WQ0006017_2023 Residual Annual Report_20240219 (2)

Initial Review
Reviewer
nathaniel.thorn burg
Is this submittal an application? (Excluding additional information.) *
Yes No
If not an application what is the submittal type?* Annual Report
Residual Annual Report
Additional Information
Other
Annual Report Year* 2023
Permit Number (IR) * WQ0006017
Applicant/Permittee Town of Beaufort
Email Notifications
Does this need review by the hydrogeologist? * Yes U No
Regional Office Wilmington
CO Reviewer
Admin Reviewer Wanda Gerald

Submittal Form
Project Contact Information
Please provide information on the person to be contacted by NDB Staff regarding electronic submittal, confirmation of receipt, and other correspondence.
Name* Lysa Finnerty
Email Address*
[e-mail]
Project Information
.........................
Application/Document Type*
New (Fee Required)
Modification - Major (Fee Required)
Renewal with Major Modification (Fee
Required)
Annual Report
Additional Information
Other
Phone Number*
4105376150
Modification - Minor
Renewal
GW-59, NDMR, NDMLR, NDAR-1,
N DAR-2
Residual Annual Report
Change of Ownership
We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form.
https://edoes.deq.nc.gov/Forms/NonDischarge_Monitoring_Report
Permit Type:*
Wastewater Irrigation
High -Rate Infiltration
Other Wastewater
Reclaimed Water
Closed -Loop Recycle
Residuals
Single -Family Residence Wastewater
Other
Irrigation
Permit Number:*
WQ0006017
Has Current Existing permit number
Applicant/Permittee Address*
435 Williams Court, Ste 100, Baltimore, MD 21220
Facility Name*
Town of Beaufort Class B Residuals Program
Please provide comments/notes on your current submittal below.
Submission of the 2023 Annual Report for Town of Beaufort, NC
At this time, paper copies are no longer required. If you have any questions about what is required, please contact Nathaniel Thornburg
at [e-mail].
Please attach all information required or requested for this submittal to be reviewed here.
(Application Form, Engineering Plans, Specifications, Calculations, Etc.)
Beaufort NC 2023 Annual Report FINAL.pdf 3.23MB
Upload only 1 PDF document (less than 250 MB). Multiple documents must be combined into one PDF file unless file is larger
than upload limit.
* By checking this box, I acknowledge that I understand the application will not be accepted for pre -review until the fee (if required) has
been received by the Non -Discharge Branch. Application fees must be submitted by check or money order and made payable to the
North Carolina Department of Environmental Quality (NCDEQ). I also confirm that the uploaded document is a single PDF with all parts
of the application in correct order (as specified by the application).
Mail payment to:
NCDEQ — Division of Water Resources
Attn: Non -Discharge Branch
1617 Mail Service Center
Raleigh, NC 27699-1617
Signature
Alva �Cit'wt%tt,
Submission Date 2/19/2024

435 Williams Court, Suite 100
Baltimore, MD 21220
www.synagro.com
FEBRUARY 17, 2024
NCDEQ
Division of Water Resources
Information Processing Unit
1617 Mail Service Center
Raleigh, NC 27699-1617
Re: 2023 Annual Report for Permit No. WQ0006017
Dear NCDEQ:
SYNAGRO
Synagro is submitting one electronic copy of the above referenced report on behalf of the Town
of Beaufort, NC.
If you have any questions or need additional information, please do not hesitate to contact
Donovan Willis at [phone] or Matthew Carter at 336-705-9886.
Sincerely,
OP1Ul" .Shhf= R11
Derrick Shivar
Environmental Compliance Manager
Enclosures
cc: Donovan Willis — Town of Beaufort
Matthew Carter, Synagro
YOUR PARTNER FORA CLEANER, GREENERWORLD

TOWN OF BEAUFORT, NC
RESIDUALS LAND APPLICATION PROGRAM
Permit No. WQ0006017
2023 ANNUAL REPORT

Town of Beaufort, NC
Residuals Land Application Program
2023 Annual Report
TABLE OF CONTENTS
1. Certification Form and Annual Operations Summary
2. Annual Residual Sampling Summary Forms and Residuals
Analyses
3. Annual Land Application Field Summary Form
4. TCLP Analysis
5. Pathogen Reduction/Vector Attraction Reduction
6. Soil pH & Lime Application Records
7. Soil Analysis

SECTION 1

ANNUAL LAND APPLICATION CERTIFICATION FORM
Permit Number W00006017 County Carteret Year 2023
Facility Name (as shown on permit) Beaufort WWTP NPDES No. NCO021831
Land Application Operator Synagro Phone# [phone]
Land application of residuals as allowed by the above permit occurred during the past calendar year
X YES NO. If NO, skip Part A, and PartB and proceed to Part C. Also, if residuals were generated but not land applied,
please attach an explanation on how the residuals were handled.
Part A — Residuals Application Summary
*Total number of application fields in permit. 2
*Total number of fields utilized for land application during the year. 1
*Total amount of dry tons applied during the year for all application sites. 40.79
*Total number of acres utilized for land application during the year. 23.40
Part B — Annual Compliance Statement
Facility was compliant during calendar year 2023 with all conditions of the land application permit (including but not limited to items
1-13 below) issued by the Division of Water Quality X YES NO.
If no, please provide a written description why the facility was not compliant, the dates, and explain corrective action taken.
1. Only residuals approved for this permit were applied to the permitted sites.
2. Soil pH was adjusted as specified in the permit and time was applied (if needed) to achieve a soil pH of at least 6.0 or the
limit specified in the permit.
3. Annual soils analysis was performed on each site receiving residuals during the past calendar year and three (3) copies of
laboratory results are attached.
4. Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5. All other monitoring was performed in accordance with the permit and reported during the year as required and three (3 )
copies of certified laboratory results are attached.
6. The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .1105(a) or the Pollutant Loading
Rates in 15A NCAC 02T .l 105(b) (Applicable to 40 CFR Part 503 regulated facilities).
7. All general requirements as specified in the Land Application Permit were complied with (applicable to 40 CFR Part 503
regulated facilities).
8. All monitoring and reporting requirements in 15A NCAC 02T .1111 were complied with (applicable to 40 CFR Part 503
regulated facilities).
9. All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Quality.
10. No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
IL Vegetative cover was maintained and proper crop management was performed on each site receiving residuals, as specified
in the permit.
12. No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13. All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C — Certification
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate, and complete.
am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for
knowing violations."
Donovan Willis. Public Utilities Director
Permittee Name and Title (type or print)
Signature of Preparer* Date
(if different from Permittee)
Signature ofreripittee Date
1 / 1 /2024
S ature of L Applier Date
(if different from Permittee and Preparer)
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 02T .1102 (26) DENR FORM ACF (12/2006)

OPERATIONS SUMMARY - LAND APPLICATION - NORTH CAROLINA
ALL COUNTIES - ALL SITES
DATE RANGE: 1/1/2023 - 12/31/2023
BEAUFORT,NC
BEAUFORT, NC AEROBICALLY DIGESTED CAKE
MONTH/YEAR
May 2023
TOTAL
Units Key: D - Dry Tons; G — Gallons; W — Wet Tons; Y — Cubic Yards
Report Date: 1/29/2024 3:59:17 PM
AMOUNT UNIT DRY TONS UNIT DRY METRIC TONS
325.00 Y 40.79 D 36.99
325.00 Y 40.79 D 36.99

SECTION 2

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B
WQ Permit Number: W00006017 Laboratory:
Facility Name: BEAUFORT, NC Waypoint Analytical Virginia Inc.
Residual Source WQ # or
NPDES#: NCO021831
WWTP Name: BEAUFORT
Residual Analysis Data
Product Type
Sample or Composite Date
AEDCAK
03/30/23
Parameter (mg/kg dry weight)
Ceiling Conc.
Limit
Percent Solids (%)
NA
14.90
Arsenic
75
11.2
Cadmium
85
1.36
Copper
4300
579
Chromium
NA
26.1
Lead
840
24.3
Mercury
57
<1.23
Molybdenum
75
7.11
Nickel
420
16.8
Selenium
100
7.72
Zinc
7500
1200
Total Phosphorus
NA
23100
TKN
NA
69100
Ammonia -Nitrogen
NA
1050
Nitrate and Nitrite
NA
893
For surface disposal facilities the ceiling concentration limits listed in this form are not applicable. Reference the individual permit for metals limits
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified
personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the
possibility of fines and imprisonment for knowing violations."
/ � 1
Signature of Preparer' Date
'Preparer is defined in 40 CFR Part 503.9(r) and 15 A NCAC 2T.1102(26) DENR FORM RSSF (12/2006)
Printed: 1/29/2024 4:52:52 PM For: 2226 01

ANNUAL RESIDUAL SAMPLING SUMMARY FORM - B
Report all sampling analysis results for parameters not listed in FORM RSSF that are part of the WO permit or were analyzed for over the past
calendar year. Use additional forms as needed.
WQ Permit Number:
W00006017
Facility Name:
BEAUFORT, NC
Residual Source
NPDES # or WQ#:
NCO021831
WWTP Name:
BEAUFORT
Residual Analysis Data
Product Type
AEDCAK
Sample or Composite Date
03/30/23
Parameters (mg/kg dry weight)
Aluminium
7380
Calcium
36200
Magnesium
3560
pH (s.u.)
6.60
Potassium
2090
Sodium
2910
PAN
21833
SAR (Ratio)
1.5048
Laboratory:
Waypoint Analytical Virginia Inc.
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordiance with a system designed to assure that qualified
personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the
possibility of fines and imprisonment for knowing violations."
Signature of Preparer " Date
'Preparer is defined in 40 CFR Part 503.9(r) and 15 A NCAC 2T.1102(26)
Pnnted: V2912024 4:58:22 PM For: 2226 01 DENR FORM RSSF-B (12/2006)

Waypointo
ANALYTICAL
4/10/2023
Synagro Central LLC
Matthew Carter
284 Boger Rd
Mocksville, NC, 27028
Ref: Analytical Testing
Report Number: 23-090-0003
Project Description: Beaufort WWTP
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Dear Matthew Carter:
Waypoint Analytical Virginia, Inc. received sample(s) on 3/31/2023 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Brandi Watson
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 1 of 6

(D
waypoint 7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
ANALYTICAL www.waypointanalytical.com
Sample Summary Table
Report Number: 23-090-0003
Client Project Description: Beaufort WWTP
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
61565
61565
61565
61565
61565
61565
61565
61565
Beaufort WWTP N+M
Beaufort WWTP N+M
Beaufort WWTP N+M
Beaufort WWTP N+M
Beaufort WWTP N+M
Beaufort WWTP N+M
Beaufort WWTP N+M
Beaufort WWTP N+M
Solids
Solids
Solids
Solids
Solids
Solids
Solids
Solids
03/30/2023
07:00
03/31/2023
03/30/2023
07:00
03/31/2023
03/30/2023
07:00
03/31/2023
03/30/2023
07:00
03/31/2023
03/30/2023
07:00
03/31/2023
03/30/2023
07:00
03/31/2023
03/30/2023
07:00
03/31/2023
03/30/2023
07:00
03/31/2023
SM-4500-NH3C
WP MTN
9045D
WP MTN
4500NO3F-2011
WP MTN
6010D
WP MTN
SW-7471B
WP MTN
SM-4500-NH3C-TKN
WP MTN
SM-2540G
WP MTN
WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN
Page 2 of 6

0
Waypoint.
7621 Whitepine
Road, Richmond,
VA 23237
Main 804-743-9401 ° Fax
804-271-6446
ANALYTICAL
www.waypointanalytical.com
46431
Synagro Central LLC
Project
Beaufort WWTP
Matthew Carter
Report Date : 04/10/2023
284 Boger Rd
Information :
Received : 03/31/2023
Mocksville , NC 27028
(j
Brandi Watson
Report Number : 23-090-0003
REPOR T OF A NA L YSIS
Lab No : 61565
Matrix: Solids
Sample ID : Beaufort WWTP N+M
Sampled: 3/30/2023 7:00
Test
Results
Units
MQL
DF
Date / Time
By Analytical
Analyzed
Method
Moisture
85.1
%
0.010
1
04/05/2316:16
JLS SM-2540G
Phosphorus
23100
mg/Kg - dry
33.6
1
04/06/23 04:14
TJS 6010D
Sulfur
12600
mg/Kg - dry
67.1
1
04/06/23 04:14
TJS 6010D
Calcium
36200
mg/Kg - dry
336
1
04/06/23 04:14
TJS 6010D
Aluminum
7380
mg/Kg - dry
33.6
1
04/06/23 04:14
TJS 6010D
Manganese
596
mg/Kg - dry
3.36
1
04/06/23 04:14
TJS 6010D
Copper
579
mg/Kg - dry
3.36
1
04/06/23 04:14
TJS 6010D
Zinc
1200
mg/Kg - dry
8.39
1
04/06/23 04:14
TJS 6010D
Organic N
68050
mg/Kg - dry
1678
1
04/06/23 05:50
CALCULATION
Nickel
16.8
mg/Kg - dry
1.68
1
04/06/23 04:14
TJS 6010D
Lead
24.3
mg/Kg - dry
2.01
1
04/06/23 04:14
TJS 6010D
Arsenic
11.2
mg/Kg - dry
3.36
1
04/06/23 04:14
TJS 6010D
Selenium
7.72
mg/Kg - dry
3.36
1
04/06/23 04:14
TJS 6010D
Test
Results
Units
MQL
DF
Date / Time
By Analytical
Analyzed
Method
Total Solids 14.9 % 0.010 1 04/05/23 16:16 JLS SM-2540G
Qualifiers/ DF Dilution Factor
Definitions
MQL Method Quantitation Limit
Page 3 of 6

Waypointo
ANALYTICAL
46431
Synagro Central LLC
Project
Matthew Carter
284 Boger Rd
Information
Mocksville , NC 27028
Report Number : 23-090-0003
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Beaufort WWTP
REPORT OF ANAL YSIS
Report Date : 04/10/2023
Received : 03/31/2023
Brandi Watson
Lab No : 61565
Sample ID : Beaufort WWTP N + M
Matrix: Solids
Sampled: 3/30/2023 7:00
Total Kjeldahl Nitrogen
69100
mg/Kg - dry
1680
1
04/07/23 11:00
CLP ;M-4500-NH3C-TKP
Potassium
2090
mg/Kg - dry
67.1
1
04/06/23 22:16
BKN
6010D
Magnesium
3560
mg/Kg - dry
33.6
1
04/06/23 04:14
TJS
6010D
Sodium
2910
mg/Kg - dry
168
1
04/06/23 22:16
BKN
6010D
Iron
27900
mg/Kg - dry
67.1
1
04/06/23 04:14
TJS
6010D
Ammonia Nitrogen
1050
mg/Kg - dry
671
1
04/06/23 05:50
JPJ
SM-4500-NH3C
Nitrate+Nitrite-N
893
mg/Kg - dry
33.6
1
04/06/23 14:53
ZBD
4500NO3F-2011
Cadmium
1.36
mg/Kg - dry
0.671
1
04/06/23 04:14
TJS
6010D
Chromium
26.1
mg/Kg - dry
1.68
1
04/06/23 04:14
TJS
6010D
Mercury
<1.23
mg/Kg - dry
1.23
1
04/05/23 12:47
FDS
SW-7471B
pH
6.6
S.U.
1
04/06/2316:10
HBT
9045D
Total Volatile Solids
72.4
%
0.010
1
04/05/23 16:16
JLS
SM-2540G
Molybdenum
7.11
mg/Kg - dry
1.68
1
04/06/23 04:14
TJS
6010D
Qualifiers/ DF Dilution Factor
Definitions
MQL Method Quantitation Limit
Page 4 of 6

(2)
WayPAo Int..
NALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
www.waypointanalytical.com
Shipment Receipt Form
Customer Number: 46431
Customer Name: Synagro Central LLC
Report Number: 23-090-0003
Shipping Method
0 Fed Ex 0 US Postal 0 Lab 0 Other:
* UPS 0 Client 0 Courier Thermometer ID:
Shipping container/cooler uncompromised?
* Yes
0 No
Number of coolers/boxes received
F
Custody seals intact on shipping container/cooler?
0 Yes
0 No
Not Present
Custody seals intact on sample bottles?
0 Yes
0 No
Not Present
Chain of Custody (COC) present?
Yes
0 No
COC agrees with sample label(s)?
U Yes
0 No
COC properly completed
U Yes
0 No
Samples in proper containers?
U Yes
0 No
Sample containers intact?
Yes
0 No
Sufficient sample volume for indicated test(s)?
Yes
0 No
All samples received within holding time?
Yes
0 No
Cooler temperature in compliance?
Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
Yes
0 No
Water - Sample containers properly preserved
0 Yes
0 No
N/A
Water - VOA vials free of headspace
0 Yes
0 No
N/A
Trip Blanks received with VOAs
0 Yes
0 No
0 N/A
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
0 N/A
F_ High concentration container (48 hr) F Low concentration EnCore samplers (48 hr)
F_ High concentration pre -weighed (methanol -14 d) Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included?
0 Yes
0 No
Comments:
Signature: David Lennon Date & Time: 03/31/2023 08:48:46
Page 5 of 6

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Page 6 of 6

SECTION 3

FACILITY NAME: BEAUFORT, NC
LAND OWNER: WALTER WETHERINGTON
OPERATOR: ROBERT RIGGS
CROP 1 NAME: SOYBEANS (SB)
RESIDUAL SOURCE(S): * See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM Page: 1
WQ PERMIT #: W00006017 FIELD#: NC-CR-00007-0-0003-A ACRES UTILIZED: 23.4
ANNUAL DRY TONS APPLIED: 40.79 SITE #: NC CR 00007 ACRES PERMITTED: 23.4
PREDOMINANT SOIL SERIES: NORFOLK CATION EXCHANGE CAPACITY (NON-503):
CROP 1 MAX. PAN: 137 CROP 2 NAME: CROP 2 MAX. PAN:
Gallons (G)
Site
Name of Crop Type
or Cubic Yards (Y)
Cond.
Precip
Volati-
Mineral-
Ammonia
Nitrate
PAN Applied
Receiving Residual
Date or
or Wet Tons (W)
%
Residual
Dry, Wet,
Past 24 Hrs.
Application
lization
ization
TKN
Nitrogen
and Nitrite
(Ibs/acre)
Application
Month
Solids
Dry Tons/Ac
Source
Moist
Inches
Method*
Rate—
Rate'"
mg/kg
mg/kg
mg/kg
Amount
UOM
Crop 1
Crop 2
Crop 1
Crop 2
5/2/2023
250.00
(Y)
14.900
1.341
BAEDC
DRY
0-<1/2""
SURIN
1.0
0.30
69,100.00
1,050.00
893.00
59.952
SB
5/3/2023
75.00
(Y)
14.900
0.402
BAEDC
DRY
0-<1/2""
SURIN
1.0
0.30
69,100.00
1,050.00
893.00
17.986
SB
May-23
325.00
M
iotai 1.743 Total 77.938 0.000
AS CD CU CR PB HG MO NI SE ZN P Lime Applied
Annual Ibs/acre Applied 0.039 0.005 2.018 0.091 0.085 0.004 0.025 0.059 0.027 4.183 80.524 Date Lbs/Ac
Cumulative Ibs/acre Applied 0.629 I 0.248 I 48.939 I 6.455 I 2.967 I 0.163 I 0.501 I 3.027 0.409 77.006
Permit PAN Limit (Ibs/acre) 1st Crop 137
Federal C.P.L.R. (Ibs/acre)"""' 36.6 34.8 1,339.0 267.9 15.0 375.0 89.0 2,500.0
BAEDC = BEAUFORT, NC AEROBICALLY DIGESTED CAKE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am
aware that there are significant pe es o bmittin f e information, including the possibility of fines and imprisonment for knowing violations."
SIGNATURE OF LAND APPLIER DATE
NR = Not Reported or Not Required *"* Mineralization Rates: Compost-0.1, Anaerobically digested-0.2, Aerobically digested-0.3, Raw Sludge-0.4
Application Method: SUR - Surface, [NJ - Injection, SURIN - Incorporation "*** C.P.L.R.: Cumulative Pollutant Loading Rate
* Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 `**** See Site pH & Lime Application Records Section of Report
Printed: 1/24/2024 DENR FORM FSF (1212006)

SECTION 4

SUMMIT
ENVIRONMENTAL TECHNOLOGIES, INC
Analytical Laboratories
April 13, 2023
Matthew Carter
Synagro
284 Boger Rd.
Mocksville, NC 27028
TEL:
FAX:
RE: Beaufort WWTP
Dear Matthew Carter:
Summit Environmental Technologies, Inc.
3310 Win St.
Cuyahoga Falls, Ohio 44223
TEL: [phone] FAX.- [phone]
Website: http:llwww.settek.com
Order No.: 23032301
Summit Environmental Technologies, Inc. received 1 sample(s) on 3/31/2023 for the
analyses presented in the following report.
There were no problems with the analytical events associated with this report unless noted
in the Case Narrative.
Quality control data is within laboratory defined or method specified acceptance limits
except where noted.
If you have any questions regarding these tests results, please feel free to call the
laboratory.
Sincerely,
i 7,
Jennifer Woolf
Project Manager
3310 Win St.
Cuyahoga Falls, Ohio 44223
Arkansas 88-0735, California 2943, Colorado, Connecticut PH-0108, Florida NELAC E87688, Idaho OH00923, Illinois 200061, Indiana C-OH-13,
ISO/IEC 17025:2017 119125 L22-544, Kansas E-10347, Kentucky (Underground Storage Tank) 3, Kentucky 90146, Maryland 339, Michigan 9988,
Minnesota 1780279, Nevada 011009232020-1, New Hampshire 2996, New Jersey OH006, New York 11777, North Carolina 39705 and 631, North Dakota
R-201, Ohio DW, Ohio VAP C1,0052, Oklahoma 2019-155, Oregon OH2O0001, Pennsylvania 68-01335, Rhode Island LA000317, South Carolina
92016001, Texas T104704466-19-16, Utah OH009232020-12, Virginia VELAP 10381, West Virginia 9957C
Page 1 of 31

summly Summit Environmental Technologies, Inc. Case Narrative
3310 Win St.
ENVIRONMENTAL TECHNOLOGIES, INC. Cuyahoga Falls, Ohio 44223 wo#: 23032301
Analytical Laboratories TEL: [phone] FAX.- [phone]
Website: http://www.settek.com Date: 4/13/2023
CLIENT: Synagro
Project: Beaufort WWTP
WorkOrder Narrative:
23032301: This report in its entirety consists of the following documents: Cover Letter, Case Narrative,
Analytical Results, QC Summary Report, Applicable Accreditation Information, Chain -of -Custody,
Cooler Receipt Form, and other applicable forms as necessary. All documents contain the Summit
Environmental Technologies, Inc., Work Order Number assigned to this report.
Summit Environmental Technologies, Inc., holds the accreditations/certifications listed at the bottom of
the cover letter that may or may not pertain to this report. Please refer to the "Accreditation Program
Analytes Report" for accredited analytes list.
The information contained in this analytical report is the sole property of Summit Environmental
Technologies, Inc. and that of the customer. It cannot be reproduced in any form without the consent of
Summit Environmental Technologies, Inc. or the customer for which this report was issued. The results
contained in this report are only representative of the samples received. Conditions can vary at different
times and at different sampling conditions. Summit Environmental Technologies, Inc. is not responsible
for use or interpretation of the data included herein.
All results for Solid Samples are reported on an "as received" or "wet weight" basis unless indicated as
"dry weight" using the "-dry" designation on the reporting units.
This report is believed to meet all of the requirements of the accrediting agency, where applicable. Any
comments or problems with the analytical events associated with this report are noted below.
Analytical Sequence Sample Notes:
23032301-OOIA TCLP-SVOC_8270E: CCV exhibited high recovery for 2,4,5-Trichlorophenol. Sample
is ND for this analyte. Possible low bias for Pyridine due to low recovery in LCS-64065. LCSD-64065
demonstrates control for this analyte.
23032301-OOIA TCLP-VOC-MSTR_8260D: LCS-R161468 exhibited high recovery for Vinyl
Chloride. Sample is ND for this analyte.
Original
Page 2 of 31

SUMMIT Summit Environmental Technologies, In Qualifiers and Acronyms
3310 Win,'
ENVIRONMENTAL TECHNOLOGIES, INC Cuyahoga Falls, Ohio 442, WO#: 23032301
Analytical Laboratories TEL: [phone] FAX.- (330) 253-44E
Website: httv:11Www.settek.co Date: 4/13/2023
These commonly used Qualifiers and Acronyms may or may not be present in this report.
Qualifiers
U The compound was analyzed for but was not detected.
J The reported value is greater than the Method Detection Limit but less than the Reporting Limit.
H The hold time for sample preparation and/or analysis was exceeded.
D The result is reported from a dilution.
E The result exceeded the linear range of the calibration or is estimated due to interference.
MC The result is below the Minimum Compound Limit.
* The result exceeds the Regulatory Limit or Maximum Contamination Limit.
m Manual integration was used to determine the area response.
d Manual integration in which peak was deleted
N The result is presumptive based on a Mass Spectral library search assuming a 1:1 response.
P The second column confirmation exceeded 25% difference.
C The result has been confirmed by GC/MS.
X The result was not confirmed when GUMS Analysis was performed.
B/MB+ The analyte was detected in the associated blank.
G The ICB or CCB contained reportable amounts of analyte.
QC-/+ The CCV recovery failed low (-) or high (+).
R/QDR The RPD was outside of accepted recovery limits.
QL-/+ The LCS or LCSD recovery failed low (-) or high (+).
QLR The LCS/LCSD RPD was outside of accepted recovery limits.
QM-/+ The MS or MSD recovery failed low (-) or high (+).
QMR The MS/MSD RPD was outside of accepted recovery limits.
QV-/+ The ICV recovery failed low (-) or high (+).
S The spike result was outside of accepted recovery limits.
Z Deviation; A deviation from the method was performed; Please refer to the Case Narrative for
additional information
Acronyms
ND
Not Detected
RL
Reporting Limit
QC
Quality Control
MDL
Method Detection Limit
NIB
Method Blank
LOD
Level of Detection
LCS
Laboratory Control Sample
LOQ
Level of Quantitation
LCSD
Laboratory Control Sample Duplicate
PQL
Practical Quantitation Limit
QCS
Quality Control Sample
CRQL
Contract Required Quantitation Limit
DUP
Duplicate
PL
Permit Limit
MS
Matrix Spike
RegLvl
Regulatory Limit
MSD
Matrix Spike Duplicate
MCL
Maximum Contamination Limit
RPD
Relative Percent Different
MinCL
Minimum Compound Limit
ICV
Initial Calibration Verification
RA
Reanalysis
ICB
Initial Calibration Blank
RE
Reextraction
CCV
Continuing Calibration Verification
TIC
Tentatively Identified Compound
CCB
Continuing Calibration Blank
RT
Retention Time
RLC
Reporting Limit Check
CF
Calibration Factor
DF
Dilution Factor
RF
Response Factor
This list of Qualifiers and Acronyms reflects the most commonly utilized Qualifiers and Acronyms for reporting.
Please refer to the Analytical Notes in the Case Narrative for any Qualifiers or Acronyms that do not appear in this
list or for additional information regarding the use of these Qualifiers on reported data.
Original
Page 3 of 31

SUMMIT Summit Environmental Technologies, Inc.
3310 Win St.
ENVIRONMENTAL TECHNOLOGIES, INC Cuyahoga Falls, Ohio 44223
Analytical Laboratories TEL: [phone] FAX.- [phone]
Website: http://www.settek.com
CLIENT: Synagro
Project: Beaufort WWTP
Lab SampleID Client Sample ID
23032301-001 Beaufort WWTP TCLP
Tag No Date Collected
3/30/2023 7:00:00 AM
Workorder
Sample Summary
WO#: 23032301
Date Received
3/31/2023 10:05:00 AM
13 Apr-23
Matrix
Sludge
Page 4 of 31

SUMMIT
Summit Environmental Technologies, Inc.
3310 Win St.
DATES REPORT
ENVIRONMENTAL TECHNOLOGIES, INC
Cuyahoga Falls, Ohio 44223
WO#: 23032301
Analytical Laboratories
TEL: [phone] FAX.- [phone]
Website: http://www.settek.com
13 Apr-23
Client:
Synagro
Project:
Beaufort WWTP
Sample ID
Client Sample ID Collection Date Matrix Test Name Leachate Date
Prep Date Analysis Date
23032301-OOIA Beaufort WWTP TCLP 3/30/2023 7:00:00 AM Sludge Ignitability of Solids (SW-846: 1030)
4/5/2023 5:20:43 PM
pH (SW9045D)
4/5/2023 2:20:28 PM
Reactive Cyanide (9014/7.3.3.2)-Solid
4/5/2023 7:58:00 AM
Reactive Sulfide (9034)/7.3.4.2
4/4/2023 10:10:00 AM
TCLP Herbicides by EPA 8321B
4/5/2023 10:00:00 AM
TCLP Mercury Analysis (SW1311/7474/4/2023 3:35:00 PM
4/5/2023 2:15:00 PM 4/6/2023 9:21:00 AM
TCLP Metals Analysis (SW1311/6010'4/4/2023 3:35:00 PM
4/6/2023 11:26:00 AM
TCLP Pesticides Analysis (SW1311/8(4/4/2023 3:35:00 PM
4/6/2023 9:30:00 AM 4/12/2023 5:30:00 AM
TCLP Semi-Volatiles Analysis 4/4/2023 3:35:00 PM
4/5/2023 11:10:00 AM 4/7/2023 10:30:00 AM
(SW1311/8270)
TCLP Volatiles Analysis
4/5/2023 3:49:00 PM 4/7/2023 12:48:00 AM
Original
Page 5 of 31

SUMMIT Summit Environmental Technologies, Inc.
3310 Win St.
ENVIRONMENTAL TECHNOLOGIES, INC Cuyahoga Falls, Ohio 44223
Analytical Laboratories TEL: [phone] FAX: [phone]
Website: htW.-Ilwww.settek.com
CLIENT:
Synagro
Matrix:
SLUDGE
Lab ID:
23032301-OOIA
Project:
Beaufort WWTP
Client Sample ID Beaufort WWTP TCLP
Analytical Report
(base report)
WO#: 23032301
Date Reported: 4/13/2023
Tag Number:
Collection Date: 3/30/2023 7:00:00 AM
Analyses Result
RL
Qual
Units
DF
Date Analyzed
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
SW7470A
SW7470A Analyst: MP
TCLP MERCURY ANALYSIS (SW1311/7470)
TCLP Mercury
ND
0.00200
mg/L
1
4/6/2023 9:21:00 AM
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
SW6010
Analyst: RJE
TCLP METALS ANALYSIS (SW1311/6010)
TCLP Arsenic(As)
ND
0.500
mg/L
1
4/6/2023 11:26:00 AM
TCLP Barium(Ba)
ND
1.00
mg/L
1
4/6/2023 11:26:00 AM
TCLP Cadmium(Cd)
ND
0.100
mg/L
1
4/6/2023 11:26:00 AM
TCLP Chromium(Cr)
ND
0.200
mg/L
1
4/6/2023 11:26:00 AM
TCLP Lead(Pb)
ND
0.500
mg/L
1
4/6/2023 11:26:00 AM
TCLP Selenium(Se)
ND
0.0500
mg/L
1
4/6/2023 11:26:00 AM
TCLP Silver(Ag)
ND
0.500
mg/L
1
4/6/2023 11:26:00 AM
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
SW8270
SW3510C Analyst: JAP
TCLP SEMI-VOLATILES ANALYSIS (SW1311/8270)
1,4-Dichlorobenzene
ND
0.100
mg/L
1
4/7/2023 10:30:00 AM
2,4,5-Trichlorophenol
ND
0.250
QC+
mg/L
1
4/7/2023 10:30:00 AM
2,4,6-Trichlorophenol
ND
0.250
mg/L
1
4/7/2023 10:30:00 AM
2,4-Dinitrotoluene
ND
0.0500
mg/L
1
4/7/2023 10:30:00 AM
Cresols, Total
ND
5.00
mg/L
1
4/7/2023 10:30:00 AM
Hexachloro-1,3-butadiene
ND
0.0200
mg/L
1
4/7/2023 10:30:00 AM
Hexachlorobenzene
ND
0.0500
mg/L
1
4/7/2023 10:30:00 AM
Hexachloroethane
ND
0.100
mg/L
1
4/7/2023 10:30:00 AM
Nitrobenzene
ND
0.100
mg/L
1
4/7/2023 10:30:00 AM
Pentachlorophenol
ND
0.250
mg/L
1
4/7/2023 10:30:00 AM
Pyridine
ND
0.250
QL-
mg/L
1
4/7/2023 10:30:00 AM
Surr: 2-Fluorophenol
64.8
10 - 157
m
%Rec
1
4/7/2023 10:30:00 AM
Surr: Phenol-d6
62.4
10 - 169
%Rec
1
4/7/2023 10:30:00 AM
Surr: Nitrobenzene-d5
67.3
32.1 - 130
%Rec
1
4/7/2023 10:30:00 AM
Surr: 2,4,6-Tribromophenol
76.7
45.4 - 166
%Rec
1
4/7/2023 10:30:00 AM
Surr: 2-Fluorobiphenyl
70.4
35.7 - 130
%Rec
1
4/7/2023 10:30:00 AM
Surr: p-Terphenyl-d14
86.9
70 - 145
%Rec
1
4/7/2023 10:30:00 AM
Qualifiers: B
Analyte detected in the associated Method Blank
H
Holding times for preparation or analysis exceeded
MC
Value is below Minimum Compound Limit.
ND
Not Detected
P
Second column confirmation exceeds
R
RPD outside accepted recovery limits
E
M
N
OGl
PL
RL
Value above quantitation range
Manual Integration used to determine area response
Tentatively identified compounds
Permit Limit
Reporting Detection Limit
Original
Page 6of31

SUMMIT
Summit Environmental Technologies, Inc. Analytical Report
3310 Win St.
ENVIRONMENTAL TECHNOLOGIES, INC Cuyahoga Falls, Ohio 44223 (base report)
Analytical Laboratories TEL: [phone] FAX: [phone] WO#: 23032301
Website: htW.-Ilwww.settek.com Date Reported: 4/13/2023
CLIENT:
Synagro
Matrix:
SLUDGE
Lab ID:
23032301-OOIA
Project:
Beaufort WWTP
Client Sample ID Beaufort WWTP TCLP
Tag Number:
Collection Date: 3/30/2023 7:00:00 AM
Analyses
Result
RL
Qual Units
DF
Date Analyzed
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
SW8081
SW3510C Analyst: PGP
TCLP PESTICIDES ANALYSIS (SW1311/8081)
Chlordane, total
ND
0.0250
mg/L
10
4/12/2023 5:30:00 AM
Toxaphene
ND
0.0500
mg/L
10
4/12/2023 5:30:00 AM
Endrin
ND
0.00500
mg/L
10
4/12/2023 5:30:00 AM
gamma-BHC
ND
0.00500
mg/L
10
4/12/2023 5:30:00 AM
Heptachlor
ND
0.00500
mg/L
10
4/12/2023 5:30:00 AM
Heptachlor epoxide
ND
0.00500
mg/L
10
4/12/2023 5:30:00 AM
Methoxychlor
ND
0.00500
mg/L
10
4/12/2023 5:30:00 AM
Surr: TCMX
86.2
10 - 119
%Rec
10
4/12/2023 5:30:00 AM
Surr: DCB
83.1
10 - 119
%Rec
10
4/12/2023 5:30:00 AM
TCLP HERBICIDES BY EPA 8321 B
SW8321
Analyst: JDB
2,4-D
ND
0.500
mg/L
50
4/5/2023 10:00:00 AM
2,4,5-TP
ND
0.500
mg/L
50
4/5/2023 10:00:00 AM
Surr: 2,4-Dichlorophenylacetic aci
104
70 - 130
%Rec
50
4/5/2023 10:00:00 AM
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
SW8260
SW1311M
Analyst: EMB
TCLP VOLATILES ANALYSIS
1,1-Dichloroethene
ND
0.100
mg/L
20
4/7/2023 12:48:00 AM
1,2-Dichloroethane
ND
0.100
mg/L
20
4/7/2023 12:48:00 AM
MEK
ND
2.00
mg/L
20
4/7/2023 12:48:00 AM
Benzene
ND
0.100
mg/L
20
4/7/2023 12:48:00 AM
Carbon tetrachloride
ND
0.100
mg/L
20
4/7/2023 12:48:00 AM
Chlorobenzene
ND
1.00
mg/L
20
4/7/2023 12:48:00 AM
Chloroform
ND
0.100
mg/L
20
4/7/2023 12:48:00 AM
Tetrachloroethene
ND
0.100
mg/L
20
4/7/2023 12:48:00 AM
Trichloroethene
ND
0.100
mg/L
20
4/7/2023 12:48:00 AM
Vinyl chloride
ND
0.0400
QL+ mg/L
20
4/7/2023 12:48:00 AM
Surr: 4-Bromofluorobenzene
95.2
70 - 130
%Rec
20
4/7/2023 12:48:00 AM
Surr: Dibromofluoromethane
102
70 - 130
%Rec
20
4/7/2023 12:48:00 AM
Surr: Toluene-d8
97.3
70 - 130
%Rec
20
4/7/2023 12:48:00 AM
Qualifiers: B
Analyte detected in the associated Method Blank
E
Value above quantitation range
H
Holding times for preparation or analysis exceeded
M
Manual Integration used to determine area response
MC
Value is below Minimum Compound Limit.
N
Tentatively identified compounds
ND
Not Detected
OGI
P
Second column confirmation exceeds
PL
Permit Limit Original
R
RPD outside accepted recovery limits
RL
Reporting Detection Limit
Page 7of31

SUMMIT Summit Environmental Technologies, Inc. Analytical Report
3310 Win St.
ENVIRONMENTAL TECHNOLOGIES, INC Cuyahoga Falls, Ohio 44223 (base report)
Analytical Laboratories TEL: [phone] FAX.- [phone] WO#: 23032301
Website: http://www.settek.com Date Reported: 4/13/2023
CLIENT: Synagro Tag Number:
Matrix: SLUDGE Collection Date: 3/30/2023 7:00:00 AM
Lab ID: 23032301-OOIA
Project: Beaufort WWTP
Client Sample ID Beaufort WWTP TCLP
Analyses Result RL Qual Units DF Date Analyzed
RCI SW9014 Analyst: KMS
REACTIVE CYANIDE (9014/7.3.3.2)-SOLID
Cyanide, Reactive ND 12.4 mg/Kg 1 4/5/2023 7:58:00 AM
IGNITABILITY OF SOLIDS (SW-846: 1030) SW1030 Analyst: SMZ
Ignitability non-flammable mm/sec 1 4/5/2023 5:20:43 PM
RCI SW9045D Analyst: SMZ
PH (SW9045D)
pH 8.5 s.u.@21.8C 1 4/5/2023 2:20:28 PM
RCI SW9034 Analyst: KMS
REACTIVE SULFIDE (9034)/7.3.4.2
Sulfide, Reactive ND 25.0 mg/Kg 1 4/4/2023 10:10:00 AM
Qualifiers: B
Analyte detected in the associated Method Blank
H
Holding times for preparation or analysis exceeded
MC
Value is below Minimum Compound Limit.
ND
Not Detected
P
Second column confirmation exceeds
R
RPD outside accepted recovery limits
E Value above quantitation range
M Manual Integration used to determine area response
N Tentatively identified compounds
OGl
PL Permit Limit Original
RL Reporting Detection Limit
Page 8 of 31

Summit Environmental Technologies, Inc.
Accreditation
Program
3310 Win St.
SUMMIEF
Anal te5 Report
Y p
ENVIRONMENTAL TECHNOLOGIES,
INC Cuyahoga Falls, Ohio 44223
Analytical Laboratories
TEL: [phone] FAX.- [phone]
WO#:
23032301
Website: hgp:llwww.settek.com
13 Apr-23
Client: Synagro
State: NW
Project: Beaufort WWTP
Program Name: NC WW SCM
Sample ID Matrix
Test Name
Analyte
Status
23032301-OOIA Sludge
Ignitability of Solids (SW-846: 1030)
Ignitability
A
Sludge
pH (SW9045D)
Hydrogen Ion (pH)
A
Sludge
Reactive Cyanide (9014/7.3.3.2)-Solid
Cyanide, Reactive
U
Sludge
Reactive Sulfide (9034)/7.3.4.2
Sulfide, Reactive
U
Sludge
TCLP Herbicides by EPA 8321B
2,4,5-TP
A
Sludge
TCLP Herbicides by EPA 8321B
2,4-D
A
Sludge
TCLP Mercury Analysis (SW1311/7470)
Mercury
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Arsenic
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Barium
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Cadmium
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Chromium
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Lead
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Selenium
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Silver
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
Chlordane, total
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
Endrin
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
gamma-BHC
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
Heptachlor
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
Heptachlor epoxide
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
Methoxychlor
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
Toxaphene
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
1,4-Dichlorobenzene
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
2,4,5-Trichlorophenol
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
2,4,6-Trichlorophenol
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
2,4-Dinitrotoluene
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Cresols, Total
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Hexachlorobenzene
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Hexachlorobutadiene
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Hexachloroethane
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Nitrobenzene
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Pentachlorophenol
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Pyridine
A
Key
Key
NC WW SCM A Accredited
NC WW SCM U Unavailable
Original #1
Page 9 of 31

Summit Environmental Technologies, Inc.
Accreditation
Program
3310 Win St.
SUMMIEF
Anal te5 Report
Y p
ENVIRONMENTAL TECHNOLOGIES,
INC Cuyahoga Falls, Ohio 44223
Analytical Laboratories
TEL: [phone] FAX.- [phone]
WO#:
23032301
Website: hgp:llwww.settek.com
13 Apr-23
Client: Synagro
State: NW
Project: Beaufort WWTP
Program Name: NC WW SCM
Sample ID Matrix
Test Name
Analyte
Status
23032301-OOIA Sludge
TCLP Volatiles Analysis
1, 1 -Dichloroethene
A
Sludge
TCLP Volatiles Analysis
1,2-Dichloroethane
A
Sludge
TCLP Volatiles Analysis
2-Butanone
A
Sludge
TCLP Volatiles Analysis
Benzene
A
Sludge
TCLP Volatiles Analysis
Carbon tetrachloride
A
Sludge
TCLP Volatiles Analysis
Chlorobenzene
A
Sludge
TCLP Volatiles Analysis
Chloroform
A
Sludge
TCLP Volatiles Analysis
Tetrachloroethene
A
Sludge
TCLP Volatiles Analysis
Trichloroethene
A
Sludge
TCLP Volatiles Analysis
Vinyl chloride
A
NC WW SCM A Accredited NC WW SCM U Unavailable
Original #1
Page 10 of 31

SUMMIT Summit Environmental Technologies, Inc.
3310 Win St.
ENVIRONMENTAL TECHNOLOGIES, INC Cuyahoga Falls, Ohio 44223
Analytical Laboratories TEL: [phone] FAX: [phone]
Website: http://www.settek.coni
Client: Synagro
Project: Beaufort WWTP
QC SUMMARY REPORT
BatchlD: 64065
WO#: 23032301
13 Apr-23
Sample ID: MB-64065
SampType: MBLK
TestCode: SVOC-BNA_T Units: mg/L
Prep Date: 4/5/2023
RunNo: 161430
3lient ID: PBS
Batch ID: 64065
TestNo: SW8270 SW3510C
Analysis Date: 4/7/2023
SegNo: 4290266
analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
1,4-Dichlorobenzene
ND
0.0250
2,4,5-Trichlorophenol
ND
0.0250
2,4,6-Trichlorophenol
ND
0.0250
2,4-Dinitrotoluene
ND
0.0250
o-Cresol
ND
0.250
Cresols, Total
ND
0.0500
Hexachloro-1,3-butadiene
ND
0.0250
Hexachlorobenzene
ND
0.0250
Hexachloroethane
ND
0.0250
Nitrobenzene
ND
0.0250
Pentachlorophenol
ND
0.0250
Pyridine
ND
0.0250
Surr: 2-Fluorophenol
0.569
Surr: Phenol-d6
0.640
Surr: Nitrobenzene-d5
0.477
Surr: 2,4,6-Tribromophenol
0.771
Surr: 2-Fluorobiphenyl
0.490
Surr: p-Terphenyl-d14
0.897
1.000
56.9
10
135
1.000
64.0
10
161
1.000
47.7
16.8
150
1.000
77.1
32.5
179
1.000
49.0
34
133
1.000
89.7
60.8
163
QC+
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal,
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected OGl P Second column confirmation exceeds Original
PL Permit Limit R RPD outside accepted recovery limits RL Reporting Detection Limit
Page 11 of 31

SUMMIT Summit Environmental Technologies, Inc.
3310 Win St.
ENVIRONMENTAL TECHNOLOGIES, INC Cuyahoga Falls, Ohio 44223
Analytical Laboratories TEL: [phone] FAX: [phone]
Website: http://www.settek.coni
Client: Synagro
Project: Beaufort WWTP
QC SUMMARY REPORT
BatchlD: 64065
WO#: 23032301
13 Apr-23
Sample ID: LCS-64065
SampType: LCS
TestCode: SVOC-BNA_T Units: mg/L
Prep Date: 4/5/2023
RunNo: 161430
3lient ID: LCSS
Batch ID: 64065
TestNo: SW8270 SW3510C
Analysis Date: 4/7/2023
SegNo: 4290267
analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
1,4-Dichlorobenzene
0.353
0.0250
0.8000
0
44.2
35
130
2,4,5-Trichlorophenol
0.589
0.0250
0.8000
0
73.6
44
144
2,4,6-Trichlorophenol
0.558
0.0250
0.8000
0
69.8
45
141
2,4-Dinitrotoluene
0.640
0.0250
0.8000
0
80.0
56
136
o-Cresol
0.410
0.250
0.8000
0
51.2
36
134
Cresols, Total
0.936
0.0500
1.600
0
58.5
36
135
Hexachloro-1,3-butadiene
0.309
0.0250
0.8000
0
38.6
30
130
Hexachlorobenzene
0.531
0.0250
0.8000
0
66.4
58
130
Hexachloroethane
0.323
0.0250
0.8000
0
40.4
28
130
Nitrobenzene
0.512
0.0250
0.8000
0
64.0
39
133
Pentachlorophenol
0.587
0.0250
0.8000
0
73.4
33
151
Pyridine
0.0750
0.0250
0.8000
0
9.38
10
130
Surr: 2-Fluorophenol
0.530
1.000
53.0
10
135
Surr: Phenol-d6
0.592
1.000
59.2
10
161
Surr: Nitrobenzene-d5
0.469
1.000
46.9
16.8
150
Surr:2,4,6-Tribromophenol
0.764
1.000
76.4
32.5
179
Surr:2-Fluorobiphenyl
0.504
1.000
50.4
34
133
Surr: p-Terphenyl-d14
0.705
1.000
70.5
60.8
163
QC+
SmQLR
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal,
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected OGl P Second column confirmation exceeds Original
PL Permit Limit R RPD outside accepted recovery limits RL Reporting Detection Limit
Page 12 of 31

SUMMIT Summit Environmental Technologies, Inc.
3310 Win St.
ENVIRONMENTAL TECHNOLOGIES, INC Cuyahoga Falls, Ohio 44223
Analytical Laboratories TEL: [phone] FAX: [phone]
Website: http://www.settek.coni
Client: Synagro
Project: Beaufort WWTP
QC SUMMARY REPORT
BatchlD: 64065
WO#: 23032301
13 Apr-23
Sample ID: LCSD-64065
SampType: LCSD
TestCode: SVOC-BNA_T Units: mg/L
Prep Date: 4/5/2023
RunNo: 161430
3lient ID: LCSS02
Batch ID: 64065
TestNo: SW8270 SW3510C
Analysis Date: 4/7/2023
SegNo: 4290268
analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
1,4-Dichlorobenzene
0.355
0.0250
0.8000
0
44.4
35
130
0.3532
0.621
30
2,4,5-Trichlorophenol
0.499
0.0250
0.8000
0
62.4
44
144
0.5892
16.6
30 QC+
2,4,6-Trichlorophenol
0.485
0.0250
0.8000
0
60.6
45
141
0.5584
14.0
30
2,4-Dinitrotoluene
0.547
0.0250
0.8000
0
68.4
56
136
0.6396
15.6
30
o-Cresol
0.366
0.250
0.8000
0
45.8
36
134
0.4096
11.2
30
Cresols, Total
0.831
0.0500
1.600
0
51.9
36
135
0.9360
11.9
30
Hexachloro-1,3-butadiene
0.334
0.0250
0.8000
0
41.7
30
130
0.3088
7.78
30
Hexachlorobenzene
0.571
0.0250
0.8000
0
71.4
58
130
0.5314
7.25
30
Hexachloroethane
0.339
0.0250
0.8000
0
42.4
28
130
0.3234
4.83
30
Nitrobenzene
0.460
0.0250
0.8000
0
57.5
39
133
0.5122
10.7
30
Pentachlorophenol
0.550
0.0250
0.8000
0
68.8
33
151
0.5870
6.51
30
Pyridine
0.143
0.0250
0.8000
0
17.8
10
130
0.07500
62.1
30 Rm
Surr: 2-Fluorophenol
0.486
1.000
48.6
10
135
0
Surr: Phenol-d6
0.520
1.000
52.0
10
161
0
Surr: Nitrobenzene-d5
0.511
1.000
51.1
16.8
150
0
Surr: 2,4,6-Tribromophenol
0.631
1.000
63.1
32.5
179
0
Surr:2-Fluorobiphenyl
0.607
1.000
60.7
34
133
0
Surr: p-Terphenyl-d14
0.643
1.000
64.3
60.8
163
0
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal,
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected OGl P Second column confirmation exceeds Original
PL Permit Limit R RPD outside accepted recovery limits RL Reporting Detection Limit
Page 13 of 31

SUMMIT Summit Environmental Technologies, Inc.
3310 Win St.
ENVIRONMENTAL TECHNOLOGIES, INC Cuyahoga Falls, Ohio 44223
Analytical Laboratories TEL: [phone] FAX: [phone]
Website: http://www.settek.coni
QC SUMMARY REPORT
WO#: 23032301
13 Apr-23
Client: Synagro
Project: Beaufort WWTP BatchlD: 64086
TCLP Mercury ND 0.00200
TCLP Mercury 0.00403 0.00200 0.00400 0 101 80 120
TCLP Mercury 0.00411 0.00200 0.00400 0 103 75 125
Sample ID: 23032338-001AMSD
SampType: MSD
TestCode: HG_TCLP(74 Units: PPM
Prep Date: 4/5/2023
RunNo: 161324
Client ID: BatchQC
Batch ID: 64086
TestNo: SW7470A SW7470A
Analysis Date: 4/6/2023
SegNo: 4287390
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
TCLP Mercury 0.00405 0.00200
0.00400 0 101 75
125
0.00411 1.47 20
Qualifiers: B Analyte detected in the associated Method Blank
E Value above quantitation range
H
Holding times for preparation or anal,
J Analyte detected below quantitation limits
M Manual Integration used to determine area response
MC
Value is below Minimum Compound
Original
ND Not Detected
OGl
P
Second column confirmation exceeds
PL Permit Limit
R RPD outside accepted recovery limits
RL
Reporting Detection Limit
Page 14 of 31

SUMMIT Summit Environmental Technologies, Inc.
3310 Win St.
ENVIRONMENTAL TECHNOLOGIES, INC Cuyahoga Falls, Ohio 44223
Analytical Laboratories TEL: [phone] FAX.- [phone]
Website: hgp:llwww.settek.com
QC SUMMARY REPORT
Client: Synagro
Project: Beaufort WWTP BatchID: 64086
WO#: 23032301
13-Apr-23
Sample ID: 23032338-001AMSD
SampType: MSD
TestCode: HG_TCLP(74 Units: PPM
Prep Date: 4/5/2023
RunNo: 161324
Dient ID: BatchQC
Batch ID: 64086
TestNo: SW7470A SW7470A
Analysis Date: 4/6/2023
SegNo: 4287390
4nalyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal,
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected OGl P Second column confirmation exceeds Original
PL Permit Limit R RPD outside accepted recovery limits RL Reporting Detection Limit
Page 15 of 31

SUMMIT Summit Environmental Technologies, Inc.
3310 Win St.
ENVIRONMENTAL TECHNOLOGIES, INC Cuyahoga Falls, Ohio 44223
Analytical Laboratories TEL: [phone] FAX: [phone]
Website: http://www.settek.coni
Client: Synagro
Project: Beaufort WWTP
QC SUMMARY REPORT
WO#: 23032301
13 Apr-23
BatchlD: 64091
Sample ID: MB-64091
SampType: MBLK
TestCode: TCLP-SVOC- Units: mg/L
Prep Date: 4/6/2023
RunNo: 161689
Client ID: PBS
Batch ID: 64091
TestNo: SW8081 SW3510C
Analysis Date: 4/11/2023
SegNo: 4297191
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Chlordane, total
ND
0.00250
Toxaphene
ND
0.00500
Endrin
ND
0.000500
gamma-BHC
ND
0.000500
Heptachlor
ND
0.000500
Heptachlor epoxide
ND
0.000500
Methoxychlor
ND
0.000500
Sum TCMX
13.9
Sum DCB
9.11
20.00 69.5 10 119
20.00 45.6 10 119
Sample ID: LCS-64091
SampType: LCS
TestCode: TCLP-SVOC- Units: mg/L
Prep Date: 4/6/2023
RunNo: 161689
Client ID: LCSS
Batch ID: 64091
TestNo: SW8081 SW3510C
Analysis Date: 4/11/2023
SegNo: 4297192
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Chlordane, tota
Toxaphene
Endrin
gamma-BHC
Heptachlor
Heptachlor epo
Methoxychlor
Surr: TCMX
Qualifiers:
1 0.0203
0.0
ND
0.0
0.0104
0.00
0.00922
0.00
0.0101
0.00
xide 0.0101
0.00
0.0116
0.00
13.7
B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
PL Permit Limit
0250
0
0
70
0500
0
0
70
0500
0.0100 0
104
10
0500
0.0100 0
92.2
10
0500
0.0100 0
101
10
0500
0.0100 0
101
10
0500
0.0100 0
116
10
20.00
68.7
10
E Value above quantitation range
M Manual Integration used to determine area response
OGl
R RPD outside accepted recovery
limits
130
130
130
130
130
130
178
130
H Holding times for preparation or anal,
MC Value is below Minimum Compound
P Second column confirmation exceeds
RL Reporting Detection Limit
Original
Page 16 of 31

SUMMIT Summit Environmental Technologies, Inc.
3310 Win St.
ENVIRONMENTAL TECHNOLOGIES, INC Cuyahoga Falls, Ohio 44223
Analytical Laboratories TEL: [phone] FAX: [phone]
Website: http://www.settek.coni
Client: Synagro
Project: Beaufort WWTP
QC SUMMARY REPORT
WO#: 23032301
13 Apr-23
BatchlD: 64091
Sample ID: LCS-64091
SampType: LCS
TestCode: TCLP-SVOC- Units: mg/L
Prep Date: 4/6/2023
RunNo: 161689
Client ID: LCSS
Batch ID: 64091
TestNo: SW8081 SW3510C
Analysis Date: 4/11/2023
SegNo: 4297192
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Surr: DCB 12.1 20.00 60.6 10 130
Sample ID: LCSD-64091
SampType: LCSD
TestCode: TCLP-SVOC- Units: mg/L
Prep Date: 4/6/2023
RunNo: 161689
Client ID: LCSS02
Batch ID: 64091
TestNo: SW8081 SW3510C
Analysis Date: 4/11/2023
SegNo: 4297193
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Chlordane, total
0.0207
0.00250
0
0
70
130
0.0203
2.01
30
Toxaphene
ND
0.00500
0
0
70
130
0
0
30
Endrin
0.0112
0.000500
0.0100
0
112
10
130
0.0104
7.40
30
gamma-BHC
0.00957
0.000500
0.0100
0
95.7
10
130
0.00922
3.72
30
Heptachlor
0.0107
0.000500
0.0100
0
107
10
130
0.0101
5.26
30
Heptachlor epoxide
0.0106
0.000500
0.0100
0
106
10
130
0.0101
4.99
30
Methoxychlor
0.0130
0.000500
0.0100
0
130
10
178
0.0116
10.9
30
Sum TCMX
14.2
20.00
71.1
10
130
0
Sum DCB
7.87
20.00
39.3
10
130
0
Qualifiers: B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
PL Permit Limit
E Value above quantitation range H Holding times for preparation or anal,
M Manual Integration used to determine area response MC Value is below Minimum Compound
OGl P Second column confirmation exceeds
R RPD outside accepted recovery limits RL Reporting Detection Limit
Original
Page 17 of 31

SUMMIT Summit Environmental Technologies, Inc.
3310 Win St.
ENVIRONMENTAL TECHNOLOGIES, INC Cuyahoga Falls, Ohio 44223
Analytical Laboratories TEL: [phone] FAX: [phone]
Website: http://www.settek.coni
Client: Synagro
Project: Beaufort WWTP
QC SUMMARY REPORT
WO#: 23032301
13 Apr-23
BatchlD: R161235
Sample ID: 23032117-001AMS
SampType: MS
TestCode: Sulfide,React Units: mg/Kg
Prep Date:
RunNo: 161235
Client ID: Batch=
Batch ID: R161235
TestNo: SW9034
Analysis Date: 4/4/2023
SegNo: 4284904
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Sulfide, Reactive 3960 25.0 4580 0 86.5 80 120
Sample ID: 23032117-001AMSD
SampType: MSD
TestCode: Sulfide,React Units: mg/Kg
Prep Date:
RunNo: 161235
Client ID: Batch=
Batch ID: R161235
TestNo: SW9034
Analysis Date: 4/4/2023
SegNo: 4284905
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Sulfide, Reactive 3850 25.0 4580 0 84.1 80 120 3960 2.79 30
Qualifiers: B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
PL Permit Limit
E Value above quantitation range H Holding times for preparation or anal,
M Manual Integration used to determine area response MC Value is below Minimum Compound
OGl P Second column confirmation exceeds
R RPD outside accepted recovery limits RL Reporting Detection Limit
Original
Page 18 of 31

SUMMIT Summit Environmental Technologies, Inc.
3310 Win St.
ENVIRONMENTAL TECHNOLOGIES, INC Cuyahoga Falls, Ohio 44223
Analytical Laboratories TEL: [phone] FAX: [phone]
Website: http://www.settek.coni
Client: Synagro
Project: Beaufort WWTP
QC SUMMARY REPORT
WO#: 23032301
13 Apr-23
BatchlD: R161235
Sample ID: MB-R161235
SampType: MBLK
TestCode: Sulfide,React Units: mg/L
Prep Date:
RunNo: 161235
Client ID: PBW
Batch ID: R161235
TestNo: SW9034
Analysis Date: 4/4/2023
SegNo: 4284895
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Sulfide, Reactive ND 25.0
Sample ID: LCS-111161235
SampType: LCS
TestCode: Sulfide,React Units: mg/L
Prep Date:
RunNo: 161235
Client ID: LCSW
Batch ID: R161235
TestNo: SW9034
Analysis Date: 4/4/2023
SegNo: 4284896
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Sulfide, Reactive
4250 25.0 4580 0 92.8 85 115
Qualifiers: B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
PL Permit Limit
E Value above quantitation range H Holding times for preparation or anal,
M Manual Integration used to determine area response MC Value is below Minimum Compound
OGl P Second column confirmation exceeds
R RPD outside accepted recovery limits RL Reporting Detection Limit
Original
Page 19 of 31

SUMMIT Summit Environmental Technologies, Inc
3310 Win St
ENVIRONMENTAL TECHNOLOGIES, INC Cuyahoga Falls, Ohio 44223
Analytical Laboratories TEL: [phone] FAX: [phone]
Website: http://www.settek.coni
Client: Synagro
Project: Beaufort WWTP
Cyanide, Reactive ND 12.5
QC SUMMARY REPORT
WO#: 23032301
13 Apr-23
BatchlD: R161250
Cyanide, Reactive ND 12.5 10.00 0 95.5 85 115
Cyanide, Reactive ND 12.5 0.5000 0 57.5 50 150
Sample ID: 23032117-001AMS
SampType: MS
TestCode: Cyanide,Rea Units: mg/Kg
Prep Date:
RunNo: 161250
Client ID: BatchQC
Batch ID: R161250
TestNo: SW9014
Analysis Date: 4/5/2023
SegNo: 4285564
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
Cyanide, Reactive
ND 12.3
1.000 0 40.4 75
125
S
Qualifiers: B
Analyte detected in the associated Method Blank
E Value above quantitation range
H
Holding times for preparation or anal,
J
Analyte detected below quantitation limits
M Manual Integration used to determine area response
MC
Value is below Minimum Compound
Original
ND
Not Detected
OGl
P
Second column confirmation exceeds
PL
Permit Limit
R RPD outside accepted recovery limits
RL
Reporting Detection Limit
Page 20 of 31

SUMMIT Summit Environmental Technologies, Inc.
3310 Win St.
ENVIRONMENTAL TECHNOLOGIES, INC Cuyahoga Falls, Ohio 44223
Analytical Laboratories TEL: [phone] FAX: [phone]
Website: http://www.settek.coni
Client: Synagro
Project: Beaufort WWTP
QC SUMMARY REPORT
WO#: 23032301
13 Apr-23
BatchlD: R161250
Sample ID: 23032117-001AMS
SampType: MS
TestCode: Cyanide,Rea Units: mg/Kg
Prep Date:
RunNo: 161250
Client ID: Batch=
Batch ID: R161250
TestNo: SW9014
Analysis Date: 4/5/2023
SegNo: 4285564
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Sample ID: 23032117-001AMSD
SampType: MSD
TestCode: Cyanide,Rea Units: mg/Kg
Prep Date:
RunNo: 161250
Client ID: Batch=
Batch ID: R161250
TestNo: SW9014
Analysis Date: 4/5/2023
SegNo: 4285565
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Cyanide, Reactive ND 12.1 1.000 0 41.7 75 125 0 0 10 S
Qualifiers: B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
PL Permit Limit
E Value above quantitation range H Holding times for preparation or anal,
M Manual Integration used to determine area response MC Value is below Minimum Compound
OGl P Second column confirmation exceeds
R RPD outside accepted recovery limits RL Reporting Detection Limit
Original
Page 21 of 31

SUMMIT Summit Environmental Technologies, Inc
3310 Win St
ENVIRONMENTAL TECHNOLOGIES, INC Cuyahoga Falls, Ohio 44223
Analytical Laboratories TEL: [phone] FAX: [phone]
Website: http://www.settek.coni
Client: Synagro
Project: Beaufort WWTP
QC SUMMARY REPORT
WO#: 23032301
13 Apr-23
BatchlD: R161269
Sample ID: 23032266-001ADUP
SampType: DUP
TestCode: pH_S(9045D) Units: s.u.@22.1C
Prep Date:
RunNo: 161269
Client ID: Batch=
Batch ID: R161269
TestNo: SW9045D
Analysis Date: 4/5/2023
SegNo: 4287007
Analyte
Result
PQL SPK value SPK Ref Val %REC
Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
pH 9.2
0 0 0 0 9.2 0.2 10
Sample ID: LCS-R161269
SampType: LCS
TestCode: pH_S(9045D) Units: s.u.@22.00
Prep Date:
RunNo: 161269
Client ID: LCSS
Batch ID: R161269
TestNo: SW9045D
Analysis Date: 4/5/2023
SegNo: 4287017
Analyte
Result
PQL SPK value SPK Ref Val %REC
Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
pH 7.0
7.0 0 101 90 110
Sample ID: 23032266-011ADUP
SampType: DUP
TestCode: pH_S(9045D) Units: s.u.@21.9C
Prep Date:
RunNo: 161269
Client ID: Batch=
Batch ID: R161269
TestNo: SW9045D
Analysis Date: 4/5/2023
SegNo: 4287019
Analyte
Result
PQL SPK value SPK Ref Val %REC
Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
pH 9.4
0 0 0 0 9.4 0.1 10
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal,
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected OGI P Second column confirmation exceeds
PL Permit Limit R RPD outside accepted recovery limits RL Reporting Detection Limit
Original
Page 22 of 31

SUMMIT Summit Environmental Technologies, Inc.
3310 Win St.
ENVIRONMENTAL TECHNOLOGIES, INC Cuyahoga Falls, Ohio 44223
Analytical Laboratories TEL: [phone] FAX.- [phone]
Website: hgp:llwww.settek.com
QC SUMMARY REPORT
WO#: 23032301
13-Apr-23
Client: Synagro
Project: Beaufort WWTP BatchID: R161269
Sample ID: LCS-R161269
SampType: LCS
TestCode: pH_Oil(9045D Units: s.u.@22.2C
Prep Date:
RunNo: 161269
Client ID: LCSW
Batch ID: R161269
TestNo: SW9045D
Analysis Date: 4/5/2023
SegNo: 4286135
Analyte
Result
PQL SPK value SPK Ref Val %REC
LowLimit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
pH
7.0
7.0 0 101 90 110
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal,
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected OGl P Second column confirmation exceeds Original
PL Permit Limit R RPD outside accepted recovery limits RL Reporting Detection Limit
Page 23 of 31

SUMMIT Summit Environmental Technologies, Inc.
3310 Win St.
ENVIRONMENTAL TECHNOLOGIES, INC Cuyahoga Falls, Ohio 44223
Analytical Laboratories TEL: [phone] FAX: [phone]
Website: http://www.settek.coni
Client: Synagro
Project: Beaufort WWTP
QC SUMMARY REPORT
WO#: 23032301
13 Apr-23
BatchlD: R161269
Sample ID: LCS-R161269
SampType: LCS
TestCode: pH_NPW(450 Units: s.u.@22.00
Prep Date:
RunNo: 161269
Client ID: LCSW
Batch ID: R161269
TestNo: SW9045D
Analysis Date: 4/5/2023
SegNo: 4286111
Analyte
Result
PQL SPK value SPK Ref Val %REC
Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
pH 7.0 7.0 0 100 98.6 101.4
Sample ID: LCS-R161269
SampType: LCS
TestCode: pH_NPW(450 Units: s.u.@21.7C
Prep Date:
RunNo: 161269
Client ID: LCSW
Batch ID: R161269
TestNo: SW9045D
Analysis Date: 4/5/2023
SegNo: 4291244
Analyte
Result
PQL SPK value SPK Ref Val %REC
Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
pH 7.0 7.0 0 101 98.6 101.4
Qualifiers: B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
PL Permit Limit
E Value above quantitation range H Holding times for preparation or anal,
M Manual Integration used to determine area response MC Value is below Minimum Compound
OGl P Second column confirmation exceeds
R RPD outside accepted recovery limits RL Reporting Detection Limit
Original
Page 24 of 31

SUMMIT Summit Environmental Technologies, Inc.
3310 Win St.
ENVIRONMENTAL TECHNOLOGIES, INC Cuyahoga Falls, Ohio 44223
Analytical Laboratories TEL: [phone] FAX: [phone]
Website: http://www.settek.coni
Client: Synagro
Project: Beaufort WWTP
QC SUMMARY REPORT
WO#: 23032301
13 Apr-23
BatchlD: R161269
Sample ID: 23030959-001ADUP
SampType: DUP
TestCode: pH_NPW(450 Units: sm.@23.1C
Prep Date:
RunNo: 161269
Client ID: Batch=
Batch ID: R161269
TestNo: SW9045D
Analysis Date: 4/5/2023
SegNo: 4286128
Analyte
Result
PQL SPK value SPK Ref Val %REC
Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
pH 10.6 13.3 22.3 5 RH
Sample ID: LCS-R161269
SampType: LCS
TestCode: pH_NPW(450 Units: s.u.@21.6C
Prep Date:
RunNo: 161269
Client ID: LCSW
Batch ID: R161269
TestNo: SW9045D
Analysis Date: 4/5/2023
SegNo: 4291249
Analyte
Result
PQL SPK value SPK Ref Val %REC
Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
pH 7.0 7.0 0 101 98.6 101.4
Qualifiers: B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
PL Permit Limit
E Value above quantitation range H Holding times for preparation or anal,
M Manual Integration used to determine area response MC Value is below Minimum Compound
OGl P Second column confirmation exceeds
R RPD outside accepted recovery limits RL Reporting Detection Limit
Original
Page 25 of 31

SUMMIT Summit Environmental Technologies, Inc.
3310 Win St.
ENVIRONMENTAL TECHNOLOGIES, INC Cuyahoga Falls, Ohio 44223
Analytical Laboratories TEL: [phone] FAX.- [phone]
Website: hgp:llwww.settek.com
Client: Synagro
Project: Beaufort WWTP
QC SUMMARY REPORT
WO#: 23032301
13-Apr-23
BatchID: R161313
Sample ID: LCS-R161313
SampType: LCS
TestCode: Ignitability_S Units: mm/sec
Prep Date:
RunNo: 161313
Client ID: LCSS
Batch ID: R161313
TestNo: SW1030
Analysis Date: 4/5/2023
SegNo: 4286983
Analyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
Ignitability
8.33
7.240 0 115 70 130
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal,
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected OGl P Second column confirmation exceeds Original
PL Permit Limit R RPD outside accepted recovery limits RL Reporting Detection Limit
Page 26 of 31

SUMMIT Summit Environmental Technologies, Inc.
3310 Win St.
ENVIRONMENTAL TECHNOLOGIES, INC Cuyahoga Falls, Ohio 44223
Analytical Laboratories TEL: [phone] FAX: [phone]
Website: http://www.settek.coni
Client: Synagro
Project: Beaufort WWTP
QC SUMMARY REPORT
WO#: 23032301
13 Apr-23
BatchlD: R161320
Sample ID: RLC TCLP 0.01ppm
SampType: RLC
TestCode: TCLP-SVOC- Units: mg/L
Prep Date:
RunNo: 161320
Client ID: Batch=
Batch ID: R161320
TestNo: SW8321
Analysis Date: 4/5/2023
SegNo: 4287128
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
2,4-D
0.0149
0.0100 0.01000
0 149
50
150
2,4,5-TP
ND
0.0100 0.01000
0 78.0
50
150
Sum 2,4-Dichlorophenylacetic acid
0.00990
0.01000
99.0
70
130
Sample ID: MB TCLP
SampType: MBLK
TestCode: TCLP-SVOC- Units: mg/L
Prep Date:
RunNo: 161320
Client ID: PBS
Batch ID: R161320
TestNo: SW8321
Analysis Date: 4/5/2023
SegNo: 4287129
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
2,4-D ND 0.0100
2,4,5-TP ND 0.0100
Surr: 2,4-Dichlorophenylacetic acid 0.950 1.000 95.0 70 130
Sample ID: LCS TCLP 0.3 ppm
SampType: LCS
TestCode: TCLP-SVOC- Units: mg/L
Prep Date:
RunNo: 161320
Client ID: LCSS
Batch ID: R161320
TestNo: SW8321
Analysis Date: 4/5/2023
SegNo: 4287130
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
2,4-D 0.270 0.0100
0.3000 0 89.9 60.5
141
2,4,5-TP 0.272 0.0100
0.3000 0 90.6 68.3
144
Surr: 2,4-Dichlorophenylacetic acid 0.272
0.3000 90.8 70
130
Qualifiers: B Analyte detected in the associated Method Blank
E Value above quantitation range
H
Holding times for preparation or anal,
J Analyte detected below quantitation limits
M Manual Integration used to determine area response
MC
Value is below Minimum Compound
Original
ND Not Detected
OGl
P
Second column confirmation exceeds
PL Permit Limit
R RPD outside accepted recovery limits
RL
Reporting Detection Limit
Page 27 of 31

SUMMIT Summit Environmental Technologies, Inc.
3310 Win St.
ENVIRONMENTAL TECHNOLOGIES, INC Cuyahoga Falls, Ohio 44223
Analytical Laboratories TEL: [phone] FAX: [phone]
Website: http://www.settek.coni
Client: Synagro
Project: Beaufort WWTP
QC SUMMARY REPORT
WO#: 23032301
13 Apr-23
BatchlD: R161320
Sample ID:
LCSD TCLP 0.3 ppm SampType: LCSD
TestCode: TCLP-SVOC- Units: mg/L
Prep Date:
RunNo: 161320
Client ID:
LCSS02 Batch ID: R161320
TestNo: SW8321
Analysis Date: 4/5/2023
SegNo: 4287131
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
2,4-D 0.284 0.0100 0.3000 0 94.6 60.5 141 0.2697 5.06 30
2,4,5-TP 0.285 0.0100 0.3000 0 94.9 68.3 144 0.2718 4.60 30
Sum 2,4-Dichlorophenylacetic acid 0.287 0.3000 95.6 70 130 0 0
Qualifiers: B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
PL Permit Limit
E Value above quantitation range
M Manual Integration used to determine area response
OGl
R RPD outside accepted recovery limits
Page 28 of 31
H Holding times for preparation or anal,
MC Value is below Minimum Compound
P Second column confirmation exceeds
RL Reporting Detection Limit
Original

SUMMIT Summit Environmental Technologies, Inc.
3310 Win St.
ENVIRONMENTAL TECHNOLOGIES, INC Cuyahoga Falls, Ohio 44223
Analytical Laboratories TEL: [phone] FAX: [phone]
Website: http://www.settek.coni
Client: Synagro
Project: Beaufort WWTP
QC SUMMARY REPORT
WO#: 23032301
13 Apr-23
BatchlD: R161342
Sample ID: RLC1
SampType: RLC
TestCode: Mtl-ICP_NPW Units: mg/L
Prep Date:
RunNo: 161342
Client ID: Batch=
Batch ID: R161342
TestNo: SW6010
Analysis Date: 4/6/2023
SegNo: 4287873
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
TCLP Arsenic(As)
0.0126
0.0100
0.008000
0
158
70
130 S
TCLP Barium(Ba)
0.0100
0.0100
0.01000
0
100
70
130
TCLP Cadmium(Cd)
0.00200
0.00200
0.002000
0
100
70
130
TCLP Chromium(Cr)
ND
0.00800
0.008000
0
93.8
70
130
TCLP Lead(Pb)
0.0173
0.0100
0.02000
0
86.5
70
130
TCLP Selenium(Se)
0.0156
0.00800
0.01000
0
156
70
130 S
TCLP Silver(Ag)
ND
0.00400
0.002000
0
0
70
130 S
Sample ID: RLC2
SampType: RLC
TestCode: Mtl-ICP_NPW Units: mg/L
Prep Date:
RunNo: 161342
Client ID: Batch=
Batch ID: R161342
TestNo: SW6010
Analysis Date: 4/6/2023
SegNo: 4287874
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
TCLP Arsenic(As)
0.0170
0.0100
0.01600
0
106
70
130
TCLP Barium(Ba)
0.0207
0.0100
0.02000
0
104
70
130
TCLP Cadmium(Cd)
0.00410
0.00200
0.004000
0
103
70
130
TCLP Chromium(Cr)
0.0164
0.00800
0.01600
0
103
70
130
TCLP Lead(Pb)
0.0396
0.0100
0.04000
0
99.0
70
130
TCLP Selenium(Se)
0.0237
0.00800
0.02000
0
119
70
130
TCLP Silver(Ag)
ND
0.00400
0.004000
0
93.3
70
130
Qualifiers: B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
PL Permit Limit
E Value above quantitation range
M Manual Integration used to determine area response
OGl
R RPD outside accepted recovery limits
Page 29 of 31
H Holding times for preparation or anal,
MC Value is below Minimum Compound
P Second column confirmation exceeds
RL Reporting Detection Limit
Original

Page 30 of 31

�� � � Summit Environmental Technologies, Inc.
3310 Win St.
ENVIRONMENTAL TECHNOLOGIES, INC Cuyahoga Falls, Ohio44223 Sample Log -in Check List
Analytical Laboratories TEL: [phone] FAX [phone]
Website: http://www.settek.coni
Client Name: SYN-NC-27028 Work Order Number: 23032301
Logged by: Tegan A. Richards
Completed By: Tegan A. Richards
Reviewed By: Jennifer Woolf
3/31/2023 10:05:00 AM
3/31/2023 3:49:08 PM
4/3/2023 11:38:19 AM
RcptNo: 1
Chain of Custody
1. Is Chain of Custody complete?
Yes
❑
No
❑
Not Present
2. How was the sample delivered?
UPS
Loa In
3, Coolers are present?
Yes
C
No
F
NA F
4. Shipping container/cooler in good condition?
Yes
0
No
Custody seals intact on shipping container/cooler?
Yes
❑
No
❑
Not Present
No. Seal Date:
Signed By:
5. Was an attempt made to cool the samples?
Yes
❑
No
F—
NA
6. Were all samples received at a temperature of >0° C to 6.0°C
Yes
d❑
No
❑
NA
7, Sample(s) in proper container(s)?
Yes
J❑
No
❑
8. Sufficient sample volume for indicated test(s)?
Yes
d❑
No
❑
g, Are samples (except VOA and ONG) properly preserved?
Yes
J❑
No
❑
10. Was preservative added to bottles?
Yes
❑
No
d❑
NA ❑
11. Is the headspace in the VOA vials less than 1/4 inch or 6 mm?
Yes
No
❑
No VOA Vials ❑�
12. Were any sample containers received broken?
Yes
No
d❑
13. Does paperwork match bottle labels?
Yes
No
❑
(Note discrepancies on chain of custody)
14. Are matrices correctly identified on Chain of Custody?
Yes
No
❑
15. Is it clear what analyses were requested?
Yes
No
❑
16. Were all holding times able to be met?
Yes
No
❑
(If no, notify customer for authorization.)
Special Handling (if applicable)
17. Was client notified of all discrepancies with this order?
Yes
No
❑
NA ❑d
Person Notified: Date:
By Whom: Via:
❑ eMail
❑ Phone
❑
Fax
❑ In Person
Regarding:
Client Instructions:
18. Additional remarks:
Cooler Information
Cooler No
Temp °C
Condition
Seal Intact
Seal No
Seal Date
Signed By
1
1.8
Good
Not Present
Page 31 of 31

SECTION 5

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Town of Beaufort WQ Permit Number: WQ0006017
WWTP Name: Town of Beaufort WWTP NPDES Number: NCO021831
Monitoring Period: From 01/01/2023 To 12/31/2023
Pathogen Reduction (40 CFR 50332/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. 1/A (time/temp) Alt. 2B (Alk Treatment) Alt. 3/C (Prior Testing)
Alt. 4/D (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic
Beta Ray Gamma Ray Pasteurization
Class B:
Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying Composting Aerobic Digestion
Anaerobic Digestion
tt applicable to alternative perlormea q-
ass A or l.lass D corn Jere me iotiowing monnornn
nata:
Parameter
Allowable Level in Sludge
Pathogen Density
No. of
Frequency
Sample
Analytical
Excee-
of
Type
Technique
Minimum Geo. Mean Maximum Units
dences
Analysis
Fecal
2x 10 to the Wh
MPN
2127
3736
7703
MPN/g
0
Annually
Grab
SM 9221 C
Coliform
power per gram
of total solids
C'1=1 Ug
CFU
1000 MPN per gram of
MPN/g
total solids (dry weight)
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed:
Option/Alt. 1
Option/Alt. 2
Option/Alt. 3 Option/Alt. 4
(VS reduction)
(40-day bench)
(30-day bench) (Spec. 02 uptake)
Option/Alt. 5
Option/Alt. 6
Option/Alt. 7 Option/Alt. 8
(14-Day Aerobic)
(Alk Stabilization)
(Drying — Stable) (Drying — Unstable)
Option/Alt. 9
Option/Alt. 10
(Injection)
(Incorporation) X
No vector attraction reduction alternatives were performed
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
% reduction requirement In 40 CFR 503.33/15A NCAC 02T.1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement In 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified
personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have
been met. I am aware that there are significant penalties for false certification including fine and imprisonment."
Donovan Willis. Public Utilities Director
Preparer Name and Title (type or print)
Y
Signature of Preparer* Date
Todd Larson Operations Director
.and Appl ier Nam • • Title (if applicable) (type or print)
1 /31 /2024
Signatur of Land Ap er (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26)

FF0"--- Environmental Chemists, Inc.
envirochem 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252,473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS info+« environmentalchemists.com
Synagro Date of Report: Apr 27, 2023
284 Boger Road Customer PO #:
Mocksville INC 27028 Customer ID: 13010013
Attention: Report #: 2023-07901
Project ID: Beaufort WWTP
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
23-20021 Site: 1 4/24/2023 6:00 AM Solid/Sludge Matthew C.
Test Method Results Date Analyzed
Total Solids (%) SM 2540 B 15.6 % 04/24/2023
Fecal Density SM 9221C E-2014 7703 MPN/g 04/24/2023
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
23-20022 Site: 2 4/24/2023 6:00 AM Solid/Sludge Matthew C.
Test Method Results Date Analyzed
Total Solids (%) SM 2540 B 14.2 % 04/24/2023
Fecal Density SM 9221C E-2014 2326 MPN/g 04/24/2023
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
23-20023 Site: 3 4/24/2023 6:00 AM Solid/Sludge Matthew C.
Test Method Results Date Analyzed
Total Solids (%
Fecal Density
Lab ID Sample ID:
23-20024 Site:4
Test
Total Solids (%)
Fecal Density
Lab ID
23-20025
Test
Sample ID:
Site: 5
SM 2540 B
SM 9221 C E-2014
Collect Date/Time
4/24/2023 6:00 AM
Method
SM 2540 B
SM 9221 C E-2014
Method
Collect Date/Time
4/24/2023 6:00 AM
14.9 % 04/24/2023
4686 MPN/g 04/24/2023
Matrix Sampled by
Solid/Sludge Matthew C.
Results Date Analyzed
14.8 % 04/24/2023
5320 MPN/g 04/24/2023
Matrix Sampled by
Solid/Sludge Matthew C.
Results Date Analyzed
Total Solids (%) SM 2540 B 15.5 % 04/24/2023
Fecal Density SM 9221C E-2014 2127 MPN/g 04/24/2023
Report #:: 2023-07901 Page 1 of 2

F"W'T
Cnviroche]m
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910,392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
infora environmentalchemists.com
Synagro
Date of Report:
Apr 27, 2023
284 Boger Road
Customer PO #:
Mocksville NC 27028
Customer ID:
13010013
Attention:
Report #:
2023-07901
Project ID: Beaufort WWTP
Lab ID Sample ID:
Collect Date/Time Matrix
Sampled by
23-20026 Site: 6
4/24/2023 6.00 AM Solid/Sludge
Matthew C.
Test
Method
Results
Date Analyzed
Total Solids (%)
SM 2540 B
15.4 %
04/24/2023
Fecal Density
SM 9221c E-2014
3180 MPN/g
04/24/2023
Lab ID Sample ID:
Collect DatelTime
Matrix Sampled by
23-20027 Site: 7
4/24/2023 6:00 AM
Solid/Sludge Matthew C.
Test
Method
Results
Date Analyzed
Total Solids (%)
SM 2540 B
14.6 %
04/24/2023
Fecal Density
SM 9221C E-2014
3368 MPN/g
04/24/2023
Comment: Results reported on a dry weight basis.
Reviewed by: Y::,
Report # 2023-07931 Page 2 of 2

Environmental Chemist, Inc., Wilmington, NC Lab #94
Sample Receipt Checklist
Client: i( C-)
Receipt of sample: ECHEM Pickup I
❑ YES ❑ NO N/A 1
❑ YES ❑ NO N/A 2
Original temperature upon receipt
6602 Windmill Way
Wilmington, NC 28405
910.392.0223
Date: 4JZ-J 2-3 -Report Number: 3 -c D
IL
Client Delive I UPS ❑ FedEx ❑ Other ❑
Were custody seals present on the cooler?
If custody seals were present, were they intact/unbroken?
°C Corrected temperature upon receipt —
How temperature taken: ❑ Temperature Blank Against Bottles
IR Gun ID: Thomas Traceable S/N 210886869 IR Gun Correction Factor °C: 0.0
YES ❑ NO 3. If temperature of cooler exceeded 6°C, was Project Mgr./QA notified?
YE5 O NO 4. Were proper custody procedures (relinquished/received) followed?
YES
❑ NO
5. Were sample ID's listed on the COC?
YES
❑ NO
6. Were samples ID's listed on sample containers?
YES
❑ NO
7. Were collection date and time listed on the COC?
YES
❑ NO
8. Were tests to be performed listed on the COC?
RYES
❑ NO
9. Did samples arrive in proper containers for each test?
YES
❑ NO
10. Did samples arrive in good condition for each test?
5( YES
❑ NO
11. Was adequate sample volume available?'
if YES
❑ NO
12 W
O YES
❑
ere samples received within proper holding time for requested tests?
NO
13. Were acid preserved samples received at a pH of <2?
❑ YES
❑ NO 114.
Were cyanide samples received at a pH >12?
❑ YES
❑ NO
15. Were sulfide samples received at a pH >9?
❑ YES
❑ NO
16. Were NH3/TKN/Phenol received at a chlorine residual of <0.5 m/L? **
❑ YES
❑ NO
17. Were Sulfide/Cyanide received at a chlorine residual of <0.5 m/L?
❑ YES
O NO
18. Were orthophosphate samples filtered in the field within 15 minutes?
* TOC/Volatiles are pH checked at time of analysis and recorded on the benchsheet.
** Bacteria samples are checked for Chlorine at time of analysis and recorded on the benchsheet
Sample Preservation:
Sample(s)
by adding (circle one):
(Must be completed for any sample(s) incorrectly preserved or with headspace)
were received incorrectly preserved and were adjusted accordingly
H2SO4 HNO3 HCI NaOH
Time of preservation: If more than one preservative is needed, notate in comments below
Note: Notify customer service immediately for incorrectly preserved samples. Obtain a new sample or
iotify the state lab if directed to analyzed by the customer. Who was notified, date and time:
atiles Sample(s)
were received with headspace
COMMENTS:
DOC. QA.002 Rev 1
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SECTION 6

Agricultural Lime Application Log
Year2023
Project Beaufort
Fields
Soil
Lime Requirements
Tons/Acre
Date
(state -county -site -field)
PH
(from soil analysis)
AR limed
A limed
CR-7-3A
6
0 T
N/A
CR-7-313
5.5
0.8 T
N A
N/A -Did not apply in 2023
*Lime will be applied when field conditions/cropping pattern permits

SECTION 7

NCDA&CS Agronomic Division Phone: [phone]
Website: www.ncagr.gov/agronomi/
Report No. FY24-SL002245
Predictive
Client:
Bobby Riggs
483 Weatherington Landing Rd
Advisor: Matthew Carter
4894 Liddell Rd
£
x Soil Report Mehlich-3
Extraction
Stella, NC 28582
Seven Springs, NC 28578
Sampled County: Craven
„r
Links to Helpful Information
Client ID: 467267
Advisor ID: 546169
Sampled: Received: 08/18/2023 Completed: 08/29/2023
Farm:
Sample ID: CR73A
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P2O5
K2O
Mg S Mn
Zn
Cu B
Information
Lime History:
1 -Corn, grain 0.0
120 - 160 0
40
0 0 0
0
0 0
Note: 3
2- 0.0
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class: Mineral
HM% W/V CEC BS% Ac pH P-1 K-1
Ca% Mg%
S-1
Mn-I
Mn-All Mn-Al2 Zn-I
Zn-AI
Cu-I Na ESP SS -I NO3-N
1.02 1.19 6.4 81 1.2 6.0 220 53
52 25
50
47
45 206
206
287 0.1 2
Sample ID: CR73B
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P2O5
K2O
Mg S Mn
Zn
Cu B
Information
Lime History:
1 -Corn, grain 0.8
120 - 160 0
40
0 0 0
0
0 0
Note: 3
2- 0.0
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class: Mineral
HM% W/V CEC BS% Ac pH P-1 K-1
Ca% Mg%
S-1
Mn-I
Mn-All Mn-AI2 Zn-I
Zn-AI
Cu-I Na ESP SS-1 NO3-N
1.08 1.23 5.5 69 1.7 5.5 300 49
50 14
56
53
49 316
316
398 0.1 2
North Carolina
f. 1 ' >
I0WOOLO iiu%t lLaW Ctwnawukm
Reprogramming of the laboratory -information -management system that makes this report possible is being funded
through a grant from the North Carolina Tobacco Trust Fund Commission.
Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
- Steve Troxler. Commissioner of Agriculture

NCDA&CS Agronomic Division Phone:
[phone]
Website: www.ncagr.gov/agronomi/
Report No. FY24-SL002245
Bobby Riggs
Page 2 of 3
Sample ID: CR702
Recommendations:
Lime
Nutrients (lb/acre)
More
Crop
(tons/acre)
N P2O5 K2O
Mg
S
Mn Zn
Cu B
Information
Lime History:
1 -Corn, grain
0.7
120 - 160 0 60
0
0
0 0
0 0
Note: 3
2 -
0.0
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm):
Soil Class:
Mineral
HM% W/V CEC BS% Ac pH
P-1 K-1
Ca% Mg% S-1 Mn-I
Mn-All
Mn-Al2
Zn-I Zn-AI
Cu-I Na ESP SS-1 NO3-N
0.71 1.37 3.8 67 1.3 5.4
272 39
47 14 48 41
42
157 157
244 0.1 3

NCDA&CS Agronomic Division Phone: [phone] Website: www.ncagr.gov/agronomi/
Report No. FY24-SL002245
Bobby Riggs
Page 3 of 3
Understanding the Soil Report: explanation of measurements, abbreviations and units
Recommendations
Report Abbreviations
Lime
Ac
exchangeable acidity
If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either
B
boron
ton/acre or Ib/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting.
BS%
% CEC occupied by basic cations
For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 Ib/1000 sq ft) at on
Ca%
% CEC occupied by calcium
time, even if the report recommends more. You can apply the rest in similar increments every six months until the full rate
CEC
cation exchange capacity
is applied. If MG is recommended and lime is needed, use dolomitric lime.
Cu-I
copper index
ESP
exchangeable sodium percent
Fertilizer
HM%
percent humic matter
Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of
K-I
potassium index
lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies
K20
potash
for the crop being grown, not on soil test results. K-1 and P-1 values are based on test results and should be > 50. If they
Mg%
% CEC occupied by magnesium
are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is
MIN
mineral soil class
an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS-1 levels appear
Mn
manganese
only on reports for greenhouse soil or problem samples.
Mn-All
Mn-availability index for crop 1
Mn-Al2
Mn-availability index for crop 2
Mn-I
manganese index
Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z
Mn-
mineral -organic soil class
notations appear on the soil report, refer to $Note: Secondary Nutrients and Micronutrients. In general, homeowners do not
N
nitrogen
need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit
Na
sodium
ncagr.gov/agronomi/pubs.htm.
NO3-N
nitrate nitrogen
ORG
organic soil class
Recommendations for small areas, such as home lawns/gardens, are listed in units of Ib/1000 sq ft. If you cannot find
pH
current soil pH
the exact fertilizer grade recommended on the report, visit www.ncagr.gov/apronomi/obpart4.htm1 #sfind information that
P-1
phosphorus index
may help you choose a comparable alternate. For more information, read A Homeowner's Guide to Fertilizer.
P205
phosphate
S-1
sulfur index
Test Results
SS-1
soluble salt index
W/V
weight per volume
The first seven values [soil class, HM%, W/V, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The
Zn-AI
zinc availability index
Zn-I
zinc index
remaining 16 [P-I, K-I, Ca%, Mg%, Mn-I, Mn-All, Mn-AI2, Zn-I, Zn-AI, Cu-I, S-I, SS -I, Na, ESP, SS -I, NO3-N (not routinel
available)] indicate levels of plant nutrients or other fertility measurement. Visit www.ncapr.gov/agronomi/uyrst.htm