WQ0000672_2023 Residual Annual Report_20240301 (2)

Initial Review
Reviewer
nathaniel.thorn burg
Is this submittal an application? (Excluding additional information.) *
Yes No
If not an application what is the submittal type?* Annual Report
Residual Annual Report
Additional Information
Other
Annual Report Year* 2023
Permit Number (IR) * WQ0000672
Applicant/Permittee City of Lumberton
Email Notifications
Does this need review by the hydrogeologist? * Yes U No
Regional Office Fayetteville
CO Reviewer
Admin Reviewer Wanda Gerald

Submittal Form
Project Contact Information
Please provide information on the person to be contacted by NDB Staff regarding electronic submittal, confirmation of receipt, and other correspondence.
Name* Michael Hunt
Email Address*
[e-mail]
Project Information
.........................
Application/Document Type*
New (Fee Required)
Modification - Major (Fee Required)
Renewal with Major Modification (Fee
Required)
Annual Report
Additional Information
Other
Phone Number*
9107385311
Modification - Minor
Renewal
GW-59, NDMR, NDMLR, NDAR-1,
N DAR-2
Residual Annual Report
Change of Ownership
We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form.
https://edoes.deq.nc.gov/Forms/NonDischarge_Monitoring_Report
Permit Type:*
Wastewater Irrigation
High -Rate Infiltration
Other Wastewater
Reclaimed Water
Closed -Loop Recycle
Residuals
Single -Family Residence Wastewater
Other
Irrigation
Permit Number:*
WQ0000672
Has Current Existing permit number
Applicant/Permittee Address*
700 Lafayette Street, Lumberton, NC 28358
Facility Name*
City of Lumberton Class B Residuals Program
Please provide comments/notes on your current submittal below.
At this time, paper copies are no longer required. If you have any questions about what is required, please contact Nathaniel Thornburg
at [e-mail].
Please attach all information required or requested for this submittal to be reviewed here.
(Application Form, Engineering Plans, Specifications, Calculations, Etc.)
2023 Annual Report.pdf 30.58MB
Upload only 1 PDF document (less than 250 MB). Multiple documents must be combined into one PDF file unless file is larger
than upload limit.
* By checking this box, I acknowledge that I understand the application will not be accepted for pre -review until the fee (if required) has
been received by the Non -Discharge Branch. Application fees must be submitted by check or money order and made payable to the
North Carolina Department of Environmental Quality (NCDEQ). I also confirm that the uploaded document is a single PDF with all parts
of the application in correct order (as specified by the application).
Mail payment to:
NCDEQ — Division of Water Resources
Attn: Non -Discharge Branch
1617 Mail Service Center
Raleigh, NC 27699-1617
Signature
1&&IIIIe
Submission Date 3/1/2024

ENVIRO.. H ICE
W
PO Box 309
Lumberton, NC 28359
Phone: [phone]
Fax: [phone]
February 21, 2024
NC Environmental Quality-DWQ
Information Processing Unit
1617 Mail Service Center
Raleigh, NC 27699-1617
Attention: Compliance Representative
Subject: 2023 Annual Report for City of Lumberton Land Application Program
(City of Lumberton WQ0000672)
Dear Compliance Representative,
Enclosed is (1) copy of the monitoring and reporting information as requited in the referenced
permit for the City of Lumberton, North Carolina. This report was complied from land
application records provided by the City of Lumberton and Enviro-Choice Recycling. The report
includes: 1) a state required annual certification for and facility information page, 2) the 2023
annual application summary table, 3) annual residual sampling summary form and laboratory
analysis reports, 4) field loading reports, 5) pathogen and vector reduction documentation, and 6)
soil analysis reports.
Should you need more information regarding this land application program, please contact me at
910-738-5311 or envirochoicenc a,gmail.com.
A -4,J
Michael C. Hunt
Enviro-Choice Recycling
CC: Henry Harper, Wastewater ORC, City of Lumberton WWTP
Office: 910-671-3859 hharperkci.lumberton.nc.us

ANNUAL LAND APPLICATION CERTIFICATION FORM
WQ Permit#: WQ0000672 County:
Facility Name (as shown on permit):
Robeson
Year: 2023
City of Lumberton
Land Application Operator: Enviro-Choice Recycling, LLC Phone:
Land application of residuals as allowed by the permit occurred during the past calendar year?
❑2 Yes ❑ No - If No, skip Part A, and Part B and proceed to Part C. Also, If residuals were
generated but not land applied, please attach an explanation on how the residuals were handled.
Part A - Residuals Application Summary:
910-738-5311
Total number of application fields in thepermit:
1 63
Total number of fields utilized for land application during the year:
24
Total amount of dry tons applied during the year for all application sites:
1445.82
Total number of acres utilizes for land application during the year:
504.32
Part B - Annual Compiance Statement:
Facility was compliant during calendar year 2023 with all conditions of the land application permit
(including but not limited to items 1-13 below) issued by the Division of Water Resources. El Yes ❑ No
If no please, provide a written description why the facility was not compliant, the dates, and explain corrective action
taken.
1) Only residuals approved for this permit were applied to the permitted sites.
2) Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or
the limit specified in the permit.
3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies
of laboratory results are attached.
4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5) All other monitoring was performed in accordance with the permit and reported during the year as required and three (3)
copies of certified laboratory results are attached.
6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .1105(a) or the Pollutant
Loading Rates in 15A NCAC 02T .1105(b) (applicable to 40 CFR Part 503 regulated facilities).
7) All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part
503 regulated facilities).
8) All monitoring and reporting requirements in 15A NCAC 02T .1111 were complied with (applicable to 40 CFR Part
503 regulated facilities).
9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Resources.
10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
11) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as
specified in the permit.
12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13) All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C - Certification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate,
and complete. I am aware that there are significant penalties for submitting false information, including the
possibility of fines and imprisonment for knowing violations."
Henry Harper WWTP/ORC
Permii/ttt�e�� e Name and Title (type or print)
D"U�^u�' 1-u 2/21/2024
Signatu o Permittee Date
Signature of Prep6er* Date Signature of Land Applier Date
(if different from Permittee) (if different from Permittee and Preparer)
* Preparer is defined in 40 CFR Part 503.9 (r) and 15A NCAC 02T .1102 (26) DENR FORM ACF (12/2006)

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B
WQ Permit Number: WQ0000672
Facility Name:
Residual Source WQ # or
NPDES #:
City of Lumberton
WQ0000672
WWTP Name: City of Lumberton
Residual Analysis Data
Laboratory: 1) Eurofins
2) Cameron Analytical
3)
4)
5)
Parameter
(mg/kg)
Conc.
Limit
m /k a
Sample or Composite Date
3/28/23
6/2/23
9/22/23
12/7/202
3
Percent Solids (%)
NA
2.9
2.6
1.6
1.9
Arsenic
75
35
46
69
55
Cadmium
85
3
3.8
5.8
4.6
Copper
4,300
15
440
310
360
Chromium
NA
0.06
0.06
220
190
Lead
840
18
23
35
28
Mercury
57
0.22
0.31
0.5
0.41
Molybdenum
75
7.7
9.9
15
12
Nickel
420
29
34
52
42
Selenium
100
32
42
63
51
Zinc
7,500
590
720
780
750
Total Phosphorus
NA
16000
15000
15000
11000
TKN
NA
55000
68000
63000
120000
Ammonia -Nitrogen
NA
2600
150
600
180
Nitrate and Nitrite
NA
2300
820
920
200
a For surface disposal facilities the ceiling concentration limits listed in this form are not applicable. Reference the individual permit for metals limits.
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant
penalties for submitting falser information, including the possibility of fines and imprisonment for knowing violations."
un� 2/20/2024
Signature of Preparer *
Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM RSSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
City of Lumberton Total Dry Tons Applied (Annual):
WQ000672 Cation Exchange Capacity (non 503 only):
Ozzell Baker Owner: Ozzell Baker Predominant Soil Series:
8.7 Acres Permitted: 8.7 Site #: NC-RO-16 Field #
22.85
NoA- Norfolk
5
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample or
Com-
posite
Date
11
3/28/23
21
6/2/23
3
9/22/23
4
12/7/23
5
6
7
8
9
10
11
12
% Solids
2.9
2.6
1.6
1 1.9
Arsenic
35
46
69
55
Cadmium
3
3.8
5.8
4.6
Copper
15
440
310
360
Chronuum
0.06
0.06
220
190
Lead
18
23
35
28
Mercury
0.22
0.31
0.5
0.41
Molyb-
denum
7.7
9.9
15
12
Nickel
29
34
52
42
Selenium
32
42
63
51
Zinc
590
720
780
750
Total
Phos-
horus 1
16000
1 15000
15000
11000
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
D
Event
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
�
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
� �
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
�
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
®
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
Total
Phos-
1 111
:: 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
:: 1
phorus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Signature of Land Applie
2/20/2024
Date
DENR FORM MFLSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
Facility Name: City of Lumberton
Land Owner: Ozzell Baker
Operator: Ozzell Baker
Crop 1 Name: Bermuda
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
WQ Permit #: WQ0000672 Field #: NC-RO-16-05
Annual Dry Tons Applied: 22.8549 Site #: 5
. Ra-Rains Sandy
Crop 1 Max. PAN: 113.25 Crop 2 Name:
Acres Utilized: 8.7
Acres Permitted: 8.7
Cation Exchange Capacity (non 503):
Crop 2 Max. PAN:
o
Q
Volume applied
(enter one) Solids/
Liquid
Cu. Yds Gallons
oho
Solids
1 2.6
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
Soil
Cond.
(Diy,
Wet
Moist)
Precip.
past 24
Hrs.
inches
a
� ��
+ o
o
?
� �
* w
F
��,
F*, �
*
�*.
1'KN
mg/kg
68000
Z�
0 �
= o
�.
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
(lbs/acre)
Name of Crop Type
Receivin Residual
g
Application
Crop 1
Crop 2
Crop 1
Crop 2
4/4
1
37200
0.464
WQ0000672
Dry
1 0
S
0.5
0.3
150
820
19.703
NA
Ber
4/5
111600
2.6
1.391
WQ0000672
Dry
0
S
0.5
0.3
68000
150
820
59.108
NA
Ber
4/6
62000
2.6
0.773
WQ0000672
Dry
0
S
0.5
0.3
68000
150
820
32.838
NA
Ber
0
0
20000
Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form):
0.000
0.000
TOTALS: --017 210800
Annuallbs/acre 42000
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn
P
111.648
0.000
Lime A lied
0.000
0.000
0.000
0.121
0.000
0.000
0.000
0.000
0.000
78.810
Date
lbs/ac
Prior Years Cumulative lbs/ac 4400
Current Cumulative lbs/ac ND
0.000
0.000
0.000
0.121
0.000
0.000
0.000
0.000
0.000
Permitted C. P. L. R.****
Permit PAN Limit 1 st/2nd Crop
113.25
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
informati n, including the possibility of 'nes and imprisonment for knowing violations."
_ *Application Method: S - Surface, IN - Injection, INC - Incorporation
2/20/2024 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of LafQ Applier Date * * * Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
City of Lumberton Total Dry Tons Applied (Annual):
WQ000672 Cation Exchange Capacity (non 503 only):
Ozzell Baker Owner: Ozzell Baker Predominant Soil Series:
14.8 Acres Permitted: 14.8 Site #: NC-RO-16 Field #
49.40
NoA- Norfolk
6
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample or
Com-
posite
Date
1
3/28/23
2
6/2/23
3
9/22/23
4
12/7/23
5
6
7
8
9
10
11
12
% Solids
2.9
2.6
1.6
1 1.9
Arsenic
35
46
69
55
Cadmium
3
3.8
5.8
4.6
Copper
15
440
310
360
Chronuum
0.06
0.06
220
190
Lead
18
23
35
28
Mercury
0.22
0.31
0.5
0.41
Molyb-
denum
7.7
9.9
15
12
Nickel
29
34
52
42
Selenium
32
42
63
51
Zinc
590
720
780
750
Total
Phos-
horus 1
16000
1 15000
15000
11000
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
D
Event
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
�
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
� �
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
�
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
®
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
Total
Phos-
1 111
11 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
11 1
phorus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
impriso ment for knowing violations".
&a &4
UA 2/20/2024
Signature of Land Applier 0 Date
DENR FORM MFLSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
Facility Name: City of Lumberton
Land Owner: Ozzell Baker
Operator: Ozzell Baker
Crop 1 Name: Bermuda
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
WQ Permit #: WQ0000672 Field #: NC-RO-16-06
Annual Dry Tons Applied: 49.3962 Site #: 6
Crop 1 Max. PAN:
NoA- Norfolk
172.5
Crop 2 Name:
Acres Utilized: 14.8
Acres Permitted: 14.8
Cation Exchange Capacity (non 503):
Crop 2 Max. PAN:
0 p
A
Volume applied
(enter one) Solids/
Liquid
Cu. Yds Gallons
%
Solids
2.6
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
Soil
Cond.
(Dry,
Wet
Moist)
Precip.
past 24
Firs.
inches
a
F �
� o
0 w
o
N
0
w `I
=
N
� 0
TKN
mg/kg
68000
Z a
o
qQ 0
�
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
(lbs/acre)
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Crop 1
Crop 2
4/6
77400
0.567
WQ0000672
Dry
0
S
0.5
0.3
150
820
24.098
NA
Ber
4/7
37200
2.6
0.273
WQ0000672
Dry
0
S
0.5
0.3
68000
150
820
11.582
NA
Ber
4/11
130200
2.6
0.954
WQ0000672
Dry
0
S
0.5
0.3
68000
150
820
40.537
NA
Ber
4/12
86800
2.6
0.636
WQ0000672
Dry
0
S
0.5
0.3
68000
150
820
27.024
NA
Ber
4/13
124000
2.6
0.908
WQ0000672
Dry
0
S
0.5
0.3
68000
150
820
38.606
NA
Ber
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1 0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0
0
0.000
Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form):
0.000
1 0.000
TOTALS:
01
4556001
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn
P
141.8471
0.000
Lime Applied
Annuallbs/acre
0.000
0.000
0.000
0.000
0.154
0.000
0.000
0.000
0.000
0.000
100.140
Date
lbs/ac
Prior Years Cumulative lbs/ac
Current Cumulative lbs/ac
0.000
0.000
0.000
0.000
0.154
0.000
0.000
0.000
0.000
0.000
Permitted C. P. L. R.****
Permit PAN Limit 1 st/2nd Crop
F172.5T
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information includi g the ossibility of fines nd imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
2/20/2024 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land
Date
*** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
The City of Lumberton Total Dry Tons Applied (Annual):
WQ0000672 Cation Exchange Capacity (non 503 only):
Owner:
17.5 Acres Permitted:
17.5 Site #:
Predominant Soil Series:
Field #
44.36
NoA-Norfolk
NC-RO-16-07
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample or
Com-
posite
Date
1
3/28/23
2
6/2/23
3
9/22/23
4
12/7/23
5
6
7
8
9
10
11
12
% Solids
2.9
2.6
1.6
1 1.9
Arsenic
35
46
69
55
Cadmium
3
3.8
5.8
4.6
Copper
15
440
310
360
Chronuum
0.06
0.06
220
190
Lead
18
23
35
28
Mercury
0.22
0.31
0.5
0.41
Molyb-
denum
7.7
9.9
15
12
Nickel
29
34
52
42
Selenium
32
42
63
51
Zinc
590
720
780
750
Total
Phos-
horus 1
16000
1 15000
15000
11000
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
D
Event
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
�
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
� �
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
�
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
®
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
Total
Phos-
phorus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
impris nment f • kno ing violatio s".
2/20/2024
Signature of Land Applier Date
DENR FORM MFLSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
Facility Name: City of Lumberton
Land Owner: Ozzell Baker
Operator: Ozzell Baker
Crop 1 Name: Bermuda
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
WQ Permit #: WQ0000672 Field #: NC-RO-16-07
Annual Dry Tons Applied: 44.3655 Site #: 7
Predominant Soil Series: NoA-Norfolk
Crop 1 Max. PAN:
172.5
Crop 2 Name:
Acres Utilized: 17.5
Acres Permitted: 17.5
Cation Exchange Capacity (non 503):
Crop 2 Max. PAN:
0 o
A
Volume applied
(enter one) Solids/
Liquid
Cu. Yds Gallons
%
Solids
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
(NpDES #, WQ#,
Fert., Animal
Waste, etc)
Soil
Cond.
(Dry,
Wet
Moist)
Precip.
past 24
Firs.
inches
a
F �
�
0 w
o
N
0
w `I
N
� 0
TKN
mg/kg
68000
Z a
o
qQ 0
�
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
(lbs/acre)
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Crop 1
Crop 2
4/20
93000
2.6
0.576
WQ0000672
Dry
0
S
0.5
0.3
150
820
24.487
24.487
4/21
105400
2.6
0.653
WQ0000672
Dry
0
S
0.5
0.3
68000
150
820
27.752
27.752
4/25
130200
2.6
0.807
WQ0000672
Dry
0
S
0.5
0.3
68000
150
820
34.282
34.282
5/3
62000
2.6
0.384
WQ0000672
Dry
0
S
0.5
0.3
68000
150
820
16.325
16.325
5A
18600
2.6
0.115
WQ0000672
Dry
0
S
0.5
0.3
68000
150
820
4.897
4.897
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1 0.000
0.000
1
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0
0
0.000
Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form):
0.000
0.000
TOTALS:
01
409200
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn
P
107.745
107.745
Lime Applied
Annuallbs/acre
0.000
0.000
0.000
0.000
0.117
0.000
0.000
0.000
0.000
0.000
76.050
Date
lbs/ac
Prior Years Cumulative lbs/ac
2.26
Current Cumulative lbs/ac
2.260
0.000
0.000
0.000
0.117
0.000
0.000
0.000
0.000
0.000
Permitted C. P. L. R.****
Permit PAN Limit 1 st/2nd Crop
172.5
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
informat on, incl ing t possibility o fines nd imprisonment for knowing violations."
- 2/20/2024 *Application Method: S - Surface, IN - Injection, INC - Incorporation
**Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land
Date
*** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
City of Lumberton Total Dry Tons Applied (Annual):
WQ0000672 Cation Exchange Capacity (non 503 only):
Ozzell Baker
Owner: James Campen Predominant Soil Series:
Acres Permitted: 5 Site #: 16 Field #:
13.24
WaB-Wagram
NC-RO-16-16
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample or
Com-
posite
Date
1
3/28/23
2
6/2/23
3
9/22/23
4
12/7/23
5
6
7
8
9
10J
11
12
% Solids
2.9
2.6
1.6
1 1.9
Arsenic
35
46
69
55
Cadmium
3
3.8
5.8
4.6
Copper
15
440
310
360
Chronuum
0.06
0.06
220
190
Lead
18
23
35
28
Mercury
0.22
0.31
0.5
0.41
Molyb-
denum
7.7
9.9
15
12
Nickel
29
34
52
42
Selenium
32
42
63
51
Zinc
590
720
780
750
Total
Phos-
horus 1
16000
1 15000
15000
11000
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
D
Event
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
�
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
�
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
• •
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
•
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
®
1 111
1 111
�
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
Total
Phos-
phorus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Signature of Land Applier
2/20/2024
Date
DENR FORM MFLSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
Facility Name: City of Lumberton
Land Owner: James Campen
Operator: Ozzell Baker
Crop 1 Name: Bermuda
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
WQ Permit #: WQ0000672 Field #: NGRO-16-16
Annual Dry Tons Applied: 13.2372 Site #: 16
Predominant Soil Series: WaB-Wagram
Crop 1 Max. PAN: 192 Crop 2 Name:
Acres Utilized: 5
Acres Permitted: 5
Cation Exchange Capacity (non 503):
Crop 2 Max. PAN:
0 p
A
Volume applied
(enter one) Solids/
Liquid
Cu. Yds Gallons
%
Solids
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
Soil
Cond.
(Dry,
Wet
Moist)
Precip.
past 24
Hrs.
inches
a
� o
0 w
o.
o
N
0
w `1
=
0
TKN
mg/kg
63000
Z a
o �
D °�
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
( lbs/acre)
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Crop 1
Crop 2
9/6
148800
1.6
1.986
WQ0000672
Dry
0
S
0.5
0.3
600
920
79.185
NA
Bermuda
9/7
49600
1.6
0.662
WQ0000672
Dry
0
S
0.5
0.3
63000
600
920
26.395
NA
Bermuda
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0
0
0.000
Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form):
0.000
0.000
TOTALS:
01
198400
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn P
105.5801
0.000
Lime Applied
Annuallbs/acre
0.000
0.000
1.641
1.165
0.185
0.000
0.000
0.000
0.000
4.129 79.410
Date
lbs/ac
Prior Years Cumulative lbs/ac
0.278
0.127
39.385
3.861
0.044
3.283
0.25
32.459
36.588
1 2498
Current Cumulative lbs/ac
0.278
0.127
41.026
1.165
4.046
0.044
0.000
3.283
0.250
Permitted C. P. L. R.****
1 36
1 34
1338
1
1 267
1 15
1
1 374
1 89
Permit PAN Limit 1 st/2nd Crop
1
1 192
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
2/20/2024 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
City of Lumberton Total Dry Tons Applied (Annual):
WQ0000672 Cation Exchange Capacity (non 503 only):
Ozzell Baker
Owner: James Campen Predominant Soil Series:
Acres Permitted: 6 Site #: 17 Field #:
14.89
WaB-Wagram
NC-RO-16-17
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample or
Com-
posite
Date
11
3/28/23
21
6/2/23
3
9/22/23
4
12/7/23
5
6
7
8
9
10
11
12
% Solids
2.9
2.6
1.6
1 1.9
Arsenic
35
46
69
55
Cadmium
3
3.8
5.8
4.6
Copper
15
440
310
360
Chronuum
0.06
0.06
220
190
Lead
18
23
35
28
Mercury
0.22
0.31
0.5
0.41
Molyb-
denum
7.7
9.9
15
12
Nickel
29
34
52
42
Selenium
32
42
63
51
Zinc
590
720
780
750
Total
Phos-
horus 1
16000
1 15000
15000
11000
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
D
Event
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
�
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
rom
1 111
1 111
1•
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1•
1 111
1 111
�
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
• •
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
•
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
®
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
Total
Phos-
phorus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
A 41
Signature of Land Applier
2/20/2024
Date
DENR FORM MFLSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: City of Lumberton
Land Owner: James Campen
Operator: Ozzell Baker
Crop 1 Name:
Bermuda
WQ Permit #: WQ0000672 Field #: NC-RO-16-17
Annual Dry Tons Applied: 14.8919 Site #: 17
Predominant Soil Series: WaB-Wagram
Crop 1 Max. PAN: 192 Crop 2 Name:
Acres Utilized: 6
Acres Permitted: 6.0
Cation Exchange Capacity (non 503):
Crop 2 Max. PAN:
p
Volume applied
(enter one) Solids/
Liquid
Cu. Yds Gallons
%
Solids
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
(NpDES #, WQ#,
Fert., Animal
Waste, etc)
Soil
Cond.
(Dry,
Wet
Moist)
precip.
past 24
Firs.
inches
�
n ''2
5 o'
0 w
o
:
0 '
`;
=.
TKN
mg/kg
Z
o
� 0
�.
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied ( lbs/acre)
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Crop 1
Crop 2
9/7
111600
1.6
1.241
WQ0000672
Dry
0
S
0.5
1 0.3
63000
600
920
49.491
NA
Bermuda
9/8
111600
1.6
1.241
WQ0000672
Dry
0
S
0.5
0.3
63000
600
920
49.491
NA
Bermuda
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1 0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0
0
0.000
Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form):
0.000
0.000
TOTALS:
01
223200
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn
P
98.982
0.000
Lime Applied
Annuallbs/acre
0.000
0.000
1.539
1.092
0.174
0.000
0.000
0.000
0.000
3.872
74.460
Date
lbs/ac
Prior Years Cumulative lbs/ac
0.196
0.118
37.845
3.94
0.169
0.751
3.02
0.16
32.775
Current Cumulative lbs/ac
0.196
0.118
39.384
1.092
4.114
0.169
0.751
3.020
0.160
36.647
Permitted C. P. L. R.****
36
34
1338
1
267
15
1 N/A
1 374
89
1 2498
Permit PAN Limit 1 st/2nd Crop
1
1 192
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified
personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the
possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation /L a 2/20/2024 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature oan f Ld ° -1;-,- D *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3,
Me raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
City of Lumberton Total Dry Tons Applied (Annual):
WQ0000672 Cation Exchange Capacity (non 503 only):
Ozzell Baker
Owner: James Campen Predominant Soil Series:
12.3 Acres Permitted: 12.3 Site #: 18 Field #:
28.95
WaB-Wagram
NC-RO-16-18
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample or
Com-
posite
Date
1
3/28/23
2
6/2/23
3
9/22/23
4
12/7/23
5
6
7
8
9
10J
11
12
% Solids
2.9
2.6
1.6
1 1.9
Arsenic
35
46
69
55
Cadmium
3
3.8
5.8
4.6
Copper
15
440
310
360
Chronuum
0.06
0.06
220
190
Lead
18
23
35
28
Mercury
0.22
0.31
0.5
0.41
Molyb-
denum
7.7
9.9
15
12
Nickel
29
34
52
42
Selenium
32
42
63
51
Zinc
590
720
780
750
Total
Phos-
horus 1
16000
1 15000
15000
11000
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
D
Event
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
�
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1•
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1•
1 111
1 111
1•
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1•
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
� �
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
�
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
®
1 111
1 111
�
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
Total
Phos-
phorus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
A,��j cj�c 4A
Signature of Land Applier
2/20/2024
Date
DENR FORM MFLSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
Facility Name: City of Lumberton
Land Owner: James Campen
Operator: Ozzell Baker
Crop 1 Name: Bermuda
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
WQ Permit #: WQ0000672 Field #: NC-RO-16-18 Acres Utilized: 12.3
Annual Dry Tons Applied: 28.9565 Site #: 18 Acres Permitted: 12.3
Predominant Soil Series: WaB-Wagram
Crop 1 Max. PAN: 192 Crop 2 Name:
Cation Exchange Capacity (non 503):
Crop 2 Max. PAN:
p =
r
Volume applied
(enter one) Solids/
Liquid
Cu. Yds Gallons
oho
Solids
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert, Animal
Waste, etc)
Soil
Cond.
Moist)
Precip.
Past 24
Hrs.
inches
y
? �
� S
�:
a a
* °�
o
c.
o'
7�
w
N'
o
8
TKN
mg/kg
Z
9.
o
M o
mgtkg
Nitrate
and
Nitrite
mg/kg
PAN Applied
(lbs/acre)
Name of Crop Type
Receiving Residual
Application
Crop 1
FCrop 2
Crop 1
Crop 2
9/11/23
148800
1.6
0.807
W00000672
Dry
0
S
0.5
0.3
63000
600
920
32.189
NA
Bermuda
9/12/23
161200
1.6
1 0.874
W00000672
Dry
1 0
S
0.5
0.3
1 63000
600
1 920
34.872
NA
Bermuda
9/13/23
124000
1.6
0.673
W00000672
Dry
0
S
0.5
0.3
63000
600
920
26.824
NA
Bermuda
0.000
0.000
NA
Bermuda
0.000
0.000
NA
Bermuda
0.000
0.000
NA
Bermuda
0.000
0.000
NA
Bermuda
0.000
0.000
NA
Bermuda
0.000
0.000
NA
Bermuda
0.000
0.000
NA
Bermuda
0.000
0.000
NA
Bermuda
0.000
0.000
NA
Bermuda
0
0
0.000
Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form):
0.000
0.000
TOTALS:
01
434000
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn
I P
93.885
o.000
Lime Aliplied
Annuallbs/acre
0.000
0.000
1.459
1.036
0.165
0.000
0.000
0.000
0.000
3.672
70.620
Date
lbs/ac
Prior Years Cumulative lbs/ac
0.282
0.127
44.95
4.36
0.047
0.777
3.11
0.257
41.931
Current Cumulative lbs/ac
0.282
0.127
46.409
1.036
4.525
0.047
0.777
3.110
0.257
45.603
Permitted C. P. L. R.****
36
34
1338
267
15
N/A
374
89
2498
Permit PAN Limit 1st/2nd Crop
192
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of tines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
2/20/2024 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier Date Mineralization Rates: Compost -0. 1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
* * * * C.P.L.R: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: City of Lumberton Total Dry Tons Applied (Annual): 130.89
Permit #: WQ0000672 Cation Exchange Capacity (non 503 only):
Operator: Delois Allen Owner: City of Lumberton Predominant Soil Series: Jo -Johns Sandy
Acres Used: 36.4 Acres Permitted: 36.4 Site #: 1 Field #: NC-RO-17-01
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample or
Com-
posite
Date
1
3/28/23
2
6/2/23
3
9/22/23
4
12/7/23
5
6
7
8
9
10
11
12
% Solids
2.9
2.6
1.6
1 1.9
Arsenic
35
46
69
55
Cadmium
3
3.8
5.8
4.6
Copper
15
440
310
360
Chromium
0.06
0.06
220
190
Lead
18
23
35
28
Mercury
0.22
0.31
0.5
0.41
Molyb-
denum
7.7
9.9
15
12
Nickel
29
34
52
42
Selenium
32
42
63
51
Zinc
590
720
780
750
Total
Phos-
horns
16000
15000
15000
11000
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
11
21
3
4
5
6
7
9
10
11
12
DT/Ac./
-81
App.
Event
2.61
0.27
0.72
Arsenic
1 0.000
0.240
0.038
0.079
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.356
Cadmium
0.000
0.020
0.003
0.007
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.030
Copper
0.000
2.295
0.169
0.515
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
2.979
Chromium
0.000
0.000
0.120
0.272
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.392
Lead
0.000
0.120
0.019
0.040
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.179
Mercury
0.000
0.002
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.002
Molyb-
0.000
0.052
0.008
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.060
denum
Nickel
0.000
0.177
0.028
0.060
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.266
Selenium
0.000
0.219
0.034
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.253
Zinc
0.000
3.756
0.426
1.073
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
5.254
Total
Phos-
0.000
78.240
8.190
15.730
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
102.160
horns
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with
a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am
aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
PLki 4j
Signature of Land Applier
2/20/2024
Date
DENR FORM MFLSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: City of Lumberton WQ Permit #: WQ0000672 Field #: NC-RO-17-01 Acres Utilized: 36.4
Land Owner: City of Lumberton Annual Dry Tons Applied: 130.8988 Site #: I Acres Permitted: 36.4
Operator: Delois Allen Predominant Soil Series: Jo -Johns Sandy Cation Exchange Capacity (non 503):
Crop 1 Name: Soybeans Crop 1 Max. PAN: 174 Crop 2 Name: Wheat Crop 2 Max. PAN: 106
0 p
A
Volume applied
(enter one) Solids/
Liquid
Cu. Yds Gallons
%
Solids
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
Soil
Cond.
(Dry,
Wet
Moist)
Precip.
past 24
Hrs.
inches
a
� -
� o
0 w
o.
o
i
F -
N
°�
w `;
F =
TKN
mg/kg
68000
Z a
o
°�
�
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
( lbs/acre)
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Crop 1
Crop 2
6/14/23
86800
2.6
0.259
WQ0000672
Dry
0
S
0.5
1 0.3
1 150
1 820
10.988
NA
Soy
6/15/23
124000
2.6
0.369
WQ0000672
Dry
0
S
0.5
0.3
68000
150
820
15.697
NA
Soy
6/16/23
93000
1.6
0.170
WQ0000672
Dry
0
S
0.5
0.3
68000
150
820
7.245
NA
Soy
6/17/23
49600
2.6
0.148
WQ0000672
Dry
0
S
0.5
0.3
68000
150
820
6.279
NA
Soy
6/19/23
105400
2.6
0.314
WQ0000672
Dry
0
S
0.5
0.3
68000
150
820
13.343
NA
Soy
6/27/23
24800
2.6
0.074
WQ0000672
Dry
0
S
1 0.5
0.3
68000
150
820
3.139
NA
Soy
6/28/23
124000
2.6
0.369
WQ0000672
Dry
0
S
0.5
0.3
68000
150
820
15.697
NA
Soy
6/29/23
136400
2.6
0.406
WQ0000672
Dry
0
S
0.5
0.3
68000
150
820
1 17.267
NA
Soy
6/30/23
167400
2.6
0.499
WQ0000672
Dry
0
S
0.5
0.3
68000
150
820
21.191
NA
Soy
7/3/23
1
148800
1.6
0.273
WQ0000672
Dry
0
S
0.5
1 0.3
1 63000
600
920
10.877
NA
Soy
11/13/23
161200
1.9
0.351
WQ0000672
Dry
0
S
0.5
1 0.3
1 120000
180
200
Na
25.429
Wheat
11/15/23
161200
1.9
0.351
WQ0000672
Dry
0
S
1 0.5
1 0.3
1 1200001
180
200
Na
25.429
Wheat
0
6202.608
0.013
Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp
to this form):
0.000
0.978
TOTALS:
01
1388802.61
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn
P
121.7231
51.835
Lime Applied
Annuallbs/acre
0.356
0.030
2.979
0.392
0.179
0.002
0.060
0.266
0.253
5.254
102.160
Date
lbs/ac
Prior Years Cum12.608
0.09
0.04
11.175
1.87
0.02
0.624
1.052
0.0178
8.745
1/22
0.64
Current Cumulative lbs/ac
0.446
0.070
14.154
0.392
2.049
0.022
0.684
1.318
0.271
13.999
Permitted C. P. L. R.****
36
34
1 1338
267
1 15
1 N/A
1 374
89
2498
Permit PAN Limit 1 st/2nd Crop
1 174 1 106
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
4J *Application Method: S - Surface, IN - Injection, INC - Incorporation
2/20/2024 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
Supplemental Information
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: City of Lumberton
Land Owner: City of Lumberton
Operator: Delois Allen
Crop 1 Name:
Soybeans
WQ Permit #: W00000672
Annual Dry Tons Applied: 130.898802
Predominant Soil Series: Jo -Johns Sandy
Crop 1 Max. PAN:
174.00
Field #: NC-RO-17-01 Acres Utilized: 36.4
Site #: 1 Acres Permitted: 36.4
Crop 2 Name:
Cation Exchange Capacity (non 503):
Wheat Crop 2 Max PAN:
106
o
+, o
Volume applied (enter
one )
Cu. Yds Gallons
Solids
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES 4, WQ4,
Fert., Animal
Waste, etc)
Soil
Cond.
D
�et�
Moist)
Preci p
Past 24
Hrs.
inches
y
co
�
0 w
oCD
o
Fd
N
w
o
TKN
mg/kg
120000
Z
o
�.
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
(lbs/acre)
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Crop 1
Crop 2
11/29/23
6200
1.9
0.013
WQ0000672
Dry
0
S
0.5
0.3
180
200
Na
0.978
Wheat
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
TOTALS:
0
6202.608
0.013
0.000
0.978
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
Signature of Lan&Applier
2/20/2024
Date
*Application Method: S - Surface, IN - Injection, INC - Incorporation
**Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
***C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (SUPP) (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: City of Lumberton Total Dry Tons Applied (Annual): 55.12
Permit #: WQ0000672 Cation Exchange Capacity (non 503 only):
Operator: Delois Allen Owner: City of Lumberton Predominant Soil Series: Lu-Lumbee
Acres Used: 25.4 Acres Permitted: 25.4 Site #: 2 Field #: NC-RO-17-02
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample or
Com-
posite
Date
1
3/28/23
2
6/2/23
3
9/22/23
4
12/7/23
5
6
7
8
9
10
11
12
% Solids
2.9
2.6
1.6
1 1.8
Arsenic
35
46
69
55
Cadmium
3
3.8
5.8
4.6
Copper
15
440
310
360
Chromium
0.06
0.06
220
190
Lead
18
23
35
28
Mercury
0.22
0.31
0.5
0.41
Molyb-
denum
7.7
9.9
15
12
Nickel
29
34
52
42
Selenium
32
42
63
51
Zinc
590
720
780
750
Total
Phos-
horns
16000
15000
15000
11000
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Totalnow
D
Emma
NUMEN00010
Event
1 111
1 11
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 11
1 111
1 1 •
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1 •
1 111
• 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
• 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 11
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 11
1 111
1 11
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 11
•
1 111
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
••
1 111
1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1
1 111
1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1
®
1 111
®
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
Total
Phos-
phorus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Signature of Land Applier
2/20/2024
Date
DENR FORM MFLSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
Facility Name: City of Lumberton
Land Owner: City of Lumberton
Operator: Delois Allen
Crop 1 Name: Soybeans
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
WQ Permit #: WQ0000672 Field #: NC-RO-17-02
Annual Dry Tons Applied: 55.1207 Site #: 2
Predominant Soil Series: Lu-Lumbee
Crop 1 Max. PAN:
174
Crop 2 Name:
Acres Utilized: 25.4
Acres Permitted: 25.4
Cation Exchange Capacity (non 503):
Crop 2 Max. PAN:
0 p
A
Volume applied
(enter one) Solids/
Liquid
Cu. Yds Gallons
%
Solids
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
Soil
Cond.
(Dry,
Wet
Moist)
Precip.
past 24
Hrs.
inches
a
S
� o
0 w
o.
o
N
0
w `;
=
TKN
mg/kg
68000
Z a
o
qQ 0
�
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
(lbs/acre)
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Crop 1
Crop 2
6/7
80600
2.6
0.344
WQ0000672
Dry
0
S
0.5
0.3
150
820
14.622
NA
Soy
6/8
167400
2.6
0.715
WQ0000672
Dry
0
S
0.5
0.3
68000
150
820
30.368
NA
Soy
6/9
74400
2.6
0.318
WQ0000672
Dry
0
S
0.5
0.3
68000
150
820
13.497
NA
Soy
6/10
49600
2.6
0.212
WQ0000672
Dry
0
S
0.5
0.3
68000
150
820
8.998
NA
Soy
6/11
37200
2.6
0.159
WQ0000672
Dry
0
S
0.5
0.3
68000
150
820
6.749
NA
Soy
6/13
99200
2.6
0.423
WQ0000672
Dry
0
S
1 0.5
0.3
68000
150
820
17.996
NA
Soy
0.000
0.000
0.000
0.000
0.000
1 0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0
0
0.000
Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form):
0.000
0.000
TOTALS:
01
508400
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn P
92.230
0.000
Lime Applied
Annuallbs/acre
0.200
0.016
1.910
0.000
0.100
0.001
0.043
0.148
0.182
3.125 65.100
Date
lbs/ac
Prior Years Cumulative lbs/ac
0.16
0.087
20.128
1.667
0.035
0.419
1.969
0.193
20.616
23.741
1 2498
1/22
0.64
Current Cumulative lbs/ac
0.360
0.103
22.038
0.000
1.767
0.036
0.462
2.117
0.375
Permitted C. P. L. R.****
36
34
1338
267
15
N/A
374
1 89
Permit PAN Limit 1 st/2nd Crop
1 174
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
(� *Application Method: S - Surface, IN - Injection, INC - Incorporation
2/20/2024 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: City of Lumberton Total Dry Tons Applied (Annual): 148.29
Permit #: WQ0000672 Cation Exchange Capacity (non 503 only):
Operator: Delois Allen Owner: City of Lumberton Predominant Soil Series: Lu-Lumbee
Acres Used: 28 Acres Permitted: 28 Site #: 3 Field #: NC-RO-17-03
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample or
Com-
posite
Date
11
3/28/23
21
6/2/23
3
9/22/23
4
12/7/23
5
6
7
8
9
10
11
12
% Solids
2.9
2.6
1.6
1 1.8
Arsenic
35
46
69
55
Cadmium
3
3.8
5.8
4.6
Copper
15
440
310
360
Chronuum
0.06
0.06
220
190
Lead
18
23
35
28
Mercury
0.22
0.31
0.5
0.41
Molyb-
denum
7.7
9.9
15
12
Nickel
29
34
52
42
Selenium
32
42
63
51
Zinc
590
720
780
750
Total
Phos-
horus 1
16000
1 15000
15000
11000
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
D
-
Event
1
•
1 111
�
1 111
1 •
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
1 111
1 1
1 111
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
1 111
�
1 111
1 •1•
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 :1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 :1
1 111
1:•
1 111
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 •
1 111
1 11
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 11
� �
1 111
1 1:1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1:1
�
1 111
�
1 111
1 1•
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 :1
1 111
1 •
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 •
®
1 111
:1:
1 111
:•
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
Total
Phos-
phorus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
&tJ
Signature of Land Applier
2/20/2024
Date
DENR FORM MFLSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: City of Lumberton WQ Permit #: WQ0000672 Field #: NC-RO-17-03 Acres Utilized: 28
Land Owner: City of Lumberton Annual Dry Tons Applied: 148.2985 Site #: 3 Acres Permitted: 28
Operator: Delois Allen Predominant Soil Series: Lu-Lumbee Cation Exchange Capacity (non 503):
Crop 1 Name: Soybeans Crop 1 Max. PAN: 174 Crop 2 Name: Wheat Crop 2 Max. PAN: 96
0 p
A
Volume applied
(enter one) Solids/
Liquid
Cu. Yds Gallons
%
Solids
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
Soil
Cond.
(Dry,
Wet
Moist)
Precip.
past 24
Hrs.
inches
a
� -
� o
0 w
o.
o
i
F -
N
°�
w `;
F =
TKN
mg/kg
68000
Z a
o
°�
�
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
( lbs/acre)
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Crop 1
Crop 2
4/12/23
173600
2.6
0.672
WQ0000672
Dry
0
S
0.5
1 0.3
1 150
1 820
28.569
NA
Soybeans
4/13/23
179800
2.6
0.696
WQ0000672
Dry
0
S
0.5
0.3
68000
150
820
29.589
NA
Soybeans
4/14/23
192200
2.6
0.744
WQ0000672
Dry
0
S
0.5
0.3
68000
150
820
31.630
NA
Soybeans
4/19/23
99200
2.6
0.384
WQ0000672
Dry
0
S
0.5
0.3
68000
150
820
16.325
NA
ISoybeans
4/20/23
241800
2.6
0.936
WQ0000672
Dry
0
S
0.5
0.3
68000
150
820
39.792
NA
Soybeans
4/21/23
155000
2.6
0.600
WQ0000672
Dry
0
S
1 0.5
0.3
68000
150
820
25.508
NA
Soybeans
10/25/23
93000
1.9
0.263
WQ0000672
Dry
0
S
0.5
0.3
120000
180
200
Na
19.071
Wheat
10/27/23
260400
1.9
0.737
WQ0000672
Dry
0
S
0.5
0.3
120000
180
200
Na
53.400
Wheat
12/4/23
93000
1.9
0.263
WQ0000672
Dry
0
S
0.5
0.3
120000
180
200
Na
19.071
Wheat
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0
0
0.000
Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp
to this form):
0.000
0.000
TOTALS:
01
1488000
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn
P
171,412
F91.543
Lime Applied
Annuallbs/acre
0.510
0.042
4.458
0.480
0.256
0.003
0.080
0.380
0.339
7.702
148.776
Date
lbs/ac
Prior Years Cumulative lbs/ac
0.1
0.06
9.674
0.494
0.012
0.192
0.963
0.14
15.75
1/22
0.64
Current Cumulative lbs/ac
0.610
0.102
14.132
0.480
0.750
0.015
0.272
1.343
0.479
23.452
Permitted C. P. L. R.****
36
34
1338
1
1 267
1 15
1 N/A
1 374
1 89
1 2498
Permit PAN Limit 1 st/2nd Crop
1 174 1 96
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
2/20/2024 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: City of Lumberton Total Dry Tons Applied (Annual): 130.75
Permit #: WQ0000672 Cation Exchange Capacity (non 503 only):
Operator: Delois Allen Owner: City of Lumberton Predominant Soil Series: Jo -Johns Sandy
Acres Used: 47.7 Acres Permitted: 47.7 Site #: 4 Field #: NC-RO-17-04
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample or
Com-
posite
Date
11
3/28/23
21
6/2/23
3
9/22/23
4
12/7/23
5
6
7
8
9
10
11
12
% Solids
2.9
2.6
1.6
1 1.8
Arsenic
35
46
69
55
Cadmium
3
3.8
5.8
4.6
Copper
15
440
310
360
Chronuum
0.06
0.06
220
190
Lead
18
23
35
28
Mercury
0.22
0.31
0.5
0.41
Molyb-
denum
7.7
9.9
15
12
Nickel
29
34
52
42
Selenium
32
42
63
51
Zinc
590
720
780
750
Total
Phos-
horus 1
16000
1 15000
15000
11000
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
D
-
Event
:1
1 •
1 111
1 ••
1 111
1 1
1 111
1111
1 111
1111
1 111
1 111
1111
1 111
1 ••
1 111
1 1
1 111
1 11 •
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
1 111
::
1 111
1•
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 •
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 •
1 111
1 1:
1 111
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 11
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 11
•
1 111
1 1 •
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1 •
••
1 111
1 111
1 1 •
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
1 111
�
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
®
1 111
•:
1 111
1•
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
11
Total
Phos-
phorus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
pLI _�L
Signature of Land Applie
2/20/2024
Date
DENR FORM MFLSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: City of Lumberton WQ Permit #: WQ0000672 Field #: NC-RO-17-04 Acres Utilized: 47.7
Land Owner: City of Lumberton Annual Dry Tons Applied: 130.7437 Site #: 4 Acres Permitted: 47.7
Operator: Delois Allen Predominant Soil Series: Jo -Johns Sandy Cation Exchange Capacity (non 503):
Crop 1 Name: Soybeans Crop 1 Max. PAN: 174 Crop 2 Name: Wheat Crop 2 Max. PAN: 106
0 p
A
Volume applied
(enter one) Solids/
Liquid
Cu. Yds Gallons
%
Solids
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal Waste,
etc)
Soil
Cond.
(Dry,
Wet
Moist)
Precip.
past 24
Hrs.
inches
a
� o
w
o
o
N
w CD
=
N
TKN
mg/kg
1 68000
Z a
°�
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
( lbs/acre)
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Crop 1
Crop 2
4/12/23
179800
2.6
0.409
WQ0000672
Dry
0
S
1 0.5
0.3
150
820
17.369
NA
Soybeans
4/13/23
93000
2.6
0.211
WQ0000672
Dry
0
S
0.5
0.3
68000
150
820
8.984
NA
Soybeans
4/14/23
105400
2.6
0.240
WQ0000672
Dry
0
S
0.5
0.3
68000
150
820
10.182
1 NA
Soybeans
4/19/23
136400
2.6
0.310
WQ0000672
Dry
0
S
0.5
0.3
68000
150
820
13.176
NA
Soybeans
4/20/231
155000
2.6
0.352
WQ0000672
Dry
0
S
0.5
0.3
68000
150
820
14.973
NA
Soybeans
4/21/23
124000
2.6
0.282
WQ0000672
Dry
0
S
0.5
0.3
68000
150
820
11.978
NA
Soybeans
10/28/23
272800
1.9
0.453
WQ0000672
Dry
0
S
0.5
0.3
120000
180
200
Na
32.839
Wheat
11/9/23
24800
1.9
0.041
WQ0000672
Dry
0
S
0.5
0.3
120000
180
200
Na
2.985
Wheat
11/10/23
167400
1.9
1 0.278
WQ0000672
Dry
0
S
0.5
0.3
120000
180
200
Na
20.151
Wheat
12/15/23
99200
1.9
0.165
WQ0000673
Dry
0
S
0.5
0.3
1 120000
180
200
Na
11.941
0.000
0.000
0.000
0.000
0.000
0.000
0
0
0.000
Residuals Applications
totals on FORM FSF supp ( attach FORM FSF supp to this form):
0.000
0.000
TOTALS:
01
1357800
As
Cd
Cu
Cr
Pb
H
Mo
Ni
Se
Zn P
76.662
67.916
Lime A lied
Annuallbs/acre
0.269
0.022
2.262
0.356
0.135
0.001
0.036
0.201
0.152
4.003 74.734
16.43
20.433
1 2498
Date
lbs/ac
Prior Years Cumulative lbs/ac
0.157
0.073
28.421
1.75
0.017
0.461
1.698
0.108
1/22
0.64
Current Cumulative lbs/ac
0.426
1 0.095
30.683
0.356
1.885
0.018
0.497
1.899
0.260
Permitted C. P. L. R.****
1 36
34
1338
267
1 15
1 N/A
1 374
89
Permit PAN Limit 1 st/2nd Crop
I
F 147 106
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
`lbI w4 *Application Method: S - Surface, IN - Injection, INC - Incorporation
G/ 2/20/2024 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically
digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: City of Lumberton Total Dry Tons Applied (Annual): 51.58
Permit #: WQ0000672 Cation Exchange Capacity (non 503 only):
Operator: Delois Allen Owner: City of Lumberton Predominant Soil Series: Lu-Lumbee
Acres Used: 35.82 Acres Permitted: 35.82 Site #: 5 Field #: NC-RO-17-05
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample or
Com-
posite
Date
1
3/28/23
2
6/2/23
3
9/22/23
4
12/7/23
5
6
7
8
9
10J
11
12
% Solids
2.9
2.6
1.6
1 1.9
Arsenic
35
46
69
55
Cadmium
3
3.8
5.8
4.6
Copper
15
440
310
360
Chronuum
0.06
0.06
220
190
Lead
18
23
35
28
Mercury
0.22
0.31
0.5
0.41
Molyb-
denum
7.7
9.9
15
12
Nickel
29
34
52
42
Selenium
32
42
63
51
Zinc
590
720
780
750
Total
Phos-
horus 1
16000
1 15000
15000
11000
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
D
Event
1 111
1 111
1 111
1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1
1 111
1 111
1 111
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
1 111
1 111
1 111
�
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
�
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1:
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1:
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
� �
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
�
1 111
1 111
1 111
�
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
®
1 111
1 111
1 111
•1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
•1
Total
Phos-
phorus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Signature of Land Applier
2/20/2024
Date
DENR FORM MFLSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: City of Lumberton WQ Permit #: WQ0000672 Field #: NGRO-17-05 Acres Utilized: 35.82
Land Owner: City of Lumberton Annual Dry Tons Applied: 51.5787 Site #: 5 Acres Permitted: 35.82
Operator: Delois Allen Predominant Soil Series: JO-Johns Sandy Loam Cation Exchange Capacity (non 503):
Crop 1 Name: Wheat Crop 1 Max. PAN: 106 Crop 2 Name: Crop 2 Max. PAN:
0 15%
0 p
A
Volume applied
(enter one) Solids/
Liquid
Cu. Yds Gallons
Solids
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
Soil
Cond.
(Dry,
Wet
Moist)
Precip.
past 24
Hrs.
inches
a
o
0 w
o.
o
N
0
w `;
=
0
TKN
mg/kg
Z a
o
°�
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
( lbs/acre)
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Crop 1
Crop 2
12/4/23
49600
1.9
0.110
WQ0000672
Dry
0
S
0.5
1 0.3
120000
180
200
7.951
NA
Wheat
12/5/23
111600
1.9
0.247
WQ0000672
Dry
0
S
0.5
0.3
120000
180
200
17.890
NA
Wheat
12/6/23
80600
1.9
0.178
WQ0000672
Dry
0
S
0.5
0.3
120000
180
200
12.920
NA
Wheat
12/7/23
167400
1.9
0.370
WQ0000672
Dry
0
S
0.5
0.3
120000
180
200
26.834
NA
Wheat
12/8/231
12400
1 1.9
0.027
WQ0000672
Dry
0
S
0.5
0.3
120000
180
200
1.988
NA
Wheat
12/13/23
99200
1.9
0.219
WQ0000672
Dry
0
S
0.5
0.3
120000
180
200
15.902
NA
Wheat
12/14/23
130200
1.9
0.288
WQ0000672
Dry
0
S
0.5
0.3
120000
180
200
20.871
NA
Wheat
0.000
0.000
1
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0
0
0.000
Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp
to this form):
0.000
1 0.000
TOTALS:
01
651000
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn
P
104.355
0.000
Lime Applied
Annuallbs/acre
0.158
0.013
1.037
0.547
0.081
0.000
0.000
0.121
0.000
2.160
11.680
Date
lbs/ac
Prior Years Cumulative lbs/ac
0.1
0.06
9.674
0.494
0.012
0.192
0.963
0.14
15.75
1/22
0.64
Current Cumulative lbs/ac
0.258
1 0.073
10.711
0.547
0.575
0.012
0.192
1.084
0.140
17.910
Permitted C. P. L. R.****
1 36
34
1338
1
1 267
15
N/A
374
1 89
1 2498
Permit PAN Limit 1 st/2nd Crop
1
1 106
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
€ I *Application Method: S - Surface, IN - Injection, INC - Incorporation
2/20/2024 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
City of Lumberton Total Dry Tons Applied (Annual):
WQ0000672 Cation Exchange Capacity (non 503 only):
Ronald Hammonds Owner: Ronald Hammonds Predominant Soil Series:
24.9 Acres Permitted: 24.9 Site #:
Field #
58.44
WkB-Wakulla
NC-RO-20-03
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample or
Com-
posite
Date
1
3/28/23
2
6/2/23
3
9/22/23
4
12/7/23
5
6
7
8
9
10J
11
12
% Solids
2.9
2.6
1.6
1 1.8
Arsenic
35
46
69
55
Cadmium
3
3.8
5.8
4.6
Copper
15
440
310
360
Chronuum
0.06
0.06
220
190
Lead
18
23
35
28
Mercury
0.22
0.31
0.5
0.41
Molyb-
denum
7.7
9.9
15
12
Nickel
29
34
52
42
Selenium
32
42
63
51
Zinc
590
720
780
750
Total
Phos-
horus 1
16000
1 15000
15000
11000
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
D
-
Event
11
1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 •
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 •
1 111
1 111
�
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1•
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 •
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
� �
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
�
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
®
1 111
1 111
�
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
Total
Phos-
phorus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
�/L- a crC4 - �L4
Signature of Land Applier
2/20/2024
Date
DENR FORM MFLSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
Facility Name: City of Lumberton
Land Owner: Ronald Hammonds
Operator: Ronalld Hammonds
Crop 1 Name: Bermuda
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
WQ Permit #: WQ0000672 Field #: NC-RO-20-03
Annual Dry Tons Applied: 58.4300 Site #: 3
Predominant Soil Series: Wkb-Wakulla
Crop 1 Max. PAN:
110.25
Crop 2 Name:
Acres Utilized: 24.9
Acres Permitted: 24.9
Cation Exchange Capacity (non 503):
Crop 2 Max. PAN:
0 p
A
Volume applied
(enter one) Solids/
Liquid
Cu. Yds Gallons
68200
%
Solids
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
(NpDES #, WQ#,
Fert., Animal
Waste, etc)
Soil
Cond.
(Dry,
Wet
Moist)
Precip.
past 24
Firs.
inches
a
F �
� o
0 w
o
N
0
w `I
=
N
� 0
TKN
mg/kg
68000
Z a
o
qQ 0
�
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
(lbs/acre)
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Crop 1
Crop 2
5/5/23
r 2.6
0.297
WQ0000672
Dry
0
S
0.5
0.3
r 150
820
12.621
NA
Bermuda
5/8/23
130200
2.6
0.567
WQ0000672
Dry
0
S
0.5
0.3
68000
150
820
24.094
NA
Bermuda
5/9/23
124000
2.6
0.540
WQ0000672
Dry
0
S
0.5
0.3
68000
150
820
22.947
NA
Bermuda
5/10/23
18600
2.6
0.081
WQ0000672
Dry
0
S
0.5
0.3
68000
150
820
3.442
NA
Bermuda
5/11/23
117800
2.6
1 0.513
WQ0000672
Dry
0
1 S
0.5
1 0.3
68000
150
1 820
21.799
NA
Bermuda
9/5/23
1
105400
1.6
0.282
WQ0000672
Dry
0
S
0.5
0.3
63000
600
920
11.263
NA
Bermuda
9/6/23
24800
1.6
0.066
WQ0000672
Dry
0
S
0.5
0.3
63000
600
920
2.650
NA
Bermuda
0.000
1
0.000
0.000
0.000
0.000
0.000
0.000
4
0.000
0.000
0.000
0.000
0.000
0
0
0.000
Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form):
0.000
0.000
TOTALS:
01
589000
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn
P
98.816
0.000
Lime Applied
Annuallbs/acre
0.000
0.000
0.216
0.154
0.116
0.000
0.000
0.000
0.000
0.544
70.410
Date
lbs/ac
Prior Years Cumulative lbs/ac
0.15
0.062
12.305
2.036
0.026
0.261
1.433
0.13
22.131
1/22
0.869
Current Cumulative lbs/ac
0.150
0.062
12.521
0.154
2.152
0.026
0.261
1.433
0.130
22.675
Permitted C. P. L. R.****
36
1 34
1338
267
15
374
1 89
1 2498
Permit PAN Limit 1 st/2nd Crop
1
1 110.25
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
f,L�J � A �L4 *Application Method: S - Surface, IN - Injection, INC - Incorporation
2/20/2024 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Ladd Applier
Date
*** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
City of Lumberton Total Dry Tons Applied (Annual):
WQ0000672 Cation Exchange Capacity (non 503 only):
Ronald Hammonds Owner: Charles Brown Predominant Soil Series:
31.2 Acres Permitted: 31.2 Site #: 4 Field #
79.97
WkB-Wakulla
NC-RO-20-4
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample or
Com-
posite
Date
1
3/28/23
2
6/2/23
3
9/22/23
4
12/7/23
5
6
7
8
9
10J
11
12
% Solids
2.9
2.6
1.6
1 1.9
Arsenic
35
46
69
55
Cadmium
3
3.8
5.8
4.6
Copper
15
440
310
360
Chronuum
0.06
0.06
220
190
Lead
18
23
35
28
Mercury
0.22
0.31
0.5
0.41
Molyb-
denum
7.7
9.9
15
12
Nickel
29
34
52
42
Selenium
32
42
63
51
Zinc
590
720
780
750
Total
Phos-
horus 1
16000
1 15000
15000
11000
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
D
-
Event
•
1 ••
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1•
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1•
1 111
1 111
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
1 111
1 1:
1 1 •
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
� �
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
�
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
®
1 111
1 111
®
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
Total
Phos-
phorus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
A&JIJ �_, 4—L4
Signature of Land Applier
2/20/2024
Date
DENR FORM MFLSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
Facility Name: City of Lumberton
Land Owner: Charles Brown
Operator: Ronald Hammond
Crop 1 Name: Bermuda
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
WQ Permit #: WQ0000672 Field #: NC-RO-20-04
Annual Dry Tons Applied: 79.9406 Site #: 4
Predominant Soil Series: WkB-Wakulla
Crop 1 Max. PAN:
147
Crop 2 Name:
Acres Utilized: 31.2
Acres Permitted: 31.2
Cation Exchange Capacity (non 503):
Crop 2 Max. PAN:
15
0 p
A
Volume applied
(enter one) Solids/
Liquid
Cu. Yds Gallons
%
Solids
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal Waste,
etc)
Soil
Cond.
(Dry,
Wet
Moist)
Precip.
past 24
Hrs.
inches
a
o
0 w
o
o
N
°�0
w `;
=
TKN
mg/kg
1 68000
Z a
o 0
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
(lbs/acre)
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Crop 1
Crop 2
4/15/22
161200
2.6
0.560
WQ0000672
Dry
0
S
0.5
0.3
150
1 820
23.807
NA
Bermuda
4/16/22
117800
2.6
0.409
WQ0000672
Dry
0
S
0.5
0.3
68000
150
820
17.398
NA
Bermuda
4/19/22
37200
2.6
0.129
WQ0000672
Dry
0
S
0.5
0.3
68000
150
820
5.494
NA
Bermuda
4/21/22
68200
2.6
0.237
WQ0000672
Dry
0
S
0.5
0.3
68000
150
820
10.072
NA
Bermuda
4/22/221
124000
1 2.6
0.431
WQ0000672
Dry
0
S
0.5
0.3
68000
150
820
18.313
NA
Bermuda
9/19/23
136400
1.6
0.292
WQ0000672
Dry
0
S
0.5
0.3
1 63000
600
920
11.632
NA
Bermuda
9/20/23
99200
1.6
0.212
WQ0000672
Dry
0
S
0.5
0.3
63000
600
920
8.460
NA
Bermuda
9/21/23
136400
1.6
0.292
WQ0000672
Dry
0
S
0.5
0.3
63000
600
920
1 11.632
NA
Bermuda
0.000
1
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Residuals Applications totals on FORM FSF supp ( attach FORM
FSF supp to this form):
0.000
0.000
TOTALS:
Ar
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn P
106.809
o.000
Lime Applied
Annuallbs/acre
0.000
0.000
0.494
0.350
0.137
0.000
0.000
0.000
0.000
1.242 76.890
31.217
32.459
2498
Date
lbs/ac
Prior Years Cumulative lbs/ac
0.249
0.078
17.582
1.957
0.038
0.364
2.001
0.183
1/22
0.869
Current Cumulative lbs/ac
0.249
0.078
18.076
0.350
2.094
0.038
0.364
2.001
0.183
Permitted C. P. L. R.****
36
34
1338
267
1 15
1 N/A
374
1 89
Permit PAN Limit 1 st/2nd Crop
i
1 147
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
//�Uj Lpa�-� 4J 2/20/2024 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land
Date
*** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
City of Lumberton Total Dry Tons Applied (Annual):
WQ0000672 Cation Exchange Capacity (non 503 only):
Ronald G. Hammonds Owner: Ronald G. Hammonds Predominant Soil Series:
6.7 Acres Permitted: 6.7 Site #:
Field #
26.99
NoA - Norfolk
NC-RO-20-06
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample or
Com-
posite
Date
1
3/28/23
2
6/2/23
3
9/22/23
4
12/7/23
5
6
7
8
9
10J
11
12
% Solids
2.9
2.6
1.6
1 1.9
Arsenic
35
46
69
55
Cadmium
3
3.8
5.8
4.6
Copper
15
440
310
360
Chronuum
0.06
0.06
220
190
Lead
18
23
35
28
Mercury
0.22
0.31
0.5
0.41
Molyb-
denum
7.7
9.9
15
12
Nickel
29
34
52
42
Selenium
32
42
63
51
Zinc
590
720
780
750
Total
Phos-
horus 1
16000
1 15000
15000
11000
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
D
-
Event
1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
��
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
��
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
• •
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
•
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
®®
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
Total
Phos-
phorus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
k�j ��� 4_�j
Signature of Land Applier
2/20/2024
Date
DENR FORM MFLSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: City of Lumberton WQ Permit #: WQ0000672 Field #: NC-RO-20-06 Acres Utilized: 6.7
Land Owner: Ronald G. Hammonds Annual Dry Tons Applied: 26.9916 Site #: 6 Acres Permitted: 6.7
Operator: Ronald G. Hammonds
Crop 1 Name: Soy
Predominant Soil Series: NoA-Norfolk
Crop 1 Max. PAN: 164 Crop 2 Name:
Cation Exchange Capacity (non 503):
Crop 2 Max. PAN:
+�
+; o
Volume applied
(enter one) Solids/
Liquid
Cu. Yds Gallons
%
Solids
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
Soil
Cond.
(Dry,
Wet
Moist)
precip.
Past 24
Hrs.
inches
a
4 '�pt
a '5
5- �-
0 w
o
o
0
w 2
co
TKN
mg/kg
Z a
o
5.
mg/kg
Nitrate
and
Nitrite
mg/kg
(lbs/acre)
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Crop 1
Crop 2
1/18/23
43400
2.9
0.783
WQ0000672
Dry
0
S
0.5
0.3
55000
2600
2300
30.268
NA
Soy
1/19/23
179800
2.9
3.245
WQ0000672
Dry
0
S
0.5
0.3
55000
2600
2300
125.397
NA
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0
0
0.000
Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form):
0.000
0.000
TOTALS:
01
223200
As
Cd
Cu
Cr
Pb
Hgr
Mo
Ni
Se
Zn
P
155.665T
0.000
Lime Applied
Annuallbs/acre
0.000
0.000
0.121
0.000
0.145
0.000
0.000
0.000
0.000
4.754
128.9281
Date
lbs/ac
Prior Years Cumulative lbs/ac
0.007
0.001
2.625
1.562
0
0.069
0.391
0.003
5.839
11/22
0.54
Current Cumulative lbs/ac
0.007
0.001
2.746
0.000
1.707
0.000
0.069
0.391
0.003
10.593
Permitted C. P. L. R. * * * *
36
34
1 1338
1
1 267
1 15
1 N/A
1 374
1 89
1 2498
Permit PAN Limit lst/2nd Crop
1 1 164
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
„ ^ , I *Application Method: S - Surface, IN - Injection, INC - Incorporation
2/20/2024 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
City of Lumberton Total Dry Tons Applied (Annual):
WQ0000672 Cation Exchange Capacity (non 503 only):
Ronald G. Hammonds Owner: Ronald G Hammonds Predominant Soil Series:
13 Acres Permitted: 13 Site #:
Field #
56.24
GoA-Goldsboro
NC-RO-20-07
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample or
Com-
posite
Date
1
3/28/23
2
6/2/23
3
9/22/23
4
12/7/23
5
6
7
8
9
10J
11
12
% Solids
2.9
2.6
1.6
1 1.9
Arsenic
35
46
69
55
Cadmium
3
3.8
5.8
4.6
Copper
15
440
310
360
Chronuum
0.06
0.06
220
190
Lead
18
23
35
28
Mercury
0.22
0.31
0.5
0.41
Molyb-
denum
7.7
9.9
15
12
Nickel
29
34
52
42
Selenium
32
42
63
51
Zinc
590
720
780
750
Total
Phos-
horus 1
16000
1 15000
15000
11000
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
D
Event
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
1 11
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 11
1 •
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 •
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
� �
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
�
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
®�
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
Total
Phos-
phorus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Signature of Land Applier
2/24/2024
Date
DENR FORM MFLSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: City of Lumberton WQ Permit #: WQ0000672 Field #: NC-RO-20-07 Acres Utilized: 13
Land Owner: Ronald G. Hammonds Annual Dry Tons Applied: 56.2325 Site #: 7 Acres Permitted: 13
Operator: Ronald G. Hammonds
Crop 1 Name: Soy
Predominant Soil Series: GoA-Goldsboro
Crop 1 Max. PAN: 176 Crop 2 Name:
Cation Exchange Capacity (non 503):
Crop 2 Max. PAN:
+�
+; o
Volume applied
(enter one) Solids/
Liquid
Cu. Yds Gallons
%
Solids
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
Soil
Cond.
(Dry,
Wet
Moist)
precip.
Past 24
Hrs.
inches
a
4 '�pt
a '5
5- �-
0 w
o
o
0
w 2
co
TKN
mg/kg
Z a
o
5.
mg/kg
Nitrate
and
Nitrite
mg/kg
(lbs/acre)
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Crop 1
Crop 2
1/18/23
80600
2.9
0.750
WQ0000672
Dry
0
S
0.5
0.3
55000
2600
2300
28.971
NA
Soy
1/19/23
31000
2.9
0.288
WQ0000672
Dry
0
S
0.5
0.3
55000
2600
2300
11.143
NA
Soy
2/28/23
31000
2.9
0.288
WQ0000672
Dry
0
S
0.5
0.3
55000
2600
2300
11.143
NA
Soy
3/l/23
167400
2.9
1.557
WQ0000672
Dry
0
S
0.5
0.3
55000
2600
2300
60.170
NA
Soy
3/2/23
155000
2.9
1.442
WQ0000672
Dry
0
S
0.5
0.3
55000
2600
2300
55.713
NA
Soy
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1
0
0
0.000
Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form):
0.000
0.000
TOTALS:
01
465000
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn
P
167.140
0.000
Lime Applied
Annuallbs/acre
0.000
0.000
0.130
0.001
0.156
0.000
0.000
0.000
0.000
5.105
138.432
Date
lbs/ac
Prior Years Cumulative lbs/ac
0.05
0.006
4.093
1.758
0.003
1 0.767
1 0.559
0.048
9.417
11/22
0.54
Current Cumulative lbs/ac
0.050
0.006
4.223
0.001
1.914
0.003
1
0.767
0.559
0.048
14.522
Permitted C. P. L. R. * * * *
36
34
1 1338
1
1 267
15
N/A
1 374
1 89
1 2498
Permit PAN Limit lst/2nd Crop
1 176
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
2/20/2024 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
City of Lumberton Total Dry Tons Applied (Annual):
WQ0000672 Cation Exchange Capacity (non 503 only):
Ronald Hammonds Owner: Ronald Hammonds Predominant Soil Series:
73.2 Acres Permitted: 73.2 Site #:
Field #
255.18
GoA-Goldsboro
NC-RO-20-08
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample or
Com-
posite
Date
1
3/28/23
2
6/2/23
3
9/22/23
4
12/7/23
5
6
7
8
9
10J
11
12
% Solids
2.9
2.6
1.6
1 1.9
Arsenic
35
46
69
55
Cadmium
3
3.8
5.8
4.6
Copper
15
440
310
360
Chronuum
0.06
0.06
220
190
Lead
18
23
35
28
Mercury
0.22
0.31
0.5
0.41
Molyb-
denum
7.7
9.9
15
12
Nickel
29
34
52
42
Selenium
32
42
63
51
Zinc
590
720
780
750
Total
Phos-
horus 1
16000
1 15000
15000
11000
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
D
-
Event
1 •
1 111
1 111
1 111
1 1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1 1
1 111
1 111
1 111
1 11
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 11
1 1•
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1•
1 111
1 111
1 111
1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1
��
1 111
1 111
1 1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
� �
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
�
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
®
•:•
1111
1 111
1111
1 111
1111
1 111
1111
1 111
1 111
1111
1 111
•:•
Total
Phos-
phorus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
t&j (?�4 4
Signature of Land Applier
2/20/2024
Date
DENR FORM MFLSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: City of Lumberton WQ Permit #: WQ0000672 Field #: NC-RO-20-08 Acres Utilized: 73.2
Land Owner: Ronald Hammonds
Operator: Ronald Hammonds
Annual Dry Tons Applied: 255.2048 Site #: 8
Acres Permitted: 73.2
Predominant Soil Series: GoA-Goldsboro Cation Exchange Capacity (non 503):
Crop 1 Name: Soy Crop 1 Max. PAN: 176 Crop 2 Name:
Crop 2 Max. PAN:
Volume applied
PP
enter one Solids/
( )
Liquid
Cu. Yds Gallons
o
/o
Solids
Volume
Applied per
pp p
Acre
(DryTons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
Soil
Cond.
( Dry
Wet,'
Moist)
Precip.
Past 24
Hrs.
inches
y
a '
F
0
o
qy :
�. -
N'
�.
5
o'
TKN
mg/kg
Z
Mo o
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
( lbs/acre)
Name of Crop Type
Receiving Residual
Application
Crop 1
FCrop 2
Crop 1
Crop 2
1/11/23
142600
2.9
0.236
W00000672
Dry
0
S
0.5
0.3
55000
2600
2300
9.103
NA
Soy
1/12/23
155000
2.9
0.256
W00000672
Dry
0
S
0.5
0.3
55000
2600
2300
9.894
NA
Soy
1/16/23
217000
2.9
0.358
W00000672
Dry
0
S
0.5
0.3
55000
2600
2300
13.852
NA
Soy
1/17/23
210800
2.9
0.348
W00000672
Dry
0
S
0.5
0.3
55000
2600
2300
13.456
NA
Soy
2/22/23
167400
2.9
0.277
W00000672
Dry
0
S
0.5
0.3
55000
2600
2300
10.686
NA
Soy
2/23/23
148800
2.9
0.246
W00000672
Dry
0
S
0.5
0.3
55000
2600
2300
9.499
NA
Soy
2/24/23
142600
2.9
0.236
1 W00000672
Dry
0
S
0.5
1 0.3
55000
2600
2300
1 9.103
NA
Soy
2/27/23
136400
2.9
0.225
W00000672
Dry
0
S
0.5
0.3
55000
1 2600
2300
8.707
NA
Soy
2/28/23
31000
2.9
0.051
W00000672
Dry
0
S
0.5
0.3
55000
2600
2300
1.979
NA
Soy
3/20/23
111600
2.9
0.184
W00000672
Dry
0
S
0.5
0.3
55000
2600
2300
7.124
NA
Soy
3/21/23
93000
2.9
0.154
W00000673
Dry
0
S
0.5
0.3
55000
2600
2300
5.937
NA
Soy
3/22/23
136400
2.9
0.225
W00000674
Dry
0
S
0.5
0.3
55000
2600
2300
8.707
NA
Soy
3/23/23
161200
2.9
0.266
1 W00000675
Dry
0
S
0.5
1 0.3
55000
2600
2300
1 10.290
NA
Soy
3/24/23
37200
2.9
0.061
W00000676
Dry
0
S
0.5
0.3
55000
2600
2300
2.375
NA
Soy
12/13/231
99200
1.9
0.107
W00000677
Dry
0
S
0.5
0.3
120000
180
200
7.781
NA
Soy
12/14/23
130200
1.9
0.141
W00000678
Dry
0
S
0.5
0.3
120000
180
200
10.213
NA
Soy
12/15/23
105400
1.9
0.114
W00000679
Dry
0
S
0.5
0.3
120000
180
200
8.268
NA
Soy
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0
0
3.486
Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form):
0.000
0.000
TOTALS:
01
2225800
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn
P
146.975
o.000
Lime Applied
Annuallbs/acre
0.040
0.003
0.094
0.138
0.133
0.000
0.000
0.000
0.000
3.686
107.9321
Date
11/22
lbs/ac
0.54
Prior Years Cumulative lbs/ac
0.074
0.003
3.84
1.208
0.01
0.063
0.327
0.093
6.684
Current Cumulative lbs/ac
0.114
0.006
3.934
0.138
1.341
0.010
0.063
0.327
0.093
10.370
Permitted C. P. L. R.****
36
34
1338
267
15
N/A
374
89
2498
Permit PAN Limit 1 st/2nd Crop
1 176
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
r ^ *Application Method: S - Surface, IN - Injection, INC - Incorporation
2/20/2024 **Volatilization Rate: Surface - 0.5, Injection/Incorporation -1.0
Signature of Land Applier Date * * * Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: City of Lumberton Total Dry Tons Applied (Annual): 46.48
Permit #: WQ0000672 Cation Exchange Capacity (non 503 only):
Operator: Ronald G. Hammonds Owner: Taylco, INC Predominant Soil Series: GoA-Goldsboro
Acres Used: 10.6 Acres Permitted: 10.6 Site #: 14 Field #: NC-RO-20-14
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample or
Com-
posite
Date
—11
3/28/23
1
6/2/23
3i
9/22/23
4
12/7/23
5
6
7
8
9
10
11
12
% Solids
2.9
2.6
1.6
1.9
Arsenic
35
46
69
55
Cadmium
3
3.8
5.8
4.6
Copper
15
440
310
360
Chromium
0.06
0.06
220
190
Lead
18
23
35
28
Mercury
0.22
0.31
0.5
0.41
Molyb-
denum
7.7
9.9
15
12
Nickel
29
34
52
42
Selenium
32
42
63
51
Zinc
590
720
780
750
Total
Phos-
horus 1
16000
115000
15000
11000
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
E
D
NEEM
MEMEMEMEMEMEMEMM
on
Event
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
��
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 11
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 11
1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
� �
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
�
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
®®
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
Total
Phos-
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
phorus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information
submitted. I am aware that there are significant penalties for submitting false information, including the possibility
of fines and imprisonment for knowing violations".
Signature of Land Applier
2/ 16/2023
Date
DENR FORM MFLSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
Facility Name: City of Lumberton
Land Owner: Taylco, Inc
Operator: Ronald G. Hammonds
Crop 1 Name:
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
WQ Permit #: WQ0000672 Field #: NC-RO-20-14
Annual Dry Tons Applied: 46.4855 Site #: 14
Predominant Soil Series: GoA-Goldsboro
Crop 1 Max. PAN:
176
Crop 2 Name:
Acres Utilized: 10.6
Acres Permitted: 10.6
Cation Exchange Capacity (non 503):
Crop 2 Max. PAN:
0 p
A
Volume applied
(enter one) Solids/
Liquid
Cu. Yds Gallons
186000
%
Solids
2.9
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
Soil
Cond.
(Dry,
Wet
Moist)
Precip.
past 24
Firs.
inches
a
o
0 w
o
N
w `;
=
N
TKN
mg/kg
Z a
o
0
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
( lbs/acre)
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Crop 1
Crop 2
3/8/23
2.122
WQ0000672
Dry
0
S
0.5
1 0.3
55000
2600
1 2300
81.993
NA
Soy
3/9/23
111600
2.9
1.273
WQ0000672
Dry
0
S
0.5
0.3
55000
2600
2300
49.196
NA
Soy
3/15/23
49600
2.9
0.566
WQ0000672
Dry
0
S
0.5
0.3
55000
2600
2300
21.865
NA
Soy
3/16/23
37200
2.9
0.424
WQ0000672
Dry
0
S
0.5
0.3
55000
2600
2300
16.399
NA
Soy
0.000
1
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1 0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0
0
0.000
Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form):
0.000
0.000
TOTALS:
01
198400
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn
P
169.4531
o.000
Lime Applied
Annuallbs/acre
0.000
0.000
0.132
0.001
0.158
0.000
0.000
0.000
0.000
5.174
140.320
Date
lbs/ac
Prior Years Cumulative lbs/ac
0.001
0
10.033
0.33
0
0
0
0
14.341
11/22
0.54
Current Cumulative lbs/ac
0.001
0.000
10.165
0.001
0.488
0.000
0.000
0.000
0.000
19.515
Permitted C. P. L. R.****
36
1 34
1 1338
1
1 267
1 15
1 N/A
1 374
1 89
1 2498
Permit PAN Limit 1 st/2nd Crop
1
1 176
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
2/16/2023 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
City of Lumberton Total Dry Tons Applied (Annual):
WQ0000672 Cation Exchange Capacity (non 503 only):
Carrell Locklear Owner: Robert Baskersville Predominant Soil Series:
11.6 Acres Permitted: 11.6 Site #:
Field #
16.70
Ra
NC-RO-28-1
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample or
Com-
posite
Date
1
3/28/23
2
6/2/23
3
9/22/23
4
12/7/23
5
6
7
8
9
10J
11
12
% Solids
2.9
2.6
1.6
1 1.9
Arsenic
35
46
69
55
Cadmium
3
3.8
5.8
4.6
Copper
15
440
310
360
Chronuum
0.06
0.06
220
190
Lead
18
23
35
28
Mercury
0.22
0.31
0.5
0.41
Molyb-
denum
7.7
9.9
15
12
Nickel
29
34
52
42
Selenium
32
42
63
51
Zinc
590
720
780
750
Total
Phos-
horus 1
16000
1 15000
15000
11000
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
D
Event
1 111
1 111
1 111
1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1
1 111
1 111
1 111
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
�
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1:
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1:
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
� �
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
�
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
®
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
Total
Phos-
phorus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
�W � -6 A 4j
Signature of Land Applier
2/20/2024
Date
DENR FORM MFLSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: City of Lumberton WQ Permit #: WQ0000672 Field #: NC-RO-28-1 Acres Utilized: 11.6
Land Owner: Robert Baskerville
Operator: Carnell Locklear
Crop 1 Name: Wheat
Annual Dry Tons Applied: 16.7017
Site #: 1
Predominant Soil Series: Ra - Rains Sandy
Crop 1 Max. PAN: 106 Crop 2 Name:
Acres Permitted: 11.6
Cation Exchange Capacity (non 503):
Crop 2 Max. PAN:
+�
+; o
Volume applied
(enter one) Solids/
Liquid
Cu. Yds Gallons
117800
%
Solids
1.9
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
Soil
Cond.
(Dry,
Wet
Moist)
Precip.
Past 24
Hrs.
inches
a
'�pt
rn �
5-
0 w
o
o
0
w
co
0
TKN
mg/kg
120000
Z a
o 5
5.
mg/kg
Nitrate
and
Nitrite
mg/kg
(lbs/acre)
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Crop 1
Crop 2
10/23/23
0.805
WQ0000672
Dry
0
S
0.5
0.3
180
200
58.311
NA
Corn
10/24/23
93000
1.9
0.635
WQ0000672
Dry
0
S
0.5
0.3
120000
180
200
46.035
NA
Corn
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0
0
0.000
Residuals Applications totals on FORM FSF supp ( attach FORM
FSF supp to this form):
0.000
0.000
TOTALSI
01
210800
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn
P
104.3451
0.000
Lime Applied
Annuallbs/acre
0.158
0.013
0.000
0.547
0.081
0.000
0.000
0.000
0.000
0.000
31.680
F 106
Date
lbs/ac
Prior Years Cumulative lbs/ac
0.061
0.012
3.569
0.236
0.006
0.066
0.501
0.062
4.955
11/22
0.59
Current Cumulative lbs/ac
0.219
0.025
3.569
0.547
0.317
0.006
0.066
0.501
0.062
4.955
Permitted C. P. L. R. * * * *
1 0.061
34
1 1998
1
1 267
1 15
1 N/A
1 374
1 89
1 2498
Permit PAN Limit Ist/2nd Crop
I
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified
personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including
the possibility of fines and imprnent for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
2/20/2024 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically
digested -0.3, raw sludge -0.4
****C.P.L.R: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
City of Lumberton Total Dry Tons Applied (Annual):
WQ0000672 Cation Exchange Capacity (non 503 only):
Carrell Locklear Owner: Robert Baskersville Predominant Soil Series:
10.4 Acres Permitted: 10.4 Site #:
Field #
19.16
GoA
NC-RO-28-3
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample or
Com-
posite
Date
1
3/28/23
2
6/2/23
3
9/22/23
4
12/7/23
5
6
7
8
9
10J
11
12
% Solids
2.9
2.6
1.6
1 1.9
Arsenic
35
46
69
55
Cadmium
3
3.8
5.8
4.6
Copper
15
440
310
360
Chronuum
0.06
0.06
220
190
Lead
18
23
35
28
Mercury
0.22
0.31
0.5
0.41
Molyb-
denum
7.7
9.9
15
12
Nickel
29
34
52
42
Selenium
32
42
63
51
Zinc
590
720
780
750
Total
Phos-
horus 1
16000
1 15000
15000
11000
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
D
Event
1 111
1 111
1 111
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
1 111
1 111
1 111
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 11
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 11
1 111
1 111
1 111
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
� �
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
�
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
®
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
Total
Phos-
1 111
1 111
1 111
1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1
phorus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Signature of Land Applier
2/20/2024
Date
DENR FORM MFLSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: City of Lumberton WQ Permit #: W00000672 Field #: NC-RO-28-3 Acres Utilized: 104
Land Owner: Robert Baskerville Annual Dry Tons Applied: 19.1578 Site #: 3 Acres Permitted
Operator: Carnell Locklear
Crop 1 Name: Wheat
Predominant Soil Series: Goldsboro GoA
Crop 1 Max. PAN: 135
Crop 2 Name:
Cation Exchange Capacity (non 503):
Crop 2 Max. PAN:
10.4
0 o
A
Volume applied
(enter one) Solids/
Liquid
Cu. Yds Gallons
105400
%
Solids
1.9
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
Soil
Cond.
(Dry,
Wet
Moist)
Precip.
past 24
Firs.
inches
a
w
o.
o
N
w `;
TKN
mg/kg
120000
Z a
o
CD �
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
( lbs/acre)
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Crop 1
Crop 2
10/16/23
0.803
WQ0000672
Dry
0
S
0.5
0.3
180
200
58.193
NA
Corn
10/19/23
117800
1.9
0.897
WQ0000672
Dry
0
S
0.5
0.3
120000
180
200
65.039
NA
Corn
10/20/23
18600
1.9
0.142
WQ0000672
Dry
1
S
0.5
0.3
120000
180
200
10.269
NA
Corn
0.000
0.000
NA
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1 0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0
0
0.000
Residuals Applications totals on FORM FSF supp ( attach FORM
FSF supp to this form):
0.000
0.000
TOTALS:
01
241800
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn
P
133.500
0.000
Lime Applied
Annuallbs/acre
0.203
0.017
0.000
0.700
0.103
0.000
0.000
0.000
0.000
0.000
40.524
Date
lbs/ac
Prior Years Cumulative lbs/ac
0.061
0.012
3.569
0.236
0.006
0.066
0.501
0.062
4.955
11/22
0.59
Current Cumulative lbs/ac
0.264
0.029
3.569
0.700
0.339
0.006
0.066
0.501
0.062
4.955
Permitted C. P. L. R.****
0.061
1 34
1998
1
267
15
N/A
374
89
2498
Permit PAN Limit 1 st/2nd Crop
1
1 135
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified
personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including
the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
2/20/2024 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically
digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: City of Lumberton Total Dry Tons Applied (Annual): 9.98
Permit #: WQ0000672 Cation Exchange Capacity (non 503 only):
Operator: Tracy Bullard Owner: Tracy Bullard Predominant Soil Series: Ra-Rains
Acres Used: 5.1 Acres Permitted: 5.1 Site #: 3 Field #: NC-RO-39-03
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample or
Com-
posite
Date
11
3/28/23
21
6/2/23
3
9/22/23
4
12/7/23
5
6
7
8
9
10
11
12
% Solids
2.9
2.6
1.6
1 1.8
Arsenic
35
46
69
55
Cadmium
3
3.8
5.8
4.6
Copper
15
440
310
360
Chronuum
0.06
0.06
220
190
Lead
18
23
35
28
Mercury
0.22
0.31
0.5
0.41
Molyb-
denum
7.7
9.9
15
12
Nickel
29
34
52
42
Selenium
32
42
63
51
Zinc
590
720
780
750
Total
Phos-
horus 1
16000
1 15000
15000
11000
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
D
-
Event
1
1 111
1 111
1 111
1 1•
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1•
1 111
1 111
1 111
1 11
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 11
1 111
1 111
1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1
1 111
1 111
1 •1
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1: •
1 111
1 111
1 1•
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 •
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
� �
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
�
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
®
1 111
1 111
®
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
Total
Phos-
phorus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Signature of Land Applier
2/20/2024
Date
DENR FORM MFLSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
Facility Name: City of Lumberton
Land Owner: Tracy Bullard
Operator: Tracy Bullard
Crop 1 Name: Bermuda
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
WQ Permit #: WQ0000672 Field #: NC-RO-39-03
Annual Dry Tons Applied: 9.9796 Site #: 3
Predominant Soil Series: Ra-Rains
Crop 1 Max. PAN: 113.25 Crop 2 Name:
Acres Utilized: 5.1
Acres Permitted: 5.1
Cation Exchange Capacity (non 503):
Crop 2 Max. PAN:
o
Volume applied
(enter one) Solids/
Liquid
9
Cu. Yds Gallons
%
Solids
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
(NpDES #, WQ#,
Fert.,Animal
Waste, etc)
Soil
Cond.
fin'
Wet
Moist)
Precip.
Past 24
Hrs.
inches
a
o w
* °�
o
N
o
7
w
o
TKN
mg/kg
63000
Z a
o
ac o
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
(lbs/acre)
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Crop 1
Crop 2
7/19
55800
1.6
0.730
WQ0000672
Dry
0
S
0.5
0.3
1 600
920
29.112
NA
Ber
7/20
49600
1.6
0.649
WQ0000672
Dry
0
S
0.5
0.3
63000
600
920
25.878
NA
Ber
10/18
37200
1.9
0.578
WQ0000673
Dry
0
S
0.5
0.3
120000
180
200
41.883
NA
Ber
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0
0
0.000
Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form):
0.000
0.000
TOTALS:
01
142600
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn
P
96.872
0.000
Lime Applied
Annuallbs/acre
0.064
0.005
0.855
0.826
0.129
0.000
0.000
0.000
0.000
2.151
54.086
Date
lbs/ac
Prior Years Cumulative lbs/ac
Current Cumulative lbs/ac
0.064
0.005
0.855
0.826
0.129
0.000
0.000
0.000
0.000
2.151
Permitted C. P. L. R. * * * *
Permit PAN Limit 1 st/2nd Crop
113.25
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility f fines and imprisonment for knowing violations."
61 � � *Application Method: S - Surface, IN - Injection, INC - Incorporation
2/20/2024 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
* * * * C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: City of Lumberton Total Dry Tons Applied (Annual): 32.07
Permit #: WQ0000672 Cation Exchange Capacity (non 503 only):
Operator: Tracy Bullard Owner: Tracy Bullard Predominant Soil Series: Ly-Lynchburg
Acres Used: 14.8 Acres Permitted: 14.8 Site #: 4 Field #: NC-RO-39-04
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample or
Com-
posite
Date
11
3/28/23
21
6/2/23
3
9/22/23
4
12/7/23
5
6
7
8
9
10
11
12
% Solids
2.9
2.6
1.6
1 1.9
Arsenic
35
46
69
55
Cadmium
3
3.8
5.8
4.6
Copper
15
440
310
360
Chronuum
0.06
0.06
220
190
Lead
18
23
35
28
Mercury
0.22
0.31
0.5
0.41
Molyb-
denum
7.7
9.9
15
12
Nickel
29
34
52
42
Selenium
32
42
63
51
Zinc
590
720
780
750
Total
Phos-
horus 1
16000
1 15000
15000
11000
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
D
-
Event
1 :1
1 111
1 111
1 111
1 1::
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1::
1 111
1 111
1 111
1 11
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 11
1 111
1 111
1•
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1•
1 111
1 111
1 •1
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 •1•
1 111
1 111
1 1••
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
• •
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
•
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
®
1 111
1 111
®
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
Total
Phos-
phorus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Vy�
Signature of Land Applier
2/20/2024
Date
DENR FORM MFLSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
Facility Name: City of Lumberton
Land Owner: Tracy Bullard
Operator: Tracy Bullard
Crop 1 Name: Bermuda
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
WQ Permit #: WQ0000672 Field #: NC-RO-39-04
Annual Dry Tons Applied: 32.0590 Site #: 4
Predominant Soil Series: Ly-Lynchburg
Crop 1 Max. PAN: 129 Crop 2 Name:
Acres Utilized: 14.8
Acres Permitted: 14.8
Cation Exchange Capacity (non 503):
Crop 2 Max. PAN:
o
Volume applied
(enter one) Solids/
Liquid
9
Cu. Yds Gallons
%
Solids
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
(NpDES #, WQ#,
Fert.,Animal
Waste, etc)
Soil
Cond.
fin'
Wet
Moist)
Precip.
Past 24
Hrs.
inches
a
4-,
o w
* °�
o
N
o
7
0
o
TKN
mg/kg
63000
Z a
o
ac o
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
(lbs/acre)
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Crop 1
Crop 2
7/25/23
80600
1.6
0.363
WQ0000672
Dry
0
S
0.5
0.3
600
920
14.491
NA
Ber
8/7/23
99200
1.6
0.447
WQ0000672
Dry
0
S
0.5
0.3
63000
600
920
17.835
NA
Ber
8/8/23
62000
1.6
0.280
WQ0000672
Dry
0
S
0.5
0.3
63000
600
920
11.147
NA
Ber
9/25/23
62000
1.6
0.280
WQ0000672
Dry
1
S
0.5
0.3
63000
600
920
11.147
NA
Ber
10/16/23
74400
1.9
0.398
WQ0000672
Dry
2
S
0.5
0.3
120000
180
200
28.865
NA
Ber
10/20/23
49600
1.9
0.266
WQ0000672
Dry
3
S
0.5
0.3
120000
180
200
19.243
NA
Ber
10/23/23
24800
1.9
0.133
WQ0000672
Dry
4
S
0.5
0.3
120000
180
200
9.622
NA
Ber
0.000
0.000
0.000
0.000
1
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0
0
2.166
Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form):
0.000
0.000
TOTALS:
01
452600
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn
P
112.348
0.000
Lime Applied
Annuallbs/acre
0.088
0.007
0.849
0.906
0.141
0.000
0.000
0.000
0.000
2.137
58.634
Date
lbs/ac
Prior Years Cumulative lbs/ac
0.001
0
0.023
0.001
0
0
0.002
0.001
0.1
Current Cumulative lbs/ac
0.089
0.007
0.872
0.906
0.142
0.000
0.000
0.002
0.001
2.237
Permitted C. P. L. R.****
36
34
1 1338
267
15
N/A
374
1 89
1 2498
Permit PAN Limit 1 st/2nd Crop
129
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
(} *Application Method: S - Surface, IN - Injection, INC - Incorporation
`mow 2/20/2024 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
* * * * C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: City of Lumberton Total Dry Tons Applied (Annual): 9.10
Permit #: WQ0000672 Cation Exchange Capacity (non 503 only):
Operator: Tracy Bullard Owner: Tracy Bullard Predominant Soil Series: Ly-Lynchburg
Acres Used: 3.8 Acres Permitted: 3.8 Site #: 5 Field #: NC-RO-39-05
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample or
Com-
posite
Date
11
3/28/23
21
6/2/23
3
9/22/23
4
12/7/23
5
6
7
8
9
10
11
12
% Solids
2.9
2.6
1.6
1 1.9
Arsenic
35
46
69
55
Cadmium
3
3.8
5.8
4.6
Copper
15
440
310
360
Chronuum
0.06
0.06
220
190
Lead
18
23
35
28
Mercury
0.22
0.31
0.5
0.41
Molyb-
denum
7.7
9.9
15
12
Nickel
29
34
52
42
Selenium
32
42
63
51
Zinc
590
720
780
750
Total
Phos-
horus 1
16000
1 15000
15000
11000
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
D
-
Event
1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
�
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 •:
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 •:
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
� �
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
�
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
®
1 111
1 111
�
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
Total
Phos-
phorus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
&a L,3, 4j
Signature of Land App1
2/20/2024
Date
DENR FORM MFLSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: City of Lumberton WQ Permit #: WQ0000672 Field #: NC-RO-39-05 Acres Utilized: 3.8
Land Owner: Tracy Bullard Annual Dry Tons Applied: 9.1006 Site #: 5 Acres Permitted: 3.8
Operator: Tracy Bullard
Crop 1 Name:
Bermuda
Predominant Soil Series: Ly-Lynchburg
Crop 1 Max. PAN: 129 Crop 2 Name:
Cation Exchange Capacity (non 503):
Crop 2 Max. PAN:
o S
Volume applied
(enter one) Solids/
Liquid
Cu. Yds Gallons
%
Solids
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
(NpDES #, WQ#,
Fert., Animal
Waste, etc)
Soil
Cond.
�e '
Moist)
Precip.
Past 24
Hrs.
inches
a
4 �
n
w
* °�
o
o
7
w
o
TKN
mg/kg
Z a
o
ac o
�.
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
(lbs/acre)
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Crop 1
Crop 2
7/21
55800
1.6
0.980
WQ0000672
Dry
0
1 S
0.5
1 0.3
630001
600
920
39.072
NA
Bermuda
7/27
80600
1.6
1.415
WQ0000672
Dry
0
S
0.5
0.3
63000
600
920
56.437
NA
Bermuda
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0
0
0.000
Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form):
0.000
0.000
TOTALS:
0
136400
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn
P
95.508
0.000
Lime Applied
Annuallbs/acre
0.000
0.000
1.485
1.054
0.168
0.000
0.000
0.000
0.000
3.736
71.850
Date
lbs/ac
Prior Years Cumulative lbs/ac
0.001
0
0.024
0.001
0
0
0.002
0.001 0.102
0.001 3.838
89 1 2498
Current Cumulative lbs/ac
0.001
1 0.000
1.509
1.054
0.169
0.000
0.000
0.002
Permitted C. P. L. R.****
1 36
34
1 1338
1
267
15
1 N/A
1 374
Permit PAN Limit 1 st/2nd Crop
F 129
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
2/20/2024 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
* * * * C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: City of Lumberton Total Dry Tons Applied (Annual): 2.07
Permit #: WQ0000672 Cation Exchange Capacity (non 503 only):
Operator: Tracy Bullard Owner: Tracy Bullard Predominant Soil Series: Wab-Wagram
Acres Used: 2.9 Acres Permitted: 2.9 Site #: 6 Field #: NC-RO-39-06
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample or
Com-
posite
Date
1
3/28/23
2
6/2/23
3
9/22/23
4
12/7/23
5
6
7
8
9
10J
11
12
% Solids
2.9
2.6
1.6
1 1.9
Arsenic
35
46
69
55
Cadmium
3
3.8
5.8
4.6
Copper
15
440
310
360
Chronuum
0.06
0.06
220
190
Lead
18
23
35
28
Mercury
0.22
0.31
0.5
0.41
Molyb-
denum
7.7
9.9
15
12
Nickel
29
34
52
42
Selenium
32
42
63
51
Zinc
590
720
780
750
Total
Phos-
horus 1
16000
1 15000
15000
11000
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
D
-
Event
1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
�
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
�
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
• •
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
•
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
®
1 111
1 111
®
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
Total
Phos-
phorus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
fiW � A �L�
Signature of Land Applier
2/20/2024
Date
DENR FORM MFLSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: City of Lumberton WQ Permit #: WQ0000672 Field #: NC-RO-39-06 Acres Utilized: 2.9
Land Owner: Tracy Bullard Annual Dry Tons Applied: 2.0683 Site #: 6 Acres Permitted: 2.9
Operator: Tracy Bullard
Crop 1 Name:
Bermuda
Predominant Soil Series: WaB-Wagram
Crop 1 Max. PAN: 150 Crop 2 Name:
Cation Exchange Capacity (non 503):
Crop 2 Max. PAN:
o S
Volume applied
(enter one) Solids/
Liquid
Cu. Yds Gallons
%
Solids
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
(NpDES #, WQ#,
Fert., Animal
Waste, etc)
Soil
Cond.
�e '
Moist)
Precip.
Past 24
Hrs.
inches
a
4 �
w
* °�
o
�
o
7
w
o
TKN
mg/kg
63000
Z a
o
ac o
�.
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
(lbs/acre)
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Crop 1
Crop 2
7/26
31000
1.6
0.713
TQ0000672
Dry
0
S
1 0.5
0.3
600
1 920
28.443
NA
Ber
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1 0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0
0
0.000
Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form):
0.000
0.000
TOTALS:
0
31000
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn P
28.443
0.000
Lime Applied
Annuallbs/acre
0.000
0.000
0.442
0.314
0.050
0.000
0.000
0.000
0.000
1.112 21.390
Date
lbs/ac
Prior Years Cumulative lbs/ac
Current Cumulative lbs/ac
0.000
0.000
0.442
0.314
0.050
0.000
0.000
0.000
0.000
1.112
Permitted C. P. L. R. * * *
Permit PAN Limit 1 st/2nd Crop
1 150
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fi s and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
!�
U LJ � 2/20/2024 **Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
Signature of
Date
* * * Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
* * * * C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: City of Lumberton Total Dry Tons Applied (Annual): 139.31
Permit #: WQ0000672 Cation Exchange Capacity (non 503 only):
Operator: Tracy Bullard Owner: Tracy Bullard Predominant Soil Series: Wab-Wagram
Acres Used: 62.5 Acres Permitted: 62.5 Site #: 9 Field #: NC-RO-39-09
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample or
Com-
posite
Date
1
3/28/23
2
6/2/23
3
9/22/23
4
12/7/23
5
6
7
8
9
10
11
12
% Solids
2.9
2.6
1.6
1 1.9
Arsenic
35
46
69
55
Cadmium
3
3.8
5.8
4.6
Copper
15
440
310
360
Chronuum
0.06
0.06
220
190
Lead
18
23
35
28
Mercury
0.22
0.31
0.5
0.41
Molyb-
denum
7.7
9.9
15
12
Nickel
29
34
52
42
Selenium
32
42
63
51
Zinc
590
720
780
750
Total
Phos-
horus 1
16000
1 15000
15000
11000
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
D
-
Event
••
1
1 111
1 111
1 111
1 1•
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1•
1 111
1 111
1 111
1 11
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 11
1 111
1 111
1•
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1•
1 111
1 111
1
1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1• •
1 111
1 111
1 •
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
� �
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
�
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
®
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
Total
Phos-
phorus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
4j
— A��j � - � Signature of Land Applier
2/20/2024
Date
DENR FORM MFLSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: City of Lumberton
Land Owner: Tracy Bullard
Operator: Tracy Bullard
Crop 1 Name: Bermuda
WQ Permit #: WQ0000672 Field #: NC-RO-39-09
Annual Dry Tons Applied: 139.2755 Site #: 9
Predominant Soil Series: WaB-Wagram
Crop 1 Max. PAN: 192 Crop 2 Name:
Acres Utilized: 62.5
Acres Permitted: 62.5
Cation Exchange Capacity (non 503):
Crop 2 Max. PAN:
o
Volume applied
(enter one) Solids/
Liquid
Cu. Yds Gallons
oho
Solids
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
Soil
Cond.
(Dry,
Moist)
Precip.
past 24
Hrs.
inches
a
* Z
?
* w
0
��,
F*,
*
* Z
1'KN
mg/kg
a
o o
�.
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
( lbs/acre)
Name of Crop Type
Receivin Residual
g
Application
Crop 1
Crop 2
Crop 1
Crop 2
7/6/23
111600
1.6
0.119
WQ0000672
Dry
0
S
0.5
0.3
63000
600
920
4.751
NA
Bermuda
7/7/23
117800
1.6
0.126
WQ0000672
Dry
0
S
0.5
0.3
63000
600
920
5.015
NA
Bermuda
7/13/23
142600
1.6
0.152
WQ0000672
Dry
0
S
0.5
0.3
63000
600
920
6.071
NA
Bermuda
7/14/23
86800
1.6
0.093
WQ0000672
Dry
0
S
0.5
0.3
63000
600
920
3.695
NA
Bermuda
8/11/23
105400
1.6
0.113
WQ0000672
Dry
0
S
0.5
0.3
63000
600
920
4.487
NA
Bermuda
8/12/23
62000
1.6
0.066
WQ0000672
Dry
0
S
0.5
0.3
63000
600
920
2.640
NA
Bermuda
8/14/23
6200
1.6
0.007
WQ0000672
Dry
0
S
0.5
0.3
63000
600
920
0.264
NA
Bermuda
8/15/23
105400
1.6
0.113
WQ0000672
Dry
0
S
0.5
0.3
63000
600
920
4.487
NA
Bermuda
8/21/23
99200
1.6
0.106
WQ0000672
Dry
0
S
0.5
0.3
63000
600
920
4.223
NA
Bermuda
8/22/23
167400
1.6
0.179
WQ0000672
Dry
0
S
0.5
0.3
63000
600
920
7.127
NA
Bermuda
8/23/23
173600
1.6
0.185
WQ0000672
Dry
0
S
0.5
0.3
63000
600
920
7.391
NA
Bermuda
8/24/23
148800
1.6
0.159
WQ0000672
Dry
0
S
0.5
0.3
63000
600
920
6.335
NA
Bermuda
8/25/23
142600
1.6
0.152
WQ0000672
Dry
0
S
0.5
0.3
63000
600
920
6.071
NA
Bermuda
8/26/23
80600
1.6
0.086
WQ0000672
Dry
0
S
0.5
0.3
63000
600
920
3.431
NA
Bermuda
10/25/23
74400
1.9
0.094
WQ0000672
Dry
0
S
0.5
0.3
120000
180
200
6.835
NA
Bermuda
0
1 378200
0.479
Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form):
34.746
0.000
TOTALS:
01
2002600
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn
P
107.5691
0.000
Lime Applied
Annuallbs/acre
0.063
0.005
1.026
0.946
0.148
0.000
0.000
0.000
0.000
2.582
62.278
Date
lbs/ac
Prior Years Cumulative lbs/ac
0.03
0.002
7.196
0.692
0.004
0.082
0.456
0.036
13.331
Current Cumulative lbs/ac
0.093
0.007
8.222
0.946
0.840
0.004
0.082
0.456
0.036
15.913
Permitted C. P. L. R.****
36
34
1338
267
15
N/A
374
89
2498
Permit PAN Limit 1 st/2nd Crop
1 192
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
p 414*Application Method: S - Surface, IN - Injection, INC - Incorporation
2/20/2024 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier Date * * * Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
Supplemental Information
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: City of Lumberton
Land Owner: Tracy Bullard
Operator: Tracy Bullard
Crop 1 Name:
Bermuda
WQ Permit #: W00000672
Annual Dry Tons Applied: 139.275498
Predominant Soil Series: WaB-Wagram
Crop 1 Max. PAN:
192.00
Field #: NC-RO-39-09
Site #: 9
Crop 2 Name:
Acres Utilized: 62.5
Acres Permitted: 62.5
Cation Exchange Capacity (non 503):
Crop 2 Max PAN:
o
+, o
Volume applied (enter
one )
Cu. Yds Gallons
Solids
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES 4, WQ4,
Fert., Animal
Waste, etc)
Soil
Cond.
D
�et�
Moist)
Preci p
Past 24
Hrs.
inches
y
co
��
0 w
oCD
o
Fo
N
w
o
TKN
mg/kg
Z
o 5
M °
�.
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
lbs/acre)
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Crop 1
Crop 2
1026/23
86800
1.9
0.110
WQ0000672
Dry
0
S
0.5
0.3
120000
180
200
7.974
NA
10/27/23
93000
1.9
0.118
WQ0000672
Dry
0
S
0.5
0.3
120000
180
200
8.544
NA
10/30/23
93000
1.9
0.118
WQ0000672
Dry
0
S
0.5
0.3
120000
180
200
8.544
NA
10/31/23
105400
1.9
1 0.134
WQ0000672
Dry
0
S
0.5
0.3
120000
180
200
9.683
NA
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
TOTALS:
0
378200
0.479
34.746
0.000
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
2/20/2024 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of L d Applier Date ***C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (SUPP) (12/2006)

tiff eurofins 0
Environment Testing
ANALYTICAL REPORT
PREPARED FOR
Attn: Cody Hunt
Hunt Environmental Associates ■�
3330 Saddletree Rd
Lumberton, North Carolina 28360
Generated 3/28/2023 6:49:11 AM Revision 1
JOB DESCRIPTION
City of Lumberton- TCLP
r* JOB NUMBER
752-2248-1
1

The test results in this report relate only to the samples as received by the laboratory and will meet all requirements of the
methodology, with any exceptions noted. This report shall not be reproduced except in full, without the express written
approval of the laboratory. All questions should be directed to the Eurofins Environment Testing Southeast, LLC Project
Manager.
/�// - (Ca' �- /
Authorized for release by
Bill Scott, Project Manager
Bill. [e-mail]
Designee for
Stephanie Franz, Project Manager
stephanie.franzaet.eurofinsus.com
[phone]
Generated
3/28/2023 6:49:11 AM
Revision 1
12
13
14
Eurofins Savannah is a laboratory within Eurofins Environment Testing Southeast, LLC, a company within Eurofins Environment Testing Group of Companies
Page 2 of 40 3/28/2023 (Rev. 1)

Client: Hunt Environmental Associates
Project/Site: City of Lumberton- TCLP
Laboratory Job ID: 752-2248-1
Table of Contents
Cover Page ..............................................
1
Table of Contents .........................................
3
Definitions/Glossary.......................................
4
Case Narrative ...........................................
5
Detection Summary ........................................
6
Client Sample Results ......................................
7
Surrogate Summary .......................................
12
QC Sample Results ........................................
15
QC Association Summary ...................................
27
Lab Chronicle ............................................
31
Certification Summary ......................................
33
Method Summary .........................................
34
Sample Summary .........................................
35
Chain of Custody ..........................................
36
Receipt Checklists .........................................
38
12
13
14
Page 3 of 40
Eurofins Raleigh
3/28/2023 (Rev. 1)

Definitions/Glossary
Client: Hunt Environmental Associates
Project/Site: City of Lumberton- TCLP
Qualifiers
GC Semi VOA
Qualifier Qualifier Description
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
Metals
Qualifier Qualifier Description
F1 MS and/or MSD recovery exceeds control limits.
F2 MS/MSD RPD exceeds control limits
General Chemistry
Qualifier Qualifier Description
HF Field parameter with a holding time of 15 minutes. Test performed by laboratory at client's request.
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
Glossary
Abbreviation These commonly used abbreviations may or may not be present in this report.
II Listed under the "D" column to designate that the result is reported on a dry weight basis
%R Percent Recovery
CFL Contains Free Liquid
CFU Colony Forming Unit
CNF Contains No Free Liquid
DER Duplicate Error Ratio (normalized absolute difference)
Dil Fac Dilution Factor
DL Detection Limit (DoD/DOE)
DL, RA, RE, IN Indicates a Dilution, Re -analysis, Re -extraction, or additional Initial metals/anion analysis of the sample
DLC Decision Level Concentration (Radiochemistry)
EDL Estimated Detection Limit (Dioxin)
LOD Limit of Detection (DoD/DOE)
LOQ Limit of Quantitation (DoD/DOE)
MCL EPA recommended "Maximum Contaminant Level"
MDA Minimum Detectable Activity (Radiochemistry)
MDC Minimum Detectable Concentration (Radiochemistry)
MDL Method Detection Limit
ML Minimum Level (Dioxin)
MPN Most Probable Number
MQL Method Quantitation Limit
NC Not Calculated
ND Not Detected at the reporting limit (or MDL or EDL if shown)
NEG Negative / Absent
POS Positive / Present
PQL Practical Quantitation Limit
PRIES Presumptive
QC Quality Control
RER Relative Error Ratio (Radiochemistry)
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
TNTC Too Numerous To Count
Job ID: 752-2248-1
Eurofins Raleigh
Page 4 of 40 3/28/2023 (Rev. 1)

Case Narrative
Client: Hunt Environmental Associates
Project/Site: City of Lumberton- TCLP
Job ID: 752-2248-1
Laboratory: Eurofins Raleigh
Narrative
Job ID: 752-2248-1
0
Job Narrative
752-2248-1
Comments
No additional comments.
Receipt
The samples were received on 2/3/2023 10:46 AM. Unless otherwise noted below, the samples arrived in good condition, and where
required, properly preserved and on ice. The temperature of the cooler at receipt was 3.00 C.
GC/MS VOA
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.
GC/MS Semi VOA
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.
GC Semi VOA
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.
Metals
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.
General Chemistry
Methods 335.4, 9012B, SM 4500 CN E: The matrix spike / matrix spike duplicate (MS/MSD) recoveries for preparation batch 680-762486
and analytical batch 680-762691 were outside control limits for one or more analytes, see QC Sample Results for detail. Sample matrix
interference and/or non -homogeneity are suspected because the associated laboratory control sample (LCS) recovery is within
acceptance limits.
Method 9034: The matrix spike / matrix spike duplicate (MS/MSD) recoveries for preparation batch 680-762213 and analytical batch
680-762259 were outside control limits for one or more analytes, see QC Sample Results for detail. Sample matrix interference and/or
non -homogeneity are suspected because the associated laboratory control sample (LCS) recovery is within acceptance limits.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
Organic Prep
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.
VOA Prep
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.
Eurofins Raleigh
Page 5 of 40 3/28/2023 (Rev. 1)

Detection Summary
Client: Hunt Environmental Associates
Job ID: 752-2248-1
Project/Site: City of Lumberton- TCLP
Client Sample ID: WWTP-Q1
Lab Sample ID: 752-2248-1
Analyte
Result
Qualifier
RL
MDL
Unit
Dil Fac D Method Prep Type
Cyanide, Total
2.7
J
4.2
1.1
mg/Kg
1 * 335.4-1993 R1.0 Total/NA
soil pH measured in water at deg C
7.2
HF
SU
1 9045C Total/NA
Temperature
17.1
HF
Degrees C
1 9045C Total/NA
Client Sample ID: WTP
Lab Sample ID: 752-2248-2
Analyte
Result
Qualifier
RL
MDL
Unit
Dil Fac D Method Prep Type
Cyanide, Total
5.4
J
5.7
1.5
mg/Kg
1 "� 335.4-1993 R1.0 Total/NA
soil pH measured in water at deg C
5.7
HF
SU
1 9045C Total/NA
Temperature
17.1
HF
Degrees C
1 9045C Total/NA
Client Sample ID: WTP-Q1
Lab Sample ID: 752-2248-3
CAnalyte
Result
Qualifier
RL
MDL
Unit
Dil Fac D Method Prep Type
Flashpoint
>140
Degrees F
1 1010B Total/NA
Client Sample ID: WTP
Lab Sample ID: 752-2248-4
CAnalyte
Result
Qualifier
RL
MDL
Unit
Dil Fac D Method Prep Type
Flashpoint
>140
Degrees F
1 1010B Total/NA
This Detection Summary does not include radiochemical test results.
Page 6 of 40
Eurofins Raleigh
3/28/2023 (Rev. 1)

Client Sample Results
Client: Hunt Environmental Associates
Job ID: 752-2248-1
Project/Site: City of Lumberton- TCLP
Client Sample ID: WWTP-Q1
Lab Sample ID: 752-2248-1
Date Collected: 02/02/23 11:30
Matrix: Solid
Date Received: 02/03/23 10:46
Method: SW846 8260D - Volatile Organic
Compounds by GC/MS - TCLP
Analyte
Result Qualifier
RL
MDL
Unit
D Prepared Analyzed
Dil Fac
1,1-Dichloroethene
<0.0072
0.020
0.0072
mg/L
02/19/23 20:48
20
1,2-Dichloroethane
<0.010
0.020
0.010
mg/L
02/19/23 20:48
20
1,4-Dichlorobenzene
<0.0092
0.020
0.0092
mg/L
02/19/23 20:48
20
Methyl Ethyl Ketone
<0.068
0.20
0.068
mg/L
02/19/23 20:48
20
Benzene
<0.0086
0.020
0.0086
mg/L
02/19/23 20:48
20
Carbon tetrachloride
<0.0066
0.020
0.0066
mg/L
02/19/23 20:48
20
Chlorobenzene
<0.0052
0.020
0.0052
mg/L
02/19/23 20:48
20
Chloroform
<0.010
0.020
0.010
mg/L
02/19/23 20:48
20
Hexachlorobutadiene
<0.050
0.10
0.050
mg/L
02/19/23 20:48
20
Tetrachloroethylene
<0.015
0.020
0.015
mg/L
02/19/23 20:48
20
Trichloroethylene
<0.0096
0.020
0.0096
mg/L
02/19/23 20:48
20
Vinyl chloride
<0.010
0.020
0.010
mg/L
02/19/23 20:48
20
Surrogate %Recovery Qualifier
Limits
Prepared Analyzed
Dil Fac
4-Bromofluorobenzene (Surr)
106
70 -130
02119123 20:48
20
Dibromofluoromethane (Surr)
100
70 -130
02119123 20:48
20
Toluene-d8 (Surr)
105
70 -130
02119123 20:48
20
1,2-Dichloroethane-d4 (Surr)
96
60-124
02119123 20:48
20
Method: SW846 8270E - Semivolatile Organic Compounds (GC/MS) - TCLP
Analyte
Result Qualifier
RL
MDL
Unit
D Prepared
Analyzed
Dil Fac
1,4-Dichlorobenzene
<0.016
0.050
0.016
mg/L
02/19/23 07:59
02/20/23 18:04
1
Pyridine
<0.037
0.25
0.037
mg/L
02/19/23 07:59
02/20/23 18:04
1
Hexachlorobenzene
<0.0080
0.050
0.0080
mg/L
02/19/23 07:59
02/20/23 18:04
1
2,4-Dinitrotoluene
<0.012
0.050
0.012
mg/L
02/19/23 07:59
02/20/23 18:04
1
Hexachloroethane
<0.018
0.050
0.018
mg/L
02/19/23 07:59
02/20/23 18:04
1
Hexachlorobutadiene
<0.020
0.050
0.020
mg/L
02/19/23 07:59
02/20/23 18:04
1
Pentachlorophenol
<0.050
0.25
0.050
mg/L
02/19/23 07:59
02/20/23 18:04
1
2,4,6-Trichlorophenol
<0.011
0.050
0.011
mg/L
02/19/23 07:59
02/20/23 18:04
1
2,4,5-Trichlorophenol
<0.016
0.050
0.016
mg/L
02/19/23 07:59
02/20/23 18:04
1
Nitrobenzene
<0.018
0.050
0.018
mg/L
02/19/23 07:59
02/20/23 18:04
1
o-Cresol
<0.0090
0.050
0.0090
mg/L
02/19/23 07:59
02/20/23 18:04
1
m & p - Cresol
<0.0070
0.050
0.0070
mg/L
02/19/23 07:59
02/20/23 18:04
1
Cresol
<0.0090
0.050
0.0090
mg/L
02/19/23 07:59
02/20/23 18:04
1
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed
Dil Fac
2,4,6-Tribromophenol(Surr)
81
30-130
02119123 07:59
0212012318:04
1
2-Fluorobiphenyl (Surr)
83
25 -130
02119123 07:59
02120123 18:04
1
2-Fluorophenol (Surr)
37
10 -130
02119123 07:59
02120123 18:04
1
Terphenyl-d14 (Surr)
110
35-131
02119123 07:59
02120123 18:04
1
Phenol-d5 (Surr)
25
10 -130
02119123 07:59
02120123 18:04
1
Nitrobenzene-d5 (Surr)
71
30 -130
02119123 07:59
02120123 18:04
1
Method: SW846 8081 B - Organochlorine Pesticides (GC) - TCLP
Analyte
Result Qualifier
RL
MDL
Unit
D Prepared
Analyzed
Dil Fac
Chlordane (technical)
<0.0080
0.025
0.0080
mg/L
02/19/23 08:03
02/20/23 17:32
1
Endrin
<0.0000050
0.0025
0.0000050
mg/L
02/19/23 08:03
02/20/23 17:32
1
gamma-BHC (Lindane)
<0.0000050
0.0025
0.0000050
mg/L
02/19/23 08:03
02/20/23 17:32
1
Heptachlor
<0.0000050
0.0025
0.0000050
mg/L
02/19/23 08:03
02/20/23 17:32
1
Heptachlor epoxide
<0.000010
0.0025
0.000010
mg/L
02/19/23 08:03
02/20/23 17:32
1
Eurofins Raleigh
Page 7 of 40 3/28/2023 (Rev. 1)

Client Sample Results
Client: Hunt Environmental Associates
Project/Site: City of Lumberton- TCLP
Client Sample ID: WWTP-Q1
Date Collected: 02/02/23 11:30
Date Received: 02/03/23 10:46
Job ID: 752-2248-1
Lab Sample ID: 752-2248-1
Matrix: Solid
Method: SW846 8081 B - Organochlorine Pesticides (GC) - TCLP (Continued)
Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac
Methoxychlor <0.000010 0.0025 0.000010 mg/L 02/19/23 08:03 02/20/23 17:32 1
-- .- -. -- ............ --
Toxaphene <0.016 0.25 0.016 mg/L 02/19/23 08:03 02/20/23 17:32 1 �
Surrogate
%Recovery Qualifier
DCB Decachlorobiphenyl
92
Tetrachloro-m-xylene
62
Method: SW846 8151A - Herbicides (GC) - TCLP
Analyte
Result Qualifier
2,4-D
<0.0018
Silvex (2,4,5-TP)
<0.00097
Surrogate
DCAA
Limits
30-130
30-130
RL MDL Unit
0.011 0.0018 mg/L
0.0089 0.00097 mg/L
%Recovery Qualifier Limits
97 26-137
Method: SW846 6010D - Metals (ICP) - TCLP
Analyte
Result Qualifier
Arsenic
<0.20
Barium
<1.0
Cadmium
<0.10
Chromium
.. ....... ..
<0.20
Lead
<0.20
Selenium
<0.50
.....
Silver
... ...... ....
<0.10 F1
Method: SW846 7470A - Mercury (CVAA)
- TCLP
Analyte
Result Qualifier
Mercury
<0.020 F1 F2
General Chemistry
Analyte
Result Qualifier
soil pH measured in water at deg
7.2 HF
C (SW846 9045C)
Temperature (SW846 9045C)
17.1 HF
Client Sample ID: WWTP-Q1
Date Collected: 02/02/23 11:30
Date Received: 02/03/23 10:46
General Chemistry
Prepared
Analyzed
Dil Fac
02/19/23 08:03
02120123 17:32
1
02/19/23 08:03
02120123 17:32
1
D Prepared
Analyzed
Dil Fac
02/20/23 09:22
02/22/23 02:06
1
02/20/23 09:22
02/22/23 02:06
1
Prepared
Analyzed
Dil Fac
02120123 09:22
02/22/23 02:06
1
RL
MDL
Unit
D Prepared
Analyzed
Dil Fac
0.20
0.20
mg/L
02/17/2313:14
02/20/2313:32
1
1.0
1.0
mg/L
02/17/2313:14
02/20/2313:32
1
0.10
0.10
mg/L
02/17/2313:14
02/20/2313:32
1
0.20
0.20
------
mg/L
-- ---------- -
02/17/2313:14
02/20/2313:32
1
0.20
0.20
mg/L
02/17/2313:14
02/20/2313:32
1
0.50
0.50
mg/L
02/17/2313:14
02/20/2313:32
1
0.10
0.10
...........................
mg/L
02/17/2313:14
..................
02/20/2313:32
.
1
RL
MDL
Unit
D Prepared
Analyzed
Dil Fac
0.020
0.020
mg/L
02/20/2312:38
02/21/2310:56
1
RL MDL Unit D Prepared Analyzed Dil Fac
Su 02/16/23 14:42 1
Degrees C 02/16/23 14:42 1
Lab Sample ID: 752-2248-1
Matrix: Solid
Percent Solids: 2.9
Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac
Cyanide, Total (MCAWW 2.7 J 4.2 1.1 mg/Kg 0 02/08/23 10:11 02/09/23 10:31 1
335.4-1993 R1.0)
Sulfide (SW846 9034) <2100 2100 2100 mg/Kg 0 02/07/23 07:08 02/07/23 09:31 1
Client Sample ID: WTP Lab Sample ID: 752-2248-2
Date Collected: 02/02/23 12:00 Matrix: Solid
Date Received: 02/03/23 10:46
Method: SW846 8260D - Volatile Organic Compounds by GC/MS - TCLP
Analyte Result Qualifier RL MDL Unit
1,1-Dichloroethene <0.0072 0.020 0.0072 mg/L
D Prepared Analyzed Dil Fac
02/19/23 21:07 20
Page 8 of 40
Eurofins Raleigh
3/28/2023 (Rev. 1)

Client Sample Results
Client: Hunt Environmental Associates
Job ID: 752-2248-1
Project/Site: City of Lumberton- TCLP
Client Sample ID: WTP
Lab Sample ID: 752-2248-2
Date Collected: 02/02/23 12:00
Matrix: Solid
Date Received: 02/03/23 10:46
Method: SW846 8260D - Volatile
Organic Compounds by GC/MS - TCLP
(Continued)
Analyte
Result Qualifier
RL
MDL
Unit D
Prepared Analyzed
Dil Fac
1,2-Dichloroethane
<0.010
0.020
0.010
mg/L
02/19/23 21:07
20
1,4-Dichlorobenzene
<0.0092
0.020
0.0092
mg/L
02/19/23 21:07
20
Methyl Ethyl Ketone
<0.068
0.20
0.068
mg/L
02/19/23 21:07
20
Benzene
<0.0086
0.020
0.0086
mg/L
02/19/23 21:07
20
Carbon tetrachloride
<0.0066
0.020
0.0066
mg/L
02/19/23 21:07
20
Chlorobenzene
<0.0052
0.020
0.0052
mg/L
02/19/23 21:07
20
Chloroform
<0.010
0.020
0.010
mg/L
02/19/23 21:07
20
Hexachlorobutadiene
<0.050
0.10
0.050
mg/L
02/19/23 21:07
20
Tetrachloroethylene
<0.015
0.020
0.015
mg/L
02/19/23 21:07
20
Trichloroethylene
<0.0096
0.020
0.0096
mg/L
02/19/23 21:07
20
Vinyl chloride
<0.010
0.020
0.010
mg/L
02/19/23 21:07
20
Surrogate
%Recovery Qualifier
Limits
Prepared Analyzed
Dil Fac
4-Bromofluorobenzene (Surr)
109
70 -130
02119123 21:07
20
Dibromofluoromethane (Surr)
100
70 -130
02119123 21:07
20
Toluene-d8 (Surr)
104
70 -130
02119123 21:07
20
1,2-Dichloroethane-d4 (Surr)
95
60-124
02119123 21:07
20
Method: SW846 8270E - Semivolatile Organic Compounds (GC/MS) - TCLP
Analyte
Result Qualifier
RL
MDL
Unit
D Prepared
Analyzed
Dil Fac
1,4-Dichlorobenzene
<0.016
0.050
0.016
mg/L
02/19/23 07:59
02/20/23 17:38
1
Pyridine
<0.037
0.25
0.037
mg/L
02/19/23 07:59
02/20/23 17:38
1
Hexachlorobenzene
<0.0080
0.050
0.0080
mg/L
02/19/23 07:59
02/20/23 17:38
1
2,4-Dinitrotoluene
<0.012
0.050
0.012
mg/L
02/19/23 07:59
02/20/23 17:38
1
Hexachloroethane
<0.018
0.050
0.018
mg/L
02/19/23 07:59
02/20/23 17:38
1
Hexachlorobutadiene
<0.020
0.050
0.020
mg/L
02/19/23 07:59
02/20/23 17:38
1
Pentachlorophenol
<0.050
0.25
0.050
mg/L
02/19/23 07:59
02/20/23 17:38
1
2,4,6-Trichlorophenol
<0.011
0.050
0.011
mg/L
02/19/23 07:59
02/20/23 17:38
1
2,4,5-Trichlorophenol
<0.016
0.050
0.016
mg/L
02/19/23 07:59
02/20/23 17:38
1
Nitrobenzene
<0.018
0.050
0.018
mg/L
02/19/23 07:59
02/20/23 17:38
1
o-Cresol
<0.0090
0.050
0.0090
mg/L
02/19/23 07:59
02/20/23 17:38
1
m & p - Cresol
<0.0070
0.050
0.0070
mg/L
02/19/23 07:59
02/20/23 17:38
1
Cresol
<0.0090
0.050
0.0090
mg/L
02/19/23 07:59
02/20/23 17:38
1
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed
Dil Fac
2, 4, 6-Tribromophenol (Surr)
69
30 -130
02119123 07:59
02120123 17:38
1
2-Fluorobiphenyl (Surr)
63
25 -130
02119123 07:59
02120123 17:38
1
2-Fluorophenol (Surr)
29
10 -130
02119123 07:59
02120123 17:38
1
Terphenyl-d14 (Surr)
105
35-131
02119123 07:59
02120123 17:38
1
Phenol-d5 (Surr)
19
10 -130
02119123 07:59
02120123 17:38
1
Nitrobenzene-d5 (Surr)
57
30 -130
02119123 07:59
02120123 17:38
1
Method: SW846 8081 B - Organochlorine
Pesticides
(GC) - TCLP
Analyte
Result Qualifier
RL
MDL
Unit
D Prepared
Analyzed
Dil Fac
Chlordane (technical)
<0.0080
0.025
0.0080
mg/L
02/19/23 08:03
02/20/23 17:51
1
Endrin
<0.0000050
0.0025
0.0000050
mg/L
02/19/23 08:03
02/20/23 17:51
1
gamma-BHC (Lindane)
<0.0000050
0.0025
0.0000050
mg/L
02/19/23 08:03
02/20/23 17:51
1
Heptachlor
<0.0000050
0.0025
0.0000050
mg/L
02/19/23 08:03
02/20/23 17:51
1
Heptachlor epoxide
<0.000010
0.0025
0.000010
mg/L
02/19/23 08:03
02/20/23 17:51
1
Methoxychlor
<0.000010
0.0025
0.000010
mg/L
02/19/23 08:03
02/20/23 17:51
1
Eurofins Raleigh
Page 9 of 40 3/28/2023 (Rev. 1)

Client Sample Results
Client: Hunt Environmental Associates
Project/Site: City of Lumberton- TCLP
Job ID: 752-2248-1
Client Sample ID: WTP Lab Sample ID: 752-2248-2
Date Collected: 02/02/23 12:00 Matrix: Solid
Date Received: 02/03/23 10:46
Method: SW846 8081 B - Organochlorine Pesticides (GC) - TCLP (Continued)
Analyte
Result Qualifier
RL
MDL
Unit
Toxaphene
<0.016
0.25
0.016
mg/L
Surrogate
%Recovery Qualifier
Limits
DCB Decachlorobiphenyl
94
30 -130
Tetrachloro-m-xylene
72
30 -130
Method: SW846 8151A - Herbicides
(GC) - TCLP
Analyte
Result Qualifier
RL
MDL
Unit
2,4-D
<0.0019
0.012
0.0019
mg/L
Silvex (2,4,5-TP)
<0.0010
0.0094
0.0010
mg/L
Surrogate
%Recovery Qualifier
Limits
DCAA
91
26.137
Method: SW846 6010D - Metals
(ICP) - TCLP
Analyte
Result Qualifier
RL
MDL
Unit
Arsenic
<0.20
0.20
0.20
mg/L
Barium
<1.0
1.0
1.0
mg/L
Cadmium
<0.10
0.10
0.10
mg/L
Chromium
<0.20
0.20
0.20
mg/L
Lead
<0.20
0.20
0.20
mg/L
Selenium
<0.50
0.50
0.50
mg/L
Silver
<0.10
0.10
0.10
mg/L
Method: SW846 7470A - Mercury (CVAA) - TCLP
Analyte
Result Qualifier
RL
MDL
Unit
Mercury
<0.020
0.020
0.020
mg/L
General Chemistry
Analyte
Result Qualifier
RL
MDL
Unit
soil pH measured in water at deg
5.7 HF
SU
C (SW846 9045C)
Temperature (SW846 9045C)
17.1 HF
Degrees C
D Prepared
Analyzed
Dil Fac
02/19/23 08:03
02/20/23 17:51
1
Prepared
Analyzed
DY Fac
02119123 08:03
02120123 17:51
1
02119123 08:03
02120123 17:51
1
D Prepared
Analyzed
Dil Fac
02/20/23 09:22
02/22/23 01:01
1
02/20/23 09:22
02/22/23 01:01
1
Prepared
Analyzed
DY Fac
02120123 09:22
02122123 01:01
1
D Prepared
Analyzed
Dil Fac
02/17/2313:14
02/20/2313:40
1
02/17/2313:14
02/20/2313:40
1
02/17/2313:14
02/20/2313:40
1
02/17/2313:14
02/20/2313:40
1
02/17/2313:14
02/20/2313:40
1
02/17/2313:14
02/20/2313:40
1
02/17/2313:14
02/20/2313:40
1
D Prepared
Analyzed
Dil Fac
02/20/2312:38
02/21/2311:07
1
D Prepared Analyzed Dil Fac
02/16/23 14:42 1
02/16/23 14:42 1
Client Sample ID: WTP
Lab Sample ID: 752-2248-2
Date Collected: 02/02/23 12:00
Matrix: Solid
Date Received: 02/03/23 10:46
Percent Solids: 2.0
General Chemistry
Analyte
Result Qualifier
RL MDL Unit
D Prepared Analyzed Dil Fac
Cyanide, Total (MCAWW
5.4 J
5.7 1.5 mg/Kg
02/08/23 10:11 02/09/23 11:24 1
335.4-1993 R1.0)
Sulfide (SW846 9034)
<2900
2900 2900 mg/Kg
02/07/23 07:08 02/07/23 09:31 1
Client Sample ID: WTP-Q1
Lab Sample ID: 752-2248-3
Date Collected: 02/02/23 11:30
Matrix: Water
Date Received: 02/03/23 10:46
General Chemistry
Analyte
Result Qualifier
RL MDL Unit
D Prepared Analyzed Dil Fac
Flash point (SW846 101013)
>140
Degrees F
02/09/23 10:00 1
Eurofins Raleigh
Page 10 of 40 3/28/2023 (Rev. 1)

Client Sample Results
Client: Hunt Environmental Associates Job ID: 752-2248-1
Project/Site: City of Lumberton- TCLP
Client Sample ID: WTP Lab Sample ID: 752-2248-4
Date Collected: 02/02/23 12:00 Matrix: Water
Date Received: 02/03/23 10:46
General Chemistry
LAnalyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac
Flashpoint (SW846 101013) >140 Degrees F 02/09/23 10:45 1
Eurofins Raleigh
Page 11 of 40 3/28/2023 (Rev. 1)

Surrogate Summary
Client: Hunt Environmental Associates
Job ID: 752-2248-1
Project/Site: City of Lumberton- TCLP
Method: 8260D - Volatile Organic Compounds by GC/MS
Matrix: Solid
Prep Type: Total/NA
Percent Surrogate Recovery (Acceptance Limits)
BFB DBFM
TOL
DCA
Lab Sample ID Client Sample ID (70-130) (70-130)
(70-130)
(60-124)
LCS 680-763978/4 Lab Control Sample 102 97
99
93
LCSD 680-763978/5 Lab Control Sample Dup 103 97
100
98
MB 680-763978/8 Method Blank 108 100
104
95
Surrogate Legend
BFB = 4-Bromofluorobenzene (Surr)
DBFM = Dibromofluoromethane (Surr)
TOL = Toluene-d8 (Surr)
DCA = 1,2-Dichloroethane-d4 (Surr)
Method: 8260D - Volatile Organic Compounds by GC/MS
Matrix: Solid
Prep Type: TCLP
Percent Surrogate Recovery (Acceptance Limits)
BFB DBFM
TOL
DCA
Lab Sample ID Client Sample ID (70-130) (70-130)
(70-130)
(60-124)
752-2248-1 WWFP-Q1 106 100
105
96
752-2248-2 WTP 109 100
104
95
LB 680-763738/1-A Method Blank 109 100
106
96
Surrogate Legend
BFB = 4-Bromofluorobenzene (Surr)
DBFM = Dibromofluoromethane (Surr)
TOL = Toluene-d8 (Surr)
DCA = 1,2-Dichloroethane-d4 (Surr)
Method: 8270E - Semivolatile Organic Compounds (GC/MS)
Matrix: Solid
PreD TVDe: Total/NA
Percent Surrogate Recovery (Acceptance Limits)
TBP
FBP
2FP
TPHL
PHL
NBZ
Lab Sample ID Client Sample ID (30-130)
(25-130)
(10-130)
(35-131)
(10-130)
(30-130)
LCS 680-763973/2-A Lab Control Sample 84
76
35
104
25
75
MB 680-763973/1-A Method Blank 71
73
34
110
23
65
Surrogate Legend
TBP = 2,4,6-Tribromophenol (Surr)
FBP = 2-Fluorobiphenyl (Surr)
2FP = 2-Fluorophenol (Surr)
TPHL = Terphenyl-d14 (Surr)
PHL = Phenol-d5 (Surr)
NBZ = Nitrobenzene-d5 (Surr)
Method: 8270E - Semivolatile Organic Compounds (GC/MS)
Matrix: Solid Prep Type: TCLP
Percent Surrogate Recovery (Acceptance Limits)
TBP
FBP
2FP
TPHL
PHL
NBZ
Lab Sample ID
Client Sample ID
(30-130)
(25-130)
(10-130)
(35-131)
(10-130)
(30-130)
752-2248-1
WWFP-Q1
81
83
37
110
25
71
752-2248-2
WTP
69
63
29
105
19
57
752-2248-2 MS
WTP
81
76
33
100
23
77
Eurofins Raleigh
Page 12 of 40 3/28/2023 (Rev. 1)

Surrogate Summary
Client: Hunt Environmental Associates
Job ID: 752-2248-1
Project/Site: City of Lumberton- TCLP
Method: 8270E - Semivolatile Organic
Compounds
(GC/MS) (Continued)
Matrix: Solid
Prep Type: TCLP
Percent Surrogate Recovery (Acceptance Limits)
TBP
FBP 2FP TPHL PHL
NBZ
Lab Sample ID Client Sample ID
(30-130)
(25-130) (10-130) (35-131) (10-130)
(30-130)
752-2248-2 MSD VVTP
83
72 31 103 22
70
LB 680-763695/1-D Method Blank
75
66 29 105 19
57
Surrogate Legend
TBP = 2,4,6-Tribromophenol (Surr)
FBP = 2-Fluorobiphenyl (Surr) Y
2FP = 2-Fluorophenol (Surr)
TPHL = Terphenyl-d14 (Surr)
PHL = Phenol-d5 (Surr)
NBZ = Nitrobenzene-d5 (Surr)
Method: 8081 B - Organochlorine Pesticides (GC)
Matrix: Solid Prep Type: Total/NA
Percent Surrogate Recovery (Acceptance Limits)
DCBP1 TCX1
Lab Sample ID Client Sample ID (30-130) (30-130)
MB 680-763974/1-A Method Blank 105 76
Surrogate Legend
DCBP = DCB Decachlorobiphenyl
TCX = Tetrachloro-m-xylene
Method: 8081 B - Organochlorine Pesticides (GC)
Matrix: Solid Prep Type: Total/NA
Percent Surrogate Recovery (Acceptance Limits)
DCBP2 TCX1
Lab Sample ID Client Sample ID (30-130) (30-130)
LCS 680-763974/2-A Lab Control Sample 95 60
Surrogate Legend
DCBP = DCB Decachlorobiphenyl
TCX = Tetrachloro-m-xylene
Method: 8081 B - Organochlorine Pesticides (GC)
Matrix: Solid Prep Type: TCLP
Percent Surrogate Recovery (Acceptance Limits)
DCBP2 TCX2
Lab Sample ID Client Sample ID (30-130) (30-130)
752-2248-1 VVVVTP-Q1 92 62
Surrogate Legend
DCBP = DCB Decachlorobiphenyl
TCX = Tetrachloro-m-xylene
Method: 8081 B - Organochlorine Pesticides (GC)
Matrix: Solid
Prep Type: TCLP
Percent Surrogate Recovery (Acceptance Limits)
DCBP1 TCX1
Lab Sample ID Client Sample ID (30-130) (30-130)
752-2248-1 MS VVVVTP-Q1 96 67
Page 13 of 40
Eurofins Raleigh
3/28/2023 (Rev. 1)

Surrogate Summary
Client: Hunt Environmental Associates Job ID: 752-2248-1
Project/Site: City of Lumberton- TCLP
Method: 8081 B - Organochlorine Pesticides (GC) (Continued)
Matrix: Solid Prep Type: TCLP
Percent Surrogate Recovery (Acceptance Limits)
DCBP1 TCx1
Lab Sample ID Client Sample ID (30-130) (30-130)
752-2248-1 MSD WWFP-Q1 93 66
752-2248-2 WTP 94 72
Surrogate Legend
DCBP = DCB Decachlorobiphenyl
TCX = Tetrachloro-m-xylene
Method: 8081 B - Organochlorine Pesticides (GC)
Matrix: Solid
DCBP1
Lab Sample ID Client Sample ID (30-130)
LB 680-763695/1-E Method Blank 102
Surrogate Legend
Prep Type: TCLP
Percent Surrogate Recovery (Acceptance Limits)
TCX2
(30-130)
DCBP = DCB Decachlorobiphenyl
LTCX = Tetrachloro-m-xylene
Method: 8151A - Herbicides (GC)
Matrix: Solid
DCPAA2
Lab Sample ID Client Sample ID
(26-137)
LB 680-764058/7-A Method Blank
90
LCS 680-764058/2-A Lab Control Sample
85
MB 680-764058/1-A Method Blank
89
Surrogate Legend
DCPAA = DCAA
Method: 8151A - Herbicides (GC)
Matrix: Solid
Lab Sample ID
752-2248-1
752-2248-2
752-2248-2 MS
752-2248-2 MSD
Surrogate Legend
DCPAA = DCAA
Client Sample ID
DCPAA2
(26-137)
WWTP-Q1
97
WTP
91
WTP
88
WTP
93
Prep Type: Total/NA
Percent Surrogate Recovery (Acceptance Limits)
Prep Type: TCLP
Percent Surrogate Recovery (Acceptance Limits)
Eurofins Raleigh
Page 14 of 40 3/28/2023 (Rev. 1)

QC Sample Results
Client: Hunt Environmental Associates
Job ID: 752-2248-1
Project/Site: City of Lumberton- TCLP
Method: 8260D - Volatile Organic
Compounds
by GC/MS
Lab Sample ID: MB 680-763978/8
Client Sample ID: Method
Blank
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 763978
MB MB
Analyte
Result Qualifier
RL
MDL
Unit
D Prepared Analyzed
Dil Fac
1,1-Dichloroethene
<0.00036
0.0010
0.00036
mg/L
02/19/23 14:24
1
1,2-Dichloroethane
<0.00050
0.0010
0.00050
mg/L
02/19/23 14:24
1
1,4-Dichlorobenzene
<0.00046
0.0010
0.00046
mg/L
02/19/23 14:24
1
Methyl Ethyl Ketone
<0.0034
0.010
0.0034
mg/L
02/19/23 14:24
1
Benzene
<0.00043
0.0010
0.00043
mg/L
02/19/23 14:24
1
Carbon tetrachloride
<0.00033
0.0010
0.00033
mg/L
02/19/23 14:24
1
Chlorobenzene
<0.00026
0.0010
0.00026
mg/L
02/19/23 14:24
1
Chloroform
<0.00050
0.0010
0.00050
mg/L
02/19/23 14:24
1
Hexachlorobutadiene
<0.0025
0.0050
0.0025
mg/L
02/19/23 14:24
1
Tetrachloroethylene
<0.00075
0.0010
0.00075
mg/L
02/19/23 14:24
1
Trichloroethylene
<0.00048
0.0010
0.00048
mg/L
02/19/23 14:24
1
Vinyl chloride
<0.00050
0.0010
0.00050
mg/L
02/19/23 14:24
1
MB MB
Surrogate
%Recovery Qualifier
Limits
Prepared Analyzed
Dil Fac
4-Bromofluorobenzene (Surr)
108
70 -130
02119123 14:24
1
Dibromofluoromethane (Surr)
100
70 -130
02119123 14:24
1
Toluene-d8 (Surr)
104
70 -130
02119123 14:24
1
1,2-Dichloroethane-d4 (Surr)
95
60-124
02119123 14:24
1
Lab Sample ID: LCS 680-763978/4
Client Sample ID: Lab Control Sample
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 763978
Spike
LCS LCS
%Rec
Analyte
Added
Result Qualifier
Unit
D %Rec
Limits
1,1-Dichloroethene
0.0500
0.0507
mg/L
101
70-130
1,2-Dichloroethane
0.0500
0.0505
mg/L
101
70 - 130
1,4-Dichlorobenzene
0.0500
0.0501
mg/L
100
70 - 130
Methyl Ethyl Ketone
0.250
0.214
mg/L
86
69 - 114
Benzene
0.0500
0.0502
mg/L
100
70 - 130
Carbon tetrachloride
0.0500
0.0509
mg/L
102
70 - 130
Chlorobenzene
0.0500
0.0507
mg/L
101
70 - 130
Chloroform
0.0500
0.0506
mg/L
101
70 - 130
Hexachlorobutadiene
0.0500
0.0494
mg/L
99
70 - 130
Tetrachloroethylene
0.0500
0.0495
mg/L
99
70 - 130
Trichloroethylene
0.0500
0.0509
mg/L
102
70 - 130
Vinyl chloride
0.0500
0.0486
mg/L
97
66 - 129
LCS LCS
Surrogate %Recovery Qualifier Limits
4-Bromofluorobenzene (Surr) 102 70- 130
Dibromofluoromethane (Surr) 97 70- 130
Toluene-d8 (Surr) 99 70 - 130
1,2-Dichloroethane-d4 (Surr) 93 60- 124
Eurofins Raleigh
Page 15 of 40 3/28/2023 (Rev. 1)

QC Sample Results
Client: Hunt Environmental Associates
Job ID:
752-2248-1
Project/Site: City of Lumberton- TCLP
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
Lab Sample ID: LCSD 680-763978/5
Client Sample
ID: Lab Control Sample Dup
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 763978
Spike
LCSD LCSD
%Rec
RPD
Analyte
Added
Result Qualifier Unit
D %Rec
Limits
RPD
Limit
1,1-Dichloroethene
0.0500
0.0503
mg/L
101
70-130
1
20
1,2-Dichloroethane
0.0500
0.0501
mg/L
100
70 - 130
1
50
1,4-Dichlorobenzene
0.0500
0.0503
mg/L
101
70 - 130
0
30
Methyl Ethyl Ketone
0.250
0.211
mg/L
84
69 - 114
2
30
Benzene
0.0500
0.0502
mg/L
100
70 - 130
0
30
Carbon tetrachloride
0.0500
0.0513
mg/L
103
70 - 130
1
30
Chlorobenzene
0.0500
0.0509
mg/L
102
70-130
0
30
Chloroform
0.0500
0.0501
mg/L
100
70 - 130
1
30
Hexachlorobutadiene
0.0500
0.0499
mg/L
100
70 - 130
1
20
Tetrachloroethylene
0.0500
0.0497
mg/L
99
70 - 130
0
30
Trichloroethylene
0.0500
0.0506
mg/L
101
70 - 130
1
30
Vinyl chloride
0.0500
0.0491
mg/L
98
66 - 129
1
30
LCSD LCSD
Surrogate %Recovery Qualifier Limits
4-Bromofluorobenzene (Surr) 103 70- 130
Dibromofluoromethane (Surr) 97 70- 130
Toluene-d8 (Surr) 100 70 - 130
1,2-Dichloroethane-d4 (Surr) 98 60- 124
Lab Sample ID: LB 680-763738/1-A
Client Sample ID: Method Blank
Matrix: Solid
Prep Type:
TCLP
Analysis Batch: 763978
LB LB
Analyte
Result Qualifier
RL
MDL
Unit
D Prepared Analyzed
Dil Fac
1,1-Dichloroethene
<0.0072
0.020
0.0072
mg/L
02/19/23 15:35
20
1,2-Dichloroethane
<0.010
0.020
0.010
mg/L
02/19/23 15:35
20
1,4-Dichlorobenzene
<0.0092
0.020
0.0092
mg/L
02/19/23 15:35
20
Methyl Ethyl Ketone
<0.068
0.20
0.068
mg/L
02/19/23 15:35
20
Benzene
<0.0086
0.020
0.0086
mg/L
02/19/23 15:35
20
Carbon tetrachloride
<0.0066
0.020
0.0066
mg/L
02/19/23 15:35
20
Chlorobenzene
<0.0052
0.020
0.0052
mg/L
02/19/23 15:35
20
Chloroform
<0.010
0.020
0.010
mg/L
02/19/23 15:35
20
Hexachlorobutadiene
<0.050
0.10
0.050
mg/L
02/19/23 15:35
20
Tetrachloroethylene
<0.015
0.020
0.015
mg/L
02/19/23 15:35
20
Trichloroethylene
<0.0096
0.020
0.0096
mg/L
02/19/23 15:35
20
Vinyl chloride
<0.010
0.020
0.010
mg/L
02/19/23 15:35
20
LB LB
Surrogate
%Recovery Qualifier
Limits
Prepared Analyzed
Dil Fac
4-Bromofluorobenzene(Surr)
109
70-130
02119123 15:35
20
Dibromofluoromethane(Surr)
100
70-130
02119123 15:35
20
Toluene-d8 (Surr)
106
70 -130
02119123 15:35
20
1,2-Dichloroethane-d4 (Surr)
96
60-124
02119123 15:35
20
Eurofins Raleigh
Page 16 of 40 3/28/2023 (Rev. 1)

QC Sample Results
Client: Hunt Environmental Associates
Job ID: 752-2248-1
Project/Site: City of Lumberton-
TCLP
Method: 8270E - Semivolatile
Organic Compounds (GC/MS)
Lab Sample ID: MB 680-763973/1-A
Client Sample ID: Method Blank
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 764133
Prep Batch: 763973
MB MB
Analyte
Result Qualifier
RL
MDL
Unit
D Prepared
Analyzed Dil Fac
1,4-Dichlorobenzene
<0.0032
0.010
0.0032
mg/L
02/19/23 07:59
02/20/23 15:06 1
Pyridine
<0.0074
0.050
0.0074
mg/L
02/19/23 07:59
02/20/23 15:06 1
Hexachlorobenzene
<0.0016
0.010
0.0016
mg/L
02/19/23 07:59
02/20/23 15:06 1
2,4-Dinitrotoluene
<0.0024
0.010
0.0024
mg/L
02/19/23 07:59
02/20/23 15:06 1
Hexachloroethane
<0.0036
0.010
0.0036
mg/L
02/19/23 07:59
02/20/23 15:06 1
Hexachlorobutadiene
<0.0040
0.010
0.0040
mg/L
02/19/23 07:59
02/20/23 15:06 1
Pentachlorophenol
<0.010
0.050
0.010
mg/L
02/19/23 07:59
02/20/23 15:06 1
2,4,6-Trichlorophenol
<0.0022
0.010
0.0022
mg/L
02/19/23 07:59
02/20/23 15:06 1
2,4,5-Trichlorophenol
<0.0032
0.010
0.0032
mg/L
02/19/23 07:59
02/20/23 15:06 1
Nitrobenzene
<0.0036
0.010
0.0036
mg/L
02/19/23 07:59
02/20/23 15:06 1
o-Cresol
<0.0018
0.010
0.0018
mg/L
02/19/23 07:59
02/20/23 15:06 1
m & p - Cresol
<0.0014
0.010
0.0014
mg/L
02/19/23 07:59
02/20/23 15:06 1
Cresol
<0.0018
0.010
0.0018
mg/L
02/19/23 07:59
02/20/23 15:06 1
MB MB
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed
Dil Fac
2, 4, 6-Tribromophenol (Surr)
71
30 -130
02119123 07:59
02120123 15:06
1
2-Fluorobiphenyl (Surr)
73
25 -130
02119123 07:59
02120123 15:06
1
2-Fluorophenol (Surr)
34
10 -130
02119123 07:59
02120123 15:06
1
Terphenyl-d14 (Surr)
110
35-131
02119123 07:59
02120123 15:06
1
Phenol-d5 (Surr)
23
10 -130
02119123 07:59
02120123 15:06
1
Nitrobenzene-d5 (Surr)
65
30 -130
02119123 07:59
02120123 15:06
1
Lab Sample ID: LCS 680-763973/2-A
Matrix: Solid
Analysis Batch: 764133
Analyte
1,4-Dichlorobenzene
Pyridine
Hexachlorobenzene
2,4-Dinitrotoluene
Hexachloroethane
Hexachlorobutadiene
Pentachlorophenol
2,4,6-Trichlorophenol
2,4,5-Trichlorophenol
Nitrobenzene
o-Cresol
m & p - Cresol
Cresol
Surrogate
2,4,6-Tribromophenol (Surr)
2-Fluorobiphenyl (Surr)
2-Fluorophenol (Surr)
Terphenyl-d14 (Surr)
Phenol-d5 (Surr)
Nitrobenzene-d5 (Surr)
LCS LCS
%Recovery Qualifier
84
76
35
104
25
75
Spike
Added
0.200
0.400
0.200
0.200
0.200
0.200
0.400
0.200
0.200
0.200
0.200
0.200
0.400
Limits
30-130
25-130
10-130
35-131
10-130
30-130
LCS LCS
Result Qualifier
0.136
0.183
0.175
0.196
0.129
0.146
0.386
0.190
0.180
0.152
0.109
0.103
0.212
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Prep Batch: 763973
% Rec
Unit
D %Rec
Limits
mg/L
68
13 - 130
mg/L
46
10 - 130
mg/L
88
30 - 130
mg/L
98
37 - 130
mg/L
65
12 - 130
mg/L
73
12 - 130
mg/L
97
24 - 130
mg/L
95
28 - 130
mg/L
90
26 - 130
mg/L
76
32 - 130
mg/L
54
21 - 130
mg/L
52
19 - 130
mg/L
53
20 - 130
Page 17 of 40
Eurofins Raleigh
3/28/2023 (Rev. 1)

QC Sample Results
Client: Hunt Environmental Associates
Job ID: 752-2248-1
Project/Site: City of Lumberton-
TCLP
Method: 8270E - Semivolatile
Organic Compounds (GC/MS)
Lab Sample ID: LB 680-763695/1-D
Client Sample ID: Method Blank
Matrix: Solid
Prep Type: TCLP
Analysis Batch: 764133
Prep Batch: 763973
LB LB
Analyte
Result Qualifier
RL
MDL
Unit
D Prepared
Analyzed Dil Fac
1,4-Dichlorobenzene
<0.016
0.050
0.016
mg/L
02/19/23 07:59
02/20/23 15:56 1
Pyridine
<0.037
0.25
0.037
mg/L
02/19/23 07:59
02/20/23 15:56 1
Hexachlorobenzene
<0.0080
0.050
0.0080
mg/L
02/19/23 07:59
02/20/23 15:56 1
2,4-Dinitrotoluene
<0.012
0.050
0.012
mg/L
02/19/23 07:59
02/20/23 15:56 1
Hexachloroethane
<0.018
0.050
0.018
mg/L
02/19/23 07:59
02/20/23 15:56 1
Hexachlorobutadiene
<0.020
0.050
0.020
mg/L
02/19/23 07:59
02/20/23 15:56 1
Pentachlorophenol
<0.050
0.25
0.050
mg/L
02/19/23 07:59
02/20/23 15:56 1
2,4,6-Trichlorophenol
<0.011
0.050
0.011
mg/L
02/19/23 07:59
02/20/23 15:56 1
2,4,5-Trichlorophenol
<0.016
0.050
0.016
mg/L
02/19/23 07:59
02/20/23 15:56 1
Nitrobenzene
<0.018
0.050
0.018
mg/L
02/19/23 07:59
02/20/23 15:56 1
o-Cresol
<0.0090
0.050
0.0090
mg/L
02/19/23 07:59
02/20/23 15:56 1
m & p - Cresol
<0.0070
0.050
0.0070
mg/L
02/19/23 07:59
02/20/23 15:56 1
Cresol
<0.0090
0.050
0.0090
mg/L
02/19/23 07:59
02/20/23 15:56 1
LB LB
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed Dil Fac
2, 4, 6-Tribromophenol (Surr)
75
30 -130
02119123 07:59
02120123 15:56 1
2-Fluorobiphenyl (Surr)
66
25 -130
02119123 07:59
02120123 15:56 1
2-Fluorophenol (Surr)
29
10 -130
02119123 07:59
02120123 15:56 1
Terphenyl-d14 (Surr)
105
35-131
02119123 07:59
02120123 15:56 1
Phenol-d5 (Surr)
19
10 -130
02119123 07:59
02120123 15:56 1
Nitrobenzene-d5 (Surr)
57
30 -130
02119123 07:59
02120123 15:56 1
Lab Sample ID: 752-2248-2 MS
Client
Sample ID: WTP
Matrix: Solid
Prep Type: TCLP
Analysis Batch: 764133
Prep Batch: 763973
Sample
Sample
Spike
MS MS
%Rec
Analyte
Result
Qualifier
Added
Result Qualifier
Unit
D %Rec
Limits
1,4-Dichlorobenzene
<0.016
1.00
0.654
mg/L
65
13-130
Pyridine
<0.037
2.00
0.874
mg/L
44
10-130
Hexachlorobenzene
<0.0080
1.00
0.858
mg/L
86
30-130
2,4-Dinitrotoluene
<0.012
1.00
0.969
mg/L
97
37 - 130
Hexachloroethane
<0.018
1.00
0.669
mg/L
67
12 - 130
Hexachlorobutadiene
<0.020
1.00
0.730
mg/L
73
12 - 130
Pentachlorophenol
<0.050
2.00
1.87
mg/L
94
24 - 130
2,4,6-Trichlorophenol
<0.011
1.00
0.950
mg/L
95
28 - 130
2,4,5-Trichlorophenol
<0.016
1.00
0.900
mg/L
90
26 - 130
Nitrobenzene
<0.018
1.00
0.763
mg/L
76
32 - 130
o-Cresol
<0.0090
1.00
0.542
mg/L
54
21 - 130
m & p - Cresol
<0.0070
1.00
0.507
mg/L
51
19 - 130
Cresol
<0.0090
2.00
1.05
mg/L
52
20 - 130
Surrogate
MS MS
%Recovery Qualifier
Limits
2, 4, 6-Tribromophenol (Surr)
81
30 - 130
2-Fluorobiphenyl (Surr)
76
25- 130
2-Fluorophenol (Surr)
33
10 - 130
Terphenyl-d14 (Surr)
100
35- 131
Phenol-d5 (Surr)
23
10 - 130
Nitrobenzene-d5 (Surr)
77
30 - 130
Eurofins Raleigh
Page 18 of 40 3/28/2023 (Rev. 1)

QC Sample Results
Client: Hunt Environmental Associates
Job ID: 752-2248-1
Project/Site: City of Lumberton-
TCLP
Method: 8270E - Semivolatile Organic Compounds (GC/MS)
Lab Sample ID: 752-2248-2 MSD
Client
Sample ID:
WTP
Matrix: Solid
Prep Type:
TCLP
Analysis Batch: 764133
Prep Batch: 763973
Sample Sample
Spike
MSD MSD
%Rec
RPD
Analyte
Result Qualifier
Added
Result Qualifier
Unit
D %Rec
Limits RPD
Limit
1,4-Dichlorobenzene
<0.016
1.00
0.607
mg/L
61
13 - 130 7
50
Pyridine
<0.037
2.00
0.840
mg/L
42
10-130 4
50
Hexachlorobenzene
<0.0080
1.00
0.876
mg/L
88
30-130 2
50
2,4-Dinitrotoluene
<0.012
1.00
0.973
mg/L
97
37 - 130 0
50
Hexachloroethane
<0.018
1.00
0.611
mg/L
61
12 - 130 9
50
Hexachlorobutadiene
<0.020
1.00
0.670
mg/L
67
12 - 130 9
50
Pentachlorophenol
<0.050
2.00
1.97
mg/L
99
24 - 130 5
50
2,4,6-Trichlorophenol
<0.011
1.00
0.933
mg/L
93
28 - 130 2
50
2,4,5-Trichlorophenol
<0.016
1.00
0.866
mg/L
87
26 - 130 4
50
Nitrobenzene
<0.018
1.00
0.693
mg/L
69
32 - 130 10
50
o-Cresol
<0.0090
1.00
0.488
mg/L
49
21 - 130 10
50
m & p - Cresol
<0.0070
1.00
0.475
mg/L
47
19 - 130 7
50
Cresol
<0.0090
2.00
0.963
mg/L
48
20 - 130 9
50
MSD MSD
Surrogate
%Recovery Qualifier
Limits
2, 4, 6-Tribromophenol (Surr)
83
30 - 130
2-Fluorobiphenyl (Surr)
72
25- 130
2-Fluorophenol (Surr)
31
10 - 130
Terphenyl-d14 (Surr)
103
35- 131
Phenol-d5 (Surr)
22
10 - 130
Nitrobenzene-d5 (Surr)
70
30 - 130
Method: 8081 B - Organochlorine Pesticides (GC)
Lab Sample ID: MB 680-763974/1-A
Client Sample ID: Method
Blank
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 764106
Prep Batch: 763974
MB MB
Analyte
Result Qualifier
RL
MDL
Unit
D Prepared
Analyzed
Dil Fac
Chlordane (technical)
<0.00016
0.00050
0.00016
mg/L
02/19/23 08:03
02/20/23 15:24
1
Endrin
<0.00000010
0.000050
0.0000001
mg/L
02/19/23 08:03
02/20/23 15:24
1
0
gamma-BHC (Lindane)
<0.00000010
0.000050
0.0000001
mg/L
02/19/23 08:03
02/20/23 15:24
1
0
Heptachlor
<0.00000010
0.000050
0.0000001
mg/L
02/19/23 08:03
02/20/23 15:24
1
0
Heptachlor epoxide
<0.00000020
0.000050
0.0000002
mg/L
02/19/23 08:03
02/20/23 15:24
1
0
Methoxychlor
<0.00000020
0.000050
0.0000002
mg/L
02/19/23 08:03
02/20/23 15:24
1
0
Toxaphene
<0.00032
0.0050
0.00032
mg/L
02/19/23 08:03
02/20/23 15:24
1
MB MB
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed
Dil Fac
DCB Decachlorobiphenyl
105
30 -130
02119123 08:03
02120123 15:24
1
Tetrachloro-m-xylene
76
30 -130
02119123 08:03
02120123 15:24
1
Eurofins Raleigh
Page 19 of 40 3/28/2023 (Rev. 1)

QC Sample Results
Client: Hunt Environmental Associates
Job ID: 752-2248-1
Project/Site: City of Lumberton- TCLP
Method: 8081 B - Organochlorine Pesticides (GC) (Continued)
Lab Sample ID: LCS 680-763974/2-A
Client Sample ID:
Lab Control Sample
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 764106
Prep Batch: 763974
Spike LCS LCS
%Rec
Analyte
Added Result Qualifier
Unit D %Rec
Limits
Endrin
0.0000400 0.0000388 J
mg/L 97
30 - 130
gamma-BHC (Lindane)
0.0000400 0.0000334 J
mg/L 83
30. 130
Heptachlor
0.0000400 0.0000388 J
mg/L 97
30. 130
Heptachlor epoxide
0.0000400 0.0000352 J
mg/L 88
30. 130
Methoxychlor
0.0000400 0.0000479 J
mg/L 120
30. 130
•
LCS LCS
Surrogate %Recovery Qualifier
Limits
DCB Decachlorobiphenyl 95
30- 130
Tetrachloro-m-xylene 60
30 - 130
Lab Sample ID: LB 680-763695/1-E
Client Sample ID: Method Blank
Matrix: Solid
Prep Type: TCLP
Analysis Batch: 764106
Prep Batch: 763974
LB LB
Analyte Result Qualifier RL MDL
Unit
D Prepared
Analyzed Dil Fac
Chlordane (technical) <0.0080
0.025 0.0080
mg/L
02/19/23 08:03
02/20/23 15:06 1
Endrin <0.0000050
0.0025 0.0000050
mg/L
02/19/23 08:03
02/20/23 15:06 1
gamma-BHC (Lindane) <0.0000050
0.0025 0.0000050
mg/L
02/19/23 08:03
02/20/23 15:06 1
Heptachlor <0.0000050
0.0025 0.0000050
mg/L
02/19/23 08:03
02/20/23 15:06 1
Heptachlor epoxide <0.000010
0.0025 0.000010
mg/L
02/19/23 08:03
02/20/23 15:06 1
Methoxychlor <0.000010
0.0025 0.000010
mg/L
02/19/23 08:03
02/20/23 15:06 1
Toxaphene <0.016
0.25 0.016
mg/L
02/19/23 08:03
02/20/23 15:06 1
LB LB
Surrogate %Recovery Qualifier Limits
Prepared
Analyzed Dil Fac
DCB Decachlorobiphenyl 102
30 -130
02119123 08:03
02120123 15:06 1
Tetrachloro-m-xylene 66
30 -130
02119123 08:03
02120123 15:06 1
Lab Sample ID: 752-2248-1 MS
Client Sample ID: WWTP-Q1
Matrix: Solid
Prep Type: TCLP
Analysis Batch: 764106
Prep Batch: 763974
Sample Sample
Spike
MS
MS
%Rec
Analyte
Result Qualifier
Added
Result
Qualifier
Unit
D %Rec
Limits
Endrin
<0.0000050
0.00200
0.00205
J
mg/L
103
30 - 130
gamma-BHC (Lindane)
<0.0000050
0.00200
0.00179
J
mg/L
89
30- 130
Heptachlor
<0.0000050
0.00200
0.00217
J
mg/L
109
30-130
Heptachlor epoxide
<0.000010
0.00200
0.00190
J
mg/L
95
30. 130
Methoxychlor
<0.000010
0.00200
0.00232
J
mg/L
116
30. 130
MS MS
Surrogate
%Recovery Qualifier
Limits
DCB Decachlorobiphenyl
96
30- 130
Tetrachloro-m-xylene
67
30 - 130
Lab Sample ID: 752-2248-1 MSD Client Sample ID: WWTP-Q1
Matrix: Solid Prep Type: TCLP
Analysis Batch: 764106 Prep Batch: 763974
Sample Sample Spike MSD MSD %Rec RPD
Analyte Result Qualifier Added Result Qualifier Unit D %Rec Limits RPD Limit
Endrin <0.0000050 0.00200 0.00213 J mg/L 107 30 - 330 4
Eurofins Raleigh
Page 20 of 40 3/28/2023 (Rev. 1)

QC Sample Results
Client: Hunt Environmental Associates
Project/Site: City of Lumberton- TCLP
Job ID: 752-2248-1
Method: 8081 B - Organochlorine Pesticides (GC) (Continued)
Lab Sample ID: 752-2248-1 MSD
Client Sample ID: WWTP-Q1
Matrix: Solid
Prep Type: TCLP
Analysis Batch: 764106
Prep Batch: 763974
Sample Sample
Spike
MSD MSD
%Rec RPD
Analyte Result Qualifier
Added
Result Qualifier
Unit
D %Rec
Limits RPD Limit
gamma-BHC (Lindane) <0.0000050
0.00200
0.00207 J
mg/L
103
30 - 130 15
Heptachlor <0.0000050
0.00200
0.00234 J
mg/L
117
30 -130 8
Heptachlor epoxide <0.000010
0.00200
0.00190 J
mg/L
95
30 -130 0
Methoxychlor <0.000010
0.00200
0.00256
mg/L
128
30 -130 10
MSD MSD
Surrogate %Recovery Qualifier
Limits
DCB Decachlorobiphenyl 93
30 - 130
Tetrachloro-m-xylene 66
30- 130
Method: 8151A - Herbicides (GC)
Lab Sample ID: LB 680-764058/7-A
Matrix: Solid
Analysis Batch: 764347
LB LB
Analyte Result Qualifier
RL MDL Unit
Client Sample ID: Method Blank
Prep Type: Total/NA
Prep Batch: 764058
D Prepared Analyzed Dil Fac
2,4-D
<0.0019
0.012 0.0019 mg/L
02/20/23 09:22
02/21/23 23:57 1
Silvex (2,4,5-TP)
<0.0010
0.0096 0.0010 mg/L
02/20/23 09:22
02/21/23 23:57 1
LB LB
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed Dil Fac
DCAA
90
26 -137
02120123 09:22
02121123 23:57 1
Lab Sample ID: MB 680-764058/1-A
Client Sample ID: Method Blank
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 764347
Prep Batch: 764058
MB MB
Analyte
Result Qualifier
RL MDL Unit
D Prepared
Analyzed Dil Fac
2,4-D
<0.00018
0.0011 0.00018 mg/L
02/20/23 09:22
02/22/23 00:18 1
Silvex (2,4,5-TP)
<0.000096
0.00088 0.000096 mg/L
02/20/23 09:22
02/22/23 00:18 1
MB MB
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed Dil Fac
DCAA
89
26 -137
02120123 09:22
02/22/23 00:18 1
Lab Sample ID: LCS 680-764058/2-A
Client Sample ID:
Lab Control Sample
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 764347
Prep Batch: 764058
Spike LCS LCS
%Rec
Analyte
Added Result Qualifier
Unit D %Rec
Limits
2,4-D
0.00640 0.00445
mg/L 70
21 -130
Silvex (2,4,5-TP)
0.00160 0.00121
mg/L 76
31 -144
LCS LCS
Surrogate
%Recovery Qualifier
Limits
DCAA
85
26-137
Eurofins Raleigh
Page 21 of 40 3/28/2023 (Rev. 1)

QC Sample Results
Client: Hunt Environmental Associates
Project/Site: City of Lumberton- TCLP
Job ID: 752-2248-1
Method: 8151A - Herbicides (GC) (Continued)
Lab Sample ID: 752-2248-2 MS Client Sample ID: WTP
Matrix: Solid Prep Type: TCLP
Analysis Batch: 764347 Prep Batch: 764058
Sample Sample Spike MS MS %Rec
Analyte Result Qualifier Added Result Qualifier Unit D %Rec Limits
2,4-D <0.0019 0.0650 0.0495 mg/L 76 21 - 147
Silvex (2,4,5-TP) <0.0010 0.0163 0.0136 mg/L 84 31 - 144
MS MS
Surrogate
%Recovery Qualifier
Limits
DCAA
88
26-137
•
Lab Sample ID: 752-2248-2 MSD
Client Sample ID: WTP
Matrix: Solid
Prep Type: TCLP
Analysis Batch: 764347
Prep Batch: 764058
Sample Sample
Spike
MSD MSD
%Rec RPD
Analyte
Result Qualifier
Added
Result Qualifier Unit
D %Rec Limits RPD Limit
2,4-D
<0.0019
0.0684
0.0542 mg/L
79 21 - 147 9 50
Silvex (2,4,5-TP)
<0.0010
0.0171
0.0158 mg/L
92 31 - 144 15 50
MSD MSD
Surrogate %Recovery Qualifier
Limits
DCAA 93
26-137
Method: 6010D - Metals (ICP)
Lab Sample ID: MB 680-763918/1-A
Client Sample ID: Method Blank
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 764151
Prep Batch: 763918
MB MB
Analyte Result Qualifier
RL
MDL
Unit
D Prepared
Analyzed Dil Fac
Arsenic <0.020
0.020
0.020
mg/L
02/17/2313:14
02/20/2313:19 1
Barium <0.10
0.10
0.10
mg/L
02/17/2313:14
02/20/2313:19 1
Cadmium <0.010
0.010
0.010
mg/L
02/17/2313:14
02/20/2313:19 1
Chromium <0.020
0.020
0.020
mg/L
02/17/2313:14
02/20/2313:19 1
Lead <0.020
0.020
0.020
mg/L
02/17/2313:14
02/20/2313:19 1
Selenium <0.050
0.050
0.050
mg/L
02/17/2313:14
02/20/2313:19 1
Silver <0.010
0.010
0.010
mg/L
02/17/2313:14
02/20/2313:19 1
Lab Sample ID: LCS 680-763918/2-A
Client Sample ID: Lab Control Sample
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 764151
Prep Batch: 763918
Spike
LCS LCS
%Rec
Analyte
Added
Result Qualifier
Unit
D %Rec
Limits
Arsenic
2.00
2.01
mg/L
100
80 - 120
Barium
2.00
2.11
mg/L
106
80 - 120
Cadmium
1.00
0.994
mg/L
99
80 - 120
Chromium
2.00
2.10
mg/L
105
80 - 120
Lead
10.1
10.2
mg/L
101
80 - 120
Selenium
2.00
1.96
mg/L
98
80 - 120
Silver
1.00
0.989
mg/L
99
80 - 120
Eurofins Raleigh
Page 22 of 40 3/28/2023 (Rev. 1)

QC Sample Results
Client: Hunt Environmental Associates
Job ID: 752-2248-1
Project/Site: City of Lumberton- TCLP
Method: 6010D - Metals (ICP) (Continued)
Lab Sample ID: LB 680-763695/1-C
Client Sample ID: Method Blank
Matrix: Solid
Prep Type: TCLP
Analysis Batch: 764151
Prep Batch: 763918
LB LB
Analyte
Result Qualifier
RL
MDL
Unit
D Prepared
Analyzed Dil Fac
Arsenic
<0.20
0.20
0.20
mg/L
02/17/2313:14
02/20/2313:30 1
Barium
<1.0
1.0
1.0
mg/L
02/17/2313:14
02/20/2313:30 1
Cadmium
<0.10
0.10
0.10
mg/L
02/17/2313:14
02/20/2313:30 1
Chromium
<0.20
0.20
0.20
mg/L
02/17/2313:14
02/20/2313:30 1
Lead
<0.20
0.20
0.20
mg/L
02/17/2313:14
02/20/2313:30 1
Selenium
<0.50
0.50
0.50
mg/L
02/17/2313:14
02/20/2313:30 1
Silver
<0.10
0.10
0.10
mg/L
02/17/2313:14
02/20/2313:30 1
Lab Sample ID: LB2 680-763695/4-C
Client Sample ID: Method Blank
Matrix: Solid
Prep Type: TCLP
Analysis Batch: 764151
Prep Batch: 763918
LB2 LB2
Analyte
Result Qualifier
RL
MDL
Unit
D Prepared
Analyzed Dil Fac
Arsenic
<0.20
0.20
0.20
mg/L
02/17/2313:14
02/20/2313:43 1
Barium
<1.0
1.0
1.0
mg/L
02/17/2313:14
02/20/2313:43 1
Cadmium
<0.10
0.10
0.10
mg/L
02/17/2313:14
02/20/2313:43 1
Chromium
<0.20
0.20
0.20
mg/L
02/17/2313:14
02/20/2313:43 1
Lead
<0.20
0.20
0.20
mg/L
02/17/2313:14
02/20/2313:43 1
Selenium
<0.50
0.50
0.50
mg/L
02/17/2313:14
02/20/2313:43 1
Silver
<0.10
0.10
0.10
mg/L
02/17/2313:14
02/20/2313:43 1
Lab Sample ID: 752-2248-1 MS
Client Sample ID: WWTP-Q1
Matrix: Solid
Prep Type: TCLP
Analysis Batch: 764151
Prep Batch: 763918
Sample
Sample
Spike
MS MS
%Rec
Analyte
Result
Qualifier
Added
Result Qualifier
Unit
D %Rec
Limits
Arsenic
<0.20
3.20
3.26
mg/L
102
75 - 125
Barium
<1.0
3.20
3.15
mg/L
99
75. 125
Cadmium
<0.10
1.60
1.67
mg/L
104
75. 125
Chromium
<0.20
1.60
1.70
mg/L
106
75 - 125
Lead
<0.20
1.60
1.70
mg/L
106
75 - 125
Selenium
<0.50
3.20
3.12
mg/L
97
75 - 125
Silver
<0.10
F1
1.60
0.291 F1
mg/L
18
75-125
Lab Sample ID: 752-2248-1 MSD
Client Sample ID: WWTP-Q1
Matrix: Solid
Prep Type: TCLP
Analysis Batch: 764151
Prep Batch: 763918
Sample
Sample
Spike
MSD MSD
%Rec RPD
Analyte
Result
Qualifier
Added
Result Qualifier
Unit
D %Rec
Limits RPD Limit
Arsenic
<0.20
3.20
3.14
mg/L
98
75 - 125 4 20
Barium
<1.0
3.20
3.04
mg/L
95
75 - 125 4 20
Cadmium
<0.10
1.60
1.59
mg/L
100
75 - 125 4 20
Chromium
<0.20
1.60
1.63
mg/L
102
75 - 125 4 20
Lead
<0.20
1.60
1.61
mg/L
101
75 - 125 5 20
Selenium
<0.50
3.20
2.96
mg/L
92
75-125 5 20
Silver
<0.10
F1
1.60
0.277 F1
mg/L
17
75. 125 5 20
Eurofins Raleigh
Page 23 of 40 3/28/2023 (Rev. 1)

QC Sample Results
Client: Hunt Environmental Associates
Job ID: 752-2248-1
Project/Site: City of Lumberton- TCLP
Method: 7470A - Mercury (CVAA)
Lab Sample ID: MB 680-764125/12-A
Client Sample ID: Method Blank
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 764337
Prep Batch: 764125
MB MB
Analyte Result Qualifier
RL MDL Unit
D Prepared Analyzed Dil Fac
Mercury <0.00020
0.00020 0.00020 mg/L
02/20/2312:38 02/21/2310:46 1
Lab Sample ID: LCS 680-764125/13-A
Client Sample ID: Lab Control Sample
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 764337
Prep Batch: 764125
Spike LCS LCS
%Rec
Analyte
Added Result Qualifier Unit
D %Rec Limits
Mercury
0.250 0.248 mg/L
99 80 -120
Lab Sample ID: LB 680-763695/1-F
Client Sample ID: Method Blank
Matrix: Solid
Prep Type: TCLP
Analysis Batch: 764337
Prep Batch: 764125
LB LB
Analyte Result Qualifier
RL MDL Unit
D Prepared Analyzed Dil Fac
Mercury <0.020
0.020 0.020 mg/L
02/20/2312:38 02/21/2310:53 1
Lab Sample ID: LB2 680-763695/4-D
Client Sample ID: Method Blank
Matrix: Solid
Prep Type: TCLP
Analysis Batch: 764337
Prep Batch: 764125
LB2 LB2
Analyte Result Qualifier
RL MDL Unit
D Prepared Analyzed Dil Fac
Mercury <0.020
0.020 0.020 mg/L
02/20/2312:38 02/21/2311:10 1
Lab Sample ID: 752-2248-1 MS
Client Sample ID: WWTP-Q1
Matrix: Solid
Prep Type: TCLP
Analysis Batch: 764337
Prep Batch: 764125
Sample Sample
Spike MS MS
%Rec
Analyte Result Qualifier
Added Result Qualifier Unit
D %Rec Limits
Mercury <0.020 F1 F2
0.0830 0.0646 F1 mg/L
78 80 - 120
Lab Sample ID: 752-2248-1 MSD
Client Sample ID: WWTP-Q1
Matrix: Solid
Prep Type: TCLP
Analysis Batch: 764337
Prep Batch: 764125
Sample Sample
Spike MSD MSD
%Rec RPD
Analyte Result Qualifier
Added Result Qualifier Unit
D %Rec Limits RPD Limit
Mercury <0.020 F1 F2
0.0830 0.0846 F2 mg/L
102 80 -120 27 20
Method: 1010B - Ignitability, Pensky-Martens
Closed -Cup Method
Lab Sample ID: MB 680-762640/1
Client Sample ID: Method Blank
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 762640
MB MB
Analyte Result Qualifier
RL MDL Unit
D Prepared Analyzed Dil Fac
Flashpoint >140
Degrees F
02/09/23 07:59 1
Eurofins Raleigh
Page 24 of 40 3/28/2023 (Rev. 1)

QC Sample Results
Client: Hunt Environmental Associates
Project/Site: City of Lumberton- TCLP
Job ID: 752-2248-1
Method: 1010B - Ignitability, Pensky-Martens Closed -Cup Method (Continued)
Lab Sample ID: LCS 680-762640/2 Client Sample ID: Lab Control Sample
Matrix: Water Prep Type: Total/NA
Analysis Batch: 762640
Spike
Analyte Added
Flashpoint 147
Lab Sample ID: LCSD 680-762640/5
Matrix: Water
Analysis Batch: 762640
Spike
Analyte Added
Flashpoint 147
Method: 335.4-1993 111.0 - Cyanide, Total
Lab Sample ID: MB 680-762486/1-A
Matrix: Solid
Analysis Batch: 762691
LCS LCS %Rec
Result Qualifier Unit D %Rec Limits
147 Degrees F 100 96 - 106
Client Sample ID: Lab Control Sample Dup
Prep Type: Total/NA
LCSD LCSD %Rec RPD
Result Qualifier Unit D %Rec Limits RPD Limit
147 Degrees F 100 96 - 106 0
Client Sample ID: Method Blank
Prep Type: Total/NA
Prep Batch: 762486
MB MB
Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac
Cyanide, Total <0.028 0.11 0.028 mg/Kg 02/08/23 10:11 02/09/23 11:08 1
Lab Sample ID: LCS 680-762486/2-A Client Sample ID: Lab Control Sample
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 762691 Prep Batch: 762486
Spike LCS LCS %Rec
Analyte Added Result Qualifier Unit D %Rec Limits
Cyanide, Total 0.600 0.658 mg/Kg 110 90 - 110
Method: 9034 - Sulfide, Acid Soluble and Insoluble (Titrimetric)
Lab Sample ID: MB 680-762213/1-A Client Sample ID: Method Blank
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 762259 Prep Batch: 762213
MB MB
Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac
Sulfide <60 60 60 mg/Kg 02/07/23 07:08 02/07/23 09:31 1
Lab Sample ID: LCS 680-762213/2-A Client Sample ID: Lab Control Sample
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 762259 Prep Batch: 762213
Spike LCS LCS %Rec
Analyte Added Result Qualifier Unit D %Rec Limits
Sulfide 1250 797 mg/Kg 64 50 - 150
Lab Sample ID: LCSD 680-762213/3-A Client Sample ID: Lab Control Sample Dup
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 762259 Prep Batch: 762213
Spike LCSD LCSD %Rec RPD
Analyte Added Result Qualifier Unit D %Rec Limits RPD Limit
Sulfide 1210 973 mg/Kg 80 50 - 150 20 50
Eurofins Raleigh
Page 25 of 40 3/28/2023 (Rev. 1)

QC Sample Results
Client: Hunt Environmental Associates
Project/Site: City of Lumberton- TCLP
Method: 9045C - pH
Lab Sample ID: LCS 680-763776/4
Matrix: Solid
Analysis Batch: 763776
Spike
Analyte Added
soil pH measured in water at deg 7.01
C
Job ID: 752-2248-1
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
LCS LCS
Result Qualifier Unit
7.0 Su
% Rec
D %Rec Limits
100 79-126
Eurofins Raleigh
Page 26 of 40 3/28/2023 (Rev. 1)

QC Association Summary
Client: Hunt Environmental Associates
Project/Site: City of Lumberton- TCLP
GC/MS VOA
Leach Batch: 763738
Lab Sample ID
Client Sample ID
752-2248-1
VMVVTP-Q1
752-2248-2
VVTP
LB 680-763738/1-A
Method Blank
Analysis Batch: 763978
Prep Type
Matrix
Method
TCLP
Solid
1311
TCLP
Solid
1311
TCLP
Solid
1311
Job ID: 752-2248-1
Prep Batch
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
752-2248-1
VVVVTP-Q1
TCLP
Solid
8260D
763738
752-2248-2
VVTP
TCLP
Solid
8260D
763738
LB 680-763738/1-A
Method Blank
TCLP
Solid
8260D
763738
MB 680-763978/8
Method Blank
Total/NA
Solid
8260D
LCS 680-763978/4
Lab Control Sample
Total/NA
Solid
8260D
LCSD 680-763978/5
Lab Control Sample Dup
Total/NA
Solid
8260D
GC/MS Semi VOA
Leach Batch: 763695
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method Prep Batch
752-2248-1
VVVVTP-Q1
TCLP
Solid
1311
752-2248-2
VVTP
TCLP
Solid
1311
LB 680-763695/1-D
Method Blank
TCLP
Solid
1311
752-2248-2 MS
VVTP
TCLP
Solid
1311
752-2248-2 MSD
VVTP
TCLP
Solid
1311
Prep Batch: 763973
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
752-2248-1
VVVVTP-Q1
TCLP
Solid
3510C
763695
752-2248-2
VVTP
TCLP
Solid
3510C
763695
LB 680-763695/1-D
Method Blank
TCLP
Solid
3510C
763695
MB 680-763973/1-A
Method Blank
Total/NA
Solid
3510C
LCS 680-763973/2-A
Lab Control Sample
Total/NA
Solid
3510C
752-2248-2 MS
VVTP
TCLP
Solid
3510C
763695
752-2248-2 MSD
VVTP
TCLP
Solid
3510C
763695
Analysis Batch: 764133
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
752-2248-1
VVVVTP-Q1
TCLP
Solid
8270E
763973
752-2248-2
VVTP
TCLP
Solid
8270E
763973
LB 680-763695/1-D
Method Blank
TCLP
Solid
8270E
763973
MB 680-763973/1-A
Method Blank
Total/NA
Solid
8270E
763973
LCS 680-763973/2-A
Lab Control Sample
Total/NA
Solid
8270E
763973
752-2248-2 MS
VVTP
TCLP
Solid
8270E
763973
752-2248-2 MSD
VVTP
TCLP
Solid
8270E
763973
GC Semi VOA
Leach Batch: 763695
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method Prep Batch
752-2248-1
VVVVTP-Q1
TCLP
Solid
1311
752-2248-2
VVTP
TCLP
Solid
1311
LB 680-763695/1-E
Method Blank
TCLP
Solid
1311
752-2248-1 MS
VVVVTP-Q1
TCLP
Solid
1311
752-2248-1 MSD
VVVVTP-Q1
TCLP
Solid
1311
Page 27 of 40
Eurofins Raleigh
3/28/2023 (Rev. 1)

QC Association Summary
Client: Hunt Environmental Associates
Project/Site: City of Lumberton- TCLP
Job ID: 752-2248-1
GC Semi VOA (Continued)
Leach Batch: 763695 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
752-2248-2 MS WTP TCLP Solid 1311
752-2248-2 MSD WTP TCLP Solid 1311
Prep Batch: 763974
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
752-2248-1
WWFP-Q1
TCLP
Solid
3510C
763695
752-2248-2
WTP
TCLP
Solid
3510C
763695
LB 680-763695/1-E
Method Blank
TCLP
Solid
3510C
763695
MB 680-763974/1-A
Method Blank
Total/NA
Solid
3510C
LCS 680-763974/2-A
Lab Control Sample
Total/NA
Solid
3510C
752-2248-1 MS
WWFP-Q1
TCLP
Solid
3510C
763695
752-2248-1 MSD
WWFP-Q1
TCLP
Solid
3510C
763695
Prep Batch: 764058
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
752-2248-1
WWFP-Q1
TCLP
Solid
8151A
763695
752-2248-2
WTP
TCLP
Solid
8151A
763695
LB 680-764058/7-A
Method Blank
Total/NA
Solid
8151A
MB 680-764058/1-A
Method Blank
Total/NA
Solid
8151A
LCS 680-764058/2-A
Lab Control Sample
Total/NA
Solid
8151A
752-2248-2 MS
WTP
TCLP
Solid
8151A
763695
752-2248-2 MSD
WTP
TCLP
Solid
8151A
763695
Analysis Batch: 764106
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
752-2248-1
WWFP-Q1
TCLP
Solid
8081 B
763974
752-2248-2
WTP
TCLP
Solid
8081 B
763974
LB 680-763695/1-E
Method Blank
TCLP
Solid
8081 B
763974
MB 680-763974/1-A
Method Blank
Total/NA
Solid
8081 B
763974
LCS 680-763974/2-A
Lab Control Sample
Total/NA
Solid
8081 B
763974
752-2248-1 MS
WWFP-Q1
TCLP
Solid
8081 B
763974
752-2248-1 MSD
WWFP-Q1
TCLP
Solid
8081 B
763974
Analysis Batch: 764347
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
752-2248-1
WWFP-Q1
TCLP
Solid
8151A
764058
752-2248-2
WTP
TCLP
Solid
8151A
764058
LB 680-764058/7-A
Method Blank
Total/NA
Solid
8151A
764058
MB 680-764058/1-A
Method Blank
Total/NA
Solid
8151A
764058
LCS 680-764058/2-A
Lab Control Sample
Total/NA
Solid
8151A
764058
752-2248-2 MS
WTP
TCLP
Solid
8151A
764058
752-2248-2 MSD
WTP
TCLP
Solid
8151A
764058
Metals
Leach Batch: 763695
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method Prep Batch
752-2248-1
WWTP-Q1
TCLP
Solid
1311
752-2248-2
WTP
TCLP
Solid
1311
LB 680-763695/1-C
Method Blank
TCLP
Solid
1311
LB 680-763695/1-F
Method Blank
TCLP
Solid
1311
Eurofins Raleigh
Page 28 of 40 3/28/2023 (Rev. 1)

QC Association Summary
Client: Hunt Environmental Associates
Project/Site: City of Lumberton- TCLP
Job ID: 752-2248-1
Metals (Continued)
Leach Batch: 763695 (Continued)
Lab Sample ID Client Sample ID
Prep Type
Matrix
Method Prep Batch
LB2 680-763695/4-C Method Blank
TCLP
Solid
1311
LB2 680-763695/4-D Method Blank
TCLP
Solid
1311
752-2248-1 MS WWFP-Q1
TCLP
Solid
1311
752-2248-1 MSD WWFP-Q1
TCLP
Solid
1311
Prep Batch: 763918
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
752-2248-1
WWFP-Q1
TCLP
Solid
3010A
763695
752-2248-2
WTP
TCLP
Solid
3010A
763695
LB 680-763695/1-C
Method Blank
TCLP
Solid
3010A
763695
LB2 680-763695/4-C
Method Blank
TCLP
Solid
3010A
763695
MB 680-763918/1-A
Method Blank
Total/NA
Solid
3010A
LCS 680-763918/2-A
Lab Control Sample
Total/NA
Solid
3010A
752-2248-1 MS
WWFP-Q1
TCLP
Solid
3010A
763695
752-2248-1 MSD
WWFP-Q1
TCLP
Solid
3010A
763695
Prep Batch: 764125
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
752-2248-1
WWFP-Q1
TCLP
Solid
7470A
763695
752-2248-2
WTP
TCLP
Solid
7470A
763695
LB 680-763695/1-F
Method Blank
TCLP
Solid
7470A
763695
LB2 680-763695/4-D
Method Blank
TCLP
Solid
7470A
763695
MB 680-764125/12-A
Method Blank
Total/NA
Solid
7470A
LCS 680-764125/13-A
Lab Control Sample
Total/NA
Solid
7470A
752-2248-1 MS
WWFP-Q1
TCLP
Solid
7470A
763695
752-2248-1 MSD
WWFP-Q1
TCLP
Solid
7470A
763695
Analysis Batch: 764151
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
752-2248-1
WWFP-Q1
TCLP
Solid
6010D
763918
752-2248-2
WTP
TCLP
Solid
6010D
763918
LB 680-763695/1-C
Method Blank
TCLP
Solid
6010D
763918
LB2 680-763695/4-C
Method Blank
TCLP
Solid
6010D
763918
MB 680-763918/1-A
Method Blank
Total/NA
Solid
6010D
763918
LCS 680-763918/2-A
Lab Control Sample
Total/NA
Solid
6010D
763918
752-2248-1 MS
WWFP-Q1
TCLP
Solid
6010D
763918
752-2248-1 MSD
WWFP-Q1
TCLP
Solid
6010D
763918
Analysis Batch: 764337
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
752-2248-1
WWFP-Q1
TCLP
Solid
7470A
764125
752-2248-2
WTP
TCLP
Solid
7470A
764125
LB 680-763695/1-F
Method Blank
TCLP
Solid
7470A
764125
LB2 680-763695/4-D
Method Blank
TCLP
Solid
7470A
764125
MB 680-764125/12-A
Method Blank
Total/NA
Solid
7470A
764125
LCS 680-764125/13-A
Lab Control Sample
Total/NA
Solid
7470A
764125
752-2248-1 MS
WWFP-Q1
TCLP
Solid
7470A
764125
752-2248-1 MSD
WWFP-Q1
TCLP
Solid
7470A
764125
Eurofins Raleigh
Page 29 of 40 3/28/2023 (Rev. 1)

QC Association Summary
Client: Hunt Environmental Associates
Project/Site: City of Lumberton- TCLP
Job ID: 752-2248-1
General Chemistry
Analysis Batch: 762190
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
752-2248-1 WWTP-Q1 Total/NA Solid Moisture
752-2248-2 WTP Total/NA Solid Moisture
Prep Batch: 762213
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method Prep Batch
752-2248-1
WWTP-Q1
Total/NA
Solid
9030B
752-2248-2
WTP
Total/NA
Solid
9030B
MB 680-762213/1-A
Method Blank
Total/NA
Solid
9030B
LCS 680-762213/2-A
Lab Control Sample
Total/NA
Solid
9030B
LCSD 680-762213/3-A
Lab Control Sample Dup
Total/NA
Solid
9030B n
Analysis Batch: 762259
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
752-2248-1
WWFP-Q1
Total/NA
Solid
9034
762213
752-2248-2
WTP
Total/NA
Solid
9034
762213
MB 680-762213/1-A
Method Blank
Total/NA
Solid
9034
762213
LCS 680-762213/2-A
Lab Control Sample
Total/NA
Solid
9034
762213
LCSD 680-762213/3-A
Lab Control Sample Dup
Total/NA
Solid
9034
762213
Prep Batch: 762486
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method Prep Batch
752-2248-1
WWFP-Q1
Total/NA
Solid
Distill/CN
752-2248-2
WTP
Total/NA
Solid
Distill/CN
MB 680-762486/1-A
Method Blank
Total/NA
Solid
Distill/CN
LCS 680-762486/2-A
Lab Control Sample
Total/NA
Solid
Distill/CN
Analysis Batch: 762640
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method Prep Batch
752-2248-3
WTP-Q1
Total/NA
Water
1010B
752-2248-4
WTP
Total/NA
Water
1010B
MB 680-762640/1
Method Blank
Total/NA
Water
1010B
LCS 680-762640/2
Lab Control Sample
Total/NA
Water
1010B
LCSD 680-762640/5
Lab Control Sample Dup
Total/NA
Water
1010B
Analysis Batch: 762691
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
752-2248-1
WWTP-Q1
Total/NA
Solid
335.4-1993 R1.0
762486
752-2248-2
WTP
Total/NA
Solid
335.4-1993 R1.0
762486
MB 680-762486/1-A
Method Blank
Total/NA
Solid
335.4-1993 R1.0
762486
LCS 680-762486/2-A
Lab Control Sample
Total/NA
Solid
335.4-1993 R1.0
762486
Analysis Batch: 763776
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
752-2248-1
WWFP-Q1
Total/NA
Solid
9045C
752-2248-2
WTP
Total/NA
Solid
9045C
LCS 680-763776/4
Lab Control Sample
Total/NA
Solid
9045C
Eurofins Raleigh
Page 30 of 40 3/28/2023 (Rev. 1)

Lab Chronicle
Client: Hunt Environmental Associates
Project/Site: City of Lumberton- TCLP
Job ID: 752-2248-1
Client Sample ID: WWTP-Q1 Lab Sample ID: 752-2248-1
Date Collected: 02/02/23 11:30 Matrix: Solid
Date Received: 02/03/23 10:46
Prep Type
Batch
Type
Batch
Method
Dilution
Run Factor
Batch
Number Analyst
Lab
Prepared
or Analyzed
TCLP
Leach
1311
763738
KF
EET SAV
02/16/23 15:53
TCLP
Analysis
8260D
20
763978
UI
EET SAV
02/19/23 20:48
TCLP
Leach
1311
763695
KF
EET SAV
02/16/23 15:53
TCLP
Prep
3510C
763973
MR
EET SAV
02/19/23 07:59
TCLP
Analysis
8270E
1
764133
OK
EET SAV
02/20/23 18:04
TCLP
Leach
1311
763695
KF
EET SAV
02/16/23 15:53
TCLP
Prep
3510C
763974
MR
EET SAV
02/19/23 08:03
TCLP
Analysis
8081 B
1
764106
JCK
EET SAV
02/20/23 17:32
TCLP
Leach
1311
763695
KF
EET SAV
02/16/23 15:53
TCLP
Prep
8151A
764058
KD
EET SAV
02/20/23 09:22
TCLP
Analysis
8151A
1
764347
JCK
EET SAV
02/22/23 02:06
TCLP
Leach
1311
763695
KF
EET SAV
02/16/23 15:53
TCLP
Prep
3010A
763918
RR
EET SAV
02/17/23 13:14
TCLP
Analysis
6010D
1
764151
BCB
EET SAV
02/20/23 13:32
TCLP
Leach
1311
763695
KF
EET SAV
02/16/23 15:53
TCLP
Prep
7470A
764125
JKL
EET SAV
02/20/23 12:38
TCLP
Analysis
7470A
1
764337
BJB
EET SAV
02/21/23 10:56
Total/NA
Analysis
9045C
1
763776
SM
EET SAV
02/16/23 14:42
Total/NA
Analysis
Moisture
1
762190
TD
EET SAV
02/06/23 20:36
Client Sample ID: WWTP-Q1 Lab Sample ID: 752-2248-1
Date Collected: 02/02/23 11:30 Matrix: Solid
Date Received: 02/03/23 10:46 Percent Solids: 2.9
Prep Type
Batch
Type
Batch
Method
Dilution
Run Factor
Batch
Number Analyst
Lab
Prepared
or Analyzed
Total/NA
Prep
Distill/CN
762486 JAS
EET SAV
02/08/23 10:11
Total/NA
Analysis
335.4-1993 R1.0
1
762691 JAS
EET SAV
02/09/23 10:31
Total/NA
Prep
9030B
762213 JAS
EET SAV
02/07/23 07:08
Total/NA
Analysis
9034
1
762259 JAS
EET SAV
02/07/23 09:31
Client Sample ID: WTP
Date Collected:
02/02/23 12:00
Date Received: 02/03/23 10:46
Batch
Batch
Prep Type
Type
Method
TCLP
Leach
1311
TCLP
Analysis
8260D
TCLP
Leach
1311
TCLP
Prep
3510C
TCLP
Analysis
8270E
TCLP
Leach
1311
TCLP
Prep
3510C
TCLP
Analysis
8081 B
TCLP
Leach
1311
TCLP
Prep
8151A
TCLP
Analysis
8151A
Lab Sample ID: 752-2248-2
Matrix: Solid
Dilution
Run Factor
Batch
Number Analyst
Lab
Prepared
or Analyzed
763738
KF
EET SAV
02/16/23 15:53
20
763978
UI
EET SAV
02/19/23 21:07
763695
KF
EET SAV
02/16/23 15:53
763973
MR
EET SAV
02/19/23 07:59
1
764133
OK
EET SAV
02/20/23 17:38
763695
KF
EET SAV
02/16/23 15:53
763974
MR
EET SAV
02/19/23 08:03
1
764106
JCK
EET SAV
02/20/23 17:51
763695
KF
EET SAV
02/16/23 15:53
764058
KD
EET SAV
02/20/23 09:22
1
764347
JCK
EET SAV
02/22/23 01:01
Eurofins Raleigh
Page 31 of 40 3/28/2023 (Rev. 1)

Lab Chronicle
Client: Hunt Environmental Associates
Job ID: 752-2248-1
Project/Site: City of Lumberton- TCLP
Client Sample ID: WTP
Lab Sample ID: 752-2248-2
Date Collected: 02/02/23 12:00
Matrix: Solid
Date Received: 02/03/23 10:46
Batch Batch
Dilution
Batch
Prepared
Prep Type Type Method
Run
Factor
Number
Analyst
Lab or Analyzed
TCLP Leach 1311
763695
KF
EET SAV 02/16/23 15:53
TCLP Prep 3010A
763918
RR
EET SAV 02/17/23 13:14
TCLP Analysis 6010D
1
764151
BCB
EET SAV 02/20/23 13:40
TCLP Leach 1311
763695
KF
EET SAV 02/16/23 15:53
TCLP Prep 7470A
764125
JKL
EET SAV 02/20/23 12:38
TCLP Analysis 7470A
1
764337
BJB
EET SAV 02/21/23 11:07
Total/NA Analysis 9045C
1
763776
SM
EET SAV 02/16/23 14:42
Total/NA Analysis Moisture
1
762190
TD
EET SAV 02/06/23 20:36
Client Sample ID: WTP
Lab Sample ID: 752-2248-2 ml
Date Collected: 02/02/23 12:00
Matrix: Solid
Date Received: 02/03/23 10:46
Percent Solids: 2.0
Batch Batch
Dilution
Batch
Prepared
Prep Type Type Method
Run
Factor
Number
Analyst
Lab or Analyzed
Total/NA Prep Distill/CN
762486
JAS
EET SAV 02/08/23 10:11
Total/NA Analysis 335.4-1993 R1.0
1
762691
JAS
EET SAV 02/09/23 11:24
Total/NA Prep 9030B
762213
JAS
EET SAV 02/07/23 07:08
Total/NA Analysis 9034
1
762259
JAS
EET SAV 02/07/23 09:31
Client Sample ID: WTP-Q1
Lab Sample ID: 752-2248-3
Date Collected: 02/02/23 11:30
Matrix: Water
Date Received: 02/03/23 10:46
Batch Batch
Dilution
Batch
Prepared
Prep Type Type Method
Run
Factor
Number
Analyst
Lab or Analyzed
Total/NA Analysis 1010B
1
762640
AS
EET SAV 02/09/23 10:00
Client Sample ID: WTP
Lab Sample ID: 752-2248-4
Date Collected: 02/02/23 12:00
Matrix: Water
Date Received: 02/03/23 10:46
Batch Batch
Dilution
Batch
Prepared
Prep Type Type Method
Run
Factor
Number
Analyst
Lab or Analyzed
Total/NA Analysis 1010B
1
762640
AS
EET SAV 02/09/23 10:45
Laboratory References:
EET SAV = Eurofins Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL [phone]
Eurofins Raleigh
Page 32 of 40 3/28/2023 (Rev. 1)

Accreditation/Certification Summary
Client: Hunt Environmental Associates Job ID: 752-2248-1
Project/Site: City of Lumberton- TCLP
Laboratory: Eurofins Savannah
Unless otherwise noted, all analytes for this laboratory were covered under each accreditation/certification below.
Authority Program Identification Number Expiration Date
North Carolina (WW/SW) State 269 12-31-23
The following analytes are included in this report, but the laboratory is not certified by the governing authority. This list may include analytes for which
the agency does not offer certification.
Analysis Method
Prep Method
Matrix
Analyte
1010B
Water
Flashpoint
335.4-1993 R1.0
Distill/CN
Solid
Cyanide, Total
7470A
7470A
Solid
Mercury
8270E
3510C
Solid
Cresol
9045C
Solid
soil pH measured in water at deg C
9045C
Solid
Temperature
Moisture
Solid
Percent Moisture
Moisture
Solid
Percent Solids
Eurofins Raleigh
Page 33 of 40 3/28/2023 (Rev. 1)

Method Summary
Client: Hunt Environmental Associates
Project/Site: City of Lumberton- TCLP
Job ID: 752-2248-1
Method
Method Description
Protocol
Laboratory
8260D
Volatile Organic Compounds by GC/MS
SW846
EET SAV
8270E
Semivolatile Organic Compounds (GC/MS)
SW846
EET SAV
8081 B
Organochlorine Pesticides (GC)
SW846
EET SAV
8151A
Herbicides (GC)
SW846
EET SAV
6010D
Metals (ICP)
SW846
EET SAV
7470A
Mercury (CVAA)
SW846
EET SAV
1010B
Ignitability, Pensky-Martens Closed -Cup Method
SW846
EET SAV
335.4-1993 R1.0
Cyanide, Total
MCAWW
EET SAV
9034
Sulfide, Acid Soluble and Insoluble (Titrimetric)
SW846
EET SAV
9045C
pH
SW846
EET SAV
Moisture
Percent Moisture
EPA
EET SAV
1311
TCLP Extraction
SW846
EET SAV
3010A
Preparation, Total Metals
SW846
EET SAV
3510C
Liquid -Liquid Extraction (Separatory Funnel)
SW846
EET SAV
5030B
Purge and Trap
SW846
EET SAV
7470A
Preparation, Mercury
SW846
EET SAV
8151A
Extraction (Herbicides)
SW846
EET SAV
9030B
Sulfide, Distillation (Acid Soluble and Insoluble)
SW846
EET SAV
Distill/CN
Distillation, Cyanide
None
EET SAV
Protocol References:
EPA = US Environmental Protection Agency
MCAWW = "Methods For Chemical Analysis Of Water And Wastes", EPA-600/4-79-020, March 1983 And Subsequent Revisions.
None = None
SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.
Laboratory References:
EET SAV = Eurofins Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL [phone]
Eurofins Raleigh
Page 34 of 40 3/28/2023 (Rev. 1)

Sample Summary
Client: Hunt Environmental Associates
Project/Site: City of Lumberton- TCLP
Lab Sample ID
Client Sample ID
Matrix
Collected
Received
752-2248-1
WWFP-Q1
Solid
02/02/2311:30
02/03/2310:46
752-2248-2
WTP
Solid
02/02/2312:00
02/03/2310:46
752-2248-3
WFP-Q1
Water
02/02/2311:30
02/03/2310:46
752-2248-4
WTP
Water
02/02/2312:00
02/03/2310:46
Job ID: 752-2248-1
Page 35 of 40 )

Eurofins Raleigh
102-A Woodwinds Industrial Court Chain of Custody Record tiff eurofins
Cary, NC 27511 Environment Testing
Phone [phone]
Sampler
Lab PM
Carrier Tracking No(s).
COC No:
Client Information
CAV
Franz, Stephanie
752-3773-577 1
Client Contact:
Phone:
E-Mail:
State of Odgim
Page,
Cody Hunt
Stephanie [e-mail] com
Page 1 of 1
Company'
PWSID'
Job #:
Hunt Environmental Associates
Analysis Requested
Address.
Due Date Requested
�: _5
Preservation Codes:
3330 Saddletree Rd
s
-'-- :
M - Hexane
A - HCL N - None
B -NaOH
City
TAT Requested (days):
Lumberton
71
-:
r y •,
It
0-AsNaO2
C - Zn Acetate p _ Na204S
D -Nitric Acid
E - NaHSO4 Q - Na2S03
State, Zip:
'28360
Compliance Project: 0 Yes A No
iv
NC,
�'•
•+%;
F - McOH R - Na2S203
G - gmchlor S - H2SO4 .
T-TSP Dodecahydrate
Phone: C
It
PO #:
-
Purchase Order not required,o.
2i
o
H -Ascorbic Acid
I -Ice U -Acetone
V -
Email.
WO #:
m2hunt22 @gma11 com
m
N
d
G
752-2248 COC
�`
m
J - DI Water
W- pH 4-
K-EDTA
Trtzma
L - EDA
Project Name:
Project #:
TCLP
75201362
m
ro
m
a
,_;
Z - other (specify)
Other
Site T
SSOW#:
is
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Sample Identification
Sample Date
Time
G= rab)
aT-T%su%A=a.
LL
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Special Instructions/Note:
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N
N.
N
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Possible Hazard Identffication
Sample Disposal (A fee may be assessed if samples are retained longer than 1 month)
do Non -Hazard = Flammable Skin Irritant Poison 8 Unknown Radiological
O Retum To Client 11 Disposal By Lab Archive For Months
Deliverable Requested I, II, III, IV, Other (specify)
Special Instructions/QC Requirements
Empty Kit Relinquished by Date Time. Method of shipment:
Relinquished by
Daten'ime' t
Company F .
Received by,
Daterrime,Company
ll 21
Relinquished by
Daterrime:
Company
Received by
Date/Time:L
Company
Relinquished by
Daterrime:
Company
Received by,
Daterrime:
Company
Custody Seals Intact
Custody Seal No
Cooler Temperature(s) °C and Other Remarks 7-7
A Yes A No
C�
Ver 06/08/2021

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kaleigh
102-A Woodwinds Industrial Court Chain of CustodyRecord eurofsns
Cary, NC 27511' . ! En =rcnr eat T=� tsng
Phone: [phone]
Sampler
Lab PM
Carrier Tracking No(s).
COC No:
Client Information Sub Contract Lab
Franz, Stephanie
752-161 1
Client Contact
Phone:
E-Mail:
State of Origin-
Page
Shipping/Receiving
stephanie [e-mail] coin
North Carolina
Page 1 of 1
Company
Accreditation Required (See note)
Job #
Eurofins Environment Testing Southeast,
State - North Carolina (VWV/SW)
752-2248-1
Address:
Due Date Requested-
Preservation Codes
5102 LaRoche Avenue,
2/1612023
Analysis
Requested
A HCL M Hexane
B NaOH N None
City
TAT Requested (days)
`.
Savannah
--'
0 AsNaO2
C Zn Acetate p Na204S
D -Nitric Acid O Na2SO3
State Zip
GA, 31404
�-
E - NaHSO4 R Na2S203
F - McOHG Amchlor S H2SO4
Phone-
PO #�
912-354-7858 Te! -- Fax
( ) 9123520165 ) (
T- TSP Dodephydrate
H Ascorbic Acid
ice U Acetone
Email
WO #
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DI Water V W pH 4-pH 4- 5
EDTA
K-Y Tnzma
Project Name:
Project*
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75201362
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Orrasteloll.
BT=Tissue
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Sam le Identification - Client ID Lab ID
Sample Date
Time
G= rab
A=Air
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Special Instructions/Note
tile- „
=
WWTP-Q1 (752-2248-1)
2/2123
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Solid
X
X
X
X
X
X
X
X
X
X
'8
Eastern
WTP (752-2248-2)
2/2123
12 DO
Solid
X
X
X
X
X
X
X
X
X
X
$'
Eastern
Note Since laboratory accreditations are subject to change, Eurofins Environment Testing Southeast, LLC places the ownership of method analyte & accreditation compliance upon our subcontract laboratories. This sample shipment is forwarded under chain -of -custody If the
laboratory does not currently maintain accreditation in the State of Origin listed above for analysisltests/matrix being analyzed the samples must be shipped back to the Eurofins Environment Testing Southeast, LLC laboratory or other instructions will be provided. Any changes to
accreditation status should be brought to Eurofins Environment Testing Southeast, LLC attention immediately if all requested accreditations are current to date return the signed Chain of Custody attesting to said compliance to Eurofins Environment Testing Southeast, LLC
Possible Hazard Identification
Sample Disposal (A fee may be assessed if samples are retained longer than 1 month)
Unconfirmed
=Return To Client = Disposal By Lab it Archive For Months
Deliverable Requeste 1 II III IV Other (specify) Primary Deliverable Rank 2
Special Instrucbons/QC Requirements.
Empty Kit Relinquish d by
Date.
Time
M oil of Shipment:
Relinquished by
DateM e.
,rt /'�
5 D /�
Company Received by
D terrime
p
Relinquished by
Datefrime
Company Received ly
Date/Time
Company
Relinquished by
DateTme
Company Received by
Date/Time
Company
Custody Seals Intact.
Custody Sea] No CoolerTemperature(s) °C and Other Remarks _ r j
A Yes No
2

Login Sample Receipt Checklist
Client: Hunt Environmental Associates Job Number: 752-2248-1
Login Number: 2248
List Number: 1
Creator: Yonish, Rachel
Question
List Source: Eurofins Raleigh
Answer Comment
Radioactivity wasn't checked or is </= background as measured by a survey
True
meter.
The cooler's custody seal, if present, is intact.
True
Sample custody seals, if present, are intact.
True
The cooler or samples do not appear to have been compromised or
True
tampered with.
Samples were received on ice.
True
Cooler Temperature is acceptable.
True
Cooler Temperature is recorded.
True
COC is present.
True
COC is filled out in ink and legible.
True
COC is filled out with all pertinent information.
True
Is the Field Sampler's name present on COC?
True
There are no discrepancies between the containers received and the COC.
True
Samples are received within Holding Time (excluding tests with immediate
True
HTs)
Sample containers have legible labels.
True
Containers are not broken or leaking.
True
Sample collection date/times are provided.
True
Appropriate sample containers are used.
True
Sample bottles are completely filled.
True
Sample Preservation Verified.
True
There is sufficient vol. for all requested analyses, incl. any requested
True
MS/MSDs
Containers requiring zero headspace have no headspace or bubble is
True
<6mm (1/4").
Multiphasic samples are not present.
True
Samples do not require splitting or compositing.
True
Residual Chlorine Checked.
True
Eurofins Raleigh
Page 38 of 40 3/28/2023 (Rev. 1)

Login Sample Receipt Checklist
Client: Hunt Environmental Associates Job Number: 752-2248-1
Login Number: 2248
List Number: 2
Creator: Givens, Keshia
Question
List Source: Eurofins Savannah
List Creation: 02/04/23 11:53 AM
Answer Comment
Radioactivity wasn't checked or is </= background as measured by a survey
N/A
meter.
The cooler's custody seal, if present, is intact.
True
Sample custody seals, if present, are intact.
True
The cooler or samples do not appear to have been compromised or
True
tampered with.
Samples were received on ice.
True
Cooler Temperature is acceptable.
True
Cooler Temperature is recorded.
True
COC is present.
True
COC is filled out in ink and legible.
True
COC is filled out with all pertinent information.
True
Is the Field Sampler's name present on COC?
N/A
There are no discrepancies between the containers received and the COC.
True
Samples are received within Holding Time (excluding tests with immediate
True
HTs)
Sample containers have legible labels.
True
Containers are not broken or leaking.
True
Sample collection date/times are provided.
True
Appropriate sample containers are used.
True
Sample bottles are completely filled.
True
Sample Preservation Verified.
N/A
There is sufficient vol. for all requested analyses, incl. any requested
True
MS/MSDs
Containers requiring zero headspace have no headspace or bubble is
N/A
<6mm (1/4").
Multiphasic samples are not present.
True
Samples do not require splitting or compositing.
True
Residual Chlorine Checked.
N/A
Eurofins Raleigh
Page 39 of 40 3/28/2023 (Rev. 1)

Login Sample Receipt Checklist
Client: Hunt Environmental Associates Job Number: 752-2248-1
Login Number: 2248 List Source: Eurofins Savannah
List Number: 3 List Creation: 02/20/23 01:16 PM
Creator: Ogletree, Emma
Question Answer Comment
Radioactivity wasn't checked or is </= background as measured by a survey
meter.
The cooler's custody seal, if present, is intact.
Sample custody seals, if present, are intact.
The cooler or samples do not appear to have been compromised or
tampered with.
Samples were received on ice.
Cooler Temperature is acceptable.
Cooler Temperature is recorded.
COC is present.
COC is filled out in ink and legible.
COC is filled out with all pertinent information.
Is the Field Sampler's name present on COC?
There are no discrepancies between the containers received and the COC.
Samples are received within Holding Time (excluding tests with immediate
HTs)
Sample containers have legible labels.
Containers are not broken or leaking.
Sample collection date/times are provided.
Appropriate sample containers are used.
Sample bottles are completely filled.
Sample Preservation Verified.
There is sufficient vol. for all requested analyses, incl. any requested
MS/MSDs
Containers requiring zero headspace have no headspace or bubble is
<6mm (1/4").
Multiphasic samples are not present.
Samples do not require splitting or compositing.
Residual Chlorine Checked.
Eurofins Raleigh
Page 40 of 40 3/28/2023 (Rev. 1)

tiff eurofins 0
Environment Testing
ANALYTICAL REPORT
PREPARED FOR
Attn: Cody Hunt
Hunt Environmental Associates ■r�
3330 Saddletree Rd
Lumberton, North Carolina 28360
Generated 3/9/2023 8:20:19 AM
JOB DESCRIPTION
City of Lumberton
JOB NUMBER
752-3600-1
1

The test results in this report relate only to the samples as received by the laboratory and will meet all requirements of the
methodology, with any exceptions noted. This report shall not be reproduced except in full, without the express written
approval of the laboratory. All questions should be directed to the Eurofins Environment Testing Southeast, LLC Project
Manager.
Generated
3/9/2023 8:20:19 AM
Authorized for release by
Stephanie Franz, Project Manager
stephanie.franz(a-)et.eurofinsus.com
[phone]
12
13
14
Eurofins Savannah is a laboratory within Eurofins Environment Testing Southeast, LLC, a company within Eurofins Environment Testing Group of Companies
Page 2 of 27 3/9/2023

Client: Hunt Environmental Associates
Project/Site: City of Lumberton
Laboratory Job ID: 752-3600-1
Table of Contents
Cover Page ..............................................
1
Table of Contents .........................................
3
Definitions/Glossary.......................................
4
Case Narrative ...........................................
5
Detection Summary ........................................
6
Client Sample Results ......................................
7
QC Sample Results ........................................
9
QC Association Summary ...................................
13
Lab Chronicle ............................................
16
Certification Summary ......................................
18
Method Summary .........................................
20
Sample Summary .........................................
21
Chain of Custody ..........................................
22
Receipt Checklists .........................................
25
12
13
14
Page 3 of 27
Eurofins Raleigh
3/9/2023

Definitions/Glossary
Client: Hunt Environmental Associates
Project/Site: City of Lumberton
Qualifiers
Metals
Qualifier Qualifier Description
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
General Chemistry
Job ID: 752-3600-1
Qualifier Qualifier Description
4 MS, MSD: The analyte present in the original sample is greater than 4 times the matrix spike concentration; therefore, control limits are not
applicable.
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
Glossary
Abbreviation These commonly used abbreviations may or may not be present in this report.
a Listed under the "D" column to designate that the result is reported on a dry weight basis
%R Percent Recovery
CFL Contains Free Liquid
CFU Colony Forming Unit
CNF Contains No Free Liquid
DER Duplicate Error Ratio (normalized absolute difference)
Dil Fac Dilution Factor
DL Detection Limit (DoD/DOE)
DL, RA, RE, IN Indicates a Dilution, Re -analysis, Re -extraction, or additional Initial metals/anion analysis of the sample
DLC Decision Level Concentration (Radiochemistry)
EDL Estimated Detection Limit (Dioxin)
LOD Limit of Detection (DoD/DOE)
LOQ Limit of Quantitation (DoD/DOE)
MCL EPA recommended "Maximum Contaminant Level"
MDA Minimum Detectable Activity (Radiochemistry)
MDC Minimum Detectable Concentration (Radiochemistry)
MDL Method Detection Limit
ML Minimum Level (Dioxin)
MPN Most Probable Number
MQL Method Quantitation Limit
NC Not Calculated
ND Not Detected at the reporting limit (or MDL or EDL if shown)
NEG Negative / Absent
POS Positive / Present
PQL Practical Quantitation Limit
FIRES Presumptive
QC Quality Control
RER Relative Error Ratio (Radiochemistry)
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
TNTC Too Numerous To Count
12
13
14
Eurofins Raleigh
Page 4 of 27 3/9/2023

Case Narrative
Client: Hunt Environmental Associates
Project/Site: City of Lumberton
Job ID: 752-3600-1
Laboratory: Eurofins Raleigh
Narrative
Job Narrative
752-3600-1
Comments
No additional comments.
Job ID: 752-3600-1
Receipt
The samples were received on 2/27/2023 1:22 PM. Unless otherwise noted below, the samples arrived in good condition, and where
required, properly preserved and on ice. The temperature of the cooler at receipt was 2.60 C.
Metals
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.
General Chemistry
Method 351.2: The matrix spike / matrix spike duplicate (MS/MSD) recoveries for preparation batch 680-765497 and analytical batch
680-765770 were outside control limits for one or more analytes, see QC Sample Results for detail. Sample matrix interference and/or
non -homogeneity are suspected because the associated laboratory control sample (LCS) recovery is within acceptance limits.
F47
Method 365.4: The instrument blank for analytical batch 680-765771 contained Phosphorus greater than the method detection limit (MDL) M
but less than the RL. M
Method 353.2: The instrument blank for analytical batch 680-766049 contained nitrate nitrite as N greater than the method detection limit
(MDL), and were not reanalyzed because detection <1/2RL. The data have been qualified and reported.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
Eurofins Raleigh
Page 5 of 27 3/9/2023

Detection Summary
Client: Hunt Environmental Associates
Job ID:
752-3600-1
Project/Site: City of Lumberton
Client Sample ID: Q1-2 TCLP WWTP
Lab
Sample ID: 752-3600-1
Analyte
Result Qualifier
RL
MDL
Unit
Dil Fac
D
Method
Prep Type
Sodium Adsorption Ratio
76
0.10
0.10
NONE
1
20B
Soluble
Aluminum
16000
590
200
mg/Kg
1
*
6010D
Total/NA
Calcium
9900
1500
220
mg/Kg
1
*
6010D
Total/NA
Copper
310
74
15
mg/Kg
1
*
6010D
Total/NA
Magnesium
1700
1500
270
mg/Kg
1
*
6010D
Total/NA
Nickel
29 J
120
27
mg/Kg
1
*
6010D
Total/NA
Potassium
4300
3000
320
mg/Kg
1
6010D
Total/NA
Sodium
31000
5900
1600
mg/Kg
1
6010D
Total/NA
Zinc
590
59
17
mg/Kg
1
6010D
Total/NA
Ammonia
2600
90
39
mg/Kg
10
350.1-1993 R2.0
Total/NA
Nitrogen, Kjeldahl
55000
15000
8900
mg/Kg
20
351.2-1993 R2.0
Total/NA
Phosphorus
16000
1500
810
mg/Kg
5
365.4-1974
Total/NA
Total Solids
2.8
0.10
0.10
%
1
SM 254OG
Total/NA
Nitrate Nitrite as N
2300 J
3000
820
mg/Kg
50
353.2-1993 R2.0
Soluble
pH
6.4
1
1
Su
1
9045D
Soluble
Temperature
19.8
1
1
Degrees C
1
9045D
Soluble
Client Sample ID: Q1-2 WTP
Lab
Sample ID: 752-3600-2
Analyte
Result Qualifier
RL
MDL
Unit
Dil Fac
D
Method
Prep Type
Aluminum
160000
920
310
mg/Kg
1
*
6010D
Total/NA
Calcium
3700
2300
340
mg/Kg
1
*
6010D
Total/NA
Copper
50 J
110
23
mg/Kg
1
*
6010D
Total/NA
Zinc
140
92
27
mg/Kg
1
*
6010D
Total/NA
Ammonia
24
16
6.9
mg/Kg
1
*
350.1-1993 R2.0
Total/NA
Nitrogen, Kjeldahl
6500
1300
780
mg/Kg
1
*
351.2-1993 R2.0
Total/NA
Phosphorus
3600
520
290
mg/Kg
1
*
365.4-1974
Total/NA
Total Solids
1.6
0.10
0.10
%
1
SM 254OG
Total/NA
pH
5.8
1
1
Su
1
9045D
Soluble
Temperature
19.9
1
1
Degrees C
1
9045D
Soluble
This Detection Summary does not include radiochemical test results.
Eurofins Raleigh
Page 6 of 27 3/9/2023

Client Sample Results
Client: Hunt Environmental Associates
Project/Site: City of Lumberton
Job ID: 752-3600-1
Client Sample ID: Q1-2 TCLP WWTP Lab Sample ID: 752-3600-1
Date Collected: 02/27/23 09:00 Matrix: Solid
Date Received: 02/27/23 13:22 Percent Solids: 3.3
Method: USDA 20B - Sodium Adsorption Ratio - Soluble
Analyte
Result Qualifier
Sodium Adsorption Ratio
76
Method: SW846 6010D - Metals (ICP)
Analyte
Result Qualifier
Aluminum
16000
Arsenic
<35
Cadmium
<3.0
Calcium
9900
Copper
310
Lead
<18
Magnesium
1700
Molybdenum
<7.7
Nickel
29 J
Potassium
4300
Selenium
<32
Sodium
31000
Zinc
590
Method: SW846 7471 B - Mercury (CVAA)
Analyte
Result Qualifier
Mercury
<0.22
General Chemistry
Analyte
Result Qualifier
Ammonia (MCAWW 350.1-1993
2600
R2.0)
Nitrogen, Kjeldahl (MCAWW
55000
351.2-1993 R2.0)
Phosphorus (EPA 365.4-1974)
16000
Total Solids (SM 2540G)
2.8
General Chemistry - Soluble
Analyte
Result Qualifier
Nitrate Nitrite as N (MCAWW
2300 J
353.2-1993 R2.0)
pH (SW846 9045D)
6.4
Temperature (SW846 9045D)
19.8
Client Sample ID: Q1-2 WTP
Date Collected: 02/27/23 09:30
Date Received: 02/27/23 13:22
RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
0.10
0.10
NONE
03/06/2314:06
1
RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
590
200
mg/Kg
*
02/28/2315:49
03/02/2319:53
1
59
35
mg/Kg
*
02/28/2315:49
03/02/2319:53
1
15
3.0
mg/Kg
*
02/28/2315:49
03/02/2319:53
1
1500
220
mg/Kg
02/28/2315:49
03/02/2319:53
1
74
15
mg/Kg
02/28/2315:49
03/02/2319:53
1
30
18
mg/Kg
02/28/2315:49
03/02/2319:53
1
1500
270
mg/Kg
02/28/2315:49
03/02/2319:53
1
30
7.7
mg/Kg
02/28/2315:49
03/02/2319:53
1
120
27
mg/Kg
02/28/2315:49
03/02/2319:53
1
3000
320
mg/Kg
02/28/2315:49
03/02/2319:53
1
74
32
mg/Kg
02/28/2315:49
03/02/2319:53
1
Is
5900
1600
mg/Kg
02/28/2315:49
03/02/2319:53
1
59
17
mg/Kg
02/28/2315:49
03/02/2319:53
1
RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
M
0.68
0.22
mg/Kg
*
03/01/23 08:18
03/01/23 17:20
1
RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
90
39
mg/Kg
*
03/07/23 19:40
03/08/23 00:25
10
15000
8900
mg/Kg
*
03/01/23 09:35
03/02/23 12:56
20
1500
810
mg/Kg
03/01/23 09:35 03/02/23 10:58 5
0.10
0.10
%
03/01/2315:30 1
RL
MDL
Unit
D Prepared Analyzed Dil Fac
3000
820
mg/Kg
03/04/2317:49 50
1
1
Su
02/28/2311:51 1
1
1
Degrees C
02/28/23 11:51 1
Lab Sample ID: 752-3600-2
Matrix: Solid
Percent Solids: 1.9
Method: USDA 20B - Sodium Adsorption Ratio - Soluble
Analyte Result Qualifier
RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
Sodium Adsorption Ratio <0.10
0.10
0.10
NONE
03/06/23 14:06
1
Method: SW846 6010D - Metals (ICP)
Analyte Result Qualifier
RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
Aluminum 160000
920
310
mg/Kg
*
02/28/2315:49
03/02/2319:56
1
Arsenic <55
92
55
mg/Kg
*
02/28/2315:49
03/02/2319:56
1
Cadmium <4.6
23
4.6
mg/Kg
*
02/28/2315:49
03/02/2319:56
1
Calcium 3700
2300
340
mg/Kg
*
02/28/2315:49
03/02/2319:56
1
Page 7 of 27
Eurofins Raleigh
3/9/2023

Client Sample Results
Client: Hunt Environmental Associates
Project/Site: City of Lumberton
Job ID: 752-3600-1
Client Sample ID: Q1-2 WTP Lab Sample ID: 752-3600-2
Date Collected: 02/27/23 09:30 Matrix: Solid
Date Received: 02/27/23 13:22 Percent Solids: 1.9
Method: SW846 6010D - Metals (ICP) (Continued)
Analyte
Result Qualifier
Copper
50 J
Lead
<28
Magnesium
<420
Molybdenum
<12
Nickel
<41
Potassium
<500
Selenium
<50
Sodium
<2500
Zinc
140
Method: SW846 7471 B - Mercury (CVAA)
Analyte
Result Qualifier
Mercury
<0.42
General Chemistry
Analyte
Result Qualifier
Ammonia (MCAWW 350.1-1993
24
R2.0)
Nitrogen, Kjeldahl (MCAWW
6500
351.2-1993 R2.0)
Phosphorus (EPA 365.4-1974)
3600
Total Solids (SM 2540G)
1.6
General Chemistry - Soluble
Analyte
Result Qualifier
Nitrate Nitrite as N (MCAWW
<29
353.2-1993 R2.0)
pH (SW846 9045D)
5.8
Temperature (SW846 9045D)
19.9
RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
110
23
mg/Kg
*
02/28/2315:49
03/02/2319:56
1
46
28
mg/Kg
*
02/28/2315:49
03/02/2319:56
1
2300
420
mg/Kg
*
02/28/2315:49
03/02/2319:56
1
46
12
mg/Kg
*
02/28/2315:49
03/02/2319:56
1
180
41
mg/Kg
*
02/28/2315:49
03/02/2319:56
1
4600
500
mg/Kg
*
02/28/2315:49
03/02/2319:56
1
110
50
mg/Kg
*
02/28/2315:49
03/02/2319:56
1
9200
2500
mg/Kg
*
02/28/2315:49
03/02/2319:56
1
92
27
mg/Kg
*
02/28/2315:49
03/02/2319:56
1
RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
1.3
0.42
mg/Kg
*
03/01/23 08:18
03/01/23 17:23
1
RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
Is
16
6.9
mg/Kg
*
03/07/23 19:40
03/07/23 22:38
1
1300
780
mg/Kg
*
03/01/23 09:35
03/02/23 10:20
1
M
520
290
mg/Kg
*
03/01/23 09:35
03/02/23 08:16
1
0.10
0.10
%
03/01/2315:30
1
RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
110
29
mg/Kg
03/04/2317:49
1
1
1
Su
02/28/2311:51
1
1
1
Degrees C
02/28/23 11:51
1
Eurofins Raleigh
Page 8 of 27 3/9/2023

QC Sample Results
Client: Hunt Environmental Associates
Job ID: 752-3600-1
Project/Site: City of Lumberton
Method: 6010D - Metals (ICP)
Lab Sample ID: MB 680-765412/1-A
Client Sample ID: Method Blank
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 765840
Prep Batch: 765412
MB MB
Analyte
Result Qualifier
RL
MDL
Unit
D Prepared
Analyzed Dil Fac
Aluminum
<6.4
19
6.4
mg/Kg
02/28/2315:49
03/02/2319:05 1
Arsenic
<1.1
1.9
1.1
mg/Kg
02/28/2315:49
03/02/2319:05 1
Cadmium
<0.094
0.47
0.094
mg/Kg
02/28/2315:49
03/02/2319:05 1
Calcium
<7.0
47
7.0
mg/Kg
02/28/2315:49
03/02/2319:05 1
Copper
<0.47
2.4
0.47
mg/Kg
02/28/2315:49
03/02/2319:05 1
Lead
<0.58
0.94
0.58
mg/Kg
02/28/2315:49
03/02/2319:05 1
Magnesium
<8.6
47
8.6
mg/Kg
02/28/2315:49
03/02/2319:05 1
Molybdenum
<0.25
0.94
0.25
mg/Kg
02/28/2315:49
03/02/2319:05 1
Nickel
<0.85
3.8
0.85
mg/Kg
02/28/2315:49
03/02/2319:05 1
Potassium
<10
94
10
mg/Kg
02/28/2315:49
03/02/2319:05 1
Selenium
<1.0
2.4
1.0
mg/Kg
02/28/2315:49
03/02/2319:05 1
Sodium
<52
190
52
mg/Kg
02/28/2315:49
03/02/2319:05 1
Zinc
<0.55
1.9
0.55
mg/Kg
02/28/2315:49
03/02/2319:05 1
Lab Sample ID: LCS 680-765412/2-A
Client Sample ID: Lab Control Sample
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 765840
Prep Batch: 765412
Spike
LCS LCS
%Rec
Analyte
Added
Result Qualifier
Unit
D %Rec
Limits
Aluminum
455
451
mg/Kg
99
80 - 120
Arsenic
9.09
7.84
mg/Kg
86
80. 120
Cadmium
4.55
4.20
mg/Kg
92
80. 120
Calcium
455
438
mg/Kg
96
80. 120
Copper
9.09
9.35
mg/Kg
103
80. 120
Lead
45.9
43.4
mg/Kg
95
80. 120
Magnesium
455
443
mg/Kg
97
80 - 120
Molybdenum
9.09
8.73
mg/Kg
96
80 - 120
Nickel
9.09
8.60
mg/Kg
95
80 - 120
Potassium
634
632
mg/Kg
100
80 - 120
Selenium
9.09
7.34
mg/Kg
81
80 - 120
Sodium
459
450
mg/Kg
98
80 - 120
Zinc
9.09
8.68
mg/Kg
95
80 - 120
Method: 7471 B - Mercury (CVAA)
Lab Sample ID: MB 680-765452/12-A
Client Sample ID: Method Blank
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 765728
Prep Batch: 765452
MB MB
Analyte Result Qualifier
RL
MDL Unit
D Prepared
Analyzed Dil Fac
Mercury <0.0067
0.021
0.0067 mg/Kg
03/01/23 08:18
03/02/23 08:18 1
Lab Sample ID: LCS 680-765452/13-A Client Sample ID: Lab Control Sample
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 765728 Prep Batch: 765452
Spike LCS LCS %Rec
Analyte Added Result Qualifier Unit D %Rec Limits
Mercury 0.212 0.219 mg/Kg 103 80 - 120
Eurofins Raleigh
Page 9 of 27 3/9/2023

QC Sample Results
Client: Hunt Environmental Associates
Project/Site: City of Lumberton
Job I D: 752-3600-1
Method: 350.1-1993 R2.0 - Nitrogen, Ammonia
Lab Sample ID: MB 680-766455/1-A Client Sample ID: Method Blank
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 766466 Prep Batch: 766455
MB MB
Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac
Ammonia <0.13 0.30 0.13 mg/Kg 03/07/23 19:40 03/07/23 22:34 1
Lab Sample ID: LCS 680-766455/2-A Client Sample ID: Lab Control Sample
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 766466 Prep Batch: 766455
Spike LCS LCS %Rec
Analyte Added Result Qualifier Unit D %Rec Limits
Ammonia 4.99 3.77 mg/Kg 76 75 -125
Method: 351.2-1993 R2.0 - Nitrogen, Total Nitrogen
Lab Sample ID: MB 680-765497/1-A
Client Sample ID: Method Blank
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 765770
Prep Batch: 765497
MB MB
Analyte Result Qualifier
RL
MDL Unit D Prepared Analyzed Dil Fac
Nitrogen, Kjeldahl <12
20
12 mg/Kg 03/01/23 09:35 03/02/23 10:07 1
Lab Sample ID: LCS 680-765497/2-A
Client Sample ID: Lab Control Sample
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 765770
Prep Batch: 765497
Spike
LCS LCS %Rec
Analyte
Added
Result Qualifier Unit D %Rec Limits
Nitrogen, Kjeldahl
159
164 mg/Kg 103 75-125
Lab Sample ID: 752-3600-1 MS
Client Sample ID: Q1-2 TCLP WWTP
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 765770
Prep Batch: 765497
Sample Sample
Spike
MS MS %Rec
Analyte Result Qualifier
Added
Result Qualifier Unit D %Rec Limits
Nitrogen, Kjeldahl 55000
5960
53100 4 mg/Kg -25 75 -125
Lab Sample ID: 752-3600-1 MSD
Client Sample ID: Q1-2 TCLP WWTP
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 765770
Prep Batch: 765497
Sample Sample
Spike
MSD MSD %Rec RPD
Analyte Result Qualifier
Added
Result Qualifier Unit D %Rec Limits RPD Limit
Nitrogen, Kjeldahl 55000
5800
61300 4 mg/Kg # 116 75 -125 14 40
Method: 353.2-1993 R2.0 - Nitrogen, Nitrate -Nitrite
Lab Sample ID: MB 680-766049/3
Client Sample ID: Method Blank
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 766049
MB MB
Analyte Result Qualifier
RL
MDL Unit D Prepared Analyzed Dil Fac
Nitrate Nitrite as N <0.028
0.10
0.028 mg/Kg 03/04/23 17:10 1
Eurofins Raleigh
Page 10 of 27 3/9/2023

QC Sample Results
Client: Hunt Environmental Associates
Project/Site: City of Lumberton
Job I D: 752-3600-1
Method: 353.2-1993 R2.0 - Nitrogen, Nitrate -Nitrite (Continued)
Lab Sample ID: LCS 680-766049/4
Client Sample ID: Lab Control Sample
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 766049
Spike
LCS LCS
%Rec
Analyte
Added
Result Qualifier
Unit D %Rec Limits
Nitrate Nitrite as N
1.00
1.02
mg/Kg 102 80 - 120
Lab Sample ID: MB 680-766047/1-A
Client Sample ID: Method Blank
Matrix: Solid
Prep Type: Soluble
Analysis Batch: 766049
MB
MB
Analyte Result
Qualifier
RL MDL Unit
D Prepared Analyzed Dil Fac
Nitrate Nitrite as N <0.55
2.0 0.55 mg/Kg
03/04/23 17:33 1
Lab Sample ID: LCS 680-766047/2-A
Client Sample ID: Lab Control Sample
Matrix: Solid
Prep Type: Soluble
Analysis Batch: 766049
Spike
LCS LCS
%Rec
Analyte
Added
Result Qualifier
Unit D %Rec Limits
Nitrate Nitrite as N
19.8
21.2
mg/Kg 107 80 - 120
Lab Sample ID: LCSD 680-766047/3-A
Client
Sample ID: Lab Control Sample Dup
Matrix: Solid
Prep Type: Soluble
Analysis Batch: 766049
Spike
LCSD LCSD
%Rec RPD
Analyte
Added
Result Qualifier
Unit D %Rec Limits RPD Limit
Nitrate Nitrite as N
19.9
21.1
mg/Kg 106 80 - 120 0 20
Method: 365.4-1974 - Phosphorus, Total
Lab Sample ID: MB 680-765497/1-A
Client Sample ID: Method Blank
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 765771
Prep Batch: 765497
MB MB
Analyte Result Qualifier
RL MDL Unit D Prepared Analyzed Dil Fac
Phosphorus <4.4
7.9 4.4 mg/Kg 03/01/23 09:35 03/02/23 09:23 1
Lab Sample ID: LCS 680-765497/2-A
Client Sample ID: Lab Control Sample
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 765771
Prep Batch: 765497
Spike
LCS LCS %Rec
Analyte
Added
Result Qualifier Unit D %Rec Limits
Phosphorus
159
169 mg/Kg 107 70-130
Lab Sample ID: 752-3600-1 MS
Client Sample ID: Q1-2 TCLP WWTP
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 765771
Prep Batch: 765497
Sample Sample
Spike
MS MS %Rec
Analyte Result Qualifier
Added
Result Qualifier Unit D %Rec Limits
Phosphorus 16000
5960
23400 mg/Kg 125 70-130
Eurofins Raleigh
Page 11 of 27 3/9/2023

QC Sample Results
Client: Hunt Environmental Associates
Project/Site: City of Lumberton
Method: 365.4-1974 - Phosphorus, Total (Continued)
Lab Sample ID: 752-3600-1 MSD
Matrix: Solid
Analysis Batch: 765771
Sample Sample Spike
Analyte Result Qualifier Added
Phosphorus 16000 5800
Method: 9045D - pH
Lab Sample ID: 752-3600-1 DU
Matrix: Solid
Analysis Batch: 1505
Sample Sample
Analyte Result Qualifier
pH 6.4
Temperature 19.8
Method: SM 254OG - Total, Fixed, and Volatile Solids
Lab Sample ID: MB 680-765594/1
Matrix: Solid
Analysis Batch: 765594
MB MB
Analyte Result Qualifier RL
Total Solids 100 0.10
Lab Sample ID: 752-3600-1 DU
Matrix: Solid
Analysis Batch: 765594
Sample Sample
Analyte Result Qualifier
Total Solids 2.8
Job I D: 752-3600-1
Client Sample ID: Q1-2 TCLP WWTP
Prep Type: Total/NA
Prep Batch: 765497
MSD
MSD
%Rec RPD
Result
Qualifier
Unit D %Rec Limits RPD Limit
23100
mg/Kg # 124 70-130 1 30
Client Sample ID: Q1-2 TCLP WWTP
Prep Type: Soluble
DU
DU
RPD
Result
Qualifier
Unit D RPD Limit
6.4
SU 0.6 25
19.4
Degrees C 2
Client Sample ID: Method Blank
Prep Type: Total/NA
MDL Unit
D Prepared Analyzed Dil Fac
0.10 %
03/01/2315:30 1
Client Sample ID: Q1-2 TCLP WWTP
Prep Type: Total/NA
DU
DU
RPD
Result
Qualifier
Unit D RPD Limit
2.83
% 0.4 5
Eurofins Raleigh
Page 12 of 27 3/9/2023

QC Association Summary
Client: Hunt Environmental Associates
Job ID: 752-3600-1
Project/Site: City of Lumberton
Metals
Analysis Batch: 428267
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
752-3600-1
Q1-2 TCLP VWVTP
Soluble
Solid
20B
752-3600-2
Q1-2 VVTP
Soluble
Solid
20B
Prep Batch: 765412
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
752-3600-1
Q1-2 TCLP VWVTP
Total/NA
Solid
3050B
752-3600-2
Q1-2 VVTP
Total/NA
Solid
3050B
MB 680-765412/1-A
Method Blank
Total/NA
Solid
3050B
LCS 680-765412/2-A
Lab Control Sample
Total/NA
Solid
3050B
Prep Batch: 765452
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
752-3600-1
Q1-2 TCLP VWVTP
Total/NA
Solid
7471 B
752-3600-2
Q1-2VVTP
Total/NA
Solid
7471B
MB 680-765452/12-A
Method Blank
Total/NA
Solid
7471 B
LCS 680-765452/13-A
Lab Control Sample
Total/NA
Solid
7471 B
Analysis Batch: 765728
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
752-3600-1
Q1-2 TCLP VWVTP
Total/NA
Solid
7471 B
765452
752-3600-2
Q1-2VVTP
Total/NA
Solid
7471B
765452
MB 680-765452/12-A
Method Blank
Total/NA
Solid
7471 B
765452
LCS 680-765452/13-A
Lab Control Sample
Total/NA
Solid
7471 B
765452
Analysis Batch: 765840
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
752-3600-1
Q1-2 TCLP VWVTP
Total/NA
Solid
6010D
765412
752-3600-2
Q1-2 VVTP
Total/NA
Solid
6010D
765412
MB 680-765412/1-A
Method Blank
Total/NA
Solid
6010D
765412
LCS 680-765412/2-A
Lab Control Sample
Total/NA
Solid
6010D
765412
General Chemistry
Leach Batch: 1500
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
752-3600-1
Q1-2 TCLP VWVTP
Soluble
Solid
DI Leach
752-3600-2
Q1-2 VVTP
Soluble
Solid
DI Leach
752-3600-1 DU
Q1-2 TCLP VWVTP
Soluble
Solid
DI Leach
Analysis Batch: 1505
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
752-3600-1
Q1-2 TCLP VWVTP
Soluble
Solid
9045D
1500
752-3600-2
Q1-2 VVTP
Soluble
Solid
9045D
1500
LCS 752-1505/2
Lab Control Sample
Total/NA
Solid
9045D
752-3600-1 DU
Q1-2 TCLP VWVTP
Soluble
Solid
9045D
1500
Prep Batch: 765497
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
752-3600-1
Q1-2 TCLP VWVTP
Total/NA
Solid
Digestion
752-3600-2
Q1-2 VVTP
Total/NA
Solid
Digestion
MB 680-765497/1-A
Method Blank
Total/NA
Solid
Digestion
0
Eurofins Raleigh
Page 13 of 27 3/9/2023

QC Association Summary
Client: Hunt Environmental Associates
Job ID:
752-3600-1
Project/Site: City of Lumberton
General Chemistry (Continued)
Prep Batch: 765497 (Continued)
Lab Sample ID Client Sample ID
Prep Type
Matrix
Method
Prep Batch
LCS 680-765497/2-A Lab Control Sample
Total/NA
Solid
Digestion
752-3600-1 MS Q1-2 TCLP VWVTP
Total/NA
Solid
Digestion
752-3600-1 MSD Q1-2 TCLP VWVTP
Total/NA
Solid
Digestion
Analysis Batch: 765594
Lab Sample ID Client Sample ID
Prep Type
Matrix
Method
Prep Batch
752-3600-1 Q1-2 TCLP VWVTP
Total/NA
Solid
SM 254OG
752-3600-2 Q1-2 VVTP
Total/NA
Solid
SM 254OG
MB 680-765594/1 Method Blank
Total/NA
Solid
SM 254OG
752-3600-1 DU Q1-2 TCLP VWVTP
Total/NA
Solid
SM 254OG
Analysis Batch: 765697
Lab Sample ID Client Sample ID
Prep Type
Matrix
Method
Prep Batch
752-3600-1 Q1-2 TCLP VWVTP
Total/NA
Solid
Moisture
752-3600-2 Q1-2 VVTP
Total/NA
Solid
Moisture
Analysis Batch: 765770
Lab Sample ID Client Sample ID
Prep Type
Matrix
Method
Prep Batch
752-3600-1 Q1-2 TCLP VWVTP
Total/NA
Solid
351.2-1993 R2.0
765497
752-3600-2 Q1-2 VVTP
Total/NA
Solid
351.2-1993 R2.0
765497
MB 680-765497/1-A Method Blank
Total/NA
Solid
351.2-1993 R2.0
765497
LCS 680-765497/2-A Lab Control Sample
Total/NA
Solid
351.2-1993 R2.0
765497
752-3600-1 MS Q1-2 TCLP VWVTP
Total/NA
Solid
351.2-1993 R2.0
765497
752-3600-1 MSD Q1-2 TCLP VWVTP
Total/NA
Solid
351.2-1993 R2.0
765497
Analysis Batch: 765771
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
752-3600-1
Q1-2 TCLP VWVTP
Total/NA
Solid
365.4-1974
765497
752-3600-2
Q1-2 VVTP
Total/NA
Solid
365.4-1974
765497
MB 680-765497/1-A
Method Blank
Total/NA
Solid
365.4-1974
765497
LCS 680-765497/2-A
Lab Control Sample
Total/NA
Solid
365.4-1974
765497
752-3600-1 MS
Q1-2 TCLP VWVTP
Total/NA
Solid
365.4-1974
765497
752-3600-1 MSD
Q1-2 TCLP VWVTP
Total/NA
Solid
365.4-1974
765497
Leach Batch: 766047
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method Prep Batch
752-3600-1
Q1-2 TCLP VWVTP
Soluble
Solid
DI Leach
752-3600-2
Q1-2 VVTP
Soluble
Solid
DI Leach
MB 680-766047/1-A
Method Blank
Soluble
Solid
DI Leach
LCS 680-766047/2-A
Lab Control Sample
Soluble
Solid
DI Leach
LCSD 680-766047/3-A
Lab Control Sample Dup
Soluble
Solid
DI Leach
Analysis Batch: 766049
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
752-3600-1
Q1-2 TCLP VWVTP
Soluble
Solid
353.2-1993 R2.0
766047
752-3600-2
Q1-2 VVTP
Soluble
Solid
353.2-1993 R2.0
766047
MB 680-766047/1-A
Method Blank
Soluble
Solid
353.2-1993 R2.0
766047
MB 680-766049/3
Method Blank
Total/NA
Solid
353.2-1993 R2.0
LCS 680-766047/2-A
Lab Control Sample
Soluble
Solid
353.2-1993 R2.0
766047
LCS 680-766049/4
Lab Control Sample
Total/NA
Solid
353.2-1993 R2.0
LCSD 680-766047/3-A
Lab Control Sample Dup
Soluble
Solid
353.2-1993 R2.0
766047
Eurofins Raleigh
Page 14 of 27 3/9/2023

QC Association Summary
Client: Hunt Environmental Associates
Project/Site: City of Lumberton
General Chemistry
Prep Batch: 766455
Lab Sample ID
Client Sample ID
752-3600-1
Q1-2 TCLP VWVTP
752-3600-2
Q1-2 VVTP
MB 680-766455/1-A
Method Blank
LCS 680-766455/2-A
Lab Control Sample
Analysis Batch: 766466
Lab Sample ID
Client Sample ID
752-3600-1
Q1-2 TCLP VWVTP
752-3600-2
Q1-2 VVTP
MB 680-766455/1-A
Method Blank
LCS 680-766455/2-A
Lab Control Sample
Job ID: 752-3600-1
Prep Type
Matrix
Method
Prep Batch
Total/NA
Solid
3-154
Total/NA
Solid
3-154
Total/NA
Solid
3-154
Total/NA
Solid
3-154
Prep Type
Matrix
Method
Prep Batch
Total/NA
Solid
350.1-1993 R2.0
766455
Total/NA
Solid
350.1-1993 R2.0
766455
Total/NA
Solid
350.1-1993 R2.0
766455
Total/NA
Solid
350.1-1993 R2.0
766455
12
13
14
Eurofins Raleigh
Page 15 of 27 3/9/2023

Lab Chronicle
Client: Hunt Environmental Associates
Job ID: 752-3600-1
Project/Site: City of Lumberton
Client Sample ID: Q1-2 TCLP WWTP
Lab Sample ID: 752-3600-1
Date Collected: 02/27/23 09:00
Matrix: Solid
Date Received: 02/27/23 13:22
Batch Batch
Dilution
Batch
Prepared
Prep Type Type Method Run
Factor
Number
Analyst
Lab or Analyzed
Soluble Analysis 20B
1
428267
RSR
EET PIT 03/06/23 14:06
Soluble Leach DI Leach
1500
CB
EET ESC 02/28/23 10:25
Soluble Analysis 9045D
1
1505
CB
EET ESC 02/28/23 11:51
Total/NA Analysis Moisture
1
765697
KG
EET SAV 03/02/23 11:09
Total/NA Analysis SM 2540G
1
765594
PG
EET SAV 03/01/23 15:30
Client Sample ID: Q1-2 TCLP WWTP
Lab Sample ID: 752-3600-1
Date Collected: 02/27/23 09:00
Matrix: Solid '
Date Received: 02/27/23 13:22
Percent Solids: 3.3
Batch Batch
Prep Type Type Method
Dilution
Run Factor
Batch
Number Analyst
Lab
Prepared
or Analyzed
Total/NA Prep 3050B
765412
BCB
EET SAV
02/28/2315:49
Total/NA Analysis 6010D
1
765840
BJB
EET SAV
03/02/23 19:53
Total/NA Prep 7471 B
765452
JKL
EET SAV
03/01/23 08:18
Total/NA Analysis 7471 B
1
765728
JKL
EET SAV
03/01/23 17:20
Total/NA Prep 3-154
766455
PB
EET SAV
03/07/23 19:40
Total/NA Analysis 350.1-1993 R2.0
10
766466
PB
EET SAV
03/08/23 00:25 m
Total/NA Prep Digestion
765497
SM
EET SAV
03/01/23 09:35
Total/NA Analysis 351.2-1993 R2.0
20
765770
AS
EET SAV
03/02/23 12:56
Soluble Leach DI Leach
766047
EO
EET SAV
03/03/23 12:00
Soluble Analysis 353.2-1993 R2.0
50
766049
EO
EET SAV
03/04/23 17:49
Total/NA Prep Digestion
765497
SM
EET SAV
03/01/23 09:35
Total/NA Analysis 365.4-1974
5
765771
AS
EET SAV
03/02/23 10:58
Client Sample ID: Q1-2 WTP
Lab Sample ID: 752-3600-2
Date Collected: 02/27/23 09:30
Matrix: Solid
Date Received: 02/27/23 13:22
Batch Batch
Prep Type Type Method
Dilution
Run Factor
Batch
Number Analyst
Lab
Prepared
or Analyzed
Soluble Analysis 20B
1
428267
RSR
EET PIT
03/06/23 14:06
Soluble Leach DI Leach
1500
CB
EET ESC
02/28/23 10:25
Soluble Analysis 9045D
1
1505
CB
EET ESC
02/28/23 11:51
Total/NA Analysis Moisture
1
765697
KG
EET SAV
03/02/23 11:09
Total/NA Analysis SM 254OG
1
765594
PG
EET SAV
03/01/23 15:30
Client Sample ID: Q1-2 WTP
Lab Sample ID: 752-3600-2
Date Collected: 02/27/23 09:30
Matrix: Solid
Date Received: 02/27/23 13:22
Percent Solids: 1.9
Prep Type
Batch
Type
Batch
Method
Dilution
Run Factor
Batch
Number Analyst
Lab
Prepared
or Analyzed
Total/NA
Prep
3050B
765412 BCB
EET SAV
02/28/23 15:49
Total/NA
Analysis
6010D
1
765840 BJB
EET SAV
03/02/23 19:56
Total/NA
Prep
7471 B
765452 JKL
EET SAV
03/01/23 08:18
Total/NA
Analysis
7471 B
1
765728 JKL
EET SAV
03/01/23 17:23
Eurofins Raleigh
Page 16 of 27 3/9/2023

Lab Chronicle
Client: Hunt Environmental Associates
Project/Site: City of Lumberton
Job ID: 752-3600-1
Client Sample ID: Q1-2 WTP Lab Sample ID: 752-3600-2
Date Collected: 02/27/23 09:30 Matrix: Solid
Date Received: 02/27/23 13:22 Percent Solids: 1.9
Batch
Batch
Dilution
Batch
Prepared
Prep Type
Type
Method
Run Factor
Number
Analyst
Lab
or Analyzed
Total/NA
Prep
3-154
766455
PB
EET SAV
03/07/23 19:40
Total/NA
Analysis
350.1-1993 R2.0
1
766466
PB
EET SAV
03/07/23 22:38
Total/NA
Prep
Digestion
765497
SM
EET SAV
03/01/23 09:35
Total/NA
Analysis
351.2-1993 R2.0
1
765770
AS
EET SAV
03/02/23 10:20
Soluble
Leach
DI Leach
766047
EO
EET SAV
03/03/23 12:00
Soluble
Analysis
353.2-1993 R2.0
1
766049
EO
EET SAV
03/04/23 17:49
Total/NA
Prep
Digestion
765497
SM
EET SAV
03/01/23 09:35
Total/NA
Analysis
365.4-1974
1
765771
AS
EET SAV
03/02/23 08:16
Laboratory References:
EET ESC = Eurofins Raleigh, 102-A Woodwinds Industrial Court, Cary, NC 27511, TEL [phone]
EET PIT = Eurofins Pittsburgh, 301 Alpha Drive, RIDC Park, Pittsburgh, PA 15238, TEL [phone]
EET SAV = Eurofins Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL [phone]
0
12
13
14
Page 17 of 27
Eurofins Raleigh
3/9/2023

Accreditation/Certification Summary
Client: Hunt Environmental Associates Job ID: 752-3600-1
Project/Site: City of Lumberton
Laboratory: Eurofins Raleigh
Unless otherwise noted, all analytes for this laboratory were covered under each accreditation/certification below.
Authority Program Identification Number Expiration Date
North Carolina (VWV/SV) State 591 12-31-23
The following analytes are included in this report, but the laboratory is not certified by the governing authority. This list may include analytes for which
the agency does not offer certification.
Analysis Method Prep Method Matrix Analyte
9045D Solid Temperature
Laboratory: Eurofins Pittsburgh
All accreditations/certifications held by this laboratory are listed. Not all accreditations/certifications are applicable to this report.
Authority
Program
Identification Number
Expiration Date
Arkansas DEQ
State
19-033-0
06-27-23
California
State
2891
04-30-23
Connecticut
State
PH-0688
09-30-22
Florida
NELAP
E871008
06-30-23
Georgia
State
PA 02-00416
04-30-23
Illinois
NELAP
004375
06-30-23
Kansas
NELAP
E-10350
03-31-23
Kentucky (UST)
State
162013
04-30-23
Kentucky (WW)
State
KY98043
12-31-23
Louisiana
NELAP
04041
06-30-22
Louisiana (All)
NELAP
04041
06-30-23
Maine
State
PA00164
03-06-24
Minnesota
NELAP
042-999-482
12-31-23
New Hampshire
NELAP
2030
04-04-23
New Jersey
NELAP
PA005
06-30-23
New York
NELAP
11182
04-01-23
North Carolina (VWV/SVV)
State
434
12-31-23
North Dakota
State
R-227
04-30-23
Oregon
NELAP
PA-2151
02-06-24
Pennsylvania
NELAP
02-00416
04-30-23
Rhode Island
State
LAO00362
12-31-22'
South Carolina
State
89014
04-30-23
Texas
NELAP
T104704528
03-31-23
US Fish & Wildlife
US Federal Programs
058448
03-31-23
USDA
US Federal Programs
P330-16-00211
06-21-24
Utah
NELAP
PA001462019-8
05-31-23
Virginia
NELAP
10043
09-14-23
West Virginia DEP
State
142
03-31-23
Wisconsin
State
998027800
08-31-23
Laboratory: Eurofins Savannah
Unless otherwise noted, all analytes for this laboratory were covered under each accreditation/certification below.
Authority
North Carolina (VWV/SVV)
Program
State
Identification Number Expiration Date
269 12-31-23
The following analytes are included in this report, but the laboratory is not certified by the governing authority. This list may include analytes for which
the agency does not offer certification.
Analysis Method Prep Method Matrix Analyte
350.1-1993 R2.0 3-154 Solid Ammonia
351.2-1993 R2.0 Digestion Solid Nitrogen, Kjeldahl
Accreditation/Certification renewal pending - accreditation/certification considered valid.
12
13
14
Eurofins Raleigh
Page 18 of 27 3/9/2023

Accreditation/Certification Summary
Client: Hunt Environmental Associates Job ID: 752-3600-1
Project/Site: City of Lumberton
Laboratory: Eurofins Savannah (Continued)
Unless otherwise noted, all analytes for this laboratory were covered under each accreditation/certification below.
Authority Program Identification Number Expiration Date
The following analytes are included in this report, but the laboratory is not certified by the governing authority. This list may include analytes for which
the agency does not offer certification.
Analysis Method Prep Method
Matrix
Analyte
353.2-1993 R2.0
Solid
Nitrate Nitrite as N
365.4-1974 Digestion
Solid
Phosphorus
Moisture
Solid
Percent Solids
SM 254OG
Solid
Total Solids
12
13
14
Eurofins Raleigh
Page 19 of 27 3/9/2023

Method Summary
Client: Hunt Environmental Associates
Project/Site: City of Lumberton
Job ID: 752-3600-1
Method
Method Description
Protocol
Laboratory
20B
Sodium Adsorption Ratio
USDA
EET PIT
6010D
Metals (ICP)
SW846
EET SAV
7471 B
Mercury (CVAA)
SW846
EET SAV
350.1-1993 R2.0
Nitrogen, Ammonia
MCAWW
EET SAV
351.2-1993 R2.0
Nitrogen, Total Nitrogen
MCAWW
EET SAV
353.2-1993 R2.0
Nitrogen, Nitrate -Nitrite
MCAWW
EET SAV
365.4-1974
Phosphorus, Total
EPA
EET SAV
9045D
pH
SW846
EET ESC
Moisture
Percent Moisture
EPA
EET SAV
SM 2540G
Total, Fixed, and Volatile Solids
SM
EET SAV
3050B
Preparation, Metals
SW846
EET SAV
3-154
Ammonia ( Sediments)
EPA
EET SAV
7471 B
Preparation, Mercury
SW846
EET SAV
DI Leach
Deionized Water Leaching Procedure
ASTM
EET ESC
DI Leach
Deionized Water Leaching Procedure
ASTM
EET SAV
Digestion
Digestion, Hot Block
EPA
EET SAV
Protocol References:
ASTM = ASTM International
EPA= US Environmental Protection Agency
MCAWW = "Methods For Chemical Analysis Of Water And Wastes", EPA-600/4-79-020, March 1983 And Subsequent Revisions.
SM = "Standard Methods For The Examination Of Water And Wastewater"
SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.
USDA = "USDA Agriculture Handbook 60, section 2013".
Laboratory References:
EET ESC = Eurofins Raleigh, 102-A Woodwinds Industrial Court, Cary, NC 27511, TEL [phone]
EET PIT = Eurofins Pittsburgh, 301 Alpha Drive, RIDC Park, Pittsburgh, PA 15238, TEL [phone]
EET SAV = Eurofins Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL [phone]
11
12
13
14
Eurofins Raleigh
Page 20 of 27 3/9/2023

Sample Summary
Client: Hunt Environmental Associates
Project/Site: City of Lumberton
Lab Sample ID Client Sample ID Matrix Collected Received
752-3600-1 Q1-2 TCLP VWVTP Solid 02/27/23 09:00 02/27/23 13:22
752-3600-2 Q1-2 VVTP
Solid 02/27/23 09:30 02/27/23 13:22
Job ID: 752-3600-1
12
13
74
Page 21 of 27
Eurofins §4403

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Page 24 of 27
3/9/2023

Login Sample Receipt Checklist
Client: Hunt Environmental Associates Job Number: 752-3600-1
Login Number: 3600
List Number: 1
Creator: Yonish, Rachel
Question
List Source: Eurofins Raleigh
Answer Comment
Radioactivity wasn't checked or is </= background as measured by a survey
True
meter.
The cooler's custody seal, if present, is intact.
True
Sample custody seals, if present, are intact.
True
The cooler or samples do not appear to have been compromised or
True
tampered with.
Samples were received on ice.
True
Cooler Temperature is acceptable.
True
Cooler Temperature is recorded.
True
COC is present.
True
COC is filled out in ink and legible.
True
COC is filled out with all pertinent information.
True
Is the Field Sampler's name present on COC?
True
There are no discrepancies between the containers received and the COC.
True
Samples are received within Holding Time (excluding tests with immediate
True
HTs)
Sample containers have legible labels.
True
Containers are not broken or leaking.
True
Sample collection date/times are provided.
True
Appropriate sample containers are used.
True
Sample bottles are completely filled.
True
Sample Preservation Verified.
True
There is sufficient vol. for all requested analyses, incl. any requested
True
MS/MSDs
Containers requiring zero headspace have no headspace or bubble is
True
<6mm (1/4").
Multiphasic samples are not present.
True
Samples do not require splitting or compositing.
True
Residual Chlorine Checked.
True
12
13
14
Eurofins Raleigh
Page 25 of 27 3/9/2023

Login Sample Receipt Checklist
Client: Hunt Environmental Associates Job Number: 752-3600-1
Login Number: 3600
List Number: 3
Creator: Watson, Debbie
Question
List Source: Eurofins Pittsburgh
List Creation: 03/01/23 12:43 PM
Answer Comment
Radioactivity wasn't checked or is </= background as measured by a survey
N/A
meter.
The cooler's custody seal, if present, is intact.
True
Sample custody seals, if present, are intact.
True
The cooler or samples do not appear to have been compromised or
True
tampered with.
Samples were received on ice.
True
Cooler Temperature is acceptable.
True
Cooler Temperature is recorded.
True
COC is present.
True
COC is filled out in ink and legible.
True
COC is filled out with all pertinent information.
True
Is the Field Sampler's name present on COC?
N/A
There are no discrepancies between the containers received and the COC.
True
Samples are received within Holding Time (excluding tests with immediate
True
HTs)
Sample containers have legible labels.
True
Containers are not broken or leaking.
True
Sample collection date/times are provided.
True
Appropriate sample containers are used.
True
Sample bottles are completely filled.
True
Sample Preservation Verified.
True
There is sufficient vol. for all requested analyses, incl. any requested
True
MS/MSDs
Containers requiring zero headspace have no headspace or bubble is
True
<6mm (1/4").
Multiphasic samples are not present.
True
Samples do not require splitting or compositing.
True
Residual Chlorine Checked.
N/A
12
13
14
Eurofins Raleigh
Page 26 of 27 3/9/2023

Login Sample Receipt Checklist
Client: Hunt Environmental Associates Job Number: 752-3600-1
Login Number: 3600
List Number: 2
Creator: Sims, Robert D
Question
List Source: Eurofins Savannah
List Creation: 02/28/23 11:23 AM
Answer Comment
Radioactivity wasn't checked or is </= background as measured by a survey
N/A
meter.
The cooler's custody seal, if present, is intact.
True
Sample custody seals, if present, are intact.
True
The cooler or samples do not appear to have been compromised or
True
tampered with.
Samples were received on ice.
True
Cooler Temperature is acceptable.
True
Cooler Temperature is recorded.
True
COC is present.
True
COC is filled out in ink and legible.
True
COC is filled out with all pertinent information.
True
Is the Field Sampler's name present on COC?
True
There are no discrepancies between the containers received and the COC.
True
Samples are received within Holding Time (excluding tests with immediate
True
HTs)
Sample containers have legible labels.
True
Containers are not broken or leaking.
True
Sample collection date/times are provided.
True
Appropriate sample containers are used.
True
Sample bottles are completely filled.
True
Sample Preservation Verified.
N/A
There is sufficient vol. for all requested analyses, incl. any requested
True
MS/MSDs
Containers requiring zero headspace have no headspace or bubble is
N/A
<6mm (1/4").
Multiphasic samples are not present.
True
Samples do not require splitting or compositing.
True
Residual Chlorine Checked.
N/A
12
13
14
Eurofins Raleigh
Page 27 of 27 3/9/2023

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Lumberton
W W TP Name: City of Lumberton
Monitoring Period: From l/l/2023 To
WQ Permit Number:
NPDES Number:
3/31/2023
WQ0000672
NCL-024571
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. A (time/temp) ❑
1 Alt B (Alk Treatment) ❑
I Alt. C (Prior Testing) ❑
Alt.D (No Prior Test) ❑
I Process to Further Reduce Pathogengs ❑
If applicable to alternative
performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost 01
Heat Drying ❑
Heat Treatment ❑
Thermophilic ❑
Beta Ray 01
Gamma Ray ❑
Pasteurization ❑
Class B:
JAIL (1) Fecal Density p
Alt. (2) Process to Significantly Reduce Pathogens C,
If applicable to alternative
performed (Class
B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization ❑
I Air Drying ❑
Composting ❑
Aerobic Digestion ❑
Anaerobic Digestion ❑
If applicable to alternative performed (Class A or Class B) complete the following
monitoring data:
Parameter
Allowable Level
in Sludge
Pathogen Density
Number o
Excee-
n
Frequency
of Analysis
Sample
Type
Analytical
Tech -
nioue
MinimumGeo.
Mean
MaximumUnits
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
CFU
144000
470000
1440000
CFU/g
Quarterly
Grab
9222-MF
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per 4 grams
total solid (dry
weight)
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed:
Alt.1 (VS reduction) ❑
Alt. 2 (40-day bench) ❑
Alt. 3 (30-day bench) ,J
Alt. 4 (Spec. OZ uptake) ❑
Alt. 5 (14-Day Aerobic) ❑
Alt. 6 (Alk. Stabilization ❑
Alt 7 (Drying - Stable) ❑
Alt. 8 (Drying - Unstable) ❑
Alt. 9 (Injection) ❑
Alt. 10 (Incorporation) ❑
No vector attraction reduction alternatives were performed ❑
CERTIFICATION STATEMENT (please check the appropriate statement)
`'❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
0 "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note
if you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Michael C Hunt, ORC Michael C Hunt, ORC
Preparer Name and Title (type or print)
i-!wt`l, " 2/20/2024
Land Applier Name and Title (if applicable)(type or print)
Signature of Prepay r* Date Signature of Land Applier (if applicable)
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
Date
DENR FORM PVRF 02T (12/2006)

Cameron Testing Services, Inc. Laboratory Report
NC DENR#654
NC PHHS #37799
US EPA #NC01918
Client:
Enviro-Choice Recycling
CTS Proj.
2302-0028
DWCert#37799
Project:
City of Lumberton
Regulatory
Yes
Sample Information
Sampled
Date 02/02/23
Received
K.
Woodard
Date
02/02/23
Analyses and Results
Lab ID
x a
Sample ID o Analyte
Result
m E
y
in
,
Std. Methods
-s
c
Reference
2302-0028 01
-1 3ludN Or Fec. Coliform-S
1440000
CFUIg
144300
02/03/23 PD
9222D - MF
-2
1150000
CFUIg
1443CO
-3
433000
CFUIg
144300
-4
144000
CFUIg
144300
-5
144000
CFUIg
144300
-6
721429
CFUIg
144300
-7
721000
CFUIg
144300
Geomean
470000
2302-0028 01
02 Sludge cr TS (%)
2.82
^r
001
02/03/23 PD
2540 G JS
03
2.83
°A
0.01
04
2.82
i
0.01
05
2.82
%
0.01
06
2.83
%
C.C1
07
2.82
%
0.01
Report
Review /ej' j��
Project Manager Date c�0� OC L�
219 S. Steele Str. 919-208-4240
Sanford NC 27330 [e-mail]

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tiff eurofins 0
Environment Testing
ANALYTICAL REPORT
PREPARED FOR
Attn: Cody Hunt
Hunt Environmental Associates ■r�
3330 Saddletree Rd
Lumberton, North Carolina 28360
Generated 6/2/2023 12:33:44 PM
JOB DESCRIPTION
City of Lumberton
%� JOB NUMBER
752-7043-1
1

This report may not be reproduced except in full, and with written approval from the laboratory. The results relate only to the
samples tested. For questions please contact the Project Manager at the e-mail address or telephone number listed on this
page.
The test results in this report relate only to the samples as received by the laboratory and will meet all requirements of the
methodology, with any exceptions noted. This report shall not be reproduced except in full, without the express written
approval of the laboratory. All questions should be directed to the Eurofins Environment Testing Southeast, LLC Project
Manager.
IlJI�1'�`11(o Ip
Authorized for release by
Heather Trotter, Project Manager
Heather.Trottera-et.eurofinsus.com
[phone]
Generated
6/2/2023 12:33:44 PM
12
13
14
Eurofins Savannah is a laboratory within Eurofins Environment Testing Southeast, LLC, a company within Eurofins Environment Testing Group of Companies
Page 2 of 29 6/2/2023

Client: Hunt Environmental Associates
Project/Site: City of Lumberton
Laboratory Job ID: 752-7043-1
Table of Contents
Cover Page ..............................................
1
Table of Contents .........................................
3
Definitions/Glossary.......................................
4
Case Narrative ...........................................
5
Detection Summary ........................................
6
Client Sample Results ......................................
7
QC Sample Results ........................................
9
QC Association Summary ...................................
14
Lab Chronicle ............................................
18
Certification Summary ......................................
20
Method Summary .........................................
22
Sample Summary .........................................
23
Chain of Custody ..........................................
24
Receipt Checklists .........................................
27
12
13
14
Page 3 of 29
Eurofins Raleigh
6/2/2023

Definitions/Glossary
Client: Hunt Environmental Associates
Project/Site: City of Lumberton
Qualifiers
Metals
Qualifier Qualifier Description
B Compound was found in the blank and sample.
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
General Chemistry
Job ID:752-7043-1
Qualifier Qualifier Description
4 MS, MSD: The analyte present in the original sample is greater than 4 times the matrix spike concentration; therefore, control limits are not
applicable.
F1 MS and/or MSD recovery exceeds control limits.
HF Field parameter with a holding time of 15 minutes. Test performed by laboratory at client's request.
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
Glossary
Abbreviation These commonly used abbreviations may or may not be present in this report.
tt Listed under the "D" column to designate that the result is reported on a dry weight basis
%R Percent Recovery
CFL Contains Free Liquid
CFU Colony Forming Unit
CNF Contains No Free Liquid
DER Duplicate Error Ratio (normalized absolute difference)
oil Fac Dilution Factor
DL Detection Limit (DoD/DOE)
DL, RA, RE, IN Indicates a Dilution, Re -analysis, Re -extraction, or additional Initial metals/anion analysis of the sample
DLC Decision Level Concentration (Radiochemistry)
EDL Estimated Detection Limit (Dioxin)
LOD Limit of Detection (DoD/DOE)
LOQ Limit of Quantitation (DoD/DOE)
MCL EPA recommended "Maximum Contaminant Level"
MDA
Minimum Detectable Activity (Radiochemistry)
MDC
Minimum Detectable Concentration (Radiochemistry)
MDL
Method Detection Limit
ML
Minimum Level (Dioxin)
MPN
Most Probable Number
MQL
Method Quantitation Limit
NC
Not Calculated
ND
Not Detected at the reporting limit (or MDL or EDL if shown)
NEG
Negative / Absent
POS
Positive / Present
PQL
Practical Quantitation Limit
PRES
Presumptive
QC
Quality Control
RER
Relative Error Ratio (Radiochemistry)
RL
Reporting Limit or Requested Limit (Radiochemistry)
RPD
Relative Percent Difference, a measure ofthe relative difference between two points
TEF
Toxicity Equivalent Factor (Dioxin)
TEQ
Toxicity Equivalent Quotient (Dioxin)
TNTC
Too Numerous To Count
Eurofins Raleigh
Page 4 of 29 6/2/2023

Case Narrative
Client: Hunt Environmental Associates
Project/Site: City of Lumberton
Job ID: 752-7043-1
Laboratory: Eurofins Raleigh
Narrative
Job Narrative
752-7043-1
Comments
No additional comments.
Receipt
The samples were received on 5/16/2023 4:15 PM. Unless otherwise noted below, the samples arrived in good condition, and where
required, properly preserved and on ice. The temperature of the cooler at receipt was 3.60 C.
Metals
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.
General Chemistry
Method Moisture: The following samples were unable to be prepared and/or analyzed for %moisture due to sample matrix (water) : S-2
WTP (752-7043-2).
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
Job ID: 752-7043-1
F47
12
13
14
Eurofins Raleigh
Page 5 of 29 6/2/20g3

Detection Summary
Client: Hunt Environmental Associates
Project/Site: City of Lumberton
Job ID: 752-7043-1
Client Sample ID: S-2 WWTP Lab Sample ID: 752-7043-1
Analyte
Result Qualifier
RL
MDL
Unit
Dil Fac
D
Method
Prep Type
Sodium Adsorption Ratio
34
0.10
0.10
NONE
1
20B
Soluble
Aluminum
16000
760
260
mg/Kg
1
3�
601OD
Total/NA
Calcium
13000 B------------------1900
280
mg/Kg-------------
1
*
601OD
Total/NA
Copper
440
95
19
mg/Kg
1
*
601OD
Total/NA
Magnesium
2500
1900
350
mg/Kg
1
*
601OD
Total/NA
Potassium
4500
3800
420
mg/Kg
1
*
601OD
Total/NA
-----------------------------------------------------------------------------------------------------------------------------------------
Sodium
16000
7600
2100
mg/Kg
1
*
601OD
Total/NA
Zinc
720
76
22
mg/Kg
1
*
601OD
Total/NA
Mercury
0.31 J
0.88
0.28
mg/Kg
1
#
7471B
Total/NA
Ammonia
150
6.0
2.6
mg/Kg
20
350.1-1993 R2.0
Total/NA
Nitrogen, Kjeldahl
68000
19000
11000
mg/Kg
20
*
351.2-1993 R2.0
Total/NA
Phosphorus
15000
1900
1000
mg/Kg
5
*
365.4-1974
Total/NA
Total Solids
2.6
0.10
0.10
%
1
SM 2540G
Total/NA
Nitrate Nitrite as N
820
76
21
mg/Kg
1
*
353.2-1993 R2.0
Soluble
pH
7.2
1
1
SU
1
9045D
Soluble
Temperature
24.7
1
1
Degrees C
1
9045D
Soluble
Client Sample ID: S-2 WTP
Lab Sample ID: 752-7043-2 VA
Analyte
Result
Qualifier
RL
MDL
Unit
Dil Fac D Method Prep Type
Aluminum
990
17
5.9
mg/Kg
1 601OD Total/NA
Calcium
24
J B
43
6.4
mg/Kg
1 601 OD Total/NA
Zinc
0.60
J
1.7
0.50
mg/Kg
1 601OD Total/NA
Nitrogen, Kjeldahl
22
J
24
15
mg/Kg
1 351.2-1993 R2.0 Total/NA
Phosphorus
9.6
J
9.7
5.4
mg/Kg
1 365.4-1974 Total/NA
Temperature
16.3
HF
0.1
0.1
Celsius
1 9045D Total/NA
Soil pH in Water
5.8
HF
0.1
0.1
PH Units
1 9045D Total/NA
Total Solids
0.67
0.10
0.10
%
1 SM 2540G Total/NA
Client Sample ID: S-2 WWTP
Lab Sample ID: 752-7043-3
CAnalyte
Result
Qualifier
RL
MDL
Unit
Dil Fac D Method Prep Type
Flashpoint
>140
Degrees F
1 1010A Total/NA
Client Sample ID: S-2 WTP
Lab Sample ID: 752-7043-4
Analyte
Result
Qualifier
RL
MDL
Unit
Dil Fac D Method Prep Type
Flashpoint
>140
Degrees F
1 1010A Total/NA
This Detection Summary does not include radiochemical test results.
Eurofins Raleigh
Page 6 of 29 6/2/2023

Client Sample Results
Client: Hunt Environmental Associates
Job ID: 752-7043-1
Project/Site: City of Lumberton
Client Sample ID: S-2 WWTP
Lab Sample ID: 752-7043-1
Date Collected: 05/16/23 09:43
Matrix: Solid
Date Received: 05/16/23 16:15
Percent Solids: 2.6
Method: USDA 20B - Sodium Adsorption
Ratio
- Soluble
Analyte
Result
Qualifier
RL
MDL
Unit
D
Prepared
Analyzed oil Fac
Sodium Adsorption Ratio
34
0.10
0.10
NONE
06/02/23 14:17 1
,
Method: SW846 6010D - Metals (ICP)
Analyte
Result
Qualifier
RL
MDL
Unit
D
Prepared
Analyzed oil Fac
Aluminum
16000
760
260
mg/Kg
*
05/18/2316:05
05/19/2317:47 1
Arsenic
<46
76
46
mg/Kg
*
05/18/2316:05
05/19/2317:47 1
Cadmium
<3.8
19
3.8
mg/Kg
*
05/18/2316:05
05/19/2317:47 1
Calcium
13000
B
1900
280
mg/Kg
*
05/18/2316:05
05/19/2317:47 1
Copper
440
95
19
mg/Kg
*
05/18/2316:05
05/19/2317:47 1
Lead
<23
38
23
mg/Kg
*
05/18/2316:05
05/19/2317:47 1
Magnesium
2500
1900
350
mg/Kg
*
05/18/2316:05
05/19/2317:47 1
Molybdenum
<9.9
38
9.9
mg/Kg
*
05/18/2316:05
05/19/2317:47 1
Nickel
<34
150
34
mg/Kg
*
05/18/2316:05
05/19/2317:47 1
Potassium
4500
3800
420
mg/Kg
*
05/18/2316:05
05/19/2317:47 1
Selenium
<42
95
42
mg/Kg
*
05/18/2316:05
05/19/2317:47 1 Is
Sodium
16000
7600
2100
mg/Kg
*
05/18/2316:05
05/19/2317:47 1
Zinc
720
76
22
mg/Kg
*
05/18/2316:05
05/19/2317:47 1
Method: SW846 7471B - Mercury (CVAA)
M
Analyte
Result
Qualifier
RL
MDL
Unit
D
Prepared
Analyzed oil Fac
Mercury
0.31
J
0.88
0.28
mg/Kg
*
05/18/2315:40
05/18/2318:32 1
General Chemistry
Analyte
Result
Qualifier
RL
MDL
Unit
D
Prepared
Analyzed oil Fac
Ammonia (MCAWW 350.1-1993
150
6.0
2.6
mg/Kg
05/20/23 14:15
05/20/23 18:32 20
R2.0)
Nitrogen, Kjeldahl (MCAWW
68000
19000
11000
mg/Kg
*
05/19/23 09:58
05/22/23 14:38 20
351.2-1993 R2.0)
Phosphorus (EPA 365.4-1974)
15000
1900
1000
mg/Kg
*
05/19/23 09:58
05/22/23 09:21 5
Cyanide, Reactive (SW846 9014)
<0.25
0.25
0.25
mg/Kg
05/25/23 00:24
05/30/23 21:01 1
Sulfide, Reactive (SW846 9034)
<150
150
150
mg/Kg
05/25/23 00:22
05/31/23 09:36 1
Total Solids (SM 2540G)
2.6
0.10
0.10
%
05/18/23 16:24 1
General Chemistry - Soluble
Analyte
Result
Qualifier
RL
MDL
Unit
D
Prepared
Analyzed oil Fac
Nitrate Nitrite as N (MCAWW
820
76
21
mg/Kg
05/22/23 17:57 1
353.2-1993 R2.0)
pH (SW846 9045D)
7.2
1
1
Su
05/22/23 14:02 1
Temperature (SW846 9045D)
24.7
1
1
Degrees C
05/22/23 14:02 1
Client Sample ID: S-2 WTP
Lab Sample ID: 752-7043-2
Date Collected: 05/16/23 10:25
Matrix: Solid
Date Received: 05/16/23 16:15
Method: USDA 20B - Sodium Adsorption
Ratio
- Soluble
Analyte
Result
Qualifier
RL
MDL
Unit
D
Prepared
Analyzed oil Fac
Sodium Adsorption Ratio
<0.10
0.10
0.10
NONE
06/02/23 14:18 1
Method: SW846 6010D - Metals (ICP)
Analyte
Result
Qualifier
RL
MDL
Unit
D
Prepared
Analyzed oil Fac
Aluminum
990
17
5.9
mg/Kg
05/18/2316:05
05/19/2317:51 1
Arsenic
<1.0
1.7
1.0
mg/Kg
05/18/2316:05
05/19/2317:51 1
Eurofins Raleigh
Page 7 of 29
6/2/2023

Client Sample Results
Client: Hunt Environmental Associates
Project/Site: City of Lumberton
Job ID: 752-7043-1
Client Sample ID: S-2 WTP Lab Sample ID: 752-7043-2
Date Collected: 05/16/23 10:25 Matrix: Solid
Date Received: 05/16/23 16:15
Method: SW846 6010D - Metals (ICP) (Continued)
Analyte
Result Qualifier
RL
MDL
Unit
D Prepared
Analyzed
Dil Fac
Cadmium
<0.086
0.43
0.086
mg/Kg
05/18/2316:05
05/19/2317:51
1
Calcium
24 J B
43
6.4
mg/Kg
05/18/23 16:05
05/19/23 17:51
1
Copper
<0.43
2.2
0.43
mg/Kg
05/18/2316:05
05/19/2317:51
1
Lead
<0.53
0.86
0.53
mg/Kg
05/18/2316:05
05/19/2317:51
1
-------------------------------------------------------------------------------------------------------------------------------------
Magnesium
<7.8
43
7.8
mg/Kg
05/18/2316:05
05/19/2317:51
1
Molybdenum
<0.22
0.86
0.22
mg/Kg
05/18/2316:05
05/19/2317:51
1
Nickel
<0.78
3.4
0.78
mg/Kg
05/18/2316:05
05/19/2317:51
1
Potassium
<9.5
86
9.5
mg/Kg
05/18/2316:05
05/19/2317:51
1
Selenium
<0.95
2.2
0.95
mg/Kg
05/18/2316:05
05/19/2317:51
1
Sodium
<47
170
47
mg/Kg
05/18/2316:05
05/19/2317:51
1
Zinc
0.60 J
1.7
0.50
mg/Kg
05/18/2316:05
05/19/2317:51
1
Method: SW846 7471B - Mercury (CVAA)
Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac
Mercury <0.0074 0.023 0.0074 mg/Kg 05/18/2315:39 05/18/2318:28 1
General Chemistry
Analyte
Result
Qualifier
RL
MDL
Unit
D Prepared
Analyzed
Dil Fac
Ammonia (MCAWW 350.1-1993 R2.0)
<0.13
F1
0.30
0.13
mg/Kg
05/20/23 14:15
05/20/23 17:39
1
Nitrogen, Kjeldahl (MCAWW
22
J
24
15
mg/Kg
05/19/23 09:58
05/22/23 13:00
1
351.2-1993 R2.0)
Phosphorus (EPA 365.4-1974)
9.6
J
9.7
5.4
mg/Kg
05/19/23 09:58
05/22/23 08:33
1
-----------------------------------------------------------------------------------------------------------------------------------------
Cyanide, Reactive (SW846 9014)
<0.25
0.25
0.25
mg/Kg
05/25/23 00:24
05/30/23 21:02
1
Sulfide, Reactive (SW846 9034)
<150
150
150
mg/Kg
05/25/23 00:22
05/31/23 09:36
1
Temperature (SW846 9045D)
16.3
HF
0.1
0.1
Celsius
05/22/23 16:31
1
-----------------------------------------------------------------------------------------------------------------------------------------
Soil pH in Water (SW846 9045D)
5.8
HF
0.1
0.1
PH Units
05/22/23 16:31
1
Total Solids (SM 2540G)
0.67
0.10
0.10
%
05/18/23 16:24
1
General Chemistry -Soluble
Analyte
Result Qualifier
RL MDL Unit
D Prepared Analyzed Dil Fac
Nitrate Nitrite as N (MCAWW
<0.55
2.0 0.55 mg/Kg
05/22/23 17:58 1
353.2-1993 R2.0)
Client Sample ID: S-2 WWTP
Lab Sample ID: 752-7043-3
Date Collected: 05/16/23 09:43
Matrix: Water
Date Received: 05/16/23 16:15
General Chemistry
Analyte
Result Qualifier
RL MDL Unit
D Prepared Analyzed Dil Fac
Flashpoint (SW846 1010A)
>140
Degrees F
05/22/23 10:02 1
Client Sample ID: S-2 WTP
Lab Sample ID: 752-7043-4
Date Collected: 05/16/23 10:25
Matrix: Water
Date Received: 05/16/23 16:15
General Chemistry
Analyte
Result Qualifier
RL MDL Unit
D Prepared Analyzed Dil Fac
Flashpoint (SW846 1010A)
>140
Degrees F
05/22/23 11:00 1
Eurofins Raleigh
Page 8 of 29 6/2/2023

QC Sample Results
Client: Hunt Environmental Associates
Project/Site: City of Lumberton
Job ID: 752-7043-1
Method: 6010D - Metals (ICP)
Lab Sample ID: MB 680-779368/1-A Client Sample ID: Method Blank
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 779595 Prep Batch: 779368
Analyte
MB MB
Result Qualifier
RL
MDL
Unit
Aluminum
<6.7
20
6.7
mg/Kg
Arsenic
<1.2
2.0
1.2
mg/Kg
Cadmium
<0.098
0.49
0.098
mg/Kg
Calcium
8.64 J
49
7.3
mg/Kg
Copper
<0.49
2.5
0.49
mg/Kg
Lead
<0.60
0.98
0.60
mg/Kg
Magnesium
<8.9
49
8.9
mg/Kg
Molybdenum
<0.25
0.98
0.25
mg/Kg
Nickel
<0.88
3.9
0.88
mg/Kg
Potassium
<11
98
11
mg/Kg
Selenium
<1.1
2.5
1.1
mg/Kg
Sodium
<54
200
54
mg/Kg
Zinc
<0.57
2.0
0.57
mg/Kg
Lab Sample ID: LCS 680-779368/2-A
Matrix: Solid
Analysis Batch: 779595
Analyte
Spike
Added
LCS LCS
Result Qualifier
Unit
Aluminum
472
483
mg/Kg
Arsenic
9.43
8.80
mg/Kg
Cadmium
4.72
4.62
mg/Kg
Calcium
472
486
mg/Kg
Copper
9.43
9.97
mg/Kg
Lead
47.2
43.9
mg/Kg
Magnesium
472
467
mg/Kg
Molybdenum
9.43
9.30
mg/Kg
Nickel
9.43
9.08
mg/Kg
Potassium
660
673
mg/Kg
Selenium
9.43
7.64
mg/Kg
Sodium
472
468
mg/Kg
Zinc
9.43
9.50
mg/Kg
D Prepared
Analyzed
oil Fac
05/18/2316:05
05/19/2316:57
1
05/18/2316:05
05/19/2316:57
1
05/18/2316:05
05/19/2316:57
1
05/18/2316:05
05/19/2316:57
1
05/18/2316:05
05/19/2316:57
1
05/18/2316:05
05/19/2316:57
1
05/18/2316:05
05/19/2316:57
1
05/18/2316:05
05/19/2316:57
1
05/18/2316:05
05/19/2316:57
1
05/18/2316:05
05/19/2316:57
1
05/18/2316:05
05/19/2316:57
1
05/18/2316:05
05/19/2316:57
1
05/18/2316:05
05/19/2316:57
1
Client Sample ID: Lab Control
Sample
Prep Type: Total/NA
Prep Batch:
779368
%Rec
D %Rec
Limits
102
80 _ 120
93
80 _ 120
98
80 _ 120
103
80 _ 120
106
80 _ 120
93
80 _ 120
99
80 _ 120
99
80 _ 120
96
80 _ 120
102
80 _ 120
81
80 _ 120
99
80 _ 120
101
80 _ 120
Method: 7471 B - Mercury (CVAA)
Lab Sample ID: MB 680-779365/12-A Client Sample ID: Method Blank
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 779598 Prep Batch: 779365
Analyte
Mercury
Lab Sample ID: LCS 680-779365/13-A
Matrix: Solid
Analysis Batch: 779598
Analyte
Mercury
MB MB
Result Qualifier RL MDL Unit
<0.0078 0.025 0.0078 mg/Kg
D Prepared Analyzed oil Fac
05/18/2315:39 05/18/2317:33 1
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Prep Batch: 779365
Spike LCS LCS %Rec
Added Result Qualifier Unit D %Rec Limits
0.223 0.218 mg/Kg 97 80 _ 120
Eurofins Raleigh
Page 9 of 29 6/2/2023

QC Sample Results
Client: Hunt Environmental Associates
Project/Site: City of Lumberton
Job ID: 752-7043-1
Method: 1010A - Ignitability, Pensky-Martens Closed -Cup Method
Lab Sample ID: MB 680-779676/1 Client Sample ID: Method Blank
Matrix: Water Prep Type: Total/NA
Analysis Batch: 779676
MB MB
Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac
Flashpoint >140.0 Degrees F 05/22/23 07:16 1
Lab Sample ID: LCS 680-779676/2 Client Sample ID: Lab Control Sample
Matrix: Water Prep Type: Total/NA
Analysis Batch: 779676
Spike LCS LCS %Rec
Analyte Added Result Qualifier Unit D %Rec Limits
Flashpoint 140 148.0 Degrees F 106 96 _ 106
Lab Sample ID: LCSD 680-779676/7 Client Sample ID: Lab Control Sample Dup
Matrix: Water Prep Type: Total/NA
Analysis Batch: 779676
Spike LCSD LCSD %Rec
Analyte Added Result Qualifier Unit D %Rec Limits
Flashpoint 140 148.0 Degrees F 106 96 _ 106
Method: 350.1-1993 R2.0 - Nitrogen, Ammonia
RPD
RPD Limit
0 2
Lab Sample ID: MB 680-779615/1-A
Client Sample ID: Method Blank
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 779618
Prep Batch: 779615
MB MB
Analyte
Result Qualifier
RL
MDL Unit
D Prepared Analyzed Dil Fac
Ammonia
<0.13
0.30
0.13 mg/Kg
05/20/2314:15 05/20/2317:39 1
Lab Sample ID: LCS 680-779615/2-A
Client Sample ID: Lab Control Sample
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 779618
Prep Batch: 779615
Spike
LCS
LCS
%Rec
Analyte
Added
Result
Qualifier
Unit
D %Rec Limits
Ammonia
4.97
3.90
mg/Kg
78 75 _ 125
Lab Sample ID: 752-7043-2 MS
Client Sample ID: S-2 WTP
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 779618
Prep Batch: 779615
Sample
Sample
Spike
MS
MS
%Rec
Analyte
Result
Qualifier
Added
Result
Qualifier
Unit
D %Rec Limits
Ammonia
<0.13
F1
5.00
2.84
F1
mg/Kg
57 75 _ 125
Lab Sample ID: 752-7043-2 MSD
Client Sample ID: S-2 WTP
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 779618
Prep Batch: 779615
Sample
Sample
Spike
MSD
MSD
%Rec RPD
Analyte
Result
Qualifier
Added
Result
Qualifier
Unit
D %Rec Limits RPD Limit
Ammonia
<0.13
F1
4.98
3.05
F1
mg/Kg
61 75 _ 125 7 30
Eurofins Raleigh
Page 10 of 29 6/2/2023

QC Sample Results
Client: Hunt Environmental Associates
Job ID: 752-7043-1
Project/Site: City of Lumberton
Method: 351.2-1993 R2.0 - Nitrogen, Total Nitrogen
Lab Sample ID: MB 680-779465/1-A
Client Sample ID: Method Blank
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 779839
Prep Batch: 779465
MB MB
Analyte Result Qualifier
RL MDL Unit
D Prepared Analyzed Dil Fac
Nitrogen, Kjeldahl <11
19 11 mg/Kg
05/19/23 09:58 05/22/23 12:47 1
Lab Sample ID: LCS 680-779465/2-A
Client Sample ID: Lab Control Sample
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 779839
Prep Batch: 779465
Spike
LCS LCS
%Rec
Analyte
Added
Result Qualifier Unit
D %Rec Limits
Nitrogen, Kjeldahl
150
140 mg/Kg
94 75 _ 125
Lab Sample ID: 752-7043-1 MS
Client Sample ID: S-2 WWTP
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 779839
Prep Batch: 779465
Sample Sample
Spike
MS MS
%Rec
Analyte Result Qualifier
Added
Result Qualifier Unit
D %Rec Limits
Nitrogen, Kjeldahl 68000
7640
76700 4 mg/Kg
112 75 _ 125
Lab Sample ID: 752-7043-1 MSD
Client Sample ID: S-2 WWTP
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 779839
Prep Batch: 779465
Sample Sample
Spike
MSD MSD
%Rec RPD
Analyte Result Qualifier
Added
Result Qualifier Unit
D %Rec Limits RPD Limit
Nitrogen, Kjeldahl 68000
7580
69900 4 mg/Kg
22 75 _ 125 9 40
Method: 353.2-1993 R2.0 - Nitrogen, Nitrate -Nitrite
Lab Sample ID: MB 680-779783/1-A
Client Sample ID: Method Blank
Matrix: Solid
Prep Type: Soluble
Analysis Batch: 780018
MB MB
Analyte
Result Qualifier
RL
MDL Unit
D Prepared Analyzed Dil Fac
Nitrate Nitrite as N
<0.54
2.0
0.54 mg/Kg
05/22/23 17:48 1
Lab Sample ID: LCS 680-779783/4-A
Client Sample ID: Lab Control Sample
Matrix: Solid
Prep Type: Soluble
Analysis Batch: 780018
Spike
LCS
LCS
%Rec
Analyte
Added
Result
Qualifier
Unit D %Rec Limits
Nitrate Nitrite as N
19.6
18.7
mg/Kg 96 80 _ 120
Lab Sample ID: LCSD 680-779783/5-A
Client Sample ID: Lab Control Sample Dup
Matrix: Solid
Prep Type: Soluble
Analysis Batch: 780018
Spike
LCSD
LCSD
%Rec RPD
Analyte
Added
Result
Qualifier
Unit D %Rec Limits RPD Limit
Nitrate Nitrite as N
20.0
18.8
mg/Kg 94 80 _ 120 0 20
Eurofins Raleigh
Page 11 of 29 6/2/2023

QC Sample Results
Client: Hunt Environmental Associates
Job ID: 752-7043-1
Project/Site: City of Lumberton
Method: 365.4-1974 - Phosphorus, Total
Lab Sample ID: MB 680-779465/1-A
Client Sample ID: Method Blank
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 779732
Prep Batch: 779465
MB MB
Analyte Result Qualifier
RL MDL Unit
D Prepared Analyzed Dil Fac
Phosphorus <4.1
7.5 4.1 mg/Kg
05/19/23 09:58 05/22/23 08:23 1
Lab Sample ID: LCS 680-779465/2-A
Client Sample ID: Lab Control Sample
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 779732
Prep Batch: 779465
Spike
LCS LCS
%Rec
Analyte
Added
Result Qualifier Unit
D %Rec Limits
Phosphorus
150
151 mg/Kg
101 70.130
Lab Sample ID: 752-7043-1 MS
Client Sample ID: S-2 WWTP
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 779732
Prep Batch: 779465
Sample Sample
Spike
MS MS
%Rec
Analyte Result Qualifier
Added
Result Qualifier Unit
D %Rec Limits
Phosphorus 15000
7640
23000 mg/Kg
106 70_130
Lab Sample ID: 752-7043-1 MSD
Client Sample ID: S-2 WWTP
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 779732
Prep Batch: 779465
Sample Sample
Spike
MSD MSD
%Rec RPD
Analyte Result Qualifier
Added
Result Qualifier Unit
D %Rec Limits RPD Limit
Phosphorus 15000
7580
23600 mg/Kg
115 70_130 3 30
Method: 9014 - Cyanide, Reactive
Lab Sample ID: MB 400-626429/1-A
Client Sample ID: Method Blank
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 627136
Prep Batch: 626429
MB MB
Analyte Result Qualifier
RL MDL Unit
D Prepared Analyzed Dil Fac
Cyanide, Reactive <0.25
0.25 0.25 mg/Kg
05/24/23 23:08 05/30/23 20:51 1
Lab Sample ID: LCS 400-626429/2-A
Client Sample ID: Lab Control Sample
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 627136
Prep Batch: 626429
Spike
LCS LCS
%Rec
Analyte
Added
Result Qualifier Unit
D %Rec Limits
Cyanide, Reactive
1.00
0.619 mg/Kg
62 10 _ 110
Lab Sample ID: MRL 400-627136/13
Client Sample ID: Lab Control Sample
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 627136
Spike
MRL MRL
%Rec
Analyte
Added
Result Qualifier Unit
D %Rec Limits
Cyanide, Reactive
0.00500
<0.25 mg/Kg
112 50 _ 150
Eurofins Raleigh
Page 12 of 29 6/2/2023

QC Sample Results
Client: Hunt Environmental Associates
Project/Site: City of Lumberton
Job ID: 752-7043-1
Method: 9034 - Sulfide, Reactive
Lab Sample ID: MB 400-626428/1-A Client Sample ID: Method Blank
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 627171 Prep Batch: 626428
MB MB
Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac
Sulfide, Reactive <150 150 150 mg/Kg 05/24/23 23:07 05/31/23 09:36 1
Lab Sample ID: LCS 400-626428/2-A Client Sample ID: Lab Control Sample
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 627171 Prep Batch: 626428
Spike LCS LCS %Rec
Analyte Added Result Qualifier Unit D %Rec Limits
Sulfide, Reactive 993 151 mg/Kg 15 10 _ 110
Method: 9045D - pH
Lab Sample ID: LCS 680-779868/4
Matrix: Solid
Analysis Batch: 779868
Spike
Analyte
Added
pH
7.01
Lab Sample ID: 752-7043-1 DU
Matrix: Solid
Analysis Batch: 2919
Sample Sample
Analyte
Result Qualifier
pH
7.2
Temperature
24.7
Method: SM 2540G - Total, Fixed, and Volatile Solids
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
LCS
LCS
%Rec
Result
Qualifier
Unit
D %Rec Limits
7.0
PH Units
100 79 _ 126
Client Sample ID: S-2 WWTP
Prep Type: Soluble
DU
DU
RPD
Result
Qualifier
Unit
D RPD Limit
7.2
SU
0.06 25
24.7
Degrees C
0
Lab Sample ID: MB 680-779376/1 Client Sample ID: Method Blank
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 779376
MB MB
Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac
Total Solids 100 0.10 0.10 % 05/18/23 16:24 1
Lab Sample ID: 752-7043-1 DU Client Sample ID: S-2 WWTP
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 779376
Sample Sample DU DU RPD
Analyte Result Qualifier Result Qualifier Unit D RPD Limit
Total Solids 2.6 2.61 % 0.6 5
Page 13 of 29
Eurofins Raleigh
6/2/2023

QC Association Summary
Client: Hunt Environmental Associates
Project/Site: City of Lumberton
Metals
Analysis Batch: 436876
Job ID: 752-7043-1
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
752-7043-1
S-2 WVVrP
Soluble
Solid
20B
752-7043-2
S-2 WTP
Soluble
Solid
20B
Prep Batch: 779365
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
752-7043-1
S-2 WWTP
Total/NA
Solid
7471B
752-7043-2
S-2 WTP
Total/NA
Solid
7471B
MB 680-779365/12-A
Method Blank
Total/NA
Solid
7471B
------------------------------------------
�LCS 680-779365/13-A
Lab Control Sample
Total/NA
Solid
7471B
Prep Batch: 779368
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
752-7043-1
S-2 WWTP
Total/NA
Solid
3050B
752-7043-2
S-2 WTP
Total/NA
Solid
3050B
MB 680-779368/1-A
Method Blank
Total/NA
Solid
3050B
-----------------------------------------------------------------------------------------------------------------------------------------
LCS 680-779368/2-A
Lab Control Sample
Total/NA
Solid
3050B
Analysis Batch: 779595
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
752-7043-1
S-2 WWTP
Total/NA
Solid
601 OD
779368
752-7043-2
S-2 WTP
Total/NA
Solid
601 OD
779368
MB 680-779368/1-A
Method Blank
Total/NA
Solid
601 OD
779368
LCS 680-779368/2-A
Lab Control Sample
Total/NA
Solid
601 OD
779368
Analysis Batch: 779598
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
752-7043-1
S-2 WWTP
Total/NA
Solid
7471B
779365
752-7043-2
S-2 WTP
Total/NA
Solid
7471B
779365
MB 680-779365/12-A
Method Blank
Total/NA
Solid
7471B
779365
LCS 680-779365/13-A
Lab Control Sample
Total/NA
Solid
7471B
779365
General Chemistry
Analysis Batch: 2919
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
752-7043-1
S-2 WWTP
Soluble
Solid
9045D
3032
LCS 7523032/2-A
Lab Control Sample
Soluble
Solid
9045D
3032
752-7043-1 DU
S-2 WWTP
Soluble
Solid
9045D
3032
Leach Batch: 3032
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
752-7043-1
S-2 WWTP
Soluble
Solid
DI Leach
LCS 7523032/2-A
Lab Control Sample
Soluble
Solid
DI Leach
752-7043-1 DU
S-2 WWTP
Soluble
Solid
DI Leach
Prep Batch: 626428
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
752-7043-1
S-2 WWTP
Total/NA
Solid
7.3.4
752-7043-2
S-2 WTP
Total/NA
Solid
7.3.4
MB 400-626428/1-A
Method Blank
Total/NA
Solid
7.3.4
LLCS 400-626428/2-A Lab Control Sample Total/NA Solid 7.3.4
0
Eurofins Raleigh
Page 14 of 29 6/2/2023

QC Association Summary
Client: Hunt Environmental Associates
Job ID: 752-7043-1
Project/Site: City of Lumberton
General Chemistry
Prep Batch: 626429
Lab Sample ID Client Sample ID
Prep Type
Matrix
Method Prep Batch
752-7043-1 S-2 WWTP
Total/NA
Solid
7.3.3
752-7043-2 S-2 WTP
Total/NA
Solid
7.3.3
MB 400-626429/1-A Method Blank
Total/NA
Solid
7.3.3
LCS 400-626429/2-A Lab Control Sample
Total/NA
Solid
7.3.3
Analysis Batch: 627136
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
752-7043-1
S-2 WWTP
Total/NA
Solid
9014
626429
752-7043-2
S-2 WTP
Total/NA
Solid
9014
626429
MB 400-626429/1-A
Method Blank
Total/NA
Solid
9014
626429
-----------------------------------------------------------------------------------------------------------------------------------------
LCS 400-626429/2-A
Lab Control Sample
Total/NA
Solid
9014
626429
MRL 400-627136/13
Lab Control Sample
Total/NA
Solid
9014
Analysis Batch: 627171
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
752-7043-1
S-2 WWTP
Total/NA
Solid
9034
626428
752-7043-2
S-2 WTP
Total/NA
Solid
9034
626428
MB 400-626428/1-A
Method Blank
Total/NA
Solid
9034
626428
LCS 400-626428/2-A
Lab Control Sample
Total/NA
Solid
9034
626428
Analysis Batch: 779376
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
752-7043-1
S-2 WWTP
Total/NA
Solid
SM 2540G
752-7043-2
S-2 WTP
Total/NA
Solid
SM 2540G
MB 680-779376/1
Method Blank
Total/NA
Solid
SM 2540G
752-7043-1 DU
S-2 WWTP
Total/NA
Solid
SM 2540G
Prep Batch: 779465
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
752-7043-1
S-2 WWTP
Total/NA
Solid
Digestion
752-7043-2
S-2 WTP
Total/NA
Solid
Digestion
MB 680-779465/1-A
--------------------------------------------------------------------------------------------------------------------------
Method Blank
Total/NA
Solid
Digestion
LCS 680-779465/2-A
Lab Control Sample
Total/NA
Solid
Digestion
752-7043-1 MS
S-2 WWTP
Total/NA
Solid
Digestion
752-7043-1 MSD
S-2 WWTP
Total/NA
Solid
Digestion
Analysis Batch: 779483
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
752-7043-1
S-2 WWTP
Total/NA
Solid
Moisture
Prep Batch: 779615
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method Prep Batch
752-7043-1
S-2 WWTP
Total/NA
Solid
3-154
752-7043-2
S-2 WTP
Total/NA
Solid
3-154
MB 680-779615/1-A
Method Blank
Total/NA
Solid
3-154
------------------------------------------------------------------------------------------------------------------------------
LCS 680-779615/2-A
Lab Control Sample
Total/NA
Solid
3-154
752-7043-2 MS
S-2 WTP
Total/NA
Solid
3-154
752-7043-2 MSD
S-2 WTP
Total/NA
Solid
3-154
Eurofins Raleigh
Page 15 of 29 6/2/2023

QC Association Summary
Client: Hunt Environmental Associates
Project/Site: City of Lumberton
General Chemistry
Analysis Batch: 779618
Job ID: 752-7043-1
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
752-7043-1
S-2 WWTP
Total/NA
Solid
350.1-1993 R2.0
779615
752-7043-2
S-2 WTP
Total/NA
Solid
350.1-1993 R2.0
779615
MB 680-779615/1-A
Method Blank
Total/NA
Solid
350.1-1993 R2.0
779615
LCS 680-779615/2-A
- - - - - -
Lab Control Sample
- - - -
Total/NA
Solid
350.1-1993 R2.0
779615
752-7043-2 MS
S-2 WTP
Total/NA
Solid
350.1-1993 R2.0
779615
752-7043-2 MSD
S-2 WTP
Total/NA
Solid
350.1-1993 R2.0
779615
Analysis Batch: 779676
0
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
752-7043-3
S-2 WWTP
Total/NA
Water
1010A
752-7043-4
S-2 WTP
Total/NA
Water
1010A
MB 680-779676/1
Method Blank
Total/NA
Water
1010A
-----------------------------------------------------------------------------------------------------------------------
LCS 680-779676/2
Lab Control Sample
Total/NA
Water
1010A
LCSD 680-779676/7
Lab Control Sample Dup
Total/NA
Water
1010A
Analysis Batch: 779732
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
752-7043-1
S-2 WWTP
Total/NA
Solid
365.4-1974
752-7043-2
S-2 WTP
Total/NA
Solid
365.4-1974
MB 680-779465/1-A
Method Blank
Total/NA
Solid
365.4-1974
--------------------------------------------------------------------------------
LCS 680-779465/2-A
Lab Control Sample
------
Total/NA
------------------
Solid
----------------------
365.4-1974
752-7043-1 MS
S-2 WWTP
Total/NA
Solid
365.4-1974
752-7043-1 MSD
S-2 WWTP
Total/NA
Solid
365.4-1974
Leach Batch: 779783
Prep Batch
Prep Batch
779465
779465
779465
779465
779465
779465
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method Prep Batch
752-7043-1
S-2 WWTP
Soluble
Solid
DI Leach
752-7043-2
S-2 WTP
Soluble
Solid
DI Leach
MB 680-779783/1-A
Method Blank
Soluble
Solid
DI Leach
---------------------------------------------------------------------------------------------------------------------------
LCS 680-779783/4-A
Lab Control Sample
Soluble
Solid
DI Leach
LCSD 680-779783/5-A
Lab Control Sample Dup
Soluble
Solid
DI Leach
Analysis Batch: 779839
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
752-7043-1
S-2 WWTP
Total/NA
Solid
351.2-1993 R2.0
779465
752-7043-2
S-2 WTP
Total/NA
Solid
351.2-1993 R2.0
779465
MB 680-779465/1-A
Method Blank
Total/NA
Solid
351.2-1993 R2.0
779465
-----------------------------------------------------------------------------------------------------------------------------------
LCS 680-779465/2-A
Lab Control Sample
Total/NA
Solid
351.2-1993 R2.0
779465
752-7043-1 MS
S-2 WWTP
Total/NA
Solid
351.2-1993 R2.0
779465
752-7043-1 MSD
S-2 WWTP
Total/NA
Solid
351.2-1993 R2.0
779465
Analysis Batch: 779868
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
752-7043-2
S-2 WTP
Total/NA
Solid
9045D
LCS 680-779868/4
Lab Control Sample
Total/NA
Solid
9045D
Analysis Batch: 780018
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
752-7043-1
S-2 WWTP
Soluble
Solid
353.2-1993 R2.0
779783
752-7043-2
S-2 WTP
Soluble
Solid
353.2-1993 R2.0
779783
MB 680-779783/1-A
Method Blank
Soluble
Solid
353.2-1993 R2.0
779783
Eurofins Raleigh
Page 16 of 29 6/2/2023

QC Association Summary
Client: Hunt Environmental Associates
Project/Site: City of Lumberton
General Chemistry (Continued)
Analysis Batch: 780018 (Continued)
Lab Sample ID Client Sample ID
LCS 680-779783/4-A Lab Control Sample
LCSD 680-779783/5-A Lab Control Sample Dup
Job ID:752-7043-1
Prep Type Matrix Method Prep Batch
Soluble Solid 353.2-1993 R2.0 779783
Soluble Solid 353.2-1993 R2.0 779783
0
12
13
14
Eurofins Raleigh
Page 17 of 29 6/2/2023

Lab Chronicle
Client: Hunt Environmental Associates
Project/Site: City of Lumberton
Job ID: 752-7043-1
Client Sample ID: S-2 WWTP Lab Sample ID: 752-7043-1
Date Collected: 05/16/23 09:43 Matrix: Solid
Date Received: 05/16/23 16:15
Prep Type
Batch
Type
Batch
Method
Dilution
Run Factor
Batch
Number Analyst
Lab
Prepared
or Analyzed
Soluble
Analysis
20B
1
436876
RSR
EET PIT
06/02/23 14:17
Total/NA
Prep
3-154
779615
PB
EET SAV
05/20/23 14:15
Total/NA
Analysis
350.1-1993 R2.0
20
779618
PB
EET SAV
05/20/23 18:32
Total/NA
Prep
7.3.3
626429
JP
EET PEN
05/25/23 00:24
Total/NA
Analysis
9014
1
627136
DEK
EET PEN
05/30/23 21:01
Total/NA
Prep
7.3.4
626428
JP
EET PEN
05/25/23 00:22
Total/NA
Analysis
9034
1
627171
JP
EET PEN
05/31/23 09:36
Soluble
Leach
DI Leach
3032
MDF
EET ESC
05/22/23 13:31
Soluble
Analysis
9045D
1
2919
CB
EET ESC
05/22/23 14:02
Total/NA
Analysis
Moisture
1
779483
KF
EET SAV
05/19/23 10:56
Total/NA
Analysis
SM 2540G
1
779376
PG
EET SAV
05/18/23 16:24
Client Sample ID: S-2 WWTP
Date Collected: 05/16/23 09:43
Date Received: 05/16/23 16:15
Batch
Prep Type Type
Batch
Method Run
Total/NA Prep
3050B
Total/NA Analysis
601OD
Total/NA Prep
7471 B
Total/NA Analysis
7471B
Total/NA Prep
Digestion
Total/NA Analysis
351.2-1993 R2.0
Soluble Leach
DI Leach
Soluble Analysis
353.2-1993 R2.0
Total/NA Prep
Digestion
Total/NA Analysis
365.4-1974
Client Sample ID: S-2 WTP
Date Collected: 05/16/23 10:25
Date Received: 05/16/23 16:15
Lab Sample ID: 752-7043-1
Matrix: Solid
Percent Solids: 2.6
0
Dilution
Batch
Prepared
Factor
Number
Analyst
Lab
or Analyzed
m
779368
BCB
EET SAV
05/18/23 16:05
1
779595
BJB
EET SAV
05/19/23 17:47
779365
BCB
EET SAV
05/18/23 15:40
1
779598
BCB
EET SAV
05/18/23 18:32
779465
SM
EET SAV
05/19/23 09:58
20
779839
AS
EET SAV
05/22/23 14:38
779783
AF
EET SAV
05/22/23 13:12
1
780018
AF
EET SAV
05/22/23 17:57
779465
SM
EET SAV
05/19/23 09:58
5
779732
AS
EET SAV
05/22/23 09:21
Lab Sample ID: 752-7043-2
Matrix: Solid
Prep Type
Batch
Type
Batch
Method
Dilution
Run Factor
Batch
Number Analyst
Lab
Prepared
or Analyzed
Soluble
Analysis
20B
1
436876
RSR
EET PIT
06/02/23 14:18
Total/NA
Prep
3050B
779368
BCB
EET SAV
05/18/23 16:05
Total/NA
Analysis
6010D
1
779595
BJB
EET SAV
05/19/23 17:51
Total/NA
Prep
7471 B
779365
BCB
EET SAV
05/18/23 15:39
Total/NA
Analysis
7471B
1
779598
BCB
EET SAV
05/18/2318:28
Total/NA
Prep
3-154
779615
PB
EET SAV
05/20/23 14:15
Total/NA
Analysis
350.1-1993 R2.0
1
779618
PB
EET SAV
05/20/23 17:39
Total/NA
Prep
Digestion
779465
SM
EET SAV
05/19/23 09:58
Total/NA
Analysis
351.2-1993 R2.0
1
779839
AS
EET SAV
05/22/23 13:00
Soluble
Leach
DI Leach
779783
AF
EET SAV
05/22/23 13:12
Soluble
Analysis
353.2-1993 R2.0
1
780018
AF
EET SAV
05/22/23 17:58
Eurofins Raleigh
Page 18 of 29 6/2/2023

Lab Chronicle
Client: Hunt Environmental Associates
Job ID: 752-7043-1
Project/Site: City of Lumberton
Client Sample ID: S-2 WTP
Lab Sample ID: 752-7043-2
Date Collected: 05/16/23 10:25
Matrix: Solid
Date Received: 05/16/23 16:15
Batch Batch
Dilution
Batch
Prepared
Prep Type Type Method
Run Factor
Number
Analyst
Lab
or Analyzed
Total/NA Prep Digestion
779465
SM
EET SAV
05/19/23 09:58
Total/NA Analysis 365.4-1974
1
779732
AS
EET SAV
05/22/23 08:33
Total/NA Prep 7.3.3
626429
JP
EET PEN
05/25/23 00:24
Total/NA Analysis 9014
1
627136
DEK
EET PEN
05/30/23 21:02
Total/NA Prep 7.3.4
626428
JP
EET PEN
05/25/23 00:22
Total/NA Analysis 9034
1
627171
JP
EET PEN
05/31/23 09:36
Total/NA Analysis 9045D
1
779868
SM
EET SAV
05/22/23 16:31
•
Total/NA Analysis SM 2540G
1
779376
PG
EET SAV
05/18/23 16:24
Client Sample ID: S-2 WWTP
Lab Sample ID: 752-7043-3
Date Collected: 05/16/23 09:43
Matrix: Water
Date Received: 05/16/23 16:15
Batch Batch
Dilution
Batch
Prepared
Prep Type Type Method
Run Factor
Number
Analyst
Lab
or Analyzed
Total/NA Analysis 1010A
1
779676
AS
EET SAV
05/22/23 10:02
Client Sample ID: S-2 WTP
Lab Sample ID: 752-7043-4
Date Collected: 05/16/23 10:25
Matrix: Water
Date Received: 05/16/23 16:15
Batch Batch
Dilution
Batch
Prepared
Prep Type Type Method
Run Factor
Number
Analyst
Lab
or Analyzed
Total/NA Analysis 1010A
1
779676
AS
EET SAV
05/22/23 11:00
Laboratory References:
EET ESC = Eurofins Raleigh, 102-A Woodwinds Industrial
Court, Cary, NC 27511, TEL [phone]
EET PEN = Eurofins Pensacola, 3355 McLemore Drive, Pensacola, FL 32514, TEL [phone]
EET PIT = Eurofins Pittsburgh, 301 Alpha Drive, RIDC Park, Pittsburgh, PA 15238, TEL [phone]
EET SAV = Eurofins Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL [phone]
Page 19 of 29
Eurofins Raleigh
6/2/2023

Accreditation/Certification Summary
Client: Hunt Environmental Associates Job ID: 752-7043-1
Project/Site: City of Lumberton
Laboratory: Eurofins Raleigh
Unless otherwise noted, all analytes for this laboratory were covered under each accreditation/certification below.
Authority Program Identification Number Expiration Date
North Carolina (WW/SW) State 591 12-31-23
The following analytes are included in this report, but the laboratory is not certified by the governing authority. This list may include analytes for which
the agency does not offer certification.
Analysis Method Prep Method Matrix Analyte
9045D Solid Temperature
Laboratory: Eurofins Pensacola
All accreditations/certifications held by this laboratory are listed. Not all accreditations/certifications are applicable to this report.
Authority
Program
Identification Number
Expiration Date
Alabama
State
40150
06-30-23
ANAB
ISO/IEC 17025
L2471
02-22-26
Arkansas DEQ
State
88-0689
09-01-23
-----------------------------------------------
California
--------------------------
State
-------------------------
2510
----------------------
06-30-23
Florida
NELAP
E81010
06-30-23
Georgia
State
E81010(FL)
06-30-23
Illinois
NELAP
200041
10-09-23
Kansas
NELAP
E-10253
10-31-23
Kentucky (UST)
State
53
06-30-23
------------------------------------------------------------------------------------------------------------------------
Louisiana (All)
NELAP
30976
06-30-23
Louisiana (DW)
State
LA017
12-31-23
Maryland
State
233
09-30-23
Michigan
State
9912
06-30-23
North Carolina (WW/SW)
State
314
12-31-23
Oklahoma
NELAP
9810
08-31-23
Pennsylvania
NELAP
68-00467
01-31-24
South Carolina
State
96026
06-30-23
Tennessee
State
TN02907
06-30-23
------------------------------------------------------------------------------------------------------------------------
Texas
NELAP
T104704286
09-30-23
US Fish & Wildlife
US Federal Programs
A22340
06-30-23
USDA
US Federal Programs
FLGNV23001
01-08-26
------------------------------------------------------------------------------------------------------------------------
USDA
US Federal Programs
P330-21-00056
05-17-24
Virginia NELAP 460166 06-14-23
West Virginia DEP State 136 03-31-24
Laboratory: Eurofins Pittsburgh
All accreditations/certifications held by this laboratory are listed. Not all accreditations/certifications are applicable to this report.
Authority
Program
Identification Number
Expiration Date
Arkansas DEQ
State
19-033-0
06-27-23
California
State
2891
04-30-24
Connecticut
State
PH-0688
09-30-24
Florida
NELAP
E871008
06-30-23
Georgia
State
PA 02-00416
04-30-24
Illinois
NELAP
004375
06-30-24
Kansas
NELAP
E-10350
01-31-24
Kentucky (UST)
State
162013
04-30-23
Kentucky (WW)
State
KY98043
12-31-23
Louisiana
NELAP
04041
06-30-22
Louisiana (All)
NELAP
04041
06-30-23
Accreditation/Certification renewal pending - accreditation/certification considered valid.
12
13
14
Eurofins Raleigh
Page 20 of 29 6/2/2023

Accreditation/Certification Summary
Client: Hunt Environmental Associates
Project/Site: City of Lumberton
Laboratory: Eurofins Pittsburgh (Continued)
All accreditations/certifications held by this laboratory are listed. Not all accreditations/certifications are applicable to this report.
Job ID:752-7043-1
Authority
Program
Identification Number
Expiration Date
Maine
State
PA00164
03-06-24
-----------------------------------------------
Minnesota
--------------------------
NELAP
-------------------------
042-999-482
----------------------
12-31-23
New Hampshire
NELAP
2030
04-04-24
New Jersey
NELAP
PA005
06-30-23
New York
NELAP
11182
04-01-24
North Carolina (WW/SW)
State
434
12-31-23
North Dakota
State
R-227
04-30-23'
Oregon
NELAP
PA-2151
02-06-24
Pennsylvania
NELAP
02-00416
04-30-24
Rhode Island
State
LA000362
12-31-22'
------------------------------------------------------------------------------------------------------------------------
South Carolina
State
89014
04-30-23'
Texas
NELAP
T104704528
03-31-24
US Fish & Wildlife
US Federal Programs
058448
03-31-24
------------------------------------------------------------------------------------------------------------------------
USDA
US Federal Programs
P330-16-00211
06-21-24
Utah
NELAP
PA001462019-8
05-31-23'
Virginia
NELAP
10043
09-14-23
------------------------------------------------------------------------------------------------------------------------
West Virginia DEP
State
142
03-31-24
Wisconsin
State
998027800
08-31-23
Laboratory: Eurofins Savannah
Unless otherwise noted, all analytes for this laboratory were covered under each accreditation/certification below.
Authority
North Carolina (WW(SW)
Program
State
Identification Number Expiration Date
269 12-31-23
The following analytes are included in this report, but the laboratory is not certified by the governing authority. This list may include analytes for which
the agency does not offer certification.
Analysis Method Prep Method Matrix Analyte
1010A Water Flashpoint
350.1-1993 R2.0
3-154
Solid
Ammonia
351.2-1993 R2.0
Digestion
Solid
Nitrogen, Kjeldahl
353.2-1993 R2.0
Solid
Nitrate Nitrite as N
365.4-1974
Digestion
Solid
Phosphorus
9045D
Solid
Soil pH in Water
9045D
Solid
Temperature
Moisture
Solid
Percent Moisture
Moisture
Solid
Percent Solids
SM 2540G
Solid
Total Solids
Accreditation/Certification renewal pending - accreditation/certification considered valid.
12
13
14
Eurofins Raleigh
Page 21 of 29 6/2/2023

Method Summary
Client: Hunt Environmental Associates
Project/Site: City of Lumberton
Job ID:752-7043-1
Method
Method Description
Protocol
Laboratory
20B
Sodium Adsorption Ratio
USDA
EET PIT
601 OD
Metals (ICP)
SW846
EET SAV
7471B
Mercury (CVAA)
SW846
EET SAV
1010A
Ignitability, Pensky-Martens Closed -Cup Method
SW846
EET SAV
350.1-1993 R2.0
Nitrogen, Ammonia
MCAWW
EET SAV
351.2-1993 R2.0
Nitrogen, Total Nitrogen
MCAWW
EET SAV
353.2-1993 R2.0
Nitrogen, Nitrate -Nitrite
MCAWW
EET SAV
365.4-1974
Phosphorus, Total
EPA
EET SAV
9014
Cyanide, Reactive
SW846
EET PEN
------------------------------------------------------------------------------------------------------------------------------------------
9034
Sulfide, Reactive
SW846
EET PEN
9045D
pH
SW846
EET ESC
9045D
pH
SW846
EET SAV
------------------------------------------------------------------------------------------------------------------------------------------
Moisture
Percent Moisture
EPA
EET SAV
SM 2540G
Total, Fixed, and Volatile Solids
SM
EET SAV
3050B
Preparation, Metals
SW846
EET SAV
------------------------------------------------------------------------------------------------------------------------------------------
3-154
Ammonia ( Sediments)
EPA
EET SAV
7.3.3
Cyanide, Reactive
SW846
EET PEN
7.3.4
Sulfide, Reactive
SW846
EET PEN
7471 B
Preparation, Mercury
SW846
EET SAV
DI Leach
Deionized Water Leaching Procedure
ASTM
EET ESC
DI Leach
Deionized Water Leaching Procedure
ASTM
EET SAV
Digestion
Digestion, Hot Block
EPA
EET SAV
Protocol References:
ASTM = ASTM International
EPA = US Environmental Protection Agency
MCAWW = "Methods For Chemical Analysis Of Water And Wastes", EPA-600/4-79-020, March 1983 And Subsequent Revisions.
SM = "Standard Methods For The Examination OF Water And Wastewater"
SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.
USDA = "USDA Agriculture Handbook 60, section 2013".
Laboratory References:
EET ESC = Eurofins Raleigh, 102-A Woodwinds Industrial Court, Cary, NC 27511, TEL [phone]
EET PEN = Eurofins Pensacola, 3355 McLemore Drive, Pensacola, FL 32514, TEL [phone]
EET PIT = Eurofins Pittsburgh, 301 Alpha Drive, RIDC Park, Pittsburgh, PA 15238, TEL [phone]
EET SAV = Eurofins Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL [phone]
11
12
13
14
Eurofins Raleigh
Page 22 of 29 6/2/2023

Sample Summary
Client: Hunt Environmental Associates
Project/Site: City of Lumberton
Lab Sample ID
Client Sample ID
Matrix
Collected
Received
752-7043-1
S-2 WWTP
Solid
05/16/23 09:43
05/16/23 16:15
752-7043-2
S-2 WTP
Solid
05/16/23 10:25
05/16/23 16:15
752-7043-3
S-2 WWTP
Water
05/16/23 09:43
05/16/23 16:15
752-7043-4
S-2 WTP
Water
05/16/23 10:25
05/16/23 16:15
Job ID: 752-7043-1
12
13
74
Eurofins Raleigh
Page 23 of 29 6/2/20g3

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Page 26 of 29
6/2/2023

Login Sample Receipt Checklist
Client: Hunt Environmental Associates Job Number: 752-7043-1
Login Number: 7043
List Number: 1
Creator: Yonish, Rachel
Question
List Source: Eurofins Raleigh
Answer Comment
Radioactivity wasn't checked or is </= background as measured by a survey
True
meter.
The cooler's custody seal, if present, is intact.
True
Sample custody seals, if present, are intact.
True
The cooler or samples do not appear to have been compromised or
True
tampered with.
Samples were received on ice.
True
Cooler Temperature is acceptable.
True
Cooler Temperature is recorded.
True
COC is present.
True
COC is filled out in ink and legible.
True
COC is filled out with all pertinent information.
True
Is the Field Sampler's name present on COC?
True
There are no discrepancies between the containers received and the COC.
True
Samples are received within Holding Time (excluding tests with immediate
True
HTs)
Sample containers have legible labels.
True
Containers are not broken or leaking.
True
Sample collection date/times are provided.
True
Appropriate sample containers are used.
True
Sample bottles are completely filled.
True
Sample Preservation Verified.
True
There is sufficient vol. for all requested analyses, incl. any requested
True
MS/MSDs
Containers requiring zero headspace have no headspace or bubble is
True
<6mm (1/4").
Multiphasic samples are not present.
True
Samples do not require splitting or compositing.
True
Residual Chlorine Checked.
True
[L4
Eurofins Raleigh
Page 27 of 29 6/2/2023

Login Sample Receipt Checklist
Client: Hunt Environmental Associates Job Number: 752-7043-1
Login Number: 7043
List Number: 3
Creator: Peckinpaugh, Marshall
Question
List Source: Eurofins Pensacola
List Creation: 05/20/23 09:14 AM
Answer Comment
Radioactivity wasn't checked or is </= background as measured by a survey
True
meter.
The cooler's custody seal, if present, is intact.
True
Sample custody seals, if present, are intact.
N/A
The cooler or samples do not appear to have been compromised or
True
tampered with.
Samples were received on ice.
True
Cooler Temperature is acceptable.
True
Cooler Temperature is recorded.
True 4.2°C IR8
COC is present.
True
COC is filled out in ink and legible.
True
COC is filled out with all pertinent information.
True
Is the Field Sampler's name present on COC?
True
There are no discrepancies between the containers received and the COC.
True
Samples are received within Holding Time (excluding tests with immediate
True
HTs)
Sample containers have legible labels.
True
Containers are not broken or leaking.
True
Sample collection date/times are provided.
True
Appropriate sample containers are used.
True
Sample bottles are completely filled.
True
Sample Preservation Verified.
N/A
There is sufficient vol. for all requested analyses, incl. any requested
True
MS/MSDs
Containers requiring zero headspace have no headspace or bubble is
True
<6mm (1/4").
Multiphasic samples are not present.
True
Samples do not require splitting or compositing.
True
Residual Chlorine Checked.
N/A
[L4
Eurofins Raleigh
Page 28 of 29 6/2/2023

Login Sample Receipt Checklist
Client: Hunt Environmental Associates Job Number: 752-7043-1
Login Number: 7043
List Number: 2
Creator: Harley, Tynisha
Question
List Source: Eurofins Savannah
List Creation: 05/18/23 12:43 PM
Answer Comment
Radioactivity wasn't checked or is </= background as measured by a survey
N/A
meter.
The cooler's custody seal, if present, is intact.
True
Sample custody seals, if present, are intact.
True
The cooler or samples do not appear to have been compromised or
True
tampered with.
Samples were received on ice.
True
Cooler Temperature is acceptable.
True
Cooler Temperature is recorded.
True
COC is present.
True
COC is filled out in ink and legible.
True
COC is filled out with all pertinent information.
True
Is the Field Sampler's name present on COC?
True
There are no discrepancies between the containers received and the COC.
True
Samples are received within Holding Time (excluding tests with immediate
True
HTs)
Sample containers have legible labels.
True
Containers are not broken or leaking.
True
Sample collection date/times are provided.
True
Appropriate sample containers are used.
True
Sample bottles are completely filled.
True
Sample Preservation Verified.
N/A
There is sufficient vol. for all requested analyses, incl. any requested
True
MS/MSDs
Containers requiring zero headspace have no headspace or bubble is
N/A
<6mm (1/4").
Multiphasic samples are not present.
True
Samples do not require splitting or compositing.
True
Residual Chlorine Checked.
N/A
[L4
Eurofins Raleigh
Page 29 of 29 6/2/2023

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Lumberton
W W TP Name: City of Lumberton
Monitoring Period: From 4/l/2023 To
WQ Permit Number:
NPDES Number:
6/30/2023
WQ0000672
NCL-024571
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. A (time/temp) ❑
1 Alt B (Alk Treatment) ❑
I Alt. C (Prior Testing) ❑
Alt.D (No Prior Test) ❑
I Process to Further Reduce Pathogengs ❑
If applicable to alternative
performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost 01
Heat Drying ❑
Heat Treatment ❑
Thermophilic ❑
Beta Ray 01
Gamma Ray ❑
Pasteurization ❑
Class B:
JAIL (1) Fecal Density p
Alt. (2) Process to Significantly Reduce Pathogens C,
If applicable to alternative
performed (Class
B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization ❑
I Air Drying ❑
Composting ❑
Aerobic Digestion ❑
Anaerobic Digestion ❑
If applicable to alternative performed (Class A or Class B) complete the following
monitoring data:
Parameter
Allowable Level
in Sludge
Pathogen Density
Number o
Excee-
n
Frequency
of Analysis
Sample
Type
Analytical
Tech -
nioue
MinimumGeo.
Mean
MaximumUnits
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
CFU
414000
617000
1140000
CFU/g
Quarterly
Grab
9222-MF
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per 4 grams
total solid (dry
weight)
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed:
Alt.1 (VS reduction) ❑
Alt. 2 (40-day bench) ❑
Alt. 3 (30-day bench) ,J
Alt. 4 (Spec. OZ uptake) ❑
Alt. 5 (14-Day Aerobic) ❑
Alt. 6 (Alk. Stabilization ❑
Alt 7 (Drying - Stable) ❑
Alt. 8 (Drying - Unstable) ❑
Alt. 9 (Injection) ❑
Alt. 10 (Incorporation) ❑
No vector attraction reduction alternatives were performed ❑
CERTIFICATION STATEMENT (please check the appropriate statement)
`'❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
0 "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note
if you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Michael C Hunt, ORC Michael C Hunt, ORC
PreparNand Title pe r print)
Signature of Preparer
Land Applier Name and Title (if applicable)(type or print)
2/20/2024
Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 02T (12/2006)

Cameron Testing Services, Inc. Laboratory Report
Client:
Project:
Sampled
Lab ID
2305-0146
2305-0146
NC DENR #654
NC PHHS #37799
US EPA #NC01918
Enviro-Choice Recycling
CTS Proj.
2305-0146
DW Cert # 37799
City of Lumberton
Regulatory
Yes
Sample Information
Date 05/16/23
Received
M. Sims Date
05/16/23
Analyses and Results
�
K Q ,49
Sample ID m o Analyte
Result
CL E
H
T -E
Std. Methods
U
a
c o E
Reference
4
-01
Swdgc Gr Fec. Coliform-S
518000
crufg
103590
05/17/23 PD
9222D - MF
-02
518000
CFurg
103590
-03
599000
cFUrg
99753
-04
622000
cFurg
103590
-05
725000
CFU1g
103590
-06
414000
cFUrg
103590
-07
1140000
CFU19
103590
Geomean
617000
-01
3Iudge Gr TS (%)
2.59
ro
0.01
06/17/23 PD
2540 G -TS
-02
2.61
i
0.01
-03
2.65
0A
0.01
-04
2.58
%
0,01
-05
2.59
i
001
-06
2.60
%
0.01
-07
2.58
i
C 01
Report
Review ��
Project Manager ❑ate O Cx (J
219 S. Steele Str. 919-208-4240
Sanford NC 27330 chris@catnerontesting,com

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tiff eurofins 0
Environment Testing
ANALYTICAL REPORT
PREPARED FOR
Attn: Cody Hunt
Hunt Environmental Associates ■r�
3330 Saddletree Rd
Lumberton, North Carolina 28360
Generated 9/22/2023 1:46:09 PM
JOB DESCRIPTION
City of Lumberton
JOB NUMBER
752-11592-1

This report may not be reproduced except in full, and with written approval from the laboratory. The results relate only to the
samples tested. For questions please contact the Project Manager at the e-mail address or telephone number listed on this
page.
The test results in this report relate only to the samples as received by the laboratory and will meet all requirements of the
methodology, with any exceptions noted. This report shall not be reproduced except in full, without the express written
approval of the laboratory. All questions should be directed to the Eurofins Environment Testing Southeast, LLC Project
Manager.
IlJI�1'�`11(o Ip
Authorized for release by
Heather Trotter, Project Manager
Heather.Trottera-et.eurofinsus.com
[phone]
Generated
9/22/2023 1:46:09 PM
12
13
14
Eurofins Savannah is a laboratory within Eurofins Environment Testing Southeast, LLC, a company within Eurofins Environment Testing Group of Companies
Page 2 of 32 9/22/2023

Client: Hunt Environmental Associates
Project/Site: City of Lumberton
Laboratory Job ID: 752-11592-1
Table of Contents
Cover Page ..............................................
1
Table of Contents .........................................
3
Definitions/Glossary.......................................
4
Case Narrative ...........................................
5
Detection Summary ........................................
6
Client Sample Results ......................................
7
QC Sample Results ........................................
9
QC Association Summary ...................................
14
Lab Chronicle ............................................
17
Certification Summary ......................................
19
Method Summary .........................................
21
Sample Summary .........................................
22
Chain of Custody ..........................................
23
Receipt Checklists .........................................
29
12
13
14
Page 3 of 32
Eurofins Raleigh
9/22/2023

Definitions/Glossary
Client: Hunt Environmental Associates
Project/Site: City of Lumberton
Qualifiers
Metals
Qualifier Qualifier Description
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
General Chemistry
Qualifier Qualifier Description
E Result exceeded calibration range.
F1 MS and/or MSD recovery exceeds control limits.
Glossary
Abbreviation These commonly used abbreviations may or may not be present in this report.
II Listed under the "D" column to designate that the result is reported on a dry weight basis
%R Percent Recovery
CFL Contains Free Liquid
CFU Colony Forming Unit
CNF Contains No Free Liquid
DER Duplicate Error Ratio (normalized absolute difference)
Dil Fac Dilution Factor
DL Detection Limit (DoD/DOE)
DL, RA, RE, IN Indicates a Dilution, Re -analysis, Re -extraction, or additional Initial metals/anion analysis of the sample
DLC Decision Level Concentration (Radiochemistry)
EDL Estimated Detection Limit (Dioxin)
LOD Limit of Detection (DoD/DOE)
LOQ Limit of Quantitation (DoD/DOE)
MCL EPA recommended "Maximum Contaminant Level"
MDA Minimum Detectable Activity (Radiochemistry)
MDC Minimum Detectable Concentration (Radiochemistry)
MDL Method Detection Limit
ML Minimum Level (Dioxin)
MPN Most Probable Number
MQL Method Quantitation Limit
NC Not Calculated
ND Not Detected at the reporting limit (or MDL or EDL if shown)
NEG Negative / Absent
POS Positive / Present
PQL Practical Quantitation Limit
PRIES Presumptive
QC Quality Control
RER Relative Error Ratio (Radiochemistry)
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
TNTC Too Numerous To Count
Job ID: 752-11592-1
12
13
14
Eurofins Raleigh
Page 4 of 32 9/22/2023

Case Narrative
Client: Hunt Environmental Associates
Project/Site: City of Lumberton
Job ID: 752-11592-1
Laboratory: Eurofins Raleigh
Narrative
Job Narrative
752-11592-1
Job ID: 752-11592-1
Receipt
The samples were received on 9/14/2023 4:43 PM. Unless otherwise noted below, the samples arrived in good condition, and where
required, properly preserved and on ice. The temperature of the cooler at receipt was 2.40 C.
Metals
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.
General Chemistry
Method 350.1: The matrix spike / matrix spike duplicate (MS/MSD) recoveries for preparation batch 680-798376 and analytical batch
680-798458 were outside control limits for one or more analytes. See QC Sample Results for detail. Sample matrix interference and/or
non -homogeneity are suspected because the associated laboratory control sample (LCS) recovery is within acceptance limits.
Methods 1010A, 101OB: No samples ignited, therefore, there were no sample duplicates. A LCSD was added which met acceptability
criteria.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
F47
12
13
14
Eurofins Raleigh
Page 5 of 32 9/22/2023

Detection Summary
Client: Hunt Environmental Associates
Job ID: 752-11592-1
Project/Site: City of Lumberton
Client Sample ID: S-2 WWTP
Lab Sample ID: 752-11592-1
Analyte
Result Qualifier
RL
MDL
Unit
Dil Fac
D
Method Prep Type
Sodium Adsorption Ratio
2.3
0.10
0.10
NONE
1
20B Soluble
Aluminum
23000
1200
390
mg/Kg
1
*
6010D Total/NA
Calcium
17000
2900
430
mg/Kg
1
*
6010D Total/NA
Copper
310
140
29
mg/Kg
1
*
6010D Total/NA
Magnesium
2700 J
2900
530
mg/Kg
1
*
6010D Total/NA
Potassium
6900
5800
630
mg/Kg
1
*
6010D Total/NA
Chromium
220
58
9.8
mg/Kg
1
6010D Total/NA
Sodium
39000
12000
3200
mg/Kg
1
6010D Total/NA
Zinc
780
120
33
mg/Kg
1
6010D Total/NA
Ammonia
600 F1
19
8.2
mg/Kg
1
350.1-1993 R2.0 Total/NA
Nitrogen, Kjeldahl
63000
16000
9500
mg/Kg
10
351.2-1993 R2.0 Total/NA
Phosphorus
15000
630
350
mg/Kg
1
365.4-1974 Total/NA
Total Solids
2.0
0.10
0.10
%
1
SM 254OG Total/NA
Nitrate Nitrite as N
920
130
35
mg/Kg
1
353.2-1993 R2.0 Soluble
pH
7.5
1.0
1.0
Su
1
9045D Soluble
Temperature
20.9
1.0
1.0
Degrees C
1
9045D Soluble
Client Sample ID: S-2 WTP
Lab Sample ID: 752-11592-2
Analyte
Result Qualifier
RL
MDL
Unit
Dil Fac
D
Method Prep Type
Aluminum
150000
890
300
mg/Kg
1
*
6010D Total/NA
Calcium
3100
2200
330
mg/Kg
1
*
6010D Total/NA
Potassium
580 J
4400
490
mg/Kg
1
��
6010D Total/NA
Chromium
18 J
44
7.6
mg/Kg
1
*
6010D Total/NA
Zinc
89
89
26
mg/Kg
1
*
6010D Total/NA
Ammonia
29
14
6.0
mg/Kg
1
*
350.1-1993 R2.0 Total/NA
Nitrogen, Kjeldahl
9000
1100
670
mg/Kg
1
*
351.2-1993 R2.0 Total/NA
Phosphorus
3900
450
250
mg/Kg
1
*
365.4-1974 Total/NA
Total Solids
2.7
0.10
0.10
%
1
SM 254OG Total/NA
pH
6.5
1.0
1.0
Su
1
9045D Soluble
Temperature
20.7
1.0
1.0
Degrees C
1
9045D Soluble
Client Sample ID: S-2 WWTP
Lab Sample ID: 752-11592-3
CAnalyte
Result Qualifier
RL
MDL
Unit
Dil Fac
D
Method Prep Type
Flashpoint
>140
Degrees F
1
1010A Total/NA
Client Sample ID: S-2 WTP
Lab Sample ID: 752-11592-4
CAnalyte
Result Qualifier
RL
MDL
Unit
Dil Fac
D
Method Prep Type
Flashpoint
>140
Degrees F
1
1010A Total/NA
This Detection Summary does not include radiochemical test results.
Eurofins Raleigh
Page 6 of 32 9/22/2023

Client Sample Results
Client: Hunt Environmental Associates
Job ID: 752-11592-1
Project/Site: City of Lumberton
Client Sample ID: S-2 WWTP
Lab Sample ID: 752-11592-1
Date Collected: 09/14/23 09:00
Matrix: Solid
Date Received: 09/14/23 16:43
Percent Solids:
1.6
Method: USDA 20B - Sodium Adsorption
Ratio - Soluble
Analyte
Result Qualifier
RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
Sodium Adsorption Ratio
2.3
0.10
0.10
NONE
09/18/23 06:43
1
Method: SW846 6010D - Metals (ICP)
Analyte
Result Qualifier
RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
Aluminum
23000
1200
390
mg/Kg
*
09/18/2310:04
09/19/2312:33
1
Arsenic
<69
120
69
mg/Kg
*
09/18/2310:04
09/19/2312:33
1
Cadmium
<5.8
29
5.8
mg/Kg
*
09/18/2310:04
09/19/2312:33
1
Calcium
17000
2900
430
mg/Kg
*
09/18/2310:04
09/19/2312:33
1
Copper
310
140
29
mg/Kg
*
09/18/2310:04
09/19/2312:33
1
Lead
<35
58
35
mg/Kg
*
09/18/2310:04
09/19/2312:33
1
Magnesium
2700 J
2900
530
mg/Kg
*
09/18/2310:04
09/19/2312:33
1
Molybdenum
<15
58
15
mg/Kg
*
09/18/2310:04
09/19/2312:33
1
Nickel
<52
230
52
mg/Kg
*
09/18/2310:04
09/19/2312:33
1
Potassium
6900
5800
630
mg/Kg
09/18/2310:04
09/19/2312:33
1
Chromium
220
58
9.8
mg/Kg
09/18/2310:04
09/19/2312:33
1 Is
Selenium
<63
140
63
mg/Kg
09/18/2310:04
09/19/2312:33
1
Sodium
39000
12000
3200
mg/Kg
09/18/2310:04
09/19/2312:33
1
Zinc
780
120
33
mg/Kg
09/18/2310:04
09/19/2312:33
1
Method: SW846 7471 B - Mercury (CVAA)
M
Analyte
Result Qualifier
RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
Mercury
<0.50
1.6
0.50
mg/Kg
*
09/18/2314:33
09/19/2316:24
1
General Chemistry
Analyte
Result Qualifier
RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
Ammonia (MCAWW 350.1-1993
600 F1
19
8.2
mg/Kg
*
09/18/23 10:01
09/18/23 13:32
1
R2.0)
Nitrogen, Kjeldahl (MCAWW
63000
16000
9500
mg/Kg
*
09/18/23 11:19
09/19/23 16:15
10
351.2-1993 R2.0)
Phosphorus (EPA 365.4-1974)
15000
630
350
mg/Kg
09/18/23 11:19
09/19/23 09:36
1
Cyanide, Reactive (SW846 9014)
<0.25
0.25
0.25
mg/Kg
09/19/23 14:00
09/20/23 17:40
1
Sulfide, Reactive (SW846 9034)
<150
150
150
mg/Kg
09/19/23 14:01
09/20/23 10:24
1
Total Solids (SM 2540G)
2.0
0.10
0.10
%
09/19/23 15:19
1
General Chemistry - Soluble
Analyte
Result Qualifier
RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
Nitrate Nitrite as N (MCAWW
920
130
35
mg/Kg
1
09/19/23 15:05
1
353.2-1993 R2.0)
pH (SW846 9045D)
7.5
1.0
1.0
Su
09/18/23 10:22
1
Temperature (SW846 9045D)
20.9
1.0
1.0
Degrees C
09/18/23 10:22
1
Client Sample ID: S-2 WTP
Lab Sample ID: 752-11592-2
Date Collected: 09/14/23 09:35
Matrix: Solid
Date Received: 09/14/23 16:43
Percent Solids:
2.2
Method: USDA 20B - Sodium Adsorption
Ratio - Soluble
Analyte
Result Qualifier
RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
Sodium Adsorption Ratio
<0.10
0.10
0.10
NONE
09/18/23 06:43
1
Method: SW846 6010D - Metals (ICP)
Analyte
Result Qualifier
RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
Aluminum
150000
890
300
mg/Kg
*
09/18/2310:04
09/19/2312:35
1
Eurofins Raleigh
Page 7 of 32 9/22/2023

Client Sample Results
Client: Hunt Environmental Associates
Job ID: 752-11592-1
Project/Site: City of Lumberton
Client Sample ID: S-2 WTP
Lab Sample ID: 752-11592-2
Date Collected: 09/14/23 09:35
Matrix: Solid
Date Received: 09/14/23 16:43
Percent Solids:
2.2
Method: SW846 6010D - Metals (ICP) (Continued)
Analyte
Result Qualifier
RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
Arsenic
<53
89
53
mg/Kg
*
09/18/2310:04
09/19/2312:35
1
Cadmium
<4.4
22
4.4
mg/Kg
*
09/18/2310:04
09/19/2312:35
1
Calcium
3100
2200
330
mg/Kg
*
09/18/2310:04
09/19/2312:35
1
Copper
<22
110
22
mg/Kg
*
09/18/2310:04
09/19/2312:35
1
Lead
<27
44
27
mg/Kg
*
09/18/2310:04
09/19/2312:35
1
Magnesium
<400
2200
400
mg/Kg
*
09/18/2310:04
09/19/2312:35
1
Molybdenum
<12
44
12
mg/Kg
*
09/18/2310:04
09/19/2312:35
1
Nickel
<40
180
40
mg/Kg
*
09/18/2310:04
09/19/2312:35
1
Potassium
580 J
4400
490
mg/Kg
*
09/18/2310:04
09/19/2312:35
1
Chromium
18 J
44
7.6
mg/Kg
*
09/18/2310:04
09/19/2312:35
1
Selenium
<49
110
49
mg/Kg
09/18/2310:04
09/19/2312:35
1
Sodium
<2400
8900
2400
mg/Kg
09/18/2310:04
09/19/2312:35
1
Zinc
89
89
26
mg/Kg
09/18/2310:04
09/19/2312:35
1
Method: SW846 7471 B - Mercury (CVAA)
Analyte
Result Qualifier
RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
Mercury
<0.35
1.1
0.35
mg/Kg
*
09/18/2314:33
09/19/2316:25
1
General Chemistry
Analyte
Result Qualifier
RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
Ammonia (MCAWW 350.1-1993
29
14
6.0
mg/Kg
*
09/18/23 10:01
09/18/23 12:06
1
R2.0)
Nitrogen, Kjeldahl (MCAWW
9000
1100
670
mg/Kg
09/18/23 11:19
09/19/23 14:25
1
351.2-1993 R2.0)
Phosphorus (EPA 365.4-1974)
3900
450
250
mg/Kg
09/18/23 11:19
09/19/23 09:35
1
Cyanide, Reactive (SW846 9014)
<0.25
0.25
0.25
mg/Kg
09/19/23 14:00
09/20/23 17:41
1
Sulfide, Reactive (SW846 9034)
<150
150
150
mg/Kg
09/19/23 14:01
09/20/23 10:24
1
Total Solids (SM 2540G)
2.7
0.10
0.10
%
09/19/23 15:19
1
General Chemistry - Soluble
Analyte
Result Qualifier
RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
Nitrate Nitrite as N (MCAWW
<25
91
25
mg/Kg
1
09/19/23 15:06
1
353.2-1993 R2.0)
pH (SW846 9045D)
6.5
1.0
1.0
Su
09/18/23 10:22
1
Temperature (SW846 9045D)
20.7
1.0
1.0
Degrees C
09/18/23 10:22
1
Client Sample ID: S-2 WWTP
Lab Sample ID: 752-11592-3
Date Collected: 09/14/23 09:00
Matrix:
Water
Date Received: 09/14/23 16:43
General Chemistry
Analyte
Result Qualifier
RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
Flash point (SW846 1010A)
>140
Degrees F
09/21/23 10:08
1
Client Sample ID: S-2 WTP
Lab Sample ID: 752-11592-4
Date Collected: 09/14/23 09:35
Matrix:
Water
Date Received: 09/14/23 16:43
General Chemistry
Analyte
Result Qualifier
RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
Flash point (SW846 1010A)
>140
Degrees F
09/21/23 11:03
1
Eurofins Raleigh
Page 8 of 32 9/22/2023

QC Sample Results
Client: Hunt Environmental Associates
Job ID: 752-11592-1
Project/Site: City of Lumberton
Method: 6010D - Metals (ICP)
Lab Sample ID: MB 680-798381/1-A
Client Sample ID: Method Blank
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 798641
Prep Batch: 798381
MB MB
Analyte
Result Qualifier
RL
MDL
Unit
D Prepared
Analyzed Dil Fac
Aluminum
<6.8
20
6.8
mg/Kg
09/18/2310:04
09/19/2311:37 1
Arsenic
<1.2
2.0
1.2
mg/Kg
09/18/2310:04
09/19/2311:37 1
Cadmium
<0.10
0.50
0.10
mg/Kg
09/18/2310:04
09/19/2311:37 1
Calcium
<7.4
50
7.4
mg/Kg
09/18/2310:04
09/19/2311:37 1
Copper
<0.50
2.5
0.50
mg/Kg
09/18/2310:04
09/19/2311:37 1
Lead
<0.61
1.0
0.61
mg/Kg
09/18/2310:04
09/19/2311:37 1
Magnesium
<9.1
50
9.1
mg/Kg
09/18/2310:04
09/19/2311:37 1
Molybdenum
<0.26
1.0
0.26
mg/Kg
09/18/2310:04
09/19/2311:37 1
Nickel
<0.90
4.0
0.90
mg/Kg
09/18/2310:04
09/19/2311:37 1
Potassium
<11
100
11
mg/Kg
09/18/2310:04
09/19/2311:37 1
Chromium
<0.17
1.0
0.17
mg/Kg
09/18/2310:04
09/19/2311:37 1
Selenium
<1.1
2.5
1.1
mg/Kg
09/18/2310:04
09/19/2311:37 1
Sodium
<55
200
55
mg/Kg
09/18/2310:04
09/19/2311:37 1
Zinc
<0.58
2.0
0.58
mg/Kg
09/18/2310:04
09/19/2311:37 1
Lab Sample ID: LCS 680-798381/2-A
Client Sample ID: Lab Control Sample
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 798641
Prep Batch: 798381
Spike
LCS LCS
%Rec
Analyte
Added
Result Qualifier
Unit
D %Rec
Limits
Aluminum
468
473
mg/Kg
101
80-120
Arsenic
9.26
8.46
mg/Kg
91
80. 120
Cadmium
4.63
4.47
mg/Kg
97
80. 120
Calcium
463
469
mg/Kg
101
80. 120
Copper
9.26
9.31
mg/Kg
101
80. 120
Lead
46.3
45.5
mg/Kg
98
80. 120
Magnesium
463
460
mg/Kg
99
80 - 120
Molybdenum
9.26
8.76
mg/Kg
95
80 - 120
Nickel
9.26
8.96
mg/Kg
97
80 - 120
Potassium
648
690
mg/Kg
106
80 - 120
Chromium
9.26
9.19
mg/Kg
99
80 - 120
Selenium
9.26
7.80
mg/Kg
84
80 - 120
Sodium
463
458
mg/Kg
99
80 - 120
Zinc
9.26
9.21
mg/Kg
99
80 - 120
Method: 7471 B - Mercury (CVAA)
Lab Sample ID: MB 680-798463/1-A
Client Sample ID: Method Blank
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 798682
Prep Batch: 798463
MB MB
Analyte Result Qualifier
RL
MDL Unit
D Prepared
Analyzed Dil Fac
Mercury <0.0071
0.022
0.0071 mg/Kg
09/18/2314:33
09/19/2315:46 1
Eurofins Raleigh
Page 9 of 32 9/22/2023

QC Sample Results
Client: Hunt Environmental Associates
Project/Site: City of Lumberton
Method: 7471 B - Mercury (CVAA) (Continued)
Lab Sample ID: LCS 680-798463/2-A
Matrix: Solid
Analysis Batch: 798682
Spike
Analyte
Added
Mercury
0.231
Lab Sample ID: 752-11592-2 MS
Matrix: Solid
Analysis Batch: 798682
Sample
Sample
Spike
Analyte Result
Qualifier
Added
Mercury <0.35
4.20
Lab Sample ID: 752-11592-2 MSD
Matrix: Solid
Analysis Batch: 798682
Sample
Sample
Spike
Analyte Result
Qualifier
Added
Mercury <0.35
4.28
Job ID: 752-11592-1
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Prep Batch: 798463
LCS LCS %Rec
Result Qualifier Unit D %Rec Limits
0.212 mg/Kg 92 80 - 120
Client Sample ID: S-2 WTP
Prep Type: Total/NA
Prep Batch: 798463
MS MS %Rec
Result Qualifier Unit D %Rec Limits
3.90 mg/Kg 93 80 - 120
Client Sample ID: S-2 WTP
Prep Type: Total/NA
Prep Batch: 798463
MSD MSD %Rec RPD
Result Qualifier Unit D %Rec Limits RPD Limit
3.97 mg/Kg # 93 80 - 120 2 20
Method: 1010A - Ignitability, Pensky-Martens Closed -Cup Method w
Lab Sample ID: MB 680-799046/1
Client Sample ID: Method Blank
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 799046
MB MB
Analyte Result Qualifier
RL
MDL Unit D
Prepared Analyzed Dil Fac
Flashpoint >140.0
Degrees F
09/21/23 07:44 1
Lab Sample ID: LCS 680-799046/2
Client
Sample ID: Lab Control Sample
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 799046
Spike
LCS
LCS
%Rec
Analyte
Added
Result
Qualifier Unit
D %Rec Limits
Flashpoint
140
146.0
Degrees F
104 96 - 106
Lab Sample ID: LCSD 680-799046/3
Client Sample ID: Lab Control Sample Dup
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 799046
Spike
LCSD
LCSD
%Rec RPD
Analyte
Added
Result
Qualifier Unit
D %Rec Limits RPD Limit
Flashpoint
140
144.0
Degrees F
103 96 - 106 1 4
Method: 350.1-1993 R2.0 - Nitrogen, Ammonia
Lab Sample ID: 752-11592-1 MS
Client Sample ID: S-2 WWTP
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 798458
Prep Batch: 798376
Sample Sample
Spike
MS
MS
%Rec
Analyte Result Qualifier
Added
Result
Qualifier Unit
D %Rec Limits
Ammonia 600 F1
317
768
E F1 mg/Kg
52 75 - 125
Eurofins Raleigh
Page 10 of 32 9/22/2023

QC Sample Results
Client: Hunt Environmental Associates
Job I D: 752-11592-1
Project/Site: City of Lumberton
Method: 350.1-1993 R2.0 - Nitrogen, Ammonia (Continued)
Lab Sample ID: 752-11592-1 MSD
Client Sample ID: S-2 WWTP
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 798458
Prep Batch: 798376
Sample Sample
Spike
MSD MSD %Rec RPD
Analyte Result Qualifier
Added
Result Qualifier Unit D %Rec Limits RPD Limit
Ammonia 600 F1
317
757 EF1 mg/Kg 48 75-125 1 30
Method: 351.2-1993 R2.0 - Nitrogen, Total Nitrogen
Lab Sample ID: MB 680-798415/1-A
Client Sample ID: Method Blank
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 798715
Prep Batch: 798415
MB MB
Analyte Result Qualifier
RL
MDL Unit D Prepared Analyzed Dil Fac
Nitrogen, Kjeldahl <11
19
11 mg/Kg 09/18/23 11:19 09/19/23 14:06 1
Lab Sample ID: LCS 680-798415/2-A
Client Sample ID: Lab Control Sample
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 798715
Prep Batch: 798415
Spike
LCS LCS %Rec
Analyte
Added
Result Qualifier Unit D %Rec Limits
Nitrogen, Kjeldahl
149
151 mg/Kg 102 75-125
Method: 353.2-1993 R2.0 - Nitrogen, Nitrate -Nitrite
Lab Sample ID: MB 680-798530/1-A
Client Sample ID: Method Blank
Matrix: Solid
Prep Type: Soluble
Analysis Batch: 798763
MB MB
Analyte Result Qualifier
RL
MDL Unit D Prepared Analyzed Dil Fac
Nitrate Nitrite as N <0.55
2.0
0.55 mg/Kg 09/19/23 14:54 1
Lab Sample ID: LCS 680-798530/2-A
Client Sample ID: Lab Control Sample
Matrix: Solid
Prep Type: Soluble
Analysis Batch: 798763
Spike
LCS LCS %Rec
Analyte
Added
Result Qualifier Unit D %Rec Limits
Nitrate Nitrite as N
20.0
19.2 mg/Kg 96 80 - 120
Lab Sample ID: LCSD 680-798530/3-A
Client Sample ID: Lab Control Sample Dup
Matrix: Solid
Prep Type: Soluble
Analysis Batch: 798763
Spike
LCSD LCSD %Rec RPD
Analyte
Added
Result Qualifier Unit D %Rec Limits RPD Limit
Nitrate Nitrite as N
20.0
19.8 mg/Kg 99 80 - 120 3 20
Method: 365.4-1974 - Phosphorus, Total
Lab Sample ID: MB 680-798415/1-A
Client Sample ID: Method Blank
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 798610
Prep Batch: 798415
MB MB
Analyte Result Qualifier
RL
MDL Unit D Prepared Analyzed Dil Fac
Phosphorus <4.2
7.6
4.2 mg/Kg 09/18/2311:19 09/19/2311:04 1
Eurofins Raleigh
Page 11 of 32 9/22/2023

QC Sample Results
Client: Hunt Environmental Associates
Project/Site: City of Lumberton
Job ID: 752-11592-1
Method: 365.4-1974 - Phosphorus, Total (Continued)
Lab Sample ID: LCS 680-798415/2-A Client Sample ID: Lab Control Sample
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 798610 Prep Batch: 798415
Spike LCS LCS %Rec
Analyte Added Result Qualifier Unit D %Rec Limits
Phosphorus 149 151 mg/Kg 101 70-130
Method: 9014 - Cyanide, Reactive
Lab Sample ID: MB 400-641693/1-A
Matrix: Solid
Analysis Batch: 641978
MB MB
Analyte Result Qualifier RL
Cyanide, Reactive <0.25 0.25
Lab Sample ID: LCS 400-641693/2-A
Matrix: Solid
Analysis Batch: 641978
Spike
Analyte Added
Cyanide, Reactive 1.00
Client Sample ID: Method Blank
Prep Type: Total/NA
Prep Batch: 641693
MDL Unit D Prepared Analyzed Dil Fac
0.25 mg/Kg 09/19/2314:00 09/20/2317:29 1
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Prep Batch: 641693
LCS LCS %Rec
Result Qualifier Unit D %Rec Limits
0.565 mg/Kg 57 10 - 110
Method: 9034 - Sulfide, Reactive
Lab Sample ID: MB 400-641694/1-A Client Sample ID: Method Blank
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 641842 Prep Batch: 641694
MB MB
Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac
Sulfide, Reactive <150 150 150 mg/Kg 09/19/23 14:01 09/20/23 10:24 1
Lab Sample ID: LCS 400-641694/2-A Client Sample ID: Lab Control Sample
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 641842 Prep Batch: 641694
Spike LCS LCS %Rec
Analyte Added Result Qualifier Unit D %Rec Limits
Sulfide, Reactive 993 183 mg/Kg 18 10 - 110
Method: 9045D - pH
Lab Sample ID: 752-11592-1 DU Client Sample ID: S-2 WWTP
Matrix: Solid Prep Type: Soluble
Analysis Batch: 4484
Sample Sample DU DU RPD
Analyte Result Qualifier Result Qualifier Unit D RPD Limit
pH 7.5 7.6 SU 0.8 25
Temperature 20.9 20.8 Degrees C 0.5
Eurofins Raleigh
Page 12 of 32 9/22/2023

QC Sample Results
Client: Hunt Environmental Associates
Project/Site: City of Lumberton
Job I D: 752-11592-1
Method: SM 254OG - Total, Fixed, and Volatile Solids
Lab Sample ID: MB 680-798648/1 Client Sample ID: Method Blank
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 798648
MB MB
Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac
Total Solids 99.9 0.10 0.10 % 09/19/23 15:19 1
12
13
14
Eurofins Raleigh
Page 13 of 32 9/22/2023

QC Association Summary
Client: Hunt Environmental Associates
Job ID:
752-11592-1
Project/Site: City of Lumberton
Metals
Analysis Batch: 446786
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
752-11592-1
S-2 WWTP
Soluble
Solid
20B
752-11592-2
S-2 WTP
Soluble
Solid
20B
Prep Batch: 798381
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
752-11592-1
S-2 WWTP
Total/NA
Solid
3050B
752-11592-2
S-2 WTP
Total/NA
Solid
3050B
MB 680-798381/1-A
Method Blank
Total/NA
Solid
3050B
LCS 680-798381/2-A
Lab Control Sample
Total/NA
Solid
3050B
Prep Batch: 798463
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
752-11592-1
S-2 WWTP
Total/NA
Solid
7471 B
752-11592-2
S-2 WTP
Total/NA
Solid
7471 B
MB 680-798463/1-A
Method Blank
Total/NA
Solid
7471 B
LCS 680-798463/2-A
Lab Control Sample
Total/NA
Solid
7471 B
752-11592-2 MS
S-2 WTP
Total/NA
Solid
7471 B
752-11592-2 MSD
S-2 WTP
Total/NA
Solid
7471 B
Analysis Batch: 798641
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
752-11592-1
S-2 WWTP
Total/NA
Solid
6010D
798381
752-11592-2
S-2 WTP
Total/NA
Solid
6010D
798381
MB 680-798381/1-A
Method Blank
Total/NA
Solid
6010D
798381
LCS 680-798381/2-A
Lab Control Sample
Total/NA
Solid
6010D
798381
Analysis Batch: 798682
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
752-11592-1
S-2 WWTP
Total/NA
Solid
7471 B
798463
752-11592-2
S-2 WTP
Total/NA
Solid
7471 B
798463
MB 680-798463/1-A
Method Blank
Total/NA
Solid
7471 B
798463
LCS 680-798463/2-A
Lab Control Sample
Total/NA
Solid
7471 B
798463
752-11592-2 MS
S-2 WTP
Total/NA
Solid
7471 B
798463
752-11592-2 MSD
S-2 WTP
Total/NA
Solid
7471 B
798463
General Chemistry
Leach Batch: 4483
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method Prep Batch
752-11592-1
S-2 WWTP
Soluble
Solid
DI Leach
752-11592-2
S-2 WTP
Soluble
Solid
DI Leach
LCS 752-4483/2-A
Lab Control Sample
Soluble
Solid
DI Leach
752-11592-1 DU
S-2 WWTP
Soluble
Solid
DI Leach
Analysis Batch: 4484
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
752-11592-1
S-2 WWTP
Soluble
Solid
9045D
4483
752-11592-2
S-2 WTP
Soluble
Solid
9045D
4483
LCS 752-4483/2-A
Lab Control Sample
Soluble
Solid
9045D
4483
752-11592-1 DU
S-2 WWTP
Soluble
Solid
9045D
4483
0
Eurofins Raleigh
Page 14 of 32 9/22/2023

QC Association Summary
Client: Hunt Environmental Associates
Job ID:
752-11592-1
Project/Site: City of Lumberton
General Chemistry
Prep Batch: 641693
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
752-11592-1
S-2 WWTP
Total/NA
Solid
7.3.3
752-11592-2
S-2 WTP
Total/NA
Solid
7.3.3
MB 400-641693/1-A
Method Blank
Total/NA
Solid
7.3.3
LCS 400-641693/2-A
Lab Control Sample
Total/NA
Solid
7.3.3
Prep Batch: 641694
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
752-11592-1
S-2 WWTP
Total/NA
Solid
7.3.4
752-11592-2
S-2 WTP
Total/NA
Solid
7.3.4
MB 400-641694/1-A
Method Blank
Total/NA
Solid
7.3.4
LCS 400-641694/2-A
Lab Control Sample
Total/NA
Solid
7.3.4
Analysis Batch: 641842
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
752-11592-1
S-2 WWTP
Total/NA
Solid
9034
641694
752-11592-2
S-2 WTP
Total/NA
Solid
9034
641694
MB 400-641694/1-A
Method Blank
Total/NA
Solid
9034
641694
LCS 400-641694/2-A
Lab Control Sample
Total/NA
Solid
9034
641694
Analysis Batch: 641978
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
752-11592-1
S-2 WWTP
Total/NA
Solid
9014
641693
752-11592-2
S-2 WTP
Total/NA
Solid
9014
641693
MB 400-641693/1-A
Method Blank
Total/NA
Solid
9014
641693
LCS 400-641693/2-A
Lab Control Sample
Total/NA
Solid
9014
641693
Prep Batch: 798376
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method Prep Batch
752-11592-1
S-2 WWTP
Total/NA
Solid
3-154
752-11592-2
S-2 WTP
Total/NA
Solid
3-154
752-11592-1 MS
S-2 WWTP
Total/NA
Solid
3-154
L752-11592-1 MSD
S-2 WWTP
Total/NA
Solid
3-154
Prep Batch: 798415
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method Prep Batch
752-11592-1
S-2 WWTP
Total/NA
Solid
Digestion
752-11592-2
S-2 WTP
Total/NA
Solid
Digestion
MB 680-798415/1-A
Method Blank
Total/NA
Solid
Digestion
LCS 680-798415/2-A
Lab Control Sample
Total/NA
Solid
Digestion
Analysis Batch: 798458
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
752-11592-1
S-2 WWTP
Total/NA
Solid
350.1-1993 R2.0
798376
752-11592-2
S-2 WTP
Total/NA
Solid
350.1-1993 R2.0
798376
752-11592-1 MS
S-2 WWTP
Total/NA
Solid
350.1-1993 R2.0
798376
752-11592-1 MSD
S-2 WWTP
Total/NA
Solid
350.1-1993 R2.0
798376
Analysis Batch: 798509
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
752-11592-1
S-2 WWTP
Total/NA
Solid
Moisture
752-11592-2
S-2 WTP
Total/NA
Solid
Moisture
Eurofins Raleigh
Page 15 of 32 9/22/2023

QC Association Summary
Client: Hunt Environmental Associates
Job ID: 752-11592-1
Project/Site: City of Lumberton
General Chemistry
Leach Batch: 798530
Lab Sample ID Client Sample ID
Prep Type
Matrix
Method Prep Batch
752-11592-1 S-2 VWVTP
Soluble
Solid
DI Leach
752-11592-2 S-2 VVTP
Soluble
Solid
DI Leach
MB 680-798530/1-A Method Blank
Soluble
Solid
DI Leach
LCS 680-798530/2-A Lab Control Sample
Soluble
Solid
DI Leach
LCSD 680-798530/3-A Lab Control Sample Dup
Soluble
Solid
DI Leach
Analysis Batch: 798610
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
752-11592-1
S-2 VWVTP
Total/NA
Solid
365.4-1974
798415
752-11592-2
S-2 WTP
Total/NA
Solid
365.4-1974
798415
MB 680-798415/1-A
Method Blank
Total/NA
Solid
365.4-1974
798415
LCS 680-798415/2-A
Lab Control Sample
Total/NA
Solid
365.4-1974
798415
Analysis Batch: 798648
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method Prep Batch
752-11592-1
S-2 VWVTP
Total/NA
Solid
SM 254OG
752-11592-2
S-2 WTP
Total/NA
Solid
SM 254OG
MB 680-798648/1
Method Blank
Total/NA
Solid
SM 254OG
Analysis Batch: 798715
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
752-11592-1
S-2 VWVTP
Total/NA
Solid
351.2-1993 R2.0
798415
752-11592-2
S-2 WTP
Total/NA
Solid
351.2-1993 R2.0
798415
MB 680-798415/1-A
Method Blank
Total/NA
Solid
351.2-1993 R2.0
798415
LCS 680-798415/2-A
Lab Control Sample
Total/NA
Solid
351.2-1993 R2.0
798415
Analysis Batch: 798763
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
752-11592-1
S-2 VWVTP
Soluble
Solid
353.2-1993 R2.0
798530
752-11592-2
S-2 WTP
Soluble
Solid
353.2-1993 R2.0
798530
MB 680-798530/1-A
Method Blank
Soluble
Solid
353.2-1993 R2.0
798530
LCS 680-798530/2-A
Lab Control Sample
Soluble
Solid
353.2-1993 R2.0
798530
LCSD 680-798530/3-A
Lab Control Sample Dup
Soluble
Solid
353.2-1993 R2.0
798530
Analysis Batch: 799046
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method Prep Batch
752-11592-3
S-2 WWTP
Total/NA
Water
1010A
752-11592-4
S-2 WTP
Total/NA
Water
1010A
MB 680-799046/1
Method Blank
Total/NA
Water
1010A
LCS 680-799046/2
Lab Control Sample
Total/NA
Water
1010A
LCSD 680-799046/3
Lab Control Sample Dup
Total/NA
Water
1010A
Eurofins Raleigh
Page 16 of 32 9/22/2023

Lab Chronicle
Client: Hunt Environmental Associates
Project/Site: City of Lumberton
Job ID: 752-11592-1
Client Sample ID: S-2 WWTP Lab Sample ID: 752-11592-1
Date Collected: 09/14/23 09:00 Matrix: Solid
Date Received: 09/14/23 16:43
Batch
Batch
Prep Type
Type
Method
Soluble
Analysis
20B
Total/NA
Prep
7.3.3
Total/NA
Analysis
9014
Total/NA
Prep
7.3.4
Total/NA
Analysis
9034
Soluble
Leach
DI Leach
Soluble
Analysis
9045D
Total/NA
Analysis
Moisture
Total/NA
Analysis
SM 254OG
Client Sample ID: S-2
WWTP
Date Collected:
09/14/23 09:00
Date Received: 09/14/23 16:43
Dilution
Batch
Prepared
Run Factor
Number
Analyst
Lab
or Analyzed
1
446786
RJR
EET PIT
09/18/23 06:43
641693
JP
EET PEN
09/19/23 14:00
1
641978
DEK
EET PEN
09/20/23 17:40
641694
JP
EET PEN
09/19/23 14:01
1
641842
JP
EET PEN
09/20/23 10:24
4483
CB
EET ESC
09/18/23 10:19
1
4484
CB
EET ESC
09/18/23 10:22
•
1
798509
KG
EET SAV
09/19/23 09:24
1
798648
PG
EET SAV
09/19/23 15:19
Lab Sample ID: 752-11592-1
Matrix: Solid
Percent Solids: 1.6
Prep Type
Batch
Type
Batch
Method
Dilution
Run Factor
Total/NA
Prep
3050B
Total/NA
Analysis
6010D
1
Total/NA
Prep
7471 B
Total/NA
Analysis
7471 B
1
Total/NA
Prep
3-154
Total/NA
Analysis
350.1-1993 R2.0
1
Total/NA
Prep
Digestion
Total/NA
Analysis
351.2-1993 R2.0
10
Soluble
Leach
DI Leach
Soluble
Analysis
353.2-1993 R2.0
1
Total/NA
Prep
Digestion
Total/NA
Analysis
365.4-1974
1
Client Sample ID: S-2
WTP
Date Collected:
09/14/23 09:35
Date Received: 09/14/23 16:43
Batch
Prepared
Number
Analyst
Lab
or Analyzed
798381
BCB
EET SAV
09/18/23 10:04
798641
BJB
EET SAV
09/19/23 12:33 m
798463
DW
EET SAV
09/18/23 14:33
798682
BCB
EET SAV
09/19/23 16:24
798376
TD
EET SAV
09/18/23 10:01
798458
TD
EET SAV
09/18/23 13:32
798415
SM
EET SAV
09/18/23 11:19
798715
AS
EET SAV
09/19/23 16:15
798530
AF
EET SAV
09/19/23 10:11
798763
AF
EET SAV
09/19/23 15:05
798415
SM
EET SAV
09/18/23 11:19
798610
AS
EET SAV
09/19/23 09:36
Lab Sample ID: 752-11592-2
Matrix: Solid
Prep Type
Batch
Type
Batch
Method
Dilution
Run Factor
Batch
Number Analyst
Lab
Prepared
or Analyzed
Soluble
Analysis
20B
1
446786
RJR
EET PIT
09/18/23 06:43
Total/NA
Prep
7.3.3
641693
JP
EET PEN
09/19/23 14:00
Total/NA
Analysis
9014
1
641978
DEK
EET PEN
09/20/23 17:41
Total/NA
Prep
7.3.4
641694
JP
EET PEN
09/19/23 14:01
Total/NA
Analysis
9034
1
641842
JP
EET PEN
09/20/23 10:24
Soluble
Leach
DI Leach
4483
CB
EET ESC
09/18/23 10:21
Soluble
Analysis
9045D
1
4484
CB
EET ESC
09/18/23 10:22
Total/NA
Analysis
Moisture
1
798509
KG
EET SAV
09/19/23 09:24
Total/NA
Analysis
SM 254OG
1
798648
PG
EET SAV
09/19/23 15:19
Eurofins Raleigh
Page 17 of 32 9/22/2023

Lab Chronicle
Client: Hunt Environmental Associates
Job ID: 752-11592-1
Project/Site: City of Lumberton
Client Sample ID: S-2 WTP
Lab Sample ID: 752-11592-2
Date Collected: 09/14/23 09:35
Matrix: Solid
Date Received: 09/14/23 16:43
Percent Solids: 2.2
Batch Batch
Dilution
Batch
Prepared
Prep Type Type Method
Run Factor
Number
Analyst
Lab
or Analyzed
Total/NA Prep 3050B
798381
BCB
EET SAV
09/18/23 10:04
Total/NA Analysis 6010D
1
798641
BJB
EET SAV
09/19/23 12:35
Total/NA Prep 7471 B
798463
DW
EET SAV
09/18/23 14:33
Total/NA Analysis 7471 B
1
798682
BCB
EET SAV
09/19/23 16:25
Total/NA Prep 3-154
798376
TD
EET SAV
09/18/23 10:01
Total/NA Analysis 350.1-1993 R2.0
1
798458
TD
EET SAV
09/18/23 12:06
Total/NA Prep Digestion
Total/NA Analysis 351.2-1993 R2.0
1
798415
798715
SM
AS
EET SAV
EET SAV
09/18/23 11:19
09/19/23 14:25
Soluble Leach DI Leach
798530
AF
EET SAV
09/19/23 10:11
Soluble Analysis 353.2-1993 R2.0
1
798763
AF
EET SAV
09/19/23 15:06
Total/NA Prep Digestion
798415
SM
EET SAV
09/18/23 11:19
Total/NA Analysis 365.4-1974
1
798610
AS
EET SAV
09/19/23 09:35
Client Sample ID: S-2 WWTP
Lab Sample ID: 752-11592-3
Date Collected: 09/14/23 09:00
Matrix: Water
Date Received: 09/14/23 16:43
Batch Batch
Dilution
Batch
Prepared
m
Prep Type Type Method
Run Factor
Number
Analyst
Lab
or Analyzed
Total/NA Analysis 1010A
1
799046
AS
EET SAV
09/21/23 10:08
Client Sample ID: S-2 WTP
Lab Sample ID: 752-11592-4
Date Collected: 09/14/23 09:35
Matrix: Water
Date Received: 09/14/23 16:43
Batch Batch Dilution Batch Prepared
Prep Type Type Method Run Factor Number Analyst Lab or Analyzed
Total/NA Analysis 1010A 1 799046 AS EET SAV 09/21/23 11:03
Laboratory References:
EET ESC = Eurofins Raleigh, 102-A Woodwinds Industrial Court, Cary, NC 27511, TEL [phone]
EET PEN = Eurofins Pensacola, 3355 McLemore Drive, Pensacola, FL 32514, TEL [phone]
EET PIT = Eurofins Pittsburgh, 301 Alpha Drive, RIDC Park, Pittsburgh, PA 15238, TEL [phone]
EET SAV = Eurofins Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL [phone]
Eurofins Raleigh
Page 18 of 32 9/22/2023

Accreditation/Certification Summary
Client: Hunt Environmental Associates Job ID: 752-11592-1
Project/Site: City of Lumberton
Laboratory: Eurofins Raleigh
Unless otherwise noted, all analytes for this laboratory were covered under each accreditation/certification below.
Authority Program Identification Number Expiration Date
North Carolina (VWV/SV) State 591 12-31-23
The following analytes are included in this report, but the laboratory is not certified by the governing authority. This list may include analytes for which
the agency does not offer certification.
Analysis Method Prep Method Matrix Analyte
9045D Solid Temperature
Laboratory: Eurofins Pensacola
All accreditations/certifications held by this laboratory are listed. Not all accreditations/certifications are applicable to this report.
Authority
Program
Identification Number
Expiration Date
Alabama
State
40150
06-30-24
ANAB
ISO/IEC 17025
L2471
02-22-26
Arkansas DEQ
State
88-00689
08-01-24
California
State
2510
06-30-24
Florida
NELAP
E81010
06-30-24
Georgia
State
E81010(FL)
06-30-24
Illinois
NELAP
200041
10-09-23
Kansas
NELAP
E-10253
10-31-23
Kentucky (UST)
State
53
06-30-24
Louisiana (All)
NELAP
30976
06-30-24
Louisiana (DVV)
State
LA017
12-31-23
Maryland
State
233
09-30-23
North Carolina (VWV/SVV)
State
314
12-31-23
Oklahoma
NELAP
9810
12-31-23
Pennsylvania
NELAP
68-00467
01-31-24
South Carolina
State
96026
06-30-24
Tennessee
State
TN02907
06-30-24
Texas
NELAP
T104704286
09-30-23
US Fish & Wildlife
US Federal Programs
A22340
06-30-24
USDA
US Federal Programs
FLGNV23001
01-08-26
USDA
US Federal Programs
P330-21-00056
05-17-24
Virginia
NELAP
460166
06-14-24
West Virginia DEP
State
136
03-31-24
Laboratory: Eurofins Pittsburgh
All accreditations/certifications held by this laboratory are listed. Not all accreditations/certifications are applicable to this report.
Authority
Program
Arkansas DEQ
State
California
State
Connecticut
State
Florida
NELAP
Georgia
State
Illinois
NELAP
Kansas
NELAP
Kentucky (UST)
State
Kentucky (WW)
State
Louisiana
NELAP
Louisiana (All)
NELAP
Maine
State
Identification Number Expiration Date
19-033-0
06-27-24
2891
04-30-24
PH-0688
09-30-24
E871008
06-30-24
PA 02-00416
04-30-24
004375
06-30-24
E-10350
01-31-24
162013
04-30-23
KY98043
12-31-23
04041
06-30-22
04041
06-30-24
PA00164
03-06-24
Accreditation/Certification renewal pending - accreditation/certification considered valid.
12
13
14
Eurofins Raleigh
Page 19 of 32 9/22/2023

Accreditation/Certification Summary
Client: Hunt Environmental Associates
Job ID: 752-11592-1
Project/Site: City of Lumberton
Laboratory: Eurofins Pittsburgh (Continued)
All accreditations/certifications held by this laboratory are listed. Not all accreditations/certifications are applicable to this report.
Authority Program
Identification Number
Expiration Date
Minnesota NELAP
042-999-482
12-31-23
New Hampshire NELAP
2030
04-04-24
New Jersey NELAP
PA005
06-30-24
New York NELAP
11182
04-01-24
North Carolina (WW/SW) State
434
12-31-23
North Dakota State
R-227
04-30-24
Oregon NELAP
PA-2151
02-06-24
Pennsylvania NELAP
02-00416
04-30-24
Rhode Island State
LAO00362
12-31-22'
South Carolina State
89014
04-30-23'
Texas NELAP
T104704528
03-31-24
US Fish & Wildlife US Federal Programs
058448
03-31-24
USDA US Federal Programs
P330-16-00211
04-11-26
Utah NELAP
PA001462019-8
05-31-24
Virginia NELAP
10043
09-14-23'
West Virginia DEP State
142
01-31-24
Wisconsin State
998027800
08-31-24
Laboratory: Eurofins Savannah
Unless otherwise noted, all analytes for this laboratory were covered under each
accreditation/certification below.
Authority
North Carolina (WW/SW)
Program
State
Identification Number Expiration Date
269 09-21-23
The following analytes are included in this report, but the laboratory is not certified by the governing authority
the agency does not offer certification.
Analysis Method
Prep Method
Matrix
Analyte
1010A
Water
Flashpoint
350.1-1993 R2.0
3-154
Solid
Ammonia
351.2-1993 R2.0
Digestion
Solid
Nitrogen, Kjeldahl
353.2-1993 R2.0
Solid
Nitrate Nitrite as N
365.4-1974
Digestion
Solid
Phosphorus
Moisture
Solid
Percent Moisture
Moisture
Solid
Percent Solids
SM 2540G
Solid
Total Solids
Accreditation/Certification renewal pending - accreditation/certification considered valid.
This list may include analytes for which
12
13
14
Eurofins Raleigh
Page 20 of 32 9/22/2023

Method Summary
Client: Hunt Environmental Associates
Project/Site: City of Lumberton
Job ID: 752-11592-1
Method
Method Description
Protocol
Laboratory
20B
Sodium Adsorption Ratio
USDA
EET PIT
6010D
Metals (ICP)
SW846
EET SAV
7471 B
Mercury (CVAA)
SW846
EET SAV
1010A
Ignitability, Pensky-Martens Closed -Cup Method
SW846
EET SAV
350.1-1993 R2.0
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MCAWW
EET SAV
351.2-1993 R2.0
Nitrogen, Total Nitrogen
MCAWW
EET SAV
353.2-1993 R2.0
Nitrogen, Nitrate -Nitrite
MCAWW
EET SAV
365.4-1974
Phosphorus, Total
EPA
EET SAV
9014
Cyanide, Reactive
SW846
EET PEN
9034
Sulfide, Reactive
SW846
EET PEN
9045D
pH
SW846
EET ESC
Moisture
Percent Moisture
EPA
EET SAV
SM 254OG
Total, Fixed, and Volatile Solids
SM
EET SAV
3050B
Preparation, Metals
SW846
EET SAV
3-154
Ammonia ( Sediments)
EPA
EET SAV
7.3.3
Cyanide, Reactive
SW846
EET PEN
7.3.4
Sulfide, Reactive
SW846
EET PEN
7471 B
Preparation, Mercury
SW846
EET SAV
DI Leach
Deionized Water Leaching Procedure
ASTM
EET ESC
DI Leach
Deionized Water Leaching Procedure
ASTM
EET SAV
Digestion
Digestion, Hot Block
EPA
EET SAV
Protocol References:
ASTM = ASTM International
EPA= US Environmental Protection Agency
MCAWW = "Methods For Chemical Analysis Of Water And Wastes", EPA-600/4-79-020, March 1983 And Subsequent Revisions.
SM = "Standard Methods For The Examination Of Water And Wastewater"
SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.
USDA = "USDA Agriculture Handbook 60, section 2013".
Laboratory References:
EET ESC = Eurofins Raleigh, 102-A Woodwinds Industrial Court, Cary, NC 27511, TEL [phone]
EET PEN = Eurofins Pensacola, 3355 McLemore Drive, Pensacola, FL 32514, TEL [phone]
EET PIT = Eurofins Pittsburgh, 301 Alpha Drive, RIDC Park, Pittsburgh, PA 15238, TEL [phone]
EET SAV = Eurofins Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL [phone]
Eurofins Raleigh
Page 21 of 32 9/22/2023

Sample Summary
Client: Hunt Environmental Associates
Project/Site: City of Lumberton
Lab Sample ID
Client Sample ID
Matrix
Collected
Received
752-11592-1
S-2 WWTP
Solid
09/14/23 09:00
09/14/23 16:43
752-11592-2
S-2 WTP
Solid
09/14/23 09:35
09/14/23 16:43
752-11592-3
S-2 WWTP
Water
09/14/23 09:00
09/14/23 16:43
752-11592-4
S-2 WTP
Water
09/14/23 09:35
09/14/23 16:43
Job ID: 752-11592-1
12
13
74
Eurofins Raleigh
Page 22 of 32 9/22/2023

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Eurofins Raleigh
102-A Woodwinds Industrial Court
Cary, NC 27511
Phone: [phone]
Chain of Custody Record
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Environment Testing
Sampler.
Lab PM:
Carder Tracking No(s):
COC No:
Client Information Sub Contract Lab
Trotter, Heather
752-1493.1
Client Contact:
Phone:
E-Mail:
State of Origin:
Page:
Shipping/Receiving
[e-mail]
North Carolina
Page 1 of 1
Company:
Accreditations Required (See note):
Job #:
Eurofins Environment Testing Southeast,
State - North Carolina (1M/V/SW)
752-11592-1
Address:
Due Date Requested:
Preservation Codes:
5102 LaRoche Avenue,
9/19/2023
Analysis
Requested
M - Hexane
FiCL
A - NaO IN -None
16 - NaOH
City:
TAT Requested (days):
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Savannah
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D - Nitric Acid O - Na2SO3
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GA, 31404
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X
Eastern
Note: Since laboratory accredtations are subject to change, Eurofins Environment Testing Southeast LLC places the ownership of method, analyte & accreditation compliance upon our subcontract laboratories. This sample shipment is forwarded under chain -of -custody. If the laboratory
does not currently maintain accreditation in the State of Origin listed above for analysis/tests/matrix being analyzed, the samples must be shipped back to the Eurofins Environment Testing Southeast, LLC laboratory or other instructions will be provided. Any changes to accreditation
status should be brought to Eurofins Environment Testing Southeast, LLC attention immediately. If all requested accreditations are current to date, return the signed Chain of Custody attesting to said compliance to Eurofins Environment Testing Southeast LLC.
Possible Hazard Identification
Sample Disposal (A fee may be assessed if samples are retained longer than 1 month)
Unconfirmed
I 0 Return To Client 0 Disposal By Lab Archive For Months
Deliverable Requested: I, II, III, IV, Other (specify) Primary Deliverable Rank: 2
Special Instructions/QC Requirements:
Empty Kit Relinquished by:
OR
Date:
Time:
Method of shipment:
Relinquished .l
Company
Received by:
Daterfime:
Company
`
r ✓ l
Relinquished by:
Date 'me:
Company
Received by.
Dalerrime:
Company
Relinquished by:
Date/Time:
Company
Receivey /� ^
D�tNJT��e
Company
11
LL I
Custody Seals Intact:
Custody Seal No.:
Cooler Temperature(s) °C and Other
A Yes A No
/I c
0
0
n
0
0
Page 28 of 32 Ver.06/08/206!122/2023

Login Sample Receipt Checklist
Client: Hunt Environmental Associates Job Number: 752-11592-1
Login Number: 11592
List Number: 1
Creator: Hyatt, Samantha
Question
List Source: Eurofins Raleigh
Answer Comment
Radioactivity wasn't checked or is </= background as measured by a survey
True
mete r.
The cooler's custody seal, if present, is intact.
True
Sample custody seals, if present, are intact.
True
The cooler or samples do not appear to have been compromised or
True
tampered with.
Samples were received on ice.
True
Cooler Temperature is acceptable.
True
Cooler Temperature is recorded.
True
COC is present.
True
COC is filled out in ink and legible.
True
COC is filled out with all pertinent information.
True
Is the Field Sampler's name present on COC?
True
There are no discrepancies between the containers received and the COC.
True
Samples are received within Holding Time (excluding tests with immediate
True
HTs)
Sample containers have legible labels.
True
Containers are not broken or leaking.
True
Sample collection date/times are provided.
True
Appropriate sample containers are used.
True
Sample bottles are completely filled.
True
Sample Preservation Verified.
True
There is sufficient vol. for all requested analyses, incl. any requested
True
MS/MSDs
Containers requiring zero headspace have no headspace or bubble is
True
<6mm (1/4").
Multiphasic samples are not present.
True
Samples do not require splitting or compositing.
True
Residual Chlorine Checked.
True
[L4
Eurofins Raleigh
Page 29 of 32 9/22/2023

Client: Hunt Environmental Associates
Login Number: 11592
List Number: 4
Creator: Roberts, Alexis J
Question
Login Sample Receipt Checklist
Answer Comment
Radioactivity wasn't checked or is </= background as measured by a survey
N/A
mete r.
The cooler's custody seal, if present, is intact.
N/A
Sample custody seals, if present, are intact.
N/A
The cooler or samples do not appear to have been compromised or
True
tampered with.
Samples were received on ice.
True
Cooler Temperature is acceptable.
True
Cooler Temperature is recorded.
True
COC is present.
True
COC is filled out in ink and legible.
True
COC is filled out with all pertinent information.
True
Is the Field Sampler's name present on COC?
True
There are no discrepancies between the containers received and the COC.
True
Samples are received within Holding Time (excluding tests with immediate
True
HTs)
Sample containers have legible labels.
True
Containers are not broken or leaking.
True
Sample collection date/times are provided.
True
Appropriate sample containers are used.
True
Sample bottles are completely filled.
True
Sample Preservation Verified.
N/A
There is sufficient vol. for all requested analyses, incl. any requested
True
MS/MSDs
Containers requiring zero headspace have no headspace or bubble is
N/A
<6mm (1/4").
Multiphasic samples are not present.
True
Samples do not require splitting or compositing.
True
Residual Chlorine Checked.
N/A
0.0°C IR8
Job Number: 752-11592-1
List Source: Eurofins Pensacola
List Creation: 09/16/23 04:36 PM
[L4
Eurofins Raleigh
Page 30 of 32 9/22/2023

Login Sample Receipt Checklist
Client: Hunt Environmental Associates Job Number: 752-11592-1
Login Number: 11592
List Number: 2
Creator: Watson, Debbie
Question
List Source: Eurofins Pittsburgh
List Creation: 09/16/23 12:20 PM
Answer Comment
Radioactivity wasn't checked or is </= background as measured by a survey
N/A
mete r.
The cooler's custody seal, if present, is intact.
True
Sample custody seals, if present, are intact.
True
The cooler or samples do not appear to have been compromised or
True
tampered with.
Samples were received on ice.
True
Cooler Temperature is acceptable.
True
Cooler Temperature is recorded.
True
COC is present.
True
COC is filled out in ink and legible.
True
COC is filled out with all pertinent information.
True
Is the Field Sampler's name present on COC?
N/A
There are no discrepancies between the containers received and the COC.
True
Samples are received within Holding Time (excluding tests with immediate
True
HTs)
Sample containers have legible labels.
True
Containers are not broken or leaking.
True
Sample collection date/times are provided.
True
Appropriate sample containers are used.
True
Sample bottles are completely filled.
True
Sample Preservation Verified.
True
There is sufficient vol. for all requested analyses, incl. any requested
True
MS/MSDs
Containers requiring zero headspace have no headspace or bubble is
True
<6mm (1/4").
Multiphasic samples are not present.
True
Samples do not require splitting or compositing.
True
Residual Chlorine Checked.
N/A
[L4
Eurofins Raleigh
Page 31 of 32 9/22/2023

Login Sample Receipt Checklist
Client: Hunt Environmental Associates Job Number: 752-11592-1
Login Number: 11592
List Number: 3
Creator: Sims, Robert D
Question
List Source: Eurofins Savannah
List Creation: 09/16/23 01:29 PM
Answer Comment
Radioactivity wasn't checked or is </= background as measured by a survey
N/A
mete r.
The cooler's custody seal, if present, is intact.
True
Sample custody seals, if present, are intact.
True
The cooler or samples do not appear to have been compromised or
True
tampered with.
Samples were received on ice.
True
Cooler Temperature is acceptable.
True
Cooler Temperature is recorded.
True
COC is present.
True
COC is filled out in ink and legible.
True
COC is filled out with all pertinent information.
True
Is the Field Sampler's name present on COC?
True
There are no discrepancies between the containers received and the COC.
True
Samples are received within Holding Time (excluding tests with immediate
True
HTs)
Sample containers have legible labels.
True
Containers are not broken or leaking.
True
Sample collection date/times are provided.
True
Appropriate sample containers are used.
True
Sample bottles are completely filled.
True
Sample Preservation Verified.
N/A
There is sufficient vol. for all requested analyses, incl. any requested
True
MS/MSDs
Containers requiring zero headspace have no headspace or bubble is
N/A
<6mm (1/4").
Multiphasic samples are not present.
True
Samples do not require splitting or compositing.
True
Residual Chlorine Checked.
N/A
[L4
Eurofins Raleigh
Page 32 of 32 9/22/2023

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Lumberton
W W TP Name: City of Lumberton
Monitoring Period: From 7/l/2023 To
WQ Permit Number:
NPDES Number:
9/30/2023
WQ0000672
NCL-024571
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. A (time/temp) ❑
1 Alt B (Alk Treatment) ❑
I Alt. C (Prior Testing) ❑
Alt.D (No Prior Test) ❑
I Process to Further Reduce Pathogengs ❑
If applicable to alternative
performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost 01
Heat Drying ❑
Heat Treatment ❑
Thermophilic ❑
Beta Ray 01
Gamma Ray ❑
Pasteurization ❑
Class B:
JAIL (1) Fecal Density p
Alt. (2) Process to Significantly Reduce Pathogens C,
If applicable to alternative
performed (Class
B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization ❑
I Air Drying ❑
Composting ❑
Aerobic Digestion ❑
Anaerobic Digestion ❑
If applicable to alternative performed (Class A or Class B) complete the following
monitoring data:
Parameter
Allowable Level
in Sludge
Pathogen Density
Number o
Excee-
n
Frequency
of Analysis
Sample
Type
Analytical
Tech -
nioue
MinimumGeo.
Mean
MaximumUnits
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
CFU
4620000
6000000
7490000
CFU/ g
Quarterly
Q y
Grab
9222-MF
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per 4 grams
total solid (dry
weight)
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed:
Alt.1 (VS reduction) ❑
Alt. 2 (40-day bench) ❑
Alt. 3 (30-day bench) ,J
Alt. 4 (Spec. OZ uptake) ❑
Alt. 5 (14-Day Aerobic) ❑
Alt. 6 (Alk. Stabilization ❑
Alt 7 (Drying - Stable) ❑
Alt. 8 (Drying - Unstable) ❑
Alt. 9 (Injection) ❑
Alt. 10 (Incorporation) ❑
No vector attraction reduction alternatives were performed ❑
CERTIFICATION STATEMENT (please check the appropriate statement)
`'❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
0 "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note
if you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Michael C Hunt, ORC Michael C Hunt, ORC
Preparer Name and Title (ter print)
2/20/2024
Signature of Preparer* U Date
Land Applier Name and Title (if applicable)(type or print)
Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 02T (12/2006)

Cameron Testing Services, Inc. Laboratory Report
NC DENR#654
NC PHHS #37799
US EPA #NC01918
Client:
Enviro Choice Recycling
CTS prof.
2309-0133
DWCert#37799
Project:
City of Lumberton
Regulatory
Yes
Sample Information
Sampled
Date 09/14/23
Received
AML pate
09/14/23
Analyses and Results
Lab ID
Sam le ID E
P m o Analyte
Result
Mn
`y, °' +:
v E ,�
Std. Methods
c =
Reference
2309-0133
-01 3ludgE Gr Fec. Coliform-S
7490000
CFu1g
36700 09/15/23 PD
9222D - MF
-02
5840000
cFurg
31100
-03
6460000
CFurg
57700
-04
5080000
CFutg
28900
-05
4620000
CFU19
28900
-06
6140000
CFulg
40400
-07
6900000
CFulg
36700
Geomean
6000000
2309-0133
-01 SlUdgE Gr TS (%)
1.10
%
0.01 09/15/23
2540 G -TS
-02
1.30
%
0.01
-03
0.69
%
0.01
-04
1.41
%
0.01
-05
1.37
%
OV
-06
0.96
%
0.01
-07
1.11
%
0.01
Report
Review
i
iD �
C/pG
Project Manager
Date
219 S. Steele Str. 919-208-4240
Sanford NC 27330 [e-mail] camerontesting.com

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Environment Testing
ANALYTICAL REPORT
PREPARED FOR
Attn: Cody Hunt
Hunt Environmental Associates ■r�
3330 Saddletree Rd
Lumberton, North Carolina 28360
Generated 12/7/2023 2:19:22 PM
JOB DESCRIPTION
City of Lumberton Soil
JOB NUMBER
752-13830-1

This report may not be reproduced except in full, and with written approval from the laboratory. The results relate only to the
samples tested. For questions please contact the Project Manager at the e-mail address or telephone number listed on this
page.
The test results in this report relate only to the samples as received by the laboratory and will meet all requirements of the
methodology, with any exceptions noted. This report shall not be reproduced except in full, without the express written
approval of the laboratory. All questions should be directed to the Eurofins Environment Testing Southeast, LLC Project
Manager.
IlJI�1'�`11(o Ip
Authorized for release by
Heather Trotter, Project Manager
Heather.Trottera-et.eurofinsus.com
[phone]
Generated
12/7/2023 2:19:22 PM
12
13
14
Eurofins Savannah is a laboratory within Eurofins Environment Testing Southeast, LLC, a company within Eurofins Environment Testing Group of Companies
Page 2 of 30 12/7/2023

Client: Hunt Environmental Associates
Project/Site: City of Lumberton Soil
Laboratory Job ID: 752-13830-1
Table of Contents
Cover Page ..............................................
1
Table of Contents .........................................
3
Definitions/Glossary.......................................
4
Case Narrative ...........................................
5
Detection Summary ........................................
6
Client Sample Results ......................................
7
QC Sample Results ........................................
8
QC Association Summary ...................................
13
Lab Chronicle ............................................
16
Certification Summary ......................................
17
Method Summary .........................................
19
Sample Summary .........................................
20
Chain of Custody ..........................................
21
Receipt Checklists .........................................
26
12
13
14
Page 3 of 30
Eurofins Raleigh
12/7/2023

Definitions/Glossary
Client: Hunt Environmental Associates
Project/Site: City of Lumberton Soil
Qualifiers
General Chemistry
Job ID: 752-13830-1
Qualifier Qualifier Description
4 MS, MSD: The analyte present in the original sample is greater than 4 times the matrix spike concentration; therefore, control limits are not
applicable.
HF Parameter with a holding time of 15 minutes. Test performed by laboratory at client's request. Sample was analyzed outside of hold time.
Glossary
Abbreviation These commonly used abbreviations may or may not be present in this report.
rl Listed under the "D" column to designate that the result is reported on a dry weight basis
%R Percent Recovery
CFL Contains Free Liquid
CFU Colony Forming Unit
CNF Contains No Free Liquid
DER Duplicate Error Ratio (normalized absolute difference)
Dil Fac Dilution Factor
DL Detection Limit (DoD/DOE)
DL, RA, RE, IN Indicates a Dilution, Re -analysis, Re -extraction, or additional Initial metals/anion analysis of the sample
DLC Decision Level Concentration (Radiochemistry)
EDL Estimated Detection Limit (Dioxin)
LOD Limit of Detection (DoD/DOE)
LOQ Limit of Quantitation (DoD/DOE)
MCL EPA recommended "Maximum Contaminant Level"
MDA Minimum Detectable Activity (Radiochemistry)
MDC Minimum Detectable Concentration (Radiochemistry)
MDL Method Detection Limit
ML Minimum Level (Dioxin)
MPN Most Probable Number
MQL Method Quantitation Limit
NC Not Calculated
ND Not Detected at the reporting limit (or MDL or EDL if shown)
NEG Negative / Absent
POS Positive / Present
PQL Practical Quantitation Limit
PRIES Presumptive
QC Quality Control
RER Relative Error Ratio (Radiochemistry)
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
TNTC Too Numerous To Count
12
13
14
Eurofins Raleigh
Page 4 of 30 12/7/2023

Case Narrative
Client: Hunt Environmental Associates
Project/Site: City of Lumberton Soil
Job ID: 752-13830-1
Laboratory: Eurofins Raleigh
Narrative
Job Narrative
752-13830-1
Job ID: 752-13830-1
Receipt
The samples were received on 11/16/2023 4:28 PM. Unless otherwise noted below, the samples arrived in good condition, and where
required, properly preserved and on ice. The temperature of the cooler at receipt was 3.50 C.
Metals
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.
General Chemistry
Method 351.2: The matrix spike / matrix spike duplicate (MS/MSD) recoveries for preparation batch 680-809235 and analytical batch
680-809544 were outside control limits for one or more analytes. See QC Sample Results for detail. Sample matrix interference and/or
non -homogeneity are suspected because the associated laboratory control sample (LCS) recovery is within acceptance limits.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
F47
12
13
14
Eurofins Raleigh
Page 5 of 30 12/7/2023

Detection Summary
Client: Hunt Environmental Associates
Job ID: 752-13830-1
Project/Site: City of Lumberton Soil
Client Sample ID: S-4 WWTP
Lab Sample ID: 752-13830-1
Analyte
Result Qualifier
RL
MDL
Unit
Dil Fac
D
Method
Prep Type
Sodium Adsorption Ratio
3.3
0.10
0.10
NONE
1
20B
Soluble
Aluminum
17000
920
310
mg/Kg
1
*
6010D
Total/NA
Calcium
14000
2300
340
mg/Kg
1
*
6010D
Total/NA
Copper
360
120
23
mg/Kg
1
*
6010D
Total/NA
Magnesium
3100
2300
420
mg/Kg
1
*
6010D
Total/NA
Potassium
8000
4600
510
mg/Kg
1
*
6010D
Total/NA
Chromium
190
46
7.9
mg/Kg
1
6010D
Total/NA
Sodium
53000
9200
2500
mg/Kg
1
6010D
Total/NA
Zinc
750
92
27
mg/Kg
1
#
6010D
Total/NA
Ammonia
180
16
6.8
mg/Kg
1
#
350.1-1993 R2.0
Total/NA
Nitrogen, Kjeldahl
120000
26000
15000
mg/Kg
20
351.2-1993 R2.0
Total/NA
Phosphorus
11000
510
280
mg/Kg
1
365.4-1974
Total/NA
Temperature
13.9 HF
0.1
0.1
Celsius
1
9045D
Total/NA
Soil pH in Water
7.8 HF
0.1
0.1
PH Units
1
9045D
Total/NA
Total Solids
1.8
0.10
0.10
%
1
SM 254OG
Total/NA
Nitrate Nitrite as N
200
110
29
mg/Kg
1
#
353.2-1993 R2.0
Soluble
Client Sample ID: S-4 WWTP
Lab Sample ID: 752-13830-2
CAnalyte
Result Qualifier
RL
MDL
Unit
Dil Fac
D
Method
Prep Type
Flashpoint
>200
1.0
1.0
Degrees F
1
EPA 1010B
Total/NA
m
This Detection Summary does not include radiochemical test results.
Eurofins Raleigh
Page 6 of 30 12/7/2023

Client Sample Results
Client: Hunt Environmental Associates
Project/Site: City of Lumberton Soil
Job ID: 752-13830-1
Client Sample ID: S-4 WWTP Lab Sample ID: 752-13830-1
Date Collected: 11/16/23 13:00 Matrix: Solid
Date Received: 11/16/23 16:28 Percent Solids: 1.9
Method: USDA 20B - Sodium Adsorption Ratio - Soluble
Analyte
Result Qualifier
Sodium Adsorption Ratio
3.3
Method: SW846 6010D - Metals
(ICP)
Analyte
Result Qualifier
Aluminum
17000
Arsenic
<55
Cadmium
<4.6
Calcium
14000
Copper
360
Lead
<28
Magnesium
3100
Molybdenum
<12
Nickel
<42
Potassium
8000
Chromium
190
Selenium
<51
Sodium
53000
Zinc
750
Method: SW846 7471 B - Mercury (CVAA)
Analyte
Result Qualifier
Mercury
<0.41
General Chemistry
Analyte
Result Qualifier
Ammonia (MCAWW 350.1-1993
180
R2.0)
Nitrogen, Kjeldahl (MCAWW
120000
351.2-1993 R2.0)
Phosphorus (EPA 365.4-1974)
11000
Cyanide, Reactive (SW846 9014)
<0.25
Sulfide, Reactive (SW846 9034)
<150
Temperature (SW846 9045D)
13.9 HF
Soil pH in Water (SW846 9045D)
7.8 HF
Total Solids (SM 2540G)
1.8
General Chemistry - Soluble
Analyte
Result Qualifier
Nitrate Nitrite as N (MCAWW
200
353.2-1993 R2.0)
RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
0.10
0.10
NONE
11/22/23 07:36
1
•
RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
920
310
mg/Kg
*
11/20/23 13:27
11/21/23 23:14
1
92
55
mg/Kg
*
11/20/23 13:27
11/21/23 23:14
1
23
4.6
mg/Kg
*
11/20/23 13:27
11/21/23 23:14
1
2300
340
mg/Kg
*
11/20/23 13:27
11/21/23 23:14
1
120
23
mg/Kg
*
11/20/23 13:27
11/21/23 23:14
1
46
28
mg/Kg
*
11/20/23 13:27
11/21/23 23:14
1
2300
420
mg/Kg
*
11/20/23 13:27
11/21/23 23:14
1
46
12
mg/Kg
*
11/20/23 13:27
11/21/23 23:14
1
180
42
mg/Kg
*
11/20/23 13:27
11/21/23 23:14
1
4600
510
mg/Kg
*
11/20/23 13:27
11/21/23 23:14
1
46
7.9
mg/Kg
*
11/20/23 13:27
11/21/23 23:14
1
Is
120
51
mg/Kg
*
11/20/23 13:27
11/21/23 23:14
1
9200
2500
mg/Kg
*
11/20/23 13:27
11/21/23 23:14
1
92
27
mg/Kg
*
11/20/23 13:27
11/21/23 23:14
1
M
RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
1.3
0.41
mg/Kg
*
11/22/2310:57
11/22/2317:20
1
RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
16
6.8
mg/Kg
*
11/20/2312:45
11/20/2314:27
1
26000
15000
mg/Kg
*
11/20/2311:48
11/21/2314:17
20
510
280
mg/Kg
11/20/23 11:48
11/21/23 08:37
1
0.25
0.25
mg/Kg
11/28/2316:11
11/29/2310:12
1
150
150
mg/Kg
11/28/2316:12
11/29/2310:09
1
0.1
0.1
Celsius
11/22/2313:34
1
0.1
0.1
PH Units
11/22/23 13:34
1
0.10
0.10
%
11/20/2312:12
1
RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
110
29
mg/Kg
11/27/2315:37
1
Client Sample ID: S-4 WWTP Lab Sample ID: 752-13830-2
Date Collected: 11/16/23 13:00 Matrix: Water
Date Received: 11/16/23 16:28
General Chemistry
Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac
Flash point (SW846 EPA 101013) >200 1.0 1.0 Degrees F 11/28/23 09:28 1
Page 7 of 30
Eurofins Raleigh
12/7/2023

QC Sample Results
Client: Hunt Environmental Associates
Job ID: 752-13830-1
Project/Site: City of Lumberton Soil
Method: 6010D - Metals (ICP)
Lab Sample ID: MB 680-809290/1-A
Client Sample ID: Method Blank
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 809730
Prep Batch: 809290
MB MB
Analyte
Result Qualifier
RL
MDL
Unit
D Prepared
Analyzed Dil Fac
Aluminum
<6.8
20
6.8
mg/Kg
11/20/23 13:27
11/21/23 22:30 1
Arsenic
<1.2
2.0
1.2
mg/Kg
11/20/23 13:27
11/21/23 22:30 1
Cadmium
<0.10
0.50
0.10
mg/Kg
11/20/23 13:27
11/21/23 22:30 1
Calcium
<7.4
50
7.4
mg/Kg
11/20/23 13:27
11/21/23 22:30 1
Copper
<0.50
2.5
0.50
mg/Kg
11/20/23 13:27
11/21/23 22:30 1
Lead
<0.61
1.0
0.61
mg/Kg
11/20/23 13:27
11/21/23 22:30 1
Magnesium
<9.1
50
9.1
mg/Kg
11/20/23 13:27
11/21/23 22:30 1
Molybdenum
<0.26
1.0
0.26
mg/Kg
11/20/23 13:27
11/21/23 22:30 1
Nickel
<0.90
4.0
0.90
mg/Kg
11/20/23 13:27
11/21/23 22:30 1
Potassium
<11
100
11
mg/Kg
11/20/23 13:27
11/21/23 22:30 1
Chromium
<0.17
1.0
0.17
mg/Kg
11/20/23 13:27
11/21/23 22:30 1
Selenium
<1.1
2.5
1.1
mg/Kg
11/20/23 13:27
11/21/23 22:30 1
Sodium
<55
200
55
mg/Kg
11/20/23 13:27
11/21/23 22:30 1
Zinc
<0.58
2.0
0.58
mg/Kg
11/20/23 13:27
11/21/23 22:30 1
Lab Sample ID: LCS 680-809290/2-A
Client Sample ID: Lab Control Sample
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 809730
Prep Batch: 809290
Spike
LCS LCS
%Rec
Analyte
Added
Result Qualifier
Unit
D %Rec
Limits
Aluminum
459
474
mg/Kg
103
80-120
Arsenic
9.09
9.36
mg/Kg
103
80. 120
Cadmium
4.55
4.89
mg/Kg
108
80. 120
Calcium
455
463
mg/Kg
102
80. 120
Copper
9.18
10.0
mg/Kg
109
80. 120
Lead
45.5
45.9
mg/Kg
101
80. 120
Magnesium
455
461
mg/Kg
101
80 - 120
Molybdenum
9.09
9.06
mg/Kg
100
80 - 120
Nickel
9.09
9.41
mg/Kg
103
80 - 120
Potassium
636
668
mg/Kg
105
80 - 120
Chromium
9.13
9.38
mg/Kg
103
80 - 120
Selenium
9.09
7.98
mg/Kg
88
80 - 120
Sodium
457
465
mg/Kg
102
80 - 120
Zinc
4.59
4.93
mg/Kg
107
80 - 120
Method: 7471 B - Mercury (CVAA)
Lab Sample ID: MB 680-809677/1-A
Client Sample ID: Method Blank
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 810051
Prep Batch: 809677
MB MB
Analyte Result Qualifier
RL
MDL Unit
D Prepared
Analyzed Dil Fac
Mercury <0.0075
0.024
0.0075 mg/Kg
11/22/2310:57
11/22/2314:26 1
Eurofins Raleigh
Page 8 of 30 12/7/2023

QC Sample Results
Client: Hunt Environmental Associates
Project/Site: City of Lumberton Soil
Job ID: 752-13830-1
Method: 7471 B - Mercury (CVAA) (Continued)
Lab Sample ID: LCS 680-809677/2-A Client Sample ID: Lab Control Sample
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 810051 Prep Batch: 809677
Spike LCS LCS %Rec
Analyte Added Result Qualifier Unit D %Rec Limits
Mercury 0.219 0.218 mg/Kg 99 80 - 120
Method: 350.1-1993 R2.0 - Nitrogen, Ammonia
Lab Sample ID: MB 680-809282/1-A
Matrix: Solid
Analysis Batch: 809328
MB MB
Analyte Result Qualifier RL
Ammonia <0.13 0.30
Lab Sample ID: LCS 680-809282/2-A
Matrix: Solid
Analysis Batch: 809328
Spike
Analyte Added
Ammonia 5.00
Client Sample ID: Method Blank
Prep Type: Total/NA
Prep Batch: 809282
MDL Unit D Prepared Analyzed Dil Fac
0.13 mg/Kg 11/20/2312:45 11/20/2314:08 1
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Prep Batch: 809282
LCS LCS %Rec
Result Qualifier Unit D %Rec Limits
4.59 mg/Kg 92 75 - 125
Method: 351.2-1993 R2.0 - Nitrogen, Total Nitrogen
Lab Sample ID: MB 680-809235/1-A
Client Sample ID: Method Blank
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 809544
Prep Batch: 809235
MB MB
Analyte Result Qualifier
RL
MDL Unit
D Prepared Analyzed Dil Fac
Nitrogen, Kjeldahl <11
19
11 mg/Kg
11/20/23 11:48 11/21/23 15:00 1
Lab Sample ID: LCS 680-809235/2-A
Client Sample ID: Lab Control Sample
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 809544
Prep Batch: 809235
Spike
LCS LCS
%Rec
Analyte
Added
Result Qualifier
Unit D %Rec Limits
Nitrogen, Kjeldahl
149
161
mg/Kg 108 75 - 125
Lab Sample ID: 752-13830-1 MS
Client Sample ID: S-4 WWTP
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 809544
Prep Batch: 809235
Sample Sample
Spike
MS MS
%Rec
Analyte Result Qualifier
Added
Result Qualifier
Unit D %Rec Limits
Nitrogen, Kjeldahl 120000
10100
107000 4
mg/Kg -178 75 - 125
Lab Sample ID: 752-13830-1 MSD
Client Sample ID: S-4 WWTP
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 809544
Prep Batch: 809235
Sample Sample
Spike
MSD MSD
%Rec RPD
Analyte Result Qualifier
Added
Result Qualifier
Unit D %Rec Limits RPD Limit
Nitrogen, Kjeldahl 120000
10100
85500 4
mg/Kg * -387 75 - 125 22 40
Eurofins Raleigh
Page 9 of 30 12/7/2023

QC Sample Results
Client: Hunt Environmental Associates
Project/Site: City of Lumberton Soil
Method: 353.2-1993 R2.0 - Nitrogen, Nitrate -Nitrite
Lab Sample ID: MB 680-810064/1-A
Matrix: Solid
Analysis Batch: 810141
MB MB
Analyte Result Qualifier
RL
Nitrate Nitrite as N <0.55
2.0
Lab Sample ID: LCS 680-810064/2-A
Matrix: Solid
Analysis Batch: 810141
Spike
Analyte
Added
Nitrate Nitrite as N
20.0
Lab Sample ID: LCSD 680-810064/3-A
Matrix: Solid
Analysis Batch: 810141
Spike
Analyte
Added
Nitrate Nitrite as N
20.0
Lab Sample ID: 752-13830-1 MS
Matrix: Solid
Analysis Batch: 810141
Sample Sample
Spike
Analyte Result Qualifier
Added
Nitrate Nitrite as N 200
1050
Lab Sample ID: 752-13830-1 MSD
Matrix: Solid
Analysis Batch: 810141
Sample Sample
Spike
Analyte Result Qualifier
Added
Nitrate Nitrite as N 200
1050
Job ID: 752-13830-1
Client Sample ID: Method Blank
Prep Type: Soluble
MDL Unit
D
Prepared Analyzed Dil Fac
0.55 mg/Kg
11/27/2315:32 1
Client
Sample ID: Lab Control Sample
Prep Type: Soluble
LCS
LCS
% Rec
Result
Qualifier
Unit
D %Rec Limits
23.4
mg/Kg
117 80 - 120
Client
Sample
ID: Lab Control Sample Dup
Prep Type: Soluble
LCSD
LCSD
%Rec RPD
Result
Qualifier
Unit
D %Rec Limits RPD Limit
23.5
mg/Kg
117 80 - 120 0 20
Client Sample ID: S-4 WWTP
Prep Type: Soluble
MS
MS
%Rec
Result
Qualifier
Unit
D %Rec Limits
1200
mg/Kg
96 80-120
Client Sample ID: S-4 WWTP
Prep Type: Soluble
MSD
MSD
%Rec RPD
Result
Qualifier
Unit
D %Rec Limits RPD Limit
1120
mg/Kg
88 80-120 7 20
Method: 365.4-1974 - Phosphorus, Total
Lab Sample ID: MB 680-809235/1-A Client Sample ID: Method Blank
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 809495 Prep Batch: 809235
MB MB
Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac
Phosphorus <4.2 7.6 4.2 mg/Kg 11/20/23 11:48 11/21/23 08:35 1
Lab Sample ID: LCS 680-809235/2-A Client Sample ID: Lab Control Sample
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 809495 Prep Batch: 809235
Spike LCS LCS %Rec
Analyte Added Result Qualifier Unit D %Rec Limits
Phosphorus 149 144 mg/Kg 96 70-130
Eurofins Raleigh
Page 10 of 30 12/7/2023

QC Sample Results
Client: Hunt Environmental Associates
Job I D: 752-13830-1
Project/Site: City of Lumberton Soil
Method: 365.4-1974 - Phosphorus, Total (Continued)
Lab Sample ID: 752-13830-1 MS
Client Sample ID: S-4 WWTP
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 809495
Prep Batch: 809235
Sample Sample
Spike
MS MS %Rec
Analyte Result Qualifier
Added
Result Qualifier Unit D %Rec Limits
Phosphorus 11000
10100
21300 mg/Kg 100 70-130
Lab Sample ID: 752-13830-1 MSD
Client Sample ID: S-4 WWTP
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 809495
Prep Batch: 809235
Sample Sample
Spike
MSD MSD %Rec RPD
Analyte Result Qualifier
Added
Result Qualifier Unit D %Rec Limits RPD Limit
Phosphorus 11000
10100
21100 mg/Kg 98 70-130 1 30
Method: 9014 - Cyanide, Reactive
Lab Sample ID: MB 400-652039/1-A
Client Sample ID: Method Blank
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 652136
Prep Batch: 652039
MB MB
Analyte Result Qualifier
RL
MDL Unit D Prepared Analyzed Dil Fac
Cyanide, Reactive <0.25
0.25
0.25 mg/Kg 11/28/23 16:11 11/29/23 10:00 1
Lab Sample ID: LCS 400-652039/2-A
Client Sample ID: Lab Control Sample
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 652136
Prep Batch: 652039
Spike
LCS LCS %Rec
Analyte
Added
Result Qualifier Unit D %Rec Limits
Cyanide, Reactive
1.00
0.575 mg/Kg 58 10 - 110
Lab Sample ID: MRL 400-652136/3
Client Sample ID: Lab Control Sample
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 652136
Spike
MRL MRL %Rec
Analyte
Added
Result Qualifier Unit D %Rec Limits
Cyanide, Reactive
0.00400
<0.25 mg/Kg 119 50 - 150
Method: 9034 - Sulfide, Reactive
Lab Sample ID: MB 400-652041/1-A
Client Sample ID: Method Blank
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 652117
Prep Batch: 652041
MB MB
Analyte Result Qualifier
RL
MDL Unit D Prepared Analyzed Dil Fac
Sulfide, Reactive <150
150
150 mg/Kg 11/28/23 16:12 11/29/23 10:09 1
Lab Sample ID: LCS 400-652041/2-A
Client Sample ID: Lab Control Sample
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 652117
Prep Batch: 652041
Spike
LCS LCS %Rec
Analyte
Added
Result Qualifier Unit D %Rec Limits
Sulfide, Reactive
1010
439 mg/Kg 43 10 - 110
Eurofins Raleigh
Page 11 of 30 12/7/2023

QC Sample Results
Client: Hunt Environmental Associates
Project/Site: City of Lumberton Soil
Job I D: 752-13830-1
Method: 9045D - pH
Lab Sample ID: LCS 680-809726/4 Client Sample ID: Lab Control Sample
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 809726
Spike LCS LCS %Rec
Analyte Added Result Qualifier Unit D %Rec Limits
pH 7.01 7.1 PH Units 101 79 -126
Method: EPA 1010B - Ignitability, Pensky-Martens Closed -Cup Method
Lab Sample ID: LCS 180-452887/1
Client Sample ID: Lab Control Sample
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 452887
Spike LCS LCS
%Rec
Analyte
Added Result Qualifier
Unit D %Rec Limits
Flashpoint
81.0 82.3
Degrees F 102 96 - 103
Lab Sample ID: LCSD 180-452887/7
Client Sample ID: Lab Control Sample Dup
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 452887
Spike LCSD LCSD
%Rec RPD
Analyte
Added Result Qualifier
Unit D %Rec Limits RPD Limit
Flashpoint
81.0 82.1
Degrees F 101 96 -103 0 20
Method: SM 254OG - Total, Fixed, and Volatile Solids
Lab Sample ID: MB 680-809259/1
Client Sample ID: Method Blank
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 809259
MB MB
Analyte Result Qualifier
RL MDL Unit
D Prepared Analyzed Dil Fac
Total Solids 99.9
0.10 0.10 %
11/20/23 12:12 1
Lab Sample ID: 752-13830-1 DU
Client Sample ID: S-4 WWTP
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 809259
Sample Sample
DU DU
RPD
Analyte Result Qualifier
Result Qualifier
Unit D RPD Limit
Total Solids 1.8
1.86
% 3 5
Eurofins Raleigh
Page 12 of 30 12/7/2023

QC Association Summary
Client: Hunt Environmental Associates
Job ID:
752-13830-1
Project/Site: City of Lumberton Soil
Metals
Analysis Batch: 452624
Lab Sample ID Client Sample ID
Prep Type
Matrix
Method
Prep Batch
752-13830-1 S-4 VVVVTP
Soluble
Solid
20B
Prep Batch: 809290
Lab Sample ID Client Sample ID
Prep Type
Matrix
Method
Prep Batch
752-13830-1 S-4 VVVVTP
Total/NA
Solid
3050B
MB 680-809290/1-A Method Blank
Total/NA
Solid
3050B
LCS 680-809290/2-A Lab Control Sample
Total/NA
Solid
3050B
Prep Batch: 809677
Lab Sample ID Client Sample ID
Prep Type
Matrix
Method
Prep Batch
752-13830-1 S-4 VVVVTP
Total/NA
Solid
7471 B
MB 680-809677/1-A Method Blank
Total/NA
Solid
7471 B
LCS 680-809677/2-A Lab Control Sample
Total/NA
Solid
7471 B
Analysis Batch: 809730
0
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
752-13830-1
S-4 VVWTP
Total/NA
Solid
6010D
809290
MB 680-809290/1-A
Method Blank
Total/NA
Solid
6010D
809290
LCS 680-809290/2-A
Lab Control Sample
Total/NA
Solid
6010D
809290
Analysis Batch: 810051
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
752-13830-1
S-4 VVWTP
Total/NA
Solid
7471 B
809677
MB 680-809677/1-A
Method Blank
Total/NA
Solid
7471 B
809677
LCS 680-809677/2-A
Lab Control Sample
Total/NA
Solid
7471 B
809677
General Chemistry
Analysis Batch: 452887
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
752-13830-2
S-4 WWTP
Total/NA
Water
EPA 1010B
LCS 180-452887/1
Lab Control Sample
Total/NA
Water
EPA 1010B
LCSD 180-452887/7
Lab Control Sample Dup
Total/NA
Water
EPA 1010B
Prep Batch: 652039
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
752-13830-1
S-4 WWTP
Total/NA
Solid
7.3.3
MB 400-652039/1-A
Method Blank
Total/NA
Solid
7.3.3
LCS 400-652039/2-A
Lab Control Sample
Total/NA
Solid
7.3.3
Prep Batch: 652041
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
752-13830-1
S-4 WWTP
Total/NA
Solid
7.3.4
MB 400-652041/1-A
Method Blank
Total/NA
Solid
7.3.4
LCS 400-652041/2-A
Lab Control Sample
Total/NA
Solid
7.3.4
Analysis Batch: 652117
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
752-13830-1
S-4 WWTP
Total/NA
Solid
9034
652041
MB 400-652041/1-A
Method Blank
Total/NA
Solid
9034
652041
LCS 400-652041/2-A
Lab Control Sample
Total/NA
Solid
9034
652041
Eurofins Raleigh
Page 13 of 30 12/7/2023

QC Association Summary
Client: Hunt Environmental Associates
Project/Site: City of Lumberton Soil
General Chemistry
Analysis Batch: 652136
Lab Sample ID
Client Sample ID
752-13830-1
S-4 WWTP
MB 400-652039/1-A
Method Blank
LCS 400-652039/2-A
Lab Control Sample
MRL 400-652136/3
Lab Control Sample
Prep Batch: 809235
Lab Sample ID
Client Sample ID
752-13830-1
S-4 WWTP
MB 680-809235/1-A
Method Blank
LCS 680-809235/2-A
Lab Control Sample
752-13830-1 MS
S-4 WWTP
752-13830-1 MSD
S-4 WWTP
Analysis Batch: 809259
Job ID: 752-13830-1
Prep Type
Matrix
Method
Total/NA
Solid
9014
Total/NA
Solid
9014
Total/NA
Solid
9014
Total/NA
Solid
9014
Prep Type
Matrix
Method
Total/NA
Solid
Digestion
Total/NA
Solid
Digestion
Total/NA
Solid
Digestion
Total/NA
Solid
Digestion
Total/NA
Solid
Digestion
Prep Batch
652039
652039
652039
Prep Batch
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
752-13830-1
S-4 WWTP
Total/NA
Solid
SM 254OG
MB 680-809259/1
Method Blank
Total/NA
Solid
SM 2540G
Is
752-13830-1 DU
S-4 WWTP
Total/NA
Solid
SM 254OG
Prep Batch: 809282
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
752-13830-1
S-4 WWTP
Total/NA
Solid
3-154
MB 680-809282/1-A
Method Blank
Total/NA
Solid
3-154
LCS 680-809282/2-A
Lab Control Sample
Total/NA
Solid
3-154
Analysis Batch: 809328
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
752-13830-1
S-4 WWTP
Total/NA
Solid
350.1-1993 R2.0
809282
MB 680-809282/1-A
Method Blank
Total/NA
Solid
350.1-1993 R2.0
809282
LCS 680-809282/2-A
Lab Control Sample
Total/NA
Solid
350.1-1993 R2.0
809282
Analysis Batch: 809405
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
752-13830-1
S-4 WWTP
Total/NA
Solid
Moisture
Analysis Batch: 809495
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
752-13830-1
S-4 WWTP
Total/NA
Solid
365.4-1974
809235
MB 680-809235/1-A
Method Blank
Total/NA
Solid
365.4-1974
809235
LCS 680-809235/2-A
Lab Control Sample
Total/NA
Solid
365.4-1974
809235
752-13830-1 MS
S-4 WWTP
Total/NA
Solid
365.4-1974
809235
752-13830-1 MSD
S-4 WWTP
Total/NA
Solid
365.4-1974
809235
Analysis Batch: 809544
Lab Sample ID
Client Sample ID
752-13830-1
S-4 WWTP
MB 680-809235/1-A
Method Blank
LCS 680-809235/2-A
Lab Control Sample
752-13830-1 MS
S-4 WWTP
752-13830-1 MSD
S-4 WWTP
Prep Type
Matrix
Total/NA
Solid
Total/NA
Solid
Total/NA
Solid
Total/NA
Solid
Total/NA
Solid
Method
Prep Batch
351.2-1993
R2.0
809235
351.2-1993
R2.0
809235
351.2-1993
R2.0
809235
351.2-1993
R2.0
809235
351.2-1993
R2.0
809235
Page 14 of 30
Eurofins Raleigh
12/7/2023

QC Association Summary
Client: Hunt Environmental Associates Job ID: 752-13830-1
Project/Site: City of Lumberton Soil
General Chemistry
Analysis Batch: 809726
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
752-13830-1 S-4 WWTP Total/NA Solid 9045D
LCS 680-809726/4 Lab Control Sample Total/NA Solid 9045D
Leach Batch: 810064
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
752-13830-1
S-4 WWTP
Soluble
Solid
DI Leach
MB 680-810064/1-A
Method Blank
Soluble
Solid
DI Leach
LCS 680-810064/2-A
Lab Control Sample
Soluble
Solid
DI Leach
LCSD 680-810064/3-A
Lab Control Sample Dup
Soluble
Solid
DI Leach
752-13830-1 MS
S-4 WWTP
Soluble
Solid
DI Leach
752-13830-1 MSD
S-4 WWTP
Soluble
Solid
DI Leach
Analysis Batch: 810141
Prep Batch
0
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
752-13830-1
S-4 WWTP
Soluble
Solid
353.2-1993 R2.0
810064
MB 680-810064/1-A
Method Blank
Soluble
Solid
353.2-1993 R2.0
810064
LCS 680-810064/2-A
Lab Control Sample
Soluble
Solid
353.2-1993 R2.0
810064
LCSD 680-810064/3-A
Lab Control Sample Dup
Soluble
Solid
353.2-1993 R2.0
810064
752-13830-1 MS
S-4 WWTP
Soluble
Solid
353.2-1993 R2.0
810064
752-13830-1 MSD
S-4 WWTP
Soluble
Solid
353.2-1993 R2.0
810064
Eurofins Raleigh
Page 15 of 30 12/7/2023

Lab Chronicle
Client: Hunt Environmental Associates
Job ID: 752-13830-1
Project/Site: City of Lumberton Soil
Client Sample ID: S-4 WWTP
Lab Sample ID: 752-13830-1
Date Collected: 11/16/23 13:00
Matrix: Solid
Date Received: 11/16/23 16:28
Batch Batch
Dilution
Batch
Prepared
Prep Type Type Method
Run Factor
Number
Analyst
Lab
or Analyzed
Soluble Analysis 20B
1
452624
RJR
EET PIT
11/22/23 07:36
Total/NA Prep 7.3.3
652039
JP
EET PEN
11/28/23 16:11
Total/NA Analysis 9014
1
652136
KWS
EET PEN
11/29/23 10:12
Total/NA Prep 7.3.4
652041
JP
EET PEN
11/28/23 16:12
Total/NA Analysis 9034
1
652117
JP
EET PEN
11/29/23 10:09
Total/NA Analysis 9045D
1
809726
SM
EET SAV
11/22/23 13:34
Total/NA Analysis Moisture
1
809405
KG
EET SAV
11/21/23 10:01
Total/NA Analysis SM 254OG
1
809259
AS
EET SAV
11/20/23 12:12
Client Sample ID: S-4 WWTP
Lab Sample ID: 752-13830-1
Date Collected: 11/16/23 13:00
Matrix: Solid
Date Received: 11/16/23 16:28
Percent Solids: 1.9
Batch Batch
Dilution
Batch
Prepared
Prep Type Type Method
Run Factor
Number
Analyst
Lab
or Analyzed
Total/NA Prep 3050B
809290
BCB
EET SAV
11/20/23 13:27
Total/NA Analysis 6010D
1
809730
BCB
EET SAV
11/21/23 23:14
Total/NA Prep 7471 B
809677
DW
EET SAV
11/22/23 10:57 m
Total/NA Analysis 7471 B
1
810051
BCB
EET SAV
11/22/23 17:20
Total/NA Prep 3-154
809282
TD
EET SAV
11/20/23 12:45
Total/NA Analysis 350.1-1993 R2.0
1
809328
TD
EET SAV
11/20/23 14:27
Total/NA Prep Digestion
809235
SM
EET SAV
11/20/23 11:48
Total/NA Analysis 351.2-1993 R2.0
20
809544
NVF
EET SAV
11/21/23 14:17
Soluble Leach DI Leach
810064
NVF
EET SAV
11/27/23 11:16
Soluble Analysis 353.2-1993 R2.0
1
810141
NVF
EET SAV
11/27/23 15:37
Total/NA Prep Digestion
809235
SM
EET SAV
11/20/23 11:48
Total/NA Analysis 365.4-1974
1
809495
NVF
EET SAV
11/21/23 08:37
Client Sample ID: S-4 WWTP
Lab Sample ID: 752-13830-2
Date Collected: 11/16/23 13:00
Matrix: Water
Date Received: 11/16/23 16:28
Batch Batch
Dilution
Batch
Prepared
Prep Type Type Method
Run Factor
Number
Analyst
Lab
or Analyzed
Total/NA Analysis EPA 1010B
1
452887
SNR
EET PIT
11/28/23 09:28
Laboratory References:
EET PEN = Eurofins Pensacola, 3355 McLemore Drive, Pensacola, FL 32514, TEL [phone]
EET PIT = Eurofins Pittsburgh, 301 Alpha Drive, RIDC Park, Pittsburgh, PA 15238, TEL [phone]
EET SAV = Eurofins Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL [phone]
Eurofins Raleigh
Page 16 of 30 12/7/2023

Accreditation/Certification Summary
Client: Hunt Environmental Associates
Job ID: 752-13830-1
Project/Site: City of Lumberton Soil
Laboratory: Eurofins Pensacola
All accreditations/certifications held by this laboratory are listed. Not all accreditations/certifications are applicable to this report.
Authority Program
Identification Number
Expiration Date
Alabama State
40150
06-30-24
ANAB ISO/IEC 17025
L2471
02-22-26
Arkansas DEQ State
88-00689
08-01-24
California State
2510
06-30-24
Florida NELAP
E81010
06-30-24
Georgia State
E81010(FL)
06-30-24
Illinois NELAP
200041
10-09-24
Kansas NELAP
E-10253
10-31-24
Kentucky (UST) State
53
06-30-24
Louisiana (All) NELAP
30976
06-30-24
Louisiana (DVV) State
LA017
12-31-23
North Carolina (VWV/SV) State
314
12-31-23
Oklahoma NELAP
9810
08-31-24
Pennsylvania NELAP
68-00467
01-31-24
South Carolina State
96026
06-30-24
Tennessee State
TN02907
06-30-24
Texas NELAP
T104704286
09-30-24
US Fish & Wildlife US Federal Programs
A22340
06-30-24
USDA US Federal Programs
FLGNV23001
01-08-26
USDA US Federal Programs
P330-21-00056
05-17-24
Virginia NELAP
460166
06-14-24
West Virginia DEP State
136
03-31-24
West Virginia DEP State
136
03-31-24
Laboratory: Eurofins Pittsburgh
All accreditations/certifications held by this laboratory are listed. Not all accreditations/certifications are applicable to this report.
Authority
Program
Identification Number
Expiration Date
Arkansas DEQ
State
19-033-0
06-27-24
California
State
2891
04-30-24
Connecticut
State
PH-0688
09-30-24
Florida
NELAP
E871008
06-30-24
Georgia
State
PA 02-00416
04-30-24
Illinois
NELAP
004375
06-30-24
Kansas
NELAP
E-10350
01-31-24
Kentucky (UST)
State
162013
04-30-23'
Kentucky (WW)
State
KY98043
12-31-23
Louisiana
NELAP
04041
06-30-22
Louisiana (All)
NELAP
04041
06-30-24
Maine
State
PA00164
03-06-24
Minnesota
NELAP
042-999-482
12-31-23
New Hampshire
NELAP
2030
04-04-24
New Jersey
NELAP
PA005
06-30-24
New York
NELAP
11182
04-01-24
North Carolina (VWV/SVV)
State
434
12-31-23
North Dakota
State
R-227
04-30-24
Oregon
NELAP
PA-2151
02-06-24
Pennsylvania
NELAP
02-00416
04-30-24
Rhode Island
State
LAO00362
12-31-22'
South Carolina
State
89014
04-30-23'
Accreditation/Certification renewal pending - accreditation/certification considered valid.
12
13
14
Eurofins Raleigh
Page 17 of 30 12/7/2023

Accreditation/Certification Summary
Client: Hunt Environmental Associates
Job ID: 752-13830-1
Project/Site: City of Lumberton Soil
Laboratory: Eurofins Pittsburgh (Continued)
All accreditations/certifications held by this laboratory are listed. Not all accreditations/certifications are applicable to this report.
Authority Program
Identification Number
Expiration Date
Texas NELAP
T104704528
03-31-24
US Fish & Wildlife US Federal Programs
058448
03-31-24
USDA US Federal Programs
P330-16-00211
04-11-26
Utah NELAP
PA001462019-8
05-31-24
Virginia NELAP
10043
07-14-24
West Virginia DEP State
142
01-31-24
Wisconsin State
998027800
08-31-24
Laboratory: Eurofins Savannah
Unless otherwise noted, all analytes for this laboratory were covered under each
accreditation/certification below.
Authority Program
Identification Number
Expiration Date
North Carolina (WW/SW) State
269
12-31-23
m
The following analytes are included in this report, but the laboratory is not certified by the governing authority
for which the agency does not offer certification.
Analysis Method
Prep Method
Matrix
Analyte
350.1-1993 R2.0
3-154
Solid
Ammonia
351.2-1993 R2.0
Digestion
Solid
Nitrogen, Kjeldahl
353.2-1993 R2.0
Solid
Nitrate Nitrite as N
365.4-1974
Digestion
Solid
Phosphorus
9045D
Solid
Soil pH in Water
9045D
Solid
Temperature
Moisture
Solid
Percent Moisture
Moisture
Solid
Percent Solids
SM 254OG
Solid
Total Solids
This list may include analytes
12
13
14
Eurofins Raleigh
Page 18 of 30 12/7/2023

Method Summary
Client: Hunt Environmental Associates
Project/Site: City of Lumberton Soil
Job ID: 752-13830-1
Method
Method Description
Protocol
Laboratory
20B
Sodium Adsorption Ratio
USDA
EET PIT
6010D
Metals (ICP)
SW846
EET SAV
7471 B
Mercury (CVAA)
SW846
EET SAV
350.1-1993 R2.0
Nitrogen, Ammonia
MCAWW
EET SAV
351.2-1993 R2.0
Nitrogen, Total Nitrogen
MCAWW
EET SAV
353.2-1993 R2.0
Nitrogen, Nitrate -Nitrite
MCAWW
EET SAV
365.4-1974
Phosphorus, Total
EPA
EET SAV
9014
Cyanide, Reactive
SW846
EET PEN
9034
Sulfide, Reactive
SW846
EET PEN
9045D
pH
SW846
EET SAV
EPA 1010B
Ignitability, Pensky-Martens Closed -Cup Method
SW846
EET PIT
Moisture
Percent Moisture
EPA
EET SAV
SM 2540G
Total, Fixed, and Volatile Solids
SM
EET SAV
3050B
Preparation, Metals
SW846
EET SAV
3-154
Ammonia ( Sediments)
EPA
EET SAV
7.3.3
Cyanide, Reactive
SW846
EET PEN
7.3.4
Sulfide, Reactive
SW846
EET PEN
7471 B
Preparation, Mercury
SW846
EET SAV
DI Leach
Deionized Water Leaching Procedure
ASTM
EET SAV
Digestion
Digestion, Hot Block
EPA
EET SAV
Protocol References:
ASTM = ASTM International
EPA= US Environmental Protection Agency
MCAWW = "Methods For Chemical Analysis Of Water And Wastes", EPA-600/4-79-020, March 1983 And Subsequent Revisions.
SM = "Standard Methods For The Examination Of Water And Wastewater"
SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.
USDA = "USDA Agriculture Handbook 60, section 2013".
Laboratory References:
EET PEN = Eurofins Pensacola, 3355 McLemore Drive, Pensacola, FL 32514, TEL [phone]
EET PIT = Eurofins Pittsburgh, 301 Alpha Drive, RIDC Park, Pittsburgh, PA 15238, TEL [phone]
EET SAV = Eurofins Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL [phone]
11
12
13
14
Eurofins Raleigh
Page 19 of 30 12/7/2023

Sample Summary
Client: Hunt Environmental Associates
Project/Site: City of Lumberton Soil
Lab Sample ID Client Sample ID Matrix Collected Received
752-13830-1 S-4 VVWTP Solid 11/16/23 13:00 11/16/23 16:28
752-13830-2 S-4 VVVVTP
Water 11/16/2313:00 11/16/2316:28
Job I D: 752-13830-1
12
13
74
Page 20 of 30
Eurofins Raleigh
12/7/2023

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Eurofins Raleigh a
102-A Woodwinds Industrial Court Chain of Custody Record •'r titi eurofins
Cary, NC 27511 i Environment Testing
Phone: [phone]
Sampler. Lab PM:
Camer Tracking No(s):
COC No:
Client Information Sub Contract Lab
Trotter, Heather
752-1867.1
Client Contact
Phone: E-Mail:
State of Origin:
Page:
Shipping/Receiving
[e-mail]
North Carolina
Page 1 of 1
Company:
Accreditation Required (See note):
Job #:
Eurofins Environment Testing Southeast,
State - North Carolina (WWISW)
752-13830-1
Address:
Due Date Requested:
Preservation Codes:
5102 LaRoche Avenue,
11/27/2023
Analysis
Requested
A-HCL M-Hexane
B - NaOH N - None
City:
TAT Requested (days):
Savannah
—
C - Zn Acetate O - AsNa02
D - Nitric Acid P - Na2043
O - Na2S03
State, Zip:m
GA, 31404
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x
A
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E - NaHSO4
03
F- McOH S- H2SO4
Phone:
PO #;
912-354-7858 el 912-352-0165 Fax
(T ) ( )
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Z
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=
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0
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A
0
-
2
H-Amchlor
H - Amchlor Acid T - TSP Dodecahydrate
U-Acetone
-Ice V- MCAA
Email:
WO #:
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J- E Water W- pH 4-5
L - EDTA Y - Trizma
L- EDA
Project Name:
Project #:
City of Lumberton
75201611
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Special Instructions/Note:
Preservation Code:
S-4 WWTP (752-13830-1)
11/16/23
Solid
X
X
X
X
X
X
X
X
X
X
10
Eastern
aster
Note: Since laboratory accreditations are subject to change, Eurofins Environment Testing Southeast, LLC places the ownership of method, analyte & accreditation compliance upon our subcontract laboratories. This sample shipment is forwarded under chain -of -custody. If the laboratory
does not currently maintain accreditation in the State of Origin listed above for analysishestslmatrix being analyzed, the samples must be shipped bark to the Eurofins Environment Testing Southeast, LLC laboratory or other instructions will be provided. Any changes to accreditation
status should be brought to Eurofins Environment Testing Southeast, LLC attention immediately. If all requested accreditations are current to date, return the signed Chain of Custody attesting to said compliance to Eurofins Environment Testing Southeast, LLC.
Possible Hazard Identification
Sample Disposal (A fee may be assessed if samples are retained longer than 1 month)
Unconfirmed
= Return To Client 0 Disposal By Lab Archive For Months
I
Deliverable Requested: I, II, III, IV, Other (specify) Primary Deliverable Rank: 2
Special Instructions/QC Requirements:
Empty Kit Relinquished by:
Date:
Time:
Method of shipment
Relinquished b
Date lime:
r� Company
Received by.
Date/Time:
Company
Relinquished by.
Date ime: Company
Received by.
Date/Time:
Company
Relinquished by
DatelTime: Company
Received by.J
i'ro ^
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ymQ�any�/_7�t_7
,V_1
Custody Seals Intact:
Custody Seal No.:
Cooler Temperature(s) °C and other Remarks:
A Yes A No
Page 25 of 30 Ver: 06/08/20FL/7/2023

Login Sample Receipt Checklist
Client: Hunt Environmental Associates Job Number: 752-13830-1
Login Number: 13830
List Number: 1
Creator: Yonish, Rachel
Question
List Source: Eurofins Raleigh
Answer Comment
Radioactivity wasn't checked or is </= background as measured by a survey
True
meter.
The cooler's custody seal, if present, is intact.
True
Sample custody seals, if present, are intact.
True
The cooler or samples do not appear to have been compromised or
True
tampered with.
Samples were received on ice.
True
Cooler Temperature is acceptable.
True
Cooler Temperature is recorded.
True
COC is present.
True
COC is filled out in ink and legible.
True
COC is filled out with all pertinent information.
True
Is the Field Sampler's name present on COC?
True
There are no discrepancies between the containers received and the COC.
True
Samples are received within Holding Time (excluding tests with immediate
True
HTs)
Sample containers have legible labels.
True
Containers are not broken or leaking.
True
Sample collection date/times are provided.
True
Appropriate sample containers are used.
True
Sample bottles are completely filled.
True
Sample Preservation Verified.
True
There is sufficient vol. for all requested analyses, incl. any requested
True
MS/MSDs
Containers requiring zero headspace have no headspace or bubble is
True
<6mm (1/4").
Multiphasic samples are not present.
True
Samples do not require splitting or compositing.
True
Residual Chlorine Checked.
True
12
13
14
Eurofins Raleigh
Page 26 of 30 12/7/2023

Client: Hunt Environmental Associates
Login Number: 13830
List Number: 4
Creator: Pardonner, Brett
Question
Login Sample Receipt Checklist
Answer Comment
Radioactivity wasn't checked or is </= background as measured by a survey
N/A
meter.
The cooler's custody seal, if present, is intact.
N/A
Sample custody seals, if present, are intact.
N/A
The cooler or samples do not appear to have been compromised or
True
tampered with.
Samples were received on ice.
True
Cooler Temperature is acceptable.
True
Cooler Temperature is recorded.
True
COC is present.
True
COC is filled out in ink and legible.
True
COC is filled out with all pertinent information.
True
Is the Field Sampler's name present on COC?
True
There are no discrepancies between the containers received and the COC.
True
Samples are received within Holding Time (excluding tests with immediate
True
HTs)
Sample containers have legible labels.
True
Containers are not broken or leaking.
True
Sample collection date/times are provided.
True
Appropriate sample containers are used.
True
Sample bottles are completely filled.
True
Sample Preservation Verified.
N/A
There is sufficient vol. for all requested analyses, incl. any requested
True
MS/MSDs
Containers requiring zero headspace have no headspace or bubble is
N/A
<6mm (1/4").
Multiphasic samples are not present.
True
Samples do not require splitting or compositing.
True
Residual Chlorine Checked.
N/A
0.7°C IR8
Job Number: 752-13830-1
List Source: Eurofins Pensacola
List Creation: 11/18/23 06:00 PM
12
13
14
Eurofins Raleigh
Page 27 of 30 12/7/2023

Login Sample Receipt Checklist
Client: Hunt Environmental Associates Job Number: 752-13830-1
Login Number: 13830
List Number: 3
Creator: Oster, Rachel A
Question
List Source: Eurofins Pittsburgh
List Creation: 11/18/23 03:14 PM
Answer Comment
Radioactivity wasn't checked or is </= background as measured by a survey
N/A
meter.
The cooler's custody seal, if present, is intact.
True
Sample custody seals, if present, are intact.
True
The cooler or samples do not appear to have been compromised or
True
tampered with.
Samples were received on ice.
True
Cooler Temperature is acceptable.
True
Cooler Temperature is recorded.
True
COC is present.
True
COC is filled out in ink and legible.
True
COC is filled out with all pertinent information.
True
Is the Field Sampler's name present on COC?
N/A
There are no discrepancies between the containers received and the COC.
True
Samples are received within Holding Time (excluding tests with immediate
True
HTs)
Sample containers have legible labels.
True
Containers are not broken or leaking.
True
Sample collection date/times are provided.
True
Appropriate sample containers are used.
True
Sample bottles are completely filled.
True
Sample Preservation Verified.
True
There is sufficient vol. for all requested analyses, incl. any requested
True
MS/MSDs
Containers requiring zero headspace have no headspace or bubble is
True
<6mm (1/4").
Multiphasic samples are not present.
True
Samples do not require splitting or compositing.
True
Residual Chlorine Checked.
N/A
12
13
14
Eurofins Raleigh
Page 28 of 30 12/7/2023

Login Sample Receipt Checklist
Client: Hunt Environmental Associates Job Number: 752-13830-1
Login Number: 13830
List Number: 5
Creator: Kovitch, Christina M
Question
List Source: Eurofins Pittsburgh
List Creation: 11/28/23 09:21 AM
Answer Comment
Radioactivity wasn't checked or is </= background as measured by a survey
N/A
meter.
The cooler's custody seal, if present, is intact.
True
Sample custody seals, if present, are intact.
True
The cooler or samples do not appear to have been compromised or
True
tampered with.
Samples were received on ice.
True
Cooler Temperature is acceptable.
True
Cooler Temperature is recorded.
True
COC is present.
True
COC is filled out in ink and legible.
True
COC is filled out with all pertinent information.
True
Is the Field Sampler's name present on COC?
True
There are no discrepancies between the containers received and the COC.
True
Samples are received within Holding Time (excluding tests with immediate
True
HTs)
Sample containers have legible labels.
True
Containers are not broken or leaking.
True
Sample collection date/times are provided.
True
Appropriate sample containers are used.
True
Sample bottles are completely filled.
True
Sample Preservation Verified.
True
There is sufficient vol. for all requested analyses, incl. any requested
True
MS/MSDs
Containers requiring zero headspace have no headspace or bubble is
True
<6mm (1/4").
Multiphasic samples are not present.
True
Samples do not require splitting or compositing.
True
Residual Chlorine Checked.
N/A
12
13
14
Eurofins Raleigh
Page 29 of 30 12/7/2023

Login Sample Receipt Checklist
Client: Hunt Environmental Associates Job Number: 752-13830-1
Login Number: 13830
List Number: 2
Creator: Watters, David
Question
List Source: Eurofins Savannah
List Creation: 11/18/23 12:53 PM
Answer Comment
Radioactivity wasn't checked or is </= background as measured by a survey
N/A
meter.
The cooler's custody seal, if present, is intact.
True
Sample custody seals, if present, are intact.
True
The cooler or samples do not appear to have been compromised or
True
tampered with.
Samples were received on ice.
True
Cooler Temperature is acceptable.
True
Cooler Temperature is recorded.
True
COC is present.
True
COC is filled out in ink and legible.
True
COC is filled out with all pertinent information.
True
Is the Field Sampler's name present on COC?
N/A
There are no discrepancies between the containers received and the COC.
True
Samples are received within Holding Time (excluding tests with immediate
True
HTs)
Sample containers have legible labels.
True
Containers are not broken or leaking.
True
Sample collection date/times are provided.
True
Appropriate sample containers are used.
True
Sample bottles are completely filled.
True
Sample Preservation Verified.
N/A
There is sufficient vol. for all requested analyses, incl. any requested
True
MS/MSDs
Containers requiring zero headspace have no headspace or bubble is
False
<6mm (1/4").
Multiphasic samples are not present.
True
Samples do not require splitting or compositing.
True
Residual Chlorine Checked.
N/A
12
13
14
Eurofins Raleigh
Page 30 of 30 12/7/2023

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Lumberton
W W TP Name: City of Lumberton
Monitoring Period: From 10/1/2023 To
WQ Permit Number:
NPDES Number:
12/31 /2023
WQ0000672
NCL-024571
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. A (time/temp) ❑
1 Alt B (Alk Treatment) ❑
I Alt. C (Prior Testing) ❑
Alt.D (No Prior Test) ❑
I Process to Further Reduce Pathogengs ❑
If applicable to alternative
performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost 01
Heat Drying ❑
Heat Treatment ❑
Thermophilic ❑
Beta Ray 01
Gamma Ray ❑
Pasteurization ❑
Class B:
JAIL (1) Fecal Density p
Alt. (2) Process to Significantly Reduce Pathogens C,
If applicable to alternative
performed (Class
B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization ❑
I Air Drying ❑
Composting ❑
Aerobic Digestion ❑
Anaerobic Digestion ❑
If applicable to alternative performed (Class A or Class B) complete the following
monitoring data:
Parameter
Allowable Level
in Sludge
Pathogen Density
Number o
Excee-
n
Frequency
of Analysis
Sample
Type
Analytical
Tech -
nioue
MinimumGeo.
Mean
MaximumUnits
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
CFU
3300000
4090000
4680000
CFU/ g
Quarterly
Q y
Grab
9222-MF
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per 4 grams
total solid (dry
weight)
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed:
Alt.1 (VS reduction) ❑
Alt. 2 (40-day bench) ❑
Alt. 3 (30-day bench) ,J
Alt. 4 (Spec. OZ uptake) ❑
Alt. 5 (14-Day Aerobic) ❑
Alt. 6 (Alk. Stabilization ❑
Alt 7 (Drying - Stable) ❑
Alt. 8 (Drying - Unstable) ❑
Alt. 9 (Injection) ❑
Alt. 10 (Incorporation) ❑
No vector attraction reduction alternatives were performed ❑
CERTIFICATION STATEMENT (please check the appropriate statement)
`'❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
0 "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note
if you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Michael C Hunt, ORC Michael C Hunt, ORC
Prepar r Name and Title (ty e or int)
2/20/2024
Signature of Preparer* Date
Land Applier Name and Title (if applicable)(type or print)
Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 02T (12/2006)

Cameron Testing Services, Inc. Laboratory Report
NC DENR#654
NC PHHS #37799
US EPA#NC01918
Client:
Enviro-Choice Recycling CTS Prof.
2311-0180
DWCert#37799
Project:
City of Lumberton Regulatory
Yes
Sample Information
Sampled
CS Date 11/16/23 Received
KJW Date
11/16/23
Analyses and Results
Lab ID
Sample ID y E
P o Analyte Result
N�
Q
m E
} °5
M
Std. Methods
U
n
Reference
2311- 01
1 1 /16 1:00 Sludge Gr Fec. Coliform-S 3930000
CFUIg
26600
11/17/23 PD
9222D - MF
0 4250000
CFUIg
26600
0 4680000
CFUIg
26600
0 4250000
CFUIg
266o0
0 4570000
CFUIg
266CO
0 3830000
CFUIg
26600
0 3300000
CFUIg
26600
Geomean 4090000
2311- Q1
11/16 1:00 31udge Gr TS (%) 1.86
%
0.01
11/17/23 PD
2540 G -TS
0 1.86
%
0.01
0 1.86
%
001
0 1.85
%
001
0 1,86
%
aoi
0 1.86
%
0.01
0 1.86
%
0.01
Report
Review
Project Manager Date
219 S. Steele Str. 919-208-4240
Sanford NC 27330 chrisocamerontesting.com

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WAT R5 IC L RAL
LA O IE , INC.
Soil Analysis Report - NCDA Index
Waters Agricultural Laboratories, Inc
364 W. Park Drive I Warsaw, NC 28398- 1 Phone [phone]
cth/ S GLt "1Z?%}
ENVIRO CHOICE RECYCLING [21100] Grower: RONALD HAMMONDS Page 1
Farm: RO-20
PO BOX 390 LID: Target pH: 6
LUMBERTON, NC 28359- Test Method: Mehlich III Received: 1/25/2024 Processed: 1/29/2024
P-1
K-1
Mg (%)
Ca (%)
pHw
Ac
S-1
Zn-1
Zn-AI
Mn-1
Mn-AI
Cu-1
Na
ESP
CEC
BS (%)
HM (%)
Soil Class
HF 3
898020ZW
453
101
17
53
5.3
3.2
97
1654
1654
112
84
772
0.3
2
12.2
74
0.61
Min
HF 4
898021ZW
463
63
19
48
5.4
3.2
77
1340
1340
78
64
708
0.3
2
10.7
70
0.86
Min
RC 6
898022ZW
138
81
20
58
6.1
2.0
41
324
324
50
45
198
0.3
3
10.8
81
1.27
Min
RC 7
898023ZW
177
109
13
63
5.9
1.8
64
311
311
34
37
225
0.3
2
9.4
81
1.47
Min
RC 8
898024ZW
195
119
13
49
5.4
2.8
67
355
355
41
42
235
0.3
2
9.1
69
1.62
Min
RC 14
898025ZW
199
144
12
65
6.1
1.6
61
404
404
44
42
268
0.2
2
10.4
84
1.71
Min
Explanation of Symbols - % (percent), -1 (Index); Sodium (Na) and CEC reported in meq/100cm3 (milli -equivalent per 100 cubic centimeters)
Abbreviations: Ac (Acidity), CEC (Cation Exchange Capacity), BS (Base Saturation), HM (Humic Matter), ESP (Exchangeable Sodium Percentage)
NCDA Soil Fertility Recommendations (Ibs/A)
•
Lime
Tons/Acre
N
Nitrogen
P205
Phosphate
K20
Potash
Mg
Magnesium
s
Sulfur
B
Boron
Zn
Zinc
Mn
Manganese
Cu
Copper
See Note
HF 3
BERMUDA PASTURE M
1.7
220
30
12
HF 4
BERMUDA PASTURE M
1.6
220
80
12
RC 6
CORN GRAIN
160
20
3
RC 7
CORN GRAIN
0.3
160
3
RC 8
CORN GRAIN
1.4
160
3
RC 14
CORN GRAIN
160
3
Explanation of Symbols - Ibs/A (pounds per acre)
Fertilizer recommendations are based on the philosophy and recommendations of the NCDA Agronomic Division
DWQ Laboratory Certification Number 635
This document may be reproduced only in its entirety. Waters Agricutural Laboratories has no control over the manner in which samples are taken, therefore, analysis is based solely on the sample as received. Laboratory liability is limited to the fee assessed on the referenced sample.

WAT R5 IC L RAL
LA O IE , INC.
Soil Analysis Report - NCDA Index
Waters Agricultural Laboratories, Inc
364 W. Park Drive I Warsaw, NC 28398- 1 Phone [phone]
cth/ S GLt "1Z?%}
ENVIRO CHOICE RECYCLING [21100] Grower: PATRICK BULLARD Page 1
Farm: RO-39
PO BOX 390 LID: Target pH: 6
LUMBERTON, NC 28359- Test Method: Mehlich III Received: 1/25/2024 Processed: 1/29/2024
RmIlTilralP-1
K-1
Mg (%)
Ca (%)
pHw
Ac
S-1
Zn-1
Zn-AI
Mn-1
Mn-AI
Cu-1
Na
ESP
CEC
BS (%)
HM (%)
Soil Class
3903
898012ZW
25
31
11
40
5.4
2.8
38
90
90
22
30
35
0.2
2
6.0
53
1.30
Min
3904
898013ZW
60
51
15
56
6.1
1.4
33
98
98
34
36
70
0.2
3
5.7
76
0.86
Min
3905
898014ZW
66
87
14
46
5.8
2.0
35
138
138
31
36
78
0.2
2
6.2
67
0.68
Min
3906
898015ZW
113
51
15
51
5.6
1.6
52
131
131
34
37
102
0.2
2
5.4
70
0.55
Min
3909
898016ZW
282
29
14
46
5.5
2.0
59
391
391
56
51
322
0.3
4
5.4
63
0.49
Min
Explanation of Symbols - % (percent), -1 (Index); Sodium (Na) and CEC reported in meq/100cm3 (milli -equivalent per 100 cubic centimeters)
Abbreviations: Ac (Acidity), CEC (Cation Exchange Capacity), BS (Base Saturation), HM (Humic Matter), ESP (Exchangeable Sodium Percentage)
NCDA Soil Fertility Recommendations (Ibs/A)
_
Lime
Tons/Acre
N
Nitrogen
P205
Phosphate
K20
Potash
Mg
Magnesium
s
Sulfur
B
Boron
Zn
Zinc
Mn
Manganese
Cu
Copper
See Note
3903
BERMUDA PASTURE M
1.4
220
80
160
12
3904
BERMUDA PASTURE M
220
20
110
12
3905
BERMUDA PASTURE M
0.5
220
20
50
12
3906
BERMUDA PASTURE M
0.6
220
110
12
3909
BERMUDA PASTURE M
0.9
220
160
12
Explanation of Symbols - Ibs/A (pounds per acre)
Fertilizer recommendations are based on the philosophy and recommendations of the NCDA Agronomic Division
DWQ Laboratory Certification Number 635
This document may be reproduced only in its entirety. Waters Agricutural Laboratories has no control over the manner in which samples are taken, therefore, analysis is based solely on the sample as received. Laboratory liability is limited to the fee assessed on the referenced sample.

WAT R5 IC L RAL
LA O IE , INC.
Soil Analysis Report - NCDA Index
Waters Agricultural Laboratories, Inc
364 W. Park Drive I Warsaw, NC 28398- 1 Phone [phone]
cth/ S GLt "1Z?%}
ENVIRO CHOICE RECYCLING [21100] Grower: OZZEL BAKER Page 1
Farm: RO-16
PO BOX 390 LID: Target pH: 6
LUMBERTON, NC 28359- Test Method: Mehlich III Received: 1/25/2024 Processed: 1/29/2024
P-1
K-1
Mg (%)
Ca (%)
pHw
Ac
S-1
Zn-1
Zn-AI
Mn-1
Mn-AI
Cu-1
Na
ESP
CEC
BS (%)
HM (%)
Soil Class
1605
898031ZW
133
55
14
51
5.6
2.2
45
245
245
25
32
75
0.2
2
7.0
69
1.67
Min
1606
898032ZW
138
47
14
53
6.0
1.4
52
129
129
38
40
80
0.2
2
5.0
72
0.97
Min
1607
898033ZW
152
43
13
51
6.0
1.4
38
151
151
50
47
75
0.2
3
4.4
68
0.89
Min
1616
898034ZW
267
27
10
53
5.4
3.4
64
666
666
53
49
492
0.3
3
9.5
64
0.91
Min
1617
898035ZW
303
25
15
60
5.5
2.8
70
852
852
56
51
470
0.3
3
11.7
76
0.86
Min
1618
898036ZW
350
26
16
58
5.7
2.2
69
699
699
44
43
515
0.3
2
9.1
76
1.01
Min
1619
898037ZW
196
14
14
71
6.6
0.6
38
268
268
22
21
292
0.2
3
4.5
87
0.41
Min
Explanation of Symbols - % (percent), -1 (Index); Sodium (Na) and CEC reported in meq/100cm3 (milli -equivalent per 100 cubic centimeters)
Abbreviations: Ac (Acidity), CEC (Cation Exchange Capacity), BS (Base Saturation), HM (Humic Matter), ESP (Exchangeable Sodium Percentage)
NCDA Soil Fertility Recommendations (Ibs/A)
•
Lime
Tons/Acre
N
Nitrogen
P205
Phosphate
K20
Potash
Mg
Magnesium
s
Sulfur
B
Boron
Zn
Zinc
Mn
Manganese
Cu
Copper
See Note
1605
BERMUDA PASTURE M
0.9
220
100
12
1606
BERMUDA PASTURE M
220
120
12
1607
BERMUDA PASTURE M
220
120
12
1616
BERMUDA PASTURE M
1.7
220
180
12
1617
BERMUDA PASTURE M
1.3
220
180
12
1618
BERMUDA PASTURE M
0.7
220
180
12
1619
BERMUDA PASTURE M
220
200
UH
12
Explanation of Symbols - Ibs/A (pounds per acre)
Fertilizer recommendations are based on the philosophy and recommendations of the NCDA Agronomic Division
DWQ Laboratory Certification Number 635
This document may be reproduced only in its entirety. Waters Agricutural Laboratories has no control over the manner in which samples are taken, therefore, analysis is based solely on the sample as received. Laboratory liability is limited to the fee assessed on the referenced sample.

WAT R5 IC L RAL
LA O IE , INC.
Soil Analysis Report - NCDA Index
Waters Agricultural Laboratories, Inc
364 W. Park Drive I Warsaw, NC 28398- 1 Phone [phone]
cth/ S GLt "1Z?%}
ENVIRO CHOICE RECYCLING [21100] Grower: JESSIE OXENDINE Page 1
Farm: RO-17
PO BOX 390 LID: Target pH: 6
LUMBERTON, NC 28359- Test Method: Mehlich III Received: 1/25/2024 Processed: 1/29/2024
P-1
K-1
Mg (%)
Ca (%)
pHw
Ac
S-1
Zn-1
Zn-AI
Mn-1
Mn-AI
Cu-1
Na
ESP
CEC
BS (%)
HM (%)
Soil Class
1701
898026ZW
92
40
17
52
6.1
1.6
50
172
172
25
23
150
0.2
3
5.9
73
1.49
Min
1702
898027ZW
184
20
15
45
5.5
2.2
57
236
236
22
23
185
0.2
3
5.9
62
1.76
Min
1703
898028ZW
171
25
17
52
5.9
2.2
46
259
259
25
25
145
0.2
2
7.5
71
1.82
Min
1704
898029ZW
107
19
13
68
6.3
1.2
35
136
136
16
15
162
0.2
2
6.8
83
1.63
Min
1705
898030ZW
97
43
10
43
5.5
3.0
31
89
89
16
20
42
0.2
2
6.9
56
2.34
Min
Explanation of Symbols - % (percent), -1 (Index); Sodium (Na) and CEC reported in meq/100cm3 (milli -equivalent per 100 cubic centimeters)
Abbreviations: Ac (Acidity), CEC (Cation Exchange Capacity), BS (Base Saturation), HM (Humic Matter), ESP (Exchangeable Sodium Percentage)
NCDA Soil Fertility Recommendations (Ibs/A)
•
Lime
Tons/Acre
N
Nitrogen
P205
Phosphate
K20
Potash
Mg
Magnesium
s
Sulfur
B
Boron
Zn
Zinc
Mn
Manganese
Cu
Copper
See Note
1701
SOYBEANS
60
10
3
1702
SOYBEANS
1.0
100
10
3
1703
SOYBEANS
0.3
90
3
1704
SOYBEANS
100
10
3
1705
SOYBEANS
1.4
50
10
3
Explanation of Symbols - Ibs/A (pounds per acre)
Fertilizer recommendations are based on the philosophy and recommendations of the NCDA Agronomic Division
DWQ Laboratory Certification Number 635
This document may be reproduced only in its entirety. Waters Agricutural Laboratories has no control over the manner in which samples are taken, therefore, analysis is based solely on the sample as received. Laboratory liability is limited to the fee assessed on the referenced sample.

WAT R5 IC L RAL
LA O IE , INC.
Soil Analysis Report - NCDA Index
Waters Agricultural Laboratories, Inc
364 W. Park Drive I Warsaw, NC 28398- 1 Phone [phone]
cth/ S GLt "1Z?%}
ENVIRO CHOICE RECYCLING [21100] Grower: CARNELL LOCKLEAR Page 1
Farm: RO-28
PO BOX 390 LID: Target pH: 6
LUMBERTON, NC 28359- Test Method: Mehlich III Received: 1/25/2024 Processed: 1/29/2024
P-1
K-1
Mg (%)
Ca (%)
pHw
Ac
S-1
Zn-1
Zn-AI
Mn-1
Mn-AI
Cu-1
Na
ESP
CEC
BS (%)
HM (%)
Soil Class
2801
898017ZW
300
94
10
48
5.2
2.8
66
560
560
97
75
330
0.3
4
7.9
65
1.07
Min
2802
898018ZW
341
88
20
61
6.3
1.6
53
578
578
59
48
410
0.2
1
10.7
85
1.40
Min
2803
898019ZW
313
68
18
53
5.5
1.8
65
540
540
162
114
280
0.4
4
7.3
75
0.82
Min
Explanation of Symbols - % (percent), -1 (Index); Sodium (Na) and CEC reported in meq/100cm3 (milli -equivalent per 100 cubic centimeters)
Abbreviations: Ac (Acidity), CEC (Cation Exchange Capacity), BS (Base Saturation), HM (Humic Matter), ESP (Exchangeable Sodium Percentage)
NCDA Soil Fertility Recommendations (Ibs/A)
•
Lime
Tons/Acre
N
Nitrogen
P205
Phosphate
K20
Potash
Mg
Magnesium
s
Sulfur
B
Boron
Zn
Zinc
Mn
Manganese
Cu
Copper
See Note
2801
CORN GRAIN
1.6
160
3
2802
CORN GRAIN
160
3
2803
CORN GRAIN
0.8
160
20
3
Explanation of Symbols - Ibs/A (pounds per acre)
Fertilizer recommendations are based on the philosophy and recommendations of the NCDA Agronomic Division
DWQ Laboratory Certification Number 635
This document may be reproduced only in its entirety. Waters Agricutural Laboratories has no control over the manner in which samples are taken, therefore, analysis is based solely on the sample as received. Laboratory liability is limited to the fee assessed on the referenced sample.

City of Lumberton
Environmental Laboratory
Specific Oxygen Uptake Rate (SOUR) Worksheet
Date & Analyst: Tues 2-14-23 @0600 kcl Dig #2 Day 1
Total Solids
Sample volume used for total solids test: 5 mL
Weight of dish: 126.9171 g
Weight of dish + dried solids: 127.0070 g
Weight of dried solids: 0.0899 g
Total Solids: 17.98 g/L
SOUR
Time
(Minutes)
Temperature
Dissolved
Oxygen (mg/L)
oC
0
15.00
6.08
1
15.00
5.27
2
15.00
3.17
3
15.00
2.03
4
15.00
1.35
5
15.00
1.08
6
15.00
0.95
7
15.00
0.90
8
15.00
0.86
9
15.00
0.82
10
15.00
0.77
11
15.00
0.72
12
15.00
0.65
13
15.00
0.57
14
15.00
0.51
15
16.00
0.47
Oxygen Consumption Rate 0.28 mg/L/minute
SOUR 0.95 (mg/g)/hr
SOUR Temperature Correction
Average Sewage Sludge
Temperature During Test
°C
15.0625
If sewage sludge is > 20°C, SOUR = 1.21 (mg/g)/hr
If sewage sludge is < 20oC, SOUR = 1.33 (mg/g)/hr
SOUR passes if result is:5 1.5 (mg/g)hr
Version 11/1/11

City of Lumberton
Environmental Laboratory
Specific Oxygen Uptake Rate (SOUR) Worksheet
Date & Analyst: Wed 2-15-23 @0604 kcl Dig #2 Day 2
Total Solids
Sample volume used for total solids test: 5 mL
Weight of dish: 121.2473 g
Weight of dish + dried solids: 121.3399 g
Weight of dried solids: 0.0926 g
Total Solids: 18.52 g/L
SOUR
Time
(Minutes)
Temperature
Dissolved
Oxygen (mg/L)
oC
0
16.00
8.06
1
15.00
4.50
2
15.00
2.82
3
15.00
1.70
4
15.00
1.14
5
15.00
0.92
6
15.00
0.81
7
15.00
0.75
8
15.00
0.70
9
15.00
0.63
10
15.00
0.58
11
15.00
0.52
12
15.00
0.47
13
15.00
0.42
14
15.00
0.38
15
16.00
0.35
Oxygen Consumption Rate
SOUR
SOUR Temperature Correction
0.31 mg/L/minute
1.02 (mg/g)/hr
Average Sewage Sludge
Temperature During Test
oC
15.125
If sewage sludge is > 20°C, SOUR = 1.29 (mg/g)/hr
If sewage sludge is < 20°C, SOUR = 1Al (mg/g)/hr
SOUR passes if result is:5 1.5 (mg/g)hr
Version 11/1/11

City of Lumberton
Environmental Laboratory
Specific Oxygen Uptake Rate (SOUR) Worksheet
Date & Analyst: Thurs 2-16-23 @0603 kcl Dig #2 Day 3
Total Solids
Sample volume used for total solids test: 5 mL
Weight of dish: 89.0353 g
Weight of dish + dried solids: 89.1271 g
Weight of dried solids: 0.0918 g
Total Solids: 18.36 g/L
SOUR
Time
(Minutes)
Temperature
Dissolved
Oxygen (mg/L)
oC
0
19.00
8.03
1
17.00
4.33
2
17.00
2.62
3
17.00
1.57
4
17.00
1.05
5
17.00
0.91
6
17.00
0.86
7
17.00
0.82
8
17.00
0.78
9
17.00
0.75
10
17.00
0.72
11
17.00
0.68
12
17.00
0.60
13
17.00
0.53
14
17.00
0.47
15
17.00
0.41
Oxygen Consumption Rate
SOUR
SOUR Temperature Correction
0.29 mg/L/minute
0.96 (mg/g)/hr
Average Sewage Sludge
Temperature During Test
oC
17.125
If sewage sludge is > 20°C, SOUR = (mg/g)/hr
If sewage sludge is < 20°C, SOUR = 1.17 (mg/g)/hr
SOUR passes if result is:5 1.5 (mg/g)hr
Version 11/1/11

City of Lumberton
Environmental Laboratory
Specific Oxygen Uptake Rate (SOUR) Worksheet
Date & Analyst: Fri 2-17- 23 @0549 kcl Dig #2 Day 4
Total Solids
Sample volume used for total solids test: 5 mL
Weight of dish: 111.4085 g
Weight of dish + dried solids: 111.5019 g
Weight of dried solids: 0.0934 g
Total Solids: 18.68 g/L
SOUR
Time
(Minutes)
Temperature
Dissolved
Oxygen (mg/L)
oC
0
19.00
8.04
1
18.00
3.95
2
18.00
2.00
3
18.00
1.72
4
18.00
0.94
5
18.00
0.84
6
18.00
0.81
7
18.00
0.79
8
18.00
0.77
9
18.00
0.74
10
18.00
0.69
11
18.00
0.64
12
18.00
0.57
13
19.00
0.50
14
19.00
0.42
15
19.00
0.38
Oxygen Consumption Rate
SOUR
SOUR Temperature Correction
Average Sewage Sludge
Temperature During Test
°C
18.25
0.28 mg/L/minute
0.90 (mg/g)/hr
If sewage sludge is > 20°C, SOUR = 0.98 (mg/g)/hr
If sewage sludge is < 20°C, SOUR = 1.01 (mg/g)/hr
SOUR passes if result is:5 1.5 (mg/g)hr
Version 11/1/11

City of Lumberton
Environmental Laboratory
Specific Oxygen Uptake Rate (SOUR) Worksheet
Date & Analyst: Mon 2-20-23 @0559 kc4 Dig #2 Day 5
Total Solids
Sample volume used for total solids test:M125.5454
ml-
Weight of dish: g
Weight of dish + dried solids: g
Weight of dried solids: g
Total Solids: g/L
SOUR
Oxygen Consumption Rate 0.29
SOUR 0.99
SOUR Temperature Correction
Average Sewage Sludge
Temperature During Test
°C
15.25
mg/L/minute
(mg/g)/hr
If sewage sludge is > 20°C, SOUR = 1.25 (mg/g)/hr
If sewage sludge is < 20°C, SOUR = 1.36 (mg/g)/hr
SOUR passes if result is < 1.5 (mg/g)hr
Version 1111/11

City of Lumberton
Environmental Laboratory
Specific Oxygen Uptake Rate (SOUR) Worksheet
Date & Analyst: Tues 2-21-23 @0554 kc1l Dig #2 Day 6
Total Solids
Sample volume used for total solids test: 5 mL
Weight of dish: 43.9518 g
Weight of dish + dried solids: 44.0434 g
Weight of dried solids: 0.0916 g
Total Solids: 18.32 g/L
SOUR
Time
(Minutes)
Temperature
Dissolved
Oxygen (mg/L)
pC
0
18.00
8.07
1
17.00
4.56
2
17.00
2.62
3
17.00
1.50
4
17.00
0.99
5
16.00
0.82
6
16.00
0.78
7
17.00
0.75
8
17.00
0.75
9
17.00
0.74
10
17.00
0.73
11
17.00
0.72
12
17.00
0.70
13
17.00
0.67
14
17.00-1-0.64
15
17.00
1 0.60
Oxygen Consumption Rate
SOUR
SOUR Temperature Correction
Average Sewage Sludge
Temperature During Test
°C
16.9375
0.29 mg/L/minute
0.93 (mg/g)/hr
If sewage sludge is > 20°C, SOUR = 1}19 , (mg/g)/hr
If sewage sludge is < 20°C, SOUR = 1.15 (mg/g)/hr
SOUR passes if result is:5 1.5 (mg/g)hr
Version 11/1/11

City of Lumberton
Environmental Laboratory
Specific Oxygen Uptake Rate (SOUR) Worksheet
Date & Analyst: Wed 2-22-23 @0607 kcl Dig #2 Day 7
Total Solids
Sample volume used for total solids test: 5 mL
Weight of dish: 46.1036 g
Weight of dish + dried solids: 46.18§25 g
Weight of dried solids: 0.0789 g
Total Solids: 15.78 g/L
SOUR
Time
(Minutes)
Temperature
Dissolved
Oxygen (mg/L)
oC
0
18.00
8.25
1
18.00
5.80
2
17.00
3.74
3
17.00
2.75
4
17.00
1.97
5
17.00
1.38
6
17.00
0.92
7
17.00
0.70
g
17.00
0.68
9
17.00
0.68
10
18.00
0.68
11
18.00
0.67
12
18.00
0.67
13
18.00
0.66
14
18.00
0.63
15
18.00
0.61
Oxygen Consumption Rate 0.36 mg/L/minute
SOUR 1.39 (mg/g)/hr
SOUR Temperature Correction
i
Average Sewage Sludge
Temperature During Test
°C
17.5
If sewage sludge is > 20°C, SOUR =
If sewage sludge is < 20°C, SOUR =
SOUR passes if result is <_ I.
76M
Version 11/1/11

City of Lumberton
Environmental Laboratory
Specific Oxygen
Uptake Rate (SOUR) Worksheet
Date & Analyst: Thurs 2-23-23 @0606 kcl Dig #2 Day 7
Total Solids
5 mL
Sample volume used for total solids test: 46.9125 g
Weight of dish: 47.0030 g
Weight of dish + dried solids: 0.0030 g
Weight of dried solids: 18 02 g/L
Total Solids:
SOUR
Oxygen Consumption Rate
SOUR
SOUR Temperature Correction
U.JU
1.02
mg/L/minute
(mg/g)/hr
Average Sewage Sludge
Temperature During Test
°C
19
If sewage sludge is > 20-C, SOUR =
9.07 a(rnmg/g)/hr
g/g)/hr
If sewage sludge is < 20°C, SOUR =
SOUR passes if result is <_ 1.5 (mg/g)hr
Version 1111/11

City of Lumberton
Environmental Laboratory
Specific Oxygen Uptake Rate (SOUR) Worksheet
Date & Analyst: Mon 4-17-23 @0655 kcl Dig #2 Day1
Total Solids
Sample volume used for total solids test: 5 mL
Weight of dish: 125.4546 g
Weight of dish + dried solids: 125.5551 g
Weight of dried solids: 0.1005 g
Total Solids: 20.1 g/L
SOUR
Time
(Minutes)
Temperature
Dissolved
Oxygen (mg/L)
oC
0
21.00
6.16
1
20.00
1.14
2
21.00
0.64
3
21.00
0.44
4
21.00
0.39
5
21.00
0.35
6
21.00
0.32
7
21.00
0.30
8
21.00
0.29
9
21.00
0.28
10
21.00
0.27
11
21.00
0.26
12
21.00
0.25
13
21.00
0.24
14
21.00
0.24
15 1
19.00
0.24
Oxygen Consumption Rate
SOUR
SOUR Temperature Correction
Average Sewage Sludge
Temperature During Test
°C
20.8125
0.16 mg/L/minute
0.47 (mg/g)/hr
If sewage sludge is > 20°C, SOUR = 0.46 (mg/g)/hr
If sewage sludge is < 20°C, SOUR = 0.45 (mg/g)/hr
SOUR passes if result is:5 1.5 (mg/g)hr
Version 11/1/11

City of Lumberton
Environmental Laboratory
Specific Oxygen Uptake Rate (SOUR) Worksheet
Date & Analyst: Tues 4/18/23 @0634 kca Dig #2 Day 2
Total Solids
Sample volume used for total solids test: 5 mL
Weight of dish: 89.0606 g
Weight of dish + dried solids: 89.1341 g
Weight of dried solids: 0.0735 g
Total Solids: 14.7 g/L
SOUR
Time
(Minutes)
Temperature
Dissolved
Oxygen (mg/L)
oC
0
18.00
6.61
1
18.00
1.49
2
18.00
0.77
3
18.00
0.53
4
18.00
0.44
5
18.00
0.38
6
19.00
0.35
7
19.00
0.33
8
19.00
0.31
9
19.00
0.29
10
19.00
0.28
11
19.00
0.27
12
19.00
0.26
13
19.00
0.25
14
19.00
0.25
15
19.00
0.24
Oxygen Consumption Rate
SOUR
SOUR Temperature Correction
0.18 mg/L/minute
0.73 (mg/g)/hr
Average Sewage Sludge
Temperature During Test
°C
18.625
If sewage sludge is > 20°C, SOUR = 0.78 (mg/g)/hr
If sewage sludge is < 20°C, SOUR = 0.80 (mg/g)/hr
SOUR passes if result is <_ 1.5 (mg/g)hr
Version 11/1/11

City of Lumberton
Environmental Laboratory
Specific Oxygen Uptake Rate (SOUR) Worksheet
Date & Analyst: Wed 4/19/23 @0630 kci Dig #2 Day 3
Total Solids
Sample volume used for total solids test: 5 mL
Weight of dish: 121.9534 g
Weight of dish + dried solids: 122.0543 g
Weight of dried solids: 0.1009 g
Total Solids: 20.18 g/L
SOUR
Time
(Minutes)
Temperature
Dissolved
Oxygen (mg/L)
oC
0
19.00
6.19
1
19.00
1.28
2
19.00
0.72
3
19.00
0.50
4
19.00
0.43
5
19.00
0.38
6
19.00
0.35
7
19.00
0.33
8
19.00
0.31
9
19.00
0.29
10
19.00
0.28
11
19.00
0.27
12
19.00
0.26
13
19.00
0.26
14
19.00
0.25
15
19.00
0.24
Oxygen Consumption Rate
SOUR
SOUR Temperature Correction
Average Sewage Sludge
Temperature During Test
°C
19
0.16 mg/L/minute
0.49 (mg/g)/hr
If sewage sludge is > 20°C, SOUR = 0.51 (mg/g)/hr
If sewage sludge is < 20°C, SOUR = 0.52 (mg/g)/hr
SOUR passes if result is:5 1.5 (mg/g)hr
Version 11/1/11

City of Lumberton
Environmental Laboratory
Specific Oxygen Uptake Rate (SOUR) Worksheet
Date & Analyst: Thur 4120/23 @0651 kcl Dig #2 Day 4
Total Solids
Sample volume used for total solids test: 5 mL
Weight of dish: 89.0333 g
Weight of dish + dried solids: 89.1327 g
Weight of dried solids: 0.0994 g
Total Solids: 19.88 g/L
SOUR
Time
(Minutes)
Temperature
Dissolved
Oxygen (mg/L)
oC
0
20.00
7.61
1
20.00
7.37
2
21.00
6.89
3
18.00
1.31
4
18.00
0.78
5
18.00
0.56
6
18.00
0.47
7
18.00
0.42
8
18.00
0.42
9
19.00
0.35
10
19.00
0.33
11
19.00
0.34
12
19.00
0.34
13
19.00
0.34
14
19.00
0.34
15
19.00
0.28
Oxygen Consumption Rate 0.42 mg/L/minute
SOUR 1.27 (mg/g)/hr
SOUR Temperature Correction
Average Sewage Sludge
Temperature During Test
°C
18.875
If sewage sludge is > 20°C, SOUR = 1.34 (mg/g)/hr
If sewage sludge is < 20°C, SOUR = 1.37 (mg/g)/hr
SOUR passes if result is:5 1.5 (mg/g)hr
Version 11/1/11

City of Lumberton
Environmental Laboratory
Specific Oxygen Uptake Rate (SOUR) Worksheet
Date & Analyst: Fri 4/21123 @0648 kcl Dig #2 Day 5
Total Solids
Sample volume used for total solids test: 5 mL
Weight of dish: 111.4761 g
Weight of dish + dried solids: 111.5050 g
Weight of dried solids: 0.0289 g
Total Solids: 5.78 g/L
SOUR
Time
(Minutes)
Temperature
Dissolved
Oxygen (mg/L)
oC
0
20.00
6.91
1
19.00
1.53
2
19.00
0.75
3
20.00
0.56
4
20.00
0.44
5
20.00
0.39
6
20.00
0.35
7
20.00
0.33
8
20.00
0.31
9
19.00
0.30
10
19.00
0.29
11
19.00
0.28
12
19.00
0.27
13
19.00
0.26
14
20.00
0.25
15
20.00
0.25
Oxygen Consumption Rate 0.19 mg/L/minute
SOUR 1.93 (mg/g)/hr
SOUR Temperature Correction
Average Sewage Sludge
Temperature During Test
oC
19.5625
If sewage sludge is > 20°C, SOUR = 1.97 (mg/g)/hr
If sewage sludge is < 20°C, SOUR = 1.99 (mg/g)/hr
SOUR passes if result is:5 1.5 (mg/g)hr
Version 11/1/11

City of Lumberton
Environmental Laboratory
Specific Oxygen Uptake Rate (SOUR) Worksheet
Date & Analyst: Mon 4/24/23 @0654 kcl Dig #2 Day 5 repeat
Total Solids
Sample volume used for total solids test: 5 mL
Weight of dish: 125.4561 g
Weight of dish + dried solids: 125.5505 g
Weight of dried solids: 0.0944 g
Total Solids: 18.88 g/L
SOUR
Time
(Minutes)
Temperature
Dissolved
Oxygen (mg/L)
oC
0
19.00
6.12
1
19.00
1.82
2
19.00
0.86
3
19.00
0.58
4
19.00
0.46
5
19.00
0.40
6
19.00
0.37
7
19.00
0.34
8
19.00
0.33
9
19.00
0.31
10
19.00
0.30
11
19.00
0.29
12
19.00
0.28
13
19.00
0.27
14
19.00
0.26
15
19.00
0.25
Oxygen Consumption Rate
SOUR
SOUR Temperature Correction
0.18 mg/L/minute
0.56 (mg/g)/hr
Average Sewage Sludge
Temperature During Test
°C
19
If sewage sludge is > 20°C, SOUR = 0.59 (mg/g)/hr
If sewage sludge is < 20°C, SOUR = 0.60 (mg/g)/hr
SOUR passes if result is:5 1.5 (mg/g)hr
Version 11/1/11

City of Lumberton
Environmental Laboratory
Specific Oxygen Uptake Rate (SOUR) Worksheet
Date & Analyst: Tues 4/25/23 @0655 kcl Dig #2 Day 6
Total Solids
Sample volume used for total solids test: 5 mL
Weight of dish: 89.0338 g
Weight of dish + dried solids: 89.1290 g
Weight of dried solids: 0.0952 g
Total Solids: 19.04 g/L
SOUR
Time
(Minutes)
Temperature
Dissolved
Oxygen (mg/L)
oC
0
17.00
6.64
1
17.00
4.28
2
17.00
2.80
3
17.00
1.50
4
17.00
0.68
5
17.00
0.50
6
17.00
0.42
7
17.00
0.38
8
17.00
0.35
9
17.00
0.33
10
17.00
0.31
11
17.00
0.30
12
17.00
0.28
13
17.00
0.27
14
17.00
0.27
15
17.00
0.26
Oxygen Consumption Rate
SOUR
SOUR Temperature Correction
0.28 mg/L/minute
0.88 (mg/g)/hr
Average Sewage Sludge
Temperature During Test
oC
17
If sewage sludge is > 20°C, SOUR = 1.02 (mg/g)/hr
If sewage sludge is < 20°C, SOUR = 1.08 (mg/g)/hr
SOUR passes if result is:5 1.5 (mg/g)hr
Version 11/1/11

Date & Analyst:
Total Solids
City of Lumberton
Environmental Laboratory
Specific Oxygen Uptake Rate (SOUR) Worksheet
Wed 4/26123 @0649 kcl Dig #2 Day 7
Sample volume used for total solids test: 5 mL
Weight of dish: 130.0799 g
Weight of dish + dried solids: 130.1754 g
Weight of dried solids: 0.0955 g
Total Solids: 19.1 g/L
SOUR
Time
(Minutes)
Temperature
Dissolved
Oxygen (mg/L)
oC
0
17.00
6.69
1
18.00
3.97
2
17.00
2.51
3
17.00
1.14
4
18.00
0.59
5
18.00
0.46
6
18.00
0.40
7
17.00
0.36
8
18.00
0.34
9
18.00
0.32
10
18.00
0.31
11
18.00
0.30
12
18.00
0.28
13
18.00
0.27
14
18.00
0.26
15
18.00
0.26
Oxygen Consumption Rate
SOUR
SOUR Temperature Correction
0.26 mg/L/minute
0.83 (mg/g)/hr
Average Sewage Sludge
Temperature During Test
°C
17.75
If sewage sludge is > 20°C, SOUR = 0.93 (mg/g)/hr
If sewage sludge is < 20°C, SOUR = 0.97 (mg/g)/hr
SOUR passes if result is <_ 1.5 (mg/g)hr
Version 11/1/11

City of Lumberton
Environmental Laboratory
Specific Oxygen Uptake Rate (SOUR) Worksheet
Date & Analyst: Mon W14-23 Q 0640 kcl Dig #2 Day I
Total Solids
Sample volume used for total solids test: 5 mL
Weight of dish: 43.9527 g
Weight of dish + dried solids: 44.0642 g
Weight of dried solids: 0.1115 g
Total Solids: 22.3 g/L
SOUR
Time
(Minutes)
Temperature
Dissolved
Oxygen (mg/L)
oC
0
24.00
7.79
1
23.00
5.74
2
25.00
1.94
3
25.00
0.66
4
25.00
0.42
5
25.00
0.38
6
24.00
0.34
7
24.00
0.34
8
24.00
0.33
9
24.00
0.32
10
24.00
0.31
11
24.00
0.30
12
24.00
0.29
13
24.00
0.29
14
24.00
0.28
15
24.00
0.28
Oxygen Consumption Rate
SOUR
SOUR Temperature Correction
0.30 mg/L/minute
0.82 (mg/g)/hr
Average Sewage Sludge
Temperature During Test
°C
24.1875
If sewage sludge is > 20°C, SOUR = 0.67 (mg/g)/hr
If sewage sludge is < 20°C, SOUR = 0.62 (mg/g)/hr
SOUR passes if result is:5 1.5 (mg/g)hr
Version 11/1/11

City of Lumberton
Environmental Laboratory
Specific Oxygen Uptake Rate (SOUR) Worksheet
Date & Analyst: Tues 7/18123 @ 0644 kcl Dig #2 Day 2
Total Solids
Sample volume used for total solids test: 5 mL
Weight of dish: 47.0191 g
Weight of dish + dried solids: 47.1327 g
Weight of dried solids: 0.1136 g
Total Solids: 22.72 g/L
SOUR
Time
(Minutes)
Temperature
Dissolved
Oxygen (mg/L)
oC
0
24.00
7.24
1
24.00
5.21
2
24.00
1.24
3
24.00
0.70
4
24.00
0.52
5
24.00
0.46
6
24.00
0.40
7
24.00
0.38
8
24.00
0.35
9
24.00
0.33
10
24.00
0.32
11
24.00
0.31
12
24.00
0.31
13
24.00
0.31
14
24.00
0.30
15
24.00
0.29
Oxygen Consumption Rate
SOUR
SOUR Temperature Correction
0.27 mg/L/minute
0.72 (mg/g)/hr
Average Sewage Sludge
Temperature During Test
°C
24
If sewage sludge is > 20°C, SOUR (mg/g)/hr
If sewage sludge is < 20°C, SOUR = tl55 (mg/g)/hr
SOUR passes if result is:5 1.5 (mg/g)hr
Version 11/1/11

City of Lumberton
Environmental Laboratory
Specific Oxygen Uptake Rate (SOUR) Worksheet
Date & Analyst: Wed 7/19123 @ 0646 kcl Dig #2 Day 3
Total Solids
Sample volume used for total solids test: 5 mL
Weight of dish: 43.9530 g
Weight of dish + dried solids: 44.0749 g
Weight of dried solids: 0.1219 g
Total Solids: 24.38 g/L
SOUR
Time
(Minutes)
Temperature
Dissolved
Oxygen (mg/L)
oC
0
24.00
7.54
1
24.00
1.10
2
24.00
0.61
3
24.00
0.50
4
25.00
0.43
5
25.00
0.40
6
25.00
0.37
7
25.00
0.36
8
25.00
0.35
9
25.00
0.34
10
25.00
0.32
11
25.00
0.31
12
25.00
0.31
13
25.00
0.30
14
25.00
0.29
15
25.00
0.29
Oxygen Consumption Rate 0.18 mg/L/minute
SOUR 0.46 (mg/g)/hr
SOUR Temperature Correction
Average Sewage Sludge
Temperature During Test
°C
24.75
If sewage sludge is > 20°C, SOUR = 0.36 (mg/g)/hr
If sewage sludge is < 20°C, SOUR = 0.33 (mg/g)/hr
SOUR passes if result is:5 1.5 (mg/g)hr
Version 11/1/11

City of Lumberton
Environmental Laboratory
Specific Oxygen Uptake Rate (SOUR) Worksheet
Date & Analyst: Thur 7/20123 Q 0646 kci Dig #2 Day 4
Total Solids
Sample volume used for total solids test: 5 mL
Weight of dish: 47.0193 g
Weight of dish + dried solids: 47.1324 g
Weight of dried solids: 0.1131 g
Total Solids: 22.62 g/L
SOUR
Time
(Minutes)
Temperature
Dissolved
Oxygen (mg/L)
oC
0
24.00
7.28
1
24.00
1.03
2
24.00
0.63
3
24.00
0.50
4
24.00
0.44
5
24.00
0.40
6
24.00
0.38
7
24.00
0.36
8
24.00
0.35
9
24.00
0.34
10
24.00
0.32
11
24.00
0.32
12
24.00
0.31
13
24.00
0.30
14
24.00
0.29
15
24.00
0.29
Oxygen Consumption Rate
SOUR
SOUR Temperature Correction
0.18 mg/L/minute
0.47 (mg/g)/hr
Average Sewage Sludge
Temperature During Test
°C
24
If sewage sludge is > 20°C, SOUR = 0.39 (mg/g)/hr
If sewage sludge is < 20°C, SOUR = 0.36 (mg/g)/hr
SOUR passes if result is:5 1.5 (mg/g)hr
Version 11/1/11

Date & Analyst:
Total Solids
City of Lumberton
Environmental Laboratory
Specific Oxygen Uptake Rate (SOUR) Worksheet
Fri 7121123 @ 0641 kcl Dig #2 Day 5
Sample volume used for total solids test: 5 mL
Weight of dish: 43.9528 g
Weight of dish + dried solids: 44.0653 g
Weight of dried solids: 0.1125 g
Total Solids: 22.5 g/L
SOUR
Time
(Minutes)
Temperature
Dissolved
Oxygen (mg/L)
oC
0
23.00
7.25
1
24.00
1.12
2
24.00
0.68
3
24.00
0.52
4
24.00
0.45
5
23.00
0.41
6
23.00
0.38
7
23.00
0.36
8
23.00
0.35
9
23.00
0.33
10
23.00
0.33
11
23.00
0.31
12
23.00
0.31
13
23.00
0.30
14
23.00
0.30
15
23.00
0.29
Oxygen Consumption Rate
SOUR
SOUR Temperature Correction
0.18 mg/L/minute
0.48 (mg/g)/hr
Average Sewage Sludge
Temperature During Test
°C
23.25
If sewage sludge is > 20°C, SOUR = 0.41 (mg/g)/hr
If sewage sludge is < 20°C, SOUR = 0.39 (mg/g)/hr
SOUR passes if result is <_ 1.5 (mg/g)hr
Version 11/1/11

City of Lumberton
Environmental Laboratory
Specific Oxygen Uptake Rate (SOUR) Worksheet
Date & Analyst: Mon 7/24/23 @ 0645 kcl Dig#2 Day 6
Total Solids
Sample volume used for total solids test: 5 mL
Weight of dish: 46.0919 g
Weight of dish + dried solids: 46.2051 g
Weight of dried solids: 0.1132 g
Total Solids: 22.64 g/L
SOUR
Time
(Minutes)
Temperature
Dissolved
Oxygen (mg/L)
oC
0
23.00
7.42
1
23.00
1.84
2
23.00
0.67
3
23.00
0.46
4
23.00
0.42
5
23.00
0.39
6
23.00
0.37
7
23.00
0.35
8
23.00
0.34
9
23.00
0.33
10
23.00
0.32
11
23.00
0.31
12
23.00
0.31
13
23.00
0.30
14
23.00
0.29
15
23.00
0.29
Oxygen Consumption Rate 0.20 mg/L/minute
SOUR 0.52 (mg/g)/hr
SOUR Temperature Correction
Average Sewage Sludge
Temperature During Test
°C
23
If sewage sludge is > 20°C, SOUR = 0.45 (mg/g)/hr
If sewage sludge is < 20°C, SOUR = 0.43 (mg/g)/hr
SOUR passes if result is <_ 1.5 (mg/g)hr
Version 11/1/11

Date & Analyst:
`FTRI& :11517
City of Lumberton
Environmental Laboratory
Specific Oxygen Uptake Rate (SOUR) Worksheet
Tues 7/25/23 @ 0648 kci Dig #2 Day 7
Sample volume used for total solids test: 5 mL
Weight of dish: 47.0194 g
Weight of dish + dried solids: 47.1430 g
Weight of dried solids: 0.1236 g
Total Solids: 24.72 g/L
SOUR
Time
(Minutes)
Temperature
Dissolved
Oxygen (mg/L)
oC
0
23.00
7.72
1
23.00
1.42
2
23.00
0.69
3
23.00
0.54
4
23.00
0.46
5
23.00
0.42
6
23.00
0.41
7
23.00
0.39
8
23.00
0.37
9
23.00
0.35
10
23.00
0.34
11
23.00
0.34
12
23.00
0.31
13
23.00
0.30
14
23.00
0.30
15
23.00
0.30
Oxygen Consumption Rate 0.20 mg/L/minute
SOUR 0.48 (mg/g)/hr
SOUR Temperature Correction
Average Sewage Sludge
Temperature During Test
°C
23
If sewage sludge is > 20°C, SOUR = 0.41 (mg/g)/hr
If sewage sludge is < 20°C, SOUR = 0.39 (mg/g)/hr
SOUR passes if result is:5 1.5 (mg/g)hr
Version 11/1/11

Date & Analyst:
Total Solids
City of Lumberton
Environmental Laboratory
Specific Oxygen Uptake Rate (SOUR) Worksheet
Mon 10/2/2023 @ 0621 kcl big #2 Day 1
Sample volume used for total solids test: 5 mL
Weight of dish: 47.0191 g
Weight of dish + dried solids: 47.1140 g
Weight of dried solids: 0.0949 g
Total Solids: 18.98 g/L
SOUR
Time
(Minutes)
Temperature
Dissolved
Oxygen (mg/L)
oC
0
21.00
8.70
1
21.00
8.43
2
21.00
8.23
3
21.00
8.03
4
21.00
7.89
5
21.00
7.71
6
21.00
7.52
7
21.00
7.29
8
21.00
7.07
9
21.00
6.97
10
21.00
6.79
11
21.00
6.59
12
21.00
6.44
13
21.00
6.21
14
21.00
6.04
15
21.00
5.85
Oxygen Consumption Rate
SOUR
SOUR Temperature Correction
0.19 mg/L/minute
0.59 (mg/g)/hr
Average Sewage Sludge
Temperature During Test
°C
21
If sewage sludge is > 20°C, SOUR = 0.56 (mg/g)/hr
If sewage sludge is < 20°C, SOUR = 0.55 (mg/g)/hr
SOUR passes if result is:5 1.5 (mg/g)hr
Version 11/1/11

City of Lumberton
Environmental Laboratory
Specific Oxygen Uptake Rate (SOUR) Worksheet
Date & Analyst: Tues 10/3/2023 @ 0637 kcl Dig #2 Day 2
Total Solids
Sample volume used for total solids test: 5 mL
Weight of dish: 47.6152 g
Weight of dish + dried solids: 47.7126 g
Weight of dried solids: 0.0974 g
Total Solids: 19.48 g/L
SOUR
Time
(Minutes)
Temperature
Dissolved
Oxygen (mg/L)
oC
0
20.00
8.74
1
20.00
8.47
2
20.00
8.33
3
20.00
8.16
4
20.00
8.01
5
20.00
7.82
6
20.00
7.66
7
20.00
7.52
8
20.00
7.35
9
20.00
7.13
10
20.00
6.97
11
20.00
6.86
12
20.00
6.63
13
20.00
6.43
14
20.00
6.33
15
20.00
6.13
Oxygen Consumption Rate
SOUR
SOUR Temperature Correction
0.17 mg/L/minute
0.52 (mg/g)/hr
Average Sewage Sludge
Temperature During Test
°C
20
If sewage sludge is > 20°C, SOUR = 0.52 (mg/g)/hr
If sewage sludge is < 20°C, SOUR = 0.52 (mg/g)/hr
SOUR passes if result is:5 1.5 (mg/g)hr
Version 11/1/11

City of Lumberton
Environmental Laboratory
Specific Oxygen Uptake Rate (SOUR) Worksheet
Date & Analyst: Wed 10/4f2023 @ 0639 kcl Dig #2 Day 3 i
Total Solids
Sample volume used for total solids test: 5 mL
Weight of dish: 47.0192 g
Weight of dish + dried solids: 47.1158 g
Weight of dried solids: 0.0966 g
Total Solids: 19.32 g/L
SOUR
Time
(Minutes)
Temperature
Dissolved
Oxygen (mg/L)
oC
0
20.00
8.99
1
20.00
7.96
2
20.00
7.76
3
20.00
7.57
4
20.00
7.36
5
20.00
7.22
6
20.00
7.06
7
20.00
6.95
8
20.00
6.77
9
20.00
6.60
10
20.00
6.45
11
20.00
6.29
12
20.00
6.13
13
20.00
5.95
14
20.00
5.80
15
20.00
5.64
Oxygen Consumption Rate
SOUR
SOUR Temperature Correction
0.18 mg/L/minute
0.57 (mg/g)/hr
Average Sewage Sludge
Temperature During Test
oC
20
If sewage sludge is > 20°C, SOUR = 0.57 (mg/g)/hr
If sewage sludge is < 20°C, SOUR = 057 (mg/g)/hr
SOUR passes if result is:5 1.5 (mg/g)hr
Version 11/1/11

City of Lumberton
Environmental Laboratory
Specific Oxygen Uptake Rate (SOUR) Worksheet
Date & Analyst: Thur 1015/2023 @ 0629 kcl D19 #2 Day 4
Total Solids
Sample volume used for total solids test: 5 mL
Weight of dish: 47.7738 g
Weight of dish + dried solids: 47.8726 g
Weight of dried solids: 0.0988 g
Total Solids: 19.76 g/L
SOUR
Time
(Minutes)
Temperature
Dissolved
Oxygen (mg/L)
oC
0
20.00
8.85
1
20.00
8.04
2
20.00
7.82
3
20.00
7.67
4
20.00
7.52
5
20.00
7.34
6
20.00
7.21
7
20.00
7.04
8
20.00
6.91
9
20.00
6.72
10
20.00
6.53
11
19.00
6.41
12
19.00
6.24
13
20.00
6.06
14
20.00
5.87
15
20.00
5.76
Oxygen Consumption Rate 0.18 mg/L/minute
SOUR 0.54 (mg/g)/hr
SOUR Temperature Correction
Average Sewage Sludge
Temperature During Test
°C
19.875
If sewage sludge is > 20°C, SOUR = 0.54 (mg/g)/hr
If sewage sludge is < 20°C, SOUR = 0.54 (mg/g)/hr
SOUR passes if result is:5 1.5 (mg/g)hr
Version 11/1/11

City of Lumberton
Environmental Laboratory
Specific Oxygen Uptake Rate (SOUR) Worksheet
Date & Analyst: Fri 10/6/2023 @ 0636 kcl Dig #2 Day 5
Total Solids
Sample volume used for total solids test: 5 mL
Weight of dish: 46.0909 g
Weight of dish + dried solids: 46.1989 g
Weight of dried solids: 0.1080 g
Total Solids: 21.6 g/L
SOUR
Time
(Minutes)
Temperature
Dissolved
Oxygen (mg/L)
oC
0
20.00
8.72
1
20.00
8.06
2
20.00
7.78
3
20.00
7.68
4
20.00
7.49
5
20.00
7.34
6
20.00
7.16
7
20.00
6.94
8
20.00
6.76
9
20.00
6.63
10
20.00
6.44
11
20.00
6.25
12
20.00
6.10
13
20.00
5.91
14
20.00
5.78
15
20.00
5.60
Oxygen Consumption Rate
SOUR
SOUR Temperature Correction
0.19 mg/L/minute
0.52 (mg/g)/hr
Average Sewage Sludge
Temperature During Test
°C
20
If sewage sludge is > 20°C, SOUR = 0.52 (mg/g)/hr
If sewage sludge is < 20°C, SOUR = 0.52 (mg/g)/hr
SOUR passes if result is:5 1.5 (mg/g)hr
Version 11/1/11

City of Lumberton
Environmental Laboratory
Specific Oxygen Uptake Rate (SOUR) Worksheet
Date & Analyst: Mon 10f9/2023 @ 0644 tis Dig #2 Day 6
Total Solids
Sample volume used for total solids test: 5 mL
Weight of dish: 89.0355 g
Weight of dish + dried solids: 89.1378 g
Weight of dried solids: 0.1023 g
Total Solids: 20.46 g/L
Time
(Minutes)
Temperature
Dissolved
Oxygen (mg/L)
oC
0
19.00
8.81
1
19.00
8.33
2
19.00
7.95
3
19.00
7.84
4
19.00
7.80
5
19.00
7.59
6
19.00
7.48
7
19.00
7.36
8
19.00
7.16
9
19.00
6.99
10
19.00
6.81
11
19.00
6.67
12
19.00
6.54
13
19.00
6.43
14
19.00
6.24
15
19.00
6.09
Oxygen Consumption Rate 0.16 mg/L/minute
SOUR 0.47 (mg/g)/hr
SOUR Temperature Correction
Average Sewage Sludge
Temperature During Test
°C
19
If sewage sludge is > 20°C, SOUR = 0.50. (mg/g)/hr
If sewage sludge is < 20oC, SOUR = 0.51 (mg/g)/hr
SOUR passes if result is:5 1.5 (mg/g)hr
Version 11/1/11

City of Lumberton
Environmental Laboratory
Specific Oxygen Uptake Rate (SOUR) Worksheet
Date & Analyst: Tues 10/10/2023 @ 0629 tts Dig #2 Day 7
Total Solids
Sample volume used for total solids test: 5 mL
Weight of dish: 120.9173 g
Weight of dish + dried solids: 121.0175 g
Weight of dried solids: 0.1002 g
Total Solids: 20.04 g/L
SOUR
Time
(Minutes)
Temperature
Dissolved
Oxygen (mg/L)
oC
0
21.00
7.56
1
21.00
7.46
2
21.00
7.35
3
21.00
7.31
4
21.00
7.21
5
21.00
7.18
6
21.00
6.99
7
21.00
6.92
8
21.00
6.85
9
21.00
6.75
10
21.00
6.60
11
21.00
6.42
12
21.00
6.35
13
21.00
6.16
14
21.00
6.10
15
20.00
6.09
Oxygen Consumption Rate
SOUR
SOUR Temperature Correction
0.10 mg/L/minute
0.31 (mg/g)/hr
Average Sewage Sludge
Temperature During Test
°C
20.9375
If sewage sludge is > 20°C, SOUR (mg/g)/hr
If sewage sludge is < 20°C, SOUR = 0f (mg/g)/hr
SOUR passes if result is:5 1.5 (mg/g)hr
Version 11/1/11