WQ0041666_2023 Residual Annual Report_20240301 (2)

Initial Review
Reviewer
nathaniel.thorn burg
Is this submittal an application? (Excluding additional information.) *
Yes No
If not an application what is the submittal type?* Annual Report
Residual Annual Report
Additional Information
Other
Annual Report Year* 2023
Permit Number (IR) * WQ0041666
Applicant/Permittee EMA Resources, Inc.
Email Notifications
Does this need review by the hydrogeologist? * Yes U No
Regional Office Winston-Salem
CO Reviewer
Admin Reviewer Wanda Gerald

Submittal Form
Project Contact Information
Please provide information on the person to be contacted by NDB Staff regarding electronic submittal, confirmation of receipt, and other correspondence.
Name* Brent Collins
Email Address*
[e-mail]
Project Information
.........................
Application/Document Type*
New (Fee Required)
Modification - Major (Fee Required)
Renewal with Major Modification (Fee
Required)
Annual Report
Additional Information
Other
Phone Number*
3363993646
Modification - Minor
Renewal
GW-59, NDMR, NDMLR, NDAR-1,
N DAR-2
Residual Annual Report
Change of Ownership
We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form.
https://edoes.deq.nc.gov/Forms/NonDischarge_Monitoring_Report
Permit Type:*
Wastewater Irrigation
High -Rate Infiltration
Other Wastewater
Reclaimed Water
Closed -Loop Recycle
Residuals
Single -Family Residence Wastewater
Other
Irrigation
Permit Number:*
WQ0041666
Has Current Existing permit number
Applicant/Permittee Address*
755 Yadkinville Rd, Mocksville, NC 27028
Facility Name*
EMA Resources Class A Residuals Program
Please provide comments/notes on your current submittal below.
At this time, paper copies are no longer required. If you have any questions about what is required, please contact Nathaniel Thornburg
at [e-mail].
Please attach all information required or requested for this submittal to be reviewed here.
(Application Form, Engineering Plans, Specifications, Calculations, Etc.)
2023 EMA Resources Inc. Annual Report - WQ0041666.pdf 7.64MB
Upload only 1 PDF document (less than 250 MB). Multiple documents must be combined into one PDF file unless file is larger
than upload limit.
* By checking this box, I acknowledge that I understand the application will not be accepted for pre -review until the fee (if required) has
been received by the Non -Discharge Branch. Application fees must be submitted by check or money order and made payable to the
North Carolina Department of Environmental Quality (NCDEQ). I also confirm that the uploaded document is a single PDF with all parts
of the application in correct order (as specified by the application).
Mail payment to:
NCDEQ — Division of Water Resources
Attn: Non -Discharge Branch
1617 Mail Service Center
Raleigh, NC 27699-1617
Signature
Submission Date 3/1/2024

EMA Resources Inc. - DCAR
2023 Annual Report
Residuals Land Application
Permit No. WQ0041666
Prepared By:
EMA Resources, Inc.
Phone [phone] — Fax [phone]
755 Yadkinville Rd — Mocksville, NC 27028

It
MI. � A,
sources, Inc.
February 29, 2024
DENR/Water Quality Section
Non -Discharge Compliance Unit
1617 Mail Service Center
Raleigh, NC 27699-1617
Re: 2023 Annual Report — EMA Resources Inc.
Treatment and Land Application of Residuals
Permit No. WQ0041666
Dear Sir or Madam:
Enclosed is the 2023 Annual Report for the above referenced land application permit.
During 2023 EMA Resources, Inc. land applied 2902.58 total dry tons of wastewater
residuals to 350.42 acres of private farmland. EMA Resources land applied more than
was expected from the Brown WTP and subsequently went over the dry ton amount that
was permitted. We will be submitting a modification to increase the dry tonnage within
the next week.
Please contact Brent Collins - Director of Technical Services if you have any further
questions regarding this report.
Sincerely,
Z_�Z4;2�_
Brent Collins
Director of Technical Services
brent.collinsgemaresourcesinc.com
Phone [phone] — Fax [phone]
755 Yadkinville Rd — Mocksville, NC 27028

G/ SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM CLASS A ANNUAL DISTRIBUTION AND NIARKIETIN
WQ PERMIT 4: WQ004 1 666 FACILITV NAME: E%TA Resources inc.
PHONE: [phone] COUNTY: Da- ie CWERATOR: EMA I?Wsaurres
FACILITY TYPE (please chect; oney ED Surface Disposal (tomplete Pan A (Source(s) and "Residual in Volume only) and Part C)
Eif Dist0budon and Marketing (complete Parts A, B, and Q
Was the f-acilk; in operation during the past calendar car? Ves 01 No 1fNo skip pans A, B, C and cerfify form below
Part A,-: Pan W:
Volunle (dn- tons) I—Ree-hpient ln%mutwn
Sources(s) (include NPDFS 4 if
Month At-nendment i
appmeaIM %WingAgent ReAdiralin Boduct -' Out N arn c (s) Volume (dr� tons) inwndcd use(s)
January
February
March
April
May
June
july
August
SephnAer
October
lNoveraher
Deceinher
Total from FORM D&IS11F (suld 0 2 9 02 0 88 2902.58 =-€?<-.✓S
-eta-.. Annual (dry tons): 0 290158 290218 2W21-9
Anwncirnent(O uw& 1 Bullcing Agenifo und:
if more sDac-- is required, attach additional infisri-nation sheets tFOR\l DNISDF ,supp)): Total Number of Forn- ')%ISF)F (Supp)j 0
Pan C:
FacHhy was compliant during Me pm-- calendar year with all_ conditions of the land appHeation perndt [I its
(including but not limited to items 1�3 below) issued by the Division of Water Quality: R No Iff No, Explain in Narritive
1 All monitoring was clone in accordance whh Be parnii and reported lbr ffie year as required and three (3) copies of cerfific-d lahoraioes It are attached,
1 All operation and maintenance requArnents - eree compiled Wth or, in the case of a devAtion, prior authorization mys receAd from the Division ofWater Quality.
3. No cmemTrolion of Ground U'ater Quality Standards occurred at a monitoring well.
I cerrifvt under -nnaltv of law, that the above infortuation is. to the best of mv knowtedee anti belief true, accurate and complete. .1 am miare that there are sianificant
penalties for submitting false- information, including the possibility of fines a nimprisonment My kno-wing- violations
Q4
Eli 4i LUU 1 K to tj - 02/2CV2,
03/01/2z
Signature of Permittee
Date Signature of Preparer��-
(if differcn, from Perminee)
"I'mParer is &thred MAO CFRPan 50-1 -9(r) and 15A NCAC 2T 1102(26)
DENR FORM DMSDF (12 200M

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Piedmont Water 1/9/23
mg/kg mg/L Equiv Weight Milli Equiv
Sodium 381 74.295 23 3.230217
Calcium 3100 604.5 20 30.225
Magnesium 438 85.41 12 7.1175
Percent Solids 19.5
SAR
0.75
SAR Na+
a (Ca2+ + M92+)
3.23022
'',::: 0.5( 30.225 2 + 7.11750 2 )

Piedmont Water 4/5/23
mg/kg mg/L Equiv Weight Milli Equiv
Sodium 313 64.791 23 2.817
Calcium 1700 351.9 20 17.595
Magnesium 455 94.185 12 7.84875
Percent Solids 20.7
SAR
0.79
SAR Na+
a (Ca2+ + M92+)
2.81700
'',::: 0.5( 17.595 2 + 7.84875 2 )

Piedmont Water 7/10/23
mg/kg
mg/L
Equiv Weight Milli Equiv
Sodium
372
75.144
23 3.26713
Calcium
3330
672.66
20 33.633
Magnesium
698
140.996
12 11.74967
Percent Solids
20.2
SAR
0.69
SAR
Na+
a (Ca2+ + M92+)
3.26713
'',::: 0.5( 33.633 2 + 11.74967 2 )

Piedmont Water 10/3/23
mg/kg
mg/L
Equiv Weight Milli Equiv
Sodium
1030
210.12
23 9.135652
Calcium
4950
1009.8
20 50.49
Magnesium
760
155.04
12 12.92
Percent Solids
20.4
SAR
1.62
SAR
Na+
a (Ca2+ + M92+)
9.13565
'',::: 0.5( 50.49 2 + 12.92000 2 )

mil ,
1 /18/2023
EMA Resources Inc
Mr. Brent Collins
755 Yadkinville Road
Mocksville, NC, 27028
Ref: Analytical Testing
Lab Report Number: 23-010-0010
Client Project Description: Asheboro, NC
Dear Mr. Brent Collins:
Waypoint Analytical, LLC. received sample(s) on 1/10/2023 for the analyses presented in the following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Where the laboratory was not responsible for the sampling
stage (refer to the chain of custody) results apply to the sample as received.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2021) and NELAC unless otherwise indicated. Any parameter
for which the laboratory is not officially NELAP accredited is indicated by a '—'symbol. These are not included in
the scope because NELAP accreditation is either not available or has not been applied for. Additional
certifications may be held/are available for parameters, where NELAP accreditation is not required or applicable.
A full list of certifications is available upon request.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Connie Cook
Project Manager
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 1 of 9

Way to
PM�
WRTIA"Wi
tMain 901.213.2400 0 Fax u f,
www.waypointanalyticaLcom
Certification Summary
Laboratory ID: WP MTN: Waypoint Analytical, LLC., Memphis, TN
State
Program
Lab ID
Expiration Date
Alabama
State Program
40750
02/28/2023
Arkansas
State Program
88-0650
02/07/2023
California
State Program
2904
06/30/2023
Florida
State Program
- NELAP
E871157
06/30/2023
Georgia
State Program
C044
02/18/2023
Georgia
State Program
04015
06/30/2023
Illinois
State Program
- NELAP
200078
10/10/2023
Kentucky
State Program
80215
06/30/2023
Kentucky
State Program
KY90047
12/31/2023
Louisiana
State Program
- NELAP
LA037
12/31/2023
Louisiana
State Program
- NELAP
04015
06/30/2023
Mississippi
State Program
MS
02/11/2023
North Carolina
State Program
47701
07/31/2023
North Carolina
State Program
415
12/31/2023
Pennsylvania
State Program
- NELAP
68-03195
05/31/2023
South Carolina
State Program
84002
06/30/2023
Tennessee
State Program
02027
02/11/2023
Texas
State Program
- NELAP
T104704180
09/30/2023
Virginia
State Program
00106
06/30/2023
Virginia
State Program
- NELAP
460181
09/14/2023
Page 1 of 1 00001/23-010-0010
Page 2 of 9

Way lht,(2)
PM�TICAL'
Sample Summary Table
Report Number: 23-010-0010
Client Project Description: Asheboro, NC
Lab No Client Sample ID Matrix Date Collected Date Received
91173 Piedmont Water Solids 01/09/2023 10:45 01/10/2023
Page 3 of 9

to
Way� PA
► x
Client: EMA Resources Inc
Project: Asheboro, NC
Lab Report Number: 23-010-0010
Date: 1 /18/2023
Main 901.213.2400 .41
wwwmaypointanalyticaLcorn
CASE NARRATIVE
Metals Analysis Method 601 OD
Sample 91048 (Grab)
Analyte: Aluminum
QC Batch No: L658387/L657717
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 91048 (Grab)
Analyte: Calcium
QC Batch No: 1-658650/1-657717
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 91048 (Grab)
Analyte: Iron
QC Batch No: L658387/L657717
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 91048 (Grab)
Analyte: Potassium
QC Batch No: L658387/L657717
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Sample 91048 (Grab)
Analyte: Magnesium
QC Batch No: 1-658650/1-657717
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 91048 (Grab)
Analyte: Manganese
QC Batch No: L658387/L657717
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 91048 (Grab)
Analyte: Sulfur
QC Batch No: L658387/L657717
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Solids Total Mercury Analysis - CVAA Method 7471A
Page 4 of 9

to
Way� PA
► x
Main 901.213.2400 .41
wwwmaypointanalyticaLcorn
Sample 91191 (Annapolis Truck Chute)
Analyte: Mercury
QC Batch No: 1-658555/1-658246
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Page 5 of 9

Way to
PM�
46245
EMA Resources Inc
Mr. Brent Collins
755 Yadkinville Road
Mocksville , NC 27028
Project Asheboro, NC
Information :
Report Date : 01/18/2023
Received �.�101/10/2023
-
Connie Cook
Report Number : 23-010-0010
REPORT OFANALYSIS
Project
Manager
Lab No : 91173
Matrix:
Solids
Sample ID : Piedmont Water
Sampled:
1/9/2023
10:45
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Method
Moisture
80.5
%
1
01/12/23 16:03
FMM
SW-DRYWT
Ammonia Nitrogen
3693
mg/Kg -
dry
82.1
513
1
01/18/23 09:00
JPJ
4500NH3C-2011
Nitrate+Nitrite-N
<25.5
mg/Kg -
dry
25.5
25.5
1
01/17/23 13:54
ZBD
4500NO3F-2016
Organic N
131703
mg/Kg -
dry
82.05
512.8
1
01/17/23 10:45
CALCULATION
pH
6.1
S.U.
1
01/17/2315:30
SAR
9045D
Total Solids
19.5
%
0.010
0.010
1
01/12/23 16:03
FMM
2540G-2011
Total Volatile Solids
31.8
%
0.010
0.010
1
01/12/23 16:03
FMM
2540G-2011
Total Kjeldahl Nitrogen
13500
mg/Kg -
dry
51.3
1280
1
01/17/23 10:45
JPJ ;M-4500-NH3C-TKl`
Phosphorus
1020
mg/Kg -
dry
14.2
25.6
1
01/12/23 22:06
TJS
6010D
Aluminum
4840
mg/Kg -
dry
23.7
25.6
1
01/12/23 22:06
TJS
6010D
Arsenic
<1.23
mg/Kg -
dry
1.23
2.56
1
01/12/23 22:06
TJS
6010D
Cadmium
14.5
mg/Kg -
dry
0.103
0.513
1
01/12/23 22:06
TJS
6010D
Calcium
3100
mg/Kg -
dry
198
256
1
01/12/23 22:06
TJS
6010D
Chromium
13.0
mg/Kg -
dry
1.21
1.28
1
01/12/23 22:06
TJS
6010D
Copper
17.5
mg/Kg -
dry
1.59
2.56
1
01/12/23 22:06
TJS
6010D
Iron
408000
mg/Kg -
dry
872
1030
20
01/13/23 20:10
TJS
6010D
Lead
5.49
mg/Kg -
dry
0.923
1.54
1
01/12/23 22:06
TJS
6010D
Magnesium
438
mg/Kg -
dry
13.2
25.6
1
01/12/23 22:06
TJS
6010D
Manganese
1950
mg/Kg -
dry
1.67
2.56
1
01/12/23 22:06
TJS
6010D
Mercury
<0.0311
mg/Kg -
dry
0.0311
0.713
1
01/13/23 16:20
JTR
7471A
Molybdenum
12.0
mg/Kg -
dry
0.692
1.28
1
01/12/23 22:06
TJS
6010D
Nickel
12.4
mg/Kg -
dry
0.615
1.28
1
01/12/23 22:06
TJS
6010D
Potassium
201
mg/Kg -
dry
31.7
51.3
1
01/12/23 22:06
TJS
6010D
Qualifiers/ DF Dilution Factor
J
Estimated value
Definitions MQL Method Quantitation Limit
Page 6 of 9

0
Waypoeint2790
Whitten
Road, Memphis, TN 38133
Main 901.213.2400 0 Fax [phone]
ANALYTICAL
www.waypoiintanalyticaLcom
46245
EMA Resources Inc
Project
Asheboro,
NC
Mr. Brent Collins
Report Date : 01/18/2023
755 Yadkinville Road
Information :
Received : 01/10/2023
Mocksville , NC 27028
Connie Cook
Report Number : 23-010-0010
REPORT OFANALYSIS
Project Manager
Lab No : 91173
Matrix: Solids
Sample ID : Piedmont Water
Sampled: 1/9/2023 10:45
Test
Results
Units
MDL
MQL DF Date / Time By Analytical
Analyzed Method
Selenium
11.0
mg/Kg - dry
1.64
2.56 1 01/12/23 22:06 TJS 6010D
Sodium
381
mg/Kg - dry
66.7
128 1 01/12/23 22:06 TJS 6010D
Zinc
17.4
mg/Kg - dry
4.15
6.41 1 01/12/23 22:06 TJS 6010D
Sulfur
4160
mg/Kg - dry
26.6
51.3 1 01/12/23 22:06 TJS 6010D
Sodium Absorption Ratio
0.74
Ratio
0.01
0.01 1 01/12/23 22:06 CALCULATION
Qualifiers/ DF Dilution Factor
Definitions
J Estimated value
Page 7 of 9

l0
Waypoint",
J123.8224
Shipment Receipt Form
Customer Number: 46245
Customer Name: EMA Resources Inc
Report Number: 23-010-0010
Shipping Method
0 Fed Ex 0 US Postal 0 Lab
0 UPS 0 Client 0 Courier
0 Other
Thermometer ID:
T135
Shipping container/cooler uncompromised?
Yes
0 No
Number of coolers/boxes received
1
Custody seals intact on shipping container/cooler?
0 Yes
0 No
Not Present
Custody seals intact on sample bottles?
0 Yes
0 No
Not Present
Chain of Custody (COC) present?
# Yes
0 No
COC agrees with sample label(s)?
# Yes
0 No
COC properly completed
# Yes
0 No
Samples in proper containers?
# Yes
0 No
Sample containers intact?
# Yes
0 No
Sufficient sample volume for indicated test(s)?
# Yes
0 No
All samples received within holding time?
# Yes
0 No
Cooler temperature in compliance?
# Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
# Yes
0 No
Water - Sample containers properly preserved
0 Yes
0 No
N/A
Water - VOA vials free of headspace
0 Yes
0 No
N/A
Trip Blanks received with VOAs
0 Yes
0 No
N/A
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
0 N/A
F_ High concentration container (48 hr)
F_ High concentration pre -weighed (methanol -14 d)
F_ Low concentration EnCore samplers (48 hr)
F_ Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included? 0 Yes * No
Comments:
Signature: lEmily M. Peterson Date & Time: 01/10/2023 08:57:55
Page 8 of 9

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0
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.r *�
wm
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0 o�Y �:.° W? }w MM.M bs
Page 9 of 9

mil ,
4/13/2023
EMA Resources Inc
Mr. Brent Collins
755 Yadkinville Rd
Mocksville, NC, 27028
Ref: Analytical Testing
Lab Report Number: 23-096-0016
Client Project Description: Piedmont Water
Dear Mr. Brent Collins:
Waypoint Analytical, LLC. received sample(s) on 4/6/2023 for the analyses presented in the following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Where the laboratory was not responsible for the sampling
stage (refer to the chain of custody) results apply to the sample as received.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2021) and NELAC unless otherwise indicated. Any parameter
for which the laboratory is not officially NELAP accredited is indicated by a '—'symbol. These are not included in
the scope because NELAP accreditation is either not available or has not been applied for. Additional
certifications may be held/are available for parameters, where NELAP accreditation is not required or applicable.
A full list of certifications is available upon request.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Connie Cook
Project Manager
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 1 of 8

Way to
PM�
WRTIA"Wi
tMain 901.213.2400 0 Fax u f,
www.waypointanalyticaLcom
Certification Summary
Laboratory ID: WP MTN: Waypoint Analytical, LLC., Memphis, TN
State
Program
Lab ID
Expiration Date
Alabama
State Program
40750
02/29/2024
Arkansas
State Program
88-0650
02/07/2024
California
State Program
2904
06/30/2023
Florida
State Program
- NELAP
E871157
06/30/2023
Georgia
State Program
C044
11/14/2025
Georgia
State Program
04015
06/30/2023
Illinois
State Program
- NELAP
200078
10/10/2023
Kentucky
State Program
80215
06/30/2023
Kentucky
State Program
KY90047
12/31/2023
Louisiana
State Program
- NELAP
LA037
12/31/2023
Louisiana
State Program
- NELAP
04015
06/30/2023
Mississippi
State Program
MS
11/14/2025
North Carolina
State Program
47701
07/31/2023
North Carolina
State Program
415
12/31/2023
Pennsylvania
State Program
- NELAP
68-03195
05/31/2024
South Carolina
State Program
84002
06/30/2023
Tennessee
State Program
02027
11/14/2025
Texas
State Program
- NELAP
T104704180
09/30/2023
Virginia
State Program
00106
06/30/2023
Virginia
State Program
- NELAP
460181
09/14/2023
Page 1 of 1 00001/23-096-0016
Page 2 of 8

Way lht,(2)
PM�TICAL'
Sample Summary Table
Report Number: 23-096-0016
Client Project Description: Piedmont Water
Lab No Client Sample ID Matrix Date Collected Date Received
93340 Piedmont Water Solids 04/05/2023 11:15 04/06/2023
Page 3 of 8

to
Way� PA
► x
Client: EMA Resources Inc
Project: Piedmont Water
Lab Report Number: 23-096-0016
Date: 4/13/2023
Main 901.213.2400 .41
wwwmaypointanalyticaLcorn
CASE NARRATIVE
Metals Analysis Method 601 OD
Sample 93340 (Piedmont Water)
QC Batch No: 1-675382/1-674801
This sample was analyzed at a dilution due to IEC interference/matrix interference.
Sample 93829 (#2)
Analyte: Aluminum
QC Batch No: 1-675666/1-674801
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 93829 (#2)
Analyte: Iron
QC Batch No: 1-675666/1-674801
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 93829 (#2)
Analyte: Potassium
QC Batch No: 1-675666/1-674801
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 93829 (#2)
Analyte: Magnesium
QC Batch No: 1-675666/1-674801
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 93829 (#2)
Analyte: Sulfur
QC Batch No: 1-675666/1-674801
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Solids Total Mercury Analysis - CVAA Method 7471A
Sample 93833 (San Elijo)
Analyte: Mercury
QC Batch No: 1-675254/1-674948
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Page 4 of 8

Way to
PM�
46245
EMA Resources Inc
Mr. Brent Collins
755 Yadkinville Rd
Mocksville , NC 27028
Project Piedmont Water
Information :
IT
Report Date : 04/13/2023
Received �.���y04/06/2023
-
Connie Cook
Report Number : 23-096-0016
REPORT OFANALYSIS
Project
Manager
Lab No : 93340
Matrix:
Solids
Sample ID : Piedmont Water
Sampled:
4/5/2023
11:15
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Method
Moisture
78.9
%
1
04/12/2315:19
JLS
SW-DRYWT
Ammonia Nitrogen
882
mg/Kg -
dry
75.8
474
1
04/13/23 13:30
JPJ
4500NH3C-2011
Nitrate+Nitrite-N
<4.74
mg/Kg -
dry
4.74
23.7
1
04/11/23 12:56
ZBD
4500NO3F-2016
Organic N
10490
mg/Kg -
dry
568.7
1147
1
04/10/23 14:45
CALCULATION
pH
5.8
S.U.
1
04/11/2311:25
HBT
9045D
Total Solids
20.7
%
0.010
0.010
1
04/12/23 15:13
JLS
2540G-2011
Total Kjeldahl Nitrogen
11400
mg/Kg -
dry
1150
1
04/10/23 14:45
ANH 4500NORGD-2011
Phosphorus
1210
mg/Kg -
dry
65.4
118
5
04/11/23 23:16
JTR
6010D
Aluminum
6820
mg/Kg -
dry
109
118
5
04/11/23 23:16
JTR
6010D
Arsenic
<5.69
mg/Kg -
dry
5.69
11.8
5
04/11/23 23:16
JTR
6010D
Cadmium
4.10
mg/Kg -
dry
0.474
2.37
5
04/11/23 23:16
JTR
6010D
Calcium
1700
mg/Kg -
dry
919
1180
5
04/11/23 23:16
JTR
6010D
Chromium
13.8
mg/Kg -
dry
5.59
5.92
5
04/11/23 23:16
JTR
6010D
Copper
71.6
mg/Kg -
dry
7.35
11.8
5
04/11/23 23:16
JTR
6010D
Iron
344000
mg/Kg -
dry
2020
2370
50
04/11/23 23:21
JTR
6010D
Lead
<4.27
mg/Kg -
dry
4.27
7.11
5
04/11/23 23:16
JTR
6010D
Magnesium
455
mg/Kg -
dry
61.1
118
5
04/11/23 23:16
JTR
6010D
Manganese
1630
mg/Kg -
dry
7.73
11.8
5
04/11/23 23:16
JTR
6010D
Mercury
<0.102
mg/Kg -
dry
0.102
0.848
1
04/10/23 14:15
FDS
7471A
Molybdenum
13.6
mg/Kg -
dry
3.20
5.92
5
04/11/23 23:16
JTR
6010D
Nickel
16.3
mg/Kg -
dry
2.84
5.92
5
04/11/23 23:16
JTR
6010D
Potassium
1473
mg/Kg -
dry
146
237
5
04/11/23 23:16
JTR
6010D
Selenium
<7.58
mg/Kg -
dry
7.58
11.8
5
04/11/23 23:16
JTR
6010D
Qualifiers/ DF Dilution Factor
J
Estimated value
Definitions MQL Method Quantitation Limit
Page 5 of 8

0
Waypoeint2790
Whitten
Road, Memphis, TN 38133
Main 901.213.2400 0 Fax [phone]
ANALYTICAL
www.waypoiintanalyticaLcom
46245
EMA Resources Inc
Project
Piedmont Water
Mr. Brent Collins
Report Date : 04/13/2023
755 Yadkinville Rd
Information :
Received : 04/06/2023
Mocksville , NC 27028
Connie Cook
Report Number : 23-096-0016
REPORT OFANALYSIS
Project Manager
Lab No : 93340
Matrix: Solids
Sample ID : Piedmont Water
Sampled: 4/5/2023 11:15
Test
Results
Units
MDL
MQL DF Date / Time By Analytical
Analyzed Method
Sodium
3133
mg/Kg - dry
308
592 5 04/11/23 23:16 JTR 6010D
Zinc
<19.2
mg/Kg - dry
19.2
29.6 5 04/11/23 23:16 JTR 6010D
Sulfur
5880
mg/Kg - dry
123
237 5 04/11/23 23:16 JTR 6010D
Sodium Absorption Ratio
0.793
Ratio
0.01
0.01 5 04/11/23 23:16 CALCULATION
Qualifiers/ DF Dilution Factor
Definitions MQL Method Quantitation Limit
J Estimated value
Page 6 of 8

l0
Waypoint",
J123.8224
Shipment Receipt Form
Customer Number: 46245
Customer Name: EMA Resources Inc
Report Number: 23-096-0016
Shipping Method
0 Fed Ex 0 US Postal 0 Lab
0 UPS 0 Client 0 Courier
0 Other
Thermometer ID:
T135
Shipping container/cooler uncompromised?
Yes
0 No
Number of coolers/boxes received
1
Custody seals intact on shipping container/cooler?
0 Yes
0 No
Not Present
Custody seals intact on sample bottles?
0 Yes
0 No
Not Present
Chain of Custody (COC) present?
# Yes
0 No
COC agrees with sample label(s)?
# Yes
0 No
COC properly completed
# Yes
0 No
Samples in proper containers?
# Yes
0 No
Sample containers intact?
# Yes
0 No
Sufficient sample volume for indicated test(s)?
# Yes
0 No
All samples received within holding time?
# Yes
0 No
Cooler temperature in compliance?
# Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
# Yes
0 No
Water - Sample containers properly preserved
Yes
0 No
0 N/A
Water - VOA vials free of headspace
0 Yes
0 No
N/A
Trip Blanks received with VOAs
0 Yes
0 No
N/A
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
0 N/A
F_ High concentration container (48 hr)
F_ High concentration pre -weighed (methanol -14 d)
F_ Low concentration EnCore samplers (48 hr)
F_ Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included? 0 Yes * No
Comments:
Signature: lEmily M. Peterson Date & Time: 04/06/2023 09:30:29
Page 7 of 8

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Page 8 of 8

mil ,
7/28/2023
EMA Resources Inc
Mr. Brent Collins
755 Yadkinville Rd
Mocksville, NC, 27028
Ref: Analytical Testing
Lab Report Number: 23-192-0035
Client Project Description: Piedmont
Dear Mr. Brent Collins:
Waypoint Analytical, LLC. received sample(s) on 7/11/2023 for the analyses presented in the following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Where the laboratory was not responsible for the sampling
stage (refer to the chain of custody) results apply to the sample as received.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2021) and NELAC unless otherwise indicated. Any parameter
for which the laboratory is not officially NELAP accredited is indicated by a '—'symbol. These are not included in
the scope because NELAP accreditation is either not available or has not been applied for. Additional
certifications may be held/are available for parameters, where NELAP accreditation is not required or applicable.
A full list of certifications is available upon request.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Connie Cook
Project Manager
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 1 of 9

Way to
PM�
WRTIA"Wi
tMain 901.213.2400 0 Fax u f,
www.waypointanalyticaLcom
Certification Summary
Laboratory ID: WP MTN: Waypoint Analytical, LLC., Memphis, TN
State
Program
Lab ID
Expiration Date
Alabama
State Program
40750
02/29/2024
Arkansas
State Program
88-0650
02/07/2024
California
State Program
2904
06/30/2024
Florida
State Program
- NELAP
E871157
06/30/2024
Georgia
State Program
C044
11/14/2025
Georgia
State Program
04015
06/30/2024
Illinois
State Program
- NELAP
200078
10/10/2023
Kentucky
State Program
80215
06/30/2024
Kentucky
State Program
KY90047
12/31/2023
Louisiana
State Program
- NELAP
LA037
12/31/2023
Louisiana
State Program
- NELAP
04015
06/30/2024
Mississippi
State Program
MS
11/14/2025
North Carolina
State Program
47701
07/31/2023
North Carolina
State Program
415
12/31/2023
Pennsylvania
State Program
- NELAP
68-03195
05/31/2024
South Carolina
State Program
84002
06/30/2023
Tennessee
State Program
02027
11/14/2025
Texas
State Program
- NELAP
T104704180
09/30/2023
Virginia
State Program
00106
06/30/2024
Virginia
State Program
- NELAP
460181
09/14/2023
Page 1 of 1 00001/23-192-0035
Page 2 of 9

Way lht,(2)
PM�TICAL'
Sample Summary Table
Report Number: 23-192-0035
K]immt Project Description: Piedmont
Lab No Client Sample zo Matrix Date Collected Date Received
97973 Piedmont Water Solids 07/10/202309:30 07/11/2023
Page 3 of 9

to
Way� PA
► x
Client: EMA Resources Inc
Project: Piedmont
Lab Report Number: 23-192-0035
Date: 7/28/2023
Main 901.213.2400 .41
wwwmaypointanalyticaLcorn
CASE NARRATIVE
Metals Analysis Method 601 OD
Sample 97975 (Shelby WTP)
Analyte: Aluminum
QC Batch No: 1-693030/1-692238
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 97975 (Shelby WTP)
Analyte: Arsenic
QC Batch No: 1-692735/1-692238
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Sample 97975 (Shelby WTP)
Analyte: Calcium
QC Batch No: 1-692735/1-692238
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Sample 97975 (Shelby WTP)
Analyte: Chromium
QC Batch No: 1-692735/1-692238
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 97975 (Shelby WTP)
Analyte: Copper
QC Batch No: 1-692735/1-692238
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 97975 (Shelby WTP)
Analyte: Iron
QC Batch No: 1-693030/1-692238
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 97975 (Shelby WTP)
Analyte: Potassium
QC Batch No: 1-693030/1-692238
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Page 4 of 9

to
Way� PA
► x
Main 901.213.2400 .41
wwwmaypointanalyticaLcorn
Sample 97975 (Shelby WTP)
Analyte: Magnesium
QC Batch No: 1-692735/1-692238
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 97975 (Shelby WTP)
Analyte: Manganese
QC Batch No: 1-692735/1-692238
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 97975 (Shelby WTP)
Analyte: Lead
QC Batch No: 1-692735/1-692238
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 97975 (Shelby WTP)
Analyte: Sulfur
QC Batch No: 1-692735/1-692238
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 97973 (Piedmont Water)
Analyte: Selenium
QC Batch No: 1-692735/1-692238
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Sample 97975 (Shelby WTP)
Analyte: Selenium
QC Batch No: 1-692735/1-692238
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Solids Total Mercury Analysis - CVAA Method 7471A
Sample 97975 (Shelby WTP)
Analyte: Mercury
QC Batch No: 1-692588/1-692341
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Page 5 of 9

Way to
PM�
46245
EMA Resources Inc
Mr. Brent Collins
755 Yadkinville Rd
Mocksville , NC 27028
Project Piedmont
Information :
IT
Report Date : 07/28/2023
Received �.���y07/11/2023
-
Connie Cook
Report Number : 23-192-0035
REPORT OFANALYSIS
Project
Manager
Lab No : 97973
Matrix:
Solids
Sample ID : Piedmont Water
Sampled:
7/10/2023
9:30
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Method
Moisture
79.8
%
1
07/14/2318:53
KDO
SW-DRYWT
Ammonia Nitrogen
713
mg/Kg -
dry
79.2
495
1
07/28/23 07:30
JPJ
4500NH3C-2011
Nitrate+Nitrite-N
<4.95
mg/Kg -
dry
4.95
24.8
1
07/13/23 14:51
CLP
4500NO3F-2016
Organic N
8099
mg/Kg -
dry
1025
2064
1
07/17/23 13:43
CALCULATION
pH
6.7
S.U.
1
07/12/2317:00
CNB
9045D
Total Solids
20.2
%
0.010
0.010
1
07/14/23 18:53
KDO
2540G-2011
Total Kjeldahl Nitrogen
8810
mg/Kg -
dry
2060
1
07/17/23 13:43
ANH 4500NORGD-2011
Phosphorus
1050
mg/Kg -
dry
13.9
24.8
1
07/13/23 23:49
TJS
6010D
Aluminum
9550
mg/Kg -
dry
23.0
24.8
1
07/13/23 23:49
BKN
6010D
Arsenic
4.28
mg/Kg -
dry
1.24
2.48
1
07/13/23 23:49
TJS
6010D
Cadmium
22.8
mg/Kg -
dry
0.248
0.495
1
07/13/23 23:49
TJS
6010D
Calcium
3330
mg/Kg -
dry
192
248
1
07/13/23 23:49
TJS
6010D
Chromium
20.4
mg/Kg -
dry
1.24
1.24
1
07/13/23 23:49
TJS
6010D
Copper
64.4
mg/Kg -
dry
1.49
2.48
1
07/13/23 23:49
TJS
6010D
Iron
378000
mg/Kg -
dry
847
990
20
07/15/23 00:11
BKN
6010D
Lead
4.88
mg/Kg -
dry
0.990
1.49
1
07/13/23 23:49
TJS
6010D
Magnesium
698
mg/Kg -
dry
12.9
24.8
1
07/13/23 23:49
TJS
6010D
Manganese
1410
mg/Kg -
dry
1.73
2.48
1
07/13/23 23:49
TJS
6010D
Mercury
<0.108
mg/Kg -
dry
0.108
0.896
1
07/13/23 11:18
MRE
7471A
Molybdenum
19.1
mg/Kg -
dry
0.742
1.24
1
07/13/23 23:49
TJS
6010D
Nickel
51.5
mg/Kg -
dry
0.742
1.24
1
07/13/23 23:49
TJS
6010D
Potassium
279
mg/Kg -
dry
30.7
49.5
1
07/13/23 23:49
TJS
6010D
Selenium
<34.7
mg/Kg -
dry
34.7
49.5
20
07/15/23 00:11
BKN
6010D
Qualifiers/ DF Dilution Factor
MQL
Method Quantitation Limit
Definitions
Page 6 of 9

0
Waypoeint790
Whitten
Road, Memphis, TN 38133
Main 901.213.2400 0 Fax [phone]
ANALYTICAL
www.waypoiintanalyticaLcom
46245
EMA Resources Inc
Project
Piedmont
Mr. Brent Collins
Report Date : 07/28/2023
755 Yadkinville Rd
Information :
Received : 07/11/2023
Mocksville , NC 27028
Connie Cook
Report Number : 23-192-0035
REPORT OFANALYSIS
Project Manager
Lab No : 97973
Matrix: Solids
Sample ID : Piedmont Water
Sampled: 7/10/2023 9:30
Test
Results
Units
MDL
MQL DF Date / Time By Analytical
Analyzed Method
Sodium
372
mg/Kg - dry
64.4
124 1 07/13/23 23:49 TJS 6010D
Zinc
18.6
mg/Kg - dry
4.21
6.19 1 07/13/23 23:49 TJS 6010D
Sulfur
2200
mg/Kg - dry
25.7
49.5 1 07/13/23 23:49 TJS 6010D
Sodium Absorption Ratio
0.68
Ratio
0.01
0.01 1 07/13/23 23:49 CALCULATION
Qualifiers/ DF Dilution Factor
Definitions
MQL Method Quantitation Limit
Page 7 of 9

l0
Waypoint",
J123.8224
Shipment Receipt Form
Customer Number: 46245
Customer Name: EMA Resources Inc
Report Number: 23-192-0035
Shipping Method
0 Fed Ex 0 US Postal 0 Lab
0 UPS 0 Client 0 Courier
0 Other
Thermometer ID:
T135
Shipping container/cooler uncompromised?
Yes
0 No
Number of coolers/boxes received
1
Custody seals intact on shipping container/cooler?
0 Yes
0 No
Not Present
Custody seals intact on sample bottles?
0 Yes
0 No
Not Present
Chain of Custody (COC) present?
# Yes
0 No
COC agrees with sample label(s)?
# Yes
0 No
COC properly completed
# Yes
0 No
Samples in proper containers?
# Yes
0 No
Sample containers intact?
# Yes
0 No
Sufficient sample volume for indicated test(s)?
# Yes
0 No
All samples received within holding time?
# Yes
0 No
Cooler temperature in compliance?
# Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
# Yes
0 No
Water - Sample containers properly preserved
Yes
0 No
0 N/A
Water - VOA vials free of headspace
0 Yes
0 No
N/A
Trip Blanks received with VOAs
0 Yes
0 No
N/A
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
0 N/A
F_ High concentration container (48 hr)
F_ High concentration pre -weighed (methanol -14 d)
F_ Low concentration EnCore samplers (48 hr)
F_ Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included? 0 Yes * No
Comments:
Signature: lEmily M. Peterson Date & Time: 07/11/2023 10:13:08
Page 8 of 9

Page 9 of 9

mil ,
10/18/2023
EMA Resources Inc
Mr. Brent Collins
755 Yadkinville Rd
Mocksville, NC, 27028
Ref: Analytical Testing
Lab Report Number: 23-277-0014
Client Project Description: Piedmont Water
Dear Mr. Brent Collins:
Waypoint Analytical, LLC. received sample(s) on 10/4/2023 for the analyses presented in the following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Where the laboratory was not responsible for the sampling
stage (refer to the chain of custody) results apply to the sample as received.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2021) and NELAC unless otherwise indicated. Any parameter
for which the laboratory is not officially NELAP accredited is indicated by a '—'symbol. These are not included in
the scope because NELAP accreditation is either not available or has not been applied for. Additional
certifications may be held/are available for parameters, where NELAP accreditation is not required or applicable.
A full list of certifications is available upon request.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Connie Cook
Project Manager
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 1 of 11

Way to
PM�
WRTIA"Wi
tMain 901.213.2400 0 Fax u f,
www.waypointanalyticaLcom
Certification Summary
Laboratory ID: WP MTN: Waypoint Analytical, LLC., Memphis, TN
State
Program
Lab ID
Expiration Date
Alabama
State Program
40750
02/29/2024
Arkansas
State Program
88-0650
02/07/2024
California
State Program
2904
06/30/2024
Florida
State Program
- NELAP
E871157
06/30/2024
Georgia
State Program
C044
11/14/2025
Georgia
State Program
04015
06/30/2024
Illinois
State Program
- NELAP
200078
10/31/2024
Kentucky
State Program
80215
06/30/2024
Kentucky
State Program
KY90047
12/31/2023
Louisiana
State Program
- NELAP
LA037
12/31/2023
Louisiana
State Program
- NELAP
04015
06/30/2024
Mississippi
State Program
MS
11/14/2025
North Carolina
State Program
47701
07/31/2024
North Carolina
State Program
415
12/31/2023
Pennsylvania
State Program
- NELAP
68-03195
05/31/2024
South Carolina
State Program
84002
06/30/2024
Tennessee
State Program
02027
11/14/2025
Texas
State Program
- NELAP
T104704180
09/30/2024
Virginia
State Program
00106
06/30/2024
Virginia
State Program
- NELAP
460181
09/14/2024
Page 1 of 1 00001/23-277-0014
Page 2 of 11

Way lht,(2)
PM�TICAL'
Sample Summary Table
Report Number: 23-277-0014
Client Project Description: Piedmont Water
Lab No Client Sample ID Matrix Date Collected Date Received
98036 Piedmont Water Solids 10/03/2023 14:10 10/04/2023
Page 3 of 11

to
Way� PA
► x
Client: EMA Resources Inc
Project: Piedmont Water
Lab Report Number: 23-277-0014
Date: 10/18/2023
Main 901.213.2400 .41
wwwmaypointanalyticaLcorn
CASE NARRATIVE
Metals Analysis Method 601 OD
Sample 98702
Analyte: Aluminum
QC Batch No: 1-709731/1-709182
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Sample 98702
Analyte: Aluminum
QC Batch No: 1-710024/1-709182
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 98036 (Piedmont Water)
Analyte: Arsenic
QC Batch No: 1-709731/1-709182
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Sample 98702
Analyte: Arsenic
QC Batch No: 1-709731/1-709182
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Sample 98702
Analyte: Arsenic
QC Batch No: 1-710024/1-709182
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Sample 98702
Analyte: Calcium
QC Batch No: 1-709731/1-709182
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Sample 98702
Analyte: Cadmium
QC Batch No: 1-709731/1-709182
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Sample 98702
Analyte: Cadmium
QC Batch No: 1-710024/1-709182
The matrix spike, matrix spike duplicate and the dilution test were all outside of the quality control acceptance
ranges. Matrix interference is suspected.
Page 4 of 11

to
Way� PA
► x
Main 901.213.2400 .41
wwwmaypointanalyticaLcorn
Sample 98702
Analyte: Chromium
QC Batch No: 1-709731/1-709182
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Sample 98702
Analyte: Chromium
QC Batch No: 1-710024/1-709182
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 98702
Analyte: Copper
QC Batch No: 1-709731/1-709182
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Sample 98702
Analyte: Copper
QC Batch No: 1-710024/1-709182
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 98702
Analyte: Iron
QC Batch No: 1-709731/1-709182
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Sample 98702
Analyte: Iron
QC Batch No: 1-710024/1-709182
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 98702
Analyte: Potassium
QC Batch No: 1-709731/1-709182
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Sample 98702
Analyte: Potassium
QC Batch No: 1-710024/1-709182
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Sample 98702
Analyte: Magnesium
QC Batch No: 1-709731/1-709182
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Sample 98702
Analyte: Magnesium
QC Batch No: 1-710024/1-709182
Page 5 of 11

to
Way� PA
► x
Main 901.213.2400 .41
wwwmaypointanalyticaLcorn
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 98702
Analyte: Manganese
QC Batch No: 1-709731/1-709182
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Sample 98702
Analyte: Manganese
QC Batch No: 1-710024/1-709182
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 98702
Analyte: Molybdenum
QC Batch No: 1-709731/1-709182
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Sample 98702
Analyte: Molybdenum
QC Batch No: 1-710024/1-709182
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 98702
Analyte: Sodium
QC Batch No: 1-709731/1-709182
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Sample 98702
Analyte: Sodium
QC Batch No: 1-710024/1-709182
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 98702
Analyte: Nickel
QC Batch No: 1-709731/1-709182
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Sample 98702
Analyte: Nickel
QC Batch No: 1-710024/1-709182
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 98702
Analyte: Phosphorus
QC Batch No: 1-709731/1-709182
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Sample 98702
Page 6 of 11

to
Way� PA
► x
Main 901.213.2400 .41
wwwmaypointanalyticaLcorn
Analyte: Lead
QC Batch No: 1-709731/1-709182
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Sample 98702
Analyte: Lead
QC Batch No: 1-710024/1-709182
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Sample 98702
Analyte: Sulfur
QC Batch No: 1-709731/1-709182
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Sample 98702
Analyte: Selenium
QC Batch No: 1-709731/1-709182
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Sample 98702
Analyte: Selenium
QC Batch No: 1-710024/1-709182
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Sample 98702
Analyte: Selenium
QC Batch No: 1-710024/1-709182
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Sample 98702
Analyte: Zinc
QC Batch No: 1-709731/1-709182
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Solids Total Mercury Analysis - CVAA Method 7471A
Sample 97716 (Annual Sludge)
Analyte: Mercury
QC Batch No: 1-709569/1-709290
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Page 7 of 11

Way to
PM�
46245
EMA Resources Inc
Mr. Brent Collins
755 Yadkinville Rd
Mocksville , NC 27028
Project Piedmont Water
Information :
IT
Report Date : 10/18/2023
Received 1��0yy/04/2023
�.�-
Connie Cook
Report Number : 23-277-0014
REPORT OFANALYSIS
Project
Manager
Lab No : 98036
Matrix:
Solids
Sample ID : Piedmont Water
Sampled:
10/3/2023
14:10
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Method
Moisture
79.6
%
0.010
0.010
1
10/06/2316:00
CAH
SW-DRYWT
Ammonia Nitrogen
2193
mg/Kg -
dry
78.4
490
1
10/18/23 14:37
JPJ
4500NH3C-2011
Nitrate+Nitrite-N
<4.90
mg/Kg -
dry
4.90
24.5
1
10/11/23 15:30
CLP
4500NO3F-2016
Organic N
89463
mg/Kg -
dry
892.2
1799
1
10/06/23 12:02
CALCULATION
pH
5.9
S.U.
1
10/06/2316:07
CNB
9045D
Total Solids
20.4
%
0.010
0.010
1
10/06/23 16:00
CAH
2540G-2011
Total Kjeldahl Nitrogen
9170
mg/Kg -
dry
1800
1
10/06/23 12:02
ANH 4500NORGD-2011
Phosphorus
1570
mg/Kg -
dry
13.7
24.5
1
10/09/23 19:27
TJS
6010D
Aluminum
6570
mg/Kg -
dry
22.8
24.5
1
10/09/23 19:27
TJS
6010D
Arsenic
7.21
mg/Kg -
dry
1.23
2.45
1
10/10/23 12:27
BKN
6010D
Cadmium
31.3
mg/Kg -
dry
0.245
0.490
1
10/09/23 19:27
BKN
6010D
Calcium
4950
mg/Kg -
dry
190
245
1
10/09/23 19:27
TJS
6010D
Chromium
11.2
mg/Kg -
dry
1.23
1.23
1
10/09/23 19:27
TJS
6010D
Copper
44.6
mg/Kg -
dry
1.47
2.45
1
10/09/23 19:27
TJS
6010D
Iron 409000
mg/Kg -
dry
838
980
20
10/10/23 12:38
BKN
6010D
Lead
6.72
mg/Kg -
dry
0.980
1.47
1
10/09/23 19:27
TJS
6010D
Magnesium
760
mg/Kg -
dry
12.7
24.5
1
10/09/23 19:27
BKN
6010D
Manganese
7060
mg/Kg -
dry
8.58
12.3
5
10/10/23 12:33
BKN
6010D
Mercury
<0.102
mg/Kg -
dry
0.102
0.848
1
10/09/23 11:50
MRE
7471A
Molybdenum
23.2
mg/Kg -
dry
0.735
1.23
1
10/09/23 19:27
TJS
6010D
Nickel
28.7
mg/Kg -
dry
0.735
1.23
1
10/09/23 19:27
TJS
6010D
Potassium
238
mg/Kg -
dry
30.4
49.0
1
10/10/23 12:27
BKN
6010D
Selenium
10.4
mg/Kg -
dry
1.72
2.45
1
10/09/23 19:27
TJS
6010D
Qualifiers/ DF Dilution Factor
J
Estimated value
Definitions MQL Method Quantitation Limit
Page 8 of 11

0
Waypoeint790
Whitten
Road, Memphis, TN 38133
Main 901.213.2400 0 Fax [phone]
ANALYTICAL
www.waypoiintanalyticaLcom
46245
EMA Resources Inc
Project
Piedmont Water
Mr. Brent Collins
Report Date : 10/18/2023
755 Yadkinville Rd
Information :
Received : 10/04/2023
Mocksville , NC 27028
Connie Cook
Report Number : 23-277-0014
REPORT OFANALYSIS
Project Manager
Lab No : 98036
Matrix: Solids
Sample ID : Piedmont Water
Sampled: 10/3/2023 14:10
Test
Results
Units
MDL
MQL DF Date / Time By Analytical
Analyzed Method
Sodium
1030
mg/Kg - dry
63.7
123 1 10/10/23 12:27 BKN 6010D
Zinc
19.2
mg/Kg - dry
4.17
6.13 1 10/09/23 19:27 TJS 6010D
Sulfur
2750
mg/Kg - dry
25.5
49.0 1 10/09/23 19:27 TJS 6010D
Sodium Absorption Ratio
1.62
Ratio
0.01
0.01 1 10/09/23 19:27 CALCULATION
Qualifiers/ DF Dilution Factor
Definitions MQL Method Quantitation Limit
J Estimated value
Page 9 of 11

l0
Waypoint",
J123.8224
Shipment Receipt Form
Customer Number: 46245
Customer Name: EMA Resources Inc
Report Number: 23-277-0014
Shipping Method
0 Fed Ex 0 US Postal 0 Lab
0 UPS 0 Client 0 Courier
0 Other
Thermometer ID:
T99
Shipping container/cooler uncompromised?
Yes
0 No
Number of coolers/boxes received
1
Custody seals intact on shipping container/cooler?
0 Yes
0 No
Not Present
Custody seals intact on sample bottles?
0 Yes
0 No
Not Present
Chain of Custody (COC) present?
# Yes
0 No
COC agrees with sample label(s)?
# Yes
0 No
COC properly completed
# Yes
0 No
Samples in proper containers?
# Yes
0 No
Sample containers intact?
# Yes
0 No
Sufficient sample volume for indicated test(s)?
# Yes
0 No
All samples received within holding time?
# Yes
0 No
Cooler temperature in compliance?
# Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
# Yes
0 No
Water - Sample containers properly preserved
0 Yes
0 No
N/A
Water - VOA vials free of headspace
0 Yes
0 No
N/A
Trip Blanks received with VOAs
0 Yes
0 No
N/A
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
0 N/A
F_ High concentration container (48 hr)
F_ High concentration pre -weighed (methanol -14 d)
F_ Low concentration EnCore samplers (48 hr)
F_ Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included? 0 Yes * No
Comments:
Signature: IMakayla Weaver Date & Time: 10/04/2023 10:01:17
Page 10 of 11

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Page 11 of 11

(� aceAnalytical ° ANALYTICAL REPORT
January 19, 2023
EMA Resources
Sample Delivery Group: L1574641
Samples Received: 01/10/2023
Project Number:
Description: Sludge
Report To: Mr. Brent Collins
755 Yadkinville Road
Mocksville, NC 27028
Entire Report Reviewed By:
�w
1`l1�
Cassandra Foster
Project Manager
Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be
reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pace
Analytical National is performed per guidance provided in laboratory standard operating procedures ENV-SOP-MTJL-0067and
ENV-SOP-MTJL-0068. Where sampling conducted by the customer, results relate to the accuracy ofthe information provided,
and as the samples are received.
%yp
[Cn
�'Sr
Sc
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1574641 01/19/23 12:12 1 of 23

TABLE OF CONTENTS
cj'x
11 . c iI M")fle' of Coil
2
Ss: Sample Summary
3
Cn: Case Narrative
4
Sr: Sample Results
5
SS
PIEDMONT WATER L1574641-01
5
Fn
oc ouaHblt bil 111 0 1 11,11,1111,11,11 a II""
Wet ( 1'ieinnIIstii ),It 'n't ftflhod 9012
"7
1711-1
Ll
Wet ( 1'ieinn�stii ),It 'n't ftflhod 903A1, 9030��1113
77 .......................
Wet ( 1'ie11"Instii ),It :n't ftflhod 9G�15)
9
Wet ( 1'ieinnIstii ),It :n't ftflhod ���)93/1010A
10
FGI
Meii 4: 1 � I )t w ftflh�'d 7A170A
11
M et a �� s fl :n't ftflhod
12
.. ......................................
11111(datflie Oil gaink binniq!)Ourlds (G( Y�MS) 'n't ftflhod 82(150)
I II 0 1 firlated Acod Ieii ',)llddes (G( ',nit Ilftfl1 od 8151A
177-1
ILI
':��Iesflddes (G( bait Vlietlhod 808"V:1113
17
Serninii 1111datflie Oil gaink 011,11n11!1Mourids (G( PMS) 'n't ftflhod 8270�:
18
GI: Glossary of Terms
20
AL AccriedftatJoins & d"e'.atJoris
1
Sc: Sample Chain of Custody
22
ACCOUNT: PROJECT: SDG:
DATE/TIME:
PAGE:
EMA Resources L1574641
01/19/23 12:12
2 of 23

SAMPLE SUMMARY
Collected by
Collected date/time
Received date/time
PIEDMONT' WATER 1 1574641-01 Waste
Brent Collins
01/09/23 10 45
01/10/23 08 45
...................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................
Method
Batch
Dilution Preparation
Analysis
Analyst
...............
Location'
date/time
date/time
Preparation by Method 1311
WG1986135
1 01/11/23 1123
01/11/23 1123
JTM
Mt. Juliet, 1
Preparation by Method 1311
WG1986615
1 01/11/23 09 20
01/11/23 09 20
BTP
Mt. Juliet, TN
Wet Chemistry by Method 9012 B
WG1986823
1 01/12/23 16 11
01/12/23 23 10
LDT
Mt. Juliet, TN
III
Wet Chemistry by Method 9034-9030B
WG1986127
1 01/13/23 15 00
01/13/23 19 30
AW
Mt. Juliet, TN
Wet Chemistry by Method 9045D
WG1987054
1 01/12/23 16 00
01/12/23 18 25
KAD
Mt. Juliet, TN
Fn
Wet Chemistry by Method D93/1010A
WG1989070
1 01/16/23 0109
01/16/23 0109
CRB
Mt. Juliet, TN
Mercury by Method 7470A
WG1987570
1 01/12/23 10 56
01/13/23 09 28
SRT
Mt. Juliet, TN
Metals (ICP) by Method 6010D
WG1987930
1 01/12/23 18 48
01/12/23 23 29
ABL
Mt. Juliet, TN
Ll
Volatile Organic Compounds (GC/MS) by Method 8260D
WG1987508
1 01/12/23 14 36
01/12/23 14 36
ADM
Mt. Juliet, TN
Chlorinated Acid Herbicides (GC) by Method 8151A
WG1988910
1 01/17/23 09 56
01/18/23 14 53
DLH
Mt. Juliet, TN
Pesticides (GC) by Method 8081B
WG1989109
1 01/16/23 09 32
01/16/23 15 27
-D-1
Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
WG1985658
1 01/13/23 05 38
01/13/23 19 10
JRM
Mt. Juliet, TN
GI
.. ......................................
) Ll
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1574641 01/19/23 12:12 3 of23

CASE NARRATIVE
All sample aliquots were received at the correct temperature, in the proper containers, with the
appropriate preservatives, and within method specified holding times, unless qualified or notated within
the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples
have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control
are within established criteria except where addressed in this case narrative, a non-conformance form
or properly qualified within the sample results. By my digital signature below, I affirm to the best of my
knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the
.......................
quality of the data have been identified by the laboratory, and no information or data have been
knowingly withheld that would affect the quality of the data.
Sr
Cassandra Foster
Project Manager
�
Project Narrative L
All Reactive Cyanide results reported in the attached report were determined as totals using method 9012 B.
All Reactive Sulfide results reported in the attached report were determined as totals using method 9034-903013.
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1574641 01/19/23 12:12 4 of 23

f�'r�'n�!dfN��T"�!WL�I��,F�k���✓T^�,N rah/��,F�Y����✓T^�,N�✓��IIVIIIIIIVIIIVIIVIIIIIIIIIVIIVIIVIIIIIIIIIVIIIIIIVIIIVIIIIVIIIIIIVIIIVIIVIIIIIIIIIVIIVIIVIIIIIIIIIVIIIIIIVIIIVIIIIVIIIIIIVIIIVIIVIIIIIIIIIVIIVIIVIIIIIIIIIVIIIIIIVIIh
PIEDMONT WATER
SAMPLE RESULTS
-
01
Collected date/time: 01/09/23 10:45
-1574641
Preparation by Method 1311
Result Qualifier
Prep
Batch
Analyte
date / time
TCLP Extraction
1/11/20231123:05 AM
WG1986135
TCLP ZHE Extraction -
1/11/2023 9:20:45 AM
WG1986615
Fluid 1
1/11/20231123:05 AM
WG1986135
.�S
Initial pH 6.64
1/11/20231123:05 AM
WG1986135
.......................
Final pH 4.80
1/11/20231123:05 AM
WG1986135
Fn
Wet Chemistry by Method 9012 B
Result Qualifier
RDL Dilution
Analysis
Batch
N
Analyte mg/kg
mg/kg
date / time
Reactive Cyanide 0.532
0.250 1
01/12/2023 23:10
WG1986823
Wet Chemistry by Method 9034-9030B
GI
Result Qualifier
RDL Dilution
Analysis
Batch
Analyte mg/kg
mg/kg
date / time
Reactive Sulfide ND
75.0 1
01/13/202319:30
WG1986127
" I
Wet Chemistry by Method 9045D
` Sc
Result Qualifier
Dilution Analysis
Batch
Analyte su
date / time
Corrosivity by pH 5.92 TC
1 01/12/202318:25 WG1987054
Sample Narrative:
L1574641-01 WG1987054: 5.92 at19.9C
Wet Chemistry by Method D93/1010A
Result Qualifier
Dilution Analysis
Batch
Analyte Deg. F
date / time
Ignitability DNI at170
1 01/16/2023 0109 WG1989070
Mercury by Method 7470A
Result Qualifier
RDL Limit
Dilution
Analysis
Batch
Analyte mg/I
mg/I mg/I
date/time
Mercury ND
0.0100 0.20
1
01/13/2023 09:28
WG1987570
Metals (ICP) by Method 6010D
Result Qualifier
RDL Limit
Dilution
Analysis
Batch
Analyte mg/I
mg/I mg/I
date/time
Arsenic ND
0.100 5
1
01/12/2023 23:29
WG1987930
Barium 0.210
0.100 100
1
01/12/2023 23:29
WG1987930
Cadmium ND
0.100 1
1
01/12/2023 23:29
WG1987930
Chromium ND
0.100 5
1
01/12/2023 23:29
WG1987930
Lead ND
0.100 5
1
01/12/2023 23:29
WG1987930
Selenium ND
0.100 1
1
01/12/2023 23:29
WG1987930
Silver ND
0.100 5
1
01/12/2023 23:29
WG1987930
Volatile Organic Compounds (GC/MS) by Method 8260D
Result Qualifier
RDL Limit
Dilution
Analysis
Batch
Analyte mg/I
mg/I mg/I
date/time
Benzene ND
0.0500 0.50
1
01/12/202314:36
WG1987508
Carbon tetrachloride ND
0.0500 0.50
1
01/12/202314:36
WG1987508
Chlorobenzene ND
0.0500 100
1
01/12/202314:36
WG1987508
Chloroform ND
0.250 6
1
01/12/202314:36
WG1987508
ACCOUNT:
PROJECT:
SDG:
DATE/TIME:
PAGE:
EMA Resources
L1574641
01/19/23 12:12
5 of 23

PIEDMONT WATER
SAMPLE RESULTS
- 01
Collected date/time: 01/09/23 10:45
-1574641
Volatile Organic Compounds (GC/MS) by Method 8260D
Result
Qualifier RDL
Limit
Dilution
Analysis
Batch
Analyte
mg/I
mg/I
mg/I
date/time
1,2-Dichloroethane
ND
0.0500
0.50
1
01/12/202314:36
WG1987508
1,1-Dichloroethene
ND
0.0500
0.70
1
01/12/202314:36
WG1987508
2-Butanone (MEK)
ND
0.500
200
1
01/12/202314:36
WG1987508
Tetrachloroethene
ND
0.0500
0.70
1
01/12/202314:36
WG1987508
Trichloroethene
ND
0.0500
0.50
1
01/12/202314:36
WG1987508
Vinyl chloride
ND
0.0500
0.20
1
01/12/202314:36
WG1987508
Fn
(S) Toluene-dH
110
80.0-120
011121202314.36
WG1987508
(S) 4-Bromofluorobenzene
90.9
77.0-126
011121202314.36
WG1987508
(S) 1,2-Dichloroethane-d4
101
70.0-130
011121202314.36
WG1987508
Chlorinated Acid Herbicides (GC) by
Method 8151A
Result
Qualifier RDL
Limit
Dilution
Analysis
Batch
Analyte
mg/I
mg/I
mg/I
date/time
7G1
2,4,5-TP (Silvex)
ND
0.00200
1
1
01/18/202314:53
WG1988910
2,4-D
ND
0.00200
10
1
01/18/202314:53
WG1988910
(S)2,4-DichlorophenylAcetic Acid
89.0
14.0-158
011181202314.53
WG1988910
I u
Pesticides (GC) by Method 8081B
Sc
Result
Qualifier RDL
Limit
Dilution
Analysis
Batch
Analyte
mg/I
mg/I
mg/I
date/time
Chlordane
ND
0.00500
0.03
1
01/16/202315:27
WG1989109
Endrin
ND
0.00500
0.02
1
01/16/202315:27
WG1989109
Heptachlor
ND
0.00500
0.0080
1
01/16/202315:27
WG1989109
Heptachlor epoxide
ND
0.00500
0.0080
1
01/16/202315:27
WG1989109
Lindane
ND
0.00500
0.40
1
01/16/202315:27
WG1989109
Methoxychlor
ND
0.00500
10
1
01/16/202315:27
WG1989109
Toxaphene
ND
0.0100
0.50
1
01/16/202315:27
WG1989109
(S) Decochlorobiphenyl
63.5
10.0-128
011161202315.27
WG1989109
(S) Tetrochloro-m-xylene
73.6
10.0-127
011161202315.27
WG1989109
Semi Volatile Organic Compounds
(GC/MS) by Method 8270E
Result
Qualifier RDL
Limit
Dilution
Analysis
Batch
Analyte
mg/I
mg/I
mg/I
date/time
1,4-Dichlorobenzene
ND
0.100
7.50
1
01/13/202319:10
WG1985658
2,4-Dinitrotoluene
ND
0.100
0.13
1
01/13/202319:10
WG1985658
Hexachlorobenzene
ND
0.100
0.13
1
01/13/202319:10
WG1985658
Hexachloro-1,3-butadiene
ND
0.100
0.50
1
01/13/202319:10
WG1985658
Hexachloroethane
ND
0.100
3
1
01/13/202319:10
WG1985658
Nitrobenzene
ND
0.100
2
1
01/13/202319:10
WG1985658
Pyridine
ND
0.100
5
1
01/13/202319:10
WG1985658
3&4-Methyl Phenol
ND
0.100
400
1
01/13/202319:10
WG1985658
2-Methylphenol
ND
0.100
200
1
01/13/202319:10
WG1985658
Pentachlorophenol
ND
0.100
100
1
01/13/202319:10
WG1985658
2,4,5-Trichlorophenol
ND
0.100
400
1
01/13/202319:10
WG1985658
2,4,6-Trichlorophenol
ND
0.100
2
1
01/13/202319:10
WG1985658
(S) 2-Fluorophenol
42.4
10.0-120
011131202319.10
WG1985658
(S) Phenol-d5
24.5
10.0-120
011131202319.10
WG1985658
(S) Nitrobenzene-d5
75.8
10.0-127
011131202319.10
WG1985658
(S) 2-Fluorobiphenyl
79.1
10.0-130
011131202319.10
WG1985658
(S)2,4,6-Tribromophenol
84.5
10.0-155
011131202319.10
WG1985658
(S) p-Terphenyl-d14
89.2
10.0-128
011131202319.10
WG1985658
ACCOUNT:
PROJECT:
SDG:
DATE/TIME:
PAGE:
EMA Resources
L1574641
01/19/23 12:12
6 of 23

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GLOSSARY OF TERMS
Guide to Reading and Understanding Your Laboratory Report
The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not
intended as a comprehensive explanation, and ifyou have additional questions please contact your project representative.
Results Disclaimer - Information that may be provided by the customer, and contained within this report, include Permit Limits, Project Name,
Sample ID, Sample Matrix, Sample Preservation, Field Blanks, Field Spikes, Field Duplicates, On -Site Data, Sampling Collection Dates/Times, and
Sampling Location. Results relate to the accuracy of this information provided, and as the samples are received.
Abbreviations and Definitions
MDL
Method Detection Limit.
ND
Not detected at the Reporting Limit (or MDL where applicable).
RDL
Reported Detection Limit.
Rec.
Recovery.
RPD
Relative Percent Difference.
SDG
Sample Delivery Group.
Surrogate (Surrogate Standard) - Analytes added to every blank, sample, Laboratory Control Sample/Duplicate and
(S)
Matrix Spike/Duplicate; used to evaluate analytical efficiency by measuring recovery. Surrogates are not expected to be
detected in all environmental media.
U
Not detected at the Reporting Limit (or MDL where applicable).
Analyte
The name ofthe particular compound or analysis performed. Some Analyses and Methods will have multiple analytes
reported.
Ifthe sample matrix contains an interfering material, the sample preparation volume or weight values differ from the
Dilution
standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the
laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the
result reported has already been corrected for this factor.
These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal
Limits
for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or
duplicated within these ranges.
Original Sample
The non -spiked sample in the prep batch used to determine the Relative Percent Difference (RPD) from a quality control
sample. The Original Sample may not be included within the reported SDG.
This column provides a letter and/or number designation that corresponds to additional information concerning the result
Qualifier
reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and
potentially a discussion of possible implications ofthe Qualifier in the Case Narrative if applicable.
The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. Ifthere was
no measurable result returned for a specific analyte, the result in this column may state "ND" (Not Detected) or "BDL"
Result
(Below Detectable Levels). The information in the results column should always be accompanied by either an MDL
(Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect
or report for this analyte.
Uncertainty
(Radiochemistry)
Confidence level of 2 sigma.
A brief discussion about the included sample results, including a discussion of any non -conformances to protocol
Case Narrative (Cn)
observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will
be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report.
Quality Control
This section ofthe report includes the results ofthe laboratory quality control analyses required by procedure or
Summary (Qc)
analytical methods to assist in evaluating the validity ofthe results reported for your samples. These analyses are not
being performed on your samples typically, but on laboratory generated material.
This is the document created in the field when your samples were initially collected. This is used to verify the time and
Sample Chain of
date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This
Custody (Sc)
chain of custody also documents all persons (excluding commercial shippers) that have had control or possession ofthe
samples from the time of collection until delivery to the laboratory for analysis.
This section ofyour report will provide the results of all testing performed on your samples. These results are provided
Sample Results (Sr)
by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for
each sample will provide the name and method number for the analysis reported.
Sample Summary (Ss)
This section ofthe Analytical Report defines the specific analyses performed for each sample ID, including the dates and
times of preparation and/or analysis.
Qualifier
Description
J3
The associated batch QC was outside the established quality control range for precision.
J6
The sample matrix interfered with the ability to make any accurate determination, spike value is low.
T8
Sample(s) received past/too close to holding time expiration.
ACCOUNT:
PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources
L1574641 01/19/23 12:12 20 of 23

ACCREDITATIONS & LOCATIONS
!Ninl',71cl I\h ll+"inl l 12065 I cd it I+:+I""I
Alabama
40660
Nebraska
N E-OS-15-05
Alaska
17-026
Nevada
TN000032021-1
Arizona
AZ0612
New Hampshire
2975
Arkansas
88-0469
New Jersey—NELAP
TNO02
California
2932
New Mexico
TN00003
Colorado
TN00003
New York
11742
Connecticut
PH-0197
North Carolina
Env375
Florida
E87487
North Carolina'
DW21704
Georgia
NELAP
North Carolina 3
41
Georgia'
923
North Dakota
R-140
Idaho
TN00003
Ohio—VAP
CL0069
Illinois
200008
Oklahoma
9915
Indiana
C-TN-01
Oregon
TN200002
Iowa
364
Pennsylvania
68-02979
Kansas
E-10277
Rhode Island
LA000356
Kentucky' 6
KY90010
South Carolina
84004002
Kentucky 2
16
South Dakota
n/a
Louisiana
A130792
Tennessee' 4
2006
Louisiana
LA018
Texas
T104704245-20-18
Maine
TN00003
Texas5
LABO152
Maryland
324
Utah
TN000032021-11
Massachusetts
M-TNO03
Vermont
VT2006
Michigan
9958
Virginia
110033
Minnesota
047-999-395
Washington
C847
Mississippi
TN00003
West Virginia
233
Missouri
340
Wisconsin
998093910
Montana
CERT0086
Wyoming
A2 LA
A2LA— ISO 17025
1461.01
AIHA-LAP,LLC EMLAP
100789
A2 LA — ISO 17025 5
1461.02
DOD
1461.01
Canada
1461.01
USDA
P330-15-00234
EPA—Crypto
TN00003
Drinking Water 2 Underground Storage Tanks 3 Aquatic Toxicity "Chemical/Microbiological 5 Mold 6 Wastewater n/a Accreditation not applicable
Not all certifications held by the laboratory are applicable to the results reported in the attached report.
Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace Analytical.
ACCOUNT: PROJECT: SDG: DATE/TIME:
EMA Resources L1574641 01/19/23 12:12
PAGE:
21 of 23

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Brown WTP 1 /5/23
mg/kg mg/L Equiv Weight Milli Equiv
Sodium 268 57.62 23 2.505217
Calcium 1050 225.75 20 11.2875
Magnesium 278 59.77 12 4.980833
Percent Solids 21.5
SAR
9Y
SAR Na+
a (Ca2+ + M92+)
2.50522
'',::: 0.5( 11.288 2 + 4.98083 2 )

Brown WTP 4/11/23
mg/kg
mg/L Equiv Weight Milli Equiv
Sodium
378
90.72 23 3.944348
Calcium
1480
355.2 20 17.76
Magnesium
533
127.92 12 10.66
Percent Solids
24
SAR
1.05
SAR
Na+
a (Ca2+ + M92+)
3.94435
'',::: 0.5( 17.76 2 + 10.66000 2 )

Brown WTP 7/18/23
mg/kg mg/L Equiv Weight Milli Equiv
Sodium 327 65.073 23 2.829261
Calcium 990 197.01 20 9.8505
Magnesium 207 41.193 12 3.43275
Percent Solids 19.9
SAR
1.10
SAR Na+
a (Ca2+ + M92+)
2.82926
'',::: 0.5( 9.8505 2 + 3.43275 2 )

Brown WTP 10/5/23
mg/kg
mg/L
Equiv Weight Milli Equiv
Sodium
327
64.419
23 2.800826
Calcium
22100
4353.7
20 217.685
Magnesium
9700
1910.9
12 159.2417
Percent Solids
19.7
SAR
0.20
SAR
Na+
a (Ca2+ + M92+)
2.80083
'',::: 0.5( 217.69 2 + 159.24167 2 )

mil ,
1 /16/2023
EMA Resources Inc
Mr. Brent Collins
755 Yadkinville Rd
Mocksville, NC, 27028
Ref: Analytical Testing
Lab Report Number: 23-006-0005
Client Project Description: Durham, NC
Dear Mr. Brent Collins:
Waypoint Analytical, LLC. received sample(s) on 1/6/2023 for the analyses presented in the following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Where the laboratory was not responsible for the sampling
stage (refer to the chain of custody) results apply to the sample as received.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2021) and NELAC unless otherwise indicated. Any parameter
for which the laboratory is not officially NELAP accredited is indicated by a '—'symbol. These are not included in
the scope because NELAP accreditation is either not available or has not been applied for. Additional
certifications may be held/are available for parameters, where NELAP accreditation is not required or applicable.
A full list of certifications is available upon request.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Connie Cook
Project Manager
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 1 of 8

Way to
PM�
WRTIA"Wi
tMain 901.213.2400 0 Fax u f,
www.waypointanalyticaLcom
Certification Summary
Laboratory ID: WP MTN: Waypoint Analytical, LLC., Memphis, TN
State
Program
Lab ID
Expiration Date
Alabama
State Program
40750
02/28/2023
Arkansas
State Program
88-0650
02/07/2023
California
State Program
2904
06/30/2023
Florida
State Program
- NELAP
E871157
06/30/2023
Georgia
State Program
C044
02/18/2023
Georgia
State Program
04015
06/30/2023
Illinois
State Program
- NELAP
200078
10/10/2023
Kentucky
State Program
80215
06/30/2023
Kentucky
State Program
KY90047
12/31/2023
Louisiana
State Program
- NELAP
LA037
12/31/2023
Louisiana
State Program
- NELAP
04015
06/30/2023
Mississippi
State Program
MS
02/11/2023
North Carolina
State Program
47701
07/31/2023
North Carolina
State Program
415
12/31/2023
Pennsylvania
State Program
- NELAP
68-03195
05/31/2023
South Carolina
State Program
84002
06/30/2023
Tennessee
State Program
02027
02/11/2023
Texas
State Program
- NELAP
T104704180
09/30/2023
Virginia
State Program
00106
06/30/2023
Virginia
State Program
- NELAP
460181
09/14/2023
Page 1 of 1 00001/23-006-0005
Page 2 of 8

Way lht,(2)
PM�TICAL'
Sample Summary Table
Report Number: 23-006-0005
K]immt Project Description: Durham, NC
Lab No Client Sample zo Matrix Date Collected Date Received
90145 umwnwvp Solids 01/05/202308:15 01/00/2023
Page 3 of 8

to
Way� PA
► x
Client: EMA Resources Inc
Project: Durham, NC
Lab Report Number: 23-006-0005
Date: 1 /16/2023
Main 901.213.2400 .41
wwwmaypointanalyticaLcorn
CASE NARRATIVE
Block Digestion and FIA Method 4500NORGD-2011
QC Batch No: 1-657953/1-657591
Matrix spike recovery is outside of control limits. Acceptable LCS recovery indicates the system was in control,
but the reported result could be affected by matrix interference.
Metals Analysis Method 6010D
Sample 99364
Analyte: Aluminum
QC Batch No: 1-657906/1-657395
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 99364
Analyte: Calcium
QC Batch No: 1-657906/1-657395
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 99364
Analyte: Iron
QC Batch No: 1-657906/1-657395
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 99364
Analyte: Potassium
QC Batch No: 1-657906/1-657395
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 99364
Analyte: Manganese
QC Batch No: 1-657730/1-657395
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 99364
Analyte: Lead
QC Batch No: 1-657730/1-657395
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Page 4 of 8

Way to
PM�
46245
EMA Resources Inc
Mr. Brent Collins
755 Yadkinville Rd
Mocksville , NC 27028
Project Durham, NC
Information :
Report Date : 01/16/2023
Received �.�101/06/2023
-
Connie Cook
Report Number : 23-006-0005
REPORT OFANALYSIS
Project
Manager
Lab No : 90145
Matrix:
Solids
Sample ID: Brown WTP
Sampled:
1/5/2023
8:15
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Method
Moisture
78.5
%
1
01/06/2315:55
FMM
SW-DRYWT
Ammonia Nitrogen
856
mg/Kg -
dry
74.4
465
1
01/16/23 14:00
JPJ
4500NH3C-2011
Nitrate+Nitrite-N
<22.3
mg/Kg -
dry
22.3
22.3
1
01/13/23 14:25
ZBD
4500NO3F-2016
Organic N
6819
mg/Kg -
dry
576.7
1158
1
01/11/23 16:35
CALCULATION
pH
5.3
S.U.
1
01/13/2313:23
SAR
9045D
Total Solids
21.5
%
0.010
0.010
1
01/09/23 15:55
FMM
2540G-2011
Total Volatile Solids
33.5
%
0.010
0.010
1
01/09/23 15:55
FMM
2540G-2011
Total Kjeldahl Nitrogen
7670
mg/Kg -
dry
1160
1
01/11/23 16:35
ANH 4500NORGD-2011
Phosphorus
940
mg/Kg -
dry
12.8
23.3
1
01/09/23 20:33
TJS
6010D
Aluminum
5860
mg/Kg -
dry
21.5
23.3
1
01/09/23 20:33
TJS
6010D
Arsenic
<1.12
mg/Kg -
dry
1.12
2.33
1
01/09/23 20:33
TJS
6010D
Cadmium
11.5
mg/Kg -
dry
0.0930
0.465
1
01/09/23 20:33
TJS
6010D
Calcium
1050
mg/Kg -
dry
180
233
1
01/09/23 20:33
TJS
6010D
Chromium
14.3
mg/Kg -
dry
1.10
1.16
1
01/09/23 20:33
TJS
6010D
Copper
614
mg/Kg -
dry
1.44
2.33
1
01/09/23 20:33
TJS
6010D
Iron
390000
mg/Kg -
dry
396
465
10
01/10/23 20:58
TJS
6010D
Lead
9.58
mg/Kg -
dry
0.837
1.40
1
01/09/23 20:33
TJS
6010D
Magnesium
278
mg/Kg -
dry
12.0
23.3
1
01/09/23 20:33
TJS
6010D
Manganese
7630
mg/Kg -
dry
15.1
23.3
10
01/10/23 20:58
TJS
6010D
Mercury
0.04203
mg/Kg -
dry
0.0288
0.660
1
01/11/23 13:57
JTR
7471A
Molybdenum
2.37
mg/Kg -
dry
0.627
1.16
1
01/09/23 20:33
TJS
6010D
Nickel
82.3
mg/Kg -
dry
0.558
1.16
1
01/09/23 20:33
TJS
6010D
Potassium
238
mg/Kg -
dry
28.7
46.5
1
01/09/23 20:33
TJS
6010D
Qualifiers/ DF
Dilution Factor
J
Estimated value
Definitions MQL
Method Quantitation Limit
Page 5 of 8

0
Waypoeint790
Whitten
Road, Memphis, TN 38133
Main 901.213.2400 0 Fax [phone]
ANALYTICAL
www,waypoiintanalyticaLcom
46245
EMA Resources Inc
Project
Durham, NC
Mr. Brent Collins
Report Date : 01/16/2023
755 Yadkinville Rd
Information :
Received : 01/06/2023
Mocksville , NC 27028
Connie Cook
Report Number : 23-006-0005
REPORT OFANALYSIS
Project Manager
Lab No : 90145
Matrix: Solids
Sample ID: Brown WTP
Sampled: 1/5/2023 8:15
Test
Results
Units
MDL
MQL DF Date / Time By Analytical
Analyzed Method
Selenium
3.88
mg/Kg - dry
1.49
2.33 1 01/09/23 20:33 TJS 6010D
Sodium
268
mg/Kg - dry
60.5
116 1 01/09/23 20:33 TJS 6010D
Zinc
99.5
mg/Kg - dry
3.77
5.81 1 01/09/23 20:33 TJS 6010D
Sulfur
4790
mg/Kg - dry
24.1
46.5 1 01/09/23 20:33 TJS 6010D
Sodium Absorption Ratio
0.88
Ratio
0.01
0.01 1 01/09/23 20:33 CALCULATION
Qualifiers/ DF Dilution Factor
Definitions
J Estimated value
Page 6 of 8

l0
Waypoint",
J123.8224
Shipment Receipt Form
Customer Number: 46245
Customer Name: EMA Resources Inc
Report Number: 23-006-0005
Shipping Method
0 Fed Ex 0 US Postal 0 Lab
0 UPS 0 Client 0 Courier
0 Other
Thermometer ID:
T102
Shipping container/cooler uncompromised?
Yes
0 No
Number of coolers/boxes received
1
Custody seals intact on shipping container/cooler?
0 Yes
0 No
Not Present
Custody seals intact on sample bottles?
0 Yes
0 No
Not Present
Chain of Custody (COC) present?
# Yes
0 No
COC agrees with sample label(s)?
# Yes
0 No
COC properly completed
# Yes
0 No
Samples in proper containers?
# Yes
0 No
Sample containers intact?
# Yes
0 No
Sufficient sample volume for indicated test(s)?
# Yes
0 No
All samples received within holding time?
# Yes
0 No
Cooler temperature in compliance?
# Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
# Yes
0 No
Water - Sample containers properly preserved
0 Yes
0 No
N/A
Water - VOA vials free of headspace
0 Yes
0 No
N/A
Trip Blanks received with VOAs
0 Yes
0 No
N/A
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
0 N/A
F_ High concentration container (48 hr)
F_ High concentration pre -weighed (methanol -14 d)
F_ Low concentration EnCore samplers (48 hr)
F_ Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included? 0 Yes * No
Comments:
Signature: IMakayla Weaver Date & Time: 01/06/2023 10:57:42
Page 7 of 8

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Page 8 of 8

mil ,
4/20/2023
EMA Resources Inc
Mr. Brent Collins
755 Yadkinville Rd
Mocksville, NC, 27028
Ref: Analytical Testing
Lab Report Number: 23-102-0007
Client Project Description: Brown WTP
Dear Mr. Brent Collins:
Waypoint Analytical, LLC. received sample(s) on 4/12/2023 for the analyses presented in the following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Where the laboratory was not responsible for the sampling
stage (refer to the chain of custody) results apply to the sample as received.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2021) and NELAC unless otherwise indicated. Any parameter
for which the laboratory is not officially NELAP accredited is indicated by a '—'symbol. These are not included in
the scope because NELAP accreditation is either not available or has not been applied for. Additional
certifications may be held/are available for parameters, where NELAP accreditation is not required or applicable.
A full list of certifications is available upon request.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Connie Cook
Project Manager
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 1 of 9

Way to
PM�
WRTIA"Wi
tMain 901.213.2400 0 Fax u f,
www.waypointanalyticaLcom
Certification Summary
Laboratory ID: WP MTN: Waypoint Analytical, LLC., Memphis, TN
State
Program
Lab ID
Expiration Date
Alabama
State Program
40750
02/29/2024
Arkansas
State Program
88-0650
02/07/2024
California
State Program
2904
06/30/2023
Florida
State Program
- NELAP
E871157
06/30/2023
Georgia
State Program
C044
11/14/2025
Georgia
State Program
04015
06/30/2023
Illinois
State Program
- NELAP
200078
10/10/2023
Kentucky
State Program
80215
06/30/2023
Kentucky
State Program
KY90047
12/31/2023
Louisiana
State Program
- NELAP
LA037
12/31/2023
Louisiana
State Program
- NELAP
04015
06/30/2023
Mississippi
State Program
MS
11/14/2025
North Carolina
State Program
47701
07/31/2023
North Carolina
State Program
415
12/31/2023
Pennsylvania
State Program
- NELAP
68-03195
05/31/2024
South Carolina
State Program
84002
06/30/2023
Tennessee
State Program
02027
11/14/2025
Texas
State Program
- NELAP
T104704180
09/30/2023
Virginia
State Program
00106
06/30/2023
Virginia
State Program
- NELAP
460181
09/14/2023
Page 1 of 1 00001/23-102-0007
Page 2 of 9

Way lht,(2)
PM�TICAL'
Sample Summary Table
Report Number: 23-102-0007
Client Project Description: Brown WTP
Lab No Client Sample ID Matrix Date Collected Date Received
95461 Brown WFP Solids 04/11/2023 08:15 04/12/2023
Page 3 of 9

to
Way� PA
► x
Client: EMA Resources Inc
Project: Brown WTP
Lab Report Number: 23-102-0007
Date: 4/20/2023
Main 901.213.2400 .41
wwwmaypointanalyticaLcorn
CASE NARRATIVE
Block Digestion and FIA Method 4500NORGD-2011
Analyte: Total Kjeldahl Nitrogen
QC Batch No: 1-675945/1-675754
The MS recovery is outside QC limits due to the level of analyte present in the parent sample relative to the spike
level.
Metals Analysis Method 6010D
Sample 96083 (SS-2)
Analyte: Aluminum
QC Batch No: 1-676920/1-676041
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 95461 (Brown WTP)
Analyte: Arsenic
QC Batch No: 1-676414/1-676041
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Sample 96083 (SS-2)
Analyte: Iron
QC Batch No: 1-676920/1-676041
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 96083 (SS-2)
Analyte: Potassium
QC Batch No: 1-676920/1-676041
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Sample 96083 (SS-2)
Analyte: Manganese
QC Batch No: 1-676414/1-676041
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 96083 (SS-2)
Analyte: Lead
QC Batch No: 1-676414/1-676041
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Solids Total Mercury Analysis - CVAA Method 7471A
Sample 95708
Page 4 of 9

Way� to
PA
wwwmaypointanalyticaLcorn
Analyte:K8ercury
QCBatch No: LG7G255/LG7GO23
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. Nnmatrix interference is
suspected.
Page 5 of 9

Way to
PM�
46245
EMA Resources Inc
Mr. Brent Collins
755 Yadkinville Rd
Mocksville , NC 27028
Project Brown WTP
Information :
Report Date : 04/20/2023
Received �.���y04/12/2023
-
Connie Cook
Report Number : 23-102-0007
REPORT OFANALYSIS
Project
Manager
Lab No : 95461
Matrix:
Solids
Sample ID: Brown WTP
Sampled:
4/11/2023
8:15
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Method
Moisture
86.1
%
1
04/18/2316:10
JLS
SW-DRYWT
Ammonia Nitrogen
1000
mg/Kg -
dry
115
719
1
04/20/23 06:00
JPJ
4500NH3C-2011
Nitrate+Nitrite-N
<7.19
mg/Kg -
dry
7.19
36.0
1
04/18/23 13:23
ZBD
4500NO3F-2016
Organic N
12310
mg/Kg -
dry
492.1
992.8
1
04/13/23 13:23
CALCULATION
pH
5.0
S.U.
1
04/18/23 14:52
JJJ
9045D
Total Solids
24.0
%
0.010
0.010
1
04/17/23 15:25
JLS
2540G-2011
Total Kjeldahl Nitrogen
13300
mg/Kg -
dry
993
1
04/13/23 13:23
ANH 4500NORGD-2011
Phosphorus
1450
mg/Kg -
dry
19.9
36.0
1
04/15/23 07:31
BKN
6010D
Aluminum
13900
mg/Kg -
dry
33.2
36.0
1
04/15/23 07:31
BKN
6010D
Arsenic
<17.3
mg/Kg -
dry
17.3
36.0
10
04/18/23 18:50
BKN
6010D
Cadmium
20.6
mg/Kg -
dry
0.144
0.719
1
04/15/23 07:31
BKN
6010D
Calcium
1480
mg/Kg -
dry
278
360
1
04/15/23 07:31
BKN
6010D
Chromium
26.2
mg/Kg -
dry
1.70
1.80
1
04/15/23 07:31
BKN
6010D
Copper
386
mg/Kg -
dry
2.23
3.60
1
04/15/23 07:31
BKN
6010D
Iron
547000
mg/Kg -
dry
613
719
10
04/18/23 18:50
BKN
6010D
Lead
16.8
mg/Kg -
dry
1.29
2.16
1
04/15/23 07:31
BKN
6010D
Magnesium
533
mg/Kg -
dry
18.6
36.0
1
04/15/23 07:31
BKN
6010D
Manganese
4320
mg/Kg -
dry
23.4
36.0
10
04/18/23 18:50
BKN
6010D
Mercury
<0.155
mg/Kg -
dry
0.155
1.28
1
04/14/23 12:05
FDS
7471A
Molybdenum
3.32
mg/Kg -
dry
0.971
1.80
1
04/15/23 07:31
BKN
6010D
Nickel
40.1
mg/Kg -
dry
0.863
1.80
1
04/15/23 07:31
BKN
6010D
Potassium
458
mg/Kg -
dry
44.5
71.9
1
04/15/23 07:31
BKN
6010D
Selenium
24.5
mg/Kg -
dry
2.30
3.60
1
04/15/23 07:31
BKN
6010D
Qualifiers/ DF Dilution Factor
MQL
Method Quantitation Limit
Definitions
Page 6 of 9

0
Waypoeint2790
Whitten
Road, Memphis, TN 38133
Main 901.213.2400 0 Fax [phone]
ANALYTICAL
www.waypoiintanalyticaLcom
46245
EMA Resources Inc
Project
Brown WTP
Mr. Brent Collins
Report Date : 04/20/2023
755 Yadkinville Rd
Information :
Received : 04/12/2023
Mocksville , NC 27028
Connie Cook
Report Number : 23-102-0007
REPORT OFANALYSIS
Project Manager
Lab No : 95461
Matrix: Solids
Sample ID: Brown WTP
Sampled: 4/11/2023 8:15
Test
Results
Units
MDL
MQL DF Date / Time By Analytical
Analyzed Method
Sodium
378
mg/Kg - dry
93.5
180 1 04/15/23 07:31 BKN 6010D
Zinc
83.5
mg/Kg - dry
5.83
8.99 1 04/15/23 07:31 BKN 6010D
Sulfur
8490
mg/Kg - dry
37.3
71.9 1 04/15/23 07:31 BKN 6010D
Sodium Absorption Ratio
0.79
Ratio
0.01
0.01 1 04/15/23 07:31 CALCULATION
Qualifiers/ DF Dilution Factor
Definitions
MQL Method Quantitation Limit
Page 7 of 9

l0
Waypoint",
J123.8224
Shipment Receipt Form
Customer Number: 46245
Customer Name: EMA Resources Inc
Report Number: 23-102-0007
Shipping Method
0 Fed Ex 0 US Postal 0 Lab
0 UPS 0 Client 0 Courier
0 Other
Thermometer ID:
T135
Shipping container/cooler uncompromised?
Yes
0 No
Number of coolers/boxes received
1
Custody seals intact on shipping container/cooler?
0 Yes
0 No
Not Present
Custody seals intact on sample bottles?
0 Yes
0 No
Not Present
Chain of Custody (COC) present?
# Yes
0 No
COC agrees with sample label(s)?
# Yes
0 No
COC properly completed
# Yes
0 No
Samples in proper containers?
# Yes
0 No
Sample containers intact?
# Yes
0 No
Sufficient sample volume for indicated test(s)?
# Yes
0 No
All samples received within holding time?
# Yes
0 No
Cooler temperature in compliance?
# Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
# Yes
0 No
Water - Sample containers properly preserved
0 Yes
0 No
N/A
Water - VOA vials free of headspace
0 Yes
0 No
N/A
Trip Blanks received with VOAs
0 Yes
0 No
N/A
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
0 N/A
F_ High concentration container (48 hr)
F_ High concentration pre -weighed (methanol -14 d)
F_ Low concentration EnCore samplers (48 hr)
F_ Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included? 0 Yes * No
Comments:
Signature: ICarleen Qualls Date & Time: 04/12/2023 09:00:26
Page 8 of 9

Page 9 of 9

mil ,
8/2/2023
EMA Resources Inc
Mr. Brent Collins
755 Yadkinville Rd
Mocksville, NC, 27028
Ref: Analytical Testing
Lab Report Number: 23-200-0015
Client Project Description: Brown WTP
Dear Mr. Brent Collins:
Waypoint Analytical, LLC. received sample(s) on 7/19/2023 for the analyses presented in the following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Where the laboratory was not responsible for the sampling
stage (refer to the chain of custody) results apply to the sample as received.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2021) and NELAC unless otherwise indicated. Any parameter
for which the laboratory is not officially NELAP accredited is indicated by a '—'symbol. These are not included in
the scope because NELAP accreditation is either not available or has not been applied for. Additional
certifications may be held/are available for parameters, where NELAP accreditation is not required or applicable.
A full list of certifications is available upon request.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Connie Cook
Project Manager
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 1 of 9

Way to
PM�
WRTIA"Wi
tMain 901.213.2400 0 Fax u f,
www.waypointanalyticaLcom
Certification Summary
Laboratory ID: WP MTN: Waypoint Analytical, LLC., Memphis, TN
State
Program
Lab ID
Expiration Date
Alabama
State Program
40750
02/29/2024
Arkansas
State Program
88-0650
02/07/2024
California
State Program
2904
06/30/2024
Florida
State Program
- NELAP
E871157
06/30/2024
Georgia
State Program
C044
11/14/2025
Georgia
State Program
04015
06/30/2024
Illinois
State Program
- NELAP
200078
10/10/2023
Kentucky
State Program
80215
06/30/2024
Kentucky
State Program
KY90047
12/31/2023
Louisiana
State Program
- NELAP
LA037
12/31/2023
Louisiana
State Program
- NELAP
04015
06/30/2024
Mississippi
State Program
MS
11/14/2025
North Carolina
State Program
47701
07/31/2024
North Carolina
State Program
415
12/31/2023
Pennsylvania
State Program
- NELAP
68-03195
05/31/2024
South Carolina
State Program
84002
06/30/2023
Tennessee
State Program
02027
11/14/2025
Texas
State Program
- NELAP
T104704180
09/30/2023
Virginia
State Program
00106
06/30/2024
Virginia
State Program
- NELAP
460181
09/14/2023
Page 1 of 1 00001/23-200-0015
Page 2 of 9

Way lht,(2)
PM�TICAL'
Sample Summary Table
Report Number: 23-200-0015
Client Project Description: Brown WTP
Lab No Client Sample ID Matrix Date Collected Date Received
82401 Brown WFP Solids 07/18/2023 10:30 07/19/2023
Page 3 of 9

to
Way� PA
► x
Client: EMA Resources Inc
Project: Brown WTP
Lab Report Number: 23-200-0015
Date: 8/2/2023
Main 901.213.2400 .41
wwwmaypointanalyticaLcorn
CASE NARRATIVE
Block Digestion and FIA Method 4500NORGD-2011
Analyte: Total Kjeldahl Nitrogen
QC Batch No: L694182/L694149
The MS recovery is outside QC limits due to the level of analyte present in the parent sample relative to the spike
level.
Metals Analysis Method 6010D
Sample 82652
QC Batch No: L694427/L694031
One or more Internal Standards are outside method acceptance criteria. Re -analysis and/or sample dilutions are
required.
Sample 82652
Analyte: Aluminum
QC Batch No: L694693/L694031
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 82652
Analyte: Arsenic
QC Batch No: L694693/L694031
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Sample 82652
Analyte: Iron
QC Batch No: L694693/L694031
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 82652
Analyte: Potassium
QC Batch No: L694693/L694031
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Sample 82652
Analyte: Magnesium
QC Batch No: L694693/L694031
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 82652
Page 4 of 9

to
Way� PA
► x
Main 901.213.2400 .41
wwwmaypointanalyticaLcorn
Analyte: Manganese
QC Batch No: 1-694693/1-694031
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Sample 82652
Analyte: Phosphorus
QC Batch No: 1-694693/1-694031
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Sample 82652
Analyte: Lead
QC Batch No: 1-694693/1-694031
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Page 5 of 9

Way to
PM�
46245
EMA Resources Inc
Mr. Brent Collins
755 Yadkinville Rd
Mocksville , NC 27028
Project Brown WTP
Information :
Report Date : 08/02/2023
Received �.���y07/19/2023
-
Connie Cook
Report Number : 23-200-0015
REPORT OFANALYSIS
Project
Manager
Lab No : 82401
Matrix:
Solids
Sample ID: Brown WTP
Sampled:
7/18/2023
10:30
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Method
Moisture
80.1
%
1
07/24/2317:31
KDO
SW-DRYWT
Ammonia Nitrogen
3923
mg/Kg -
dry
80.4
503
1
08/02/23 13:00
JPJ
4500NH3C-2011
Nitrate+Nitrite-N
<5.03
mg/Kg -
dry
5.03
25.1
1
07/24/23 14:36
CLP
4500NO3F-2016
Organic N
86533
mg/Kg -
dry
643.2
1302
1
07/21/23 15:30
CALCULATION
pH
5.1
S.U.
1
07/25/2314:55
CNB
9045D
Total Solids
19.9
%
0.010
0.010
1
07/24/23 17:31
KDO
2540G-2011
Total Kjeldahl Nitrogen
9050
mg/Kg -
dry
1300
1
07/21/23 15:30
ANH 4500NORGD-2011
Phosphorus
769
mg/Kg -
dry
70.4
126
5
07/24/23 22:08
JTR
6010D
Aluminum
4900
mg/Kg -
dry
117
126
5
07/24/23 22:08
JTR
6010D
Arsenic
<6.28
mg/Kg -
dry
6.28
12.6
5
07/24/23 22:08
JTR
6010D
Cadmium
2.86
mg/Kg -
dry
1.26
2.51
5
07/24/23 22:08
JTR
6010D
Calcium
9903
mg/Kg -
dry
975
1260
5
07/24/23 22:08
JTR
6010D
Chromium
21.4
mg/Kg -
dry
6.28
6.28
5
07/24/23 22:08
JTR
6010D
Copper
1690
mg/Kg -
dry
7.54
12.6
5
07/24/23 22:08
JTR
6010D
Iron
330000
mg/Kg -
dry
430
503
10
07/24/23 22:13
JTR
6010D
Lead
<10.1
mg/Kg -
dry
10.1
15.1
10
07/24/23 22:13
JTR
6010D
Magnesium
207
mg/Kg -
dry
65.3
126
5
07/24/23 22:08
JTR
6010D
Manganese
6680
mg/Kg -
dry
8.79
12.6
5
07/24/23 22:08
JTR
6010D
Mercury
<0.116
mg/Kg -
dry
0.116
0.960
1
07/21/23 16:16
FDS
7471A
Molybdenum
6.93
mg/Kg -
dry
3.77
6.28
5
07/24/23 22:08
JTR
6010D
Nickel
77.4
mg/Kg -
dry
3.77
6.28
5
07/24/23 22:08
JTR
6010D
Potassium
<156
mg/Kg -
dry
156
251
5
07/24/23 22:08
JTR
6010D
Selenium
<17.6
mg/Kg -
dry
17.6
25.1
10
07/24/23 22:13
JTR
6010D
Qualifiers/ DF
Dilution Factor
J
Estimated value
Definitions MQL
Method Quantitation Limit
Page 6 of 9

0
Waypoeint790
Whitten
Road, Memphis, TN 38133
Main 901.213.2400 0 Fax [phone]
ANALYTICAL
www.waypoiintanalyticaLcom
46245
EMA Resources Inc
Project
Brown WTP
Mr. Brent Collins
Report Date : 08/02/2023
755 Yadkinville Rd
Information :
Received : 07/19/2023
Mocksville , NC 27028
Connie Cook
Report Number : 23-200-0015
REPORT OFANALYSIS
Project Manager
Lab No : 82401
Matrix: Solids
Sample ID: Brown WTP
Sampled: 7/18/2023 10:30
Test
Results
Units
MDL
MQL DF Date / Time By Analytical
Analyzed Method
Sodium
<327
mg/Kg - dry
327
628 5 07/24/23 22:08 JTR 6010D
Zinc
50.3
mg/Kg - dry
21.4
31.4 5 07/24/23 22:08 JTR 6010D
Sulfur
3140
mg/Kg - dry
131
251 5 07/24/23 22:08 JTR 6010D
Sodium Absorption Ratio
<0.01
Ratio
0.01
0.01 5 07/24/23 22:08 CALCULATION
Qualifiers/ DF Dilution Factor
Definitions MQL Method Quantitation Limit
J Estimated value
Page 7 of 9

l0
Waypoint",
J123.8224
Shipment Receipt Form
Customer Number: 46245
Customer Name: EMA Resources Inc
Report Number: 23-200-0015
Shipping Method
0 Fed Ex 0 US Postal 0 Lab
0 UPS 0 Client 0 Courier
0 Other
Thermometer ID:
T135
Shipping container/cooler uncompromised?
Yes
0 No
Number of coolers/boxes received
1
Custody seals intact on shipping container/cooler?
0 Yes
0 No
Not Present
Custody seals intact on sample bottles?
0 Yes
0 No
Not Present
Chain of Custody (COC) present?
# Yes
0 No
COC agrees with sample label(s)?
# Yes
0 No
COC properly completed
# Yes
0 No
Samples in proper containers?
# Yes
0 No
Sample containers intact?
# Yes
0 No
Sufficient sample volume for indicated test(s)?
# Yes
0 No
All samples received within holding time?
# Yes
0 No
Cooler temperature in compliance?
# Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
# Yes
0 No
Water - Sample containers properly preserved
0 Yes
0 No
N/A
Water - VOA vials free of headspace
0 Yes
0 No
N/A
Trip Blanks received with VOAs
0 Yes
0 No
N/A
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
0 N/A
F_ High concentration container (48 hr)
F_ High concentration pre -weighed (methanol -14 d)
F_ Low concentration EnCore samplers (48 hr)
F_ Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included? 0 Yes * No
Comments:
Signature: IMakayla Weaver Date & Time: 07/19/2023 10:40:37
Page 8 of 9

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Page 9 of 9

mil ,
10/18/2023
EMA Resources Inc
Mr. Brent Collins
755 Yadkinville Rd
Mocksville, NC, 27028
Ref: Analytical Testing
Lab Report Number: 23-279-0052
Client Project Description: Brown WTP
Dear Mr. Brent Collins:
Waypoint Analytical, LLC. received sample(s) on 10/6/2023 for the analyses presented in the following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Where the laboratory was not responsible for the sampling
stage (refer to the chain of custody) results apply to the sample as received.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2021) and NELAC unless otherwise indicated. Any parameter
for which the laboratory is not officially NELAP accredited is indicated by a '—'symbol. These are not included in
the scope because NELAP accreditation is either not available or has not been applied for. Additional
certifications may be held/are available for parameters, where NELAP accreditation is not required or applicable.
A full list of certifications is available upon request.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Connie Cook
Project Manager
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 1 of 11

Way to
PM�
WRTIA"Wi
tMain 901.213.2400 0 Fax u f,
www.waypointanalyticaLcom
Certification Summary
Laboratory ID: WP MTN: Waypoint Analytical, LLC., Memphis, TN
State
Program
Lab ID
Expiration Date
Alabama
State Program
40750
02/29/2024
Arkansas
State Program
88-0650
02/07/2024
California
State Program
2904
06/30/2024
Florida
State Program
- NELAP
E871157
06/30/2024
Georgia
State Program
C044
11/14/2025
Georgia
State Program
04015
06/30/2024
Illinois
State Program
- NELAP
200078
10/31/2024
Kentucky
State Program
80215
06/30/2024
Kentucky
State Program
KY90047
12/31/2023
Louisiana
State Program
- NELAP
LA037
12/31/2023
Louisiana
State Program
- NELAP
04015
06/30/2024
Mississippi
State Program
MS
11/14/2025
North Carolina
State Program
47701
07/31/2024
North Carolina
State Program
415
12/31/2023
Pennsylvania
State Program
- NELAP
68-03195
05/31/2024
South Carolina
State Program
84002
06/30/2024
Tennessee
State Program
02027
11/14/2025
Texas
State Program
- NELAP
T104704180
09/30/2024
Virginia
State Program
00106
06/30/2024
Virginia
State Program
- NELAP
460181
09/14/2024
Page 1 of 1 00001/23-279-0052
Page 2 of 11

Way lht,(2)
PM�TICAL'
Sample Summary Table
Report Number: 23-279-0052
Client Project Description: Brown WTP
Lab No Client Sample ID Matrix Date Collected Date Received
99272 Brown WFP Solids 10/05/2023 12:00 10/06/2023
Page 3 of 11

to
Way� PA
► x
Client: EMA Resources Inc
Project: Brown WTP
Lab Report Number: 23-279-0052
Date: 10/18/2023
Main 901.213.2400 .41
wwwmaypointanalyticaLcorn
CASE NARRATIVE
Metals Analysis Method 601 OD
Sample 81146 (Land Applied Sludge)
Analyte: Aluminum
QC Batch No: 1-710015/1-709635
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Sample 81146 (Land Applied Sludge)
Analyte: Arsenic
QC Batch No: 1-710015/1-709635
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Sample 81146 (Land Applied Sludge)
Analyte: Arsenic
QC Batch No: 1-710352/1-709635
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Sample 81146 (Land Applied Sludge)
Analyte: Calcium
QC Batch No: 1-710015/1-709635
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Sample 81146 (Land Applied Sludge)
Analyte: Cadmium
QC Batch No: 1-710015/1-709635
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Sample 81146 (Land Applied Sludge)
Analyte: Cadmium
QC Batch No: 1-710352/1-709635
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Sample 81146 (Land Applied Sludge)
Analyte: Chromium
QC Batch No: 1-710015/1-709635
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Sample 81146 (Land Applied Sludge)
Analyte: Chromium
QC Batch No: 1-710352/1-709635
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Page 4 of 11

to
Way� PA
► x
Main 901.213.2400 .41
wwwmaypointanalyticaLcorn
Sample 81146 (Land Applied Sludge)
Analyte: Copper
QC Batch No: 1-710015/1-709635
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Sample 81146 (Land Applied Sludge)
Analyte: Copper
QC Batch No: 1-710352/1-709635
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 81146 (Land Applied Sludge)
Analyte: Iron
QC Batch No: 1-710015/1-709635
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Sample 81146 (Land Applied Sludge)
Analyte: Iron
QC Batch No: 1-710352/1-709635
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 81146 (Land Applied Sludge)
Analyte: Potassium
QC Batch No: 1-710015/1-709635
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Sample 81146 (Land Applied Sludge)
Analyte: Potassium
QC Batch No: 1-710352/1-709635
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Sample 81146 (Land Applied Sludge)
Analyte: Magnesium
QC Batch No: 1-710015/1-709635
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Sample 81146 (Land Applied Sludge)
Analyte: Manganese
QC Batch No: 1-710015/1-709635
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Sample 81146 (Land Applied Sludge)
Analyte: Manganese
QC Batch No: 1-710352/1-709635
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 81146 (Land Applied Sludge)
Analyte: Molybdenum
Page 5 of 11

to
Way� PA
► x
Main 901.213.2400 .41
wwwmaypointanalyticaLcorn
QC Batch No: 1-710015/1-709635
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Sample 81146 (Land Applied Sludge)
Analyte: Molybdenum
QC Batch No: 1-710352/1-709635
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 81146 (Land Applied Sludge)
Analyte: Sodium
QC Batch No: 1-710015/1-709635
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Sample 81146 (Land Applied Sludge)
Analyte: Sodium
QC Batch No: 1-710352/1-709635
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Sample 81146 (Land Applied Sludge)
Analyte: Nickel
QC Batch No: 1-710015/1-709635
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Sample 81146 (Land Applied Sludge)
Analyte: Nickel
QC Batch No: 1-710352/1-709635
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 81146 (Land Applied Sludge)
Analyte: Phosphorus
QC Batch No: 1-710015/1-709635
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Sample 81146 (Land Applied Sludge)
Analyte: Lead
QC Batch No: 1-710015/1-709635
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Sample 81146 (Land Applied Sludge)
Analyte: Lead
QC Batch No: 1-710352/1-709635
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Sample 81146 (Land Applied Sludge)
Analyte: Sulfur
QC Batch No: 1-710015/1-709635
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Page 6 of 11

to
Way� PA
► x
Main 901.213.2400 .41
wwwmaypointanalyticaLcorn
Sample 81146 (Land Applied Sludge)
Analyte: Selenium
QC Batch No: 1-710015/1-709635
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Sample 81146 (Land Applied Sludge)
Analyte: Selenium
QC Batch No: 1-710352/1-709635
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Sample 81146 (Land Applied Sludge)
Analyte: Zinc
QC Batch No: 1-710015/1-709635
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Sample 81146 (Land Applied Sludge)
Analyte: Zinc
QC Batch No: 1-710352/1-709635
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Page 7 of 11

Way to
PM�
46245
EMA Resources Inc
Mr. Brent Collins
755 Yadkinville Rd
Mocksville , NC 27028
Project Brown WTP
Information :
Report Date : 10/18/2023
Received 1��0yy/06/2023
�.�-
Connie Cook
Report Number : 23-279-0052
REPORT OFANALYSIS
Project
Manager
Lab No : 99272
Matrix:
Solids
Sample ID: Brown WTP
Sampled:
10/5/2023
12:00
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Method
Moisture
80.3
%
1
10/06/2316:00
CAH
SW-DRYWT
Ammonia Nitrogen
2263
mg/Kg -
dry
81.2
508
1
10/18/23 14:37
JPJ
4500NH3C-2011
Nitrate+Nitrite-N
<5.08
mg/Kg -
dry
5.08
25.4
1
10/11/23 15:34
CLP
4500NO3F-2016
Organic N
102803
mg/Kg -
dry
634.5
1284
1
10/10/23 15:16
CALCULATION
pH
5.5
S.U.
1
10/10/2316:44
CNB
9045D
Total Solids
19.7
%
0.010
0.010
1
10/06/23 16:00
CAH
2540G-2011
Total Kjeldahl Nitrogen
10500
mg/Kg -
dry
1280
1
10/10/23 15:16
ANH 4500NORGD-2011
Phosphorus
3620
mg/Kg -
dry
14.2
25.4
1
10/10/23 18:05
TJS
6010D
Aluminum
32800
mg/Kg -
dry
23.6
25.4
1
10/10/23 18:05
TJS
6010D
Arsenic
14.5
mg/Kg -
dry
1.27
2.54
1
10/10/23 18:05
TJS
6010D
Cadmium
1.36
mg/Kg -
dry
0.254
0.508
1
10/10/23 18:05
TJS
6010D
Calcium
22100
mg/Kg -
dry
196
254
1
10/10/23 18:05
TJS
6010D
Chromium
39.9
mg/Kg -
dry
1.27
1.27
1
10/10/23 18:05
TJS
6010D
Copper
80.2
mg/Kg -
dry
1.52
2.54
1
10/10/23 18:05
TJS
6010D
Iron
42700
mg/Kg -
dry
43.4
50.8
1
10/10/23 18:05
TJS
6010D
Lead
97.0
mg/Kg -
dry
1.02
1.52
1
10/10/23 18:05
TJS
6010D
Magnesium
9700
mg/Kg -
dry
13.2
25.4
1
10/10/23 18:05
TJS
6010D
Manganese
1620
mg/Kg -
dry
1.78
2.54
1
10/10/23 18:05
TJS
6010D
Mercury
<0.102
mg/Kg -
dry
0.102
0.848
1
10/10/23 12:01
MRE
7471A
Molybdenum
1.80
mg/Kg -
dry
0.761
1.27
1
10/10/23 18:05
TJS
6010D
Nickel
35.0
mg/Kg -
dry
0.761
1.27
1
10/10/23 18:05
TJS
6010D
Potassium
3210
mg/Kg -
dry
31.5
50.8
1
10/10/23 18:05
TJS
6010D
Selenium
<2.54
mg/Kg -
dry
1.78
2.54
1
10/10/23 18:05
TJS
6010D
Qualifiers/ DF
Dilution Factor
J
Estimated value
Definitions MQL
Method Quantitation Limit
Page 8 of 11

0
Waypoeint2790
Whitten
Road, Memphis, TN 38133
Main 901.213.2400 0 Fax [phone]
ANALYTICAL
www.waypoiintanalyticaLcom
46245
EMA Resources Inc
Project
Brown WTP
Mr. Brent Collins
Report Date : 10/18/2023
755 Yadkinville Rd
Information :
Received : 10/06/2023
Mocksville , NC 27028
Connie Cook
Report Number : 23-279-0052
REPORT OFANALYSIS
Project Manager
Lab No : 99272
Matrix: Solids
Sample ID: Brown WTP
Sampled: 10/5/2023 12:00
Test
Results
Units
MDL
MQL DF Date / Time By Analytical
Analyzed Method
Sodium
327
mg/Kg - dry
66.0
127 1 10/10/23 18:05 TJS 6010D
Zinc
234
mg/Kg - dry
4.31
6.35 1 10/10/23 18:05 TJS 6010D
Sulfur
2080
mg/Kg - dry
26.4
50.8 1 10/10/23 18:05 TJS 6010D
Sodium Absorption Ratio
0.20
Ratio
0.01
0.01 1 10/10/23 18:05 CALCULATION
Qualifiers/ DF Dilution Factor
Definitions MQL Method Quantitation Limit
J Estimated value
Page 9 of 11

l0
Waypoint",
J123.8224
Shipment Receipt Form
Customer Number: 46245
Customer Name: EMA Resources Inc
Report Number: 23-279-0052
Shipping Method
0 Fed Ex 0 US Postal 0 Lab
0 UPS 0 Client 0 Courier
0 Other
Thermometer ID:
T100
Shipping container/cooler uncompromised?
Yes
0 No
Number of coolers/boxes received
1
Custody seals intact on shipping container/cooler?
0 Yes
0 No
Not Present
Custody seals intact on sample bottles?
0 Yes
0 No
Not Present
Chain of Custody (COC) present?
# Yes
0 No
COC agrees with sample label(s)?
# Yes
0 No
COC properly completed
# Yes
0 No
Samples in proper containers?
# Yes
0 No
Sample containers intact?
# Yes
0 No
Sufficient sample volume for indicated test(s)?
# Yes
0 No
All samples received within holding time?
# Yes
0 No
Cooler temperature in compliance?
# Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
# Yes
0 No
Water - Sample containers properly preserved
0 Yes
0 No
N/A
Water - VOA vials free of headspace
0 Yes
0 No
N/A
Trip Blanks received with VOAs
0 Yes
0 No
N/A
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
0 N/A
F_ High concentration container (48 hr)
F_ High concentration pre -weighed (methanol -14 d)
F_ Low concentration EnCore samplers (48 hr)
F_ Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included? 0 Yes * No
Comments:
Signature: ICarleen Qualls Date & Time: 10/06/2023 10:45:59
Page 10 of 11

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Page 11 of 11

(� aceAnalytical ° ANALYTICAL REPORT
January 31, 2023
EMA Resources
Sample Delivery Group: L1577759
Samples Received: 01/20/2023
Project Number:
Description: Sludge
Report To: Mr. Brent Collins
755 Yadkinville Road
Mocksville, NC 27028
Entire Report Reviewed By:
�w
1`l1�
Cassandra Foster
Project Manager
Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be
reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pace
Analytical National is performed per guidance provided in laboratory standard operating procedures ENV-SOP-MTJL-0067and
ENV-SOP-MTJL-0068. Where sampling conducted by the customer, results relate to the accuracy ofthe information provided,
and as the samples are received.
%yp
[Cn
�'Sr
Sc
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1577759 01/31/23 13:10 1 of 21

TABLE OF CONTENTS
i� . c il M")fle' of Coil
Ss: Sample Summary
Cn: Case Narrative
Sr: Sample Results
BROWN WTP L1577759-01
oc ouaHb ( �, t �� r�
,It .'Orl 11 0 a I � I I a 11 ),It
Wet ( Iheinn�stii ),It 'n't Meflhod 9012 IkIIR
Wet ( Iheinn�stii ),It 'n't IlMehll od 903A1...90301113
Wet ( Iheinnistii ),It :n't IlMeh 11 od 9G�15':�')
Wet ( Ih1einu,.o stii ),It :n't Meflhod ':�'�)93/1010A
Meii 4: 1 u I )t w Meflhd 7A170A
M et a s fl :n't Meflhod
11111(datflie Oil gaink binniq!)Ourlds (G( AMS) 'n't Ilan eflhod 82(150l)
I II 0 1 firlated AcA Ieii 'Addes (G( IIDw,a Meflhod 8151A
Iesflddes (G( IIDw,a Mietlhod 808"V:1113
Serninii 1111datflie Oil gaink a 011,11niq!)ourids (G( PMS) 'n't IlMehllood 82'M:��
GI: Glossary of Terms
AL AccriedftatJoins & d"e'.atJoris
Sc: Sample Chain of Custody
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1577759 01/31/23 13:10 2 of 21

SAMPLE SUMMARY
Collected by
Collected date/time
Received date/time
BROWN WIT 1 1577759-01 Waste
Brent Collins
01/19/23 10 00
01120123 09 00
.............................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................
Method
Batch
Dilution Preparation
Analysis
Analyst
Location
date/time
date/time
Preparation by Method 1311
WG1991870
1 01/21/23 15 06
01/21/23 15 06
_WS
Mt. Juliet, TN
Preparation by Method 1311
WG1992825
1 01/23/23 14 13
01/23/23 14 13
JTM
Mt. Juliet, TN
Wet Chemistry by Method 9012 B
WG1992325
1 01/23/23 19 20
01/24/23 00 11
LDT
Mt. Juliet, TN
Wet Chemistry by Method 9034-9030B
WG1993877
1 01/25/23 12 05
01/28/23 03 42
RCD
Mt. Juliet, TN
Wet Chemistry by Method 9045D
WG1992209
1 01/20/23 15 00
01/20/23 17 28
KAD
Mt. Juliet, TN
Wet Chemistry by Method D93/1010A
WG1992863
1 01/23/23 02 41
01/23/23 02 41
CRB
Mt. Juliet, TN
Mercury by Method 7470A
WG1992813
1 01/22/23 16 10
01/23/23 10 44
SRT
Mt. Juliet, TN
Metals (ICP) by Method 6010D
WG1992947
1 01/23/23 08 05
01/23/23 14 33
SPL
Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260D
WG1994068
1 01/25/23 14 10
01/25/23 1410
JHH
Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260D
WG1994068
1 01/26/23 16 18
01/26/23 16 18
ACG
Mt. Juliet, TN
Chlorinated Acid Herbicides (GC) by Method 8151A
WG1996036
1 01/28/23 10 17
01/30/23 16 00
AMM
Mt. Juliet, TN
Pesticides (GC) by Method 8081B
WG1992848
1 01/23/23 08 02
01/23/23 17 19
-MB
Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
WG1992847
1 01/23/23 06 15
01/23/23 17 59
HLA
Mt. Juliet, TN
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1577759 01/31/23 13:10 3 of 21

CASE NARRATIVE
All sample aliquots were received at the correct temperature, in the proper containers, with the
appropriate preservatives, and within method specified holding times, unless qualified or notated within
the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples
have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control
are within established criteria except where addressed in this case narrative, a non-conformance form
or properly qualified within the sample results. By my digital signature below, I affirm to the best of my
knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the
.......................
quality of the data have been identified by the laboratory, and no information or data have been
knowingly withheld that would affect the quality of the data.
Sr
Cassandra Foster
Project Manager
�
Project Narrative L
All Reactive Cyanide results reported in the attached report were determined as totals using method 9012 B.
All Reactive Sulfide results reported in the attached report were determined as totals using method 9034-903013.
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1577759 01/31/23 13:10 4 of 21

BROWN WTP
Collected date/time: 01/19/23 10:00
Preparation by Method 1311
Result
Analyte
TCLP Extraction
TCLP ZHE Extraction -
Fluid 1
Initial pH 5.24
Final pH 4.95
Wet Chemistry by Method 9012 6
Result
SAMPLE RESULTS - 01
L1577759
Qualifier Prep
Batch
date / time
1/21/2023 3:06:36 PM
WG1991870
1/23/2023 2:13:05 PM
WG1992825
1/21/2023 3:06:36 PM
WG1991870
1/21/2023 3:06:36 PM
WG1991870
1/21/2023 3:06:36 PM
WG1991870
Qualifier RDL
Analyte mg/kg
mg/kg
Reactive Cyanide 0.603
0.250
Wet Chemistry by Method 9034-9030B
Result Qualifier
RDL
Analyte mg/kg
mg/kg
Reactive Sulfide ND J6
75.0
Wet Chemistry by Method 9045D
Dilution Analysis Batch
date / time
1 01/24/2023 00:11 WG1992325
Dilution Analysis Batch
date / time
1 01/28/2023 03:42 WG1993877
Result Qualifier Dilution Analysis Batch
Analyte su date / time
Corrosivity by pH 5.54 TC 1 01/20/202317:28 WG1992209
Sample Narrative:
L1577759-01 WG1992209: 5.54 at19.6C
Wet Chemistry by Method D93/1010A
Result
Qualifier
Dilution
Analysis
Batch
Analyte Deg. F
date / time
Ignitability DNI at170
1
01/23/2023 02:41
WG1992863
Mercury by Method 7470A
Result
Qualifier
RDL
Limit
Dilution Analysis
Batch
Analyte mg/I
mg/I
mg/I
date/time
Mercury ND
0.0100
0.20
1 01/23/202310:44
WG1992813
Metals (ICP) by Method 6010D
Result
Qualifier
RDL
Limit
Dilution Analysis
Batch
Analyte mg/I
mg/I
mg/I
date/time
Arsenic ND
0.100
5
1 01/23/202314:33
WG1992947
Barium 0.198
0.100
100
1 01/23/202314:33
WG1992947
Cadmium ND
0.100
1
1 01/23/202314:33
WG1992947
Chromium ND
0.100
5
1 01/23/202314:33
WG1992947
Lead ND
0.100
5
1 01/23/202314:33
WG1992947
Selenium ND
0.100
1
1 01/23/202314:33
WG1992947
Silver ND
0.100
5
1 01/23/202314:33
WG1992947
Volatile Organic Compounds (GC/MS) by Method
8260D
Result
Qualifier
RDL
Limit
Dilution Analysis
Batch
Analyte mg/I
mg/I
mg/I
date/time
Benzene 0.0553
0.0500
0.50
1 01/26/202316:18
WG1994068
Carbon tetrachloride ND
0.0500
0.50
1 01/25/202314:10
WG1994068
Chlorobenzene ND
0.0500
100
1 01/25/202314:10
WG1994068
Chloroform ND
0.250
6
1 01/25/202314:10
WG1994068
ACCOUNT:
PROJECT:
SDG:
DATE/TIME: PAGE:
EMA Resources
L1577759
01/31/23 13:10 5 of 21

BROWN WTP
SAMPLE RESULTS
- 01
Collected date/time: 01/19/23 10:00
L1577759
Volatile Organic Compounds (GC/MS) by Method 8260D
Result
Qualifier RDL
Limit Dilution
Analysis
Batch
Analyte
mg/I
mg/I
mg/I
date/time
1,2-Dichloroethane
ND
0.0500
0.50 1
01/25/202314:10
WG1994068
1,1-Dichloroethene
ND
0.0500
0.70 1
01/25/202314:10
WG1994068
2-Butanone (MEK)
ND
0.500
200 1
01/25/202314:10
WG1994068
Tetrachloroethene
ND
0.0500
0.70 1
01/25/202314:10
WG1994068
Trichloroethene
ND
0.0500
0.50 1
01/25/202314:10
WG1994068
Vinyl chloride
ND
0.0500
0.20 1
01/25/202314:10
WG1994068
Fn
(S) Toluene-dH
106
80.0-120
011251202314.10
WG1994068
(S) Toluene-dH
109
80.0-120
011261202316.18
WG1994068
(S) 4-Bromofluorobenzene
96.6
77.0-126
011261202316.18
WG1994068
(S) 4-Bromofluorobenzene
96.3
77.0-126
011251202314.10
WG1994068
(S) 1,2-Dichloroethane-d4
94.8
70.0-130
011261202316.18
WG1994068
,
(S) 1,2-Dichloroethane-d4
113
70.0-130
011251202314.10
WG1994068
Chlorinated Acid Herbicides (GC) by Method 8151A
GI
Result
Qualifier RDL
Limit Dilution
Analysis
Batch
Analyte
g/I
mg/I
mg/I
date / time
e
"NI
2,4,5-TP (Silvex)
ND
0.00200
1 1
01/30/202316:00
WG1996036
2,4-D
ND
0.00200
10 1
01/30/202316:00
WG1996036
(S)2,4-DichlorophenylAcetic Acid
79.8
14.0-158
011301202316.00
WG1996036El
Pesticides (GC) by Method 8081B
Result
Qualifier RDL
Limit
Dilution Analysis
Batch
Analyte
mg/I
mg/I
mg/I
date/time
Chlordane
ND
0.00500
0.03
1 01/23/202317:19
WG1992848
Endrin
ND
0.00500
0.02
1 01/23/202317:19
WG1992848
Heptachlor
ND
0.00500
0.0080
1 01/23/202317:19
WG1992848
Heptachlor epoxide
ND
0.00500
0.0080
1 01/23/202317:19
WG1992848
Lindane
ND
0.00500
0.40
1 01/23/202317:19
WG1992848
Methoxychlor
ND
0.00500
10
1 01/23/202317:19
WG1992848
Toxaphene
ND
0.0100
0.50
1 01/23/202317:19
WG1992848
(S) Decachlorobiphenyl
59.6
10.0-128
0112312023 17.19
WG1992848
(S) Tetrochloro-m-xylene
58.4
10.0-127
0112312023 17.19
WG1992848
Semi Volatile Organic Compounds
(GC/MS) by Method 8270E
Result
Qualifier RDL
Limit
Dilution Analysis
Batch
Analyte
mg/I
mg/I
mg/I
date/time
1,4-Dichlorobenzene
ND
0.100
7.50
1 01/23/202317:59
WG1992847
2,4-Dinitrotoluene
ND
0.100
0.13
1 01/23/202317:59
WG1992847
Hexachlorobenzene
ND
0.100
0.13
1 01/23/202317:59
WG1992847
Hexachloro-1,3-butadiene
ND
0.100
0.50
1 01/23/202317:59
WG1992847
Hexachloroethane
ND
0.100
3
1 01/23/202317:59
WG1992847
Nitrobenzene
ND
0.100
2
1 01/23/202317:59
WG1992847
Pyridine
ND
0.100
5
1 01/23/202317:59
WG1992847
3&4-Methyl Phenol
ND
0.100
400
1 01/23/202317:59
WG1992847
2-Methylphenol
ND
0.100
200
1 01/23/202317:59
WG1992847
Pentachlorophenol
ND
0.100
100
1 01/23/202317:59
WG1992847
2,4,5-Trichlorophenol
ND
0.100
400
1 01/23/202317:59
WG1992847
2,4,6-Trichlorophenol
ND
0.100
2
1 01/23/202317:59
WG1992847
(S) 2-Fluorophenol
40.3
10.0-120
0112312023 17.59
WG1992847
(S) Phenol-d5
25.9
10.0-120
0112312023 17.59
WG1992847
(S) Nitrobenzene-d5
82.4
10.0-127
0112312023 17.59
WG1992847
(S) 2-Fluorobiphenyl
91.2
10.0-130
0112312023 17.59
WG1992847
(S)2,4,6-Tribromophenol
81.5
10.0-155
011231202317.59
WG1992847
(S) p-Terphenyl-d14
H7.7
10.0-128
0112312023 17.59
WG1992847
ACCOUNT:
PROJECT:
SDG:
DATE/TIME: PAGE:
EMA Resources
L1577759
01/31/23 13:10 6 of 21

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GLOSSARY OF TERMS
Guide to Reading and Understanding Your Laboratory Report
The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not
intended as a comprehensive explanation, and ifyou have additional questions please contact your project representative.
Results Disclaimer - Information that may be provided by the customer, and contained within this report, include Permit Limits, Project Name,
Sample ID, Sample Matrix, Sample Preservation, Field Blanks, Field Spikes, Field Duplicates, On -Site Data, Sampling Collection Dates/Times, and
Sampling Location. Results relate to the accuracy of this information provided, and as the samples are received.
Abbreviations and Definitions
MDL
Method Detection Limit.
ND
Not detected at the Reporting Limit (or MDL where applicable).
RDL
Reported Detection Limit.
Rec.
Recovery.
RPD
Relative Percent Difference.
SDG
Sample Delivery Group.
Surrogate (Surrogate Standard) - Analytes added to every blank, sample, Laboratory Control Sample/Duplicate and
(S)
Matrix Spike/Duplicate; used to evaluate analytical efficiency by measuring recovery. Surrogates are not expected to be
detected in all environmental media.
U
Not detected at the Reporting Limit (or MDL where applicable).
Analyte
The name ofthe particular compound or analysis performed. Some Analyses and Methods will have multiple analytes
reported.
Ifthe sample matrix contains an interfering material, the sample preparation volume or weight values differ from the
Dilution
standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the
laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the
result reported has already been corrected for this factor.
These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal
Limits
for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or
duplicated within these ranges.
Original Sample
The non -spiked sample in the prep batch used to determine the Relative Percent Difference (RPD) from a quality control
sample. The Original Sample may not be included within the reported SDG.
This column provides a letter and/or number designation that corresponds to additional information concerning the result
Qualifier
reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and
potentially a discussion of possible implications ofthe Qualifier in the Case Narrative if applicable.
The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. Ifthere was
no measurable result returned for a specific analyte, the result in this column may state "ND" (Not Detected) or "BDL"
Result
(Below Detectable Levels). The information in the results column should always be accompanied by either an MDL
(Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect
or report for this analyte.
Uncertainty
(Radiochemistry)
Confidence level of 2 sigma.
A brief discussion about the included sample results, including a discussion of any non -conformances to protocol
Case Narrative (Cn)
observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will
be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report.
Quality Control
This section ofthe report includes the results ofthe laboratory quality control analyses required by procedure or
Summary (Qc)
analytical methods to assist in evaluating the validity ofthe results reported for your samples. These analyses are not
being performed on your samples typically, but on laboratory generated material.
This is the document created in the field when your samples were initially collected. This is used to verify the time and
Sample Chain of
date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This
Custody (Sc)
chain of custody also documents all persons (excluding commercial shippers) that have had control or possession ofthe
samples from the time of collection until delivery to the laboratory for analysis.
This section ofyour report will provide the results of all testing performed on your samples. These results are provided
Sample Results (Sr)
by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for
each sample will provide the name and method number for the analysis reported.
Sample Summary (Ss)
This section ofthe Analytical Report defines the specific analyses performed for each sample ID, including the dates and
times of preparation and/or analysis.
Qualifier
Description
J6
The sample matrix interfered with the ability to make any accurate determination, spike value is low.
T8
Sample(s) received past/too close to holding time expiration.
U
Below Detectable Limits: Indicates that the analyte was not detected.
ACCOUNT:
PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources
L1577759 01/31/23 13:10 19 of 21

ACCREDITATIONS & LOCATIONS
!Ninl',71cl I\h ll+"inl l 12065 I cd it I+:+I""I
Alabama
40660
Nebraska
N E-OS-15-05
Alaska
17-026
Nevada
TN000032021-1
Arizona
AZ0612
New Hampshire
2975
Arkansas
88-0469
New Jersey—NELAP
TNO02
California
2932
New Mexico
TN00003
Colorado
TN00003
New York
11742
Connecticut
PH-0197
North Carolina
Env375
Florida
E87487
North Carolina'
DW21704
Georgia
NELAP
North Carolina 3
41
Georgia'
923
North Dakota
R-140
Idaho
TN00003
Ohio—VAP
CL0069
Illinois
200008
Oklahoma
9915
Indiana
C-TN-01
Oregon
TN200002
Iowa
364
Pennsylvania
68-02979
Kansas
E-10277
Rhode Island
LA000356
Kentucky' 6
KY90010
South Carolina
84004002
Kentucky 2
16
South Dakota
n/a
Louisiana
A130792
Tennessee' 4
2006
Louisiana
LA018
Texas
T104704245-20-18
Maine
TN00003
Texas5
LABO152
Maryland
324
Utah
TN000032021-11
Massachusetts
M-TNO03
Vermont
VT2006
Michigan
9958
Virginia
110033
Minnesota
047-999-395
Washington
C847
Mississippi
TN00003
West Virginia
233
Missouri
340
Wisconsin
998093910
Montana
CERT0086
Wyoming
A2 LA
A2LA— ISO 17025
1461.01
AIHA-LAP,LLC EMLAP
100789
A2 LA — ISO 17025 5
1461.02
DOD
1461.01
Canada
1461.01
USDA
P330-15-00234
EPA—Crypto
TN00003
Drinking Water 2 Underground Storage Tanks 3 Aquatic Toxicity "Chemical/Microbiological 5 Mold 6 Wastewater n/a Accreditation not applicable
Not all certifications held by the laboratory are applicable to the results reported in the attached report.
Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace Analytical.
ACCOUNT: PROJECT: SDG: DATE/TIME:
EMA Resources L1577759 01/31/23 13:10
PAGE:
20 of 21

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ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
EMA Resources Inc.
Total Dry Tons Applied (Annual):
WQ0041666 Cation Exchange Capacity (non 503 only):
Roger Spillman Owner: Roger Spillman Predominant Soil Series:
23.67 Acres Permitted: 23.67 Site #: DV08 Field #:
61.19
MrB2
9
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Com-
posite
Date
Total
Phos-
phorusMENEENEENEEN
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total•
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D
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1 111
1 111
1 111
1 111
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1 111
1 111
1 111
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"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
t
2/19/2024
Signature of Land Applier
Date
DENR FORM MFLSF (12/2006)

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ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
EMA Resources Inc.
Total Dry Tons Applied (Annual):
WQ0041666 Cation Exchange Capacity (non 503 only):
Roger Spillman Owner: Roger Spillman Predominant Soil Series:
22.98 Acres Permitted: 22.98 Site #: DV8 Field #:
182.53
WeC
10
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample or
......1......
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4....
5.....
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8....
9
10
11
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Com-
Davidson
Piedmont
Water
Water
polite
4/12/23
4/5/23
Date
% Solids
4.24
20.7
Arsenic
5.22
5.69
Cadmium
1.41
4.1
Copper
23
71.6
Chromium
38
13.8
Lead
18.5
4.27
Mercury
0.472
0.102
Molyb-
6.54
13.6
dencm
Nickel
16
16.3
Selenium
18.8
7.58
Zinc
68.9
19.2
Total
Phos-
3000
1210
horus
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total•
•
D
App-
Event
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1 1� 1
1 1�
1 111
1 111
1 111
1 111
1 111
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1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with
a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am
aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
zl-e 2/19/2024
Signature of Land Applier
Date
DENR FORM MFLSF (12/2006)

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ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
EMA Resources Inc.
Total Dry Tons Applied (Annual):
WQ0041666 Cation Exchange Capacity (non 503 only):
Roger Spillman Owner: Roger Spillman Predominant Soil Series:
6.03 Acres Permitted: 6.03 Site #: DV8 Field #:
204.34
RnC
11
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample or
.......1......
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4....1IF
6....1
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1..0....
1..1......1
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Com-
Davidson
Piedmont
Water
Water
polite
4/12/23
4/5/23
Date
% Solids
4.24
20.7
Arsenic
5.22
5.69
Cadmium
1.41
4.1
Copper
23
71.6
Chromium
38
13.8
Lead
18.5
4.27
Mercury
0.472
0.102
Molyb-
6.54
13.6
dencm
Nickel
16
16.3
Selenium
18.8
7.58
Zinc
68.9
19.2
Total
Phos-
3000
1210
horus
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total•
•
D
App-
Event
1 •
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1 111
1 111
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"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with
a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am
aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
zl-e 2/19/2024
Signature of Land Applier
Date
DENR FORM MFLSF (12/2006)

Pr
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ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
EMA Resources Inc
WQ0041666
Operator: Ryan Hiatt Owner:
Acres Used: 7.28 Acres Permitted:
Total Dry Tons Applied (Annual):
Cation Exchange Capacity (non 503 only):
EMH Farms LLC Predominant Soil Series:
7.28 Site #: GU28 Field #:
19.90
EnB
2A-Buffer
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Com-
posite
Date
Total
Phos-
phorusMENEENEENEEN
Annual Heavv Metal Field Loadings (Calculated in lbs/acre):
Total•
•
D
App-
Event
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
®�
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
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1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
®
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
®
1 11
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 11
®
1 1�
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1�
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1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1
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1 •1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 •1
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1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
Total
'
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
"I certity, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
2/19/2024
Signature of Land Applier
Date
DENR FORM MFLSF (12/2006)

OC
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ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
EMA Resources Inc
WQ0041666
Operator: Ryan Hiatt Owner:
Acres Used: 5.33 Acres Permitted:
Total Dry Tons Applied (Annual):
Cation Exchange Capacity (non 503 only):
EMH Farms LLC Predominant Soil Series:
5.33 Site #: GU28 Field #:
39.81
EnB
4-Buffer
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Com-
posite
Date
Total
Phos-
phorusMENEENEENEEN
Annual Heavv Metal Field Loadings (Calculated in lbs/acre):
Total•
•
D
App-
Event
1 1 �
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
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1�
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1
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1•
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1•
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
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1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
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1 11
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 11
®
1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1
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1 •
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 •
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1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1
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1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1
Total
'
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
"I certity, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
2/19/2024
Signature of Land Applier
Date
DENR FORM MFLSF (12/2006)

O
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ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
EMA Resources Inc
WQ0041666
Operator: Ryan Hiatt Owner:
Acres Used: 8.61 Acres Permitted:
Total Dry Tons Applied (Annual):
Cation Exchange Capacity (non 503 only):
EMH Farms LLC Predominant Soil Series:
8.61 Site #: GU28 Field #:
53.08
EnB
6-Buffer
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Com-
posite
Date
Total
Phos-
phorusMENEENEENEEN
Annual Heavv Metal Field Loadings (Calculated in lbs/acre):
Total•
•
D
App-
Event
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
®
1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1
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1 •.
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 •.
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
®
1 1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1 1
®
1 11
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 11
®�
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
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1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
®
1�
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1
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1 •
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 •
Total
'
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111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111M
"I certity, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
2/19/2024
Signature of Land Applier
Date
DENR FORM MFLSF (12/2006)

O
N
4t 4t
U
N
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SE
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ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
EMA Resources Inc
WQ0041666
Operator: Ryan Hiatt Owner:
Acres Used: 3 Acres Permitted:
Total Dry Tons Applied (Annual):
Cation Exchange Capacity (non 503 only):
EMH Farms LLC Predominant Soil Series:
3 Site #: GU28 Field #:
19.91
BtC2
7X
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Com-
posite
Date
Total
Phos-
phorusMENEENEENEEN
Annual Heavv Metal Field Loadings (Calculated in lbs/acre):
Total•
•
D
App-
Event
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
®
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
®
1:
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
®
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
®
1 11
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 11
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1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
®
1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1
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1� 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1� 1
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1�
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1
Total
'
•
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
•
"I certity, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
2/19/2024
Signature of Land Applier
Date
DENR FORM MFLSF (12/2006)

M
M
N
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N
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ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
EMA Resources Inc
WQ0041666
Richard Vanhook Owner:
8.5 Acres Permitted:
Total Dry Tons Applied (Annual):
Cation Exchange Capacity (non 503 only):
Richard Vanhook Predominant Soil Series:
8.5 Site #: OR15 Field #:
103.91
GeB
3
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample or
.......1......F
2.....
3
4....
5.....
9
z....
8....
9.....
1......
1..1......
1..2....
Brown
Com-
SD
Hillsb
wTP
posite
1/5/23
8/3/23
10/5/23
Date
% Solids
16.1
2.73
19.7
Arsenic
3.8
9.26
14.5
Cadmium
0.988
1.85
1.36
Copper
430
46.3
80.2
Chromium
19.9
134
39.9
Lead
13.5
12.7
97
Mercury
0.764
0.774
0.102
Molyb-
24.6
5.56
1.8
denum
Nickel
17.7
9.3
35
Selenium
4.05
13
2.54
Zinc
2800
105
234
Total
Phos-
36800
1410
3620
horus
Annual Heavv Metal Field Loadings (Calculated in lbs/acre):
Total
1......
2.....
9.....
1......
1..1......
1..�....
.....3.....
.....4....
.....5.....
.....6....
.....�.....
......8....
DT/Ac./
0
App.
Event
3.11
2.26
6.85
Arsenic
0.024
1 0.042
0.199
1 0.000
0.000
0.000
1 0.000
0.000
0.000
1 0.000
0.000
0.000
1 0.264
Cadmium
0.006
0.008
0.019
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.033
Copper
2.675
0.210
1.099
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
3.984
Chromium
0.124
0.606
0.547
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1.277
Lead
0.084
0.057
1.329
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1.471
Mercury
0.005
1 0.004
0.001
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1 0.010
Molyb-
0.153
0.025
0.025
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.203
denum
Nickel
0.110
0.042
0.480
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.632
Selenium
0.025
0.059
0.035
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.119
Zinc
17.422
1 0.475
3.206
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1 21.103
Total
Phos-
228.970
6.382
49.601
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
284.953
horus
"I certity, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
2/19/2024
Signature of Land Applier Date
DENR FORM MFLSF (12/2006)

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ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
EMA Resources Inc
WQ0041666
Richard Vanhook Owner:
5 Acres Permitted:
Total Dry Tons Applied (Annual):
Cation Exchange Capacity (non 503 only):
Richard Vanhook Predominant Soil Series:
5 Site #: OR15 Field #:
140.48
GeB
4X
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample or
......1......
2
..........Hillsb
3
4
........Brown
5.....
..........
6....
7.....
8....
9.....
10
11
12
Com-
Brown
Brown
P3
WTP
posite
R TP
8l3/23
�wg
10/5/23
Date
% Solids
21.5
2.73
19.9
19.7
Arsenic
1.12
9.26
6.28
14.5
Cadmium
11.5
1.85
2.86
1.36
Copper
614
46.3
1690
80.2
Chromium
14.3
134
21.4
39.9
Lead
9.58
12.7
10.1
97
Mercury
0.042
0.774
0.116
0.102
Molyb-
2.37
5.56
6.93
1.8
denum
Nickel
82.3
9.3
77.4
35
Selenium
3.88
13
17.6
2.54
Zinc
99.5
105
50.3
234
Total
Phos-
940
1410
769
3620
horus
Annual Heavv Metal Field Loadings (Calculated in lbs/acre):
Total
1......
2.....
9.....
1......
1..1......
1..�....
.....3.....
.....4....
.....5.....
.....6....
.....�.....
......8....
DT/Ac./
0
App.
Event
14.12
2.22
10.46
1.29
Arsenic
0.032
1 0.041
0.131
1 0.038
0.000
0.000
1 0.000
0.000
0.000
1 0.000
0.000
0.000
1 0.242
Cadmium
0.325
0.008
0.060
0.004
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.396
Copper
17.343
0.206
35.348
0.208
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
53.104
Chromium
0.404
0.595
0.448
0.103
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1.550
Lead
0.271
0.056
0.211
0.251
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.789
Mercury
0.001
0.003
0.002
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.007
Molyb-
0.067
0.025
0.145
0.005
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.241
denum
Nickel
2.325
0.041
1.619
0.091
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
4.075
Selenium
0.110
0.058
0.368
0.007
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.542
Zinc
2.810
0.466
1.052
0.606
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
4.934
Total
Phos-
26.551
6.260
16.084
9.369
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
58.265
horus
"I certity, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
2/19/2024
Signature of Land Applier Date
DENR FORM MFLSF (12/2006)

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ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
EMA Resources Inc
WQ0041666
Richard Vanhook Owner:
6.6 Acres Permitted:
Total Dry Tons Applied (Annual):
Cation Exchange Capacity (non 503 only):
Richard Vanhook Predominant Soil Series:
6.6 Site #: OR15 Field #:
177.84
Geb
5X
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample or
......1......
2
..........Hillsb
3
4
........Brown
5.....
..........
6....
7.....
8....
9.....
10
11
12
Com-
Brown
Brown
P3
WTP
posite
R TP
8l3/23
�wg
10/5/23
Date
% Solids
21.5
2.73
19.9
19.7
Arsenic
1.12
9.26
6.28
14.5
Cadmium
11.5
1.85
2.86
1.36
Copper
614
46.3
1690
80.2
Chromium
14.3
134
21.4
39.9
Lead
9.58
12.7
10.1
97
Mercury
0.042
0.774
0.116
0.102
Molyb-
2.37
5.56
6.93
1.8
denum
Nickel
82.3
9.3
77.4
35
Selenium
3.88
13
17.6
2.54
Zinc
99.5
105
50.3
234
Total
Phos-
940
1410
769
3620
horus
Annual Heavv Metal Field Loadings (Calculated in lbs/acre):
Total
1......
2.....
9.....
1......
1..1......
1..�....
.....3.....
.....4....
.....5.....
.....6....
.....�.....
......8....
DT/Ac./
0
App.
Event
12.84
2.24
9.90
1.96
Arsenic
0.029
1 0.042
0.124
1 0.057
0.000
0.000
1 0.000
0.000
0.000
1 0.000
0.000
0.000
1 0.252
Cadmium
0.295
0.008
0.057
0.005
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.366
Copper
15.766
0.208
33.472
0.315
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
49.761
Chromium
0.367
0.601
0.424
0.156
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1.548
Lead
0.246
0.057
0.200
0.380
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.883
Mercury
0.001
0.003
0.002
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.007
Molyb-
0.061
0.025
0.137
0.007
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.230
denum
Nickel
2.113
0.042
1.533
0.137
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
3.825
Selenium
0.100
0.058
0.349
0.010
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.516
Zinc
2.555
0.471
0.996
0.918
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
4.940
Total
Phos-
24.137
6.322
15.231
14.198
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
59.888
horus
"I certity, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
2/19/2024
Signature of Land Applier Date
DENR FORM MFLSF (12/2006)

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ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
EMA Resources Inc
WQ0041666
Richard Vanhook Owner:
6.9 Acres Permitted:
Total Dry Tons Applied (Annual):
Cation Exchange Capacity (non 503 only):
Richard Vanhook Predominant Soil Series:
6.9 Site #: OR15 Field #:
157.28
GeB
6X
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample or
......1......
2
..........Hillsb
3
4
........Brown
5.....
..........
6....
7.....
8....
9.....
10
11
12
Com-
Brown
Brown
P3
WTP
posite
R TP
8l3/23
�wg
10/5/23
Date
% Solids
21.5
2.73
19.9
19.7
Arsenic
1.12
9.26
6.28
14.5
Cadmium
11.5
1.85
2.86
1.36
Copper
614
46.3
1690
80.2
Chromium
14.3
134
21.4
39.9
Lead
9.58
12.7
10.1
97
Mercury
0.042
0.774
0.116
0.102
Molyb-
2.37
5.56
6.93
1.8
denum
Nickel
82.3
9.3
77.4
35
Selenium
3.88
13
17.6
2.54
Zinc
99.5
105
50.3
234
Total
Phos-
940
1410
769
3620
horus
Annual Heavv Metal Field Loadings (Calculated in lbs/acre):
Total
1......
2.....
9.....
1......
1..1......
1..�....
.....3.....
.....4....
.....5.....
.....6....
.....�.....
......8....
DT/Ac./
0
App.
Event
6.14
2.15
3.26
11.25
Arsenic
0.014
1 0.040
0.041
1 0.326
0.000
0.000
1 0.000
0.000
0.000
1 0.000
0.000
0.000
1 0.421
Cadmium
0.141
0.008
0.019
0.031
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.198
Copper
7.541
0.199
11.002
1.805
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
20.547
Chromium
0.176
0.575
0.139
0.898
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1.788
Lead
0.118
0.054
0.066
2.183
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
2.421
Mercury
0.001
0.003
0.001
0.002
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.007
Molyb-
0.029
0.024
0.045
0.041
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.139
denum
Nickel
1.011
0.040
0.504
0.788
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
2.342
Selenium
0.048
0.056
0.115
0.057
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.275
Zinc
1.222
0.450
0.327
5.266
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
7.266
Total
Phos-
11.545
6.049
5.006
81.472
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
104.072
horus
"I certity, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
2/19/2024
Signature of Land Applier Date
DENR FORM MFLSF (12/2006)

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ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: EMA Resources Inc. Total Dry Tons Applied (Annual): 78.83
Permit #: WQ0041666 Cation Exchange Capacity (non 503 only):
Operator: Larry Rogers Owner: Larry Rogers Predominant Soil Series: HeB
Acres Used: 6.1 Acres Permitted: 6.1 Site #: OR93 Field #: 2X
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
4/11/23
Date
Total
Phos-
phorusMENEENEENEEN
Annual Heavv Metal Field Loadings (Calculated in lbs/acre):
Total
D
App-
Event
1 ..
1 111
1 111
1 111
1 111
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1 111
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1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
Total
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1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
"I certity, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
2/19/2024
Signature of Land Applier
Date
DENR FORM MFLSF (12/2006)

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ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: EMA Resources Inc. Total Dry Tons Applied (Annual): 111.97
Permit #: WQ0041666 Cation Exchange Capacity (non 503 only):
Operator: Larry Rogers Owner: Larry Rogers Predominant Soil Series: HeB
Acres Used: 15.05 Acres Permitted: 15.05 Site #: OR93 Field #: 03X
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Com-
Brown
4/11/23
Date
Total
Phos-
phorusMENEENEENEEN
Annual Heavv Metal Field Loadings (Calculated in lbs/acre):
Total•
•
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1 111
1 111
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1 111
1 111
1 111
1 111
1 111
1 111
1 111
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1 111
1 111
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1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
Total
'
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1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
"I certity, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
2/19/2024
Signature of Land Applier
Date
DENR FORM MFLSF (12/2006)

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ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: EMA Resources Inc. Total Dry Tons Applied (Annual): 115.42
Permit #: WQ0041666 Cation Exchange Capacity (non 503 only):
Operator: Larry Rogers Owner: Larry Rogers Predominant Soil Series: VaB
Acres Used: 10.01 Acres Permitted: 10.01 Site #: OR93 Field #: 4X
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
4/11/23
Date
Total
Phos-
phorusMENEENEENEEN
Annual Heavv Metal Field Loadings (Calculated in lbs/acre):
Total•
•
D
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Event
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1 111
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1 111
1 111
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"I certity, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
2/19/2024
Signature of Land Applier
Date
DENR FORM MFLSF (12/2006)

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ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: EMA Resources Inc. Total Dry Tons Applied (Annual): 117.02
Permit #: WQ0041666 Cation Exchange Capacity (non 503 only):
Operator: Larry Rogers Owner: Larry Rogers Predominant Soil Series: VaB
Acres Used: 10.2 Acres Permitted: 10.2 Site #: OR93 Field #: 6X
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Com-
Brown
4/11/23
Date
Total
Phos-
phorusMENEENEENEEN
Annual Heavv Metal Field Loadings (Calculated in lbs/acre):
Total•
•
D
App-
Event
1•
1 111
1 111
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1 111
1 111
1 111
Total
'
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
"I certity, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
2/19/2024
Signature of Land Applier
Date
DENR FORM MFLSF (12/2006)

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ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: EMA Resources Inc. Total Dry Tons Applied (Annual): 127.74
Permit #: WQ0041666 Cation Exchange Capacity (non 503 only):
Operator: Larry Rogers Owner: Larry Rogers Predominant Soil Series: VaB
Acres Used: 14.81 Acres Permitted: 14.81 Site #: OR93 Field #: 21X
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Com-
Brown
4/11/23
Date
Total
Phos-
phorusMENEENEENEEN
Annual Heavv Metal Field Loadings (Calculated in lbs/acre):
Total•
•
D
App-
Event
1 •:
1 111
1 111
1 111
1 111
1 111
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1 111
1 111
1 111
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1
"I certity, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
2/19/2024
Signature of Land Applier
Date
DENR FORM MFLSF (12/2006)

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W
0

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: EMA Resources Inc. Total Dry Tons Applied (Annual): 86.11
Permit #: WQ0041666 Cation Exchange Capacity (non 503 only):
Operator: Larry Rogers Owner: Larry Rogers Predominant Soil Series:
Acres Used: 17.15 Acres Permitted: 17.15 Site #: OR93 Field #: 28X
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Com-
Brown
4/11/23
Date
Total
Phos-
phorusMENEENEENEEN
Annual Heavv Metal Field Loadings (Calculated in lbs/acre):
Total•
•
D
App-
Event
1
1 �
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1
®
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
®
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
®
1 •
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 •
®
1 11
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 11
®
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
®
1� 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1� 1
®
1�
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1
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1 : •
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 : •
Total
'
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
"I certity, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
2/19/2024
Signature of Land Applier
Date
DENR FORM MFLSF (12/2006)

O
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ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: EMA Resources Inc. Total Dry Tons Applied (Annual): 239.40
Permit #: WQ0041666 Cation Exchange Capacity (non 503 only):
Operator: Sidney Thompson Owner: Sidney Thompson Predominant Soil Series: FaB3
Acres Used: 42 Acres Permitted: 134.1 Site #: PS01 Field #: 1
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Com-
Brown
10/5/23
Date
Total
Phos-
phorusMENEENEENEEN
Annual Heavv Metal Field Loadings (Calculated in lbs/acre):
Total•
•
D
App-
Event
1
��
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
®
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
®
1 •
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 • .
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1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1
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1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
®
1 11
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 11
®
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
®
1 ••
1111
1111
1111
1111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 ••
®
1 1 •
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1 •
®
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
Total
'
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
"I certity, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
2/19/2024
Signature of Land Applier
Date
DENR FORM MFLSF (12/2006)

O
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ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: EMA Resources Inc. Total Dry Tons Applied (Annual): 103.53
Permit #: WQ0041666 Cation Exchange Capacity (non 503 only):
Operator: Sidney Thompson Owner: Sidney Thompson Predominant Soil Series: FaB3
Acres Used: 37.2 Acres Permitted: 37.2 Site #: PS01 Field #: 4
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
10/5/23
Date
Total
Phos-
phorusMENEENEENEEN
Annual Heavv Metal Field Loadings (Calculated in lbs/acre):
Total•
•
D
App-
Event
1 1:
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1:
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1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 11:
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1 ..
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 ..
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
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1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
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1 11
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 11
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1 1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1 1
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1•
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
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1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
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1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
Total
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1 111
1111
1111
1111
1 111
1 111
1 111
1 111
1 111
1 111
1 111M
"I certity, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
2/19/2024
Signature of Land Applier
Date
DENR FORM MFLSF (12/2006)

O
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ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
EMA Resources Inc.
Total Dry Tons Applied (Annual):
WQ0041666 Cation Exchange Capacity (non 503 only):
Kenny McMahan Owner: Kenny McMahan Predominant Soil Series:
16 Acres Permitted: 16 Site #: PS30 Field #:
322.21
GeC
1X
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample or
......1......
....2.....
.....3.....
.....4....
.....5.....
......6....
..........
8....
.....9.....
10
11
12
Com-
Brown
Brown
R TP
WTP
polite
4/11/23
7/18/23
Date
% Solids
24
19.9
Arsenic
17.3
6.28
Cadmium
20.6
2.86
Copper
386
1690
Chromium
26.2
21.4
Lead
16.8
10.1
Mercury
0.155
0.116
Molyb-
3.32
6.93
denum
Nickel
40.1
77.4
Selenium
24.5
17.6
Zinc
83.5
50.3
Total
Phos-
1450
769
horus
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total•
•
D
App-
Event
��
1 �
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1
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1 1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1•
®
1:
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1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
� 1:
1�
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1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1•
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1 �:
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
®
1 11
1 11
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 11
®
1 1
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
®�
:•
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
®
1
1�
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1
®®®
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
• •
Total
'
M
1111
1111
1111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1•
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
t
2/19/2024
Signature of Land Applier
Date
DENR FORM MFLSF (12/2006)

O
:M :M
w
o N
U
N
O
N
n
OC
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CZ
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O
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o
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ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
EMA Resources Inc.
Total Dry Tons Applied (Annual):
WQ0041666 Cation Exchange Capacity (non 503 only):
Kenny McMahan Owner: Kenny McMahan Predominant Soil Series:
7 Acres Permitted: 7 Site #: PS30 Field #:
58.83
HrC
2X
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
7/18/23
Date
Total
Phos-
phorusMENEENEENEEN
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total•
•
D
App-
Event
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
®
1 1�:
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1�:
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1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
: � 1
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
®
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
®
1 11
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 11
®�
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
®�
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
®
1•
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1•
®
1 :�
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 :�
Total
'
•
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
•
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
t
2/19/2024
Signature of Land Applier
Date
DENR FORM MFLSF (12/2006)

O
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ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
EMA Resources Inc.
Total Dry Tons Applied (Annual):
WQ0041666 Cation Exchange Capacity (non 503 only):
Kenny McMahan Owner: Kenny McMahan Predominant Soil Series:
9 Acres Permitted: 9 Site #: PS30 Field #:
78.44
GeC
3X
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
7/18/23
Date
Total
Phos-
phorusMENEENEENEEN
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total•
•
D
App-
Event
1 1•
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1•
®
1 1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1 1
®
• '
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
• .
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
®�
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
®
1 11
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 11
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1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
®
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1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
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1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
®
1:
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1
Total
'
m
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111M
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
t
2/19/2024
Signature of Land Applier
Date
DENR FORM MFLSF (12/2006)

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ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
EMA Resources Inc.
Total Dry Tons Applied (Annual):
WQ0041666 Cation Exchange Capacity (non 503 only):
Ted Oakley Owner: Ted Oakley Predominant Soil Series:
16 Acres Permitted: 16 Site #: PS31 Field #:
203.22
VaB
1X
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample or
.......1......F
?
3.....lI
4....
5.....
9
z ....
8....
9.....
1..0....
1..1......
1..2....
Brown
Brown
Com-
WTP
WTP
polite
4/11/23
7/18/23
Date
% Solids
24
19.9
Arsenic
17.3
6.28
Cadmium
20.6
2.86
Copper
386
1690
Chromium
26.2
21.4
Lead
16.8
10.1
Mercury
0.155
0.116
Molyb-
3.32
6.93
denum
Nickel
40.1
77.4
Selenium
24.5
17.6
Zinc
83.5
50.3
Total
Phos-
1450
769
horus
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
1......
2.....
9.....
....0....
1..1......
1..�....
.....3.....
.....4....
.....5.....
.....6....
.....�.....
......8....
DT/Ac./
0
App.
Event
7.39
5.31
Arsenic
0.256
1 0.067
0.000
1 0.000
0.000
0.000
1 0.000
0.000
0.000
1 0.000
0.000
0.000
1 0.322
Cadmium
0.304
0.030
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.335
Copper
5.705
17.951
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
23.656
Chromium
0.387
0.227
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.615
Lead
0.248
0.107
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.356
Mercury
0.002
0.001
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.004
Molyb-
0.049
0.074
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.123
denum
Nickel
0.593
0.822
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1.415
Selenium
0.362
0.187
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.549
Zinc
1.234
0.534
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1 1.768
Total
Phos-
21.431
8.168
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
29.599
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
t
2/19/2024
Signature of Land Applier
Date
DENR FORM MFLSF (12/2006)

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ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
EMA Resources Inc
WQ0041666
Operator: Ted Oakley Owner:
Acres Used: 11 Acres Permitted:
Total Dry Tons Applied (Annual): 111.11
Cation Exchange Capacity (non 503 only):
Donald Brooks Predominant Soil Series: LgB
11 Site #: PS32 Field #: 1X
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Com-
Brown
7/18/23
Date
Total
Phos-
phorusMENEENEENEEN
Annual Heavv Metal Field Loadings (Calculated in lbs/acre):
Total
D
App-
Event
1 1
��
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
®
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
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1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1�
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1
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1 1�
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1�
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1 11
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 11
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1� 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1� 1
®�
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
®�
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
®�
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
Total
'
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
"I certity, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
2/19/2024
Signature of Land Applier
Date
DENR FORM MFLSF (12/2006)

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ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
EMA Resources Inc
WQ0041666
Gene Hiatt Owner:
5 Acres Permitted:
Total Dry Tons Applied (Annual):
Cation Exchange Capacity (non 503 only):
Gene Hiatt Predominant Soil Series:
5 Site #: RD43 Field #:
33.18
BtC2
4X
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Com-
posite
Date
Total
Phos-
phorusMENEENEENEEN
Annual Heavv Metal Field Loadings (Calculated in lbs/acre):
Total•
•
D
App-
Event
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
®
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
®
1:
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
®
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
®
1 11
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 11
®�
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
®
1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1
®
1� 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1� 1
®
1�
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1
Total
'
•
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
•
"I certity, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
2/19/2024
Signature of Land Applier Date
DENR FORM MFLSF (12/2006)

�I
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ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
EMA Resources Inc.
Total Dry Tons Applied (Annual):
WQ0041666 Cation Exchange Capacity (non 503 only):
Doug Hensley Owner: Doug Hensley Predominant Soil Series:
30 Acres Permitted: 30 Site #: RD46 Field #:
299.37
BtB2
3X
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample or
.......?......
2....
3.....
4....
5.....
6.........
8....
9.....
1......
1..1......
1..2....
Piedmont
Piedmon
Com-
Water
t Water
polite
1/9/23
10/3/23
Date
% Solids
19.5
20.4
Arsenic
1.23
7.21
Cadmium
14.5
31.3
Copper
17.5
44.6
Chromium
13
11.2
Lead
5.49
6.72
Mercury
0.0311
0.102
Molyb-
12
23.2
denum
Nickel
12.4
28.7
Selenium
11
10.4
Zinc
17.4
19.2
Total
Phos-
1020
1570
horus
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total•
•
D
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1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
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1
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1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
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1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
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1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
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1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
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1 111
1 11
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 11
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1 111
1 111
1 111
1 111
1 111
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1 111
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1 111
1 111
1 111
1 111
1 111
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"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
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2/19/2024
Signature of Land Applier
Date
DENR FORM MFLSF (12/2006)

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[","ages �frar�ri 2023 ", M A e s o i urces �h�r�ic
.............. WQ004�1666
Final Audit Report 2024-02-20
Created: 2024-02-19
By: Brent Collins ([e-mail])
Status: Signed
Transaction ID: CBJCHBCAABAAt723pLEI ES—MxhbSqbk71 FJjiuAfBwED
"Pages from 2023 EMA Resources Inc. Annual Report - WQ004
1666" History
7111..31, Document created by Brent Collins ([e-mail])
2024-02-19 - 6:43:01 PM GMT- IP address: 206.85.202.26
I...........
,t, Document emailed to Erik Blankenship (erik.blankenship Qemaresourcesinc.corn) for signature
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T . . . . .. . . . . 11 Email viewed by Erik Blankenship ([e-mail])
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Document e-signed by Erik Blankenship ([e-mail])
Signature Date: 2024-02-20 - 1:23:37 PM GMT - Time Source: server- IP address: 206.85.202.92
Agreement completed.
2024-02-20 - 1:23:37 PM GMT

[","ages �frar�ri 2023 ", M A e s o i urces �h�r�ic
.............. WQ004�1666
Final Audit Report 2024-03-01
Created: 2024-03-01
By: Brent Collins ([e-mail])
Status: Signed
Transaction ID: CBJCHBCAABAADUX4Pj44HhxljmP-mUWeinB-Lfq—mSjH
"Pages from 2023 EMA Resources Inc. Annual Report - WQ004
1666" History
Document created by Brent Collins ([e-mail])
2024-03-01 - 5:21:16 PM GMT- IP address: 206.85.202.26
I...........
Document emailed to Brent Collins ([e-mail]) for signature
2024-03-01 - 5:21:19 PM GMT
Document e-signed by Brent Collins ([e-mail])
E-signature obtained using URL retrieved through the Adobe Acrobat Sign AN
Signature Date: 2024-03-01 - 5:21:42 PM GMT - Time Source: server- IP address: 206.85.202.26
Agreement completed.
2024-03-01 - 5:21:42 PM GMT