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WQ0003281_2023 Residual Annual Report_20240214 (2)
Initial Review Reviewer nathaniel.thorn burg Is this submittal an application? (Excluding additional information.) * Yes No If not an application what is the submittal type?* Annual Report Residual Annual Report Additional Information Other Annual Report Year* 2023 Permit Number (IR) * WQ0003281 Applicant/Permittee City of Belmont Email Notifications Does this need review by the hydrogeologist? * Yes No Regional Office Mooresville CO Reviewer Admin Reviewer Wanda Gerald Submittal Form Project Contact Information Please provide information on the person to be contacted by NDB Staff regarding electronic submittal, confirmation of receipt, and other correspondence. Name* Tanya S Carter Email Address* tsetzer@cityofbelmont.org Project Information ......................... Application/Document Type* New (Fee Required) Modification - Major (Fee Required) Renewal with Major Modification (Fee Required) Annual Report Additional Information Other Phone Number* 7048253791 Modification - Minor Renewal GW-59, NDMR, NDMLR, NDAR-1, N DAR-2 Residual Annual Report Change of Ownership We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form. https://edoes.deq.nc.gov/Forms/NonDischarge_Monitoring_Report Permit Type:* Wastewater Irrigation High -Rate Infiltration Other Wastewater Reclaimed Water Closed -Loop Recycle Residuals Single -Family Residence Wastewater Other Irrigation Permit Number:* WQ0003281 Has Current Existing permit number Applicant/Permittee Address* P.O. Box 431 Belmont, NC 28012 Facility Name* City of Belmont Class B Residuals Program Please provide comments/notes on your current submittal below. Attached is the 2023 Land Application Report At this time, paper copies are no longer required. If you have any questions about what is required, please contact Nathaniel Thornburg at nathaniel.thornburg@ncdenr.gov. Please attach all information required or requested for this submittal to be reviewed here. (Application Form, Engineering Plans, Specifications, Calculations, Etc.) Signed WAR 2023.pdf 812.48KB Upload only 1 PDF document (less than 250 MB). Multiple documents must be combined into one PDF file unless file is larger than upload limit. * By checking this box, I acknowledge that I understand the application will not be accepted for pre -review until the fee (if required) has been received by the Non -Discharge Branch. Application fees must be submitted by check or money order and made payable to the North Carolina Department of Environmental Quality (NCDEQ). I also confirm that the uploaded document is a single PDF with all parts of the application in correct order (as specified by the application). Mail payment to: NCDEQ — Division of Water Resources Attn: Non -Discharge Branch 1617 Mail Service Center Raleigh, NC 27699-1617 Signature 0 Ja 45'&&wlt Submission Date 2/14/2024 CITY OF BELMONT 2023 Wastewater Treatment Plant Annual Report Land Application Program Permit # WQ0003281 ANNUAL LAND APPLICATION CERTIFICATION FORM WQ Permit#: WQ0003281 County: Gaston Year: 2023 Facility Name (as shown on permit); City of Belmont Land Application Operator: U.S. Biosolids, Inc. Phone: 336-777-6909 Land application of residuals as allowed by the permit occurred during the past calendar year? El Yes ❑ No - If No, skip Part A, and Part B and proceed to Part C. Also, If residuals were generated but not land applied, please attach an explanation on how the residuals rvere handled. Part A - Residuals Application Summary: Total number of application fields in the RLmit: 1 3 Total number of fields utilized for land application during the year: 1 Total amount of dry tons applied during the year for all application sites: 97.22 Total number of acres utilizes for land application during the year; 42.4 Part B - Annual Compiance Statement: Facility was compliant during calendar year 2023 with all conditions of the land application permit (including but not limited to items 1-13 below) issued by the Division of Water Resources. © Yes ❑ No If no please, provide a written description why the facility was not compliant, the dates, and explain corrective action taken. 1.) Only residuals approved for this permit were applied to the permitted sites. 2) Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or the limit specified in the permit. 3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies of laboratory results are attached. 4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached. 5) All other monitoring was performed in accordance with the permit and reported during the year as required and three (3) copies of certified laboratory results are attached. 6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .1105(a) or the Pollutant Loading Rates in 15A NCAC 02T .1105(b) (applicable to 40 CFR Part 503 regulated facilities). 7) All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part 503 regulated facilities). E) All monitoring and reporting requirements in 15A NCAC 02T .1111 were complied with (applicable to 40 CFR Part 503 regulated facilities). 9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation; prior authorization was received from the Division of Water Resources. 10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are attached to include appropriate actions and remediations. 11) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as specified in the permit. 12) No runoff of residuals fiorn the application sites onto adjacent property or nearby surface waters has occurred. 13) All buffer requirements as specified on the permit were maintained during each application of residuals. Part C - Certification: "I certify, under penalty of law, that the above information is, to the best of my knowledge and belie€, true, accurate, and complete. I am aware that there are significant penalties for subnutt' g false information, including the possibility of fine and imprisonment for knowing violations." Permittee Name and Title (type or print) Signature NPermittee Date J0J)1, //1 X�- cmuA C� �f% 2-5-2024 Signature R Preparer* Date Signature of Land Xpplier Date (if different from Permittee) (if different from Permittec and Preparer) * Preparer is defined in 40 CFR Part 503.9 (r) and 15A NCAC 02T .1102 (26) DENR FORM ACF (12/2006) ANNUAL RESIDUAL SAMPLING SUMMARY FORM Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B WQ Permit Number: WQ0003281 Laboratory: Facility Name: City of Belmont Residual Source WQ # or NPDES #: WQ0003281 WWTP Name: City of Belmont Residual Analysis Data 1) Waypoint Analytical 2) 3) 4) 5) Parameter (mg/1Lg) Conc. Limit Ina )a Sample or Composite Date 3-1b-23 Percent Solids (%} NA 3.04 Arsenic 75 16.7 Cadmium 85 3.33 Copper 4,300 329 Cb3rom ium NA 60.3 Lead 840 17.7 Mercury 57 6.17 Molybdenum 75 8.33 Nickel 420 21.1 Selenium 100 16.7 Zinc 7,500 1880 Total Phosphorus NA 27900 TKN NA 149000 Ammonia -Nitrogen NA 3330 Nitrate and Nitrite NA 343 For surface disposal facilities the ceiling concentration limits listed in this form are not applicable. Reference the individual permit for metals Iimits. "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Signature lff Preparer * Q? 1hA")6,-w Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 27.1102 (26) DENR FORM RSSF (12/2006) (900Z90 a - JssIJ wUoi ldNiIG (96 ZOI I - .LZ DVDN V5I PUu WC SOS :�md WJO Otl u? PauHaP s?-MxRdeid- QIUQ * iamdax o amleuz2ig 1 r-91 0 «•suot;eJOIA 3umoun aoj;uautuosiAtut put; saug;o 4q!gtssod aq; aKpnraui luol;eutao3ui asls uY;;tntgns xoj sat;luuad;uuagxu�xs oAu aaaq�;eq; axeesu tau I -pa;.;tutgns trot;eumojul aq; pa4imleea put; paxaq;u-o Slaadoad lauuosaad pagllunb;eq; axnssu o-I pauttsop uta;sSs u q;ie& aauupaoaau in uotswadns ao uot;aamp Siu aapun paaudaxd sumjuautnaop stq;;uq;'Mnllo f4puad xapun'Sp taa I„ (S (Z I93rjAiEU-V;ulodrCLJA (I :S.to;E.togE-I e;eQ s►seluuv lunp!sag luor�zlag�o ';3MYN JIAAL 41 ISZ£000b1A :#OAX xo # SaG&K aaanos 1pnplsag I.rxoUjlag jo X4i0 muum ippat'3 I8Z£000OAk :aagmnu;!nuaa bAAj •papoau se sluxo3 leuol;lppe osn •xea.0 aepualua Ind aq; .tano xo; pazSluuu ami ao ilutaad bM oq;;o ped am 3SSd NUOj ul pa;sq Ion saapmexud aoj s;lnsaa sisSirm; Sulidutes lle;xodaa s - ViNO3 Auvwwns Ohuzdwvs lvnaisau zvflKNV ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: City of Belmont Total Dry Tons Applied (Annual): 97.22 Permit #: WQ0003281 Cation Exchange Capacity (non 503 only): Operator: Thomas Warren Owner: Thomas Warren Predominant Soil Series: GaB2 Acres Used: 42.4 Acres Permitted: 42.4 Site #: BT 9-1 Field #: BT 9-1 Residual Analysis Data (Heavy Metals and Total Phos horus use mg/kg, % Solids use Raw Percent #): r , Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Total 1 3j 4 61 L7 1 8 101 11 12 DT/Ac./ _2j _.5�j __2j 0 App. Event 2.29 Arsenic 0.077 0.000 .0.000 .0.000 O.000 .0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.077 Cadmium 0.015 0.000 0.000 0000 0.000 0:000 0.000 0.000 0.000 0A00 , 0.000 0.000 0.015 Copper . 1.509 :0.000. .0.000. .0:060. 0:000 .-0.000 0.060. 6.060 -0.000 .0.060 0.0.601 0.000. 1.509 Chromium 0.277 0.000 0.000 _ 0.000 0.000 0.000 0.000 0.000 0.000 1 6.000 0.000 0.000 0.277 Lead 81 :0.000 .0.000 .0.000 0.000 -0.000 - - 0.000 0.000 0.000 0.000 0.000 0.000 . 0.081 Mercury 0.000 0.000 .0.000- :0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.028 Molyb- 38 !28 0.000 0.000 0:000 0.000 0:000 0000 0:000 0:000 0.000 0.000 0.000 0.038 denumNickel 97 �.0.000 .O.O .0.000 .0.000 0.000 0.000 0.000 0,000 0.000 0.0.00 .0.000 0.097 Selenium :0.077 '0.000 0.000 0.000 .0.000- . 0.000 0.000 -0.000 0.000 0.000 0.000 0.000 0077 Zinc 8.622' ' : '0:000 0:000 0.000' '0.600. 0:000 0:000' ' 0,600 ' 0.060 . ' 0.000 0.000 0.060 8.622 Total Phos- 127.949 ' 0:000 0.000 0.000 0.000 0.000 0,000 0.000 0.000 0.000 0.000 0.00.0 #009 horus "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". 2-5-2024 Signature of Land A plier Date DBNR FORM MFLSF (120006) V'ZV :Pallsmxad sexiv rzt, :Pazgl}IZ saxa (r (900Z/z 4) 3 S3 ?J N30 aIrW �n!PEo'T fuujnlloa an,4$inenQ t,,W aopnls niex `£'fl P;4SAP ,f)teargaxae `Z p- pa;sarp,�[Islgoxasas `l Isodma� :sa;sg nol}ezr[gxamjgl x O i - aogelodYoa a aopaafai `50 - aax3.mS :u4wa UO'.49z!i!#EToA* -not e-rod.xoanI - jM `uopaaftq - lg `aalgjauS - S :Pogialq nogea[IddV,R aTeQ ioilddv pus -I jo au4zu2IS «•suoi;aJorn 2u!mom[ aox;uou[uosixdun put; samj jo d;ilzgissod aq# Balpnlaul `nor;auixojui as[eI 3oai##[mgns io3 saylsuad #usagiu2is axe axaq;;aql ajumu tue I •pa;puigns umsem to;ul aq; pa;en[sAa pug paaaq#ed djaadwd lauuosaad paW[enb ;eq# a insse o; panalsap taa;sds a q;rm aauapxoaae ut aoisivadns ro uollaaalp Xw xapnn paxadaxd sane #uamn3op szq};aq; gl;o S4 unad xapun'l;xaz1„ ..IXf •.. 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LLO'0 L60'0 S£0'0: 8Z0'0 180'0 LLVO 60S'C SID'O LLO'O aroe/sq[ lmruy PaTIddV 'I 000'O S£9'60Z d nZ aS im OF H qd j nD PD 000L9L o szVz�t o1 saoea*:(wxoT s!R; ol ddns 3S3 R03 zlav7a)ddns 3S3 u0 as sfagTsa2 g vfiM3 00WO 000'0 000'0 000'0 000'0 NOT 000`O 000.0 000'0 000'0 000'0 NOT 000'0 000'0 000'0 000'0 000'0 0OVO 000'0 00WO 000'0 . 00TO .000.0 .000.0 000'0 000'0 000'0 000'0 OOD'O 000'0 anasad VN 68V'66 £V£ OE£E 0006VT £'O 9'0 s 0 Sip I8ZEOOOOM S801 WE OOME £ZOZ-8 anosa3 VAT 6VI-DTI EVE OE££ MOT £"0 9.0 s 0 LIP TSZ£OOOaM 90T1 V0'£ 0000V £ZOZ-£ Zdozo I doiD Z doiD T doza rnl/Bw ai 1 pue a N S)Ow a o Z 64w K}I,I, c m 5 o e, " Bayou; _ sill VZ �d -ao (;'�o�i .�� uo RoS (ata `alsehl � � ° 3 `#a A `# Saidi� saaznoS IenpTsa�I (OVrsuotfJ(3) are V sad patlddV auznlon sP?ToS % suolleE) spy -n0 pinbl I lspliog (auo as;aa) patIdda aumjoh o d o nosldd�r Ienppoaj$urnraaag ad�� do{�;o auteAl � /s91? Pa?Tdd6 AIVd :NVd •xuN Z doxQ :amuK Z dwD i iZ :NVa'xujAi I do.t, amsa3 :maul I doxa :Q£0S uoa) f4jndua 92aeg3xg uol;sa ZgeJ :salxaS poS jurtamopaxd 1-6 ,LEI :# aITS I I EVL6 :Pa!lddV suol fr([ 3enuuv Y-6 ,I.$ :# PIaT d 'Isz£000ah1 :# IIUMM am uaueM sewoLll :xojuaad0 MM81SL SeMOU :xamaO puerj luouzlag,lo ,f1rQ :aazg�l.tlgFaeg ,aaavOI IddV .LOAI AmaETM XOa 2I0 ?II via V I+II v aQV'm NmO cancidV Q'IaI3 HDVa wa [a.LZIwafls aN (191'allawOJ ag OJL WHOA xxV`IS SIHi 30 AdO3 V 3DIVN ASVa'Id WwO3 AUIV IkTfis Q131a NOUNDIlidav amyl rfvnNxv ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name, City of Belmont WQ Permit Number: WQ0003281 W WTP Name: City of Belmont NPDES Number: NCO21181 Monitoring Period: From 1/1/2023 To 12131/2023 Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed: Class A: Alt. A (time/temp) E3 I Alt B (Alk Treatment) ❑ Alt. C (Prior Testing)!] Alt.D (No Prior Test) El Process to Further Reduce Pathogengs 0W 00 If applicable to alternative performed (Class A only) indicate "Process to further Reduce Pathogens'% Compost ❑ Heat Drying E3 Heat Treatment ❑ Thermophilic CI Beta Ray ❑ Gamma Ray C] Pasteurization ❑ cd%�:. y;<.•:v =t`Y ...k NO, , 'a :.,..%,:tr :xy kk Class B: jAlt. (1) Fecal Density-.© Alt. (2) Process to Significantly Reduce Pathogens E3 If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization i1. Air Drying E3 Composting © Aerobic Digestion Anaerobic Digestion '.J>:t::•:o:,a.,; .,j;...:».. .. ..: ..2. ..: ; .Y.tr::y` ':.:Y.:: . 6•..:.::�::.:j:�.t.;o:::..5:.�::.::: f<.is:$' ink: k: < ,s.i.%:i,Y.. .",#t. Y:?wR• .... 7v.y:�:£.�..�t.�;�...x. ,r,::t� .��:�:� µ:�:,�<r;:::.:.�, If applicable to alternative performed (Class A or Class B) complete the followin monitoring data: Allowable Level Pathogen Density Number ° Frequency Sample Analytical Parameter Excee- Tech- inimu Geo. Mean Maxim Units Sludge g of Analysis ys Type nWUC 2 x 10 to the WN 158833 250495 390724 MPN/g 0 7 grab sm9221 6th power per gram of Fecal Coliform total solids CFU 1000 mpn per gram of total solid (dry weight) Salmonella bacteria 3 NVN per 4 grams (in lieu of fecal total solid (dry coliform) weight) Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed: Alt.1 (VS reduction) 0 Alt. 2 (40-day bench) ❑ Alt. 3 (30-daybench) 0 Alt. 4 (Spec. 02 uptake) ❑ Alt. 5 (14-Day Aerobic) ❑ Alt. 6 (Alk. Stabilization El Alt 7 (Drying - Stable) ❑ Alt. 8 (Drying -Unstable) ❑ Alt. 9 (Injection) E3 Alt. 10 (incorporation) © No vector attiaction.reduction alternatives were perfomned ❑ CERTIFICATION STATEMENT (please cheek the appropriate statement) "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have been met." 0 "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under -my direction and supervision in accordance with the system - designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment" �(�r, ' 6, f tY,-4Cc&cn4- Zach Key U.S. BiosoIids, Inc. Prepares Name and Title Ztype or print) Land Appher Name and Title (if applicable)(type or print) A coAl'!�1_� ,� 2-5-2024 Signaud of Prepwer* Date Signature of Land A plier (if applicable) Date *Prepares is defiled in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM PVRF 02T (1212006) 0 Waypoint ANALYTICAL 3/29/2023 US Biosolids Inc Dennis Key 958 Hoots Road Roaring River, NC, 28669 Ref: Analytical Testing Report Number: 23-080-0005 Project Description: Belmont 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804.271-6446 www-waypointanatytical:com Dear Dennis Key: Waypoint Analytical Virginia, Inc, received sample(s) on 3/21/2023 for the analyses presented in the following report, The above referenced project has been analyzed per your instructions. The analyses were performed in accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table - if applicable. The analytical data has been validated using standard quality control measures performed as required by the analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA (including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time Refer to sample analysis time for confirmation of holding time compliance, The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as - received basis unless otherwise indicated, This report shall not be reproduced except in full and relates only to the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information Sincerely, Brandi Watson Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the analysis In question at laboratory's expense, or the refund of the charges paid for performance of said analysis. Page 1 of 7 �' �� 7621 Whitepine Road,. Richmond, VA 23237 Main 304-743-9401 ° Fax 804-271.6446 ANALYTICAL wwwwaypointanalytical.com Sample Summary Table Repo rt N um ber: 23-080-0005 Client Project Description: Belmont Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID 61416 Belmont Solids 03/161202310:30 03/21/2023 61416 Belmont Solids 03/16/202310:30 03/21/2023 61416 Belmont Solids 03/161202310:30 03/21/2023 61416 Belmont Solids 03/16/202310:30 03/21/2023 61416 Belmont Solids 03/16/2023 10:30 03/21/2023 61416 Belmont Solids 03116/202310.30 03/21/2023 61416 Belmont Solids 03/16/202310.30 03/21/2023 61416 Belmont Solids 03/16/202310:30 03/21/2023 WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN SM-4500-NH3C WP MTN 9045D WP MTN 4500NO3F-2011 WP MTN 60100 WP MTN SW-747113 WP MTN SM-4500-NH3C-TKN WP MTN SM-254OG WP MTN Page 2 of 7 r � ��� � 7521 (D Whitepine Road, Rkhmond, VA 23237 Main 804-743.4401° Fax 86M271.6"6 46381 ANALYTICAL wwwwaypolntanalytieal.com US Biosolids Inc Project Belmont Dennis Key Report pate : 03/29/2023 958 Hoots Road Information : Received ; 03/21/2023 Roaring River , NC 28669 Report Number: 23-080-0005 REPORT OFANALYSIS Brands Watson Lab No : 61416 Matrix: Solids Sample ID: Belmont Sampled: 3/16/2023 10,30 Test Results Units MQL DF Date ITime By Analytical Analyzed Method Moisture 97.0 % 0.010 1 03/22/2315.43 CJD SM-254OG Sulfur 9400 mg/Kg - dry 333 1 03/25/23 05:46 JTR 6010D Calcium 16500 mg/Kg - dry 1670 1 03/25/23 05:46 JTR 6010D Aluminum 43700 mg/Kg - dry 167 1 03/25/23 05:46 JTR 6010D Manganese _ 823 mg/Kg - dry 16.7 1 03/25/23 05:46 JTR 6010D Organic N 148700 mg/Kg - dry 8333 1 03/28/23 14:00 CALCULATION Nickel 21.1 mg/Kg - dry 8.33 1 03/25/23 05:46 JTR 6010D Lead 17.7 mg/Kg - dry 10.0 1 03/25/23 05:46 JTR 60101) Arsenic <16.7 mg/Kg - dry 16.7 1 03/28/23 00:13 JTR 6010D Selenium <16.7 mg/Kg - dry 16.7 1 03/25/23 05:46 JTR 6010D Test Results Units MQL DF Date/Time By Analytical Analyzed Method Total Solids 3.04 % 0.010 1 03/22/23 15:43 CJD SM-254OG Phosphorus 27900 mg/Kg - dry 167 1 03/25/23 05:46 JTR 6010D Copper 329 mg/Kg - dry 16.7 1 03/25/23 05:46 JTR 6010D Total Kjeldahl Nitrogen 149000 mg/Kg - dry 8330 1 03/28/23 14:00 CLP ;M-4500-NH3C-TKA Qualifiers/ DF Dilution Factor MQL Method Quantitation Limit Definitions Page 3 of 7 or . 0 Waypoint ANALYTICAL 46381 US Biosoilds Inc Project Belmont Dennis Key 958 Hoots Road Information Roaring River, NC 28669 Report Number : 23-oa0-0005 7621 Whitepine Road, Richmond, VA.23237 Main 804-743-9401 ° Fax 804.271.6446 www.wayooltitanalytical.com REPORTOF'ANAL YSI.S Report Date ; 03/29/2023 Received ; 03/21/2023 '6 Brandl Watson Lab No: 61416 Sample ID : Belmont Matrix: Solids Sampled: 3/16/2023 10:30 Potassium 4570 mgJKg - dry 333 1 03/25/23 05:46 JTR 6010D Magnesium 4130 mg/Kg - dry 167 1 03/25/23 05:46 JTR 6010D Sodium 5400 mg/Kg - dry 833 1 03/25/23 05:46 JTR 6010D Iron 22900 mg/Kg - dry 333 1 03/25/23 05:46 JTR 6010D Zinc 1880 mg/Kg - dry 41.7 1 03/25/23 05:46 JTR 6010D Ammonia Nitrogen <3330 mg/Kg - dry 3330 1 03/28/23 15:30 CLP SM-4500-NH3C Nitrate+Nitrite-N 343 mg/Kg - dry 167 1 03/23/23 14:36 ZBD 4500NO3F-2011 Cadmium <3,33 mg/Kg - dry 3.33 1 03/25/23 05:46 JTR 6010D Chromium 60.3 mg/Kg - dry 8.33 1 03/25/23 05:46 JTR 6010D Mercury <6A7 mg/Kg - dry 6.17 1 03/27/23 12:22 FDS SW-7471B pH 6.4 S.U. 1 C3/27/2317:15 CNB 9045D Molybdenum <8.33 mg/Kg - dry 8.33 1 03/25/23 05:46 JTR 6010D Qualifiers/ DF Dilution Factor MQL Method Quantitation Limit Definitions Page 4 of 7 Wayl3oint.(D ANALYTICAL Client: US BiosDlids Inc Project: Belmont Lab Report Number: 23-080-0005 Date: 3/29/2023 7621 Whitepine Road, Richmond, VA 23237 Main 804.743-9401 ° Fax 804-277.-6446 wwwmaypo€ntana lytical.com CASE NARRATIVE Metals Analysis Method 6010D Sample 61454 (Tyson Blowntsville) Analyte; Aluminum QC Batch No: L672212/L671763 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 61454 (Tyson Blowntsville) Analyte: Calcium QC Batch No: 1-672212/1-671763 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 61454 (Tyson Blowntsville) Analyte: Potassium QC Batch No: 1-672521/1-671763 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A past digestion spike was performed and passed quality control acceptance ranges. No matrix interference is suspected. Solids Total Mercury Analysis - CVAA Method 7471A Sample 61457 (NG5) Analyte: Mercury QC Batch No: 1-672319/1-672056 The matrix spike, matrix spike duplicate and the post digestion spike were all outside of the quality control acceptance ranges. Matrix interference is suspected Page 5 of 7 co 0 o CD A7 �Q CD (D Q S w O Q o� co 0 o r CD p NO CC3 = zr m Ia. =1 0 C N CD 03 � N Q a ao w m" 00 .� m Q v D 0 w 0 0 R a cD C 0 !ll CD 0 133 cu phi D A 0 w 0 O ►l 0 ¢1 3 .K CD 0 CD 0 0 CD CD Co Co CD CD C. N of O�O�O p W o 030 (D ch CL CD (TC(D� co A(On O R N C L cAi CD (D cr ao N Q o � 0 :3N u ' 0 N 0 O n 0 0 m CD CD 3• 0 O pi A CD •J 0 N 0 0 A fA 0. 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US Biosolids Inc. 958 Hoots Road 958 Hoots Road 958 Hoots Road Roaring River, NC 28669 Roaring River, NC 28669 Roaring River, NC 28669 Project 1 J 6 Irr► on `�' Sant le Information Lai) Number collection lriforrrialion Container Information Please Check Desired Tests Sample ID (Lab Use Only) Type Date Time Number Type Volume SLi SL.2 503 Nitrogen pH CCE Ag C1 Volatile Others of Bottles Metals Series Sorids t ^} d Grab 3-tfc_s3 iot3oq s Glass Plastic — oz —Pint Composite �{ qt Grab Giass — ptnt Com osite _ _ Plastic t — Grab Glass Qz _ Plastic mint Composite t — Grab Glass — P composite Plastic pint i clt Relin uished By: Si nature) Date Time Received By: (Signature) Date Time Test Packa e Details S ecial Instructions or Remarks SLI: Tn;al So iii,; jNinislum) Total l;iiidaW ,14nrogen. Phosphorus and Potasstr n: d � Sty: Baste rrsl SI.1 ply, Sulfur. Iron. Alumu:=,, Ma sar�ese. Copper And Zinc 503 Metals: Arsenic. Cadmium, Chromium, Mercury, Molybdenum, Lead, Nickel, Selenium. (Copper & Zinc included in SL2) Nhrxi,eta Series: Total Kiddahl. Ammonium. Nitrate e, Organic Nilrovcn CCE: Calcium Carbonate Equivalent or Toial neutralization Value (For Lime Treated Sludge) L'AR) �"C- I.AT3 RELIABLE LS, INC REPORT OF ANALYSES Attn: ZAC KEY U.S. BIOS LIDS, INC. PROJECT NAME: MAR 23 PO BOX 146 DATE: 04/26/23 RONDA, NC 28670- SAMPLE NU ER- 146747 SAMPLE ID- BELMONT DATE SAMP ED- 03/16/23 DATE RECEIVED- 03/16/23 SAMPLER- ZK TIME RECEIVED- 1120 DELIVERED BY- Zit Page 1 0$ 1 SAMPLE MATRIX- WW TIME SAMPLED- 1030 RECEIVED BY- DJ TYPE SAMPLE- Grab ANALYSIS ANALYSIS METHOD DATE TIME BY RESULT UNITS FECAL COLIFORM (GEOM. MEAN) SM 9221 E 03/16/23 16.20 RE 250,495 MPN/g LABORATORY DIRECTOR�- 2217 Graham Park Drive • Charlotte, NC 28273 Phone: (704) 588-8333 • Fax: (704) 588-8335 2217 Graham Park Drive PO Box 411483 Charlotte, NC 28241-1483 P DM PT.A❑ LlRATE•REL..IA BLE X.ABOR-11--EORX.ES, 11-4C NCCert#20;SCCert#99003= U.S. BIOSOLIDS e BELMONT • 03/16/23 FECAL COLIF.ORM, GEOMETRIC MEAN m e SM 9221 E 146747 1 5,030 3.17% 158,833.16 2 9,966 3.14% 317 456.02 3 12;500 3.20% 390724.88 4 7,407 3.51% 211037,25 5 7,532 3.18% - 236 851.12 6 $ 969 3.10% 289,310.00 7 6,994 3,22% 217,217.53 250,495 PNdM W'r�� UttItAT •RtL.tAI�LS LABO ORIES� iNC CHAIN OF CUSTODY Phone (7G4)588-8333 Fax (704) 588-8335 Shipping & Mailing: 2717 G -aham Park Drive Chariotl!te, NC 28273 It is esseh 1al that alt information be recorded on ha Ghafn of Custody document for wxeptance by PAR Laboratories, In--. ana the Norm carnllna apartment of Environmental and NalvraI Resources. Company Name ibtlllnftl Comments! Special Instructions U.S. B solids, Inc, Address _ PO Bo(946 City, State & zip code Ronda NC 28670 Paint of Contact ri Telephone Number Zach Key 336-467-3550 Sample Taken By: SIGNATURE ?#..A_ PRINTED NAME ARE SAMPL�S FOR STAT5or EPA REPORTING? YES 4>a NO 'Sample Type: Ow ww �� Gf Mw _ HW Solt Other Sample Tem� at time of sampling: ° C Sample Temp upon receipt: a C "'Field Pros road: Yes No _Teflon Liner/Zero Headspace: Yes No _ nla Residual Ch rine checked at time of sampling (YIN): Dechlorination Necessary (YIN): trVo�1 l�vw!eJ vf'' lcSP .f. .1�I.VN - rk�!!,!� 7 -1 Mie 1 .1. •!}T.Inm� .. P.7 i 3 a len it ` o r e A Ff CEO 'i I i ! J— Kaunquisneo oy uater! rme klzel Ratirlquished, Oateffime Reoelved by: oateffima ' C=Composite (i=Grab DW=brinking Water WW=Wastewater G4VMW=Groundwater Mon'doring Well HW=Hazardous Waste FZ F wr-ACCUR TE.RELIABLE QRAT RIES, INC WWW.PAR ABS.COM REPORT OF ANALYSES Attn: ZAC KEY U.S. BIOS LIDS, INC. PROJECT NAME: MAR 23 PO BOX 14 DATE: 04/26/23 RONDA, NCI 28670- SAMPLE NU BER- 146746 SAMPLE ID- BELMONT DATE SAMP ED- 03/16/23 DATE RECE VED- 03/16/23 SAMPLER- ZK TIME RECEIVED- 1120 DELIVERED BY- ZK Page 1 0 2 ANALYSIS TCLP CHAR pH VALUE CORROSIVI REACTIVIT FLASH POT IGNITABIL PAINT FIL TCLP META ARSENIC BARIUM CADMIUM CHROMIUM LEAD MERCURY SELENIUM SILVER TCLP PESZ ENDRIN LINDANE METHOXYCE TOXAPHENE ANALYSIS METHOD DATE TIME BY 1CTERISTICS TCLP 04/04/23 1149 CB TCLP 04/04/23 1149 CB PY TCLP 04/04/23 1149 CB e TCLP 04/04/23 1149 CB JT TCLP 04/04/23 1149 CB CTY TCLP 04/04/23 1149 CB PER TEST TCLP 03/23/23 0926 CB IS TCLP 03/27/23 1158 JR TCLP 03/27/23 1158 JR TCLP 03/27/23 1159 JR TCLP 03/21/23 1158 JR TCLP 03/27/23 1158 JR TCLP 03/27/23 1158 JR TCLP 03/27/23 1158 JR TCLP 03/27/23 1158 JR TCLP 03/27/23 1158 JR ICIDES TCLP 03/25/23 1558 VC TCLP 03/25/23 1558 VC TCLP 03/25/23 1558 VC LOR TCLP 03/25/23 1558 VC TCLP 03/25/23 1558 VC 2217 Graham Park Drive • Charlotte; NC 28273 Phone; (704) 588-8333 • Fax: (704) 588-8335 SAMPLE MATRIX- WW TIME SAMPLED- 1030 RECEIVED BY- DJ TYPE SAMPLE- Grab RESULT UNITS 6.6 S.U. NON NON 5 200 degrees F NON FL < 0.5 ppm < 10 ppm < 0.1 ppm < 0.5 ppm < 0.5 ppm < 0.02 ppm < 0.1 ppm < 0.5 ppm < 0.002 ppm < 0.04 ppm < 1 ppm < 0.05 ppm C NNF3 HrDrCI Z�xxxNF�YY a O nnn WH NNHxn H` - PamKM Hmt'3MM` � 1 I I xx>Mn` C]MM z a.aH'-3x! z �31-3>CXXjC nnnrr zr:Ar4ror 'd 'u 0 U1 N •` I v y 0 ro,v,oF<nnnvv00L'I yM M40m utv �� I I t' nI"'}nO3L-4 HI-IC7tatn00zz0 i `Xn0 n�-3i-30=z==-M L• t74r Z0 n 0 0 0 0 7w Mw H wM xzsxszt+mszm000Hxxx>~rroreH 0D a �dtyz rHHo0 NH]0g�;!-3L,tir zm a! — wOM -v�— > z > r < U] H cn n O z H H 2 C � H ro W 4 (D N o a6ria , c1 U ;`, Q.>`L� 3 z +rd pC 'X H MO z K M CO 06 O s .a P3 m ;U H H n H O i 'h Hrrx H ru MtrHgc 1H000 z n r +-I - z N L07�5dt•+k M 7C>ONCH�M 5n0 LC=T t0r1z 0 0i•3r z mzHm m = = z r X isV r+1 x+0ZN O +-3mm20 -G );�N O -- MxM r Q ZMMt4ZM H o 'Z' m LTJ z El LA I>i z Or [ 3 [T1 02 ti m t-q L� rp r-.y O O H b � ro r � > H 1-9+-3.31-3HH H+3+-3HHHH-3H}-3q- 313 -3HHH y13+AH913 9 m nnnnnnnnnncannnnnnnnc3nnnnnnnnn m z o rrt-'L'rrrrrrrrt-.1 rrrrrrrrrrrrrrrr H c 'd 'b ro rO ro ro ro rO 'D ro 'a ro '0 'd ro 'V +D rO ro ry 'O rd h7 r<J ro :O 'O 'o Z o a 0 x W 00000o C? 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Southern Soil Builders G r Stanley, NC 28164 958 Hoots Rd Soil Report Extraction Roaring River, NC 28669 ? Sampled Sampled County: Gaston �aiirnSF''- Soil T esting Seetian Client ID: 478946 Advisor ID: 231531 Sampled; 11/20/2023 Received: 11/2712023 Compieted: 01/2612024 Farm: Sample ID: BT91 Recommendations: Lime Nutrients (lb/acre) More Crop (tonslacre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1-Fescue/OGrass/T-im, M 0.0 120-200 0 10 0 0 0 0 0 0 Note: 12 11 2- Fescue/OGrassfrim, M 0.0 120-200 0 10 0 0 0 0 0 0 Note: 12 Test Results [units - W!Y in glcm3; CEC and Na in megi100 cm3; NO3-N in mgldm3]: Soil Class: Mineral HM% WN GEC BS% Ac pH P-1 K-I Ca% Mg% S-1 Mn-I Mn-AI1 Mn-A]2 Zn4 Zn-AI Cu-1 Na ESP SS-1 NOs-N 0.60 0.95 13.3 89 1.4 6.4 444 70 79 - 7 53 128 88 88 657 657 1145 0.0 North Carolina •1. Irotiacco Trot F and ccramlNssicm Reprogramming of the laboratory -information -management system that makes this report possible is being funded through a grant from the North Carolina Tobacco Trust Fund Commission. 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