WQ0019960_2023 Residual Annual Report_20240222 (2)

Initial Review
Reviewer
nathaniel.thorn burg
Is this submittal an application? (Excluding additional information.) *
Yes No
If not an application what is the submittal type?* Annual Report
Residual Annual Report
Additional Information
Other
Annual Report Year* 2023
Permit Number (IR) * WQ0019960
Applicant/Permittee City of Marion
Email Notifications
Does this need review by the hydrogeologist? * Yes U No
Regional Office Asheville
CO Reviewer
Admin Reviewer Wanda Gerald

Submittal Form
Project Contact Information
Please provide information on the person to be contacted by NDB Staff regarding electronic submittal, confirmation of receipt, and other correspondence.
Name* Tim Horton
Email Address*
[e-mail]
Project Information
.........................
Application/Document Type*
New (Fee Required)
Modification - Major (Fee Required)
Renewal with Major Modification (Fee
Required)
Annual Report
Additional Information
Other
Phone Number*
8286528843
Modification - Minor
Renewal
GW-59, NDMR, NDMLR, NDAR-1,
N DAR-2
Residual Annual Report
Change of Ownership
We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form.
https://edoes.deq.nc.gov/Forms/NonDischarge_Monitoring_Report
Permit Type:*
Wastewater Irrigation
High -Rate Infiltration
Other Wastewater
Reclaimed Water
Closed -Loop Recycle
Residuals
Single -Family Residence Wastewater
Other
Irrigation
Permit Number:*
WQ0019960
Has Current Existing permit number
Applicant/Permittee Address*
City of Marion, PO Drawer 700, Marion, NC 28752
Facility Name*
City of Marion Class B Residuals Program
Please provide comments/notes
on your current submittal below.
At this time, paper copies are no longer required. If you have any questions about what is required, please contact Nathaniel Thornburg
at [e-mail].
Please attach all information required or requested for this submittal to be reviewed here.
(Application Form, Engineering Plans, Specifications, Calculations, Etc.)
2023 Marion WWTP Annual Report--Signed--2.22.24.pdf 1.63MB
Upload only 1 PDF document (less than 250 MB). Multiple documents must be combined into one PDF file unless file is larger
than upload limit.
* By checking this box, I acknowledge that I understand the application will not be accepted for pre -review until the fee (if required) has
been received by the Non -Discharge Branch. Application fees must be submitted by check or money order and made payable to the
North Carolina Department of Environmental Quality (NCDEQ). I also confirm that the uploaded document is a single PDF with all parts
of the application in correct order (as specified by the application).
Mail payment to:
NCDEQ — Division of Water Resources
Attn: Non -Discharge Branch
1617 Mail Service Center
Raleigh, NC 27699-1617
Signature
r%/�A' `7Y4ttAY
Submission Date 2/22/2024

EleIe1111 a KleI_IZ:19 > a-COYAN I CIUK0 D] "A Y_I_y CKr Y_DUN all) R►i I
WQ Permit#: WQ0019960 County:
Facility Name (as shown on permit):
McDowell Year: 2023
City of Marion
Land Application Operator: U.S. Biosolids, Inc. Phone: [phone]
Land application of residuals as allowed by the permit occurred during the past calendar year?
R1 Yes ❑ No - If No, skip Part A, and Part B and proceed to Part C. Also, If residuals were
generated but not land applied, please attach an explanation on how the residuals were handled.
Part A - Residuals Application Summary:
Total number of application fields in thepermit:
116
Total number of fields utilized for land application during the year:
4
Total amount of dry tons applied during the year for all application sites:
143.07
Total number of acres utilizes for land application during the year:
26
Part B - Annual Compiance Statement:
Facility was compliant during calendar year 2023 with all conditions of the land application permit
(including but not limited to items 1-13 below) issued by the Division of Water Resources. 0 Yes ❑ No
If no please, provide a written description why the facility was not compliant, the dates, and explain corrective action
taken.
1) Only residuals approved for this permit were applied to the permitted sites.
2) Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or the
limit specified in the permit.
3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies of
laboratory results are attached.
4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5) All other monitoring was performed in accordance with the permit and reported during the year as required and three (3)
copies of certified laboratory results are attached.
6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T. I 105(a) or the Pollutant Loading
Rates in 15A NCAC 02T .I 105(b) (applicable to 40 CFR Part 503 regulated facilities).
7) All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part
503 regulated facilities).
8) All monitoring and reporting requirements in 15A NCAC 02T .I I I I were complied with (applicable to 40 CFR Part 503
regulated facilities).
9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Resources.
10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
11) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as specified
in the permit.
12) No runoff' of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13) All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C - Certification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate,
and complete. I am aware that there are significant penalties for submitting false information, including the possibility
of fines and imprisonment for knowing violations."
Permittee Name and Title (type or rint) ignat a of Pe ttee Date
-- 4�(Vkvl Z. 01.2� aci 2-1-2024
Signature of Preparer* Date Erignature of L d Applier Date
(if different from Permittee) (if different from Permittee and Preparer)
* Preparer is defined in 40 CFR Part 503.9 (r) and 15A NCAC 02T .1102 (26) DENR FORM ACF (12/2006)

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - I
WQ Permit Number: WQ0019960
Facility Name: ' City of Marion
Residual Source WQ # or NCO031879
NPDES #:
WWTP Name: Corpening Creek
Residual Analvsis Data
Laboratory: 1)
2)
3)
4)
5)
Enviromental Chemist!
Parameter
(mg/kg)
Conc.
Limit
m /k a
Sample or Composite Date
2-13-23
Percent Solids (%)
NA
3.32
Arsenic
75
25.6
Cadmium
85
25.6
Copper
4,300
566
Chromium
NA
NA
Lead
840
70.5
Mercury
57
0.711
Molybdenum
75
66.6
Nickel
420
25.6
Selenium
100
25.6
Zinc
7,500
1530
Total Phosphorus
NA
23600
TICN
NA
39600
Ammonia -Nitrogen
NA
580
Nitrate and Nitrite
NA
14.6
For surface disposal facilities the ceiling concentration limits listed in this form are not applicable. Reference the individual permit for metals limits.
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a systen
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there a
significant pen ties for submitting false information, including the possibility of fines and imprisonment for knowing violations.
Signature of Preparer * Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM RSSF

ANNUAL RESIDUAL SAMPLING SUMMARY FORM - B
Report all sampling analysis results for parameters not listed in FORM RSSF that are part of th'e WQ permit or were analyzed for over the 1
calendar year. Use additional forms as needed.
WQ Permit Number: WQ0019960
Facility Name: City of Marion
Residual Source
NPDES # or WQ#:
NCO031879
WWTP Name: Corpening Creek
Residual Analysis Data
Laboratory: 1)
2)
3)
4)
5)
Environmental Chemists, Inc
, Of 0 i.Parameter
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a systen
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there a
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations.
Signature ofPreparer * Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM RSSF - B

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: City of Marion Total Dry Tons Applied (Annual): 38.69
Permit #: WQ0019960 Cation Exchange Capacity (non 503 only):
Operator: John Fisher Owner: John Fisher Predominant Soil Series: BrB2
Acres Used: 9.9 Acres Permitted: 9.9 Site #: F1 Field #: FI
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
1
2
3
4j
5
6
7
8
9
11
12
DT/Ac./
0
App.
r
Event
3.91
Arsenic
0.200
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.200
Cadmium
0.200
0.000
0.000
0.000
0.000
0.000
0.000'
_ 0.000
0.000
0.000
0.060
0.000
0.200
Copper
4.424
0.000
0.000
0.000
0.000
0.000
0.000
0.000 `
0.000
0.000
0.060
0.000
4.424
Chromium
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Lead
0.551
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.551
Mercury
0.006
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.006
Molyb-
0.521
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.521
denum
Nickel
0.200
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.060
0.000
0.200
Selenium
0.200
0.000
0.000
0.000
0.000
0.000
0.000
` 0.000
0.000
0.000
1 0.000
0.000
1 0.200
Zinc
11.958
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
11.958
Total
Phos-
184.458
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
######
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a
system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am
aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Al 2-12024
Signature of Land Ap ier Date
DENR FORM MFLSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: City of Marion
Land Owner: John Fisher
Operator: John Fisher
Crop 1 Name: Fescue
WQ Permit #: WQ0019960 Field #: F1
Annual Dry Tons Applied:'38.6951 Site #: F1
Predominant Soil Series: BrB2
Crop 1 Max. PAN: 239 Crop 2 Name:
Acres Utilized: 9.9
Acres Permitted: 9.9
Cation Exchange Capacity (non 503):
Crop 2 Max. PAN:
o c
° °
Q
Volume applied
(enter one) Solids/
Liquid
Cu. Yds Gallons
%
Solids
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
SoilPrecip.
Cond.
(Dry'
Wet,
Moist)inches
Past 24
Hrs.
y
0 'n
Q t?
o �
a -•
0
o
,��
=
S
:o
-
*
TKN
mg/kg
z Y
= �
o
❑ 2
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
(lbs/acre)
Name of Crop
Receiving Re;
Applicatic
Crop I
Crop 2
Crop 1
CI
4-2023
110500
3.32
1.545
WQ0019960
dry
0
s
0.5
0.3
39600
580
14.6
37.119
NA
Fescue
8-2023
169000
3.32
2.363
WQ0019960
dry
0
s
0.5
0.3
39606
580
14.6
56.770
NA :
Fescue
0:000
0.000 ,
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000 `
0.000:
0.000
0.000
0.000
0.000
0:000
0:000
0.000
0.000':
0.000
0.000
0.000"'
0.000
0.000
0.000
0.000
Residuals Applications totals on FORM FSF supp ( attach FORM FSF. supp to this form):
TOTALS
01
2795001,
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se i
Zn
P
93:889
0.000
Lime App
Annual Ibs/acre
0.200
0.200
4.424
0.000
0.551
0:006
0.521 -
0.200 .
0.200`;
11.958
184.458 .
Date
lb
Prior Years Cumulative lbs/ac
0.269
0.184
9.789
0
1.293
0.33
0.684
0.564
0.267
27.668
10-23
21
Current Cumulative lbs/ac
0.469
0.384
14.213
_ 0.000
1.844
0.336
1.205
0.764
0.461
39.626:
Permitted C. P. L. R.****
36
1 34
1338
NA
267
15
NA
374
89
2498
Permit PAN Limit Ist/2nd Crop
239 ;
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure tha
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
ac/G /5 2-1-2024 **Volatilization Rate: Surface - 0.5, Injection/Incorporation -1.0
Signature o and Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobi
digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSI

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Marion
WWTP Name: Corpening Creek
WQ Permit Number:
NPDES Number:
Monitoring Period: From 1/1/2023 To 12/31/2023
WQ0019960
NCO031879
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. A (time/temp) ❑ Alt B (Alk Treatment)[] Alt. C (Prior Testing)[]
A1t.D (No Prior Test) ❑ Process to Further Reduce Pathogengs ❑
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost ❑
Heat Drying ❑
Heat Treatment ❑
Thermophilic ❑
Beta Ray ❑
Gamma Ray ❑
Pasteurization ❑
Class B:
Alt. (1) Fecal Density p
Alt. (2) Process to Significantly Reduce Pathogens ❑
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization ❑ Air Drying ❑
Composting ❑ Aerobic, Digestion ❑
Anaerobic Digestion ❑
...........................................................................................:.............................. .
If applicable to alternative performed (Class A or Class B) complete the following monitoring data:
Parameter
Allowable Level
in Sludge
Pathogen Density
Number of
Excee-
dences
Frequency
of Analysis
Sample
Type
Anal�°
Tech -
n cue
Minimurr
Geo. Mean
Maximum
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
4290
7995.7
16170
MPN/g
0
7
grab
sm9221
CFU
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per 4 grams
total solid (dry
I weight)
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed:
Alt.I (VS reduction) ❑
Alt. 2 (40-day bench) ❑Alt.
3 (30-day bench) ❑
I Alt. 4 (Spec. 02 uptake) ❑..
Alt. 5 (14-Day Aerobic) ❑
Alt. 6 (Alk. Stabilization ❑
Alt 7 (Drying - Stable) ❑
1 Alt. 8 (Drying - Unstable) ❑
Alt. 9 (Injection) ❑
Alt. 10 (Incorporation) ❑
No vector attraction reduction alternatives, were performed ❑
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note
if you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment"
Zach Key U.S. Biosolids, Inc.
Preparer mes and Title (type or print) Land Applier Name and Title (if applicable)(type or print)
Zr R r J� �% 2-1-2024
Signature of reparer* Date Signature of Land pplier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 02T (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: City of Marion WQ Permit #: WQ0019960 Field #: F2 Acres Utilized: 2.4
Land Owner: John Fisher Annual Dry Tons Applied: 16.1979 Site #: F2 Acres Permitted: 2.4
Operator: John Fisher Predominant Soil Series: BrB2 Cation Exchange Capacity (non 503):
Crop 1 Name: Fescue Crop 1 Max. PAN: 239 Crop 2 Name: Crop 2 Max. PAN:
y
U
Q
Volume applied
enter one Solids/
( )
Liquid
9
Cu. Yds Gallons
u
/o
Solids
Volume
A hed er
pp p
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
Soil
Cond.
(Dry'
Wet
Moistinches
Precip.
past 24
Hrs.
y
4 �
o w
a o
o
%n
m �,
Z3
4
Q
Z
TKN
mg/kg
z Y
D
�o o
g
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
(Ibs/acre)
Name of Cror
Receiving Re,
Applicatic
Crop 1
Crop 2
Crop 1
Ci
4-2023
58500
3.32
3.375
W00019960
dry
0
s
0.5
0.3
39600
580
14.6
81.061
NA
Fescue
8-2023
58500
3.32
3.375
WQ0019960
dry
0
s
0.5
0.3
39600
580
14.6
81.061
NA
Fescue
0.000
0.000
0.000
0.000
0.000
0:000:
0.000
0.000
0.000 '
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
ELE0.000
0.000
0.000
Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form):
TOTALS
0
117000
As
Cd
Cu
Cr
PbrH
Mo
Ni
Se''
Zn
P
162,123
0000
LimeAAnnual
lbs/acre
0.346
0,346-
7.641
0.000 -
0.952
0.899
0.346
0.346.
20.655
318.600Date
lb
Prior Years Cumulative lbs/ac
0.326
0.346
9.653
0
1.187
2.364
0.497
0.272
26.637
10-23
2,
Current Cumulative lbs/ac
0.672
0.692
17.294
0.000
2.139
3.263
0.843
0.618
47.292
Permitted C. P. L. R.****
36
34
1338
NA
267
NA
374
891
2498
Permit PAN Limit lst/2nd Crop
:. :.; :, 239
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure tha
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
Signature of Land Applier
*Application Method: S - Surface, IN - Injection, INC - Incorporation
2024 **Volatilization Rate: Surface - 0.5, Injection/incorporation -1.0
Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobi
digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSI

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: City of Marion Total Dry Tons Applied (Annual): 16.20
Permit #: WQ0019960 Cation Exchange Capacity (non 503 only):
Operator: John Fisher Owner: John Fisher Predominant Soil Series: BrB2
Acres Used: 2.4 Acres Permitted: 2.4 Site #: F2 Field #: F2
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw': Percent #):
Sample
or Corn
posite
Date
o
©
©
a
©
o
0
0
o
m
m
m
FIRM
91 NMI
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
1
2
3
4
5
6j
7j
8
9
1101
1
12
DT/Ac./
o
App.
14
Event
6.75
Arsenic
0.346
1 0.000
0.000
1 0.000
0.000
1 0.000
0.000
1 0.000
'0.000
0.000
0.000
0.000
1 0.346
Cadmium
0.346
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.346
Copper
7.641
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
7.641
Chromiurr
0.000
0.000
0.000
0.000
0.000
.0.000`
0.000'
0.000
0.000
0.000
0.000
0.000
0.000
Lead
0.952
0.000
0.000
0.000
0.000
0.000
0.000
0.000'
0.000
0000
0.000'
0.000
0.952
Mercury
0.010
0.000
0.000
0.000
0.000
0.000
0.000 `
0.000
0.000
0.000
0.000
0.000
0.010
Molyb-
0.899
0.000
0.000
0.000
0.000
0.000
0.000
0.000'
0.000
0.000
0.000
0.000
0.899
denum
Nickel
0.346
0.000
0.000
0.000
0.000
0.000
-0.000 -
0.000,
0.000
0.000
0.000
0.000
0.346
Selenium
0.346
0.000
0.000
0.000
0.000
- 0.000
0.000
0.000
1 0.000
0.000
0.000
0.000
0.346
Zinc
20.655
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
20.655
Total
Phos-
318.600
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
######
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a
system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am
aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
�� �i. L 2-1-2024
Signature of LanffApplier Date
DENR FORM MFLSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: City of Marion
Land Owner: John Fisher
Operator: John Fisher
Crop 1 Name: Fescue
WQ Permit #: WQ0019960 Field #: F3 Acres Utilized: 7
Annual Dry Tons Applied: 44.0944 Site #: F3 Acres Permitted: 7
Predominant Soil Series: HaC ,Cation Exchange Capacity (non 503):
Crop 1 Max. PAN: 202 Crop 2 Name: Crop 2 Max. PAN:
o C
O
Q
Volume applied
PP
(enter one) Solids/
Liquid
Cu. Yds Gallons
%
Solids
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
Soil
Cond.
(Dry,
Moist
Precip.
Past 24
Hrs.
inches
y
4 'b
rn S.
o a
a
* �
o
w
v �.
N
m
0
�
7y
*
* 0
TKN
mg/kg
Z Y
�o o
q ?
w
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
(1bs/acre)
Name of Crop
Receiving Re
Applicatic
Crop 1
Crop 2
Crop 1
Cr
4-2023
84500
3.32
1.671
WQ0019960
dry
0
s
0.5
0.3
39600
580
14.6
40.145
NA '
Fescue
6-2023
110500
3.32
2.185
W00019960
dry
0
s
0.5
0.3
39600
580
14.6
52.497
NA
Fescue
11-20231
123500
3.32
2.443
WQ0019960
dry
0
s
0.5
0.3
39600
580
14.6
58.673
NA
Fescue
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000'
0.000
0.000
0.000
0.000
1 0.000
Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form):
TOTALS
o
318500
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn
I P
151.314
o:Obo
Lime App
Annual lbs/acre
0.323
0.323
7.130
0.000-
- 0.888
0,009
0.839
0.323
0.323
19.275
297.313
Date
lb
Prior Years Cumulative Jbs/ac
0.538
0.285
16.415
0
2.136
0.064
1.096
0.878
0.534
43.835
10-23
2
Current Cumulative lbs/ac
0.861 -'
0.608
23.545
0.000
3.024
0.073
1,935':
1.201
0.857
63.110
Permitted C. P. L. R.****
36
34
1338
NA
267
15
NA
374
89'
2498
Permit PAN Limit l st/2nd Crop
:. - : 202
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure tha
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
Signature oftand Applier
2-1-2024
Date
*Application Method: S - Surface, IN - Injection, INC - Incorporation
**Volatilization Rate: Surface - 0.5, Injection/Incorporation -1.0
*** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobi
digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSI

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: City of Marion Total Dry Tons Applied (Annual): 44.09
Permit #: WQ0019960 Cation Exchange Capacity (non 503 only):
Operator: John Fisher Owner: John Fisher Predominant Soil Series: HaC
Acres Used: 7 Acres Permitted: 7 Site #: F3 Field #: F3
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw''Percent #):
Sample
. Com-
posite
Date I
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
1
_2j
3
4
5
6
7
8
9
10
11
12
DT/Ac./
o
App.
Event
6.30
Arsenic
0.323
1 0.000
0.000
- 0.000
0.000
' 0.000
'0.000
0.000
0.000
0.000
1 0.000
0.000
0.323:
Cadmium
0.323
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.0000..000
0.323
Copper
7.130
0.000
0.000
0.000
0.000
0.000
0.000
0.000
' 0.000
0.000
0.000
0.000
' 7.130
hromi
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000 `
0.000
0.000'
0.000
0.000
0.000
Lead
0.888-
0.000
0.000
0.000
0.000
0.000
0.000
0.000`
0.000
0.000
0.600
0.000
0.888
Mercury
0.009
0.000
0.000-
-0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.009
Molyb-
0.839
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.839
denum
Nickel
0.323'
0.000
0.000
0.000
0.000
0.000
> 0.000
0.000
0.000
0.000
0.000
0.000
0.323
Selenium
0.323
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1 0.000
0.000
0.323
Zinc
19.275
0.000
0000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
19.275
Total
Phos-
297.313
0.000
0.000'
0.000
0.000
0.000
0.000
0.000 '
0.000
0.000'
0.0.00
0.000
######
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a
system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am
aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
4a /l 2-1-2024
Signatu a of Land A lier Date
DENR FORM MFLSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: City of Marion WQ Permit #: W00019960 Field #: F4 Acres Utilized: 6.7
Land Owner: John Fisher Annual Dry Tons Applied: 44.0944 Site #: F4 Acres Permitted: 6.7
Operator: John Fisher Predominant Soil Series: HaC Cation Exchange Capacity (non 503):
Crop 1 Name: Fescue Crop 1 Max. PAN: 202 Crop 2 Name: Crop 2 Max. PAN:
° y
i °
-1
Volume applied
(enter one) Solids/
Liquid
Cu. Yds Gallons
�/a
Solids
Volume
A lied er
pp p
Acre
(DryTons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
SoilPrecip.
Cond.
(Dry'
pjst
Past 24
Hrs.
inches
y
t?
o
o. _
* °
o
N'
w
�
°
*
TKN
mg/kg
z Y
Ei
o 3
�.
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
(lbs/acre)
Name of Crop
Receiving Re.
Applicatir
Crop 1
Crop 2
Crop 1
Cr
4-2023
130000
3.32
2.686
W00019960
dry
0
s
0.5
0.3
39600
580
14.6
64.526
NA
Fescue
6-2023
97500
3.32
2.015
WQ0019960
dry
0
s
0.5
0.3
39600
580
14.6
48.395
NA
Fescue
11-2023
91000
3.32
1.880
W00019960
dry
0
s
0.5
0.3
39600
580
14.6
45.168
NA -
Fescue
0.000
0.000
0.000 "
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000 -
0.000
0.000`
0.000
0.000
0.000
0.000
0.000
0.000 '
0.000
0.000
0.000 `
0.000
0.000
0.000
0.000
Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form):
TOTALS
01
318500
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn
P
158090
0.000
Lime App
Annuallbs/acre
0.337
0.337
7.450
0.000
0.928
0.009
0.877
0.337
0.337
20.138
310.623
Date
lb
Prior Years Cumulative lbs/ac
1 0.525
1.036
20.494
0
2.585
0.077
1.12
1.063
0.535
50.385
10-23
2,
Current Cumulative lbs/ac
0.862
1.373
27.944
0.000
3.513
0.086
1.997
1.400
0.872
70.523
Permitted C. P. L. R.****
36
34
1338
NA
267
15
NA
374
89,
2498
Permit PAN Limit Ist/2nd Crop
202
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure tha
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
2-1-2024
Signature of Land Applier Date
*Application Method: S - Surface, IN - Injection, INC - Incorporation
**Volatilization Rate: Surface - 0.5, Injection/Incorporation -1.0
*** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobi
digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSI

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: City of Marion Total Dry Tons Applied (Annual): 44.09
Permit #: WQ0019960 Cation Exchange Capacity (non 503 only):
Operator: John Fisher Owner: John Fisher Predominant Soil Series: HaC
Acres Used: 6.7 Acres Permitted: 6.7 Site #: F4 Field #: F4
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
cc .
Annual Heavy Metal Field Loadinj4s (Calculated in lbs/acre):
Total
1
2
3
4
5j
6
7
8
9
10
11 1121
DT/Ac./
0
0
App.
y
Event
6.58
Arsenic
0.337
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
O.600
0.000
0.337
Cadmium
0.337
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.600
' 0.000
0.337-
Copper
7.450
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.600
0.000
7.450
Chromium
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Lead
0.928
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.928
Mercury
0.009
0.000
0.000
0.000
0.000 -
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.009
Molyb-
0.877
0.000
0.000
0.000 `
0.000 '
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.877
denum
Nickel
0.337
0.000
0.000
0.000-
0.000
'.0.000
0.000
0.000
0.000
0.000
0.000
:0.000
0.337'
Selenium
0.337
0.000
0.000
0.000
0.000
0.000
.0.000
0.000
0.000'
, 0.000
0.000
0.000
0.337
Zinc
20.138
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000-
0.000
0.000
0.000
20.138
Total
Phos-
310.623
0.000
0.000
0.000
0.000
0.000
0.000 '
0.000
0.000
0.000
0.000
0.000
######
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a
system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am
aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
K 2-1-2024
Signature f Land App r Date
DENR FORM MFLSF (12/2006)

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
i
Specific Oxygen Uptake Rate
SOUR j
e: Corpening Creek
Biosolids Permit Nu
Sampling Date/Time
Sampled By
Analysis Date/Time
Analyzed By
Sample Volume
Total Solids
Beginning Temperature
End Temperature
Dissolved Oxygen Level
Celsius
milliliters
Yo Dry Solids
iegrees Celsius
iegrees Celsius
Slope:
0.11
Intercept:
8.0!
Correlation'Coefficient:
1.01
Oxygen Uptake Rate:
3.53 mg Oxygen/hr
Ambient Specific Oxygen Uptake Rate:
0.18 mg Oxygen/g/hr
Average Temperature:
251degrees Celsius
Temperature Correction Factor: 0.783526'
Temperature Corrected Specific Oxygen Uptake R<
Instructions: Enter Data in the Blue Boxes. The Calculation
0.14mg Oxygen/glhr
i
I the Spreadsheet execute automatically.

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen L
SOUR
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor: 0.
Rate
Celsius
Dry Solids,
grees Celsius
orees Celsius
0.1''.
8.41
1.0
3.38i mg Oxygen/hr
0 18 mg Oxygen/g/hr
25 degrees Celsius
Temperature Corrected.SpeciftcOxygen Uptake Ri
Instructions: Enter Data in the Blue Boxes. The Calculation
Oxygen/g/hr
J the Spreadsheet. execute automatically.

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility
Biosolids Permit.N
Digester Temperat
Sampling Datefri
Sampled
Analysis Datelr
Analyzed
Sample Volu
Total Sol
Beginning Temperat
End Temperat
Dissolved Oxygen Level
rees Celsius
% Dry Solids
degrees Celsius
degrees Celsius
Slope: 0.1
Intercept: 8:9!.
Correlation Coefficient: 1.0•
Oxygen Uptake Rate: 3,621 mg Oxygen/hr
Ambient Specific Oxygen Uptake Rate: 0.191 mg Oxygen/g/hr
Average Temperature: 251'degrees Celsius
Temperature Correction Factor: 0.783526166'
Temperature Corrected Specific Oxygen Uptake Rate:1 0.15 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
Specific Oxygen Uptake Rate
SOUR
Facility Name
Biosolids Permit Number
Date
Digester Temperature
Sampling Date/Time
Sampled By
Analysis Date/Time
Analyzed By
Sample. Volume
Total Solids
Beginning Temperature
End Temperature
Dissolved Oxygen Level
Corpening Creek
WQ 0019960
3/11/2023
15
3111123 0819
JW
3111 /23 0825
RGC'
1000
1.94
25
25
iegrees Celsius
milliliters
% Dry Solids
degrees Celsius
degrees Celsius
15 1
Slope: 0.1
Intercept: 8.2
Correlation Coefficient: 1.0
Oxygen Uptake Rate: 3.00 mg Oxygen/hr
Ambient Specific Oxygen Uptake Rate: 0.15 mg Oxygen/g/hr
Average Temperature: 25 degrees Celsius
Temperature Correction Factor: 0.783526166
Temperature Corrected Specific Oxygen Uptake Rate�� 0.12 mg Oxygentg/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Specific Oxygen Uptake Rate
SOUR
Facility Name
Biosolids Permit Number
Date
Digester Temperature
Sampling Date/Time
Sampled By
Analysis Date/Time
Analyzed By
Sample Volume
Total S01ids
Beginning Temperature
End Temperature
Time
(minutes)
0
1
2
3
4
5
6'
7
8
9
10
11
12
13
14
15
Corpening Creek
WQ 0019960
3/10/2023
16
3/10123 0835
TH
3/10/23 091.1
NR
1000
25
25
3egrees Celsius
milliliters
legrees Celsius
Degrees Celsius
Slope: 0.1-
Intercept: 7.6
Correlation Coefficient: 1.0
Oxygen Uptake Rate: 3.27 mg Oxygen/hr
Ambient Specific Oxygen Uptake Rate: 0:16 mg Oxygen/g/hr
Average Temperature: 25degrees Celsius
TemperatureCorrection Factor: 0.783526166
Temperature Corrected Specific Oxygen Uptake Rate:— 0:13 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Time
(minutes).
0
1
2
3
4
5
6
7
8
9
Specific Oxygen Uptake Rate
SOUR
Facility Name
Biosolids Permit Number
Date
Digester Temperature
Sampling Date/Time
SampledBy
Analysis Date/Time
Analyzed By
Sample Volume
Total' Solids
Beginning Temperature
End Temperature
Dissolved .Oxygen Level
Corpening
Creek
WQ 0019960
3/9/2023
19
3/9/23
0925
im
3/9/23
1106
RGC
1000
1.99
2511
25
iegrees Celsius
Milliliters
'lo Dry Solids
jegrees Celsius
9egrees Celsius
10 7.86
11 7.81
12 7.76
13 7.71
14 7.65
15 7.6
Slope: 0.1
Intercept: 8.4
Correlation Coefficient: 1.0
Oxygen Uptake Rate: 3.26 mg Oxygen/hr
Ambient Specific Oxygen Uptake Rate: 0.16 mg Oxygen/g/hr
Average Temperature: 25 degrees, Celsius
Temperature Correction Factor: 0.783526166'
Temperature Corrected Specific Oxygen UptakeRate:l 013 mg'Oxygen/g/ir
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name
Biosolids Permit Number
Date
Digester Temperature
Sampling Date/Time
Sampled By
Analysis DatefTime
Analyzed By
Sample Volume
Total Solids
Beginning Temperature
End Temperature
Dissolved Oxygen Level
Corpening Creek
WQ 0019960
3/8/2023
19
3/8/23 1610
DS
3/8/23 1640
RGC
1000
1.96
25
25
iegrees Celsius
milliliters
%. Dry Solids
iegrees Celsius
iegrees Celsius
Slope: 0.1
Intercept: 7.2-!
Correlation Coefficient: 1.0
Oxygen Uptake Rate: 3.57;mg Oxygen/hr
Ambient Specific Oxygen Uptake Rate: 0.18;mg Oxygen/g/hr
Average Temperature: 25 degrees Celsius
Temperature Correction Factor: 0.783526166
Temperature Corrected Specific Oxygen Uptake Rate:1 41mg Oxygen/g/hr
Instructions: Enter Data in the BlueBoxes. The Calculation and the Spreadsheet' execute automatically.

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name
Biosolids Permit Number
Date
Digester Temperature
Sampling DatelTime
Sampled By.
Analysis Date/Time
Analyzed By
Sample Volume.
Total Solids
Beginning Temperature
End Temperature
Slope:
Intercept:
Correlation Coefficient:
Corpening Creek
WQ 0019960
3/7/2023
19
317/23 1358
Dustin Saine
3/7/23 1436
R. Carter
1000
1.94
25
25
OA
7.9
1.0
milliliters
-Dry Solids.
iegrees Celsius
legrees Celsius
Oxygen Uptake Rate: 2.96 mg Oxygen/hr
Ambient Specific Oxygen Uptake Rate: 0.15'mg Oxygen/g/hr
Average Temperature: 25 degrees Celsius
Temperature Correction Factor: 0.783526166
Temperature Corrected Specific Oxygen Uptake Rate:i�" 121mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

�mr P,0 Box 7565
Asheville, NC 28802
=" i Phone: [phone]
I� Fax: [phone]
Environmental Testing Solutions, Inc. Certificate of Analysis
Project name: Marion WNVTP Project number: 230206.504
Collection date: 6-Feb 23
Date received: 6-Feb-23
Sample identification: Sludge#i - Grah
Sample number:
234729
Parameter
Method
Result
RL
Units
Date' Analyst
Footnotes
Analyzed
%TS
SM 2540 G
3.3
0.10
%
6:F6.23 KEK
Mulitple Tube Fermentation Procedure
SM 9221-E
4950
5.9
MPN
6-Fc6.23 KEK
Sample identification: Sludge #2 - Grab
Sample number:
23473.0
Parameter
Method
Result
RL
Units
Date
Y Anal st
Footnotes
Analysed
%TS
SM 2540 G
3.4
0.10
%
6-Fcb-23 KEK
Mulitple Tube Fermentation Procedure
SM 0221-E
5780
6.1
MPN
6-Feb-23 KEK
Sample identification: Sludge #. Grab Sample number: 234731
Parameter Method Result RL Units pate Analyst Footnotes
Analyzed
%TS SM 2540 G 3.3 0a0 % 6-Feb-23 KEK
Mulitpic Tube Fermentation Procedure SM 9221-E 4290 5.9 MPN 6-Feb-23 KEK
Sample identification: Sludge #4 Grab Sample number: 234732-
Parameter Method Result RL Units Date Analyst Footnotes
Analyzed
%TS SM 2540 G 3.3 0.10 % 6-Fcb-23 KEK
Mulitple Tube Fermentation Procedure SM 9221-E 6600 5.9 MPN 6.r&-23 KEK
Footnotes:
RL = Reporting Limit. Values are reported down to the Reporting Limit only.
Date reviewed: NC Certification Number: 600
Data reviewed by: Kelley E. Keenan SC Certification Number: 99053
Signature: NC Drinking Water Certification Number:: 37786
This report should not be reproduced, ,exepttn its entirety; without theamlten consent of Environmental Testing Solutions, Inc
The results in this report relate only to the samples submitted for analysis.

PO Box 7565
Asheville, NC 28802
Phone: [phone]
1 Fax: [phone]
' Environmental Testing Solutions, Inc- Certificate of Analysis
Project name: Marion WWTP
Project number:
230113.503
Collection date:
13-Feb-23
Date received:
13-Feb-23
Sample identification:
Sludge #5 - Grab
Sample number:
235088
Parameter
Method
Result
RL
Units
Date
Analyst
Footnotes
Analyzed
%TS
SM 2540 G
3.3
0.10
%
13-Feb-23 KEK
Mulitple Tube -Fermentation Procedure
SM 9221-E
16170
5.9
MPN
13-Feb-23 KEK
Sample identification:
Sludge tf6 - Grab
Sample number:
235089
Parameter
Method
Result
RL
Units
Date:
Analyst
Footnotes
Analyzed
SM 2540 G 3.3 0.10 % 13-Fob-23
Tube Formentatio
Sample identification: Sludge#7 Grab Sample number: 235090.
Parameter Method Result RL Units Date Analyst Footnotes
Analyzed
%TS SM 2540 G 3.3 0.10 % 13-Feb-23 KEK
Mulitple Tube Fermentation Procedure SM 9221-E 10890 5.9 MPN 13-Fob-23 KEK
rootnotes:
RL = Reporting Limit. Values are reported down.to the Reporting Limit only.
Date reviewed: NC Certification Number: 600
Data reviewed by: _ Kelley E. Keenan SC Certification Number: 99053
NC Drinking Water, Certification Number: 37786
Signatures P11-1
This report should not be reproduced, exept in its entirety, without the written consent of Environmental Testing Solutions; Inc
The results in this report relate only to the samples submitted for analysis.

r PO Box 7565
Asheville; NC 28802
Phone: [phone]
May, tax: [phone]
t
Environmental Testing Solutions, Inc. Cutificate Of Analysis
Project name: City of Marion Project number: 230213.505
Collection date: 13-Feb-23
Date received: 1.3-Feb-23
Sample identification: FS TCLP - Grab
Sample number:
235094
Parameter
Method
Result
RL
Units
Date
Analyst
Footnotes
Analyzed.
Arsenic-TCLP
200.7
<1.0
1.0
mg/L
10-et,-23
ECHEM
I
Barium - TCLP
200.7
<1.0
1.0
mg(L
2o-F.b-23
ECHEM
1
Cadmium -TCLP
200.7
<1.0
1.0
mg(L
20-Fdr23
ECHEM
1
Chromium- TCLP
200.7
<1.0
1.0
mg/L
20-F6-23
ECHEM
1
Lead - TCLP
200.7
<1.0
1.0
mg/L
20-FA-23
ECHEM
1
Selenium -TCLP
200.7
<1.0
1.0
mg(L
20.Fcb-23
ECHEM
I
Silver-TCLP
200.7
<1.0
1.0
mg(L
20-F&-23
ECHEM
I
Mercury- TCLP
245.1
<0.0002
0.0002
mg(L
20-17643
ECHEM
1
Full. Scan TCLP Organics
See attached sheets
ECHEM
1,2
Reactive Cyanide
335.4
1.30
mg/kg
is-Fl b-23
ECHEM
t
Reactive Sulfide
SM4500SD
0.09
0.05
mg/kg
15-Fc6-23
ECHEM
I
Ignitability
SW 846 1010
>157
157
eF
i5-Fcw32
ECHEM
I
Arsenic
200.7
<25.6
mg/kg
20-Fcb-23
ECHEM
I
Cadmium
200.7
<25.6
mg/kg
20-frii.23
ECHEM
1
Copper
200.7
566
mg/kg
2o-Feb-23
ECHEM
I
Lead
200.7
70.5
mg/kg
2o-r b-23
ECHEM
1
Molybdenum
200.7
66.6
mg(kg
20-Feb-23
ECHEM
1
Nickel
200.7
<25.6
mg/kg
20 Feb-23
ECHEM
1
Selenium
200.7
<25.6
mg/kg
2o-Feb-23
ECHEM
I
Zinc
200.7
1530
mg/kg
20-Feb-23
ECHEM
1
Aluminium
200.7
13100
mg/kg
23.Fcn-23
ECHEM
Calcium
200.7
16800
mg/kg
20•Feb-23
ECHEM
1
Magnesium
200.7
5090.
mg/kg
20-FcW3
ECHEM
I
Potassium
200.7
4490
mg/kg
20-Feb-23
ECHEM
I
Sodium
200.7
1460
mg(kg
20-Fea23
ECHEM
1
Mercury
SW84674719
0.711
mg/kg
2o-Feb-23
ECHEM
1
Total KjcldahlNitrogen
351.2
39600
mg(kg
3-M.-23
ECHEM
1
Nitrate +Nitrate - Nitrogen
353.2
14.6
mg/kg
i7-Febc23
ECHEM
I
Total Phosphorus
200.7
23600
mg/kg
2-Mar-23
ECHEM
1
Total Solids (%)
SM 2540 B
3.32
%16•Fcb-23
ECHEM
I
% Total Solid
SM 2540 G
3.3
%
13-176-23
KEK
Ammonia Nitrogen
SM 4500 NH3 D
580
61
mg/kg
i6-Feb 23
KEK
N- Pav
Calculation
12011
mg/kg
10-Mar-23
KEK
Sodium Adsorption Ratio (SAR)
Calculation
14
mg/kg
10-Mar-23
KEK
pH
SW9469040C
5.0
0.1
S.U.
134.b-23
KEK
3_
not oe reproaucca, excpcm its enarety, wnnout inc }mucu consent m
The results in this report relate only to the samples submitted

ELM
Environmental Testing Solutions, Inc. Certificate of Analysis
Pa Box 7565
Asheville; NC 28802
Phone: [phone]
Tax: [phone]
Footnotes:
RL = Reporting Limit. Values are reported down to the Reporting Limit only.
1. Sample analzyed by Enviro Chemists, Inc.
2. Analyzed on 02-I6-23,02-18-23 and 02-22-23.
3. Sample received and analzyed outside hold time.
Date reviewed:' •� 5'2 3 NC.Certification,Number: 600
Data reviewed by: Kelley E. Keenan SC Certification Number: 99053
t 1 NC Drinking Water Certification Number: 37786
Signature: V"
This report should not be reproduced, exeptin its entirety, without the written consent of Environmental Testing Solutions; Inc.
The results in this report relate only to the samples submitted for analysis.

Environmental Chemists, Inc.
• 6602 Windmill Way, Wilmington, NC 28405 91.0.392.0223 Lab . 910.392.4424 Fax
710 Bowsertown Road„Manteo, NC 27954 . 252.4735702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 + 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS [e-mail]
Environmental Testing Solutions, Inc. Revised Report: Mar 14, 2023
Post Office Box 7665Original Report Date: Mar 08, 2023
Asheville NC 28802 Report#: 2023-02965
Attention: Customer ID: 08100055
Project;10: Marion WWfPSludge
Lab ID Sample ID: Collect DatefTime Matrix Sampled, by
23-07308 Site: CC - Sludge 2/13/2023 7:32 AM Sofid/Sludge Client
Test Method Results Date Analyzed
Aluminum
EPA' MY. Rev.4.4,1904
13100mglkg
02/23/2023
Arsenic
EPA 200.7. Rev. 4.4,1464
<25.6; mglkg
02/20/2023
Cadmium
EPA200,T Rev, 4A.1994
<25.6mglkg
02/20/2023
Calcium
EPA 2W.7. Rev.4A. teal
16800 mglkg
0212012023
Copper
EPA 2007.,Rev. 4.4, IM
566 mglkg
02/20/2023
Lead
EPA 200.7, Rev, 4.4.1994
70.5 mg/kg
02/20/2023
Magnesium
EPA 200.7. Rev. 4.4.1994
5090mg/kg
02/20/2023
Molybdenum
EPA 200.7.ReP.4A, IM
66.6mg/kg
02/20/2023
Nickel
EPA 200.7. Rev. 4.4.104
<25.6 mglkg
02/20/2023
Potassium
EPA 2W.7.Rev. 4.4,t094
4490mg/kg
02/20/2023
Selenium
EPA 20o.T, Rev.4.4,1004
<25.6 mglkg
0212072023
Sodium
EPA2W.7, Rev.4.4aa94.
1460 mglkg
02/20/2023
Zinc
EPA 200.7, Rev.4.4,1004
1530 mglkg
02/20/2023
Total Solids (%)
sM2540 8
3 32 %
02/16/2023
Total Kieldahl Nitrogen (TKN)
SM45W"8-2011
39600mglkg
03/03/2023
Total Phosphorus
SM4500P(F-0•2at1
23600mg/kg
03fO2/2023
Mercury
SW -US 7471 B
0.711 mg/kg
02/20/2023
Chlordane (TCLP)
SW_"a owl a
<0.02 mg/L
02/16/2023
Endrim(TCLP)
SW-e46 eo81 a
<0.0005mg/L
02/16/2023
Heptachlor (TCLP)
SWS48 $0818
<0.0005 mg/L
02/16/2023
Heptachlor epoxide (TCLP)
Sw-s4sWei e
<0.0005mg1L
02/16/2023
Undane (TCLP)
SW448 $081. a
<0.0005 mg/L
02/1W2023
Methoxychlor (TCLP)
SW-848 goal a
<0.0005 mg/L
02/16/2023
Toxaphene (TCLP)
sw-ma 8081 a
<0.05 mg/L
02116/2023
2,4,5-TP (TCLP)
SWU68151 A
<0.003 mg/L
02/1612023
2,4-D (TCLP)
SW-8458151 A
<0.603 mg1L
02/16/2023
RepodC. 2023-02065
Pape 1013

PPPPEnvironmental
Chemists, Inc.
/
6602 Windmill Way, Wilmington, NC 28405 . 910.392.0223 Lab '. 910392.4424 Fax
710136wsertown Road, Manteo, NC 27954 . ,252:473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 . 910.347.5843Lab/Fax
ANALYTICAL $ CONSULTING, CHEMISTS
info 'genvironmentalchemismcom
Environmental Testing Solutions, Inc.
RevisedReport: Mar 14, 2023
Post Office Box 7565
Original Report Date: Mar 08, 2023
Asheville NC 28802
Report#: `2023-02965
Attention:
Customer ID: 08100055
Project 10: Marion WWTP Sludge
1,4-Dichlorobenzene(TCLP)
SW-9468270E
<0.050mg/L
02/22/2023
2,4,5-Trichlorophenol (TCLP)
sw-8488270 E
<0.050 mg/L
02122/2023
2,4,6-Trichiorophenol (TCLP)
SW-W 8270 E
<0.050 mg/L
02/22/2023
2,4-Dinitrotoluene (TCLP)
SW-848 8270 E
<0.050 mg/L
02122/2023
Cresol (TCLP)
SW-848 8270 a
<0.050 mg/L
0212=023
Hexachloro-1,3-butadiene (TCLP)
SW-8 e270 E
<0.050 mg/L
02122/2023
Hexachlorobenzene (TCLP)
swa48 827o a
<0.050 mg/L
02122/2023
Hexachloroethane (TCLP)
SW-8480270E
<0.050mg/L
02122/2023
m + p-Cresol (TCLP)
SW,848 8270 E
<0.050 mg/L
02/22/2023
Nitrobenzene (TCLP)
SW448 8270 E
<0.050 mg/L
02/22/2023
o-Cresol (TCLP)
SW-848 6270 E
<0.050 mg/L
02122/2023
Pentachlorophenol (TCLP)
SW-84e 8270 E
<O.250 mg/L
02122/2023
Pyridine (TCLP)
SW-8468270E
<0:650mg/L
02/22/2023
1,1-Dichioroethylene(TCLP)
$w-84eMe#W82M
<0.01mg/L
2118/2023
1,2-Dichloroethane (TCLP)
sw-846 Mest,od e2eoo
< 0.01 mg/l.
2/18/2023:
Benzene (TCLP)
SW-848 McNod 8260D
< 0.01 mg/L
2/18/2023
Carbon Tetrachloride (TCLP)
sw-U8 Meelod e2wo
< 0.01 mg/L
2/1,812023
Chlorobenzene (TCLP)
SW448 Magw! VwD
<0.01 mg/L
2/18/2023
Chloroform (TCLP)
SW446 Me#W 82800
<0.01 mg/L
211W023
Methylethylketone (TCLP)
SW446 Me#W 82WD
< 0.05 mg/L
2/1812023
Tetrachloroethylene (TCLP)
SW448 McOW 82600
< 0.01 mg/L
2/18/2023
Trichloroethylene(TCLP)
SW446Method02ND
<0.01mg/L
211WO23
Vinyl Chloride (TCLP)
SW446 Method 82800-
< 0.01 mg/L
211.8/2023
Total Nitrogen
Total Hihr W
39600mg/kg
03/0712023
RCI
Cyanide
SM 4500 CN D•2018
1.30mglkg
02/15/2023
Sulfide
SM4660S0
0.09mglkg
02/15/2023'
Ignitability
SW 848 me&W 1010
>157 °F
02/15/2023
TCLP Metals
Report B:: 202"2885 Pape 2 0 3

. F ---71 Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 . 910.392.0223 Lab . 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 . 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 . 910.3473M3 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS [e-mail]
Environmental Testing Solutions, Inc,
Revised Report:
Mar 14, 2023
Post Office Box 7665
Original Report Date:, Mar 08, 2023
Asheville NC
28.802
Report #:
2023-02965
Attention:
Customer ID:
08100055
Project ID:
Marion WWTP Sludge
Arsenic (TCLP)
EPA 200.7, Rev. 4.4.1984
<1.0 mg/L
02/20/2023
Barium (TCLP)
EPA 200.7, Rev. 4.4,1994
<1.0 mg/L
02/2012023
Cadmium (TCLP)
EPA200.7, Rev.4A,1994
<1.0'mg/L
02120/2023
Chromium (TCLP)
EPA200.7, Rev, 4.4.1994
0.0 mg/L
02/20/2023
Lead (TCLP)
EPA200.7, Rev.4A,.1994
<1,0 mg/L
02/20/2023
Selenium (TCLP)
EPA200.7,Revr4.4.1994
<'1.0mg/L
02/20/2023
Silver (TCLP)
EPA200.7, Rev; 4.4,1994
<1.0 mg/L
02/20/2023
Mercury (TCLP)
EPA245.1
<0.0002 mg1L
02/20/2023
Total Nitrogen (calc)
EPA 353:2
Comment: Sludqe residual results reported on a;dry
Reviewed by:
02/17/2023
AMENDED 03-14-2023to add Selenium
Pap 3:or3
Reportlt: 2023.02065

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Environmental Chemist, Inc., Wilmington, NC Lab #94
6602 Windmill Way
Wilmington, NC 28405
n ,� Sample Receipt Checklist 910.392.0223
Client: 3 `rt a.t'i or1, ET'S Date:
1 �?� iseport Number: 2023- 2_ Dcj
Receipt of sample: ECHV Pickup ❑ Client Deliver ❑ ��
YES ❑ NO ❑ N Y UPS'O iedEr. Other 1. Were custody seals present on the cooler? YES ❑ NO ❑ N(A 2: if custody seals were present, were they intaoct/unbrken?
Original temperature upon receipt I -C
—j— Corrected temperature upon receipt _
How temperature taken: ❑ Temperature Blank 'C
Itgainst Bottles
IR Gun ID: Thomas Traceable SJN 210886869 IR Gun Correction Factor'C: 0;0
YES ❑ NO 3. If temperature of cooleuexceeded 6'C, was Praject Mgr./QA, notified?
YES ❑ NO 4. Were proper custodyprocedures(relinquished/ret;eived)fotlowed?'
YES ❑ NO 5. Were sample 10's listed on the COC?
YES ❑ NO 6. Were samples ID's listed on sample containers?
YES ❑ NO 7. Were collection date and time listed on the COC?
YES ❑ NO 8. Were tests to be performed listed on the COC?
YES ❑ NO 9. Did samples arrive in proper containers for each test?
YES ❑ NO 10. Did samptesarrive in good condition for each test,
YES ❑ NO 11. Was adequate sample volume available?'
YES ❑ NO 12. Were samples received within proper holding time for ❑ YES ❑ NO 13. Were --I----- . samples received at a;pH of cz? requested tests?
❑ YES O NO 14. Were cyanide .samples received at a pH >12?
❑ YES ❑ NO 15. Were sulfide samples received at a pHa9?
❑ YES ❑ NO 16. Were NH3/TKN/phenol received at a chlorine residual of <D,5 m/L?
❑ YES ❑ NO 17. Were>Suffide/Cyanide received at a chlorinresidual of <0:5 m/L?
D YES ❑ NO 18. e Were orthophosphate samples filtered in the field within 15 minutes?
' TOE/votatiles are pH checked at time of analysis and recorded on the benchsheel
't Bacteria samples are checked for Chlorine at time of analysis and recorded on the benchsheet.
Sample Preservation: (Must be completed for any sample(s) incorrectly prese
;ample(s) rved or with headspace).
were received incorrectly preserved and were adjusted accordingly
)y adding (circle one): H2S0_ HNO3 MCI NaOH
rime of preservation: If more than one preservative is needed, notate in comments
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cufy the state tab rf d,reaed to anaiyxed by thocustomer, Suno::as nobr•eo. cote<ard t••ne• —
'olafiles 5ample(sj were received with headspaee

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NCDA&CS Agronomic Division Phone: [phone]Website: www.ncagr.gov/Divisions/Agronomic-Services
Report No.
,c-uGJutie.t,
Client: John Fisher,
Advisor: Zach Key
Predictive
400 Dairy Rd.
Southern S
Maggie Valley, NC 28751
958 Hoots
Mehlich-3 Extraction
Soil R� po �
Roaring Ri,
Sampled County :McDowell
Soil Testing Section
Client ID: 478472
Advisor ID: 231 E
Sampled:11120/2023 Received: 11/27/2023 Completed: 01/26/2024 Farm:
Sample ID: F1
Recommendations: Lime
Nutrients (lb/acre)
Crop (tons/acre) N P205
K20 Mg S Mn
Zn
Cu B
Lime History:
1- Fescue/OGrass/Tim, M 0.0 120-200 0
0 0 0 pH$
0
0 0
2- Fescue/OGrass/Tim, M 0.0 120-200 0
0 0 0 pH$
0
0 0
Test Results [units - WN in g/crrli; CEC and Na in meg1100 cm?; NO3-N in mg/dm3]:
Soil Class: Mineral
HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg%
S-1
Mn-I Mn-All Mn-AI2 Zn-I
Zn-AI
Cu-I Na ESI
0.46 0.86 19.5 94 1.2 6.8 490 121 83 8
60
80 54 54 994
994
1708 0.0
Sample ID: F2
Recommendations: Lime
Nutrients (lb/acre)
Crop (tons/acre) N P205
K20 Mg S Mn
Zn
Cu B
Lime History:
1- Fescue/OGrass/Tim, M 0.0 120-200 0
30 0 0 0
0
0 0
2- Fescue/OGrass/Tim, M 0.0 120-200 0
30 0 0 0
0
0 0
Test Results [units - WN in g/cd; CEC and Na in meq/100 cm3; NO3-N in mgldrrr3]:
Soil Class: Mineral
HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg%
S-1
Mn-I Mn-All Mn-Al2 Zn-I
Zn-AI
Cu-1 Na ESI
0.51 0.97 13.6 89 1.6 6.3 432 59 79 7
54
130 90 90 691
691
1201 0.0
North Carolina
Ak -
Tc3tmm) Trust FmW CtN iri%ilm
Reprogramming of the laboratory -information -management system that makes this report possibl
through a grant from the North Carolina Tobacco Trust F
Thank you for using agronomic services to manage nutrients and safeguard envir
- Steve Troxler, Commissioner of A,

NCDA&CS Agronomic Division Phone: [phone] Website: www.ncagr.gov/Divisions/Agronomic-Services
Report No.
John Fisher
Sample ID: F3
Recommendations: Lime
Nutrients (lb/acre)
Crop (tons/acre)
N P2O5
K2O
Mg S
Mn
Zn
Cu
B
Lime History:
1- Fescue/OGrass/Tim, M 0.0
120-200 0
0
0 0
pH$
0
0
0
2- Fescue/OGrass/Tim, M 0.0
120-200 0
0
0 0
pH$
0
0
0
Test Results [units - WN in
g/crrt?; CEC and Na in meq/100 cm3; NOS-N in mg/dm3]:
Soil Class:
Mineral
HM% WN CEC BS% Ac pH P-1 K-1
Ca% Mg%
S-1
Mn-1
Mn-All Mn-Al2
Zn-I
Zn-AI
Cu-1
Na
ESI
0.46 0.84 22.2
95 1.2 6.8 469 88
85 8
70
92
60 60
1144
1144
1828
0.1
0
Sample ID: F4
Recommendations: Lime
Nutrients (lb/acre)
Crop (tons/acre)
N P2O5
K2O
Mg S
Mn
Zn
Cu
B
Lime History:
1- Fescue/OGrass/Tim, M 0.0
120-200 0
0
0 0
pH$
0
0
0
2- Fescue/OGrass/Tim, M 0.0
120-200 0
0
0 0
pH$
0
0
0
Test Results [units - WN in
g/crrl?; CEC and Na in meq/100 cm3; NOS-N in mg/drrt?]:
Soil Class:
Mineral
HM% WN CEC BS% Ac pH P-1 K-1
Ca% Mg%
S-1
Mn-I
Mn-All Mn-Al2
Zn-I
Zn-AI
Cu-1
Na
ESI
0.51 0.84 18.0
94 1.2 6.7 488 93
83 8
68
94
64 64
941
941
1592
0.1
1

NCDA&CS Agronomic Division Phone: [phone] Website: www.ncagr.gov/Divisions/Agronomic-Services .
Report No.
John Fisher
Understanding the Soil Report: explanation of measurements, abbreviations and units
Recommendations
Report Abbreviations
Ac
exchangeable acic
Lime
B
boron
If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either
BS%
% CEC occupied I
ton/acre or Ib/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting.
cations
For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 to 75 Ib/1000 sq ft)
Ca%
% CEC occupied I
at one time, even if the report recommends more. You can apply the rest in similar increments every six months until the
CEC
cation exchange c
full rate is applied. If Mg is recommended and lime is needed, use dolomitic lime.
Cu-I
copper index
ESP
exchangeable sod
Fertilizer
HM%
percent humic ma
Each nutrient recommendation for field crops or other large areas are listed separately in units of lb/acre unless
K-I
potassium index
otherwise specified. Recommendations for N (and sometimes for B) are based on research/field studies for the crop
K20
potash
being grown, not on soil test results. Recommendations for K and P will depend on K-1 and P-1 soil test results and the
Mg%
% CEC occupied I
crop to be grown. Generally, at K-1 and P-1 values > 50, recommendations will be minimal. If Mg is needed band no lime is
MIN
mineral soil class
recommended, 0-0-22 (11.5% Mg) is an excellent source; 175 to 250 lb/acre alone or in a fertilizer blend will usually
Mn
manganese
satisfy crop needs. Soluble salt levels (SS-1) appear only on reports for diagnostic/problem samples.
Mn-All
Mn-availability ind
Mn-Al2
Mn-availability ind
Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z
Mn-1
manganese index
notations appear on the soil report in the recommendation section, refer to NCDA&CS
M-0
mineral -organic sc
$Note: Secondary Nutrients and Micronutrients. Various NCDA&CS crop notes also address lime and fertilizer needs.
N
nitrogen
Na
sodium
Recommendations for small areas, such as home lawns/gardens, are listed in units of Ib/1000 sq ft. If you cannot find
NOs-N
nitrate nitrogen
ORG
cl
organic soil class
ass
the exact fertilizer grade recommended on the report, visit NCDA&CS Fertilizer Substitutionsto find information that may
pH
current soil pH
help you choose a comparable alternate. For more information, read NCSU publication,
P-1
phosphorus index
A Homeowner's Guide to Fertilizer. In general, homeowners do not need to be concerned about micronutrients.
P205
phosphate
S-1
sulfur index
Test Results
SS-1
soluble salt index
W/V
weight per volume
The first seven parameters [soil class, HM%, W/V, CEC, BS%, Ac and pH] describe the soil and its degree of acidity.
Zn-AI
zinc availability in
The remaining 16 parameters [P-I, K-1, Ca%, Mg%, Mn-1, Mn-All, Mn-AI2, Zn-I, Zn-Al, Cu-I, S-I, SS -I, Na, ESP, SS -I,
NOs-N (not routinely available)] indicate levels of plant nutrients or other fertility measurement. Visit NCDA&CS
Understand Your Report for more information.