WQ0039552_2023 Residual Annual Report_20240229 (2)

Initial Review
Reviewer
nathaniel.thorn burg
Is this submittal an application? (Excluding additional information.) *
Yes No
If not an application what is the submittal type?* Annual Report
Residual Annual Report
Additional Information
Other
Annual Report Year* 2023
Permit Number (IR) * WQ0039552
Applicant/Permittee Town of Mocksville
Email Notifications
Does this need review by the hydrogeologist? * Yes U No
Regional Office Winston-Salem
CO Reviewer
Admin Reviewer Wanda Gerald

Submittal Form
Project Contact Information
Please provide information on the person to be contacted by NDB Staff regarding electronic submittal, confirmation of receipt, and other correspondence.
Name* Brent Collins
Email Address*
[e-mail]
Project Information
.........................
Application/Document Type*
New (Fee Required)
Modification - Major (Fee Required)
Renewal with Major Modification (Fee
Required)
Annual Report
Additional Information
Other
Phone Number*
3363993646
Modification - Minor
Renewal
GW-59, NDMR, NDMLR, NDAR-1,
N DAR-2
Residual Annual Report
Change of Ownership
We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form.
https://edoes.deq.nc.gov/Forms/NonDischarge_Monitoring_Report
Permit Type:*
Wastewater Irrigation
High -Rate Infiltration
Other Wastewater
Reclaimed Water
Closed -Loop Recycle
Residuals
Single -Family Residence Wastewater
Other
Irrigation
Permit Number:*
WQ0039552
Has Current Existing permit number
Applicant/Permittee Address*
171 Clement Street, Mocksville, NC 27028
Facility Name*
Town of Mocksville Class A Residuals Program
Please provide comments/notes on your current submittal below.
At this time, paper copies are no longer required. If you have any questions about what is required, please contact Nathaniel Thornburg
at [e-mail].
Please attach all information required or requested for this submittal to be reviewed here.
(Application Form, Engineering Plans, Specifications, Calculations, Etc.)
2023 Mocksville WTP Annual Report - WQ0039552.pdf 4.88MB
Upload only 1 PDF document (less than 250 MB). Multiple documents must be combined into one PDF file unless file is larger
than upload limit.
* By checking this box, I acknowledge that I understand the application will not be accepted for pre -review until the fee (if required) has
been received by the Non -Discharge Branch. Application fees must be submitted by check or money order and made payable to the
North Carolina Department of Environmental Quality (NCDEQ). I also confirm that the uploaded document is a single PDF with all parts
of the application in correct order (as specified by the application).
Mail payment to:
NCDEQ — Division of Water Resources
Attn: Non -Discharge Branch
1617 Mail Service Center
Raleigh, NC 27699-1617
Signature
Submission Date 2/29/2024

Town of Mocksville WTP
2023 Annual Report
Residuals Land Application
Permit No. WQ0039552
Prepared By:
EMA Resources, Inc.
Phone [phone] — Fax [phone]
755 Yadkinville Rd — Mocksville, NC 27028

It
MI. � A,
sources, Inc.
February 27, 2024
DENR/Water Quality Section
Non -Discharge Compliance Unit
1617 Mail Service Center
Raleigh, NC 27699-1617
Re: 2023 Annual Report — Mocksville WTP
Treatment and Land Application of Residuals
Permit No. WQ0039552
Dear Sir or Madam:
Enclosed is the 2023 Annual Report for the above referenced land application permit.
During 2023 EMA Resources, Inc. land applied 87.13 dry tons of wastewater residuals to
42 acres of private farmland. Please contact Brent Collins - Director of Technical
Services if you have any further questions regarding this report.
Sincerely,
Brent Collins
Director of Technical Services
brent.collinsLemaresourcesinc.com
Phone [phone] — Fax [phone]
755 Yadkinville Rd — Mocksville, NC 27028

G/ SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM CLASS A ANNUAL DISTRIBUTION AND NIARKIETIN
WQ PERMIT 4: WQ0039552 FACILITY NAME: Town of ', locksville - W a-er Treatment Plant
PHONE: COUNTY: Da- ie CWERATOR: Town of MmicsAlle
FACILITY TYPE (ptease check one): [0 Surface iMposel (coinplek Part A (Source(s) and"Residual in Volume only) and Part C)
Eif DistHbudon and Marketing (complete Parts A, B, and Q
MAS Me fiaellit; in operation during the past calendar car? Ves 51 No if No skip parts A, B, C and cerfify form below
Part A,-: Pan W:
Volume (dry tons) Recipient infiormutwn
Sources(s) (include NPDFS 4 if I
Month At-nendment
appmeable) Residiral in Product (Out N arne lking (s) Volume (dr tons) fi--tendcd use(s)
BuAgent
january
February
March
April
Alay Nlocks0le VVTP
7LLRopr Spillman amend.-nent
8 78 so
june Mockwille WTP 15 11 1533 Roger Spillman 153-1 soil amendment
July
August
Septenther
October
lNoveraher
liecember
Total from FORM DMSDF (sup)l 0 0 is 10
Annual (dry tons): 0 ST11 -ST13 8 7. 11
AnnnchmnKO und: 1 Bulking %genifs) used:
if more space is required, attach additional infisri-nation sheets tFORM DNISDF ,supp)): Total'Number of Forn- ')%ISF)F iSuDp)l 0 _j
Pan C:
AS; was compliant during Me pm-- calendar year with all_ conditions of the land applicadon perndt its
(including but not limited to items 1�3 below) issued by the Division of Water Quality: No Iff No, Explain in Narritive
1 All monitoring was clone in accordance whh Be parnii and reported for the year as required and three (3) copies of cerfific-d lahoraioes It are attached,
1 All operation and maintenance requirements - eree compiled Wth or, in the case of a devAtio, prior authorization mys receAd from the Division ofWater Quality.
3. No cmrmTMMn of Ground U'ater Quality Standards occurred at a monitoring well.
I ce-rifv, under -nnaltv of law, that the above infortuation is. to the best of mv knowkdae anti belief true, accurate and complete. .1 am a,*,,, are that there are sianificant
penalties for submitting false- information, including the possibility of fines a nimprisonment My kno-wing- violations
t
02/22/2z 02/19/24
d Ro-�b 19 15:5S �S-
e ccc --
Signature of Permittee
Date Signature of Preparer��-
(if diff�rcnl from Perminee)
"I'mParer is &thred MAO CFRPan 50-1 -9(r) and 15A NCAC 2T 1102(26)
DENR FORM DMSDF (12 200M

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5/15/2023
mg/kg mg/L Equiv Weight Milli Equiv
Sodium 2290 19.6024 23 0.852278
Calcium 4300 36.808 20 1.8404
Magnesium 5240 44.8544 12 3.737867
Percent Solids 0.856
SAR
0.51
SAR Na+
a (Ca2+ + M92+)
0.85228
'',::: 0.5( 1.8404 2 + 3.73787 2 )

12/6/2023
mg/kg
mg/L
Equiv Weight Milli Equiv
Sodium
394
12.8838
23 0.560165
Calcium
1980
64.746
20 3.2373
Magnesium
4580
149.766
12 12.4805
Percent Solids
3.27
SAR
0.20
SAR
Na+
a (Ca2+ + M92+)
0.56017
'',::: 0.5( 3.2373 2 + 12.48050 2 )

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
Town of Mocksville-WTP Total Dry Tons Applied (Annual):
WQ0039552 Cation Exchange Capacity (non 503 only):
Roger Spillman Owner: Roger Spillman Predominant Soil Series:
22.92 Acres Permitted: 22.92 Site #: NC-DV08 Field #:
59.48
CeB2
1
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample Or
pose
Date
......1......IF
4/5/23
2.....
7/18/23
3.....1
12/6/23
4....1
6.........
8....
9.....
10
11
12
% Solids
1.87
1.24
3.27
Arsenic
26.3
20.8
8.27
Cadmium
5.26
4.17
1.52
Copper
157
133
32.4
Chromium
16.9
20.8
80.3
Lead
15.8
16.7
33
Mercury
1.13
1.75
0.655
Molyb-
denum
7.11
12.5
4.55
Nickel
13.9
14.8
33.6
Selenium
26.3
29.2
10.6
Zinc
435
269
105
Total
Phos-
horus
33500
27000
1680
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
1......
2.....
9.....
1......
1..1......
1..�....
.....3.....
.....4....
.....5.....
.....6....
.....�.....
......8....
DT/Ac./
App.
Event
1.38
0.55
0.67
Arsenic
0.072
0.023
0.011
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.106
Cadmium
0.014
0.005
0.002
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.021
Copper
0.433
0.146
0.043
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.622
Chromium
0.047
0.023
0.107
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.177
Lead
0.044
0.018
0.044
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.106
Mercury
0.003
0.002
0.001
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.006
Molyb-
0.020
0.014
0.006
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.039
denum
Nickel
0.038
0.016
0.045
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.099
Selenium
0.072
0.032
0.014
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.119
Zinc
1.199
0.295
0.140
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1.634
Total
Phos-
92.326
29.592
2.248
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
124.166
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with
a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am
aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Signature of Land Applier
2/19/2024
Date
DENR FORM MFLSF (12/2006)

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ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
Town of Mocksville-WTP Total Dry Tons Applied (Annual):
WQ0039552 Cation Exchange Capacity (non 503 only):
Roger Spillman Owner: Roger Spillman Predominant Soil Series:
19.08 Acres Permitted: 19.08 Site #: NC-DVO08 Field #:
163.27
MrB2
6
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample or
.......1......F
2.....F
3.....IF
4....
5.....
6.........I1
9.....
1..2....
1..1......
1..2....
Com-
W1'P
Neilson
WTP
posite
12/6/23
May Avg
Date
% Solids
3.27
22.3
Arsenic
8.27
6.2
Cadmium
1.52
0.6
Copper
32.4
43.4
Chromim
80.3
53.7
Lead
33
28.1
Mercury
0.655
0.1
Molyb-
4.55
1.5
denum
Nickel
33.6
24.7
Selenium
10.6
1.5
Zinc
105
134
Total
Phos-
1680
2330
horus
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
D
000000000111H
Event
1 1
1 1 •
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
1 11
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
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1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
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1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
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1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
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1 11
1 11
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 11
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1 1 �
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
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1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
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1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1•.
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1 •1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
Total
' •
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1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
•:�
•
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with
a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am
aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
t
Signature of Land Applier
2/19/2024
Date
DENR FORM MFLSF (12/2006)

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mil ,
6/1 /2023
EMA Resources Inc
Mr. Brent Collins
755 Yadkinville Rd
Mocksville, NC, 27028
Ref: Analytical Testing
Lab Report Number: 23-137-0095
Client Project Description: Mocksville, NC
Dear Mr. Brent Collins:
Waypoint Analytical, LLC. received sample(s) on 5/17/2023 for the analyses presented in the following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Where the laboratory was not responsible for the sampling
stage (refer to the chain of custody) results apply to the sample as received.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2021) and NELAC unless otherwise indicated. Any parameter
for which the laboratory is not officially NELAP accredited is indicated by a '—'symbol. These are not included in
the scope because NELAP accreditation is either not available or has not been applied for. Additional
certifications may be held/are available for parameters, where NELAP accreditation is not required or applicable.
A full list of certifications is available upon request.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Connie Cook
Project Manager
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 1 of 8

Way to
PM�
WRTIA"Wi
tMain 901.213.2400 0 Fax u f,
www.waypointanalyticaLcom
Certification Summary
Laboratory ID: WP MTN: Waypoint Analytical, LLC., Memphis, TN
State
Program
Lab ID
Expiration Date
Alabama
State Program
40750
02/29/2024
Arkansas
State Program
88-0650
02/07/2024
California
State Program
2904
06/30/2023
Florida
State Program
- NELAP
E871157
06/30/2023
Georgia
State Program
C044
11/14/2025
Georgia
State Program
04015
06/30/2023
Illinois
State Program
- NELAP
200078
10/10/2023
Kentucky
State Program
80215
06/30/2023
Kentucky
State Program
KY90047
12/31/2023
Louisiana
State Program
- NELAP
LA037
12/31/2023
Louisiana
State Program
- NELAP
04015
06/30/2023
Mississippi
State Program
MS
11/14/2025
North Carolina
State Program
47701
07/31/2023
North Carolina
State Program
415
12/31/2023
Pennsylvania
State Program
- NELAP
68-03195
05/31/2024
South Carolina
State Program
84002
06/30/2023
Tennessee
State Program
02027
11/14/2025
Texas
State Program
- NELAP
T104704180
09/30/2023
Virginia
State Program
00106
06/30/2023
Virginia
State Program
- NELAP
460181
09/14/2023
Page 1 of 1 00001/23-137-0095
Page 2 of 8

Way lht,(2)
PM�TICAL'
Sample Summary Table
Report Number: 23-137-0095
Client Project Description: Mocksville, NC
Lab No Client Sample ID Matrix Date Collected Date Received
94920 Mocksville VVTP Solids 05/15/2023 11:15 05/17/2023
Page 3 of 8

to
Way� PA
► x
Client: EMA Resources Inc
Project: Mocksville, NC
Lab Report Number: 23-137-0095
Date: 6/1 /2023
Main 901.213.2400 .41
wwwmaypointanalyticaLcorn
CASE NARRATIVE
Metals Analysis Method 601 OD
Sample 95251 (Pilgrims Hickory Hatchery PILHIHA)
Analyte: Aluminum
QC Batch No: 1-683237/1-682745
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 95251 (Pilgrims Hickory Hatchery PILHIHA)
Analyte: Calcium
QC Batch No: 1-683237/1-682745
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 95251 (Pilgrims Hickory Hatchery PILHIHA)
Analyte: Potassium
QC Batch No: 1-683237/1-682745
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 95251 (Pilgrims Hickory Hatchery PILHIHA)
Analyte: Phosphorus
QC Batch No: 1-683237/1-682745
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Solids Total Mercury Analysis - CVAA Method 7471A
Sample 59842
Analyte: Mercury
QC Batch No: 1-683650/1-683458
The matrix spike, matrix spike duplicate and the post digestion spike were all outside of the quality control
acceptance ranges. Matrix interference is suspected
Page 4 of 8

Way to
PM�
46245
EMA Resources Inc
Mr. Brent Collins
755 Yadkinville Rd
Mocksville , NC 27028
Project Mocksville, NC
Information :
Report Date : 06/01/2023
Received �.���y05/17/2023
-
Connie Cook
Report Number : 23-137-0095
REPORT OFANALYSIS
Project
Manager
Lab No : 94920
Matrix:
Solids
Sample ID : Mocksville WTP
Sampled:
5/15/2023
11:15
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Method
Moisture
99.1
%
1
05/22/2317:15
JLS
SW-DRYWT
Ammonia Nitrogen
15400
mg/Kg -
dry
1780
11100
1
06/01/23 06:45
JPJ
4500NH3C-2011
Nitrate+Nitrite-N
306 JB
mg/Kg -
dry
111
556
1
05/18/23 14:55
ZBD
4500NO3F-2016
Organic N
16330
mg/Kg -
dry
1778
11110
1
05/30/23 12:30
CALCULATION
pH
6.5
S.U.
1
05/23/2316:00
CNB
9045D
Total Solids
0.856
%
0.010
0.010
1
05/22/23 17:15
JLS
2540G-2011
Total Kjeldahl Nitrogen
31800
mg/Kg -
dry
1110
27800
1
05/30/23 12:30
JPJ ;M-4500-NH3C-TKlN
Phosphorus
2390
mg/Kg -
dry
307
556
1
05/20/23 08:08
BKN
6010D
Aluminum
138000
mg/Kg -
dry
513
556
1
05/20/23 08:08
BKN
6010D
Arsenic
<26.7
mg/Kg -
dry
26.7
55.6
1
05/20/23 08:08
BKN
6010D
Cadmium
<2.22
mg/Kg -
dry
2.22
11.1
1
05/20/23 08:08
BKN
6010D
Calcium
<4300
mg/Kg -
dry
4300
5560
1
05/20/23 08:08
BKN
6010D
Chromium
95.2
mg/Kg -
dry
26.2
27.8
1
05/20/23 08:08
BKN
6010D
Copper
41.73
mg/Kg -
dry
34.4
55.6
1
05/20/23 08:08
BKN
6010D
Iron
55100
mg/Kg -
dry
947
1110
1
05/20/23 08:08
BKN
6010D
Lead
43.8
mg/Kg -
dry
20.0
33.3
1
05/20/23 08:08
BKN
6010D
Magnesium
5240
mg/Kg -
dry
287
556
1
05/20/23 08:08
BKN
6010D
Manganese
1260
mg/Kg -
dry
36.1
55.6
1
05/20/23 08:08
BKN
6010D
Mercury
<2.53
mg/Kg -
dry
2.53
21.0
1
05/23/23 10:51
FDS
7471A
Molybdenum
<15.0
mg/Kg -
dry
15.0
27.8
1
05/20/23 08:08
BKN
6010D
Nickel
42.1
mg/Kg -
dry
13.3
27.8
1
05/20/23 08:08
BKN
6010D
Potassium
4660
mg/Kg -
dry
687
1110
1
05/20/23 08:08
BKN
6010D
Selenium
<35.6
mg/Kg -
dry
35.6
55.6
1
05/20/23 08:08
BKN
6010D
Qualifiers/ B
Analyte detected in blank
DF
Dilution Factor
Definitions J
Estimated value
MQL
Method Quantitation Limit
Page 5 of 8

0
Waypoeint2790
Whitten
Road, Memphis, TN 38133
Main 901.213.2400 0 Fax [phone]
ANALYTICAL
www.waypoiintanalyticaLcom
46245
EMA Resources Inc
Project
Mocksville, NC
Mr. Brent Collins
Report Date : 06/01/2023
755 Yadkinville Rd
Information :
Received : 05/17/2023
Mocksville , NC 27028
Connie Cook
Report Number : 23-137-0095
REPORT OFANALYSIS
Project Manager
Lab No : 94920
Matrix: Solids
Sample ID : Mocksville WTP
Sampled: 5/15/2023 11:15
Test
Results
Units
MDL
MQL DF Date / Time By Analytical
Analyzed Method
Sodium
22903
mg/Kg - dry
1440
2780 1 05/20/23 08:08 BKN 6010D
Zinc
186
mg/Kg - dry
90.0
139 1 05/20/23 08:08 BKN 6010D
Sulfur
3080
mg/Kg - dry
576
1110 1 05/20/23 08:08 BKN 6010D
Sodium Absorption Ratio
0.643
Ratio
0.01
0.01 1 05/20/23 08:08 CALCULATION
Qualifiers/ B Analyte detected in blank
Definitions J Estimated value
DF Dilution Factor
MQL Method Quantitation Limit
Page 6 of 8

l0
Waypoint",
J123.8224
Shipment Receipt Form
Customer Number: 46245
Customer Name: EMA Resources Inc
Report Number: 23-137-0095
Shipping Method
0 Fed Ex 0 US Postal 0 Lab
0 UPS 0 Client 0 Courier
0 Other
Thermometer ID:
T136
Shipping container/cooler uncompromised?
Yes
0 No
Number of coolers/boxes received
1
Custody seals intact on shipping container/cooler?
0 Yes
0 No
Not Present
Custody seals intact on sample bottles?
0 Yes
0 No
Not Present
Chain of Custody (COC) present?
# Yes
0 No
COC agrees with sample label(s)?
# Yes
0 No
COC properly completed
# Yes
0 No
Samples in proper containers?
# Yes
0 No
Sample containers intact?
# Yes
0 No
Sufficient sample volume for indicated test(s)?
# Yes
0 No
All samples received within holding time?
# Yes
0 No
Cooler temperature in compliance?
# Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
# Yes
0 No
Water - Sample containers properly preserved
0 Yes
0 No
N/A
Water - VOA vials free of headspace
0 Yes
0 No
N/A
Trip Blanks received with VOAs
0 Yes
0 No
N/A
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
0 N/A
F_ High concentration container (48 hr)
F_ High concentration pre -weighed (methanol -14 d)
F_ Low concentration EnCore samplers (48 hr)
F_ Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included? 0 Yes * No
Comments:
Signature: IMakayla Weaver Date & Time: 05/17/2023 11:59:14
Page 7 of 8

Page 8 of 8

mil ,
12/18/2023
EMA Resources Inc
Mr. Brent Collins
755 Yadkinville Rd
Mocksville, NC, 27028
Ref: Analytical Testing
Lab Report Number: 23-341-0064
Client Project Description: Mocksville, NC
Dear Mr. Brent Collins:
Waypoint Analytical, LLC. received sample(s) on 12/7/2023 for the analyses presented in the following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Where the laboratory was not responsible for the sampling
stage (refer to the chain of custody) results apply to the sample as received.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2021) and NELAC unless otherwise indicated. Any parameter
for which the laboratory is not officially NELAP accredited is indicated by a '—'symbol. These are not included in
the scope because NELAP accreditation is either not available or has not been applied for. Additional
certifications may be held/are available for parameters, where NELAP accreditation is not required or applicable.
A full list of certifications is available upon request.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Connie Cook
Project Manager
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 1 of 8

Way to
PM�
WRTIA"Wi
tMain 901.213.2400 0 Fax u f,
www.waypointanalyticaLcom
Certification Summary
Laboratory ID: WP MTN: Waypoint Analytical, LLC., Memphis, TN
State
Program
Lab ID
Expiration Date
Alabama
State Program
40750
02/29/2024
Arkansas
State Program
88-0650
02/07/2024
California
State Program
2904
06/30/2024
Florida
State Program
- NELAP
E871157
06/30/2024
Georgia
State Program
C044
11/14/2025
Georgia
State Program
04015
06/30/2024
Illinois
State Program
- NELAP
200078
10/31/2024
Kentucky
State Program
80215
06/30/2024
Kentucky
State Program
KY90047
12/31/2023
Louisiana
State Program
- NELAP
LA037
12/31/2023
Louisiana
State Program
- NELAP
04015
06/30/2024
Mississippi
State Program
MS
11/14/2025
North Carolina
State Program
47701
07/31/2024
North Carolina
State Program
415
12/31/2023
Pennsylvania
State Program
- NELAP
68-03195
05/31/2024
South Carolina
State Program
84002
06/30/2024
Tennessee
State Program
02027
11/14/2025
Texas
State Program
- NELAP
T104704180
09/30/2024
Virginia
State Program
00106
06/30/2024
Virginia
State Program
- NELAP
460181
09/14/2024
Page 1 of 1 00001/23-341-0064
Page 2 of 8

Way lht,(2)
PM�TICAL'
Sample Summary Table
Report Number: 23-341-0064
Client Project Description: Mocksville, NC
Lab No Client Sample ID Matrix Date Collected Date Received
88990 Mocksville VVTP Solids 12/06/2023 09:00 12/07/2023
Page 3 of 8

to
Way� PA
► x
Client: EMA Resources Inc
Project: Mocksville, NC
Lab Report Number: 23-341-0064
Date: 12/15/2023
Main 901.213.2400 .41
wwwmaypointanalyticaLcorn
CASE NARRATIVE
Nitrate + Nitrite Nitrogen Method 4500NO3F-2016
Analyte: Nitrate+Nitrite N
QC Batch No: 1-722647/1-721814
Target analyte(s) was identified in the method blank associated with this project, below the Method Quantitation
Limit. Per laboratory protocol any associated affected sample result is flagged "B" to indicate that it was detected
in the method blank.
Metals Analysis Method 6010D
Sample 97425
Analyte: Calcium
QC Batch No: 1-721808/1-721313
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 97425
Analyte: Sulfur
QC Batch No: 1-721808/1-721313
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Solids Total Mercury Analysis - CVAA Method 7471A
Sample 88986 (Dust)
Analyte: Mercury
QC Batch No: 1-722057/1-721777
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Page 4 of 8

Way to
PM�
46245
EMA Resources Inc
Mr. Brent Collins
755 Yadkinville Rd
Mocksville , NC 27028
Project Mocksville, NC
Information :
Report Date : 12/18/2023
Received �.���y12/07/2023
-
Connie Cook
Report Number : 23-341-0064
REPORT OFANALYSIS
Project
Manager
Lab No : 88990
Matrix:
Solids
Sample ID : Mocksville WTP
Sampled:
12/6/2023
9:00
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Method
Moisture
96.7
%
0
0.050
1
12/13/2316:17
A.B
SW-DRYWT
Ammonia Nitrogen
27003
mg/Kg -
dry
485
3030
1
12/15/23 12:13
JPJ
4500NH3C-2011
Nitrate+Nitrite-N
192 B
mg/Kg -
dry
30.3
152
1
12/15/23 10:05
CLP
4500NO3F-2016
Organic N
166003
mg/Kg -
dry
484.8
3030
1
12/14/23 07:59
CALCULATION
pH
6.7
S.U.
1
12/08/2311:35
CNB
9045D
Total Solids
3.27
%
0.010
0.010
1
12/08/23 16:00
CAH
2540G-2011
Total Kjeldahl Nitrogen
19300
mg/Kg -
dry
303
7580
1
12/14/23 07:59
JPJ ;M-4500-NH3C-TKlN
Phosphorus
1680
mg/Kg -
dry
84.8
152
1
12/12/23 19:59
TJS
6010D
Aluminum
95200
mg/Kg -
dry
141
152
1
12/12/23 05:35
TJS
6010D
Arsenic
8.273
mg/Kg -
dry
7.58
15.2
1
12/12/23 05:35
TJS
6010D
Cadmium
<1.52
mg/Kg -
dry
1.52
3.03
1
12/12/23 05:35
TJS
6010D
Calcium
1980
mg/Kg -
dry
1170
1520
1
12/12/23 05:35
TJS
6010D
Chromium
80.3
mg/Kg -
dry
7.58
7.58
1
12/12/23 05:35
TJS
6010D
Copper
32.4
mg/Kg -
dry
9.09
15.2
1
12/12/23 19:59
TJS
6010D
Iron
41500
mg/Kg -
dry
259
303
1
12/12/23 19:59
TJS
6010D
Lead
33.0
mg/Kg -
dry
6.06
9.09
1
12/12/23 05:35
TJS
6010D
Magnesium
4580
mg/Kg -
dry
78.8
152
1
12/12/23 05:35
TJS
6010D
Manganese
991
mg/Kg -
dry
10.6
15.2
1
12/12/23 05:35
TJS
6010D
Mercury
<0.655
mg/Kg -
dry
0.655
5.42
1
12/12/23 12:44
FDS
7471A
Molybdenum
<4.55
mg/Kg -
dry
4.55
7.58
1
12/12/23 19:59
TJS
6010D
Nickel
33.6
mg/Kg -
dry
4.55
7.58
1
12/12/23 19:59
TJS
6010D
Potassium
3360
mg/Kg -
dry
188
303
1
12/12/23 05:35
TJS
6010D
Selenium
<10.6
mg/Kg -
dry
10.6
15.2
1
12/12/23 19:59
TJS
6010D
Qualifiers/ B Analyte detected in blank
DF
Dilution Factor
Definitions J Estimated value
MQL
Method Quantitation Limit
Page 5 of 8

0
Waypoeint2790
Whitten
Road, Memphis, TN 38133
Main 901.213.2400 0 Fax [phone]
ANALYTICAL
www,waypoiintanalyticaLcom
46245
EMA Resources Inc
Project
Mocksville, NC
Mr. Brent Collins
Report Date : 12/18/2023
755 Yadkinville Rd
Information :
Received : 12/07/2023
Mocksville , NC 27028
Connie Cook
Report Number : 23-341-0064
REPORT OFANALYSIS
Project Manager
Lab No : 88990
Matrix: Solids
Sample ID : Mocksville WTP
Sampled: 12/6/2023 9:00
Test
Results
Units
MDL
MQL DF Date / Time By Analytical
Analyzed Method
Sodium
<394
mg/Kg - dry
394
758 1 12/12/23 05:35 TJS 6010D
Zinc
105
mg/Kg - dry
25.8
37.9 1 12/12/23 05:35 TJS 6010D
Sulfur
1270
mg/Kg - dry
158
303 1 12/12/23 05:35 TJS 6010D
Sodium Absorption Ratio
<0.01
Ratio
0.01
0.01 1 12/12/23 05:35 CALCULATION
Qualifiers/ B Analyte detected in blank
Definitions J Estimated value
DF Dilution Factor
MQL Method Quantitation Limit
Page 6 of 8

l0
Waypoint",
J123.8224
Shipment Receipt Form
Customer Number: 46245
Customer Name: EMA Resources Inc
Report Number: 23-341-0064
Shipping Method
0 Fed Ex 0 US Postal 0 Lab
0 UPS 0 Client 0 Courier
0 Other
Thermometer ID:
T100
Shipping container/cooler uncompromised?
Yes
0 No
Number of coolers/boxes received
1
Custody seals intact on shipping container/cooler?
0 Yes
0 No
Not Present
Custody seals intact on sample bottles?
0 Yes
0 No
Not Present
Chain of Custody (COC) present?
# Yes
0 No
COC agrees with sample label(s)?
# Yes
0 No
COC properly completed
# Yes
0 No
Samples in proper containers?
# Yes
0 No
Sample containers intact?
# Yes
0 No
Sufficient sample volume for indicated test(s)?
# Yes
0 No
All samples received within holding time?
# Yes
0 No
Cooler temperature in compliance?
# Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
# Yes
0 No
Water - Sample containers properly preserved
0 Yes
0 No
N/A
Water - VOA vials free of headspace
0 Yes
0 No
N/A
Trip Blanks received with VOAs
0 Yes
0 No
N/A
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
0 N/A
F_ High concentration container (48 hr)
F_ High concentration pre -weighed (methanol -14 d)
F_ Low concentration EnCore samplers (48 hr)
F_ Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included? 0 Yes * No
Comments:
Signature: ICarleen Qualls Date & Time: 12/07/2023 11:41:46
Page 7 of 8

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Page 8 of

aceAnalytical° ANALYTICAL REPORT
June 01, 2023
EMA Resources
Sample Delivery Group: L1616826
Samples Received: 05/16/2023
Project Number:
Description: Sludge
Report To: Mr. Brent Collins
755 Yadkinville Road
Mocksville, NC 27028
Entire Report Reviewed By:
Jason Romer
Project Manager
Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be
reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pace
Analytical National is performed per guidance provided in laboratory standard operating procedures ENV-SOP-MTJL-0067and
ENV-SOP-MTJL-0068. Where sampling conducted by the customer, results relate to the accuracy ofthe information provided,
and as the samples are received.
%yp
[Cn
Sc
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1616326 06/01/23 03:37 1 of 22

TABLE OF CONTENTS
cj'x
11 . c iI M")fle' of Coil
2
Ss: Sample Summary
3
Cn: Case Narrative
4
Sr: Sample Results
5
SS
MOCKSVILLE WTP L1616826-01
5
Fn
oc ouaHblt bil 111 0 1 11,11,1111,11,11 a II""
Wet ( IheinnIIstii ),It 'n't Meflhod 9012
"7
1711-1
Ll
Wet ( Iheinn�stii ),It 'n't Meflhod 903A1, 9030��1113
77 .......................
Wet ( Iheinnstii ),It :n't Meflhod 9G�15L)
9
Wet ( IheinnIstii ),It :n't Meflhod ���)93/1010A
10
FGI
Meii 4: 1 � I )t w Meflh�'d 7A170A
11
M et a �� s fl :n't Meflhod
12
.. ......................................
11111(datflie Oil gaink binniq!)Ourlds (G( AMS) 'n't Meflhod 82(150����)
I �I 0 1 firlated AcA 1eii 'Addes (G( ',nit Meflhod 8"III 1
I
177-1
ILI
':��Iesflddes (G( b�it Vlietlhod 808"V:1113
17
Serninii 1111datflie it gaink 011,11n11!1Mourids (G( PMS) 'n't Meel hod 82'M:
18
GI: Glossary of Terms
20
AL AccriedftatJoins & M"e'.atJoII" is
1
Sc: Sample Chain of Custody
22
ACCOUNT: PROJECT: SDG:
DATE/TIME:
PAGE:
EMA Resources L1616326
06/01/23 03:37
2 of22

SAMPLE SUMMARY
Collected by
Collected date/time
Received date/time
MOCKSVII I E WT' P 1 1616826-01 Waste
Brent Collins
05/15/23 1115
05/16/23 09 00
...................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................
Method
Batch
Dilution Preparation
Analysis
Analyst
...............
Location'
date/time
date/time
Preparation by Method 1311
WG2061232
1 05/18/23 15 01
05/18/23 15 01
_WS
Mt. Juliet, 1
Preparation by Method 1311
WG2062582
1 05/19/23 1116
05/19/23 1116
BTP
Mt. Juliet, TN
Wet Chemistry by Method 9012 B
WG2061580
1 05/17/23 20 26
05/18/23 00 24
LDT
Mt. Juliet, TN
III
Wet Chemistry by Method 9034-9030B
WG2062811
1 05/17/23 19 52
05/19/23 0147
RCD
Mt. Juliet, TN
Wet Chemistry by Method 9045D
WG2063275
1 05/20/23 12 35
05/22/23 08 37
MCC
Mt. Juliet, TN
Fn
Wet Chemistry by Method D93/1010A
WG2064034
1 05/22/23 00 59
05/22/23 00 59
CRB
Mt. Juliet, TN
Mercury by Method 7470A
WG2063312
1 05/22/23 13 44
05/31/23 18 13
LAS
Mt. Juliet, TN
Metals (ICP) by Method 6010D
WG2064577
1 05/23/23 08 37
05/23/23 17 31
ZSA
Mt. Juliet, TN
Ll
Volatile Organic Compounds (GC/MS) by Method 8260D
WG2063681
1 05/22/23 03 23
05/22/23 03 23
ACG
Mt. Juliet, TN
Chlorinated Acid Herbicides (GC) by Method 8151A
WG2064076
1 05/23/23 15 20
05/24/23 16 28
DLH
Mt. Juliet, TN
Pesticides (GC) by Method 8081B
WG2064735
1 05/23/23 22 05
05/24/23 05 59
RDH
Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
WG2064734
1 05/23/23 06 21
05/25/23 02 58
AED
Mt. Juliet, TN
GI
.. ......................................
) Ll
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1616326 06/01/23 03:37 3 of 22

CASE NARRATIVE
All sample aliquots were received at the correct temperature, in the proper containers, with the
appropriate preservatives, and within method specified holding times, unless qualified or notated within
the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples
have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control
are within established criteria except where addressed in this case narrative, a non-conformance form
or properly qualified within the sample results. By my digital signature below, I affirm to the best of my
S
knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the
.......................
quality of the data have been identified by the laboratory, and no information or data have been
knowingly withheld that would affect the quality of the data.
Sr
Jason Romer
Project Manager
C
SC
Project Narrative
All Reactive Cyanide results reported in the attached report were determined as totals using method 9012 B.
All Reactive Sulfide results reported in the attached report were determined as totals using method 9034-903013.
Sample Narrative
Pyridine and Benzidine are reporting with critically low recovery in the laboratory control sample(s). These compounds are
method defined poor performers. Results are estimated.
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1616326 06/01/23 03:37 4 of 22

f�'r�'n�!dfN��T"�!WL�I��,F�k���✓T^�,N rah/��,F�Y����✓T^�,N�✓��IIVIIIIIIVIIIVIIVIIIIIIIIIVIIVIIVIIIIIIIIIVIIIIIIVIIIVIIIIVIIIIIIVIIIVIIVIIIIIIIIIVIIVIIVIIIIIIIIIVIIIIIIVIIIVIIIIVIIIIIIVIIIVIIVIIIIIIIIIVIIVIIVIIIIIIIIIVIIIIIIVIIh
MOCKSVILLE WTP
SAMPLE RESULTS
- 01
Collected date/time: 05/15/23 11:15
L1616826
Preparation by Method 1311
Result
Qualifier
Prep
Batch
Analyte
date / time
TCLP Extraction
5/18/2023 3:0138 PM
WG2061232
TCLP ZHE Extraction
5/19/20231116:09 AM
WG2062582
Initial pH N/A
5/18/2023 3:0138 PM
WG2061232
Final pH N/A
5/18/2023 3:0138 PM
WG2061232
Wet Chemistry by Method 9012 6
Fn
Result
Qualifier
RDL Dilution
Analysis Batch
Analyte mg/kg
mg/kg
date / time
Reactive Cyanide ND
0.250 1
05/18/2023 00:24 WG2061580
Wet Chemistry by Method 9034-90306
Result
Qualifier
RDL Dilution
Analysis Batch
7GI
Analyte mg/kg
mg/kg
date / time
Reactive Sulfide ND
75.0 1
05/19/2023 0147 WG2062811
r, "NI
Wet Chemistry by Method 9045D
Result
Qualifier
Dilution Analysis
Batch
SC
Analyte su
date / time
Corrosivity by pH 6.33
TC
1 05/22/2023 08:37 WG2063275
Sample Narrative:
L1616826-01 WG2063275: 6.33 at20.6C
Wet Chemistry by Method D93/1010A
Result
Qualifier
Dilution Analysis
Batch
Analyte Deg. F
date / time
Ignitability DNI at170
1 05/22/2023 00:59 WG2064034
Mercury by Method 7470A
Result
Qualifier
RDL Limit
Dilution Analysis Batch
Analyte mg/I
mg/I mg/I
date/time
Mercury ND
0.0100 0.20
1 05/31/202318:13 WG2063312
Metals (ICP) by Method 6010D
Result
Qualifier RDL
Limit
Dilution Analysis
Batch
Analyte
mg/I
mg/I
mg/I
date/time
Arsenic
ND
0.100
5
1 05/23/202317:31
WG2064577
Barium
0.141
0.100
100
1 05/23/202317:31
WG2064577
Cadmium
ND
0.100
1
1 05/23/202317:31
WG2064577
Chromium
ND
0.100
5
1 05/23/202317:31
WG2064577
Lead
ND
0.100
5
1 05/23/202317:31
WG2064577
Selenium
ND
0.100
1
1 05/23/202317:31
WG2064577
Silver
ND
0.100
5
1 05/23/202317:31
WG2064577
Volatile Organic
Compounds (GC/MS) by Method
8260D
Result
Qualifier RDL
Limit
Dilution Analysis
Batch
Analyte
mg/I
mg/I
mg/I
date/time
Benzene
ND
0.0500
0.50
1 05/22/2023 03:23
WG2063681
Carbon tetrachloride
ND
0.0500
0.50
1 05/22/2023 03:23
WG2063681
Chlorobenzene
ND
0.0500
100
1 05/22/2023 03:23
WG2063681
Chloroform
ND
0.250
6
1 05/22/2023 03:23
WG2063681
1,2-Dichloroethane
ND
0.0500
0.50
1 05/22/2023 03:23
WG2063681
ACCOUNT:
PROJECT:
SDG:
DATE/TIME: PAGE:
EMA Resources
L1616326
06/01/23 08:37 5 of 22

MOCKSVILLE WTP
SAMPLE RESULTS
- 01
Collected date/time: 05/15/23 11:15
L1616826
Volatile Organic Compounds (GC/MS) by Method 8260D
Result
Qualifier RDL Limit Dilution
Analysis
Analyte
mg/I
mg/I mg/I
date/time
1,1-Dichloroethene
ND
0.0500 0.70 1
05/22/2023 03:23
2-Butanone (MEK)
ND
0.500 200 1
05/22/2023 03:23
Tetrachloroethene
ND
0.0500 0.70 1
05/22/2023 0323
Trichloroethene
ND
0.0500 0.50 1
05/22/2023 0323
Vinyl chloride
ND
0.0500 0.20 1
05/22/2023 0323
(S) Toluene-dH
95.6
80.0-120
0512212023 03.23
(S) 4-Bromofluorobenzene
101
77.0-126
0512212023 03.23
(S)1,2-Dichloroethene-d4
99.7
70.0-130
051221202303.23
Chlorinated Acid Herbicides (GC) by Method 8151A
Result
Qualifier RDL Limit
Dilution Analysis
Analyte
mg/I
mg/I mg/I
date/time
2,4,5-TP (Silvex)
ND
0.00200
1 05/24/202316:28
2,4-D
ND
0.00200
1 05/24/202316:28
(S) 2,4-Dichlorophenyl Acetic Acid
72.4
14.0-158
0512412023 16.28
Pesticides (GC) by Method 8081B
Result
Qualifier
RDL
Limit
Dilution Analysis
Analyte
mg/I
mg/I
mg/I
date/time
Chlordane
ND
0.00500
0.03
1 05/24/2023 0559
Endrin
ND
0.00500
0.02
1 05/24/2023 0559
Heptachlor
ND
0.00500
0.0080
1 05/24/2023 0559
Heptachlor epoxide
ND
0.00500
0.0080
1 05/24/2023 0559
Lindane
ND
0.00500
0.40
1 05/24/2023 0559
Methoxychlor
ND
0.00500
10
1 05/24/2023 0559
Toxaphene
ND
0.0100
0.50
1 05/24/2023 0559
(S) Decochlorobiphenyl
44.3
10.0-128
0512412023 05.59
(S) Tetrochloro-m-xylene
61.4
10.0-127
0512412023 05.59
Semi Volatile Organic Compounds
(GC/MS) by Method 8270E
Result
Qualifier
RDL
Limit
Dilution Analysis
Analyte
mg/I
mg/I
mg/I
date/time
1,4-Dichlorobenzene
ND
0.100
7.50
1 05/25/2023 02:58
2,4-Dinitrotoluene
ND
0.100
0.13
1 05/25/2023 02:58
Hexachlorobenzene
ND
0.100
0.13
1 05/25/2023 02:58
Hexachloro-1,3-butadiene
ND
0.100
0.50
1 05/25/2023 02:58
Hexachloroethane
ND
0.100
3
1 05/25/2023 02:58
Nitrobenzene
ND
0.100
2
1 05/25/2023 02:58
Pyridine
ND
J4
0.100
5
1 05/25/2023 02:58
3&4-Methyl Phenol
ND
J4
0.100
400
1 05/25/2023 02:58
2-Methylphenol
ND
J4
0.100
200
1 05/25/2023 02:58
Pentachlorophenol
ND
0.100
100
1 05/25/2023 02:58
2,4,5-Trichlorophenol
ND
0.100
400
1 05/25/2023 02:58
2,4,6-Trichlorophenol
ND
J4
0.100
2
1 05/25/2023 02:58
(S) 2-Fluorophenol
20.4
10.0-120
0512512023 02:58
(S) Phenol-d5
18.8
10.0-120
0512512023 02:58
(S) Nitrobenzene-d5
62.3
10.0-127
0512512023 02:58
(S) 2-Fluorobiphenyl
45.4
10.0-130
0512512023 02:58
(S) 2,4, 6-Tribromophenol
46.4
10.0-155
0512512023 02:58
(S) p-Terphenyl-d14
74.2
10.0-128
0512512023 02:58
Sample Narrative:
L1616826-01 WG2064734: Duplicate Analysis performed due to QC failure. Reporting mostcompliant data.
Batch
WG2063681
WG2063681
WG2063681
WG2063681
WG2063681
WG2063681
WG2063681
WG2063681
Batch
WG2064076
WG2064076
WG2064076
Batch
WG2064735
WG2064735
WG2064735
WG2064735
WG2064735
WG2064735
WG2064735
WG2064735
WG2064735
Batch
WG2064734
WG2064734
WG2064734
WG2064734
WG2064734
WG2064734
WG2064734
WG2064734
WG2064734
WG2064734
WG2064734
WG2064734
WG2064734
WG2064734
WG2064734
WG2064734
WG2064734
WG2064734
ACCOUNT: PROJECT: SDG: DATE/TIME:
EMA Resources L1616326 06/01/23 08:37
PAGE:
6 of 22

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GLOSSARY OF TERMS
Guide to Reading and Understanding Your Laboratory Report
The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not
intended as a comprehensive explanation, and ifyou have additional questions please contact your project representative.
Results Disclaimer - Information that may be provided by the customer, and contained within this report, include Permit Limits, Project Name,
Sample ID, Sample Matrix, Sample Preservation, Field Blanks, Field Spikes, Field Duplicates, On -Site Data, Sampling Collection Dates/Times, and
Sampling Location. Results relate to the accuracy of this information provided, and as the samples are received.
Abbreviations and Definitions
MDL
Method Detection Limit.
ND
Not detected at the Reporting Limit (or MDL where applicable).
RDL
Reported Detection Limit.
Rec.
Recovery.
RPD
Relative Percent Difference.
SDG
Sample Delivery Group.
Surrogate (Surrogate Standard) - Analytes added to every blank, sample, Laboratory Control Sample/Duplicate and
(S)
Matrix Spike/Duplicate; used to evaluate analytical efficiency by measuring recovery. Surrogates are not expected to be
detected in all environmental media.
U
Not detected at the Reporting Limit (or MDL where applicable).
Analyte
The name ofthe particular compound or analysis performed. Some Analyses and Methods will have multiple analytes
reported.
Ifthe sample matrix contains an interfering material, the sample preparation volume or weight values differ from the
Dilution
standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the
laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the
result reported has already been corrected for this factor.
These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal
Limits
for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or
duplicated within these ranges.
Original Sample
The non -spiked sample in the prep batch used to determine the Relative Percent Difference (RPD) from a quality control
sample. The Original Sample may not be included within the reported SDG.
This column provides a letter and/or number designation that corresponds to additional information concerning the result
Qualifier
reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and
potentially a discussion of possible implications ofthe Qualifier in the Case Narrative if applicable.
The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. Ifthere was
no measurable result returned for a specific analyte, the result in this column may state "ND" (Not Detected) or "BDL"
Result
(Below Detectable Levels). The information in the results column should always be accompanied by either an MDL
(Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect
or report for this analyte.
Uncertainty
(Radiochemistry)
Confidence level of 2 sigma.
A brief discussion about the included sample results, including a discussion of any non -conformances to protocol
Case Narrative (Cn)
observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will
be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report.
Quality Control
This section ofthe report includes the results ofthe laboratory quality control analyses required by procedure or
Summary (Qc)
analytical methods to assist in evaluating the validity ofthe results reported for your samples. These analyses are not
being performed on your samples typically, but on laboratory generated material.
This is the document created in the field when your samples were initially collected. This is used to verify the time and
Sample Chain of
date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This
Custody (Sc)
chain of custody also documents all persons (excluding commercial shippers) that have had control or possession ofthe
samples from the time of collection until delivery to the laboratory for analysis.
This section ofyour report will provide the results of all testing performed on your samples. These results are provided
Sample Results (Sr)
by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for
each sample will provide the name and method number for the analysis reported.
Sample Summary (Ss)
This section ofthe Analytical Report defines the specific analyses performed for each sample ID, including the dates and
times of preparation and/or analysis.
Qualifier
Description
J2
Surrogate recovery limits have been exceeded, values are outside lower control limits.
J3
The associated batch QC was outside the established quality control range for precision.
J4
The associated batch QC was outside the established quality control range for accuracy.
P
RPD between the primary and confirmatory analysis exceeded 40%.
T8
Sample(s) received past/too close to holding time expiration.
ACCOUNT:
PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources
L1616326 06/01/23 03:37 20 of 22

ACCREDITATIONS & LOCATIONS
!Ninl',71cl I\h ll+"inl l 12065 I cd it I+:+I""I
Alabama
40660
Nebraska
N E-OS-15-05
Alaska
17-026
Nevada
TN000032021-1
Arizona
AZ0612
New Hampshire
2975
Arkansas
88-0469
New Jersey—NELAP
TNO02
California
2932
New Mexico
TN00003
Colorado
TN00003
New York
11742
Connecticut
PH-0197
North Carolina
Env375
Florida
E87487
North Carolina'
DW21704
Georgia
NELAP
North Carolina 3
41
Georgia'
923
North Dakota
R-140
Idaho
TN00003
Ohio—VAP
CL0069
Illinois
200008
Oklahoma
9915
Indiana
C-TN-01
Oregon
TN200002
Iowa
364
Pennsylvania
68-02979
Kansas
E-10277
Rhode Island
LA000356
Kentucky' 6
KY90010
South Carolina
84004002
Kentucky 2
16
South Dakota
n/a
Louisiana
A130792
Tennessee' 4
2006
Louisiana
LA018
Texas
T104704245-20-18
Maine
TN00003
Texas5
LABO152
Maryland
324
Utah
TN000032021-11
Massachusetts
M-TNO03
Vermont
VT2006
Michigan
9958
Virginia
110033
Minnesota
047-999-395
Washington
C847
Mississippi
TN00003
West Virginia
233
Missouri
340
Wisconsin
998093910
Montana
CERT0086
Wyoming
A2 LA
A2LA— ISO 17025
1461.01
AIHA-LAP,LLC EMLAP
100789
A2 LA — ISO 17025 5
1461.02
DOD
1461.01
Canada
1461.01
USDA
P330-15-00234
EPA—Crypto
TN00003
Drinking Water 2 Underground Storage Tanks 3 Aquatic Toxicity "Chemical/Microbiological 5 Mold 6 Wastewater n/a Accreditation not applicable
Not all certifications held by the laboratory are applicable to the results reported in the attached report.
Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace Analytical.
ACCOUNT: PROJECT: SDG: DATE/TIME:
EMA Resources L1616326 06/01/23 03:37
PAGE:
21 of 22

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2`0231 Moa 'iiiddb W ...........
WQ0039552
Final Audit Report 2024-02-19
By: Brent Collins ([e-mail])
Status: Signed
Transaction ID: CBJCHBCAABAA]kanWAce3wDohuYiDahVl6HmwigHDraY
T . . . . .. . . . . Document created by Brent Collins ([e-mail])
J
2024-02-19 - 2:32:08 PM GMT- IP address: 206.85.202.26
ii Document emailed to Todd Robinson ([e-mail]) for signature
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If . . . .. . . . . 11 Email viewed by Todd Robinson (trobinson CO)enviroli n kin c.com)
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Document e-signed by Todd Robinson ([e-mail])
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