WQ0010059_2023 Residual Annual Report_20240215 (2)

Initial Review
Reviewer
nathaniel.thorn burg
Is this submittal an application? (Excluding additional information.) *
Yes No
If not an application what is the submittal type?* Annual Report
Residual Annual Report
Additional Information
Other
Annual Report Year* 2023
Permit Number (IR) * WQ0010059
Applicant/Permittee City of Lenoir
Email Notifications
Does this need review by the hydrogeologist? * Yes U No
Regional Office Asheville
CO Reviewer
Admin Reviewer Wanda Gerald

Submittal Form
Project Contact Information
Please provide information on the person to be contacted by NDB Staff regarding electronic submittal, confirmation of receipt, and other correspondence.
Name* Elisa Triplett
Email Address*
[e-mail]
Project Information
.........................
Application/Document Type*
New (Fee Required)
Modification - Major (Fee Required)
Renewal with Major Modification (Fee
Required)
Annual Report
Additional Information
Other
Phone Number*
8287574462
Modification - Minor
Renewal
GW-59, NDMR, NDMLR, NDAR-1,
N DAR-2
Residual Annual Report
Change of Ownership
We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form.
https://edoes.deq.nc.gov/Forms/NonDischarge_Monitoring_Report
Permit Type:*
Wastewater Irrigation
High -Rate Infiltration
Other Wastewater
Reclaimed Water
Closed -Loop Recycle
Residuals
Single -Family Residence Wastewater
Other
Irrigation
Permit Number:*
WQ0010059
Has Current Existing permit number
Applicant/Permittee Address*
1905 Broadland Road
Facility Name*
City of Lenoir Class A Residuals Program
Please provide comments/notes on your current submittal below.
At this time, paper copies are no longer required. If you have any questions about what is required, please contact Nathaniel Thornburg
at [e-mail].
Please attach all information required or requested for this submittal to be reviewed here.
(Application Form, Engineering Plans, Specifications, Calculations, Etc.)
2023 Combined Sheets for State Report.pdf 2.2MB
Upload only 1 PDF document (less than 250 MB). Multiple documents must be combined into one PDF file unless file is larger
than upload limit.
* By checking this box, I acknowledge that I understand the application will not be accepted for pre -review until the fee (if required) has
been received by the Non -Discharge Branch. Application fees must be submitted by check or money order and made payable to the
North Carolina Department of Environmental Quality (NCDEQ). I also confirm that the uploaded document is a single PDF with all parts
of the application in correct order (as specified by the application).
Mail payment to:
NCDEQ — Division of Water Resources
Attn: Non -Discharge Branch
1617 Mail Service Center
Raleigh, NC 27699-1617
Signature
Submission Date 2/15/2024

February 15, 2024
City of Lenoir
P.O. Box 958 Lenoir, NC 28645-0958
Subject: Annual Residuals Report CY 2023
Enclosed is a copy of the 2023 calendar year Annual Residuals Report for the City of Lenoir's
Lower Creek WWTP Residuals Facility; permit number WQ0010059.
Blowing Rock has not brought any of their sludge to our facility the entire year of 2022,
however they are listed as a source.
The regular quarterly samples as per the permit were not collected or analyzed for the 1s'
quarter 2023. There has been significant turnover in lab personnel and the sample collection
was inadvertently missed.
If there are any questions or if any further information is needed please call me at (828) 757-
4462 or email me at [e-mail]
Sincerely,
Elisa R. Triplett
Superintendent WWTP

CLASS A ANNUAL DISTRIBUTION AND MARKETING/ SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM
WQ PERMIT #: WQ0010059 FACILITY NAME:
PHONE: [phone] COUNTY:
Caldwell
Lower Creek WWTP
Jake soots
FACILITY TYPE (please check one): ❑ Surface Disposal (complete Part A (Source(s) and "Residual In" Volume only) and Part C)
❑r Distribution and Marketing (complete Parts A, B, and C)
Was the facility in operation during the past calendar year? Yes ❑,. No ❑ 0 If No skip parts A, B, C and certify form below
Part A*:
Part B*:
Month
Sources(s) (include NPDES # if
applicable)
Volume (dry tons)
Recipient Information
Amendment/
Bulking Agent
Residual In
Product Out
Name(s)
Volume (dry tons)
Intended use(s)
January
WWTP sludge from the
0
71.37
71.37
David Powell
60
Ha
February
following sources:
0
94.82
94.82
Clay Wilson, Tony Ramsey
54
Ha
March
0
61.96
61.96
Jeff Branch, David Spears
20
Ha
April
Lower Creek WWTP
0
54.38
54.38
onnie Cardwell, Lynn Bean
49
Ha
May
Gunpowder Creek WWTP
0
96.54
96.54
Ronnie Cardwell
12
Ha
June
Lenoir Water Treatment Plant
0
66.41
66.41
City of Lenoir
24
Ball field
July
0
101.88
101.88
David Powell
25
Ha
August
0
220.25
220.25
ell,lackey, Chuck Calloway,
191
Ha
September
0
150.89
150.89
David Powell'Hendersonvillc
98
Ha
October
0
196.07
196.07
ell,lackey, Chuck Calloway,
165
Ha
November
1
0
158.37
158.37
David Powell, John Moore
III
Ha
December
1
0
92.05
92.05
David Powell
12
Ha
Total from FORM DMSDF (sup)
Totals:
I Annual (dry tons):
0
1364.99
1364.99
821
Amendment(s) used: I I Bulking Agent(s) used:
* If more space is required, attach additional information sheets (FORM DMSDF (supp)): Total Number of Form DMSDF (Supp)
Part C:
Facility was compliant during the past calendar year with all conditions of the land application permit ❑ Yes
(including but not limited to items 1-3 below) issued by the Division of Water Resources: El No 0, If No, Explain in Narritive
1. All monitoring was done in accordance with the permit and reported for the year as required and three (3) copies of certified laboratory results are attached.
2. All operation and maintenance requirements were compiled with or, in the case of a deviation, prior authorization was received from the Division of Water Resources.
3. No contravention of Ground Water Quality Standards occurred at a monitoring well.
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate and complete. I am aware that there are significant
penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
Signature of Permittee
Date Signature of Preparer**
(if different from Permittee)
**Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
Date
DENR FORM DMSDF (12/2006)

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B
WQ Permit Number: WQ0010059 Laboratory: 1) Meritech
Facility Name: City of Lenoir - Lower Creek WWTP 2) Statesville Analytical
Residual Source WQ # or NCO023981 3)
NPDES #: 4)
WWTP Name: Lower Creek WWTP 5)
Residual Analvsis Data
Parameter
(mg/kg)
Ceiling
Conc.
Limit
Sample or Composite Date
MISSED
6/6/2023
8/22/23
12/19/23
Percent Solids (%)
NA
89.6
81.8
77.6
Arsenic
75
4.79
1.81
1.91
Cadmium
85
1.13
0.924
0.398
Copper
4,300
438
312
405
Chromium
NA
19.6
16.3
14.8
Lead
840
20.9
18.1
18.2
Mercury
57
0.29
0.232
0.316
Molybdenum
75
5.45
2.65
3.16
Nickel
420
22.8
21.1
25.8
Selenium
100
3.86
1.6
<0.644
Zinc
7,500
633
522
711
Total Phosphorus
NA
15,100
11,400
16,900
TKN
NA
2,450
39,400
6,850
Ammonia -Nitrogen
NA
1,92E
4,84E
123
Nitrate and Nitrite
NA
<11.2
<12.2
<12.9
a For surface disposal facilities the ceiling concentration limits listed in this form are not applicable. Reference the individual permit for metals limits.
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant
penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
2-15-2024
Signature of Preparer *
Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM RSSF (12/2006)

ANNUAL RESIDUAL SAMPLING SUMMARY FORM - B
Report all sampling analysis results for parameters not listed in FORM RSSF that are part of the WQ permit or were analyzed for over the past
calendar year. Use additional forms as needed.
WQ Permit Number: WQ0010059
Facility Name: City of Lenoir - Lower Creek WWTP
Residual Source
NPDES # or WQ#:
WWTP Name:
Residual Analvsis Data
NCO023981
Lower Creek WWTP
Laboratory: 1) Meritech
2) Statesville Analytical
3)
4)
5)
Parameter
Sample or Composite Date
1 •1 1
1 1 1
'• 1 1
--------
------------
------------
------------
------------
------------
------------
------------
------------
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
Alp
Signature of Preparer *
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
2-15-2024
Date
DENR FORM RSSF - B (12/2006)

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Lenoir -Lower Creek WWTP WQ Permit Number: WQ0010059
WWTP Name: Lower Creek WWTP
NPDES Number: NCO023981
Monitoring Period: From l/l/2023 To 12/31/2023
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. A (time/temp) ❑
Alt B (Alk Treatment)❑
Alt. C (Prior Testing)❑
Alt.D (No Prior Test) ❑
Process to Further Reduce Pathogeng, 0
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost
Heat Drying 0
Heat Treatment ❑
Thermophilic ❑
Beta Ray
Gamma Ray ❑
Pasteurization ❑
Class B:
jAlt. (1) Fecal Density ❑
Alt. (2) Process to Significantly Reduce Pathogens L]
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization ❑
1 Air Drying ❑ Composting ❑ jAerobic Digestion ❑
Anaerobic Digestion ❑
If applicable to alternative performed (Class A or Class B) complete the following monitoring data:
Parameter
Allowable Level
in Sludge
Pathogen Density
g Ty
Number o
Excee-
dences
Frequency
of Analysis
Sample
Type
Analytical
Tech -
ni ue
Minimum
Geo. Mean
Maxffn
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
CFU
1000 mpn per gram
of total solid (dry
weight)
<1000
<1000
<1000
MPN/G
0
7
G
Mult.tube
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per 4 grams
total solid (dry
I weight)
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed:
Alt.I (VS reduction) ❑
Alt. 2 (40-day bench) ❑
Alt. 3 (30-day bench) ❑
Alt. 4 (Spec. 02 uptake) ❑
Alt. 5 (14-Day Aerobic) ❑
Alt. 6 (Alk. Stabilization ❑
Alt 7 (Drying - Stable) ❑
jAlt. 8 (Drying - Unstable) ❑�
Alt. 9 (Injection) ❑
Alt. 10 (Incorporation) ❑
No vector attraction reduction alternatives were performed ❑
CERTIFICATION STATEMENT (please check the appropriate statement)
0 "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note
if you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Elisa Triplett, WWTP Superintendent
Preparer Name and Title (type or print)
2-15-2024
Signature of Preparer* Date
Land Applier Name and Title (if applicable)(type or print)
Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 5039(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 02T (12/2006)

CITY OF LENOI R
LENOIR BLEND
INFORMATION AND INSTRUCTIONS
PERSON(S) PREPARING THE RESIDUALS: Jake Soots, Biosolids Operator
ADDRESS OF BIOSOLIDS TREATMENT
CONTACT TELEPHONE NUMBER:
ALTERNATE CONTACT:
City of Lenoir, Lower Creek WWTP Biosolids Treatment
P.O. Box 958, 1905 Broadland Road
Lenoir, NC 28645
828-757-2198
Elisa Triplett, WWT Supt. (same phone #)
No- The land application of the residuals is prohibited except in accordance with the instructions
on this information sheet.
No- The residuals shall not be applied to any site that is flooded, frozen or snow-covered.
►Adequate procedures shall be provided to prevent surface runnoff from carrying any
disposed or stored residuals into any surface waters.
No- There shall be a 50 foot buffer between application site and any public or private water
supply source (including wells) and any stream, lake, river or natural drainage way.
► Person(s) accepting the residuals shall be responsible for soil testing their own sites to
ensure that the receiving soil can accept the residuals and to ensure that the crop or plants
will not be harmed.

Lower Creek WWTP Biosolids Test Results
Residuals Facility Permit # WQ0010059
NPDES # NCO023981
MISSED
o
Plant
SAMPLE
a,
o 0,
:tf0,
�, 0,
N
Available
o
E o
M z o
o
Nitrogen
COLLECTION
I° Y z
Q WM z
z- z
z z
m
(P.A.N.)
Quarter
(mq/kq)
(mq/kq)
(mq/kq)
(mq/kq)
(mq/kq)
1st QTR 2023
0.35
-
0.00%
NOTES:
10,000 mg/L
= 1 %
P.A.N. = (Min.
Rate) x (TKN - Ammonia)
+ 0.5 x Ammonia + Nitrate
+ Nitrite
Other Parameters:
Total Phosphorous
Calcium (as Ca)
Percent Solids
Fecal Coliform Maximum
Fecal Coliform Geometric Mean
pH
OTHER LIMITED PARAMETERS
C
O
L
� U �
� U)
U U �
Arsenic (As) *
75
Cadmium (Cd)
85
Chromium (Cr)
3,000
Copper (Cu)
4,300
Lead (Pb) *
840
Mercury (Hg)
57
Molybdenum (Mo)
75
Nickel (Ni)
420
Selenium (Se) *
100
Zinc (Zn)
7,500
mg/kg 0.0000%
mg/kg 0.00% CCE
counts/kg
counts/kg (Limit is 1,000,000 counts/kg)
S.U.
O J
O)
O O
N
E c3 E
Q E
COMMENTS
41
39
1,500
All Parameters are
300
below allowable
17
----
permit limits.
420
100
2,800
All samples were collected by City of Lenoir laboratory personnel and analyzed by Statesville Analytical,
and Meritech Labs
The samples collected were representative of what is distributed to end users.
The samples collected were representative of what is distributed to end users.

Lower Creek WWTP Biosolids Test Results
Residuals Facility Permit # WQ0010059
NPDES # NCO023981
_r_
cU
to
cU
..
c
o
Plant
c
Y �,
E c
o 0,
c
m ��,
c
N a
Available
cU o
E o
C Z o
m�
L o
Nitrogen
O
z
E �
Q z
z z
z z
P.A.N.
( )
July, August, Sept. (mq/kq)
(mq/kq)
(mq/kq)
(mq/kq)
�
(mq/kq)
3rd quarter 2023 39,400
4,840
12.2
---
0.35
14,528.20
(collected 8/22/2023)
1.45%
NOTES: 10,000 mg/L =
1 %
P.A.N. = (Min.
Rate) x (TKN - Ammonia) + 0.5 x Ammonia + Nitrate + Nitrite
Other Parameters:
Total Phosphorous
11,400
mg/kg
1.1400%
Calcium (as Ca)
7,180
mg/kg
1.80%
CCE
Percent Solids
81.8
%
Fecal Coliform Maximum
<1000
counts/kg
Fecal Coliform Geometric Mean
<1000
counts/kg
(Limit is 1,000,000 counts/kg)
OTHER LIMITED PARAMETERS
0
0�
U)
L
L
E
}�
CU
E
UU
2<U�
Qo'
U
Arsenic (As)*
75
41
1.81
Cadmium (Cd)
85
39
0.924
Chromium (Cr)
3,000
16.3
All
Copper (Cu)
4,300
1,500
312
Parameters
Lead (Pb)*
840
300
18.1
are below
Mercury (Hg)
57
17
0.232
allowable
Molybdenum (Mo)
75
----
2.65
permit
Nickel (Ni)
420
420
21.1
limits.
Selenium (Se)*
100
100
1.6
Zinc (Zn)
7,500
2,800
522
SAR (Sodium Adsorption Ratio) __> 10 3.14
Limit Result
All samples were collected by City of Lenoir laboratory personnel and analyzed by Statesville Analytical,
and Meritech Labs
The samples collected were representative of what is distributed to end users.

Lower Creek WWTP Biosolids Test Results
Residuals Facility Permit # WQ0010059
NPDES # NCO023981
c�
g
Plant
o
0)
N m
Available
ohoo
zoo
m�
��
Nitrogen
� Y z
Q z
z� z
z z
(P.A.N.)
Oct, Nov Dec (mq/kq)
(mq/kq)
(mq/kq)
(mq/kq)
(mq/kq)
4t" quarter 2023 6,850
123
12.9
0.35
2,428.85
(collected 12/19/2023)
0.24%
NOTES: 10,000 mg/L =
1 %
P.A.N. = (Min.
Rate) x (TKN - Ammonia) + 0.5 x Ammonia
+ Nitrate + Nitrite
Other Parameters:
Total Phosphorous
16,900
mg/kg
1.6900%
Calcium (as Ca)
0
mg/kg
0.00%
CCE
Percent Solids
77.6
%
Fecal Coliform Maximum
<1000
counts/kg
Fecal Coliform Geometric Mean
<1000
counts/kg
(Limit is 1,000,000 counts/kg)
OTHER LIMITED PARAMETERS
0
03
E
Z O
O> O i=
C N E
U U
2 Q U
Qa�
Arsenic (As) 75
41
1.91
Cadmium (Cd) 85
39
0.398
Chromium (Cr) 3,000
14.8
Copper (Cu) 4,300
1,500
405
Lead (Pb) 840
300
18.2
Mercury (Hg) 57
17
0.316
Molybdenum (Mo) 75
----
3.16
Nickel (Ni) 420
420
25.8
Selenium (Se) 100
100 <
0.644
Zinc (Zn) 7,500
2,800
711
All samples were collected by City of Lenoir laboratory personnel and analyzed by Statesville Analytical,
and Meritech Labs
The samples collected were representative of what is distributed to end users.

Lower Creek WWTP Biosolids Test Results
Residuals Facility Permit # WQ0010059
NPDES # NCO023981
c�
g
Plant
N
m
Available
ohoo
0)
zoo
m�
��
Nitrogen
�Yz
Qz
z�z
zz
Cam'
(P.A.N.)
Quarter (mq/kq)
(mq/kq)
(mq/kq)
(mq/kq)
(mq/kq)
2nd quarter 2023 2,450 1,920 11.2 0.35 1,156.70
(Collected: 6/6/2023) 0.12%
10,000 mg/L = 1 %
P.A.N. = (Min. Rate) x (TKN - Ammonia) + 0.5 x Ammonia + Nitrate + Nitrite
Other Parameters:
Total Phosphorous
15,100
mg/kg
Calcium (as Ca)
9,600
mg/kg
Percent Solids
89.6
%
Fecal Coliform Maximum
<1000
counts/kg
Fecal Coliform Geometric Mean
<1000
counts/kg
OTHER LIMITED PARAMETERS
O J
O)
'P
0) O Y
S O Y
> Y
- C
U
C U)
U
CO
U
E
Q
Arsenic (As)
75
41
4.79
Cadmium (Cd)
85
39
1.13
Chromium (Cr)
3,000
19.60
Copper (Cu)
4,300
1,500
438
Lead (Pb) *
840
300
20.9
Mercury (Hg)
57
17
0.29
Molybdenum (Mo)
75
----
5.45
Nickel (Ni)
420
420
22.8
Selenium (Se)
100
100
3.86
Zinc (Zn)
7,500
2,800
633
SAR (Sodium Adsorption Ratio) ==>
1.5100%
2.40% CCE
(Limit is 1,000,000 counts/kg)
10
Limit Result
All samples were collected by City of Lenoir laboratory personnel and analyzed by Statesville Analytical,
and Meritech Labs
The samples collected were representative of what is distributed to end users.

2023 Temperature and %Solids of Dry Product
Date
% Dry
Temp
Date
% Dry
Temp
Date
% Dry
Temp
1/2
91
201
2/1
94
205
3/6
92
211
1/3
91
202
2/6
93
208
3/7
91
213
1/4
94
201
2/7
92
210
3/8
92
209
1/9
92
205
2/13
94
214
3/12
91
207
1/10
99
212
2/14
93
209
3/14
92
207
1/11
95
210
2/15
92
208
3/15
91
206
1/16
96
214
2/20
92
207
3/20
92
203
1/17
93
216
2/21
92
210
3/21
92
203
1/18
93
217
2/22
94
213
3/22
92
205
1/23
90
206
2/27
92
211
3/27
92
209
1/24
92
204
2/28
93
214
3/29
91
208
1/25
91
212
1/30
93
202
1/31
91
206
Date
% Dry
Temp
Date
% Dry
Temp
Date
% Dry
Temp
4/3
91
208
5/1
91
209
6/1
93
217
4/4
92
209
5/2
91
207
6/5
91
220
4/5
91
210
5/3
91
210
6/6
91
219
4/10
92
207
5/8
92
213
6/7
91
215
4/11
92
209
5/9
91
214
6/12
91
217
4/12
91
210
5/10
92
213
6/13
91
218
4/17
92
212
5/15
91
216
6/14
92
218
4/18
91
214
5/16
92
214
6/20
91
212
4/24
91
210
5/17
91
217
6/22
97
214
4/25
92
208
5/22
92
215
6/26
92
220
5/23
92
212
6/27
91
213
5/24
91
218
6/28
91
216
5/29
92
215
5/30
91
217
Date
% Dry
Temp
Date
% Dry
Temp
Date
% Dry
Temp
7/10
99
220
8/1
92
215
9/2
92
217
7/11
10
218
8/2
91
217
9/4
93
221
7/12
92
218
8/7
92
213
9/5
96
220
7/17
93
217
8/8
91
213
9/11
91
214
7/18
92
214
8/9
91
217
9/12
91
219
7/19
92
218
8/14
91
215
9/13
92
221
7/24
91
216
8/15
92
218
9/18
91
217
7/25
91
220
8/16
92
246
9/19
93
215
7/26
93
216
8/21
92
220
9/20
93
217
7/31
91
219
8/22
92
217
9/25
92
220
8/23
91
218
9/26
92
215
8/28
92
216
9/27
91
219
8/29
90
1 219
8/30
92
221

2023 Temperature and %Solids of Dry Product

Contact: Lisa Triplett
Client: City of Lenoir
1905 Broadland Road
Lenoir NC 28645
Meritech Work Order # 060623146
Meritech, Inc.
Environmental Laboratory
Laboratory Certification No.165
Sample: 060623-Biosolids Grab
Report Date: 6/15/2023
NPDES #: NCO023981
Date Sample Rcvd: 6/6/2023
6/6/2023
Parameters
Results
Analysis Date
Reporting Limit
Method
% Total Solids
89.6 %
6/6/23
0-100 %
SM 2540E
Ammonia, Nitrogen
1,920 mg/kg
6/8/23
10 mg/kg
EPA 350.1
TKN
2,450 mg/kg
6/9/23
20 mg/kg
EPA 351.1
Nitrate/Nitrite, Nitrogen
<11.2 mg/kg
6/13/23
11.2 mg/kg
EPA 353.2
Nitrogen, total
2,450 mg/kg
6/13/23
20.0 mg/kg
EPA 353.2
Aluminum, total
10,600 mg/kg
6/13/23
2.50 mg/kg
EPA 200.7
Arsenic, total
4.79 mg/kg
6/13/23
0.060 mg/kg
EPA 200.7
Cadmium, total
1.13 mg/kg
6/13/23
0.100 mg/kg
EPA 200.7
Calcium, total
9,600 mg/kg
6/13/23
10.0 mg/kg
EPA 200.7
Chromium, total
19.6 mg/kg
6/13/23
0.250 mg/kg
EPA 200.7
Copper, total
438 mg/kg
6/13/23
1.00 mg/kg
EPA 200.7
Lead, total
20.9 mg/kg
6/13/23
0.500 mg/kg
EPA 200.7
Magnesium, total
2,900 mg/kg
6/13/23
10.0 mg/kg
EPA 200.7
Mercury, total
0.290 mg/kg
6/13/23
0.02 mg/kg
EPA 245.1
Molybdenum, total
5.45 mg/kg
6/13/23
0.500 mg/kg
EPA 200.7
Nickel, total
22.8 mg/kg
6/13/23
2.0 mg/kg
EPA 200.7
Phosphorus, total
15,100 mg/kg
6/13/23
2.00 mg/kg
EPA 200.7
Selenium, total
3.86 mg/kg
6/13/23
0.500 mg/kg
EPA 200.7
Silver, total
5.12 mg/kg
6/13/23
0.250 mg/kg
EPA 200.7
Sodium, total
484 mg/kg
6/13/23
20.0 mg/kg
EPA 200.7
Zinc, total
633 mg/kg
6/13/23
0.500 mg/kg
EPA 200.7
Cyanide, total
<0.558 mg/L
6/8/23
0.558 mg/L
EPA 335.4
1 hereby certify that 1 have reviewed and approve these data. az�L'::�tL
Laboratory Representative
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

Analytical Results
City of Lenoir
1905 Broadland Road
Lenoir, NC 28633
Receive Date: 05/30/2023
Reported: 06/05/2023
For:
Comments: GEOMETRIC MEAN: 9.0 MPNIg
Sample Number
Parameter
Sample ID
Result
Unit
Method
Analyzed
Analyst
230530-13-01
Fecal Coliforms
1
9.3
MPNIg
SM92210E-2006
05/30/2023
MD
230530-13-01
Percent Solids
1
86.1
%
SM254OB-2011
05/30/2023
MD
230530-13-02
Fecal Coliforms
2
9.4
MPNIg
SM92210E-2006
05/30/2023
MD
230530-13-02
Percent Solids
2
85.5
%
SM25409-2011
05/30/2023
MD
230530-13-03
Fecal Coliforms
3
3.5
MPNIg
SM92210E-2006
05/30/2023
MD
230530-13-03
Percent Solids
3
86.1
ova
SM2540B-2011
05/30/2023
MD
230530-13-04
Fecal Coliforms
4
5.8
MPNIg
SM92210E-2006
05/30/2023
MD
230530-13-04
Percent Solids
4
86.2
%
SM254OB-2011
05/30/2023
MD
230530-13-05
Fecal Coliforms
5
87.9
MPNIg
SM92210E-2006
05/30/2023
MD
230530-13-05
Percent Solids
5
86.0
%
SM254OB-2011
05/30/2023
MD
230530-13-06
Fecal Coliforms
6
9.3
MPN/g
SM92210E-2006
05/30/2023
MD
230530-13-06
Percent Solids
6
86.0
%
SM254OB-2011
05/30/2023
MD
230530-13-07
Fecal Coliforms
7
12.8
MPNIg
SM92210E-2006
05/30/2023
MD
230530-13-07
Percent Solids
7
86.0
%
SM254OB-2011
05/30/2023
MD
Respectfully submitted,
Melissa Myers
NC Cert #440,
NCDW Cert #37755,
EPA #NC00909
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 1 of 4

Contact: Lisa Triplett
Client: City of Lenoir
1905 Broadland Road
Lenoir NC 28645
Mer itech, Inc.
Environmental Laboratory
Laboratory Certification No. 165
Zr
aoG3
Report Date: 9/7/2023
NPDES #: NC0023981
Date Sample Rcvd: 8/22/2023
Meritech Work Order # 082223138 Sample: 082223-Biosolids Grab 8/22/2023
Parameters Results Analysis Date Reporting Limit Method
% Total Solids
81.8 %
8/23/23
0-100 %
SM 2540E
Ammonia, Nitrogen
4,840 mg/kg
8/28/23
10 mg/kg
EPA 350.1
TKN
39,400 mg/kg
8/29/23
20 mg/kg
EPA 351.1
Nitrate/Nitrite, Nitrogen
<1.2.2 mg/kg
9/6/23
12.2 mg/kg
EPA 353.2
Nitrogen, total
39,400 mg/kg
9/6/23
20.0 mg/kg
EPA 353.2
Aluminum, total
8,000 mg/kg
8/24/23
2.50 mg/kg
EPA 200.7
Arsenic, total
1.81 mg/kg
8/24/23
0.060 mg/kg
EPA 200.7
Cadmium, total
0.924 mg/kg
8/24/23
0.100 mg/kg
EPA 200.7
Calcium, total
7,180 mg/kg
8/24/23
10.0 mg/kg
EPA 200.7
Chromium, total
16.3 mg/kg
8/24/23
0.250 mg/kg
EPA 200.7
Copper, total
312 mg/kg
8/24/23
1.00 mg/kg
EPA 200.7
Lead, total
18.1 mg/kg
8/24/23
0.500 mg/kg
EPA 200.7
Magnesium, total
2,600 mg/kg
8/24/23
10.0 mg/kg
EPA 200.7
Mercury, total
0.232 mg/kg
8/29/23
0.02 mg/kg
EPA 245.1
Molybdenum, total
2.65 mg/kg
8/24/23
0.500 mg/kg
EPA 200.7
Nickel, total
21.1 mg/kg
8/24/23
2.0 mg/kg
EPA 200.7
Phosphorus, total
11,400 mg/kg
8/24/23
2.00 mg/kg
EPA 200.7
Selenium, total
1.60 mg/kg
8/24/23
0.500 mg/kg
EPA 200.7
Silver, total
2.35 mg/kg
8/24/23
0.250 mg/kg
EPA 200.7
Sodium, total
1,280 mg/kg
8/24/23
20.0 mg/kg
EPA 200.7
Zinc, total
522 mg/kg
8/24/23
0.500 mg/kg
EPA 200.7
Cyanide, total
1.43 mg/L
8/24/23
0.558 mg/L
EPA 335.4
1 hereby certify that I have reviewed and approve these data.
Laboratory Representative
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

Analytical Results
City of Lenoir
1905 Broadland Road �r ! (;} r
Lenoir, NC 28633 Cat `�
Receive Date: 08/23/2023
Reported: 08/25/2023
For: 082323 Biosolids
Comments: Geometric Mean: 320 MPN/g
STATESVI L.LE
ANALYTICAL.
Sample Number Parameter Sample ID Result Unit Method Analyzed Analyst
230823-15-01
Fecal Coliforms
F-1
1916%
MPN/g
SM9221 CE-2014
08/23/2023
CL
230823-15-01
Percent Solids
F-1
83.5
%
SM264OB•2011
08/23/2023
CL
230823-15-02
Fecal Coliforms
F-2
C1065
MPN/g
SM9221 CE-2014
08/23/2023
CL
230823-15-02
Percent Solids
F-2
84.5
%
sM254as zo11
08/23/2023
CL
230823-15-03
Fecal Coliforms
F-3
108 J
MPN/g
SM9221 CE-2014
08/23/2023
CL
230823-15-03
Percent Solids
F-3
83.2
%
SM254OB-2011
08/23/2023
CL
230823-15-04
Fecal Coliforms
F-4
q!5�9z
MPN/g
SM9221 cs-2014
08/23/2023
CL
230823-15-04
Percent Solids
F-4
%
SM254OB-2011
08/23/2023
CL
230823-15-05
Fecal Coliforms
F-5
98
MPN/g
SM9221 CE-2014
08/23/2023
CL
230823-15-05
Percent Solids
F-5
85.9
%
SM254OB-2011
08/23/2023
CL
230823-15-06
Fecal Coliforms
F-6
200
MPN/g
SM9221 CE-2014
08/23/2023
CL
230823-15-06
Percent Solids
F-6
84.9
%
SM254OB-2011
08/23/2023
CL
230823-15-07 Fecal Coliforms F-7
/200 MPN/g SM9221 cE-2014 08/23/2023 CL
230823-15-07 Percent Solids F-7
h qo SM254OB-2011 08/23/2023 CL
Respectfully submitted,
� 0
C)t tiyJ
Melissa Myers
NC Cert #440,
NCDW Cert #37755,
EPA #NC00909
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 1 of 4

Contact: Lisa Triplett
Client: City of Lenoir
1905 Broadland Road
Lenoir NC 28645
Meritech, Inc.
Environmental Laboratory
Laboratory Certification No.165
aoa3
Report Date: 1/2/2024
NPDES #: NCO023981
Date Sample Rcvd: 12/19/2023
Meritech Work Order #
121923195
Sample: 121923-Biosolids Grab
12/19/2023
Parameters
Results
Analysis Date Reporting Limit
Method
% Total Solids
77.6 %
12/19/23
0-100 %
SM 2540E
Ammonia, Nitrogen
123 mg/kg
12/27/23
10 mg/kg
EPA 350.1
TKN
6,850 mg/kg
12/27/23
20 mg/kg
EPA 351.1
Nitrate/Nitrite, Nitrogen
<12.9 mg/kg
12/22/23
12.9 mg/kg
EPA 353.2
Nitrogen, total
6,850 mg/kg
12/27/23
20.0 mg/kg
EPA 353.2
Aluminum, total
14,900 mg/kg
12/20/23
2.50 mg/kg
EPA 200.7
Arsenic, total
1.91 mg/kg
12/20/23
0.060 mg/kg
EPA 200.7
Cadmium, total
0.398 mg/kg
12/20/23
0.100 mg/kg
EPA 200.7
Calcium, total
9,380 mg/kg
12/20/23
10.0 mg/kg
EPA 200.7
Chromium, total
14.8 mg/kg
12/20/23
0.250 mg/kg
EPA 200.7
Copper, total
405 mg/kg
12/20/23
1.00 mg/kg
EPA 200.7
Lead, total
18.2 mg/kg
12/20/23
0.500 mg/kg
EPA 200.7
Magnesium, total
2,840 mg/kg
12/20/23
10.0 mg/kg
EPA 200.7
Mercury, total
0.316 mg/kg
12/26/23
0.02 mg/kg
EPA 245.1
Molybdenum, total
3.16 mg kg
12/20/23
0.500 mg/kg
EPA 200.7
Nickel, total
25.8 mg/kg
12/20/23
2.0 mg/kg
EPA 200.7
Phosphorus, total
16,900 mg/kg
12/20/23
2.00 mg/kg
EPA 200.7
Selenium, total
<0.644 mg/kg
12/20/23
0.644 mg/kg
EPA 200.7
Silver, total
1.57 mg/kg
12/20/23
0.250 mg/kg
EPA 200.7
Sodium, total
514 mg/kg
12/20/23
20.0 mg/kg
EPA 200.7
Zinc, total
711 mg/kg
12/20/23
0.500 mg/kg
EPA 200.7
SAR
1.05 -
12/20/23
-
-
Cyanide, total
<0.500 mg/L
12/28/23
0.500 mg/L
EPA 335.4
pH
•6.9 S.U.
12/22/23
1.0 - 14.0 S.U.
SM 4500-HB
1 hereby certify that I have reviewed and approve these data. - 5�� -'/�
Laboratory Representative
642 Tarnco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

Analytical Results STATESVILLE
ANALYTICAL
L
City of Lenoir
1905 Broadland Road
Lenoir, NC 28633 r f ^ r r
Receive Date: 12/19/2023 b&3
Reported: 12/20/2023
For:
Comments: GEOMETRIC MEAN: 398 MPN/g
Sample Number Parameter Sample ID Result Unit Method Analyzed Analyst
231219-14-01
Fecal Coliforms
F1
1990
MPN/g
SMM21 CE-2014
12/19/2023
CL
231219-14-01
Percent Solids
F1
80.4
%
SM254OB-2011
12/19/2023
MD
231219-14-02
Fecal Coliforms
F2
108
MPN/g
SM9221 CE-2014
12/19/2023
CL
231219-14-02
Percent Solids
F2
83.4
%
SM25403-2011
12/19/2023
MD
231219-14-03
Fecal Coliforms
F3
1944
MPN/g
SM9221 CE-2014
12/19/2023
CL
231219-14-03
Percent Solids
F3
82.3
%
SM2540B-2011
12/19/2023
MD
231219-14-04
Fecal Coliforms
F4
87
MPN/g
SM9221 CE-2014
12/19/2023
CL
231219-14-04
Percent Solids
F4
80.8
%
SM254OB-2011
12/19/2023
MD
231219-14-05
Fecal Coliforms
FS
1993
MPN/g
SM9221 CE-2014
12/19/2023
CL
231219-14-05
Percent Solids
F5
80.3
%
SM254OB-2011
12/19/2023
MD
231219-14-06
Fecal Coliforms
F6
298
MPN/g
SM9221 CE-2014
12/19/2023
CL
231219-14-06
Percent Solids
F6
80.8
%
SM25406-2011
12/19/2023
MD
231219-14-07
Fecal Coliforms
F7
74
MPN/g
SM9221 CE-2014
12/19/2023
CL
231219-14-07
Percent Solids
F7
80.8
%
SM254OB-2011
12/19/2023
MD
Respectfully submitted,
Melissa Myers
NC Cert #440,
NCDW Cert #37755,
EPA #NC00909
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 1 of 4