WQ0003902_2023 Residual Annual Report_20240219 (2)

Initial Review
Reviewer
nathaniel.thorn burg
Is this submittal an application? (Excluding additional information.) *
Yes No
If not an application what is the submittal type?* Annual Report
Residual Annual Report
Additional Information
Other
Annual Report Year* 2023
Permit Number (IR) * WQ0003902
Applicant/Permittee City of Newton
Email Notifications
Does this need review by the hydrogeologist? * Yes No
Regional Office Mooresville
CO Reviewer
Admin Reviewer Wanda Gerald

Submittal Form
Project Contact Information
Please provide information on the person to be contacted by NDB Staff regarding electronic submittal, confirmation of receipt, and other correspondence.
Name* Lysa Finnerty
Email Address*
[e-mail]
Project Information
.........................
Application/Document Type*
New (Fee Required)
Modification - Major (Fee Required)
Renewal with Major Modification (Fee
Required)
Annual Report
Additional Information
Other
Phone Number*
4105376150
Modification - Minor
Renewal
GW-59, NDMR, NDMLR, NDAR-1,
N DAR-2
Residual Annual Report
Change of Ownership
We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form.
https://edoes.deq.nc.gov/Forms/NonDischarge_Monitoring_Report
Permit Type:*
Wastewater Irrigation
High -Rate Infiltration
Other Wastewater
Reclaimed Water
Closed -Loop Recycle
Residuals
Single -Family Residence Wastewater
Other
Irrigation
Permit Number:*
WQ0003902
Has Current Existing permit number
Applicant/Permittee Address*
435 Williams Court, Ste 100, Baltimore, MD 21220
Facility Name*
City of Newton Class B Residuals Program
Please provide comments/notes on your current submittal below.
Submission of the 2023 Annual Report for City of Newton, NC
At this time, paper copies are no longer required. If you have any questions about what is required, please contact Nathaniel Thornburg
at [e-mail].
Please attach all information required or requested for this submittal to be reviewed here.
(Application Form, Engineering Plans, Specifications, Calculations, Etc.)
Newton NC 2023 Annual Report FINAL.pdf 26.06MB
Upload only 1 PDF document (less than 250 MB). Multiple documents must be combined into one PDF file unless file is larger
than upload limit.
* By checking this box, I acknowledge that I understand the application will not be accepted for pre -review until the fee (if required) has
been received by the Non -Discharge Branch. Application fees must be submitted by check or money order and made payable to the
North Carolina Department of Environmental Quality (NCDEQ). I also confirm that the uploaded document is a single PDF with all parts
of the application in correct order (as specified by the application).
Mail payment to:
NCDEQ — Division of Water Resources
Attn: Non -Discharge Branch
1617 Mail Service Center
Raleigh, NC 27699-1617
Signature
Alva �Cit'wt%tt,
Submission Date 2/19/2024

435 Williams Court, Suite 100
Baltimore, MD 21220
www.synagro.com
FEBRUARY 17, 2024
NCDEQ
Division of Water Resources
Information Processing Unit
1617 Mail Service Center
Raleigh, NC 27699-1617
Re: 2023 Annual Report for Permit No. WQ0003902
Dear NCDEQ:
SYNAGRO
Synagro is submitting one electronic copy of the above referenced report on behalf of the City
of Newton, NC.
If you have any questions or need additional information, please do not hesitate to contact
Eric Jones at [phone] or Alex Fox at [phone].
Sincerely,
Derrick Shivar
Environmental Compliance Manager
Enclosures
cc: Eric Jones — City of Newton
Alex Fox, Synagro
YOUR PARTNER FORA CLEANER, GREENERWORLD

CITY OF NEWTON, NC
RESIDUALS LAND APPLICATION PROGRAM
Permit No. WQ0003902
2023 ANNUAL REPORT

City of Newton, NC
Residuals Land Application Program
2023 Annual Report
TABLE OF CONTENTS
1. Certification Form and Annual Operations Summary
2. Annual Residual Sampling Summary Forms and Residuals
Analyses
3. Annual Land Application Field Summary Forms
4. TCLP Analysis
5. Pathogen Reduction/Vector Attraction Reduction
6. Soil pH & Lime Application Records
7. Soil Analyses

SECTION 1

ANNUAL LAND APPLICATION CERTIFICATION FORM
WQ Permit #: W00003902 County Catawba Year 2023
Facility Name (as shown on permit) City of Newton, Clark Creek W WTP NPDES No. NC0036196
Land Application Operator S na ro Phone# [phone]
Land application of residuals as allowed by the above permit occurred during the past calendar year?
X YES NO. If NO, skip Part A, and Part B and proceed to Part C. Also, if residuals were generated but not Iand applied,
please attach an explanation on how the residuals were handled.
Part A — Residuals Application Summary -
Total number of application fields in the permit: 50
Total number of fields utilized for land application during the year: 7
Total amount of dry tons applied during the year for all application sites: 658.66
Total number of acres utilized for land application during the year: 199.70
Part B — Annual Compliance Statement
Facility was compliant during calendar year 22023 with all conditions of the land application permit (including but not limited to items
1-13 below) issued by the Division of Water QualityX YES NO.
If no, please provide a written description why the facility was not compliant, the dates, and explain corrective action taken.
t. Only residuals approved for this permit were applied to the permitted sites.
2. Soil pH was adjusted as specified in the permit and time was applied (if needed) to achieve a soil pH of at least 6,0 or the
limit specified in the permit.
3. Annual soils analysis was performed on each site receiving residuals during the past calendar year and three (3) copies of
laboratory results are attached.
4. Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5. All other monitoring was performed in accordance with the permit and reported during the year as required and three (3)
copies of certified laboratory results are attached.
6. The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .I 105(a) or the Pollutant Loading
Rates in 15A NCAC 02T .l 105(b) (Applicable to 40 CFR Part 503 regulated facilities).
7. All general requirements as specified in the Land Application Permit were complied with (applicable to 40 CFR Part 503
regulated facilities).
8. All monitoring and reporting requirements in 15A NCAC 02T .1 I I I were complied with (applicable to 40 CFR Part 503
regulated facilities).
9. All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Quality.
to. No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
I t . Vegetative cover was maintained and proper crop management was performed on each site receiving residuals, as specified
in the permit_
12. No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13. All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C — Certification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate, and complete. 1
am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for
knowing violations."
James Wentz: Public Works Director
Permi(tee Name and Title (type or print)
Signature of Preparer* Date
(if different from Permittee)
�1
Signature bf Permittee Date
1/31 /2024
Si a an pplier Date
(if different in Permittee and Preparer)
*Preparer is defined in 40 CPR Pail 503.9(r) and 15A NCAC 02T .1102 (26) DENR FORM ACF (12/2006)

OPERATIONS SUMMARY - LAND APPLICATION - NORTH CAROLINA
ALL COUNTIES - ALL SITES
PERMIT # WQ0003902
DATE RANGE: 1/1/2023 - 12/31/2023
NEWTON, NC
NEWTON, NC CLARK CREEK LIME STABILIZED LIQUID
MONTH/YEAR
AMOUNT
UNIT
DRY TONS
UNIT
DRY METRIC TONS
January 2023
264,000.00
G
106.90
D
96.95
February 2023
390,000.00
G
157.91
D
143.23
April2023
624,000.00
G
170.96
D
155.06
September 2023
558,000.00
G
36.07
D
32.71
November 2023
570,000.00
G
186.82
D
169.45
TOTAL
Units Key: D - Dry Tons; G — Gallons; W — Wet Tons; Y — Cubic Yards
Report Date: 1/23/2024 8:58:03 PM
2,406,000.00 G 658.66 D 597.40

SECTION 2

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B
WQ Permit Number: WQ0003902 Laboratory:
Facility Name: NEWTON, NC PACE ANALYTICAL; Waypoint Analytical Virginia
Residual Source WQ # or Inc.
NPDES#: NC0036196
WWTP Name: CLARK CREEK
Residual Analysis Data
Product Type
Sample or Composite Date
LSLIQ
01 /11123
LSLIQ
04/04/23
LSLIQ
07/05/23
LSLIQ
10/03/23
Parameter (mg/kg dry weight)
Ceiling Conc.
Limit
Percent Solids (%)
NA
9.71
6.57
1.55
7.86
Arsenic
75
2.5
3.1
<26
<6.33
Cadmium
85
0.58
1 A
<6.5
<1.27
Copper
4300
190
240
720
142
Chromium
NA
42
36
170
30.4
Lead
840
10
9.5
32
8.23
Mercury
57
<0.19
<0.27
<1.2
<2.15
Molybdenum
75
3.2
5.3
<52
4.66
Nickel
420
13
16
<54
12.1
Selenium
100
4.2
2.3
<42
<6.33
Zinc
7500
790
840
2600
622
Total Phosphorus
NA
15000
8700
35000
10200
TKN
NA
18000
27000
56000
25800
Ammonia -Nitrogen
NA
960
8500
31000
4290
Nitrate and Nitrite
NA
134
97.4
142
<63.3
For surface disposal facilities the ceiling concentration limits listed in this form are not applicable. Reference the individual permit for metals limits.
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified
personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the
possibility of fines and impri onmont for knowing violations."
l U
Signature of Preparer' Date
`Preparer is defined in 40 CF Part 503.9(r) and 15 A NCAC 2T.1102(26) DENR FORM RSSF (12/2006)
Printed: 1/24/2024 5:52:19 PM For: 2025 01

ANNUAL RESIDUAL SAMPLING SUMMARY FORM - B
Report all sampling analysis results for parameters not listed in FORM RSSF that are part of the WQ permit or were analyzed for over the past
calendar year. Use additional forms as needed.
WQ Permit Number W00003902
Laboratory:
Facility Name: NEWTON, NC
PACE ANALYTICAL; Waypoint Analytical Virginia
Residual Source
Inc.
NPDES # or WQ#: NCO036196
WWTP Name: CLARK CREEK
Residual Analysis Data
Product Type
LSLIQ
LSLIQ
LSLIQ
LSLIQ
Sample or Composite Date
01/11/23
04/04/23
07/05/23
10/03/23
Parameters (mg/kg dry weight)
Aluminium
16000
18000
61000
20800
Calcium
18000D
270000
730000
180000
Magnesium
5300
5200
18000
5220
PH (s_u.)
11.70
6.50
7.10
9.70
Potassium
900
1300
3900
862
Sodium
750
1000
4300
856
PAN
5726
9897
23142
8667
SAR (Ratio)
0.1479
0.1335
0.1689
0.1519
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordiance with a system designed to assure that qualified
Personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the
possibility of fines and imprisonment for knowing violations."
Signature Preparer ` �~ Date
`Preparer is defined in 40 CFR Part 503.9(r) and 15 A NCAC 2T.1102(26)
Printed: 1/24/2024 5:56:40 PM For; 2025 01 DENR FORM RSSF-B (12/2006)

aceAnalytical
an-
Report of Analysis
Synagro
12701 Lancaster Hwy
Pineville, NC 28134
Attention: Alex Fox
Project Name: Newton
Lot Number:YA12093
Date Completed:01/30/2023
01/30/2023 3:04 PM
Approved and released by:
Project Manager II: Lucas Odom
4�Q pC14A
"
ANSI National AnnMdWon BWd
ACCREDITED
TESTING LABORATORY
The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced, except in its entirety, without the written approval of Pace Analytical Services, LLC.
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172
Tel:[phone] Fax:[phone] www.pacelabs.com
Page 1 of 7

PACE ANALYTICAL SERVICES, LLC
SC DHEC No: 32010001 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639
Case Narrative
Synagro
Lot Number: YA12093
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary
following this Case Narrative. The sample receiving date is documented in the header information
associated with each sample.
All results listed in this report relate only to the samples that are contained within this report. Where
sampling is conducted by the client, results relate to the accuracy of the information provided, and as the
samples are received.
Sample receipt, sample analysis, and data review have been performed in accordance with the most
current approved The NELAC Institute (TNI) standards, the Pace Analytical Services, LLC ("Pace")
Laboratory Quality Manual, standard operating procedures (SOPS), and Pace policies. Any exceptions to
the TNI standards, the Laboratory Quality Manual, SOPS or policies are qualified on the results page or
discussed below.
Pace is a TNI accredited laboratory; however, the following analyses are currently not listed on our TNI
scope of accreditation: Drinking Water: VOC (excluding BTEX, MTBE, Naphthalene, & 1,2-
dichloroethane) EPA 524.2, E. coli and Total coliforms SM 9223 B-2004, Solid Chemical Material: TOC
Walkley-Black, Biological Tissue: All, Non -Potable Water: SGT-HEM EPA 1664B, Silica EPA 200.7,
Boron, Calcium, Silicon, Strontium EPA 200.8, Bicarbonate, Carbonate, and Hydroxide Alkalinity SM 2320
B-2011, SM 9221 C E-2006 & SM 9222D-2006, Strontium SW-846 6010D, VOC SM 6200 B-2011, Fecal
Coliform Colilert-18.
Where applicable, all soil sample results (including LOQ and DL if requested) are corrected for dry weight
unless flagged with a "W" qualifier.
If you have any questions regarding this report, please contact the Pace Project Manager listed on the
cover page.
The pH analysis associated with the sample(s) in this report was/were performed after the method
recommended 15 minute holding time.
Inorganic Metals
Sample -001 has been analyzed using approximately three grams of sample due to the low percent solid
level. The LOQs have been adjusted accordingly.
Pace Analytical Services, LLC (formerly Shealy Environmetal Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 2 of 7

Client:Synagro Laboratory ID:YA12093-001
Description: NEWTON Matrix: Solid
Date Sampled:01/11/2023 1200 % Solids: 9.71 01/16/2023 1842
Date Received:01/12/2023
Inorganic non-metals
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1
(% Solids) SM 254OG
1 01/16/2023 1842 TAD
65010
1 350.1
(Ammonia - N ) 350.1
5 01/25/2023 1223 DMA
65582
1
(Nitrate - N ) 353.2
1 01/26/2023 1126 CMM
66119
1
(Nitrite - N ) 353.2
1 01/26/2023 1126 CMM
66116
1
(Phosphorus) 365.1
50 01/16/2023 1849 DMA
01/16/2023 0859 64846
1
(Soil pH meas) 9045D
1 01/13/2023 1431 BMG2
64417
1 351.4
(TKN) 351.2
2 01/18/2023 1813 DMA
01/17/2023 1258 64991
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
% Solids
SM 2540G
9.71
%
1
Ammonia - N (gas diffusion)
350.1
960
51
27
mg/kg
1
Nitrate - N (soluble)
353.2
120
2.1
0.28
mg/kg
1
Nitrite - N (soluble)
353.2
14
2.1
0.27
mg/kg
1
Phosphorus
7723-14-0 365.1
15000 S
2600
510
mg/kg
1
Soil pH measured in water @ 18.5 ° C
9045D
11.7
su
1
TKN
351.2
18000
1000
510
mg/kg
1
CVAA
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 7471B
7471B
1 01/14/2023 1358 MRW2
01/14/2023 1025 64810
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Mercury
7439-97-6 7471B
ND
0.80
0.19
mg/kg
1
ICP-AES
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 3050B
601OD
1 01/18/2023 0003 JMH
01/17/2023 0843 64804
2 3050B
601OD
1 01/19/2023 0057 JMH
01/17/2023 0843 64804
3 3050B
601OD
5 01/19/2023 0133 JMH
01/17/2023 0843 64804
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Aluminum
7429-90-5 6010D
16000
68
26
mg/kg
1
Arsenic
7440-38-2 6010D
2.5 J
2.6
0.85
mg/kg
1
Cadmium
7440-43-9 6010D
0.58 J
0.85
0.22
mg/kg
1
Calcium
7440-70-2 6010D 180000
4300
530
mg/kg
3
Chromium
7440-47-3 6010D
42
1.7
0.43
mg/kg
1
Copper
7440-50-8 6010D
190
8.5
3.8
mg/kg
3
Iron
7439-89-6 6010D
13000
17
7.8
mg/kg
1
Lead
7439-92-1 6010D
10
1.7
0.77
mg/kg
1
Magnesium
7439-95-4 6010D
5300
850
110
mg/kg
1
Manganese
7439-96-5 6010D
400
2.6
1.0
mg/kg
1
LOQ = Limit of Quantitation
B = Detected in the method blank
E = Quantitation of compound exceeded the
calibration range DL = Detection Limit
Q = Surrogate failure
ND = Not detected at or above the DL
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 % J
= Estimated result <
LOQ and > DL
L = LCS/LCSD
failure
H = Out of holding time
W = Reported on wet weight basis
S = MS/MSD
failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 3 of 7

Client:Synagro Laboratory ID:YA12093-001
Description: NEWTON Matrix: Solid
Date Sampled:01/11/2023 1200 % Solids: 9.71 01/16/2023 1842
Date Received:01/12/2023
ICP-AES
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date Batch
1 3050B
601OD
1 01/18/2023 0003 JMH
01/17/2023 0843 64804
2 3050B
601OD
1 01/19/2023 0057 JMH
01/17/2023 0843 64804
3 3050B
601OD
5 01/19/2023 0133 JMH
01/17/2023 0843 64804
CAS Analytical
Parameter
Number Method
Result Q LOQ
DL
Units
Run
Molybdenum
7439-98-7 6010D
3.2 J 6.8
1.7
mg/kg
1
Nickel
7440-02-0 6010D
13 6.8
1.8
mg/kg
2
Potassium
7440-09-7 6010D
900 850
110
mg/kg
1
Selenium
7782-49-2 6010D
4.2 3.4
1.4
mg/kg
1
Sodium
7440-23-5 6010D
750 J 850
110
mg/kg
1
Zinc
7440-66-6 6010D
790 8.5
2.1
mg/kg
2
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit Q = Surrogate failure
ND = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 4 of 7

Chain of Custody
and
Miscellaneous Documents
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 5 of 7

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Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 6 of 7

PACE ANALYTICAL SERVICES, LLC
XaTitl•: ENV-FRM-WCOL-0286 02_Samplas Receipt Checklist (SRC)
Effective bate: 8/2/2022
Sample Receipt Checklist (SRC)
clitaw sYNAGRO COLAs • itl ctcd byidete: MNR i 014 23 Lot 4: YA 12003
ears of receipt: ,/ l ace C 1Cnt UPS F Other:
Yes Lvf Nol 11, Were custody icais present on thecoolei?
Yes No ✓ NA 2. ff ctzfod seals we►cptrcnk were they intact and unbroken! /
pH 5fi-p M): NA__ Chlorine Strip ID. N A Tested b�� Zrw
Dnk nal tcmperttltre upon receipt i Derived (Corrected) tenLcrattre Upon mccipt %Solid Snap-C t ID: -'_-' -'o_'
1, 5 �,1.5 oC NA I NA vC '4A 1 NA oC NA / Nei uC
Hetltod: ��Tetiritcrahlttir Blank ❑ Against Buttlrs IR Grin ID. tt _ iR Gtv► Correction ecrian Factor: ° cc
\Method of Coolaltt: n Wet Ice Ice PH&—s ❑ Dry ke 71 Nntle
✓❑Yell ❑Not ❑NA13' were all coolers received at or below 6.0°C.'1 Ifni. was Project bulaegrr uutified?
I PM was Notified by. phone I email ; face-to-face (circle onc).
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No
,/ INA14.
Is die comnrrci.al courier's paeidkg 2k attached to this font?
J.(1ye-sJ
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Yes
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6. vliLiv sam ple EDs listed on for C'OC and all sample
contailx"Y
7. Was collection date & tulle listed on llic (W. and till san1ple en;tlaiucn7
t/
Yes
No
Ycs
-
No
R. Did all container label infomiaticw (ill, date, tittle? wit11 t11C Cam?
Cam?
Yes
No
Mcc
9. Were tests to be pesfornu:d listed otl the COC?
©Yes [:]No 10. Did all samples arrive iu the proper containers for each test andlor in rood condition
(unbroken, lids on, eic.)? _
✓-Yes No 11. Was adequate sample valtlllle available?
No 12. ZVcrc all sanlNl:a received w9thiM'» the bolding d►rtc or 1S ho u; �vllicltrver c�nncs fir,
[2]Yes r�]_No 13. Were all samples c:ntlainers accolulted for? (No missirg.'excess) � 1
Dyes ❑No [Z]NA 14. Were VOA. 8015C and RSK-175 saalples km of bubbles >'pea size" ('/r"or 61um in
diaatctcr) in. any of the VOA vials?
Yes No 1V INA 15. Were all DROtatetaisinutricnt samples received at ii lil i of < 2?
yes No ✓ A 16. Were all cyanide saluples received no a 41 > 13 and sulfide sau lcs rl ceiN'ed at a p71
]Yes [JNo A 7. Were all applicable NH, cy�ttnt a;'pJxmo '6,?s.1 .3 ;< 0,5uipt sa1Ml�les fire of
residual cll brute?
❑Ycs ONo F�NA 19. Was the quNc uwAler listed on the coutainer label? If yes. Quote s`
Sample Preservatiou (Must be completed for allysatuple(s) incnrrectly preserved as with iteadspace.)
anwic(s) NA }vere received iccolrecth,• presented and'`rte Misled accordingly
2 st111�►1e t1 CP1�r1IIa :rzt11 NA ni - of circle our MSO4. HNO3, I I(- A11()H using Sit �! _�' __ '7
ituc Of pt'esenration NA . Iftnore than one presen,-atme Ls act" please uatc In the Comm' ens.; below.
NA
were received Aidi bubbles a6 tstn in dia►nrter,
aawkic�al w= received with TRC > 0,5 iv_w2 (If 9191s no) 411d were
djusted accoidfi*y ut sxagtle receiving vtltlt sodium Odosul&tc (N32S203) wide 03jgtte ID: NA
Catuutletlts:
Qualtrax 1D: 56360 Pecal Analytical Services, LLC Page 1 of I
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 7 of 7

Sodium Absorption Ratio Calculation (SAR)
Product Code Product Name
2025-01-LSLIQ-NC NEWTON, NC CLARK CREEK LIME STABILIZED
LIQUID
Na mg/I = (Na mg/kg x % Solids) = 100 = (750 x 9.7100) = 100 = 72.825
Ca mg/I = (Ca mg/kg x % Solids) = 100 = (180000 x 9.7100) = 100 = 17478
Mg mg/I = (mg mg/kg x % Solids) = 100 = (5300 x 9.7100) = 100 = 514.63
Na meq = Na mg/I + Molec.Wgt.Na = 72.825 = 23 = 3.1663
Ca meq = Ca mg/I + Molec.Wgt.Ca = 17478 = 20 = 873.9
Mg meq = Mg mg/I = Molec.Wgt.Mg = 514.63 = 12 = 42.8858
Sample Date Report Range Ratio
1 /11 /2023 1 /1 /2023 - 3/31 /2023 0.1479
SAR = Na meq + SgrRoot[0.5 x (Ca meq + Mg meq)] = 3.1663 = SgrRoot[0.5(873.9+42.8858)] = 0.147888

aceAnalytical
Report of Analysis
Synagro
12701 Lancaster Hwy
Pineville, NC 28134
Attention: Adam Brigman
Project Name: Newton
Lot Number:YD05128
Date Completed:04/26/2023
Project Manager:Lucas Odom
04/26/2023 4:15 PM
Approved and released by:
Project Coordinator 1: Jenna S. Holliday
4�Q pCAA
M
ANSI NeNonat A"MdMion BWd
qeo
A C C R E D I T E D
�—
TESTING LABORATORY
The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced, except in its entirety, without the written approval of Pace Analytical Services, LLC.
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172
Tel:[phone] Fax:[phone] www.pacelabs.com
Page 1 of 7

PACE ANALYTICAL SERVICES, LLC
SC DHEC No: 32010001 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639
Case Narrative
Synagro
Lot Number: YD05128
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary
following this Case Narrative. The sample receiving date is documented in the header information
associated with each sample.
All results listed in this report relate only to the samples that are contained within this report. Where
sampling is conducted by the client, results relate to the accuracy of the information provided, and as the
samples are received.
Sample receipt, sample analysis, and data review have been performed in accordance with the most
current approved The NELAC Institute (TNI) standards, the Pace Analytical Services, LLC ("Pace")
Laboratory Quality Manual, standard operating procedures (SOPS), and Pace policies. Any exceptions to
the TNI standards, the Laboratory Quality Manual, SOPS or policies are qualified on the results page or
discussed below.
Pace is a TNI accredited laboratory; however, the following analyses are currently not listed on our TNI
scope of accreditation: Drinking Water: VOC (excluding BTEX, MTBE, Naphthalene, & 1,2-
dichloroethane) EPA 524.2, E. coli and Total coliforms SM 9223 B-2004, Solid Chemical Material: TOC
Walkley-Black, Biological Tissue: All, Non -Potable Water: SGT-HEM EPA 1664B, Silica EPA 200.7,
Boron, Calcium, Silicon, Strontium EPA 200.8, Bicarbonate, Carbonate, and Hydroxide Alkalinity SM 2320
B-2011, SM 9221 C E-2006 & SM 9222D-2006, Strontium SW-846 6010D, VOC SM 6200 B-2011, Fecal
Coliform Colilert-18.
Where applicable, all soil sample results (including LOQ and DL if requested) are corrected for dry weight
unless flagged with a "W" qualifier.
If you have any questions regarding this report, please contact the Pace Project Manager listed on the
cover page.
The pH analysis associated with the sample(s) in this report was/were performed after the method
recommended 15 minute holding time.
Metals Analysis
Sample YD05128-001 was classified as biosolids therefore in order to ensure proper digestion, the
samples were weighed out around 3.00-3.50 grams. The LOQ has been adjusted accordingly.
Pace Analytical Services, LLC (formerly Shealy Environmetal Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 2 of 7

Client: Synagro Laboratory ID:YD05128-001
De s cription: Ne wto n Matrix: Solid
Date Sampled:04/04/2023 0900 % Solids: 6.57 04/10/2023 1756
Date Received:04/05/2023
Inorganic
non-metals
Run Prep Method Analytical Method
Dilution
Analysis Date Analyst
Prep Date Batch
1 (% Solids) SM2540G
1
04/10/2023 1756 TAD
72264
1 350.1 (Ammonia - N) 350.1
25
04/14/2023 1620 CMM
72694
1 (Nitrate - N) 353.2
1
04/19/2023 1431 CLL2
73337
1 (Nitrite - N) 353.2
1
04/19/2023 1431 CLL2
73569
1 (Phosphorus) 365.1
25
04/11/2023 1739 DMA
04/07/2023 1132 71968
3 (Soil pH meas) 9045D
1
04/13/2023 2008 CLL
72714
1 351.4 (TKN) 351.2
2
04/10/2023 1314 BMG2
04/07/2023 1040 71967
Parameter
CAS Analytical
Number Method
Result Q
LOQ
DL
Units Run
%Solids
SM2540G
6.57
% 1
Ammonia -N (gas diffusion)
350.1
8500
380
200
mg/kg 1
Nitrate - N(soluble)
353.2
93
3.0
0.41
mg/kg 1
Nitrite - N(soluble)
353.2
4.4
3.0
0.40
mg/kg 1
Phosphorus
7723-14-0 365.1
8700
1900
380
mg/kg 1
Soil pH measured in water @ 19.8 ° C
9045D
6.5
su 3
TKN
351.2
27000
1500
760
mg/kg 1
CVAA
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date Batch
1 7471B
7471B
1 04/18/2023 1815 KAJ
04/13/2023 1410 72168
CAS Analytical
Parameter
Number Method
Result Q LOQ
DL
Units
Run
Mercury
7439-97-6 7471B
ND 1.1
0.27
mg/kg
1
IC P -AE S
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date Batch
1 3050B
6010D
1 04/13/2023 1106 JMH
04/08/2023 1347 71943
2 3050B
6010D
5 04/13/2023 1122 JMH
04/08/2023 1347 71943
3 3050B
6010D
1 04/20/2023 0758 JMH
04/08/2023 1347 71943
5 3050B
6010D
1 04/24/2023 2117 JMH
04/08/2023 1347 71943
CAS Analytical
Parameter
Number Method
Result Q LOQ
DL
Units
Run
Aluminum
7429-90-5 6010D
18000 93
35
mg/kg
I
Arsenic
7440-38-2 6010D
3.1 J 3.5
1.2
mg/kg
I
Cadmium
7440-43-9 6010D
1.1 J 1.2
0.29
mg/kg
I
Calcium
7440-70-2 6010D 270000 5800
720
mg/kg
2
Chromium
7440-47-3 6010D
36 2.3
0.58
mg/kg
I
Copper
7440-50-8 6010D
240 12
5.2
mg/kg
2
Iron
7439-89-6 6010D
13000 23
11
mg/kg
5
Lead
7439-92-1 6010D
9.5 2.3
1.0
mg/kg
1
Magnesium
7439-95-4 6010D
5200 1200
140
mg/kg
3
LOQ = Limit of Quantitation
B = Detected in the method blank
E = Quantitation ofcompound exceeded the calibration range DL = Detection Limit
Q = Surrogate failure
ND = Not detected at or above the DL
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40% J = Estimated result <
LOQ and > DL
L = LCS/LCSD
failure
H = Out ofholding time
W = Reported on wet weight basis
S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 3 of 7

Client: Synagro Laboratory ID:YD05128-001
De s cription: Ne wto n Matrix: Solid
Date Sampled:04/04/2023 0900 % Solids: 6.57 04/10/2023 1756
Date Received:04/05/2023
IC P -AE S
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date Batch
1 3050B
6010D
1 04/13/2023 1106 JMH
04/08/2023 1347 71943
2 3050B
6010D
5 04/13/2023 1122 JMH
04/08/2023 1347 71943
3 3050B
6010D
1 04/20/2023 0758 JMH
04/08/2023 1347 71943
5 3050B
6010D
1 04/24/2023 2117 JMH
04/08/2023 1347 71943
CAS Analytical
Parameter
Number Method
Result Q LOQ
DL
Units
Run
Manganese
7439-96-5 6010D
610 3.5
1.4
mg/kg
1
Molybdenum
7439-98-7 6010D
5.3 J 9.3
2.3
mg/kg
1
Nickel
7440-02-0 6010D
16 9.3
2.4
mg/kg
1
Potassium
7440-09-7 6010D
1300 1200
140
mg/kg
5
Selenium
7782-49-2 6010D
2.3 J 4.6
1.9
mg/kg
1
Sodium
7440-23-5 6010D
1000 J 1200
140
mg/kg
3
Zinc
7440-66-6 6010D
840 12
2.9
mg/kg
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation ofcompound exceeded the calibration range DL= Detection Limit Q = Surrogate failure
ND = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40% J = Estimated result < LOQ and > DL L = LCS/LCSD failure
H = Out ofholding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 4 of 7

Chain of Custody
and
Miscellaneous Documents
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 5 of 7

PACE ANALYTICAL SERVICES, LLC
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106 Vantage Point Drive West Columbia, SC 29172 (803) 79 1-9700 Fax [phone] www.pacelabs.com
Page 6 of 7
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PACE ANALYTICAL SERVICES, LLC
DC# Titl9: ENV FRN1-WOOL 0286 vO2_Samples Receipt Checklist {$Kj
Effective Date: Sj2, 202Z
Sample Receipt Checklist (SRC)
Clitut: SYNrAGRO__ Cooler Llspeeicd by?,hate: BRB i 04'O M Lot #: YDD5128
Tvlemis cif recei i I,/1 7gce I F,T-w n UF'S Fe. E1% 0711nl --- --
Iffiesi
cr, ✓ No 1. `i1r�CIC LUSIud seals iesnit t11r die cooler'?
Nu ✓ NA 2. Xf custody seals were present, mere they; intact �wd iwbro1.-en'? _
ilI Strip W: `A Chlorine Strip ID: NA Tested by:-11L
Original tt3r4wrallre upon receipt ! Derived (Corrected) tetv(lerattlre upon receipt %oSo[id S p Ctip ID- 13-244
1.0 / 1.8 eC WA / NA eC NA / NA °C PIA 1 NA Ir �
Method:07eo4xmtirre BlarkF�a uist Aoc'es TR Csnn m: s TR G11:1 C'orrecti.�,t Frictar: o °C.
Method of coolant: wc' lcc lcc packs DIv Fee Norc I
©YCS E]WO LJKA 3. Wcrc all coolers received at or below 6.0°C? lfw, was Pro; l ]lager Imiftc1?
PlVi was Irait'icd by: p[ranc ; entail : faceto-face (circle one).
Yes LjWkl ✓ INA 4. r; the cmirkwn-ial cutuiec's patking, slit attached to this f nn?
✓ Yes No 5. 4V= prolx:r cusrodv procedures (relitigttisWleceived) fbllowe&
Yes l�n 6 Were sawl 'i1v_II3s listed on the COC and all sainple cmitaiuers? �
Yes itio 7_ Was colkctiou catc & time listed oil tte COC and ail sample colt ii=9
,/ Yes QNo 8. Did all container label iufornution (ID, date, tune) spec -Aith ticCOC?
✓ Yes Ttia . Wcrc tests to be perfarmed listed oil the COC?
©Yes DNo f1iuutiroLm
0. Did, all swuples alive in the proper eoutainas for each Icst.an[4in good cotxlition
lids on. etc.)? ---
✓ Yes No 11. Was adequate ;ample volanle available? I
✓ Y�c Nc 12. Were all isinples received witil uM2 tlx: lwltWlg lime or 48 lrot whichever comes jarse
✓❑ 1'Cs M 13. Wcrc all saruples cmtainers accounted far? (No nrissinglexcesr)
14. Were VOA. 8015t' and 1i,5K-175 samples fret of Nibbles >"'pea�ize" C/;'Or ulluil iII
�y� N° QN_A diaulelrr) ill ally of the V0A vials?
Yes Na ✓ NA 15. Were all DROimetalslnttnient sawp!cs rcccrvt<1 at a pH of < 27 �
1c'c No ,/ - A 16, Were all crnjli& samples received to a pH > i2 and-,idfide samples received at a pH > 9?
OYes [:]No ✓[�NA 17. Afcreall applicable !--HggF.W+'cyst ip xnio 625.U60F.? (f
residua! chlorine?
UYes [Nu EjNq 13. `Mas the quote uwllbcr lis_cd ort the container label? If yes, `11011
S;i tuple Preservation (Vi t be completed for tiny s unpk(s) incolTectly prese ed or with il+-pace.)
sanIPlel5I N xn %vere received incorrectly prevm-Ned anal r;:re adinstert;lernrdingh
at saiuple receiving with r 1't tor. of circle nne H2Q.0-1. HNO3. HC1 NaOH usitlg SR N"
Tiute of pmsalvation NA 3r tit tllall one plesen�ative s ncedecL lsler se txYc i1_ 'llc c 111a ncr I S below.
Sample(s) x4 vvere received wide bubt les>61Wit in diiiint:ler.
Samples(s) MA _ Nvere received with TRC > 0.5 utgtl. f 419 is no) and wtir
ad�ttsled accordir�ly in sauopiC arriving wir'I sotliutn d»osnlfate (Na S,O,J with Unique ID: '`
C'clutnrcut5:
Pace' Analytical Services, LLC
Page 1 of 1
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 7 of 7

Sodium Absorption Ratio Calculation (SAR)
Product Code Product Name
2025-01-LSLIQ-NC NEWTON, NC CLARK CREEK LIME STABILIZED
LIQUID
Na mg/I = (Na mg/kg x % Solids) = 100 = (1000 x 6.5700) = 100 = 65.7
Ca mg/I = (Ca mg/kg x % Solids) = 100 = (270000 x 6.5700) = 100 = 17739
Mg mg/I = (mg mg/kg x % Solids) = 100 = (5200 x 6.5700) = 100 = 341.64
Na meq = Na mg/I + Molec.Wgt.Na = 65.7 = 23 = 2.85652
Ca meq = Ca mg/I + Molec.Wgt.Ca = 17739 = 20 = 886.95
Mg meq = Mg mg/I = Molec.Wgt.Mg = 341.64 = 12 = 28.47
Sample Date Report Range Ratio
4/4/2023 4/1/2023 - 6/30/2023 0.1335
SAR = Na meq + SgrRoot[0.5 x (Ca meq + Mg meq)] = 2.85652 = SgrRoot[0.5(886.95+28.47)] = 0.133519

aceAnalytical
an-
Report of Analysis
Synagro
12701 Lancaster Hwy
Pineville, NC 28134
Attention: Adam Brigman
Project Name: Newton
Lot Number:YG07062
Date Completed:07/25/2023
07/25/2023 7:12 PM
Approved and released by:
Project Manager II: Lucas Odom
4�Q pC14A
"
ANSI National AnnMdWon BWd
ACCREDITED
TESTING LABORATORY
The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced, except in its entirety, without the written approval of Pace Analytical Services, LLC.
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172
Tel:[phone] Fax:[phone] www.pacelabs.com
Page 1 of 7

PACE ANALYTICAL SERVICES, LLC
SC DHEC No: 32010001 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639
Case Narrative
Synagro
Lot Number: YG07062
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary
following this Case Narrative. The sample receiving date is documented in the header information
associated with each sample.
All results listed in this report relate only to the samples that are contained within this report. Where
sampling is conducted by the client, results relate to the accuracy of the information provided, and as the
samples are received.
Sample receipt, sample analysis, and data review have been performed in accordance with the most
current approved The NELAC Institute (TNI) standards, the Pace Analytical Services, LLC ("Pace")
Laboratory Quality Manual, standard operating procedures (SOPS), and Pace policies. Any exceptions to
the TNI standards, the Laboratory Quality Manual, SOPS or policies are qualified on the results page or
discussed below.
Pace is a TNI accredited laboratory; however, the following analyses are currently not listed on our TNI
scope of accreditation: Drinking Water: VOC (excluding BTEX, MTBE, Naphthalene, & 1,2-
dichloroethane) EPA 524.2, E. coli and Total coliforms SM 9223 B-2004, Solid Chemical Material: TOC
Walkley-Black, Biological Tissue: All, Non -Potable Water: SGT-HEM EPA 1664B, Silica EPA 200.7,
Boron, Calcium, Silicon, Strontium EPA 200.8, Bicarbonate, Carbonate, and Hydroxide Alkalinity SM 2320
B-2011, SM 9221 C E-2006 & SM 9222D-2006, Strontium SW-846 6010D, VOC SM 6200 B-2011, Fecal
Coliform Colilert-18, PFAS by Isotope Dilution SOP.
Pace is a DoD/DoE and TNI accredited laboratory; however, Pace is not accredited for PFAS Direct
Aqueous Injection or Method D8421.
Where applicable, all soil sample results (including LOQ and DL if requested) are corrected for dry weight
unless flagged with a "W" qualifier.
If you have any questions regarding this report, please contact the Pace Project Manager listed on the
cover page.
The pH analysis associated with the sample(s) in this report was/were performed after the method
recommended 15 minute holding time.
Inorganic Metals
Sample -001 was classified as biosolids therefore in order to ensure proper digestion, the sample was
weighed out to between 3.0 - 3.5 grams. The LOQ has been adjusted accordingly.
The method blank for analytical batch 80621 contained Copper greater than the acceptance criteria. The
associated samples contained detections for this analyte at concentrations greater than 1 OX the value
found in the method blank; therefore sample results are not impacted. The data has been reported.
Inorganic Non -Metals
The method blank for prep batch 79588 contained total phosphate greater than the method acceptance
criteria. The associated samples contained detections for this analyte at concentrations greater than 1 OX
the value found in the method blank; therefore sample results are not impacted. The data has been
reported.
Pace Analytical Services, LLC (formerly Shealy Environmetal Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 2 of 7

Client: Synagro Laboratory ID:YG07062-001
De s cription: Ne wto n Matrix: Solid
Date Sampled:07/05/2023 0830 % Solids: 1.55 07/11/2023 1543
Date Received:07/07/2023
Inorganic
non-metals
Run Prep Method
Analytical Method
Dilution
Analysis Date Analyst
Prep Date Batch
1
(% Solids) SM2540G
1
07/11/2023 1543 CVR
79671
1 350.1
(Ammonia - N) 350.1
25
07/10/2023 1217 CMM
79501
2
(Nitrate - N) 353.2
1
07/22/2023 1359 CLL2
80779
2
(Nitrite - N) 353.2
1
07/22/2023 1359 CLL2
80778
1
(Phosphorus) 365.1
20
07/14/2023 1531 DMA
07/10/2023 2319 79588
1
(Soil pH meas) 9045D
1
07/11/2023 1307 LMM2
79636
1 351.4
(TKN) 351.2
1
07/10/2023 1440 BMG2
07/09/2023 1855 79567
Parameter
CAS Analytical
Number Method
Result Q
LOQ
DL
Units Run
%Solids
SM2540G
1.55
% 1
Ammonia -N (gas diffusion)
350.1
31000
1600
840
mg/kg 1
Nitrate - N(soluble)
353.2
130 S
13
1.7
mg/kg 2
Nitrite - N(soluble)
353.2
12 J
13
1.7
mg/kg 2
Phosphorus
7723-14-0 365.1
35000
6500
1300
mg/kg 1
Soil pH measured in water @ 9.8 ° C
9045D
7.1
su 1
TKN
351.2
56000
3200
1600
mg/kg 1
CVAA
Run Prep Method Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 7471B 7471B
1 07/14/2023 0316 KJEW
07/13/2023 2210
79760
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Mercury 7439-97-6 7471B ND 5.2 1.2 mg/kg 1
IC P -AE S
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst Prep Date
Batch
1 3050B
6010D
5 07/19/2023 1823 LAB
07/12/2023 1123 79687
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units Run
Aluminum
7429-90-5 6010D
61000
2100
780
mg/kg l
Arsenic
7440-38-2 6010D
ND
78
26
mg/kg l
Cadmium
7440-43-9 6010D
ND
26
6.5
mg/kg l
Calcium
7440-70-2 6010D
730000
26000
3200
mg/kg l
Chromium
7440-47-3 6010D
170
52
13
mg/kg l
Copper
7440-50-8 6010D
720
52
23
mg/kg 1
Iron
7439-89-6 6010D
43000
520
240
mg/kg 1
Lead
7439-92-1 6010D
32 J
52
23
mg/kg 1
Magnesium
7439-95-4 6010D
18000 J
26000
3200
mg/kg 1
Manganese
7439-96-5 6010D
1700
78
31
mg/kg 1
Molybdenum
7439-98-7 6010D
ND
210
52
mg/kg 1
Nickel
7440-02-0 6010D
ND
210
54
mg/kg 1
LOQ = Limit of Quantitation
B = Detected in the method blank
E = Quantitation of compound exceeded the
calibration range
DL= Detection Limit
Q = Surrogate failure
ND = Not detected at or above the DL
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40%
J = Estimated result < LOQ and > DL
L = LCS/LCSD failure
H = Out of holding time
W = Reported on wet weight basis
S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 3 of 7

Client: Synagro Laboratory ID:YG07062-001
De s cription: Ne wto n Matrix: Solid
Date Sampled:07/05/2023 0830 % Solids: 1.55 07/11/2023 1543
Date Received:07/07/2023
IC P -AE S
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 3050B
6010D 5 07/19/2023 1823 LAB
07/12/2023 1123 79687
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units Run
Potassium
7440-09-7 6010D
3900 J
26000
3200
mg/kg 1
Selenium
7782-49-2 6010D
ND
100
42
mg/kg 1
Sodium
7440-23-5 6010D
4300 J
26000
3200
mg/kg 1
Zinc
7440-66-6 6010D
2600
260
65
mg/kg 1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation ofcompound exceeded the calibration range DL= Detection Limit Q = Surrogate failure
ND = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40% J = Estimated result < LOQ and > DL L = LCS/LCSD failure
H = Out ofholding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 4 of 7

Chain of Custody
and
Miscellaneous Documents
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 5 of 7

PACE ANALYTICAL SERVICES. LLC
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Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 6 of 7
7-1

PACE ANALYTICAL SERVICES, LLC
DC#. Ttle: ENV-FIRM-INCOL-0286 %#02 Samples Receipt Checklist 1SFC1
Effective Date: 9121702;
Sample Receipt Checklist (SRC)
Client: SILNI AGRO Cooler Inspected b5.'cLite: i31iS? i 07.W)23 T.ntt: YG07062
Yes
Ko
1. Were Custody -seats prewAlt on the cooler^ f
Mv-j
!
IN o
I I ✓ INTA
12. If Custody .waIs were present. were they intacr slrid imbroken? I!
H Suip U NA Chlorine Strip ID: `A Tested by. NA
i0al tcnWahrre upnn teccip; l Derived (Corrected) rem1peratin-e tw. n receipt %Solid Stop -Cup ID: 23-t215
1.3 f 1.3 oC NA i NA � NA i NA :C. NA jNA jC
Nhod:017cnipettature BlaakDAgaiuit Bottles IRGttn ID: $ M 01111 Crn15:clion Factor: o °C:
Method of cooiaw: i� Wet Ice ❑ Ice Nc)-s ❑ D1vIce r ]�I
JNA 3. Were all coolers received at or below 6.ON7? If no, was Project ti9anager
P&M WAS 1NOti(icd by-, ]A W I retail i &M-to-fact: (circle on::).
NA 4. Ls the conriKiz l courier's aclduG slip attached to tir:s fo ut?
6. Were proper eitstody procedures (relmoui.ltedlreceived) followed')
_ 6. Were sample IDs listed on the COC and all ;awhile containers?
7. wis collection time & true listed oil :lie COC art all ss:wple cor; Aneni'2
S. Did all cnntainer label ittf+untatku (ID. date. lime) agcv %*Mh thy: COC?
9. Wcw ;cs;s to be Uellauied iistrd oil the COO!
[ZlYel- DNo 10. Diet till saniples auive in thr. proper contaiuns for each test an4lor iri good ceadition
(1tnbruiien, lids on- etc.y? _
✓ Yes Nc 11. W.s adegikate :z.niple volume ava ilable?
✓ Yes ❑No 112. Were all saniplc3 received within'h the holdiiig tine or 48 hours, whichever corues 1r.0
Iy J Ycs ENO 13. Wcre all samples containers accounted for" No missinecxccss)
D)'cs DNo [Z]NA 14, Wete VOA. 80t5C wd RSK-175 sauipks free of bubbles 'pea-size";V� or 6inm iii
diitnieted in arty of the Z'OA via:s"
Yes No, ✓ 'A 15. were all DROlntetalstntitrienl sail les received at a l l of 2'�
Ycs lib ✓ NA 16. Wcrc all c . Bide samples received at a H 12 and suffildc Saiuples receiv�l nt a PH : 97
DYCS Dl�o D✓ NA 17. Wire all applicabic Nllii rKN+cyantde plienoLe62S.li6O8 3 (< 0.51rgIL) sxWles free of
Iesidual c1dofinr
DYcs QNo [jNA 13, Was the quote nturL� listed art the Lmttahwr lalxl? if yes, Quotc 0
'agile Frtsei-wi ien (MiLst he complctcd far auy sarnpk(s) iiicorrectly preserved or with licadspace.)
rT
011TIC(S) r+ were received incorrectly preservedand were adjusted accordingly
S.ruple L'le WithNAntL of circic one: IMO-1. HNO3, HCI. NaOH using Slt # NA_
uue of lrrc crtiatien "^. Ifinore than on: preservative is needetL pk =r nulr in the anuiitlits belou%
NA
'wet received with bubbles >b nun in diameter.
salryiles(s) NA _ _ were received i%ith TRC >- 0,5 ut ,IL (U#19 is no) and were
djusted accordingly in sample receiving with sodium thimfifate iVarSA) wi,11 Lniquc Ill: NA
Cmrnrents:
Qualtrax ID: 56360 Par -ell Analytica Services, U-C: Page 1 of 1
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 (803) 79 1-9700 Fax [phone] www.pacelabs.com
Page 7 of 7

Sodium Absorption Ratio Calculation (SAR)
Product Code Product Name
2025-01-LSLIQ-NC NEWTON, NC CLARK CREEK LIME STABILIZED
LIQUID
Na mg/I = (Na mg/kg x % Solids) = 100 = (4300 x 1.5500) = 100 = 66.65
Ca mg/I = (Ca mg/kg x % Solids) = 100 = (730000 x 1.5500) = 100 = 11315
Mg mg/I = (mg mg/kg x % Solids) = 100 = (18000 x 1.5500) = 100 = 279
Na meq = Na mg/I + Molec.Wgt.Na = 66.65 = 23 = 2.89783
Ca meq = Ca mg/I + Molec.Wgt.Ca = 11315 = 20 = 565.75
Mg meq = Mg mg/I = Molec.Wgt.Mg = 279 = 12 = 23.25
Sample Date Report Range Ratio
7/5/2023 7/1/2023 - 9/30/2023 0.1689
SAR = Na meq + SgrRoot[0.5 x (Ca meq + Mg meq)] = 2.89783 = SgrRoot[0.5(565.75+23.25)] = 0.168861

Waypointo
ANALYTICAL
10/18/2023
Synagro Central LLC/ Technical
Mary Brewer
284 Boger Road
Mocksville, NC, 27028
Ref: Analytical Testing
Report Number: 23-277-0007
Project Description: Newton
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Dear Mary Brewer:
Waypoint Analytical Virginia, Inc. received sample(s) on 10/4/2023 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Brandi Watson
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 1 of 10

(2)WaYPO*Int 7621 ain 80 -7 Road, Richmond, 27 -6446
Main 804-743 9401 °Fax [phone]
ANALYTICAL www.waypointanalytical.com
Sample Summary Table
Report Number: 23-277-0007
Client Project Description: Newton
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
63609
Newton
Solids
10/03/2023
11:30
10/04/2023
63609
Newton
Solids
10/03/2023
11:30
10/04/2023
63609
Newton
Solids
10/03/2023
11:30
10/04/2023
63609
Newton
Solids
10/03/2023
11:30
10/04/2023
63609
Newton
Solids
10/03/2023
11:30
10/04/2023
63609
Newton
Solids
10/03/2023
11:30
10/04/2023
63609
Newton
Solids
10/03/2023
11:30
10/04/2023
63609
Newton
Solids
10/03/2023
11:30
10/04/2023
SM-4500-NH3C
WP MTN
9045D
WP MTN
4500NO3F-2016
WP MTN
6010D
WP MTN
SW-7471B
WP MTN
SM-4500-NH3C-TKN
WP MTN
SM-2540G
WP MTN
WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN
Page 2 of 10

0
Waypoint.
7621 Whitepine
Road, Richmond,
VA 23237
Main 804-743-9401 ° Fax
804-271-6446
ANALYTICAL
www.waypointanalytical.com
46622
Synagro Central LLC/ Technical
Project
Newton
Mary Brewer
Report Date : 10/18/2023
284 Boger Road
Information :
Received : 10/04/2023
Mocksville , NC 27028
(j
Brandi Watson
Report Number : 23-277-0007
REPOR T OF A NA L YSIS
Lab No : 63609
Matrix: Solids
Sample ID : Newton
Sampled: 10/3/2023 11:30
Test
Results
Units
MQL
DF
Date / Time
By Analytical
Analyzed
Method
Moisture
92.1
%
0.010
1
10/05/2316:10
CAH SM-2540G
Phosphorus
10200
mg/Kg - dry
63.3
1
10/07/23 02:12
BKN 6010D
Sulfur
5010
mg/Kg - dry
127
1
10/07/23 02:12
BKN 6010D
Calcium
180000
mg/Kg - dry
6330
10
10/09/23 13:14
TJS 6010D
Aluminum
20800
mg/Kg - dry
63.3
1
10/07/23 02:12
TJS 6010D
Manganese
568
mg/Kg - dry
6.33
1
10/07/23 02:12
BKN 6010D
Copper
142
mg/Kg - dry
6.33
1
10/07/23 02:12
BKN 6010D
Zinc
622
mg/Kg - dry
15.8
1
10/07/23 02:12
BKN 6010D
Organic N
21530
mg/Kg - dry
3165
1
10/16/23 14:30
CALCULATION
Nickel
12.1
mg/Kg - dry
3.16
1
10/11/23 13:57
TJS 6010D
Lead
8.23
mg/Kg - dry
3.80
1
10/07/23 02:12
BKN 6010D
Arsenic
<6.33
mg/Kg - dry
6.33
1
10/07/23 02:12
BKN 6010D
Selenium
<6.33
mg/Kg - dry
6.33
1
10/07/23 02:12
BKN 6010D
Test
Results
Units
MQL
DF
Date / Time
By Analytical
Analyzed
Method
Total Solids 7.86 % 0.010 1 10/05/23 16:10 CAH SM-2540G
Qualifiers/ DF Dilution Factor
Definitions
MQL Method Quantitation Limit
Page 3 of 10

0
Waypoint.
7621 Whitepine
Road, Richmond,
VA 23237
Main 804-743-9401 ° Fax
804-271-6446
ANALYTICAL
www.waypointanalytical.com
46622
Synagro Central LLC/ Technical
Project
Newton
Mary Brewer
Report Date : 10/18/2023
284 Boger Road
Information :
Received : 10/04/2023
Mocksville , NC 27028
(j
Brandi Watson
Report Number : 23-277-0007
REPOR T OF A NA L YSIS
Lab No : 63609
Matrix: Solids
Sample ID : Newton
Sampled: 10/3/2023 11:30
Test
Results
Units
MQL
DF
Date / Time
By Analytical
Analyzed
Method
Total Kjeldahl Nitrogen
25800
mg/Kg - dry
3160
1
10/18/23 10:30
JPJ ;M-4500-NH3C-TKP
Potassium
862
mg/Kg - dry
127
1
10/07/23 02:12
BKN 6010D
Magnesium
5220
mg/Kg - dry
63.3
1
10/07/23 02:12
BKN 6010D
Sodium
856
mg/Kg - dry
316
1
10/07/23 02:12
BKN 6010D
Iron
12200
mg/Kg - dry
127
1
10/07/23 02:12
BKN 6010D
Ammonia Nitrogen
4290
mg/Kg - dry
1270
1
10/16/23 14:30
JPJ SM-4500-NH3C
Nitrate+Nitrite-N
<63.3
mg/Kg - dry
63.3
1
10/11/23 15:36
CLP 4500NO3F-2016
Cadmium
<1.27
mg/Kg - dry
1.27
1
10/07/23 02:12
BKN 6010D
Chromium
30.4
mg/Kg - dry
3.16
1
10/07/23 02:12
BKN 6010D
Mercury
<2.15
mg/Kg - dry
2.15
1
10/09/23 11:29
MRE SW-7471B
pH
9.7
S.U.
1
10/06/2316:07
CNB 9045D
Total Volatile Solids
38.3
%
0.010
1
10/05/23 16:10
CAH SM-2540G
Molybdenum
4.66
mg/Kg - dry
3.16
1
10/07/23 02:12
BKN 6010D
Qualifiers/ DF Dilution Factor
Definitions
MQL Method Quantitation Limit
Page 4 of 10

Waypointo
ANALYTICAL
Client: Synagro Central LLC/ Technical
Project: Newton
Lab Report Number: 23-277-0007
Date: 10/18/2023
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
CASE NARRATIVE
Metals Analysis Method 6010D
Sample 63602 (61A-0146-Syncon-Replace Cooling Tower)
Analyte: Aluminum
QC Batch No: 1-709731/1-709057
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 63602 (61A-0146-Syncon-Replace Cooling Tower)
Analyte: Calcium
QC Batch No: 1-709473/1-709057
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 63602 (61A-0146-Syncon-Replace Cooling Tower)
Analyte: Cadmium
QC Batch No: 1-709473/1-709057
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Sample 63602 (61A-0146-Syncon-Replace Cooling Tower)
Analyte: Copper
QC Batch No: 1-709473/1-709057
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 63602 (61A-0146-Syncon-Replace Cooling Tower)
Analyte: Iron
QC Batch No: 1-709473/1-709057
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 63602 (61A-0146-Syncon-Replace Cooling Tower)
Analyte: Potassium
QC Batch No: 1-709473/1-709057
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 63602 (61A-0146-Syncon-Replace Cooling Tower)
Analyte: Magnesium
QC Batch No: 1-709473/1-709057
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 63602 (61A-0146-Syncon-Replace Cooling Tower)
Page 5 of 10

Waypointo
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Analyte: Manganese
QC Batch No: 1-709473/1-709057
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 63602 (61A-0146-Syncon-Replace Cooling Tower)
Analyte: Phosphorus
QC Batch No: 1-709473/1-709057
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 63602 (61A-0146-Syncon-Replace Cooling Tower)
Analyte: Lead
QC Batch No: 1-709473/1-709057
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 63602 (61A-0146-Syncon-Replace Cooling Tower)
Analyte: Zinc
QC Batch No: 1-709473/1-709057
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 81582 (WRC Topsoil (Oct))
Analyte: Arsenic
QC Batch No: 1-710201/1-709902
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Sample 81582 (WRC Topsoil (Oct))
Analyte: Calcium
QC Batch No: 1-710659/1-709902
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 81582 (WRC Topsoil (Oct))
Analyte: Cadmium
QC Batch No: 1-710201/1-709902
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Sample 81582 (WRC Topsoil (Oct))
Analyte: Iron
QC Batch No: 1-710659/1-709902
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 81582 (WRC Topsoil (Oct))
Analyte: Potassium
QC Batch No: 1-710659/1-709902
Page 6 of 10

Waypointo
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 81582 (WRC Topsoil (Oct))
Analyte: Magnesium
QC Batch No: 1-710201/1-709902
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 81582 (WRC Topsoil (Oct))
Analyte: Manganese
QC Batch No: 1-710659/1-709902
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 81582 (WRC Topsoil (Oct))
Analyte: Nickel
QC Batch No: 1-710201/1-709902
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 81582 (WRC Topsoil (Oct))
Analyte: Lead
QC Batch No: 1-710201/1-709902
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 81582 (WRC Topsoil (Oct))
Analyte: Sulfur
QC Batch No: 1-710201/1-709902
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 81582 (WRC Topsoil (Oct))
Analyte: Selenium
QC Batch No: 1-710201/1-709902
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Sample 81582 (WRC Topsoil (Oct))
Analyte: Selenium
QC Batch No: 1-710659/1-709902
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Sample 81582 (WRC Topsoil (Oct))
Analyte: Zinc
QC Batch No: 1-710201/1-709902
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Solids Total Mercury Analysis - CVAA Method 7471A
Sample 97716 (Annual Sludge)
Page 7 of 10

Waypointo
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
www.waypointanalytical.com
Analyte: Mercury
QC Batch No: 1-709569/1-709290
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Page 8 of 10

(2)
WayPAo Int..
NALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
www.waypointanalytical.com
Shipment Receipt Form
Customer Number: 46622
Customer Name: Synagro Central LLC/ Technical
Report Number: 23-277-0007
Shipping Method
0 Fed Ex 0 US Postal 0 Lab 0 Other:
* UPS 0 Client 0 Courier Thermometer ID:
Shipping container/cooler uncompromised?
* Yes
0 No
Number of coolers/boxes received
F
Custody seals intact on shipping container/cooler?
0 Yes
0 No
Not Present
Custody seals intact on sample bottles?
0 Yes
0 No
Not Present
Chain of Custody (COC) present?
Yes
0 No
COC agrees with sample label(s)?
U Yes
0 No
COC properly completed
U Yes
0 No
Samples in proper containers?
U Yes
0 No
Sample containers intact?
Yes
0 No
Sufficient sample volume for indicated test(s)?
Yes
0 No
All samples received within holding time?
Yes
0 No
Cooler temperature in compliance?
Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
Yes
0 No
Water - Sample containers properly preserved
0 Yes
0 No
N/A
Water - VOA vials free of headspace
0 Yes
0 No
N/A
Trip Blanks received with VOAs
0 Yes
0 No
0 N/A
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
0 N/A
F_ High concentration container (48 hr) F Low concentration EnCore samplers (48 hr)
F_ High concentration pre -weighed (methanol -14 d) Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included?
0 Yes
0 No
Comments:
Signature: David Lennon Date & Time: 10/04/2023 10:09:51
Page 9 of 10

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Page 10 of 10

Sodium Absorption Ratio Calculation (SAR)
Product Code Product Name
2025-01-LSLIQ-NC NEWTON, NC CLARK CREEK LIME STABILIZED
LIQUID
Na mg/I = (Na mg/kg x % Solids) = 100 = (856 x 7.8600) = 100 = 67.2816
Ca mg/I = (Ca mg/kg x % Solids) = 100 = (180000 x 7.8600) = 100 = 14148
Mg mg/I = (mg mg/kg x % Solids) = 100 = (5220 x 7.8600) = 100 = 410.292
Na meq = Na mg/I + Molec.Wgt.Na = 67.2816 = 23 = 2.92529
Ca meq = Ca mg/I + Molec.Wgt.Ca = 14148 = 20 = 707.4
Mg meq = Mg mg/I = Molec.Wgt.Mg = 410.292 = 12 = 34.191
Sample Date Report Range Ratio
10/3/2023 10/1/2023 - 0.1519
12/31 /2023
SAR = Na meq + SgrRoot[0.5 x (Ca meq + Mg meq)] = 2.92529 = SgrRoot[0.5(707.4+34.191)] = 0.151915

SECTION 3

ANNUAL LAND APPLICATION FIELD SUMMARY FORM Page: 1
FACILITY NAME: NEWTON, INC WQ PERMIT #: WQ0003902 FIELD#: NC-CA-00020-0-0010- ACRES UTILIZED: 36.0
LAND OWNER: HAROLD SHERRILL ANNUAL DRY TONS APPLIED: 94.75 SITE #: NC CA 00020 ACRES PERMITTED: 36.0
OPERATOR: TIM WOODRIFF PREDOMINANT SOIL SERIES: LLOYD CATION EXCHANGE CAPACITY (NON-503):
CROP 1 NAME: FESCUE HAY (FSH) CROP 1 MAX. PAN: 216 CROP 2 NAME: CROP 2 MAX. PAN:
RESIDUAL SOURCE(S): * See list at bottom of report
Gallons (G)
Site
Name of Crop Type
or Cubic Yards (Y)
Cond.
Precip
Volati-
Mineral-
Ammonia
Nitrate
PAN Applied
Receiving Residual
Date or
or Wet Tons (W)
% Residual
Dry, Wet,
Past 24 Hrs.
Application
lization
ization
TKN
Nitrogen
and Nitrite
(Ibs/acre)
Application
Month
Amount UOM
Solids Dry Tons/Ac
Source
Moist
Inches
Method*
Rate**
Rate***
mg/kg
mg/kg
mg/kg
Crop 1 Crop 2
Crop 1 Crop 2
2/11/2023
162,000.00
(G)
9.710 1.822 NCCLSL
DRY
0-<1/2""
SUR
0.5
0.30
18,000.00
960.00
134.00
20.866
FSH
2/20/2023
72,000.00
(G)
9.710 0.810 NCCLSL
DRY
0-<1/2""
SUR
0.5
0.30
18,000.00
960.00
134.00
9.274
FSH
Feb-23
234,000.00
(G)
Total 2.632
Total
30.140 0.000
AS
CD
CU
CR
PB
HG
MO
NI
SE
ZN
P
Lime Applied
Annual Ibs/acre Applied
0.013
1 0.003
1.000
0.221
0.053
0.001
0.017
0.068
0.022 1
4.158
78.957
Date J Lbs/Ac
Cumulative Ibs/acre Applied 0.058 I 0,021 B 4.214 I 1.059 0.259 f 0.014 0.108 I 0.353 B 0.049 I 14.590 I O
Permit PAN Limit (Ibs/acre) 1st Crop I I 3 I I I 216
Federal C.P.L.R. (Ibs/acre)**** 36.6 34.8 1,339.0 267.9 15.0 375.0 89.0 2,500.0
NCCLSL = NEWTON, NC CLARK CREEK LIME STABILIZED LIQUID
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am
aware that there are significant pen ti tfor sub g false information, including the possibility of fines and imprisonment for knowing violations."
2- b -
_tIGNATURr= OF LAND APPLIER DATE
NR = Not Reported or Not Required *** Mineralization Rates: Compost-0.1, Anaerobically digested-0.2, Aerobically digested-0.3, Raw Sludge-0.4
* Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation *'* C.P.L.R.: Cumulative Pollutant Loading Rate
*' Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 *"'" See Site pH & Lime Application Records Section of Report
Printed: 1/24/2024 DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Total Dry Tons Applied (Annual):
Facility Name: NEWTON, NC 94.75
Permit #: WQ0003902 Cation Exchange Capacity (non 503 only):
Operator: TIM WOODRIFF HAROLD SHERRILL Predominant Soil Series: LLOYD
Owner:
Acres Used: 36.00 Acres Permitted: 36.00 Site #: Field #: NC CA 00020 0010
NC CA 00020
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Source
NCCLSL
Sample or
Composite
Date
1
1/11/23
2
3
4
5
6
7
8
9
10
11
12
Solids
9.71
Arsenic
2.500
Cadmium
0.580
Copper
190
Chromium
42.00
Lead
10.00
Mercury
0.190
Molybdenum
3.20
Nickel
13.00
Selenium
4.20
Zinc
790
Total Phosphorus
15000
Annual Heavy Metal Field Loadings (Calculated in Ibs/acre):
Source
NCCLSL
Total DT/Ac.
/ App.Event
1
2.63
2
3
4
5
6
7
8
9
10
11
12
Totals
Arsenic
0.013
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.013
Cadmium
0.003
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.003
Copper
1.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1.000
Chromium
0.221
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.221
Lead
0.053
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.053
Mercury
0.001
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.001
Molybdenum
0.017
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.017
Nickel
0.068
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.068
Selenium
0.022
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.022
Zinc
4.158
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
4.158
Total Phosphorus
78.957
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
78.957
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that
there are significMpnalties for submitting false information, including the possibility of fines and imprisonment for knowing violations".
Signature of Land Applier Date DENR FORM MFLSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM Page: 1
FACILITY NAME: NEWTON, NC WQ PERMIT #: WQ0003902 FIELD#: NC-CA-00020-0-0013- ACRES UTILIZED: 22.1
LANDOWNER: SHERRILL FURNITURE COMPANY ANNUAL DRY TONS APPLIED: 108.16 SITE #: NC CA 00020 ACRES PERMITTED: 22.1
OPERATOR: TIM WOODRIFF PREDOMINANT SOIL SERIES: LLOYD CATION EXCHANGE CAPACITY (NON-503):
CROP 1 NAME: FESCUE HAY (FSH) CROP 1 MAX. PAN: 226 CROP 2 NAME: CROP 2 MAX. PAN:
RESIDUAL SOURCE(S): * See list at bottom of report
Gallons (G)
Site
Name of Crop Type
or Cubic Yards (Y)
Cond.
Precip
Volati-
Mineral-
Ammonia
Nitrate
PAN Applied
Receiving Residual
Date or
or Wet Tons (W)
%
Residual
Dry, Wet,
Past 24 Hrs.
Application
lization
ization
TKN
Nitrogen
and Nitrite
(Ibs/acre)
Application
Month
Amount UOM
Solids
Dry Tons/Ac
Source
Moist
Inches
Method*
Rate**
Rate***
mg/kg
mg/kg
mg/kg
Crop 1 Crop 2
Crop 1 Crop 2
11/8/2023
132,000.00 (G)
7.860
1.958
NCCLSL
DRY
0-<1/2""
SUR
0.5
0.30
25,800.00
4,290.00
63.30
33.935
FSH
11/9/2023
108,000.00 (G)
7.860
1.602
NCCLSL
DRY
0-<1/2""
SUR
0.5
0.30
25,800.00
4,290.00
63.30
27.765
FSH
11/10/2023
90,000.00 (G)
7.860
1.335
NCCLSL
DRY
0-<1/2""
SUR
0.5
0.30
25,800.00
4,290.00
63.30
23.138
FSH
Nov-23
330,000.00 (G)
Total 4.895
Total
84.838 0.000
AS CD
CU
CR
PB
HG
MO
NI
SE
ZN
P
Lime Applied
Annual Ibs/acre Applied
0.062 1 0.012
1 1.390
0.298
0.081
0.021
0.046
0.118
0.062
6.088
99.841
Date Lbs/Ac
Cumulative Ibs/acre Applied 0.075 [ 0.017 I 2.705 I 0.526 0.162 3 0.023 { 0.087 I 0.218 0.087 s 10.765 I I f 1 1
Permit PAN Limit (Ibs/acre) 1st Crop 226
Federal C.P.L.R. (Ibs/acre)**** 36.6 34.8 1,339.0 267.9 15.0 375.0 89.0 2,500.0
NCCLSL = NEWTON, NC CLARK CREEK LIME STABILIZED LIQUID
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am
aware that there are significant pen t' s for submitting false information, including the possibility of fines and imprisonment for knowing violations."
SIGNATURE OF LAND APPLIER DATE
NR = Not Reported or Not Required *** Mineralization Rates: Compost-0.1, Anaerobically digested-0.2, Aerobically digested-0.3, Raw Sludge-0.4
* Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation **** C.P.L.R.: Cumulative Pollutant Loading Rate
** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 ***** See Site pH & Lime Application Records Section of Report
Printed: 1/24/2024 DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Total Dry Tons Applied (Annual):
Facility Name: NEWTON, NC
Permit #: W00003902 Cation Exchange Capacity (non 503 only):
Operator: TIM WOODRIFF SHERRILL FURNITURE COMPANY Predominant Soil Series:
Owner:
Acres Used: 22.10 Acres Permitted: 22.10 Site #: Field #:
NC CA 00020
Raeidual Analvcic Data 114- Matalc and Tntal Phncnhnnic ilea mn/kn ^/ Cnlide .ica Raw P-... t Al-
108.16
LLOYD
NC CA 00020 0013
Source
NCCLSL
Sample or
Composite
Date
1
10/03/23
2
3
4
5
6
7
8
9
10
11
12
Solids
7.86
Arsenic
6.330
Cadmium
1.270
Copper
142
Chromium
30.40
Lead
8.23
Mercury
2.150
Molybdenum
4.66
Nickel
12.10
Selenium
6.33
Zinc
622
Total Phosphorus
10200
Annual Heavy Metal Field Loadings (Calculated in Ibs/acre):
Source
NCCLSL
Total DT/Ac.
/App. Event
1
4.89
2
3
4
5
6
7
8
9
10
11
12
Totals
Arsenic
0.062
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.062
Cadmium
0.012
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.012
Copper
1.390
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1.390
Chromium
0.298
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.298
Lead
0.081
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.081
Mercury
0.021
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.021
Molybdenum
0.046
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.046
Nickel
0.118
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.118
Selenium
0.062
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.062
Zinc
6.088
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0,000
6.088
Total Phosphorus
99.841
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
99.841
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that
there are si 'ficant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations".
0 �_.
Signature of Land Applief Date DENR FORM MFLSF (12/2006)

FACILITY NAME: NEWTON, NC
LAND OWNER: THOMAS WARLICK
OPERATOR: TIM WOODRIFF
CROP 1 NAME: FESCUE HAY (FSH)
RESIDUAL SOURCE(S): * See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
WQ PERMIT #: WQ0003902 FIELD#: NC-CA-00021-0-0001-
ANNUAL DRY TONS APPLIED: 196.82 SITE #: NC CA 00021
PREDOMINANT SOIL SERIES: LLOYD
CROP 1 MAX. PAN: 216 CROP 2 NAME:
ACRES UTILIZED: 27.5
ACRES PERMITTED: 27.5
CATION EXCHANGE CAPACITY (NON-503):
CROP 2 MAX. PAN:
Page: 1
Gallons (G)
Site
Name of Crop Type
or Cubic Yards (Y)
Cond.
Precip
Volati-
Mineral-
Ammonia
Nitrate
PAN Applied
Receiving Residual
Date or
or Wet Tons (W)
%
Residual
Dry, Wet,
Past 24 Hrs.
Application
lization
ization
TKN
Nitrogen
and Nitrite
(Ibs/acre)
Application
Month
Amount UOM
Solids
Dry Tons/Ac
Source
Moist
Inches
Method*
Rate**
Rate***
mg/kg
mg/kg
mg/kg
Crop 1 Crop 2
Crop 1 Crop 2
1/18/2023
6,000.00 (G)
9.710
0.088
NCCLSL
MOIST
0-<1/2""
SUR
0.5
0.30
18,000.00
960.00
134.00
1.012
FSH
1/19/2023
6,000.00 (G)
9.710
0.088
NCCLSL
MOIST
0-<1/2""
SUR
0.5
0.30
18,000.00
960.00
134.00
1.012
FSH
1/20/2023
120,000.00 (G)
9.710
1.767
NCCLSL
MOIST
0-<1/2""
SUR
0.5
0.30
18,000.00
960.00
134.00
20.234
FSH
1/21/2023
132,000.00 (G)
9.710
1.944
NCCLSL
DRY
0-<1/2""
SUR
0.5
0.30
18,000.00
960.00
134.00
22.258
FSH
Jan-23
26400.00 (G)
E
2/10/2023
156,000.00 (G)
9.710
2.297
NCCLSL
DRY
0-<1/2""
SUR
0.5
0.30
18,000.00
960.00
134.00
26.304
FSH
Feb-23
156,000.00 (G)
9/7/2023
174,000.00 (G)
1.550
0.409
NCCLSL
DRY
0-<1/2""
SUR
0.5
0.30
56,000.00
31,000.00
142.00
18.928
FSH
9/8/2023
180,000.00 (G)
1.550
0.423
NCCLSL
DRY
0-<1/2""
SUR
0.5
0.30
56,000.00
31,000.00
142.00
19.581
FSH
9/12/2023
60,000.00 (G)
1.550
0.141
NCCLSL
DRY
0-<1/2""
SUR
0.5
0.30
56,000.00
31,000.00
142.00
6.527
FSH
Sep-23
1 414,000.00 (G)
Total 7.157 Total 115.856 0.000
AS CD CU CR PB HG MO NI SE ZN P Lime Applied
Annual Ibs/acre Applied 0.082 1 0.020 3.751 0.850 0.186 1 0.005 1 0.141 0.266 0.134 14.831 253.634 ; Date I Lbs/Ac
Cumulative Ibs/acre Applied 0.195 0.062 1 10.684 I 2.464 1 0.669 1 0.022 i 0.320 0.933 I I 0.248 41.136 I
Permit PAN Limit (Ibs/acre) 1st Crop 216
Federal C.P.L.R. (Ibs/acre)**** 36.6 34.8 I 1,339.0 267.9 15.0 375.0 89.0 2,500.0
NCCLSL = NEWTON, NC CLARK CREEK LIME STABILIZED LIQUID
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am
aware that there are significant ties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
SIGNATURE OF LAND APPLIER DATE
NR = Not Reported or Not Required *** Mineralization Rates: Compost-0.1, Anaerobically digested-0.2, Aerobically digested-0.3, Raw Sludge-0.4
* Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation **** C.P.L.R.: Cumulative Pollutant Loading Rate
** Volatilization Rate: Surface 0.5, InjectionfIncorporation 1.0 '**** See Site pH & Lime Application Records Section of Report
Printed: 1/24/2024 DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Total Dry Tons Applied (Annual):
Facility Name: NEWTON, NC
Permit #: WQ0003902 Cation Exchange Capacity (non 503 only):
196.82
Operator: TIM WOODRIFF THOMAS WARLICK Predominant Soil Series: LLOYD
Owner:
Acres Used: 27.50 Acres Permitted: 27.50 Site #: Field #: NC CA 00021 0001
NC CA 00021
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Source
NCCLSL
NCCLSL
Sample or
Composite
Date
1
1/11/23
2
7/05/23
3
4
5
6
7
8
9
10
11
12
Solids
9.71
1.55
Arsenic
2,500
26.000
Cadmium
0.580
6.500
Copper
190
720
Chromium
42.00
170.00
Lead
10.00
32.00
Mercury
0.190
1.200
Molybdenum
3.20
52.00
Nickel
13.00
54.00
Selenium
4.20
42.00
Zinc
790
2600
Total Phosphorus
15000
35000
Annual Heavy Metal Field Loadings (Calculated in Ibs/acre):
Source
NCCLSL
NCCLSL
Total DT/Ac.
/ App.Event
1
6.18
2
0.97
3
4
5
6
7
8
9
10
11
12
Totals
Arsenic
0.031
0.051
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.082
Cadmium
0.007
0.013
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.020
Copper
2.350
1.401
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
3.751
Chromium
0.519
0.331
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.850
Lead
0.124
0.062
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.186
Mercury
0.002
0.002
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.005
Molybdenum
0.040
0.101
0.000
0.000
0.000
0.000
0.000
0.000
0,000
0.000
0.000
0.000
0.141
Nickel
0.161
0.105
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.266
Selenium
0.052
0.082
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.134
Zinc
9.771
5.060
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
14.831
Total Phosphorus
185.521
68.114
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
253.634
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that
there are significt nalties for submitting false information, including the possibility of fines and imprisonment for knowing violations".
Signature of Land Applier Date DENR FORM MFLSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM Page: 1
FACILITY NAME: NEWTON, NC WQ PERMIT #: WQ0003902 FIELD#: NC-CA-00021-0-0002- ACRES UTILIZED: 50.7
LAND OWNER: THOMAS WARLICK ANNUAL DRY TONS APPLIED: 170.96 SITE #: NC CA 00021 ACRES PERMITTED: 50.7
OPERATOR: TIM WOODRIFF PREDOMINANT SOIL SERIES: LLOYD CATION EXCHANGE CAPACITY (NON-503):
CROP 1 NAME: FESCUE HAY (FSH) CROP 1 MAX. PAN: 216 CROP 2 NAME: CROP 2 MAX. PAN:
RESIDUAL SOURCE(S): * See list at bottom of report
Gallons (G)
Site
Name of Crop Type
or Cubic Yards (Y)
Cond.
Precip
Volati-
Mineral-
Ammonia
Nitrate
PAN Applied
Receiving Residual
Date or
or Wet Tons (W)
%
Residual
Dry, Wet,
Past 24 Hrs.
Application
lization
ization
TKN
Nitrogen
and Nitrite
(Ibs/acre)
Application
Month
Amount UOM
Solids
Dry Tons/Ac
Source
Moist
Inches
Method*
Rate**
Rate***
mg/kg
mg/kg
mg/kg
Crop 1 Crop 2
Crop 1 Crop 2
4/11/2023
174,000.00
(G)
6.570
0.940
NCCLSL
MOIST
0-<14
SUR
0.5
0.30
27,000.00
8,500.00
97.40
18.612
FSH
4/12/2023
120,000.00
(G)
6.570
0.648
NCCLSL
DRY
0-<1/2""
SUR
0.5
0.30
27,000.00
8,500.00
97.40
12.836
FSH
4/13/2023
192,000.00
(G)
6.570
1.038
NCCLSL
DRY
0-<1/2""
SUR
0.5
0.30
27,000.00
8,500.00
97.40
20.537
FSH
4/17/2023
138,000.00
(G)
6.570
0.746
NCCLSL
MOIST
0-<1/2""
SUR
0.5
0.30
27,000,00
8,500.00
97.40
14.761
FSH
Apr-23
624,000.00
(G)
Total 3.372
Total
66.746 0.000
AS
CD
CU
CR
PB
HG
MO
NI
SE
ZN
P
Lime Applied
Annual Ibs/acre Applied
0.021
1 0.007
1,619
0.243
0.064
0.002 1
0.036
1 0.108
0.016
1 5.665 1
58.672
Date Lbs/Ac
Cumulative Ibs/acre Applied 0.199 ( 0.058 9.936 I 2.231 I 0.663 1 0.023 1 0.270 0.895 I 0.178 36.724
Permit PAN Limit (Ibs/acre) 1st Crop: }} 216
Federal C.P.L.R. (Ibs/acre)**** 31 34.8 1,339.0 267.9 15.0 375.0 89.0 2,500.0
NCCLSL = NEWTON, NC CLARK CREEK LIME STABILIZED LIQUID
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am
aware that there are significant peiAa 'es for submitting false information, including the possibility of fines and imprisonment for knowing violations."
SIGNAT RE OF LAND APPLIER DATE
NR = Not Reported or Not Required *** Mineralization Rates: Compost-0.1, Anaerobically digested-0.2, Aerobically digested-0.3, Raw Sludge-0.4
* Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation **** C.P.L.R.: Cumulative Pollutant Loading Rate
* Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 ***** See Site pH & Lime Application Records Section of Report
Printed: 1/24/2024 DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Total Dry Tons Applied (Annual):
Facility Name: NEWTON, NC 170.96
Permit #: WQ0003902 Cation Exchange Capacity (non 503 only):
Operator: TIM WOODRIFF THOMAS WARLICK Predominant Soil Series: LLOYD
Owner:
Acres Used: 50.70 Acres Permitted: 50.70 Site #: Field #: NO CA 00021 0002
NC CA 00021
Source
NCCLSL
Sample or
Composite
Date
1
4/04/23
2
3
4
5
6
7
8
9
10
11
12
Solids
6.57
Arsenic
3.100
Cadmium
1.100
Copper
240
Chromium
36.00
Lead
9.50
Mercury
0.270
Molybdenum
5.30
Nickel
16.00
Selenium
2.30
Zinc
840
Total Phosphorus
8700
Annual W.-, Mafal Fialrl I nariinnc !(`.alunlafarl in the/aural'
Source
NCCLSL
Total DT/Ac.
/ App.Event
1
3.37
2
3
4
5
6
7
8
9
10
11
12
Totals
Arsenic
0.021
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.021
Cadmium
0.007
0.000
0.000
0.000
0.000
0.000
0.000
0,000
0.000
0.000
0.000
0.000
0.007
Copper
1.619
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1.619
Chromium
0.243
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.243
Lead
0.064
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0,000
0.000
0,000
0.064
Mercury
0.002
0,000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.002
Molybdenum
0.036
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.036
Nickel
0.108
0.000
0,000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.108
Selenium
0.016
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.016
Zinc
5.665
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
5.665
Total Phosphorus
58.672
0.000
0.000
0.000
0.000
0.000
0.000
0,000
0.000
0.000
0.000
0.000
58.672
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that
there are signific t cnalties for submitting false information, including the possibility of fines and imprisonment for ]mowing violations".
-z' Z `{
Signature of Land Applier Date DENR FORM MFLSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM Page: 1
FACILITY NAME: NEWTON, NC WQ PERMIT M WQ0003902 FIELD#: NC-CA-00025-0-0002- ACRES UTILIZED: 43.8
LANDOWNER: GARY DELLINGER ANNUAL DRY TONS APPLIED: 9.31 SITE #: NC CA 00025 ACRES PERMITTED: 43.8
OPERATOR: GARY DELLINGER PREDOMINANT SOIL SERIES: PACOLET CATION EXCHANGE CAPACITY (NON-503):
CROP 1 NAME: FESCUE HAY (FSH) CROP 1 MAX. PAN: 194 CROP 2 NAME: CROP 2 MAX. PAN:
RESIDUAL SOURCE(S): * See list at bottom of report
Date or
Month
Gallons (G)
or Cubic Yards (Y)
or Wet Tons (W)
Amount UOM
%
Solids Dry Tons/Ac
Residual
Source
Site
Cond.
Dry, Wet,
Moist
Precip
Past 24 Hrs.
Inches
Application
Method*
Volati-
lization
Rate**
Mineral-
ization
Rate***
TKN
mg/kg
Ammonia
Nitrogen
mg/kg
Nitrate
and Nitrite
mg/kg
PAN Applied
(Ibs/acre)
Crop 1 Crop 2
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
9/12/2023
9/14/2023
Sep-23
54,000.00
90,000.00
144,000.00
(G)
(G)
(G)
1.550 0.080
1.550 0.133
NCCLSL
NCCLSL
DRY
MOIST
0-<1/2""
0-<1/2""
SUR
SUR
0.5
0.5
0.30
0.30
56,000.00
56,000.00
31,000.00
31,000.00
142.00
142.00
3.688
6.147
FSH
FSH
Total 0.213
Total
9.835 0.000
Annual Ibs/acre Applied
AS CD
0.011 1 0.003
CU
0.306
CR
0.072
PB
HG
MO
NI
SE
ZN
P
Lime Applied
0.014 <0.001 0.022 0.023 0.018 1.105 14.875 Date Lbs/Ac
Cumulative Ibs/acre Applied
0.022 0.004
0.882
0.207
0.044
<0.001
0.034
1 0.059
0.026
3.054
Permit PAN Limit (Ibs/acre)
1st Crop
194
Federal C.P.L.R. (Ibs/acre)**** 36.6 1 34.8 1 1,339.0 I I 267.9 15.0 I 375.0 1 89.0 I 2,500.0 '
NCCLSL = NEWTON, NC CLARK CREEK LIME STABILIZED LIQUID
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am
aware that there are signifi, penalties fors brnitting false information, including the possibility of fines and imprisonment for knowing violations."
SI NATURE OF LAND APPLIER DATE
NR = Not Reported or Not Required *** Mineralization Rates: Compost-0.1, Anaerobically digested-0.2, Aerobically digested-0.3, Raw Sludge-0.4
* Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation **** C.P.L.R.: Cumulative Pollutant Loading Rate
" Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * * * See Site pH & Lime Application Records Section of Report
Printed: 1/24/2024 DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Total Dry Tons Applied (Annual):
Facility Name: NEWTON, NC
Permit #: WQ0003902 Cation Exchange Capacity (non 503 only):
Operator: GARY DELLINGER GARY DELLINGER Predominant Soil Series:
Owner:
9.31
PACOLET
Acres Used: 43.80 Acres Permitted: 43.80 Site #: Field #: NC CA 00025 0002
NC CA 00025
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kq, % Solids use Raw Percent #):
Source
NCCLSL
Sample or
Composite
Date
1
7105/23
2
3
4
5
6
7
8
9
10
11
12
Solids
1.55
Arsenic
26.000
Cadmium
6.500
Copper
720
Chromium
170.00
Lead
32.00
Mercury
1.200
Molybdenum
52.00
Nickel
54.00
Selenium
4200.
Zinc
2600
Total Phosphorus
35000
Annual Heavy Metal Field Loadings (Calculated in Ibs/acre):
Source
NCCLSL
Total DT/Ac.
/App.Event
1
0.21
2
3
4
5
6
7
8
9
10
11
12
Totals
Arsenic
0.011
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.011
Cadmium
0.003
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.003
Copper
0.306
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.306
Chromium
0.072
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.072
Lead
0.014
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.014
Mercury
0.001
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.001
Molybdenum
0.022
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.022
Nickel
0.023
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0,000
0.000
0.000
0.023
Selenium
0.018
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.018
Zinc
1.105
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1.105
Total Phosphorus
14.875
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
14.875
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that
there are significant py1o,
ies for submitting false information, including the possibility of fines and imprisonment for knowing violations".
--L-b 7�
Signature of Land App ier Date DENR FORM MFLSF (1212006)

FACILITY NAME: NEWTON, NC
LAND OWNER: RONNIE SIGMON
OPERATOR: RONNIE SIGMON
CROP 1 NAME: FESCUE HAY (FSH)
RESIDUAL SOURCE(S): * See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM Page: 1
WQ PERMIT #: WQ0003902 FIELD#: NC-CA-00032-0-0001- ACRES UTILIZED: 12.2
ANNUAL DRY TONS APPLIED: 51.13 SITE #: NC CA 00032 ACRES PERMITTED: 12.2
PREDOMINANT SOIL SERIES: APPLING CATION EXCHANGE CAPACITY (NON-503):
CROP 1 MAX. PAN: 237 CROP 2 NAME: CROP 2 MAX. PAN:
Gallons (G)
Site
Name of Crop Type
or Cubic Yards (Y)
Cond.
Precip
Volati-
Mineral-
Ammonia
Nitrate
PAN Applied
Receiving Residual
Date or or Wet Tons (W)
%
Residual
Dry, Wet,
Past 24 Hrs.
Application
lization
ization
TKN
Nitrogen
and Nitrite
(Ibs/acre)
Application
Month Amount UOM
Solids
Dry Tons/Ac
Source
Moist
Inches
Method*
Rate**
Rate***
mg/kg
mg/kg
mg/kg
Crop 1 Crop 2
Crop 1 Crop 2
11/10/2023 12,000.00 (G)
7.860
0.322
NCCLSL
DRY
0-<1/2"
SUR
0.5
0.30
25,800.00
4,290.00
63.30
5.588
FSH
11/13/2023 108,000.00 (G)
7.860
2.902
NCCLSL
DRY
0-<1/2""
SUR
0.5
0.30
25,800.00
4,290.00
63.30
50.296
FSH
11/14/2023 36,000.00 (G)
7.860
0.967
NCCLSL
DRY
0-<1/2""
SUR
0.5
0.30
25,800.00
4,290.00
63.30
16,765
FSH
Nov-23 156,000.00 (G)
Total 4.191
Total
72.649 0.000
AS CD
CU
CR
PB
HG
MO
NI
SE
ZN
P
Lime Applied
Annual Ibs/acre Applied
0.053 0.011
1.190
0.255
0.069
0.018
0.039
0.101
0.053
5.214
85.497
Date Lbs/Ac
Cumulative Ibs/acre Applied
0.209 0.069
1 11.630
J 2.223
1 0.771 1
0.028 1
0.250
1 0.999
1 0.291 1
40.816
I I I I ➢ I I 1 ➢ 1 1 1 1 ➢ 1
Permit PAN Limit (Ibs/acre) 1st Crop 237
Federal C.P.L.R. (Ibs/acre)**** 36.6 1 34.8 1 1,339.0 267.9 1 15.0 375.0 1 89.0 1 2,500.0
NCCLSL = NEWTON, NC CLARK CREEK LIME STABILIZED LIQUID
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am
aware that there are significant pen i for submitting false information, including the possibility of fines and imprisonment for knowing violations."
SIGNATURE OF LAND APPLIER DATE
NR = Not Reported or Not Required *** Mineralization Rates: Compost-0.1, Anaerobically digested-0.2, Aerobically digested-0.3, Raw Sludge-0.4
* Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation **** C.P.L.R.: Cumulative Pollutant Loading Rate
*` Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 ***'* See Site pH & Lime Application Records Section of Report
Printed: 1/24/2024 DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM'
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Total Dry Tons Applied (Annual):
Facility Name: NEWTON, NC
Permit #: WQ0003902 Cation Exchange Capacity (non 503 only)
51.13
Operator: RONNIE SIGMON RONNIE SIGMON Predominant Soil Series: APPLING
Owner:
Acres Used: 12.20 Acres Permitted: 12.20 Site #: Field #: NC CA 00032 0001
NC CA 00032
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Source
NCCLSL
Sample or
Composite
Date
1
10/03/23
2
3
4
5
6
7
8
9
10
11
12
Solids
7.86
Arsenic
6.330
Cadmium
1.270
Copper
142
Chromium
30.40
Lead
8.23
Mercury
2.150
Molybdenum
4.66
Nickel
12.10
Selenium
6.33
Zinc
622
Total Phosphorus
10200
Annual Heavy Metal Field Loadings (Calculated in Ibs/acre):
Source
NCCLSL
Total DT/Ac.
I App.Event
1
4.19
2
3
4
5
6
7
8
9
10
11
12
Totals
Arsenic
0.053
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.053
Cadmium
0.011
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.011
Copper
1.190
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1.190
Chromium
0.255
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.255
Lead
0.069
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.069
Mercury
0.018
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.018
Molybdenum
0.039
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.039
Nickel
0.101
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.101
Selenium
0.053
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.053
Zinc
5.214
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
5.214
Total Phosphorus
85.497
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
85.497
"7 certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that
there are sigmfican jlhes for submitli g false information, including the possibility offines and imprisonment for knowing violations".
Signature of Land Applier Date DENR FORM MFLSF (12/2006)

FACILITY NAME: NEWTON, NC
LAND OWNER: RONNIE SIGMON
OPERATOR: RONNIE SIGMON
CROP 1 NAME: FESCUE HAY (FSH)
RESIDUAL SOURCE(S): * See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
WQ PERMIT #: W00003902 FIELD#: NC-CA-00032-0-0002-
ANNUAL DRY TONS APPLIED: 27.53 SITE #: NC CA 00032
PREDOMINANT SOIL SERIES: APPLING
CROP 1 MAX. PAN: 237 CROP 2 NAME:
ACRES UTILIZED: 7.4
ACRES PERMITTED: 7.4
CATION EXCHANGE CAPACITY (NON-503):
CROP 2 MAX. PAN:
Page: 1
Gallons (G)
Site
Name of Crop Type
or Cubic Yards (Y)
Cond.
Precip
Volati-
Mineral-
Ammonia
Nitrate
PAN Applied
Receiving Residual
Date or
or Wet Tons (W)
%
Residual Dry, Wet,
Past 24 Hrs. Application
lization
ization TKN
Nitrogen
and Nitrite
(Ibs/acre)
Application
Month
Amount UOM
Solids
Dry Tons/Ac Source Moist
Inches Method*
Rate"
Rate*** mg/kg
mg/kg
mg/kg
Crop 1 1 Crop 2
Crop 1 Crop 2
11/14/2023
84,000.00
(G)
7.860
3.721 NCCLSL DRY
0-<1/2"" SUR
0.5
0.30 25,800.00
4,290.00
63.30
64.494
FSH
Nov-23
84,000.00
(G)„
Total 3.721 1 vlM
AS CD CU CR PB HG MO NI SE ZN P Lime
Ibs/acre Applied 0.047 0.009 1.057 0.226 0.061 1 0.016 0.035 0.090 0.047 4.628 75.899 Date
tive Ibs/acre Applied 0.137 0.044 8.648 1.688 0.451 0.025 0.183 0.626 0.177 32.652
PAN Limit (Ibs/acre) 1 st Crop. 237
Federal C.P.L.R. (Ibs/acre)'*** 36.6 1 34.8 T 1,339.0 267.9 i 15.0 I I 375.0 1 89.0 1 2,500.0
NCCLSL = NEWTON, NC CLARK CREEK LIME STABILIZED LIQUID
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am
aware that there are significant penalties for s ng false info ation, including the possibility of fines and imprisonment for knowing violations."AAI SIGNATURE OF LAN APPLIER DATE
NR = Not Reported or Not Required *** Mineralization Rates: Compost-0.1, Anaerobically digested-0.2, Aerobically digested-0.3, Raw Sludge-0.4
* Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation **** C.P.L.R.: Cumulative Pollutant Loading Rate
** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 *`*** See Site pH & Lime Application Records Section of Report
Printed: 1/24/2024 DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Total Dry Tons Applied (Annual):
Facility Name: NEWTON, NC 27.53
Permit #: W00003902 Cation Exchange Capacity (non 503 only):
Operator: RONNIE SIGMON RONNIE SIGMON Predominant Soil Series: APPLING
Owner:
Acres Used: 7.40 Acres Permitted: 7.40 Site #: Field #: NC CA 00032 0002
NC CA 00032
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Source
NCCLSL
Sample or
Composite
Date
1
10/03/23
2
3
4
5
6
7
8
9
10
11
12
Solids
7.86
Arsenic
6.330
Cadmium
1.270
Copper
142
Chromium
30.40
Lead
8.23
Mercury
2.150
Molybdenum
4.66
Nickel
12.10
Selenium
6.33
Zinc
622
Total Phosphorus
10200
Annual Heavy Metal Field Loadings (Calculated in Ibs/acre):
Source
NCCLSL
Total DT/Ac.
/App.Event
1
3.72
2
3
4
5
6
7
8
9
10
11
12
Totals
Arsenic
0.047
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.047
Cadmium
0.009
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.009
Copper
1.057
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1.057
Chromium
0.226
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.226
Lead
0.061
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.061
Mercury
0.016
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.016
Molybdenum
0.035
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.035
Nickel
0.090
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.090
Selenium
0.047
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.047
Zinc
4.628
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
4.628
Total Phosphorus
75.899
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
75.899
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that
there are significant Ities for submitting false information, including the possibility of fines and imprisonment for knowing violations".
Z-- & ✓2q
Signature of Land Applier r Date DENR FORM MFLSF (12/2006)

SECTION 4

SUMMIT
ENVIRONMENTAL TECHNOLOGIES, INC
Analytical Laboratories
January 24, 2023
Alex Fox
Synagro
284 Boger Rd.
Mocksville, NC 27028
TEL:
FAX:
RE: Newton
Dear Alex Fox:
Summit Environmental Technologies, Inc.
3310 Win St.
Cuyahoga Falls, Ohio 44223
TEL: [phone] FAX.- [phone]
Website: http:llwww.settek.com
Order No.: 23010834
Summit Environmental Technologies, Inc. received 1 sample(s) on 1/13/2023 for the
analyses presented in the following report.
There were no problems with the analytical events associated with this report unless noted
in the Case Narrative.
Quality control data is within laboratory defined or method specified acceptance limits
except where noted.
If you have any questions regarding these tests results, please feel free to call the
laboratory.
Sincerely,
i 7,
Jennifer Woolf
Project Manager
3310 Win St.
Cuyahoga Falls, Ohio 44223
Arkansas 88-0735, California 2943, Colorado, Connecticut PH-0108, Florida NELAC E87688, Idaho OH00923, Illinois 200061, Indiana C-OH-13,
ISO/IEC 17025:2017 119125 L22-544, Kansas E-10347, Kentucky (Underground Storage Tank) 3, Kentucky 90146, Maryland 339, Michigan 9988,
Minnesota 1780279, Nevada 011009232020-1, New Hampshire 2996, New Jersey OH006, New York 11777, North Carolina 39705 and 631, North Dakota
R-201, Ohio DW, Ohio VAP C1,0052, Oklahoma 2019-155, Oregon OH2O0001, Pennsylvania 68-01335, Rhode Island LA000317, South Carolina
92016001, Texas T104704466-19-16, Utah OH009232020-12, Virginia VELAP 10381, West Virginia 9957C
Page 1 of 39

summly Summit Environmental Technologies, Inc. Case Narrative
3310 Win St.
ENVIRONMENTAL TECHNOLOGIES, INC. Cuyahoga Falls, Ohio 44223 wo#: 23010834
Analytical Laboratories TEL: [phone] FAX.- [phone]
Website: http://www.settek.com Date: 1/24/2023
CLIENT: Synagro
Project: Newton
WorkOrder Narrative:
23010834: This report in its entirety consists of the following documents: Cover Letter, Case Narrative,
Analytical Results, QC Summary Report, Applicable Accreditation Information, Chain -of -Custody,
Cooler Receipt Form, and other applicable forms as necessary. All documents contain the Summit
Environmental Technologies, Inc., Work Order Number assigned to this report.
Summit Environmental Technologies, Inc., holds the accreditations/certifications listed at the bottom of
the cover letter that may or may not pertain to this report. Please refer to the "Accreditation Program
Analytes Report" for accredited analytes list.
The information contained in this analytical report is the sole property of Summit Environmental
Technologies, Inc. and that of the customer. It cannot be reproduced in any form without the consent of
Summit Environmental Technologies, Inc. or the customer for which this report was issued. The results
contained in this report are only representative of the samples received. Conditions can vary at different
times and at different sampling conditions. Summit Environmental Technologies, Inc. is not responsible
for use or interpretation of the data included herein.
All results for Solid Samples are reported on an "as received" or "wet weight" basis unless indicated as
"dry weight" using the "-dry" designation on the reporting units.
This report is believed to meet all of the requirements of the accrediting agency, where applicable. Any
comments or problems with the analytical events associated with this report are noted below.
Analytical Sequence Sample Notes:
23010834-OOIA TCLP-VOC-MSTR_8260D: CCV and LCS-R156775 exhibited high recoveries for
Vinyl chloride, Carbon tetrachloride, and Trichloroethene. Sample is ND for these analyzes. Possible
low bias for 1, 1 -Dichloroethene due to low recovery in CCV. Compound demostrates adequate
instrument sensitivity in RLC. Sample is ND for 1, 1 -Dichloroethene.
Analytical Sequence QC Notes:
MBLK VOC-MSTR_NPW(8260): Possible low bias for 1, 1 -Dichloroethene due to low recovery in
CCV. Compound demostrates adequate instrument sensitivity in RLC.
23010834-OOIAMS/MSD TCLP-VOC-MSTR_8260D: Possible high bias for Vinyl chloride, Carbon
tetrachloride, and Trichloroethene due to high recoveries in CCV and LCS-R156775. Parent sample is
Original
Page 2 of 39

summly Summit Environmental Technologies, Inc. Case Narrative
3310 Win St.
ENVIRONMENTAL TECHNOLOGIES, INC. Cuyahoga Falls, Ohio 44223 wo#: 23010834
Analytical Laboratories TEL: [phone] FAX.- [phone]
Website: http://www.settek.com Date: 1/24/2023
CLIENT: Synagro
Project: Newton
ND for these analytes. Possible low bias for 1, 1 -Dichloroethene due to low recovery in CCV.
Compound demostrates adequate instrument sensitivity in RLC.
LCS VOC-MSTR_NPW(8260): LCS-R156775 exhibited high recoveries for for Vinyl chloride, Carbon
tetrachloride, and Trichloroethene. Associated samples are ND for these analytes. Possible high bias
for Vinyl chloride due to high recovery in CCV. Possible low bias for 1, 1 -Dichloroethene due to low
recovery in CCV. Compound demostrates adequate instrument sensitivity in RLC.
Original
Page 3 of 39

SUMMIT Summit Environmental Technologies, In Qualifiers and Acronyms
3310 Win,'
ENVIRONMENTAL TECHNOLOGIES, INC Cuyahoga Falls, Ohio 442, WO#: 23010834
Analytical Laboratories TEL: [phone] FAX.- (330) 253-44E
Website: httv:11Www.settek.co Date: 1/24/2023
These commonly used Qualifiers and Acronyms may or may not be present in this report.
Qualifiers
U The compound was analyzed for but was not detected.
J The reported value is greater than the Method Detection Limit but less than the Reporting Limit.
H The hold time for sample preparation and/or analysis was exceeded.
D The result is reported from a dilution.
E The result exceeded the linear range of the calibration or is estimated due to interference.
MC The result is below the Minimum Compound Limit.
* The result exceeds the Regulatory Limit or Maximum Contamination Limit.
m Manual integration was used to determine the area response.
d Manual integration in which peak was deleted
N The result is presumptive based on a Mass Spectral library search assuming a 1:1 response.
P The second column confirmation exceeded 25% difference.
C The result has been confirmed by GC/MS.
X The result was not confirmed when GUMS Analysis was performed.
B/MB+ The analyte was detected in the associated blank.
G The ICB or CCB contained reportable amounts of analyte.
QC-/+ The CCV recovery failed low (-) or high (+).
R/QDR The RPD was outside of accepted recovery limits.
QL-/+ The LCS or LCSD recovery failed low (-) or high (+).
QLR The LCS/LCSD RPD was outside of accepted recovery limits.
QM-/+ The MS or MSD recovery failed low (-) or high (+).
QMR The MS/MSD RPD was outside of accepted recovery limits.
QV-/+ The ICV recovery failed low (-) or high (+).
S The spike result was outside of accepted recovery limits.
Z Deviation; A deviation from the method was performed; Please refer to the Case Narrative for
additional information
Acronyms
ND
Not Detected
RL
Reporting Limit
QC
Quality Control
MDL
Method Detection Limit
NIB
Method Blank
LOD
Level of Detection
LCS
Laboratory Control Sample
LOQ
Level of Quantitation
LCSD
Laboratory Control Sample Duplicate
PQL
Practical Quantitation Limit
QCS
Quality Control Sample
CRQL
Contract Required Quantitation Limit
DUP
Duplicate
PL
Permit Limit
MS
Matrix Spike
RegLvl
Regulatory Limit
MSD
Matrix Spike Duplicate
MCL
Maximum Contamination Limit
RPD
Relative Percent Different
MinCL
Minimum Compound Limit
ICV
Initial Calibration Verification
RA
Reanalysis
ICB
Initial Calibration Blank
RE
Reextraction
CCV
Continuing Calibration Verification
TIC
Tentatively Identified Compound
CCB
Continuing Calibration Blank
RT
Retention Time
RLC
Reporting Limit Check
CF
Calibration Factor
DF
Dilution Factor
RF
Response Factor
This list of Qualifiers and Acronyms reflects the most commonly utilized Qualifiers and Acronyms for reporting.
Please refer to the Analytical Notes in the Case Narrative for any Qualifiers or Acronyms that do not appear in this
list or for additional information regarding the use of these Qualifiers on reported data.
Original
Page 4 of 39

SUMMIT Summit Environmental Technologies, Inc.
3310 Win St.
ENVIRONMENTAL TECHNOLOGIES, INC Cuyahoga Falls, Ohio 44223
Analytical Laboratories TEL: [phone] FAX.- [phone]
Website: http://www.settek.com
CLIENT: Synagro
Project: Newton
Lab SampleID Client Sample ID
23010834-001 Newton
Tag No Date Collected
1/12/2023 8:00:00 AM
Workorder
Sample Summary
Wo#: 23010834
Date Received
1/13/2023 10:20:00 AM
24-Jan-23
Matrix
Solid
Page 5 of 39

SUMMIT
Summit Environmental Technologies, Inc.
3310 Win St.
DATES REPORT
ENVIRONMENTAL TECHNOLOGIES, INC
Cuyahoga Falls, Ohio 44223
WO#: 23010834
Analytical Laboratories
TEL: [phone] FAX.- [phone]
Website: http://www.settek.com
24-Jan-23
Client:
Synagro
Project:
Newton
Sample ID
Client Sample ID Collection Date Matrix Test Name Leachate Date
Prep Date Analysis Date
23010834-OOIA Newton 1/12/2023 8:00:00 AM Solid Ignitability of Solids (SW-846: 1030)
1/18/2023 7:17:11 PM
pH (SW9045D)
1/20/2023 4:11:32 PM
Reactive Cyanide (9014/7.3.3.2)-Solid
1/23/2023 1:45:00 PM
Reactive Sulfide (9034)/7.3.4.2
1/23/2023 1:45:00 PM
TCLP Herbicides by EPA 8321B
1/17/2023 4:07:00 PM
TCLP Mercury Analysis (SW1311/7471/16/2023 2:00:00 PM
1/17/2023 1:30:00 PM 1/18/2023 1:03:00 PM
TCLP Metals Analysis (SW1311/6010'1/16/2023 2:00:00 PM
1/17/2023 1:00:00 PM 1/18/2023 1:09:00 PM
TCLP Pesticides Analysis (SW1311/8(1/16/2023 2:00:00 PM
1/18/2023 10:31:44 AM 1/19/2023 12:24:00 AM
TCLP Pesticides Analysis (SW1311/8(1/16/2023 2:00:00 PM
1/18/2023 10:31:44 AM 1/19/2023 12:24:00 AM
TCLP Semi-Volatiles Analysis 1/16/2023 2:00:00 PM
1/17/2023 11:20:00 AM 1/18/2023 3:15:00 AM
(SW1311/8270)
TCLP Volatiles Analysis
1/19/2023 3:35:00 PM
Original
Page 6 of 39

SUMMIT
Summit Environmental Technologies, Inc. Analytical Report
3310 Win St.
ENVIRONMENTAL TECHNOLOGIES, INC Cuyahoga Falls, Ohio 44223 (base report)
Analytical Laboratories TEL: [phone] FAX: [phone] WO#: 23010834
Website: htW.-Ilwww.settek.com Date Reported: 1/24/2023
CLIENT: Synagro Tag Number:
Matrix: SOLID Collection Date: 1/12/2023 8:00:00 AM
Lab ID: 23010834-001A
Project: Newton
Client Sample ID Newton
Analyses Result
RL
Qual Units
DF
Date Analyzed
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
SW7470A
SW7470A
Analyst: JJF
TCLP MERCURY ANALYSIS (SW1311/7470)
TCLP Mercury
ND
0.00200
mg/L
1
1/18/2023 1:03:00 PM
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
SW6010
SW3010A
Analyst: RJE
TCLP METALS ANALYSIS (SW1311/6010)
TCLP Arsenic(As)
ND
0.500
mg/L
1
1/18/2023 1:09:00 PM
TCLP Barium(Ba)
ND
5.00
mg/L
1
1/18/2023 1:09:00 PM
TCLP Cadmium(Cd)
ND
0.100
mg/L
1
1/18/2023 1:09:00 PM
TCLP Chromium(Cr)
ND
0.200
mg/L
1
1/18/2023 1:09:00 PM
TCLP Lead(Pb)
ND
0.500
mg/L
1
1/18/2023 1:09:00 PM
TCLP Selenium(Se)
ND
0.0500
mg/L
1
1/18/2023 1:09:00 PM
TCLP Silver(Ag)
ND
0.500
mg/L
1
1/18/2023 1:09:00 PM
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
SW8270
SW3510C
Analyst: JAP
TCLP SEMI-VOLATILES ANALYSIS (SW1311/8270)
1,4-Dichlorobenzene
ND
0.100
mg/L
1
1/18/2023 3:15:00 AM
2,4,5-Trichlorophenol
ND
0.250
mg/L
1
1/18/2023 3:15:00 AM
2,4,6-Trichlorophenol
ND
0.250
mg/L
1
1/18/2023 3:15:00 AM
2,4-Dinitrotoluene
ND
0.0500
mg/L
1
1/18/2023 3:15:00 AM
Cresols, Total
ND
5.00
mg/L
1
1/18/2023 3:15:00 AM
Hexachloro-1,3-butadiene
ND
0.0200
mg/L
1
1/18/2023 3:15:00 AM
Hexachlorobenzene
ND
0.0500
mg/L
1
1/18/2023 3:15:00 AM
Hexachloroethane
ND
0.100
mg/L
1
1/18/2023 3:15:00 AM
Nitrobenzene
ND
0.100
mg/L
1
1/18/2023 3:15:00 AM
Pentachlorophenol
ND
0.250
mg/L
1
1/18/2023 3:15:00 AM
Pyridine
ND
0.250
mg/L
1
1/18/2023 3:15:00 AM
Surr: 2-Fluorophenol
54.5
10 - 157
%Rec
1
1/18/2023 3:15:00 AM
Surr: Phenol-d6
58.4
10 - 169
%Rec
1
1/18/2023 3:15:00 AM
Surr: Nitrobenzene-d5
55.6
32.1 - 130
%Rec
1
1/18/2023 3:15:00 AM
Surr: 2,4,6-Tribromophenol
76.4
45.4 - 166
%Rec
1
1/18/2023 3:15:00 AM
Surr: 2-Fluorobiphenyl
59.8
35.7 - 130
%Rec
1
1/18/2023 3:15:00 AM
Surr: p-Terphenyl-d14
87.2
70 - 145
%Rec
1
1/18/2023 3:15:00 AM
Qualifiers: B
Analyte detected in the associated Method Blank
H
Holding times for preparation or analysis exceeded
MC
Value is below Minimum Compound Limit.
ND
Not Detected
P
Second column confirmation exceeds
R
RPD outside accepted recovery limits
E
M
N
OGl
PL
RL
Value above quantitation range
Manual Integration used to determine area response
Tentatively identified compounds
Permit Limit
Reporting Detection Limit
Original
Page 7 of 39

SUMMIT Summit Environmental Technologies, Inc.
3310 Win St.
ENVIRONMENTAL TECHNOLOGIES, INC Cuyahoga Falls, Ohio 44223
Analytical Laboratories TEL: [phone] FAX: [phone]
Website: htW.-Ilwww.settek.com
CLIENT:
Synagro
Matrix:
SOLID
Lab ID:
23010834-001A
Project:
Newton
Client Sample ID Newton
Analytical Report
(base report)
WO#: 23010834
Date Reported: 1/24/2023
Tag Number:
Collection Date: 1/12/2023 8:00:00 AM
Analyses
Result
RL
Qual
Units
DF
Date Analyzed
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
SW8081
SW3510C
Analyst: PGP
TCLP PESTICIDES ANALYSIS (SW1311/8081)
Chlordane, total
ND
0.00250
mg/L
1
1/19/2023 12:24:00 AM
Toxaphene
ND
0.00500
mg/L
1
1/19/2023 12:24:00 AM
Endrin
ND
0.000500
mg/L
1
1/19/2023 12:24:00 AM
gamma-BHC
ND
0.000500
mg/L
1
1/19/2023 12:24:00 AM
Heptachlor
ND
0.000500
mg/L
1
1/19/2023 12:24:00 AM
Heptachlor epoxide
ND
0.000500
mg/L
1
1/19/2023 12:24:00 AM
Methoxychlor
ND
0.000500
mg/L
1
1/19/2023 12:24:00 AM
Surr: TCMX
58.0
10 - 119
%Rec
1
1/19/2023 12:24:00 AM
Surr: DCB
58.8
10 - 119
%Rec
1
1/19/2023 12:24:00 AM
TCLP HERBICIDES BY EPA 8321 B
SW8321
Analyst: SRA
2,4-D
ND
0.500
mg/L
50
1/17/20234:07:00 PM
2,4,5-TP
ND
0.500
mg/L
50
1/17/20234:07:00 PM
Surr: 2,4-Dichlorophenylacetic aci
98.5
70 - 130
%Rec
50
1/17/2023 4:07:00 PM
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
SW8260
Analyst: EMB
TCLP VOLATILES ANALYSIS
1,1-Dichloroethene
ND
0.100
QC-
mg/L
20
1/19/2023 3:35:00 PM
1,2-Dichloroethane
ND
0.100
mg/L
20
1/19/2023 3:35:00 PM
MEK
ND
2.00
mg/L
20
1/19/2023 3:35:00 PM
Benzene
ND
0.100
mg/L
20
1/19/2023 3:35:00 PM
Carbon tetrachloride
ND
0.100
QL+
mg/L
20
1/19/2023 3:35:00 PM
Chlorobenzene
ND
1.00
mg/L
20
1/19/2023 3:35:00 PM
Chloroform
ND
0.100
mg/L
20
1/19/2023 3:35:00 PM
Tetrachloroethene
ND
0.100
mg/L
20
1/19/2023 3:35:00 PM
Trichloroethene
ND
0.100
QL+
mg/L
20
1/19/2023 3:35:00 PM
Vinyl chloride
ND
0.0400 QC+QL+ mg/L
20
1/19/2023 3:35:00 PM
Surr: 4-Bromofluorobenzene
97.0
70 - 130
%Rec
20
1/19/2023 3:35:00 PM
Surr: Dibromofluoromethane
97.1
70 - 130
%Rec
20
1/19/2023 3:35:00 PM
Surr: Toluene-d8
106
70 - 130
%Rec
20
1/19/2023 3:35:00 PM
Qualifiers: B
Analyte detected in the associated Method Blank
H
Holding times for preparation or analysis exceeded
MC
Value is below Minimum Compound Limit.
ND
Not Detected
P
Second column confirmation exceeds
R
RPD outside accepted recovery limits
E
M
N
OGl
PL
RL
Value above quantitation range
Manual Integration used to determine area response
Tentatively identified compounds
Permit Limit
Reporting Detection Limit
Original
Page 8 of 39

SUMMIT Summit Environmental Technologies, Inc. Analytical Report
3310 Win St.
ENVIRONMENTAL TECHNOLOGIES, INC Cuyahoga Falls, Ohio 44223 (base report)
Analytical Laboratories TEL: [phone] FAX.- [phone] WO#: 23010834
Website: http://www.settek.com Date Reported: 1/24/2023
CLIENT: Synagro Tag Number:
Matrix: SOLID Collection Date: 1/12/2023 8:00:00 AM
Lab ID: 23010834-OOIA
Project: Newton
Client Sample ID Newton
Analyses Result RL Qual Units DF Date Analyzed
RCI SW9014 Analyst: MS
REACTIVE CYANIDE (9014/7.3.3.2)-SOLID
Cyanide, Reactive ND 0.495 mg/Kg 1 1/23/2023 1:45:00 PM
IGNITABILITY OF SOLIDS (SW-846: 1030) SW1030 Analyst: SMZ
Ignitability Non-flammable mm/sec 1 1/18/2023 7:17:11 PM
RCI SW9045D Analyst: SMZ
PH (SW9045D)
pH 11.8 s.u.@20.5C 1 1/20/2023 4:11:32 PM
RCI SW9034 Analyst: MS
REACTIVE SULFIDE (9034)/7.3.4.2
Sulfide, Reactive ND 25.0 mg/Kg 1 1/23/2023 1:45:00 PM
Qualifiers: B
Analyte detected in the associated Method Blank
H
Holding times for preparation or analysis exceeded
MC
Value is below Minimum Compound Limit.
ND
Not Detected
P
Second column confirmation exceeds
R
RPD outside accepted recovery limits
E Value above quantitation range
M Manual Integration used to determine area response
N Tentatively identified compounds
OGl
PL Permit Limit Original
RL Reporting Detection Limit
Page 9 of 39

Summit Environmental Technologies, Inc.
Accreditation
Program
3310 Win St.
SUMMIEF
Anal te5 Report
Y p
ENVIRONMENTAL TECHNOLOGIES,
INC Cuyahoga Falls, Ohio 44223
Analytical Laboratories
TEL: [phone] FAX.- [phone]
WO#:
23010834
Website: hgp:llwww.settek.com
24-Jan-23
Client: Synagro
State: NW
Project: Newton
Program Name: NC WW SCM
Sample ID Matrix
Test Name
Analyte
Status
23010834-OOIA Solid
Ignitability of Solids (SW-846: 1030)
Ignitability
A
Solid
pH (SW9045D)
Hydrogen Ion (pH)
A
Solid
Reactive Cyanide (9014/7.3.3.2)-Solid
Cyanide, Reactive
U
Solid
Reactive Sulfide (9034)/7.3.4.2
Sulfide, Reactive
U
Solid
TCLP Herbicides by EPA 8321B
2,4,5-TP
A
Solid
TCLP Herbicides by EPA 8321B
2,4-D
A
Solid
TCLP Mercury Analysis (SW1311/7470)
Mercury
A
Solid
TCLP Metals Analysis (SW1311/6010)
Arsenic
A
Solid
TCLP Metals Analysis (SW1311/6010)
Barium
A
Solid
TCLP Metals Analysis (SW1311/6010)
Cadmium
A
Solid
TCLP Metals Analysis (SW1311/6010)
Chromium
A
Solid
TCLP Metals Analysis (SW1311/6010)
Lead
A
Solid
TCLP Metals Analysis (SW1311/6010)
Selenium
A
Solid
TCLP Metals Analysis (SW1311/6010)
Silver
A
Solid
TCLP Pesticides Analysis (SW1311/8081)
Chlordane, total
A
Solid
TCLP Pesticides Analysis (SW1311/8081)
Endrin
A
Solid
TCLP Pesticides Analysis (SW1311/8081)
gamma-BHC
A
Solid
TCLP Pesticides Analysis (SW1311/8081)
Heptachlor
A
Solid
TCLP Pesticides Analysis (SW1311/8081)
Heptachlor epoxide
A
Solid
TCLP Pesticides Analysis (SW1311/8081)
Methoxychlor
A
Solid
TCLP Pesticides Analysis (SW1311/8081)
Toxaphene
A
Solid
TCLP Semi-Volatiles Analysis (SW1311/8270)
1,4-Dichlorobenzene
A
Solid
TCLP Semi-Volatiles Analysis (SW1311/8270)
2,4,5-Trichlorophenol
A
Solid
TCLP Semi-Volatiles Analysis (SW1311/8270)
2,4,6-Trichlorophenol
A
Solid
TCLP Semi-Volatiles Analysis (SW1311/8270)
2,4-Dinitrotoluene
A
Solid
TCLP Semi-Volatiles Analysis (SW1311/8270)
Cresols, Total
A
Solid
TCLP Semi-Volatiles Analysis (SW1311/8270)
Hexachlorobenzene
A
Solid
TCLP Semi-Volatiles Analysis (SW1311/8270)
Hexachlorobutadiene
A
Solid
TCLP Semi-Volatiles Analysis (SW1311/8270)
Hexachloroethane
A
Solid
TCLP Semi-Volatiles Analysis (SW1311/8270)
Nitrobenzene
A
Solid
TCLP Semi-Volatiles Analysis (SW1311/8270)
Pentachlorophenol
A
Solid
TCLP Semi-Volatiles Analysis (SW1311/8270)
Pyridine
A
Original #1
Page 10 of 39

Summit Environmental Technologies, Inc.
Accreditation
Program
3310 Win St.
SUMMIEF
Anal te5 Report
Y p
ENVIRONMENTAL TECHNOLOGIES,
INC Cuyahoga Falls, Ohio 44223
Analytical Laboratories
TEL: [phone] FAX.- [phone]
WO#:
23010834
Website: hgp:llwww.settek.com
24-Jan-23
Client: Synagro
State: NW
Project: Newton
Program Name: NC WW SCM
Sample ID Matrix
Test Name
Analyte
Status
23010834-OOIA Solid
TCLP Volatiles Analysis
1,1-Dichloroethene
A
Solid
TCLP Volatiles Analysis
1,2-Dichloroethane
A
Solid
TCLP Volatiles Analysis
2-Butanone
A
Solid
TCLP Volatiles Analysis
Benzene
A
Solid
TCLP Volatiles Analysis
Carbon tetrachloride
A
Solid
TCLP Volatiles Analysis
Chlorobenzene
A
Solid
TCLP Volatiles Analysis
Chloroform
A
Solid
TCLP Volatiles Analysis
Tetrachloroethene
A
Solid
TCLP Volatiles Analysis
Trichloroethene
A
Solid
TCLP Volatiles Analysis
Vinyl chloride
A
Original #1
Page 11 of 39

SUMMIT Summit Environmental Technologies, Inc.
3310 Win St.
ENVIRONMENTAL TECHNOLOGIES, INC Cuyahoga Falls, Ohio 44223
Analytical Laboratories TEL: [phone] FAX: [phone]
Website: http://www.settek.coni
Client: Synagro
Project: Newton
QC SUMMARY REPORT
BatchlD: 62252
WO#: 23010834
24-Jan-23
Sample ID: MB-62252
SampType: MBLK
TestCode: SVOC-BNA_T Units: mg/L
Prep Date: 1/17/2023
RunNo: 156649
3lient ID: PBS
Batch ID: 62252
TestNo: SW8270 SW3510C
Analysis Date: 1/17/2023
SegNo: 4170702
analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
1,4-Dichlorobenzene
ND
0.0250
2,4,5-Trichlorophenol
ND
0.0250
2,4,6-Trichlorophenol
ND
0.0250
2,4-Dinitrotoluene
ND
0.0250
o-Cresol
ND
0.250
Cresols, Total
ND
0.0500
Hexachloro-1,3-butadiene
ND
0.0250
Hexachlorobenzene
ND
0.0250
Hexachloroethane
ND
0.0250
Nitrobenzene
ND
0.0250
Pentachlorophenol
ND
0.0250
Pyridine
ND
0.0250
Surr: 2-Fluorophenol
0.426
Surr: Phenol-d6
0.526
Surr: Nitrobenzene-d5
0.431
Surr: 2,4,6-Tribromophenol
0.818
Surr: 2-Fluorobiphenyl
0.481
Surr: p-Terphenyl-d14
0.805
1.000
42.6
10
135
1.000
52.6
10
161
1.000
43.1
16.8
150
1.000
81.8
32.5
179
1.000
48.1
34
133
1.000
80.5
60.8
163
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal,
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected OGl P Second column confirmation exceeds Original
PL Permit Limit R RPD outside accepted recovery limits RL Reporting Detection Limit
Page 12 of 39

SUMMIT Summit Environmental Technologies, Inc.
3310 Win St.
ENVIRONMENTAL TECHNOLOGIES, INC Cuyahoga Falls, Ohio 44223
Analytical Laboratories TEL: [phone] FAX: [phone]
Website: http://www.settek.coni
Client: Synagro
Project: Newton
QC SUMMARY REPORT
BatchlD: 62252
WO#: 23010834
24-Jan-23
Sample ID: LCS-62252
SampType: LCS
TestCode: SVOC-BNA_T Units: mg/L
Prep Date: 1/17/2023
RunNo: 156649
client ID: LCSS
Batch ID: 62252
TestNo: SW8270 SW3510C
Analysis Date: 1/17/2023
SegNo: 4170703
4nalyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
1,4-Dichlorobenzene
0.297
0.0250
0.8000
0
37.1
35
130
2,4,5-Trichlorophenol
0.660
0.0250
0.8000
0
82.6
44
144
2,4,6-Trichlorophenol
0.671
0.0250
0.8000
0
83.9
45
141
2,4-Dinitrotoluene
0.679
0.0250
0.8000
0
84.9
56
136
o-Cresol
0.494
0.250
0.8000
0
61.7
36
134
Cresols, Total
1.03
0.0500
1.600
0
64.3
36
135
Hexachloro-1,3-butadiene
0.341
0.0250
0.8000
0
42.6
30
130
Hexachlorobenzene
0.620
0.0250
0.8000
0
77.5
58
130
Hexachloroethane
0.290
0.0250
0.8000
0
36.3
28
130
Nitrobenzene
0.432
0.0250
0.8000
0
54.0
39
133
Pentachlorophenol
0.606
0.0250
0.8000
0
75.8
33
151
Pyridine
0.265
0.0250
0.8000
0
33.1
10
130
Surr: 2-Fluorophenol
0.477
1.000
47.7
10
135
Surr: Phenol-d6
0.565
1.000
56.5
10
161
Surr: Nitrobenzene-d5
0.430
1.000
43.0
16.8
150
Surr:2,4,6-Tribromophenol
0.926
1.000
92.6
32.5
179
Surr:2-Fluorobiphenyl
0.532
1.000
53.2
34
133
Surr: p-Terphenyl-d14
0.756
1.000
75.6
60.8
163
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal,
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected OGl P Second column confirmation exceeds Original
PL Permit Limit R RPD outside accepted recovery limits RL Reporting Detection Limit
Page 13 of 39

SUMMIT Summit Environmental Technologies, Inc.
3310 Win St.
ENVIRONMENTAL TECHNOLOGIES, INC Cuyahoga Falls, Ohio 44223
Analytical Laboratories TEL: [phone] FAX: [phone]
Website: http://www.settek.coni
Client: Synagro
Project: Newton
QC SUMMARY REPORT
BatchlD: 62252
WO#: 23010834
24-Jan-23
Sample ID: 23010716-008AMS
SampType: MS
TestCode: SVOC-BNA_T Units: mg/L
Prep Date: 1/17/2023
RunNo: 156649
client ID: Batch=
Batch ID: 62252
TestNo: SW8270 SW3510C
Analysis Date: 1/17/2023
SegNo: 4170705
4nalyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
1,4-Dichlorobenzene
0.358
0.0250
0.8000
0
44.8
38.3
130
2,4,5-Trichlorophenol
0.638
0.0250
0.8000
0
79.8
43.9
157
2,4,6-Trichlorophenol
0.649
0.0250
0.8000
0
81.1
37.5
159
2,4-Dinitrotoluene
0.619
0.0250
0.8000
0
77.4
52.1
151
o-Cresol
0.531
0.250
0.8000
0
66.4
25.1
143
Cresols, Total
1.08
0.0500
1.600
0
67.8
10
184
Hexachloro-1,3-butadiene
0.407
0.0250
0.8000
0
50.8
36.2
130
Hexachlorobenzene
0.597
0.0250
0.8000
0
74.6
57.1
139
Hexachloroethane
0.350
0.0250
0.8000
0
43.8
30.4
130
Nitrobenzene
0.501
0.0250
0.8000
0
62.7
34
140
Pentachlorophenol
0.582
0.0250
0.8000
0
72.7
24.1
171
Pyridine
0.327
0.0250
0.8000
0
40.8
10
130
Surr: 2-Fluorophenol
0.531
1.000
53.1
10
135
Surr: Phenol-d6
0.598
1.000
59.8
10
161
Surr: Nitrobenzene-d5
0.470
1.000
47.0
16.8
150
Surr:2,4,6-Tribromophenol
0.805
1.000
80.5
32.5
179
Surr:2-Fluorobiphenyl
0.537
1.000
53.7
34
133
Surr: p-Terphenyl-d14
0.711
1.000
71.1
60.8
163
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal,
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected OGl P Second column confirmation exceeds Original
PL Permit Limit R RPD outside accepted recovery limits RL Reporting Detection Limit
Page 14 of 39

SUMMIT Summit Environmental Technologies, Inc.
3310 Win St.
ENVIRONMENTAL TECHNOLOGIES, INC Cuyahoga Falls, Ohio 44223
Analytical Laboratories TEL: [phone] FAX: [phone]
Website: http://www.settek.coni
Client: Synagro
Project: Newton
QC SUMMARY REPORT
BatchlD: 62252
WO#: 23010834
24-Jan-23
Sample ID: 23010716-008AMSD
SampType: MSD
TestCode: SVOC-BNA_T Units: mg/L
Prep Date: 1/17/2023
RunNo: 156649
client ID: Batch=
Batch ID: 62252
TestNo: SW8270 SW3510C
Analysis Date: 1/17/2023
SegNo: 4170706
4nalyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
1,4-Dichlorobenzene
0.419
0.0250
0.8000
0
52.4
38.3
130
0.3580
15.7
30
2,4,5-Trichlorophenol
0.729
0.0250
0.8000
0
91.2
43.9
157
0.6382
13.3
30
2,4,6-Trichlorophenol
0.741
0.0250
0.8000
0
92.6
37.5
159
0.6486
13.3
30
2,4-Dinitrotoluene
0.756
0.0250
0.8000
0
94.5
52.1
151
0.6194
19.9
30
o-Cresol
0.592
0.250
0.8000
0
74.1
25.1
143
0.5312
10.9
30
Cresols, Total
1.22
0.0500
1.600
0
76.2
10
184
1.085
11.7
30
Hexachloro-1,3-butadiene
0.448
0.0250
0.8000
0
56.0
36.2
130
0.4066
9.60
30
Hexachlorobenzene
0.732
0.0250
0.8000
0
91.6
57.1
139
0.5968
20.4
30
Hexachloroethane
0.400
0.0250
0.8000
0
50.0
30.4
130
0.3504
13.3
30
Nitrobenzene
0.547
0.0250
0.8000
0
68.4
34
140
0.5012
8.74
30
Pentachlorophenol
0.756
0.0250
0.8000
0
94.5
24.1
171
0.5818
26.0
30
Pyridine
0.309
0.0250
0.8000
0
38.6
10
130
0.3266
5.60
30
Surr: 2-Fluorophenol
0.601
1.000
60.1
10
135
0
Surr: Phenol-d6
0.686
1.000
68.6
10
161
0
Surr: Nitrobenzene-d5
0.535
1.000
53.5
16.8
150
0
Surr:2,4,6-Tribromophenol
0.988
1.000
98.8
32.5
179
0
Surr:2-Fluorobiphenyl
0.615
1.000
61.5
34
133
0
Surr: p-Terphenyl-d14
0.834
1.000
83.4
60.8
163
0
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal,
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected OGl P Second column confirmation exceeds Original
PL Permit Limit R RPD outside accepted recovery limits RL Reporting Detection Limit
Page 15 of 39

SUMMIT Summit Environmental Technologies, Inc.
3310 Win St.
ENVIRONMENTAL TECHNOLOGIES, INC Cuyahoga Falls, Ohio 44223
Analytical Laboratories TEL: [phone] FAX: [phone]
Website: http://www.settek.coni
Client: Synagro
Project: Newton
QC SUMMARY REPORT
WO#: 23010834
24-Jan-23
BatchlD: 62265
Sample ID: MB-62265
SampType: MBLK
TestCode: Mtl-TCLP-7(6 Units: mg/L
Prep Date: 1/17/2023
RunNo: 156653
Client ID: PBS
Batch ID: 62265
TestNo: SW6010 SW3010A
Analysis Date: 1/18/2023
SegNo: 4170960
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
TCLP Arsenic(As)
ND
0.100
TCLP Barium(Ba)
ND
5.00
TCLP Cadmium(Cd)
ND
0.100
TCLP Chromium(Cr)
ND
0.200
TCLP Lead(Pb)
ND
0.100
TCLP Selenium(Se)
ND
0.100
TCLP Silver(Ag)
ND
0.100
Sample ID: LCS-62265
SampType: LCS
TestCode: Mtl-TCLP-7(6 Units: mg/L
Prep Date: 1/17/2023
RunNo: 156653
Client ID: LCSS
Batch ID: 62265
TestNo: SW6010 SW3010A
Analysis Date: 1/18/2023
SegNo: 4170964
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
TCLP Arsenic(As)
2.12
0.100
2.000
0
106
80
120
TCLP Barium(Ba)
ND
5.00
2.000
0
102
80
120
TCLP Cadmium(Cd)
2.03
0.100
2.000
0
101
80
120
TCLP Chromium(Cr)
2.10
0.200
2.000
0
105
80
120
TCLP Lead(Pb)
2.10
0.100
2.000
0
105
80
120
TCLP Selenium(Se)
1.92
0.100
2.000
0
96.2
80
120
TCLP Silver(Ag)
2.11
0.100
2.000
0
105
80
120
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal,
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected OGl P Second column confirmation exceeds Original
PL Permit Limit R RPD outside accepted recovery limits RL Reporting Detection Limit
Page 16 of 39

SUMMIT Summit Environmental Technologies, Inc.
3310 Win St.
ENVIRONMENTAL TECHNOLOGIES, INC Cuyahoga Falls, Ohio 44223
Analytical Laboratories TEL: [phone] FAX: [phone]
Website: http://www.settek.coni
Client: Synagro
Project: Newton
QC SUMMARY REPORT
WO#: 23010834
24-Jan-23
BatchlD: 62265
Sample ID: 23010805-001AMS
SampType: MS
TestCode: Mtl-TCLP-7(6 Units: mg/L
Prep Date: 1/17/2023
RunNo: 156653
Client ID: Batch=
Batch ID: 62265
TestNo: SW6010 SW3010A
Analysis Date: 1/18/2023
SegNo: 4170970
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
TCLP Arsenic(As)
2.00
0.100
2.000
0
99.9
70
130
TCLP Barium(Ba)
ND
5.00
2.000
0.5863
76.0
70
130
TCLP Cadmium(Cd)
1.78
0.100
2.000
0
89.0
70
130
TCLP Chromium(Cr)
1.84
0.200
2.000
0
92.0
70
130
TCLP Lead(Pb)
1.81
0.100
2.000
0
90.7
70
130
TCLP Selenium(Se)
1.90
0.100
2.000
0
94.9
70
130
TCLP Silver(Ag)
1.99
0.100
2.000
0
99.4
70
130
Sample ID: 23010805-001AMSD
SampType: MSD
TestCode: Mtl-TCLP-7(6 Units: mg/L
Prep Date: 1/17/2023
RunNo: 156653
Client ID: Batch=
Batch ID: 62265
TestNo: SW6010 SW3010A
Analysis Date: 1/18/2023
SegNo: 4170971
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
TCLP Arsenic(As)
1.99
0.100
2.000
0
99.7
70
130
1.997
0.150
20
TCLP Barium(Ba)
ND
5.00
2.000
0.5863
76.8
70
130
0
0
20
TCLP Cadmium(Cd)
1.76
0.100
2.000
0
88.1
70
130
1.780
1.04
20
TCLP Chromium(Cr)
1.82
0.200
2.000
0
91.1
70
130
1.841
1.05
20
TCLP Lead(Pb)
1.80
0.100
2.000
0
89.8
70
130
1.814
1.01
20
TCLP Selenium(Se)
1.89
0.100
2.000
0
94.4
70
130
1.899
0.523
20
TCLP Silver(Ag)
1.97
0.100
2.000
0
98.4
70
130
1.987
0.929
20
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal,
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected OGl P Second column confirmation exceeds Original
PL Permit Limit R RPD outside accepted recovery limits RL Reporting Detection Limit
Page 17 of 39

SUMMIT Summit Environmental Technologies, Inc.
3310 Win St.
ENVIRONMENTAL TECHNOLOGIES, INC Cuyahoga Falls, Ohio 44223
Analytical Laboratories TEL: [phone] FAX: [phone]
Website: http://www.settek.coni
QC SUMMARY REPORT
WO#: 23010834
24-Jan-23
Client: Synagro
Project: Newton BatchlD: 62271
TCLP Mercury ND 0.00200
TCLP Mercury 0.00403 0.00200 0.00400 0 101 80 120
TCLP Mercury 0.00444 0.00200 0.00400 0.0000260 110 75 125
Sample ID: 23010805-001AMSD
SampType: MSD
TestCode: HG_TCLP(74 Units: PPM
Prep Date: 1/17/2023
RunNo: 156669
Client ID: BatchQC
Batch ID: 62271
TestNo: SW7470A SW7470A
Analysis Date: 1/18/2023
SegNo: 4171496
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
TCLP Mercury 0.00405 0.00200
0.00400 0.0000260 101 75
125
0.00444 9.19 20
Qualifiers: B Analyte detected in the associated Method Blank
E Value above quantitation range
H
Holding times for preparation or anal,
J Analyte detected below quantitation limits
M Manual Integration used to determine area response
MC
Value is below Minimum Compound
Original
ND Not Detected
OGl
P
Second column confirmation exceeds
PL Permit Limit
R RPD outside accepted recovery limits
RL
Reporting Detection Limit
Page 18 of 39

SUMMIT Summit Environmental Technologies, Inc.
3310 Win St.
ENVIRONMENTAL TECHNOLOGIES, INC Cuyahoga Falls, Ohio 44223
Analytical Laboratories TEL: [phone] FAX.- [phone]
Website: hgp:llwww.settek.com
QC SUMMARY REPORT
Client: Synagro
Project: Newton BatchID: 62271
WO#: 23010834
24-Jan-23
Sample ID: 23010805-001AMSD
SampType: MSD
TestCode: HG_TCLP(74 Units: PPM
Prep Date: 1/17/2023
RunNo: 156669
Dient ID: BatchQC
Batch ID: 62271
TestNo: SW7470A SW7470A
Analysis Date: 1/18/2023
SegNo: 4171496
4nalyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal,
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected OGl P Second column confirmation exceeds Original
PL Permit Limit R RPD outside accepted recovery limits RL Reporting Detection Limit
Page 19 of 39

SUMMIT Summit Environmental Technologies, Inc.
3310 Win St.
ENVIRONMENTAL TECHNOLOGIES, INC Cuyahoga Falls, Ohio 44223
Analytical Laboratories TEL: [phone] FAX: [phone]
Website: http://www.settek.coni
Client: Synagro
Project: Newton
QC SUMMARY REPORT
WO#: 23010834
24-Jan-23
BatchlD: 62279
Sample ID: MB-62279
SampType: MBLK
TestCode: TCLP-SVOC- Units: mg/L
Prep Date: 1/18/2023
RunNo: 156731
Client ID: PBS
Batch ID: 62279
TestNo: SW8081 SW3510C
Analysis Date: 1/18/2023
SegNo: 4172749
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Chlordane, total
ND
0.00250
Toxaphene
ND
0.00500
Endrin
ND
0.000500
gamma-BHC
ND
0.000500
Heptachlor
ND
0.000500
Heptachlor epoxide
ND
0.000500
Methoxychlor
ND
0.000500
Sum TCMX
11.7
Sum DCB
11.6
20.00 58.4 10 119
20.00 57.8 10 119
d
d
d
d
d
Sample ID: LCS-62279
SampType: LCS
TestCode: TCLP-SVOC- Units: mg/L
Prep Date: 1/18/2023
RunNo: 156731
Client ID: LCSS
Batch ID: 62279
TestNo: SW8081 SW3510C
Analysis Date: 1/18/2023
SegNo: 4172750
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Chlordane, tota
Toxaphene
Endrin
gamma-BHC
Heptachlor
Heptachlor epo
Methoxychlor
Surr: TCMX
Qualifiers:
1 0.0183
0.0
ND
0.0
0.0108
0.00
0.00848
0.00
0.0103
0.00
xide 0.00917
0.00
0.0114
0.00
12.0
B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
PL Permit Limit
0250
0
0
70
0500
0
0
70
0500
0.0100 0
108
10
0500
0.0100 0
84.8
10
0500
0.0100 0
103
10
0500
0.0100 0
91.7
10
0500
0.0100 0
114
10
20.00
60.1
10
E Value above quantitation range
M Manual Integration used to determine area response
OGl
R RPD outside accepted recovery
limits
130
130
130
130
130
130
178
130
H Holding times for preparation or anal,
MC Value is below Minimum Compound
P Second column confirmation exceeds
RL Reporting Detection Limit
Original
Page 20 of 39

SUMMIT Summit Environmental Technologies, Inc.
3310 Win St.
ENVIRONMENTAL TECHNOLOGIES, INC Cuyahoga Falls, Ohio 44223
Analytical Laboratories TEL: [phone] FAX.- [phone]
Website: hgp:llwww.settek.com
QC SUMMARY REPORT
WO#: 23010834
24-Jan-23
Client: Synagro
Project: Newton BatchID: 62279
Sample ID: LCS-62279
SampType: LCS
TestCode: TCLP-SVOC- Units: mg/L
Prep Date: 1/18/2023
RunNo: 156731
:lient ID: LCSS
Batch ID: 62279
TestNo: SW8081 SW3510C
Analysis Date: 1/18/2023
SegNo: 4172750
analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
Surr: DCB
8.64
20.00
43.2 10 130
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal,
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected OGl P Second column confirmation exceeds Original
PL Permit Limit R RPD outside accepted recovery limits RL Reporting Detection Limit
Page 21 of 39

SUMMIT Summit Environmental Technologies, Inc.
3310 Win St.
ENVIRONMENTAL TECHNOLOGIES, INC Cuyahoga Falls, Ohio 44223
Analytical Laboratories TEL: [phone] FAX: [phone]
Website: http://www.settek.coni
Client: Synagro
Project: Newton
QC SUMMARY REPORT
WO#: 23010834
24-Jan-23
BatchlD: R156631
Sample ID: MB TCLP
SampType: MBLK
TestCode: TCLP-SVOC- Units: mg/L
Prep Date:
RunNo: 156631
Client ID: PBS
Batch ID: R156631
TestNo: SW8321
Analysis Date: 1/17/2023
SegNo: 4170271
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
2,4-D ND 0.0100
2,4,5-TP ND 0.0100
Sum 2,4-Dichlorophenylacetic acid 0.945 1.000 94.5 70 130
Sample ID: RLC TCLP
SampType: RLC
TestCode: TCLP-SVOC- Units: mg/L
Prep Date:
RunNo: 156631
Client ID: Batch=
Batch ID: R156631
TestNo: SW8321
Analysis Date: 1/17/2023
SegNo: 4170272
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
2,4-D
0.0195
0.0100 0.01000
0 195
50
150 S
2,4,5-TP
ND
0.0100 0.01000
0 83.0
50
150
Surr: 2,4-Dichlorophenylacetic acid
0.00850
0.01000
85.0
70
130
Sample ID: LCS TCLP 0.3 ppm
SampType: LCS
TestCode: TCLP-SVOC- Units: mg/L
Prep Date:
RunNo: 156631
Client ID: LCSS
Batch ID: R156631
TestNo: SW8321
Analysis Date: 1/17/2023
SegNo: 4170273
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
2,4-D 0.302 0.0100
0.3000 0 101 60.5
141
2,4,5-TP 0.287 0.0100
0.3000 0 95.7 68.3
144
Surr: 2,4-Dichlorophenylacetic acid 0.287
0.3000 95.5 70
130
Qualifiers: B Analyte detected in the associated Method Blank
E Value above quantitation range
H
Holding times for preparation or anal,
J Analyte detected below quantitation limits
M Manual Integration used to determine area response
MC
Value is below Minimum Compound
Original
ND Not Detected
OGl
P
Second column confirmation exceeds
PL Permit Limit
R RPD outside accepted recovery limits
RL
Reporting Detection Limit
Page 22 of 39

SUMMIT Summit Environmental Technologies, Inc.
3310 Win St.
ENVIRONMENTAL TECHNOLOGIES, INC Cuyahoga Falls, Ohio 44223
Analytical Laboratories TEL: [phone] FAX.- [phone]
Website: hgp:llwww.settek.com
QC SUMMARY REPORT
WO#: 23010834
24-Jan-23
Client: Synagro
Project: Newton BatchlD: R156631
Sample ID:
LCSD TCLP 0.3 ppm SampType: LCSD
TestCode: TCLP-SVOC- Units: mg/L
Prep Date:
RunNo: 156631
Client ID:
LCSS02 Batch ID: R156631
TestNo: SW8321
Analysis Date: 1/17/2023
SegNo: 4170274
Analyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
2,4-D 0.296 0.0100 0.3000 0 98.8 60.5 141 0.3023 2.00 30
2,4,5-TP 0.278 0.0100 0.3000 0 92.8 68.3 144 0.2872 3.08 30
Surr: 2,4-Dichlorophenylacetic acid 0.279 0.3000 93.1 70 130 0 0
Qualifiers: B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
PL Permit Limit
E Value above quantitation range
M Manual Integration used to determine area response
OGl
R RPD outside accepted recovery limits
Page 23 of 39
H Holding times for preparation or anal,
MC Value is below Minimum Compound
P Second column confirmation exceeds
RL Reporting Detection Limit
Original

SUMMIT Summit Environmental Technologies, Inc.
3310 Win St.
ENVIRONMENTAL TECHNOLOGIES, INC Cuyahoga Falls, Ohio 44223
Analytical Laboratories TEL: [phone] FAX.- [phone]
Website: hgp:llwww.settek.com
Client: Synagro
Project: Newton
QC SUMMARY REPORT
WO#: 23010834
24-Jan-23
BatchID: R156695
Sample ID: LCS-R156695
SampType: LCS
TestCode: Ignitability_S Units: mm/sec
Prep Date:
RunNo: 156695
Client ID: LCSS
Batch ID: R156695
TestNo: SW1030
Analysis Date: 1/18/2023
SegNo: 4171894
Analyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
Ignitability
7.69
7.240 0 106 70 130
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal,
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected OGl P Second column confirmation exceeds Original
PL Permit Limit R RPD outside accepted recovery limits RL Reporting Detection Limit
Page 24 of 39

SUMMIT Summit Environmental Technologies, Inc.
3310 Win St.
ENVIRONMENTAL TECHNOLOGIES, INC Cuyahoga Falls, Ohio 44223
Analytical Laboratories TEL: [phone] FAX: [phone]
Website: http://www.settek.coni
Client: Synagro
Project: Newton
QC SUMMARY REPORT
WO#: 23010834
24-Jan-23
BatchlD: R156775
Sample ID: MBLK
SampType: MBLK
TestCode: VOC-MSTR_ Units: mg/L
Prep Date:
RunNo: 156775
Client ID: PBW
Batch ID: R156775
TestNo: SW8260
Analysis Date: 1/19/2023
SegNo: 4173516
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
1,1-Dichloroethene
ND
0.00500 QC-
1,2-Dichloroethane
ND
0.00500
MEK
ND
0.0250
Benzene
ND
0.00500
Carbon tetrachloride
ND
0.00500
Chlorobenzene
ND
0.00500
Chloroform
ND
0.00500
Tetrachloroethene
ND
0.00500
Trichloroethene
ND
0.00500
Vinyl chloride
ND
0.00200 QC+
Sum 4-Bromofluorobenzene
49.6
50.00 99.3 70 130
Sum Dibromofluoromethane
49.6
50.00 99.2 70 130
Surr: Toluene-d8
50.2
50.00 100 70 130
Sample ID: LCS
SampType: LCS
TestCode: VOC-MSTR_ Units: mg/L
Prep Date:
RunNo: 156775
Client ID: LCSW
Batch ID: R156775
TestNo: SW8260
Analysis Date: 1/19/2023
SegNo: 4174204
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
1,1-Dichloroethene
0.0286
0.00500
0.0200 0 143
49
161
QC-
1,2-Dichloroethane
0.0271
0.00500
0.0200 0 135
48
151
MEK
0.0970
0.0250
0.100 0 97.0
10
190
Benzene
0.0275
0.00500
0.0200 0 138
34
169
Qualifiers: B
Analyte detected in the associated Method Blank
E Value above quantitation range
H
Holding times for preparation or anal,
J
Analyte detected below quantitation limits
M Manual Integration used to determine area response
MC
Value is below Minimum Compound
Original
ND
Not Detected
OGl
P
Second column confirmation exceeds
PL
Permit Limit
R RPD outside accepted recovery limits
RL
Reporting Detection Limit
Page 25 of 39

SUMMIT Summit Environmental Technologies, Inc.
3310 Win St.
ENVIRONMENTAL TECHNOLOGIES, INC Cuyahoga Falls, Ohio 44223
Analytical Laboratories TEL: [phone] FAX: [phone]
Website: http://www.settek.coni
Client: Synagro
Project: Newton
QC SUMMARY REPORT
WO#: 23010834
24-Jan-23
BatchlD: R156775
Sample ID: LCS
SampType: LCS
TestCode: VOC-MSTR_ Units: mg/L
Prep Date:
RunNo: 156775
Client ID: LCSW
Batch ID: R156775
TestNo: SW8260
Analysis Date: 1/19/2023
SegNo: 4174204
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
Carbon tetrachloride
0.0290
0.00500
0.0200
0
145
76
134 S
Chlorobenzene
0.0264
0.00500
0.0200
0
132
54
144
Chloroform
0.0258
0.00500
0.0200
0
129
70
130
Tetrachloroethene
0.0259
0.00500
0.0200
0
130
66
134
Trichloroethene
0.0285
0.00500
0.0200
0
142
70
136 S
Vinyl chloride
0.0339
0.00200
0.0200
0
170
49
136 SQC+
Sum 4-Bromofluorobenzene
49.7
50.00
99.4
70
130
Sum Dibromofluoromethane
51.0
50.00
102
70
130
Sum Toluene-d8
48.2
50.00
96.5
70
130
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal,
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected OGl P Second column confirmation exceeds Original
PL Permit Limit R RPD outside accepted recovery limits RL Reporting Detection Limit
Page 26 of 39

SUMMIT Summit Environmental Technologies, Inc.
3310 Win St.
ENVIRONMENTAL TECHNOLOGIES, INC Cuyahoga Falls, Ohio 44223
Analytical Laboratories TEL: [phone] FAX: [phone]
Website: http://www.settek.coni
Client: Synagro
Project: Newton
QC SUMMARY REPORT
WO#: 23010834
24-Jan-23
BatchlD: R156775
Sample ID: MBLK
SampType: MBLK
TestCode: TCLP-VOC-M Units: mg/L
Prep Date:
RunNo: 156775
Client ID: PBS
Batch ID: R156775
TestNo: SW8260
Analysis Date: 1/19/2023
SegNo: 4173517
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
1,1-Dichloroethene
ND
0.100 QC-
1,2-Dichloroethane
ND
0.100
MEK
ND
2.00
Benzene
ND
0.100
Carbon tetrachloride
ND
0.100
Chlorobenzene
ND
1.00
Chloroform
ND
0.100
Tetrachloroethene
ND
0.100
Trichloroethene
ND
0.100
Vinyl chloride
ND
0.0400 QC+
Sum 4-Bromofluorobenzene
1000
1000 100 70 130
Sum Dibromofluoromethane
980
1000 98.0 70 130
Surr: Toluene-d8
1020
1000 102 70 130
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal,
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected OGl P Second column confirmation exceeds Original
PL Permit Limit R RPD outside accepted recovery limits RL Reporting Detection Limit
Page 27 of 39

SUMMIT Summit Environmental Technologies, Inc.
3310 Win St.
ENVIRONMENTAL TECHNOLOGIES, INC Cuyahoga Falls, Ohio 44223
Analytical Laboratories TEL: [phone] FAX: [phone]
Website: http://www.settek.coni
Client: Synagro
Project: Newton
QC SUMMARY REPORT
WO#: 23010834
24-Jan-23
BatchlD: R156775
Sample ID: 23010834-001AMS
SampType: MS
TestCode: TCLP-VOC-M Units: mg/L
Prep Date:
RunNo: 156775
Client ID: Newton
Batch ID: R156775
TestNo: SW8260
Analysis Date: 1/19/2023
SegNo: 4173523
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
1,1-Dichloroethene
0.599
0.100
0.400
0
150
13.6
202
1,2-Dichloroethane
0.495
0.100
0.400
0
124
55.7
138
MEK
2.08
2.00
2.00
0
104
65.3
118
Benzene
0.559
0.100
0.400
0
140
49.2
145
Carbon tetrachloride
0.486
0.100
0.400
0
121
26.7
156
Chlorobenzene
ND
1.00
0.400
0
126
33.7
159
Chloroform
0.499
0.100
0.400
0
125
48.5
145
Tetrachloroethene
0.469
0.100
0.400
0
117
19.2
191
Trichloroethene
0.471
0.100
0.400
0
118
38.4
167
Vinyl chloride
0.620
0.0400
0.400
0
155
27.3
161
Sum 4-Bromofluorobenzene
986
1000
98.6
91.7
109
Sum Dibromofluoromethane
957
1000
95.7
75.5
118
Surr: Toluene-d8
1050
1000
105
94.1
105
QC-
QL+
QL+
QL+QC+
S
Sample ID: 23010834-001AMSD
SampType: MSD
TestCode: TCLP-VOC-M Units: mg/L
Prep Date:
RunNo: 156775
Client ID: Newton
Batch ID: R156775
TestNo: SW8260
Analysis Date: 1/19/2023
SegNo: 4173524
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
1,1-Dichloroethene
0.537 0.100
0.400 0 134
13.6
202
0.599 10.9
25 QC-
1,2-Dichloroethane
0.469 0.100
0.400 0 117
55.7
138
0.495 5.48
25
MEK
2.21 2.00
2.00 0 110
65.3
118
2.08 5.84
25
Benzene
0.499 0.100
0.400 0 125
49.2
145
0.559 11.4
25
Qualifiers: B
Analyte detected in the associated Method Blank
E
Value above quantitation range
H
Holding times for preparation or anal,
J
Analyte detected below quantitation limits
M
Manual Integration used to determine area
response
MC
Value is below Minimum Compound
Original
ND
Not Detected
OGl
P
Second column confirmation exceeds
PL
Permit Limit
R
RPD outside accepted recovery limits
RL
Reporting Detection Limit
Page 28 of 39

SUMMIT Summit Environmental Technologies, Inc.
3310 Win St.
ENVIRONMENTAL TECHNOLOGIES, INC Cuyahoga Falls, Ohio 44223
Analytical Laboratories TEL: [phone] FAX: [phone]
Website: http://www.settek.coni
Client: Synagro
Project: Newton
QC SUMMARY REPORT
WO#: 23010834
24-Jan-23
BatchlD: R156775
Sample ID: 23010834-001AMSD
SampType: MSD
TestCode: TCLP-VOC-M Units: mg/L
Prep Date:
RunNo: 156775
Client ID: Newton
Batch ID: R156775
TestNo: SW8260
Analysis Date: 1/19/2023
SegNo: 4173524
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
Carbon tetrachloride
0.434
0.100
0.400
0
109
26.7
156
0.486
11.2
25 QL+
Chlorobenzene
ND
1.00
0.400
0
109
33.7
159
0
0
25
Chloroform
0.454
0.100
0.400
0
114
48.5
145
0.499
9.36
25
Tetrachloroethene
0.405
0.100
0.400
0
101
19.2
191
0.469
14.7
25
Trichloroethene
0.423
0.100
0.400
0
106
38.4
167
0.471
10.6
25 QL+
Vinyl chloride
0.583
0.0400
0.400
0
146
27.3
161
0.620
6.28
25 QL+QC+
Sum 4-Bromofluorobenzene
981
1000
98.1
91.7
109
0
25
Sum Dibromofluoromethane
990
1000
99.0
75.5
118
0
25
Sum Toluene-d8
1030
1000
103
94.1
105
0
25
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal,
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected OGl P Second column confirmation exceeds Original
PL Permit Limit R RPD outside accepted recovery limits RL Reporting Detection Limit
Page 29 of 39

SUMMIT Summit Environmental Technologies, Inc
3310 Win St
ENVIRONMENTAL TECHNOLOGIES, INC Cuyahoga Falls, Ohio 44223
Analytical Laboratories TEL: [phone] FAX: [phone]
Website: http://www.settek.coni
Client: Synagro
Project: Newton
QC SUMMARY REPORT
WO#: 23010834
24-Jan-23
BatchlD: R156838
pH 7.0 7.0 0 100 90 110
pH 12.5 0 0 0 0 12.5 0.2 10
pH 7.0 7.0 0 100 90 110
Sample ID: 23011173-001ADUP
SampType: DUP
TestCode: pH_S(9045D) Units: s.u.@20.5C
Prep Date:
RunNo: 156838
Client ID: BatchQC
Batch ID: R156838
TestNo: SW9045D
Analysis Date: 1/20/2023
SegNo: 4175312
Analyte
Result
PQL SPK value SPK Ref Val %REC
Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
pH 6.5 0 0 0 0 6.4 0.6 10
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal,
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected OGl P Second column confirmation exceeds Original
PL Permit Limit R RPD outside accepted recovery limits RL Reporting Detection Limit
Page 30 of 39

SUMMIT Summit Environmental Technologies, Inc.
3310 Win St.
ENVIRONMENTAL TECHNOLOGIES, INC Cuyahoga Falls, Ohio 44223
Analytical Laboratories TEL: [phone] FAX: [phone]
Website: http://www.settek.coni
Client: Synagro
Project: Newton
QC SUMMARY REPORT
WO#: 23010834
24-Jan-23
BatchlD: R156838
Sample ID: 23011173-001ADUP
SampType: DUP
TestCode: pH_S(9045D) Units: s.u.@20.5C
Prep Date:
RunNo: 156838
Client ID: Batch=
Batch ID: R156838
TestNo: SW9045D
Analysis Date: 1/20/2023
SegNo: 4175312
Analyte
Result
PQL SPK value SPK Ref Val %REC
Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Sample ID: LCS-R156838
SampType: LCS
TestCode: pH_S(9045D) Units: s.u.@20.4C
Prep Date:
RunNo: 156838
Client ID: LCSS
Batch ID: R156838
TestNo: SW9045D
Analysis Date: 1/20/2023
SegNo: 4175319
Analyte
Result
PQL SPK value SPK Ref Val %REC
Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
pH 7.0 7.0 0 100 90 110
Sample ID: 23011209-007ADUP
SampType: DUP
TestCode: pH_S(9045D) Units: s.u.@21.1C
Prep Date:
RunNo: 156838
Client ID: BatchQC
Batch ID: R156838
TestNo: SW9045D
Analysis Date: 1/20/2023
SegNo: 4175324
Analyte
Result
PQL SPK value SPK Ref Val %REC
Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
pH 7.6 0 0 0 0 7.6 0 10
Sample ID: LCS-R156838
SampType: LCS
TestCode: pH_S(9045D) Units: s.u.@20.5C
Prep Date:
RunNo: 156838
Client ID: LCSS
Batch ID: R156838
TestNo: SW9045D
Analysis Date: 1/20/2023
SegNo: 4175326
Analyte
Result
PQL SPK value SPK Ref Val %REC
Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
pH 7.0
7.0 0 101 90
110
Qualifiers: B Analyte detected in the associated Method Blank
E Value above quantitation range
H
Holding times for preparation or anal,
J Analyte detected below quantitation limits
M Manual Integration used to determine area response
MC
Value is below Minimum Compound
Original
ND Not Detected
OGl
P
Second column confirmation exceeds
PL Permit Limit
R RPD outside accepted recovery limits
RL
Reporting Detection Limit
Page 31 of 39

SUMMIT Summit Environmental Technologies, Inc.
3310 Win St.
ENVIRONMENTAL TECHNOLOGIES, INC Cuyahoga Falls, Ohio 44223
Analytical Laboratories TEL: [phone] FAX: [phone]
Website: http://www.settek.coni
QC SUMMARY REPORT
WO#: 23010834
24-Jan-23
Client: Synagro
Project: Newton BatchlD: R156838
pH 7.0 7.0 0 100 98.6 101.4
pH 6.9 6.9 0.4 5 H
pH 7.0 7.0 0 100 98.6 101.4
Sample ID: 23010912-001ADUP
SampType: DUP
TestCode: pH_NPW(450 Units: s.u.@19.7C
Prep Date:
RunNo: 156838
Client ID: BatchQC
Batch ID: R156838
TestNo: SW9045D
Analysis Date: 1/20/2023
SegNo: 4175285
Analyte
Result
PQL SPK value SPK Ref Val %REC
Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
pH 6.3 6.3 0.5 5 H
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal,
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected OGl P Second column confirmation exceeds Original
PL Permit Limit R RPD outside accepted recovery limits RL Reporting Detection Limit
Page 32 of 39

SUMMIT Summit Environmental Technologies, Inc.
3310 Win St.
ENVIRONMENTAL TECHNOLOGIES, INC Cuyahoga Falls, Ohio 44223
Analytical Laboratories TEL: [phone] FAX.- [phone]
Website: hgp:llwww.settek.com
QC SUMMARY REPORT
WO#: 23010834
24-Jan-23
Client: Synagro
Project: Newton BatchID: R156838
Sample ID: 23010912-001ADUP
SampType: DUP
TestCode: pH_NPW(450 Units: s.u.@19.7C
Prep Date:
RunNo: 156838
Dient ID: BatchQC
Batch ID: R156838
TestNo: SW9045D
Analysis Date: 1/20/2023
SegNo: 4175285
4nalyte
Result
PQL SPK value SPK Ref Val %REC
LowLimit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal,
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected OGl P Second column confirmation exceeds Original
PL Permit Limit R RPD outside accepted recovery limits RL Reporting Detection Limit
Page 33 of 39

SUMMIT Summit Environmental Technologies, Inc
3310 Win St
ENVIRONMENTAL TECHNOLOGIES, INC Cuyahoga Falls, Ohio 44223
Analytical Laboratories TEL: [phone] FAX: [phone]
Website: http://www.settek.coni
Client: Synagro
Project: Newton
Cyanide, Reactive ND 0.495
QC SUMMARY REPORT
WO#: 23010834
24-Jan-23
BatchlD: R156913
Cyanide, Reactive 9.17 0.500 10.00 0 91.7 85 115
Cyanide, Reactive ND 0.481 0.5000 0 62.0 50 150
Sample ID: 23010840-001AMS
SampType: MS
TestCode: Cyanide,Rea Units: mg/Kg
Prep Date:
RunNo: 156913
Client ID: BatchQC
Batch ID: R156913
TestNo: SW9014
Analysis Date: 1/23/2023
SegNo: 4176952
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
Cyanide, Reactive
7.77 0.495
10.00 0 77.7 75
125
Qualifiers: B
Analyte detected in the associated Method Blank
E Value above quantitation range
H
Holding times for preparation or anal,
J
Analyte detected below quantitation limits
M Manual Integration used to determine area response
MC
Value is below Minimum Compound
Original
ND
Not Detected
OGl
P
Second column confirmation exceeds
PL
Permit Limit
R RPD outside accepted recovery limits
RL
Reporting Detection Limit
Page 34 of 39

SUMMIT Summit Environmental Technologies, Inc.
3310 Win St.
ENVIRONMENTAL TECHNOLOGIES, INC Cuyahoga Falls, Ohio 44223
Analytical Laboratories TEL: [phone] FAX: [phone]
Website: http://www.settek.coni
Client: Synagro
Project: Newton
QC SUMMARY REPORT
WO#: 23010834
24-Jan-23
BatchlD: R156913
Sample ID: 23010840-001AMS
SampType: MS
TestCode: Cyanide,Rea Units: mg/Kg
Prep Date:
RunNo: 156913
Client ID: Batch=
Batch ID: R156913
TestNo: SW9014
Analysis Date: 1/23/2023
SegNo: 4176952
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Sample ID: 23010840-001AMSD
SampType: MSD
TestCode: Cyanide,Rea Units: mg/Kg
Prep Date:
RunNo: 156913
Client ID: Batch=
Batch ID: R156913
TestNo: SW9014
Analysis Date: 1/23/2023
SegNo: 4176953
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Cyanide, Reactive 8.43 0.495 10.00 0 84.3 75 125 7.772 8.19 10
Qualifiers: B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
PL Permit Limit
E Value above quantitation range H Holding times for preparation or anal,
M Manual Integration used to determine area response MC Value is below Minimum Compound
OGl P Second column confirmation exceeds
R RPD outside accepted recovery limits RL Reporting Detection Limit
Original
Page 35 of 39

SUMMIT Summit Environmental Technologies, Inc.
3310 Win St.
ENVIRONMENTAL TECHNOLOGIES, INC Cuyahoga Falls, Ohio 44223
Analytical Laboratories TEL: [phone] FAX: [phone]
Website: http://www.settek.coni
Client: Synagro
Project: Newton
QC SUMMARY REPORT
WO#: 23010834
24-Jan-23
BatchlD: R156917
Sample ID: 23010840-001AMS
SampType: MS
TestCode: Sulfide,React Units: mg/Kg
Prep Date:
RunNo: 156917
Client ID: Batch=
Batch ID: R156917
TestNo: SW9034
Analysis Date: 1/23/2023
SegNo: 4177055
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Sulfide, Reactive 1590 25.0 1710 0 93.0 80 120
Sample ID: 23010840-001AMSD
SampType: MSD
TestCode: Sulfide,React Units: mg/Kg
Prep Date:
RunNo: 156917
Client ID: Batch=
Batch ID: R156917
TestNo: SW9034
Analysis Date: 1/23/2023
SegNo: 4177056
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Sulfide, Reactive 1660 25.0 1710 0 97.1 80 120 1590 4.31 30
Qualifiers: B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
PL Permit Limit
E Value above quantitation range H Holding times for preparation or anal,
M Manual Integration used to determine area response MC Value is below Minimum Compound
OGl P Second column confirmation exceeds
R RPD outside accepted recovery limits RL Reporting Detection Limit
Original
Page 36 of 39

SUMMIT Summit Environmental Technologies, Inc.
3310 Win St.
ENVIRONMENTAL TECHNOLOGIES, INC Cuyahoga Falls, Ohio 44223
Analytical Laboratories TEL: [phone] FAX.- [phone]
Website: hgp:llwww.settek.com
Client: Synagro
Project: Newton
QC SUMMARY REPORT
WO#: 23010834
24-Jan-23
BatchID: R156917
Sample ID: MB-R156917
SampType: MBLK
TestCode: Sulfide,React Units: mg/L
Prep Date:
RunNo: 156917
Client ID: PBW
Batch ID: R156917
TestNo: SW9034
Analysis Date: 1/23/2023
SegNo: 4177039
Analyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Sulfide, Reactive ND 25.0
Sample ID: LCS-R156917
SampType: LCS
TestCode: Sulfide,React Units: mg/L
Prep Date:
RunNo: 156917
Client ID: LCSW
Batch ID: R156917
TestNo: SW9034
Analysis Date: 1/23/2023
SegNo: 4177040
Analyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Sulfide, Reactive
1670 25.0 1710 0 97.7 85 115
Qualifiers: B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
PL Permit Limit
E Value above quantitation range H Holding times for preparation or anal,
M Manual Integration used to determine area response MC Value is below Minimum Compound
OGl P Second column confirmation exceeds
R RPD outside accepted recovery limits RL Reporting Detection Limit
Original
Page 37 of 39

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Page 38 of 39

�� � � Summit Environmental Technologies, Inc.
3310 Win St.
ENVIRONMENTAL TECHNOLOGIES, INC Cuyahoga Falls, Ohio44223 Sample Log -in Check List
Analytical Laboratories TEL: [phone] FAX [phone]
Website: http://www.settek.coni
Client Name: SYN-NC-27028 Work Order Number: 23010834
Logged by: Anthony W. Britton
Completed By: Anthony W. Britton
Reviewed By: Jennifer Woolf
1/13/2023 10:20:00 AM
1/13/2023 5:36:21 PM
1/16/2023 3:06:41 PM
RcptNo: 1
Chain of Custody
1. Is Chain of Custody complete?
Yes
d❑
No
❑
Not Present ❑
2. How was the sample delivered?
UPS
Loa In
3, Coolers are present?
Yes
d❑
No
F
NA F
4. Shipping container/cooler in good condition?
Yes
d❑
No
Custody seals intact on shipping container/cooler?
Yes
❑
No
❑
Not Present
No. Seal Date:
Signed By:
5. Was an attempt made to cool the samples?
Yes
❑
No
F—
NA ❑
6. Were all samples received at a temperature of >0° C to 6.0°C
Yes
d❑
No
❑
NA
7, Sample(s) in proper container(s)?
Yes
J❑
No
❑
g. Sufficient sample volume for indicated test(s)?
Yes
d❑
No
❑
g, Are samples (except VOA and ONG) properly preserved?
Yes
J❑
No
❑
10. Was preservative added to bottles?
Yes
❑
No
d❑
NA ❑
11. Is the headspace in the VOA vials less than 1/4 inch or 6 mm?
Yes
No
❑
No VOA Vials ❑�
12. Were any sample containers received broken?
Yes
No
d❑
13. Does paperwork match bottle labels?
Yes
No
❑
(Note discrepancies on chain of custody)
14. Are matrices correctly identified on Chain of Custody?
Yes
No❑
15. Is it clear what analyses were requested?
Yes
No
❑
16. Were all holding times able to be met?
Yes
No
❑
(If no, notify customer for authorization.)
Special Handling (if applicable)
17. Was client notified of all discrepancies with this order?
Yes
No
❑
NA ❑d
Person Notified: Date:
By Whom: Via:
❑ eMail
❑ Phone
❑
Fax
❑ In Person
Regarding:
Client Instructions:
18. Additional remarks:
Cooler Information
Cooler No
Temp °C
Condition
Seal Intact
Seal No
Seal Date
Signed
By
1
5.0
Good
Not Present
Page 39 of 39

SECTION 5

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Newton
WWTP Name: Newton Clark Creek WWTP
Monitoring Period: From 01/01/23 To 3/31123
WQ Permit Number: WQ 0003902
NPDESNumber: NC0036196
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.I106) - Please indicate level achieved and alternative performed:
Class A:
Alt. I/A (time/temp) Alt. 2/B (Alk Treatment) Alt. 3/C (Prior Testing)
Alt. 4/1) (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Themmophilic
Beta Ray Gamma Ray Pasteurization
Class B:
Alt. (1) Fecal Density Alt. (2) Process to Significantly Reduce Pathogens x
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization X Air Drying Composting Aerobic Digestion
Anaerobic Digestion
if annlicahle to alternative nerfnrniM (Class A nr Class R) emmnlete the fnllmvinu mnnitnrina data -
Parameter
Allowable Level in Sludge
Pathogen Density
No. of
Frequency
Sample
Analytical
Excee-
of
Type
Technique
Minimum Geo. Mean Maximum Units
deuces
Analysis
Fecal
2x10 to the 6t1
MPN
MPN/g
Coliform
power per gram
of total solids
CFU/g
CFU
1000 MPN per gram of
10PN/g
total solids (dry weight)
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform)
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed:
Option/Alt. 1
Option/Alt. 2
Option/Alt. 3 Option/Alt. 4
(VS reduction)
(40-day bench)
(30-day bench) (Spec. 02 uptake)
Option/Alt. 5
Option/Alt. 6
Option/Alt. 7 Option/Alt. 8
(14-Day Aerobic)
(Alk Stabilization) x
(Drying-- Stable) (Drying —Unstable)
Option/Alt. 9
Option/Alt. 10
(Injection)
(Incorporation)
No vector attraction reduction alternatives were performed
CERTIFICATION STATEMENT (please check the appropriate statement)
7 certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1 106 and the vector attraction
X reduction requirement in 40 CFR 503.33/15A NCAC 02T. 1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified
personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have
been met. I am aware that there are significant penalties for false certification including fine and imprisonment."
James Wentz Public Utilities Director
Preparer Name and Title ( type or print)
Signature f Preparer* Date
Land Applier Name and Title (if applicable) (type or print)
Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26)

City of Newton - Clark Creek WWTP
Year
Sludge Grab Sampling Data
Intial Sample
2 Hour Sample
22 Hour Sample
DATE
ection
—
Analysis
Collection
Analysis
Collection
Analysis
Time
pH
Corrected
p H
Temp
Time
By
By
I
Time
pH
Corrected
Temp
Time
By
By
Date
Time
pH
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Temp
Time
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Sampling Collect #1 sample
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in s.u.
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cnllPrtinn n nL . ).1,,,,
i41'

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Newton WQ Permit Number: WQ 0003902 _
WWTP Name: Newton Clark Creek WWTP NPDES Number: NC 0036196 T
Monitoring Period: From 04/01/23 To 6/30/2023
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. 1/A (time/temp) Alt. 2B (Alk Treatment) Alt. 3/C (Prior Testing)
Alt. 4/1) (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Therrnophilic
Beta Ray Gamma Ray Pasteurization
Class B:
Alt. (1) Fecal Density Alt. (2) Process to Significantly Reduce Pathogens x
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization X Air Drying Composting Aerobic Digestion
Anaerobic Digestion
If —nlioahla M alternative nfvrm•mnd ifhac A — Vl— R1 }hn Fn11nw7nn —If-- An}. -
Parameter
Allowable Level in Sludge
Pathogen Density
No. of
Frequency
Sample
Analytical
Excee-
of
Type
Technique
Minimum Gen. Mean Maximum Units
dences
Analysis
Fecal
2x1Gto the 6'h
MPN
MPN/g
Coliform
power per gram
of total solids
CFU
CFU/g
1000 MPN per gram of
MPN/g
total solids (dry weight)
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative
performed:
0 tion/Alt. I
Option/Alt.2
0ption/Alt.3
Option/Alt.4
(VS reduction)
(40-day bench)
(30-day bench)
(Spec. 02 uptake)
Option/Alt. 5
Option/Alt, 6
Option/Alt. 7
Option/Alt. 8
(I4-DayAerobic)
(AlkStabilization) x
(Drying —Stable)
(Drying — Unstable)
Option/Ah. 9
Option/Alt. 10
(Injection)
(Incorporation)
No vector attraction reduction
alternatives were performed
CERTIFICATION STATEMENT (please check the appropriate statement)
"1 certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1 I06 and the vector attraction
X_ reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified
personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have
been met. I am aware that there are significant penalties for false certification including fine and imprisonment."
James Wentz Public Utilities Director
Preparer attle and Title ( type or print) r Land Applier Name and'ritle (if applicable) (type or print)
Signal of Preparer* Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26)

City of Newton - Clark Creek WWTP
Year
Sludge Grab Sampling Data
Intial Sample
2 Hour Sample
22 Hour Sample
DATE
ection
—
Analysis
Collection
Analysis
Collection
Analysis
Time
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Corrected
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Sampling Collect #1 sample
for pH when tank is ready for testing.
a �t -
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in s.u.
Guidelines Collect #1 sample
for pH when tank is ready for testing.
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of
cnllPrtinn n nL . ).1,,,,
i41'

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Newton
WWTP Name: Newton Clark Creek W WTP
WQ Permit Number: WQ 0003902
NPDES Number: NC 0036196
Monitoring Period: From 07/01/23 To 9/30/2023
Pathogen Reduction (40 CFR 503,32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. 1/A (time/temp) Alt. 2/13 (Alk Treatment) Alt. 3/C (Prior Testing)
Alt. 4/D (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Therniophilic
Beta Ray Gamma Ray Pasteurization
Class B:
Alt. (1) Fecal Density Alt. (2) Process to Significantly Reduce Pathogens x
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization X Air Drying Composting Aerobic Digestion
Anaerobic Digestion
If on Jirnhla to nitwrnntivo . rfnr »nrl Irl— A — f` ... M -n .dote the r.11 .... ..a A-4-.
Parameter
Allowable Level in Sludge
Pathogen Density
No. of
Frequency
Sample
Analytical
Excee-
of
Type
Technique
Minimum Geo. Mean Maximum Units
deuces
Analysis
Fecal
2x10 to the 61h
MPN
MPN/g
Coliform
power per gram
of total solids
CFU
CFU/g
1000 MPN per gram of
MPN/g
total solids (dry weight)
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform)
Vector Attraction Redaction (40 CFR 503.33/15A NCAC 02`I'.1107) - Please indicate option/alternative performed:
Option/Alt. I
Option/Alt. 2
Option/Alt. 3 Option/Alt. 4
(VS reduction)
(40-day bench)
(30-day bench) (Spec. 02 uptake)
Option/Alt. 5
Option/Alt. 6
Optiolt/Alt. 7 Optioii/Alt. 8
(14-bay Aerobic)
(Alk Stabilization) x
(Drying— Stable) (Drying Unstable)
Option/Alt. 9
Option/Alt. 10
(Injection)
(Incorporation)
No vector attraction reduction alternatives were performed ^_ _
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penally of law, that [lie pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and Elie vector attraction
X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met"
"9 certify, under penalty of law, that the pathogen re uirenients in 40 CFR 503.32/15A NCAC 02T.1 106 and the vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 02T.1 107 have not been met" (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified
personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have
been met. I am aware that there are significant penalties for false certification including fine and imprisonment."
James Wentz Public Utilities Director _
Preparer me and Title ( type or print) Land Applier Name and Title (if applicable) (type or print)
Signature f Preparer* Date Signature of Land Applier (if applicable) Date
!pPreparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 21'.1102 (26)

City of Newton - Clark Creek WWTP
Year
Sludge Grab Sampling Data
Intial Sample
2 Hour Sample
22 Hour Sample
DATE
ection
—
Analysis
Collection
Analysis
Collection
Analysis
Time
pH
Corrected
p H
Temp
Time
By
By
I
Time
pH
Corrected
Temp
Time
By
By
Date
Time
pH
Corrected
Temp
Time
By
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✓ � j�� , Sn� U)j
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5 Temperature is measured
in 'C
Method - SM2550 B-2000
Sampling Collect #1 sample
for pH when tank is ready for testing.
a �t -
--4t:_NU(d W. '+ul2�_ pH is measured
in s.u.
Guidelines Collect #1 sample
for pH when tank is ready for testing.
�� r iv W ► 6C hvUrS
Method - SM4500 H+13-2000 (Aqueous)
Sample must arrive in lab within
15 minutes
of
cnllPrtinn n nL . ).1,,,,
i41'

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Newton _ WQ Permit Number: WQ 0003902
WWTP Name: Newton Clark Creek WWTP NPDES Number: NC 0036196
Monitoring Period: From 10/01/23 To 12/31/2023
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. 1/A (time/temp) Alt. 2B (Alk Treatment) Alt. 3/C (Prior Testing)
Alt. 4/1) (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thernnophilic
Beta Ray Gamma Ray Pasteurization
Class 13:
Alt. (1) Fecal Density Alt. (2) Process to Significantly Reduce Pathogens x
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization X Air Drying Composting Aerobic Digestion
Anaerobic Digestion
If annlicahle to alternative nerfnrmed (Class A nr Class Rl rnuinle,ta the, fnnn,vina innnitnrina iinfw
Parameter
Allowable Level in Sludge
Pathogen Density
No. of
Frequency
Sample
Analytical
Excee-
of
Type
Technique
Minimum Geo. Mean Maximum Units
deuces
Analysis
Fecal
2x 10 to the 6'
MPN
MPN/g
Coliform
power per gram
of total solids
CFU
CFU/g
1000 MPN per gram of
MPN/g
total solids (dry weight)
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform)
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed:
Option/Alt. 1
Option/Alt, 2
Option/All. 3 Option/Alt. 4
(VS reduction)
(40-day bench)
(30-day bench) (Spec. 02 uptake)
Option/Alt. 5
Option/Alt. 6
Option/Alt. 7 Option/Alt. 8
(14-Day Aerobic)
(Alk Stabilization) x
(Drying — Stable) (Drying — Unstable)
Option/Alt. 9
Optionn/Alt. 10
(hijection)
(incorporation)
No vector attraction reduction alternatives were performed
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 50332/15A NCAC 02T.1106 and the vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified
personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have
been met. I ant aware that There are significant penalties for false certification including fine and imprisonment."
James Wentz Public Utilities Director _
Preparr Na e and Title ( type or print)
Signa l re of Preparer Date
Land Applier Name and Title (if applicable) (type or print)
Signature of Land Applier (if applicable) Date
'Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26)

City of Newton - Clark Creek WWTP
Year
Sludge Grab Sampling Data
Intial Sample
2 Hour Sample
22 Hour Sample
DATE
ection
—
Analysis
Collection
Analysis
Collection
Analysis
Time
pH
Corrected
p H
Temp
Time
By
By
I
Time
pH
Corrected
Temp
Time
By
By
Date
Time
pH
Corrected
Temp
Time
By
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Method - SM2550 B-2000
Sampling Collect #1 sample
for pH when tank is ready for testing.
a �t -
--4t:_NU(d W. '+ul2�_ pH is measured
in s.u.
Guidelines Collect #1 sample
for pH when tank is ready for testing.
�� r iv W ► 6C hvUrS
Method - SM4500 H+13-2000 (Aqueous)
Sample must arrive in lab within
15 minutes
of
cnllPrtinn n nL . ).1,,,,
i41'

SECTION 6

Agricultural Lime Application Log
Year: 2023
Project:
Newton
Field
Soil
Lime Requirement
Tons/Acre
Date Applied
(state -county -site -field)
pH
(from soil analysis)
Applied(CCE Eq.)
CA-20-10
7.6
O.OT/Ac.
CA-20-13
5.7
O.OT/Ac.
CA-32-1
6.9
0.0 T/AC
CA-32-2
6.7
O.OT/Ac.
CA-21-1
7.5
O.OT/Ac.
CA-21-2
7.4
O.OT/Ac.
CA-25-2
5.6 O.OT/Ac.
They get their lime in the sludge since Newton is Lime stabalized.

SECTION 7

NCDA&CS Agronomic Division Phone: [phone]
Website: www.ncagr.gov/agronomi/
Report No.
FY24-SL010165
Predictive
Client:
Alex Fox
Synagro
Advisor:
£
x
Soil Report Mehlich-3 Extraction
284 Boger Rd
Mocksville, NC27028
Links to Helpful Information
Sampled County: Catawba
Client ID: 501947
Advisor ID:
Sampled:
Received: 10/25/2023 Completed: 11/07/2023
Farm: CA-20
Sample ID: 12
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P2O5
K2O
Mg S
Mn
Zn
Cu B
Information
Lime History:
1 - Fescue/OGrass/Tim, M 0.0
120-200 30
80
0 0
0
0
0 0
Note: 12
2 - 0.0
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class:
Mineral
HM% W/V
CEC BS% Ac pH P-1 K-1
Ca% Mg%
S-1
Mn-I
Mn-All Mn-Al2
Zn-I
Zn-AI
Cu-I Na ESP
SS-1 NO3-N
0.41 1.13
7.1 83 1.2 6.0 46 30
63 18
32
518
327
134
134
163 0.1
1
Sample ID: 13
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P2O5
K2O
Mg S
Mn
Zn
Cu B
Information
Lime History:
1- Fescue/OGrass/Tim, M 0.6
120-200 80
0
0 0
0
0
0 0
Note: 12
2 - 0.0
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class:
Mineral
HM% W/V
CEC BS% Ac pH P-1 K-1
Ca% Mg%
S-1
Mn-I
Mn-All Mn-AI2
Zn-I
Zn-AI
Cu-I Na ESP
SS-1 NO3-N
0.56 0.96
8.7 79 1.8 5.7 23 83
57 17
56
329
214
145
145
143 0.1
1
North Carolina
f. 1 , >
I0WOOLO iiu%t lLaW Ctwnawukm
Reprogramming of the laboratory -information -management system that makes this report possible is being funded
through a grant from the North Carolina Tobacco Trust Fund Commission.
Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
- Steve Troxler, Commissioner of Agriculture

NCDA&CS Agronomic Division Phone: [phone]
Website: www.ncagr.gov/agronomi/
Report No. FY24-SL010165
Alex Fox
Page 2 of 3
Sample ID: 10
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P2O5 K2O
Mg
S
Mn Zn
Cu B
Information
Lime History:
1 - Fescue/OGrass/Tim, M 0.0
120-200 0 30
0
20
pH$ 0
0 0
Note: 12 Note:
2 - 0.0
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm):
Soil Class:
Mineral
HM% W/V CEC BS% Ac pH P-1 K-1
Ca% Mg% S-1 Mn-I
Mn-All
Mn-Al2
Zn-I Zn-AI
Cu-I Na ESP SS-1 NO3-N
0.18 1.12 23.5 100 0.0 7.6 80 59
80 18 22 760
449
270 270
550 0.0

NCDA&CS Agronomic Division Phone: [phone] Website: www.ncagr.gov/agronomi/
Report No. FY24-SLO10165
Alex Fox
Page 3 of 3
Understanding the Soil Report: explanation of measurements, abbreviations and units
Recommendations
Report Abbreviations
Lime
Ac
exchangeable acidity
If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either
B
boron
ton/acre or Ib/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting.
BS%
% CEC occupied by basic cations
For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 Ib/1000 sq ft) at on
Ca%
% CEC occupied by calcium
time, even if the report recommends more. You can apply the rest in similar increments every six months until the full rate
CEC
cation exchange capacity
is applied. If MG is recommended and lime is needed, use dolomitric lime.
Cu-I
copper index
ESP
exchangeable sodium percent
Fertilizer
HM%
percent humic matter
Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of
K-I
potassium index
lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies
K20
potash
for the crop being grown, not on soil test results. K-1 and P-1 values are based on test results and should be > 50. If they
Mg%
% CEC occupied by magnesium
are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is
MIN
mineral soil class
an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS-1 levels appear
Mn
manganese
only on reports for greenhouse soil or problem samples.
Mn-All
Mn-availability index for crop 1
Mn-Al2
Mn-availability index for crop 2
Mn-I
manganese index
Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z
Mn-
mineral -organic soil class
notations appear on the soil report, refer to $Note: Secondary Nutrients and Micronutrients. In general, homeowners do not
N
nitrogen
need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit
Na
sodium
ncagr.gov/agronomi/pubs.htm.
NO3-N
nitrate nitrogen
ORG
organic soil class
Recommendations for small areas, such as home lawns/gardens, are listed in units of Ib/1000 sq ft. If you cannot find
pH
current soil pH
the exact fertilizer grade recommended on the report, visit www.ncagr.gov/apronomi/obpart4.htm1 #sfind information that
P-1
phosphorus index
may help you choose a comparable alternate. For more information, read A Homeowner's Guide to Fertilizer.
P205
phosphate
S-1
sulfur index
Test Results
SS-1
soluble salt index
W/V
weight per volume
The first seven values [soil class, HM%, W/V, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The
Zn-AI
zinc availability index
Zn-I
zinc index
remaining 16 [P-I, K-I, Ca%, Mg%, Mn-I, Mn-All, Mn-AI2, Zn-I, Zn-AI, Cu-I, S-I, SS -I, Na, ESP, SS -I, NO3-N (not routinel
available)] indicate levels of plant nutrients or other fertility measurement. Visit www.ncapr.gov/agronomi/uyrst.htm

NCDA&CS Agronomic Division Phone: [phone]
Website: www.ncagr.gov/agronomi/
Report No.
FY24-SL010164
Predictive
Client:
Alex Fox
Synagro
Advisor:
£
x
Soil Report Mehlich-3 Extraction
284 Boger Rd
Mocksville, NC27028
Links to Helpful Information
Sampled County: Catawba
Client ID: 501947
Advisor ID:
Sampled:
Received: 10/25/2023 Completed: 11/07/2023
Farm: CA-21
Sample ID: 1
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P2O5
K2O
Mg S
Mn
Zn
Cu B
Information
Lime History:
1 - Fescue/OGrass/Tim, M 0.0
120-200 0
70
0 0
pH$
0
0 0
Note: 12 Note:
2 - 0.0
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class:
Mineral
HM% W/V
CEC BS% Ac pH P-1 K-1
Ca% Mg%
S-1
Mn-I
Mn-All Mn-Al2
Zn-I
Zn-AI
Cu-I Na ESP
SS-1 NO3-N
0.27 0.94
21.2 100 0.0 7.5 104 36
92 7
48
213
122
368
368
297 0.1
0
Sample ID: 2
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P2O5
K2O
Mg S
Mn
Zn
Cu B
Information
Lime History:
1 - Fescue/OGrass/Tim, M 0.0
120-200 80
80
0 20
pH$
0
0 0
Note: 12 Note:
2 - 0.0
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class:
Mineral
HM% W/V
CEC BS% Ac pH P-1 K-1
Ca% Mg%
S-1
Mn-I
Mn-All Mn-AI2
Zn-I
Zn-AI
Cu-I Na ESP
SS-1 NO3-N
0.27 1.03
10.8 100 0.0 7.4 23 27
90 8
21
312
183
143
143
140 0.1
1
North Carolina
A� `� J
lobitt o iru%( FtavJ Umnauukm
Reprogramming of the laboratory -information -management system that makes this report possible is being funded
through a grant from the North Carolina Tobacco Trust Fund Commission.
Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
- Steve Troxler, Commissioner of Agriculture

NCDA&CS Agronomic Division Phone: [phone] Website: www.ncagr.gov/agronomi/
Report No. FY24-SLO10164
Alex Fox
Page 2 of 2
Understanding the Soil Report: explanation of measurements, abbreviations and units
Recommendations
Report Abbreviations
Lime
Ac
exchangeable acidity
If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either
B
boron
ton/acre or Ib/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting.
BS%
% CEC occupied by basic cations
For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 Ib/1000 sq ft) at on
Ca%
% CEC occupied by calcium
time, even if the report recommends more. You can apply the rest in similar increments every six months until the full rate
CEC
cation exchange capacity
is applied. If MG is recommended and lime is needed, use dolomitric lime.
Cu-I
copper index
ESP
exchangeable sodium percent
Fertilizer
HM%
percent humic matter
Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of
K-I
potassium index
lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies
K20
potash
for the crop being grown, not on soil test results. K-1 and P-1 values are based on test results and should be > 50. If they
Mg%
% CEC occupied by magnesium
are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is
MIN
mineral soil class
an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS-1 levels appear
Mn
manganese
only on reports for greenhouse soil or problem samples.
Mn-All
Mn-availability index for crop 1
Mn-Al2
Mn-availability index for crop 2
Mn-I
manganese index
Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z
Mn-
mineral -organic soil class
notations appear on the soil report, refer to $Note: Secondary Nutrients and Micronutrients. In general, homeowners do not
N
nitrogen
need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit
Na
sodium
ncagr.gov/agronomi/pubs.htm.
NO3-N
nitrate nitrogen
ORG
organic soil class
Recommendations for small areas, such as home lawns/gardens, are listed in units of Ib/1000 sq ft. If you cannot find
pH
current soil pH
the exact fertilizer grade recommended on the report, visit www.ncagr.gov/apronomi/obpart4.htm1 #sfind information that
P-1
phosphorus index
may help you choose a comparable alternate. For more information, read A Homeowner's Guide to Fertilizer.
P205
phosphate
S-1
sulfur index
Test Results
SS-1
soluble salt index
W/V
weight per volume
The first seven values [soil class, HM%, W/V, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The
Zn-AI
zinc availability index
Zn-I
zinc index
remaining 16 [P-I, K-I, Ca%, Mg%, Mn-I, Mn-All, Mn-AI2, Zn-I, Zn-AI, Cu-I, S-I, SS -I, Na, ESP, SS -I, NO3-N (not routinel
available)] indicate levels of plant nutrients or other fertility measurement. Visit www.ncapr.gov/agronomi/uyrst.htm

NCDA&CS Agronomic Division Phone: [phone]
Website: www.ncagr.gov/agronomi/
Report No.
FY24-SL010161
Predictive
Client: Alex Fox
Synagro
Advisor:
£
x "
Soil Report Mehlich-3 Extraction
284 Boger Rd
Mocksville, NC27028
Links to Helpful Information
Sampled County: Catawba
Client ID: 501947
Advisor ID:
Sampled:
Received: 10/25/2023 Completed: 11/07/2023
Farm: CA-25
Sample ID: 2
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P2O5
K2O Mg S Mn Zn
Cu B
Information
Lime History:
1 - Fescue/OGrass/Tim, M 0.6
120-200 120
100 0 0 0 0
0 0
Note: 12
2 - 0.0
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class: Mineral
HM% W/V
CEC BS% Ac pH P-1 K-1
Ca% Mg%
S-1 Mn-I Mn-All Mn-Al2 Zn-I Zn-AI
Cu-I Na ESP
SS-1 NO3-N
0.41 1.07
6.8 77 1.6 5.6 11 18
52 23
48 305 200 99 99
62 0.1
1
North Carolina
lobitty lru%t FuivJ Ctwnauukm
Reprogramming of the laboratory -information -management system that makes this report possible is being funded
through a grant from the North Carolina Tobacco Trust Fund Commission.
Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
- Steve Troxler, Commissioner of Agriculture

NCDA&CS Agronomic Division Phone: [phone] Website: www.ncagr.gov/agronomi/
Report No. FY24-SLO10161
Alex Fox
Page 2 of 2
Understanding the Soil Report: explanation of measurements, abbreviations and units
Recommendations
Report Abbreviations
Lime
Ac
exchangeable acidity
If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either
B
boron
ton/acre or Ib/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting.
BS%
% CEC occupied by basic cations
For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 Ib/1000 sq ft) at on
Ca%
% CEC occupied by calcium
time, even if the report recommends more. You can apply the rest in similar increments every six months until the full rate
CEC
cation exchange capacity
is applied. If MG is recommended and lime is needed, use dolomitric lime.
Cu-I
copper index
ESP
exchangeable sodium percent
Fertilizer
HM%
percent humic matter
Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of
K-I
potassium index
lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies
K20
potash
for the crop being grown, not on soil test results. K-1 and P-1 values are based on test results and should be > 50. If they
Mg%
% CEC occupied by magnesium
are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is
MIN
mineral soil class
an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS-1 levels appear
Mn
manganese
only on reports for greenhouse soil or problem samples.
Mn-All
Mn-availability index for crop 1
Mn-Al2
Mn-availability index for crop 2
Mn-I
manganese index
Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z
Mn-
mineral -organic soil class
notations appear on the soil report, refer to $Note: Secondary Nutrients and Micronutrients. In general, homeowners do not
N
nitrogen
need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit
Na
sodium
ncagr.gov/agronomi/pubs.htm.
NO3-N
nitrate nitrogen
ORG
organic soil class
Recommendations for small areas, such as home lawns/gardens, are listed in units of Ib/1000 sq ft. If you cannot find
pH
current soil pH
the exact fertilizer grade recommended on the report, visit www.ncagr.gov/apronomi/obpart4.htm1 #sfind information that
P-1
phosphorus index
may help you choose a comparable alternate. For more information, read A Homeowner's Guide to Fertilizer.
P205
phosphate
S-1
sulfur index
Test Results
SS-1
soluble salt index
W/V
weight per volume
The first seven values [soil class, HM%, W/V, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The
Zn-AI
zinc availability index
Zn-I
zinc index
remaining 16 [P-I, K-I, Ca%, Mg%, Mn-I, Mn-All, Mn-AI2, Zn-I, Zn-AI, Cu-I, S-I, SS -I, Na, ESP, SS -I, NO3-N (not routinel
available)] indicate levels of plant nutrients or other fertility measurement. Visit www.ncapr.gov/agronomi/uyrst.htm

Page 1 of 2
Report Number: 24-002-0531
Account Number:07778
Send To: Synagro/Alex Fox
Alex Fox
284 Boger Rd
Mocksville NC 27028
Waypoint(D
ANALYTICAL
"Every acre... Every year.'4M
2850 Daisy Lane, Wilson, NC 27896
Main 252-206-1721 ° Fax [phone]
www.waypointanalytical.com
Grower: NEWTON
Farm: CA-32
SOIL ANALYSIS REPORT Analytical Method(s): Mehlich 3 Lime Index Humic Matter Loss On Ignition
Water pH
Date Received: 01 /02/2024 Date Of Analysis: 01 /03/2024 Date Of Report: 01 /03/2024
OM
W/V
ENR
Phosphorus
Potassium
Magnesium
Calcium
Sodium
pH
Acidity
C.E.0
Sample ID
Lab
Field ID
Number
%
Soil
Ibs/A
M3
K
Mg
Ca
Na
Soil
Buffer
H
Class
ppm Rate
ppm Rate
ppm Rate
ppm Rate
ppm Rate
ppm Rate
ppm Rate
pH
Index
meq/100g
meq/100g
1
24250
0.6
46
56 H
19 VL
61 VL
1911 VH
28 VL
6.9
0.7
11.0
NC=47
NC=10
2
24251
1.1
56
34 M
30 VL
114 L
1844 H
19 VL
6.7
0.9
11.3
NC=28
NC=15
Percent Base Saturation
Nitrate
Sulfur
Zinc
Manganese
Iron
Copper
Boron
Soluble Salts
Sample ID
Field ID
K
Mg
Ca
Na
H
NO3 N
S
Zn
Mn
Fe
Cu
B
SS
%
%
%
%
%
ppm Rate
ppm Rate
ppm Rate
ppm Rate
ppm Rate
ppm Rate
ppm Rate
ms/cm Rate
1
0.4
4.6
86.9
1.1
7.3
13 L
7.5 H
22 H
2.5 H
0.5 L
NC=27
NC=187.5
NC=138
NC=125.0
2
0.7
8.4
81.6
0.7
8.8
17 M
7.5 H
6 L
2.0 H
0.6 M
NC=35
NC=187.5
NC=38
NC=100.0
Values on this report represent the plant available nutrients in the Explanation of symbols: % (percent), ppm (parts per million), Ibs/A This report applies to sample(s) tested. samples are retained a
soil. Rating after each value: VL (Very Low), L (Low), M (Medium), (pounds per acre), ms/cm (milli -mhos per centimeter), meq/100g maximum of thirty days after testing.
H (High), VH (Very High). ENR - Estimated Nitrogen Release. (milli -equivalent per 100 grams). Conversions: ppm x 2 = Ibs/A, Soluble by.
C.E.C. - Cation Exchange Capacity. Salts ms/cm x 640 = ppm. Analysis prepared by: Waypoint Analytical Carolina, Inc.

Page 2 of 2
Report Number: 24-002-0531
Account Number:07778
Send To: Synagro/Alex Fox
Alex Fox
284 Boger Rd
Mocksville NC 27028
Date Received: 01/02/2024
Date Of Report: 01 /03/2024
Waypoint(D
ANALYTICAL
"Every acre... Every year.'4M
Farm: CA-32
SOIL FERTILITY RECOMMENDATIONS
2850 Daisy Lane, Wilson, NC 27896
Main 252-206-1721 ° Fax [phone]
www.waypointanalytical.com
Grower: NEWTON
Nitrogen
Phosphate
Potash
Magnesium
Sulfur
Zinc
Manganese
Iron
Copper
Boron
Sample ID
Intended Crop
Yield Goal
Lime
IN
K20
Mg
S
Zn
Mn
Fe
Cu
B
Field ID
Tons
Tons/A
Ib/A
Ib/A
Ib/A
Ib/A
Ib/A
Ib/A
Ib/A
Ib/A
Ib/A
Ib/A
1
Fescue Hay
4
0.0
200
0
180
10
10
0
3
0
0.5
2
Fescue Hay
4
0.0
200
38
180
0
9
0
4
0
0
Comments:
"The recommendations are based on research data and experience, but NO GUARANTEE or WARRANTY expressed or implied, concerning crop performance is made."
Our reports and letters are for the exclusive and confidential use of our clients„ and may not be reproduced in whole or part, nor may any reference be made to the
work,the results, or the company in any advertising, news release, or other public anouncements without obtaining our prior written authorization. Copy right 1977.