
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EMA Resources L1573606 01/16/2311:52 16 of 22

WG1985658
QUALITY CONTROL SUMMARY
Semi Volatile Organic Compounds
(GC/MS) by
Method 8270E
L1573606-01
Method Blank (MB)
(MB) R3880808-2 01/13/2311:29
MB Result
MB Qualifier
MB MDL
MB RDL
Analyte mg/I
mg/I
mg/I
1,4-Dichlorobenzene U
0.0333
0.100
2,4-Dinitrotoluene U
0.0333
0.100
Hexachlorobenzene U
0.0333
0.100
Hexachloro-1,3-butadiene U
0.0333
0.100
Hexachloroethane U
0.0333
0.100
Nitrobenzene U
0.0333
0.100
Pyridine U
0.0333
0.100
3&4-Methyl Phenol U
0.0333
0.100
2-Methylphenol U
0.0333
0.100
Pentachlorophenol U
0.0333
0.100
2,4,5-Trichlorophenol U
0.0333
0.100
2,4,6-Trichlorophenol U
0.0333
0.100
(S) 2-Fluorophenol 38.3
10.0-120
(S) Phenol-d5 22.8
10.0-120
(S) Nitrobenzene-d5 72.1
10.0-127
(S) 2-F/uorobipheny/ 72.9
10.0-130
(S) 2,4,6-Tribromophenol 72.0
10.0-155
(S) p-Terphenyl-d14 85.4
10.0-128
Laboratory Control Sample (LCS)
(LCS) R3880808-1 01/13/2311:08
Spike Amount
LCS Result
LCS Rec.
Rec. Limits LCS Qualifier
Analyte mg/I
mg/I
%
%
1,4-Dichlorobenzene 0.500
0.372
74.4
18.0-120
2,4-Dinitrotoluene 0.500
0.466
93.2
49.0-124
Hexachlorobenzene 0.500
0.427
85.4
44.0-120
Hexachloro-1,3-butadiene 0.500
0.362
72.4
19.0-120
Hexachloroethane 0.500
0.365
73.0
15.0-120
Nitrobenzene 0.500
0.351
70.2
27.0-120
Pyridine 0.500
0.0738
14.8
10.0-120
3&4-Methyl Phenol 0.500
0.222
44.4
31.0-120
2-Methylphenol 0.500
0.284
56.8
28.0-120
Pentachlorophenol 0.500
0.441
88.2
23.0-120
2,4,5-Trichlorophenol 0.500
0.448
89.6
44.0-120
2,4,6-Trichlorophenol 0.500
0.433
86.6
42.0-120
(S) 2-F/uorophenol
44.9
10.0-120
(S) Phenol-d5
27.7
10.0-120
(S) Nitrobenzene-d5
70.4
10.0-127
ACCOUNT:
PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources
L1573606 01/16/2311:52 17 of 22
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WG1985658 QUALITY CONTROL SUMMARY
Semi Volatile Organic Compounds (GC/MS) by Method 8270E L1573606-01
Laboratory Control Sample (LCS)
(LCS) R3880808-1 01/13/2311:08
Spike Amount LCS Result LCS Rec.
Analyte mg/I mg/I %
(S) 2-F/uorobipheny/ 77.2
(S) 2,4,6-Tribromopheno/ 87.0
(S) p-Terphenyl-d14 85.2
Rec. Limits LCS Qualifier
10.0-130
10.0-155
10.0-128
L1574641-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1574641-01 01/13/2319:10 • (MS) R3880808-3 01/13/2319:32 • (MSD) R3880808-4 01/13/2319:53
Spike Amount
Original Result
MS Result
MSD Result
MS Rec.
MSD Rec.
Dilution Rec. Limits
Analyte
mg/I
mg/I
mg/I
mg/I
%
%
%
1,4-Dichlorobenzene
0.500
ND
0.356
0.376
71.2
75.2
1 17.0-120
2,4-Dinitrotoluene
0.500
ND
0.449
0.486
89.8
97.2
1 39.0-125
Hexachlorobenzene
0.500
ND
0.411
0.440
82.2
88.0
1 35.0-122
Hexachloro-1,3-butadiene
0.500
ND
0.352
0.379
70.4
75.8
1 12.0-120
Hexachloroethane
0.500
ND
0.356
0.372
71.2
74.4
1 10.0-120
Nitrobenzene
0.500
ND
0.343
0.358
68.6
71.6
1 12.0-120
Pyridine
0.500
ND
ND
ND
10.2
10.1
1 10.0-120
3&4-Methyl Phenol
0.500
ND
0.258
0.279
51.6
55.8
1 10.0-120
2-Methylphenol
0.500
ND
0.262
0.290
52.4
58.0
1 10.0-120
Pentachlorophenol
0.500
ND
0.444
0.467
88.8
93.4
1 10.0-128
2,4,5-Trichlorophenol
0.500
ND
0.432
0.464
86.4
92.8
1 33.0-120
2,4,6-Trichlorophenol
0.500
ND
0.415
0.448
83.0
89.6
1 26.0-120
(S) 2-F/uorophenol
40.8
43.6
10.0-120
(S) Phenol-d5
25.7
26.1
10.0-120
(S) Nitrobenzene-d5
68.7
70.6
10.0-127
(S) 2-F/uorobipheny/
74.5
78.4
10.0-130
(S)2,4,6-Tribromopheno/
86.5
92.0
10.0-155
(S) p-Terphenyl-d14
83.6
87.0
10.0-128
MS Qualifier MSD Qualifier RPD
RPD Limits
5.46
40
7.91
25
6.82
24
7.39
34
4.40
40
4.28
30
0.786
37
7.82
36
10.1
30
5.05
37
7.14
31
7.65
31
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ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1573606 01/16/2311:52 18 of 22

GLOSSARY OF TERMS
Guide to Reading and Understanding Your Laboratory Report
The information below is
designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not
u
intended as a comprehensive explanation, and if you have additional questions please contact your project representative.
Results Disclaimer - Information
that may be provided by the customer, and contained within this report, include Permit Limits, Project Name,
FTC
Sample ID, Sample Matrix,
Sample Preservation, Field Blanks, Field Spikes, Field Duplicates, On -Site Data, Sampling Collection Dates/Times, and
Sampling Location. Results relate to the accuracy of this information provided, and as the samples are received.
Abbreviations and Definitions
FSS
MDL
Method Detection Limit.
ND
Not detected at the Reporting Limit (or MDL where applicable).
rqn
RDL
Reported Detection Limit.
Rec.
Recovery.
Fr]
RPD
Relative Percent Difference.
SDG
Sample Delivery Group.
Surrogate (Surrogate Standard) - Analytes added to every blank, sample, Laboratory Control Sample/Duplicate and
e
QC
(S)
Matrix Spike/Duplicate; used to evaluate analytical efficiency by measuring recovery. Surrogates are not expected to be
detected in all environmental media.
U
Not detected at the Reporting Limit (or MDL where applicable).
Analyte
The name of the particular compound or analysis performed. Some Analyses and Methods will have multiple analytes
reported.
If the sample matrix contains an interfering material, the sample preparation volume or weight values differ from the
a
Dilution
standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the
laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the
result reported has already been corrected for this factor.
FSC
These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal
Limits
for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or
duplicated within these ranges.
Original Sample
The non -spiked sample in the prep batch used to determine the Relative Percent Difference (RPD) from a quality control
sample. The Original Sample may not be included within the reported SDG.
This column provides a letter and/or number designation that corresponds to additional information concerning the result
Qualifier
reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and
potentially a discussion of possible implications of the Qualifier in the Case Narrative if applicable.
The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. If there was
no measurable result returned for a specific analyte, the result in this column may state "ND" (Not Detected) or "BDL"
Result
(Below Detectable Levels). The information in the results column should always be accompanied by either an MDL
(Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect
or report for this analyte.
Uncertainty
(Radiochemistry)
Confidence level of 2 sigma.
A brief discussion about the included sample results, including a discussion of any non -conformances to protocol
Case Narrative (Cn)
observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will
be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report.
Quality Control
This section of the report includes the results of the laboratory quality control analyses required by procedure or
Summary (Qc)
analytical methods to assist in evaluating the validity of the results reported for your samples. These analyses are not
being performed on your samples typically, but on laboratory generated material.
This is the document created in the field when your samples were initially collected. This is used to verify the time and
Sample Chain of
date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This
Custody (Sc)
chain of custody also documents all persons (excluding commercial shippers) that have had control or possession of the
samples from the time of collection until delivery to the laboratory for analysis.
This section of your report will provide the results of all testing performed on your samples. These results are provided
Sample Results (Sr)
by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for
each sample will provide the name and method number for the analysis reported.
Sample Summary (Ss)
This section of the Analytical Report defines the specific analyses performed for each sample ID, including the dates and
times of preparation and/or analysis.
Qualifier
Description
E
The analyte concentration exceeds the upper limit of the calibration range of the instrument established by the initial
calibration (ICAL).
J
The identification of the analyte is acceptable; the reported value is an estimate.
J6
The sample matrix interfered with the ability to make any accurate determination; spike value is low.
T8
Sample(s) received past/too close to holding time expiration.
ACCOUNT:
PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources
L1573606 01/16/23 11:52 19 of 22

ACCREDITATIONS & LOCATIONS
Pace Analytical National 12065 Lebanon Rd Mount Juliet, TN 37122
Alabama
40660
Nebraska
NE-OS-15-05
Alaska
17-026
Nevada
TN000032021-1
Arizona
AZ0612
New Hampshire
2975
Arkansas
88-0469
New Jersey—NELAP
TN002
California
2932
New Mexico
TN00003
Colorado
TN00003
New York
11742
Connecticut
PH-0197
North Carolina
Env375
Florida
E87487
North Carolina'
DW21704
Georgia
NELAP
North Carolinas
41
Georgia'
923
North Dakota
R-140
Idaho
TN00003
Ohio—VAP
CL0069
Illinois
200008
Oklahoma
9915
Indiana
C-TN-01
Oregon
TN200002
Iowa
364
Pennsylvania
68-02979
Kansas
E-10277
Rhodelsland
LA000356
Kentucky16
KY90010
South Carolina
84004002
Kentucky 2
16
South Dakota
n/a
Louisiana
A130792
Tennessee' °
2006
Louisiana
LA018
Texas
T104704245-20-18
Maine
TN00003
Texas'
LAB0152
Maryland
324
Utah
TN000032021-11
Massachusetts
M-TN003
Vermont
VT2006
Michigan
9958
Virginia
110033
Minnesota
047-999-395
Washington
C847
Mississippi
TN00003
West Virginia
233
Missouri
340
Wisconsin
998093910
Montana
CERT0086
Wyoming
A21-A
A21-A — ISO 17025
1461.01
AIHA-LAP,LLC EMLAP
100789
A21-A — ISO 17025 s
1461.02
DOD
1461.01
Canada
1461.01
USDA
P330-15-00234
EPA—Crypto
TN00003
Drinking Water 2 Underground Storage Tanks 'Aquatic Toxicity ° Chemical/Microbiological 'Mold 6 Wastewater n/a Accreditation not applicable
Not all certifications held by the laboratory are applicable to the results reported in the attached report.
Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace Analytical.
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ACCOUNT: PROJECT: SDG: DATE/TIME:
EMA Resources L1573606 01/16/23 11:52
PAGE:
20 of 22

Company Name/Address:
Billing Information:
A
ialvsis/
Container
/ Presery
Live
Chain of Custody Page _ of
EMA Resources
Mr. Brent Collins [Pres
755 Yadkinville Road Chk
755 Yadkinville Road
Mocksville, NC 27028
��aceAnalytical
Mocksville, NC 27028
17065 tebanon Rd Mount Julie+, TN 37177
Rennrt to
Email To
Mr. Brent Collins
brent.Collins@ a ma resourcesi nc.com;roy.whitak
o—dupe akomedgm t and xcepame of me
Pxe Terms and Condmons found at
ht<P innmwtNab �omiMm+iw+-.+anda.a-
e.m,odr
Project Description
Sludge
City/State /
Collected:2elclSA1,i;A/C
Please Circle
PT MT CT ET
Client Project #
Lab Project #
[SDG# L
Phone: [phone]
C163
Collect by (print)
Site/Facility ID #
P.O. #
1 CY/f }'Co�Ji�l
n
ao
Acctnum: EMARES
aJ
a
Z
I
Template:T11413
Collected b
v (s%
Rush. (Lab MUST Be Notified) Quote #
_ Same Day _ Five Day
Z
J
j
Pretog in: P895422
_ Next Day 5 Day (Rad Only) Date Results Needed
PM: 807 -Justin Carr
Immediately
Two Day _ 10 Day (Rad Only) No.
U
_�
—
PB' n
Packed on Ice N _ Y
_ Three Day of
>
Shipped via: FedEX Ground
Sample ID
Comp/Grab
Matrix'
Depth
Date
Time
ntrs
Ln
a
X
U
Remarks Sample # (lab only(
Re:ds�tUL
ss
31
11;;5
2
X
X
—d
S-23
' Matrix:Remarks:
Sample Receipt CheAI.ist
SS - Soil AIR - Air F - Filter pH Temp
COC Seal Present/Intact: NP __Y _N
GW - Groundwater B -Bioassay
COC Signed/Accurate:
WW - Waste Water Flow Other
—N
Bottles arrive intact: N
Correct bottles used:
DW - Drinking W ter
Samples returned via: ` {� /
OT Other Sd9L Tracking#
_N
Sufficient volume sent: /Y _N
If Applicable
J�-1X 7D
UPS FedEz Courier l (l
VOA Zero Headspace: _Y _`�
Preservation Correct/Checked: _Y N
RAO Screen <0.5
Relinquished b (Signature)
q y ( g )
Datt
Z
Time:
Received b (Sign
y'( g )
TripBlank Receiv Yes N
3. 30
/ MeoH
mR/hr: _N
TBRHCL
TBR
Relinquished by : (Signature)
Date
Time:
Received by: (Signature)
Temp Bottles itecgved:
It preservation required by Login: Date/Time
Relinquished by : (Signature)
Date
Time
R ed for ab b )
Date: Time:
Hold:
Condition:
�—
/ Z 3
NCF /0

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Reidsville WQ Permit Number: WQ0002376
WWTP Name: Reidsville WWTP NPDES Number: NCO024881
Monitoring Period: From l/l/2023 To 3/31/2023
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. A (time/temp) ❑
Alt B (Alk Treatment) ❑
I Alt. C (Prior Testing) ❑
A1t.D (No Prior Test) ❑
Process to Further Reduce Pathogengs ❑
If applicable to alternative
performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost ❑
Heat Drying ❑
Heat Treatment ❑
Thermophilic ❑
Beta Ray ❑
Gamma Ray ❑
Pasteurization ❑
Class B:
jAlt. (1) Fecal Density ®
Alt. (2) Process to Significantly Reduce Pathogens ❑
If applicable to alternative
performed (Class
B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization ❑
Air Drying ❑
Composting ❑
jAerobic Digestion ❑
Anaerobic Digestion ❑
If applicable to alternative performed (Class A or Class B) complete the following monitoring data:
Parameter
Allowable Level
in Sludge
Pathogen Density
Number ot
Excee-
n
Frequency
of Analysis
Sample
Type
Analytical
Tech -pique
Minimu
Geo. Mean
aximu
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
CFU
34483
41789
53097
CFU/g
0
Quarterly
G
SM9222D
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per 4 grams
total solid (dry
weight)
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed:
Alt.1 (VS reduction) ❑
Alt. 2 (40-day bench) ❑
Alt. 3 (30-daybench) r❑
Alt. 4 (Spec. OZ uptake) ❑
Alt. 5 (14-Day Aerobic) ❑
Alt. 6 (Alk. Stabilization ❑
Alt 7 (Drying - Stable) ❑
jAlt. 8 (Drying - Unstable) ❑
Alt. 9 (Injection) ❑
Alt. 10 (Incorporation) ❑
No vector attraction reduction alternatives were performed ❑
CERTIFICATION STATEMENT (please check the appropriate statement)
© "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if
you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Mourice Brothers - Superintendent of Wastewater Treatment Brent Collins; Director of Technical Services
Preparer Name and Title (type or print)
Rowice 51-0 hel-1
Mourice Brothers (Feb 9, 202410:40 EST)
Land Applier Name and Title (if applicable)(type or print)
02/09/24 t�i
2/ 1 /2024
Signature of Preparer* Date Signature of Land Applier (if applicable)
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
Date
DENR FORM PVRF 02T (12/2006)

Meritech, Inc.
Environmental Laboratory
Laboratory Certification No.165
Contact: Brent Collins
Client: EMA Resources, Inc
755 Yadkinville Road
Page 1
Report Date: 1/13/2023
Mocksville, NC 27028 Date Sample Rcvd: 1/5/2023
Meritech Work Order # 01052323 Sample: Reidsville 1 Grab 1/5/23
Parameters Result Analysis Date Reporting Limit Method
% Total Solids
1.17 %
1/6/23
0-100 %
SM 2540B
Fecal Coliform (Sludge)
51,282 CFU/g dry wt
1/5/23
130 CFU/g dry wt
SM 9222D
Meritech Work Order # 01052324 Sample: Reidsville 2 Grab 1/5/23
Parameters Result Analysis Date Reporting Limit Method
% Total Solids 1.15 % 1/6/23 0-100 % SM 2540B
Fecal Coliform (Sludge) 43,478 CFU/g dry wt 1/5/23 130 CFU/g dry wt SM 9222D
Meritech Work Order # 01052325 Sample: Reidsville 3 Grab 1/5/23
Parameters Result Analysis Date Reporting Limit Method
% Total Solids 1.16 % 1/6/23 0-100 % SM 2540B
Fecal Coliform (Sludge) 34,483 CFU/g dry wt 1/5/23 130 CFU/g dry wt SM 9222D
Meritech Work Order # 01052326 Sample: Reidsville 4 Grab 1/5/23
Parameters Result Analysis Date Reporting Limit Method
% Total Solids 1.15 % 1/6/23 0-100 % SM 2540B
Fecal Coliform (Sludge) 34,783 CFU/g dry wt 1/5/23 130 CFU/g dry wt SM 9222D
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

rAPO
Ampti——i
Contact: Brent Collins
Client: EMA Resources, Inc
755 Yadkinville Road
Mocksville, NC 27028
Meritech, Inc.
Environmental Laboratory
Laboratory Certification No. 165
Page 2
Report Date: 1/13/2023
Date Sample Rcvd: 1/5/2023
Meritech Work Order #
Parameters
% Total Solids
Fecal Coliform (Sludge)
01052327 Sample: Reidsville 5 Grab
Result Analysis Date
1.10 % 1/6/23
45,455 CFU/g dry wt 1/5/23
Reporting Limit
0-100 %
130 CFU/g drywt
1/5/23
Method
SM 2540B
SM 9222D
Meritech Work Order #
01052328 Sample: Reidsville 6 Grab
1/5/23
Parameters
Result Analysis Date
Reporting Limit
Method
% Total Solids
1.16 % 1/6/23
0-100 %
SM 2540B
Fecal Coliform (Sludge)
34,483 CFU/g dry wt 1/5/23
130 CFU/g dry wt
SM 9222D
Meritech Work Order #
01052329 Sample: Reidsville 7 Grab
1/5/23
Parameters
Result Analysis Date
Reporting Limit
Method
% Total Solids
1.13 % 1/6/23
0-100 %
SM 2540B
Fecal Coliform (Sludge)
53,097 CFU/g dry wt 1/5/23
130 CFU/g dry wt
SM 9222D
I hereby certify that I have reviewed and approve these data. S pCA0. wo auC
r
Laboratory Representative
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

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Meritech, Inc.
Environmental Laboratory
Laboratory Certification No.165
s
Contact: Brent Collins
Client: EMA Resources, Inc
755 Yadkinville Road
Mocksville, NC 27028
Report Date: 3/24/2023
Date Sample Rcvd: 2/17/2023
Vector Attraction Reduction / Aerobically Digested Sludge (30 Day Test
Meritech Work Order # 02172302 Sample: Reidsville Composite 2/17/23
Total Solids Volatile Solids % Volatile Solids
Week 1 1.04 0.76 0.736
Week 2
1.02
0.76
0.742
Week 3
0.95
0.71
0.754
Week 4
0.90
0.67
0.743
Week 5
0.84
0.62
0.739
Van Kleek Reduction (%): -1.44
I hereby certify that I have reviewed and approve these data, b1 nc C ,p
Laboratory Representative
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

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ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Reidsville WQ Permit Number: WQ0002376
WWTP Name: Reidsville WWTP NPDES Number: NCO024881
Monitoring Period: From 4/l/2023 To 6/30/2023
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. A (time/temp) ❑
Alt B (Alk Treatment) ❑
I Alt. C (Prior Testing) ❑
A1t.D (No Prior Test) ❑
--d
Process to Further Reduce Pathogengs ❑
If applicable to alternative
performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost ❑
Heat Drying ❑
Heat Treatment ❑
Thermophilic ❑
Beta Ray ❑
Gamma Ray ❑
Pasteurization ❑
Class B:
jAlt. (1) Fecal Density ®
Alt. (2) Process to Significantly Reduce Pathogens ❑
If applicable to alternative
performed (Class
B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization ❑
Air Drying ❑
Composting ❑
jAerobic Digestion ❑
Anaerobic Digestion ❑
If applicable to alternative performed (Class A or Class B) complete the following monitoring data:
Parameter
Allowable Level
in Sludge
Pathogen Density
Number ot
Excee-
n
Frequency
of Analysis
Sample
Type
Analytical
Tech -pique
Minimu
Geo. Mean
aximu
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
CFU
1884
2822
5079
CFU/g
0
Quarterly
G
SM9222D
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per 4 grams
total solid (dry
weight)
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed:
Alt.1 (VS reduction) ❑
Alt. 2 (40-day bench) ❑
Alt. 3 (30-daybench) r❑
Alt. 4 (Spec. OZ uptake) ❑
Alt. 5 (14-Day Aerobic) ❑
Alt. 6 (Alk. Stabilization ❑
Alt 7 (Drying - Stable) ❑
jAlt. 8 (Drying - Unstable) ❑
Alt. 9 (Injection) ❑
Alt. 10 (Incorporation) ❑
No vector attraction reduction alternatives were performed ❑
CERTIFICATION STATEMENT (please check the appropriate statement)
© "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if
you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Mourice Brothers - Superintendent of Wastewater Treatment Brent Collins; Director of Technical Services
Preparer Name and Title (type or print)
Rowice 51-0 hel-1
Mourice Brothers (Feb 9, 202410:40 EST)
Land Applier Name and Title (if applicable)(type or print)
02/09/24 t�i
2/ 1 /2024
Signature of Preparer* Date Signature of Land Applier (if applicable)
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
Date
DENR FORM PVRF 02T (12/2006)

Meritech, Inc.
Environmental Laboratory
Laboratory Certification No.165
Contact: Brent Collins
Client: EMA Resources, Inc
755 Yadkinville Road
Page 1
Report Date: 4/14/2023
Mocksville, NC 27028 Date Sample Rcvd: 4/5/2023
Meritech Work Order # 04052309 Sample: Reidsville Grab 4/5/23
Parameters Result Analysis Date Reporting Limit Method
% Total Solids 1.86 % 4/5/23 0-100 % SM 2540B
Fecal Coliform (Sludge) 2,933 col/g dry wt 4/5/23 1181 col/g dry wt SM 9222D
Meritech Work Order # 04052310 Sample: Reidsville Grab 4/5/23
Parameters Result Analysis Date Reporting Limit Method
% Total Solids 1.93 % 4/5/23 0-100 % SM 2540B
Fecal Coliform (Sludge) 1,884 col/g dry wt 4/5/23 348 col/g dry wt SM 9222D
Meritech Work Order #
04052311 Sample: Reidsville Grab
4/5/23
Parameters
Result Analysis Date
Reporting Limit
Method
% Total Solids
1.76 % 4/5/23
0-100 %
SM 2540B
Fecal Coliform (Sludge)
2,582 col/g dry wt 4/5/23
348 col/g dry wt
SM 9222D
Meritech Work Order #
04052312 Sample: Reidsville Grab
4/5/23
Parameters
Result Analysis Date
Reporting Limit
Method
% Total Solids
1.82 % 4/5/23
0-100 %
SM 2540B
Fecal Coliform (Sludge)
1,993 col/g dry wt 4/5/23
1181 col/g dry wt
SM 9222D
Meritech Work Order #
04052313 Sample: Reidsville Grab
4/5/23
Parameters
Result Analysis Date
Reporting Limit
Method
% Total Solids
1.79 % 4/5/23
0-100 %
SM 2540B
Fecal Coliform (Sludge)
5,079 col/g dry wt 4/5/23
348 col/g dry wt
SM 9222D
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

Meritech, Inc.
Environmental Laboratory
Laboratory Certification No.165
Contact: Brent Collins
Client: EMA Resources, Inc
755 Yadkinville Road
Page 2
Report Date: 4/14/2023
Mocksville, NC 27028 Date Sample Rcvd: 4/5/2023
Meritech Work Order # 04052314 Sample: Reidsville Grab
Parameters Result Analysis Date
% Total Solids 1.83 % 4/5/23
Fecal Coliform (Sludge) 2,484 col/g dry wt 4/5/23
Meritech Work Order # 040S2315 Sample: Reidsville Grab
Parameters Result Analysis Date
% Total Solids 1.83 % 4/5/23
Fecal Coliform (Sludge) 3,974 col/g dry wt 4/5/23
4/5/23
Reporting Limit Method
0-100 % SM 2540B
1181 col/g dry wt SM 9222D
4/5/23
Reporting Limit Method
0-100 % SM 2540B
348 col/g dry wt SM 9222D
I hereby certify that I have reviewed and approve these data.
Laboratory Representative
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

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Meritech, Inc.
Environmental Laboratory
Laboratory Certification No. 165
Contact: Brent Collins
Client: EMA Resources, Inc
755 Yadkinville Road
Mocksville, NC 27028
Report Date: 5/16/2023
Date Sample Rcvd: 4/5/2023
Vector Attraction Reduction
/ Aerobically Digested Sludge
(30 Day Test)
Meritech
Work Order # 04052308
Sample: Reidsville Composite
4/5/23
Total Solids
Volatile Solids
% Volatile Solids
Week 1
1.23
0.93
0.759
Week 2
1.24
0.94
0.758
Week 3
1.19
0.90
0.751
Week 4
1.17
0.89
0.761
Week 5
1.10
0.84
0.758
Van Kleek Reduction (%): 0.26
I hereby certify that I have reviewed and approve these data.
Laboratory Representative
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

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ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Reidsville WQ Permit Number: WQ0002376
WWTP Name: Reidsville WWTP NPDES Number: NCO024881
Monitoring Period: From 7/l/2023 To 9/30/2023
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. A (time/temp) ❑
Alt B (Alk Treatment) ❑
I Alt. C (Prior Testing) ❑
A1t.D (No Prior Test) ❑
--d
Process to Further Reduce Pathogengs ❑
If applicable to alternative
performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost ❑
Heat Drying ❑
Heat Treatment ❑
Thermophilic ❑
Beta Ray ❑
Gamma Ray ❑
Pasteurization ❑
Class B:
jAlt. (1) Fecal Density ®
Alt. (2) Process to Significantly Reduce Pathogens ❑
If applicable to alternative
performed (Class
B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization ❑
Air Drying ❑
Composting ❑
jAerobic Digestion ❑
Anaerobic Digestion ❑
If applicable to alternative performed (Class A or Class B) complete the following monitoring data:
Parameter
Allowable Level
in Sludge
Pathogen Density
Number ot
Excee-
n
Frequency
of Analysis
Sample
Type
Analytical
Tech -pique
Minimu
Geo. Mean
aximu
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
CFU
390
400
433
CFU/g
0
Quarterly
G
SM9222D
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per 4 grams
total solid (dry
weight)
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed:
Alt.1 (VS reduction) ❑
Alt. 2 (40-day bench) ❑
Alt. 3 (30-daybench) r❑
Alt. 4 (Spec. OZ uptake) ❑
Alt. 5 (14-Day Aerobic) ❑
Alt. 6 (Alk. Stabilization ❑
Alt 7 (Drying - Stable) ❑
jAlt. 8 (Drying - Unstable) ❑
Alt. 9 (Injection) ❑
Alt. 10 (Incorporation) ❑
No vector attraction reduction alternatives were performed ❑
CERTIFICATION STATEMENT (please check the appropriate statement)
© "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if
you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Mourice Brothers - Superintendent of Wastewater Treatment Brent Collins; Director of Technical Services
Preparer Name and Title (type or print)
Rowice 51-0 hel-1
Mourice Brothers (Feb 9, 202410:40 EST)
Land Applier Name and Title (if applicable)(type or print)
02/09/24 t�i
2/ 1 /2024
Signature of Preparer* Date Signature of Land Applier (if applicable)
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
Date
DENR FORM PVRF 02T (12/2006)

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Contact: Brent Collins
Client: EMA Resources, Inc
755 Yadkinville Road
Mocksville, NC 27028
Meritech, Inc.
Environmental Laboratory
Laboratory Certification No.165
Meritech Work Order # 07132304
Parameters
% Total Solids
Fecal Coliform (Class B Sludge)
Meritech Work Order # 07132305
Parameters
% Total Solids
Fecal Coliform (Class B Sludge)
Sample: Reidsville 1
Result
2.10 %
<433 CFU/g dry wt
Result
Page 1
Report Date: 7/24/2023
Date Sample Rcvd: 7/13/2023
Analysis Date Reporting Limit
7/13/23
Method
7/14/23 0-100 % SM 2540B
7/13/23 433 CFU/g dry wt SM 9222D
Sample: Reidsville 2
2.33 %
<390 CFU/g dry wt
Analysis Date Reporting Limit
7/13/23
Method
7/14/23 0-100 % SM 2540B
7/13/23 390 CFU/g dry wt SM 9222D
Meritech Work Order # 07132306 Sample: Reidsville 3 7/13/23
Parameters Result Analysis Date Reporting Limit Method
% Total Solids 2.31 % 7/14/23 0-100 % SM 2540B
Fecal Coliform (Class B Sludge) <394 CFU/g dry wt 7/13/23 394 CFU/g dry wt SM 9222D
Meritech Work Order # 07132307 Sample: Reidsville 4 7/13/23
Parameters Result Analysis Date Reporting Limit Method
% Total Solids
2.30 %
7/14/23
0-100 %
SM 2540B
Fecal Coliform (Class B Sludge)
<395 CFU/g dry wt
7/13/23
395 CFU/g dry wt
SM 9222D
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

Meritech, Inc.
Environmental Laboratory
Laboratory Certification No.165
Contact: Brent Collins
Client: EMA Resources, Inc
755 Yadkinville Road
Mocksville, NC 27028
Meritech Work Order # 07132308
Parameters
% Total Solids
Fecal Coliform (Class B Sludge)
Meritech Work Order # 07132309
Parameters
% Total Solids
Fecal Coliform (Class B Sludge)
Sample: Reidsville 5
Result
2.32 %
<392 CFU/g dry wt
Result
Page 2
Report Date: 7/24/2023
Date Sample Rcvd: 7/13/2023
Analysis Date Reporting Limit
7/13/23
Method
7/14/23 0-100 % SM 2540B
7/13/23 392 CFU/g dry wt SM 9222D
Sample: Reidsville 6
2.27 %
<400 CFU/g dry wt
Analysis Date Reporting Limit
7/13/23
Method
7/14/23 0-100 % SM 2540B
7/13/23 400 CFU/g dry wt SM 9222D
Meritech Work Order # 07132310 Sample: Reidsville 7 7/13/23
Parameters Result Analysis Date Reporting Limit Method
% Total Solids
2.30 %
7/14/23
0-100 %
SM 2540B
Fecal Coliform (Class B Sludge)
<395 CFU/g dry wt
7/13/23
395 CFU/g dry wt
SM 9222D
1 hereby certify that I have reviewed and approve these data.
Laboratory Representative
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

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Contact: Brent Collins
Client: EMA Resources, Inc
755 Yadkinville Road
Mocksville, NC 27028
Meritech, Inc.
Environmental Laboratory
Laboratory Certification No. 165
Report Date: 8/9/2023
Date Sample Rcvd: 7/6/2023
Vector Attraction Reduction
/ Aerobically Digested Sludge
(30 Day Test)
Meritech Work Order # 07062303
Sample: Reidsville Composite
7/6/23
Total Solids
Volatile Solids
% Volatile Solids
Week 1
1.03
0.75
0.734
Week 2
0.98
0.72
0.737
Week 3
0.90
0.67
0.744
Week 4
1.12
0.84
0.753
Week 5
0.84
0.62
0.731
Van Kleek Reduction (%): 1.29
hereby certify that / have reviewed and approve these data.
Laboratory Representative
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]
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ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Reidsville WQ Permit Number: WQ0002376
WWTP Name: Reidsville WWTP NPDES Number: NCO024881
Monitoring Period: From 10/1/2023 To 12/31/2023
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. A (time/temp) ❑
Alt B (Alk Treatment) ❑
I Alt. C (Prior Testing) ❑
A1t.D (No Prior Test) ❑
Process to Further Reduce Pathogengs ❑
If applicable to alternative
performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost ❑
Heat Drying ❑
Heat Treatment ❑
Thermophilic ❑
Beta Ray ❑
Gamma Ray ❑
Pasteurization ❑
Class B:
jAlt. (1) Fecal Density ®
Alt. (2) Process to Significantly Reduce Pathogens ❑
If applicable to alternative
performed (Class
B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization ❑
Air Drying ❑
Composting ❑
jAerobic Digestion ❑
Anaerobic Digestion ❑
If applicable to alternative performed (Class A or Class B) complete the following monitoring data:
Parameter
Allowable Level
in Sludge
Pathogen Density
Number ot
Excee-
n
Frequency
of Analysis
Sample
Type
Analytical
Tech -pique
Minimu
Geo. Mean
aximu
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
CFU
55556
102398
168675
CFU/g
0
Quarterly
G
SM9222D
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per 4 grams
total solid (dry
weight)
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed:
Alt.1 (VS reduction) ❑
Alt. 2 (40-day bench) ❑
Alt. 3 (30-daybench) r❑
Alt. 4 (Spec. OZ uptake) ❑
Alt. 5 (14-Day Aerobic) ❑
Alt. 6 (Alk. Stabilization ❑
Alt 7 (Drying - Stable) ❑
jAlt. 8 (Drying - Unstable) ❑
Alt. 9 (Injection) ❑
Alt. 10 (Incorporation) ❑
No vector attraction reduction alternatives were performed ❑
CERTIFICATION STATEMENT (please check the appropriate statement)
© "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if
you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Mourice Brothers - Superintendent of Wastewater Treatment Brent Collins; Director of Technical Services
Preparer Name and Title (type or print)
Rowice 51-0 hel-1
Mourice Brothers (Feb 9, 202410:40 EST)
Land Applier Name and Title (if applicable)(type or print)
02/09/24 t�i
2/ 1 /2024
Signature of Preparer* Date Signature of Land Applier (if applicable)
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
Date
DENR FORM PVRF 02T (12/2006)

Meritech, Inc.
Environmental Laboratory
Laboratory Certification No.165
Contact: Brent Collins
Client: EMA Resources, Inc
755 Yadkinville Road
Mocksville, NC 27028
Page 1
Report Date: 10/13/2023
Date Sample Rcvd: 10/5/2023
Meritech Work Order # 10052305 Sample: Reidsville 1 10/5/23
Parameters Result Analysis Date Reporting Limit Method
% Total Solids 1.76 % 10/6/23 0-100 % SM 2540B
Fecal Coliform (Class B Sludge) 85,227 CFU/g dry wt 10/5/23 433 CFU/g dry wt SM 9222D
Meritech Work Order # 10052306 Sample: Reidsville 2 10/5/23
Parameters Result Analysis Date Reporting Limit Method
% Total Solids 1.66 % 10/6/23 0-100 % SM 2540B
Fecal Coliform (Class B Sludge) 96,386 CFU/g dry wt 10/5/23 390 CFU/g dry wt SM 9222D
Meritech Work Order # 10052307 Sample: Reidsville 3 10/5/23
Parameters Resu t Analysis Date Reporting Limit Method
% Total Solids 1.62 % 10/6/23 0-100 % SM 2540B
Fecal Coliform (Class B Sludge) 55,556 CFU/g dry wt 10/5/23 394 CFU/g dry wt SM 9222D
Meritech Work Order # 10052308 Sample: Reidsville 4 10/5/23
Parameters Result Analysis Date Reporting Limit Method
% Total Solids 1.65 % 10/6/23 0-100 % SM 2540B
Fecal Coliform (Class B Sludge) 90,909 CFU/g dry wt 10/5/23 395 CFU/g dry wt SM 9222D
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

Meritech, Inc.
Environmental Laboratory
Laboratory Certification No.165
Contact: Brent Collins
Client: EMA Resources, Inc
755 Yadkinville Road
Mocksville, NC 27028
Page 2
Report Date: 10/13/2023
Date Sample Rcvd: 10/5/2023
Meritech Work Order # 10052309 Sample: Reidsville 5 10/5/23
Parameters Result Analysis Date Reporting Limit Method
% Total Solids
Fecal Coliform (Class B Sludge)
1.65 %
127,273 CFU/g dry wt
10/6/23
10/5/23
0-100 %
392 CFU/g dry wt
SM 2540B
SM 9222D
Meritech Work Order #
10052310 Sample: Reidsville 6
10/5/23
Parameters
Result
Analysis Date
Reporting Limit
Method
% Total Solids
1.66 %
10/6/23
0-100 %
SM 2540B
Fecal Coliform (Class B Sludge)
168,675 CFU/g dry wt
10/5/23
400 CFU/g dry wt
SM 9222D
Meritech Work Order # 10052311 Sample: Reidsville 7 10/5/23
Parameters Result Analysis Date Reporting Limit Method
% Total Solids 1.66 % 10/6/23 0-100 % SM 2540B
Fecal Coliform (Class B Sludge) 132,530 CFU/g dry wt 10/5/23 395 CFU/g dry wt SM 9222D
I hereby certify that 1 have reviewed and approve these data.
Qrz-�
Laboratory Representative
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

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Meritech, Inc.
Environmental Laboratory
Laboratory Certification No. 165
s
Contact: Brent Collins
Client: EMA Resources, Inc
755 Yadkinville Road
Mocksville, NC 27028
Report Date: 11/6/2023
Date Sample Rcvd: 10/3/2023
Vector Attraction Reduction / Aerobically Digested Sludge (30 Day Test)
Meritech Work Order # 10032353 Sample: Reidsville Composite 10/3/23
Total Solids Volatile Solids % Volatile Solids
Week 1 0.97 0.68 0.700
Week 2
0.94
0.67
0.710
Week 3
0.91
0.65
0.714
Week 4
0.84
0.60
0.714
Week 5
0.82
0.58
0.700
Van Kleek Reduction (%): -0.14
1 hereby certify that / have reviewed and approve these data.
Laboratory Representative
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

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NCDA&CS Agronomic Division Phone: [phone]
Website: www.ncagr.gov/agronomi/
Report No. FY24-SL007384
Client:
Daisy Purgason
Advisor: Brent Collins
Predictive
6079 NC Hwy 65
EMA Resources Inc
£
Reidsville, NC 27320
755 Yadkinville Rd
x "
Soil Report Mehlich-3 Extraction
Mocksville, NC 27028
Sampled County: Rockingham
Links to Helpful Information
Client ID: 465895
Advisor ID: 405413
Sampled:
Received: 10/10/2023 Completed: 10/20/2023
Farm: RC11
Sample ID: 00001
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P2O5
K2O
Mg S Mn
Zn
Cu B
Information
Lime History:
1 - Fescue/OGrass/Tim, M 0.0
120-200 10
110
0 0 0
0
0 0
Note: 12
2- Fescue/OGrass/Tim, M 0.0
120-200 10
110
0 0 0
0
0 0
Note: 12
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class: Mineral
HM% W/V
CEC BS% Ac pH P-1 K-1
Ca% Mg%
S-1 Mn-I
Mn-All Mn-Al2 Zn-I
Zn-AI
Cu-I Na ESP SS-1 NO3-N
0.27 1.14
7.1 82 1.3 6.0 56 15
60 21
41 120
89 89 350
350
90 0.1 1
North Carolina
lobitty lru%t FuivJ Ctwnauukm
Reprogramming of the laboratory -information -management system that makes this report possible is being funded
through a grant from the North Carolina Tobacco Trust Fund Commission.
Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
- Steve Troxler. Commissioner of Agriculture

NCDA&CS Agronomic Division Phone: [phone]
Website: www.ncagr.gov/agronomi/
Report No. FY24-SL007381
Predictive
Client:
Lawrence McCollum
434 Truman Rd
Advisor:
Brent Collins
EMA Resources Inc
£
x Soil Report Mehlich-3 Extraction
Reidsville, NC 27320
755 Yadkinville Rd
Mocksville, NC 27028
Sampled County: Rockingham
„r
Links to Helpful Information
Client ID: 289332
Advisor
ID: 405413
Sampled: Received: 10/10/2023 Completed: 10/20/2023
Farm: RC12
Sample ID: 00001
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P2O5
K2O
Mg S
Mn
Zn
Cu
B
Information
Lime History:
1- Fescue/OGrass/Tim, M 0.0
120-200 0
100
0 0
0
0
0
0
Note: 12
2- Fescue/OGrass/Tim, M 0.0
120-200 0
100
0 0
0
0
0
0
Note: 12
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class:
Mineral
HM% W/V CEC BS% Ac pH P-1 K-1
Ca% Mg%
S-1
Mn-I
Mn-All Mn-Al2
Zn-I
Zn-AI
Cu-I
Na ESP SS-1 NO3-N
0.46 1.05 8.1 84 1.3 6.2 81 18
56 26
40
192
129 129
408
408
136
0.1 1
Sample ID: 00002A
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P2O5
K2O
Mg S
Mn
Zn
Cu
B
Information
Lime History:
1 - Fescue/OGrass/Tim, M 1.1
120-200 10
90
0 20
0
0
0
0
Note: 12
2 - Fescue/OGrass/Tim, M 0.0
120-200 10
90
0 20
0
0
0
0
Note: 12
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class:
Mineral
HM% W/V CEC BS% Ac pH P-1 K-1
Ca% Mg%
S-1
Mn-I
Mn-All Mn-AI2
Zn-I
Zn-AI
Cu-I
Na ESP SS-1 NO3-N
0.32 1.09 7.4 74 2.0 5.3 61 25
45 27
21
126
93 93
99
99
63
0.1 1
North Carolina
f. 1 ' >
I0WOOLO iiu%t lLaW Ctwnawukm
Reprogramming of the laboratory -information -management system that makes this report possible is being funded
through a grant from the North Carolina Tobacco Trust Fund Commission.
Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
- Steve Troxler. Commissioner of Agriculture

NCDA&CS Agronomic Division Phone: [phone]
Website: www.ncagr.gov/agronomi/
Report No.
FY24-SL007381
Lawrence McCollum
Page 2 of 3
Sample ID: 00002B
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P2O5
K2O
Mg
S
Mn Zn
Cu B
Information
Lime History:
1 - Fescue/OGrass/Tim, M 1.0
120-200 30
80
0
0
0 0
0 0
Note: 12
2- Fescue/OGrass/Tim, M 0.0
120-200 30
80
0
0
0 0
0 0
Note: 12
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm):
Soil Class:
Mineral
HM% W/V CEC BS% Ac pH P-1 K-1
Ca% Mg% S-1
Mn-I
Mn-All
Mn-Al2 Zn-I Zn-AI
Cu-1 Na ESP
SS-1 NO3-N
0.36 1.14 4.2 57 1.8 5.2 49 28
37 17 26
219
148
148
90 90
80 0.1
2

NCDA&CS Agronomic Division Phone: [phone]
Website: www.ncagr.gov/agronomi/
Report No. FY24-SL007383
Client:
Bennett Farm
Advisor: Brent Collins
Predictive
313 Bennett Farm Road
EMA Resources Inc
£
Stokesdale, NC 27357
755 Yadkinville Rd
x "
Soil Report Mehlich-3 Extraction
Mocksville, NC 27028
Sampled County: Rockingham
Links to Helpful Information
Client ID: 530291
Advisor ID: 405413
Sampled:
Received: 10/10/2023 Completed: 10/20/2023
Farm: RC15
Sample ID: 00001
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P2O5
K2O
Mg S Mn
Zn
Cu B
Information
Lime History:
1 - Fescue/OGrass/Tim, M 0.0
120-200 60
110
0 0 0
0
0 0
Note: 12
2- Fescue/OGrass/Tim, M 0.0
120-200 60
110
0 0 0
0
0 0
Note: 12
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class: Mineral
HM% W/V
CEC BS% Ac pH P-1 K-1
Ca% Mg%
S-1 Mn-I
Mn-All Mn-Al2 Zn-I
Zn-AI
Cu-I Na ESP SS-1 NO3-N
1.74 1.10
8.6 88 1.0 6.5 31 15
60 27
65 121
82 82 369
369
55 0.2 2
North Carolina
lobitty lru%t FuivJ Ctwnauukm
Reprogramming of the laboratory -information -management system that makes this report possible is being funded
through a grant from the North Carolina Tobacco Trust Fund Commission.
Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
- Steve Troxler. Commissioner of Agriculture

NCDA&CS Agronomic Division Phone: [phone]
Website: www.ncagr.gov/agronomi/
Report No. FY23-SL029060
Predictive
Client:
Donald Lovelace
3575 NC Hwy 150
Advisor:
Brent Collins
EMA Resources Inc
£
x Soil Report Mehlich-3 Extraction
Reidsville, NC 27320
755 Yadkinville Rd
Mocksville, NC 27028
Sampled County: Rockingham
„r
Links to Helpful Information
Client ID: 535610
Advisor
ID: 405413
Sampled: Received: 04/05/2023 Completed: 04/14/2023
Farm: RC41
Sample ID: 00001
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P2O5
K2O
Mg S
Mn
Zn
Cu
B
Information
Lime History:
1- Fescue/OGrass/Tim, M 0.4
120-200 0
20
0 0
0
0
0
0
Note: 12
2- Fescue/OGrass/Tim, M 0.0
120-200 0
20
0 0
0
0
0
0
Note: 12
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class:
Mineral
HM% W/V CEC BS% Ac pH P-1 K-1
Ca% Mg%
S-1
Mn-I
Mn-All Mn-Al2
Zn-I
Zn-AI
Cu-I
Na ESP SS-1 NO3-N
0.22 0.94 11.1 87 1.4 5.8 90 65
61 24
52
382
246 246
271
271
172
0.1 1
Sample ID: 00004
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P2O5
K2O
Mg S
Mn
Zn
Cu
B
Information
Lime History:
1- Fescue/OGrass/Tim, M 0.0
120-200 0
0
0 0
0
0
0
0
Note: 12
2- Fescue/OGrass/Tim, M 0.0
120-200 0
0
0 0
0
0
0
0
Note: 12
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class:
Mineral
HM% W/V CEC BS% Ac pH P-1 K-1
Ca% Mg%
S-1
Mn-I
Mn-All Mn-AI2
Zn-I
Zn-AI
Cu-I
Na ESP SS-1 NO3-N
0.51 0.79 16.1 92 1.4 6.3 565 213
69 16
64
246
160 160
717
717
326
0.2 1
North Carolina
A� `� J
lobitt o iru%( FtavJ Umnauukm
Reprogramming of the laboratory -information -management system that makes this report possible is being funded
through a grant from the North Carolina Tobacco Trust Fund Commission.
Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
- Steve Troxler. Commissioner of Agriculture

NCDA&CS Agronomic Division Phone: [phone]
Website: www.ncagr.gov/agronomi/
Report No. FY24-SL003448
Predictive
Client:
Donald Lovelace
3575 NC Hwy 150
Advisor:
Brent Collins
EMA Resources Inc
£
x Soil Report Mehlich-3 Extraction
Reidsville, NC 27320
755 Yadkinville Rd
Mocksville, NC 27028
Sampled County: Rockingham
„r
Links to Helpful Information
Client ID: 535610
Advisor
ID: 405413
Sampled: Received: 09/07/2023 Completed: 09/14/2023
Farm: RC41
Sample ID: 00002
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P2O5
K2O
Mg S
Mn
Zn
Cu
B
Information
Lime History:
1- Fescue/OGrass/Tim, M 0.0
120-200 0
30
0 0
0
0
0
0
Note: 12
2- Fescue/OGrass/Tim, M 0.0
120-200 0
30
0 0
0
0
0
0
Note: 12
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class:
Mineral
HM% W/V CEC BS% Ac pH P-1 K-1
Ca% Mg%
S-1
Mn-I
Mn-All Mn-Al2
Zn-I
Zn-AI
Cu-I
Na ESP SS-1 NO3-N
0.32 0.96 12.6 89 1.4 6.1 304 59
70 16
85
342
221 221
656
656
357
0.2 2
Sample ID: 00003
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P2O5
K2O
Mg S
Mn
Zn
Cu
B
Information
Lime History:
1- Fescue/OGrass/Tim, M 0.0
120-200 0
60
0 0
0
0
0
0
Note: 12
2- Fescue/OGrass/Tim, M 0.0
120-200 0
60
0 0
0
0
0
0
Note: 12
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class:
Mineral
HM% W/V CEC BS% Ac pH P-1 K-1
Ca% Mg%
S-1
Mn-I
Mn-All Mn-AI2
Zn-I
Zn-AI
Cu-I
Na ESP SS-1 NO3-N
0.13 1.00 12.1 91 1.1 6.2 80 37
75 15
42
362
231 231
146
146
247
0.1 1
North Carolina
A� `� J
lobitt o iru%( FtavJ Umnauukm
Reprogramming of the laboratory -information -management system that makes this report possible is being funded
through a grant from the North Carolina Tobacco Trust Fund Commission.
Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
- Steve Troxler. Commissioner of Agriculture

NCDA&CS Agronomic Division Phone: [phone]
Website: www.ncagr.gov/agronomi/
Report No. FY24-SL003445
Predictive
Client:
Johnie Carty
350 Donathan Rd
Advisor:
Brent Collins
EMA Resources Inc
£
x Soil Report Mehlich-3 Extraction
Reidsville, NC 27320
755 Yadkinville Rd
Mocksville, NC 27028
Sampled County: Rockingham
„r
Links to Helpful Information
Client ID: 70260
Advisor
ID: 405413
Sampled: Received: 09/07/2023 Completed: 09/14/2023
Farm: RC118
Sample ID: 00001
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P2O5
K2O
Mg S
Mn
Zn
Cu
B
Information
Lime History:
1- Fescue/OGrass/Tim, M 0.0
120-200 0
80
0 0
0
0
0
0
Note: 12
2- Fescue/OGrass/Tim, M 0.0
120-200 0
80
0 0
0
0
0
0
Note: 12
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class:
Mineral
HM% W/V CEC BS% Ac pH P-1 K-1
Ca% Mg%
S-1
Mn-I
Mn-All Mn-Al2
Zn-I
Zn-AI
Cu-I
Na ESP SS-1 NO3-N
0.27 1.05 13.6 91 1.2 6.4 312 30
78 12
43
143
97 97
418
418
366
0.1 1
Sample ID: 00002
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P2O5
K2O
Mg S
Mn
Zn
Cu
B
Information
Lime History:
1- Fescue/OGrass/Tim, M 0.0
120-200 0
20
0 0
0
0
0
0
Note: 12
2- Fescue/OGrass/Tim, M 0.0
120-200 0
20
0 0
0
0
0
0
Note: 12
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class:
Mineral
HM% W/V CEC BS% Ac pH P-1 K-1
Ca% Mg%
S-1
Mn-I
Mn-All Mn-AI2
Zn-I
Zn-AI
Cu-I
Na ESP SS-1 NO3-N
0.36 0.95 16.0 92 1.4 6.3 452 64
75 15
44
214
140 140
655
655
408
0.1 1
North Carolina
A� `� J
lotwcuo iru%( FtavJ Umnauukm
Reprogramming of the laboratory -information -management system that makes this report possible is being funded
through a grant from the North Carolina Tobacco Trust Fund Commission.
Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
- Steve Troxler. Commissioner of Agriculture

NCDA&CS Agronomic Division Phone: [phone]
Website: www.ncagr.gov/agronomi/
Report No. FY24-SL003440
Client: Thomas / Tommy Carter
Advisor: Brent Collins
Predictive
381 King Carter Rd
EMA Resources Inc
£
Reidsville, NC 27320
755 Yadkinville Rd
x "
Soil Report Mehlich-3 Extraction
Mocksville, NC 27028
Sampled County: Rockingham
Links to Helpful Information
Client ID: 480518
Advisor ID: 405413
Sampled:
Received: 09/07/2023 Completed: 09/14/2023
Farm: RC119
Sample ID: 00009
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P2O5
K2O Mg S Mn
Zn
Cu B
Information
Lime History:
1- Fescue/OGrass/Tim, M 0.8
120-200 0
0 0 0 0
0
0 0
Note: 12
2- Fescue/OGrass/Tim, M 0.0
120-200 0
0 0 0 0
0
0 0
Note: 12
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class: Mineral
HM% W/V
CEC BS% Ac pH P-1 K-1
Ca% Mg%
S-1 Mn-I Mn-All Mn-Al2 Zn-I
Zn-AI
Cu-I Na ESP SS-1 NO3-N
0.46 0.93
11.0 83 1.9 5.6 241 162
53 22
65 149 106 106 460
460
174 0.1 1
North Carolina
lobitty lru%t FuivJ Ctwnauukm
Reprogramming of the laboratory -information -management system that makes this report possible is being funded
through a grant from the North Carolina Tobacco Trust Fund Commission.
Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
- Steve Troxler. Commissioner of Agriculture

NCDA&CS Agronomic Division Phone: [phone]
Website: www.ncagr.gov/agronomi/
Report No. FY24-SL007382
Client: Ken Martin
Advisor: Brent Collins
Predictive
551 Bakers Cross Rd
EMA Resources Inc
£
Reidsville, NC 27320
755 Yadkinville Rd
x "
Soil Report Mehlich-3 Extraction
Mocksville, NC 27028
Sampled County: Rockingham
Links to Helpful Information
Client ID: 329325
Advisor ID: 405413
Sampled:
Received: 10/10/2023 Completed: 10/20/2023
Farm: RC130
Sample ID: 00001
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P2O5
K2O Mg S
Mn Zn
Cu B
Information
Lime History:
1- Fescue/OGrass/Tim, M 0.7
120-200 0
90 0 0
0 0
0 0
Note: 12
2- Fescue/OGrass/Tim, M 0.0
120-200 0
90 0 0
0 0
0 0
Note: 12
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class:
Mineral
HM% W/V
CEC BS% Ac pH P-1 K-1
Ca% Mg%
S-1 Mn-I Mn-All Mn-Al2 Zn-I Zn-AI
Cu-I Na ESP SS-1 NO3-N
0.13 1.21
8.0 79 1.7 5.6 137 24
70 8
48 173 121 121
98 98
70 0.1 1
North Carolina
lobitty lru%t FuivJ Ctwnauukm
Reprogramming of the laboratory -information -management system that makes this report possible is being funded
through a grant from the North Carolina Tobacco Trust Fund Commission.
Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
- Steve Troxler. Commissioner of Agriculture

2T Annual Report Forms
Final Audit Report 2024-02-09
Created: 2024-02-09
By: Brent Collins([e-mail])
Status: Signed
Transaction ID: CBJCHBCAABAAMt7jzXj1GrYp4lRIAxAruJSmRh1vojl6
"2T Annual Report Forms" History
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WQ0002376
Final Audit Report
Reidsville Annual Report -
Created: 2024-02-12
By: Brent Collins([e-mail])
Status: Signed
Transaction ID: CBJCHBCAABAAJVInJ-oDPBXhEFuVSbjeJKYurnGCNOb1
2024-02-13
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