WQ0001346_2023 Residual Annual Report_20240222 (2)

Initial Review
Reviewer
nathaniel.thorn burg
Is this submittal an application? (Excluding additional information.) *
Yes No
If not an application what is the submittal type?* Annual Report
Residual Annual Report
Additional Information
Other
Annual Report Year* 2023
Permit Number (IR) * WQ0001346
Applicant/Permittee City of Monroe
Email Notifications
Does this need review by the hydrogeologist? * Yes No
Regional Office Mooresville
CO Reviewer
Admin Reviewer Wanda Gerald

Submittal Form
Project Contact Information
Please provide information on the person to be contacted by NDB Staff regarding electronic submittal, confirmation of receipt, and other correspondence.
Name* Kyle Ketchum
Email Address*
[e-mail]
Project Information
.........................
Application/Document Type*
New (Fee Required)
Modification - Major (Fee Required)
Renewal with Major Modification (Fee
Required)
Annual Report
Additional Information
Other
Phone Number*
7042824612
Modification - Minor
Renewal
GW-59, NDMR, NDMLR, NDAR-1,
N DAR-2
Residual Annual Report
Change of Ownership
We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form.
https://edoes.deq.nc.gov/Forms/NonDischarge_Monitoring_Report
Permit Type:*
Wastewater Irrigation
High -Rate Infiltration
Other Wastewater
Reclaimed Water
Closed -Loop Recycle
Residuals
Single -Family Residence Wastewater
Other
Irrigation
Permit Number:*
WQ0001346
Has Current Existing permit number
Applicant/Permittee Address*
775 Treeway Drive Monroe,NC 28110
Facility Name*
City of Monroe Class B Residuals Program
Please provide comments/notes on your current submittal below.
At this time, paper copies are no longer required. If you have any questions about what is required, please contact Nathaniel Thornburg
at [e-mail].
Please attach all information required or requested for this submittal to be reviewed here.
(Application Form, Engineering Plans, Specifications, Calculations, Etc.)
Residuals Land Application Program Annual Report
59.95MB
2023.pdf
Upload only 1 PDF document (less than 250 MB). Multiple documents must be combined into one PDF file unless file is larger
than upload limit.
* By checking this box, I acknowledge that I understand the application will not be accepted for pre -review until the fee (if required) has
been received by the Non -Discharge Branch. Application fees must be submitted by check or money order and made payable to the
North Carolina Department of Environmental Quality (NCDEQ). I also confirm that the uploaded document is a single PDF with all parts
of the application in correct order (as specified by the application).
Mail payment to:
NCDEQ — Division of Water Resources
Attn: Non -Discharge Branch
1617 Mail Service Center
Raleigh, NC 27699-1617
Signature
C4�;A&'W
Submission Date 2/22/2024

Monroe
North Carolina
RESIDUALS LAND APPLICATION
PROGRAM
CITY
OF
MONROE
ANNUAL REPORT
2023
PERMIT NUMBER
WQ0001346

or
Monroe
North Carolina
City of Monroe
Water & Wastewater Residuals Land Application Program
2023
Annual Report
Table of Contents
1. Certification Form & Annual Operations Summary
2. Annual Residual Sampling Summary Forms & Biosolids Analysis
3. TCLP Analysis
4. Field Summary Forms
5. Pathogen Reduction & Vector Attraction Reduction
6. Soil Analysis

SECTION
1

ANNUAL LAND APPLICATION CERTIFICATION FORM
WQ Permit#: WQ0001346
County:
Union
Year: 2023
Facility Name (as shown on permit):
Land Application Operator:
City of Monroe
Ken Morris, Land Residual Coordinator Phone: [phone]
Land application of residuals as allowed by the permit occurred during the past calendar year?
0 Yes ❑ No - If No, skip Part A, and Part B and proceed to Part C. Also, If residuals were
generated but not land applied, please attach an explanation on how the residuals were handled.
Part A - Residuals Application Summary:
Total number of application fields in thepermit:
35
Total number of fields utilized for land application during the year:
21
Total amount of dry tons applied during the year for all application sites:
941
Total number of acres utilizes for land application during the year:
274
Part B - Annual Com lance Statement:
Facility was compliant during calendar year 2023 with all conditions of the land application permit
(including but not limited to items 1-13 below) issued by the Division of Water Quality.❑ Yes ❑ No
If no please, provide a written description why the facility was not compliant, the dates, and explain corrective action
taken.
1) Only residuals approved for this permit were applied to the permitted sites.
2) SoiI pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or
the limit specified in the permit.
3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies
of laboratory results are attached.
4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5) All other monitoring was performed in accordance with the permit and reported during the year as required and three (3)
copies of certified laboratory results are attached.
6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .1105(a) or the Pollutant
Loading Rates in 15A NCAC 02T .1105(b) (applicable to 40 CFR Part 503 regulated facilities).
7) All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part
503 regulated facilities).
8) All monitoring and reporting requirements in 15A NCAC 02T .1111 were complied with (applicable to 40 CFR Part
503 regulated facilities).
9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Quality.
10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
11) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as
specified in the permit.
12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13) All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C - Certification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate,
and complete. I am aware that there are significant penalties for submitting false information, including the
possibility of fines and imprisonment for knowing violations."
Scott Clark, Water Resources Director
Permittee Name and Title (type or print)
/0
000,
��t
Signature of Permittee Date
�liyl ��y ,, ? -1,2-
Signature of Preparer* Date Signature of Land Applier Date
(if different from Permittee) (if different from Permittee and Preparer)
* Preparer is defined in 40 CFR Part 503.9 (r) and 15A NCAC 02T .1102 (26) DEN FORM AC (12/2006)

OPERATION SUMMARY
Permit # W00001346
FIELDS USED IN
2023
NAME
NO.
GALS
GALS
YARDS
YARDS
Dry Tons
Dry Tons
(16slacj
ram Morris
i
I April
11.0
1
252
31.19
66.77
NC-AN-19
Ben Myers
1
March
44.6
630
78.54
68.32
NC-UN-18
March
162
37.78
21.31
2
May
27.6
432
53.49
48.11
May
90
19.18
28.68
Sept
270
40.93
42.55
Sept
72
19.21
6.96
7
May
5.7
72
8.91
38.82
May
54
11.51
83.33
8
May
16
448
55.46
86.06
Nov
144
23.17
45.46
William Griffin
1
May
24.5
522
64.63
65.49
NC-UN-29
2
Nov
5.7
130
20.91
115.20
3
Sept
7.4
144
21.83
84.64
Sept
72
19.23
25.94
4
June
2.9
36
4.46
38.15
June
18
3.84
54.60
5
Nov
2.2
54
8.69
123.98
Tom Appenzeller
1
June
13.1
162
20.06
38.01
NC-UN-30
June
90
19.18
60.43
2
Sept
11.9
244
36.99
89.19
Sept
84
22.42
18.82
4
June
15.2
270
33.42
54.60
June
54
11.51
31.25
5
June
10.8
252
31.20
71.72
June
54
11.50
43.98
Henry Myers
3
March
2.5
54
6.73
104.48
NC-UN-31
4
March
4.7
72
8.97
74.10
5
March
17.6
273
34.02
75.03
6
March
7.8
126
15.70
78.13
Danny Baker
1
Sept
23.5
396
60.02
73.30
NC-UN-32
Sept
126
33.63
14.30
2
Sept
15.5 1
270
40.94
75.77
Sept
90
24.03
15.48
4
Sept
3.2
54
8.19
73.40
Totals
WWTP- Metric Tons 642.56
WTP- Metric Tons 211.33
Total Metric Tons 853.88

SECTION
2

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City of Monroe
Reports of Lab
Analysis
1 St Quarter

Waypoint.(D
ANALYTICAL
1 /23/2023
City of Monroe
Ken Morris
775 Treeway Dr
Monroe, NC, 28110
Ref: Analytical Testing
Report Number: 23-018-0005
Project Description: RAS
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Dear Ken Morris:
Waypoint Analytical Virginia, Inc. received sample(s) on 1/18/2023 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information
Sincerely,
Gn�.�ty
Brandi Watson
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 1 of 5

Waypoint,(D
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Sample Summary Table
Report Number: 23-018-0005
Client Project Description: RAS
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
60456 RAS Solids 01/17/2023 09:45 01/18/2023 SM-2540G WP MTN
WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN
Page 2 of 5

Waypointo
ANALYTICAL
46205
City of Monroe Project RAS
Ken Morris
775 Treeway Dr Information
Monroe , NC 28110
Report Number : 23-018-0005 REFOR7
Lab No: 60456
Sample ID: RAS
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Report Date : 01/23/2023
Received : 01/18/2023
C7lG ��
MLYSIS Brandi Watson
Matrix: Solids
Sampled: 1/17/2023 9:45
Test Results Units MOL DF Date / Time By
Analyzed
Analytical
Method
Moisture 98.4 % 0.010 1 01/20/23 16:19 FMM
SM-2540G
Test Results Units MQL DF Date I Time By
Analytical
Analyzed
Method
Total Volatile Solids 78.0 % 0.010 1 01/20/23 16:19 FMM SM-2540G
Total Solids 1.57 % 0.010 1 01/20/23 16:19 FMM SM-2540G
Qualifiers/ DF Dilution Factor
Definitions
MQL Method Quantitation Limit
Page 3 of 5

iWaypont(D
7621 Whltepi-7 Road, Richmond, V7 -6446
Main 804-743.9401 0Fax [phone]
ANALYTICAL www.waypointanalytical.com
Shipment Receipt Form
Customer Number: 46205
Customer Name: City of Monroe
Report Number: 23-018-0005
Shipping Method
Fed Ex US Postal Lab
• UPS Client Courier
Other:
Thermometer ID:
Shipping container/cooler uncompromised?
• Yes
No
Number of coolers/boxes received
1
Custody seals intact on shipping container/cooler?
Yes
No:
Not Present
Custody seals intact on sample bottles?
Yes
No
Not Present
Chain of Custody (COC) present?
• Yes
No
COC agrees with sample label(s)?
Yes
No
COC properly completed
• Yes
No
Samples in proper containers?
Yes
No
Sample containers intact?
Yes
No
Sufficient sample volume for indicated test(s)?
0 Yes
No
All samples received within holding time?
• Yes
No
Ceoler temperature in compliance?
• Yes
No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
• Yes
No
Water - Sample containers properly preserved
Yes
No
• N/A
Water - VOA vials free of headspace
Yes
No
N/A
Trip Blanks received with VOAs
Yes
No
:0 N/A
Soil VOA method 5035 — compliance criteria met
Yes
No
• NIA
High concentration container (48 hr)
High concentration pre -weighed (methanol -14 d)
Low concentration Encore samplers (48 hr)
Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included?
Yes
No
Comments:
Signature: David Lennon Date & Time: 01/18/2023 11:45:04
Page 4 of 5

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Page 5 of 5

waypoint.(D
ANALYTICAL
1 /26/2023
City of Monroe
Ken Morris
775 Treeway Dr
Monroe, NC, 28110
Ref: Analytical Testing
Report Number: 23-018-0006
Project Description: City of Monroe
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypoi nta na lytica I, tom
Dear Ken Morris:
Waypoint Analytical Virginia, Inc, received sample(s) on 1/18/2023 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information
Sincerely,
Brand) Watson
Laboratory's liability in any claim relating to analyses performed shalt be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 1 of 10

Waypoint-(2)
ANALYTICAL
Report Number: 23-018-0006
Client Project Description: City of Monroe
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytital.com
Sample Summary Table
Lab No
Client Sample ID
Matrix
Date Collected
Date Received
Method
Lab ID
60457
WWTP Cake
Solids
01/17/2023 10:30
01/18/2023
60457
WWTP Cake
Solids
01/17/2023 10:30
01/18/2023
SM-4500-NH3C
WP MTN
60457
WWTP Cake
Solids
01/17/2023 10:30
01/18/2023
SW-7471B
WP MTN
60457
WWTP Cake
Solids
01/17/2023 10:30
01/18/2023
9045D
WP MTN
60457
WWTP Cake
Solids
01/17/2023 10:30
01/18/2023
4500NO3F-2011
WP MTN
60457
WWTP Cake
Solids
01/17/2023 10:30
01/18/2023
6010D
WP MTN
60457
WWTP Cake
Solids
01/17/2023 10:30
01/18/2023
SM-4500-NH3C-TKN
WP MTN
60457
WWTP Cake
Solids
01/17/2023 10:30
01/18/2023
SM-2540G
WP MTN
60458
WTP Cake
Solids
01/17/2023 10:15
01/18/2023
60458
WTP Cake
Solids
01/17/2023 10:15
01/18/2023
6010D
WP MTN
60458
WTP Cake
Solids
01/17/2023 10:15
01/18/2023
4500NO3F-2011
WP MTN
60458
WTP Cake
Solids
01/17/2023 10:15
01/18/2023
SM-4500-NH3C-TKN
WP MTN
60458
WTP Cake
Solids
01/17/2023 10:15
01/18/2023
SM-4500-NH3C
WP MTN
60458
WTP Cake
Solids
01/17/2023 10:15
01/18/2023
SW-7471B
WP MTN
60458
WTP Cake
Solids
01/17/2023 10:15
01/18/2023
SM-254OG
WP MTN
60458
WTP Cake
Solids
01/17/2023 10:15
01/18/2023
9045D
WP MTN
WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN
Page 2 of 10

Waypointo
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
46205
City of Monroe Project City of Monroe
Ken Morris Report Date : 01/26/2023
775 Treeway Dr Information : Received ; 01/18/2023
Monroe , NC 28110
Qn v
Report Number :23-018-0006 REPORTQFANALYSIS Brandi Watson
Lab No : 60457 Matrix: Solids
Sample ID: WWTP Cake Sampled: 1/17/2023 10.30
Test Results Units MQL DF Date / Time By Analytical
Analyzed Method
Moisture
85.2
%
0.010
1
01/20/2316:19
FMM
SM-254OG
Potassium
29fi0
mg/Kg - dry
67.6
1
01/24/23 19:56
TJS
6010D
Calcium
22500
mg/Kg - dry
338
1
01/24/23 19:56
TJS
6010D
Aluminum
12000
mg/Kg - dry
33.8
1
01/24/23 19:56
TJS
6010D
Manganese
1790
mg/Kg - dry
3.38
1
01/24/23 19:56
TJS
6010D
Copper
337
mg/Kg - dry
3.38
1
01/24/23 19:56
TJS
6010D
Zinc
1300
mg/Kg - dry
8.45
1
01/24/23 19:56
TJS
6010D
Nickel
66.0
mg/Kg - dry
1.69
1
01/24/23 19:56
TJS
6010D
Lead
22.9
mg/Kg - dry
2.03
1
01/24/23 19:56
TJS
6010D
Arsenic
8.78
mg/Kg - dry
3.38
1
01/25/23 20:01
JTR
6010D
Test
Results
Units
MOL
DF
Date 1 Time
By
Analytical
Analyzed
Method
Ammonia Nitrogen
1220
mg/Kg - dry
676
1
01/25/23 13:00
JRF
SM-4500-NH3C
Organic N
61280
mg/Kg - dry
1689
1
01/25/23 10:00
CALCULATION
Total Solids
14.8
%
0.010
1
01/20/23 16:19
FMM
SM-2540G
Phosphorus
22700
mg/Kg - dry
33.8
1
01/24/23 19:56
TJS
6010D
Cadmium
0.730
mg/Kg - dry
0.676
1
01/24/23 19:56
TJS
6010D
Chromium
55.4
mg/Kg - dry
1.69
1
01/24/23 19:56
TJS
6010D
Iron
29500
mg/Kg - dry
67.6
1
01/24/23 19:56
JTR
6010D
Mercury
<1.01
mg/Kg - dry
1.01
1
01/23/23 14:26
JTR
SW-7471B
Qualifiers/ OF
Dilution Factor
MQL
Method Quantitation Limit
Definitions
Page 3 of 10

Waypointo
ANALYTICAL
46205
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
City of Monroe
Project
City of Monroe
Ken Morris
Report Date : 01/26/2023
775 Treeway Dr
Information :
Received : 01/18/2023
Monroe , NC 28110
Q
CJ/? "(t '-
Report Number : 23-018-0006
REPORT OPA/YALYSIS
Brandi Watson
Lab No: 60457
Matrix: Solids
Sample ID : WWTP Cake
Sampled: 1/17/2023 10:30
Test
Results
Units MOL
DF Date / Time By Analytical
Analyzed Method
Selenium
4.43
mg/Kg - dry 3.38
1 01/24/23 19:56 TJS 6010D
Sulfur
10300
mg/Kg - dry 67.6
1 01/24/23 19:56 TJS 6010D
Total Kjeldahl Nitrogen
62500
mg/Kg - dry
1690
1
01/25/23 10:00
CLP ;M-4500-NH3C-TKP
Magnesium
2610
mg/Kg - dry
33.8
1
01/24/23 19:56
TJS
6010D
Sodium
993
mg/Kg - dry
169
1
01/24/23 19:56
TJS
6010D
Nitrate+Nitrite-N
409
mg/Kg - dry
31.0
1
01/24/23 13:55
ZBD
4500NO3F-2011
pH
5.9
S.U.
1
01125/2314:02
SAR
9045D
Total Volatile Solids
64.7
%
0.010
1
01/20/23 16:19
FMM
SM-2540G
Molybdenum
13.6
mg/Kg - dry
1.69
1
01/24/23 19:56
TJS
6010D
Qualifiers/ DF Dilution Factor MQL Method Quantitation Limit
Definitions
Page 4 of 10

0
Waypoint,
ttr
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax $04-271-6446
ANALYTICAL
www.waypointanalytical.com
46205
City of Monroe
Project
City of Monroe
Ken Morris
Report Date : 01/26/2023
775 Treeway Dr
Information :
Received : 01/18/2023
Monroe , NC 28110
i3randi Watson
Report Number: 23-018-0006
REPORTOF.QNAL!'SIS
Lab No; 60458
Matrix:
Solids
Sample ID : WTP Cake
Sampled:
1/17/2023 10:15
Test
Results
Units
MQL
DF
Date I Time
By Analytical
Analyzed
Method
Moisture
72.3
%
0.010
1
01/20/2316:19
FMM SM-254OG
Phosphorus
2470
mg/Kg - dry
18.1
1
01/24/23 20:01
TJS 6010D
Calcium
2250
mg/Kg - dry
181
1
01/24/23 20:01
TJS 6010D
Aluminum
8450
mg/Kg - dry
18.1
1
01/24/23 20:01
TJS 6010D
Manganese
1090
mg/Kg - dry
1.81
1
01/24/23 20:01
TJS 6010D
Copper
455
mg/Kg - dry
1.81
1
01/24/23 20:01
TJS 6010D
Organic N
30900
mg/Kg - dry
902.5
1
01/25/23 10:00
CALCULATION
Nickel
28.3
mg/Kg - dry
0.902
1
01/24/23 20:01
TJS 6010D
Lead
10.1
mg/Kg - dry
1.08
1
01/24/23 20:01
TJS 6010D
Arsenic
29.3
mg/Kg - dry
1.81
1
01/24/23 20:01
TJS 6010D
Total Volatile Solids
33.4
%
0.010
1
01/20/23 16:19
FMM 5M-254OG
Test
Results
Units
MQL
DF
date / Time
By Analytical
Analyzed
Method
Ammonia Nitrogen
365
mg/Kg - dry
361
1
01/25/23 13:00
JRF SM-4500-NH3C
Total Kjeldahl Nitrogen
31300
mg/Kg - dry
903
1
01/25/23 10:00
CLP iM-4500-NH3C-TKP
Magnesium
733
mg/Kg -dry
18.1
1
01/24/23 20:01
TJS 6010D
Sodium
383
mg/Kg - dry
90.3
1
01/24/23 20:01
TJS 6010D
Qualifiers/ DF
Dilution Factor
MQL Method Quantitation Limit
Definitions
Page 5 of 10

0
7621 Whitepine Road, Richmond, VA 23237
Waypoint
Main 804-743.9401 ° Fax [phone]
ANALYTICAL www.waypoint@nalytical,corn
46205
City of Monroe Project City of Monroe
Ken Morris Report Date : 01/26/2023
775 Treeway Dr Information : Received : 01/18/2023
Monroe , NC 28110
& y
Report Number: 23-018-0006 REPORT OFANALYSIS Brandi Watson
Lab No : 60458
Sample ID : WTP Cake
Matrix: Solids
Sampled: 1/17/2023 10:15
Total Solids
27.7
%
0.010
1
01/20/23 16:19
FMM
SM-2540G
Potassium
523
mg/Kg - dry
36.1
1
01/24/23 20:01
TJS
6010D
Sulfur
3170
mg/Kg - dry
36.1
1
01/24/23 20:01
TJS
6010D
Iron
313000
mg/Kg - dry
1810
50
01/25/23 20:06
JTR
6010D
Zinc
53.4
mg/Kg - dry
4.51
1
01/24/23 20:01
TJS
6010D
Nitrate+ Nitrite-N
<17.1
mg/Kg - dry
17.1
1
01/24/23 13:55
ZBD
4500NO3F-2011
Cadmium
8.92
mg/Kg - dry
0.361
1
01/24/23 20:01
TJS
6010D
Chromium
229
mg/Kg - dry
0.902
1
01/24/23 20:01
TJS
6010D
Mercury
<0.527
mg/Kg - dry
0.527
1
01/23/23 14:28
JTR
SW-74718
Selenium
<1.81
mg/Kg - dry
1.81
1
01/24/23 20:01
TIS
6010D
pH
6.0
S.U.
1
01/25/2314:02
SAR
9045D
Molybdenum
53.8
mg/Kg - dry
0.902
1
01/24/23 20:01
TJS
6010D
Qualifiers/ DF Dilution Factor MQL Method Quantitation Limit
Definitions
Page 6 of 10

WayPAoint.
NALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Client: City of Monroe CASE NARRATIVE
Project: City of Monroe
Lab Report Number: 23-018-0006
Date: 1/26/2023
Metals Analysis Method 6010D
Sample 60459 (Bio-Solids QTRLY)
Analyte: Aluminum
QC Batch No: 1-660241/1-659906
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 60459 (Bio-Solids QTRLY)
Analyte: Calcium
QC Batch No: 1-660241/1-659906
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 60459 (Bio-Solids QTRLY)
Analyte: Iron
QC Batch No: 1-660661/1-659906
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 60459 (Bio-Solids QTRLY)
Analyte: Potassium
QC Batch No: 1-66024111-659906
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 60459 (Blo-Solids QTRLY)
Analyte: Phosphorus
QC Batch No: L6602411L659906
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 60459 (Bio-Solids QTRLY)
Analyte: Sulfur
QC Batch No: L6602411L659906
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Solids Total Mercury Analysis - CVAA Method 7471A
Sample 93349 (EB-4, GB-5 8-10)
Analyte: Mercury
QC Batch No: L66001 1 /L659744
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Page 7 of 10

Waypoint(2)
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Page 8 of 10

•
Waypo i nt .(2) �fi�i I ain 80ine Road, Richmond, 27 23237
Main 804-743-9401 0Fax 804-271-fi446
-6446
ANALYTICAL www.waypointanalytical.com
Shipment Receipt Form
Customer Number: 46205
Customer Name: City of Monroe
Report Number: 23-018-0006
Shipping Method
Fed Ex US Postal Lab Other :
• UPS Client Courier Thermometer ID:
Shipping container/cooler uncompromised?
• Yes
No
Number of coolers/boxes received
I
Custody seals intact on shipping container/cooler?
Yes
No • Not Present
Custody seals intact on sample bottles?
Yes
No 40- Not Present
Chain of Custody (COC) present?
• Yes
No
COC agrees with sample label(s)?
• Yes
No
COC properly completed
6 Yes
No
Samples in proper containers?
! Yes
No
Sample containers intact?
Yes
No
Sufficient sample volume for indicated test(s)?
0. Yes
No
All samples received within holding time?
w Yes
No
Cooler temperature in compliance?
• Yes
No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
0 Yes
No
Water - Sample containers properly preserved
Yes
No • NIA
Water - VOA vials free of headspace
Yes
No • NIA
Trip Blanks received with VOAs
Yes
No • NIA
Soil VOA method 5035 — compliance criteria met
Yes
No • NIA
High concentration container (48 hr)
High concentration pre -weighed (methanol -14 d)
Low concentration EnCore samplers (48 hr)
Low cone pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included?
Yes
* No
Comments:
Signature: David Lennon
Date & Time: 01/18/2023 11:49:11
Page 9 of 10

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Scr
CL
FUS
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VI U4
f03 3 ..
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m W o
E c g �� Er � �• �m� fir►
O� C3
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rr 'i7
00
m�� � m
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mNM
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-4:. D
Page 10 of 10

City of Monroe
Reports of Lab
Analysis
2nI Quarter

Waypoint.(2)
ANALYTICAL
4/10/2023
City of Monroe
Ken Morris
775 Treeway Dr
Monroe, NC, 28110
Ref: Analytical Testing
Report Number: 23-094-0006
Project Description: RAS
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Dear Ken Morris:
Waypoint Analytical Virginia, Inc, received sample(s) on 4/4/2023 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Anaiysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information
Sincerely,
6
Brandi Watson
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 1 of 5

(D
Waypoint, 7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
ANALYTICAL www.waypointanalytical.com
Sample Summary Table
Report Number: 23-094-0006
Client Project Description: RAS
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
61581 RAS Solids 09/03/2023 10:00 04/04/2023 SM-254OG WP MTN
WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN
Page 2 of 5

Waypointo
ANALYTICAL
46205
City of Monroe Project RA5
Ken Morris
775 Treeway Dr Information
Monroe , NC 28110
Report Number : 23-094-0006 REPORTOFA
Lab No : 61581
Sample ID: RAS
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Pax 804-271-6446
www.waypointanalytical.com
Report Date : 04/10/2023
Received : 04/04/2023
fn
NAL YSIS l3randi Watson
Matrix: Solids
Sampled: 4/3/2023 10:00
Test Results units MQL DF Date / Time
Analyzed
By
Analytical
Method
Moisture 98.2 % 0.010 1 04105/2316:16
JLS
SM-2540G
Test Results units MQL DF Date 1 Time
By
Analytical
Analyzed
Method
Total Volatile Solids 77.7 % 0.010 1 04/05/23 16:16 JLS SM-2540G
Total Solids 1.80 % 0.010 1 04/05/23 16:16 JLS SM-2540G
Qualifiers/ DF Dilution Factor MQL Method Quantitation Limit
Definitions
Page 3 of 5

•
Waypoi nt .0 »Z� Wh 804-e Road, 1 11 Fa nd,804 27 23237
-6446
Main 804-743-9401 °Fax 804-2i1-6446
ANALYTICAL www.waypointanalytical.com
Shipment Receipt Form
Customer Number: 46205
Customer Name: City of Monroe
Report Number: 23-094-0006
Shipping Method
Fed Ex US Postal Lab Other
• UPS Client Courier Thermometer ID:
Shipping container/cooler uncompromised?
• Yes
No
Number of coolers/boxes received
Custody seals intact on shipping container/cooler?
Yes
No Not Present
Custody seals intact on sample bottles?
Yes
No Not Present
Chain of Custody (COC) present?
0 Yes
No
COC agrees with sample label(s)?
Yes
No
COC properly completed,
Yes
No
Samples in proper containers?
Yes
No
Sample containers intact?
Yes
No
Sufficient sample volume for indicated test(s)?
4k Yes
No
All samples received within holding time?
Yes
No
Cooler temperature in compliance?
4 Yes
No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
• Yes
No
Water - Sample containers properly preserved
• Yes
No NIA
Water - VOA vials free of headspace
Yes
No NIA
Trip Blanks received with VOAs
Yes
No • NIA
Soil VOA method 5035 — compliance criteria met
Yes
No 0 NIA
High concentration container (48 hr)
High concentration pre -weighed (methanol -14 d)
Low concentration Encore samplers (48 hr)
Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included?
Yes
• No
Comments:
Signature: David Lennon Date & Time: 04/04/2023 11:03:45
Page 4 of 5

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.
z o
dad
Z$X � a
a �,
CL � n
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CD
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Page 5 of 5

(2)
WayPAoi nt .
NALYTICAL
4/12/2023
City of Monroe
Ken Morris
775 Treeway Dr
Monroe, NC, 28110
7621 Whitepine Road, Richmond, WA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Ref: Analytical Testing
Report Number: 23-094-0008
Project Description: WWTP Cake
Dear Ken Morris:
Waypoint Analytical Virginia, Inc, received sample(s) on 4/4/2023 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Brandi Watson
Laboratory's liability in any claim relating to analyses performed shalt be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 1 of 7

•
7621 0 Whitepine Road, Richmond, VA 23237
Waypoint.
Main 804-743-9401 ° Fax [phone]
ANALYTICAL www.waypointanaiyflcal.com
Sample Summary Table
Report Number: 23-094-0008
Client Project Description: WWTP Cake
Lab No
Client Sample ID
Matrix
Date Collected
Date Received
Method
Lab ID
61583
WWTP Cake
Solids
04/03/2023 09:20
04/04/2023
61583
WWTP Cake
Solids
04/03/2023 09:20
04/04/2023
SM-4500-NH3C
WP MTN
61583
WWTP Cake
Solids
04/03/2023 09:20
04/04/2023
9045D
WP MTN
61583
WWTP Cake
Solids
04/03/2023 09:20
04/04/2023
4500NO3F-2011
WP MTN
61583
WWTP Cake
Solids
04/03/2023 09:20
04/04/2023
6310D
WP MTN
61583
WWTP Cake
Solids
04/03/2023 09:20
04/04/2023
SW-7471B
WP MTN
61583
VVWTP Cake
Solids
04/03/2023 09:20
04/04/2023
SM-4500-NH3C-TKN
WP MTN
61583
WWTP Cake
Solids
04/03/2023 09:20
04/04/2023
SM-2540G
WP MTN
WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN
Page 2 of 7

Waypointo
ANALYTICAL
46205
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
City of Monroe Project WWTP Cake
Ken Morris
775 Treeway Dr Information
Monroe, NC 28110
Report Number : 23-094-0008 REPORT OFANALYSIS
Lab No: 61583
Sample ID; WWTP Cake
Report Date : 04/12/2023
Received : 04/04/2023
&-Q,"
Brandi Watson
Matrix: Solids
Sampled: 4/3/2023 9:20
Test Results Units MQL DF Date I Time By Analytical
Analyzed Method
Moisture
85.3
%
0.010
Phosphorus
21200
mg/Kg - dry
34.0
Sulfur
9520
mg/Kg - dry
68.0
Calcium
19900
mg/Kg - dry
340
Aluminum
11300
mg/Kg - dry
34.0
Manganese
1800
mg/Kg - dry
3.40
Copper
320
mg/Kg - dry
3.40
Zinc
1080
mg/l - dry
8.50
Organic N
3$760
mg/l - dry
1701
Nickel
67.6
mg/Kg - dry
1.70
Lead
19.5
mg/Kg - dry
2.04
Arsenic
8.91
mg/Kg - dry
3.40
Selenium
5.89
mg/Kg - dry
3.40
Test
Results
Units
MOL
1
04/07/23 15:33
JLS
SM-2540G
1
04/07/23 21:32
BKN
6010D
1
04/07/23 21:32
TJS
6010D
1
04/07/23 21:32
BKN
6010D
1
04/07/23 21:32
TJS
6010D
1
04/07/23 21:32
BKN
6010D
1
04/07/23 21:32
BKN
6010D
1
04/07/23 21:32
BKN
6010D
1
04/11/23 07:30
CALCULATION
1
04/07/23 21:32
BKN
6010D
1
04/07/23 21:32
BKN
6010D
1
04/07/23 21:32
BKN
6010D
1
04/07/23 21:32
l
6010D
DF
Date / Time
By
Analytical
Analyzed
Method
Total Solids 14.7 % 0.010 1 04/07/23 15:33 JLS SM-2540G
Qualifiers/ DF Dilution Factor MQL Method Quantitation Limit
Definitions
Page 3 of 7

Waypointo
ANALYTICAL
46205
City of Monroe Project
Ken Morris
775 Treeway Dr Information
Monroe , NC 28110
Report Number: 23-094-0008
7621 White pine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
ATL
REPORTOFANAL PSIS
Report Date : 04/12/2023
Received : 04/04/2023
Brandi Watson
Lab No : 61583
Sample ID: WWTP Cake
Matrix: Solids
Sampled: 4/3/2023 9:20
Total Kjeldahl Nitrogen
38200
mg/Kg - dry
1700
1
04/11/23 07:30
JPJ ;M-4500-NH3C-TKP
Potassium
2650
mg/Kg - dry
68.0
1
04/07/23 21:32
BKN
6010D
Magnesium
2610
mg/Kg - dry
34.0
1
04/07/23 21:32
BKN
6010D
Sodium
816
mg/Kg - dry
170
1
04/07/23 21:32
BKN
6010D
Iron
27800
mg/Kg - dry
68.0
1
04/07/23 21:32
BKN
6010D
Ammonia Nitrogen
4410
mg/Kg - dry
680
1
04/11/23 11:00
JPJ
SM-4500-NH3C
Nitrate+Nitrite-N
71.4
mg/Kg - dry
34.0
1
04/11/23 12:47
ZBD
4500NO3F-2011
Cadmium
1.10
mg/Kg - dry
0.680
1
04/07/23 21 32
BKN
6010D
Chromium
55.3
mg/Kg - dry
1.70
1
04/07/23 21:32
BKN
6010D
Mercury
<1.14
mg/Kg - dry
1.14
1
04/06/23 12:26
FDS
SW-7471B
pH
7.6
S.U.
1
04/06/2317:05
CNB
9045D
Total Volatile Solids
65.2
%
0.010
1
04/07/23 15:33
JLS
SM-2540G
Molybdenum
14.4
mg/Kg - dry
1.70
1
04/07/23 21:32
BKN
6010D
Qualifiers/ DF Dilution Factor
Definitions
MQL Method Quantitation Limit
Page 4 of 7

Waypoint(D
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
www.waypointanalytical.com
Client: City of Monroe CASE NARRATIVE
Project: WWTP Cake
Lab Report Number: 23-094-0008
Date: 4/12/2023
Metals Analysis Method 6010D
Sample 93025
Analyte: Aluminum
QC Batch No: 1-675382/1-674400
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 93025
Analyte: Calcium
QC Batch No: 1-675086/1-674400
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 93025
Analyte: Iron
QC Batch No: 1-675086/1-674400
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 93025
Analyte: Potassium
QC Batch No: L675086/L674400
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 93025
Analyte: Selenium
QC Batch No: 1-675086/1-674400
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Sample 93025
Analyte: Zinc
QC Batch No: L675086IL674400
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Page 5 of 7

(2)23237
Waypoint. 7621 Whltapi -7 Road, 1 0 Fax [phone]
Main 804-743-9401 °Fax 804-271-fi446
ANALYTICAL www.waypointanalytical.com
Shipment Receipt Form
Customer Number: 46205
Customer Name: City of Monroe
Report Number: 23.094-0008
Shipping Method
Fed Ex US Postal Lab
0 UPS Client Courier
Other
Thermometer ID:
Shipping container/cooler uncompromised?
.0 Yes
No
Number of coolers/boxes received
1 '
Custody seals intact on shipping container/cooler?
Yes
No
• Not Present
Custody seals intact on sample bottles?
Yes
No
• Not Present
Chain of Custody (COC) present?
0 Yes
No
COC agrees with sample label(s)?
Yes
No
COC properly completed
• Yes
No
Samples in proper containers?
• Yes
No
Sample containers intact?
• Yes
No
Sufficient sample volume for indicated test(s)?
Yes
No
All samples received within holding time?
Yes
No
Cooler temperature in compliance?
• Yes
No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
Yes
• No
Water - Sample containers properly preserved
• Yes
No
NIA
Water - VOA vials free of headspace
Yes
No
NIA
Trip Blanks received with VOAs
Yes
No
NIA
Soil VOA method 5035 — compliance criteria met
Yes
No
NIA
High concentration container (48 hr)
High concentration pre -weighed (methanol -14 d)
Low concentration EnCore samplers (48 hr)
Low conc pre -weighed vials (Sad Bis -14 d)
Special precautions or instructions included?
Yes
• No
Comments:
Signature: David Lennon Date & Time: .04/04/2023 11:13:38
Page 6 of 7

I
q
w �
pNp
�w
W
Page 7 of 7

Waypoint(D
ANALYTICAL
4/12/2023
City of Monroe
Ken Morris
775 Treeway Dr
Monroe, NC, 28110
Ref: Analytical Testing
Report Number: 23-094-0007
Project Description: WTP Cake
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Dear Ken Morris:
Waypoint Analytical Virginia, Inc. received sample(s) on 4/4/2023 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information
Sincerely,
&W-r(f-k"t"
Brandi Watson
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 1 of 9

Waypoint,(D
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanaiytical-corn
Sample Summary Table
Report Number: 23-094-0007
Client Project Description: WTP Cake
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
61582
WTP Cake
Solids
04/03/2023 09:40
04/04/2023
61582
WTP Cake
Solids
04/03/2023 09:40
04/04/2023
SM-4500-NH3C
WP MTN
61582
WTP Cake
Solids
04/03/2023 09:40
04/04/2023
9045D
WP MTN
61582
WTP Cake
Solids
04/03/2023 09:40
04/04/2023
4500NO3F-2011
WP MTN
61582
WTP Cake
Solids
04/03/2023 09:40
04/04/2023
6010D
WP MTN
61582
WTP Cake
Solids
04/03/2023 09:40
04/04/2023
SW-7471B
WP MTN
61582
WTP Cake
Solids
04/03/2023 WAG
04/04/2023
SM-4500-NH3C-TKN
WP MTN
61582
WTP Cake
Solids
04/03/2023 09:40
04/04/2023
SM-2540G
WP MTN
WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN
Page 2 of 9

Waypointo
ANALYTICAL
46205
City of Monroe Project WTP Cake
Ken Morris
775 Treeway Dr Information
Monroe , NC 28110
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 1 Fax [phone]
www.waypointanalyflcal.com
Report Number: 23-094-0007 REPORT OF ANALYSIS
Lab No : 61582
Sample ID : WTP Cake
Report Date: 04/12/2023
Received : 04/04/2023
Brandi Watson
Matrix: Solids
Sampled: 4/3/2023 9:40
Test Results Units MQL DF Date I Time By Analytical
Analyzed Method
Moisture
74.7
%
0.010
1
04/07/2315:33
31-S
SM-2540G
Phosphorus
3350
mg/Kg - dry
198
10
04/11/23 00:10
JTR
6010D
Sulfur
2830
mg/Kg - dry
395
10
04/11/23 00:10
JTR
6010D
Calcium
2160
mg/Kg - dry
1980
10
04/11/23 00:10
JTR
6010D
Aluminum
12900
mg/Kg - dry
198
10
04/11/23 00:10
3TR
6010D
Manganese
735
mg/Kg - dry
19.8
10
04/11/23 00:10
JTR
6010D
Copper
423
mg/Kg - dry
19.8
10
04/11/23 00:10
JTR
6010D
Zinc
63.6
mg/Kg - dry
49.4
10
04/11/23 00:10
]TR
6010D
Organic N
48770
mg/Kg - dry
988.1
1
04/11/23 07:30
CALCULATION
Nickel
35.0
mg/Kg - dry
9.88
10
04/11/23 00:10
JTR
6010D
Lead
<11.9
mg/Kg - dry
11.9
10
04/11/23 00:10
JTR
6010D
Arsenic
22.5
mg/Kg - dry
19.8
10
04/11/23 00:10
JTR
6010D
Selenium
<19.8
mg/Kg - dry
19.8
10
04/11/23 00:10
JTR
6010D
Test
Results
Units
MQL
DF
Date I Time
By
Analytical
Analyzed
Method
Total Solids 25.3 % 0.010 1 04/07/23 15:33 JLS SM-254OG
Qualifiers/ DF Dilution Factor
Definitions
MQL Method Quantitation Limit
Page 3 of 9

Waypointo
ANALYTICAL
46205
City of Monroe Project WTP Cake
Ken Morris
775 Treeway Dr Information
Monroe , NC 28110
Report Number:23-094-0007
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
REPORT OF ANALYSIS
Report Date: 04/12/2023
Received : 04/04/2023
4
Brandi Watson
Lab No; 61582
Sample ID : WrP Cake
Matrix: Solids
Sampled: 4/3/2023 9:40
Total Kjeldahl Nitrogen
51000
mg/Kg - dry
988
1
04/11/23 07:30
JPJ tM-4500-NH3C-TKP
Potassium
411
mg/Kg - dry
395
10
04/11/23 00:10
JTR
6010D
Magnesium
613
mg/Kg - dry
198
10
04/11/23 00:10
JTR
6010D
Sodium
<988
mg/Kg - dry
988
10
04/11/23 00:10
JTR
6010D
Iron
347000
mg/Kg - dry
395
10
04/11/23 00:10
JTR
6010D
Ammonia Nitrogen
2220
mg/Kg - dry
395
1
04/11/23 11:00
JPJ
SM-4500-NH3C
Nitrate+Nitrite-N
<19,8
mg/Kg - dry
19.8
1
04/11/23 12:46
ZBD
4500NO3F-2011
Cadmium
<3.95
mg/Kg - dry
3.95
10
04/11/23 00:10
JTR
6010D
Chromium
248
mg/Kg - dry
9.88
10
04/11/23 00:10
JTR
6010D
Mercury
<0.684
mg/Kg - dry
0.684
1
04/06/23 12:25
FDS
SW-7471B
pH
7,6
S.U.
1
04/06/2317:05
CNB
9045D
Total Volatile Solids
34.2
%
0.010
1
04/07/23 15:33
JLS
SM-254OG
Molybdenum
45.8
mg/Kg - dry
9.88
10
04/11/23 00:10
JTR
6010D
Qualifiers/ DF Dilution Factor
Definitions
MQL Method Quantitation Limit
Page 4 of 9

WayPAa nt .
NALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Client: City of Monroe CASE NARRATIVE
Project: WTP Cake
Lab Report Number: 23-094-0007
Date: 4/12/2023
Metals Analysis Method 6010D
Sample 61582 (WTP Cake)
Analyte: Aluminum
QC Batch No: 1-675086/1-674400
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Sample 93025
Analyte: Aluminum
QC Batch No: 1-675382/1-674400
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 61582 (WTP Cake)
Analyte: Arsenic
QC Batch No: 1-675086/1-674400
This analyte was analyzed at a dilution due to IEC interferencelmatrix interference.
Sample 61582 (WTP Cake)
Analyte: Calcium
QC Batch No: 1-675086/1-674400
This analyte was analyzed at a dilution due to IEC interferencelmatrix interference.
Sample 93025
Analyte: Calcium
QC Batch No: 1-675086/1-674400
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 61582 (WTP Cake)
Analyte: Cadmium
QC Batch No: L675086/L674400
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Sample 61582 (WTP Cake)
Analyte: Chromium
QC Batch No: 1-675086/1-674400
This analyte was analyzed at a dilution due to IEC interferencelmatrix interference.
Sample 61582 (WTP Cake)
Analyte: Copper
QC Batch No- 1-675086/1-674400
This analyte was analyzed at a dilution due to IEC interferencelmatrix interference.
Sample 61582 (WTP Cake)
Analyte: Iron
Page 5 of 9

WaYPO4Int.
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
www.waypointanalytical.com
QC Batch No: 1-675086/1-674400
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Sample 93025
Analyte: Iron
QC Batch No: 1-675086/1-674400
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 61582 (WTP Cake)
Analyte: Potassium
QC Batch No: L675086/L674400
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Sample 93025
Analyte: Potassium
QC Batch No: 1-675086/1-674400
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 61582 (WTP Cake)
Analyte: Magnesium
QC Batch No: L6750861L674400
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Sample 61582 (WTP Cake)
Analyte: Manganese
QC Batch No: L675086/1-674400
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Sample 61582 (WTP Cake)
Analyle: Molybdenum
QC Batch No: 1-675086/1-674400
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Sample 61582 (WTP Cake)
Analyte: Sodium
QC Batch No: L675086/L674400
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Sample 61582 (WTP Cake)
Analyte: Nickel
QC Batch No: L675086IL674400
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Sample 61582 (WTP Cake)
Analyte: Phosphorus
QC Batch No: 1-675086/1-674400
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Sample 61582 (WTP Cake)
Analyte: Lead
QC Batch No: 1-6750861674400
Page 6 of 9

WayR?unt(2)YTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
This analyte was analyzed at a dilution due to IEC. interference/matrix interference.
Sample 61582 (WTP Cake)
Analyte: Sulfur
QC Batch No: L675086/L674400
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Sample 61582 (WTP Cake)
Analyte: Selenium
QC Batch No: L675086/L674400
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Sample 93025
Analyte: Selenium
QC Batch No: L675086/1-674400
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Sample 61582 (WTP Cake)
Analyte: Zinc
QC Batch No: L675086/L674400
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Sample 93025
Analyte: Zinc
QC Batch No: L675086/1-674400
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Page 7 of 9

(2) 7621 Whitepine Road, Richmond, VA 23237
Waypoint,Main 804-743.9401 ° Fax [phone]
ANALYTICAL www.waypointanalytical.com
Shipment Receipt Form
Customer Number: 46205
Customer Name: City of Monroe
Report Number: 23-094-0007
Shipping Method
Fed Ex US Postal Lab Other
• UPS Client Courier Thermometer ID:
Shipping container/cooler uncompromised?
• Yes
No
Number of coolers/boxes received
F 1
Custody seals intact on shipping container/cooler?
Yes
No • Not Present
Custody seals intact on sample bottles?
Yes
No • Not Present
Chain of Custody (COC) present?
Yes
No
COG agrees with sample label(s)?
01 Yes
No
COC properly completed
Yes
No
Samples in proper containers?
Yes
No
Sample containers intact?
0 Yes
No
Sufficient sample volume for indicated test(s)?
0 Yes
No
All samples received within holding time?
• Yes
. No
Cooler temperature in compliance?
•. Yes
No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
0 Yes
No
Water - Sample containers properly preserved
Yes
No • NIA
Water - VOA vials free of headspace
Yes
No • NIA
Trip Blanks received with VOAs
Yes
No 0 NIA
Soil VOA method 5035 -- compliance criteria met
Yes
No 46 NIA
High concentration container (48 hr)
High concentration pre -weighed (methanol -14 d)
Low concentration EnCore samplers (48 hr)
Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included?
Yes
• No
Comments:
Signature: David Lennon
Date & Time: 04/04/2023 11:08:54
Page 8 of 9

I"
Page 9 of 9

City of Monroe
Reports of Lab
Analysis
3rI Quarter

Waypoolnt(2)
ANALYTICAL
7/12/2023
City of Monroe
Ken Morris
775 Treeway Dr
Monroe, NC, 28110
Ref: Analytical Testing
Report Number: 23-187-0002
Project Description: RAS
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Dear Ken Morris:
Waypoint Analytical Virginia, Inc. received sample(s) on 7/6/2023 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information
Sincerely,
Brandi Watson
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 1 of 5

(2)
Waypoint, 7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
ANALYTICAL www.waypointanalytical.com
Sample Summary Table
Report Number: 23-187-0002
Client Project Description: RAS
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
62543 RAS Solids 07/05/2023 09:25 07/06/2023 SM-2540G WP MTN
WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN
Page 2 of 5

Waypointo
ANALYTICAL
46205
City of Monroe Project RAS
Ken Morris
775 Treeway Or Information
Monroe, NC 28110
Report Number : 23-187-0002
Lab No : 62543
Sample ID : RAS
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
REPORT OFANAL Y5.75
Report Date : 07/12/2023
Received : 07/06/2023
C7 W'r t-7"
Brandi Watson
Matrix: Solids
Sampled: 7/5/2023 9:25
Test Results Units MQL DF Date / Time By Analytical
Analyzed Method
Moisture
98.5
%
0.010
Test
Results
Units
MOL
Total Solids 1.51 % 0.010
Total Volatile Solids 73.2 % 0.010
1 07/10/2316:06 KDO SM-2540G
DF Date I Time By Analytical
Analyzed Method
1 07/10/2316:06 KDO SM-2540G
1 07/10/2316:06 KOO SM-2540G
Qualifiers/ DF Dilution Factor MQL Method Quantitation Limit
Definitions
Page 3 of 5

Waypoint.(D
ANALYTICAL
7621 Whltepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Shipment Receipt Form
Customer Number: 46205
Customer Name: City of Monroe
Report Number: 23-187-0002
Shipping Method
Fed Ex US Postal Lab
• UPS Client Courier
Other
Thermometer ID:
Shipping container/cooler uncompromised?
• Yes
No
Number of coolers/boxes received
F
Custody seals intact on shipping container/cooler?
Yes
'; No
.0. Not Present
Custody seals intact on sample bottles?
Yes
No
16Not Present
Chain of Custody (COC) present?
• Yes
No
COC agrees with sample label(s)?
• Yes
No
COC properly completed
0: Yes
No
Samples in proper containers?
• Yes
No
Sample containers intact?
• Yes
j No
Sufficient sample volume for indicated test(s)?
46; Yes
No
All samples received within holding time?
Yes
No
Cooler temperature in compliance?
0 Yes
No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
0 Yes
-
No
Water - Sample containers properly preserved
• Yes
No
NIA
Water - VOA vials free of headspace
Yes
No
0 NIA
Trip Blanks received with VOAs
Yes
No
• NIA
Soil VOA method 5035 — compliance criteria met
Yes
No
• NIA
High concentration container (48 hr)
High concentration pre -weighed (methanol -14 d)
Low concentration Encore samplers (48 hr)
Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included?
Yes
• No
Comments
Signature: David Lennon Date & Time: 07/06/2023 09:31:05
Page 4 of 5

Page 5 of 5

Waypoint.(D
ANALYTICAL
7/17/2023
City of Monroe
Ken Morris
775 Treeway Dr
Monroe, NC, 28110
Ref: Analytical Testing
Report Number: 23-187-0004
Project Description: WWTP Cake
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Dear Ken Morris:
Waypoint Analytical Virginia, Inc. received sample(s) on 7/6/2023 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Q
Brandi Watson
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analys+s in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 1 of 8

Waypoint(2)
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Sample Summary Table
Report Number: 23-187-0004
Client Project Description: WWTP Cake
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
62545
WWTP Cake
Solids
07/05/2023 09:50
07/06/2023
62545
WWTP Cake
Solids
07/05/2023 09:50
07/06/2023
62545
WWTP Cake
Solids
07/05/2023 09:50
07/06/2023
62545
WWTP Cake
Solids
07/05/2023 09:50
07/06/2023
62545
VA TP Cake
Solids
07/05/2023 09:50
07/06/2023
62545
WWTP Cake
Solids
07/05/2023 09:50
07/06/2023
62545
WWTP Cake
Solids
07/05/2023 09:50
07/06/2023
62545
WWTP Cake
Solids
07/05/2023 09:50
07/06/2023
WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN
SM-4500-NH3C
WP MTN
9045D
WP MTN
4500NO3F-2011
WP MTN
6010D
WP MTN
SW-74718
WP MTN
SM-4500-NH3C-TKN
WP MTN
SM-2540G
WP MTN
Page 2 of 8

Waypointo
ANALYTICAL
46205
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
City of Monroe Project WWTP Cake
Ken Morris
775 Treeway Dr Information
Monroe, NC 28110
Report Number : 23-187-0004 REPORT OFANAL YSIS
Lab No : 62545
Sample ID: WWTP Cake
Report Date : 07/17/2023
Received : 07/06/2023
&W-wc vwt,"
Brandi Watson
Matrix: Solids
Sampled: 7/5/2023 9:50
Test Results Units MOL DF Date / Time By Analytical
Analyzed Method
Moisture
73.8
%
0.010
Phosphorus
12600
mg/Kg - dry
19.1
Sulfur
6370
mg/Kg - dry
38.2
Calcium
14600
mg/Kg - dry
191
Aluminum
6410
mg/Kg - dry
19.1
Manganese
1270
mg/Kg - dry
1.91
Copper
265
mg/Kg - dry
1.91
Zinc
679
mg/Kg - dry
4.77
Organic N
30570
mg/Kg - dry
954.2
Nickel
51.1
mg/Kg - dry
0.954
Lead
11.3
mg/Kg - dry
1.15
Arsenic
11.0
mg/Kg - dry
1.91
Selenium
<9.54
mg/Kg - dry
9.54
Test
Results
Units
MOL
1
07/10/2316:06
KDO
SM-2540G
1
07/11/23 22:44
BKN
6010D
1
07/11/23 22:44
BKN
6010D
1
07/11/23 22:44
BKN
6010D
1
07/11/23 22:44
BKN
6010D
1
07/11/23 22:44
BKN
6010D
1
07/11/23 22:44
BKN
60101)
1
07/11/23 22:44
BKN
6010D
1
07/13/23 08:30
CALCULATION
1
07/11/23 22:44
BKN
6010D
1
07/11/23 22:44
BKN
6010D
1
07/11/23 22:44
BKN
6010D
5
07/12/23 20:17
BKN
6010D
DF
Date / Time
By
Analytical
Analyzed
Method
Total Solids 26.2 % 0.010 1 07/10/23 16:06 KDO SM-254OG
Qualifiers/ DF Dilution Factor
Definitions
MQL Method Quantitation Limit
Page 3 of 8

Waypointo
ANALYTICAL
46205
City of Monroe Project
Ken Morris
775 Treeway Dr Information
Monroe, NC 28110
Report Number : 23-187-0004
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
WWfP Cake
REPORT OFANAL YSIS
Report Date : 07/17/2023
Received : 07/06/2023
&wvw
Brandi Watson
Lab No : 62545
Sample ID : WVVTP Cake
Matrix: Solids
Sampled: 7/5/2023 9:50
Total Kjeldahl Nitrogen
36300
mg/Kg - dry
954
1
07/13/23 08:30
JPJ ;M-4500-NH3C-TKt
Potassium
2100
mg/Kg - dry
38.2
1
07/14/23 18:00
BKN
6010D
Magnesium
1580
mg/Kg - dry
19.1
1
07/11/23 22:44
BKN
6010D
Sodium
691
mg/Kg - dry
95.4
1
07/13/23 12:25
BKN
6010D
Iron
104000
mg/Kg - dry
191
5
07/12/23 20:17
BKN
6010D
Ammonia Nitrogen
5690
mg/Kg - dry
382
1
07/13/23 14:00
JPJ
SM-4500-NH3C
Nitrate+Nitrite-N
<19.1
mg/Kg - dry
19.1
1
07/11/23 15:02
CLP
4500NO3F-2011
Cadmium
2.34
mg/Kg - dry
0.382
1
07/11/23 22:44
BKN
6010D
Chromium
87.4
mg/Kg - dry
0.954
1
07/11/23 22:44
BKN
6010D
Mercury
0.702
mg/Kg - dry
0.630
1
07/12/23 11:32
FDS
SW-7471B
pH
8.3
S.U.
1
07/12/2317:00
CNB
9045D
Total Volatile Solids
72.3
%
0.010
1
07/10/23 16:06
KDO
SM-254OG
Molybdenum
18.8
mg/Kg - dry
0.954
1
07/11/23 22:44
BKN
6010D
Qualifiers/ DF Dilution Factor
Definitions
MQL Method Quantitation Limit
Page 4 of 8

Waypoint(D
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Client: City of Monroe CASE NARRATIVE
Project: WWTP Cake
Lab Report Number: 23-187-0004
Date: 7/17/2023
Metals Analysis Method 6010D
Sample 97275 (6)
Analyte: Aluminum
QC Batch No: 1-692529/1-691749
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 97275 (6)
Analyte: Calcium
QC Batch No: 1-692204/1-691749
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 97275 (6)
Analyte: Iron
QC Batch No: L6922041L691749
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 97275 (6)
Analyte: Potassium
QC Batch No: 1-692204/1-691749
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Sample 97275 (6)
Analyte: Potassium
QC Batch No: 1-692529/1-691749
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Sample 99366 (Limefiber)
Analyte: Aluminum
QC Batch No: 1-693026/1-692796
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 99366 (Limefiber)
Analyte: Iron
QC Batch No: 1-693026/1-692716
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 99366 (Limefiber)
Analyte: Magnesium
Page 5 of 8

Waypdlont,(2)
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
QC Batch No: L693026IL692716
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 99366 (Limefiber)
Analyte: Molybdenum
QC Batch No: 1-693026/1-692716
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Sample 99366 (Limefiber)
Analyte: Phosphorus
QC Batch No: L693026/L692716
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 99366 (Limefiber)
Analyte: Sulfur
QC Batch No: 1-693026/1-692716
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 99366 (Limefiber)
Analyte: Selenium
QC Batch No: L693026/L692716
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Sample 99366 (Limefiber)
Analyte: Zinc
QC Batch No: 1-693026/1-692716
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Page 6 of 8

(2)Waypoint 7621 ain $ 4-7 Road, Richmond, 27 -6447
Main 8d4-743-940I 0Fax [phone]
ANALYTICAL www.waypointanalytical.com
Shipment Receipt Form
Customer Number: 46205
Customer Name: City of Monroe
Report Number: 23-187-0004
Shipping Method
Fed Ex US Postal Lab Other
• UPS Client Courier Thermometer ID:
Shipping container/cooler uncompromised?
• Yes
No
Number of coolers/boxes received
1
Custody seals intact on shipping container/cooler?
Yes
No Not Present
Custody seals intact on sample bottles?
_ , Yes
_ No Not Present
Chain of Custody (COC) present?
Yes
No
COC agrees with sample label(s)?
•) Yes
No
COC properly completed
0% Yes
No
Samples in proper containers?
• Yes
No
Sample containers intact?
91 Yes
No
Sufficient sample volume for indicated test(s)?
Yes
No
All samples received within holding time?
• Yes
No
Cooler temperature in compliance?
• Yes
No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
0. Yes
No
Water - Sample containers properly preserved
• Yes
No NIA
Water - VOA vials free of headspace
Yes
No • NIA
Trip Blanks received with VOAs
Yes
No • NIA
Soil VOA method 5035 — compliance criteria met
Yes
No NIA
High concentration container (48 hr)
High concentration pre -weighed (methanol -14 d)
Low concentration EnCore samplers (48 hr)
Low cone pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included?
Yes
No
Comments:
Signature: David Lennon
Date & Time: 07/06/2023 10:25:16
Page 7 of 8

NEI
MEE 0
MENEM
MENEM
MEMO
Page 8 of 8

Waypoint(D
ANALYTICAL
7/17/2023
City of Monroe
Ken Morris
775 Treeway Dr
Monroe, NC, 28110
Ref: Analytical Testing
Report Number: 23-187-0003
Project Description: WTP Cake
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Dear Ken Morris:
Waypoint Analytical Virginia, Inc. received sample(s) on 7/6/2023 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information
Sincerely,
Qu.�ety
Brandi Watson
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 1 of 8

Waypoint(2)
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main $04-743-9401 ° Fax [phone]
www.waypointanaiytical.com
Sample Summary Table
Report Number: 23-187-0003
Client Project Description: WTP Cake
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
62544
WTP Cake
Solids
07/05/2023 08:45
07/06/2023
62544
WTP Cake
Solids
07/05/2023 08:45
07/06/2023
62544
WTP Cake
Solids
07/05/2023 08:45
07/06/2023
62544
WTP Cake
Solids
07/05/2023 08:45
07/06/2023
62544
WTP Cake
Solids
07/05/2023 08:45
07/06/2023
62544
WTP Cake
Solids
07/05/2023 08:45
07/06/2023
62544
WTP Cake
Solids
07/05/2023 08:45
07/06/2023
62544
WTP Cake
Solids
07/05/2023 08:45
07/06/2023
WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN
SM-4500-NH3C
WP MTN
9045D
WP MTN
4500NO3F-2011
WP MTN
6010D
WP MTN
SW-74716
WP MTN
SM-4500-NH3C-TKN
WP MTN
SM-2540G
WP MTN
Page 2 of 8

Waypoeinto.
ANALYTICAL
46205
City of Monroe Project WT'P Cake
Ken Morris
775 Treeway Dr Information
Monroe , NC 28110
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Report Number : 23-187-0003 REPORTOF ANAL YSIS
Lab No : 62544
Sample ID : WTP Cake
Report Date : 07/17/2023
Received : 07/06/2023
Brand! Watson
Matrix: Solids
Sampled: 7/5/2023 8:45
Test Results Units MQL DF Date I Time Sy Analytical
Analyzed Method
Moisture
68.3
%
0.010
Phosphorus
2770
mg/Kg - dry
15.8
Sulfur
2490
mg/Kg - dry
31.5
Calcium
2210
mg/Kg - dry
158
Aluminum
4790
mg/Kg - dry
15.8
Manganese
890
mg/Kg - dry
1.58
Copper
385
mg/Kg - dry
1.58
Zinc
47.6
mg/Kg - dry
3.94
Organic N
11200
mg/Kg - dry
788.6
Nickel
52.1
mg/Kg - dry
0,788
Lead
7.82
mg/Kg - dry
0.946
Arsenic
21.5
mg/Kg - dry
1.58
Selenium
<7.89
mg/Kg - dry
7.89
Test
Results
Units
MQL
Total Solids
Qualifiers/ DF Dilution Factor
Definitions
1
07110/2316:06
KDO
SM-2540G
1
07/11/23 22:29
BKN
6010D
1
07/11/23 22:29
BKN
6010D
1
07/11/23 22.29
BKN
6010D
1
07/11/23 22:29
BKN
6010D
1
07/11/23 22:29
BKN
6010D
1
07/11/23 22:29
BKN
6010D
1
07/11/23 22:29
BKN
6010D
1
07/13/23 08:30
CALCULATION
1
07/11/23 22:29
BKN
6010D
1
07/11/23 22:29
BKN
6010D
1
07/11/23 22:29
BKN
6010D
5
07/12/23 20:07
BKN
6010D
DF
Date / Time
By
Analytical
Analyzed
Method
31.7 % 0.010 1 07/10/2316:06 KDO SM-2540G
MQL Method Quantitation Limit
Page 3 of 8

Waypointo
ANALYTICAL
46205
City of Monroe Project WTP Cake
Ken Morris
775 Treeway Dr Information
Monroe , NC 28110
Report Number : 23-187-0003
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
REPORrOFANALYSIS
Report Date : 07/17/2023
Received : 07/06/2023
Brandi Watson
Lab No : 62544
Sample ID: WTP Cake
Matrix: Solids
Sampled: 7/5/2023 8:45
Total Kjeldahl Nitrogen
12200
mg/Kg - dry
789
1
07/13/23 08:30
JPJ ;M-4500-NH3C-TKt
Potassium
246
mg/Kg - dry
31.5
1
07/14/23 17:55
BKN
6010D
Magnesium
445
mg/Kg - dry
15.8
1
07/13/23 12:10
BKN
6010D
Sodium
394
mg/Kg - dry
78.9
1
07/13/23 12:10
BKN
6010D
Iron
273000
mg/Kg - dry
631
20
07/13/23 12:20
BKN
6010D
Ammonia Nitrogen
978
mg/Kg - dry
315
1
07/13/23 14:00
JPJ
SM-4500-NH3C
Nitrate+ Nitr ite-N
<15.8
mg/Kg - dry
15.8
1
07/11/23 15:01
CLP
4500NO3F-2011
Cadmium
16.0
mg/Kg - dry
0.315
1
07/11/23 22:29
BKN
6010D
Chromium
207
mg/Kg - dry
0.788
1
07/11/23 22:29
BKN
6010D
Mercury
<0.549
mg/Kg - dry
0.549
1
07/12/23 11 31
FDS
SW-7471B
pH
6.1
S.U.
1
07/12/2317:00
CNB
9045D
Total Volatile Solids
40.6
%
0.010
1
07/10/23 16:06
KDO
SM-2540G
Molybdenum
42.3
mg/Kg - dry
0.788
1
07/11/23 22:29
BKN
6010D
Qualifiers/ DF Dilution Factor
Definitions
MQL Method Quantitation Limit
Page 4 of 8

WayPAof nt
NALYTICAL
Client: City of Monroe
Project: WTP Cake
Lab Report Number: 23-187-0003
Date: 7/17/2023
7621 Whitepine Road, Richmond, VA 23237
Main 804.743-9401 ° Fax [phone]
www.waypointanalytical.com
CASE NARRATIVE
Metals Analysis Method 6010D
Sample 97275 (6)
Analyte: Aluminum
QC Batch No: L692529/1-691749
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 97275 (6)
Analyte: Calcium
QC Batch No: L692204/L691749
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 97275 (6)
Analyte: Iron
QC Batch No: 1-692204/1-691749
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 97275 (6)
Analyle: Potassium
QC Batch No: 1-692204/1-691749
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Sample 97275 (6)
Analyte: Potassium
QC Batch No: 1-692529/1-691749
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Sample 99366 (Limefiber)
Analyte: Aluminum
QC Batch No: 1-693026/1-692716
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 99366 (Limefiber)
Analyte: Iron
QC Batch No: 1-693026/1-692716
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 99366 (Limefiber)
Analyte: Magnesium
Page 5 of 8

Waypdint-(2)
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804.743-9401 ° Fax [phone]
www.waypointanalytical.com
QC Batch No: 1-693026/1-692716
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 99366 (Limefiber)
Analyte: Molybdenum
QC Batch No: 1-693026/1-692716
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Sample 99366 (Limefiber)
Analyte: Phosphorus
QC Batch No: 1-693026/1-692716
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 99366 (Limefiber)
Analyte: Sulfur
QC Batch No: L6930261L692716
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 99366 (Limefiber)
Analyte: Selenium
QC Batch No: 1-693026/1-692716
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Sample 99366 (Limefiber)
Analyte: Zinc
QC Batch No: 1-693026/1-692716
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Page 6 of 8

WaypointO
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
www,waypointanalytical.com
Shipment Receipt Form
Customer Number: 46205
Customer Name: City of Monroe
Report Number: 23-187-0003
Shipping Method
Fed Ex US Postal Lab
0 UPS Client Courier
Other
Thermometer ID:
Shipping container/cooler uncompromised?
AD Yes
No
Number of coolers/boxes received
F 1
Custody seals intact on shipping container/cooler?
Yes
No
W Not Present
Custody seals intact on sample bottles?
Yes
No
• Not Present
Chain of Custody (COC) present?
0 Yes
No
COC agrees with sample label(s)?
• Yes
No
COC properly completed
• Yes
No
Samples in proper containers?
• Yes
No
Sample containers intact?
Yes
No
Sufficient sample volume for indicated test(s)?
• Yes
No
All samples received within holding time?
io Yes
No
Cooler temperature in compliance?
• Yes
No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
• Yes
No
Water - Sample containers properly preserved
0 Yes
No
N/A
Water - VOA vials free of headspace
Yes
No
• NIA
Trip Blanks received with VOAs
Yes
No
N/A
Soil VOA method 5035 — compliance criteria met
Yes
No
• NIA
High concentration container (48 hr)
High concentration pre -weighed (methanol -t 4 d)
Low concentration EnCore samplers (48 hr)
Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included?
Yes
� No
Comments:
Signature: David Lennon
Date & Time: 07/06/2023 09,42:53
Page 7 of 8

Page 8 of 8

Waypoint,(2)
ANALYTICAL
8/16/2023
City of Monroe
Ken Morris
775 Treeway Dr
Monroe, NC, 28110
Ref: Analytical Testing
Report Number: 23-222-0001
Project Description: RAS
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Dear Ken Morris:
Waypoint Analytical Virginia, Inc, received sample(s) on 8/10/2023 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Q
Brandi Watson
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 1 of 5

Waypoint.(D
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743.9401 ° Fax [phone]
www.waypointanalytical.com
Sample Summary Table
Report Number: 23-222-0001
Client Project Description: RAS
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
63045 RAS
Solids 08/09/2023 08:45 08/10/2023 SM-2540G WP MTN
WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN
Page 2 of 5

Waypointo
ANALYTICAL
46205
City of Monroe Project RAS
Ken Morris
775 Treeway Dr Information
Monroe , NC 28110
Report Number : 23-222-0001
Lab No : 63045
Sample ID: RAS
REPORT OF
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
www.waypointanalytical.com
Report Date : 08/16/2023
Received : 08/10/2023
&W'�v
MLYSIS Brandi Watson
Matrix: Solids
Sampled: 8/9/2023 8:45
Test Results Units MQL DF Date / Time By Analytical
Analyzed Method
Total Solids
Total Volatile Solids
Analytical Method: 5M-2540G
Test
1.63 % 0.010 1 08/14/23 16:57 CIR SM-254OG
73.8 % 0.010 1 08/14/23 16:57 OR SM-254OG
Results Units MQL DF Date / Time By Analytical
Analyzed Batch
Moisture 98.4 % 0.010
Qualifiers/ DF Dilution Factor
Definitions
1 08/14/23 16:57 CIR L698535
MQL Method Quantitation Limit
Page 3 of 5

•
Waypoi nt 7621 Whltepi -7 Road3-94 1 u Fa nd,804 27 23237
-6446
Main 804-743-9401 °Fax [phone]
ANALYTICAL www.waypointanalytical.com
Shipment Receipt Form
Customer Number: 46205
Customer Name:
City of Monroe
Report Number:
23-222-0001
Fed Ex
US Postal
• UPS
Client
Shipping Method
Lab Other
Courier Thermometer ID:
Shipping container/cooler uncompromised?
Yes
No
Number of coolers/boxes received
1 '
Custody seals intact on shipping container/cooler?
Yes
No
• Not Present
Custody seals intact on sample bottles?
Yes
, _ No
40 Not Present
Chain of Custody (COC) present?
Yes
No
COG agrees with sample label(s)?
• Yes
No
COC properly completed
• Yes
No
Samples in proper containers?
• Yes
No
Sample containers intact?
Yes
No
Sufficient sample volume for indicated test(s)?
Yes
No
All samples received within holding time?
,40 Yes
No
Cooler temperature in compliance?
• Yes
No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
0 Yes
No
Water - Sample containers properly preserved
• Yes
No
NIA
Water - VOA vials free of head space
Yes
No:
NIA
Trip Blanks received with VOAs
Yes
No
N/A
Soil VOA method 5035 — compliance criteria met
Yes
No
6 NIA
High concentration container (48 hr)
High concentration pre -weighed (methanol -14 d)
Low concentration EnCore samplers (48 hr)
Low cone pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included?
Yes
.0 No
Comments:
Signature: David Lennon Date & Time: 08/10/2023 09:05:02
Page 4 of 5

gen
wing �
� � I � �
ARN jis'IS
v
F"
CL
gala
w
FB
A
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co
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1
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V
N
Page 5 of 5

Waypoint-(21
ANALYTICAL
8/28/2023
City of Monroe
Ken Morris
775 Treeway Dr
Monroe, NC, 28110
Ref: Analytical Testing
Report Number: 23-222-0002
Project Description: WWTP Cake
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Dear Ken Morris:
Waypoint Analytical Virginia, Inc. received sample(s) on 8/10/2023 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information
Sincerely,
B racy
Brandi Watson
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 1 of 8

Waypoint.(2)
ANALYTICAL
Report Number: 23-222-0002
Client Project Description: WWTP Cake
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Sample Summary Table
Lab No
Client Sample ID
Matrix
Date Collected
Date Received
Method
Lab ID
63046
WWTP Cake
Solids
08/09/2023 09:10
08/10/2023
63046
WWTP Cake
Solids
08/09/2023 09:10
08/10/2023
SM-4500-NH3C
WP MTN
63046
WWTP Cake
Solids
08/09/2023 09:10
08/10/2023
9045D
WP MTN
63046
WWTP Cake
Solids
08/09/2023 09:10
08/10/2023
4500NO3F-2016
WP MTN
63046
WWTP Cake
Solids
08/09/2023 09:10
08/10/2023
6010D
WP MTN
63046
WWTP Cake
Solids
08/09/2023 09:10
08/10/2023
SW-7471B
WP MTN
63046
WWTP Cake
Solids
08/09/2023 09:10
08/10/2023
SM-4500-NH3C-TKN
WP MTN
63046
WWTP Cake
Solids
08/09/2023 09:10
08/10/2023
SM-254OG
WP MTN
WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN
Page 2 of 8

0
7521 Whitepine Road, Richmond, VA 23237
Waypoint,
Main 804-743-9401 ° Fax [phone]
ANALYTICAL www.waypointanalytical.com
46205
City of Monroe Project WWTP Cake
Ken Morris Report Date : 08/28/2023
775 Treeway Dr Information : Received : 08/10/2023
Monroe , NC 28110
Report Number: 23-222-0002 IeEPURTOPA/YALYSIS Brand! Watson
Lab No : 63046 Matrix: Solids
Sample ID : WVJTP Cake Sampled: 8/9/2023 9:10
Test Results Units MOL DF Date I Time By Analytical
Analyzed Method
Moisture
82.0
%
0.010
Phosphorus
22900
mg/Kg - dry
27.8
Sulfur
10800
mg/Kg - dry
55.6
Calcium
21200
mg/Kg - dry
278
Aluminum
12800
mg/Kg - dry
27.8
Manganese
2010
mg/Kg - dry
2.78
Copper
342
mg/Kg - dry
2.78
Zinc
1210
mg/Kg - dry
6.94
Organic N
44680
mg/Kg - dry
1389
Nickel
70.6
mg/Kg - dry
1.39
Lead
22.6
mgJKg - dry
1.67
Arsenic
9.39
mg/Kg - dry
2.78
Selenium
7.00
mg/Kg - dry
2.78
Test
Results
Units
MOL
1
08/16/23 17:40
CJR
5M-2540G
1
08/22/23 22:07
BKN
6010D
1
08/22/23 22:07
BKN
6010D
1
08/22/23 22:07
BKN
6010D
1
08/22/23 22:07
BKN
6010D
1
08/22/23 22:07
BKN
6010D
1
08/22/23 22:07
BKN
6010D
1
08/22/23 22:07
BKN
6010D
1
08/17/2310:00
CALCULATION
1
08/22/23 22:07
BKN
6010D
1
08/22/23 22:07
BKN
6010D
1
08/22/23 22:07
BKN
6010D
1
08/22/23 22:07
BKN
6010D
DF
Date / Time
By
Analytical
Analyzed
Method
Total Solids 18.0 % 0.010 1 08/16/23 17:40 CJR SM-254OG
Qualifiers/ DF Dilution Factor
Definitions
MQL Method Quantitation Limit
Page 3 of 8

(D
��`7621 Whitepine Raad, Richmond, VA 23237
WayP
Main 804-743-9401 0 Fax [phone]
ANALYTICAL www.waypointanalytical.com
46205
City of Monroe Project WWTP Cake
Ken Morris Report Date : 08/28/2023
775 Treeway Dr Information : Received : 08/10/2023
Monroe , NC 28110
&t,"
Report Number :23-222-0002 REFORTOFANALYS,iS Brandi Watson
Lab No : 63046
Sample ID : WWTP Cake
Matrix: Solids
Sampled: 8/9/2023 9:10
Total Kjeldahl Nitrogen
46400
mg/Kg - dry
1390
1
08/17/23 10:00
JPJ iM-4500-NH3C-TKP
Potassium
2870
mg/Kg - dry
55.6
1
08/22/23 22:07
BKN
6010D
Magnesium
2820
mg/Kg - dry
27.8
1
08/22/23 22:07
BKN
6010D
Sodium
961
mg/Kg - dry
139
1
08/22/23 22:07
BKN
6010D
Iron
31400
mg/Kg - dry
55.6
1
08/22/23 22:07
BKN
6010D
Ammonia Nitrogen
1710
mg/Kg - dry
556
1
08/25/23 15:45
JPJ
SM-4500-NH3C
Nitrate+ Nitrite-N
84.4
mg/Kg - dry
27.8
1
08/16/23 13:58
CLP
4500NO3F-2016
Cadmium
1.21
mg/Kg - dry
0.556
1
08/22/23 22:07
BKN
6010D
Chromium
60.0
mg/Kg - dry
1.39
1
08/22/23 22:07
BKN
6010D
Mercury
<0.972
mg/Kg - dry
0,972
1
08/18/23 13:01
MRE
SW-7471B
pH
8.3
S.U.
1
08/1412316:00
CNB
9045D
Total Volatile Solids
62.1
%
0.010
1
08/16/23 17:40
CJR
SM-254OG
Molybdenum
13.8
mg/Kg - dry
1.39
1
08/22/23 22:07
BKN
6010D
Qualifiers/ DF Dilution Factor MQL Method Quantitation Limit
Definitions
Page 4 of 8

(2)
WayPAoint
NALYi ICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Client: City of Monroe CASE NARRATIVE
Project: WWTP Cake
Lab Report Number: 23-222-0002
Date: 8/25/2023
Metals Analysis Method 6010D
Sample 73536 (SB-5 SWI)
Analyte: Aluminum
QC Batch No: 1-700249/1-699855
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 73536 (SB-5 SWI)
Analyte: Calcium
QC Batch No: 1-700249/1-699855
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Sample 73536 (SB-5 SWI)
Analyte: iron
QC Batch No: 1-700249/1-699855
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 73536 (SB-5 SWI)
Analyte: Potassium
QC Batch No: 1-700249/1-699855
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 73536 (SB-5 SWI)
Analyte: Magnesium
QC Batch No: 1-700249/1-699855
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 73536 (SB-5 SWI)
Analyte: Sodium
QC Batch No: 1-700249/1-699855
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Solids Total Mercury Analysis - CVAA Method 7471A
Sample 94293 (Back River Class B Cake Monthly Comp)
Analyte: Mercury
QC Batch No: 1-699597/1-699304
Page 5 of 8

WayPAoint
NALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www,waypointanalytica I.com
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Page 6 of 8

Waypoint-Q)
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 904-743.9401 0 Fax [phone]
www.waypointanalytical.com
Shipment Receipt Form
Customer Number: 46205
Customer Name: City of Monroe
Report Number: 23-222-0002
Shipping Method
Fed Ex US Postal Lab
• UPS Client Courier
Other
Thermometer ID:
Shipping container/cooler uncompromised?:
Yes
No
Number of coolers/boxes received
1
Custody seals intact on shipping container/cooler?
Yes
No
• Not Present
Custody seals intact on sample bottles?
_ Yes
No
Not Present
Chain of Custody (COC) present?
• Yes
No
COC agrees with sample label(s)?
0 Yes
No
COC properly completed
• Yes
No
Samples in proper containers?
• Yes
No
Sample containers intact?
• Yes
No
Sufficient sample volume for indicated test(s)?
• Yes
No
All samples received within holding time?
• Yes
No
Cooler temperature in compliance?
Yes
No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
• Yes
No
Water - Sample containers properly preserved
Yes
No
• NIA
Water - VOA vials free of headspace
Yes
No
0 NIA
Trip Blanks received with VOAs
Yes
-_ No
01 NIA
Soil VOA method 5035 — compliance criteria met
Yes
No
0 NIA
High concentration container (48 hr)
High concentration pre -weighed (methanol -14 d)
Low concentration EnCore samplers (48 hr)
Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included?
Yes
W No
Comments:
Signature: David Lennon Date & Time: 08/10/2023 09:10:24
Page 7 of 8

Page 8 of 8

City of Monroe
Reports of Lab
Analysis
4th Quarter

Waypoint,O
ANALYTICAL
10/6/2023
City cf Monroe
Ken Morris
775 Treeway Dr
Monroe, NC, 28110
Ref: Analytical Testing
Report Number: 23-276-0006
Project Description: RAS
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
www.waypointanalytical.com
Dear Ken Morris:
Waypoint Analytical Virginia, Inc, received sample(s) on 10/3/2023 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information
Sincerely,
Brandi Watson
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 1 of 5

Waypoint(Z)
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Sample Summary Table
Report Number: 23-276-0006
Client Project Descriptions: RAS
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
63598 RAS Solids 10/02/2023 10:45 10/03/2023 SM-254OG WP MTN
WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN
Page 2 of 5

Waypoint.o
ANALYTICAL
46205
City of Monroe Project RAS
Ken Morris
775 Treeway Dr Information
Monroe , NC 28110
Report Number: 23-276-0006 REPORT
Lab No : 63598
Sample ID RAS
7621 Whitepine Road, Richmond, VA 23237
Mein 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Report Date : 10/06/2023
Received : 10/03/2023
VALYSIS Brandi Watson
Matrix: Solids
Sampled: 10/ 2/ 2023 10:45
Test Results Units MQL DF Date / Time
Analyzed
By
Analytical
Method
Moisture 98.4 % 0.010 1 10/04/23 16:13
CAH
SM-254OG
Test Results Units MQL DF Date ! Time
By
Analytical
Analyzed
Method
Total Volatile Solids 69.8 % 0.010 1 10/04/23 16:13 CAH SM-254OG
Total Solids 1.63 % 0.010 1 10/04/23 16:13 CAH SM-2540G
Qualifiers/ DF Dilution Factor
Definitions
MQL Method Quantitation Limit
Page 3 of 5

Waypoint-Q)
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
www.waypointanalytical.com
Shipment Receipt Form
Customer Number: 46205
Customer Name: City of Monroe
Report Number: 23-276-0006
Shipping Method
Fed Ex US Postal Lab
• UPS Client Courier
Other
Thermometer ID:
Shipping container/cooler uncompromised?
• Yes
No
Number of coolers/boxes received
I '
Custody seals intact on shipping container/cooler?
Yes
No
Not Present
Custody seals intact on sample bottles?
Yes
No
40 Not Present
Chain of Custody (COC) present?
• Yes
No
COC agrees with sample label(s)?
• Yes
No
COC properly completed
• Yes
No
Samples in proper containers?
• Yes
No
Sample containers intact?
Yes
No
Sufficient sample volume for indicated test(s)?
1 Yes
No
All samples received within holding time?
Yes
No
Cooler temperature in compliance?
• Yes
No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
Yes
No
Water - Sample containers properly preserved
Yes
No
• NIA
Water - VOA vials free of headspace
Yes
No:
NIA
Trip Blanks received with VOAs
Yes
_ No
NIA
Soil VOA method 5035 — compliance criteria met
Yes
No
0 NIA
High concentration container (48 hr)
High concentration pre -weighed (methanol -14 d)
Low concentration EnCore samplers (48 hr)
Low cone pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included?
Yes
• No
Comments:
Signature: David Lennon Date & Time: 10/03/2023 10:17:28
Page 4 of 5

M
Page 5 of 5

Waypoint,(D
ANALYTICAL
10/13/2023
City of Monroe
Ken Morris
775 Treeway Dr
Monroe, NC, 28110
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
www.waypointanalytical.com
Ref: Analytical Testing
Report Number: 23-276-0007
Project Description, WWTP Cake
Dear Ken Morris:
Waypoint Analytical Virginia, Inc, received sample(s) on 10/3/2023 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information
Sincerely,
Brandi Watson
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 1 of 7

•
Waypoint, 7621 (2) Whitepine Road, Richonond,llA 23237
Main $04-743-9401 ° Fax [phone]
ANALYTICAL www.waypointanalytical.com
Sample Summary Table
Report Number: 23-276-0007
Client Project Description: WWTP Cake
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
63599
WWTP Cake
Solids
10/02/2023 09:25
10/03/2023
63599
WWTP Cake
Solids
10/02/2023 09:25
10/03/2023
63599
WWTP Cake
Solids
10/02/2023 09:25
10/03/2023
63599
WWTP Cake
Solids
10/02/2023 09:25
10/03/2023
63599
WWTP Cake
Solids
10/02/2023 09:25
10/03/2023
63599
WWTP Cake
Solids
10/02/2023 09:25
10/03/2023
63599
WWTP Cake
Solids
10/02/2023 09:25
10/03/2023
63599
WWTP Cake
Solids
10/02/2023 09:25
10/03/2023
WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN
SM-4500-NH3C
WP MTN
9045D
WP MTN
4500NO3F-2016
WP MTN
6010D
WP MTN
SW-7471B
WP MTN
SM-4500-NH3C-TKN
WP MTN
SM-2540G
WP MTN
Page 2 of 7

Waypointo
ANALYTICAL
46205
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical, com
City of Monroe Project WWTP Cake
Ken Morris
775 Treeway Dr Information
Monroe, NC 28110
Report Number. 23-276-0007
Lab No : 63599
Sample ID: WWTP Cake
REPORT OFANAL PSIS
Report Date : 10/13/2023
Received : 10/03/2023
Qt'-
Brandi Watson
Matrix: Solids
Sampled: 10/2/2023 9:25
Test Results Units MQL DF Date / Time By Analytical
Analyzed Method
Moisture
83.1
%
0.010
Phosphorus
20900
mg/Kg - dry
29.6
Sulfur
10300
mg/Kg - dry
59.2
Calcium
18100
rng/Kg - dry
296
Aluminum
11500
mg/Kg - dry
29.6
Manganese
1760
rng/Kg - dry
2.96
Copper
293
mg/Kg - dry
2.96
Zinc
1030
mg/Kg - dry
7.40
Organic N
55740
mg/Kg - dry
1479
Nickel
74.6
mg/Kg - dry
1.46
Lead
19.0
rng/Kg - dry
1.78
Arsenic
7.28
mg/Kg - dry
2.96
Selenium
6.33
mg/Kg - dry
2.96
Test
Results
Units
MQL
1
10/04/2316:13
CAH
SM-254OG
1
10/06/23 04:56
BKN
6010D
1
10/06/23 04:56
BKN
6010D
1
10/06/23 04:56
BKN
6010D
1
10/06/23 04:56
BKN
6010D
1
10/06/23 04:56
BKN
6010D
1
10/06/23 04:56
BKN
6010D
1
10/06/23 04:56
BKN
6010D
1
10/12/23 09:52
CALCULATION
1
10/06/23 04:56
BKN
6010D
1
10/06/23 04:56
BKN
6010D
1
10/06/23 04:56
BKN
6010D
1
10/06/23 04:56
BKN
6010D
DF
Date / Time
By
Analytical
Analyzed
Method
Total Solids 16.9 % 0.010 1 10/04/23 16:13 CAH SM-254OG
Qualifiers/ DF Dilution Factor
Definitions
MQL Method Quantitation Limit
Page 3 of 7

0
Waypoint,
7621 Whitepine Road, Richmond, VA
Main 804-743-9401 ° Fax [phone]
ANALYTICAL
www.waypointanalytical.com
46205
City of Monroe
Project
WWTP Cake
Ken Morris
Report Date : 10/13/2023
775 Treeway Dr
Information :
Received : 10/03/2023
Monroe, NC 28110
Brand! Watson
Report Number: 23-276-0007
REPORT OFANALYSIS
Lab No : 63599
Matrix:
Solids
Sample ID, WWTP Cake
Sampled:
10/2/2023 9:25
Test
Results
Units
MQL
DF
Date / Time
By Analytical
Analyzed
Method
Total Kjeldahl Nitrogen
55700
mg/Kg - dry
1480
1
10/12/23 12.53
JP) iM-4500-NH3C-TKP
Potassium
2820
mg/Kg - dry
59.2
1
10/06/23 04:56
BKN 6010D
Magnesium
2760
rng/K9 - dry
29.6
1
10/06/23 04:56
BKN 6010D
Sodium
1050
mg/Kg - dry
148
1
10/06/23 04:56
BKN 6010D
Iron
29100
mg/Kg - dry
59.2
1
10/06/23 04:56
BKN 6010D
Ammonia Nitrogen
<592
mg/Kg - dry
592
1
10/12/23 09:52
JPJ SM-4500-NH3C
Nitrate+Nitrite-N
722
mg/Kg - dry
29.6
1
10/06/23 14:51
CLP 4500NO3F-2016
Cadmium
1.24
mg/Kg - dry
0.592
1
10/06/23 04:56
BKN 6010D
Chromium
56.4
rri - dry
1.48
1
10/06/23 04:56
BKN 6010D
Mercury
<1.09
rng/K9 - dry
1.09
1
10/06/23 11:41
MRE SW-7471B
pH
7.4
S.U.
1
10/06/2316:07
CNB 9045D
Total Volatile Solids
62.3
%
0.010
1
10/04/23 16:13
CAH SM-254OG
Molybdenum
13.6
mg/Kg - dry
1.48
1
10/06/23 04:56
BKN 6010D
Qualifiers/ DF Dilution Factor
Definitions
MQL Method Quantitation Limit
Page 4 of 7

(D
WayPAoi nt .
NALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Client: City of Monroe CASE NARRATIVE
Project: WWTP Cake
Lab Report Number: 23-276-0007
Date: 10/12/2023
Metals Analysis Method 6010D
Sample 97763
Analyte: Aluminum
QC Batch No: L709158/L708742
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 97763
Analyte: Arsenic
QC Batch No: L70915811-708742
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Sample 97763
Analyte: Iron
QC Batch No: 1-709158/1-708742
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 97763
Analyse: Potassium
QC Batch No. 1-7091581708742
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 97763
Analyte: Manganese
QC Batch No: 1-70931511-708742
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 97763
Analyte: Lead
QC Batch No. 1-7091581708742
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Page 5 of 7

(DiWaypont
7621 ain 80 -7 Road, Richmond, V7 -6446
Main 804-743-9401 1Fax 804-271-b446
ANALYTICAL www.waypointanalytical.com
Shipment Receipt Form
Customer Number:46205
Customer Name: City of Monroe
Report Number: 23-276-0007
Shipping Method
Fed Ex US Postal Lab Other:
0 UPS Client Courier Thermometer ID:
Shipping container/cooler uncompromised?
Yes
_ No
Number of coolers/boxes received
r 1
Custody seals intact on shipping container/cooler?
Yes
No • Not Present
Custody seals intact on sample bottles?
Yes
_ No Not Present
Chain of Custody (COC) present?
! Yes
No
COC agrees with sample label(s)?
Yes
No
COC properly completed
Yes
No
Samples in proper containers?
01 Yes
No
Sample containers intact?
Yes
No
Sufficient sample volume for indicated test(s)?
Yes
No
All samples received within holding time?
• Yes
No
Cooler temperature in compliance?
• Yes
No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
• Yes
No
Water - Sample containers properly preserved
Yes
No • NIA
Water - VOA vials free of headspace
Yes
No NIA
Trip Blanks received with VOAs
Yes
No 0 NIA
Soil VOA method 5035 — compliance criteria met
Yes
No NIA
High concentration container (48 hr)
High concentration pre -weighed (methanol -14 d)
Low concentration EnCore samplers (48 hr)
Low cone pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included?
Yes
No
Comments:
Signature: David Lennon
Date & Time: 10/03/2023 10:20:05
Page 6 of 7

Page 7 of 7

WayPAoint
NALYTICAL
10/1312023
City of Monroe
Ken Morris
775 Treeway Dr
Monroe, NC, 28110
Ref: Analytical Testing
Report Number: 23-276-0008
Project Description: WTP Cake
7621 Whitepine Road, Richmond, VA 23237
Main 844-743-9401 ° Fax [phone]
www.waypointanalyticai.com
Dear Ken Morris:
Waypoint Analytical Virginia, Inc. received sample(s) on 10/3/2023 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Brand) Watson
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 1 of 7

(2)
7621 Whitepine Road, Richmond, VA 23237
Waypoint. Main 804-743-9401 ° Fax [phone]
ANALYTICAL www.waypointanalytical.com
Sample Summary Table
Report Number: 23-276-0008
Client Project Description: WTP Cake
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
63600
WTP Cake
Solids
10/02/2023 09:05
10/03/2023
63600
WTP Cake
Solids
10/02/2023 09:05
10/03/2023
SM-4500-NH3C
WP MTN
63600
WTP Cake
Solids
10/02/2023 09:05
10/03/2023
9045D
WP MTN
63600
WTP Cake
Solids
10/02/2023 09:05
10/03/2023
4500NO3F-2016
WP MTN
63600
WTP Cake
Solids
10/02/2023 09:05
10/03/2023
6010D
WP MTN
63600
WTP Cake
Solids
10/02/2023 09:05
10/03/2023
SW-74716
WP MTN
63600
WTP Cake
Solids
10/02/2023 09:05
10/03/2023
SM-4500-NH3C-TKN
WP MTN
63600
WTP Cake
Solids
10/02/2023 09:05
10/03/2023
SM-2540G
WP MTN
WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN
Page 2 of 7

Waypointo
ANALYTICAL
46205
City of Monroe Project WTP Cake
Ken Morris
775 Treeway Dr Information
Monroe, NC 28110
Report Number : 23-276-0008
Lab No : 63600
Sample ID: WTP Cake
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
REPORT OFANALYSIS
Report Date : 10/13/2023
Received : 10/03/2023
Qfk L"
Brandi Watson
Matrix: Solids
Sampled: 10/2/2023 9:05
Test Results Units MOL DF Date I Time By Analytical
Analyzed Method
Moisture
68.0
%
0.010
Phosphorus
3060
mg/Kg - dry
15.6
Sulfur
2$20
mg/Kg - dry
31.3
Calcium
2840
mg/Kg - dry
156
Aluminum
3280
mg/Kg - dry
15.6
Manganese
797
mg/Kg - dry
1.56
Copper
353
mg/Kg - dry
1.56
Zinc
39.4
mg/Kg - dry
3.91
Organic N
16550
mg/Kg - dry
781.3
Nickel
28.2
mg/Kg - dry
0.781
Lead
8.75
mg/Kg - dry
0.937
Arsenic
24.6
mg/Kg - dry
1.56
Selenium
1.84
mg/Kg - dry
1.56
Test
Results
Units
MOL
1
10/04/23 16:13
CAH
SM-254OG
1
10/06/23 05:01
BKN
6010D
1
10/06/23 05:01
BKN
6010D
1
10/06/23 05:01
BKN
6010D
1
10/06/23 05:01
BKN
6010D
1
10/06/23 05:01
BKN
6010D
1
10/06/23 05:01
BKN
6010D
1
10/06/23 05:01
BKN
6010D
1
10/12/23 09:52
CALCULATION
1
10/06/23 05:01
BKN
6010D
1
10/06/23 05:01
BKN
6010D
1
10/06/23 05:01
BKN
6010D
1
10/06/23 05:01
BKN
6010D
DF
Date I Time
By
Analytical
Analyzed
Method
Total Solids 32.0 % 0.010 1 10/04/23 16:13 CAH SM-2540G
Qualifiers/ DF Dilution Factor
Definitions
MQL Method Quantitation Limit
Page 3 of 7

0
Waypoint
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 °
Fax [phone]
ANALYTICAL
www.waypointanalyt(cal.com
46205
City of Monroe
Project
WTP Cake
Ken Morris
Report Date : 10/13/2023
775 Treeway Dr
Information :
Received : 10/03/2023
Monroe, NC 28110
Brandi Watson
Report Number : 23-276-0008
REPORT OFANAL YSIS
Lab No : 63600
Matrix:
Solids
Sample ID : WTP Cake
Sampled:
10/2/2023 9:05
Test
Results
Units
MOL
DF
Date / Time
By Analytical
Analyzed
Method
Total Kjeldahl Nitrogen
16900
mg/Kg - dry
781
1
10/12/23 12:53
JPJ ;M-4500-NH3C-TKP
Potassium
213
mg/Kg - dry
31.3
1
10/06/23 05:01
BKN 6010D
Magnesium
494
mg/Kg - dry
15.6
1
10/06/23 05:01
BKN 6010D
Sodium
240
mg/Kg - dry
78.1
1
10/06/23 05:01
BKN 6010D
Iron
325000
mg/Kg - dry
625
20
10/06/23 22:00
BKN 6010D
Ammonia Nitrogen
328
mg/Kg - dry
313
1
10/12/23 09:52
JP] SM-4500-NH3C
Nitrate+ N itr ite-N
<15.6
mg/Kg - dry
15.6
1
10/06/23 14:52
CLP 4500NO3F-2016
Cadmium
20.4
mg/Kg - dry
0.313
1
10/06/23 05:01
BKN 6010D
Chromium
201
mg/Kg - dry
0.781
1
10/06/23 05:01
BKN 6010D
Mercury
<0.534
mg/Kg - dry
0.534
1
10/06/23 11:46
MRE SW-7471B
pH
5.3
S.U.
1
10/06/2316:07
CNB 9045D
Total Volatile Solids
46.3
%
0.010
1
10/04/23 16:13
CAH SM-254OG
Molybdenum
45.0
mg/Kg - dry
0.781
1
10/06/23 05:01
BKN 6010D
Qualifiers/ DF Dilution Factor
Definitions
MQL Method Quantitation Limit
Page 4 of 7

WayPAoint
NALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Client: City of Monroe CASE NARRATIVE
Project: WTP Cake
Lab Report Number: 23-276-0008
Date: 10/12/2023
Metals Analysis Method 601 OD
Sample 97763
Analyte: Aluminum
QC Batch No: 1-709158/1-708742
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 97763
Analyte: Arsenic
QC Batch No: 1-709158/1-708742
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Sample 97763
Analyte: Iron
QC Batch No: L7091581L708742
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 97763
Analyte: Potassium
QC Batch No: L709158IL708742
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 97763
Analyte: Manganese
QC Batch No: 1-709315/1-708742
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 97763
Analyte: Lead
QC Batch No: L709158IL708742
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Page 5 of 7

Waypoint-Q)
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
www.waypointanalytical.com
Shipment Receipt Form
Customer Number: 46205
Customer Name: City of Monroe
Report Number: 23-276-0008
Shipping Method
Fed Ex US Postal Lab
0 UPS Client Courier
Other
Thermometer ID:
Shipping container/cooler uncompromised?
• Yes
No
Number of coolers/boxes received
F
Custody seals intact on shipping container/cooler?
Yes
No
• Not Present
Custody seals intact on sample bottles?
Yes
No
Not Present
Chain of Custody (COC) present?
Yes
No
COC agrees with sample label(s)?
• Yes
No
COC properly completed
• Yes
No
Samples in proper containers?
Yes
No
Sample containers intact?
0 Yes
No
Sufficient sample volume for indicated test(s)?0
Yes
No
All samples received within holding time?:
Yes
No
Cooler temperature in compliance?
0 Yes
No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
46. Yes
No
Water - Sample containers properly preserved
Yes
No
46. NIA
Water - VOA vials free of headspace
Yes
No
0. NIA
Trip Blanks received with VOAs
Yes
No
NIA
Soil VOA method 5035 — compliance criteria met
Yes
No
NIA
High concentration container (48 hr)
High concentration pre -weighed (methanol -14 d)
Low concentration EnCore samplers (48 hr)
Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included?
_ . Yes
• No
Comments:
Signature: .David Lennon
Date & Time: 10/03/2023 10:26:36
Page 6 of 7

Page 7 of 7

Waypoint(D
ANALYTICAL
10/2712023
City of Monroe
Ken Morris
775 Treeway Dr
Monroe, NC, 28110
Ref: Analytical Testing
Report Number: 23-297-0007
Project Description: RAS
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Dear Ken Morris:
Waypoint Analytical Virginia, Inc, received sample(s) on 10/24/2023 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
B
13randi Watson
Laboratory's liability in any claim relating to analyses performed shalt be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 1 of 5

Waypoint.-(2)
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Sample Summary Table
Report Number: 23-297-0007
Client Project Description: RAS
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
63788 EZAS
Solids 10/23/2023 08:25 10/24/2023 SM-2540G WP MTN
WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN
Page 2 of 5

Waypointo
ANALYTICAL
46205
City of Monroe Project RAS
Ken Morris
775 Treeway Dr Information
Monroe , NC 28110
Report Number : 23-297-0007 REPORTOF'A
Lab No : 63788
Sample ID : RAS
7621 Whitepine Road, Richmond, VA 23237
Main 304-743-9401 ° Fax [phone]
www.waypointanalytical.com
Report Date : 10/27/2023
Received : 10/24/2023
&t"
VALYSIS Brandi Watson
Matrix: Solids
Sampled: 10/23/2023 8:25
Test
Results
Units
MQL
DF Date I Time
Analyzed
By
Analytical
Method
Moisture
98,4
%
0.010
1 10/26/2316:12
CAH
SM-2540G
Test
Results
Units
MQL
DF Date / Time
By
Analytical
Analyzed
Method
Total Volatile Solids
75.4
%
0.010
1 10/26/23 16:12
CAH
5M-2540G
Test
Results
Units
MOL
DF Date / Time
By
Analytical
Analyzed
Method
Total Solids 1.57 % 0.010 1 10/26/23 16:12 CAH SM-2540G
Qualifiers/ DF Dilution Factor
Definitions
MQL Method Quantitation Limit
Page 3 of 5

Waypoint(D
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
www.waypointanalytical.com
Shipment Receipt Form
Customer Number: 46205
Customer Name: City of Monroe
Report Number: 23-297-0007
Shipping Method
Fed Ex US Postal Lab
• UPS Client Courier
Other
Thermometer ID. -
Shipping container/cooler uncompromised?
• Yes
No
Number of coolers/boxes received
F
Custody seals intact on shipping container/cooler?
Yes
No
10 Not Present
Custody seals intact on sample bottles?
_ Yes
No
4 Not Present
Chain of Custody (COC) present?
Yes
No
COC agrees with sample label(s)?
0. Yes
No
COC properly completed,
Yes
No
Samples in proper containers?
Yes
No
Sample containers intact?
• Yes
No
Sufficient sample volume for indicated test(s)?
4 Yes
No
All samples received within holding time?
V Yes
No
Cooler temperature in compliance?
• Yes
No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
491 Yes
No
Water - Sample containers properly preserved
Yes
No
N/A
Water - VOA vials free of headspace
Yes
No
NIA
Trip Blanks received with VOAs
Yes
No
NIA
Soil VOA method 5035 -- compliance criteria met
Yes
No
N/A
High concentration container (48 hr)
High concentration pre -weighed (methanol -14 d)
Low concentration EnCore samplers (48 hr)
Low cone pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included?
Yes
No
Comments:
Signature: David Lennon Date & Time: ;10/24/2023 09:22:25
Page 4 of 5

V
w
u
C?
� Q
cps
m
J
0
m
0
m
obi
R
V)
Page 5 of 5

Waypoint.(D
ANALYTICAL
11/7/2023
City of Monroe
Ken Morris
775 Treeway Dr
Monroe, NC, 28110
Ref: Analytical Testing
Report Number: 23-297-0008
Project Description: WWTP Cake
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
www.waypointanalyticat.com
Dear Ken Morris:
Waypoint Analytical Virginia, Inc, received sample(s) on 10/24/2023 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information
Sincerely,
Brandi Watson
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 1 of 8

(D
7621 Whitepine Road, Richmond, VA 23237
Waypoint. Main 804-743-9401 ° Fax [phone]
ANALYTICAL www.waypointanalytical.com
Sample Summary Table
Report Number: 23-297-0008
Client project Description: WWTP Cake
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
63789
WWTP Cake
Solids
10/23/2023 08:50
10/24/2023
63789
WWTP Cake
Solids
10/23/2023 08:50
10/24/2023
63789
WWTP Cake
Solids
10/23/2023 08:50
10/24/2023
63789
WWTP Cake
Solids
10/23/2023 08:50
10/24/2023
63789
WWTP Cake
Solids
10/23/2023 08:50
10/24/2023
63789
WWTP Cake
Solids
10/23/2023 08:50
10/24/2023
63789
WWTP Cake
Solids
10/23/2023 08:50
10/24/2023
63789
WWTP Cake
Solids
10/23/2023 08:50
10/24/2023
WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN
SM-4500-NH3C
WP MTN
9045D
WP MTN
4500NO3F-2016
WP MTN
6010D
WP MTN
SW-7471B
WP MTN
SM-4500-NH3C-TKN
WP MTN
SM-254OG
WP MTN
Page 2 of 8

Waypointo
ANALYTICAL
46205
City of Monroe
Ken Morris
775 Treeway Dr
Monroe, NC 28110
Report Number:23-297-0008
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Project WWTP Cake
Information :
REPORT OPANALYSIS
Report Date : 11/07/2023
Received : 10/24/2023
Brandi Watson
Lab No : 63789 Matrix: Solids
Sample ID: WWTP Cake Sampled: 10/23/2023 8:50
Test
Results
Units
MOL
DF
Date I Time
Analyzed
By
Analytical
Method
Total Solids
19.1
%
0.010
1
10/26/23 16:12
CAH
SM-254OG
Total Kjeldahi Nitrogen
46600
mg/Kg - dry
1310
1
11/07/23 07:09
JPJ
;M-4500-NH3C-TKP
Phosphorus
20600
mg/Kg - dry
26.2
1
10/28/23 03:00
JTR
6010D
Potassium
2650
mg/Kg - dry
52.4
1
10/28/23 03:00
JTR
6010D
Sulfur
10800
mg/Kg - dry
52.4
1
10/28/23 03:00
JTR
6010D
Calcium
20000
mg/Kg - dry
1310
5
10/30/23 14:51
TJS
6010D
Magnesium
2740
mg/Kg - dry
26.2
1
10/28/23 03:00
JTR
6010D
Sodium
984
mg/Kg - dry
131
1
10/28/23 03:00
JTR
6010D
Iron
29300
mg/Kg - dry
52.4
1
10/28/23 03:00
JTR
6010D
Manganese
1930
mg/Kg - dry
2.62
1
10/28/23 03:00
JTR
6010D
Copper
299
mg/Kg - dry
2.62
1
10/28/23 03:00
JTR
6010D
Zinc
1090
mg/Kg - dry
6.54
1
10/28/23 03:00
JTR
6010D
Organic N
46040
mg/Kg - dry
1309
1
11/07/23 07:09
CALCULATION
Nitrate+Nitrite-N
1610
mg/Kg - dry
26.2
1
10/26/23 17:43
CLP
4500NO3F-2016
Nickel
81.2
mg/Kg - dry
1.31
1
10/28/23 03:00
JTR
6010D
Mercury
<0.937
mg/Kg - dry
0.937
1
10/27/23 12:07
FDS
SW-7471B
Selenium
5.50
mg/Kg - dry
2.62
1
10/28/23 03:00
JTR
6010D
pH
5.6
S.U.
1
10/26/2314:18
ANV
9045D
Total Volatile Solids
61.6
%
0.010
1
10/26/23 16:12
CAH
SM-254OG
Qualifiers/ DF
Dilution Factor
MQL Method Quantitation Limit
Definitions
Page 3 of 8

0
7621 Whi#epine Road, Richmond, VA 23237
Waypoint. fulain 804-743-9401 ° Fax [phone]
ANALYTICAL www.waypointanalytical.com
46205
City of Monroe Project WWTP Cake
Ken Morris Report Date : 11/07/2023
775 Treeway Dr Information : Received : 10/24/2023
Monroe , NC 28110 QQ
CJ
Report Number: 23-297-0008 REFORTOFANALYSIS Brandi Watson
Lab No : 63789 Matrix: Solids
Sample ID : WVYTP Cake Sampled: 10/23/2023 8:50
Test Results Units MQL DF Date / Time By Analytical
Analyzed Method
Ammonia Nitrogen
Aluminum
Arsenic
Cadmium
Chromium
Lead
Molybdenum
Analytical Method: SM-2540G
Test
555
mg/Kg - dry
524
1
11/07/23 10:19
JPJ
SM-4500-NH3C
11900
mg/Kg - dry
26.2
1
10/28/23 03.00
JTR
6010D
7.28
mg/Kg - dry
2.62
1
10/28/23 03:00
JTR
6010D
0.853
mg/Kg - dry
0.524
1
10/28/23 03:00
JTR
6010D
60,2
mg/Kg - dry
1.31
1
10/28/23 03:00
JTR
6010D
18.7
mg/Kg - dry
1.57
1
10/28/23 03:00
JTR
6010D
14.9
mg/Kg - dry
1.31
1
10/28/23 03:00
JTR
6010D
Results Units MQL DF Date / Time By Analytical
Analyzed Batch
Moisture 80.9 % 0.010
Qualifiers/ DF Dilution Factor
Definitions
1 10/26/23 16:12 CAH L713512
MQL Method Quantitation Limit
Page 4 of 8

(2)
WaypoI nt .
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Client: City of Monroe CASE NARRATIVE
Project: WWTP Cake
Lab Report Number: 23-297-0008
Date: 11 /7/2023
Metals Analysis Method 6010D
Sample 63789 (WWTP Cake)
Analyte: Aluminum
QC Batch No: L713991/L713475
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 63789 (WWTP Cake)
Analyte: Calcium
QC Batch No: 1-714093/1-713475
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 63789 (WWTP Cake)
Analyte: Iron
QC Batch No: L713991/L713475
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 63789 (WWTP Cake)
Analyte: Potassium
QC Batch No: L713991/L713475
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 63789 (WWTP Cake)
Analyte: Magnesium
QC Batch No: L713991/L713475
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 63789 (WWTP Cake)
Analyte: Manganese
QC Batch No: L713991/L713475
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 63789 (WWTP Cake)
Analyte: Phosphorus
QC Batch No: 1-713991/1-713475
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 63789 (WWTP Cake)
Analyte: Lead
Page 5 of 8

WayPAoi nt.(2)
NALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
QC Batch No: 1-713991 /L713475
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Sample 63789 (WWTP Cake)
Analyte: Sulfur
QC Batch No: L713991/1-713475
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 63789 (WWTP Cake)
Analyte: Zinc
QC Batch No: L713991/L713475
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Solids Total Mercury Analysis - CVAA Method 7471A
Sample 63814 (23102407.01A)
Analyte: Mercury
QC Batch No: 1-713736/1-713529
The matrix spike, matrix spike duplicate and the post digestion spike were all outside of the quality control
acceptance ranges. Matrix interference is suspected.
Page 6 of 8

Waypoint(D
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
www.waypointanalytical.com
Shipment Receipt Form
Customer Number: 46205
Customer Name: City of Monroe
Report Number: 23.297.0008
Shipping Method
Fed Ex US Postal Lab
• UPS Client Courier
Other
Thermometer ID:
Shipping container/cooler uncompromised?
Yes
No
Number of coolers/boxes received
Custody seals intact on shipping container/cooler?
Yes
No
Not Present
Custody seals intact on sample bottles?
Yes
No
Not Present
Chain of Custody (COC) present?
• Yes
No
COC agrees with sample label(s)?
Yes
No
COC properly completed
• Yes
No
Samples in proper containers?
• Yes
No
Sample containers intact?
Yes
No
Sufficient sample volume for indicated test(s)?
Yes
No
All samples received within holding time?
• Yes
No
Cooler temperature in compliance?
Yes
No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
Yes
No
Water - Sample containers properly preserved
Yes
No
• NIA
Water - VOA vials free of headspace
Yes
No
• NIA
Trip Blanks received with VOAs
Yes
No
• NIA
Soil VOA method 5035 — compliance criteria met
Yes
No
NIA
High concentration container (48 hr)
High concentration pre -weighed (methanol -14 d)
Low concentration EnCore samplers (48 hr)
Low cone pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included?
Yes
0.- No
Comments:
Signature: .David Lennon Date & Time: 10/24/2023 09:24:58
Page 7 of 8

Page 8 of 8

SECTION
V�

�ce­
January 04, 2024
Ken Morris
City of Monroe
PO Box 69
Monroe, NC 28111
RE: Project: LAND APPLICATION
Pace Project No.: 92703642
Dear Ken Morris:
Pace Analytical Services, LLC
9800 Kincey Ave, Suite 100
Huntersville, NC 28078
[phone]
Enclosed are the analytical results for sample(s) received by the laboratory on December 13, 2023. The results relate only
to the samples included in this report. Results reported herein conform to the applicable TNIINELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace National - Mt. Juliet
• Pace Analytical Services -Asheville
• Pace Analytical Services - Charlotte
• Pace Analytical Services - Peachtree Corners, GA
• Pace Analytical Services - Greensburg
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Sarah Graham for
Tyriek Hooks
[e-mail]
704-977-0947
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 29

Project: LAND APPLICATION
Pace Project No.: 92703642
Pace Analytical Services, LLC
9800 Kincey Ave, Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services Pennsylvania
1638 Roseytown Rd Suites 2,3&4, Greensburg, PA 15601
ANAB DOD -FLAP Rad Accreditation #: L2417
ANABISOIIEC 17025:2017 Rad Cort#: L24170
Alabama Certification M 41590
Arizona Certification M AZ0734
Arkansas Certification
California Certification #: 2950
Colorado Certification M PA01547
Connecticut Certification #: PH-0694
EPA Region 4 DW Rad
FloridalTNI Certification #: E87683
Georgia Certification #: C040
Guam Certification
Hawaii Certif cation
Idaho Certification
Illinois Certification
Indiana Certification
Iowa Certification M 391
Kansas Certification #: E-10358
Kentucky Certification #: KY90133
KY WW Permit #: KY0098221
KY WW Permit M KY0000221
Louisiana DHHlTNI Certification #: LA010
Louisiana DEQ/TNI Certification #: 04086
Maine Certification #: 2023021
Maryland Certification #: 308
Massachusetts Certification #: M-PA1457
MichiganlPADEP Certification #: 9991
Pace Analytical Services National
12065 Lebanon Road, Mt. Juliet, TN 37122
Alabama Certification #: 40660
Alaska Certification 17-026
Arizona Certification #: AZ0612
Arkansas Certification #: 88-0469
California Certification #: 2932
Canada Certification #: 1461.01
Colorado Certification #: TN00003
Connecticut Certification #: PH-0197
DOD Certification: #1461.01
EPA# TN00003
Florida Certification #: E87467
Georgia DW Certification #: 923
Georgia Certification: NELAP
Idaho Certification #: TNO0003
Illinois Certification #: 200008
Indiana Certification #: C-TN-01
Iowa Certification M 364
Kansas Certification M E-10277
Kentucky UST Certification #: 16
Kentucky Certification #: 90010
CERTIFICATIONS
Missouri Certification #: 235
Montana Certification #: Cert0082
Nebraska Certification #: NE-OS-29-14
Nevada Certification #: PA014572023-03
New HampshirelTNI Certification #: 297622
New Jersey(TNI Certification #: PA051
New Mexico Certification #: PA01457
New YorklTNI Certification #: 10888
North Carolina Certification #: 42706
North Dakota Certification #: R-190
Ohio EPA Rad Approval #41249
OregonlTNI Certification M PA200002-015
PennsylvanialTNI Certification #: 65-00282
Puerto Rico Certification #: PA01457
Rhode Island Certification #: 65-00282
South Dakota Certification
Tennessee Certification #: TN02867
Texas TNl Certification #: T104704188-22-18
Utah/TNI Certification #: PA014572223-14
USDA Soil Permit #: 525-23-67-77263
Vermont Dept. of Health: ID# VT-0282
Virgin IslandlPADEP Certification
VirginiaNELAP Certification #: 460198
Washington Certification M C868
West Virginia DEP Certification #: 143
West Virginia DHHR Certification #: 9964C
Wisconsin Approve List for Rad
Louisiana Certification #: A130792
Louisiana DW Certification #: LA180010
Maine Certification #: TN0002
Maryland Certification M 324
Massachusetts Certification * M-TNO03
Michigan Certification #: 9958
Minnesota Certification #: 047-999-395
Mississippi Certification #: TN00003
Missouri Certification #: 340
Montana Certification #: CERT0086
Nebraska Certification #: NE-OS-15-05
Nevada Certification #: TN-03-2002-34
New Hampshire Certification #: 2975
New Jersey Certification M TNO02
New Mexico DW Certification
New York Certification M 11742
North Carolina Aquatic Toxicity Certification M 41
North Carolina Drinking Water Certification #: 21704
North Carolina Environmental Certificate #: 375
North Dakota Certification #: R-140
Ohio VAP Certification #: CL0069
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 29

�ce"
Project: LAND APPLICATION
Pace Project No.: 92703642
Pace Analytical Services National
Oklahoma Certification #: 9915
Oregon Certification #: TN200002
Pennsylvania Certification #: 68-02979
Rhode Island Certification #: LA000356
South Carolina Certification #: 84004
South Dakota Certification
Tennessee DWIChemlMicro Certification #: 2006
Texas Mold Certification #: LAB0152
Texas Certification #: T 104704245-17-14
USDA Soil Permit #: P330-15-00234
Utah Certification #: TNO0003
Pace Analytical Services, LLC
9BOOKinceyAve, Suite100
Huntersville, NC 28078
[phone]
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Laboratory ID: 99006
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
Pace Analytical Services Peachtree Corners
110 Technology Pkwy, Peachtree Corners, GA 30092
Florida DOH Certification #: E87315
Georgia DW Inorganics Certification #: 812
CERTIFICATIONS
Vermont Dept. of Health: ID# VT-2006
Virginia Certification #: VT2006
Virginia Certification #: 460132
Washington Certification #: C847
West Virginia Certification #: 233
Wisconsin Certification #: 998093910
Wyoming UST Certification #: via A21-A 2926.01
A21i 17025 Certification #: 1461.01
A21i 17025 Certification #: 1461.02
AIHA-LAPILLC EMLAP Certification #:100789
South Carolina Certification #: 99006001
South Carolina Drinking Water Cert. #: 99006003
FloridaINELAP Certification #: E87627
Kentucky UST Certification #: 84
Louisiana DoH Drinking Water #: LA029
VirginialVELAP Certification #: 460221
South Carolina Laboratory ID: 99030
South Carolina Certification #: 99030001
Virginia[VELAP Certification #: 460222
North Carolina Certification #: 381
South Carolina Certification #: 98011001
Virginia Certification #: 460204
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 3 of 29

ace"
SAMPLE ANALYTE COUNT
Project: LAND APPLICATION
Pace Project No,: 92703642
Lab ID Sample ID
92703642001 WWTP CAKE
92703642002 WTP CAKE
PAN = Pace National - Mt. Juliet
PASI-A= Pace Analytical Services -Asheville
PASI-C = Pace Analytical Services - Charlotte
PASI-GA = Pace Analytical Services - Peachtree Corners, GA
PASI-PA = Pace Analytical Services - Greensburg
Method
EPA 8151A
EPA 8081 B
EPA 8082A
EPA 6010D
EPA 7470A
EPA 8270E
EPA 8260D
SM 254OG-2015
EPA 1010E
EPA 9045D
EPA 9014
SM 4500-S2-F-2011
EPA 8151 A
EPA 8081 B
EPA 8082A
EPA 601 OD
EPA 7470A
EPA 8270E
EPA 8260D
SM 254OG-2015
EPA 1010B
EPA 9045D
EPA 9014
SM 4500-S2-F-2011
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Analytes
Analysts Reported
DLH
3
BAJ
9
BAJ
8
DRB
7
VB
1
PKS
18
SAS
14
AJG
1
YEG
1
MDW
1
PAS
1
CDD
1
DLH
3
BAJ
9
BAJ
8
DRB
7
VB
1
PKS
18
SAS
14
AJG
1
YEG
1
MDW
1
PAS
1
CDD
1
Laboratory
PAN
PAS I-C
PASI-C
PASI-GA
PASI-GA
PASI-C
PASI-C
PAS I -PA
PASI-A
PAS I -A
PAST -PA
PASI-PA
PAN
PASI-C
PASI-C
PAS I -GA
PAS I -GA
PASI-C
PASI-C
PASI-PA
PASI-A
PASI-A
PASI-PA
PAS I -PA
Page 4 of 29

(—'o "69aceM
ANALYTICAL RESULTS
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: LAND APPLICATION
Pace Project No.: 92703642
Sample: WWTP CAKE Lab ID: 92703642001 Collected: 12/13/23 10:10 Received: 12/13/23 11:50 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
Chlorinated Herb. (GC) 8151A
2,4,5-TP (Silvex)
2,4-D
Surrogates
2,4-DCAA (S)
8081 TCLP Pesticides RVE
gamma-BHC (Lindane)
Chlordane (Technical)
Endrin
Heptachlor
Heptachlor epoxide
Methoxychlor
Toxaphene
Surrogates
Decachlorobiphenyl (S)
Tetrachloro-m-xylene (S)
8082 TCLP PCBs RVE
PCB-1016 (Aroclor 1016)
PCB-1221 (Aroclor 1221)
PCB-1232 (Aroclor 1232)
PCB-1242 (Aroclor 1242)
PCB-1248 (Aroclor 1248)
PCB-1254 (Aroclor 1254)
PCB-1260 (Aroclor 1260)
Surrogates
Decachlorobiphenyl (S)
Analytical Method: EPA 8151A Preparation Method: 8151A
Leachate Method/Date: 1311; 12/19/23 13:25 Initial pH: 7.07; Final pH: 5.53
Pace National - Mt, Juliet
ND mg/L
ND mg/L
76.8 %
0.00200 1 12128/2311:41 12131/2317:09 93-72-1
0.00200 1 12/28/23 11:41 12/31 /23 17:09 94-75-7
14.0-158 1 12/28/23 11:41 12/31/23 17:09 19719-28-9
Analytical Method: EPA B081 B Preparation Method: EPA 351 OC
Leachate Method/Date:
EPA 1311; 12/14/23 10:00
Initial
pH: 7.32; Final
pH: 5
Pace Analytical
Services - Charlotte
ND
ug/L
0.50
1
1211612311:52
12/21/2313:51
58-89-9
ND
ug/L
3.0
1
12/1612311:52
12/2112313:51
57-74-9
ND
ug/L
0.50
1
12/1612311:52
12/21/2313:51
72-20-8
ND
ug/L
0.50
1
12/16/23 11:52
12/21/2313:51
76-44-8
ND
ug/L
0,50
1
12116/2311:52
12/21/2313:51
1024-57-3
ND
ug/L
1000
1
12/16/23 11:52
12/2112313:51
72-43-5
N❑
ug/L
3.0
1
12/16/23 11:52
12/2112313:51
8001-35-2
79
%
19-200
1
12116/2311:52
12121/2313:51
2051-24-3
66
%
10-137
1
12116/2311:52
12121/2313:51
877-09-8
Analytical Method:
EPA8082A Preparation Method:
EPA3510C
Leachate Method/Date: EPA 1311; 12/14/23 10:00
Initial
pH: 7.32; Final
pH: 5
Pace Analytical
Services - Charlotte
ND
ug/L
1000
1
12/16/23 11:52
12/22/23 00:36
12674-11-2
ND
ug/L
1000
1
12/16/23 11:52
12/22/23 00:36
11104-28-2
ND
ug/L
1000
1
12/16/23 11:52
12/22/23 00:36
11141-16-5
ND
ug/L
1000
1
12/16/23 11:52
12/22/23 00:36
53469-21-9
NO
ug/L
1000
1
12/16/23 11:52
12/22/23 00:36
12672-29-6
ND
ug1L
1000
1
12/16/23 11:52
12/22/23 00:36
11097-69-1
ND
ug/L
1000
1
12/16/23 11:52
12/22/23 00:36
11096-82-5
101
%
10-193
1
12/16/23 11:52
12/22/23 00:36
2051-24-3
6010D ATL ICP, TCLP
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Leachate Method/Date: EPA 1311; 12/26/23 15:00 Initial
pH: 8.94; Final
pH: 5.26
Pace Analytical Services - Peachtree Comers, GA
Arsenic
ND mg/L 1.5 5
12/2812314:10
01103/2418:45
7440-38-2
Barium
ND mg/L 0.50 1
12/28/23 14:10
12/29/23 21:14
7440-39-3
Cadmium
0.17 mg/L 0.10 1
12/28/23 14:10
12/29/23 21:14
7440-43-9
Chromium
ND mg1L 0,10 1
12/28/23 14:10
12/29/23 21:14
7440-47-3
Lead
24.4 mg/L 0.25 1
12/28/23 14:10
12/29/23 21:14
7439-92-1
Selenium
N❑ mg/L 0.40 1
12/28/23 14:10
12/29/23 21:14
7782-49-2
Silver
ND mg/L 0.10 1
12/28/23 14:10
12/29/23 21:14
7440-22-4
REPORT OF LABORATORY ANALYSIS
LO
D3
This report shall not be reproduced, except in full,
Date: 01/04/2024 05:18 PM without the written consent of Pace Analytical Services, LLC, Page 5 of 29

acem
ANALYTICAL RESULTS
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Project: LAND APPLICATION
Pace Project No.: 92703642
Sample: WWTP CAKE Lab ID: 92703642001 Collected: 12/13/23 10:10 Received: 12/13/23 11:50 Matrix: Solid
Results reported on a "dry weight' basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters
7470 Mercury, TCLP
Mercury
8270E TCLP RVE
1,4-Dichlorobenzene
2,4-Dinitrotoluene
H exachloro-1,3-butad iene
Hexachlorobenzene
Hexachloroethane
2-Methylphenol(o-Cresol)
3&4-Methylphenol(m&p Cresol)
Nitrobenzene
Penlachlorophenol
Pyridine
2,4,5-Trich lorophenol
2,4, 6-Trichlorophenol
Surrogates
Nitrobenzene-d5 (S)
2-Fluorobiphenyl (S)
Terphenyl-d14 (S)
Phenol-d6 (S)
2-Fluorophencl (S)
2,4,6-Tribromcphenol (S)
8260D NISV TCLP
Benzene
2-Butanone (MEK)
Carbon tetrachloride
Chlorobenzene
Chloroform
1,4-Dichlorobenzene
1,2-Dichloroethane
1,1-Dichloreethene
Tetrachloroethene
Trichloroethene
Vinyl chloride
Surrogates
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
4-13romo%oroben7ene (S)
Results Units Report Limit OF Prepared Analyzed CAS No. Qual
Analytical Method: EPA 7470A Preparation Method: EPA 7470A
Leachate Method/Date: EPA 1311: 12/26/23 15:00 Initial pH: 8,94; Final pH: 5.26
Pace Analytical Services - Peachtree Corners, GA
ND mg1L 0.0050 1 12/28/23 07:05 12/28/23 12:00 7439-97-6
Analytical Method: EPA 8270E Preparation Method! EPA 3510C
Leachate Method/Date: EPA 1311; 12/14/23 10:00 Initial pH: 7.32; Final pH: 5
Pace Analytical Services - Charlotte
NO
ug/L
50.0
1
1211612313:23
12/17/2313:08
106-46-7
NO
ug/L
50.0
1
1211612313:23
12/17/2313:08
121-14-2
ND
ug/L
50.0
1
1211612313:23
1211712313:08
87-68-3
NO
ug/L
50.0
1
1211612313:23
1211712313:08
118-74-1
ND
ug/L
50.0
1
1211612313:23
12117/2313:08
67-72-1
ND
ug/L
50.0
1
12116/2313:23
12/17/2313:08
9548-7
ND
ug/L
50.0
1
12116/2313:23
12/17/2313:08
15831-10-4
NO
ug/L
50.0
1
12/16/2313:23
12/17/2313:08
98-95-3
ND
ug/L
100
1
12/1612313:23
12/1712313:08
87-86-5
NO
ug/L
50.0
1
12116/2313:23
12/17/2313:08
110-86-1
NO
ug/L
50.0
1
12/16/2313:23
12117/2313:08
95-954
ND
ug/L
50.0
1
12/1612313:23
12117/2313:08
88-06-2
88
%
10-133
1
1211612313:23
12117/2313:08
4165-60-0
85
%
10-130
1
1211612313:23
12117/2313:08
321-60-8
119
%
10-193
1
12116/2313:23
12/17/2313:08
1718-51-0
47
%
10-130
1
1211612313:23
12/17/2313:08
13127-88-3
54
%
10-130
1
1211612313:23
12/1712313:08
367-12-4
103
%
10-166
1
12/16/2313:23
12/17/2313:08
118-79-6
Analytical Method: EPA 8260D Leachate Method/Date: EPA 1311: 12/14/23 13:03
Pace Analytical Services - Charlotte
NO
ug/L
100
20
12/1512319:58
71-43-2
ND
ug/L
200
20
1211512319:58
78-93-3
ND
ug/L
100
20
1211512319:58
56-23-5
ND
ug/L
100
20
12115/2319:58
108-90-7
ND
ug1L
100
20
12/15/2319:58
67-66-3
ND
ug1L
100
20
12/15/2319:58
106-46-7
NO
ug/L
100
20
12/15/2319:58
107-06-2
NO
ug/L
100
20
12/15/2319:58
75-35-4
NO
ug1L
100
20
12/15/2319:58
127-18-4
NO
ug/L
100
20
12/15/2319:58
79-01-6
NO
ug/L
100
20
12/15/2319:58
75-01-4
103
%
70-130
20
1211512319:58
17060-07-0
97
%
70-130
20
1211512319:58
2037-26-5
98
%
70-130
20
1211512319:58
460-00-4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/04/2024 05:18 PM without the written consent of Pace Analytical Services, LLC. Page 6 of 29

�cee
ANALYTICAL RESULTS
Project: LAND APPLICATION
Pace Project No.: 92703642
Pace Analytical Services, LLC
9800 KinceyAve, Suile 100
Huntersvillo, NC 28078
[phone]
Sample: WWTP CAKE Lab ID: 92703642001 Collected: 12/13/23 10:10 Received: 12/13/23 11:50 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
Percent Moisture Analytical Method: SM 254OG-2015
Pace Analytical Services - Greensburg
Percent Moisture
84.4 % 0.10 1
12/18/23 15:11
1010 Fiashpoint,Closed Cup
Analytical Method: EPA 1010B
Pace Analytical Services - Asheville
Flashpoint
a200 deg F 70.0 1
12/26/23 12:32
9045 pH Soil
Analytical Method: EPA9045D
Pace Analytical Services -Asheville
pH at 25 Degrees C
6.8 Std, Units 0.10 1
12/22/23 19:33
733C S Reactive Cyanide
Analytical Method: EPA 9014 Preparation Method: SW-846 7.3.3.2
Pace Analytical Services - Greensburg
Cyanide, Reactive
ND mg/kg 6.4 1 12/20/23 15:38
12/20/23 16:28
734S Reactive Sulfide
Analytical Method: SM 4500-S2-F-2011 Preparation Method: SW-846 7.3.4.2
Pace Analytical Services - Greensburg
Sulfide, Reactive
ND mg/kg 63.6 1 12/20/23 15:38
12/20/23 16:10
Date: 01/04/2024 05:18 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
H3
Page 7 of 29

Pace Analytical Services, LLC
t] f1 9800 Kincey Ave, Suite 100
Q f _ e� Huntersville, NC 28078
V [phone]
ANALYTICAL RESULTS
Project: LAND APPLICATION
Pace Project No.: 92703642
Sample: WTP CAKE Lab ID: 92703642002 Collected: 12/13/23 09:35 Received: 12/13/23 11:50 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
Chlorinated Herb, (GC) 8151A
2,4,5-TP (Silvex)
2,4-D
Surrogates
2,4-DCAA (S)
Analytical Method: EPA8151A Preparation Method: 8151A
Leachate Method/Date: 1311; 12/19/23 13:25 Initial pH: 5,68; Final pH: 5.54
Pace National - Mt. Juliet
ND mglL 0.00200 1 12/2812311:41 12131/2317:20 93-72-1
ND mglL 0.00200 1 12/28/2311:41 12/31/2317:20 94-75-7 LO
185 % 14.0-158 1 12/28/23 11:41 12/31 /23 17:20 19719-28-9 ST
8081 TCLP Pesticides RVE
Analytical Method: EPA 8081 B Preparation Method: EPA 351 OC
Leach ate Method/Date: EPA 1311; 12/14/23 10:00 Initial
pH: 7.36; Final
pH: 5
Pace Analytical
Services - Charlotte
gamma-BHC (Lindane)
NO
ug/L
0.50 1
12/16/23 11:52
12/21/23 14:29
58-89-9
Chlordane (Technical)
ND
ug/L
3.0 1
12/16/23 11:52
12/21/23 14:29
57-74-9
Endrin
ND
ug/L
0.50 1
12/1612311:52
1212112314:29
72-20-8
Heptachlor
ND
ug/L
0.50 1
12/16/23 11:52
12/21/2314:29
76-44-8
Heptachlor epoxide
NO
ug/L
0.50 1
12/16/23 11:52
12/21/23 14:29
1024-57-3
Methoxychlor
N❑
ug/L
1000 1
12/16/23 11:52
12/2112314:29
72-43-5
Toxaphene
ND
ug/L
3.0 1
12/16/23 11:52
12/2112314:29
8001-35-2
Surrogates
Decachlorobiphenyl (S)
66
%
19-200 1
12/16/23 11:52
12/21/23 14:29
2051-24-3
Tetrachloro-m-xylene (S)
50
%
10-137 1
12/16/23 11:52
12/21/23 14:29
877-09-8
8082 TCLP PCBs RVE
Analytical Method: EPA 8082A Preparation Method: EPA 351 OC
Leachate Method/Date:
EPA 1311; 12/14/23 10:00 Initial
pH: 7.36: Final
pH: 5
Pace Analytical
Services - Charlotte
PCB-1016 (Aroclor 1016)
ND
ug/L
1000 1
12/16/23 11:52
12/22/23 00:49
12674-11-2
PCB-1221 (Aroclor 1221)
ND
ug/L
1000 1
12/16/23 11:52
12/22/23 00:49
11104-28-2
PCB-1232 (Aroclor 1232)
ND
ug/L
1000 1
12/16/23 11:52
12/22/23 00:49
11141-16-5
PCB-1242 (Aroclor 1242)
ND
ug1L
1000 1
12/16/23 11:52
12/22/23 00:49
53469-21-9
PCB-1248 (Aroclor 1248)
ND
ug/L
1000 1
12/16/23 11:52
12/22/23 00:49
12672-29-6
PCB-1254 (Aroclor 1254)
ND
uglL
1000 1
12/16/23 11:52
12/22/23 00:49
11097-69-1
PCB-1260 (Aroclor 1260)
ND
uglL
1000 1
12/16/23 11:52
12/22/23 00:49
11096-82-5
Surrogates
Decachlorobiphenyl (S)
65
%
10-193 1
12/16/23 11:52
12/22/23 00:49
2051-24-3
601 OD ATL ICP, TCLP
Analytical Method:
EPA 601 OD Preparation Method: EPA 301 OA
Leachate Method/Date: EPA 1311; 12/26/23 15:00 Initial
pH: 9.01; Final
pH: 5.41
Pace Analytical
Services - Peachtree
Corners, GA
Arsenic
ND
mglL
0.30 1
12/28/23 14:10
12/29/23 2119
7440-38-2
Barium
ND
mg/L
0.50 1
12/28/23 14:10
12/29/23 21:19
7440-39-3
Cadmium
ND
mg/L
0.10 1
12/28/23 14:10
12/29/23 21:19
7440-43-9
Chromium
ND
mg/L
0.10 1
12/28/23 14:10
12/29/23 21:19
7440-47-3
Lead
ND
mg/L
0.25 1
12/28/23 14:10
12/29/23 21:19
7439-92-1
Selenium
ND
mg/L
0,40 1
12/28/23 14:10
12/29/23 21:19
7782-49-2
Silver
ND
mg/L
0.10 1
12/28/23 14:10
12/29/23 21:19
7440-22-4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/04/2024 05:18 PM without the written consent of Pace Analytical Services, LLC. Page 8 of 29

�ce-
ANALYTICAL RESULTS
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: LANDAPPLICATION
Pace Project No.: 92703642
Sample: WTP CAKE Lab ID: 92703642002 Collected: 12/13123 09:35 Received: 12/13/23 11:50 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual
7470 Mercury, TCLP
Mercury
8270E TCLP RVE
1,4-Dichlorobenzene
2,4-Dinitrotoluene
Hexachloro-1,3-butadiene
Hexachlorobenzene
Hexachloroethene
2-Methylphenol(o-Cresol )
3&4-Methylphenol(m&p Cresol)
Nitrobenzene
Pentachlorophenol
Pyridine
2,4, 5-Trich lorophenol
2,4,6-Trich lorophenol
Surrogates
Nitrobenzene-d5 (S)
2-Fluorobiphenyl (S)
Terphenyl-d14 (S)
Phenol-d6 (S)
2-Fluorophenol (S)
2,4,6-Tribromophenol (S)
8260D MSV TCLP
Benzene
2-Butanone (MEK)
Carbon tetrachloride
Chlorobenzene
Chloroform
1,4-Dichlorobenzene
1,2-13ichloroethane
1,1-Dichloroethene
Tetrachloroethene
Trichloroethene
Vinyl chloride
Surrogates
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
4-Bromofluorobenzene (S)
Analytical Method: EPA 7470A Preparation Method: EPA 7470A
Leachate Method/Date: EPA 1311; 12/26/23 15:00 Initial pH: 9,01; Final pH: 5.41
Pace Analytical Services - Peachtree Corners, GA
NO mg/L 0.0050 1 12/28/23 07:05 12/28/23 12:11 7439-97-6
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Leachate Method/Date: EPA 1311; 12/14/23 10:00 Initial pH: 7.36; Final pH: 5
Pace Analytical Services - Charlotte
NO
ug/L
50.0
1
1211612313:23
12/1712313:33
106-46-7
NO
ug/L
50.0
1
1211612313:23
1211712313:33
121-14-2
NO
ug1L
50.0
1
1211612313:23
12117/2313:33
87-68-3
ND
ug/L
50.0
1
12116/2313:23
12117/2313:33
118-74-1
ND
ug1L
50.0
1
12116/2313:23
12/1712313:33
67-72-1
ND
ug1L
50.0
1
12/16/2313:23
12/17/2313:33
9548-7
ND
uglL
50.0
1
12/1612313:23
12/17/2313:33
15831-10-4
NO
ug/L
50.0
1
12116/2313:23
12/17/2313:33
98-95-3
NO
ug/L
100
1
12/1612313:23
12/1712313:33
87-86-5
NO
ug/L
50.0
1
1211612313:23
12/1712313:33
110-86-1
NO
ug/L
50.0
1
1211612313:23
12/1712313:33
95-95-4
NO
ug1L
50.0
1
12116f23 13:23
1211712S 13:33
86-06-2
106
%
10-133
1
12116/2313:23
1211712313:33
4165-60-0
87
%
10-130
1
12/16/2313:23
12/17/2313:33
321-60-8
126
%
10-193
1
1211612313:23
12/17/2313:33
1718-51-0
53
%
10-130
1
12/16/2313:23
12117/2313:33
13127-88-3
75
%
10-130
1
12/1612313:23
12/1712313:33
367-12-4
114
%
10-166
1
12/1612313:23
12/1712313:33
118-79-6
Analytical Method: EPA 8260D Leachate MethodlDate: EPA 1311; 12/14/23 13:03
Pace Analytical Services - Charlotte
ND
ug/L
100
20
12/15/23 20:15 71-43-2
ND
ug/L
200
20
12/15/23 20:15 78-93-3
NO
ug/L
100
20
12/15/23 20:15 56-23-5
NO
ug/L
100
20
12/15/23 20:15 108-90-7
NO
ug/L
100
20
12/15/23 20:15 67-66-3
NO
ug/L
100
20
12/15/23 20:15 106-46-7
ND
ug/L
100
20
12/15/23 20:15 107-06-2
ND
ug1L
100
20
12/15/23 20:15 75-35-4
ND
ug/L
100
20
12/15/23 20:15 127-18-4
ND
ug/L
100
20
12/15/23 2015 79-01-6
ND
ug/L
100
20
12/15/23 20:15 75-01-4
100
%
70-130
20
12/15/23 20:15 17060-07-0
97
%
70-130
20
12/15/23 20:15 2037-26-5
97
%
70-130
20
12/15/23 20:15 460-00-4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/04/2024 05:18 PM without the written consent of Pace Analytical Services, LLC. Page 9 of 29

ace"
ANALYTICAL RESULTS
Project: LAND APPLICATION
Pace Project No.: 92703642
Paco Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Sample: WTP CAKE
Lab ID: 92703642002 Collected: 12/13/23 09:35 Received: 12/13/23 11:50 Matrix: Solid
Results reported on a 'dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters
Results Units Report Limit DF Prepared Analyzed CAS No. Qual
Percent Moisture
Analytical Method: SM 2540G-2015
Pace Analytical Services - Greensburg
Percent Moisture
68.2 % 0.10 1 12/18/23 15:11
1010 Flash po i nt,Closed Cup
Analytical Method: EPA 1010E
Pace Analytical Services -Asheville
Flashpoint
>200 deg F 70.0 1 12/26/23 13:51
9045 pH Soil
Analytical Method: EPA 9045D
Pace Analytical Services -Asheville
pH at 25 Degrees C
6.3 Std. Units 0.10 1 12/22/23 19:37 H3
733C S Reactive Cyanide
Analytical Method: EPA 9014 Preparation Method: SW-846 7.3.3.2
Pace Analytical Services - Greensburg
Cyanide, Reactive
ND mg/kg 3.2 1 12/20/23 15:38 12/20/23 16:29
734S Reactive Sulfide
Analytical Method: SM 4500-S2-F-2011 Preparation Method: SW-846 7.3.4.2
Pace Analytical Services - Greensburg
Sulfide, Reactive
ND mg/kg 31.5 1 12/20/23 15:38 12/20/23 16:10
Date: 01/04/2024 05:18 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 10 of 29

ace°
Project:
LAND APPLICATION
Pace Project No.:
92703642
QC Batch:
2194445
QC Batch Method:
8151A
Associated Lab Samples: 92703642001, 92703642002
METHOD BLANK: R4018798-1
Associated Lab Samples: 92703642001, 92703642002
Parameter Units
2,4,5-TP (Silvex) mg/L
2,4-D mg/L
2,4-DCAA (S) %
QUALITY CONTROL DATA
Analysis Method: EPA8151A
Analysis Description: Chlorinated Herb. (GC) 8151A
Laboratory: Pace National - Mt. Juliet
Matrix: Solid
Blank Reporting
Result Limit
Analyzed
ND 0.00200
12/3112313:56
ND 0.00200
12/3112313:56
91.4 14.0-158
12/31 /23 13:56
Qualifiers
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE:
R4018798-2
Spike
LCS
LCS % Rec
Parameter
Units
Conc.
Result
% Rec Limits Qualifiers
2,4,5-TP (Silvex)
mg/L
0.0500
0.0558
112 50.0-125 E,P9
2,4-0
mg/L
0.0500
0.0665
133 50.0-120 E,LO
2,4-DCAA (S)
%
93.4 14.0-158
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
R4018798-3
R4018798-4
MS
MSD
L1688914-01
Spike
Spike
MS MSD
MS
MSD % Rec
Parameter
Units
Result
Conc.
Conc.
Result Result
% Rec
% Rec Limits RPD Qual
2,4,5-TP (Silvex)
mgfL
ND
0.0500
0,0500
ND ND
172
133 50.0-125 26.0 E,MH,P9,
R1
2,4-D
mgfL
ND
0.0500
0.0500
ND ND
119
117 50.0-120 2.37 E
2,4-DCAA (S)
%
74.4
82.2 14.0-158
Results presented on this page are In the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /04/2024 05:18 PM without the written consent of Pace Analytical Services, LLC.
Page 11 of 29

�ceo
Project:
LAND APPLICATION
Pace Project No.:
92703642
QC Batch:
822245
QC Batch Method:
EPA 3010A
Associated Lab Samples: 92703642001, 92703642002
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Analysis Method: EPA 6010D
Analysis Description: 601 OD ATL TCLP
Laboratory: Pace Analytical Services - Peachtree Corners, GA
METHOD BLANK: 4252963
Matrix: Water
Associated Lab Samples:
92703642001, 92703642002
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Arsenic
mg/L
ND
0.30
12/29/23 21:04
Barium
mg/L
ND
0.50
12/29/23 21:04
Cadmium
mg/L
ND
0.10
12/29/23 21:04
Chromium
mg/L
ND
0.10
12/29/23 21:04
Lead
mg/L
ND
0.25
12/29/23 21:04
Selenium
mg/L
ND
0.40
12/29/23 21:04
Silver
mg/L
ND
0,10
1212912321:04
LABORATORY CONTROL SAMPLE:
4254626
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits Qualifiers
Arsenic
mg/L
10
10.4
104
80-120
Barium
mg/L
10
9.6
96
80-120
Cadmium
mg/L
10
10.1
101
80-120
Chromium
mg/L
10
9.8
98
80-120
Lead
mg/L
10
10.1
101
80-120
Selenium
mg/L
10
10.1
101
80-120
Silver
mg1L
10
9.7
97
80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
4254627
4254628
MS
MSD
92705425001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Arsenic
mg/L
ND
10
10
10.8
10.6
108
105
75-125
2
Barium
mg/L
ND
10
10
9.9
9.8
98
96
75-125
1
Cadmium
mg/L
ND
10
10
10.3
10.0
102
100
75-125
2
Chromium
mg/L
ND
10
10
9.8
9.7
98
97
75-125
1
Lead
mg/L
ND
10
10
10.4
10.2
104
101
75-125
2
Selenium
mg/L
ND
10
10
10.4
10.2
104
102
75-125
2
Silver
mg/L
ND
10
10
9.8
9.7
98
97
75-125
1
Results presented on this page are in the units indicated by the 'Units" column except where an alternate unit Is presented to the right of the result,
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/04/2024 05:18 PM without the written consent of Pace Analytical Services, LLC.
Page 12 of 29

�ces
QUALITY CONTROL DATA
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NO 28078
[phone]
Project: LAND APPLICATION
Pace Project No.: 92703642
QC Batch: 821958 Analysis Method: EPA 7470A
QC Batch Method: EPA 7470A Analysis Description: 7470 Mercury TCLP, ATL
Laboratory: Pace Analytical Services - Peachtree Comers, GA
Associated Lab Samples: 92703642001. 92703642002
METHOD BLANK: 4252963
Associated Lab Samples: 92703642001, 92703642002
Parameter Units
Mercury mglL
LABORATORY CONTROL SAMPLE: 4253583
Parameter Units
Mercury mg1L
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 0.0050 12128l2311:50
Spike LCS LCS % Rec
Conc. Result % Rec Limits Qualifiers
0.017 0.016 94 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4253581 4253582
MS MSD
92703642001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc, Conc. Result Result % Rec % Rec Limits RPD Qual
Mercury mglL ND 0.017 0.017 0,015 0.015 92 92 75-125 0
Results presented on this page are In the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result,
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/04/2024 05:18 PM without the written consent of Pace Analytical Services, LLC.
Page 13 of 29

we"
QUALITY CONTROL DATA
Project: LAND APPLICATION
Pace Project No.: 92703642
QC Batch: 819921 Analysis Method: EPA 8260D
QC Batch Method: EPA 8260D Analysis Description: 8260D MSV TCLP
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92703642001, 92703642002
METHOD BLANK: 4244093
Associated Lab Samples: 92703642001, 92703642002
Parameter Units
Matrix: Water
Blank Reporting
Result Limit
Analyzed
1,1-Dichloroethene
uglL
ND
5.0
1211512311:59
1,2-Dichloroethane
uglL
ND
5.0
1211512311:59
1,4-Dichlorobenzene
ug1L
ND
5.0
1211512311:59
2-Butanone (MEK)
ug1L
ND
10.0
12/15/23 11:59
Benzene
ug/L
ND
5.0
12/15/2311:59
Carbon tetrachloride
ug1L
ND
5.0
12/15/23 11:59
Chlorobenzene
ug1L
ND
5.0
12115/2311:59
Chloroform
ug1L
ND
5.0
12/15/2311:59
Tetrachloroethene
uglL
ND
5.0
12/15/2311:59
Trichloroethene
uglL
ND
5.0
12115/2311:59
Vinyl chloride
uglL
ND
5.0
12/15/23 11:59
1,2-Dichloroethane-d4 (S)
%
112
70-130
12/15/23 11:59
4-Bromofluorobenzene (S)
%
98
70-130
12/15/23 11:59
Toluene-d8 (S)
%
98
70-130
12/15/23 11:59
Qualifiers
LABORATORY CONTROL SAMPLE:
Parameter
4244092
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
1,1-Dichloroethene
uglL
20
21.4
107
69-131
1,2-Dichloroethane
uglL
20
20.1
100
70-130
1,4-Dichlorobenzene
uglL
20
22.8
114
70-130
2-Butanone (MEK)
uglL
40
42.3
106
67-133
Benzene
ug/i_
20
20.5
102
70-130
Carbon tetrachloride
ug1L
20
18.9
94
70-130
Chlorobenzene
ug1L
20
21.3
107
70-130
Chloroform
ug1L
20
18.4
92
70-130
Tetrachloroethene
ug1L
20
22.7
113
70-130
Trichloroethene
ug1L
20
20.7
103
70-130
Vinyl chloride
uglL
20
17.6
88
66-140
1,2-Dichloroethane-d4 (S)
%
94
70-130
4-Bromofluorobenzene (S)
%
94
70-130
Toluene-d8 (S)
%
95
70-130
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Qualifiers
Results presented on this page are In the units Indicated by the -Units- column except where an alternate unit Is presented to the right of the result,
REPORT OF LABORATORY ANALYSIS
This report shalt not be reproduced, except in full,
Date: 01/04/2024 05:18 PM without the written consent of Pace Analytical Services, LLC,
Page 14 of 29

(-�Face"
QUALITY CONTROL DATA
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: LAND APPLICATION
Pace Project No.: 92703642
MATRIX SPIKE & MATRIX SPIKE
DUPLICATE:
4244094
4244095
MS
MSD
92703161001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits RPD Qual
1,1-Dichloroethene
uglL
ND
20
20
ND
ND
116
107
64-162
1,2-Dichloroethane
uglL
ND
20
20
ND
ND
109
93
68-145
1,4-Dichlorobenzene
ug1L
ND
20
20
ND
ND
116
98
70-140
2-Butanone (MEK)
uglL
ND
40
40
ND
ND
130
125
57-156
Benzene
uglL
ND
20
20
ND
ND
99
105
68-144
Carbon tetrachloride
ug1L
ND
20
20
ND
ND
66
80
70-147 M1
Chlorobenzene
uglL
ND
20
20
ND
ND
116
105
70-143
Chloroform
ug1L
ND
20
20
ND
ND
93
78
67-148
Tetrachloroethene
ugOL
ND
20
20
ND
ND
120
91
70-145
Trichloroethene
ug1L
ND
20
20
ND
ND
80
85
70-152
Vinyl chloride
ug1L
ND
20
20
ND
ND
74
74
51-178
1,2-Dichloroethane-d4 (S)
%
103
107
70-130
4-Bromofluorobenzene (S)
%
100
97
70-130
Toluene-d8 (S)
%
96
98
70-130
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full.
Date: 01/04/2024 05:18 PM without the written consent of Pace Analytical Services, LLC.
Page 15 of 29

�ce¢
Project:
LAND APPLICATION
Pace Project No.:
92703642
QC Batch:
820096
QC Batch Method:
EPA 3510C
Associated Lab Samples: 92703642001, 92703642002
METHOD BLANK: 4241977
Associated Lab Samples: 92703642001, 92703642002
Parameter
Units
Chlordane (Technical)
ug/L
Endrin
ug/L
gamma-BHC (Lindane)
ug1L
Heptachlor
ug/L
Heptachlor epoxide
ug/L
Methoxychlor
ug1L
Toxaphene
ug1L
Decachlorobiphenyl (S)
%
Totrachloro-m-xylene (S)
%
LABORATORY CONTROL SAMPLE;
4245178
Parameter
Units
Endrin
ug/L
gamma-BHC (Lindane)
ug1L
Heptachlor
ug1L
Heptachlor epoxide
ug/L
Methoxychlor
ug/L
Decachlorobiphenyl (S)
%
Tetrachloro-m-xylene (5)
%
QUALITY CONTROL DATA
Analysis Method:
Analysis Description
Laboratory:
Matrix: Water
Blank
Result
Spike
Cone.
1.2
1.2
1.2
1.2
3.8
ND
ND
ND
ND
ND
ND
ND
60
65
Reporting
EPA 8081 B
8081 TCLP Pesticides RV
Pace Analytical Services - Charlotte
Limit Analyzed
Qualifiers
3.0
12/21/23 14:54
0.50
12/21/23 14:54
0.50
12/21/23 14:54
0.50
12/21/23 14:54
0.50
12/21 /23 14:54
1000
12/21 /23 14:54
3.0
12/21 /23 14:54
19-200
12/21 /23 14:54
10-137
12/21 /23 14:54
LCS
Result
0.91
0.77
0.71
0.76
2.3J
LCS
% Rec
72
61
57
61
62
70
66
% Rec
Limits
33-190
32-148
32-149
37-149
35-171
19-200
10-137
Pace Ana lyticai Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Qualifiers
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
4245179
4245180
MS
MSD
92703642001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Cone.
Cone.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Endrin
ug1L
ND
1.2
1.2
1.2
1.6
96
125
10-200
26
gamma-BHC (Lindane)
ug/L
N❑
1.2
1.2
0.96
1.3
77
104
13-163
30
Heptachlor
u911-
ND
1.2
1.2
0.96
1.3
77
104
10-172
30
Heptachlor epoxide
ug/L
ND
1.2
1.2
11
1.3
85
102
10-168
19
Methoxychlor
ug/L
ND
3.8
3.8
3.1J
3.9J
83
104
13-183
Decachlorobiphenyl (S)
%
83
88
19-200
Tetrachloro-m-xylene (S)
%
71
96
10-137
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/04/2024 05:18 PM without the written consent of Pace Analytical Services, LLC.
Page 16 of 29

(-�Face"
Project:
LAND APPLICATION
Pace Project No.:
92703642
QC Batch:
820097
QC Batch Method:
EPA 3510C
Associated Lab Samples: 92703642001, 92703642002
QUALITY CONTROL DATA
Analysis Method: EPA8082A
Analysis Description: 8082 TCLP PCB RV
Laboratory: Pace Analytical Services - Charlotte
METHOD BLANK: 4241977
Matrix: Water
Associated Lab Samples:
92703642001, 92703642002
Blank
Reporting
Parameter
units
Result
Limit
Analyzed Qualifiers
PCB-1016 (Aroclor 1016)
ug/L
ND
1000
12/22/23 01:52
PCB-1221 (Aroclor 1221)
ug/L
NO
1000
12/22/23 01:52
PCB-1232 (Aroclor 1232)
ug/L
NO
100D
12/22/23 01:52
PCB-1242 (Aroclor 1242)
ug/L
ND
1000
12/22/23 01:52
PCB-1248 (Aroclor 1248)
ug/L
ND
1000
12/22/23 01:52
PCB-1254 (Aroclor 1254)
ug/L
ND
1000
12/22/23 01:52
PCB-1260 (Aroclor 1260)
ug/L
ND
1000
12/22/23 01:52
Decachlorobiphenyl (S)
%
66
10-193
12/22/23 01:52
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE: 4245181
Spike LCS LCS % Rec
Parameter Units Cone. Result % Rec Limits Qualifiers
PCB-1016 (Aroclor 1016) ug/L 25 ND 62 34-137
PCB-1260 (Aroclor 1260) ug/L 25 ND 55 39-145
Decachlorobiphenyl (S) % 43 10-193
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
4245182
4245183
MS
MSD
92703642002 Spike
Spike MS
MSD MS
MSD
% Rec
Parameter
Units
Result Cone.
Cone, Result
Result % Rec
% Rec
Limits RPD Qua[
PCB-1016 (Aroclor 1016)
ug/L
ND 25
25 ND
NO 69
71
10-153
PCB-1260 (Aroclor 1260)
ug/L
ND 25
25 NO
NO 54
57
10-156
Decachlorobiphenyl (S)
%
85
90
10-193
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/04/2024 05:18 PM without the written consent of Pace Analytical Services, LLC.
Page 17 of 29

Pace Analytical Services, LLG
9800 Kincey Ave. Suite 100
Huntersville, NG 28078
[phone]
QUALITY CONTROL DATA
Project: LAND APPLICATION
Pace Project No,! 92703642
QC Batch: 820095
QC Batch Method: EPA 3510C
Associated Lab Samples: 92703642001, 92703642002
Analysis Method: EPA 8270E
Analysis Description: 8270E TCLP MSSV
Laboratory: Pace Analytical Services - Charlotte
METHOD BLANK: 4241977
Matrix:
Water
Associated Lab Samples: 92703642001, 92703642002
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
1,4-Dichlorobenzene
ug/L
ND
50.0
1211712314:11
2,4,5-Trichlorophenol
ug/L
ND
50.0
1211712314:11
2,4,6-Trichlorophenol
ug/L
NO
50.0
1211712314:11
2,4-Dinitrotoluene
ug/L
NO
50.0
12/17/23 14:11
2-Methylphenol(o-Cresol)
ug1L
ND
50.0
12/17/2314:11
3&4-Methylphenol(m&p Cresol)
ug/L
NO
50.0
12/17/23 14:11
Hexachloro-1,3-butadiene
ug/L
NO
50.0
12J1 7/23 14:11
Hexachlorobenzene
ug/L
ND
50.0
12J17/2314:11
Hexachloroethane
ug/L
NO
50.0
12J17/2314:11
Nitrobenzene
ug/L
ND
50,0
1211712314:11
Pentachlorophenol
ug/L
NO
100
12J17123 14:11
Pyridine
ug/L
NO
50.0
12117/2314:11
2,4,6-Tribromophenol (S)
%
112
10-166
12117/23 14:11
2-Fluorobiphenyl (S)
%
84
10-130
12/17/23 14:11
2-Fluorophenol (S)
%
69
10-130
12/17/23 14:11
Nitrobenzen"5 (S)
%
93
10-133
12/17/23 14:11
Phenol-d6 (S)
%
51
10-130
12M7123 14:11
Terphenyl-d14 (S)
%
137
10-193
12J17/23 14:11
LABORATORY CONTROL SAMPLE: 4245175
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits Qualifiers
1,4-Dichlorobenzene
ug]L
500
249
50
10-130
2,4,5-Trichlorophenol
ugJL
500
385
77
36-150
44,6-Trichlorophenol
ug/L
500
374
75
30-151
2,4-Dinitrotoluene
ug/L
500
373
75
46-160
2-Methylphenol(o-Cresol)
ug/L
500
326
65
32-130
3&4-Methylphenol(m&p Cresol)
ug/L
500
325
65
29-130
Hexachloro-1,3-butadiene
ug1L
500
263
53
10-130
Hexachlorobenzene
ug/L
500
408
82
40-139
Hexachloroethane
ug/L
500
226
45
10-130
Nitrobenzene
ug1L
500
337
67
33-136
Pentachlorophenol
ug/L
1000
817
82
19-156
Pyridine
ug/L
500
94.2
19
10-130
2,4,6-Tribromophenol (S)
%
117
10-166
2-Fluorobiphenyl (S)
%
89
10-130
2-Fluorophenol (S)
%
70
10-130
Nitrobenzene-d5 (S)
%
92
10-133
Phenol-d6 (S)
%
55
10-130
Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/04/2024 05:18 PM without the written consent of Pace Analytical Services, LLG.
Page 18 of 29

(-�FaCe'
QUALITY CONTROL DATA
Project: LAND APPLICATION
Pace Project No.: 92703642
LABORATORY CONTROL SAMPLE: 4245175
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits
Terphenyl-d14 (S) % 121 10-193
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntorsville, NC 28078
[phone]
Qualifiers
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4245176
MS
92703426001 Spike
Parameter Units Result Conc.
MSD
Spike
Conc.
4245177
MS
Result
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits
RPD Qual
1,4-Dichlorobenzene
ugfL
ND
500
500
269
359
54
72
10-130
28
2,4,5-Trichlorophenol
ugfL
N❑
500
500
431
536
86
107
10-174
22
2,4,6-Trichlorophenol
ugfL
ND
500
500
438
538
88
108
10-173
20
2,4-Dinitrotoluene
ugfL
ND
500
500
439
550
88
110
29-168
22
2-Methylphenol(o-Cresol)
ugfL
ND
500
500
322
433
64
87
10-130
29
3&4-Methylphenol(m&p
ug1L
ND
500
500
341
441
68
88
10-132
26
Cresol)
Hexachloro-1,3-butad!one
ug,'L
ND
500
500
312
447
62
89
10-130
36 R1
Hexachlorobenzene
ugfL
ND
500
500
398
501
80
100
27-145
23
Hexachloroethane
ugfL
ND
500
500
229
330
46
66
10-130
36 R1
Nitrobenzene
ugfL
NO
500
500
386
477
77
95
10-145
21
Pentachlorophenol
ugfL
ND
1000
1000
920
1140
92
114
10-178
21
Pyridine
ugfL
ND
500
500
38J
27.2J
8
5
10-130
M1
2,4,6-Tribromophenol (S)
%
104
132
10-166
2-Fluorobiphenyl (S)
°/a
87
101
10-130
2-Fluorophenol (S)
%
66
74
10-130
Nitrobenzene-d5 (S)
%
97
115
10-133
Phenol-d6 (S)
%
50
63
10-130
Terphenyl-d14 (S)
%
113
140
10-193
Results presented on this page are in the units Indicated by the "units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/04/2024 05:18 PM without the written consent of Pace Analytical Services, LLC.
Page 19 of 29

�ceP
Project: LAND APPLICATION
Pace Project No.: 92703642
QC Batch: 636715
QC Batch Method: SM 254OG-2015
Associated Lab Samples: 92703642001, 92703642002
SAMPLE DUPLICATE: 3106658
Parameter Units
Percent Moisture %
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Analysis Method: SM 254OG-2015
Analysis Description: Dry Weight/Percent Moisture
Laboratory: Pace Analytical Services - Greensburg
30646969001 Dup
Result Result RPD Qualifiers
18.7 17.1 9
SAMPLE DUPLICATE: 3105659
30646980001 Dup
Parameter Units Result Result
Percent Moisture % 15.3 17.9
RPD Qualifiers
15 D6
Results presented on this page are In the units indicated by the "Units" column except where an alternate unit is presented to the right of the result,
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/04/2024 05:18 PM without the written consent of Pace Analytical Services, LLC,
Page 20 of 29

(--Face&
Project: LANDAPPLICATION
Pace Project No.: 92703642
QC Batch: 821865
QC Batch Method: EPA 1010B
Associated Lab Samples: 92703642001, 92703642002
SAMPLE DUPLICATE: 4253242
Parameter Units
Flashpoint deg F
QUALITY CONTROL DATA
Analysis Method: EPA 1010B
Analysis Description: 1010 Flash Point, Closed Cup
Laboratory: Pace Analytical Services -Asheville
92703642001 Dup
Result Result RPD Qualifiers
>200 >200
Pace Analytical Services, LLC
9800 Kincey Ave, Suite 100
Huntersville, NC 28078
[phone]
Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result,
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/04/2024 05:1 a PM without the written consent of Pace Analytical Services, LLC.
Page 21 of 29

�ce"
Project: LAND APPLICATION
Pace Project No.: 92703642
QC Batch: 821569
QC Batch Method: EPA 9045D
Associated Lab Samples: 92703642001, 92703642002
QUALITY CONTROL DATA
Analysis Method: EPA9045D
Analysis Description: 9045 pH
Laboratory: Pace Analytical Services -Asheville
SAMPLE DUPLICATE: 4252072
92703642002 Dup
Parameter Units Result Result RPD Qualifiers
pH at 25 Degrees C Std. Units 6.3 6.2 1 H3
Pace Analytical Services, LLC
9800 Kincey Ave, Suite 100
Huntersville, 128078
(704)875-91
Results presented on this page are in the units Indicated by the "units" corumn except where an alternate unit Is presented to the right of the result,
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/04/2024 05:18 PM without the written consent of Pace Analytical Services, LLC.
Page 22 of 29

�ce"
QUALITY CONTROL DATA
Project: LAND APPLICATION
Pace Project No.: 92703642
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)B75-9092
QC Batch: 637214 Analysis Method: EPA9014
OC Batch Method: SW-846 7.3.3.2 Analysis Description: 733C Reactive Cyanide
Laboratory: Pace Analytical Services - Greensburg
Associated Lab Samples: 92703642001, 92703642002
METHOD BLANK: 3107836 Matrix: Solid
Associated Lab Samples: 92703642001, 92703642002
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Cyanide, Reactive mg/kg ND 1.0 12/20/23 16:10
LABORATORY CONTROL SAMPLE: 3107837
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Cyanide, Reactive mg/kg 99.6 7.2J 7 0-8
SAMPLE DUPLICATE: 3107838
40272282001 Dup
Parameter Units Result Result RPD Qualifiers
Cyanide, Reactive mg/kg <0.47 ND
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/04/2024 05:18 PM without the written consent of Pace Analytical Services, LLC.
Page 23 of 29

ace"
QUALITY CONTROL DATA
Project: LAND APPLICATION
Pace Project No.: 92703642
Pace Analytical Services, LLC
9800 Kincey Ave. Suite100
Huntersville, NC 28078
[phone]
QC Batch: 637210 Analysis Method: SM 4500-S2-F-2011
QC Batch Method: SW-846 7.3.4.2 Analysis Description: 734S Reactive Sulfide
Laboratory: Pace Analytical Services - Greensburg
Associated Lab Samples: 92703642001, 92703642002
METHOD BLANK: 3107832 Matrix: Solid
Associated Lab Samples: 92703642001, 92703642002
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Sulfide, Reactive mglkg ND 10.0 12/20/23 16:10
LABORATORY CONTROL SAMPLE: 3107833
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Sulfide, Reactive mg/kg 200 80.3 40 0-52
SAMPLE DUPLICATE: 3107834
40272282001 Dup
Parameter Units Result Result RPD Qualifiers
Sulfide, Reactive mg/kg <11.8 ND
Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result,
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/04/2024 05:18 PM without the written consent of Pace Analytical Services, LLC. Page 24 of 29

Pace Analytical Services, LLC
(-�Fac
9800 Kince Ave. Suite 100
em Huntesville, NC 28078
[phone]
QUALIFIERS
Project: LAND APPLICATION
Pace Project No.: 92703642
DEFINITIONS
OF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MIX -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether,
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis ofAcrolein and Acrylonitdle by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNi accredited. Contact your Pace PM for the current list of accredited analytes.
TN -The NELAC Institute.
SAMPLE QUALIFIERS
Sample: 92703642002
(1] Chlorinated Acid Herbicides (GC) by Method 8151A - Surrogate failure due to matrix interference
ANALYTE QUALIFIERS
D3 Sample was diluted due to the presence of high levels of non -target analytes or other matrix interference.
D6 The precision between the sample and sample duplicate exceeded laboratory control limits.
E Analyte concentration exceeded the calibration range. The reported result is estimated.
H3 Sample was received or analysis requested beyond the recognized method holding time.
LO Analyte recovery in the laboratory control sample (LCS) was outside QC limits.
M1 Matrix spike recovery exceeded QC limits, Batch accepted based on laboratory control sample (LCS) recovery.
MH Matrix spike recovery and/or matrix spike duplicate recovery was above laboratory control limits. Result may be biased
high.
P9 RPD between the primary and confirmatory analysis exceeded 40%.
Ri RPD value was outside control limits.
ST Surrogate recovery was above laboratory control limits. Results may be biased high.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/04/2024 05:18 PM without the written consent of Pace Analytical Services, PLC. Page 25 of 29

Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: LAND APPLICATION
Pace Project No.: 92703642
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Analytical
Batch
92703642001
WWTP CAKE
B151A
2194445
EPA8151A
2194445
92703642002
WTP CAKE
8151A
2194445
EPA 8151A
2194445
92703642001
WWTP CAKE
EPA3510C
820096
EPA808113
820175
92703642002
WTP CAKE
EPA 3510C
820096
EPA 8081 B
820175
92703642001
WWTP CAKE
EPA 3510C
820097
EPA 8082A
820176
92703642002
WTP CAKE
EPA 3510C
820097
EPA 8082A
820176
92703642001
WWTP CAKE
EPA3010A
822245
EPA6010D
822365
92703642002
WTP CAKE
EPA 3010A
822245
EPA 6010D
822365
92703642001
WWTP CAKE
EPA 7470A
821958
EPA 7470A
822220
92703642002
WTP CAKE
EPA 7470A
821958
EPA 7470A
822220
92703642001
WWTP CAKE
EPA 351 DC
820095
EPA 8270E
820164
92703642002
WTP CAKE
EPA 3510C
820095
EPA 8270E
820164
92703642001
WWTP CAKE
EPA 82600
819921
92703642002
WTP CAKE
EPA 8260D
819921
92703642001
WWTP CAKE
SM 25400-2015
536715
92703642002
WTP CAKE
SM 2540G-2015
536715
92703642001
WWTP CAKE
EPA 1010B
821865
92703642002
WTP CAKE
EPA 1010B
821865
92703642001
WWTP CAKE
EPA 9045D
821569
92703642002
WTP CAKE
EPA 9045D
821569
92703642001
WWTP CAKE
SW-846 7.3.3.2
637214
EPA 9014
637506
92703642002
WTP CAKE
SW-846 7,3.3.2
637214
EPA 9014
637506
92703642001
WWTP CAKE
SW-846 7.3.4.2
637210
SM 4500-S2-F-2011
637511
92703642002
WTP CAKE
SW-846 7.3.4.2
637210
SM 4500-S2-F-2011
637511
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/04/2024 05:18 PM without the written consent of Pace Analytical Services, LLC. Page 26 of 29

DC#_Title: ENV-FRM-HUN1-0083 v03_Sample Condition Upon Receipt
ace
Effective Date: 11/2.9/2023 4:16:30 PM
Laboratory receiving samples: If
Asheville ❑ Eden❑ Greenwood ❑ Huntersville El Raleigh❑ Mechanicsville❑ Atlanta❑ Kernersville❑
Sample Client Name: r
Upon • Receipt'_, , , Project #., WO# : 92703642
L I �'�` �i� � �! in I'i} ZJ 1111111111111111111
Courier Fed Ex uP5 USPs ClientIII
Commercial ❑ Pace ❑ Other: 92
r
42
Custody Seal Present? ❑ Yes `° No Seals Intact? ❑ Yes ❑ No ❑ N/A
li
Packing Material: ❑ Bubble wrap ❑ Bubble Bags ❑ None ❑ Other
Thermometer:
Datelinitials Person Examining Contents:
Biological Tissue Frozen?
❑ Yes ❑ No ❑ N/A
El IR Gun ID: G (� j` Type of Ice: ❑ Wet ❑ Blue ❑ None
�1 (� Correction Factor.
Cooler Temp: r u Add/Subtract ('C) !.: , E Temp should be above freezing to WC
❑ Samples out of temp criteria. Samples on ice, cooling process
Cooler Temp Corrected ('C): has begun
USDA Regulated Soil (❑ N/A, water sample)
Did samples originate in a,quarantine zone within the United States: CA. NY, or SC Did samples originate from a foreign source (inteationaily,
lcheck mansl? i7i Va. 11to Rcn Nn includinu Hawaii and Pueril? f-1Vat ; run
Comments/Discrepancy:
Chain of Custody Present?
❑Yes
[3 No
3N/A
1.
Samples Arrived within Hold Time?
tJ Yes
❑ No
❑ N/A
2.
Short Hold Time Analysis (02 hr.)?
❑ Yes
0 No
El N/A
3.
Rush Turn Around Time Requested?
oyes
dNO
❑NIA
4,
Sufficient Volume?
❑ No
❑ WA
S.
Correct Containers Used?
-Pace Containers Used?
�dies
LJ Yes
❑ Ye5
❑ Nv
❑ No
❑ NIA
❑ NIA
6.
Containers Intact?
❑ Yes
❑ No
❑ N/A
7.
Dissolved analysis: 5amples Field Filtered?
❑Yes
❑No
[I NIA
B.
Sample Labels Match C00
-Includes Date/Time/lD/Analysis Matrix:
❑Yes
El No
❑N/A
9.
Headspace in VOA Vials t>5-6mml?
❑Yei
❑ No
(3 N/A
10.
Trip Blank Present?
Trip Blank Custody Seals Present?
❑Ycs
❑Yes
❑ No
❑ No
❑N/A
d N/A
11.
COMMENTS/SAMPLE DISCREPANCY
CLIENT NOTIFICATION/RESOLLMON
Person contacted:
Project Manager SCURF Review:
Project Manager SRF Review:
Lot ID of split containers:
Date/Time:
Date:
Date:
Field Data Required? LJYes LJ No
Qualtrax ID:69614 Paae 1 of 2
Page 27 of 29

Effective Hate: 11/14/2022
"Check mark top half of box if pH and/or dechiorination is verified and
within the acceptance range for preservation samples.
Emeovans: VOA, CoGforrn. TOC.Oil and Grease, DRO/801S (water) DOC. LLHC
"Bottom half of box is to list number of bottles
"'Cheek all unpreserved Nitrates for chlorine
Project # WO# : 92703642
PM: TIH Due [late: 12/28/23
CLIENT: 92-CityofMon
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pH Adjustment Log for Preserved Samples
Type of PreServ8li,.e pH upon raceipt Dale preservation adjusted Time preservauen
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amauntofPreservative tot
added
Note whene•,er there rs a discrepancy affectind Nortn Carolina con;pliancc s-11�ples. a copy of th,s lorm will be tent to the rtort4 Carolina DENR Cert,fitauon Office (r e
Out of hold. ineo!rett preseriaLive, out rl ;emp• rncorrec[ :anla.ner5.
Qualtrax ID. 69614 Page 2 of 2
Page 28 of 29

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ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
City of Monroe Total Dry Tons Applied (Annual):
WQ0001346 Cation Exchange Capacity (non 503 only):
Calvin Morris Owner: Same Predominant Soil Series:
11.6 Acres Permitted:
11.6 Site #: NC-AN-19
31.19
N/A
GoB-Goldston
Field #: 1
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kIZ, % Solids use Raw Percent #):
Com- —
posite
Date
I R
OEM
mammon
a
t all
Total
Phos-
-phorusEMEMENEENEEN
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
o©©
o©
ENE
0
0
o
o
_••
M
on
Event
NO M.
1 111
1 1':
Ely, ffily
1 11•
1 11•
•®
®®®®®®®®®®®®®
1111
1 111
1 111
1 111
1i1
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1 111
1111
1 111
1 1i1
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1 111
!11
1 111
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1 111
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1 !11
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1 111
1 111
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1 111
1 111
111
1 111
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1 11!
! 111
WIN 1
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1 111
1 111
1 111
1 111
1 111
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certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Signature of Land Applier
Date
DENR FORM MFLSF (12/2006)

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ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: City of Monroe Total Dry Tons Applied (Annual):
Permit #: WQ0001346 Cation Exchange Capacity (non 503 only):
Operator: Ben Myers Owner: Same Predominant Soil Series:
Acres Used: 44.6 Acres Permitted: 44.6 Site #: NC-UN18 Field #:
116.32
N/A
BdB2-Badin
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent ft
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Date
Emma
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M
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. Total
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1 111
1 111
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! 111
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"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
KPIA, r4 01�
Signature of Land Applier
Date
DENR FORM MFLSF (12/2006)

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ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
City of Monroe Total Dry Tons Applied (Annual):
WQ0001346 Cation Exchange Capacity (non 503 only):
Ben Myers Owner: Same Predominant Soil Series
27.6 Acres Permitted:
27.6
Site #: NC-UN18 Field #:
132.81
NIA
GoB-Golston
2
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample or
Com-
posite
Date
Ll J
_2j
3
4
4/3123
5j
4/3/23
L6J
7
7/5/23
L8J
819123
9
10
11
12
% Solids
1 14.7
25.3
31.7
18
Arsenic
891
22.5
21.5
9.39
Cadmium
1.1
3.95
16
1.21
Copper
320
423
385
342
Chromium
55.3
248
207
60
Lead
19.5
11.9
7.82
22.6
Mercury
1.14
0.684
0.549
0.972
Molyb-
denum
14.4
45.8
42.3
13.8
Nickel
67.6
35
52.1
70.6
Selenium
5.89
19.8
7.89
7
Zinc
1080
63.6
47.6
1210
Total
Phos-
horus
21200
3350
2770
22900
Annual Heavy Metal Field Loadings (Calculated in lbslacre):
Total
1
2
3
4
5
6
7
8
9
10
11
i 2
DT/Ac./
o
App-
rt
14
Event
1.94
0.70
0.70
1.48
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0,000
0.000
0.000 1
0.035
0.031
0.000 10.030
0.028
0.000
0.000
1 0.000
0.000
1 0.124
Cadmium
0.000
0.000
0.000
0.004
0.005
0.000
0A22
1 0.004
0.000
0.000
0.000
0.000
0.036
Copper
0.000
0.000
0.000
1.240
0.588
0.000
0.536
1 1.014
0.000
0.000
0.000
0.000
3.379
Chromium
0.000
0.000
0.000
0.214
0.345
0.000
0.288
0.178
0.000
0.000
0.000
0.000
1.025
Lead
0.000
0.000
0.000
0.076
0.017
0.000
0.011
0.067
0.000
0.000
0.000
0.000
0.170
Mercury
0.000
0.000
0.000
0.004
0.001
0.000
0.001
0.003
0.000
0.000
0.000
0.000
0.009
MoIyb-
denum
0 000
0.000
0.000
0.056
0.064
0.000
0.059
0.041
0.000
0.000
0.000
0.000
0.219
Nickel
0.000
0.000
0.000
0.262
0.049
0.000
0.073
0.209
0.000
0.000
0.000
0.000
0.593
Selenium
0.000
0.000
0.000
0.023
0.028
0.000
0.011
0.021
0.000
0.000
0.000
0.000
0.082
Zinc
0.000
0.000
0.000
4.186
0.088
0.000
0.066
3.589
0.000 1
0.000
0.000
0.000
7.930
Total
Phos-
0.000
0.000
0.000
82.171
4.657
0.000
3.856
67.921
0.000
0.000
0.000
0.000
158.60
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Signature of Land Applier
-I I -.,Ly
Date
DENR FORM MFLSF (12/2006)

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ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
City of Monroe Total Dry Tons Applied (Annual):
WQ0001346 Cation Exchange Capacity (non 503 only):
Ben Myers
5.7
Owner: Same Predominant Soil Series
Acres Permitted: 5.7 Site #: NC-UN18 Field #:
20.42
NIA
CmB-Cid
7
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
- R6K1
Com-
••
Date
non
NOME
E
Non
Total
' •
• .
ll
1
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
..l
oEmmaMENWOUNN
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mmons
1 111
1 !11
l 111
1 1 :
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1 Ill
1 111
1 111
1 111
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1 lli
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1 i11
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1 lil
1 111
! 111
! i':
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i lil
1 il!
1 111
1 111
1 111
! !ll
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' .
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1 Ill
1 Ill
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! 111
1 Ili
1 111
l 1i1
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1 ill
l 1ii
' i'
• •
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Kil, m
Signature of Land Applier
a- )a-a-e/
Date
DENR FORM MFLSF (1212006)

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ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
City of Monroe
WQ0001346
Operator: Ben Myers Owner:
Acres Used: 16 Acres Permitted:
Total Dry Tons Applied (Annual): 78.62
Cation Exchange Capacity (non 503 only): N/A
Same Predominant Soil Series: CmB-Cid
16 Site #: NC-UN18 Field #: 8
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Com-
posite
Date
.___®-____
loll
�_-_�_____
Total
Phos-
phorus
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
TotalW
-
©
©
E
©
App.
Event
1111
1111
1lli
11.
llll
11l1
1111
!!11
1111
1!
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1111
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1lli
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1111
1111
1111
!11
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14 !
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1 lil
! lil
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1 ill
1 ill
! 111
1 Ili
1 ill
1
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1 41!
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1 11!
1 1i1
1 111
�
1 111
1 111
1 li!
1 111
1 ill
! 1 �
1 114
! 111
1 .'
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1 111
1 ill
1 111
1 li.
1 !11
1 lil
111!
1 111
! ill
1 11
1 ill
1 111
1 1
1 lil
! !11
1 111
1 11
i 1i1
! 11i
i 111
1 li!
1 111
1 1�
1 1i!
1 I11
1
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1 111
1 �••
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!Ili
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! lil
1 111
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1 li!
1 lli
1 !�
! 111
1 111
1 lil
1 1�
1 li!
1 ill
!ill
1 ill
1 411
1 ! .
1 lit
1 111
1 1
Total
' .
1 !li
i 111
1 114
�. '
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1 111
1 Ili
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imprisonment for knowing violations".
A -VI, M
Signature of Land Applier
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D E N R FORM MFLSF (12/2006)

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ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
City of Monroe Total Dry Tons Applied (Annual):
WQ0003146 Cation Exchange Capacity (non 503 only):
William Griffin Owner: Same Predominant Soil Series:
24.5 Acres Permitted:
24.5 Site #: NC-UN29
64.63
NIA
GoC-Goiston
Field #: 1
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Com-
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NE
MENOMONEE.
TotalDate
• +
..
11
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
1 Irl
! 1!1
1 111
1 11•
1 Ilr
1 Irl
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1 certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
V"A-�—
Signature of Land Applier
a -la: -ay
Date
DENR FORM MFLSF (12/2006)

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ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: City of Monroe Total Dry Tons Applied (Annual):
Permit #: WQ0001346 Cation Exchange Capacity (non 503 only):
Operator: William Griffin Owner: Same Predominant Soil Series:
Acres Used: 5.7 Acres Permitted: 5.7 Site #: NC-UN29 Field #:
20.91
NIA
GoC-Galdston
2
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
positeEMPUPON
Com-
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MEOW
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Total
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!•!1
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Total
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FRO M.
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"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
4� m
Signature of Land Applier
a-ra-a�
Date
DENR FORM MFLSF (12/2006)

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ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
City of Monroe Total Dry Tons Applied (Annual):
WQ0001346 Cation Exchange Capacity (non 503 only):
William Griffin
7.4
Owner: Same Predominant Soil Series:
Acres Permitted: 7.4 Site #: NC-LTN29 Field #:
41.06
NIA
BaB-Badin
3
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Com-
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Date
OEM
MENUMMEM0,300
Total
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TotalW
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"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
&6,_ M��•
Signature of Land Applier
a-ra�a�
Date
DENR FORM MFLSF (12/2006)

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ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
City of Monroe
WQ0001346
Operator: William Griffin Owner:
Acres Used: 2.9 Acres Permitted:
Total Dry Tons Applied (Annual): 8.29
Cation Exchange Capacity (non 503 only): NIA
Same Predominant Soil Series: BdB2-Badin
2.9 Site #: NC-UN29 Field #: 4
Residual Analysis Data (Heavy Metals and Total Phosphorus use mgtkg, % Solids use Raw Percent #):
..
Com-
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Date -
N
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©
EMEND
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Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
BOWEN
rMENEM
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1 111
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1 1
1 1.1
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l lil
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1 111
1 111
1 111
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"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Signature of Land Applier
-f 2-- ay
Date
DENR FORM MFLSF (12/2006)

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ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
City of Monroe
WQ0001346
Operator: William Griffin Owner:
Acres Used: 2.2 Acres Permitted:
Total Dry Tons Applied (Annual): 8.69
Cation Exchange Capacity (non 503 only): NIA
Same Predominant Soil Series: GoC-Goldston
2.2 Site #: NC-UN29 Field #: 5
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
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Date
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I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Signature of Land Applier
�-1a-ay
Date
DENR FORM MFLSF (12/2006)

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ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
City of Monroe Total Dry Tons Applied (Annual): 39.23
WQ0001346 Cation Exchange Capacity (non 503 only): N/A
Tom Appenzeller Owner: William Griffin Predominant Soil Series: BdB2-Badin
13.1 Acres Permitted: 13.1 Site #: NC-UN30 Field #: I
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
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with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
XeAl,, I✓l�
Signature of Land Applier
Date
DENR FORM MFLSF (12/2006)

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ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: City of Monroe Total Dry Tons Applied (Annual):
Permit #: WQ0001346 Cation Exchange Capacity (non 503 only):
Operator: Tom Appenzeller Owner:
Acres Used: 11.9 Acres Permitted:
Same
11.9 Site #:
Predominant Soil Series:
NC-UN30 Field #:
59.40
NIA
BaB-Badin
2
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Com-
posite
Date
Non
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"1 certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
M "- ,
Signature of Land Applier
-l9L-P-y
Date
D E N R FORM MFLSF (12/2006)

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ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: City of Monroe Total Dry Tons Applied (Annual): 44.93
Permit #: WQ0001346 Cation Exchange Capacity (non 503 only): N/A
Operator: Tom AppenzelIer Owner: Same Predominant Soil Series: BaB-Badin
Acres Used: 15.2 Acres Permitted: 15.2 Site #: NC-UN30 Field #: 4
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
• - .
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"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Signature of Land Applier
a-ja-aq
Date
DENR FORM MFLSF (12/2006)

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ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
City of Monroe
WQ0001346
Tom Appenzeller Owner:
10.8 Acres Permitted:
Total Dry Tons Applied (Annual):
Cation Exchange Capacity (non 503 only):
Same Predominant Soil Series:
10.8 Site #: NC-UN30 Field #:
42.70
NIA
BaB-Badin
5
Residual Analysis Data (Heavy Metals and Total Phosohorus use mpz/ke. % Solids use Raw Percent #):
Com-
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"1 certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
..?-i P-a'/
Signature of Land Applier
Date
❑ENR FORM MFLSF (12/2006)

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ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
City of Monroe
WQ0001346
Operator: Henry Myers Owner:
Acres Used: 2.5 Acres Permitted:
Total Dry Tons Applied (Annual):
Cation Exchange Capacity (non 503 only):
Same Predominant Soil Series:
2.5 Site #: NC-UN31 Field #:
6.73
N/A
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I am aware that there are significant penalties for submitting false information, including the possibility of flues and
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a -)a -ay
Date
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ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: City of Monroe Total Dry Tons Applied (Annual): 8.97
Permit #: WQ0001346 Cation Exchange Capacity (non 503 only): NIA
Operator: Henry Myers Owner:
Acres Used: 4.7 Acres Permitted:
4.7
Same Predominant Soil Series: BdB2-Badin
Site #: NC-LIN31 Field #:
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg,mg/kg, % Solids use Raw Percent #):
. .-.
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"1 certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Signature of Land AppIier
Date
DENR FORM MFLSF (12/2006)

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ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: City of Monroe Total Dry Tons Applied (Annual):
Permit #: WQ0001346 Cation Exchange Capacity (non 503 only):
Operator: Henry Myers Owner: Same Predominant Soil Series:
Acres Used: 17.6 Acres Permitted: 17.6 Site #: NC-UN31 Field #:
34.02
N/A
TbT2-Tatum
5
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
om-
posite
Date
Total
Phos-
phorus.MMENEEMENEEN
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Total
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"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Signature of Land Applier
01 -I,2 -.2
Date
DENR FORM MFLSF (12/2006)

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ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: City of Monroe Total Dry Tons Applied (Annual): 15.70
Permit #: WQ0001346 Cation Exchange Capacity (non 503 only): NIA
Operator: Henry Myers Owner: Same Predominant Soil Series: ChA-Chewacla
Acres Used: 7.8 Acres Permitted: 7.8 Site #: NC-UN31 Field #: 6
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Com-
Posite
Date
NEEM
Total
Phos-
Miiiiiiiiiii
nnua eavy Metal Field Loadings (Calculated in lbs/acre):
Total
r
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Event
1!
1111
lI11
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1 111
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" I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
M c?l/,&.
Signature of Land Applier
a -is-XL/
Date
D E N R FORM MFLSF (1212006)

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ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
City of Monroe Total Dry Tons Applied (Annual):
WQ0001346 Cation Exchange Capacity (non 503 only):
Danny Baker Owner: Same Predominant Soil Series:
93.65
N/A
GsB- Golston
23.5 Acres Permitted: 23.5 Site #: NC-UN32 Field #: 1
Residual Analysis Data (Heavy Metals and Total Phosphorus use rng/kg, % Solids use Raw Percent #):
Com-
posite
Date
ME
MEOW
mom
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__-__-
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"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Signature of Land Applier
a -la -ay
Date
DENR FORM MFLSF (12/2006)

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ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: City of Monroe Total Dry Tons Applied (Annual):
Permit #: WQ0001346 Cation Exchange Capacity (non 503 only):
Operator: Danny Baker Owner:
Acres Used: 15.5 Acres Permitted:
Same Predominant Soil Series:
15.5 Site #: NC-UN32
6496
N/A
BdB2-Badin
Field #: 2
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Com-
posite
Date;.
Total
•
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M
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Totalo
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"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
,kc, M Vw,
T - -
Signature of Land Applier
Date
DENR FORM MFLSF (12/2006)

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ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: City of Monroe Total Dry Tons Applied (Annual): 8.19
Permit #: WQ0001346 Cation Exchange Capacity (non 503 only): N/A
Operator: Danny Baker Owner: Same Predominant Soil Series: GSB - Goldston
Acres Used: 3.2 Acres Permitted: 3.2 Site #: NC-UN32 Field #: 4
Residual Analvsis Data (Heavv Metals and Total Phosnhorws ice mu/ku_ 0/. Rnlirls vise Raw Prrranf ffl-
Com-
posite
, Date
won
on
B
0
013
DO
_____________
Total
Phos-
iiiiiiiMiiii
1xivnuni rieavv ivietat riem Loaatn2s (uaicuiateu in insiacreE:
•
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1 111
! !11
1 111
! 1i1
! 111
1 111
1 Iil
! 1�:
1 111
1 111
1 111
1 111
1 1�
1 111
!III
1 111
1 !11
!III
1111
! 11
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1 !II
1 I11
! 111
1 11•
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1 111
1 11!
! 111
! 111
! !11
1 1!1
1 III
! 111
111
1111
! 111
1 141
1 111
! 1
1 111
! 111
1 111
1 1i1
1 1
1 111
1 111
1 1!1
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1 111
1 1i1
1 III
1 .
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1 111
1 111
1 #!1
1 •
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11l1
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1111
1111
1!
11 1
1111
11 1
1111
it
1 III
! !II
! 111
I Ili
! I11
1 1!!
1 111
1 1 .
! 111
!III
! 11!
1 1i1
1 1 •
Total
•
1 !11
1111
! 11!
1 111
1 11!
1 111
1 111
•
1 III
1 I11
1 111
1 !!1
. .
I certify, unaer penaity of iaw, tnat ims aocument was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
a -+a -ay
Signature of Land Applier Date
DENR FORM MFLSF (12/2006)

SECTION
I

Van Kleek equation
In (RAS) - Out (dige
In (RAS) - (In * Out)
Volatile Solids Reduction 2023
sl
L—
sludge) _
1st Quarter
RAS digested sludge
IN - OUT
0.7800 0.6470 0.133
IN- (IN -OUT)
0.78 0.50466 0.27534
2nd Quarter
IN -
OUT
0.7770
0.6520 0.125
lReduction
IN-
(IN -OUT)
I 46.230
0.777
0.506604 0.270396
3rd Quarter
IN- OUT
0.7320 0.7230 0.009 Reduction
IN- (IN -OUT) I 4.44%
0.732 0.529236 0.202764
IN-
OUT
0.7380
0.6210 0.117
lReduction
IN-
(IN -OUT)
I 41.83-
0.738
0.458298 0.279702
4th Quarter
IN- OUT
0.6980 0.6230 0.075 Reduction
IN- (IN -OUT) 1 28.50%
0.698 0.434854 0.263146
IN- OUT
0.754 0.6160 0.138 Reduction
IN- (IN -OUT) 1 47.66961
0.754 0.464464 0.289536

PA&F;Z
PROM PT -ACCURATE- RELIABLE
LABORATORIES, INC
W WW.PARLABS.COM
REPORT OF ANALYSES
Ak4:n: KEN MORRIS
CITY OF MONROE WASTEWATERPLANT PROJECT NAME: JAN 23
PO BOX 69 DATE: 03/07/23
MONROE, NC 28111-
SAMPLE NUMBER-
146245 SAMPLE ID- MONROE
WWTP
SAMPLE MATRIX- WW
DATE SAMPLED-
01/17/23
TIME SAMPLED- 1012
DATE RECEIVED-
01/17/23 SAMPLER- KM
RECEIVED BY- DJ
TIME RECEIVED-
1210 DELIVERED BY- KM
TYPE SAMPLE- Grab
Page 1 of 1
ANALYSIS
ANALYSIS
METHOD
DATE TIME BY
RESULT UNITS
FECAL COLIFORM
(GEOM. MEAN) SM 9221 E
01/17/23 1600 RE
46,939 MPN/9
LABORATORY DIRECTOR ;_ '� 41 L f ?�77'
2217 Graham Park Drive • Charlotte, NC 28273
Phone: [phone] - Fax: [phone]

PA&FZ
PROMPT•ACOU RATE- RELIA@4c
LABORA-rORIRS, INC
2217 Graham Park Drive
PO Box 411483
Charlotte, NC 28241-1483
NC Cert # 2Q; SC Cert # 99003001
CITY OF MONROE
MONROE WWTP
+ • 01/17/23
FECAL COLIFORM, GEOMETRIC MEAN
ROM. + SM 9221 E
rWIUSIS I.,
146245
1
21,517
19.89%
108,206.14
2
8,848
24.96%
35,449.77
3
9,459
24.58%
38,487.96
4
10,623
23.20%
45,788.19
5
9,674
25.00%
38,696.34
6
9,955
24.33%
40,915.56
7
10,395
22.16%
46,909.68
Fecal Coliform
Geometric Mean= • • '

[;��R
CHAIN OF CL/STODY
RIEPAR Laboratories, Inc
Phone [phone]
Fax [phone]
www.part4bs.com
Shippi7r: Mailing:
2217 Graham Park orive PO Sax 411483
Charlotte, NC 28273 Charlotte, NC 28241-1483
fa Menflal that ari informaDon be recarded an thJs Chain of Cu3iodv document tot acceoffnee by W Laboretwits, kK, and the N""
CaraFiny Orner[n+rnt ar &-ironmerral and Natural Rasavrc". '
ny dame (billing) Comments! 5 aisl Iruttl;
City of Monroe
PO Box 69
Crty State 8, zip coda
Mcuroe, NC 28111
Point of COwdem & T akphoFm
503 B14SOLIDS
REPORTING
MM4
... r
-Sample Taken 8y: o
IS THIS FOR STATE or EPA REPO TING? YEs JL No
*Sample type: DW WW-X GWMW _ HW Soil _ other
Sample Temp at time of sa pling: 11 .3 tlC Sampis_ Temp upon receipt:
Preserved: Yes — No Teflon liner/ Zero Headspece' Yes .,._. No `1+11A
Client Sertlpie I.U.
Sam le Location / Number
Comp
Grab
x
Presery.
NONE
Set Up
Date / Time
� —?
Collection
Date / Time
Analym kequested
FECAL COLIFORM
0 1 WwTP
4 2 W WTF
x
x
NONE
NONE
l
�'
r o - I2
FECAL COLMORM
FECAL COLMORM
-
H 3 WW-lTp
94 WwTP W
X
NONE:
1_ J 7 -.�3
1 U: 13
FECAL COLIFORM
4 S wwn
x
NONE
1 - i 7" 23
/ o : 13
FECAL COLIFORM
4 6 WWTP
X
NONE
! - I -1- a3
r
FECAL COLMORM
# 2 wwrP
x
NONE
1 _ I-�-a3
r �'
FECAL COLIFORM
;(elinqui,hed by: Dme/iime Rece'
M 1-17-23/iol'l
3erlinquishe4 by:
Date/Time Received
DawtalTuna
De teii'uT1e
C f Composite G-C-rab DW=Drinking Water WW-Wastewater GWMW-Groundwatar Monitoring Well HIN-Harardom Waste
See C"er side

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Monroe
WWTP Name: WWTP cake
WQ Permit Number: WQ0001346
NPDES Number: NCO024333
Monitoring Period: From 1/l/2023 To 3/31/2023
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. A (time/temp) ❑
1 Alt B (Alk Treatment) ❑
Alt. C (Prior Testing) ❑
A1t.D (No Prior Test) ❑
Process to Further Reduce Pathogengs ❑
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost ❑
Heat Drying ❑
Heat Treatment ❑
Thermophilic ❑
Beta Ray ❑
Gamma Ra ❑
Pasteurization ❑
Class B:
JAII. (1) Fecal Density ✓❑
Alt. (2) Process to Significantly Reduce Pathogens ❑
If applicable to alternative performed (Class
B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization ❑
Air Drying ❑
Composting ❑
Aerobic Digestion r❑
Anaerobic Digestion ❑
If applicable to alternative performed (Class A or Class B) complete the
following monitoring data:
Parameter
Allowable Level
in Sludge
Pathogen Density
Number o
Excee-
Frequency
of Analencesysis
Sample
Type
Analytical
Tech -
niaue
inimu
Geo. Mean
Maximum
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
35,449.77
46,939
108,206.14
MPN/g
0
quarterly
grab
sm9221 e
CFU
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
(in lieu of fecal
coliform) I
3 MAN per grams
total solid (dry
weight)
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed:
Alt.I (VS reduction) 0
Alt. 2 (40-day bench) ❑
Alt. 3 (30-day bench) ❑
Alt. 4 (Spec. 02 uptake) ❑
Alt. 5 (14-Day Aerobic) ❑
Alt. 6 (Alk. Stabilization ❑
Alt 7 (Drying - Stable) ❑
I Alt. 8 (Drying - Unstable) ❑
Alt. 9 (Injection) ❑
Alt. 10 (Incorporation) ❑
No vector attraction reduction alternatives were performed ❑
CERTIFICATION STATEMENT (please check the appropriate statement)
0 "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T 1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if
you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Kyle Ketchum, WWTP Superintendent
Preparer Name and Title (type or print)
Ken Morris, Residuals Coordinator
Land Applier Name and Title (if applicable)(type or print)
Signature of Preparer* Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 5039(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 02T (1212006)

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (503 Rules)
Facility Name: City of Monroe
WWTP Name: Monroe WWTP cake
WQ Permit Number: WQ0001346
NPDES Number: NCO024333
Monitoring Period: From 1/1/2023 To 3/3I/2023
Pathogen Reduction (40 CFR 503.32) - Please indicate level achieved and alternative performed:
Class A:
Alternative 1 ❑
Alternative 2 ❑
Alternative 3 ❑
Alternative 4 ElAlternative
5 ❑
Alta -native 6 ❑
If applicable to alternative
performed Class A only) indicate "Process to Further Reduce Pathogens":
Compost ❑
Heat Drying ❑
Heat Treatment ❑
Thermophilic ❑
Beta Ray ❑
Gamma Ray ❑
Pasteurization ❑
Class B:
Alternative 121
Alternative 2 ❑
If applicable to alternative
performed (Class B only) indicate "Process to Significantly
Reduce Pathogens":
Lime Stabilization ❑
Air Dryin ❑
CoMpostinE ❑ jAerobic Digestion R1
Anaerobic Digestion ❑
If applicable to alternative performed (Class A or Class B) complete the following monitoring data:
Parameter
Allowable Level
in Sludge
Pathogen Density
Number ot
Excee-
dences
Frequency
of Analysis
Sample
Type
Analytical
Tech -
i aue
Minimurn
Geo. Mean
Maximuml
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
35,449.77
46,939
108,206.14
MGN/g
0
quarterly
grab
sm9221e
CFU
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per4 grams
total solid (dry
weight)
Vector Attraction Reduction (40 CFR 503.33) - Please indicate option performed:
Alt.l (VS reduction)
R1
Alt. 2 (40-day bench)
❑
Alt. 3 (30-day bench) ❑
Alt. 4 (Spec. 02 uptake)
❑
Alt. 5 (14-Day Aerobic)
❑
Alt. 6 (Alk. Stabilization
❑
Alt 7 (Drying - Stable) ❑
Alt. 8 (Drying - Unstable)
❑
Alt. 9 (Injection)
❑
Alt. 10 (Incorporation)
❑
No vector attraction reduction alternatives were performed
❑
CERTIFICATION STATEMENT (please check the appropriate statement)
0 "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector
attraction reduction requirement in 40 CFR 503.33 have been met."
❑ "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector
attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check
this statement attach an explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Kyle Ketchum, WWTP Superintendent Ken Morris, Residuals Coordinator
Preparer Name and Title (type or print) Land Applier Name and Title (if applicable)(type or print)
lik I� ao)yerRA.• M.JA So g-I q-ac/
Signature of Preparer* Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 5039(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 503 (12/2006)

PR©MNT•ACCLJ 7E• RELkARLE
LABORATORIES, INC
WWWPARLABS.COM
Attn: KEN MORRIS
CITY OF MONROE WASTEWATERPLANT PROJECT NAME: APR 23
PO BOX 69 DATE: 04/19/23
MONROE, NC 28111-
SAMPLE NUMBER- 146872 SAMPLE ID- MONROE WWTP SAMPLE MATRIX- WW
DATE SAMPLED- 04/03/23 TIME SAMPLED- 0955
DATE RECEIVED- 04/03/23 SAMPLER- KM RECEIVED BY-- DJ
TIME RECEIVED- 1115 DELIVERED BY- KM TYPE SAMPLE- Grab
Page 1 of 1
ANALYSIS
ANALYSIS METHOD DATE TIME BY RESULT UNITS
FECAL COLIFORM (GEOM. MEAN) SM 9221 E 04/03/23 1650 RE 45,237 MPN/g
LABORATORY DIRECTOR
2217 Graham Park Drive • Charlotte, NC 28273
Phone: [phone] • Fa,\: [phone]

F A.FZ
A6l,.E
LAHORA-rC IRLES, 'lNC
2217 Graham Park Drive
PO Box 411483
Charlotte, NC 28241-1483
NC Cert # 20; SC Cert # 99003001
CITY OF MONROE
MONROE WWTP
7 . 04/03123
FECAL COLIFORM, GEOMETRIC MEAN
SM 9221 E
146872
Fecal Coliform
Geometric Mean=
1
8,335
16.12%
51,709.39
2
5,537
15.93%
34 763.07
3
7,593
16.21 %
46,828.35
4
8,288
16.30%
50, 849.06
5
7,535
16.11 %
46,772.09
6
7,583
16.18%
46,868.31
7 1
6,627 1
16.04%
41,314.20

XPAR CHAIN OF CUSTOD Y
L4SGRnTORIES.lNC. PAR Laboratories, Inc
Phone [phone]
Fax f704) 588-8335
www-parlabs-tom
Shippinc: mailing:
2217 Graham Park Drive PO Box 411463
Charlotte, NC 28273 Charlotte, NC 28241-1483
`k IA G3scnt:al That or) inrormation be recorded an;his Chain v7 Custody document for acccptancc by PAR LaporatoriCS. InC. and itm North
__ t.�roiina D•oertment oS Environmental and Natural Resources.
Ccmpeny ' Name wiling) City afMotuve Comments/ Special Inst
Addresa
PO Box 69
i City. 5Ca;a $ zip code
Monroe :LC 28111
kiMQ rr.S QMOV'ro.-. A4. t
503 BIOSOLIDS
REPORTING
Sample Taken By: 14le^4 Ir YrL '
iS-THIS FOR STATE or EPA REPO TING? YES NO
tSampie type-- DW WWX GWMW _ HW _ Soil _ other
Sample Temp at time of sampling: jfa i oC Sample Temp upon receipt: _ �r
"I Preserved: Yes _ No X Teflon Liner/ Zero Headspace: Yes No T IVIA X
Clicnllfsample E.U.
! Sam R le Location / Number
Comp
Grab
Preserv.
Set Up
Date / Time
Collectio:p
Date I Time
Anulyes Rcquosted
1 W
X
NONE
-3-
�: �S
FECAL COLIFORM
i_' 2 WWTP
X
X
NONE
NONE
_ 3 �� 3
.�cs
r
FECAL COLIFORM
FECAL COLIFORM
-
H 3
-� -
4 4 WWI TP ' -
X
NONL
:5�
FECAL COLIFORM
9 5 W1av i P
X
NONE
r a_ 3
FECAL COLIFORM
# 6 p
X
NONE
�. .a�
9 %
FECAL COLIFORM
# w
X
NONE
q--S •r� 3
q 1 7
FECAL COLIFORM
by-
ielinquished by:
Daterrime
'-;3I it:
Received by:
Datemrm
_0 q-W - -'-? II
Datefrutta
u - Car,poshe G -Grab r7W=Drinking VVa ter WW = Wastewater GWMW =Groundwater Monitoring Well HIN—Hazardous Wastes
See Other Side •

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Monroe WQ Permit Number:
WWTP Name: WWTP cake NPDFS Number:
Monitoring Period: From 4/1/2023 To 6/30/2023
WQ0001346
NCO024333
Alt. I (VS reduction)
r❑
Alt. 2 (40-day bench) ❑
Alt. 3 (30-day bench) ❑
Alt. 4 (Spec. Oz uptake)
❑
Alt. 5 (14-Day Aerobic)
❑
Alt. 6 (Alk. Stabilization ❑
Alt 7 (Drying - Stable) ❑
Alt. 8 (Drying - Unstable)
❑
Alt. 9 (Injection)
❑
Alt. 10 (Incorporation) ❑
No vector attraction reduction alternatives
were performed
❑
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note
if you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Kyle Ketchum, WWTP Superintendent
Preparer Name and Title (type or print)
Ken Morris, Residuals Coordinator
Land Applier Name and Title (if applicable)(type or print)
I 16#- - ,?11> V �<-e,, m&Vo, a- Ia-aq
Signature of Preparer* Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 02T (1212006)

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (503 Rules)
Facility Name: City of Monroe WQ Permit Number:
WWTP Name: Monroe WWTP cake NPDES Number:
WQ0001346
NCO024333
Monitoring Period: From 4/l/2023 To 6/30/2023
Pathogen Reduction (40 CFR 503.32) - Please indicate level achieved and alternative performed:
Class A:
Alternative 1 ❑
Alternative 2 ❑
Alternative 3 ❑
Alternative 4 ❑
Alternative 5 ❑
Alternative 6 ❑
If applicable to alternative
performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost ❑
Heat Drying ❑
Heat Treatment ❑ Thermophilic ❑
Beta Ray ❑
Gamma RayElPasteurization
❑
Class B:
Alternative 1 0
T Alternative 2 ❑
If applicable to alternative
performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization ❑
Air Drying❑
Composting ❑
JAcrobic. Digestion R1
Anaerobic Digestion ❑
...
If applicable to alternative performed (Class A or Class B) complete the following monitoring data:
Parameter
Allowable Level
in Sludge
Pathogen Density
Number or
Excee-
Frequency
of Analysis
Sample
Type
Analytical
Tech -
MinimumGeo.
Mean
MaximumUnitsgnces
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
34,763.07
45,237
51,709.39
MGN/g
0
quarterly
grab
sm9221e
CFU
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
(in lieu of fecal
colifonn)
3 MPN per 4 grams
total solid (dry
weight)
Vector Attraction Reduction (40 CFR 503.33) - Please indicate option performed:
Alt.1 (VS reduction)
0
Alt. 2 (40-day bench)
❑
Alt. 3 (30-day bench) ❑
Alt. 4 (Spec. Oz uptake)
❑
Alt. 5 (14-Day Aerobic)
❑
Alt. 6 (Alk. Stabilization
❑
Alt 7 (Drying - Stable) ❑
JAIt. 8 (Drying - Unstable)
❑
Alt. 9 (Injection)
❑
AIt. 10 (Incorporation)
❑
No vector attraction reduction alternatives were performed
❑
CERTIFICATION STATEMENT (please check the appropriate statement)
I] "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector
attraction reduction requirement in 40 CFR 503.33 have been met."
❑ "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector
attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check
this statement attach an explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Kyle Ketchum, WWTP Superintendent
Preparer Name and Title (type or print)
Ken Morris, Residuals Coordinator
Land Applier Name and Title (if applicable)(type or print)
1 _ > �� ov rite+•&- a �a^ a�
Signature of Preparer* Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 503 (12/2006)

PLLF;Z
PROM PT• ACC U RATE• REL I ABLE
LABORATORIES, INC
W WWTARLABS.COM
REPORT OF ANALYSES
Attn: KEN MORRIS
CITY OF MONROE WASTEWATERPLANT PROJECT NAME: JUL 23
PO BOX 69 DATE: 08/25/23
MONROE, NC 28111-
SAMPLE NUMBER-
147568
SAMPLE ID- MONROE WWTP
SAMPLE MATRIX- WW
DATE SAMPLED-
07/05/23
TIME SAMPLED- 0955
DATE RECEIVED-
07/05/23
SAMPLER- KM
RECEIVED BY- DJ
TIME RECEIVED-
1155
DELIVERED BY- KM
TYPE SAMPLE- Grab
Page 1 of 1
ANALYSIS
ANALYSIS
METHOD DATE TIME BY
RESULT UNITS
FECAL COLIFORM (GEOM. MEAN) SM 9221 E 07/05/23 1615 RE 3,561 MPN/g
LABORATORY DIRECTOR�-
2217 Graham Park Drive • Charlotte, NC 28273
Phone: [phone] • Fax: [phone]

RAI F; Z
PRC3MPY•AC OUkATE• P KL.iABLE
LABOR-j1%: 1ORIL,S, TNC
2217 Graham Park Drive
PO Box 411483
Charlotte, NC 28241-1483
NC Cert # 20; SC Cert # 99003001
CITY OF MONROE
• MONROE WWTP
• 07/05/23
FECAL COLIFORM, GEOMETRIC MEAN
•• sM9221 E
ID
Sample #
F. Coliform
T.
SolidsLAB
147568
1
719
19.50%
3,687.56
2
681
19.85%
3,431.43
3
716
20.14%
3,556.89
4
742
19.81 %
3,747.00
5
631
20.02%
3,149.38
6
734
19.74%
3,717.30
7
724
19.68%
3,678.76
Fecal Coiiform
Geometric Mean= •

PAR CHAIN OF CUSTODY
LASCRpMMES,rnC. PAR Laboratories, Inc
Phone (704.) 588-8333
Fax [phone]
www.partab.5. corn
Shipping: Mailing.
2217 Graham Park Drive PO Sox 411463
0-adorte, NC 2S273 Charlotte, NC 28241-1483
1, is C3zcntiai that aA Information tre recorded on this Chain of Custody docvment for acceptance by 1'Wr t.aboraiorles, Inc. and the i4orth
Cur0no Devanment of emArvnmen ml and NatwW Resyurcca.
Company iViome Ibillingi _ e Comments/ Special inectr d
City Q��OIIrO
r -
Addrtsa
PO Box fig 503 BXOS0.11�5
City, SW* a xip cnda P-F- TANG
Mcnroe, NC 28111
Point of Cora m & T atephocte-,
Kean More-,5 ?z)`'+ 3(al'loJ3� Krnof�is ortrro�rtGr r
Sample Token By: ,aA� Me r Y, ,
IS THIS FOR STATE or EPA RE?Q TING? YES NO._____
*Sample type_ Dw __ WW GWMW _ HW _ Soil — other
Sample Temp at time of sa pflng: �?7I,V(; Sample Temp upon receipt:
'* Preserved: Yes _ No Teflon Linerl Zero Headspace: Yes _ NoY N1A sA
Client sample I.D.
4 Suro la 1. *mtioa / Number
Comp
Grab
Prwerv.
Set Up
Date 1 Time
Collection
Date / Time
Analyes Requostetl
N 1 WWTP
X
NONE
7-5-4
�: �,;
FECAL COLIFORM
9 2 ww-FP
X
NONE
`1: 5
FECAL COLWORM
n 3 WWTP
X
NONE
7- J.-23
R 55
FECAL COLIFORM
V, 4 wwTP - -
x
NONL
3
c� : 54
FECAL COLIFORM
# 5 W\VTP
X
NONE
7_15_a3
41: 5(-
FECAL COLIFORM
4 6 WWTP
NONE
7 s a 3
FECAL. COLTORM
# 7 WWTP
EX
NONE
7.5-.23
FECAL COLMORM
by: Datefrirne Rt?cqrvkd by: DetalTrme
3aiinquiz;h¢d by: Dateffirde Received by-. I Datafrano
4�Cornposh-C G-Crab DW=Drinking Water WW=Wastewater GWMW-Groundwatar Monitoring Weil Hi:Yahiazardom Wane
See Other Side

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Monroe WQ Permit Number: WQOOOl346
WWTP Name: WWTP cake 7-5-2023 sample NPDES Number: NC0024333
Monitoring Period: From 7/l/2023 To 9/30/2023
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. A (time/temp) ❑ Alt B (Alk Treatment)❑
Alt. C (Prior Testing)❑
AIt.D (No Prior Test) ❑
Process to Further Reduce Pathogengs Cl
If applicable to alternative
performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost ❑
Heat Drying ❑
Heat Treatment ❑
Thermophilic ❑
Beta Ray ❑
Gamma Ray ❑
Pasteurization ❑
Class B:
JAIt. (1) Fecal Density p
Alt. (2) Process to Significantly Reduce Pathogens ❑
If applicable to alternative
performed (Class
B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization ❑
Air Drying ❑
Composting ❑
Aerobic Digestion 0
Anaerobic Digestion ❑
If applicable to alternative performed (Class A or Class B) complete the followin monitoring data:
Parameter
Allowable Level
in
in Sludge
Pathogen Density
Number ot
Excee-
Frequency
of Analysis
Y
Sample
Type
Analytical
Tech -
maue
Minimum
Geo. Mean
aximu
Unitsences
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
3,149.38
3,561
3,747.00
MPN/g
0
quarterly
Grab
SM9221E
GFiT
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per 4 grams
total solid (dry
weight)
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed:
Alt.l (VS reduction) 0
Alt. 2 (40-day bench) ❑
Alt. 3 (30-day bench) ❑
1 Alt. 4 (Spec. Oz uptake) ❑
Alt. 5 (14-Day Aerobic) [I
Alt. 6 (Alk. Stabilization ❑
Alt 7 (Drying - Stable) El
JAL 8 (Drying - Unstable) ❑
Alt. 9 (Injection) ❑
Alt. 10 (Incorporation) ❑
No vector attraction reduction alternatives were performed ❑
CERTIFICATION STATEMENT (please check the appropriate statement)
0 "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note
if you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Kyle Ketchum, WWTP Superintendent
Preparer Name and Title (type or print)
Ken Morris, Residuals Coordinator
Land Applier Name and Title (if applicable)(type or print)
11Alam~ Y .2 --1 Z _d 4
Signature of Preparer* Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 5039(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 02T (12/2006)

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (503 Rules)
Facility Name: City of Monroe
WWTP Name: Monroe WWTP cake 7-5-2023 sample
WQ Permit Number: WQ0001346
NPDES Number: NCO024333
Monitoring Period: From 7/1/2023 To 9/30/2023
Pathogen Reduction (40 CFR 503.32) - Please indicate level achieved and alternative performed:
Class A:
Alternative 1 ❑ Alternative 2 ❑
Alternative 3 ❑
Alternative 4 ❑ Alternative 5 ❑
Alternative 6 ❑ ..........
If applicable to alternative
performed (Class A only) indicate "Process to Further
Reduce Pathogens":
Compost 01
Heat Drying ❑
Heat Treatment ❑
Thermophilic ❑
Beta Ray 01
Gamma Ra ❑
I Pasteurization ❑
Class B:
Alternative 1 0
Alternative 2 ❑
If applicable to alternative
performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization ❑
Air Drying❑ Composting ❑
JAerobic Digestion r❑
Anaerobic Digestion 0_.
If applicable to alternative performed (Class A or Class B) complete the following monitoring data:
Parameter
Allowable Level
in Sludge
Pathogen Density
Number o
Excee-
Frequency
of Analencesysis
Sample
Type
Analytical
Tech -
nioue
MinimumGeo.
Mean
aximu
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
IvCPN
3,149.38
3,561
3,747.00
MGN/g
0
quarterly
grab
sm9221e
CFU
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
(in lieu of fecal
coliforrn)
3 MPN per 4 grams
total solid (dry
weight)
Vector Attraction Reduction (40 CFR 503.33) - Please indicate option performed:
Alt- I (VS reduction) Rl
Alt. 2 (40-day bench) ❑
Alt. 3 (30-day bench) ❑
I Alt. 4 (Spec. Oz uptake) ❑
Alt. 5 (14-Day Aerobic) ❑
Alt. 6 (Alk. Stabilization ❑
Alt 7 (Drying - Stable) ❑Alt.
8 (Drying - Unstable) ❑
Alt. 9 (Injection) ❑
Alt. 10 (Incorporation) ❑
No vector attraction reduction alternatives were performed ❑
CERTIFICATION STATEMENT (please check the appropriate statement)
0 "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector
attraction reduction requirement in 40 CFR 503.33 have been met."
❑ "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector
attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check
this statement attach an explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Kyle Ketchum, WWTP Superintendent Ken Morris, Residuals Coordinator
Preparer Name and Title (type or print) Land Applier Name and Title (if applicable)(type or print)
Signature of Preparer* Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 503 (12/2006)

P�
UR
PPOMPT• A CCU RATE• RELi ABLE
LABORATORIES, INC
WIA VIPAR1.ABS.COM
REPORT OF ANALYSES
Attn: KEN MORRIS
CITY OF MONROE WASTEWATERPLANT PROJECT NAME: AUG 23
PO BOX 69 DATE: 08/25/23
MONROE, NC 28111-
SAMPLE NUMBER- 147816 SAMPLE ID- MONROE WWTP SAMPLE MATRIX- WW
DATE SAMPLED- 08/07/23 TIME SAMPLED- 1013
DATE RECEIVED- 08/07/23 SAMPLER- KM RECEIVED BY- DJ
TIME RECEIVED-- 1145 DELIVERED BY- KM TYPE SAMPLE- Grab
Page 1 of 1
ANALYSIS
ANALYSIS METHOD DATE TIME BY RESULT UNITS
FECAL COLIFORM (GEOM. MEAN) SM 9221 E 08/07/23 1540 RE 3,178 MPN/g
LABORATORY DIRECTOR
i
2217 Graham Park Drive • Charlotte, NC 28273
Phone: [phone] • Fax: [phone]

PAR
PROM PT- ALcuYt.�kTE-Re 6.IASL F
1.ABORP,-)rCOR1 S, INC
2217 Graham Park Drive
PO Box 411483
Charlotte, NC 28241-1483
NC Cert # 20, SC Cert # 99003001
CITY OF MONROE
• MONROE WWTP
• 08/07/23
FECAL COLIFORM, GEOMETRIC MEAN
• SM 9221 E
A: ID
Sample #
F. Coliform
T. Solids %
FC/ gram
147816
1
705
19.23%
3,664.47
2
622
20.64%
3,010.62
3
585
19.99%
2,925.09
4
670
19.91 %
3,367.50
5
430
20.34%
2,115.54
6
776
19.86%
3,909.31
7
721
19.78%
3,643.91
Fecal Coliform
Geometric Mean=

�P CHAIN OF CUST49DY
4 L46CRAro iGs,IAC. PAR Laboratories, Inc
Phone (704) SSS-8333
Fax [phone]
ww► .parfabs.cvrrr
Shipping: Mailing:
2217 Graham park Drive PO Box 411463
Charlotte, NC 28273 Charlotte, NC 28241.14,93
It 4 v33WN that all Worrmoon be recorded oq Thi7 Chelp of Cuatady documsat ror accepunce br PAR Labormeax WC. VW ftNtlrt+i
C hn V� arSm�nt of Er.wi�onmer:af and Hrtuwf Raavrcq. '
COrnpany Norrle rblgng) �Grilfrfalrltti� .�! irl�
City of Monroe
aadtr��
& To
Y�%
PO Box 69
lv,Mcaroe, NC 28111
---
.4) 3!a!-15
Sample Token Sy: �� Ma rr i S
503 E10SOLIDS
REPORTING
IS THIS FOR STATE or EPA RIEPQ TIhlG1 YES , NO
o"Sample type: DW _� WW GWMW HW _ Soil _ other
Sample Temp at time of ss pang:.2 °C_ Sample Temp upon reel pt: LI °
F`rarvonred: Yes Na Teflon Unelr Zero Headspaee: Yes _ No — N!A„1
Rol W rppIo I.A.
a lA Wmi0R 1 'Number
Comp
Grab
X
X
Praserv.
NONE
NONE
Set Up
Aare / Time
2-1-� ,f
- 7 �3
Gollectioo
Date / Tire
1 v :13
to :) ;
Analyea Requerhd
FECAL COL"RM
FECAL COI ORM
# WVv CV
# 3 WWTP
X
NONE
7r. 3
r
ra': 1 If
FECAL CO It _.
# 4 wWTP, _
X
X
NON)~
NONE
F-7-� 3
S• i'.z3
i�..1
o •, !�
FECAL CUL-Hi M
FECAL,. CO
# S WWTP
# 6 WWTP
x
NONE
. 7., 3
! :15
FECAL CC}LYORM
07 WWTP
X
NONE
�.7ra3
re'.15
FECAL D UM-
Sall isr4d by: DatelTme AQc . by: Datarnm
•.� 0 8- d -7-d-S&
Wmquished by: Daterrime Received by: DatefTima
C «Composite G-Grab Div =Dri wng Water WW-Waaiawater GWMW-Groundwater MonhobritV Well HIN-Ha7bmWis Ww"
• See Other Side

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Monroe WQ Permit Number:
WWTP Name: WWTP cake NPDES Number:
Monitoring Period: From 7/1/2023
To 9/30/2023
WQ0001346
NCO024333
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. A (time/temp) ❑
Alt B (Alk Treatment) ❑
Alt. C (Prior Testing)❑
Alt.D (No Prior Test) ❑
Process to Further Reduce Pathogengs ❑
If applicable to alternative
performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost ❑
Heat Drying ❑
Heat Treatment ❑ Thermophilic ❑
Beta Ray ❑
Gamma Ray ❑
Pasteurization ❑
Class B:
Alt. (1) Fecal Density R1
Alt. (2) Process to Significantly Reduce Pathogens ❑
If applicable to alternative
performed (Class
B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization ❑
Air Drying ❑ Composting ❑
jAerobic Digestion r❑
Anaerobic Digestion ❑
...........
If applicable to alternative performed (Class A or Class B) complete the following
monitoring data:
Parameter
Allowable Level
in
in Sludge
Pathogen Density
Number o
Excee- ences
Frequency
of Analysis
y
Sample
Type
Analytical
Tech -
MOM
Minimum
Geo. Mean
aximu
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
2,115.54
3,178
3,909.31
MPN/g
0
quarterly
Grab
SM9221E
CFU
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per 4 grams
total solid (dry
weight)
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed:
Alt.1 (VS reduction)
❑
Alt. 2 (40-day bench) ❑
Alt. 3 (30-day bench) ❑ Alt. 4 (Spec. OZ uptake)
❑
Alt. 5 (14-Day Aerobic)
❑
Alt. 6 (Alk. Stabilization ❑
Alt 7 (Drying - Stable) ❑ I Alt. 8 (Drying - Unstable)
❑
Alt. 9 (Injection)
❑
Alt. 10 (Incorporation) ❑
No vector attraction reduction alternatives were performed
❑
CERTIFICATION STATEMENT (please check the appropriate statement)
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note
if you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Kyle Ketchum, WWTP Superintendent
Preparer Name and Title (type or print)
Ken Morris, Residuals Coordinator
Land Applier Name and Title (if applicable)(type or print)
Sign Lure of Preparer* Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DFNR FORM PVRF 02T (12/2006)

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (503 Rules)
Facility Name: City of Monroe
WWTP Name: Monroe WWTP cake
WQ Permit Number: WQ0001346
NPDES Number: NCO024333
Monitoring Period: From 7/l/2023 To 9/30/2023
Pathogen Reduction (40 CFR 503.32) - Please indicate level achieved and alternative performed:
Class A:
Alternative 1 ❑
Alternative 2 ❑
Alternative 3 ❑
Alternative 4 ❑
Alternative 5 ❑
Alternative 6 ❑
If applicable to alternative
performed (Class A only) indicate "Process to Further
Reduce Pathogens":
Compost ❑
Heat Drying ❑
Heat Treatment ❑
Thermophilic ❑
Beta Ray ❑
Gamma Ray ❑
Pasteurization ❑
Class B:
Alternative 1 0
Alternative 2 ❑
If applicable to alternative
performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization ❑
Air Drying❑
Composting ❑
Aerobic Digestion El
Anaerobic Digestion El
If applicable to alternative performed (Class A or Class B) complete the following
monitoring data:
Parameter
Allowable Level
in
in Sludge
Pathogen Density
Number o
Excee-
Frequency
of Analysis
y
Sample
Type
Analytical
Tech -
Wow
Minimum
Geo. Mean
aximu
UnitseLQQ_
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
2,115.54
3,178
3,909.31
MGN/g
0
quarterly
grab
sm922le
CFU
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
(in lieu of fecal
coliform) I
3 MPN per 4 grams
total solid (dry
weight)
Vector Attraction Reduction (40 CFR 503.33) - Please indicate option performed:
Alt.1 (VS reduction)
❑
Alt. 2 (40-day bench)
❑
Alt. 3 (30-day bench) ❑I
Alt. 4 (Spec. Oz uptake)
❑
Alt. 5 (14-Day Aerobic)
❑
Alt. 6 (Alk. Stabilization
❑
Alt 7 (Drying - Stable)
jAlt. 8 (Drying - Unstable)
❑
Alt. 9 (Injection)
❑
Alt. 10 (Incorporation)
❑
No vector attraction reduction alternatives were performed
❑
CERTIFICATION STATEMENT (please check the appropriate statement)
21 "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector
attraction reduction requirement in 40 CFR 503.33 have been met."
❑ "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector
attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check
this statement attach an explanation why you have not met one or both of the requirements,)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Kyle Ketchum, WWTP Superintendent
Preparer Name and Title (type or print)
Ken Morris, Residuals Coordinator
Land Applier Name and Title (if applicable)(type or print)
1 )04—" A -- 44 vino a - l p-aq
Signature of Preparer* Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 503 (1212006)

Pa
LF;Z
PROM PT•ACCU RATE -RE LI ABLE
LABORATORIES, INC
WWW,PARLABS.COM
REPORT OF ANALYSES
Attn: KEN MORRIS
CITY OF MONROE WASTEWATERPLANT PROJECT NAME: OCT 23
PO BOX 69 DATE: 11/02/23
MONROE, NC 28111-
SAMPLE NUMBER- 148190 SAMPLE ID- MONROE WWTP
DATE SAMPLED- 10/02/23
DATE RECEIVED- 10/02/23 SAMPLER- KM
TIME RECEIVED- 1200 DELIVERED BY- KM
Page 1 of 1
SAMPLE MATRIX- WW
TIME SAMPLED- 1028
RECEIVED BY-- DJ
TYPE SAMPLE- Grab
ANALYSIS
ANALYSIS METHOD DATE TIME BY RESULT UNITS
FECAL COLIFORM (GEOM. MEAN) SM 9221 E 10/02/23 1610 RE 4,434 MPN/g
LABORATORY DIRECTOR
2217 Graham Park Drive • Charlotte, NC 28273
Phone: [phone] • Fax: [phone]

PLLF;Z
PROMPT -ACCURATE- RELIABLE
LABOPATOalES, 1NC
2217 Graham Park Drive
PO Box 411483
Charlotte, NC 28241-1483
NC Cert # 20; SC Cer! # 99003001
CITY OF MONROE
i MONROE WWTP
10/02/23
FECAL COLIFORM, GEOMETRIC MEAN
• • SM 9221 E
7148190
Fecal Coliform
Geometric Mean=
1
822
21, 08%
3,897.97
2
1,022
20.70%
4,935.45
3
1,075
21.43%
5,015.00
4
866
20.15%
4 297.79
5
841
20,63%
4,075.03
6
917
20.81 %
4,407.84
7
905
19.99%
4,527.20

PA CHA11V OF CUS TOD Y
LAff0 vMwEs,jNc. PAR Laboratories, Inc
Phone [phone]
Fax {704) 588-8335
www.parfabs.cam
Shipping: Mailing:
2217 Graham Park Drive PO Box 411463
Charfot%e, NC M73 Charlotte, NC 28241-1483
It Is easanflal that al) lnrwmalfon be recorded on W3 Charn or Custody documsnt lot acceptatnce by *AR Labatttxiea, W— W4 itM Nom
G roflno Q■ artmwnt of ErMranmarrtar and Natural Rssourcas,
Camp;ny Name (a7fing) Gorrlril8iaW $ 1 Wit
' City of Monroe
PO Box 69 503 BIOSOLIDS
City. Sprte dS atip eod■ '�
N);cnREPORTING
NC 2$11 l �J
tlia'at o? C"ct &--
K�
5aarnple Token By: Ke4,1
IS THIS FOR STATE or EPA REPORTING? YES �. NO
"Sample type: DW _` WW GWMW _ HW 5oif _ cther
ti_ .
Sample Temp at me of Sa piing: 2,a°c -Sample upon receipt:16
Preserved: Yes No Teflon I ine�/ Zero Hea><dapsue. Yes _ No NIA
.r•
1 IiAt engp]G ED.
le oatiou / NuxnLmr
Comp
Grab
Prosay.
Set Up
Data / Time
Collection
Date / Time
AnKlyea KwAmw
3
X
NONE
l a ^ -
►, • a$
FECAL COLIFORN
x
NONE
o .,2-a 3
Jim 2Y
FECAL COL - RM
# 3 WWTV
X
NONE
-�3
I, : �g
FECAL CO RAM
,
# a WWTP ,
NONE
a, 3
t fl : 2g
FECAL COLIFORM
# 5 www
X
NONE
o : �
FECAL COLIFORM
# 6 WWTP
x
NONE
1
FECAL COUP RM _p
# 7 wwrP
X
NONE
-a 3
FECAL COMM
R 1) vi5het! Dy: Date/t7me c0ivaad bylf]ateffktte
larinquished by: 0staffirde Received by: - Orteffittw
c.-CornpoaitcG—GrvbDW=Drinking Water WW-Wastewater GWMWmGmundwaater MontWWrV Weil H!Y+-Huaa+dous Www
See Othor S+de

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Monroe WQ Permit Number: WQOOO l 346
WWTP Name: WWTP cake 10-2-23 sample NPDES Number: NCO024333
Monitoring Period: From 10/1/2023 To 12/31/2023
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. A (time/temp) ❑
Alt B (Alk Treatment)❑
Alt. C (Prior Testing)❑
A1t.D (No Prior Test) ❑
Process to Further Reduce Pathogengs ❑
If applicable to alternative
performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost ❑
Heat Drying ❑
Heat Treatment ❑
Thermophilic ❑
Beta Ray ❑
Gamma Ray ❑
Pasteurization ❑
Class B:
JAIL (1) Fecal Density p
Alt_ (2) Process to Significantly Reduce Pathogens ❑
If applicable to alternative
performed (Class
B only-) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization ❑
Air Drying ❑
Composting ❑
jAerobic Digestion ❑r
Anaerobic Digestion ❑
If applicable to alternative performed (Class A or Class B) complete the followin
monitoring data:
Parameter
Allowable Level
in Slud a
Pathogen Density
um er o
Exce-lof
ces
Frequency
Anal sis
Sample
Type
Analytical
Tech -
inimu
Geo. Mean
aximu
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
3,897.97
4,434
5,015.00
MGN/g
0
quarterly
grab
sm9221 e
CFU
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per 4 grams
total solid (dry
weight)
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed:
Alt.1 (VS reduction) r❑
Alt. 2 (40-day bench) ❑
Alt. 3 (30-day bench) ❑
Alt. 4 (Spec. Oz uptake) ❑
Alt. 5 (14-Day Aerobic) ❑
Alt. 6 (Alk. Stabilization ❑
Alt 7 (Drying - Stable) ❑
Alt. 8 (Drying - Unstable) ❑
Alt. 9 (Injection) ❑
Alt. 10 (Incorporation) ❑
No vector attraction reduction alternatives were performed ❑
CERTIFICATION STATEMENT (please check the appropriate statement)
0 "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note
if you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Kyle Ketchum, WWTP Superintendent
Preparer Name and Title (type or print)
Ken Morris, Residuals Coordinator
Land Applier Name and Title (if applicable)(type or print)
Signature of Preparer* Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 02T (12/2006)

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (503 Rules)
Facility Name: City of Monroe WQ Permit Number: WQ0001346
WWTP Name: Monroe WWTP cake 10-2-2023 sample NPDES Number: NCO024333
Monitoring Period: From 10/1/2023 To 12/31/2023
Pathogen Reduction (40 CFR 503.32) - Please indicate level achieved and alternative performed:
Class A:
Alternative 1 ❑
Alternative 2 ❑
Alternative 3 ❑
Alternative 4 ❑
Alternative 5 ❑
Alternative 6 ❑
If applicable to alternative
performed (Class A only) indicate "Process to Further
Reduce Pathogens":
Compost ❑
Heat Drying ❑
Heat Treatment ❑
Thermophilic ❑
Beta Ray ❑
Gamma Ra ❑
Pasteurization ❑
Class B:
Alternative 1 21
Alternative 2 ❑
If applicable to alternative
performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization ❑
Air Drying[]
Composting ❑ jAerobic Digestion 0
Anaerobic Digestion El-
...............
If applicable to alternative performed (Class A or Class B) complete the following
monitoring data:
Parameter
Allowable Level
in Sludge
Pathogen Density
Number of
Excee-
Frequency
of Analencesysis
Sample
Type
Analytical
Tech -
maue
Minimum
Geo. Mean
Maximu iii
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
3,897.97
4,434
5,015.00
MGN/g
0
quarterly
grab
sm9221 e
CFU
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacterial
(in lieu of fecal
coliform)
3 MPN per 4 grams
total solid (dry
weight)
Vector Attraction Reduction (40 CFR 503.33) - Please indicate option performed:
Alt.l (VS reduction)❑
Alt. 2 (40-day bench) ❑
Alt. 3 (30-day bench) ❑
I Alt. 4 (Spec. 02 uptake) ❑
Alt. 5 (14-Day Aerobic) ❑
Alt. 6 (Alk. Stabilization ❑
Alt 7 (Drying - Stable) ❑
JAL S (Drying - Unstable) ❑
Alt. 9 (Injection) ❑
Alt. 10 (Incorporation) ❑
No vector attraction reduction alternatives were performed ❑
CERTIFICATION STATEMENT (please check the appropriate statement)
d "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector
attraction reduction requirement in 40 CFR 503.33 have been met."
❑ "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector
attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check
this statement attach an explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Kyle Ketchum, WWTP Superintendent Ken Morris, Residuals Coordinator
Preparer Name and Title (type or print) Land Applier Name and Title (if applicable)(type or print)
Signature of Preparer* Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 503 (12/2006)

P "iFZ
AL
PROMPT- A CCU RATE• IZEL I ABLE
LABORATORIES, INC
W W W FARLABS.COINI
REPORT OF ANALYSES
Attn: KEN MORRIS
CITY OF MONROE WASTEWATERPLANT PROJECT NAME: OCT 23
PO BOX 69 DATE: 11/02/23
MONROE, NC 28111-
SAMPLE NUMBER-
14B339
SAMPLE ID- MONROE WWTP
SAMPLE MATRIX- SO
DATE SAMPLED-
10/23/23
TIME SAMPLED- 0909
DATE RECEIVED-
10/23/23
SAMPLER- KM
RECEIVED BY- RE
TIME RECEIVED-
1055
DELIVERED BY- KM
TYPE SAMPLE- Grab
Page 1 of 1
ANALYSIS
ANALYSIS
METHOD DATE TIME BY
RESULT UNITS
FECAL COLIFORM (GEOM. MEAN) SM 9221 E 10/23/23 1550 RE 4,027 MPN/g
LABORATORY DIRECTOR 1%
2217 Graham Park Drive • Charlotte, NC 28273
Phone: [phone] • Fax: [phone]

PLL R
PROMPT•^cc u RATE• RELIABLE
LALHORA.T4d)RIES, INC
148339
Fecal Coli#orm
Geometric Mean=
2217 Graham Park Drive
PO Box 411483
Charlotte, NC 28241-1483
NC Cer! # 20; SC Cert # 99003001
CITY OF MONROE
MONROE WWTP
10/23/23
FECAL COLIFORM, GEOMETRIC MEAN
SM 9221 E
1
730
18,79%
3,886.52
2
735
19.15%
3,838.66
3
847
19.37%
4,370.14
4
912
19.45%
4,686.64
5
683
19.49%
3,502.24
6
788
20.02%
3,934.07
7
772
18.93%
4,077.72

CHAIN OF CUSTODY
LaspRATWIEs.rhG PAR Laboratories, Inc
Phone [phone]
Fax [phone]
www.pafiabs.com
Shippinri: Mailing:
2217 Graham Park Drive PO Box 411483
Charlotte, NC 25273 Charlotte, NC 28241-1483
1; 4 essential Uwl all information tre recorded on this Chain of Custody docvmarn tot aceeDtance by PAR Laboratuda. Inc. and IN Nerfin
CR�oirn� Q�cartnMnl of E+*Yirwx* ai and Nowal Revourcas.
sny Blame lb -Ming) City of Monroe Comments/ Special IniA
ax .. .
$ tip aode
PO &Ix 69
Mcnme; NC 28111
503 BIOSOLIDS
REPORTING
Point Of Contact & i'skphos►e'� ..._ _' - _ - -
,rr:� � Fe l- 0.6 3� Kr►•tarY�.��c�a,�.
Sample Taken BY: ►���}V}_
IS THJS FOR STATE or EPA REPO TING7 YES �,.., NO
'Sample type_ DW VVW X GWMW _ HW _ Soil _ ether
Sample Temp at time of sa pfing: EL3 °C Sample Temp upon receipt: °
Preserved: Yes_ No X Teflon Linerl Zero Headspace• Yes_ No I /A -A
Client Semple l.D.
f Sam la Location / Nuumbt:r
Comp
Grab
Preserv.
Set Up
Date / Time
Collection
Date I Time
Anelyea Requested
# 1 WWTP
X
NONE
1,013-.23
4,
FECAL COLIFORM
N 2 W W'TP
X
NONE
t o- a 3'�
, a
FECAL COL ORORM
# 3 WWrP
x
NONE
�- 3_a
9: to
FECAL COLIFORM
9 4 WWTP, -
X
NONE
,a
: I �
FECAL COLIFORM
# s WwTP
x
NONE
_ -��
; � o
FECAL COLIFORM
# 6 WWTP
x
NONE
� f .a
� }
FECAL COLMORM
# 7 WWTP
X
NONE
i �, -�3
g : t
FECAL. COLIFORM
by:
leiinquished by:
Datomme Received by:
Dated irne Received by:
Detefi'N`w
C-Coraposrte G-Grab DW—D.rirlkirlg Water WW=Wastewater GWMW-Groandwtrtar Monitoring Well H'.V'Hazatdooa Wash
' See Other Same

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Monroe WQ Permit Number:
WWTP Name: WWTP cake NPDES Number:
Monitoring Period: From 10/1/2023 To 12/31/2023
WQ0001346
NCO024333
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. A (time/temp) ❑
Alt B (Alk Treatment) ❑
Alt. C (Prior Testing)❑
A1t.D (No Prior Test) ❑
Process to Further Reduce Pathogengs ❑
If applicable to alternative
performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost 01
Heat Drying ❑
Heat Treatment ❑
Thennophilic ❑
Beta Ray ❑
GamaL]LaL ❑
Pasteurization ❑
Class B:
JAIL (1) Fecal Density p
Alt. (2) Process to Significantly Reduce Pathogens ❑
If applicable to alternative
performed (Class
B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization ❑
Air Drying ❑
Composting ❑
jAerobic Digestion R1
Anaerobic Digestion ❑
If applicable to alternative performed (Class A or Class B) complete the following
monitoring
data:
Parameter
Allowable Level
in
in Sludge
Pathogen Density
Number o
Excee-
Frequency
of Analysis
Y
Sample
Tencesype
Analytical
Tech -
nioue
Minimum
Geo. Mean
Maximum
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
3,502.24
4,027
4,686.64
MGN/g
0
quarterly
grab
sm9221 e
CFU
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per 4 grams
total solid (dry
weight)
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed:
Alt- I (VS reduction) v❑
Alt. 2 (40-day bench) ❑
Alt. 3 (30-day bench) ❑
Alt. 4 (Spec. OZ uptake) Cl
Alt. 5 (14-Day Aerobic) ❑
Alt. 6 (Alk. Stabilization ❑
Alt 7 (Drying - Stable) ❑ JAIt.
8 (Drying - Unstable) ❑
Alt. 9 (Injection) ❑
Alt. 10 (Incorporation) ❑
No vector attraction reduction alternatives were performed ❑
CERTIFICATION STATEMENT (please check the appropriate statement)
❑� "1 certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note
if you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Kyle Ketchum, WWTP Superintendent
Preparer Name and Title (type or print)
Ken Morris, Residuals Coordinator
Land Applier Name and Title (if applicable)(type or print)
6� J04- >11rbo v 6.syn—>Q -).v-P#
Signature of Preparer* Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 02T (12/2006)

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (503 Rules)
Facility Name: City of Monroe
WQ Permit Number: WQ0001346
WWTP Name: Monroe WWTP cake NPDES Number: NCO024333
Monitoring Period: From 10/1/2023 To 12/31/2023
Pathogen Reduction (40 CFR 503.32) - Please indicate level achieved and alternative performed:
Class A:
Alternative 1 ❑ Alternative 2 ❑
Alternative 3 ❑
Alternative 4 ❑ Alternative 5 ❑
Alternative 6 ❑
If applicable to alternative
performed (Class A only) indicate "Process to Further
Reduce Pathogens":
Compost ❑
Heat Drying ❑
Heat Treatment ElThermophilic
El
Beta Ray ❑
Gamma Ray ❑
Pasteurization ❑
Class B:
Alternative I El
Alternative 2 ❑
If applicable to alternative
performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization ❑
Air Drying[]
Composting ❑
lAerobic Digestion R1
Anaerobic Digestion ❑
If applicable to alternative performed (Class A or Class B) complete the following
monitoring data:
Allowable Level
in Slud e
g
Pathogen Density
Number o
Excee-
n
Frequency
of Anal sis
Y
Sample;AnalyticalParameter
Type
ech-
Minimum
Geo. Mean
aximu
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
3,502.24
4,027
4,686.64
MGN/g
0
quarterly
grab
sm9221e
CFU
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per 4 grams
total solid (dry
weight)
Vector Attraction Reduction (40 CFR 503.33) - Please indicate option performed:
Alt.I (VS reduction) 0
Alt. 2 (40-day bench) ❑
Alt. 3 (30-day bench) ❑
Alt. 4 (Spec. Oz uptake) ❑
Alt. 5 (14-Day Aerobic) ❑
Alt. 6 (Alk. Stabilization ❑
Alt 7 (Drying - Stable) ❑
Alt. 8 (Drying - Unstable) ❑
Alt. 9 (Injection) ❑
Alt. 10 (Incorporation) ❑
No vector attraction reduction alternatives were performed ❑
CERTIFICATION STATEMENT (please check the appropriate statement)
0 "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector
attraction reduction requirement in 40 CFR 503.33 have been met."
❑ "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector
attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check
this statement attach an explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Kyle Ketchum, WWTP Superintendent
Preparer Name and Title (type or print)
Ken Morris, Residuals Coordinator
Land Applier Name and Title (if applicable)(type or print)
Signature of Preparer* Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 503 (12/2006)

SECTION
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Exchangeable Sodium Percentage
ESP= {(Na)/(Ca+Mg+K+Na)}
ESP= (B)/SUM(B,C,D,E)
Field
Na
I Ca
Mg
K
ESP
AN19-1
111
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268
325
0.0060
0.60
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18
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234
200
0.0092
0.92
UN18-2
131
601
135
308
0.0123
1.23
UN18-7
131
547
98
57
0.0182
1.82
UN18-8
17
1068
198
38
0.0129
1.29
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36
689
180
261
0.0309
3.09
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22
985
278
319
0.0137
1.37
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16
954
256
312
0.0104
1.04
UN29-4
17
983
309
294
0.0106
1.06
UN29-5
29
754
167
83
0.0281
2.81
UN30-1
19
1088
275
341
0.0110
1.10
UN30-2
13
587
112
98
0.0160
1.60
UN30-4
20
710
136
28
0.0224
2.24
UN30-5
22
678
195
21
0.0240
2.40
UN31-3
12
778
169
130
0.0110
1.10
UN31-4
12
868
215
220
0.0091
0.91
UN31-5
111
2009
402
80
0.0044
0.44
UN31-6
12
1541
336
64
0.0061
0.61
UN32-1
38
791
180
204
0.0313
3.13
UN32-2
36
520
1711
371
0.0471
4.71
UN32-4
35
831
209
378
0.0241
2.41

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