WQ0001048_2023 Residual Annual Report_20240215 (2)

Initial Review
Reviewer
nathaniel.thorn burg
Is this submittal an application? (Excluding additional information.) *
Yes No
If not an application what is the submittal type?* Annual Report
Residual Annual Report
Additional Information
Other
Annual Report Year* 2023
Permit Number (IR) * W00001048
Applicant/Permittee Contentnea Metropolitan Sewerage District
Email Notifications
Does this need review by the hydrogeologist? * Yes OO No
Regional Office Washington
CO Reviewer
Admin Reviewer Wanda Gerald

Submittal Form
Project Contact Information
Please provide information on the person to be contacted by NDB Staff regarding electronic submittal, confirmation of receipt, and other correspondence.
Name* Chuck Smithwick
Email Address*
[e-mail]
Project Information
.........................
Application/Document Type*
New (Fee Required)
Modification - Major (Fee Required)
Renewal with Major Modification (Fee
Required)
Annual Report
Additional Information
Other
Phone Number*
2524138898
Modification - Minor
Renewal
GW-59, NDMR, NDMLR, NDAR-1,
N DAR-2
Residual Annual Report
Change of Ownership
We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form.
https://edoes.deq.nc.gov/Forms/NonDischarge_Monitoring_Report
Permit Type:*
Wastewater Irrigation
High -Rate Infiltration
Other Wastewater
Reclaimed Water
Closed -Loop Recycle
Residuals
Single -Family Residence Wastewater
Other
Irrigation
Permit Number:*
WQ0001048
Has Current Existing permit number
Applicant/Permittee Address*
900 Wiley Gaskins Road
Facility Name*
Contentnea MSD Class B Residuals Program
Please provide comments/notes on your current submittal below.
Annual Sludge Application Report
At this time, paper copies are no longer required. If you have any questions about what is required, please contact Nathaniel Thornburg
at [e-mail].
Please attach all information required or requested for this submittal to be reviewed here.
(Application Form, Engineering Plans, Specifications, Calculations, Etc.)
20240215111051198.pdf 8.06MB
Upload only 1 PDF document (less than 250 MB). Multiple documents must be combined into one PDF file unless file is larger
than upload limit.
* By checking this box, I acknowledge that I understand the application will not be accepted for pre -review until the fee (if required) has
been received by the Non -Discharge Branch. Application fees must be submitted by check or money order and made payable to the
North Carolina Department of Environmental Quality (NCDEQ). I also confirm that the uploaded document is a single PDF with all parts
of the application in correct order (as specified by the application).
Mail payment to:
NCDEQ — Division of Water Resources
Attn: Non -Discharge Branch
1617 Mail Service Center
Raleigh, NC 27699-1617
Signature
Submission Date 2/15/2024

ANNUAL LAND APPLICATION CERTIFICATION FORM
WQ Permit##: ix =JCfl2 County: . �+ Year: &)n
Facility Name (as shown on permit): rnn4M4neq=rf&D
Land Application Operator: d M- W1t.J! Phone: -62a `, C
Land application of residuals as allowed by the permit occurred during the past calendar year?
.4 Yes ❑ No - If No, skip Part A, and Part B and proceed to Part C. Also, If residuals were
generated but not land applied, please attach an explanation on how the residuals were handled.
ID ,,.F A A""1;Paf;nn Cnmmarv'
Total number of application fields in thepermit:
Total number of fields utilized for land application during the year:
Total amount of dry tons applied during the year for all application sites:
L) g
Total number of acres utilizes for land application during the year:
649 HD
Part B - Annual Com iance Statement:
Facility was compliant during calendar year gn ^ with all conditions of the land application permit
(including but not limited to items 1-13 below) issued by the Division of Water Resources. ❑ Yes Y1 No
If no please, provide a written description why the facility was not compliant, the dates, and explain corrective action
taken.
1) only residuals approved for this permit were applied to the permitted sites.
2) Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or
the limit specified in the permit.
3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies
of laboratory results are attached.
4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are; attached.
5) All other monitoring was performed in accordance with the permit and reported during the year as required and three (3)
copies of certified laboratory results are attached.
6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .1105(a) or the Pollutant
Loading Rates in 15A NCAC 02T .1105(b) (applicable to 40 CFR Part 503 regulated facilities).
7) All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part
503 regulated facilities).
8) All monitoring and reporting requirements in 15A NCAC 02T .1111 were complied with (applicable to 40 CFR Part
503 regulated facilities).
9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Resources.
10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
11) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as
specified in the permit.
12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred,
ed,
13) All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C - Certification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate,
and complete. I am aware that there are significant penalties for submitting false information, including the
possibility of fines and imprisonment for knowing violations."
CT--adb-rf)-,6rnW-hk 41,
Permittee Na ane and Title (type dr print) I Signature of Permittee Date
Signature of Preparer* Date Signature of Land Applier Date
(if different from Permittee) (if different from Permittee and Preparer)
* Preparer is defined in 40 CFR Part 503.9 (r) and 15A NCAC 02T .1102 (26) DENR FORM ACF (1212006)

EXPLANATIONS FOR DEVIATIONS FOR THE 2023 ANNUAL
SLUDGE LAND APPLICATION REPORT
10-18-23 Monitoring Well #9 Ammonia Nitrogen 1.67 mg/L
10-18-23 Monitoring Well #15 Total Organic Carbon 13.79 mg/L
Monitoring Well #15 Total Chromium 12 ug/L
The TOC levels naturally run higher in this area. As cited in the report prepared by Groundwater
Management Associates, Inc. in July, 2019 the higher Chromium concentrations are most likely
associated with the higher turbidity in the samples. NCDWR-WRO is aware of these violations.
The lime was applied in January, 2023 based on the soil samples that were collected in
December, 2022. Please reference the enclosed map for lime application rates. The soil samples
were not collected during 2023 as an oversight. The soil samples were collected in early 2024
and lime will be applied accordingly. Soil samples will be collected again late 2024 to meet the
monitoring requirements for this year.

a
0
b
co
ED
m
z
0
0
-n
N
N
O
O
O
W
0
� b o
� ro
CD 0 ��
F W
C
CD
ro n
p ro
0
'0 p7
0 rn rS
',zs cpo m
add
CD p o
p
CD
o
� CV
p
R.
� n
o ^w w
,co,
O � �
G `Y
O
ID
� p 0
o�
�o
b�
a
s� n pj
rho �'
z
f
p ro
CO
CDID
A
CD
n
ro
L5
v
rw�l
lid
a.
(D
a ro
rr,
r•i�
O
�
�
�
� C
d
r
It
w
a
P-
rn-r
O
o
Co
6
ro
"
�" F1
n
o
cn
CD
�
c
o
Q.
CP

RESIDUAL SAMPLING SUMMARY
AND
LAB REPORT'S

e^•1 f�� M dam" Ef
I
a
p
Wk
MIA
C�
Y
II
II
I�
1�

WayPA®ant,
NALYTICAL
114 OAKMONT DRIVE
GREENVILLE, NC 27858
CMSD (SLUDGE & WELLS ACCT)
CONTEDITNEA METRO. SEWAGE DIST.
MS. RENEE PRIDUSN
P.O. BOX 477
GRI.FTON, NC 28530
PARAMETERS
PH (not to be used for reporting)
Aluminum, (dry wt. basis), mg/Itg
Arsenic (dry wt. basis), mg/kg
Calcium (dry wt, basis), mg/kg
Cadmium (dry wt. basis), mg/kg
Copper (dry wt, basis), mg/kg
Chromium, T.(dry wt, basis),ing/kg
Lead (dry weight basis), mg/kg
Magnesium (dry wt. basis), mg/kg
Mercury (dry wt, basis), mg/kg
]Nickel (dry wt, basis), mglkg
Potassium (dry wt. basis), mg/kg
Seleninm (dry wt. basis), mg/kg
Sodium (dry wt. basis), nig/Ug
Zinc (dry wt. basis), mg/kg
Sodium Adsorption Ratio (Cale)
Total Nitrogen, mg/kg (Cale)
Total Solids, %
TKN (dry wt.), mg/leg
Ammonia Nitrogen (dry wt.),mglkg
Nitrate Nitrogen(dry wt.), mg/kg
Nitrite Nitrogen(dry wt.), niglkg
Phosphorus, T. (dry wt.), mg/kg
Molybdenum (dry wt. basis), mg/kg
Sludge Analysis Method
Sample Date Analyst Code
4.1
05/16/23
JDJ
4500HB-11
18620
05/23/23
MTM
EPA200.7
C 2.5
05/24/23
DRC
3113B-04
18035
05/23/23
MTM
EPA200.7
2.0
05/24/23
DRC
3113E-04
244
05/23/23
MTM
EPA200.7
19
05/23/23
MTM
EPA200.7
17
05/23/23
DRC
3113E-04
7650
05/23/23
MTM
EPA200.7
0.29
05/26/23
DRC
EPA7471B
21
05/23/23
MTM
EPA200.7
11454
05/23/23
MTM
EPA200.7
C 5.0
05/25/23
DRC
3113B-04
3635
05/23/23
MTM
EPA200.7
932
05/23/23
MTM
EPA200.7
5.7
74403
1.63
05/16/23
HMV
254OG-15
c 60960
05/23/23
BMD
351.2 112-93
C 4870
05/22/23
AMC
350.1 R2-93
c 13430
05/23/23
TRJ
353.2 R2-93
c t2.95
05/23/23
TRJ
353.2 R2-93
c $2010
05/23/23
AMC
365.4-74
9.0
05/23/23
MTM
EPA200.7
Drinking Water IDr 37715
Wastewater ID! 10
PHONE [phone]
FAX [phone]
ID# : 41.6
DATE COLLECTED: 05/1.6/23
DATE REPORTED : 06/08/23
REVIEWED BY:
c Uncertified data, ❑WR does not offer non -aqueous certification for this analytical procedure.

In

Orlando, FL
The results set forth herein are provided. by SGS Nortli America I€tc.
Technical Report for
Waypoint Analytical
Contentnea Metro Sewage District; Grifton, NC
416
SGS Job Number: FC6581
Sampling Date: 05/30/23
Report to:
Environment 1, inc
PO Box 7085
Greenville, NC 27835
[e-mail]
TTN: Ann Brown
Total number of pages in report: 15
Test results contained within this data package meet the requirements
of the National Environmental Laboratory Accredltation Program
and/or state specific certification programs as applicable unless noted
in the narrative, comments or footnotes.
e-Hardc opy 2. 0
ff utowated Report
Norm Farmer
Technical Director
Client Service contact: Ariel Hartney 407-425-6700
Certifications: FL(EB3510), LA(03051), KS(E-10327), NC(573), N7(FL002), NY(12022), SC(96038001)
DoD ELAP(ANAB L2229), AZ(AZ0806), CA(2937), TX(T104704404), PA(68-03573), VA(460177),
AL, AK, AR, CT, IA, KY, MA, MI, MS, ND, NH, NV, OK, OR, IL, UT, VT, WA, WI, WV
This report shall not be reproduced, except in its entirety, without die written approval of SGS.
Test results relate only to samples analyzed.
SGS North America Inc. + 4405 Vineland Road + Suite C-15 + Orlando, FL 32811 + tel: [phone] +
SCiS is the snlc audutrity for ettidtot'iz.ing flits +� modifications to this docurnent, Pleuse shave your ideas about
Unuutlrorized mcKlitication ofthis repuvt is strictly prohibited, how wlc ccut serve you flutter at:
1f.etiet� standcttrl terms:tt: 1tttPJ?aevttisgs.corn:en?leans-asid-conditin ns l.f{S.LS.(::u5lct�xeri aFc(zr;tts,cot}t
1 of 15
rceW

Sections:T of tents
3
Section 1: Sample Summary
........ .............
4
Section2: Summary of Hits....................................................................................................
Section 3: Sample Results
.............p
6
3.1 FC65 S 1-1: SLUDGE SAMPLE ..... o....................1.....................................¢
...............
1.2
Section 4: Misc. Forms ..........................................................................
..................................
4.1: Chain of Custody...........................................................................................................
13
2of15
�css�a

SGS North America Inc.
Sample Summary
Way -point Analytical
Contentnea Metro Sewage District, Grifton, NC
Project No: 416
Job No: FC6581
Sample
Collected
Matrix
Client
Number
Date Time By
Received Code Type
Sample ID
This report contains results reported as ND Not detected. The following apples
Organics ND = Not detected above the MDL
FC6581-1 05/30/23 10:00 AE 06/02/23 SO Sludge SLUDGE SAMPLE
Soil samples reported on a dry weight basis unless otherwise indicated on result page.
-
3of45
— ..,.
FUS81

Summary of Hits Page 1 of 1
Job Dumber:
FC6581
Account:
Waypoint Analytical
Project:
Contentnea Metro Sewage Dish�ict; Grifton, NC
Collected:
05/30/23
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
FC6581-1 SLUDGE SAMPLE
Corrosivity as pH 4.0 su
Ignitability (Flashpoint) a > 200 Deg. F
(a) Not ignitable.
SW846 CHAP?
SW846 1020C MOD
4ot15
FC66S9

'la"ILS 12 7 70.�E-'!
Orlando, FL
Sample Results
Report of Analysis
I
5 of 46
FC6561

SGS North America Inc.
Report Of Analysis
Client Sample ID: SLUDGE SAMPLE
Lab Sample ID: FC6581-1 Date Sampled: 05/30/23
Matrix: SO - Sludge Date Received: 06/02/23
Method: SW846 8260D IN HOUSE Percent Solids: 1.5
Project: Contentnea Metro Sewage District; Grifton, NC
Page 1 of 1
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 5E40169.D 10 06/13/23 14:46 JL 06/12/23 12:00 OP97298 V5E1794
Run #2
Purge Volume
Run #1 5.0 ml
Run #2
VOA TCLP List
CAS No.
Compound
71-43-2
Benzene
78-93-3
2-Butanone (MEK)
56-23-5
Carbon Tetrachloride
108-90-7
Chlorobenzene
67-66-3
Chloroform
106-46-7
1,4-Dichlorobenzene
107-06-2
1,2-Dichloroethane
75-35-4
1,1-Dichloroethylene
127-18-4
Tetrachloroethylene
79-01-6
Trichloroethylene
75-01-4
Vinyl Chloride
CAS No.
Surrogate Recoveries
1868-53-7
Dibromofluoromethane
17060-07-0
1,2-Dichloroethane-D4
2037-26-5
Toluene-D8
460-00-4
4-Bromolluorobenzene
Result HW# MCL RL
ND
D018
0.50 0.010
ND
D035
200 0.050
ND
D019
0.50 0.010
ND
D021
100 0.010
ND
D022
6.0 0.010
ND
D027
7.5 0.010
ND
D028
0.50 0.010
ND
D029
0.70 0.010
ND
D039
0.70 0.010
ND
D040
0.50 0.010
ND
D043
0.20 0.010
Run# 1
Run# 2
Limits
98%
83-118%
94%
79-125%
95%
85-112%
100%
83-118%
TCLP Leachate method SW846 1311
MDL
Units Q
0.0031
mg/l
0.020
mg/l
0.0036
mg/l
0.0020
mg/l
0,0030
mg/l
0.0026
mg/1
0.0031
mg/l
0,0032
mg/I
0.0022
mg/1
0.0035
mg/l
0.0041
mg/1
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
MCL = Maximum Contamination Level (40 CFR 261 7/1/11) B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N - Indicates presumptive evidence of a compound
6of15
__. ;_.. FC6501

SGS North America Inc.
Report of Analysis
Client Sample ID: SLUDGE SAMPLE
Lab Sample ID: FC6581-1 Date Sampled: 05/30/23
Matrix: SO - Sludge Date Received: 06/02/23
Method: SW846 8270E SW846 3510C Percent Solids: 1.5
Project: Contentnea Metro Sewage District; Grifton, NC
Page 1 of 1 P
� Is
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 X087374.1) 1 06/19/23 11:42 HA 06/17/23 07:00 OP97389 SX3465
Run #2
Initial Volume Final Volume
Run #1 100 ml 1.0 ml
Run #2
ABN TCLP List
CAS No.
Compound
Result
HW#
MCL RL
95-48-7
2-Methylphenol
ND
D023
200
0.050
3&4-Methylphenol
ND
D024
200
0.050
87-86-5
Pentachlorophenol
ND
D037
100
0.25
95-95-4
2,4,5-TrichlorophenoI
ND
D041
400
0.050
88-06-2
2,4,6-Trichlorophenol
ND
D042
2.0
0.050
106-46-7
1,4-Dichlorobenzene
ND
D027
7.5
0.050
121-14-2
2,4-Dinitrotoluene
ND
D030
0.13
0.050
118-74-1
Hexachlorobenzene
ND
D032
0.13
0.050
87-68-3
Hexachlorobutadiene
ND
D033
0.50
0.050
67-72-1
Hexachloroethane
ND
D034
3.0
0.050
98-95-3
Nitrobenzene
ND
D036
2.0
0.050
110-86-1
Pyridine
ND
D038
5.0
0.10
CAS No.
Surrogate Recoveries
Run# 1
Run# 2
Limits
367-12-4
2-Fluorophenol
32%
14-67%
4165-62-2
Phenol-d5
24%
10-50%
118-79-6
2,4,6-Tribromophenol
63%
33-118%
4165-60-0
Nitrobenzene-6
54%
42-108%
321-60-8
2-Fluorobiphenyl
62%
40-106%
1718-51-0
Terphenyl-d14
70%
39-121%
TCLP Leachate method SW8461311
MDL
Units Q
0,0056
mg/l
0.0098
mg/1
0.050
mg/1
0.0074
mg/1
0.0075
mg/1
0.0050
mg/l
0.0081
mg/1
0.0069
mg/l
0.0050
mg/1
0.016
mg/i
0.0093
mgA
0.020
mg/1
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
MCL = Maximum Contamination Level (40 CFR 2617/1/11) B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
_. 7of15
FC6531

SGS North America Inc.
Report of Analysis
Client Sample ID: SLUDGE SAMPLE
Lab Sample ID: FC6581-1 Date Sampled: 05/30/23
Matrix: SO - Sludge Date Received: 06/02/23
Method: SW846 8151A SW846 3510C Percent Solids: 1.5
Project: Contentnea Metro Sewage District; Grifton, NC
Page 1 of 1
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 CC090380.1) 1 06/21/23 16:36 AF 06/17/23 09:00 OP97390 GCC2371
Run #2
Initial Volume Final Volume
[in #1 10.0 ml 5.0 Jul
Lin #2
Herbicide TCLP List
TCLP Leachate method SW846 1311
CAS No.
Compound
Result
HW#
MCL RL
MDL Units Q
94-75-7
2,4-D
ND
D016
10 0.050
0.017 mg/l
93-72-1
2,4,5-TP (Silvex)
ND
D017
1.0 0.0050
0.0013 mg/l
CAS No.
Surrogate Recoveries
Run# 1
Run# 2
Limits
19719-28-9
2,4-DCAA
79%
39-135%
ND = Not detected MDL = Method Detection Limit 1 = Indicates an estimated value
MCL = Maximum Contamination Level (40 CIiR 261 7/1/11) B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
8of15
MOW

SGS North America Inc.
Report of Analysis
Client Sample ID: SLUDGE SAMPLE
Lab Sample ID: FC6581-1 Date Sampled: 05/30/23
Matrix: SO - Sludge Date Received: 06/02/23
Method: SW846 8091E SW846 3510C Percent Solids: 1.5
Project: Contentnea Metro Sewage District, Grifton, NC
Page 1 of 1 5A
File ID DP Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 ST167645.1) 1 06/20/23 22:23 EM 06/17/23 08:30 OP97392 GST4102
Run #2
Initial Volume Final Volume
Run #1 100 ml 5.0 ml
Run #2
Pesticide TCLP List
CAS No.
Compound
58-89-9
gamma-BHC (Lindane)
12789-03-6
Chlordane
72-20-8
Endrin
76-44-8
Heptachlor
1024-57-3
Heptachlor epoxide
72-43-5
Methoxychlor
8001-35-2
Toxaphene
CAS No.
Surrogate Recoveries
877-09-8
Tetrachloro-m-xylene
2051-24-3
Decachlorobiphenyl
TCLP Leachate method SW846 1311
Result
HW#
MCL RL
MDL
Units Q
ND
D013
0.40 0.00010
0.000022
mg/l
ND
D020
0.030 0.0010
0,00038
mg/1
ND
D012
0.020 0.00020
0.000021
m9/1
ND
D031
0.0080 0.00010
0.000026
mg/1
ND
D031
0.0080 0.00010
0.000020
mg/i
ND
D014
10 0.00020
0.000050
mg/1
ND
D015
0.50 0.0050
0.0021
mg/I
Run# 1
Run# 2
Limits
866/6
42-127%
85%
27-127%
ND = Not detected MDL = Method Detection Limit d = Indicates an estimated value
MCL = Maximum Contamination Level (40 CFR 261 7/1/11) B — Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
-- - 5of15
' K6581

SGS North America Inc.
Report of Analysis
Client Sample 111): SLUDGE SAMPLE
Lab Sample ID: FC6581-1 Date Sampled: 05/30/23
Matrix: SO -Sludge Date Received: 06/02/23
Percent Solids: 1.5
Project: Contentnea Metro Sewage District; Gri€ton, NC
Page 1 of
Metals Analysis, TCLP Leachate SW846 1311
Analyte
Result
HW#
MCL
RL
Units
DF
Prep
Analyzed
By
Method
Prep Method
Arsenic
< 0.10
D004
5.0
0.10
mg/l
1
06/15/23
06/16/23
LM
SW846 6010D 2
SW846 3010A 4
Barium
< 2.0
I1005
100
2.0
mg/l
1
06/15/23
06/16/23
LM
SW846 6010D 2
SW846 3010A 4
Cadmium
< 0.050
D006
1.0
0.050
mg/1
1
06/15/23
06/16/23
LM
SW846 6010D 2
SW846 3010A 4
Chromium
< 0.10
D007
5.0
0.10
mg/I
1
06/15/23
06/16/23
LM
SW846 6010D 2
SW846 3010A 4
Lead
< 0.050
D008
5.0
0.050
mg/1
1
06/15/23
06/16/23
LM
SW846 6010D 2
SW846 3010A 4
Mercury
< 0.0050
D009
0.20
0.0050
mg/1
1
06/15/23
06/15/23
is
SW846 7470A 1
SW846 7470A 3
Selenium
< 0.10
D010
1.0
0.10
mg/I
1
06/15/23
06/16/23
LM
SW846 6010D 2
SW846 3010A 4
Silver
< 0.10
D011
5.0
0.10
mg/I
1
06/15/23
06/16/23
LM
SW846 6010D 2
SW846 3010A 4
(1) Instrument QC Batch: MA19487
(2) Instrument QC Batch: MA19490
(3) Prep QC Batch: MP42389
(4) Prep QC Batch: MP42391
RL = Reporting Limit
MCL = Maximum Contamination Level (40 CFR 261 7/1/11)
- .GS . 10 of 16
FC6581

SGS North America Inc.
Report of Analysis
Client Sample ID: SLUDGE SAMPLE
Lab Sample 10: FC6581-1 Date Sampled: 05/30/23
Matrix: SO - Sludge Date Received: 06/02/23
Percent Solids: 1.5
Project: Contentnea Metro Sewage District; Grifton, NC
Page 1 of 1
General Chemistry
Analyte
Result
RL Units
DF
Analyzed
By
Method
Corrosivity as pH
4.0
su
1
06/07/23 14:47
CC
SW846 CHAP7
Cyanide, Total
< 8.0
8.0 mg/kg
1
06/13/23 11:53
GT
SW846 9012B
ignitabtlity (Flashpoint) a
> 200
Deg. F
1
06/05/23 09:49
CC
SW846 1020C MOD
Solids, Percent
1.5
%
1
06/08/23 12:28
GT
SM19 2540G
Sulfide b
< 13000
13000 mg/kg
1
06/14/23 11:50
ST
SM4500S2- F-11 M
(a) Not ignitable.
(b) Elevated detection limit due to matrix
interference. Manually elevated.
RL = Reporting Limit
11 of 15
FG55F3 i

Misc. Forms
Custody Documents and Other Forms
Includes the following where applicable:
• Chain of Custody
Section 4
1�
_._... 12 of 15
FUS81

Waypofn t
Wnypoint Analyticul - Greenville
CHAIN OF CUSTODY RECORD FM 16r f i
Page I of 1
114 Oakmont Dr.
Greenville, NC 27858
OISINFBCTtON
CHLORINE NELI'MUZEDAT COLLECTION
www.W aypoin€Analydcol.com
Phone [phone] - Fax [phone]
❑ CHLORINE
CLIENT. 416 Week:16
uV
pHCHECKW)
CMSD (SLUDGE & WELLS ACC'O
I
f
c
G
GMAINERTYPUM
CONTENTNRA \iETRO. SEWAGE DIST,
❑ NONE
CHEMICALPRESEIT1+ATi0N
,Nf5. RENEE PRIDGEN
P.O. BOX 417
❑
GRIFTON NC 28530
E
A -NONE D-NAOH
(zsx) 51 t Ss843
B-HNO, E-HCL
aJ.
P1
0-14,60r F-ANCACETATElNAON
COLLECTION
4
¢
$
G-NATHOSULFATE
a
SAMPLELOCATION
©ATE
TIME
Sludge SampleOR
C{ASS)FICATION
C❑ WASTEWATER{NPOES)
❑ COWNOWATER
r
❑ DWR(GW
SW
WE
ff
❑ SWDWASTESECTION
tAl
EL Y
RIFI
AYl
N
CHAIN OF CUSTODY (SEAL) MAINTAINED
OuRIH MENTIOELIVERY
Y N
SAMPLES COLLECTEta BY:
T�E
(Pease P)NQ1 ]
4416.1L ds
d€lfrr
SAMPLES RECEIVED IN LABAT..- J�.°C
li SFIEDBY S .I( ER)
DATERiM�E�
RECE EDIiY SK3.
TEIOME
COMMENTS:
44
T3ELWQVISHEDBY(SIG.)
BY{slts.)
Id n .
PO r Iztn I c�fo02 2
EDBY(sq
OATEIIIME
N Y{SIG.)
TE711ME
4 A / , Coma€or ue1 n!Re a "f.` far emm�nslla sample ar a "G" far
PLEASE READ tnsfructians for camp eiing t ar E e rvers e, n
FORM se -... Grab sample in the blacks above for ouch parameter requested. iv 421846
F C.6581: Chain of Custody
y
Page 1 of 3
13 of 15
FC6se1

SGS Sample Receipt Summary
Job Number: FC6581 Client: WAYPOINT Project: CMSD (SLUDGE & WELLS ACCT)
Elate f Time Received: 612/2023 10:00:00 AM Delivery Method: FX Alrbili #'s: 638072848109
Therm ID: IR 1; Therm CF: -0.1; # of Coolers: 1
Cooler Temps (Raw Measured) °C: Cooler 1: (4.0);
Cooler Temps (Corrected) °C: Cooler 1! (3.9);
Cooler Information Y or N Samole Information Y or €y NIA
1, Custody Seals Present R/I ❑ 1. Sample labels present on bottles W ❑
2. Custody Seals Intact W) ❑ 2. Samples preserved properly W ❑
3. Temp criteria achieved G ❑ 3. Sufficient volumelcontainers recvd for analysis: 1 ❑
4. Cooler temp verification [R Gun 4. Condition of sample I to
S. Cooler media Ice.Ba 5. Sample recvd within HT R ❑
6. DatesrilmesllDs on CCC match Sample Label W
Trio Blank Information Y or N NIA 7. VOCs have headspace ❑ ❑ 91
1. Trip Blank present f cooler ❑ ❑ E/1 8. Bottles received for unspecified tests ❑ ❑�
2. Trip Blank listed on COG ❑ ❑ A 9. Composiling instructions clear ❑ ❑
W S NIA
10. Voa Soil Ki€sldars received past 48hrs? El{❑
or
11. %Solids Jar received? ❑ ❑ 0
3, Type Of TB Received ❑ ❑ F/I 12. Residual Chlorine Present? ❑ ❑ ❑�
Misc. Information
Number of Encores: 25-Gram 5-Gram Number of 5035 Field Kfls: Numbef of Lab Filtered Metals:
Test Strip Lot fts: pH 0-3 J 230320 pH 10-12 Other: (Specify) H 1�0 - 12.0 222221
Residual Chlorine Test Strip Lot M
Comments
Wool Technician: NATHANS Date: 612/2023 10:00:00 AM
R.Y. Date OW24111
Reviewer: Date:
FC6581: Chain of Custody
Page 2 of 3
14 of 15
F06581

Job Change Order:
Requested Dale: 6/8/2023 Received Date:
Account Name: Waypoint Analytical Due Date:
Project Description; Contentnea Metro Sewage District; Grifton, NC Deliverable:
CSR: AH TAT (Days):
Sample #: FC6581-1 Change:
Dept: Analyze total CN and S for reactivity
TAT: 7
SLUDGE SAMPLE.
Above Changes Per: Client
FC6581
602023
611612023
COMMA
7
Dateliime: 618/2023 9:25:04 PM
To Client: This Change Order Is confirmation of the revisions, previously discussed with the Client Service Representative,
Page t of 1
1<C6551: Chain of Custody
Page 3 of 3
16 of 16
FC6581

ro n
n.
m70
n
O rn O C'E 8
z
z
z
rn
.•
Ret
� td 7tl r t� co
trJ
n
w 00Fn e
�x1
°c
�o�COrt �r�
cn
N
0
Z
rs
dp
Ci:cii
w �'
o CIO. 97 o0
F
Qn ow
m
rn
am
�
�
z
Q
m
M
m
�10
TOTAL CHLORINE, mg/I
C7
v�
_
OR ug/I AT COLLECTION
m
o C
Rs
TEMPERATURE,°C
T
S�
AT COLLECTION
o
z
# OF CONTAINERS
f
m
m
m
4i;
O
K
t•.
`..
V ►
mm
1
�
N
W
1
n
PARAMETERS/TESTS
o
_
L L Li�
z
o
z
x
u'
� o
m z r
m
A
m
ri
m
��
F
z rn
0 n
O O m m
"'
m
C)
� j
�7
[rp"
Z _
0 m m 0 C
co
� x
a
-n-
t'
m `r
m
cni
1
M �
zz Cn
<
z
(f
m
O
b
as
O
h
r
u

t

4
d
di
N
�
O
Fa
� U
r
a
Z Z
2
R.
N
y
—s
GLatc�
a
try
�
}
��
Q
Q
aell
r�
w�
Q
o
C6
O
co
Q
�
�
Cd
%
O
U
N
o
Q
14
o�
s
P�-
P, P.
0
CD
0
N
c�
u„
LPL
0
z
w
n

ANNUAL METALS FIELD LOADING SUMMARY FOR"
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: f Total Dry Tons Applied (Annual): 7, nZ
Permit #: 6A=Ickjq Cation Exchange Capacity (non 503 only): rj
Operator: tnw l n-6mi dC,�`jr. Owner: -U)4p��i7 Predominant Soil Series: 6ff)(�
Acres Used: �_. S q Acres Permitted: _ -, qt f Site #: 3 Field #: j
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sainple or
Com-
posite
Date
1
2
6I Z5
3
4
5
6
7
8
9
10
LJ 11
12
% Solids
j - j
j _ -;5t
Arsenic
CZ.1J
Cadmiwn
Z G
Z
Copper
ZQ-q
Chromiwn G
1 Ci
Lead
1-1
Mercwy
Molyb-
denum
�' d
Nickel
Zl
-Zi
Selenium
. Q
65 D
Zinc
a 37—
G3Z
Total
Phos-
horus
57610 1
5Za+ o
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
1 Event
App-
MEN
NONE,
®•
I
�6�_______��
NOW
1
�11
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel property gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Sigi.ature of Land Applier Date
DENR FORM MFLSF (12/2006)

W
cv
0
U
U3
Ps
N
rn
tj
aG c©�
wU
U
7
Id
V�
9
s.
al
Y-
Cd
0
1
"d,
�
k
0
m
,
U
Cd
W
U
O O
Caw ,L.i
U
Qi
4
d �i-
q ` d
ac 0 x-
Z
0
a
(V
(V
O
Li
z
LU
Q

ANNUAL METALS FIELD LOADING SUMMARY FORME
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Total Dry Tons Applied (Annual):
Permit #: Cation Exchange Capacity (non 503 only):
Operator: Owner: ('C,n+epy.(ne#_ r laO Predominant Soil Series: ?Q(I�p�U
Acres Used: Z-oz, Acres Permitted: Z_(az Site #: -b Field #: 2.
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample or
Corn-
posite
Date
1
2
3
4
5
6
7
s
9
10
11
12
% Solids
.b'I
Arsenic
e-
<Z.
Cadmium
2- D
Z.
Copper
Lqa
/-44
chrom! le7
Gl
Lead
1�)
0
Mercury
0, Tq
D. z
Molyb-
denrux
ct • D
61, D
Nickel
Z!
V
Selenium
5, D
<�5B
zhic
q &z
a -&z
Total
Phos-
lror•us
162016
1 5W10
Annual Heavy Metal Field Loadings (Calculated in lbslacre):
r I
�
mom
Total
Phos-
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for luiowing violations".
Signature of Land Applier Date
DENR FORM MFLSF (1212006)

�_
0
6
U 41 hil
N
�
YY�ll
rn
�
P-I
2�Yi 1rc
V.p
y
h
(D
N
ry+�
v
OCOG
O
O
h1j.,jVk
(a-}-
�1-ca e,.
kl7J(
Gs
JN
-v-ax�rtsx
�
12
u
o
x
0
d
O
p
o
N
(�..�
H
�
U
P,
P,
w
0
0
"a
O
LL
w
0

ANNUAL METALS FIELD LOADING SUMMARY FORM'
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: (Y1>y7 Total Dry Tons Applied (Annual): rf (p,��}
Permit #: Cation Exchange Capacity (non 503 only): L115
Operator: ate }�l�cc)iCly /" - Owner: CMVer4nea— I`(I67 Predominant Soil Series: Pbf&nM,q_0
Acres Used: 7_ •'?Z Acres Permitted: V? Z Site #: 3 Field #: 3
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample or
Coin-
posite
Date
1
6-11:Z3
6-16-43
3
4
5
6
7
8
9
10
11
12
% Solids
[. 6`)D
Arsenic
< Z
< Z, 6
Cadinhun
Z•
Copper
7f (4
ZW4
Chroiniuin I q?
) ri
Lead
I-1
11
Mercury
Q," '1
p, Z5l
Molyb-
denum
q ,
Nickel
Z I
ZI
Selenium
< 5. t)
< 5. 6
Zinc
3Z
Q �jZ
Total
Phos-
horas
16WI6 162DO
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Event
MENEM
_
d
00000
00
mom
WIRMr
•
r w
MIM
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for luiowing violations".
Signature of Land Applier Date
©ENR FORM MFLSF (12/2006)

�I
SAS
N
4<
O ff a
d)
q
U
a
N
s� m
v
p
P
51
-Ftii�7F?i3c
041
'7
Gs
QIc,P
oar
U
4f1
4�
r�
°
r
U
�
N
U )2
1
o 0
U
�
O
env r
aL
0
.
a�
Q
9b
a
0
N
N_
LL
L4
Q'
0
z
LLJ

ANNUAL METALS FIELD LOADING SUMMARY FOR1VV
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: e3_)�neal rn6-j) Total Dry Tons Applied (Annual): Lk (per
Permit H. U_)Q0CoL C w+ Cation Exchange Capacity (non 503 only): �.
Operator: CiYxcl ,�,5 , c�;T[. Owner: bn�0`4n6JL01`}6-_D Predominant Soil Series: -�u5
Acres Used: �,� tf Acres Permitted: 33- "Zlq Site #: _B Field #• 9
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample or
Com-
posite
Date
1
2
3
4
5
6
7
B
9
10
11
72
% Solids
l-�3`>a
�•
Arsenic
CZ.5
<2,05
Cadmimn
Copper
I L44
Zak
cm'omim-n G
G'
Lead
j
Mercwy
p.Zcf
D.
Molyb-
denum
G
G'. D
Nickel
{
Zi
Selenium
<5. t)
<6. D
Zinc
L -i
q3z.
Total
Phos-
hoius 15WI05-W
i d
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total©
Event•
s
©
©
©
©
f7
©
Q7
Total
phorus
certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
oY
Signature of land Applier Date
DENR FORM MFLSF (12/2006)

i�
x
N
0
cd
ro
2p,
U .� R
i3
a �
o
U
��,
p
o
O
w
Z
O
(1
OrVO.T
�
J
a�
�U ors
�rh
0 0
—
�
O
O
0 v7
uz
o
04

ANNUAL METALS FIELD LOADING SUMMARY FOR"
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: _L4nPaf),O Total Dry Tons Applied (Annual):
Permit ##: o
Catr n Exchange Capacity (non 503 only): (_j,• 5
Operator: Owner; (()r)tef 4rxq3- ff6:0 Predominant Soil
Acres Used: ;�,�[�. Acres Permitted; 3.7 t-i Site #: ij Field #:
Residual Analysis Data (Heavy Metals and Total Phosphorus use mgflcg, % Solids use Raw Percent ft
Sample or
Com-
posite
Date
1
2
3
4
5
6
7
8
9
10
11
12
% Solids
Arsenic
<
Cadmium
Z- UU
Z �%
Copper
14
Clu•oznium I q
Lead
11
f ~?
Mercluy
Molyb-
denum
b
Q • b
Nickel
j
Zi
Selenium
1 ti5, D
Zinc
Z
03 z
Total
Phos-
hor is
5-Z;61 0
Lb U
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
EventSWAi
NONE
N "-w
►' r
__________
• is
"t certity, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for Knowing violations".
C -,
,Signature of Land Applier Date
DENR FORM MFLSF (12/2006)

clq
k
V
N
�y
cd
p y O
H
V
U
N
� U
Y
Savo
a --.Xi
U5
E
c]
0
C
Al 1 lx c.
0
Q
i
�
F�t
6161
rn ;,
b p
49
Q
m�
r�
rw�
P4U
�
o
�
l
Cd
o
0
o
q
cd
as
Ao�

ANNUAL METALS FIELD LOADING SUMMARY FORMV
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: e6n "(7 Total Dry Tons Applied (Annual): . 31Z
Permit #: 1.Jnj m 1 g Cation Exchange Capacity (non 503 only):
Operator: Ghade)lfl baAua, Owner: ��t� _,( " [7 _ Predominant Soil Series:
Acres Used: Ace es Permitted: `7:3 ` Site #: _ (qc4- I[_ Field #:
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/leg, % Solids use Raw Percent #):
Sample Or
Com-
posite
]date
1
! 3
L3
5
S
7
8
9
10
11
12
% Solids
J.
f -L5�b
Arsenic
C v5
Cadmium
2.0
2. D
Capper
7 qtp�((
a romirun j C/
1 a
Lead
Mercury
D.Z�
0• ZC!
Molyb-
dentun
�• !�
C(• b
Nickel
,Selenium
• C7
C . o
Zinc
Total
Phos-
honis
7Ofd
010
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
D1
p
E vent
MOM
"I eertiiy, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
6 /�44
Signature of Land Applier Date
DENR FORM MFLSF (12/2006)

ANN
nj
Uc�
wbn
o
U
N
�
w
a
�N
a�
boo
<)
2h�i�
co
a�
Np
N
0
m
+n
CIO
T
N
pk
a
Ct)
o
-0
N
P
O
o
7F
m �
z
�ap�
a
a
LL
Ll-
CK
0
Z
w
0

ANNUAL METALS FIELD LOADING SUMMARY FORA?
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Total Dry Tons Applied (Annual): 9.25Z
Permit #: Cation Exchange Capacity (non 503 only): 14- S
Operator: ChGE1�5i� �iYl!'1 111�1C�}` K Owner ���/-)e.0—D(j�Predominant Soil Series: AjctoiCL
Acres Used: 6.1rj Acres Permitted: ,51 Site #: C-TCac� j Field #:
Residual Analysis Data (heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample or
Com-
posite
Date
1
54 3
2
3
4
5
6
7
8L-9j
110111
12
% Solids
1. �
Arsenic
<
Cadlniuln
Z• b
Z- 0
2- D
Copper
4
Z 4
Z
Chromium p c(
l ci
C Ci
Lead
t')
1`1
l)
Mercury
Q, )
O,ZC
Q Zr'1
Molyb-
demmn
q b
C.4
Nickel
!
DZ4
Selenium
<5, d
� . d
Zinc
G3Z
G3Z
q3z
Total
Phos-
ho111s
ZOO
'Szolo
0
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
1
2
3
4
51
L-6j
8
9
10
11
42
DT/Ac./
App
Event
C3 Z
p,j Cp
0 41OZ
d
Arsenic
C).e >t
Cadmium
o. UU3
O.W l
0 .t)0
p.Li�Co
Copper
0-3� (a
p .l")LI
0- L5
Chroinsu
0,05 ,
0•UlC4
ov(1
a•C>
Lead
p.b
D.o1Z
c)-a t,
a+ ��
Merew-Y
0-boo
0,0b0
10.UDO
6.wo
Molyb-
denurn
0,019
0.61) U
0-tbg
0� GZg
Nickel
0,03
0,01r
©.OIG
O.
Selenium
0, Q
0�&b t-I
0•OO5
Zinc
i. {6
p, u
G +4s l
o3•G� 1
Total
Phos-
lsorus
1
......................
"I certify, udder penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for linowing violations".
— ZZ14 W 4�� C, P� -
Signature of Lased Applies 10r Date
DENR FORM MFLSF (12/2006)

a
M
clq
0
V
U
Q
v
N
a
� U
m
U
rn
o�
lo
I
�
p
q
�
O
r
Wk
'il 1 11 c
Q
�
d
n
co
9
p
o O
�
U
�
O
v
fil
N

ANNUAL METALS FIELD LOADING SUMMARY FORM'
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Con lfl(2iD Total Dry Tons Applied (Annual): ;7, - {Iq
Permit #: 404q Cation Exchange Capacity (non 503 only): q.15
Operator: CbOyle - i CLJ, .Owner: (�r-y�� ��� 1� Predominant Soil Series; +}
Acres Used: 3. oo Acres Permitted: 63 00 Site #: _ �} Field #: 14
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample or
Coln-
posite
Date
1
Z3
2
3
4
5
6
71
8
9
10
11
92
% Solids
Arsenic
Cadrniwn
Z • 0
Copper
-,q(f
Chroinivan i C)
Lead
0
Mercury
&,
Molyb-
denum
D
Nickel
j
Seleniwn
Zinc
gj3-z
Total
Phos-
phorus
5z6I6
Annual Heavy Metal Field Loadings (Calculated in s acre):
Total
DAe./
pp
1
p•�f0�
2
3
4 V
5
6
7
8
9
10
11
i 2
fl-
Arsenic:Event
,005
D,
Cadmiwn
C),Wq
I
0,6bl
Copper
Q t4tpz
(3 - t Z
Chromi
, b3
0.634
Lead
6.&3 I
a.03 f
Mercury
l
Molyb-
denw-n
.Oi
.Oi G
Nickel
Gp
Selenium
6,60q
Zinc
Total
Phos-
homs
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Signature of Land Applier Date
DENR FORM MFLSF (12/2006)

per.
T
N
d5
0
V
vi
b4,
d
v
o
V
r
a�
0
�
�
�►
�
V'J
v�i�t�i
a
p
O`n
ow
��
ro
w a
NNN
U
CT
�
w
-..
co �
R ` �
r
Se
a •�
o
CIO
_
PA
O
O a
ID
cJ
U
p-1
1-4
n^�
I-s
r'�.�,

ANNUAL METALS FIELD LOADING SUMMARY FORM"
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: ('�n j}[ l 17 Total Dry Tons Applied (Annual): 7.-? (':�'
Permit #: Cation Exchange Capacity (non 503 only): fL6
Operator: Owner: Psl�ne�-r,:�� _ Predominant Soil Series: Pp/�
Acres Used: Acres Permitted: Z.3�2 Site #: D Field ##:
Residual Analvsis Data (Heavv Metals and Total Phosphorus use mg/leg, % Solids use Raw Percent #):
Sample or
Com-
posite
Date
1 V
�3
3
5
6
7
8
9
10
11
12
% Solids
Arsenic
Cadmium
�• v
Copper
zuq
Chromium l
Lead
1
Mercury
.2G
Molyb-
denum
q- b
Nickel
I
Selenium
<<j. D
Zinc
a 3Z
Total
Phos-
phorus,
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
DT/Ac.l
App.
Event
1
1-14Z
2
3
4 W
5
6
7
8
S
10
11
12
Q
p .1 Z
Arsenic
j) LW(-
a,
Cadmium
0 pU
Copper
0 <55"J
Cluomit
D_OL43
Lead
0,p3Q
Mercury
0,001
Molyb-
denum
0•Q I
Nickel
o L.4
Selenitun
, 51 1
zhic
l ZG
Z i q
Total
Phos-
horas
114?�t I
ilk°
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
X am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Signature of Land Applier Date
DENR FORM MFLSF (12/2006)

U
a
a
N
O
�
U
U
N
a�i
a �
o
U
pq34
U
O
44
,o
N
�
�
o
Rz��raP94
a
Et�ti i �
x
\
O
Q
c
d
r
p
m
W110
O
O
0
©
Q
OJ
F-+

ANNUAL METALS FIELD LOADING SUMMARY FOR"
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: (,'@�f f i;) !7 Total Dry Tons Applied (Annual): L. �7�
Permit #: uoCtac4q _ Cation Exchange Capacity (non 503 only): q_Ij
Operator: C Ae�rn'6mI /. Owner: (�Cr)j 1,y� Predominant Soil Series:��
Acres Used: Z. q g Acres Permitted: Z-c-t 'O Site #: P Field #:
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/lcg, % Solids use Rave Percent ft
Sample or
Com-
posite
Date
�� Z
2
3
4
5
6
7
8
9
10
11
12
% Soiids
Arsenic
<Z.5
<Z,,5
Cadmium
Z
Z-d
CopperE04
Z44
Chromium 4
lQ
Lead
l7
n
Mercu►y
(}. �l
0•Z
Molyb-
denum
C1II5
Cl
Nickel
i
t
Selenium
Zinc
G3Z
�3Z
Total
Phos-
hows
5W) D
5 Z610
Annual Heavy Metal Field Loadings Calculated in lbs/acre):
Event
r.•
►R�liiiiitii�Si7iiil��ii�
� �
_�__�__�__���
�
NMI
1
� 1
"I certify, under penalty of law, that this document was prepared under my do ect►on or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of Imes and
imprisonment for luiowing violations".
Signature of Land Applier Date
iDENR FORM MFLSF (12/2006)

a
N Q
0
N
2
w
a
6
M
W
6
o
o�"3
y
O
�
ko
616101
� V
9
y
� Scy)zl-1
o
p.
o
0
�6 <711
O
Qi
U
a
0
0
N
N
LL
iL.
O
L3_
LU
0

ANNUAL METALS FIELD LOADING SUMMARY FORM
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Total Dry Tons Applied (Annual):
Permit #: mxpl C" Cation Exchange Capacity (non 503 only):
Operator: it )0-60,, Owner: Predominant Soil Series:
Acres Used: j, 691 Acres Permitted: d3. (�Z Site #: 'D Field #: I-7
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample of
Com-
posite
Date!
1
2
3
`
6
7
8
9
10
91
92
% Solids
Arsenic
CZ5
Z
Cadinium
Z. v
.v
Capper
ZJ4q-
Z
Chroinimn j '
Iq
Lead
11
n
MercLny
p.Z�r
GZ�I
Molyb-
denum
Nickel
Selenhult
< .
zinc
3Z
G{ Z
Total
Phos-
honis
16W JO
I 67DIO
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
yj
Total
Phos-
phortis
MENNEN
�►
"I certify, under penalty of law, that this document was prepared under my darectaou or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
de-4 W.2111-1sly
Signature of Land Applier Date
DEER FORM MFLSF (12/2006)

a
°J
[j
1-1
Q
TA
I ai
�n
Sv
�
C!a
o
O
CU
r
4
�'J
nn
6161
CD
(].i F-1
U d
^n
1
1{
U
w
a
y o
o
o10
00
q cr
p
G
�o
ua
PH
a
0
0
N
N
U
U-
Lc�1.
C
O
Z
w

ANNUAL METALS FIELD LOADING SUMMARY FORW
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Total Dry Tons Applied (Annual): 1. (Z j
Permit #: 14)),QQD IC49 Cation Exchange Capacity (non 503 only): 4.5
Operator: bli Owner: �'C�} r} (� yi�[� Predominant Soil Series:—AK+�kj
Acres Used: T Q_Z Acres Permitted: I-L(Z Site #: 'D Field #: 153
Residual Analvsis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample or
Com-
posite
Date
1 V
-�
2
3
4
5
6
7
8
9
10
11
12
% Solids
Arsenic
Cadmium
Z-D
Copper
I Z44
Chromiwn 19
Lead
(�
Merewy
Molyb-
denum.
Nickel
Zj
Selenium
<S
Zinc
�p3
Total
Phos-
horus
,c,
5-W 1
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
DT/Ac./
App,-l4s-Z3
Event
1
C Go LI
2
3
4
5
6
7
8
9
10
11
12
Arsenic
p,005
3
Cadmimn
0 .tO3
a `
Copper
6_3629
O.Z�
C}norni
b . bZ(,
Lead
p )Z3
C9
Mercau-y
D . 000
fs• C
Molyb-
denum
�,bl�
t5•D1Z
Nickel
Selenium.
7
C)o
,Zinc
1, 5 Ep
t-Z5�
Total
Phos-
honis
f D.)
76, 09
"I certify, under penalty of law, that this document was prepared under my direction or supervision m accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for lmowing violations".
Signature of Land Applier Date
IIFNR FORM MFLSF (1212006)

u
p
N
Lf
U
Cc
aA
v
a,
A
��.
��r�
KD
O
�
0
ap.+
�
� U0
�
o
�
O
O
�
r
�
0049
Q
l�
a
Q+ �
�]
o ro
�
�w
'd
.o •�
a `� C7
a�
as
A
b
a
4-i
Q
0
0
N
LL
EL
Of
z
w
O

ANNUAL METALS FIELD LOADING SUMMARY FOR"
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: t {1`OI� Total Dry Tons Applied (Annual): Z Qf /-)
Permit #: Cation Exchange Capacity (non 503 only): 5
Operator: �' {j n}-btns�l f Owner: Predominant Soil Series: �.
Acres Used: t 17'� Acres Permitted: ) .�5 Site #: Field #:�_
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample o1
Co111-
posite
Date
1
2
3
4
5
6
7
8
9
10
11
12
% Solids
Arsenic
< .5
Cadznirun
- 0
Copper
L44
Chrorniwn I�
Lead
Merculy
Molyb-
denum
Nickel
Sele,"hun
Zinc
cj
Total
Phos-
lhorus
57DIC)
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
DT/Ac./
App.
Event
1
2
3
L4J
5
6
7
&
S
10
11
12
Arsenic]
[
Cadrniurn
fj-tb
t
Copper
, )C)
clu-omiuly
0.4 b4
Lead
0,7
07
Mercury
p.pD
1
oa
Molyb-
deawn
t%
b•Ob�
Nickel
0,6t)9
a.CUq
Selerliwn
60'2-
1
6"5c;z
Zinc
�•3�6
D•3S�
Total
Phos-
horus
ZI-�3
Zf-63G
"I certify, under penalty of lave, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel property gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
4'' l 4k�
+ a+
Signature of Land Applier Ap Date
DENR FORM MFLSF (1212006)

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: f mJ /i� WQ Permit Number: (fC
yfq
_ `(�� _ � I7 NPDES Number:
WWTP Name: fi(�jO�ZL�7i
Monitoring Period: From C(N I e Z02,3 TojKfj _y 1, zD73
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. A (timeltemp) ❑ I
Alt B (Alk Treatment) ❑ Alt. C (Prior Testing)❑
Alt.D (No Prior Test) ❑
Process to Further Reduce Pathogengs ❑
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost ❑
Heat Drying ❑
Heat Treatment ❑
Thennopbilic ❑
Beta Ray ❑
Gam na Ray Cl
Pasteurization ❑
Class B:
Alt. (1) Fecal Density
Alt. (2) Process to Significantly Reduce Pathogens ❑
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization ❑
Air Drying ❑
Composting ❑ jAcrobic
Digestion
Anaerobic Digestion ❑
If applicable to alternative performed Class A or Class B) complete the following monitoring data:
t Densien .Number o na yhoa
Allowable Level Pathogen Frequency Sample
13xcee- Tech -
Parameter
in Sludge Minimum Geo. Mean Maximum Units deuces of Analysis Type rri ue
2 x 10 to the MPN
t Z
Z
rnW
G
Qh
GZZ) L
14
6th power
lids
per grain of
Fecal Coliform total solids CFU
1000 mpn per gran,
of total solid (dry
weight)
Salmonella bacteria 3 MPN per 4 grams
(in lieu of fecal total solid (dry
coliform) weight)
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed:
Alt, I (VS reduction) ❑
Alt, 2 (40-day bench) ❑
Alt, 3 (30-day bench) ❑
jAlt. 4 (Spec. 02 uptake) 10
Alt. 5 (14-Day Aerobic) ❑
Alt, 6 (All, Stabilization ❑
Alt 7 (Drying - Stable) ❑
I Alt. 8 (Drying - Unstable) ❑
Alt, 9 (Injection) ❑
Alt, 10 (incorporation) ❑
No vector attraction reduction alternatives were performed ❑
CERTIFICATION STATEMENT (please check the appropriate statement)
[ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1I06 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
❑ "I certify, under penalty of law, that the pathogen; requirements in 15A NCAC 02T 1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note
if you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
r�II i n cP-C.
Prepare�me and `nit e (type or print)
��
res*
Signature of PrepaDate
Land Applier Name and Title (if applicable)(type or print)
s'W
Signature of Land Applier V(if applicable) Date
*Prepares is defined in 40 CFR Part 503,9(r) and 15A NCAC 2T ,1102 (26)
DENR FORM PVRF 02T (12/2006)

CMSD (SLUDGE & WELLS ACCT)
CONTENTNEA METRO. SEWAGE DIST.
MS. RENEE PRIDGEN
P.O. BOX 477
GRIFTON, NC 28530
PARAMETERS
Total Residue, mg/l
Fecal Coliform (MPH /gram Solids
Sample Analysis Method
N1 Date Analyst Code
16780 05/17/23 HMV 2540B-15
77 05/15/23 BNC 9221E-14
Drinking Water ID; 37715
Wastewater ID; 10
PHONE [phone]
FAX [phone]
xD#: 416 A
DATE COLLECTED: 05/1.5/23
DATE REPORTED ; 05/24/23
REVIEWED BY:

CMSD (SLUDGE & WELLS ACCT)
CONTENTNEA METRO. SEWAGE DIST.
MS. RENEE PRIDGEN
P.O. BOX 477
GRIFTON, NC 28530
PARAMETERS
Total Residue, mg/l
Fecal Coliforin (MPN), /gram Solids
Sample Analysis Method
#2 Date Analyst Code
16900 05/17/23 HNIV 2540B-15
12 05/16/23 BLV 9221E-14
Drinking Water IDs 37715
Wastewater ID: 10
PHONE [phone]
FAX [phone]
ID# : 41.6 A
DATE COLLECTED: 05/16/23
DATE REPORTED : 05/24/23
REVIEWED BY:

CMSD (SLUDGE & WELLS ACCT)
CONTENTNEA METRO. SEWAGE DIST.
MS. RENEE PRIDGEN
P.O. BOX 477
GRIFTON, NC 28530
PARAMETERS
Total Residue, mg/l
Fecal Coliform WN), /gram Solids
Sample Analysis Method
#3 Date Analyst Code
15900 05/17/23 lam' 254OB-15
82 05/17/23 BGV 9221E-14
Drinking Water ID: 37715
Wastewater IDt 10
PHONE [phone]
FAX [phone]
ID#: 416 A
DATE COLLECTED: 05/17/23
DATE REPORTED : 05/24/23
REVIEWED BY: ✓✓�

•
Wayp®I nt ,a
ANALYTICAL
114 OAKMONT DRIVE
GREENVILLE, NC 27858
CMSD (SLUDGE & WELLS ACCT)
CONTENTNEA METRO. SEWAGE DIST.
MS. RENEE PRSDGEN
P.O. BOX 477
GRIFTON, NC 28530
PARAMETERS
Total Residue, mg/l
Fecal Coliform (MPN), /gram Solids
Sample Analysis Method
#4 Date Analyst Code
15300 05/24/23 JDJ 2540E-15
44 05/18/23 JDJ 9221E-14
Drinking Water IDS 37715
PqWrOL5) �t&V208
FAX [phone]
ID#: 416 A
DATE COLLECTED: 05/18/23
DATE REPORTED : 06/06/23
REVIEWED BY:

CMSD (SLUDGE & WELLS ACCT)
CONTENTNEA METRO. SEWAGE DIST.
MS. RENEE PRIDGEN
P.O, BOX 477
GRIFTON, NC 28530
PARAMETERS
Total Residue, mg/i
Fecal Coliform (MPH /gram Solids
Sample Analysis Method
#5 Date Analyst Code
14760 05/24/23 JDJ 2540E-15
C 12 06/05/23 JDJ 9221E-14
Dr�i7n_►kyiin�gg Water IDg; 337771p5
E-F""1VEVE-M 756-0008
FAX [phone]
ID#: 41.6 A
DATE COLLECTED: 05/22/23
DATE REPORTED : 06/06/23
REVIEWED BY:

o
WayPA®ant.,.
0
NALYTICAL
114 OAKMONT DRIVE
GREENVILLE, NC 27858
CMSD (SLUDGE & WELLS ACCT)
CONTENTNEA METRO. SEWAGE DIST.
MS. RENEE PRIDGEN
P.O. sox 477
GRIFTON, NC 28530
PARAMETERS
Total Residue, mg/l
Fecal Coliform (MPN), /gram Solids
Sample Analysis Method
#6 Date Analyst Code
15000 05/24/23 JDJ 254OB-15
C 12 05/23/23 ADR 9221E-14
Drinking Water ID: 37715
PFTNr(6) �W&V208
FAX [phone]
ID# : 41.6 A
DATE COLLECTED: 05/23/23
DATE REPORTED : 06/06/23
REVIEWED BY:

WaypA® nt..,
NALYTICAL 0
114 OAKMONT DRIVE
GREENVILLE, NC 27858
CMSD (SLUDGE & WELLS ACCT)
CONTENTNEA METRO. SEWAGE DIST.
MS. RENEE PRIDGEN
P.O. BOX 477
GRIFTON, NC 28530
PARAMETERS
Total Residue, mg/l
Fecal Coliform (MPN), /gram Solids
Sample Analysis Method
#7 Date Analyst Code
14080 05/24/23 dD.1 2540B-15
32 05/24/23 HMV 9221E-14
Drinking Water ID: 37715
PFTNrag�) �62&08
FAX [phone]
ID#: 416 A
DATE COLLECTED: 05/24/23
DATE REPORTED : 06/06/23
REVIEWED BY: / '�

0
Specific Oxygen Uptake Rate
SOUR
Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Facility Name
Biosolids Permit Number
Date
Digester Temperature
Sampling Date/Time
Sampled By
Analysis Date/Time
Analyzed By
Total Solids
Beginning Temperature
End Temperature
Dissolved Oxygen Level
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
)ry Solids
rees Celsius
tees Celsius
0.05
8.1
0.97
2.79 mg Oxygen/hr
0.17 mg Oxygen/hr/g
20 degrees Celsius
1.00
Temperature Corrected Specific Oxygen Uptake Rate: 0.17 mg Oxygen/hr/g
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.
Updated 10/23/2013

R
rel
u
d; N co co Co d
co co ti ti ti
(116w) uoBAxo panlossip
i
i

z
Specific Oxygen Uptake Rate
SOUR
Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Facility
Biosolids Permit N
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
048
raves uunn
nn
65 %Dry Solids
19 degrees Celsius
20 degrees Celsius
0.08
8.3
1.00
5.03 mg Oxygenlhr
0.31 mg Oxygenlhrlg
20 degrees Celsius
1.00
w
Temperature Corrected Specific Oxygen Uptake Rate: 0.31 mg Oxygenlhrlg
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.
Updated 10/23/2013

F
U
CL
O
Iq co LO F-
co ti
(116w) uoBAxp POAJOSsI❑

3
Specific Oxygen Uptake Rate
SOUR
Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Facility Blame:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time,
Analyzed By:
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
IVISD
100001048
5117
-17-231085C
ravis Dunn
-17-231115C
ravis Dunn
1.62 % Dry Solids
20 degrees Celsius
20 degrees Celsius
0.09
8.1
0.98
5.37 mg Oxygenlhr
0.33 mg Oxygenlhrlg
20 degrees Celsius
1.00
Temperature Corrected Specific Oxygen Uptake Rate: 0.33 mg Oxygenlhrlg
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.
Updated 10/23/2013

rn
N
N
00
Oj
Oj
00
0
O
FOR
r"
Lo,
C� 06 C¢ LO VT M
(I/6W) UOBAXp panlossla

y'
Specific Oxygen Uptake Rate
SOUR
Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
% Dry Solids
degrees Celsius
degrees Celsius
0.08
8.5
0.98
4.78 mg Oxygenlhr
0,29 mg Oxygenlhrlg
19 degrees Celsius
1.07
Temperature Corrected Specific Oxygen Uptake Rate: 0,31 mg Oxygenlhrlg
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically,
Updated 10/23/2013

irm
U
d
d
CL
c
Q
a
x
A
c0 (O 00 a0 (Q IT cV 00 (O
c0 Oa 00 00 [-� I- r-: (O (O
(11OW) UGBAXp POAJOssiCI

5
Specific Oxygen Uptake Rate
SOUR
Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Facility Name: CMSD
Biosolids Permit Number: WQ000104f
Date: 512,
Digester Temperature:
Sampling Date/Time: 5-22-231142
Sampled By: Travis Dunn
Analysis Date/Time: 5-22-231143
Analyzed By: Travis Dunn
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
1
59 % Dry Solids
20 degrees Celsius
21 dearees Celsius
5.17 mg Oxygenlhr
0.32 mg Oxygenlhrlg
21 degrees Celsius
0.95
Temperature Corrected Specific Oxygen Uptake Rate: 0.31 mg Oxygenlhrlg
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.
Updated 10/23/2013

RIM
co L
c
(I/Om) ua6Rxo peAlossi❑

Specific Oxygen Uptake Rate
SOUR
Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Facility Name: CMSD
Biosolids Permit Number: WQ00
Date:
Digester Temperature:
Sampling Date/Time: 5-22-2
Sampled By: Travis
Analysis Date/Time: 5-23-2
Analyzed By: Travis
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
Slope:
I ntercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
5/23/202
1
311125
Dunn
311129
Dunn
% Dry Solids
degrees Celsius
dearees Celsius
I. -
3.88 mg Oxygenlhr
0.24 mg Oxygenlhrlg
20 degrees Celsius
1.00
v�
Temperature Corrected Specific Oxygen Uptake Rate: 0.24 mg Oxygenlhrlg
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.
Updated 10/23/2013

FQ
r•1
op Iq lP N 00 00 CO
00 0o co co ti t-_:
(I/F)W) UOBAXp panlossl©
INN

Specific Oxygen Uptake Rate
SOUR
Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Facility dame: CMSD
Biosolids Permit Number: WQ0001048
Date: 51241
Digester Temperature:
Sampling Date/Time: 5-24-2311406
Sampled By: Travis Dunn
Analysis Date/Time: 5-24-23/1409
Analyzed By: Travis Dunn
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
59 % Dry Solids
19 degrees Celsius
20 degrees Celsius
0.08
8.5
0.98
4.60 mg Oxygenlhr
0.29 mg Oxygenlhrlg
20 degrees Celsius
1.00
Temperature Corrected Specific Oxygen Uptake Rate: 0.29 mg Oxygenlhrlg
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.
Updated 10/23/2013

ry
c0 14: N oo co Qo N
00 00 00 h ti ti
(I16M) UOBAXp panlossla
i

LAN J'a
� Moff.
WMA 1 *01 oil'

G W-59A COMPLIANCE REPORT FORM permit fl JtQj-e
(Yubinit one each monitoring period with. GW 59 forins )
Enter date monitoring results were due. (I! Z3 ) Will this monitoring report (GW-59 and OW-59A)
YES
NO
be submitted after the established due date?
2
Was airy required information massing on the GW-59 report forms?
YES
�O
1F the answer to question I or 2 is "YES", list in the space provided below the well identification number(s) and
explain the problems encountered in obtaining the required information.
3
Are any of the monitor wells in need of repair or maintenance (damaged casing, unlocked or rrrissing cap, missing
YES
NO
identification plate, area overgrown, etc.)? If the answer is "Yes", contact the Regional Officefor guidance.
q
Are any monitored constituents equal to or above the established standards?
S
NO
If the answer to question 4 is "NO', skip to section 8.
If the answer to question 4 is "YES" list the affected wells individually with constituent(s) and concentration(s)
exceeding standards in the space provided below,'
L3P1
Z3 I ch(c)m i udn I Z
w� io
5
For the constituents identified in question 4 above, have standards been exceeded previously for the
YES_
NO
same constituent(s) in the same well(s) in the last two years?
If the answer to question 5 is "NO", ship to section 8.
If the answer to question 51s "YES") list in the space provided below, each welt with constituent(s) exceeding
standards, concentration(s) reported, and sample collection date for each occurrence (for the last two years).
Lf -V IL
io 71j Zi —TG c�ICWp'lit tyn 70 Qqj'
14, Y)
Are the monitoring wells listed in section 5 located at or beyond the review boundary?
YES
N, Q
x
If the answer is "YES'; a groundwater quality problem maybe occurring. CONTACT THE REGIONAL
OFFICE IMMEDIATELY FOR GUIDANCE. If the answer is 'WO", monitoring wells maybe Improperly
located; contact the Regional Office.
7
is the permittee implementing previously approved actions required by the Division involving this
S
NO
groundwater quality problem?
If the answer to question 7 is 'YES", describe those actions in the space provided'below.
If the answer to question 7 is "NO" contact the Rogional Office within 90 days; an evaluation may be
required to determine the impact the waste disposal system is having at the review and compliance
boundaries surrounding this facility, Failure to do so may subject the permittee to a Notice of Violation
fines and/or penalties.7 eTG(—' IeLge I *,�)'''6AU(C-t t l'4ir) �)I lt��l�i�r�.'ft?l
C_i� �C) ! r7 � -he i `� - e xc�t �i tCur $ `let' �2Jh��`! � j ! ► G l
�7uly,Zdf��Nti�hl i)t'(Cl.,rornjUIi�r � ��
ley 1 Chi P
i li a-wa f v 4-hf i U -
g
The person completing this portion (GW-59A) of the monitoring report should sign below and submit this
form with GW-59 forms for required wells to the address provided of the top of the current GW-59 form.
�1 � '•0 111 '�' 3F ' � S aFasL4t it � '�� � � F'aY.�+� R.fi'�lF- ll��� � FSPS^S >7 5 "y1.� �•'i �1 �
�ri `' _� d le�l b�� at�t �abo�te¢irt � airy u •ash ilyat �p t ate �1 u .,�, r e�it1)��5�!%
,�°tr '�xi$�s��i.4i�,L." / ti 4i` �� EA l� 4� Al ��` '1 FL f �� � -� �%J� /•
Signature o Permittee (or Authorized Agent) Date
GW-59A 1.21812003

v
m
ED
s
p
b
C
o
Z
ro
m
a
�D t
`- O ca
m
aEi
O❑❑
O
❑
r�
CL
E
LU
a
a
CL
S]J
O
C
�
U
E p
c
o
LL
p
Z
Uj
ro R
Z U R
Imo^ Ul O
C7a
J
ro0.
U)
p
w
ro
0. II.
❑
❑
❑
❑
0. z z
0
v
N � N
z Q
m 13) ,m
LL m Lj-
o 'Q
m
0
...E N �
�
0 m E 0 .c m
cn U t
U�
0
6
a
0
Q
9 co
cii 'c
tll � rn
P
�) P
0
z a ro
C, U a
O U % a)
CL
LU X Q L]-
LL a U) Q d
iJ
O
z
i
❑
C �
C',
LU
�aa)
N
m
E °'
ro
c�
p a
uJ
ct
CL
m y
p
N
Qi
ro
❑
m
N
C
ro
�
c
d
O
rn
Z
El
CL
m
U)
L€J
�
tlS
E
N
o
�
c_ca
o
v
Q
(D
�
L
Is
O
41
`^
V 1
LL
O
D
NN
a
W
N
N
:
CL
y
ro
j
ro
Y
a°
3
L
w
A
cu 0
O
o
�I
❑ c
a
m
ro
E
a
n
E
uj
C
n
JL —
€L o
C
� z
o
CA
rn
a E
o
_
U Q r *k
CL a
o v
Q
m
o
co m m
E E
D
U a
O m
E
U
C7 '}c6
O+
U
N
v
Q
o a .`�
0 o N
� c4�i1
U O
CLro
c
CL r-
N n
' N
<
a
U as C)
IL N O
O
0
ro
0
D
E
c)
110)
t E
m i
m
_U')
OI
rn
tm
of
m
R1
07
69
E
bl 67
E
E
E
E E
E
E
a
a
E
a
Q
a a
r�
'V
u
U7
C N
O r
a
N
Ira ti
O
In
d
iO�
fo
N
V
cn
N
'd'
u7
7
a
a
h
va
1� In t`
N In P
Q% o
a
a
P
o o
o
Q
a
P
O
O
m
O
oa O O
a O P
z 5 z
z
a- ?
E
E
E
E
as
a
L,
E
E N Y
pro
a
U
E~
O
vi
*
M
'=
tca
ro
U
as
ro
'Z
o m,
�U0O
o.amU�'
3
J ;C7 (ll
co L
I
Q
CA
U
'o
U
O
Y
I I
a 'Y
m
0 O
U
rn c
2i
U
�+
o
'a
D
J
o
J
o
_I
1
J
to
r
E
o
o
E
7
E
E
as
E
E
E E
,i
u
w
--
N
V
ca
co
m
•r
Oc
P
m
o
Lo
m
U
m
O LO
N�o
co
a
m
o
0
soc0
a
a
f- aq
m n d
Z
tl E
AM
0aa
U
N
a
U
zz
mZ
O
U
l L
U
O
N
T7
p m cn
E z
ro
U)
L-
g
LL h
n
z
U
Q
ccd
ty
z
Y
LU
O
CL
'6
-
Q
U
o
U
N
a
.�
E
U
Q
M
Fo-
v
c
�4
1�1
co
O
a
0

6
z
E
0
z
0
�0
Li.
D0
N� W
uj
uj
z
❑ Q
z =i
w0
U) U
Id
U
k
C
�
7
•O
Ul
o
n
O o o
i�
,2
o
Z
S?.
U
E E
u 5
O
w
IM ��y
m
O
)J�
E
0.
r�
0.
o
y
uQi
,A
N
n
67
ii
W
ro
a 0
u
r Ln
U)
o w
102
Ow
0. ❑ ❑
El
a
a z
z
z z Q
u- Ii LL
m
r E
2z tp V) U
U
N0
L
1
0
0
E C
r-- � a �
N
L
O O
z o w c
g a U o ro
W o m -o n
LL (n0Q
�I
m
0
O
z
k
❑
C
o
m
E
ro
a�i
W
0
A
a
W
•.''a
Q
C
C1
U
IM
E
z,
a
(D
z
c
❑
0
a
IM
U
W
N
r
E
ocotl
a.
d
N
0
ro
O
O
�p
U
U
W
LU
m
R
E
�
ca
�
N
C
E
m
z
E
g
no
m
"0-
p
r_
o
N
d
=
o,
m
E
:3
n
E
s
a
>
cn
10
i
c
O
n o C�
a
W o
z
0
J .J
M
❑
E m
r
Q
U n
C7 v
n
R
C j E to
w W
0 o U
o
N
N
Q ti
a`s
0. N o
to U
o� J O
"O CJ -0
p O O
N
E E E
E
E
E
E
E
a
E
5
5
E
a=
E
E
3
C
Q
�
q
. N
Qj 0
N
ro
a
o
tl
r
N
m
V
V'
o
a2
M
"I
N
Lo
L a
o 0
p m
m
m
n
o
0
o
a
o
o
o
0 o
E ro o
z z
o
z
o
a
4?
o
E
0
E
0
E
0
E
o
o
m
0
o
1�
Z
a
E
o
E
N Y
41 N
pro
N
ro
ro
7
'C
A
7
U
7
E
O
Q
U
7
'innN
O
N U
O N
it3
R
ro
U
N
E
p
U
2)
Vo
a7
N
m _
9 Q
O
O
o-
;5
0
�
m
ro
U
o
E
E
0
U
z
a
Q
O
U
n z ,�
is z
C
ILL
>3
0
ro
a
M
O
4
`
.-1
.c
J
E
o
CD
o
E
D
E
E=
E
a
E=
E E
J
Q
V
!
a�
IM
y
t
mWF-
av
o
tag
a
v
tma
rn
a
�
m
o
tn
om0
0
m
co
o0
zo
N, O
z
tUU
N E
ro
,p
U
N
U
to
1
,ro m z
7;
L
a
„�.J
0
N
U
N
N
O ttv
C
LL
ILL w
N
a
L
U,o
¢
p,
(!i
0
Z
Q
o
U)
U
ro E
0 z
?
C7
t
urot
_
jU
W
U°,
0
07
E
U
O
O
3-
a�i
a
c
k"

N
0
gO
C
LLt
N
�
O
0
a
o
Z
o
'a
a-
o C)
Z v
n
m
O ❑ ❑ 'P4
❑
�
O
Ltj
a
N
C.
0
�
O
O
�
U
C�
li
❑
U)
c
Uj
U.
ro
i u
U) o J V)
Q
o
❑ ❑
�
El
El
n. z
}0.
z 1
N
4
Z_/
L.F..
a
O
�F
0
U.
=O
aW
�W
F LU
Z
OE
0 �C)
E
c v
U
4 0 m
tl ] rn } a) E
p
Wa
c
Z
o
El
U�,
s Q z t
o
ro
U E
LP U)'o
03
p
U O
Ul i7
Cj04
�' c
O
Q
o © U
0 o N
u
V y0+ o
0.
m
N
(D (D U
ui
T a N O
p
U
o r
-o
a
�
E
E
.0
J
J
J
-
1
J
0)
E
0) 0)
E E
d7
E
y�j}
07
—`m
0
t��
o
�
E
67
7
LJI
03
E
0) m
E 7
RI
a
.�
O
U,
v
ol
N
N
E
N
co'oO
�]
r
o
N
( n
(O o
a
o
N
A
t'
N
7
�
P
o
r,
M
ti 47
N o1
h
[O
U❑
-q
Lf.J
to
o
CO
a
9D N
o ti
r
a
O
o
rn
o
O
n
b
a
O
o
4
o
of
h
M
a
O1 4
o 0
6
0
a
ro
n- 2
ro
E
a
E
a
E
a
E
a
o.
n
i�-,
E
E m
ar
E
m
ro
ro
a� N
o
N
a
'c
m
`'
E
a
t
E
z
N
7
v O
M
O
7
C)
ro
E
LL
a
C
ro
m
Z
°¢
ro
o
_
Q
U
U
L
x
Y
rn c
OZ
Z
`-
o�
U
Z
o
e
❑
m
n
0.
4'
rn
C
4S
O r
J
o
J
J
N
0
c
J
N
CA
+� to
o
o
o
rn
E
0)
E
0,m
E
rn
E
�.
rn
rn
}'
;O
E
3
O
7
N
D
F
p
N
E
ro
w
4 22
t�l
Z
�+
N
U
Z
T
E
UQ
'
o
b
o
CNI
LO
n
<Ot
tOoo�
rob
No
L1!M
to
N a
M
P
7
Col
tD'P
t
0.
P
o
E
o
O
0o
D
m
Ou
9
pO
-00
°'�a
Om
M
zP
Q
0
nC4
oro.o
LU
a],N
Q.
Z fi U
V)
LL
�.
�- 61
Q
a-
U
ol
E 'Z
E m
*..L
0
E
U
�
0
Q
Q oE`
!
Z
w
O
f-' E
U
P
LfJ
°
Z
v
'O
N
0
I
.J3
0
o
ro
E
a
E
U m
m
Uo
o
U
0
C7
uo-
W
i�
�
C)�
7
0)
p a
'n
(A
w
I

z
FP
0
z
0
o
LL
Do
d
Lu LU
Lu W
aL)
z
Q
z .J
w0
0U
C�
rn
W
QLF
C
O
ro
Z
O o
o ._
Z m
O
Na
d
Q
o U_
E
E
0 ❑
❑
❑
E
E
0
LU
a
°-
fn
Q
❑
o
�
V
N
N N
O
O
N
E 21
w O
❑
to
Z �c
a' 0
0
T
ca M
°3
h-
O -1
w cl�
wo
0. El
El
❑
Lu o
a. z
z
d
ro
v
U
fi
h
a
4
v N
E
Z m
Z
m (D m
LL CL LL
N
pi
J f0 O .Q 0
a E E r
U'
O
0
N�
o�
0
CL
{n c
Lu
7 6
J a)
a D
z p G
U o w
_j m o a
t'T a rq CL O Q
42
t�p)
(�
N
0
$
O
z
El
r
ij
o
FBI
m
o
E
m
c
m
a)
o
❑
v
W
E
E
5
N
j
N
w
�
C
n
O
G
❑
'o
c.
W
E
uJ
o
D
m
a.
m
p
7
N
^
0
2,
pa
E
m
I
'v
n
m
O
d
a)
3
'
W
m
N
7
cL
N
m
' z
Cl) �-
D
J
_- j
❑
-
a
w
E
d
E
i �
�:
❑
2
>
co
063
5
W o n�^j
C
W Z V'
J ,J
a ❑
o
C) a v
�[ Jj E E
� N
C
U
O }
o
❑.
U E 0
E
0 5-
U 'I'O
f�.
m
CL
N
a`s
U C 9 U
u3 O
O
O
4t
p O
E E
-i
-i z:�
J
1
J
-i
-j
J
.
-j
--I-)
r
-1
�
to
rn
rn rn
rn
m
cn
�n
rn
m4
`a�
E
E
E
E E
E
a
E
c
c
E
s
c
E
c
c
Q
'o
3
O
N
v7
O r
0
N
ED i�
[a o
l,f1
o
h
a
ffl
h
N
u1
a
h
h
h
E ao
o
o
Ra to,
r
a
n
o
o
0
0
r o
n
I�
o
R
O
0
a
o 0
o
0
Z
7
7
'>
GOl Vj
w N
E
0
t
~
>
7
U
o
t°
U
ca
E
O
U
cG
Iq
o
Ql m
rM
z
I
00
Z
O
~ CL
Z
N
p
fa
-o
U
o
U
O)
I
I I
O
Uz
;t'
O Q¢
C
�
!1
W
ecc3� c
C
V
O
L
�
0.
cu
�
J
J
ul
tm
a
o
E5i
E
E
a}
a
�
�,
�n
c
z
^8
`i V7
m
W
r
t
V `pF
o
o
o
m
R
o
co
Cl
v
N
o
N
In
o
M
"n
Lr)o
M
NLO
m
N
N
M
O
(D
to Tl
'r o
co
0
o
0
0
0
O)
0
4
47
0
h
N
m m
o
0 0
0
40
0 S
(D
O
F-' R
m
m 3
h
O
o
o
R
O
M
O
o
o z
R
� ❑C3
N•Z O
6��
.0
O
O
OU
�O-
U v
U)
u
O
U
-0
2
OzW
E•zh�
d W
U)
z
j
as CY
j
tj
N
aa)i
❑ Ll
n
V7
0
0
0
E
a)
U
O
0
C
m
m
W
Iq

6
Z_
R
O
Z
Q
Li.
V a.
0:
U
Z
❑a
z -j
02
0Y O
0 0
r
iu
t7
N
L
c
C)
'0
7
W �
U
b
o
o
Z
O o
o _
❑
m
ro a
v b
m
O
Lu 0aEi
LY
ro
J
O
o ❑
❑Pq
❑
W
=
Cl
0
p
o
�
U
m
❑
W �
LL
0)
Z I-
rn
LLC
a
ro
F N
O `°
w a
m z Z
I-
m
1
U N/
M E o ��
Z Z Q
t-
Li D- LL
N
E
Z
of
W
E ro c m
U'
0
(} 0
5Vt O
.0
o �
0
0
4 `N
�c
w : rn
a
00
z o G
a S C) 0
❑ b U N
o 0
O Q 0_
u sz [n
zz
t
❑
Q4vl�
U)
ro
Cl
E
�+
U
❑
-d
lLi .°j-tl
ca
E
m
R
U)
U
Oo
N N
>
ro
m
C
❑
Li N
G
0
Io O
Z
El
O
Q.
Q)
j
U
w
C-
EFBI
o
m
a
m
m
E
0
C
o
N
a�
0
W
�
�
W
a)
M
Q
m
G
CDC
Z
a'G-+
�
0
0
a
N
O
G
'C
0
N
co
O1
�
❑
.G
w
E
4
us
/�
fLL o
G
J
W o
z
❑ '�
E
E
,(y
X - ~i
o c
Z U
U a V
� o 0
E E
O
�CD-0
a
CL
E
U E cD
C7
0
U
N
�
�
to
(
4� Q
Q o U
Q
N G
r7
a r
J
L�1 O
m U
O J >
J-i
J
__j
J
j
--�
J
J-i
J
E
E
E
E
E=
E,
`rn
mO]
�
E
1G7
n
Q
N
ro
m
u�
o
m
o
o
CS
o
E 0
z? z
0
z
0
a
11
0
E
0
E
0
E
0
E
0
m
0
a)
0
o
L." U N
in
um)
.0
C
�L
.0
O
~
Cl.
`J
c
a o N
U
"
o:3
C0
U
m
E
U
Li
°
ro
U
Z
o
ro'
E
.o
W
U
o Z
ro
ttf
oc
U
U
U
Z
C
Im
a
u
o a
E E
1 J �
E E : 7
0
N
7
0
E
c�
0
❑)
E
�
o
�
m
rn
rn
can
o
r~n
a
r,
o
o
0
0
N
7
C
C
N
Y
z
j
C:
o
N
ro
cro
z
rn
0
z
,
x
rn
c
c
j
C
>
O
J
O
J
O
N
J
...1
J
N
J
to
O
O
U)
E
cm
E
0)
E
...I
5
M
E
5
m
E
i
0)
E
0)
E
E`
a
O
O
N
Z
m
O
co
m
i
ar
o
mo
V
oo
0
OM
n
0i.
V
oO
in m
Nc
E
©b
N❑❑
M
E
0-
b
Om
U
bon
O
GI
Yo
U
b
vl
0
Om
O
$1
b
o
0m
o Z
N c
Oo
0
Z
T
z 0
N
o
ccf
o
,fj
0
�'
m
O
c
o°
LL.
a
~
~
L
L
/c��a�
E 'z
cU
C
0
N
j
a.
L
C3
Q
Gl.
�+!
l7
' 7
c
Z
�[
❑.
m
. o
co
m
C:d%'
O
U
E
"''
LLu
)
U
CQD
❑
O
D.
"
n
I)

6
z
E2
O
F-
Z
O
O
LL
�O
W
LU
QU
z
© Q
Z
wO
0 0
f `�
rn
i
o
1
uj
0
a
O 4
� C
O
O IS
o L)
O
C7
n
c
E
E o
O
€WQ
O
CL
C
O❑❑ice❑
���}},
E
(Ly7
LU
a
O
m
w
z
u
A
N ❑
0
N
r
u
t m
ro
O
R
co
p
p
ILL,L❑❑❑❑
z
a z
ia
m
N
m
a o
W a) E
Ew
QI
o
ct�
O
z
El
}
a)
U
E
m
N
v
a1
cai
O -o
LlJ
a
m c
Q
U
E
4=
m
-p
0
O'',
m
z
El
a
Ol
U
j
LLJ
41
E
�
N
❑®
m
a
m
E
U5
N
2
�
o
�
IL
o
_
m
a
E
3
ill
N
0.
N
m
'
m
D�o.
Z
o
a
o- O
N a
C
o
N
U)
41
E
°
E
Q_�
in
a
0 Q
C
W z N
O °
pp
a E
o c
U Q
Z �j
o
L o 0 o
Q r
i7
N 7-
E E E
C:
p
C7
a
U o
o
a�i
Cj E as
E
U p
U
a ro
v
Q
d 0 U
0 o N�
y
(J)
() o
ro c
(D N
m
Q
u? �
V I O
O
E
E
E E
E
E
E
a
E
E a
Q
0
Q
v
_V
V
�7
a
Vl h
a
ti
o
m
h
o
V•
0
N
0©
4'i
o
a
m m
n
n Ll h
N n 0N
m o 0
m
E i41 n
to
o
m U)
o�
0
0
o
o
a
o
o
m
ti
o
a n o
z c z
z
a °,.'
N W
E
�
E
7
E
�
E
ro
p
m
U.
p
i>-'
U
E
E
7 U
E
m0
wm Z
o—C,a°mU
U
L
pp' 'o�
)
mZ
0
a
Co
U7I
•
EO
U
Cn
❑.
�G
;?
w
to
U
U
m e
o
u Z
O
a
[>
Z
w
a
fd
n
p.
•n
o
o
E
E E
p
E
E
m
E
a
E
x
1�
Q1
s
U
'
'J
m
q
!0
N
U
d�
v,
�n
aY
o
o
o
in
o
o
Co
a
N
N
l
o
Orr
in
o N us
m
c-
0)
to
om coNoto
ooa600
oo0
z
N Z p
U
O
O
m
C
{�
U
ro
C
'o o 10
U
L,
Z
c
%r
E z z
U)
LL
°
Q
U
Q
m
D-
00
c Y
'o
m W
Ca W
o
0N
-o
m
F:
o
U
H
ro
o
E
m �
p z
m
C9
�
a�
roQ
( j
U
r°n
api
m
E
rn
E
O
ro
Fo-
m
C
i
Q
CL
.l]
J
.�rtrj
i•+
Q
y1
G
O
E
c
a
V
cu
E
0

CMSD (SLUDGE & WELLS ACCT)
CONTENTNEA METRO. SEWAGE DIST.
MS. RENEE PRIDGEN
P.O. BOX 477
GRIFTON, NC 28530
PARAMETERS
Drinking Water ID; 37715
Wastewater TD: 10
PHONE [phone]
FAX [phone]
ID#: 416
DATE COLLECTED: 10/18/23
DATE REPORTED : 1.0/27/23
REVIEWED BY;
Well #9 Well #10 Well #14 Well #15 Well #17 Analysis Method
Date Analyst Code
Fecal Coliform (MF), /100 Mls
< 1
< 1
< 1
< 1
Ammonia Nitrogen as N, mgll
1.67
0.53
Ammonia Nitrogen as N, mg/i
0.13
0.35
Nitrate Nitrogen as N, mgll
<0.04
0.75
0.18
<0.04
Total Organic Carbon, mg/I
3.83
3.25
2.48
13.79
Chloride, mg/l
3
2
4
3
Total Dissolved Residue, mg/I
M 70
M 51
M 50
M 92
Total Chromium, ug/l
<5.0
5.0
<5.0
12
Copper, 11g/1
<10
<10
<10
<10
Conductivity (at 25c), uMhos/cm
136
<50
78
65
Total Ortho-Phosphate as P, mg/l
0.04
0.07
0.05
0.06
< 1
10/18/23
HMV
9222D-15
10/23/23
BMD
350.1 112-93
0,13
10/24/23
BMD
350.1 112-93
0.04
10/19/23
ADR
353.2 112-93
3.38
10/24/23
BLV
531OC-14
3
10/23/23
ADR
4500CLB-11
M 75
10/19/23
HMV
D5907-13
8
10/23/23
MTM
EPA200.7
<10
10/23/23
MTM
EPA200.7
59
10/19/23
BNC
251OB-11
0.13
10/19/23
BLV
450OPE-11
All 4C requirements were not met; M Blank result exceeded method constant weight criteria.

Waypoel t. 0
ANALYTICAL
114 OAKMONT DRIVE
GREENVILLE, NC 27858
C14SD (SLUDGE & WELLS ACCT)
CONTENTN'EA METRO, SEWAGE DIST.
MS. RENEE PRIDGEN
P.O. BOX 477
GRIFTON, NC 28530
Well #18
Analysis
Method
PARAMETERS
Date
Analyst
Code
Fecal Coliform (IFI), /100 Mls
<1
10/18/23
HMV
9222D-15
Ammonia Nitrogen as N, mgll
0.19
10/23/23
BMD
350.1 112-93
Nitrate Nit rogeu as N, m9/1
<0.04
10/19/23
ADR
353.2 112-93
Total Organic Carbon, mg/I
8,92
10/24/23
BLV
531OC-14
Chloride, mg/l
3
10/23/23
ADR
4500CLB-11
Total Dissolved Residue, mg/1
M 110
10/19/23
HMV
D5907-13
Total Chromium, ug/l
<5.0
10/23/23
MTM
EPA200.7
Copper, ug/l
<10
10/23/23
MTM
EPA200,7
Conductivity (at 25c), uMhoslcm
150
10/19/23
BNC
251OB-11
Total Ortho-Phosphate as P, mg/I
0,03
10/19/23
BLV
4500PE-11
Drinking Water In; 37715
Wastewater Ins 10
PHONE [phone]
FAX [phone]
ID#: 416
DATE COLLECTED: 10/18/23
DATE REPORTED : 10/27/23
REVIEWED BY: * r
All QC requirements were not met; X Blank result exceeded method constant weight criteria.

Waypoent..
ANALYTICAL
114 OAKMONT DRIVE
GREENVILLE, NC 27858
CLIENT: CMSD (SLUDGE & WELLS ACCT)
CONTENTNEA METRO. SEWAGE DIST.
MS. RENEE PRIDGEN
P.O. BOX 477
GRIFTON, NC 28530
REVIEWED BY:
VOLATILE ORGANICS
qmn. MRTHODS 8260D
Drinking Water IDs 37715
Wastewater ID; 10
PHONE [phone]
FAX [phone]
CLIENT ID: 416
ANALYST; JAP
DATE COLLECTED: 10/18/23 Page: 1
DATE REPORTED: 10/27/23
Date Analyzed:
PARAMETERS, ug/l
10/24/23
Well #9
10/24/23
Well #10
10/24/23
Well #14
10/24/23
Well #15
10/25/23
Well #17
1. Benzene
<0.50
<0.50
<0.50
<0.50
<0.50
2. Bromobenzene
<0.50
<0.50
<0.50
<0,50
<0.50
3, Broinochloromethane
<0.50
<0.50
<0.50
<0.50
<0.50
4. Bromodichloromethane
<0.50
<0.50
<0.50
<0.50
<0.50
5. Bromoform
<0.50
<0.50
<0.50
<0.50
<0.50
6, Bromomethane
<0.50
<0.50
<0.50
<0.50
<0.50
7. N-Butylbenzene
<0.50
<0.50
<0.50
<0.50
<0.50
8. Sec-Butylbenzene
<0.50
<0.50
<0.50
<0.50
<0.50
9. Tert-Butylbenzene
<0.50
<0,50
<0.50
<0,50
<0.50
10, Carbon Tetrachloride
<0.50
<0.50
<0.50
<0.50
<0.50
11. Chlorobenzene
<0.50
<0.50
<0.50
<0.50
<0.50
12. Chloroethane
<0.50
<0.50
<0.50
<0.50
<0.50
13. Chloroform
<0.50
<0.50
<0.50
<0.50
<0,50
14. ChIoromethane
<0.50
<0.50
<0.50
<0.50
<0.50
1.5. 2-Chlorotoluene
< 0.50
< 0.50
< 0.50
< 0.50
<0,50
16. 4-Chlorotoluene
< 0.50
< 0.50
< 0.50
< 0.50
<0.50
17, Dibromochloromethane
<0.50
<0.50
<0.50
<0.50
<0.50
18. 1,2-Dibromo-3-Chloropropane
<0.50
<0.50
<0.50
<0.50
<0.50
19. 1,2-Dibromoethane
<0.50
<0.50
<0.50
<0.50
<0.50
20, Dibromomethane
<0.50
<0.50
<0.50
<0.50
<0.50
21, 1,2-Dichlorobenzene
<0.50
<0.50
<0.50
<0.50
<0.50
22. 1,3-Dichlorobenzene
<0.50
<0.50
<0.50
<0.50
<0.50
23. 1,4-Dichlorobenzene
<0.50
<0.50
<0.50
<0.50
<0.50
24, Dichlorodifluoromethane
<0.50
<0.50
<0.50
<0.50
<0.50
25. 1,1-Dichloroethane
<0.50
<0.50
<0.50
<0.50
<0.50
26. 1,2-Dicliloroethane
<0.50
<0.50
<0.50
<0.50
<0.50
27, 1,1-Dichloroethene
<0.50
<0.50
<0.50
<0.50
<0.50
28, Cis-1,2-Dichloroethene
<0.50
<0.50
<0.50
<0.50
<0.50
29, trans-1,2-Dichloroethene
<0.50
<0.50
<0.50
<0.50
<0.50
30, 1,2-Dichloropropane
<0.50
<0.50
<0.50
<0.50
<0.50
31, 1,3-Dichloropropane
<0.50
<0.50
<0.50
<0.50
<0.50
32, 2,2-Dichloropropane
<0.50
<0.50
<0.50
<0.50
<0.50
33, 1,1-Dichloropropene
<0.50
<0.50
<0.50
<0.50
<0.50
34, Cis-1,3-Dichloropropene
<0.50
<0,50
<0.50
<0.50
<0.50
35. trans-1,3-Dichloropropene
<0.50
<0.50
<0.50
<0.50
<0.50
36, Ethylbenzene
<0.50
<0.50
<0.50
<0.50
<0.50
37. Hexacblorobutadiene
<0.50
<0.50
<0.50
<0150
<0.50
38. Isopropylbenzene
<0.50
<0.50
<0.50
<0.50
<0.50
39, 4-Isopropyltoluene
<0.50
<0.50
<0.50
<0150
<0.50
40. Metbylene Chloride
<0.50
<0.50
<0.50
<0.50
<0.50
41, Naphthalene
<0.50
<0.50
<0.50
<0.50
<0.50
42, Propylbenzene
<0.50
<0.50
<0.50
<0.50
<0.50
43. Styrene
<0.50
<0.50
<0.50
<0.50
<0.50
44. 1,1,1,2-Tetrachloroethane
<0,50
<0.50
<0.50
<0.50
<0.50
45. 1,1,2,2-Tetrachloroethane
<0.50
<0.50
<0.50
<0.50
<0.50
46. Tetrachloroethene
<0.50
<0,50
<0.50
<0.50
<0.50
47. Toluene
<0.50
<0.50
<0.50
<0.50
<0.50

'O
l
Waypoint
ANALYTICAL
114 OAKMONT DRIVE
GREENVILLE, NC 27858
CLIENT: CMSD (SLUDGE & WELLS ACCT)
CONTENTNEA METRO. SEWAGE DIST.
MS. RENEE PRIDGEN
P.O. Box 477
GRIFTON, NC 28530
REVIEWED BY; /
VOLATILE ORGANICS
qmn _ TaSF1''1''HnnB 8260D
Drinking Water M 37715
Wastewater ID; 10
PHONE [phone]
FAX [phone]
CLIENT ID: 416
ANALYST: JAP
DATE COLLECTED: 10/18/23 Page: 2
DATE REPORTED: 10/27/23
Date Analyzed;
PARAMETERS, ugll
10/24/23
Well #9
10/24/23
Well #10
10/24/23
Well #14
10/24/23
Well #15
10/25/23
Well #17
48, 1,2,3-Trichlorobenzene
<0.50
<0.50
<0.50
<0.50
<0,50
49, 1,2,4-Trichlorobenzene
<0.50
< 0.50
< 0.50
< 0.50
< 0.50
50. 1,1,1-Trichloroethane
<0.50
<0.50
<0.50
<0.50
<0.50
51, 1,1,2-Trichloroethane
<0.50
<0,50
<0.50
<0.50
<0.50
52. Trichloroethene
<0.50
<0,50
<0.50
<0,50
<0.50
53, Trichlorofluoromethane
<0.50
<0.50
<0.50
<0.50
<0.50
54. 1,2,3-Trichloropropane
<0.50
<0.50
<0.50
<0,50
<0.50
55. 1,2,4-Trimethylbenzene
<0.50
<0.50
<0.50
<0.50
<0.50
56. 1,3,5-Trimethylbenzene
<0.50
<0.50
<0.50
<0.50
<0.50
57. Vinyl Chloride
<0,50
<0,50
<0.50
<0.50
<0.50
58, Total Xylenes
<1.00
<1.00
<1100
<1,00
<1.00
59. Methyl Tert Butyl Ether
< 1.00
< 1.00
< 1.00
<1.00
< 1.00

Rim
Waypoult
ANALYTICAL 9
114 OAKMONT DRIVE
GREENVILLE, NC 27858
CLIENT: CMSD (SLUDGE & WELLS ACCT)
CONTENTNEA METRO, SEWAGE DIST.
MS. RENEE PRIDGEN
P,O. BOX 477
GRIFTON, NC 28530
REVIEWED BY: Armr -
VOLATILE ORGANICS
STD. METHODS 8260D
Drinking Water IDi 37715
Wastewater ID1 10
PHONE [phone]
FAX [phone]
CLIENT ID: 416
ANALYST: 3AP
DATE COLLECTED; 10/18/23
DATE REPORTED: 1.0/27/23
Date Analyzed:
PARAMETERS, ug/1
10/25/23
Well #18
1.
Benzene
< 0.50
2.
Bromobenzene
<0.50
3,
Bromochloromethane
<0.50
4.
Bromodichloromethane
<0.50
5,
Bromoform
<0150
6.
Bromomethane
<0.50
7,
N-Bntylbenzene
<0.50
S.
Sec-Bntylbenzene
<0.50
9.
Tert-Bntylbenzene
<0.50
10.
Carbon Tetrachloride
<0.50
11.
Chlorobenzene
<0.50
12.
Chloroethane
<0.50
13,
Chloroform
<0.50
14.
Chloromethane
<0.50
15,
2-Clilorotoluene
<0.50
16.
4-Chlorotoluene
< 0.50
17,
Dibromochloromethane
< 0.50
18.
1,2-Dibromo-3-Chloropropane
< 0.50
19.
1,2-Dibromoethane
< 0.50
20.
Dibromomethane
< 0.50
21.
1,2-Dichlorobenzene
< 0.50
22.
1,3-Dichlorobenzene
< 0.50
23.
1,4-Dichlorobenzene
< 0.50
24,
Dichlorodifluoromethane
<0.50
25,
1,1-Dichloroethane
<0.50
26,
1,2-Dichloroethane
< 0.50
27,
i,1-Dichloroethene
< 0.50
28,
Cis-1,2-Dichloroethene
<0.50
29.
trans-1,2-Dichloroethene
< 0,50
30.
1,2-Dichloropropane
< 0.50
31.
1,3-Dichloropropane
<0.50
32,
2,2-Dichloropropane
<0.50
33,
I,1-Dichloropropene
< 0.50
34.
Cis-1,3-Dichloropropene
<0.50
35.
trans-1,3-Dichloropropene
< 0150
36,
Ethylbenzene
< 0.50
37.
Hexachlorobutadiene
< 0.50
38.
Isopropylbenzene
<0.50
39.
4-Isopropyltoluene
<0.50
40.
Methylene Chloride
<0.50
41,
Naphthalene
<0150
42.
Propylbenzene
< 0.50
43.
Styrene
<0,50
44,
1,1,1,2-Tetrachloroethaiie
<0.50
45,
1,1,2,2-Tetrachloroethane
<0.50
46,
Tetrachloroethene
<0,50
47,
Toluene
<0.50
Page: 3

114 OAKMONT DRIVE
GREENVILLE, NC 27858
CLIENT: CMSD (SLUDGE & WELLS ACCT)
CONTENTNEA METRO. SEWAGE DIST.
MS. RENEE PRIDGEN
P.O. BOX 477
GRiTON, NC 285 0
REVIEWED BY:
VOLATILE ORGANICS
STD. METHODS 8260D
Drinking Water ID: 37715
Wastewater IDI 10
PHONE [phone]
FAX [phone]
CLIENT ID: 416
ANALYST: JAP
DATE COLLECTED: 10/18/23 Page: 4
DATE REPORTED: 10/27/23
Date Analyzed:
PARAMETERS, ug/1
10/25/23
Well 1/18
48.
1,2,3-Trichlorobenzene
< 0.50
49.
1,2,4-Trichlorobenzene
<0.50
50.
1,1,1-Ti•ichloroethane
<0.50
51,
1,1,2-Trichloroethane
<0.50
52,
Trichloroethene
<0.50
53.
Trichlorofluoromethane
<0.50
54.
1,2,3-Tricbloropropane
<0.50
55,
I,2,4-Trimethylbeuzene
<0.50
56,
1,3,5-Trimethylbenzene
<0,50
57.
Vinyl Chloride
<0.50
58,
'Total X,ylenes
<1100
59.
Methyl Tert Butyl Ether
< 1.00

SOILS ANALYSIS LAB REPORT'S

W CD
O
T
N
� � m
� � N
U 0
a
Z E
L.. 0.
0 -
O N
Z
L
L
_ � o
� 10
L1.
■O tl'
V� M
N
N
N
O.
r
a
N
o �.
t--
VV
N
2
Cj
6
C]
6
6
0
0
uO
=
V
�•
It
h
M
CO
00
M
N
00
00
h
00
00
00
N
NO
C� -.
r
d
N
0
(h
0�
00
(�
W
N
r
r2
r
r
oy
N
a;
.�.
r
r
N
.N
W
C)
N
N
N
N
N
N
N
0
0
0
0
0
6
Lf)
00
h
N
h
0�0
A
(�)
w
a'
0
0
0
0
0
(D
0
.�
LO
N
N
0)
to
N
co
-.
N
N
N—
N
N
N
co
c0
(O
6)
h
N
O
r
CO
a2
N
N
It
M
'IT
LL
-':
ti
—o
N_(D�
N
N.-
<°
r
N
M
N
Z_
Y M
N
LD
N
M
N
U)
ty))
Cl)
N
(_
LO
�W Q
U) J m E
Q:
N
r
r
N
r
N
r
©
3 �°a
a
Lri
co
to
Lfl
cd
m
ffl
o IL y
LO
CO
O
CO
h
J'
N
a)V
:.
LO
CO
(D
iD
(fl
(fl
(O
-- :
tD
rn
rn
r
O
rn
h
�1}
LO
6)
N
h
N
dt
N
(0tio
�
o
Lo
co
o
0
0
d
0
O_
O
0
N
N
N
CO
(O
CO
wD
to
(.0
m
LO
fo
La
0
07
M
Ch
a0
Ch
a0
A6
0
co
Cn
t0
coN(OO
CA
O
a:
LLI Lf)
O
N
Gr, . Ci
Ln
(O
h
M
M
O
r
h z
N
N
N
N
N
M
M
} X
w
m
O
s a Q
o
1
m Ui
U W
W ro
U v
a �
C �
m
Z �U
Q
7 tlti
U
0 N
X Co
N �
a
�X
W
0
O''
rJ3
w
V 'o
d '
g
� u
N N
m
{N
o
a
O
V
a
O"
N
x�
E
OIL
IL
IN
42)
LL
Ll
Q
V
Q
M
ci
00
O
O
O
O
O
w
crC�
w
w
w
Ir
U
00
U
00
U
0
0
0
0
0
0
0
z
z
z
z
z
z
z
LO
N
CO
N
h
N
CO
N
M
N
o
M
M
Lu
U
co
f6
n
N
a
C
0
0
N
O
E
O
f=
Q
(Q
:_
_m
Q
w
ai
0
r�
F-

h
C�
rfp
a
cli
a
a w
a
x
ry
o
u
IL
m
�
N
N
u.l
N
;3
r
a
a
w.:
U
a
�
W
N
U:
rn
O
C
N
a:LO
CO
No
N
N
LO
00
co
U)
�
f/)
N
N
UQ' �
Li) —
V
O
❑ i m U
LLJ
LO N
Q :
r
U LO o
3
m E A 'a
x
LL
o
w
F^
v
a `
_.
Cl)
00
O
O
u
�2
z
V
O
m
—
z
z cn
N
a U
N
x
7 W
m
cl
a
x ¢
O
Z:
cU
V .0
u°Q
m
C+
rn
m
c
'^
43) N
�a
Q
U U)
v
a
0
u m
O
c
E
cr
N
0
U
O
LL
6 G
p
�
a
Z,
aT
E
z
c c
o
Q
�
Z
mCO
J
U w
� U
d
7:3 m
U
a
�
a
O
X a
a L
U
O
i C
O
C �
a U
U
Q, LLI
U
�
r(n
G
O C
N
C O
O
c
Qo
w Q
a�
114

N
N
N
©
N
V
O
c�
'O
M
n
N
N
5 N
M
O
n
c
x..
.' 6'.:
to
N
N
O
V >
ao
9
LLI
a1
LLB
o
LLL.
N
C
N
(V
z
Y
M00
� r
w
V
�
n
co
co
r
u
LO
Z
LU
co
4
M
w
LO
C1
N
"
Q
U
N
i�
i� Z
LLIrLLff
x
W
LQl„
❑
N
N
C
` U
�a
7
A3 "O
�0
U
,p N
Uo
(6
O m
O C
L
O U
W
C
O a-
7 tW
N
E �
E o
o
rr
•C O
Q N
�U)
U N
U m
*0 U)
@ m
m _-z,
z �
a
o U
c
X l0-U O
X
C W
F-

Nk
N
N
U)f
r
CO
d
L
CL
Nc`no
of
dm'
a
`o
61610
0
6
a,
e
N
N
:.
(3)
co
O
m
m
00
V
cD
oo
h
�ti
ao
ao
C3
a.
Ol
0):-.
N
r
N
N
N
N
W '.
W
N
N
r
N
N
O
O
T
O
N
00
CO
O
C;
O
O
O
O
O
O
N
V
M
A
dt
a
a
N
�
d
c
CD
o
ci
c
a
LL.
N
N
M
o
p
L
N
cr
Z
M
N
m
N
dam'
to
co w 0
.:
r
co
N
o
N
o
CD
n0
3
o
c?
Ln
o
�
0
0
r
3
a
1
10
LO
CO
o U.. d
•� :'
m
to
00
m
I
1--
@
cn
't
I
cn
I
�..
co
h
r
co
It
g
N
It
d
M
d
M
OO
d
0
E
4.
i[j
N
N
'V'
.
Lo
h
h
r
Lo
o
0
0
0
0
0
0
O
CA
CQ
<P
(D
W
0)
I
0)
0)
I
�
0)
0)0)
m
O
W
m
m
m
m
W
00
OO
Q
z
Z Cl)
co
Q U
h
W
N
04
h
N
N
WW X
N m iJJ
Ga
a
0. Q
m
z
6
U
v
r q
42
o
aas
E
N'N
m
O o
l0
0.
L)
�'
o
m m
r-,
z
�a
Q
O fD
0
O
al
c
+:+
lb
(D E
°1 E �
r
t0
C
O
E Z
x
d
9
U c
N
r�'
i+
L3 c
)
Q Q
E ro+
:
tit
O
CL L ,
9
C,7
O
y
c
cto
p
Z
O Ci
m
Cn
cn
a
cy
3
nID
U
J o
.a
(13
w m
C) Cy}
t
43)
M m
O
R7
E
M
aU
m
FL
0
IL
0_.
0
d
0
G-
0
d
0
w Q
0
m
a L
U
U
U
U
U
C)X
0
0
0
0
0
O
zzzzzz
w
� O
a
[U
p
U
n c
w
p
C)
N m
N =p
a
U
O `
w Q
U)
O C
I-
COO
N
N
N
m
O
O
a
m >
m
m
m
w
Q
Lil

V i m
N:
N
N
N
c
c
c
c
N
N
(D r
C'
QS N
N
-
It
r
G)
O
(D
r
cr)
r
r-
0
d El 0
�
a.
a
COO
Lf)
M
()o
0
N
'DoO
N
d.
LO
N
of
ai
oa
N
m
03
r
N
N
r
u
m
t9
N
N
N
N
N
[.0
1q,
N
O
CD
7
ti
d
o
cm
CD
(] �.
N
M
CO
t0
co
C -
a
a
C)
0
0
C
N
N
I
N
N
a
00
a
(MD
�
,-
00oL
10
LL
O
�j
rn
rn
rn
(c-Do
m
z
in
M
CONN')
(MV
O]
mORtY
cq
co
m
r
r
r
r
0
G
3
g,
cm
o
d:
M
as
3 E J s
(0
co
co
co
co
O � �
aNi
ru
(O
cD
CO
cD
h
0
-:
co
rn
(D
r-
a)
c)
M
Cl)
Lo
co
Lo
o
-
00
0
0
0
C7
O
O
C)
0
Z _
,D
(D
(D
cD
(D
w
co
(D
(0
w
(D
0
w
z
m
W
G �
Q U
N
r
m
r
It
r
LO
cD
X
f
m
ar
a ¢
to U
U
o z
�rz
c 0
O
CL
«O
N U)
U ai
U ca
m
a�
Coco
m
Z U
E ❑.
CO-0 U
O
U7
X
N
-0 U
v w
U
c U
U
Q w
U
o
N 'O
0 U
E ¢
ur Q
o 6
C O
O
m
-a 15
w ¢
a
w
V G
U
d..
iA
_ u
N N
r
3
a
N
O
O
f1�
o._
EY0.
........
_
al
r
G1:
Q a'.
GL,
c
Z.:
N
a
0
z
� w
4
a
a
a
a
a
0
0
0
0
0
af
0�
!Y
w
w
U
U
U
U
U
O
O
O
O
O
z
z
z
z
z
m
N £
'c
d)
w
FE

cn
N
N
N `r
C
C
a
s
a
N
to
co
Gi N
@ N 0
as
z
co
O
O
CL u
lC o
L
O
m '
N
a
r
-
>
'a
ur
u
m
Z.:.'
O
O
Lo
N
O
�Y
U
N
M
O
Cr
Cl)
M
C;�
a
co
co
a)
LL
L
r
O
U
Z
CO
u. :�.
N
N
A
♦��
p
u
co
O
CV
as
m G G
a
co
LO
J
O
[L
CD
�.
U)
L
v
Lo
...:'.:�.-
LO
N
-
co
ca
00
oN
O
W
co
0
co
00
Z '
M
111 �
00
>^ N
U) h Z
U w
m
a
m CL Q
a
z
m
CL
U
N
Cu '
>t
N. F
m
r/i 4'•
a
N
N
M
N
G
Q N
.
Ya
E
A
t�
to
Q= a
>+
N o
W
LL
c
'o
Z
a
U
co
d
CL
w
U
�
U
O
O
z
z
r
O
O
a3
U
(6
m
o_
w
a
C
0
Q
13
N
A
T
6
C
O
C
0.i
d
W
v
v
a
w
a
F-

Q� o
N
N
Quo
L �
U O
Z as IL
La
.
co
O 00
N
NCL z
L
L.
� � o
d; d
a�a.
•Q it
'^ M
„N
N
N
N
C
C
� r
o
00
00
z v
Ui d
S°
`
CD
O
u
�' o
12
IL
rn
m
N
N
W
O
co
I--
LO
m
LV
a,
13
U
d
O
t0
;.,.�..::
.
O
O
a>'
N
O
U..
p
N
N
z
M
N
Q)
U)
`^� to
t
lJ —
p
W 0
-j
C'4
U � o �
al E 2
3.
m
ui
In
co
3 Wi
z°,
L
•.
co
00
It
0000
ao
o
O
O
w r
(7)
m
z
111
0
co
00
OLD
M
LU to
co
i N
a
r
N
z
0 w
p
a
�
Q
M
O
O O
U U
00
z z
©M
t0
N 12
G
m
LL
11
i-

N .
N
N
N
V
.
r
�
�
V
00
Q
ar 0ccoo
ccoo
LLO
(7N)
U
=
O
N
I�
co
O
r
co
ao
O
co
rn
co
N
CJ
rn
cis
oaf
(1)
N
N
N
T
N
C.
a7
:uj
u
m
10 -:
N
N
N
N
CM
N
T.:.
O
Lo
In
N
N
N
N
co
N
CD
m
CO
M
It
N
a
O
N
OMO
T
N
N
C
r
N
co
lU
M
TO
O
co
T
U-_
nJ
M
a
r
N
O
z
NV
CO
co
(D
00 O
4
LlJ i�
-� m
Q
N
N
o
N
N
O
U o
O o
a>
Ln
o
Lq
O
Ih
Lri
o0
3 m
co
cD
cfl
co
u.43)
C7
Ti
0
---.
LO
m
o
rn
co
M
m
N
O•
-
M
Ls?
d'
cOq
(D
M
o
r
0
0
0
0
0
0
00
m
O
m
m
m
m
m
o
W
to
co
to
co
(D
(O
m
rn
a�
m
m
m
Imo"
z
co
LU n
a co
r
N
00
�z
}
O w
co
O
Qi
G
N
0) N
a_
EE
U O
U
� al
U co
o m
O �
U
Q X
w
am
W
m �
U �
O �
m 2
a
Vo
j
s
U N
Uco
0
m ca
Z U
E Q
73 l0
zG U
0 m
(a t3)
_ c
X
fU t
� X
to
i 0
O
m .
O
Z
O ;
U 'a
C is
N :N
C.
N:B.;
:
a
1
in
cc
43)
O
�
m
LCi
LL
c
m
a
U
Z
� �
o
t�
c
T
O
0
0
0
0
0
0
U
U
U
U
U
U
0
0
0
0
0
0
z
z
z
z
z
z
O
E
O F
hOi �

N
N
N
N
�'
G
o
a
•Q
�
e
H �1.
N
N
:.u)
N
u
w
C�
w.
,a
O
a
o
o
N
Ii
No
N0
VJ
_z
Y CO
N
¢ f0 —
Lo
❑
w
43)
U � a �
£ ❑
aCD
_
LO_
6 u. N
N
C1
to
V
,a
N
N
a :co
00
r
o
-
a
<o
co
0
z
LLI
t0
�
U'
000
I-
z
M
LLI M
C m
04
� U
�- z
X
W
in
0
x o ¢
�� O
U �
.O N
U �
p N
a �
t6
O U
CL x
c �
as �
c
M U
U �
o=
(D =
c o
(D
CL
U)
U 0
W w
U
U)
ca
to
Z �
g
ZI ca
u U
O di
C
X N
Q1 C
C
c
a
aJ
a
a
M
0
n-
o
rx
U
0
z
N
U
`m
CL
zi
0
0
n
¢
0
E
U)
O
s=
a
m
m
CL
6
v
m
aN
u
N
N
N
d
P
-S
rn
F-

h
�.s
S-:
'S
E-
-g
-C
-S
O
G) N
:
CO
Ln
Lo
I-
CO
N
It
Lo
0
N
'-
o
C)
O
O
O
Ci
o
C;
C. U
=
♦
0
YJ
co
a}
co
ca
co
rn
m a�
Lq
O
N
r
r
LO
O
Ln
1
N
N
b
�
w:
U
e-
r
N
N
N
Z:
ca
O
C;
o
o
C
C1
Cl
V
:
O
CO
N
o
"J
Co
LO
o
00
V/ ¢
M
M
N
N
m-
00
N
N
(�i
LO
N
LO
N
CO
O]
L �
�
M
N
N
N
N
C-4
N
N
r
00O
Z a_
a
o
f
OD
rn
Lr)
0)
d
a7
0
d
O
IT
(N
M
N
N
N
^
}� .0 Cp
m
O
L__..._
J 00
O N
:
O
(q
Ln
0
r
0
a1
0)CD
O
0')N
N
^
CL Z
-
�
N
M
N
Y
N
r
-.._.
_
Z
N
N
ti
0
N
y
(nLU
co
Q:
N
N
r
r
CV
N
O
o
todi
sLIIIIIIII
O
r
(O
M
r
N
0
I�
3 -1
a.
L. . y
o
(D
N
CO
[+
(oU
LO
co
CA
Ln
O
Lfl
i+
O
i+
D
.�
()
V �
N
LV
N
N
M
N
i~
N
CO
Iti
ci- '•`
L`90
coo
e�O
(fl
cCDa
LNn
Lrn
H
00
LO
En
LO
L0
Lit
LO
to
w
m
`C
Ln
LO
Lo
N
N
(14
Cq
N
N
N
N
N
N
N
N
o
h
z
Z M
V
W
coo
N
Q
v
C)N
o
L3TJ Z
W
w
N
N
C
i U
N �
a
0 0
U �
A N
U'O
(0
o
m
a X
C �
N CL
Z 0)
Er
m
2
') 0
U
O
d
N
C o
If
ULLJ N
US
O Cn
G �
z U
E Q
(6
0 U
O ay
00 ill
X �
O L
X
G �
o
m �?
L /1
d 0
'u
E Q
Cn Q
ca. �
t� Q
m
NI
NI
Nl
NI
r
NI
r
NI
r
NI
r
NI
r
QS
V �
U
'
N
is
C�
NN
m a0
0
0
0
O
0
0
... .,:
N
N
N
N
N
N
N
Q
O
�
13
0:
CD
Co
coo
coo
N
a
C)
ro
0
v
m
a
N
LL
c
d
N
0
N
0
N
0
N
0
IN
0
N
0
N
0
N
UJ
z
- N
N
N
N
N
N
N
N
a
V
Z
�
�o
w
W
W
W
w
w
w
W
a
a
a
a
a
a
a
a
h
h
h
I--
1--
h
h
h
Q
Q
Q
Q
Q
Q
Q
Q
a
LL
LL
>z
a
LL
a
Q
Q
Q
Q
Q
Q
Q
Q
0000❑r�C:.iC]
a
a
a
a
a
a
a
a
Ir0�
m
m
m
m
m
m
m
m
M
co
1'
ffl
Lo
(o
(o
(O
h
w
CO
w
60
(o
d
t�
N
N
N
N
N
N
N
N
N
0
G
Q �
N �
41
C
m
E z
U
r-
0 0
c V
C W
LO
0 U
o
O
O
C
O_ i
O
C J
D cy
N
n
2
m
w
C
D

N:
�
C
O
N
0 :.
N
Q
CO
G
tm d
,.
p
IL
O
� a
U) :
cri
m;
U
rn
o
a
a
w
u
m
16
Z
O
co
a'N
C
�
N
�
Cl)
N
A
..,. .'..
N
LL.
N
N
z
m
w m
a
r
C
U o 2
L 0
}i J .0
C
�
m
rt+
.;-(D
co
N
N
o
a.
ui
Lo
{�
00
z
co
LI E LO
❑ 47
w
N
Q
ti
Z
r
X
(� t w
Q p }
Q
4 C
C 0
U
po
C �
� L
Q
w Q
V �
U
Al
m:
O N
a
E.0 3
N
N
(D
Q
O
c4
a
r
E
Q
Qa
7�
N 'o
U.
Z e
a
0
v
L y
c
a
4.
a
LU
m
w
N
N �
m
u_

W �
O
M
rn
N
a�
❑ `L G
U O
Z
O
cC
o J N
2 m
N
Q �
CCi i a`
Act � (L
O
- --
- ---
----
o
N
O
47 N
[
O
0. c+
Q
Uf .
N
6i
pp
wJ -
O
O
a
di
Co..
r
.z
�
d
�Lf)
�3 ii
O
O
Q 5
O
N
C
N
a'C\l
C
N
LO
N
o
N
LL
Q
N
N
UJ
Z
Y O
T
[o
M
C)cq
C
Q
O
U 0
`)
U
o u �
co
I�
v
tf1i.:
N
C,
d'
La
(14
r
l0
O
2
wC7
Lo
oco
Q
F'
Z
M
wJ In
G 00
cV
ch t, Z
h
X
� m O
a o
x a ¢
a�
0
Z
NI
�
r
N
n
Va
'
U
N
L ;C
NF
m;
cli
N
W
rt+
O
OQ.
Lo
r
4)
�
Q a
Q. a
tD
LL
C
�O
m
Z 11
O
N
N
Z:
O
tj
F
O
w
h
Q
a
0
Elf
00

co
0
M
Cl1
❑ •� C
V
Z��
O
O J N
CLU
L 2
� N
m L Z
V+ M
To
•
U) -:
fN0
O
G
N
0
N N
cl m 0
,�
ca
o
0
0
0
0
0.
N '
m
cot-
M
O
0)a�
[�
1+
rn
00
N
Cp
I-
O
N
N
U
t-
O
Ch
(6
CO
P
N
c�
ri
a:
>_
'a
W'
u
m
r
N
0
C7
00
O
LO
CO
00
LO
I--
A
M
cD
CO
r
N
N
c.:mmc0nLoCD�~
C
r
00
t0
00
'.;
M
m
M
N
N
N
a''t-r�t�
C
N
h
^
O
O
�
N
r
r
�'
c¢
M
N
m
co
LL
❑
C �:
�
N
~'
cMD
h
O
Y
(0)
Q O
m
O
�q
CD
N
N
wU
a1
Q
N
N
N
(D
O
0
M
O
N
O
CO
r
4) O
Q'
LO
CO
lf)
M
W
ti
0 �
o
e l:
rn
N
N
N
N
d'
Cl)
0
LO
O
Cl)
.
co
LO
',t
M
n
N
a �:'
00
d•
.
(D
1­
co
O
M
LO
M
O
d'
C
Z
Ln
m
LO
Ln
to
LO
N
co
N
m
N
m
N
ao
N
00
N
oa
O
f
z
M
Z
A 03
CV
Q
co
M
CO
CO
CO
O
U1 ti Z
N
�
N
ti
N
ti
N
r
N
r�
N
X
LZL i
a�
Z
NI
NI
NI
NI
NI
NI
a
v�
U
m
y
9N
N
Q
r
V. 0
O)
@
Y
C
U
O
O
O
a
3
U O
0 N
vi
o�
°
2.
r C
�
Q 0
4)
O w 'O
O
CD
LO
CD
�
Qj
lt0
O
r
LO
(D
CO
�
� a
m
U)
w
a'
N a
0.
�a
L
U
0 2
LL
e
CJ
N
C\l
N
Cl
N
CD
N
(D
N
CD
N
N
N
N
N
N
N
E
2
C O
Q
o�
U U)
:;.� :
J
O
w @
� m
.0..'
a U)
@
X
x
O
c
LQl
G w
D
D
D
D
n:D
T 6
m CJwm.
Cwa
awl
m
m
m
i
Q
o
75
w
U) Q
CO
W
CD
O
00
w
w
C
O
�. ro
Q �o
w Q
A)
0
a
E
Ka

U)
--
C3
�.
-. •
a 0
`
IT
00
OD
0)
M
CC
aJ
N N
r2
o
C3
0
C]
r
N
c�F
m
CL
t
'�,•
O
CO
M
d)
C
N
m
oo
m
r
o0
w
o
I--
coco
Yu
oW
m
L�
N
r
r
00
CO
rn
4
a
U)_
r
a
w
a
U
a
Z:.
a
0
o
0
0
0
0
0
N
co
Lo
N
LO
u7
h 00
3
N
M
N
m
In
LO
iI-
Cl)
�Ul)
N�T
to
M
to
co
-
TVS N
I
o
'r
(D
(M
r
N
C]
h
N
- -
_
N
N
N
N
M
co
m
N
Q y O
`
rn
N
N
00
LO
(n
(s7
L ai
C) f? O
Z" N a
:
r
,-
r
�-
r
o
000�
LO6N
J
O
00
o
c
ti
Z
UJ
_.
=� m
Z
X
(
CD
m
co
M
N
m
N--
T
N
N
r
• L
� r
ti
N
d;
co
o
N
00
00
V
1205
a
—
Lam.
U
00
M
M
to
N(D
r
(p
M
(D
3 t
R
(0
[O
(Q
(D
(D
co
Q a.
O U.
rr.
O
h
�
[p
M
.'
(to
(D
((DD
co
(fl
-
Cl)
0o
t--
61
00
0)
I-
m
M
(CV
co co
N
co
(+?
N
-�
V
M
00
CDto
(o
N
co
V
M
(D
00
Lf)
d
Lo
Lo�v
M
't
(n
M
N
r
e
CT)
CD
Cq�
It
LO
ti
co
co
0o
m
00
00
00
zr
W
n+n
r
m
LO
Lo
�n
Ln
N
N
00
N
to
N
m
N
oo
N
a0
N
ao
N
00
Qe0
F-
Z
Z ih
uW
co
a
N
T
N
(')
a
0)
0)
(1)
0)
a)
4D
o
�0
U) L+ Z
N
N
N
N
N
N
N
N
X Z
0 LLI
O �
o'
Z :
NI
NI
NI
NI
NI
NI
NI
N
�
r
r
U0
U
N
N N
m o.
m:
LN
U
o
N
o
N
O
N
C�
N
C7
N
0
N
0
N
a
N
Y N
a
(A
Lo
U U)
v
�:•y
(n
m
O
o, X�.H
o
(o
0
CO(.0
o
0
tf)
0
CO
0
a
0
CO
0
00
Lx
Y
a
a
CD
2
cu
LL
c
0
_
'Q
�a, f
Z,,,, :;.0 -
o
N
0
N
0
N
o
N
o
N
0
N
0
N
o
N
'.
Z
N
N
N
N
N
N
N
N
�o
a
U
a M
o
z
Gf.a
C
U uai
rc
U EU
J
o
-
.............
.
.........,.....,
n7 �
of
GY
LY
J
D:D
m
LLI
U
L�1
El.l
W
w
w
w
w
w
a
m
m
m
m
m
m
m
m
U
o. U
vl
O U
9
U
(!) Q
N
M
d'
Ln
(D
M
0 U)
Q)
0)
Q)
D?
(3)
h
0)m
63
h
(A
ti
ti
ti
0 0
p
CL .n
L
N
U
m
as
a
c
0
0
Q
-0
E
0
c
0
M
c
m
n
W
C
a
.y
U
0
0
rn
Q
❑
U
Z
Cl)
O
cn LO
O M
2
C E
a
E z
E
o r-
0 o
a m
� U
A 'C
C Un
o
N
O Q
(wtt
LO_
O
� J
O d
a
a
ca
`1
w
0
G
O

'N
N
C
C
N
;p
N
(0
U�f N
1� O
0.
^o
co
00
W
rn
w
NO
a
a
�
W
u
m
Ld
T
T
'.
C
oo
c0
M.
'.
N
N
a'
co
,N
Cl)
a:.LO
co
N:
LO
I,--
CL.
Q
N
L
co
EL'
Z
N
rn
rn
�
Ur p�
❑ i- VM'
O
d
w in
a
r
U ? CD
N
a
C9
cq
3 m c
U.
a
N
O
6]
e
CD
0
LO
Y S
rhi
GO
(14
u
r
h
h
Z
W
T
'n
Ln
(j
ONO
ONO
O
Z
m
WLID
❑ W
N
Q
00
ONO
ti Z
ti
Cq
r x
0
a o
x a ¢
m;
T
r
CQ
V 0
.R
ql
N
N
N
j
Oi
M
ON
Lin
Lo
oo
T
E
0 a
0
N
ILL
w
�
cNv
U)
a
a
0
ww��
h
�
£Y
¢
¢
a
0-
❑
❑
w
w
in
co
00
co
h
h
N
U
co
N
O.
N
a
C
O
a
Q
w
0
.o
E
O
G
O
C
l0
O.
x
w
4)
O w
c Lo
O � �
� � N
w N
N � m
E
E z
O n
� 6
m
O U w
9
O_ () m
O �
N
0 0
Q N 0 U
g c
° C5
m
N p E
co
�a
C c
O
No
a
C
E �
'C
0
U o
L1
N L"
LL
F-

U).
N
(0 :
C
G
C
aV
N:-°O
N
(O (CV
o
r
O
t--
h y
4D
O
(10
O
r
aS
CL
O
CD
03
rn
rn
W
co
V
o
(V
:
e
a .
61
CS
CC Z.
2:
o
0
0
oo
co
0
co
(D
LO
r
N
N
'C
(3)
O)
N
a'Lr-L
c0
LD
r
o---
----- .
LLL
N
N
©
IV
rLO
(o
LO
0.r
Q (o
❑ } U
G -�
00
m
a
O
r
0
a
LO
<L u
C7
`'.
C
Y
�
�
coo
t�
U
a
N
N
N
N
X'
( )
r00i
o
r)
C)
N
N
"t
r
N
m
cq
CO
(D
(.O
to
'z
y
co
00
00
Q7
EL Lo
p oa
N
co
ti
-
h z
ti
U
O u
[f' tl° ❑
a:
m
C
N (Qj
(ll �
E
U O
U U)
7i N
U �
p C]
N �
0. X
c �
5 W
rr
U 3
o z
N
E
�a
CL
U)
U N
U s
0 U)
Co
� U
Q
7 W
`a U
o
X m
N L
'a X
w
C
O
a c
C O
R5
m:
0 '
z
41
rl
rl
rl
� a
U
U
N
d
-j
NA
m :o
a°a
o
0
0
ri....a.,'..
N
N
N
a
LA
Gp1
O
o
LO
a
co
o
co
C
N
LLtn
c
a
fA
a
V
z
u
Jam.
[Y
Of
0�
U)
U
a
a<
Q
Q
Q
❑
❑
0
n
Q
Q
ry
of
UJ
W
m
cq
)•
r-_
N
z
a
F-

00
O
r
N
aN
�L O1
U O C
Z � a
C
� o0
o J N
■avww�r �L
L�f..
A
a�
w M
N
N:
l0
o
m"
N
O'
^o
O
O
t0
N
N
IDO T
rL W.
t N
:
O
r
C]
CDo
a L)
x
o
L�
IL
?
t)
p
rn
o
00
rn
Ih
M
h
m
00
v
rn
C4 ;
LU �.
M
<--
(D
CM
00
O
N
U
ti
oa
L`
OJ
(n
h
LO
;ui
�61
U
U
-.
m
Lo
O
LO
4
00
r
co
C)
N
r
0
C) ::
M
N
CO
V'
N
N
N
M
CD
M
N
N
-
M
T
N
_LC
CO
LO
_
-
M
N
N
N
M
-.
'C")O
N
O
C:
O
M
0O
M
O
l0
ts?
co
r
O0
to
co
u7
LL
p
N z
o
co
to
w
Lo
Lo
�
T
z
M
00
N
N
N
On
0
V7
� —
O�
CC!
C�
O�
Cl)
���
U o
3 :(n
N
T
tl-
LO
CO
EA G
a
(
co
co
(ri
(o
co
aU-
w
LO
Lo
((]
(o
(O
M
N
O
M
co
�.
Ol)
N
M
C
'd
N
N
to
N
M
to
(i7
N
Q1
N
(0
co
(00
(fl
(MO
lOD
Z
LO
LO
0LO€()
r
T
l0
C)
N
ao
N
00
N
00
N
N
ao
N
ao
z
w LO
d co
}' N
(A
1--
CO
6)
O
a U
r
ill
�
ti
co
00
>` z
N
N
N
N
N
N
X
O
w
� m
Q O }
01
(a
C
i U
a(U+ N
c�
U O
U �
N
7 �
O63
0)
F
O
v )
U
0) 0_
3 w
QF
� •U
U
CD,
CF-
�
U) T-
= o
a)2
T: j
N (n
W
LU w
U m
0 N
rz
ca ro
z
a
7 (q
o C)
U
- C
X
N L
-0 X
c 11J
C
O
C M
U
U
a U
o 2;,
N =p
O (j
� Q
w Q
O c
c o
C
(U
d
W Q
w
z°
NI
rl
r
�I
rl
"1
41.
J U
`
C
:u
N.
g �:
O
d
G7
C)
C)�
N
N
N
N
N
N
N
'A
.
16
O
N
(�
O
co
0
co
C)
to
0
-t
0
0
0
m
d
Q
Q
LL
'O
O
N
O
N
d
N
0
N
0
N
0
N
V}
Z
a
n
c.�
Q
ti
w
w
LLI
LLI
w
w
0_
0_
Cl_
IY
0_
0-1
D
D
D
Z)
D
I-
h
1-
F-
I--
0.
!lQ
L¢L
a-
OQ..
Q
Q
Q
Q
Q
Q
m
d
O
m
0
D
D
D
D
mmmoamm
a
O
i`
00
07
O
W
00
N
ti���r~ti
N
N
N
N
N
N

n
N
ro
�
oV
Q
V N
N
81
0.
=
*
Iq O
D-
y�
CD
N
Lu
Li
4
�
rA
>
LU :
G
z
o
U
LO
Km
ao
O
a�
� O
Z � a
o
N
J 000
u
CL z
Qf
}1 N
U)
Z
-LO
-T
a
C.
�+a
°wok
CL
c6
aL©L
IL
o � m
rro�
w
m ..to
a
4
W
4
W
LO
C7
coo
h-
LU
:}
Z f9
LO
c
G
co
N
n
Q U
Ui I- Z
co
!�
a
CL
U
N
Y V
NN.
N
Q
iC
°Is:
a
m
r
v
a a
LL
c
"
Z
: o
N
VJ
Z
Q
0
V
0
LLJ
a
ZD
w
m
h
m

SavedRx: LIME22-23
Soil Fertility
Grower: CMSD
Farm: WILEY GASKINS RD
Field(s): Multiple Fields
Tenn Lime - Fertilizer Application (lbs/ac) -
17.5......... ............. ............. ..._.-................... ................... -_- ............. .,------ .- ----------
Crop Type:
Pick Type
Equation Variables
Target pH:
6
Lab:
Waters NC
Switch Rate:
600 Ibs/ac
Total Area:
75.85 ac
Equation:
Lab - Default
Rate Multiplier:
NIA
Total Product:
27540.64 lbs
Commodity:
Bermuda Grass
Rate Subtract:
NIA
Total Product Bulk:
13.77 ton
Sample Date:
2022-11-28
Min Application Rate:
600.0 Ibs/ac
Product Cost / Bulk:
$0.0/ton
Rec Multiplier:
NIA
Max Application Rate:
3626.52 lbslac
Total Product Price:
$0.0
Rec Subtract:
NIA
Avg Application Rate:
1537.29 Ibslac
Application Cost / Area:
$0.0/ac
Max Rate:
NIA
Application Area:
17.92 ac
Total Application Cost:
$0.0
Min Rate:
600 lbslac
Average Field Rate:
363.10 lbslac
Total Cost:
$0.0
Ayden Nitrogen 12/13/22 08:50 AM
E F C� S Y S T E M S" 4728 Old NC 11 Ayden, NC 28513
252-746-2152 1 /2

Ayden Nitrogen
4728 Old NC 11 1 P.O. Box 7
Ayden NC 28513
252-746-2152 Fax:[phone]
Contentnea Metro sewage Dist
Po Box 477
Grifton, NC 28530
Quantity Description
13.750 Tons Dolomitic lime • Sulk
13.750 Each App Pees Dry Fertz
Terms; Unless otherwise agreed in writing by Harvey Fertilizer & Gas Co, interest will
accrue at a periodic rats of 1.5% per month. To avoid additional finance charges,
payments must be In office by last day of month.
Invoice
Invoice Date
0110312023
Due Date
02102/2023
Customer ID
010202
Shipping Loc. 01
1024331
Unit Price Total $
72.50 /Tons
15.00 /Each
Sub Total
Amount Due
Remit To: Harveys
P.O. Box 189
Kinston NC 28502
Phone #: [phone]
996,88
206.25
1,203.13
1,203.13
:antentnea Metro sewage Dist Invoice 1024331
File Copy 1