WQ0034513_2023 Residual Annual Report_20240220 (2)

Initial Review
Reviewer
nathaniel.thorn burg
Is this submittal an application? (Excluding additional information.) *
Yes No
If not an application what is the submittal type?* Annual Report
Residual Annual Report
Additional Information
Other
Annual Report Year* 2023
Permit Number (IR) * WQ0034513
Applicant/Permittee Brunswick County
Email Notifications
Does this need review by the hydrogeologist? * Yes U No
Regional Office Wilmington
CO Reviewer
Admin Reviewer Wanda Gerald

Submittal Form
Project Contact Information
Please provide information on the person to be contacted by NDB Staff regarding electronic submittal, confirmation of receipt, and other correspondence.
Name* Rob Willcox
Email Address*
[e-mail]
Project Information
Application/Document Type*
New (Fee Required)
Modification - Major (Fee Required)
Renewal with Major Modification (Fee
Required)
Annual Report
Additional Information
Other
Phone Number*
3363399128
Modification - Minor
Renewal
GW-59, NDMR, NDMLR, NDAR-1,
N DAR-2
Residual Annual Report
Change of Ownership
We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form.
https://edoes.deq.nc.gov/Forms/NonDischarge_Monitoring_Report
Permit Type:*
Wastewater Irrigation
High -Rate Infiltration
Other Wastewater
Reclaimed Water
Closed -Loop Recycle
Residuals
Single -Family Residence Wastewater
Other
Irrigation
Permit Number:*
WQ0034513
Has Current Existing permit number
Applicant/Permittee Address*
Post Office Box 249; Bolivia, N.C. 28422
Facility Name*
Brunswick County Class B Residuals Program
Please provide comments/notes on your current submittal below.
2023 Annual Report - Brunswick County Class B Residuals - WQ0034513 - West Brunswick Regional WWTP
At this time, paper copies are no longer required. If you have any questions about what is required, please contact Nathaniel Thornburg
at [e-mail].
Please attach all information required or requested for this submittal to be reviewed here.
(Application Form, Engineering Plans, Specifications, Calculations, Etc.)
2023 CLASS B ANNUAL REPORT-WQ0034513 -
23.14MB
Brunswick County.pdf
Upload only 1 PDF document (less than 250 MB). Multiple documents must be combined into one PDF file unless file is larger
than upload limit.
* By checking this box, I acknowledge that I understand the application will not be accepted for pre -review until the fee (if required) has
been received by the Non -Discharge Branch. Application fees must be submitted by check or money order and made payable to the
North Carolina Department of Environmental Quality (NCDEQ). I also confirm that the uploaded document is a single PDF with all parts
of the application in correct order (as specified by the application).
Mail payment to:
NCDEQ — Division of Water Resources
Attn: Non -Discharge Branch
1617 Mail Service Center
Raleigh, NC 27699-1617
Signature
Submission Date 2/20/2024

2023 ANNUAL REPORT
BRUNSWICK COUNTY PUBLIC UTILITIES
RESIDUALS LAND APPLICATION PROGRAM
NON -DISCHARGE PERMIT #WQ0034513
Prepared For:
Brunswick County
Public Utilities
Post Office Box 249
Bolivia, North Carolina 28422
Compiled By:
Willcox & Mabe Soil Solutions, PLLC
7231 B Summerfield Road
Summerfield, North Carolina 27358
February 2024

�Wlt W6100
SOIL SOLUTIONS,
February 21, 2024
N.C. Department of Environmental Quality
Division of Water Resources — Information Processing Unit
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
Attention: Information Processing Unit
Reference: 2023 LAND APPLICATION ANNUAL REPORT
Brunswick County Public Utilities
Non -Discharge Permit No. WQ0034513
WMSS Project No. 15-04 Phase: 20
Information Processing Unit:
Willcox & Mabe Soil Solutions, PLLC (WMSS) is submitting all monitoring and reporting
requirements as specified in the above referenced permit on behalf of Brunswick County
Public Utilities (Brunswick County). WMSS compiled this report using data gathered
during the compliance year by Brunswick County and EMA Resources, Inc. This data
includes: 1) land application certification forms, 2) annual residual sampling summary
forms, 3) annual pathogen and vector attraction reduction forms, 4) annual field summary
forms and metals field loading summary forms, 5) lab sheets, and 6) soil analysis reports.
Brunswick County land applied a total of 32.99 dry tons of biosolids under Permit No.
WQ0034513 during the 2023 calendar year (West Brunswick Regional WWTP-32.99 dry
tons).
If there is any further information required or questions regarding this annual report please
do not hesitate to contact Mr. Donald Dixon, Deputy Director of Wastewater Operations
with Brunswick County at [phone] or Rob Willcox with WMSS for further
assistance.
Sincerely,
Willcox & Mabe Soil Solutions, PLLC
Martin Mabe
Agronomist/Partner
Enclosures
Rob Willcox, L.S.S.
Soil Scientist/Partner
Shared\WMSS Projects\2015\15-04 Brunswick County\Phase 20 - 2023 Annual Report\Class B\2023 CLASS B ANNUAL REPORT - Brunswick
County.doc
Willcox & Mabe Soil Solutions, PLLC / 7231 B Summerfield Road / Summelfield, NC 27358 / Rob 336.339.9128 or
Martin 336.312.1396 / www.willcoxmabesoil.com

TABLE OF CONTENTS
SECTION NO. TITLE
Annual Land Application Certification Forms
(Form ACF)
II Annual Residual Sampling Summary Forms
(Form RSSF)
III Annual Pathogen and Vector Attraction Reduction Forms
(503 Rules)
(Form PVRF 503)
IV Annual Land Application Field Summary Forms and Annual
Metals Field Loading Summary Forms
(Form FSF and MFLSF)
V Lab Sheets
VI Soil Analysis Reports

Brunswick County Public Utilities
Post Office Box 249
Bolivia, North Carolina 28422
RESIDUALS LAND APPLICATION PROGRAM
CLASS B RESIDUALS
PERMIT NO. WQ0034513
WEST BRUNSWICK REGIONAL WWTP
NON -DISCHARGE PERMIT NO. WQ0023693
Mr. Donald Dixon, Deputy Director of Wastewater Operations
Brunswick County Public Utilities
Post Office Box 249
Bolivia, North Carolina 28422
[phone]
2023 West Brunswick Regional WWTP Dry Tons - 32.99
2023 West Brunswick Regional WWTP Dry Metric Tons - 29.92

SECTION I
ANNUAL LAND APPLICATION CERTIFICATION FORMS
(Form ACF)

ANNUAL LAND APPLICATION CERTIFICATION FORM
WQ Permit#: WQ0034513 County: Brunswick Year: 2023
Facility Name (as shown on permit)- Brunswick County
Land Application Operator -
Phone:
Land application of residuals as allowed by the permit occurred during the past calendar year?
Yes-'-' No - If No, skip Part A, and Part B and proceed to Part C. Also, If residuals were
generated but not land applied, please attach an explanation on how the residuals were handled.
Part A - Residuals Application Summary West Brunswick Regional WWTP
Total number of application fields in the ermit: 31
Total number of fields utilized for [and application during he year:
Total amount of dry tons applied during the year for all on sites: 32.99
Total number of acres utilized for [and application during he year: 27.0
Part B - Anna
Facility was compliant during calendar year 2023 with all conditions of the land application permit
(including but not limited to items 1-13 below) issued by the Division of Water Resources. R Yes !21 No
If no please, provide a written description why the facility was not compliant, the dates, and explain corrective action
taken.
1) Only residuals approved for this permit were applied to the permitted sites,
2) Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6,0 or the
limit specified in the permit.
3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies of
laboratory results are attached,
4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached,
5) All other monitoring was performed in accordance with the permit and reported during the year as required and three (3)
copies of certified laboratory results are attached.
6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T I 105(a) or the Pollutant Loading
Rates in 15A NCAC 02T,1105(b) (applicable to 40 CFR Part 503 regulated facilities).
7) All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part
503 regulated facilities).
8) All monitoring and reporting requirements in 15A NCAC 02T.1 111 were complied with (applicable to 40 CFR Part 503
regulated facilities).
9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Resources.
10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
14) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as specified
in the permit.
12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13) All buffer requirements as specified on the permit were maintained during each application of residuals.
Ear, C - Certifi �Ication.-
I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate,
and complete. I am aware that there are significant penalties for submitting false information, including the possibility
of fines and imprisonment for knowing violations."
Donald B. Dixon - Deputy Director
Permittee Name and Title (type or print) Signature of Permittee Date
Signature of Preparer* West Brunswick WWTP Date Signature of Land Applier D�e_
(if different from Permittee) (if different from Permittee and Preparer)
* Preparer is defined in 40 CFR Part 50' ).9 (r) and 15A NCAC 02T 1102 (26) DENR FORM ACF (12/2006)

SECTION II
ANNUAL RESIDUAL SAMPLING SUMMARY FORMS
(Form RSSF)

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SECTION III
ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORMS
(503 RULES)
(Form PVRF 503)

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (503 Rules)
Facility Name: Brunswick County
WWTPName: West Brunswick Regional WWTP
Monitoring Period: From I/l/2023
To
WQ Permit Number:
NPDES Number:
12/31/2023
Pathogen Reduction (40 CFR 503.32) - Please indicate level achieved and alternative performed:
WQ0034513
WQ0023693
Class A:
Alternative 1 3,
Alternative 2 j
Alternative 3
Alternative 4
Alternati
Alternative 6
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost
Heat Drying rJ
Heat Treatment []
I Thermophilic
Beta Ray
Gamma Ray `s__]
Pasteurization 0
Class B:_
Alternative I E
Alternative 2 [,,]
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization EI
Air Drying[]
- Composting E]
jAerobic Digestion R!f
Anaerobic Digestion
If applicable to alternative performed (Class A or Class B) complete the following monitoring data:
Parameter
Allowable Level
in Sludge
Pathogen Density
Number of
Bence-
es
Frequency;
of Analysis il
Sample
Te
yp
Analytical
Tech -pique
Minimum
Geo. Mean
Maximud
-
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
43
44
45
MPN/
Gram
0
Annual
Grab
SM92210E
CFU
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
(in lieu of fecal
coliform)
A
3 MPN per 4 grams
total solid (dry
weight)
v ectur Attraction Reduction (40 CFR 503.33) -Please indicate option nerformed-
Alt. I (VS reduction)
Alt. 2 (40-day bench) _Fj
Alt. 3 (30-day
bench)
jAlt. 4 (Spec 02 uptake)
Alt. 5 (14-Day Aerobic)
Alt. 6 (Alk. Stabilization f7]
Alt 7 (Drying - Stable)
JAlt. 8 (Drying - Unstable)
Alt. 9 (Injection)
Alt. 10 (Incorporation) E]
No vector attraction reduction alternatives were performed El
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector
attraction reduction requirement in 40 CFR 503.33 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector
attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check this
statement attach an explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed
to ensure that qualified personnel properly gather and evaluate the information used to determine that the
pathogen and vector attraction reduction requirements have been met. I am aware that there are significant
penalties for false certification including fine and imprisonment."
Donald Dixon -Deputy Director, WW Operations
Preparer Name and Title (type or print) Land Applier Name and Title (if applicable)(type or print)
Signature of Preparer* Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503,9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 503 (12/2006)

SECTION IV
ANNUAL LAND APPLICATON FIELD SUMMARY FORMS
ANNUAL METALS LOADING SUMMARY FORMS
(Form FSF and MFLSF)

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ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: -. Brunswick County Dry Tons Applied (Annual): 17.55
Permit #: WQ0034 1 513 Predominant Soil Series: Lynchburg-Ly
Operator: --Pearly Vereen Owner: Pearly V-e-,_-
Acres Used: -12.00 Acres P­ i*+ A reen
Residual
Analysis
Data
(Heavy
Sample
or Corn-
posite
2,127/23
Date
% Solids
159
Arsenic
l&5
Cadmium
3 3.7
Chromium
9.3
Copper
44&0
Lead
14.7
Mercury
6.15
Molyb-
denum
10.4
Nickel
29.2
SdefliLlIn
18,5
Zinc
1,960
Total
Phos-
49.600
phorus
1, /-.VV Site #, NC-BR-PV Field #: 2
Metals and Total Phosphorus use rng/k,g, % Solids use Raw Percent
..........
Annual Heavy Metal F­`ield Lo-adings
Calculated in lbs/acre
o
4�
77--joil
I -f
is
M
<
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1.4625
Arsenic
0,0000
0�0000
"00'�
0,0541
0.0000
0ji0oo
0,0000
.0
0�0-0
0,0000
-070(100
0,0000
0.
0.0000
0.0541
iL
0.0000
0.0000
0.0108
0,0050
0.0000
0,0
.0000
0.0000
0.0000
0,0000
0.0000
0.0000
0.0108
'Chromiun
0.0000
0.00(o)(0)
A 150
0.0000
O.O000
0.0
.0-
0.0000
0-0000
"000
0-0000
0,0000
0,0000
0.1150
Copper
n
0,0000
0 6_
.0
0.o 0 0
1.3404
0,0000
0.0000
0.0000
1 0.00001
0.0000
0.0000
0�00(1
0�0000
0�0000
1.3104
Lead
0-0000
0.0000
-0000
0,0430
0.0000
1) 11000
0,0000
0.0000
0.0000
010000
00000
0.0000
0.0000
0.0430
Mercury
Molyb-
0,0000
-
0.6 f 8 0
0.0000
0.0000
O.O000
omoo
-TT5-655
00-000
0,0000
0.0000
0.0000
0.0180
denum
0.0000
-
0.0000
-
0.0304
- -
0.0000
0.0000
"000
0-0000
0-0000
0,0000
0,0000
10000
-
0.0000
0.0304
Nickel
�'cic �12n'
O.0000
0.0000
�.08,54
-
0.0000
-�
-00--
000
0,0000
0.0000
0,0000
0.0000
0.0000
0,
-FOOOO
0.0854
-0000
0.0000
0.a541
T 0-RO-0
-O
-(TO-00-0
�0000
-�,-Oa0-0
T-0000
7 -0000
omoo
0.0000
0.0000
0,000
0.0541
Zinc
-To-tal
0.0000
0.0000
5.4405
00-00
-0 -000-0
(L0000
--
"000
0-0000
0.0000
0.0000
4405
0.0000
0.0000
0.0000
145.080
Phos-
nhoniq
0,0000
0,0000
145-080
0.000
0.0000
0.0000
0.0000
0, 0000
0,0000 1
"I certify, under penalty of law, that this document was prepared under my direction or supervision in
accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are Significant penalties for subinitfing false information,
including the possibility of fines and imprisonment for knowing violations"
Signature of Land Applier Date
,1 See bottom of PSIS Form for helpful instructions for this MFLSF Forin and the mathematically linked FSF Form
DEAR FORM FSF (5/2003)

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ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Brunswick County Total Dry Tons Applied (Annual): 1,5.44
Permit #: WQ0034513 Predominant Soil Series: - Lynchburg-Ly
Operator: Pearly Vereen Owner: - Pearly Vereen
Acres Used: 15.00 Acres Permitted-: -15.00 Site NC-BR-PV - Field #: 3
Residual Analysis Data Me rul + I
.,j v a s and Total
rnospnorus
use
rng/kg,
% Solids
use Raw
Percent
Sample
A 1
4
7
8 i
or Com-
posite
2127/23
Date
% Solids
159
Arsenic
18.5
Cadmium
3.7
Chromium
39.3
Copper
448.0
Lead
14.
,Mcrcury
6.15
Molyb-
denum
10.
Nickel
29.2
Selenium
18.5
Zinc
1,860
Total
Phos-
49,600
horns
Annual
eavy
Metal Field Loadings (Calculated
in Iles/acre):
=_iJ 4,_
7
07
12r
7
77'
0
1,0296
Arsenic
0.0000
0.0000
0.0381
0.0000
0.aaQa-670-0TO
-5-0-000
0.0000
0.0000
6.5000
Cadmium
`hromiun
0.0000
0.0000
0.0076
O.0000
0.0000
0.00
0.0000
0,0000
0.0809
0.0000
-
Copper
0.0000
0.0000
0.9225
0.0000
Lead
0.0()no
n nnnn
Mercury
0,000U I
UMUO 1
0.0127
0.0000
0.0000
0.0000
0.0000
0.0000
0.0000
O.00a0
6-00-00
O.a0U0
0.0127
olyb-
0.0000
0.0000
0.0214
'num
0,0000
0.0000
0.0214
0'0000
0-0000
0-0000
0-0000
0-0000
0,0000
0.0000
Nickel
0.0000
o.0000
0,0601
T-0000
.0000
_0_.00001
()000
_5_000
OOTO -To-
000
0.0600
0.0000
0.0000 .-
O.0000
0.0601
Selenium
O.0000
0.0000
0.0381
T-0000
-0.00-00
-
-6-00-00
0,0000
0,0000
0.0000
0.0000
0.0000
0.0381
Zinc
.
0.0000
0.0000
3.8301
0.0000
0.0000
0.0000
0.0000
0.0000
0.0000
0.0000
0,0000
-
8301
I otal
-
-
0.0000
102,136
Phos-
0,0000
0.0000
102.136
0.0000
0.0000
o.0oo0
0.()000
0.0000
(),0000
0,0000
0.00 00
=Zhorus
"I certify,
under penalty
of
law. that
thiz ddiezimpni
- - ­ -11 .. a..,V. Alay U31 %��Zsufl or supervision in
accordance with, a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information,
including the Possibility Of fines and imprisonment for knowing violations,,
Signature of Land Applier Date
* See bottom of FSF Form for helpful instructions for this MFLSF Form and the mathematically linked FSF I-orm
DENR FORM FSFF (5/2003)

SECTION V
LAB SHEETS

BRUNSWICK COUNTY
LAND APPLICATION PROGRAM
BIOSOLIDS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: February 27, 2023
Date Reported: March 15, 2023
West Brunswick Regional WWTP
Mineralization Rate 0.30 2.59 % Solids
6.09 PH (1/17/23 TCLP
Parameter
AN (injecte(
AN (surface
ium
ium Carbonate Eq
itrate N / Nitrite N
loride
Cadmium
r
9.960
99,600.000
4.960
49,600.000
0.985
9,850.000
7.148
71,480.000
4.203
42,030.000
5.890
58,900.000
3.020
30,200.000
---
3,640.000
---
3,590.000
---
370.000
---
28,500.00
---
18.50
---
3.70
---
39.30
---
448.00
---
1.4.70
---
6.150
---
10.40
---
29.20
---
18.50
Permit No. WQ0034513
Class B
Waypoint 23-059-0015
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
199.200
99.200
19.700
142.960
84.060
117.800
60.400
7.280
7.180
0.740
57.000
0.037
0.007
0.079
0.896
0.029
0.012
0.021
0.058
0.037
3.720
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits
for calculation purposes.
SAR
0.83
Ceiling Concen.
(Mg/Kg)
75
85
4,300
840
57
75
420
100
7,500

Waypoint
ANALYTICAL
3/15/2023
Brunswick County Public Utilities
Mr. Matthew Henry
235GreywaberRoad
Supp|y, NC.28462
Ref: Analytical Testing
Lab Report Number: 23-D5Q'UO15
Client Project Description: VVBR-NEBR
��Whitten Road, Memphis, nv38133
Main e0z.2z3.240D"Fax 90l.2z3.24*U
wwm^wavpomtaoa|ydo»!.monn
Dear Mr. Matthew Henry:
Waypoint Analytical, LLC. received sample(s) on 2/28/2023 for the analyses presented in the following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Where the laboratory was not responsible for the sampling
stage (refer to the chain of custody) results apply to the sample as received.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method va|idaUons, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2021) and NELAC unless otherwise indicated.Any parameter
for which the laboratory isnot officially NELAPaccredited iaindicated byo,~'aymbo| These not included in
thenoopebeceumeNELAPoocred�ohonioeithernotevai|ab|eorhaenotbeenopp|i'~
applied for. Ad'-inno|
certifications may beheld/are available for parameters, where NELAPaccreditation ianot required orapp|ioab|e
Afull Umtofcedi�ootionoiaavailable upon request.
�
Certain parameters (chlorine, pH, dissolved oxygen, sulfite ... ) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown onthe attached Report ofAnmlyeio(e).Results for solid matrices are reported onanas-
received bouiaunk*amothonwiseindicated. This report shall not bereproduced except infull and relates only to
the samples included in this report.
Please donot hesitate hocontact moorclient services ifyou have any questions orneed additional information.
Connie Cook
Project Manager
Laboratory's liability in any claim relating toanalyses performed shall bolimited to, at 'option ~ theonaOmm analysis laboratory's --�-
Page 1 of 23

Waypointo
ANALYTICAL
2790 Whitten Road, Memphis, TN 38133
Main 901.213.24.00 0 Fax [phone]
www.waypoiaitanalytical.com
State
Program
Lab ID
Expiration Date
Alabama
State Program
40750
02/29/2024
Arkansas
State Program
88-0650
02/07/2024
California
State Program
2904
06/30/2023
Florida
State Program
- NELAP
E871157
06/30/2023
Georgia
State Program
C044
11/14/2025
Georgia
State Program
04015
06/30/2023
Illinois
State Program
- NELAP
200078
10/10/2023
Kentucky
State Program
80215
06/30/2023
Kentucky
State Program
KY90047
12/31/2023
Louisiana
State Program
- NELAP
LA037
12/31/2023
Louisiana
State Program
- NELAP
04015
06/30/2023
Mississippi
State Program
MS
02/11/2023
North Carolina
State Program
47701
07/31/2023
North Carolina
State Program
415
12/31/2023
Pennsylvania
State Program -
NELAP
68-03195
05/31/2023
South Carolina
State Program
84002
06/30/2023
Tennessee
State Program
02027
11/14/2025
Texas
State Program -
NELAP
T104704180
09/30/2023
Virginia
State Program
00106
06/30/2023
Virginia
State Program -
NELAP
460181
09/14/2023
Page 1 of 1 00001/23-059-0015
Page 2 of 23

0 0
Waypoint.
ANALYTICAL
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 Fax [phone]
w-w-waypointanalytical.com
Sample Summary Table
Report Number: 23-059-0015
Client Project Description: WBR-NEBR
Lab No Client Sample ID Matrix Date Collected Date Received
92723
WBR - SNDR
Solids
02/27/2023 10:15
02/28/2023
92724
NEBR New Post ATAD
Solids
02/27/2023 11:50
02/28/2023
92725
NEBR Old Post ATAD
Solids
02/27/2023 12:00
02/28/2023
Page 3 of 23

Waypoint
ANALYTICAL
Client: Brunswick County Public Utilities
PnojontVVBR-NEBR
Lab Report Number: 23-O59-OO15
Date: 3/15/2023
2790 Whitten Road, Memphis, nv3u133
Main 9nz.2z3.24On"Fax 9oz.2z3.244D
,"ww.wavpoimana|vhcaicom
Metals Analysis Method 6010D
Sample 82724(NEBRNew Post ATAD)
Analyte:/Uuminum
C>CBatch No: LGG8588/LGG7485
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample Q2S14(Feb 2O23Monthly Comp)
Annlyte:/Uuminum
C)CBatch No: LGG832O/LG67810
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 82Q14(Feb 2023Monthly Comp)
Anolyte: Calcium
0CBatch No: LGG832U/LS87818
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. Adilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 92B14(Feb 2D23Monthly Comp)
Anolyba: Potassium
(JCBatch No: LSG85OS/1-SG7D1G
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 82Q14(Feb 2O23Monthly Comp)
Analyte:K8egneaium
OCBatch No: LGG832O/LSG781G
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. Nomatrix interference iesuspected.
Anions byIon Chromatography Method 9056A
Sample Q27230WBR-8NDP0
QCBatch No:L6G8S59/LSG8378
The sample was diluted due hothe nature ofthe sample matrix. Reporting limits have been adjusted accordingly.
Sample 92724 (NEBR New Post ATA0
QC Batch No: 1-668659/1-668378
The sample was diluted due to the nature of the sample matrix. Reporting limits have been adjusted accordingly.
Sample 92725(NEBROld Post ATAO)
OCBatch No: LSG885g/1-QG837O
The sample was diluted due tothe nature ufthe sample matrix. Reporting limits have been adjusted accordingly.
Page 4 of 23

279OWhitten Road, Memphis, TN38133
Main g01.o13.24oV"Fax 9V1u13.2a40
vvww^wuvpaintana|rdmal.com
Report Date 03/15/2023
Received 02/28/2023
Report Number :2s-n59'nmz5 RaPORTOFAmu«L YSaS Connie Cook
Project Manager
Lab No e2723
Matrix: Solids
Sample ID: VxBR'SmDR
Test Results
Units MQL
oF Date /Time By Analytical
Analyzed Method
Moisture
97.3
%
z
03y14V2316:00
mTr
SW-DKYvm'
Ammonia Nitrogen
58900
mg/Kg 'dry
3700
z
03V13/2309:30
JFo
450Omx3ca011
mitrate(mO3'm)
<370
mg/Kg 'dry
370
zo
03/08/23 19:*9
sm
9056x
mimte(woz-N)
=JvO
mg/Kg 'dry
370
zo
03/08/23 19:*9
Spo
9056A
-
Mitrate+miuitcm
^370
mg/Kg-dry
370
0
03/08/23 1e:49
9056A
Total Solids
2.59
v+
0.010
z
03/03V23 /6:30
pMw
25406'2011
Total Kje|dah|mivngcn
99600
mg/Kg 'dry
6930
1
03/08/23 1*:38
Amx
4500NOnGoe011
Total Nitrogen
99600
mo/Kg-dry
370
z
03/08/231+:38
CALCULATION
Phosphorus
49600
mg/Kg dry
1730
z
03/08/23 14:*8
Amn
365.4
Aluminum
28500
mg/Kg dry
185
z
03/08/2321:85
eKm
6010D
Arsenic
<z8.5
mg/Kg 'dry
18.5
z
03/07y2304:54
T]3
0010o
Cadmium
<3.70
mg/Kg dry
3.70
1
03/07y2304:54
l7S
sOznm
Calcium
30200
mg/Kg 'dry
1850
z
03/08/2321:05
BKm
6010o
Chromium
3e.3
mg/Kg 'dry
9.26
z
03/08/2321:05
BKm
6010o
Copper
448
mu/Kg-dry
18.5
z
03/07y230*:5*
T]S
GulUn
Lead
14.7
mo/Kg-dry
11.1
z
03/07y2204:54
T]S
6010o
Magnesium
3640
mg/Kg 'dry
185
z
03/07y2304:54
T]S
6010o
Mercury
<6.15
mg/Kg 'dry
6.15
z
03/02/23 12:42
FDS
7471A
Molybdenum
1e.4
mg/Kg dry
926
1
03/07y2304:54
TJS
6010o
Nickel
29'2
mg/Kg 'dry
926
z
03/07/2304:5*
os
6010o
Potassium
9850
mg/Kg 'dry
370
1
03/07y230*:5*
rrn
6018o
Selenium
<zn.S
mg/Ky-dry
18.5
z
03/08/2321:05
oxm
6018o
Sodium
3590
mg/Kn-dn/
926
1
03/07/230*:54
T]S
6810o
Qualifiers/ DF
Definitions
Dilution Factor
MQL
Method Quantitation Limit
Page 5 of 23

Report Number : 23-059-0015
Lab No : 92723
Sample ID: WBR - SNDR
Test
Zinc
279G Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 Fax [phone]
www,waypointanalyticaLcom
Results Units MOL
Report Date 03/15/2023
Received 02/28/2023
" I!e�L
Connie Cook
Project Manager
Matrix: Solids
Sampled: 2/27/2023 10:15
DF Date / Time By Analytical
Analyzed Method
1860 mg/Kg - dry 46.3 1 03/08/23 21:05 BKN 6010D
Qualifiers/ DF Dilution Factor MQL Method Quantitation Limit
Definitions
Page 6 of 23

2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 Fax [phone]
www.waypointanalytical.com
Report Date 03/15/2023
Received 02/28/2023
" leg —
Report Number: 23-059-0015 REPORTOFANALYSIS Connie Cook
Project Manager
Lab No 92724 Matrix: Solids
Sample ID : NEBR. New Post ATAD Sampled: 2/27/2023 11:50
Test
Results
Units
MQL
DF
Date / Time
Analyzed
By
Analytical
Method
Moisture
97.2
%
1
03/14/23 16:00
MJT
Ammonia Nitrogen
68600
mg/Kg -dry
3570
1
03/13/23 09:30
JW"
,,,d-DRYVVT
500NH3C-2011
Nitrate (NO3-N)
<357
mg/Kg - dry
357
10
03/08/23 20:1,+`"SRJ
9056A
Nitrite (NO2-N)
<357
mg/Kg - dry
357
10
03/08/2�l,,," 0: 14
SRI
9056A
Nitrate+Nitrite-N
<357
mg/Kg - dry
357
10
03JI,09�j)' 3 20:14
9056A
Total Solids
2.81
%
0.010
IX
03/03/23 16:30
FMM
2540G-2011
Total Kjelclahl Nitrogen
I
mg/Kg - dry
6430 I/X
1
03/08/23 14:41
ANH 4500NORGD-2011
Total Nitrogen
113000
mg/Kg - dry
357
1
03/08/23 14:41
CALCULATION
Phosphorus
43600
•mQ/Kg -dry
1
03/08/23 14:52
ANH
365.4
Aluminum
8360
mgft-,dry
179
1
03/08/23 21:11
BKN
6010D
Arsenic
< 17.9
mg/Kg - dr'y'-'�
17.9
1
03/07/23 04:59
TJS
6010D
Cadmium
<3.57
mg/Kgdry
3.57
1
03/07/23 04:59
TJS
6010D
Calcium
25800
,,7
< dry
1 NP�
1
03/08/23 21:11
BKN
6010D
Chromium
49.6
mg/Kg - dry
8.93
1
03/08/23 21:11
BKN
6010D
Copper
397
mg/Kg - dry
17.9
1
03/07/23 04:59
TJS
6010D
Lead
-"1
,-"4 " 7
mg/Kg - dry
10.7
1,"03/07/23
04:59
TJS
6010D
Magnesium
3110
mg/Kg - dry
179
1
03/07/23 04:59
TJS
6010D
Mercury
<5.79
mg/Kg - dry
5.79
1
03/02/2'1412:43
FDS
7471A
Molybdenum
12.3
mg/Kg - dry
8.93
1
03/07/23 04: 11 59,,"TJS
6010D
Nickel
31.4
mg/Kg - dry
8.93
1
03/07/23 04:59
-66,.,`
6010D
Potassium
Selenium
16500
mg/Kg - dry
357
1
03/07/23 04:59
3TR
6010D
N
21.9
mg/Kg - dry
17.9
1
03/08/23 21:11
BKN
601,GQ",
2 Sodi
3710
mg/Kg -dry
893
1
03/07/23 04:59
TJS
6010D
Qualifiers/ DF Dilution Factor
Definitions
MQL
Method Quantitation Limit
Page 7 of 23

Report Number: 23-059-0015
Lab No : 92724
Sample ID : NEBR New Post ATAD
2790 Whitten Road, Memphis, TN 38133
Main 901.213,2400 0 Fax [phone]
www,waypointanalytical.com
Report Date 03/15/2023
Received 02/28/2023
e"� &IIIL
Connie Cook
Project Manager
Matrix: Solids
Sampled: 2/27/2023 11:50
Test Results Units MOL DF Date / Time By Analytical
Analyzed Method
Zinc
1 03/08/23 21:11 BKN 6010D
Qualifiers/ DF Dilution Factor MQL Method Quantitation Limit
Definitions
Page 8 of 23

2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 Fax [phone]
www.waypoiiitanalyticaf.com
Report Date 03/15/2023
Received 02/28/2023
" ee"L
Report Number : 23-059-0015 REPORT OFANAL YSIS Connie Cook
Project Manager
Lab No 92725 Matrix: Solids
Sample ID : NEBR Old Post ATAD Sampled: 2/27/2023 12:00
Test Results Units MOL DF Date / Time By Analytical
Analyzed Method
Moisture u
97.2
%
1
03/14/23 16:00
MJT Xsv�-DRYVVT
Ammonia Nitrogen�",,"""
50000
mg/Kg - dry
3570
1
03/13/23 09:30
JP'J"450ONH3C-2011
Nitrate (NO3-N)
<357
mg/Kg - dry
357
10
03/08/23 20;4�'
SR3
9056A
Nitrite (NO2-N)
<357
mg/Kg - dry
357
10
1Z
03/08P3 20:40
SR3
9056A
Nitrate+Nitrite-N
<357
mg/Kg - dry
357
10
03-168'1 /23 20:40
9056A
Total Solids
2.76
%
0.010
03/03/23 16:30
FMM
254OG-2011
Total Kjeldahl Nitrogen
8801,0
mg/Kg - dry
7710
1
03/08/23 14:42
ANH 4500NORGD-2011
Total Nitrogen
88200
mg/Kg - dry
357
1
03/08/23 14:42
CALCULATION
Phosphorus
42100
"'mg '/Kg -dry
1
03/08/23 14:53
ANH
365.4
Aluminum
8070
mg/�g,,7dry
/*0
179
1
03/08/23 02:57
BKN
6010D
Arsenic
< 17.9
mg/l<g - dk"X
17.9
1
03/08/23 02:57
BKN
6010D
Cadmium
<3.57
mg/KAdry
3.57
1
03/08/23 02:57
BKN
6010D
Calcium
25900
', gKg - dry
179
1
03/08/23 02:57
BKN
6010D
Chromium
53.9
mg/Kg - dry
8.93
1
03/08/23 02:57
BKN
6010D
Copper
20"
mg/Kg - dry
17.9
1
03/08/23 02:57
BKN
6010D
Lead
13.4
mg/Kg - dry
10.7
03/08/23 02:57
BKN
6010D
Magnesium
3220
mg/Kg - dry
179
1
03/W23 02:57
BKN
6010D
Mercury
m <6.29
mg/Kg - dry
6.29
1
03/02i21,42:45
FDS
7471A
Molybdenum
12.0
mg/Kg - dry
8.93
1
03/08/23 02:5'7,,13KN
6010D
Nickel
29.1
mg/Kg - dry
8.93
1
03/08/23 02:57
BKN,'�'
6010D
Potassium
13700
mg/Kg - dry
357
1
03/08/23 02:57
BKN "',,,
6010D
Selenium
< 17.9
mg/Kg - dry
17.9
1
03/08/23 02:57
BKN
_
Sodi
3180
mg/Kg - dry
893
1
03/08/23 02:57
BKN
6010D
Qualifiers/ DF
Definitions
Dilution Factor
MQL
Method Quantitation Limit
Page 9 of 23

Waypointo),
ANALYTICAL
30914
Brunswick County Public Utilities
Project WBR-NEBR
Mr. Matthew Henry
235 Greywater Road
Information
Supply , NC 28462
Report Number : 23-059-001.5
Lab No : 92725
Sample ID : NEBR Old Post ATAD
2790 Whitten Road, Memphis, TN 38133
Nlain 901.213.2400 0 Fax [phone]
www.waypointanalytical.com
Report Date 03/15/2023
Received 02/28/2023
" &L
Connie Cook
Project Manager
Matrix: Solids
Sampled: 2/27/2023 12:00
Test Results Units MOL DF Date / Time By Analytical
Analyzed Method
Zinc
1 03/08/23 02:57 BKN 6010D
Qualifiers/ DF Dilution Factor MQL Method Quantitation Limit
Definitions
Page 10 of 23

...........
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 Fax [phone]
www-waypointanalyticaLcom
Client ID:
Brunswick County Public Utilities
Project Description:
WBR-NEBR
Report No:
23-059-0015
QC Analytical Batch:
L667628
Analysis Method:
2540G-2011
Analysis Description:
Total, Fixed, and Volatile Solids
Duplicate L 94345-DUP
Result DUP RPD Max RPD Analyzed
Parameter Units Result
Total Solids
% 2.57 2.55 0.7 20.0 03/03/23 16:30
Date: 03/15/2023 01:23 PM Page 1 of 11
Page 11 of 23

Waypoint, 0
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 Fax [phone]
ANALYTICAL
www.waypoititariaiytical.com
Quality Control Data
Client ID: Brunswick County Public Utilities
Project Description: WBR-NEBR
Report No: 23-059-0015
QC Prep: L668169
QC Analytical Batch(es): L668412,L668413
QC Prep Batch Method: TKN/TKP Digestion
Analysis Method: 365.4
Analysis Description: Total Phosphorus
Lab Reagent Blank LRB-1-668169
Matrix: SOL
Associated Lab Samples: 92723, 92724, 92725
Blank
Parameter Units Result
MQL Analyzed
Phosphorus mg/Kg < 25.0
25.0 03/08/23 14:45
Laboratory Control Sample
LCS-L668169
Parameter
Units
Spike
Conc.
LCS
Result
LCS O/oRec % Rec
Limits
Phosphorus
mg/Kg
100
110
110 80-120
Duplicate
L 92723-DUP-L668169
Parameter
Units
Result DUP
RPD
Max RPD
Analyzed
Result
Phosphorus
mg/Kg
1340 1320
1.5
20.0
03/08/23 14:49
Matrix Spike
L 92723-MS-L668169
Parameter
Units
MS Spike
MSD
MS Result
MSD MS O/oRec Max
Result Conc.
Spike
Result O/oRec Limits RPD
Conc.
Phosphorus
mg/Kg
1340 368
1810
128 70-130
Date: 03115/2023 01:23 PM Page 2 of 11
Page 12 of 23

Way
C. ) 2790 Whitten Road, PAemphis, TN 38133
p oi n t
Main 901.213.2400 0 Fax [phone]
ANALYTICAL www.waypointai-ialytical.corn
Quality Control Data
Client ID:
Brunswick County Public Utilities
Project Description:
WBR-NEBR
Report No:
23-059-0015
QC Analytical Batch:
L669252
Analysis Method:
4500NH3C-2011
Analysis Description:
Ammonia Nitrogen
Lab Reagent Blank
LRB Matrix: SOL
Associated Lab Samples:
92723, 92724, 92725
Parameter
Blank MQL Analyzed
Units Result
Ammonia Nitrogen
mg/Kg < 100
100 03/13/23 09:30
Laboratory Control Sample
LCS
Parameter
Spike
Units Conc.
LCS LCS %Rec % Rec
Result
Limits
Ammonia Nitrogen
mg/Kg 1000
958 96.0 85-115
Matrix Spike & Matrix Spike Duplicate E 61177-MS E 61177-MSD
MS Spike MSD MS Result MSD MS MSD %Rec Max
Parameter Units Result Conc. Spike Result %Rec %Rec Limits RPD RPD
Conc.
Ammonia Nitrogen mg/Kg 534 994 1530 1520 100 0.6 70-130 0.6 20.0
Date: 03/15/2023 01:23 PM Page 3 of 11
Page 13 of 23

QC Prep:
L668169
QC Analytical Batch(es): L668412,L668413
QC Prep Batch Method:
TKN/TKP Digestion
Analysis Method: 4500NORGD-2011
Analysis Description: Block Digestion and FIA
Lab Reagent Blank
LRB-1-668169
Matrix: SOL
Associated Lab Samples:
92723, 92724, 92725
Parameter
Units
Blank
Result
MQL Analyzed
Total Kjeldahl Nitrogen
mg/Kg
< 50.0
50.0 03/08/23 14:36
Laboratory Control Sample
LCS-1-668169
Parameter
Units
Spike
Conc.
LCS LCS O/oRec % Rec
Result
Limits
Total Kjeldahl Nitrogen
mg/Kg
500
515 103 90-110
Duplicate
L 92723-DUP-L668169
Parameter
Units
Result DUP
RPD Max RPD Analyzed
Result
Total Kjeldahl Nitrogen
mg/Kg
2690 2640
1.8 20.0 03/08/23 14:39
Matrix Spike
L 92723-MS-L668169
Parameter
Units
MS Spike
Result Conc.
MSD MS Result MSD MS O/oRec Max
Spike Result O/oRec
Limits RPD
Conc.
Total Kjeldahl Nitrogen
mg/Kg
2690 1840
4930 125 70-130
Date: 03/15/2023 01:23 PM Page 4 of 11
Page 14 of 23

2790 Whitten Road, Memphis, TN 38133
Main 901.213,2400 0 Fax [phone]
www.vjaypoititatia,"ytical.com
QUality Control Data
Client ID: Brunswick County Public Utilities
Project Description: WBR-NEBR
Report No: 23-059-0015
QC Prep: L667485 QC Analytical Batch(es): L668064,L668598,L668938,L669278
QC Prep Batch Method: 3050B Analysis Method: 6010D
Analysis Description: Metals Analysis
Lab Reagent Blank LRB-1-667485 Matrix: SOL
Associated Lab Samples: 92723, 92724
Blank MQL Analyzed
Parameter Units Result
Aluminum
mg/Kg
< 5.00
5.00
03/07/23 02:51
Arsenic
mg/Kg
< 0.500
0.500
03/07/23 02:51
Cadmium
mg/Kg
< 0.100
0.100
03/07/23 02:51
Calcium
mg/Kg
< 50.0
50.0
03/07/23 02:51
Chromium
mg/Kg
< 0.250
0.250
03/07/23 02:51
Copper
mg/Kg
< 0.500
0.500
03/07/23 02:51
Lead
mg/Kg
< 0.300
0.300
03/07/23 02:51
Magnesium
mg/Kg
< 5.00
5.00
03/07/23 02:51
Molybdenum
mg/Kg
< 0.250
0.250
03/07/23 02:51
Nickel
mg/Kg
< 0.250
0.250
03/07/23 02:51
Potassium
mg/Kg
< 10.0
10.0
03/07/23 02:51
Selenium
mg/Kg
< 0.500
0.500
03/07/23 02:51
Sodium
mg/I<g
< 25.0
25.0
03/07/23 02:51
Zinc
mg/Kg
< 1.25
1.25
03/07/23 02:51
Laboratory Control Sample LCS-1-667485
Spike LCS LCS %Rec % Rec
Parameter Units Conc. Result Limits
Aluminum
mg/Kg
500
536
107
80-120
Arsenic
mg/I<g
5.00
5.92
118
80-120
Cadmium
mg/Kg
5.00
5.88
118
80-120
Calcium
mg/Kg
500
573
115
80-120
Chromium
mg/Kg
50.0
56.9
114
80-120
Copper
mg/I<g
50.0
58.2
116
80-120
Lead
mg/Kg
5.00
5.97
119
80-120
Magnesium
mg/Kg
500
556
111
80-120
Molybdenum
mg/Kg
50.0
56.6
113
80-120
Date: 03/15/2023 01:23 PM
Page 15 of 23
Page 5 of 11

0
Waypoint,
2790 Whitten Road,
Memphis, TN 38133 ,
Main
901.213.2400 ' Fax
901.213.2440
ANALYTICAL
ww%pj.iivaypoit-itat-ialytical.com
Quality Control Data
Client ID:
Brunswick County Public Utilities
Project Description:
WBR-NEBR
Report No:
23-059-0015
QC Prep:
L667485
QC Analytical Batch(es): L668064,L668598,L668938,L669278
QC Prep Batch Method:
30506
Analysis Method:
6010D
Analysis Description:
Metals Analysis
Laboratory Control Sample
LCS-1-667485
Parameter
Units
Spike
Conc.
LCS
Result
LCS O/oRec
% Rec
Limits
Nickel
mg/Kg
50.0
60.1
120
80-120
Potassium
mg/Kg
50.0
60.0
120
80-120
Selenium
mg/Kg
5.00
5.91
118
80-120
Sodium
mg/Kg
500
573
115
80-120
Zinc
mg/Kg
50.0
58.0
116
80-120
Matrix Spike & Matrix Spike
Duplicate
L 92724-MS-L667485
L 92724-MSD-L667485
Parameter
Units
MS Spike
MSD MS Result
MSD
MS
MSD
O/oRec
Max
Result Conc.
Spike
Result
O/oRec
O/oRec
Limits
RPD
RPD
Conc.
Aluminum
mg/Kg
234 480
481 843
848
127*
128*
75-125
0.5
20.0
Arsenic
mg/Kg
< 0.500 4.80
5.44
5.33
107
2.0
75-125
2.0
20.0
Cadmium
mg/Kg
< 0.100 4.80
4.81 5,14
5.27
106
108
75-125
2.4
20.0
Calcium
mg/Kg
723 480
481 1210
1240
101
108
75-125
2.4
20.0
Chromium
mg/Kg
1.39 48.0
48.1 52.4
54.6
106
ill
75-125
4.1
20.0
Copper
mg/Kg
8.59 48.0
48.1 59.2
60.9
105
109
75-125
2.8
20.0
Lead
mg/Kg
0.412 4.80
4.81 5.60
5.67
108
109
75-125
1.2
20.0
Magnesium
mg/l(g
87.2 480
481 568
579
100
102
75-125
1.9
20.0
Molybdenum
mg/Kg
0.343 48.0
48.1 49.6
51.1
103
106
75-125
2.9
20.0
Nickel
mg/Kg
0.879 48.0
48.1 53.2
54.6
109
112
75-125
2.5
20.0
Potassium
mg/1(g
397 48.0
48.1 440
449
90.0
108
75-125
2.0
20.0
Selenium
mg/Kg
0.613 4.80
4.81 5.28
5.29
97.0
97.0
75-125
0.1
20.0
Sodium
mg/Kg
104 480
481 600
612
103
106
75-125
1.9
20.0
Zinc
mg/Kg
45.5 48.0
48.1 94.5
97.3
102
108
75-125
2.9
20.0
QC Fail
Date: 03/15/2023 01:23 PM
Page
6 of 11
Page 16 of 23

Waypoint
ANALYTICAL
2790vvhitten Road, NllemphiS,nv38z33
Main 9nzzz3.z400°Fax [phone]
,vvmm,vavpom*=n=iygcmx.com
Quality Control Data
Client ID. Brunswick County Public Utilities
Project Description: xoBR-NEBm
Report No: 23-059-0e15
QC Prep: L66/816 QC Analytical Batch(es): u668320,L668596
QC Prep Batch Method: 3050e Analysis Method: 0010o
Analysis Description: Metals Analysis
Lab Reagent Blank LRB-1-667816 Matrix: SOL
Associated Lab Samples: 92725
Parameter
Units Result
Blank MQL Analyzed
Aluminum
mg/Kg
< 5.00
5.00
0/08/230n1
Arsenic
mg/Kg
<O.50m
0.500
03/09/2301:42
Cadmium
mg/Kg
<D.zoO
0.100
03/08/2302:41
Calcium
mg/Kg
^5o.o
50.0
03/08/2302:41
Chromium
mg/Kg
<u.2So
0.250
03V08/2302:*1
Copper
mg/Kg
<o.5O0
0.500
03/08/2302:41
Lead
mg/Kg
<O.so0
0.300
03/08/2302:*1
Magnesium
mg/Kg
< 5.00
5.00
03/08/2302:41
Molybdenum
mg/Kg
<O.2sn
0.250
03/08/2302s1
Nickel
mg/Kg
^ 0250
0.250
03/08/2302:+1
Potassium
mg/Kg
^ zUo
10.0
03/08/2302:*1
Selenium
mg/Kg
^0.Snn
0.500
03/08/2302:41
Sodium
mg/Kg
^2S.0
25.0
0]/08/2]02:41
Zinc
mg/mg
< 1.25
1.25
03/08/2302:*1
Laboratory Control Sample LCS-1-667816
Parameter UnitConc. Result Limits
sSpliceu� L��m� O�R�
Aluminum
mg/Kg
500
em
98.0
80-120
Arsenic
mg/Kg
5.00
4.91
98.0
80-120
Cadmium
mg/Kg
5.00
4.92
98.0
80'120
Calcium
mg/Kg
soo
499
zOn
80-120
Chromium
mg/Kg
50.0
52.7
105
80-120
Copper
mg/Kg
50.0
48.5
e7.0
80'120
Lead
mg/Kg
5.00
4.96
99.0
80-120
Magnesium
mg/Kg
500
48*
93.0
80-120
Molybdenum
mg/Kg
50.0
47.2
9+.0
80'120
Date: 03/15/202301:23pM
Page 17 of 23
Page 7ofzz

Waypoint,
ANALYTICAL
zr90Whitten Road, Memphis, nw38z9G
Main ymz.2sa.24om°Fax 901.2zs.zw4n
,vvvw^waypo/mtauavruc^l.camn
Client ID: Brunswick County Public Utilities
Project Description: xwBm-NeBR
Report No 23-059-0015
QC Prep: L667816 QC Analytical Batch(es): L668320,L668596
QC Prep Batch Method: 3050B Analysis Method: 6010D
Analysis Description: Metals Analysis
Laboratory Control Sample �S-1-667810
Spike LCS
Parameter Units Conc. Result
Nickel
mg/Kg
500
49.8
100
80-120
Potassium
mg/Kg
580
53.0
108
80-120
Selenium
mg/Kg
5.00
4.12
82.0
80-120
Sodium
mg/Kg
sno
464
e3.0
80'120
Zinc
mg/Kg
50.0
51.8
104
80'120
Matrix Spike Matrix Spike Duplicate
Parameter units
L9z9
MS Spike
Result Conc.
MSD MS Result MSD
Spike Result
Conc.
MS
O/oRec
MSD
O/oRec
O/oRes
Limits
RpD
Max
RPD
Aluminum
mg/no
2210
427
459
3240
3230
23*~
216~
75-125
0.3
20.0
Arsenic
mg/Kg
2.22
*.27
4.59
6.09
6.56
910
95.0
75'125
7.*
0.0
Cadmium
mg/Kg
0.688
4.27
4.59
4.*7
*.88
88.0
87.0
75-125
4.5
20.0
Calcium
mg/Kg
7310
127
459
9420
8050
*9*~
161*
75'125
2.0
20.0
commmm
mg/Kg
35.3
42.7
45.9
78.2
80.6
100
9e.0
75'125
3.0
20u
Copper
mg/Kg
Zoo
42./
+5.9
2*7
251
105
107
75'125
1.6
20.0
Lead
mg/Kg
9.08
4.27
4.59
13.1
13.5
9*.0
96.0
75'125
3.0
20.0
Magnesium
mg/Kg
3390
vZr
459
3990
4020
140*
87*
75-125
OJ
20.0
Molybdenum
mg/Kg
3.14
42.7
45.9
39.6
42.1
85.0
85.0
73'125
6.8
20.0
Nickel
mg/Kg
17.e
42.7
45.9
56.5
59.7
91.0
91.0
75'125
sJ
20.0
Potassium
mg/mg
3300
42.7
15.9
340
3400
491*
436*
75-125
0.2
20.0
Selenium
mg/Kg
<U.50U
*.27
4.59
3.58
4.51
8*.0
98.0
75'125
22.9*
20.0
Sodium
mg/Kg
359
427
459
783
796
99.0
95.0
75'125
1.6
20.0
Zinc
mg/Kg
376
42.7
*5.9
125
*29
115
116
75-125
019
208
Page 18 of 23

Waypoint,
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400' Fax 901.213,2440
ANALYTICAL
www.vi.iypoititatiaivtical.com
Quality Control Data
Client ID:
Brunswick County Public Utilities
Project Description:
WBR-NEBR
Report No:
23-059-0015
QC Prep:
L667045
QC Analytical Batch(es): L667310
QC Prep Batch Method:
7471A
Analysis Method: 7471A
Analysis Description: Solids Total Mercury Analysis - CVAA
Lab Reagent Blank
LRB-1-667045
Matrix: SOL
Associated Lab Samples:
92723, 92724, 92725
Parameter
Units
Blank
Result
MQL Analyzed
Mercury
mg/Kg
< 0.192
0,192 03/02/23 12:14
Laboratory Control Sample
LCS-1-667045
Parameter
Units
Spike
Conc.
LCS LCS %Rec % Rec
Result Limits
Mercury
mg/l<g
0.400
0.417 104 80-120
Matrix Spike & Matrix Spike
Duplicate
K 93579-MS-L667045
K 93579-MSD-L667045
Parameter
Units
MS Spike
MSD MS Result MSD MS MSD %Rec
Max
Result Conc.
Spike Result %Rec %Rec Limits
RPD RPD
Conc.
Mercury
mg/Kg
< 0.183 0.381
0.384 0.434 0.656 114 171* 80-120
40.7* 20.0
* QC Fail
Date: 03/15/2023
01:23 PM
Page 9 of 11
Page 19 of 23

QC Prep:
L668378
QC Analytical Batch(es): L668659
QC Prep Batch Method:
SW-9056A (PREP)
Analysis Method: 9056A
Analysis Description: Anions by Ion Chromatography
Lab Reagent Blank
LRB-L668378
Matrix: SOL
Associated Lab Samples:
92723, 92724, 92725
Parameter
Units
Blank
Result
MQL Analyzed
Nitrate (NO3-N)
mg/Kg
< 2.50
2.50 03/08/23 15:36
Nitrite (NO2-N)
mg/Kg
< 2.50
2.50 03/08/23 15:36
Laboratory Control Sample & LCSD
LCS-1-668378
LCSD-L668378
Parameter
Units
Spike
Conc.
LCS LCSD LCS LCSD
Result Result O/o Rec % Rec
% Rec
Limits
RPD Max
RPD
Nitrate (NO3-N)
mg/Kg
113
118 118 105 105
80-120
0.0 20.0
Nitrite (NO2-N)
mg/Kg
76.1
82.7 81.9 109 108
80-120
0.9 20.0
Matrix Spike & Matrix Spike Duplicate E 61170-MS-L668378 E 61170-MSD-L668378
Parameter
Units
MS Spike
MSD
MS Result MSD
MS
MSD
O/oRec
Max
Result
Conc.
Spike
Result
O/o Re c
O/oRec
Limits RPD
RPD
Conc.
Nitrate (NO3-N)
mg/Kg 381
112
109
453 444
64.0*
58.0*
80-120 2.0
15.0
Nitrite (NO2-N)
mg/Kg 591
75.3
73.4
615 599
32.0*
11.0*
80-120 2.6
15.0
* QC Fail Date: 03/15/2023 01:23 PM Page 10 of 11
Page 20 of 23

Waypoint
ANALYTICAL
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 Fax [phone]
WWW.lAjaypoititanalytical.com
Quality Control Data
Client ID: Brunswick County Public Utilities
Project Description: WBR-NEBR
Report No: 23-059-0015
QC Analytical Batch: L669660
Analysis Method: SW-DRYWT
Analysis Description: Dry Weight Determination
Duplicate L 92725-DUP
Result DUP
Parameter Units Result
Moisture % 97.2 97.2
0.0 20.0 03/14/23 16:00
Date: 03/15/2023 01:23 PM Page 11 of 11
Page 21 of 23

0
�mWm�nn�dMemph�nxau3s
WaypiRint ,momeoz.2za�nnn"�*eo1�13.z«4o
AYT/CAL www.wavpmotana/yticaLcom
Customer Number: 30914
Customer Name: Brunswick County Public Utilities
Report Number: 23-059-0015
Shipping Method
0Fed Ex 0USPostal 0Lab
�����\ UPS Client Courier
~~ `~ �/
0[8her:
Thermometer �
����-----------
�//vu
Shipping container/cooler uncompromioed?
Yes
/lNo
Number of coolers/boxes received
Custody seals intact on shipping container/cooler?
0 Yes
0 No
Not Present
Custody seals intact on sample bottles?
0 Yes
0 No
Not Present
Chain of Custody (COC) present?
Yes
0 No
COC agrees with sample label(s)?
Yes
0 No
COC properly completed
Yes
0 No
Samples in proper containers?
# Yes
0 No
Sample containers intact?
*Yeo
ONo
Sufficient sample volume for indicated test(s)?
* Yes
0 No
All samples received within holding time?
# Yes
0 No
Cooler temperature in compliance?
Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
Yes
ONo
Water - Sample containers properly preserved
Yes
ONo
0 N/A
Water - VOA vials free of headspace
0 Yes
0 No
N/A
Trip Blanks received with VOAs
0 Yes
0 No
N/A
Soil VOA method 5035 — compliance criteria met
0 Yes
ONo
N/A
High concentration container (48 hr)
�—High concentration pre -weighed (methanol '14d)
F_ Low concentration EnCore samplers (48 hr)
F— Low conopre-weighed vials (Sod Bia-14d)
Special precautions nrinstructions included?
Comments:
Signature: IMallory Earle Date &Time:
Page 22 of 23

wa *nto
11 YpAr! TICAL
Kit ID: 203303
I I_--
ia
nitiated By: Connie Cook
11 �11 n I Matedd Duate: 2/20/2023
T
Project Cornm ent
L
Main 901.213,2400 0 Fax [phone]
www,waypointanalytical.com
309 �4
HE F 1,111 E� 11 '�
,',.rBR NEBR. 01 7,3
Company Name
Company Number
Client Project Manager/Contact
Purchase Order Number
BrLMS,"NiCk Courity Public Utdities
30914
"vir NIatth,.-?,A, Her;fy
Site Name
Project Number
Method of Shipment
f
P,,
buy E--,
I —A
Cla'l- R,IulC,
UMS, Project ID
Project Manager Phone n
Project Manager Email
Site/Facility ID —H
CPU - 5l-s3 S:udlge Tettjng
K&,i31-86-16
DateT Sample ID
--� - ���
Matrix
Grab/
Cam p
fl of
, Cont
Container Type
Preservation
A nalyses
TS, To,,ab
'4 -.,2,
G I a s - 9oz
N,011,1
llho-, S013E metals Al, ,:a,
I S, of N. Ar rimonia. Tc tai.
ltr��.-Cllelt;,,,, P,11- ArAlo
90z
NONF
ph").S, �OH nieTals Al, "a,
. ......
Mqg, K, Na
G
21
Glass - 9,-
NONE
A!, C,
NIg. K, Na
For Laboratory Use Only
(ce Custody Lab Comments,
Seals
Y/N
81 a nk/Cooter Temp�,,
Sampled by (Name - Print) Client Remarks/Comments
Relinquished by: (SIGNATURE) Date Tome Received by: (SfGNATUREI Date Time
6
Relinquished by: (SIGNATURE) Date Time I Received by: (SIGNATURE) Date Time
Relinquished by: (SIGNATURE) Date Time Received by. (SIGNATURE) Date Time
Page 23 of 23

West Brunswick Regional WWTP
Non -Discharge Permit No. WQ0034513
Class B - 2023
Sample Date
Fecal Coliform
MPN per gram
Log
01/04/23
44
1.6435
01/04/23
44
1.6435
01/04/23
43
1.6335
01/04/23
44
1.6435
01/04/23
43
1,6335
01/04/23
44
1.6435
01/04/23
45
1.6532
Envirochem: 2023-00211
Total 1 11.4940
Average 1 1:6420
Geometric Mean 44 Fecal Coliform MPN / gram
Geometric Mean of Less than 2,000,000 MPN/gram meets Class B - Alternative B I Pathogen Reduction requirement

Cht Inist6w 111CCIP
411
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7,,,.0 Man�co, NIC 27954 , 252,4733.5702 Lab/Fax
255-P. IMmOgWn Qbway, 28541,0 , 9',",0347.5,11,40 Lalb/Fax
PubI, TJ 1:,� I i L11
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6602 WbdmM 121 TMmKgK% NC 2805 THUMB Lab ° 91039Z4424 Fax
710 Bowser,,ow.,n Road, Man,,ea, PIC 27954 , 252.4.1,73.5702 Lab/Fax
255-A ',/Vilmingtm-, Hljg.away, Jacksonville, -NIC 235�O 9103/17,5343 Lao/Fax
7 ";N
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POSPOWS BOX 249
Customer FI4
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Regional M/�/-[*,-
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All % OVOW023
<44 M P P,,Vg 0,1/0,4/2023
No 5N Sampld by
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Were custody seals present or, the C,oie,?
temperature
if CuVody seat vvere presc e
were the,,, inta t/unbr, k n?
li-'Clrigir,31
jHow tempenat,-tre
,P,,,,_
tai<cn:
C -orrEcted temperature upon receN
TErnperature Blank r'yj Minst Boom
Gun 3:
ThOolas
0aceab!e
S/N 210886S69 IF! Gun Cori-ecVon
� C
pa or 0.n
5" YES
11
Fj
N 0
3, If Lernperatjre of cooler exceeded was Pro ject bAgr)CIA lotiNed?
\/Vere umpor CusLod,,,, pro C edures (relin,,i�!isher-�'/�-eceiv�zd) fcllo�lved,?
r e S a M pie !D�s lisp e,i on t,,,�,c COC�r
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ES
F"
t\j n
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yiis(ed'
0- e C a n an g' t � rn (a on tnE C(DC?
YES
C1
r C,
NsK to be performed Key on me CDC?
I
YES
7T,
1 9. DO sams a
plerrive in proper &3ntainers -c)r each te5t?
L,10 sannp[es aHw2 in good condition for each
I UZI
YES
test.-�
2, s 7 je sample: VOiUnne avFilaWc .1'
le re sarnples received Whin proper hoWing time for
-j
YES
requested wscs?
T­ - -ve -,a rnipk2s
L 3, ,Ner e a c i d p re s e d
VES
a ", a PH of <22 ?
Abre cyajfdr,� Sarirjpie-� received PH'
V—
Lj
7-e
P,/e�n ?
Won Mde/Cyanide recen a,, E, r e s I cl tj a 1 o f < c,1. s
YES
Ej
P!, s p h V e s a m p 4 S p 1 h e N I d y", i t I-)
.I e checkud K tune, of J,IC:er-,ara'er,
MAN amples are checked for
Ch"ne at " Of MAYS 2nd r2DDMecj an the benchsheet.
S P &Awsir- be coj-niJk-md �,-r ary swnpok) Pr erved i- �Mth headspaQ
e s �, 1,
Wers, received "Oueck PoSeNed N
!by and vrere HOW accooky,! adding (circie on": H03 Ho N a Ql
11% of preseNaboii: cnc' PORNAve 0 d neede, nowe
1in nuornew Qwv
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nado the sn" No If "UH 10 Inalzed C�IAV Md =:
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fl;?-JIFS S2,mpi�
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SOIL ANALYSIS REPORTS

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