WQ0008778_2023 Residual Annual Report_20240219 (2)

Initial Review
Reviewer
nathaniel.thorn burg
Is this submittal an application? (Excluding additional information.) *
Yes No
If not an application what is the submittal type?* Annual Report
Residual Annual Report
Additional Information
Other
Annual Report Year* 2023
Permit Number (IR) * W00008778
Applicant/Permittee Town of Farmville
Email Notifications
Does this need review by the hydrogeologist? * Yes U No
Regional Office Washington
CO Reviewer
Admin Reviewer Wanda Gerald

Submittal Form
Project Contact Information
Please provide information on the person to be contacted by NDB Staff regarding electronic submittal, confirmation of receipt, and other correspondence.
Name* Lysa Finnerty
Email Address*
[e-mail]
Project Information
.........................
Application/Document Type*
New (Fee Required)
Modification - Major (Fee Required)
Renewal with Major Modification (Fee
Required)
Annual Report
Additional Information
Other
Phone Number*
4105376150
Modification - Minor
Renewal
GW-59, NDMR, NDMLR, NDAR-1,
N DAR-2
Residual Annual Report
Change of Ownership
We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form.
https://edoes.deq.nc.gov/Forms/NonDischarge_Monitoring_Report
Permit Type:*
Wastewater Irrigation
High -Rate Infiltration
Other Wastewater
Reclaimed Water
Closed -Loop Recycle
Residuals
Single -Family Residence Wastewater
Other
Irrigation
Permit Number:*
WQ0008778
Has Current Existing permit number
Applicant/Permittee Address*
435 Williams Court, Ste 100, Baltimore, MD 21220
Facility Name*
Town of Farmville Class B Residuals Program
Please provide comments/notes on your current submittal below.
Submission of the 2023 Annual Report for Town of Farmville, NC
At this time, paper copies are no longer required. If you have any questions about what is required, please contact Nathaniel Thornburg
at [e-mail].
Please attach all information required or requested for this submittal to be reviewed here.
(Application Form, Engineering Plans, Specifications, Calculations, Etc.)
Farmville NC 2023 Annual Report FINAL.pdf 6.18MB
Upload only 1 PDF document (less than 250 MB). Multiple documents must be combined into one PDF file unless file is larger
than upload limit.
* By checking this box, I acknowledge that I understand the application will not be accepted for pre -review until the fee (if required) has
been received by the Non -Discharge Branch. Application fees must be submitted by check or money order and made payable to the
North Carolina Department of Environmental Quality (NCDEQ). I also confirm that the uploaded document is a single PDF with all parts
of the application in correct order (as specified by the application).
Mail payment to:
NCDEQ — Division of Water Resources
Attn: Non -Discharge Branch
1617 Mail Service Center
Raleigh, NC 27699-1617
Signature
Alva �Cit'wt%tt,
Submission Date 2/19/2024

435 Williams Court, Suite 100
Baltimore, MD 21220
www.synagro.com
FEBRUARY 17, 2024
NCDEQ
Division of Water Resources
Information Processing Unit
1617 Mail Service Center
Raleigh, NC 27699-1617
Re: 2023 Annual Report for Permit No. WQ0008778
Dear NCDEQ:
SYNAGRO
Synagro is submitting one electronic copy of the above referenced report on behalf of the Town
of Farmville, NC.
If you have any questions or need additional information, please do not hesitate to contact
David Hodgkins at [phone] or Matthew Carter at [phone].
Sincerely,
Derrick Shivar
Environmental Compliance Manager
Enclosures
cc: David Hodgkins
Matthew Carter, Synagro
YOUR PARTNER FORA CLEANER, GREENERWORLD

TOWN OF FARMVILLE, NC
RESIDUALS LAND APPLICATION PROGRAM
Permit No. WQ0008778
2023 ANNUAL REPORT

Town of Farmville, NC
Residuals Land Application Program
2023 Annual Report
TABLE OF CONTENTS
1. Certification Form and Annual Operations Summary
2. Annual Residual Sampling Summary Forms and Residuals
Analyses
3. Annual Land Application Field Summary Forms
4. TCLP Analysis
5. Pathogen Reduction/Vector Attraction Reduction
6. Soil pH & Lime Application Records
7. Soil Analyses

SECTION 1

ANNUAL LAND APPLICATION CERTIFICATION FORM
WQ Permit #: W00008778 County Pitt Year 2023
Facility Name (as shown on permit) Farmville WWTP NPDES No. NCO029572
Land Application Operator Synaero Phone# [phone]
Land application of residuals as allowed by the above permit occurred during the past calendar year?
X YES NO. If NO, skip Part A, and Part Band proceed to Part C. Also, if residuals were generated but not land applied,
please attach an explanation on how the residuals were handled.
Part A — Residuals Application Summary:
Total number of application fields in the permit: 7
Total number of fields utilized for land application during the year: 2
Total amount of dry tons applied during the year for all application sites: 251.95
Total number of acres utilized for land application during the year: 44.00
Part B — Annual Compliance Statement:
Facility was compliant during calendar year 2023 with all conditions of the land application permit (including but not limited to items
1-13 below) issued by the Division of Water Quality X YES NO.
If no, please provide a written description why the facility was not compliant, the dates, and explain corrective action taken.
1. Only residuals approved for this permit were applied to the permitted sites.
2. Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or the
limit specified in the permit.
3. Annual soils analysis was performed on each site receiving residuals during the past calendar year and three (3) copies of
laboratory results are attached.
4. Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5. All other monitoring was performed in accordance with the permit and reported during the year as required and three (3)
copies of certified laboratory results are attached.
6. The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .I 105(a) or the Pollutant Loading
Rates in 15A NCAC 02T .I 105(b) (Applicable to 40 CFR Part 503 regulated facilities).
7. All general requirements as specified in the Land Application Permit were complied with (applicable to 40 CFR Part 503
regulated facilities).
8. All monitoring and reporting requirements in 15A NCAC 02T .I I I I were complied with (applicable to 40 CFR Part 503
regulated facilities).
9. All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Quality.
10. No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
11. Vegetative cover was maintained and proper crop management was performed on each site receiving residuals, as specified
in the permit.
12. No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13. All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C — Certification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate, and complete. I
am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for
knowing violations."
David P. Hodgkins, Town Manager l � Z l2
Permittee Name and Title (type or print) Signature of Peglu e Date
2/01/2024
Signature of Preparer* Date Sig ure tof Land Uplier Date
(if different from Permittee) (if different from Permittee and Preparer)
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 02T .1102 (26) DENR FORM ACF (12/2006)

OPERATIONS SUMMARY - LAND APPLICATION - NORTH CAROLINA
ALL COUNTIES - ALL SITES
DATE RANGE: 1/1/2023 - 12/31/2023
FARMVILLE, NC
FARMVILLE, NC AEROBICALLY DIGESTED LIQUID
MONTH/YEAR
AMOUNT
UNIT
DRY TONS
UNIT
DRY METRIC TONS
March 2023
508,400.00
G
60.42
D
54.80
July 2023
372,000.00
G
20.48
D
18.57
November 2023
390,600.00
G
98.87
D
89.67
December 2023
285,200.00
G
72.19
D
65.48
TOTAL
Units Key: D - Dry Tons; G — Gallons; W — Wet Tons; Y — Cubic Yards
Report Date: 1/29/2024 3:59:49 PM
1,556,200.00 G 251.95 D 228.52

SECTION 2

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B
WQ Permit Number: WQ0008778 Laboratory:
Facility Name: FARMVILLE, NC Waypoint Analytical Virginia Inc.
Residual Source WQ # or
NPDES#: NCO029572
WWTP Name: FARMVILLE WWTP
Residual Analysis Data
Product Type
Sample or Composite Date
AEDLIQ
02/28/23
AEDLIQ
05/17/23
AEDLIQ
09/26/23
Parameter (mg/kg dry weight)
Ceiling Conc.
Limit
Percent Solids (%)
NA
2.85
1.32
6.07
Arsenic
75
<17.2
<38.5
<8.2
Cadmium
85
<3.45
<7.69
<1.64
Copper
4300
316
566
91.8
Chromium
NA
21.9
34.7
5.97
Lead
840
21.9
43.6
7.98
Mercury
57
<6.1
<13.7
<2.97
Molybdenum
75
<8.62
<19.2
<4.1
Nickel
420
15.3
26.5
4.72
Selenium
100
<17.2
<38.5
<8.2
Zinc
7500
907
1550
266
Total Phosphorus
NA
20000
28200
5540
TKN
NA
49700
77700
27000
Ammonia -Nitrogen
NA
<3450
<7690
1920
Nitrate and Nitrite
NA
259
<385
744
For surface disposal facilities the ceiling concentration limits listed in this form are not applicable. Reference the individual permit for metals limits.
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified
personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the
possibility of fines and imprisonment for knowing violations."
Signature of Preparer` Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15 A NCAC 2T.1102(26) DENR FORM RSSF (12/2006)
Printed: 1/29/2024 4:53:34 PM For: 2015 01

ANNUAL RESIDUAL SAMPLING SUMMARY FORM - B
Report all sampling analysis results for parameters not listed in FORM RSSF that are part of the WQ permit or were analyzed for over the past
calendar year. Use additional forms as needed.
WQ Permit Number:
WQ0008778
Facility Name:
FARMVILLE, NC
Residual Source
NPDES # or WQ#:
NCO029572
WWTP Name:
FARMVILLE WWTP
Residual Analysis Data
Product Type
Sample or Composite Date
Parameters (mg/kg dry weight)
Aluminium
Calcium
Magnesium
pH (s.u.)
Potassium
Sodium
PAN
SAR (Ratio)
Laboratory:
Waypoint Analytical Virginia Inc.
AEDLIQ AEDLIQ AEDLIQ
02/28/23 05/17/23 09/26/23
9660
15500
2330
10400
15800
2640
2950
4220
808
6.30
6.40
3.60
4380
5870
997
2100
5150
1060
16882
27537
9243
0.7877
1.0767
1.1374
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordiance with a system designed to assure that qualified
personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the
possibility of fines and imprisonment for knowing violations."
— a J. zllZla�
Signature of Preparer ` U Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15 A NCAC 2T.1102(26)
Printed: 1/29/2024 4:59:02 PM For: 2015 01 DENR FORM RSSF-B (12/2006)

Waypointo
ANALYTICAL
3/9/2023
Synagro Central LLC
Matthew Carter
284 Boger Rd
Mocksville, NC, 27028
Ref: Analytical Testing
Report Number: 23-059-0003
Project Description: Farmville WWTP
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Dear Matthew Carter:
Waypoint Analytical Virginia, Inc. received sample(s) on 2/28/2023 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Brandi Watson
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 1 of 7

(D
waypoint 7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
ANALYTICAL www.waypointanalytical.com
Sample Summary Table
Report Number: 23-059-0003
Client Project Description: Farmville WWTP
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
61096
Farmville WWTP
Solids
02/28/2023 12:15
02/28/2023
61096
Farmville WWTP
Solids
02/28/2023 12:15
02/28/2023
61096
Farmville WWTP
Solids
02/28/2023 12:15
02/28/2023
61096
Farmville WWTP
Solids
02/28/2023 12:15
02/28/2023
61096
Farmville WWTP
Solids
02/28/2023 12:15
02/28/2023
61096
Farmville WWTP
Solids
02/28/2023 12:15
02/28/2023
61096
Farmville WWTP
Solids
02/28/2023 12:15
02/28/2023
61096
Farmville WWTP
Solids
02/28/2023 12:15
02/28/2023
SM-4500-NH3C
WP MTN
9045D
WP MTN
4500NO3F-2011
WP MTN
6010D
WP MTN
SW-7471B
WP MTN
SM-4500-NH3C-TKN
WP MTN
SM-2540G
WP MTN
WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN
Page 2 of 7

0
Waypoint.
7621 Whitepine
Road, Richmond,
VA 23237
Main 804-743-9401 ° Fax
804-271-6446
ANALYTICAL
www.waypointanalytical.com
46431
Synagro Central LLC
Project
Farmville
WWTP
Matthew Carter
Report Date : 03/09/2023
284 Boger Rd
Information :
Received : 02/28/2023
Mocksville , NC 27028
(j
Brandi Watson
Report Number : 23-059-0003
REPOR T OF A NA L YSIS
Lab No : 61096
Matrix: Solids
Sample ID : Farmville WWTP
Sampled: 2/28/2023 12:15
Test
Results
Units
MQL
DF
Date / Time
By Analytical
Analyzed
Method
Moisture
97.1
%
0.010
1
03/02/2316:00
FMM SM-2540G
Phosphorus
20000
mg/Kg - dry
172
1
03/06/23 22:04
TJS 6010D
Sulfur
9170
mg/Kg - dry
345
1
03/06/23 22:04
TJS 6010D
Calcium
10400
mg/Kg - dry
1720
1
03/06/23 22:04
TJS 6010D
Aluminum
9660
mg/Kg - dry
172
1
03/06/23 22:04
TJS 6010D
Manganese
393
mg/Kg - dry
17.2
1
03/06/23 22:04
TJS 6010D
Copper
316
mg/Kg - dry
17.2
1
03/04/23 04:19
JTR 6010D
Zinc
907
mg/Kg - dry
43.1
1
03/04/23 04:19
JTR 6010D
Organic N
49660
mg/Kg - dry
8621
1
03/07/23 09:30
CALCULATION
Nickel
15.3
mg/Kg - dry
8.62
1
03/04/23 04:19
JTR 6010D
Lead
21.9
mg/Kg - dry
10.3
1
03/04/23 04:19
JTR 6010D
Arsenic
<17.2
mg/Kg - dry
17.2
1
03/06/23 22:04
TJS 6010D
Selenium
<17.2
mg/Kg - dry
17.2
1
03/06/23 22:04
TJS 6010D
Test
Results
Units
MQL
DF
Date / Time
By Analytical
Analyzed
Method
Total Solids 2.85 % 0.010 1 03/02/23 16:00 FMM SM-2540G
Qualifiers/ DF Dilution Factor
Definitions
MQL Method Quantitation Limit
Page 3 of 7

Waypointo.
ANALYTICAL
46431
Synagro Central LLC Project
Matthew Carter
284 Boger Rd Information
Mocksville , NC 27028
Report Number : 23-059-0003
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Farmville WWTP
REPORT OF ANAL YSIS
Report Date : 03/09/2023
Received : 02/28/2023
6
Brandi Watson
Lab No : 61096
Sample ID : Farmville WWTP
Matrix: Solids
Sampled: 2/28/2023 12:15
Total Kjeldahl Nitrogen
49700
mg/Kg - dry
8620
1
03/07/23 09:30
JPJ ;M-4500-NH3C-TKP
Potassium
4380
mg/Kg - dry
345
1
03/06/23 22:04
TJS
6010D
Magnesium
2950
mg/Kg - dry
172
1
03/06/23 22:04
TJS
6010D
Sodium
2100
mg/Kg - dry
862
1
03/06/23 22:04
TJS
6010D
Iron
22400
mg/Kg - dry
345
1
03/04/23 04:19
JTR
6010D
Ammonia Nitrogen
<3450
mg/Kg - dry
3450
1
03/07/23 14:00
JPJ
SM-4500-NH3C
Nitrate+Nitrite-N
259
mg/Kg - dry
172
1
03/08/23 15:41
ZBD
4500NO3F-2011
Cadmium
<3.45
mg/Kg - dry
3.45
1
03/06/23 22:04
TJS
6010D
Chromium
21.9
mg/Kg - dry
8.62
1
03/04/23 04:19
JTR
6010D
Mercury
<6.10
mg/Kg - dry
6.10
1
03/02/23 12:36
FDS
SW-7471B
pH
6.3
S.U.
1
03/07/23 10:44
SAR
9045D
Total Volatile Solids
75.2
%
0.010
1
03/02/23 16:00
FMM
SM-2540G
Molybdenum
<8.62
mg/Kg - dry
8.62
1
03/04/23 04:19
JTR
6010D
Qualifiers/ DF Dilution Factor
Definitions
MQL Method Quantitation Limit
Page 4 of 7

Waypointo
ANALYTICAL
Client: Synagro Central LLC
Project: Farmville WWTP
Lab Report Number: 23-059-0003
Date: 3/8/2023
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
CASE NARRATIVE
Metals Analysis Method 6010D
Sample 92126 (MW2 Soil 10'-12')
Analyte: Aluminum
QC Batch No: 1-668064/1-667415
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 92126 (MW2 Soil 10'-12')
Analyte: Iron
QC Batch No: L667775/L667415
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 92126 (MW2 Soil 10'-12')
Analyte: Iron
QC Batch No: 1-668064/1-667415
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 92126 (MW2 Soil 10'-12')
Analyte: Potassium
QC Batch No: 1-668064/1-667415
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Sample 92126 (MW2 Soil 10'-12')
Analyte: Selenium
QC Batch No: 1-668064/1-667415
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Solids Total Mercury Analysis - CVAA Method 7471A
Sample 93579 (Soil)
Analyte: Mercury
QC Batch No: 1-667310/1-667045
The matrix spike, matrix spike duplicate and the post digestion spike were all outside of the quality control
acceptance ranges. Matrix interference is suspected.
Page 5 of 7

(2)
WayPAo Int..
NALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
www.waypointanalytical.com
Shipment Receipt Form
Customer Number: 46431
Customer Name: Synagro Central LLC
Report Number: 23-059-0003
Shipping Method
0 Fed Ex 0 US Postal 0 Lab 0 Other:
* UPS 0 Client 0 Courier Thermometer ID:
Shipping container/cooler uncompromised?
* Yes
0 No
Number of coolers/boxes received
F
Custody seals intact on shipping container/cooler?
0 Yes
0 No
Not Present
Custody seals intact on sample bottles?
0 Yes
0 No
Not Present
Chain of Custody (COC) present?
Yes
0 No
COC agrees with sample label(s)?
U Yes
0 No
COC properly completed
U Yes
0 No
Samples in proper containers?
U Yes
0 No
Sample containers intact?
Yes
0 No
Sufficient sample volume for indicated test(s)?
Yes
0 No
All samples received within holding time?
Yes
0 No
Cooler temperature in compliance?
Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
Yes
0 No
Water - Sample containers properly preserved
0 Yes
0 No
0 N/A
Water - VOA vials free of headspace
0 Yes
0 No
N/A
Trip Blanks received with VOAs
0 Yes
0 No
0 N/A
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
0 N/A
F_ High concentration container (48 hr) F Low concentration EnCore samplers (48 hr)
F_ High concentration pre -weighed (methanol -14 d) Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included?
0 Yes
0 No
Comments:
Signature: David Lennon Date & Time: 02/28/2023 11:46:41
Page 6 of 7

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Page 7 of 7

Waypointo
ANALYTICAL
5/31 /2023
Synagro Central LLC
Matthew Carter
284 Boger Rd
Mocksville, NC, 27028
Ref: Analytical Testing
Report Number: 23-138-0005
Project Description: Farmville WWTP
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Dear Matthew Carter:
Waypoint Analytical Virginia, Inc. received sample(s) on 5/18/2023 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Brandi Watson
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 1 of 8

(2)WaYPO*Int 7621 ain 80 -7 Road, Richmond, 27 -6446
Main 804-743 9401 °Fax [phone]
ANALYTICAL www.waypointanalytical.com
Sample Summary Table
Report Number: 23-138-0005
Client Project Description: Farmville WWTP
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
62065
Farmville WWTP
Solids
05/17/2023
08:00
05/18/2023
62065
Farmville WWTP
Solids
05/17/2023
08:00
05/18/2023
62065
Farmville WWTP
Solids
05/17/2023
08:00
05/18/2023
62065
Farmville WWTP
Solids
05/17/2023
08:00
05/18/2023
62065
Farmville WWTP
Solids
05/17/2023
08:00
05/18/2023
62065
Farmville WWTP
Solids
05/17/2023
08:00
05/18/2023
62065
Farmville WWTP
Solids
05/17/2023
08:00
05/18/2023
62065
Farmville WWTP
Solids
05/17/2023
08:00
05/18/2023
SM-4500-NH3C
WP MTN
9045D
WP MTN
4500NO3F-2011
WP MTN
6010D
WP MTN
SW-7471B
WP MTN
SM-4500-NH3C-TKN
WP MTN
SM-2540G
WP MTN
WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN
Page 2 of 8

0
Waypoint.
7621 Whitepine
Road, Richmond,
VA 23237
Main 804-743-9401 ° Fax
804-271-6446
ANALYTICAL
www.waypointanalytical.com
46431
Synagro Central LLC
Project
Farmville
WWTP
Matthew Carter
Report Date : 05/31/2023
284 Boger Rd
Information :
Received : 05/18/2023
Mocksville , NC 27028
(j
Brandi Watson
Report Number : 23-138-0005
REPOR T OF A NA L YSIS
Lab No : 62065
Matrix: Solids
Sample ID : Farmville WWTP
Sampled: 5/17/2023 8:00
Test
Results
Units
MQL
DF
Date / Time
By Analytical
Analyzed
Method
Moisture
98.7
%
0.010
1
05/24/2316:50
JLS SM-2540G
Phosphorus
28200
mg/Kg - dry
385
1
05/24/23 02:24
BKN 6010D
Sulfur
18600
mg/Kg - dry
769
1
05/24/23 02:24
BKN 6010D
Calcium
15800
mg/Kg - dry
3850
1
05/24/23 02:24
BKN 6010D
Aluminum
15500
mg/Kg - dry
385
1
05/24/23 02:24
BKN 6010D
Manganese
545
mg/Kg - dry
38.5
1
05/24/23 02:24
BKN 6010D
Copper
566
mg/Kg - dry
38.5
1
05/24/23 02:24
BKN 6010D
Zinc
1550
mg/Kg - dry
96.2
1
05/24/23 02:24
BKN 6010D
Organic N
77690
mg/Kg - dry
19230
1
05/26/23 12:00
CALCULATION
Nickel
26.5
mg/Kg - dry
19.2
1
05/24/23 02:24
BKN 6010D
Lead
43.6
mg/Kg - dry
23.1
1
05/24/23 02:24
BKN 6010D
Arsenic
<38.5
mg/Kg - dry
38.5
1
05/24/23 02:24
BKN 6010D
Selenium
<38.5
mg/Kg - dry
38.5
1
05/24/23 02:24
BKN 6010D
Test
Results
Units
MQL
DF
Date / Time
By Analytical
Analyzed
Method
Total Solids 1.32 % 0.010 1 05/24/23 16:50 JLS SM-2540G
Qualifiers/ DF Dilution Factor
Definitions
MQL Method Quantitation Limit
Page 3 of 8

Waypointo.
ANALYTICAL
46431
Synagro Central LLC Project
Matthew Carter
284 Boger Rd Information
Mocksville , NC 27028
Report Number : 23-138-0005
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Farmville WWTP
REPORT OF ANAL YSIS
Report Date : 05/31/2023
Received : 05/18/2023
6
Brandi Watson
Lab No : 62065
Sample ID : Farmville WWTP
Matrix: Solids
Sampled: 5/17/2023 8:00
Total Kjeldahl Nitrogen
77700
mg/Kg - dry
19200
1
05/30/23 12:30
JPJ ;M-4500-NH3C-TKP
Potassium
5870
mg/Kg - dry
769
1
05/25/23 12:00
BKN
6010D
Magnesium
4220
mg/Kg - dry
385
1
05/24/23 02:24
BKN
6010D
Sodium
5150
mg/Kg - dry
1920
1
05/24/23 02:24
BKN
6010D
Iron
40800
mg/Kg - dry
769
1
05/24/23 02:24
BKN
6010D
Ammonia Nitrogen
<7690
mg/Kg - dry
7690
1
05/26/23 12:00
JPJ
SM-4500-NH3C
Nitrate+Nitrite-N
<385
mg/Kg - dry
385
1
05/23/23 15:21
CLP
4500NO3F-2011
Cadmium
<7.69
mg/Kg - dry
7.69
1
05/24/23 02:24
BKN
6010D
Chromium
34.7
mg/Kg - dry
19.2
1
05/24/23 02:24
BKN
6010D
Mercury
<13.7
mg/Kg - dry
13.7
1
05/24/23 13:07
FDS
SW-7471B
pH
6.4
S.U.
1
05/23/2316:00
CNB
9045D
Total Volatile Solids
76.6
%
0.010
1
05/24/23 16:50
JLS
SM-254OG
Molybdenum
<19.2
mg/Kg - dry
19.2
1
05/24/23 02:24
BKN
6010D
Qualifiers/ DF Dilution Factor
Definitions
MQL Method Quantitation Limit
Page 4 of 8

Waypointo
ANALYTICAL
Client: Synagro Central LLC
Project: Farmville WWTP
Lab Report Number: 23-138-0005
Date: 5/31 /2023
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
CASE NARRATIVE
Metals Analysis Method 6010D
Sample 96813 (RM-2-2)
Analyte: Aluminum
QC Batch No: 1-683789/1-683512
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 96813 (RM-2-2)
Analyte: Arsenic
QC Batch No: 1-683789/1-683512
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Sample 96813 (RM-2-2)
Analyte: Calcium
QC Batch No: 1-683789/1-683512
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 96813 (RM-2-2)
Analyte: Iron
QC Batch No: 1-683789/1-683512
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 96813 (RM-2-2)
Analyte: Potassium
QC Batch No: 1-683789/1-683512
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 96813 (RM-2-2)
Analyte: Magnesium
QC Batch No: 1-683789/1-683512
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 96813 (RM-2-2)
Analyte: Manganese
QC Batch No: 1-684048/1-683512
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 96813 (RM-2-2)
Page 5 of 8

Waypointo
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
www.waypointanalytical.com
Analyte: Phosphorus
QC Batch No: 1-683789/1-683512
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 96813 (RM-2-2)
Analyte: Sulfur
QC Batch No: 1-683789/1-683512
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Page 6 of 8

(2)
WayPAo Int..
NALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
www.waypointanalytical.com
Shipment Receipt Form
Customer Number: 46431
Customer Name: Synagro Central LLC
Report Number: 23-138-0005
Shipping Method
0 Fed Ex 0 US Postal 0 Lab 0 Other:
* UPS 0 Client 0 Courier Thermometer ID:
Shipping container/cooler uncompromised?
* Yes
0 No
Number of coolers/boxes received
F
Custody seals intact on shipping container/cooler?
0 Yes
0 No
Not Present
Custody seals intact on sample bottles?
0 Yes
0 No
Not Present
Chain of Custody (COC) present?
Yes
0 No
COC agrees with sample label(s)?
U Yes
0 No
COC properly completed
U Yes
0 No
Samples in proper containers?
U Yes
0 No
Sample containers intact?
Yes
0 No
Sufficient sample volume for indicated test(s)?
Yes
0 No
All samples received within holding time?
Yes
0 No
Cooler temperature in compliance?
Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
Yes
0 No
Water - Sample containers properly preserved
0 Yes
0 No
0 N/A
Water - VOA vials free of headspace
0 Yes
0 No
N/A
Trip Blanks received with VOAs
0 Yes
0 No
0 N/A
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
0 N/A
F_ High concentration container (48 hr) F Low concentration EnCore samplers (48 hr)
F_ High concentration pre -weighed (methanol -14 d) Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included?
0 Yes
0 No
Comments:
Signature: David Lennon Date & Time: 05/18/2023 08:26:19
Page 7 of 8

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OTJ
Page 8 of 8

Waypointo
ANALYTICAL
10/6/2023
Synagro Central LLC
Matthew Carter
284 Boger Rd
Mocksville, NC, 27028
Ref: Analytical Testing
Report Number: 23-270-0008
Project Description: Farmville WWTP
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Dear Matthew Carter:
Waypoint Analytical Virginia, Inc. received sample(s) on 9/27/2023 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Brandi Watson
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 1 of 8

(2)WaYPO*Int 7621 ain 80 -7 Road, Richmond, 27 -6446
Main 804-743 9401 °Fax [phone]
ANALYTICAL www.waypointanalytical.com
Sample Summary Table
Report Number: 23-270-0008
Client Project Description: Farmville WWTP
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
63520
Farmville WWTP
Solids
09/26/2023
10:00
09/27/2023
63520
Farmville WWTP
Solids
09/26/2023
10:00
09/27/2023
63520
Farmville WWTP
Solids
09/26/2023
10:00
09/27/2023
63520
Farmville WWTP
Solids
09/26/2023
10:00
09/27/2023
63520
Farmville WWTP
Solids
09/26/2023
10:00
09/27/2023
63520
Farmville WWTP
Solids
09/26/2023
10:00
09/27/2023
63520
Farmville WWTP
Solids
09/26/2023
10:00
09/27/2023
63520
Farmville WWTP
Solids
09/26/2023
10:00
09/27/2023
SM-4500-NH3C
WP MTN
9045D
WP MTN
4500NO3F-2016
WP MTN
6010D
WP MTN
SW-7471B
WP MTN
SM-4500-NH3C-TKN
WP MTN
SM-2540G
WP MTN
WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN
Page 2 of 8

0
Waypoint.
7621 Whitepine
Road, Richmond,
VA 23237
Main 804-743-9401 ° Fax
804-271-6446
ANALYTICAL
www.waypointanalytical.com
46431
Synagro Central LLC
Project
Farmville
WWTP
Matthew Carter
Report Date : 10/06/2023
284 Boger Rd
Information :
Received : 09/27/2023
Mocksville , NC 27028
(j
Brandi Watson
Report Number : 23-270-0008
REPOR T OF A NA L YSIS
Lab No : 63520
Matrix: Solids
Sample ID : Farmville WWTP
Sampled: 9/26/2023 10:00
Test
Results
Units
MQL
DF
Date / Time
By Analytical
Analyzed
Method
Moisture
93.9
%
0.010
1
09/28/2316:16
CAH SM-2540G
Phosphorus
5540
mg/Kg - dry
82.0
1
09/30/23 05:22
BKN 6010D
Sulfur
2840
mg/Kg - dry
164
1
09/30/23 05:22
BKN 6010D
Calcium
2640
mg/Kg - dry
820
1
10/02/23 18:11
BKN 6010D
Aluminum
2330
mg/Kg - dry
82.0
1
09/30/23 05:22
BKN 6010D
Manganese
117
mg/Kg - dry
8.20
1
09/30/23 05:22
BKN 6010D
Copper
91.8
mg/Kg - dry
8.20
1
09/30/23 05:22
BKN 6010D
Zinc
266
mg/Kg - dry
20.5
1
10/02/23 18:11
BKN 6010D
Organic N
25130
mg/Kg - dry
4098
1
10/03/23 10:14
CALCULATION
Nickel
4.72
mg/Kg - dry
4.10
1
09/30/23 05:22
BKN 6010D
Lead
7.98
mg/Kg - dry
4.92
1
09/30/23 05:22
BKN 6010D
Arsenic
<8.20
mg/Kg - dry
8.20
1
09/30/23 05:22
BKN 6010D
Selenium
<8.20
mg/Kg - dry
8.20
1
09/30/23 05:22
BKN 6010D
Test
Results
Units
MQL
DF
Date / Time
By Analytical
Analyzed
Method
Total Solids 6.07 % 0.010 1 09/28/23 16:16 CAH SM-2540G
Qualifiers/ DF Dilution Factor
Definitions
MQL Method Quantitation Limit
Page 3 of 8

Waypointo.
ANALYTICAL
46431
Synagro Central LLC Project
Matthew Carter
284 Boger Rd Information
Mocksville , NC 27028
Report Number : 23-270-0008
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Farmville WWTP
REPORT OF ANAL YSIS
Report Date : 10/06/2023
Received : 09/27/2023
6
Brandi Watson
Lab No : 63520
Sample ID : Farmville WWTP
Matrix: Solids
Sampled: 9/26/2023 10:00
Total Kjeldahl Nitrogen
27000
mg/Kg - dry
4100
1
10/03/23 10:14
JPJ ;M-4500-NH3C-TKP
Potassium
997
mg/Kg - dry
164
1
09/30/23 05:22
BKN
6010D
Magnesium
808
mg/Kg - dry
82.0
1
09/30/23 05:22
BKN
6010D
Sodium
1060
mg/Kg - dry
410
1
09/30/23 05:22
BKN
6010D
Iron
7480
mg/Kg - dry
164
1
09/30/23 05:22
BKN
6010D
Ammonia Nitrogen
1920
mg/Kg - dry
1640
1
10/03/23 14:25
JPJ
SM-4500-NH3C
Nitrate+Nitrite-N
744
mg/Kg - dry
82.0
1
10/05/23 11:29
CLP
4500NO3F-2016
Cadmium
<1.64
mg/Kg - dry
1.64
1
09/30/23 05:22
BKN
6010D
Chromium
5.97
mg/Kg - dry
4.10
1
09/30/23 05:22
BKN
6010D
Mercury
<2.97
mg/Kg - dry
2.97
1
10/02/23 11:28
MRE
SW-7471B
pH
3.6
S.U.
1
10/02/2316:45
CNB
9045D
Total Volatile Solids
9.77
%
0.010
1
09/28/23 16:16
CAH
SM-2540G
Molybdenum
<4.10
mg/Kg - dry
4.10
1
09/30/23 05:22
BKN
6010D
Qualifiers/ DF Dilution Factor
Definitions
MQL Method Quantitation Limit
Page 4 of 8

Waypointo
ANALYTICAL
Client: Synagro Central LLC
Project: Farmville WWTP
Lab Report Number: 23-270-0008
Date: 10/6/2023
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
CASE NARRATIVE
Metals Analysis Method 6010D
Sample 88077 (AF-1)
Analyte: Aluminum
QC Batch No: 1-707895/1-707507
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 88077 (AF-1)
Analyte: Arsenic
QC Batch No: 1-707895/1-707507
The matrix spike, matrix spike duplicate and the post digestion spike were all outside of the quality control
acceptance ranges. Matrix interference is suspected
Sample 88077 (AF-1)
Analyte: Iron
QC Batch No: 1-707895/1-707507
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 88077 (AF-1)
Analyte: Potassium
QC Batch No: 1-707895/1-707507
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 88077 (AF-1)
Analyte: Manganese
QC Batch No: 1-707895/1-707507
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 88077 (AF-1)
Analyte: Lead
QC Batch No: 1-707895/1-707507
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Solids Total Mercury Analysis - CVAA Method 7471A
Sample 86603 (SS-10)
Analyte: Mercury
QC Batch No: 1-708004/1-707748
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Page 5 of 8

Waypointo
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
www.waypointanalytical.com
Page 6 of 8

(2)
WayPAo Int..
NALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
www.waypointanalytical.com
Shipment Receipt Form
Customer Number: 46431
Customer Name: Synagro Central LLC
Report Number: 23-270-0008
Shipping Method
0 Fed Ex 0 US Postal 0 Lab 0 Other:
* UPS 0 Client 0 Courier Thermometer ID:
Shipping container/cooler uncompromised?
* Yes
0 No
Number of coolers/boxes received
F
Custody seals intact on shipping container/cooler?
0 Yes
0 No
Not Present
Custody seals intact on sample bottles?
0 Yes
0 No
Not Present
Chain of Custody (COC) present?
Yes
0 No
COC agrees with sample label(s)?
U Yes
0 No
COC properly completed
U Yes
0 No
Samples in proper containers?
U Yes
0 No
Sample containers intact?
Yes
0 No
Sufficient sample volume for indicated test(s)?
Yes
0 No
All samples received within holding time?
Yes
0 No
Cooler temperature in compliance?
Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
Yes
0 No
Water - Sample containers properly preserved
0 Yes
0 No
N/A
Water - VOA vials free of headspace
0 Yes
0 No
N/A
Trip Blanks received with VOAs
0 Yes
0 No
0 N/A
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
0 N/A
F_ High concentration container (48 hr) F Low concentration EnCore samplers (48 hr)
F_ High concentration pre -weighed (methanol -14 d) Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included?
0 Yes
0 No
Comments:
Signature: David Lennon Date & Time: 09/27/2023 10:49:30
Page 7 of 8

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Page 8of8

SECTION 3

FACILITY NAME: FARMVILLE, NC
LAND OWNER: HAROLD FLANAGAN
OPERATOR: HAROLD FLANAGAN
CROP 1 NAME: CORN GRAIN (CGR)
RESIDUAL SOURCE(S): ' See fist at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
WO PERMIT#: WQ0008778 FIELD#: NC-P1-00001-0-0005-
ANNUAL DRY TONS APPLIED: 48.63 SITE #: NC PI 00001
PREDOMINANT SOIL SERIES: GOLDSBORO
CROP 1 MAX PAN: 147 CROP 2 NAME:
ACRES UTILIZED: 12.8
ACRES PERMITTED: 12.8
CATION EXCHANGE CAPACITY (NON-503):
CROP 2 MAX PAN:
Page: 1
Gallons (G)
Site
Name of Crop Type
or Cubic Yards (Y)
Cond.
Precip
Volati-
Mineral-
Ammonia
Nitrate
PAN Applied
Receiving Residual
Date or
or Wet Tons (W)
%
Residual
Dry, Wet,
Past 24 Hrs.
Application
lization
ization
TKN
Nitrogen
and Nitrite
(lbslacre)
Application
Month
Solids
DryTons/Ac
Source
Moist
Inches
Method`
Rate-
Rate—
mg/kg
mg/kg
mg/kg
Amount
UOM
Crap 1
Crop 2
Crop 1
Crop 2
3/2012023
130,200.00
(0)
2.850
1.209
FARAEDL
DRY
0-112"
SUR
0.5
0.30
49,700.00
3,450.00
259.00
40,816
CGR
3/21/2023
148,800.00
(G)
2.850
1.382
FARAEDL
DRY
0-<1/2"
SUR
0.5
0.30
49,700.00
3,450.00
259.00
46.647
CGR
3/2212023
130,200.00
(G)
2.850
1.209
FARAEDL
DRY
0-x112"
SUR
0.5
0.30
49,700.00
3,450.00
259.00
40,815
CGR
Mar-23
409,200.00
(G) _
,nnual Ibslacre Applied
umulative Ibslacre Applied
ermit PAN Limit (Ibslacre) 1st Crol
Iotal a.suu
AS CD CU CR PB HG MO
0.131 0.026 2.401 0.166 0.166 I 0.046 0.066
0.159 0.043 5.987 0.748 0.413 0.054 0.109
NI SE......" ZN
0.116 0.131 6.892
12.696
Total 128.279 0.000
Lime Applied
Date t
Federal C.P.L.R. (lbs/acre)-- 36.6 34.8 1 1,339.0 267.9 1 15.0 375.0 1 89.0 1 2,500.0
FARAEDL = FARMVILLE, NC AEROBICALLY DIGESTED LIQUID
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am
aware that there are sign c `t ties fo submitting false information, including the possibility of fines and imprisonment for knowing violations"
74
SIGNATURE OF LAND APPLIER DATE
NR = Not Reported or Not Required *' Mineralization Rates: Compost-0.1, Anaerobical[y digested-0.2, Aerobically digested-0.3, Raw Sludge-0.4
Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation `** C.P.L.R.: Cumulative Pollutant Loading Rate
Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 "*`* See Site pH & Lime Application Records Section of Report
Printed: 1/29/2024 DENR FORM FSF (1212006)

FACILITY NAME: FARMVILLE, NO
LAND OWNER: HAROLD FLANNAGAN
OPERATOR HAROLD FLANNAGAN
CROP 1 NAME: BERMiUDAGRASS, COMMON -
DA.CTI 10C Me nP\
RESIDUAL SOURCE(S):' See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
WQ PERMIT #: WQ0008778 FIELD#: NC-Pi-00001-0-0006-
ANNUAL DRY TONS APPLIED: 203.32 SITE #. NO PI 00001
PREDOMINANT SOIL SERIES: GOLDSBORO
CROP 1 MAX PAN: 230 CROP 2 NAME:
Page: 1
ACRES UTILIZED: 31.2
ACRES PERMITTED: 31.2
CATION EXCHANGE CAPACITY (NON-503):
CROP 2 MAX PAN:
Gallons (G)
Site
Name of Crop Type
or Cubic Yards (Y)
Cond_
Precip
Volati-
Mineral-
Ammonia
Nitrate
PAN Applied
Receiving Residual
Date or
or Wet Tons (W)
%
Residual
Dry, Wet,
Past24 Hrs.
Application
lizaticn
ization
TKN
Nitrogen
and Nitrite
(lbs/acre)
Application
Month
Solids
Dry Tons/Ac
Source
Moist
Inches
Method"
Rate"
Rate-
mg/kg
mg/kg
mg/kg
Amount
UOM
Crop 1
Crop 2
Crop 1
Crop 2
3/23/2023
99,200-00
(G)
2.850
0.37E
FARAEDL
DRY
0-<1/2"
SUR
0.5
0.30
49,700.00
3,450.00
259.00
12.758
SCOP
Mar-23
99,200.00
(G)
7/17/2023
99,200.00
(G)
1.320
0.175
FARAEDL
DRY
0-<1/2""
SUR
0.5
0.30
77,700.00
7,690.00
385.00
9.639
BCOP
7/18/2023
155,000.00
(G)
1.320
0-273
FARAEDL
DRY
0-<1/2""
SUR
0.5
0.30
7-7,700.00
7,690.00
385.00
15.060
BCOP
7/19)2023
117,800.00
(G)
1.320
0.208
FARAEDL
DRY
0-<1/2""
'SUR
0.5
0.30
T7,700.00
7,690.00
385.00
11.446
SLOP
Jul-23
372,000.00
(G)
11/14/2023
68,200.00
(G)
6.070
0,553
FARAEDL
DRY
0-<112""
SUR
0.5
0.30
27,000.00
1,920.00
744.00
10228
BCOP
11/15/2023
124,000.00
(G)
6.070
1.006
FARAEDL
DRY
0-<112"
SUR
0.5
0.30
27,000.00
1,920.00
744.00
18.597
SCOP
11/16/2023
111,600.00
(G)
6.070
0.906
FARAEDL
DRY
0-<112""
SUR
0.5
0.30
27,000.00
1,920.00
744.00
16.737
BCOP
1113OM23
86,800.00
(G)
6.070
0.704
FARAEDL
DRY
D-91/2"
SUR
0.5
0.30
27,000.00
1,920.00
744.00
13.018
SCOP
Nov-23
390,600.00
(G)
12/112023
55,800.00
(G)
6.070
0.453
FARAEDL
DRY
0-<1/2""
SUR
0.5
0.30
27.000.00
1,920.00
744.00
6.368
BCOP
12/4/2023
68,200.00
(G)
6.070
0.553
FARAEDL
DRY
0-<1/2""
SUR
0.5
0.30
27,000.00
1,920.00
744.00
10.228
BCOP
12/5/2023
111,600.00
(G)
6.070
0.905
FARAEDL
DRY
0.<1/2""
SUR
0.5
0.30
27,000.00
1,920.00
744.00
16.737
BCOP
12/6/2023
49,600.00
(G)
6.070
0.402
FARAEDL
DRY
0-<1/2""
SUR
0.5
0.30
27,000.00
1,920.00
744.00
7,439
BCOP
Dec-23
285,200.00
(G)
oral 0.010 Total 150.255 0.000
AS CD CU CR PB HQ MO NI SE ZN P Lime Applied
Annual lbs/acre Applied 0.153 1 0.031 1 1.988 0.128 0.161 0,055 0.077 0.096 0.153 5.637 112.877 Date Lbs/Ac
Cumulative lbs/acre Applied 0221 I 0.046 I 6.630 i 0.849 I 0.565 I 0.089 ! 0.151 1 0.532 0212 16.384
Permit PAN Limit (lbs/acre) 1st Crop, 230
Federal C.P.LR (lbs/acre)- 36.6 34.8 1,339.0 267.9 15.0 375.0 89.0 2,500.0
- -- -- ---
FARAEDL = FARMVILLE, NO AEROBICALLY DIGESTED LIQUID
"1 certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am
aware that there ar" enalties r ubmitting false information, including the possibility of fines and imprisonment for knowing violations."
r
SIGNATURE OF LAND APPLIER DATE
NR = Not Reported or Not Required Mineralization Rates: Compost-0.1, Anaerobical(y digested-0.2, Aerobically digested-0.3, Raw Sludge-0.4
Application Method: SUR - Surface, [NJ - Injection, SURIN - Incorporation *"" C.P.L.R.: Cumulative Pollutant Loading Rate
"* Volatilization Rate: Surface 0.5, Injection incorporation 1.0 *""*" See Site pH 8, Lime Application Records Section of Report
Printed: 1/29/2024 DENR FORM FSF (1212006)

SECTION 4

SUMMIT
ENVIRONMENTAL TECHNOLOGIES, INC.
Analytical Laboratories
September 14, 2023
Mathew Carter
Synagro
284 Boger Rd.
Mocksville, NC 27028
TEL: [phone]
FAX: [phone]
Summit Environmental Technologies, Inc.
3310 Win St.
Cuyahoga Falls, Ohio 44223
TEL: [phone] FAX.- [phone]
Website: http:llwww.settek.com
RE: Farmville WWTP - REVISED REPORT
Dear Mathew Carter:
Order No.: 23090278
Summit Environmental Technologies, Inc. received 1 sample(s) on 9/6/2023 for the
analyses presented in the following report.
There were no problems with the analytical events associated with this report unless noted
in the Case Narrative.
Quality control data is within laboratory defined or method specified acceptance limits
except where noted.
If you have any questions regarding these tests results, please feel free to call the
laboratory.
Sincerely,
Jennifer Woolf
Project Manager
3310 Win St.
Cuyahoga Falls, Ohio 44223
Arkansas 88-0735, California 2943, Colorado, Connecticut PH-0108, Florida NELAC E87688, Idaho OH00923, Illinois 200061, Indiana C-OH-13,
ISO/IEC 17025:2017 119125 L22-544, Kansas E-10347, Kentucky (Underground Storage Tank) 3, Kentucky 90146, Maryland 339, Michigan 9988,
Minnesota 1780279, Nevada OH009232020-1, New Hampshire 2996, New Jersey OH006, New York 11777, North Carolina 39705 and 631, North Dakota
R-201, Ohio DW, Ohio VAP CL0052, Oklahoma 2019-155, Oregon OH2O0001, Pennsylvania 68-01335, Rhode Island LA000317, South Carolina
92016001, Texas T104704466-19-16, Utah OH009232020-12, Virginia VELAP 10381, West Virginia 9957C
Page 1 of 35

summly Summit Environmental Technologies, Inc. Case Narrative
3310 Win St.
ENVIRONMENTAL TECHNOLOGIES, INC. Cuyahoga Falls, Ohio 44223 ` o#: 23090278
Analytical Laboratories TEL: [phone] FAX.- [phone]
Website: http://www.settek.com Date: 9/14/2023
CLIENT: Synagro
Project: Fannville WWTP - REVISED REPORT
WorkOrder Narrative:
23090278: This report in its entirety consists of the following documents: Cover Letter, Case Narrative,
Analytical Results, QC Summary Report, Applicable Accreditation Information, Chain -of -Custody,
Cooler Receipt Form, and other applicable forms as necessary. All documents contain the Summit
Environmental Technologies, Inc., Work Order Number assigned to this report.
Summit Environmental Technologies, Inc., holds the accreditations/certifications listed at the bottom of
the cover letter that may or may not pertain to this report. Please refer to the "Accreditation Program
Analytes Report" for accredited analytes list.
The information contained in this analytical report is the sole property of Summit Environmental
Technologies, Inc. and that of the customer. It cannot be reproduced in any form without the consent of
Summit Environmental Technologies, Inc. or the customer for which this report was issued. The results
contained in this report are only representative of the samples received. Conditions can vary at different
times and at different sampling conditions. Summit Environmental Technologies, Inc. is not responsible
for use or interpretation of the data included herein.
All results for Solid Samples are reported on an "as received" or "wet weight" basis unless indicated as
"dry weight" using the "-dry" designation on the reporting units.
This report is believed to meet all of the requirements of the accrediting agency, where applicable. Any
comments or problems with the analytical events associated with this report are noted below.
Analytical Sequence Sample Notes:
23090278-OOIA TCLP-SVOC-CPEST(8081B): RPD between quantitation and confirmation columns is
greater than 40%.
REVISED REPORT 9/14/23: Reporting limit raised for Heptachlor due to suspected contamination.
Revision v1
Page 2 of 35

SUMMIT Summit Environmental Technologies, In Qualifiers and Acronyms
3310 Win,'
ENVIRONMENTAL TECHNOLOGIES, INC Cuyahoga Falls, Ohio 442, Wo#: 23090278
Analytical Laboratories TEL: [phone] FAX.- (330) 253-44E
Website: httv:11Www.settek.co Date: 9/14/2023
These commonly used Qualifiers and Acronyms may or may not be present in this report.
Qualifiers
U The compound was analyzed for but was not detected.
J The reported value is greater than the Method Detection Limit but less than the Reporting Limit.
H The hold time for sample preparation and/or analysis was exceeded.
D The result is reported from a dilution.
E The result exceeded the linear range of the calibration or is estimated due to interference.
MC The result is below the Minimum Compound Limit.
* The result exceeds the Regulatory Limit or Maximum Contamination Limit.
m Manual integration was used to determine the area response.
d Manual integration in which peak was deleted
N The result is presumptive based on a Mass Spectral library search assuming a 1:1 response.
P The second column confirmation exceeded 25% difference.
C The result has been confirmed by GC/MS.
X The result was not confirmed when GUMS Analysis was performed.
B/MB+ The analyte was detected in the associated blank.
G The ICB or CCB contained reportable amounts of analyte.
QC-/+ The CCV recovery failed low (-) or high (+).
R/QDR The RPD was outside of accepted recovery limits.
QL-/+ The LCS or LCSD recovery failed low (-) or high (+).
QLR The LCS/LCSD RPD was outside of accepted recovery limits.
QM-/+ The MS or MSD recovery failed low (-) or high (+).
QMR The MS/MSD RPD was outside of accepted recovery limits.
QV-/+ The ICV recovery failed low (-) or high (+).
S The spike result was outside of accepted recovery limits.
Z Deviation; A deviation from the method was performed; Please refer to the Case Narrative for
additional information
Acronyms
ND
Not Detected
RL
Reporting Limit
QC
Quality Control
MDL
Method Detection Limit
NIB
Method Blank
LOD
Level of Detection
LCS
Laboratory Control Sample
LOQ
Level of Quantitation
LCSD
Laboratory Control Sample Duplicate
PQL
Practical Quantitation Limit
QCS
Quality Control Sample
CRQL
Contract Required Quantitation Limit
DUP
Duplicate
PL
Permit Limit
MS
Matrix Spike
RegLvl
Regulatory Limit
MSD
Matrix Spike Duplicate
MCL
Maximum Contamination Limit
RPD
Relative Percent Different
MinCL
Minimum Compound Limit
ICV
Initial Calibration Verification
RA
Reanalysis
ICB
Initial Calibration Blank
RE
Reextraction
CCV
Continuing Calibration Verification
TIC
Tentatively Identified Compound
CCB
Continuing Calibration Blank
RT
Retention Time
RLC
Reporting Limit Check
CF
Calibration Factor
DF
Dilution Factor
RF
Response Factor
This list of Qualifiers and Acronyms reflects the most commonly utilized Qualifiers and Acronyms for reporting.
Please refer to the Analytical Notes in the Case Narrative for any Qualifiers or Acronyms that do not appear in this
list or for additional information regarding the use of these Qualifiers on reported data.
Revision vl
Page 3 of 35

SUMMIT Summit Environmental Technologies, Inc.
3310 Win St.
ENVIRONMENTAL TECHNOLOGIES, INC Cuyahoga Falls, Ohio 44223
Analytical Laboratories TEL: [phone] FAX.- [phone]
Website: http://www.settek.com
CLIENT: Synagro
Project: Farmville WWTP - REVISED REPORT
Lab SampleID Client Sample ID
23090278-001 Farmville WWTP
Tag No Date Collected
9/5/2023 11:00:00 AM
Workorder
Sample Summary
WO#: 23090278
Date Received
9/6/2023 10:00:00 AM
14-Sep-23
Matrix
Solid
Page 4 of 35

SUMMIT Summit Environmental Technologies, Inc.
3310 Win St.
DATES REPORT
ENVIRONMENTAL TECHNOLOGIES, INC Cuyahoga Falls, Ohio 44223
WO#: 23090278
Analytical Laboratories TEL: [phone] FAX.- [phone]
Website: http://www.settek.com
14-Sep-23
Client:
Synagro
Project:
Fartnville WWTP - REVISED REPORT
Sample ID
Client Sample ID Collection Date Matrix Test Name
Leachate Date
Prep Date Analysis Date
23090278-OOIA Farmville WWTP 9/5/2023 11:00:00 AM Solid Ignitability of Solids (SW-846: 1030)
9/13/2023 4:00:25 PM
pH (SW9045D)
9/7/2023 4:00:00 PM
Reactive Cyanide (9014/7.3.3.2)-Solid
9/8/2023 2:45:00 PM
Reactive Sulfide (9034)/7.3.4.2
9/8/2023 12:35:00 PM
TCLP Herbicides
9/11/2023 9:03:03 PM
TCLP Mercury
9/7/2023 2:00:00 PM
9/11/2023 8:00:00 AM 9/11/2023 12:14:00 PM
TCLP Metals
9/7/2023 2:00:00 PM
9/8/2023 9:20:00 AM 9/8/2023 2:53:00 PM
TCLP Pesticides
9/7/2023 2:00:00 PM
9/11/2023 1:20:00 PM 9/12/2023 5:06:00 AM
TCLP Pesticides
9/7/2023 2:00:00 PM
9/11/2023 1:20:00 PM 9/12/2023 5:06:00 AM
TCLP Semi-Volatiles Analysis
9/7/2023 2:00:00 PM
9/11/2023 9:10:00 AM 9/11/2023 8:00:00 PM
(SW1311/8270)
TCLP Volatiles
9/7/2023 2:00:00 PM 9/9/2023 4:47:00 AM
Revision vl
Page 5 of 35

SUMMIT
Summit Environmental Technologies, Inc. Analytical Report
3310 Win St.
ENVIRONMENTAL TECHNOLOGIES, INC Cuyahoga Falls, Ohio 44223 (base report)
Analytical Laboratories TEL: [phone] FAX: [phone] WO#: 23090278
Website: htW.-Ilwww.settek.com Date Reported: 9/14/2023
CLIENT:
Synagro
Matrix:
SOLID
Lab ID:
23090278-001A
Project:
Farmville WWTP - REVISED REPORT
Client Sample ID Farmville WWTP
Tag Number:
Collection Date: 9/5/2023 11:00:00 AM
Analyses Result RL Qual Units DF Date Analyzed
FULL TCLP
TCLP MERCURY
TCLP Mercury
FULL TCLP
TCLP METALS
TCLP Arsenic(As)
TCLP Barium(Ba)
TCLP Cadmium(Cd)
TCLP Chromium(Cr)
TCLP Lead(Pb)
TCLP Selenium(Se)
TCLP Silver(Ag)
SW7470A SW7470A Analyst: MP
ND 0.00200 mg/L 1 9/11/2023 12:14:00 PM
SW6010 SW3010A Analyst: RJE
ND
0.500
mg/L
1
9/8/2023 2:53:00 PM
ND
1.00
mg/L
1
9/8/2023 2:53:00 PM
ND
0.100
mg/L
1
9/8/2023 2:53:00 PM
ND
0.200
mg/L
1
9/8/2023 2:53:00 PM
ND
0.500
mg/L
1
9/8/2023 2:53:00 PM
ND
0.0500
mg/L
1
9/8/2023 2:53:00 PM
ND
0.500
mg/L
1
9/8/2023 2:53:00 PM
FULL TCLP
TCLP SEMI-VOLATILES ANALYSIS (SW1311/8270)
1,4-Dichlorobenzene
ND
2,4,5-Trichlorophenol
ND
2,4,6-Trichlorophenol
ND
2,4-Dinitrotoluene
ND
Cresols, Total
ND
Hexachloro-1,3-butadiene
ND
Hexachlorobenzene
ND
Hexachloroethane
ND
Nitrobenzene
ND
Pentachlorophenol
ND
Pyridine
ND
Surr: 2-Fluorophenol
64.0
Surr: Phenol-d6
63.4
Surr: Nitrobenzene-d5
52.8
Surr: 2,4,6-Tribromophenol
84.1
Surr: 2-Fluorobiphenyl
58.1
Surr: p-Terphenyl-d14
67.7
SW8270 SW3510C Analyst: JAP
0.100
mg/L
1
9/11/2023 8:00:00 PM
0.250
mg/L
1
9/11/2023 8:00:00 PM
0.250
mg/L
1
9/11/2023 8:00:00 PM
0.0500
mg/L
1
9/11/2023 8:00:00 PM
5.00
mg/L
1
9/11/2023 8:00:00 PM
0.0200
mg/L
1
9/11/2023 8:00:00 PM
0.0500
mg/L
1
9/11/2023 8:00:00 PM
0.100
mg/L
1
9/11/2023 8:00:00 PM
0.100
mg/L
1
9/11/2023 8:00:00 PM
0.250
mg/L
1
9/11/2023 8:00:00 PM
0.250
mg/L
1
9/11/2023 8:00:00 PM
10 - 130
%Rec
1
9/11/2023 8:00:00 PM
10 - 130
%Rec
1
9/11/2023 8:00:00 PM
10 - 130
%Rec
1
9/11/2023 8:00:00 PM
19 - 151
%Rec
1
9/11/2023 8:00:00 PM
10 - 130
%Rec
1
9/11/2023 8:00:00 PM
20 - 181
%Rec
1
9/11/2023 8:00:00 PM
Qualifiers: B
Analyte detected in the associated Method Blank
H
Holding times for preparation or analysis exceeded
MC
Value is below Minimum Compound Limit.
ND
Not Detected
P
Second column confirmation exceeds
R
RPD outside accepted recovery limits
E Value above quantitation range
M Manual Integration used to determine area response
N Tentatively identified compounds
OGI
PL Permit Limit Revision vl
RL Reporting Detection Limit
Page 6 of 35

SUMMIT
Summit Environmental Technologies, Inc. Analytical Report
3310 Win St.
ENVIRONMENTAL TECHNOLOGIES, INC Cuyahoga Falls, Ohio 44223 (base report)
Analytical Laboratories TEL: [phone] FAX: [phone] WO#: 23090278
Website: htW.-Ilwww.settek.com Date Reported: 9/14/2023
CLIENT: Synagro
Tag Number:
Matrix: SOLID
Collection Date:
9/5/2023 11:00:00 AM
Lab ID: 23090278-001A
Project: Farmville WWTP
- REVISED REPORT
Client Sample ID Farmville WWTP
Analyses
Result
RL
Qual Units
DF
Date Analyzed
FULL TCLP
SW8081
SW3510C Analyst: PGP
TCLP PESTICIDES
Chlordane, total
ND
0.00500
mg/L
2
9/12/2023 5:06:00 AM
Toxaphene
ND
0.0100
mg/L
2
9/12/2023 5:06:00 AM
Endrin
ND
0.00100
mg/L
2
9/12/2023 5:06:00 AM
gamma-BHC
ND
0.00100
mg/L
2
9/12/2023 5:06:00 AM
Heptachlor
ND
0.00800
P mg/L
2
9/12/2023 5:06:00 AM
Heptachlor epoxide
ND
0.00100
mg/L
2
9/12/2023 5:06:00 AM
Methoxychlor
ND
0.00100
mg/L
2
9/12/2023 5:06:00 AM
Surr: TCMX
73.9
10 - 119
%Rec
2
9/12/2023 5:06:00 AM
Surr: DCB
86.2
10 - 119
%Rec
2
9/12/2023 5:06:00 AM
FULL TCLP
SW8321
Analyst: JDB
TCLP HERBICIDES
2,4-D
ND
0.500
mg/L
50
9/11/2023 9:03:03 PM
2,4,5-TP
ND
0.500
mg/L
50
9/11/2023 9:03:03 PM
Surr: DCAA
97.5
70 - 130
%Rec
50
9/11/2023 9:03:03 PM
FULL TCLP
SW8260
SW1311M Analyst: ALS
TCLP VOLATILES
M-Dichloroethene
ND
0.250
mg/L
50
9/9/2023 4:47:00 AM
1,2-Dichloroethane
ND
0.250
mg/L
50
9/9/2023 4:47:00 AM
MEK
ND
5.00
mg/L
50
9/9/2023 4:47:00 AM
Benzene
ND
0.250
mg/L
50
9/9/2023 4:47:00 AM
Carbon tetrachloride
ND
0.250
mg/L
50
9/9/2023 4:47:00 AM
Chlorobenzene
ND
2.50
mg/L
50
9/9/2023 4:47:00 AM
Chloroform
ND
0.250
mg/L
50
9/9/2023 4:47:00 AM
Tetrachloroethene
ND
0.250
mg/L
50
9/9/2023 4:47:00 AM
Trichloroethene
ND
0.250
mg/L
50
9/9/2023 4:47:00 AM
Vinyl chloride
ND
0.100
mg/L
50
9/9/2023 4:47:00 AM
Surr: 4-Bromofluorobenzene
95.9
70 - 130
%Rec
50
9/9/2023 4:47:00 AM
Surr: Dibromofluoromethane
96.9
70 - 130
%Rec
50
9/9/2023 4:47:00 AM
Surr: Toluene-d8
102
70 - 130
%Rec
50
9/9/2023 4:47:00 AM
Qualifiers: B
Analyte detected in the associated Method Blank
E
Value above quantitation range
H
Holding times for preparation or analysis exceeded
M
Manual Integration used to determine area response
MC
Value is below Minimum Compound Limit.
N
Tentatively identified compounds
ND
Not Detected
OGI
P
Second column confirmation exceeds
PL
Permit Limit Revision vl
R
RPD outside accepted recovery limits
RL
Reporting Detection Limit
Page 7 of 35

SUMMIT
Summit Environmental Technologies, Inc.
3310 Win St.
Analytical Report
ENVIRONMENTAL TECHNOLOGIES, INC
Cuyahoga Falls, Ohio 44223
(base report)
Analytical Laboratories
TEL: [phone] FAX.- [phone]
WO#: 23090278
Website: http://www.settek.com
Date Reported: 9/14/2023
CLIENT:
Synagro
Tag Number:
Matrix:
SOLID
Collection Date:
9/5/2023 11:00:00 AM
Lab ID:
23090278-OOIA
Project:
Farrnville WWTP - REVISED REPORT
Client Sample ID Farmville WWTP
Analyses
Result
RL Qual Units
DF
Date Analyzed
RCI-SOLID-W/ IGNITABILITY1030
SW9014
Analyst: HDJ
REACTIVE CYANIDE (9014/7.3.3.2)-SOLID
Cyanide, Reactive
ND
0.495 mg/Kg
1
9/8/2023 2:45:00 PM
RCI-SOLID-W/ IGNITABILITY1030
SW1030
Analyst: SMZ
IGNITABILITY OF SOLIDS (SW-846: 1030)
Ignitability non-flammable
mm/sec
1
9/13/2023 4:00:25 PM
RCI-SOLID-W/ IGNITABILITY1030
SW9045D
Analyst: GJN
PH (SW9045D)
pH
7.0
s.u.@22.2C
1
9/7/2023 4:00:00 PM
RCI-SOLID-W/ IGNITABILITY1030
SW9034
Analyst: HDJ
REACTIVE SULFIDE (9034)/7.3.4.2
Sulfide, Reactive
ND
25.0 mg/Kg
1
9/8/2023 12:35:00 PM
Qualifiers: B
Analyte detected in the associated Method Blank
H
Holding times for preparation or analysis exceeded
MC
Value is below Minimum Compound Limit.
ND
Not Detected
P
Second column confirmation exceeds
R
RPD outside accepted recovery limits
E Value above quantitation range
M Manual Integration used to determine area response
N Tentatively identified compounds
OGl
PL Permit Limit Revision vl
RL Reporting Detection Limit
Page 8 of 35

Summit Environmental Technologies, Inc.
Accreditation
Program
3310 Win St.
SUMMIEF
Anal te5 Report
Y p
ENVIRONMENTAL TECHNOLOGIES,
INC Cuyahoga Falls, Ohio 44223
Analytical Laboratories
TEL: [phone] FAX.- [phone]
WO#:
23090278
Website: hgp:llwww.settek.com
14-Sep-23
Client: Synagro
State: NW
Project: Farmville WWTP - REVISED REPORT
Program Name: NC WW SCM
Sample ID Matrix
Test Name
Analyte
Status
23090278-OOIA Solid
Ignitability of Solids (SW-846: 1030)
Ignitability
A
Solid
pH (SW9045D)
Hydrogen Ion (pH)
A
Solid
Reactive Cyanide (9014/7.3.3.2)-Solid
Cyanide, Reactive
U
Solid
Reactive Sulfide (9034)/7.3.4.2
Sulfide, Reactive
U
Solid
TCLP Herbicides
2,4,5-TP
A
Solid
TCLP Herbicides
2,4-D
A
Solid
TCLP Mercury
Mercury
A
Solid
TCLP Metals
Arsenic
A
Solid
TCLP Metals
Barium
A
Solid
TCLP Metals
Cadmium
A
Solid
TCLP Metals
Chromium
A
Solid
TCLP Metals
Lead
A
Solid
TCLP Metals
Selenium
A
Solid
TCLP Metals
Silver
A
Solid
TCLP Pesticides
Chlordane, total
A
Solid
TCLP Pesticides
Endrin
A
Solid
TCLP Pesticides
gamma-BHC
A
Solid
TCLP Pesticides
Heptachlor
A
Solid
TCLP Pesticides
Heptachlor epoxide
A
Solid
TCLP Pesticides
Methoxychlor
A
Solid
TCLP Pesticides
Toxaphene
A
Solid
TCLP Semi-Volatiles Analysis (SW1311/8270)
1,4-Dichlorobenzene
A
Solid
TCLP Semi-Volatiles Analysis (SW1311/8270)
2,4,5-Trichlorophenol
A
Solid
TCLP Semi-Volatiles Analysis (SW1311/8270)
2,4,6-Trichlorophenol
A
Solid
TCLP Semi-Volatiles Analysis (SW1311/8270)
2,4-Dinitrotoluene
A
Solid
TCLP Semi-Volatiles Analysis (SW1311/8270)
Cresols, Total
A
Solid
TCLP Semi-Volatiles Analysis (SW1311/8270)
Hexachlorobenzene
A
Solid
TCLP Semi-Volatiles Analysis (SW1311/8270)
Hexachlorobutadiene
A
Solid
TCLP Semi-Volatiles Analysis (SW1311/8270)
Hexachloroethane
A
Solid
TCLP Semi-Volatiles Analysis (SW1311/8270)
Nitrobenzene
A
Solid
TCLP Semi-Volatiles Analysis (SW1311/8270)
Pentachlorophenol
A
Solid
TCLP Semi-Volatiles Analysis (SW1311/8270)
Pyridine
A
Key
Key
NC WW SCM A Accredited
NC WW SCM U Unavailable
Version #2
Page 9 of 35

Summit Environmental Technologies, Inc.
Accreditation Program
3310 Win St.
SUMMIEF
Anal te5 Report
Y p
ENVIRONMENTAL TECHNOLOGIES, INC Cuyahoga Falls, Ohio 44223
Analytical Laboratories TEL: [phone] FAX.- [phone]
WO#: 23090278
Website: hgp:llwww.settek.com
14-Sep-23
Client: Synagro
State: NW
Project: Farmville WWTP - REVISED REPORT
Program Name: NC WW SCM
Sample ID Matrix Test Name
Analyte Status
23090278-OOIA Solid TCLP Volatiles
1,1-Dichloroethene A
Solid TCLP Volatiles
1,2-Dichloroethane A
Solid TCLP Volatiles
2-Butanone A
Solid TCLP Volatiles
Benzene A
Solid TCLP Volatiles
Carbon tetrachloride A
Solid TCLP Volatiles
Chlorobenzene A
Solid TCLP Volatiles
Chloroform A
Solid TCLP Volatiles
Tetrachloroethene A
Solid TCLP Volatiles
Trichloroethene A
Solid TCLP Volatiles
Vinyl chloride A
NC WW SCM A Accredited NC WW SCM U Unavailable
Version #2
Page 10 of 35

SUMMIT Summit Environmental Technologies, Inc.
3310 Win St.
ENVIRONMENTAL TECHNOLOGIES, INC Cuyahoga Falls, Ohio 44223
Analytical Laboratories TEL: [phone] FAX: [phone]
Website: http://www.settek.coni
Client: Synagro
Project: Farmville WWTP - REVISED REPORT
QC SUMMARY REPORT
WO#: 23090278
14 Sep-23
BatchID: 68466
Sample ID: LCS-68466
SampType: LCS
TestCode: TCLP-VOC-M Units: mg/L
Prep Date:
RunNo: 170578
Client ID: LCSS
Batch ID: 68466
TestNo: SW8260 SW1311M
Analysis Date: 9/9/2023
SegNo: 4587043
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
1,1-Dichloroethene
0.0195
0.00500
0.0200
0
97.4
64.7
136
1,2-Dichloroethane
0.0191
0.00500
0.0200
0
95.4
70
130
MEK
ND
0.100
0.100
0
89.9
55.1
149
Benzene
0.0209
0.00500
0.0200
0
105
70
130
Carbon tetrachloride
0.0196
0.00500
0.0200
0
98.0
70
130
Chlorobenzene
0.0198
0.00500
0.0200
0
98.9
70
130
Chloroform
0.0197
0.00500
0.0200
0
98.6
70
130
Tetrachloroethene
0.0197
0.00500
0.0200
0
98.7
70
134
Trichloroethene
0.0206
0.00500
0.0200
0
103
62.8
160
Vinyl chloride
0.0158
0.00200
0.0200
0
79.2
67.1
130
Sum 4-Bromofluorobenzene
50.1
50.00
100
70
130
Sum Dibromofluoromethane
49.8
50.00
99.6
70
130
Surr: Toluene-d8
51.2
50.00
102
70
130
Sample ID: EXBLK1-68466
SampType: MBLK
TestCode: TCLP-VOC-M Units: mg/L
Prep Date: 9/7/2023
RunNo: 170578
Client ID: PBS
Batch ID: 68466
TestNo: SW8260 SW1311M
Analysis Date: 9/9/2023
SegNo: 4587046
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
1,1-Dichloroethene
ND 0.100
1,2-Dichloroethane
ND 0.100
MEK
ND 2.00
Benzene
ND 0.100
Qualifiers: B
Analyte detected in the associated Method Blank
J
Analyte detected below quantitation limits
ND
Not Detected
PL
Permit Limit
E Value above quantitation range H Holding times for preparation or anal,
M Manual Integration used to determine area response MC Value is below Minimum Compound
Revision vl
OGl P Second column confirmation exceeds
R RPD outside accepted recovery limits RL Reporting Detection Limit
Page 11 of 35

SUMMIT Summit Environmental Technologies, Inc.
3310 Win St.
ENVIRONMENTAL TECHNOLOGIES, INC Cuyahoga Falls, Ohio 44223
Analytical Laboratories TEL: [phone] FAX: [phone]
Website: http://www.settek.coni
Client: Synagro
Project: Farmville WWTP - REVISED REPORT
QC SUMMARY REPORT
WO#: 23090278
14 Sep-23
BatchID: 68466
Sample ID: EXBLK1-68466
SampType: MBLK
TestCode: TCLP-VOC-M Units: mg/L
Prep Date: 9/7/2023
RunNo: 170578
Client ID: PBS
Batch ID: 68466
TestNo: SW8260 SW1311M
Analysis Date: 9/9/2023
SegNo: 4587046
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Carbon tetrachloride
ND
0.100
Chlorobenzene
ND
0.100
Chloroform
ND
0.100
Tetrachloroethene
ND
0.100
Trichloroethene
ND
0.100
Vinyl chloride
ND
0.0400
Sum 4-Bromofluorobenzene
974
Sum Dibromofluoromethane
974
Sum Toluene-d8
1030
1000 97.4 70 130
1000 97.4 70 130
1000 103 70 130
Sample ID: 23090238-001AMS
SampType: MS
TestCode: TCLP-VOC-M Units: mg/L
Prep Date:
RunNo: 170578
Client ID: BatchQC
Batch ID: 68466
TestNo: SW8260 SW1311M
Analysis Date: 9/9/2023
SegNo: 4587048
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
1,1-Dichloroethene
2.20
0.500
1,2-Dichloroethane
2.16
0.500
MEK
ND
10.0
Benzene
2.38
0.500
Carbon tetrachloride
2.20
0.500
Chlorobenzene
2.18
0.500
Chloroform
2.18
0.500
Tetrachloroethene
2.29
0.500
Qualifiers: B
Analyte detected in the associated Method Blank
J
Analyte detected below quantitation limits
ND
Not Detected
PL
Permit Limit
2.00
0
110
13.6
2.00
0
108
55.7
10.0
0
99.9
65.3
2.00
0
119
49.2
2.00
0
110
26.7
2.00
0
109
33.7
2.00
0
109
48.5
2.00
0
115
19.2
E Value above quantitation range
M Manual Integration used to determine area response
OGl
R RPD outside accepted recovery limits
Page 12 of 35
202
138
130
145
156
159
145
191
H Holding times for preparation or anal,
MC Value is below Minimum Compound
P Second column confirmation exceeds
RL Reporting Detection Limit
Revision vl

SUMMIT Summit Environmental Technologies, Inc.
3310 Win St.
ENVIRONMENTAL TECHNOLOGIES, INC Cuyahoga Falls, Ohio 44223
Analytical Laboratories TEL: [phone] FAX: [phone]
Website: http://www.settek.coni
Client: Synagro
Project: Farmville WWTP - REVISED REPORT
QC SUMMARY REPORT
BatchID: 68466
WO#: 23090278
14 Sep-23
Sample ID: 23090238-001AMS
SampType: MS
TestCode: TCLP-VOC-M Units: mg/L
Prep Date:
RunNo: 170578
3lient ID: Batch=
Batch ID: 68466
TestNo: SW8260 SW1311M
Analysis Date: 9/9/2023
SegNo: 4587048
analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Trichloroethene
2.33 0.500
2.00
0 117
38.4
167
Vinyl chloride
2.89 0.200
2.00
0 144
27.3
161
Surr: 4-Bromofluorobenzene
5050
5000
101
70
130
Surr: Dibromofluoromethane
4970
5000
99.5
70
130
Surr: Toluene-d8
5040
5000
101
70
130
Sample ID: 23090238-001AMSD
SampType: MSD
TestCode: TCLP-VOC-M Units: mg/L
Prep Date:
RunNo: 170578
3lient ID: Batch=
Batch ID: 68466
TestNo: SW8260 SW1311M
Analysis Date: 9/9/2023
SegNo: 4587049
analyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
1,1-Dichloroethene
2.24
0.500
1,2-Dichloroethane
2.14
0.500
MEK
ND
10.0
Benzene
2.36
0.500
Carbon tetrachloride
2.19
0.500
Chlorobenzene
2.16
0.500
Chloroform
2.22
0.500
Tetrachloroethene
2.19
0.500
Trichloroethene
2.36
0.500
Vinyl chloride
2.48
0.200
Surr: 4-Bromofluorobenzene
5080
Surr: Dibromofluoromethane 4930
Qualifiers: B
Analyte detected in the associated Method Blank
J
Analyte detected below quantitation limits
ND
Not Detected
PL
Permit Limit
2.00
0
112
13.6
2.00
0
107
55.7
10.0
0
100
65.3
2.00
0
118
49.2
2.00
0
110
26.7
2.00
0
108
33.7
2.00
0
ill
48.5
2.00
0
110
19.2
2.00
0
118
38.4
2.00
0
124
27.3
5000
102
70
5000
98.6
70
E Value above quantitation range
M Manual Integration used to determine area response
OGl
R RPD outside accepted recovery limits
Page 13 of 35
202
2.20
1.76
25
138
2.16
0.465
25
130
0
0
25
145
2.38
0.846
25
156
2.20
0.410
25
159
2.18
1.10
25
145
2.18
1.55
25
191
2.29
4.37
25
167
2.33
0.981
25
161
2.89
15.1
25
130
0
25
130
0
25
H Holding times for preparation or anal,
MC Value is below Minimum Compound
Revision vl
P Second column confirmation exceeds
RL Reporting Detection Limit

SUMMIT Summit Environmental Technologies, Inc.
3310 Win St.
ENVIRONMENTAL TECHNOLOGIES, INC Cuyahoga Falls, Ohio 44223
Analytical Laboratories TEL: [phone] FAX.- [phone]
Website: hgp:llwww.settek.com
QC SUMMARY REPORT
Wo#: 23090278
14-Sep-23
Client: Synagro
Project: Farmvillc WWTP - REVISED REPORT BatchID: 68466
Sample ID: 23090238-001AMSD
SampType: MSD
TestCode: TCLP-VOC-M Units: mg/L
Prep Date:
RunNo: 170578
Client ID: BatchQC
Batch ID: 68466
TestNo: SW8260 SW1311M
Analysis Date: 9/9/2023
SegNo: 4587049
Analyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
Sum Toluene-d8
5010
5000
100 70 130
0 25
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal,
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
Revision vl
ND Not Detected OGl P Second column confirmation exceeds
PL Permit Limit R RPD outside accepted recovery limits RL Reporting Detection Limit
Page 14 of 35

SUMMIT Summit Environmental Technologies, Inc.
3310 Win St.
ENVIRONMENTAL TECHNOLOGIES, INC Cuyahoga Falls, Ohio 44223
Analytical Laboratories TEL: [phone] FAX: [phone]
Website: http://www.settek.coni
Client: Synagro
Project: Farmville WWTP - REVISED REPORT
QC SUMMARY REPORT
WO#: 23090278
14 Sep-23
BatchID: 68510
Sample ID: MB-68510
SampType: MBLK
TestCode: MTL-TCLP-7( Units: mg/L
Prep Date: 9/8/2023
RunNo: 170444
Client ID: PBS
Batch ID: 68510
TestNo: SW6010 SW3010A
Analysis Date: 9/8/2023
SegNo: 4586973
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
TCLP Arsenic(As)
ND
0.500
TCLP Barium(Ba)
ND
1.00
TCLP Cadmium(Cd)
ND
0.100
TCLP Chromium(Cr)
ND
0.200
TCLP Lead(Pb)
ND
0.500
TCLP Selenium(Se)
ND
0.0500
TCLP Silver(Ag)
ND
0.500
Sample ID: LCS-68510
SampType: LCS
TestCode: MTL-TCLP-7( Units: mg/L
Prep Date: 9/8/2023
RunNo: 170444
Client ID: LCSS
Batch ID: 68510
TestNo: SW6010 SW3010A
Analysis Date: 9/8/2023
SegNo: 4586974
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
TCLP Arsenic(As)
2.22
0.500
2.000
0
ill
80
120
TCLP Barium(Ba)
1.98
1.00
2.000
0
98.9
80
120
TCLP Cadmium(Cd)
2.15
0.100
2.000
0
108
80
120
TCLP Chromium(Cr)
2.18
0.200
2.000
0
109
80
120
TCLP Lead(Pb)
2.21
0.500
2.000
0
ill
80
120
TCLP Selenium(Se)
2.10
0.0500
2.000
0
105
80
120
TCLP Silver(Ag)
2.18
0.500
2.000
0
109
80
120
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal,
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
Revision V 1
ND Not Detected OGl P Second column confirmation exceeds
PL Permit Limit R RPD outside accepted recovery limits RL Reporting Detection Limit
Page 15 of 35

SUMMIT Summit Environmental Technologies, Inc.
3310 Win St.
ENVIRONMENTAL TECHNOLOGIES, INC Cuyahoga Falls, Ohio 44223
Analytical Laboratories TEL: [phone] FAX: [phone]
Website: http://www.settek.coni
Client: Synagro
Project: Farmville WWTP - REVISED REPORT
QC SUMMARY REPORT
WO#: 23090278
14 Sep-23
BatchID: 68510
Sample ID: 23090255-001AMS
SampType: MS
TestCode: Mtl-TCLP-7(6 Units: mg/L
Prep Date: 9/8/2023
RunNo: 170444
Client ID: Batch=
Batch ID: 68510
TestNo: SW6010 SW3010A
Analysis Date: 9/8/2023
SegNo: 4586977
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
TCLP Arsenic(As)
2.04
0.100
2.000
0
102
70
130
TCLP Barium(Ba)
2.62
1.00
2.000
0.8642
87.6
70
130
TCLP Cadmium(Cd)
1.69
0.100
2.000
0.001400
84.5
70
130
TCLP Chromium(Cr)
1.78
0.200
2.000
0
88.8
70
130
TCLP Lead(Pb)
1.75
0.100
2.000
0
87.7
70
130
TCLP Selenium(Se)
2.03
0.100
2.000
0
102
70
130
TCLP Silver(Ag)
2.05
0.100
2.000
0
102
70
130
Sample ID: 23090255-001AMSD
SampType: MSD
TestCode: Mtl-TCLP-7(6 Units: mg/L
Prep Date: 9/8/2023
RunNo: 170444
Client ID: Batch=
Batch ID: 68510
TestNo: SW6010 SW3010A
Analysis Date: 9/8/2023
SegNo: 4586978
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
TCLP Arsenic(As)
2.11
0.100
2.000
0
106
70
130
2.043
3.24
20
TCLP Barium(Ba)
2.72
1.00
2.000
0.8642
92.8
70
130
2.617
3.87
20
TCLP Cadmium(Cd)
1.75
0.100
2.000
0.001400
87.3
70
130
1.692
3.25
20
TCLP Chromium(Cr)
1.83
0.200
2.000
0
91.5
70
130
1.776
3.05
20
TCLP Lead(Pb)
1.80
0.100
2.000
0
90.2
70
130
1.753
2.90
20
TCLP Selenium(Se)
2.08
0.100
2.000
0
104
70
130
2.034
2.05
20
TCLP Silver(Ag)
2.12
0.100
2.000
0
106
70
130
2.049
3.31
20
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal,
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
Revision V 1
ND Not Detected OGl P Second column confirmation exceeds
PL Permit Limit R RPD outside accepted recovery limits RL Reporting Detection Limit
Page 16 of 35

SUMMIT Summit Environmental Technologies, Inc.
3310 Win St.
ENVIRONMENTAL TECHNOLOGIES, INC Cuyahoga Falls, Ohio 44223
Analytical Laboratories TEL: [phone] FAX: [phone]
Website: http://www.settek.coni
Client: Synagro
Project: Farmville WWTP - REVISED REPORT
QC SUMMARY REPORT
WO#: 23090278
14 Sep-23
BatchID: 68547
Sample ID: MB-68547
SampType: MBLK
TestCode: HG_TCLP(74 Units: PPM
Prep Date: 9/11/2023
RunNo: 170584
Client ID: PBS
Batch ID: 68547
TestNo: SW7470A SW7470A
Analysis Date: 9/11/2023
SegNo: 4587743
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
TCLP Mercury ND 0.00200
Sample ID: LCS-68547
SampType: LCS
TestCode: HG_TCLP(74 Units: PPM
Prep Date: 9/11/2023
RunNo: 170584
Client ID: LCSS
Batch ID: 68547
TestNo: SW7470A SW7470A
Analysis Date: 9/11/2023
SegNo: 4587744
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
TCLP Mercury
0.00388 0.00200 0.00400 0 97.0 80 120
Qualifiers: B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
PL Permit Limit
E Value above quantitation range H Holding times for preparation or anal,
M Manual Integration used to determine area response MC Value is below Minimum Compound
OGl P Second column confirmation exceeds
R RPD outside accepted recovery limits RL Reporting Detection Limit
Revision vl
Page 17 of 35

SUMMIT Summit Environmental Technologies, Inc.
3310 Win St.
ENVIRONMENTAL TECHNOLOGIES, INC Cuyahoga Falls, Ohio 44223
Analytical Laboratories TEL: [phone] FAX: [phone]
Website: http://www.settek.coni
Client: Synagro
Project: Farmville WWTP - REVISED REPORT
QC SUMMARY REPORT
WO#: 23090278
14 Sep-23
BatchID: 68547
Sample ID: 23090275-001DMS
SampType: MS
TestCode: HG_NPW(747 Units: mg/L
Prep Date: 9/11/2023
RunNo: 170584
Client ID: Batch=
Batch ID: 68547
TestNo: SW7470A SW7470A
Analysis Date: 9/11/2023
SegNo: 4587740
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
TCLP Mercury 0.00395 0.000200 0.00400 0 98.8 75 125
Sample ID: 23090275-001DMSD
SampType: MSD
TestCode: HG_NPW(747 Units: mg/L
Prep Date: 9/11/2023
RunNo: 170584
Client ID: Batch=
Batch ID: 68547
TestNo: SW7470A SW7470A
Analysis Date: 9/11/2023
SegNo: 4587741
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
TCLP Mercury 0.00401 0.000200 0.00400 0 100 75 125 0.00395 1.51 20
Qualifiers: B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
PL Permit Limit
E Value above quantitation range H Holding times for preparation or anal,
M Manual Integration used to determine area response MC Value is below Minimum Compound
Revision vl
OGl P Second column confirmation exceeds
R RPD outside accepted recovery limits RL Reporting Detection Limit
Page 18 of 35

SUMMIT Summit Environmental Technologies, Inc.
3310 Win St.
ENVIRONMENTAL TECHNOLOGIES, INC Cuyahoga Falls, Ohio 44223
Analytical Laboratories TEL: [phone] FAX: [phone]
Website: http://www.settek.coni
Client: Synagro
Project: Farmville WWTP - REVISED REPORT
QC SUMMARY REPORT
WO#: 23090278
14 Sep-23
BatchID: 68553
Sample ID: MB-68553
SampType: MBLK
TestCode: SVOC-BNA_T Units: mg/L
Prep Date: 9/11/2023
RunNo: 170654
Client ID: PBS
Batch ID: 68553
TestNo: SW8270 SW3510C
Analysis Date: 9/11/2023
SegNo: 4589156
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
1,4-Dichlorobenzene
ND
0.0250
2,4,5-Trichlorophenol
ND
0.0250
2,4,6-Trichlorophenol
ND
0.0250
2,4-Dinitrotoluene
ND
0.0250
Cresols, Total
ND
0.0500
Hexachloro-1,3-butadiene
ND
0.0250
Hexachlorobenzene
ND
0.0250
Hexachloroethane
ND
0.0250
Nitrobenzene
ND
0.0250
Pentachlorophenol
ND
0.0250
Pyridine
ND
0.0250
Sum 2-Fluorophenol
3.25
Surr: Phenol-d6
3.37
Surr: Nitrobenzene-d5
2.70
Surr: 2,4,6-Tribromophenol
4.24
Surr: 2-Fluorobiphenyl
2.83
Surr: p-Terphenyl-d14
3.55
5.000
64.9
10
135
5.000
67.4
10
161
5.000
54.1
16.8
150
5.000
84.8
32.5
179
5.000
56.7
34
133
5.000
71.1
60.8
163
Sample ID: LCS-68553
SampType: LCS
TestCode: SVOC-BNA_T Units: mg/L
Prep Date: 9/11/2023
RunNo: 170654
Client ID: LCSS
Batch ID: 68553
TestNo: SW8270 SW3510C
Analysis Date: 9/11/2023
SegNo: 4589157
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal,
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
Revision V 1
ND Not Detected OGl P Second column confirmation exceeds
PL Permit Limit R RPD outside accepted recovery limits RL Reporting Detection Limit
Page 19 of 35

SUMMIT Summit Environmental Technologies, Inc.
3310 Win St.
ENVIRONMENTAL TECHNOLOGIES, INC Cuyahoga Falls, Ohio 44223
Analytical Laboratories TEL: [phone] FAX: [phone]
Website: http://www.settek.coni
Client: Synagro
Project: Farmville WWTP - REVISED REPORT
QC SUMMARY REPORT
WO#: 23090278
14 Sep-23
BatchID: 68553
Sample ID: LCS-68553
SampType: LCS
TestCode: SVOC-BNA_T Units: mg/L
Prep Date: 9/11/2023
RunNo: 170654
Client ID: LCSS
Batch ID: 68553
TestNo: SW8270 SW3510C
Analysis Date: 9/11/2023
SegNo: 4589157
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
1,4-Dichlorobenzene
2.34
0.0250
4.000
0
58.6
35
130
2,4,5-Trichlorophenol
3.59
0.0250
4.000
0
89.7
44
144
2,4,6-Trichlorophenol
3.51
0.0250
4.000
0
87.9
45
141
2,4-Dinitrotoluene
3.35
0.0250
4.000
0
83.6
56
136
Cresols, Total
5.65
0.0500
8.000
0
70.6
36
135
Hexachloro-1,3-butadiene
2.57
0.0250
4.000
0
64.2
30
130
Hexachlorobenzene
3.53
0.0250
4.000
0
88.1
58
130
Hexachloroethane
2.11
0.0250
4.000
0
52.7
28
130
Nitrobenzene
2.62
0.0250
4.000
0
65.4
39
133
Pentachlorophenol
3.56
0.0250
4.000
0
88.9
33
151
Pyridine
1.27
0.0250
4.000
0
31.7
10
130
Surr: 2-Fluorophenol
3.37
5.000
67.4
10
135
Surr: Phenol-d6
3.47
5.000
69.4
10
161
Surr: Nitrobenzene-d5
2.75
5.000
54.9
16.8
150
Surr:2,4,6-Tribromophenol
4.42
5.000
88.4
32.5
179
Surr: 2-Fluorobiphenyl
3.21
5.000
64.1
34
133
Surr: p-Terphenyl-d14
3.52
5.000
70.3
60.8
163
Sample ID: 23090137-001AMS
SampType: MS
TestCode: SVOC-BNA_T Units: mg/L
Prep Date: 9/11/2023
RunNo: 170654
Client ID: BatchQC
Batch ID: 68553
TestNo: SW8270 SW3510C
Analysis Date: 9/11/2023
SegNo: 4589158
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal,
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
Revision V 1
ND Not Detected OGl P Second column confirmation exceeds
PL Permit Limit R RPD outside accepted recovery limits RL Reporting Detection Limit
Page 20 of 35

SUMMIT Summit Environmental Technologies, Inc.
3310 Win St.
ENVIRONMENTAL TECHNOLOGIES, INC Cuyahoga Falls, Ohio 44223
Analytical Laboratories TEL: [phone] FAX: [phone]
Website: http://www.settek.coni
Client: Synagro
Project: Farmville WWTP - REVISED REPORT
QC SUMMARY REPORT
WO#: 23090278
14 Sep-23
BatchID: 68553
Sample ID: 23090137-001AMS
SampType: MS
TestCode: SVOC-BNA_T Units: mg/L
Prep Date: 9/11/2023
RunNo: 170654
Client ID: Batch=
Batch ID: 68553
TestNo: SW8270 SW3510C
Analysis Date: 9/11/2023
SegNo: 4589158
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
1,4-Dichlorobenzene
2.42
0.0250
4.000
0
60.4
38.3
130
2,4,5-Trichlorophenol
3.71
0.0250
4.000
0
92.8
43.9
157
2,4,6-Trichlorophenol
3.61
0.0250
4.000
0
90.4
37.5
159
2,4-Dinitrotoluene
3.47
0.0250
4.000
0
86.7
52.1
151
Cresols, Total
5.88
0.0500
8.000
0
73.5
10
184
Hexachloro-1,3-butadiene
2.67
0.0250
4.000
0
66.7
36.2
130
Hexachlorobenzene
3.68
0.0250
4.000
0
92.1
57.1
139
Hexachloroethane
2.23
0.0250
4.000
0
55.8
30.4
130
Nitrobenzene
2.74
0.0250
4.000
0
68.4
34
140
Pentachlorophenol
3.74
0.0250
4.000
0
93.5
24.1
171
Pyridine
1.78
0.0250
4.000
0
44.6
10
130
Surr: 2-Fluorophenol
3.64
5.000
72.8
10
135
Surr: Phenol-d6
3.77
5.000
75.4
10
161
Surr: Nitrobenzene-d5
2.98
5.000
59.7
16.8
150
Surr:2,4,6-Tribromophenol
4.67
5.000
93.4
32.5
179
Surr: 2-Fluorobiphenyl
3.50
5.000
70.1
34
133
Surr: p-Terphenyl-d14
3.72
5.000
74.5
60.8
163
QMR
Sample ID: 23090137-001AMSD
SampType: MSD
TestCode: SVOC-BNA_T Units: mg/L
Prep Date: 9/11/2023
RunNo: 170654
Client ID: BatchQC
Batch ID: 68553
TestNo: SW8270 SW3510C
Analysis Date: 9/11/2023
SegNo: 4589159
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal,
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
Revision V 1
ND Not Detected OGl P Second column confirmation exceeds
PL Permit Limit R RPD outside accepted recovery limits RL Reporting Detection Limit
Page 21 of 35

SUMMIT Summit Environmental Technologies, Inc.
3310 Win St.
ENVIRONMENTAL TECHNOLOGIES, INC Cuyahoga Falls, Ohio 44223
Analytical Laboratories TEL: [phone] FAX: [phone]
Website: http://www.settek.coni
Client: Synagro
Project: Farmville WWTP - REVISED REPORT
QC SUMMARY REPORT
BatchID: 68553
WO#: 23090278
14 Sep-23
Sample ID: 23090137-001AMSD
SampType: MSD
TestCode: SVOC-BNA_T Units: mg/L
Prep Date: 9/11/2023
RunNo: 170654
3lient ID: Batch=
Batch ID: 68553
TestNo: SW8270 SW3510C
Analysis Date: 9/11/2023
SegNo: 4589159
analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
1,4-Dichlorobenzene
1.88
0.0250
4.000
0
47.1
38.3
130
2.416
24.8
30
2,4,5-Trichlorophenol
3.11
0.0250
4.000
0
77.7
43.9
157
3.712
17.7
30
2,4,6-Trichlorophenol
3.08
0.0250
4.000
0
77.1
37.5
159
3.614
15.9
30
2,4-Dinitrotoluene
2.90
0.0250
4.000
0
72.6
52.1
151
3.469
17.7
30
Cresols, Total
4.92
0.0500
8.000
0
61.5
10
184
5.878
17.7
30
Hexachloro-1,3-butadiene
2.02
0.0250
4.000
0
50.5
36.2
130
2.668
27.6
30
Hexachlorobenzene
3.11
0.0250
4.000
0
77.8
57.1
139
3.684
16.8
30
Hexachloroethane
1.71
0.0250
4.000
0
42.7
30.4
130
2.234
26.6
30
Nitrobenzene
2.23
0.0250
4.000
0
55.8
34
140
2.735
20.3
30
Pentachlorophenol
3.09
0.0250
4.000
0
77.2
24.1
171
3.738
19.0
30
Pyridine
1.25
0.0250
4.000
0
31.1
10
130
1.784
35.6
30
Surr: 2-Fluorophenol
3.04
5.000
60.8
10
135
0
Surr: Phenol-d6
3.20
5.000
64.0
10
161
0
Surr: Nitrobenzene-d5
2.48
5.000
49.6
16.8
150
0
Surr:2,4,6-Tribromophenol
4.17
5.000
83.4
32.5
179
0
Surr:2-Fluorobiphenyl
3.00
5.000
59.9
34
133
0
Surr: p-Terphenyl-d14
3.33
5.000
66.6
60.8
163
0
R
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal,
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
Revision V 1
ND Not Detected OGl P Second column confirmation exceeds
PL Permit Limit R RPD outside accepted recovery limits RL Reporting Detection Limit
Page 22 of 35

SUMMIT Summit Environmental Technologies, Inc.
3310 Win St.
ENVIRONMENTAL TECHNOLOGIES, INC Cuyahoga Falls, Ohio 44223
Analytical Laboratories TEL: [phone] FAX: [phone]
Website: http://www.settek.coni
Client: Synagro
Project: Farmville WWTP - REVISED REPORT
QC SUMMARY REPORT
WO#: 23090278
14 Sep-23
BatchID: 68568
Sample ID: MB-68568
SampType: MBLK
TestCode: TCLP-SVOC- Units: mg/L
Prep Date: 9/11/2023
RunNo: 170728
Client ID: PBS
Batch ID: 68568
TestNo: SW8081 SW3510C
Analysis Date: 9/12/2023
SegNo: 4591119
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Chlordane, total
ND
0.00250
Toxaphene
ND
0.00500
Endrin
ND
0.000500
gamma-BHC
ND
0.000500
Heptachlor
ND
0.00400
Heptachlor epoxide
ND
0.000500
Methoxychlor
ND
0.000500
Sum TCMX
72.7
Sum DCB
89.3
100.0 72.7 10 119
100.0 89.3 10 119
QC+
QC+
QC+
QC+
QC+
Sample ID: LCS-68568
SampType: LCS
TestCode: TCLP-SVOC- Units: mg/L
Prep Date: 9/11/2023
RunNo: 170728
Client ID: LCSS
Batch ID: 68568
TestNo: SW8081 SW3510C
Analysis Date: 9/12/2023
SegNo: 4591120
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Chlordane, tota
Toxaphene
Endrin
gamma-BHC
Heptachlor
Heptachlor epo
Methoxychlor
Surr: TCMX
Qualifiers:
1 0.0775
0.0
ND
0.0
0.0410
0.00
0.0376
0.00
0.0401
0.0
xide 0.0397
0.00
0.0395
0.00
65.3
B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
PL Permit Limit
0250
0
0
70
0500
0
0
70
0500
0.0500 0
82.0
10
0500
0.0500 0
75.2
10
0400
0.0500 0
80.1
10
0500
0.0500 0
79.4
10
0500
0.0500 0
79.0
10
100.0
65.3
10
E Value above quantitation range
M Manual Integration used to determine area response
OGl
R RPD outside accepted recovery
limits
130
130
130
130
130
130
178
130
H Holding times for preparation or anal,
MC Value is below Minimum Compound
P Second column confirmation exceeds
RL Reporting Detection Limit
QC+
QC+
QC+
QC+
QC+
Revision vl
Page 23 of 35

SUMMIT Summit Environmental Technologies, Inc.
3310 Win St.
ENVIRONMENTAL TECHNOLOGIES, INC Cuyahoga Falls, Ohio 44223
Analytical Laboratories TEL: [phone] FAX.- [phone]
Website: hgp:llwww.settek.com
QC SUMMARY REPORT
Wo#: 23090278
14-Sep-23
Client: Synagro
Project: Farmvillc WWTP - REVISED REPORT BatchID: 68568
Sample ID: LCS-68568
SampType: LCS
TestCode: TCLP-SVOC- Units: mg/L
Prep Date: 9/11/2023
RunNo: 170728
Client ID: LCSS
Batch ID: 68568
TestNo: SW8081 SW3510C
Analysis Date: 9/12/2023
SegNo: 4591120
Analyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
Sum DCB
72.1
11 1
72.1 10 130
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal,
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
Revision vl
ND Not Detected OGI P Second column confirmation exceeds
PL Permit Limit R RPD outside accepted recovery limits RL Reporting Detection Limit
Page 24 of 35

SUMMIT Summit Environmental Technologies, Inc
3310 Win St
ENVIRONMENTAL TECHNOLOGIES, INC Cuyahoga Falls, Ohio 44223
Analytical Laboratories TEL: [phone] FAX: [phone]
Website: http://www.settek.coni
Client: Synagro
Project: Farmville WWTP - REVISED REPORT
QC SUMMARY REPORT
WO#: 23090278
14 Sep-23
BatchID: R170475
pH 6.9 0 0 0 0 7.0 0.9 10
pH 7.0 7.0 0 100 90 110
pH 7.0 7.0 0 100 90 110
Sample ID: IDOC GN
SampType: LCS
TestCode: pH_S(9045D) Units: s.u.@21C
Prep Date:
RunNo: 170475
Client ID: LCSS
Batch ID: R170475
TestNo: SW9045D
Analysis Date: 9/7/2023
SegNo: 4583921
Analyte
Result
PQL SPK value SPK Ref Val %REC
Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
pH 7.0
Qualifiers: B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
PL Permit Limit
7.0 0 100 90 110
E Value above quantitation range H Holding times for preparation or anal,
M Manual Integration used to determine area response MC Value is below Minimum Compound
Revision vl
OGl P Second column confirmation exceeds
R RPD outside accepted recovery limits RL Reporting Detection Limit
Page 25 of 35

SUMMIT Summit Environmental Technologies, Inc.
3310 Win St.
ENVIRONMENTAL TECHNOLOGIES, INC Cuyahoga Falls, Ohio 44223
Analytical Laboratories TEL: [phone] FAX.- [phone]
Website: hgp:llwww.settek.com
QC SUMMARY REPORT
Wo#: 23090278
14-Sep-23
Client: Synagro
Project: Farmvillc WWTP - REVISED REPORT BatchID: R170475
Sample ID: IDOC GN
SampType: LCS
TestCode: pH_S(9045D) Units: s.u.@21C
Prep Date:
RunNo: 170475
Client ID: LCSS
Batch ID: R170475
TestNo: SW9045D
Analysis Date: 9/7/2023
SegNo: 4583921
Analyte
Result
PQL SPK value SPK Ref Val %REC
LowLimit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal,
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
Revision vl
ND Not Detected OGl P Second column confirmation exceeds
PL Permit Limit R RPD outside accepted recovery limits RL Reporting Detection Limit
Page 26 of 35

SUMMIT Summit Environmental Technologies, Inc.
3310 Win St.
ENVIRONMENTAL TECHNOLOGIES, INC Cuyahoga Falls, Ohio 44223
Analytical Laboratories TEL: [phone] FAX: [phone]
Website: http://www.settek.coni
Client: Synagro
Project: Farmville WWTP - REVISED REPORT
QC SUMMARY REPORT
WO#: 23090278
14 Sep-23
BatchID: R170475
Sample ID: LCS-R170475
SampType: LCS
TestCode: pH_NPW(450 Units: s.u.@21C
Prep Date:
RunNo: 170475
Client ID: LCSW
Batch ID: R170475
TestNo: SW9045D
Analysis Date: 9/7/2023
SegNo: 4583909
Analyte
Result
PQL SPK value SPK Ref Val %REC
Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
pH 7.0 7.0 0 100 98.6 101.4
Sample ID: LCS-R170475
SampType: LCS
TestCode: pH_NPW(450 Units: s.u.@21.00
Prep Date:
RunNo: 170475
Client ID: LCSW
Batch ID: R170475
TestNo: SW9045D
Analysis Date: 9/7/2023
SegNo: 4583926
Analyte
Result
PQL SPK value SPK Ref Val %REC
Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
pH 7.0 7.0 0 100 98.6 101.4
Qualifiers: B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
PL Permit Limit
E Value above quantitation range H Holding times for preparation or anal,
M Manual Integration used to determine area response MC Value is below Minimum Compound
Revision vl
OGl P Second column confirmation exceeds
R RPD outside accepted recovery limits RL Reporting Detection Limit
Page 27 of 35

SUMMIT Summit Environmental Technologies, Inc.
3310 Win St.
ENVIRONMENTAL TECHNOLOGIES, INC Cuyahoga Falls, Ohio 44223
Analytical Laboratories TEL: [phone] FAX: [phone]
Website: http://www.settek.coni
QC SUMMARY REPORT
WO#: 23090278
14 Sep-23
Client: Synagro
Project: Farmville WWTP - REVISED REPORT BatchlD: R170532
Cyanide, Reactive ND 0.500
Cyanide, Reactive 2.76 0.500 10.00 0 27.6 22 110
Cyanide, Reactive ND 0.500 0.5000 0 16.0 14 156
Sample ID: 23090137-001AMS
SampType: MS
TestCode: Cyanide,Rea Units: mg/Kg
Prep Date:
RunNo: 170532
Client ID: BatchQC
Batch ID: R170532
TestNo: SW9014
Analysis Date: 9/8/2023
SegNo: 4585689
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
Cyanide, Reactive
1.77 0.481
10.00 0 17.7 75
125
S
Qualifiers: B
Analyte detected in the associated Method Blank
E Value above quantitation range
H
Holding times for preparation or anal,
J
Analyte detected below quantitation limits
M Manual Integration used to determine area response
MC
Value is below Minimum Compound
Revision V 1
ND
Not Detected
OGl
P
Second column confirmation exceeds
PL
Permit Limit
R RPD outside accepted recovery limits
RL
Reporting Detection Limit
Page 28 of 35

SUMMIT Summit Environmental Technologies, Inc.
3310 Win St.
ENVIRONMENTAL TECHNOLOGIES, INC Cuyahoga Falls, Ohio 44223
Analytical Laboratories TEL: [phone] FAX: [phone]
Website: http://www.settek.coni
Client: Synagro
Project: Farmville WWTP - REVISED REPORT
QC SUMMARY REPORT
WO#: 23090278
14 Sep-23
BatchID: R170532
Sample ID: 23090137-001AMS
SampType: MS
TestCode: Cyanide,Rea Units: mg/Kg
Prep Date:
RunNo: 170532
Client ID: Batch=
Batch ID: R170532
TestNo: SW9014
Analysis Date: 9/8/2023
SegNo: 4585689
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Sample ID: 23090137-001AMSD
SampType: MSD
TestCode: Cyanide,Rea Units: mg/Kg
Prep Date:
RunNo: 170532
Client ID: Batch=
Batch ID: R170532
TestNo: SW9014
Analysis Date: 9/8/2023
SegNo: 4585690
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Cyanide, Reactive 1.64 0.476 10.00 0 16.4 75 125 1.772 7.55 10 S
Qualifiers: B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
PL Permit Limit
E Value above quantitation range H Holding times for preparation or anal,
M Manual Integration used to determine area response MC Value is below Minimum Compound
Revision vl
OGl P Second column confirmation exceeds
R RPD outside accepted recovery limits RL Reporting Detection Limit
Page 29 of 35

SUMMIT Summit Environmental Technologies, Inc.
3310 Win St.
ENVIRONMENTAL TECHNOLOGIES, INC Cuyahoga Falls, Ohio 44223
Analytical Laboratories TEL: [phone] FAX: [phone]
Website: http://www.settek.coni
Client: Synagro
Project: Farmville WWTP - REVISED REPORT
QC SUMMARY REPORT
WO#: 23090278
14 Sep-23
BatchID: R170648
Sample ID: MB-R170648
SampType: MBLK
TestCode: Sulfide,React Units: mg/Kg
Prep Date:
RunNo: 170648
Client ID: PBS
Batch ID: R170648
TestNo: SW9034
Analysis Date: 9/8/2023
SegNo: 4589032
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Sulfide, Reactive ND 25.0
Sample ID: LCS-111170648
SampType: LCS
TestCode: Sulfide,React Units: mg/Kg
Prep Date:
RunNo: 170648
Client ID: LCSS
Batch ID: R170648
TestNo: SW9034
Analysis Date: 9/8/2023
SegNo: 4589033
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Sulfide, Reactive
970 25.0 2100 0 46.2 14 110
Qualifiers: B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
PL Permit Limit
E Value above quantitation range H Holding times for preparation or anal,
M Manual Integration used to determine area response MC Value is below Minimum Compound
Revision vl
OGl P Second column confirmation exceeds
R RPD outside accepted recovery limits RL Reporting Detection Limit
Page 30 of 35

SUMMIT Summit Environmental Technologies, Inc.
3310 Win St.
ENVIRONMENTAL TECHNOLOGIES, INC Cuyahoga Falls, Ohio 44223
Analytical Laboratories TEL: [phone] FAX: [phone]
Website: http://www.settek.coni
Client: Synagro
Project: Farmville WWTP - REVISED REPORT
QC SUMMARY REPORT
WO#: 23090278
14 Sep-23
BatchID: R170684
Sample ID: RLC
SampType: RLC
TestCode: TCLP-SVOC- Units: mg/L
Prep Date:
RunNo: 170684
Client ID: Batch=
Batch ID: R170684
TestNo: SW8321
Analysis Date: 9/11/2023
SegNo: 4590015
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
2,4-D
0.0114
0.0100 0.01000
0 114
50
150
2,4,5-TP
ND
0.0100 0.01000
0 66.0
50
150
Sum 2,4-Dichlorophenylacetic acid
0.00220
0.01000
22.0
70
130 S
Sample ID: MBLK
SampType: MBLK
TestCode: TCLP-SVOC- Units: mg/L
Prep Date:
RunNo: 170684
Client ID: PBS
Batch ID: R170684
TestNo: SW8321
Analysis Date: 9/11/2023
SegNo: 4590016
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
2,4-D ND 0.0100
2,4,5-TP ND 0.0100
Surr: 2,4-Dichlorophenylacetic acid 0.936 1.000 93.6 70 130
Sample ID: LCS
SampType: LCS
TestCode: TCLP-SVOC- Units: mg/L
Prep Date:
RunNo: 170684
Client ID: LCSS
Batch ID: R170684
TestNo: SW8321
Analysis Date: 9/11/2023
SegNo: 4590017
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
2,4-D 0.246 0.0100 0.3000 0 82.2 60.5 141
2,4,5-TP 0.257 0.0100 0.3000 0 85.5 68.3 144
Surr: 2,4-Dichlorophenylacetic acid 0.243 0.3000 81.0 70 130
Qualifiers: B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
PL Permit Limit
E Value above quantitation range H Holding times for preparation or anal,
M Manual Integration used to determine area response MC Value is below Minimum Compound
Revision vl
OGl P Second column confirmation exceeds
R RPD outside accepted recovery limits RL Reporting Detection Limit
Page 31 of 35

SUMMIT Summit Environmental Technologies, Inc.
3310 Win St.
ENVIRONMENTAL TECHNOLOGIES, INC Cuyahoga Falls, Ohio 44223
Analytical Laboratories TEL: [phone] FAX.- [phone]
Website: hgp:llwww.settek.com
QC SUMMARY REPORT
Wo#: 23090278
14-Sep-23
Client: Synagro
Project: Farmvillc WWTP - REVISED REPORT BatchID: R170684
Sample ID: LCSD
SampType: LCSD
TestCode: TCLP-SVOC- Units: mg/L
Prep Date:
RunNo: 170684
Client ID: LCSS02
Batch ID: R170684
TestNo: SW8321
Analysis Date: 9/11/2023
SegNo: 4590018
Analyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
2,4-D 0.266 0.0100 0.3000 0 88.6 60.5 141 0.2465 7.57 30
2,4,5-TP 0.235 0.0100 0.3000 0 78.4 68.3 144 0.2566 8.75 30
Surr: 2,4-Dichlorophenylacetic acid 0.230 0.3000 76.6 70 130 0 0
Qualifiers: B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
PL Permit Limit
E Value above quantitation range H Holding times for preparation or anal,
M Manual Integration used to determine area response MC Value is below Minimum Compound
OGI P Second column confirmation exceeds
R RPD outside accepted recovery limits RL Reporting Detection Limit
Revision vl
Page 32 of 35

SUMMIT Summit Environmental Technologies, Inc.
3310 Win St.
ENVIRONMENTAL TECHNOLOGIES, INC Cuyahoga Falls, Ohio 44223
Analytical Laboratories TEL: [phone] FAX.- [phone]
Website: hgp:llwww.settek.com
Client: Synagro
Project: Farnaville WWTP - REVISED REPORT
QC SUMMARY REPORT
Wo#: 23090278
14-Sep-23
BatchlD: R170784
Sample ID: LCS-R170784
SampType: LCS
TestCode: Ignitability_S Units: mm/sec
Prep Date:
RunNo: 170784
Client ID: LCSS
Batch ID: R170784
TestNo: SW1030
Analysis Date: 9/13/2023
SegNo: 4592680
Analyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
Ignitability
8.33
7.240 0 115 70 130
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal,
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
Revision vl
ND Not Detected OGl P Second column confirmation exceeds
PL Permit Limit R RPD outside accepted recovery limits RL Reporting Detection Limit
Page 33 of 35

r
oc
M
r-a
Page 34 of 35

�� � � Summit Environmental Technologies, Inc.
3310 Win St.
ENVIRONMENTAL TECHNOLOGIES, INC Cuyahoga Falls, Ohio44223 Sample Log -in Check List
Analytical Laboratories TEL: [phone] FAX [phone]
Website: http://www.settek.coni
Client Name:
SYN-NC-27028
Work Order Number: 23090278
RcptNo: 1
Logged by:
Christina N. Gemma
9/6/2023 10:00:00 AM
11�
V'
Completed By:
Christina N. Gemma
9/6/2023 6:08:08 PM
11�
Reviewed By:
Jennifer Woolf
9/6/2023 6:10:41 PM
V'
Chain of Custody
1. Is Chain of Custody complete?
Yes
❑
No
d❑
Not Present ❑
2. How was the sample delivered?
UPS
Loa In
3, Coolers are present?
Yes
C
No
F
NA F
4. Shipping container/cooler in good condition?
Yes
0
No
Custody seals intact on shipping container/cooler?
Yes
❑
No
❑
Not Present
No. Seal Date:
Signed By:
5. Was an attempt made to cool the samples?
Yes
❑
No
F—
NA
6. Were all samples received at a temperature of >0° C to 6.0°C
Yes
d❑
No
❑
NA
7, Sample(s) in proper container(s)?
Yes
J❑
No
❑
g. Sufficient sample volume for indicated test(s)?
Yes
d❑
No
❑
9, Are samples (except VOA and ONG) properly preserved?
Yes
J❑
No
❑
10. Was preservative added to bottles?
Yes
❑
No
d❑
NA ❑
11. Is the headspace in the VOA vials less than 1/4 inch or 6 mm?
Yes
No
❑
No VOA Vials ❑�
12. Were any sample containers received broken?
Yes
No
d❑
13. Does paperwork match bottle labels?
Yes
No
❑
(Note discrepancies on chain of custody)
14. Are matrices correctly identified on Chain of Custody?
Yes
No
❑
15. Is it clear what analyses were requested?
Yes
No
❑
16. Were all holding times able to be met?
Yes
No
❑
(If no, notify customer for authorization.)
Special Handling (if applicable)
17. Was client notified of all discrepancies with this order?
Yes
No
❑
NA ❑d
Person Notified: Date:
By Whom: Via:
❑ eMail
❑ Phone ❑
Fax
❑ In Person
Regarding:
Client Instructions:
18. Additional remarks:
state noted in comments
project address not included
Cooler Information
Cooler No
Temp °C
Condition I Seal Intact
Seal No
Seal Date
Signed
By
I1
I5.9
Good Not Present
Page 35 of 35

SECTION 5

Facility Name:
WR'TP Name:
ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Town of Farmville
Town ofFarmville WWTP
WQ Permit Number: WQ0008778
NPDES Number: NCO029572
Monitoring Period: From 01/01/2023 To 12/31/2023
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. 1/A (time/temp) Alt. 2B (Alk Treatment) Alt. 3/C (Prior Testing)
Alt. 4/D (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic
Beta Ray Gamma Ray Pasteurization
Class B:
Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying Composting Aerobic Digestion
Anaerobic Digestion
Tf —H—hla to U.—..6— —fh—d 1(9..ee A nr Pl— Rl f.11—oa mnnitnr; 1.fa-
Parameter
Allowable Level in Sludge
Pathogen Density
No. of
Frequency
Sample
Analytical
Excee-
of
Type
Technique
Minimum Gen. Mean Maximum Units
dences
Analysis
Fecal
2x10to the 61h
MPN
MPN/g
Coliform
power per gram
of total solids
21300
282000
673000
CFU/g
0
Annually
Grab
SM9222D
CFU
-MF
1000 MPN per gram of
MPN/a
total solids (dreight)
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed:
Option/Alt. 1
Option/Alt. 2
Option/Alt. 3
Option/Alt. 4
(VS reduction)
(40-day bench)
(30-day bench) X
(Spec. 02 uptake)
Option/Alt. 5
Option/Alt. 6
Option/Alt. 7
Option/Alt. 8
(14-Day Aerobic)
(Alk Stabilization)
(Drying — Stable)
(Drying —Unstable)
Option/Alt. 9
Option/Alt. 10
(Injection)
(Incorporation)
No vector attraction reduction alternatives
were performed
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
X_ reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met" (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified
persomiel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have
been met. I am aware that there are significant penalties for false certification including fine and imprisonment."
David Hodgkins, Town Manager
Preparer N and itle e or print)
G A pZ /z 2.4
Signature ofPrepar V ate
Land Applier Name and Title (if applicable) (type or print)
Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26)

Cameron Testing Services, Inc. Laboratory Report
NCDENR#654
NC PHHS #37799
Client:
Synagro CTS Proj.
US EPA #NC01918
2305-0158 DWCert#37799
Project:
Farmville
WWTP Regulatory
Yes
Sample Information
Sampled
MC
Date 05/17/23 Received
ERP Date 05/17/23
Analyses and Results
Lab ID
Sample ID
X Q M
� o L° Analyte Result
N
E T = Std. Methods
�
c o c Reference
a
2305-0158
-01
3ludge Gr Fec. Coliform-S 213000
CFU/g
213000 05/18/23 PD 9222D - MF
-02
673000
CFU/9
224000
-03
475000
CFU/9
475000
-04
192000
CFU/g
192000
-05
<21300
CFU/g
213000
-06
<23800
CFU/g
238000
-07
<21300
CFU/g
213000
Geomean 282000
2305-0158
-01
nudge Gr TS 1.93
%
0.01 05/18/23 PD 2540 G -TS
-02
1.80
%
0.01
-03
1.67
%
0.01
-04
2.07
%
0.01
-05
1.93
%
0.01
-06
1.74
%
0.01
-07
1.85
%
0.01
Report
Review
�
laiz�5
Project Manager
Date�'�/61
219 S. Steele Str.
Sanford NC 27330
919-2084240
[e-mail] camerontesting.com

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Cameron Testing Services, Inc. Laboratory Report
NC DENR #654
NC PHHS #37799
US EPA #NC01918
Client:
Synagro
CTS Proj.
2308-0237
DW Cert # 37799
Project:
Farmville WWTP
Regulatory
Yes
Sample Information
Sampled
AB
Date 08/29/23
Received
AML
Date
08/29/23
Analyses and Results
Lab ID
Sample
x G
ID m o `�° Analyte
Result
Y
i=
d E
T)
�' �'
—'
Std. Methods
c�
o
Reference
a
2308-0237
-01
SiudgE G- Fec. Coliform-S
6060000
CFU/g
135000
08/30/23 PD
9222D - MF
-02
6190000
CFU/g
135000
—03
8080000
CFU/g
135000
-04
5120000
CFU/g
135000
-05
5520000
CFU/g
135000
-06
5660000
CFU/g
135000
-07
7140000
CFU/g
135000
Geomean
6180000
2308-0237
-01
31udge Gr TS (%)
0.308
i
0.01
08/30/23 PD
2540 G -TS
-02
0.292
°i
0.01
-03
0.272
i
o o1
-04
0.267
i
001
-05
0.259
%
0.01
-06
0.289
i
001
-07
0.262
i
0.01
Report ! /�
Review _ _ __ ___�% � / %J� ✓J /70`
Project Manager Date
219 S. Steele Str, 919-208-4240
Sanford NC 27330 [e-mail]

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SECTION 6

Agricultural Lime Application Log
Year2023
Proiect Farmville
Fields Soil Lime Requirements Tons/Acre Date
(state -county -site -field) PH (from soil analysis) AAg limed A Hied
PI-1-5 1 5.61 10.8 T I N/A
PI-1-6 1 5.71 10.7 T I N/A
N/A -Did not apply in 2023

SECTION 7

NCDA&CS Agronomic Division Phone: [phone] Website: www.ncagr.govlagronomi/ Report No. FY23-SL004634
T`YunL7CT:d-t�L
4
} Predictive
Client:
Harold Flanagan
3625 Arch Flanagan Rd
Advisor: Chris Wynne
Syna
g ro LLC
Farmvilie, NC 27828
284 Boger Road
y
S ReportMehiich-3 Extraction
Mocksville, NC 27028
�r..
Links to Helpful Information
Sampled: Received: 09115/2022 completed: 09/23/2022 Farm: PI-01
Client ID:
Sampled County: Pitt
463740
Advisor ID: 509090
Sample ID:
Recommendations: Lime
Nutrients (Ib/acre)
More
Crop (tons/acre) N P205
K20
Mg S Mn Zn
Cu B
Information
Lime History:
1-Bermuda hay/past., M 0.8 180-220 0
100
0 0 0 0
0 0
Note: 12
2 - 0.0
Test Results [units - WIV in g/cm3; CEC and Na in meg1100 cm3; NO3-N in mgldmr :
Soil Class: Mineral
HM% WIV CEC BS% Ac pH P-1 K-I Ca% Mg% S-1
Mn-I
Mn-All Mn-Al2 Zn-I Zn AI
Cu-I Na ESP SS -I NO3-N
0.41 1.08 9.1 78 2.0 5.6 587 56 66 9 34
74
61 1280 1280
357 0.0
Sample ID: 6
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tonslacre) N P205
K20
Mg S Mn Zn
Cu B
Information
Lime History:
1- Bermuda hay/past., M 0.7 180-220 0
110
0 0 0 0
0 0
Note: 12
2 - 0.0
Test Results [units - WN in g1crri3; GEC and Na in meg1100 cm3; NO3-N in m9ldm3j:
Soil Class: Mineral
HM% WIV CEC BS% Ac pH P4 K-I Ca% Mg% S-I
Mn-1
Mn All Mn Al2 Zn-I Zn-AI
Cu-1 Na ESP SS -I NO3-N
1.67 1.00 13.0 83 2.2 5.7 325 53 63 17 44
83
67 1218 1218
434 0.1 1
North Carolina
I.Y� �5 J
R63ceoTrnst Fund Crkwa %ssKm
Reprogramming of the laboratory -information -management system that makes this report possible is being funded
through a grant from the North Carolina Tobacco Trust Fund Commission.
Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
- Steve Troxler. Commissioner ofA.arrculture

NCDA&CS Agronomic Division Phone: [phone] Website: www.ncagr.govlagronomi/
Report No. PY23-SL004634
Harold Flanagan
Page 2 of 2
Understanding the Soil Report: explanation of measurements, abbreviations and units
Recommendations
Report Abbreviations
Lime
Ac
exchangeable acidity
If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either
B
boron
ton/acre or Ib/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting.
BS%
% CEC occupied by basic cations
For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 ib/1000 sq ft) at on
Ca%
% CEC occupied by calcium
time, even if the report recommends more. You can apply the rest in similar increments every six months until the full rate
CEC
cation exchange capacity
is applied. If MG is recommended and lime is needed, use dolomitric lime.
Cu4
copper index
ESP
exchangeable sodium percent
Fertilizer
HM%
percent humic matter
Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of
K-1
potassium index
Ib/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies
K20
potash
for the crop being grown, not on soil test results. K-€ and P-€ values are based on test results and should be > 50. If they
Mg%
% CEC occupied by magnesium
are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is
MIN
mineral soil class
an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS-1 levels appear
Mn
manganese
only on reports for greenhouse soil or problem samples.
Mn-All
Mn-availability index for crop 1Mn-Al2
Mn-availability index for crop 2
Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z
Mn-n- 1
manganese index
a
notations appear on the sot[ report, refer to Mote: Second a Nutrients and Micronutrients In general, homeowners do not
min anese nic soil class
need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit
N
Na
nitrogen
sodium
ncagr.govlagronomi/pubs_htm.
NOs-N
nitrate nitrogen
ORG
organic soil class
Recommendations forsmall areas, such as home lawns/gardens, are listed in units of Ib/1000 sq ft . If you cannot find
pH
current soil pH
the exact fertilizer grade recommended on the report, visit www_ncagr.gov/agronomi/obparf4,htrr»sfnd information that
P-1
phosphorus index
may help you choose a comparable alternate. For more information, read A Homeowner's Guide to Fertilizer.
P205
phosphate
$d
sulfur index
Test Results
Ss-1
soluble salt index
WN
weight per volume
The first seven values [soil class HM%, W/V CEC, BS% Ac and H describe the soil and its d
, p ] degree of acidify. The
Zn-AI
zinc availability index
remaining 16 [P-I, K-€, Ca%, Mg%, Mn-1, Mn-All, Mn Al2, Zn-1, Zn-Al, Cu-1, S-1, SS -I, Na, ESP, SS -I, NO3-N (not routine]
Zn-I
zinc index
available)] indicate levels of plant nutrients or other fertility measurement. Visit WWW.nCagrgav/a=170mi/a rrsf.htm