NC0073181_Wasteload Allocation_19880727

NPDES WASTE LOAD ALLOCATION
PERMIT NO.: NCOO g3181
FACILITY NAME: f�X`AOcn 0,5Aelwill"
Facility Status: (FXLSTmr) PROPOSED
(circle one)
Permit Status: RENEWAL
(circle one)
Major—Minor�V"_
Pipe No: 001
Design.Capacity (MGD): oo
Domestic (S of Flow): 0
Industrial (% of Flow): 00
Comments:
RECEIVING STREAM:
� 2,e,
E- Y_
i2-,*\./'ey�
Class:
SC
Sub -Basin: 03-06— 11
K - '] W �l I�J/J,J\ c �
Reference USGS Quad: � (please a eh)
County: ia.,> He oyev
l
Regional Office: As Fa Mo Re We i; WS
(circle one)
Requested By! " Date: 8�
Prepared By: Date: ?:; Er
A
Reviewed
Date Rec.
rModeler
I JDV
S--aS-Pe
1 -1665 .J
Drainage Area (mid) Avg. Streamflow (cfs): Td�
7Q10 (cfs) Winter 7Q10 (cfs) 30Q2 (cfs)
Toxicity Limits: IWC % (circle one) Acute Chronic
aCaiC� CP�So�.c Mon;�ori^
Instream Monitoring: seo h4,.
Parameters
Upstream N Location
Downstream N Location
RU,VMA1Vj v9on,�or:41 gar all vn(Kmes err w siewaier
(taviny tk,_ iau ).'I+�• Con},�uous M0A;40r;A1 or weekly -Rew
Effluent
Characteristics
M on+C - J ver e.
Dall Na.
0� I �- G ceLE,,C^)IP
3o
G
SCA061e SOG Ml Q
O, I
O.Z
pH SU
6.8- 8 S
Tufb d # NtU
-nu A,s6r a 5kdii wist
r.NSt
we;V; w--6 r +.
J SD e(il.l z
6,J exu,!j4 Sp WLI
d }e aural LWroun1
XTE
I
I LD—
Retonrinanl 2 mo
e. u monioc n
%r a G
�e e an!
Tafl7 Reco
rr
i n J4 toC
T ene� bt,�unt� Xylene� kilroiene, varsol jonIA leae 6t dam,.
SI U 6L 4(,f-d 'I)1 +kA�- ✓'Mi+ 1 rdbLa A'of f�l�t((1M t'F( �'J NC�DIGCIL
o•i iolnrnn% S)toul� 'lN.� �'QP..�11i� +��.I tI'S w(tiolt�E+iiutn-f faxiu'%y 'kbf

Request No.: 4665
WASTELOAD ALLOCATION APPROVAL FORM
Facility Name: EXXON USA/WILMINGTON TERMINAL
NPDES No.: NCO073181
Type of Waste: INDUSTRIAL
Status: UNPERMITTED
Receiving Stream: CAPE FEAR RIVER
Classification: SC
Subbasin: 030617 Drainage area: sq mi
County: NEW HANOVER Summer 7010: cfs
Regional Office: WILMINGTON Winter 7Q10: cfs
Requestor: JULE SHANKLIN Average flow: cfs
Date of Request: 5/20/88 3002: cfs
Quad: K27NW
-------------------- RECOMMENDED EFFLUENT LIMITS -------------------------
Mo. Avg. Daily Max.
Wasteflow (mgd): 0.945
Oil & Grease (mg/1): 30 60
Settleable Solids (ml/1): 0.1 0.2
pH (su): 6.8-8.5 6.8-8.5
Turbidity (NTU): The discharge shall not cause the turbidity of tine
receiving waters to exceed 50 NTU. If the turbid;t.j
exceeds 50 NTU due to natural background conditia�\s
the discharge can not cause any increase in the
turbidity of the receiving water.
Toxicity Testing Req.: Acute, Episodic Monitoring (See Attached)
MONITORING
Upstream (Y/N): N Location:
Downstream (Y/N): N Location:
----------------------------- COMMENTS -----------------------------------
RECOMMEND FLOW MONITORING FOR ALL VOLUMES OF WASTEWATER LEAVING THE FACILITY.
RECOMMEND 2/MONTH EFFLUENT MO TOR%NG FOR OIL & GREASE, SETTLEABLE SOLIDS, ,I
pH, AND TURBIDITY. RECOMMENDe Ni`TDRING FOR TOLUENE, BENZENE, XYLENE, AND kL�,2i `rrc5'
LEAD BE DONE ON THE SAME SCHEDULE AS TOXICITY MONITORING (1st 5 DISCRETE 4_
DISCHARGE EVENTS). A REOPENER CLAUSE SHOULD BE PUT IN THE PERMIT TO ALLOW
FOR LIMITS TO BE PLACED ON TOXICANTS SHOULD THE FACILITY FAIL ITS WHOLE- anC QAALA0.I Foxu�1
EFFLUENT TOXICITY TEST. AbA 1'0 "r {1c t
5 act
Recommended by: ------- Date:
Reviewed by
Tech Support Supervisor:
Regional Supervisor:
Permits & Engineering:
-- Date:--��g$--
-- -- -- ---- --
- Date:
-- - - ---------
- --- -- ----- Date:---LILI---
RETURN TO TECHNICAL SERVICES BY: ___M 1 4_19B$___

Facility Narne F_k on aSA- W; jryt;n TerMiAeA j Permit # WG00-131 S i
ACUTE TOXICITY TESTING REQUIREMENT
Daphnid 48 hr - Monitoring for Episodic Events
The permittee shall conduct FIVE acute toxicity test
$ using protocols defined in E.P.A. Document
600/4-85/013 entitled "The Acute Toxicity of Effluents co Freshwater and Marine Organisms'.
The monitoring shall be performed as a Daphnia pulox or Ceriodaphnia 48 hour static test, using
effluent collected as a single grab sample. Effluent samples for self -monitoring purposes must be
obtained below all waste treatment. Sampling and subsequent testing will occur during the first five
discrete discharge events after the effective date of this permit. After monitoring of the first five
toxicity tests, the permittee will conduct one test annually, with the annual period beginning in
January of the next calendar year. The annual test requirement must be performed and reported by
June 30. If no discharge occurs by June 30, notification will be made to the Division by this date.
Toxicity testing will be performed on the next discharge event for the annual test requirement.
The parameter code for this test if using Daphnia pulex is TAA3D. The parameter code for this test
if using Ceriodaphnia is TAA3B. All toxicity testing results required as part of this permit
condition will be entered on the Effluent Discharge Form (MR-1) for the month in which it was
performed, using the appropriate parameter code. Additionally, DEM Form AT-1 (original) is to
be sent to the following address:
Attention: Technical Services Brimch
North Carolina Division of
Environmental Management
P.O. Box 27687
Raleigh, N.C. 27611
Test data shall be complete and accurate and include all supporting chemical/physical measurements
performed in association with the toxicity tests, as well as all dose/response data. Total residual
chlorine of the effluent toxicity sample must be measured and reported if chlorine is employed for
disinfection of the waste stream.
Should any test data from either these monitoring requirements or tests performed by the North
Carolina Division of Environmental Management indicate potential impacts to the receiving stream,
this permit may be re -opened and modified to include alternate monitoring requirements or limits.
NOTE: Failure to achieve test conditions as specified in the cited document, such as minimum
control organism survival and appropriate environmental controls, shall constitute an invalid test.
Failure to submit suitable test results will constitute a failure of permit condition.
7Q10 1 jdul cfs
Permitted Flow 1fa►r ;able
IWC%
MGD Recommende-J by:
Basin & Sub -Basin 430617
Receiving Stream r r
County Date 7/2G��3R
**Acute Toxicity(Daphnid 48 hr) Monitoring, EPISODIC, See Part �Conditioner.

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EX
PN COMPANY U.S.A.
BOX 4415-HOUSTON, TEXAS 77210-4415
MARKETING DEPARTMENT
REAL ESTATE III ENGINEERING
ENVIRONMENTAL SERVICES
April 22, 1988
RECEIVED
APR 2 7 1�cj
Wilmington Regional Office
DEM
Wilmington Terminal
NPDES Permit Application >!#NC0073181
N. C. Department of Natural Resources
and Community Development
Division of Environmental Management
7225 Wrightsville Avenue
Wilmington, North Carolina 28403-3696
Atten: Mr. Edward Beck
Environmental Technician
Gentlemen:
Enclosed are reports of the laboratory analyses on water samples taken on
March 8, 1988 at the Exxon Company U.S.A. marketing terminal in Wilmington,
North Carolina. These samples were taken in accordance with your letter of
February 22, 1988.
Please note that tanks 9, 11, 130 14, 15, 19, 20, 21, 22, 27, 28, 30, 31, 32,
and 33 were not sampled. These tanks did not contain a sufficient amount of
water to allow a sample to be taken. These storage tanks accumulate water at
a very slow rate and consequently are drained once a year, if even that often.
If you have any questions or need additional information, please contact me at
the letterhead address or on [phone].
Sincerely,
i • `l �i ii*; ti
Richard J. Cieri
3298D °ERNI! T S -3, E,..d E-CRINIG
RJC
enclosure
w/o enclosure
Mr. J. R. Hastings
Mr. L. W. Lindeen
A DIVISION OF EXXON CORPORATION

IL
�orrsu�a9 vad✓��ra�lca���m�sls
ESTABLISHED 1903
Main Office
1711 Castle Street
P.O. Box 629
Wilmington, N.C. 28402
979.762 7082 919.762.8956
TWX 51OL937-0280
RICHARD CATLIN 4 ASSOCIATES
POST OFFICE BOX 557
WRIGHTSVILLE BEACH, N.C. 28480
SAMPLE DESCRIPTION:
REPORT DATE: 3-25-88
.
EXXON WILMINGTON TANK BOTTOMS
G' U
Branch Office
4736 Spruill Ave.
North Charkston, S.C. 29406
803.747.1589
DATE RECEIVED: 3-08-88
DATE COLLECTED: 3-08-88
COLLECTED BY: STEVE TYLER
LAB I. D . i EW 2 033
TEST/SAMPLES
TANK # 1 TANK # 3
UNITS
TANK � 4
PARAXYLENE AV 100
DIESEL
PARAXYLENE
PPM 61.7 ---
GASOLINE
PPM --- 36.4
0.63
KEROSENE
PPM
DIESEL FUEL
rpm
- ^
15.3
TESTS/SAMPLES
PARAXYLENE
GASOLINE
KEROSENE
DIESEL FUEL
TANK f 5
UNITS UKLEADED
FEM
PPM
PPM
PPM
TANK i6 TANK V
KEROSENE RECiRJR
21.3 0.11 15.3
--- 12.4 ---
ij TORY DIRECTOR
TOTAL AMOUNT: 3,025.00

Main Office
7711 Castle Street
P.O. Box 629
Wilmington, N.C. 28402
919-762 7062 919-762.8956
TWX 510 937-0280
�ionsu%ir9 and,nallcai��i�mrs/s
ESTABLISHED 1903
REPORT DATE: 3-25-88
RICHARD CATLIN 6 ASSOCIATES
POST OFFICE BOX 557
WRIGHTSVILLE BEACH, N.C. 28480
SAMPLE DESCRIPTION: TANK BOTTOMS
TANK 112 TANK 116
TESTS/SAMPLES UNITS VARSOL tl VARSOL t18
XYLENE
FFM
A� VARSOL
PPM
N. GASOLINE
FPM
JET FUEL
FPM
TOLUENE
FPM
67.0
0.22
0.05
Branch Office
4736 SPruill Ave.
North Charleston, S.C. 29406
803-747-1589
DATE RECEIVED: 3-08-88
DATE COLLECTED: 3-08-88
COLLECTED BY: STEVE TYLER
LAB I.D. / EW 2033
TANK 117
TURBO A
31.9
TANK 1 18
XYLENE
69.8
0.55
TANK 929
TESTS/SAMPLES UNITS EXXON EXTRA
XYLENE
PPM
VARSOL
PPM ---
GASOLINE
PPM •25 9
JET FUEL
PPM ---
TOLUENE
PPM _--
`•1',
LABORATOUY• DIRECTOR

Main Office
1711 Castle St.
Wilmington, N.C. 28402
919.762.7082
T WX 510-937-0280
DEMONSTRATION FOR:
Date & Time
Waste Sampled:
IL
Qs-y� 4
ans" n. y a"cf .�'r�c,�7lca�&,e6 rrz�rls
ESTABUSM60 19M •
RICHARD CATLIN 6 ASSOCIATES Branch Office
POST OFFICE BO:► 557 4736 Spruill Ave.
WRIGHTSVILLE BEACH, N.C. 28480 North Charleston, S.C.
803-747.1589
CERTIFICATION OF HAZARDOUS WASTE ANALYSIS
EXXON GSA TANK BOTTOMS TANK 029
3-08-88 Date b Time Sample 3-08-88 2:45
Received in Lab:
Date Finished
Results
Ignitability:
I. Flash Point (*F)
3-10-88
ICONS
<-
Corrosivity:
1: pH
2. Corrosion rate
Reactivity:
s.
I. Cyanide
2. Sulfide '
Extraction (Toxicity) •
1. Arsenic ?PM
3-21-83
<0.05
2. Barium PPM
3-23-88
<0.20
3. Cadmium PPM
3-23-88
<0.01
4. Chromium PPM
3-23-88
0.39
5. Lead P?!1
3-23-88
0.02
6. Mercury PPII
3-15-88
<0.002
7. Selenium PPM
3-17-88
<0.01
8. Silver PPti
3-23-88
<0.01

Date Finished Results
11. Methoxychlor
oxap ene
13. 2, 4-D
14. 2,495-TP
All tests performed according to specifications contained in "Test Methods
for Evaluating Solid Waste" - USEPA S.N. 846)
Certification/Signacure:
I have personally examined and am familiar with the information submitted
in this certification, and I hereby certif} under' penalty of law that this in-
formation is true, accurate and complete. I am aware that there are significant
penalties For submitting false information, including the possibility of fine
and imprisonment.
Law and Company of Wilmington, Inc.
Comments:
7=

Main Office
1711 Cast/s St.
Wilmington, N.C. 28402
919.762-7082
TWX 51a937.0280
eons
uAY aftar✓�Ra��ca�i�vm���ls
WAeusHEo 19M
RICHARD CATLIN d ASSOCIATES
POST OFFICE B0� 557
WRIGHTSVILLE BEACH, N.C. 28480
Branch Office
4736 Spruill Ave.
North Charleston, S.C.
803-747 1589
CERTIFICATION OF
HAZARDOUS WASTE ANALYSIS
DEMONSTRATION
FOR:
EXXON USA
TANK BOTTOMS TANK 118
• Data b Time
3-08-88
Date b Time Sample
3-08-88 2:45
Waste Sampled:
Received in Lab:
Date
Finished
Results
Ignitabilicy:
I. Flash Point
('F)
3-10-88
NONZ
Corrosivity:
1. pH
2. Corrosion rate
a'
Reactivity:
.
I. Cyanide
2. Sulfide
Extraction (Toxicity)
1. Arsenic
PPM
3-21-83
<0.05
2. Barium
ppM
3-23-88
<0.20
3. Cadmium
ppM
3-23-88
0.01
4. Chromium
ppM
3-23-88
<0.02
5. Lead
ppti
3-23-88
0.19
6. Mercury
ppit
3-15-88
<0.002
7. Selenium
ppM
3-17-88
<0.01
8. Silver
pylg
3-23-88
<0.01

Date Finished Results
11.
Methoxychlor
12.
Toxaphene
13.
2, 4-D
14.
2 , 4 , S--TP
All tests performed according to specifications contained in "Test Methods
for Evaluating Solid Waste" - USEPA S.W. 846)
Certification/Signature:
I have personally examined and am familiar with the information submitted
In this certification, and I hereby certify under•penalty of law that this in-
formation is true, accurate and complete. I am aware that there are significant
penalties for submitting false information, including the possibility of fine
and imprisonment.
Law and Company of Wilmington, Inc.
Comments:
1

Main Office
1711 Castle St.
Wilmington, N.C. 28402
919.762 7082
TWX 510-937-0280
�orrsr��r,9 c:rrd,�riQ�lcQ���rrr��-ls
"TASusNEo 19M
RICHARD CATLIN & ASSOCIATES Branch Office
POST OFFICE B0JX 557 4736 Spruill Ave.
WRIGHTSVILLE BEACH, N.C. 28480 North Charleston, S.C.
803-7471589
CERTIFICATION OF HAZARDOUS WASTE ANALYSIS
DEMONSTRATION FOR:
E)XON USA
TANK BOTTOMS TANK #17
Data 6 Time
Date 6 Time Sample
Waste Sampled:
3-08-88
Received in Lab: 3-08-88 2:45
Date Finished
Results
Ignitabilicy:
1. Flash Point ('F)
3-10-88
NONE
Corrosivity:
1. pH
2. Corrosion rate
Reactivity:
1. Cyanide
2. Sulfide
Extraction (Toxicity)
1. Arsenic ppls
3-21-83
<0.05
2. Barium PPH
3-23-88
<0.20
3. Cadmium PPM
3-23-88
0.03
4. Chromium Pptq
3-203-88
<0.02
5. Lead ppM
3-23-88
<0.02
6. Mercury Pp11
3-15-88
0.005
7. Selenium PpM
3-17-88
<0.01
8. Silver pptl
3-23-88
0.01
9. Endrin

Date Finished
11.
Methoxychlor
12.
Toxaphene
13.
2, 4-D
14.
2.4,5-TP
Results
All tests performed according to specifications contained in "Test Methods
for Evaluating Solid Waste" - USEPA S.W. 846)
Certification/Signature:
I have personally examined and am familiar with the information submitted
in this certification, and I hereby certify under penalty of law that this in-
formation is trueg accurate and complete. I am aware that there are significant
penalties for submitting false information. including the possibility of fine
and imprisonment.
Law and Company of Wilmington. Inc.
Comments:

•
t�Orrsrrlhn►9 c1sc�.�?'nraylca! C�/t�mrs�ls
- WAausHEo 1903
Main Office
1711 Castle St.
RICHARD CATLIN 6 ASSOCIATES
Branch Office
Wilmington, N.C. ?840?
POST' OFFICE 80:: 557
4736Spruill Ave.
919-762-7082
WRIGHTSVILLE BEACH, N.C. 28480 North Charleston, S.C.
TWX 5la937.0280
803-747.1589
CERTIFICATION OF HAZARDOUS WASTE ANALYSIS
DEMONSTRATION FOR:
EXXON USA TANK BOTTONS TANK #16
Date 6 Time
Waste Sam led:
P
Date b Time Sample
3-08-88
Received in Lab:
3-08-88 2:45
Date Finished Results
Ignicability:
1. Flash Point (OF)
3-10-88 NONE
-.. Corrosivity:
--
V. pH
2. Corrosion rate
r Reactivity:
I. Cyanide
2. Sulfide
Extraction (Toxicity)
I. Arsenic PPM
3-21-83 <0.05
2. Barium PPM
3-23-88 <0.20
3. Cadmium PPM
3-23-88 <0.01
4. Chromium PPM
3-23-88 <0.02
5. Lead PPl1
3-23-88 0.02
6. Mercury PPl1
3-15-88 <0.002
7. Selenium PPM
3-17-88 <0.01
8. Silver Ppt1
3-23-88 <0.01
9_ Fndrin

Date Finished
11. Methoxychlor
12. Toxaphene
13. 2, 4-D
14. 214,5-TP
Results
All tests performed according to specifications contained in "Test Methods
for Evaluating Solid Waste" - USEPA S.W. 840)
Certification/Signature:
I have personally examined and am familiar with the information submitted
In this certification, and I hereby certify under penalty of law that this in-
formation is true, accurate and complete. I am aware that there are significant
Penalties for submitting false information, including the possibility of fine
and imprisonment.
Law and Company of Wilmington, Inc. 4U
Comments:

Main Office
1711 Castle St.
Wilmington, N.C. 28402
919-762.7082
TWX 510-937-0280
l-�Q�'G'����-ems
WAeusHEEo 19M
RICHARD CATLIN 6 ASSOCIATcS Branch Office
POST OFFICE BOX 557 4736Spruill Ave.
WRIGHTSVILLE BEACH, N.C. 28480 Norrh Charleston, S.C.
803-747.1589
CERTIFICATION OF HAZARDOUS WASTF ANALYSIS
DEMONSTRATION FOR:
EXXON USA
TANKS BOTTOMS TANK #12
' Date b Time
^•c�
3-08-88
Date b Time Sample
3-08-88 2:45
Waste Sampled:
Received in Lab:
Dace Finished
Results
Ignitabilicy:
1. Flash Point (*F)
3-10-88
NONZ
Corrosivity:
U. pH
2. Corrosion rate
Reactivity:
1. Cyanide
2. Sulfide
Extraction (Toxicity) '
1. Arsenic PP11
3-21-83
<0.05
2. Barium ppH
3-23-88
<0.20
3. Cadmium PpM
3-23-88
0.05
4. Chromium ppM
3-23-88
<0.02
5. Lead ppH
3-23-88
0.04
6. Mercury pprt
3-15-88
0.009
7. Selenium ppM
3-17-88
<0.01
8. Silver pptl
3-23-88
<0.01

'
a"SMA" a rd, �Q�lcc��i�orrr.:,-ls
9 y
. ESTAOUSME019M
Main Office
1711 Castle St.
RICHARD CATLIN & ASSOCIATES
Branch Office
Wilmington, N.C. ?8402
POST OFFICE 80:: 557
4736 Spruill Ave.
919-762-708?
�JRIGHTSVILLE BEACH N.C.
� 28480
North Charleston, S.C.
TWX 510-937-0280
803-747--1589
CERTIFICATION OF HAZARDOUS WASTR ANALYSIS
DEMONSTRATION FOR:
EXXON USA TANK BOTTOMS TANK 05
a
Date 6 Time
Waste Sampled:-08-88
Data 6 Time Sample
Received in Lab:
3-08-88 2:45
Date Finished Results
Ignitability:
I. Flash Point (OF)
3-10-88 NONL
Corrosivity:
-
I. pH
2. Corrosion rate
-
Reactivity:
I. Cyanide
J
'
2. Sulfide
Extraction (Toxicity)
1. Arsenic PPM
3-21-83 <0.05
2. Barium PPM
3-23-88 <0.20
3. Cadmium PPM
3-23-88 <0.01
4. Chromium PPM
3-25-88 <O.02
5. Lead PPH
3-23-88 0.11
6. Mercury PPt1
3-15-88 <0.002
7. Selenium PPM
3-17-88 <0.01
8. Silver PF11
3-23-80 <0.01
9. End rin
` V

Date Finished
11.
McEhoxyFhlor
12.
Toxaphene
13.
2, 4-D
14.
2,4g5-TP
Res ul is
All tests performed according to specifications contained in "Test Methods
for Evaluating Solid Waste - USEPA S.W. 646)
Certification/Signature:
I have -personally examined and am familiar with the information submitted
in this certification. and I hereby certify under penalty of law that this in-
formation is trues accurate and complete. I am aware that thert are significant
Penalties for submitting false informationg including the possibility of tine
and imprisonment.
Law and Company of Wilmington. Inc.
Comments:

G'aRs��.� Q�ar.��al'��Ql'G'�m.�•rs
9 y
WASUSHEO 1903 •
Main Office
RICHARD CATLIN 6 ASSOCIATES
Branch Office
1711 Castle St.
POST OFFICE B0� 557
4736 Spruill Ave.
Wilmington, N.C. 28402
WRIGHTSVILLE BEACH, N.C. 28480
Norrh Charleston, S. C.
919-762-7082
803-747-1589
TWX 510-937-0280
CERTIFICATION OF HAZARDOUS WASTE ANALYSIS
DEMONSTRATION FOR:
EXXON USA TANK BOTTOMS TANK f7
Date b Time
Date a Time Sample
Wasce Sampled:
3-08-88 Received in Lab:
3-08-88 2:45
Dace Finished
Results
Ignitabilicy:
1. Flash Point ('F)
3-10-88 BONE
Corros ivi ty:
L pH
2. Corrosion rate
} Reactivity:
' 1. Cyanide
2. Sulfide
Extraction (Toxicity)
'
1. Arsenic PPM
3-21-83 <0.05
2. Barium PPM
3-23-88 <0.20
3. Cadmium PPM
3-23-88 <0.01
4. Chromium PPM
3-23-88 <0.02
5. Lead Ppt!
3-23-88 0.13
6. Mercury PPII
3-15-88 0.021
7. Selenium PPM
3-17-88 <0.01
8. Silver PPri
3-23-88 <0.01

Date Finished
11. Methoxychlor
12. Toxaphene
13. 2, 4-D
14. 2.425-TP
Results
All tests performed according to specifications contained in "Test Methods
for Evaluating Solid Waste" - USEPA S.N. 846)
Certification/Signature:
I have. personally examined and am familiar with the information submitted
in this certification, and I hereby certify under penalty of law that this in-
formation is true$ accurate and complete. I am aware that there are significant
penalties for submitting false information, including the possibility of fine
and imprisonment.
Law and Company of Wilmington, Inc.
Comments:

.4
Main Office
1711 Castle St,
Wilmington, N.C. 28402
919-762-7082
TWX 510-937-0280
�a
V�RSilllllfQ Qnae.! It al[ j e-cQ! VIIQl!ll.Mv
ESTAausHEo 19M
RICHARD CATLIN & ASSOCIATES
POST OFFICE BOX' 557
WRIGHTSVILLE BEACH, N.C. 28480
CERTIFICATION OF HAZARDOUS WASTE ANALYSIS
Branch Office
4736 Spruill A ve.
North Charleston, S. C.
803-747.1589
DEMONSTRATION FOR:
EXXON USA
TANK BOTTOMS TANK f6
c
Date b Time
Date 6 Time Sample
Waste Sampled:
3-08-88
Received in Lab-: 3-OS-88 2:45
Date Finished
Results
Ignitability:
1. Flash Point (•F)
3-10-88
I;ON%
Corrosivity:
1. pH
'
2. Corrosion rate
Reactivity:
1. Cyanide
2. Sulfide
Extraction (Toxicity)
1. Arsenic ?Pis
3-2I-83
<0.05
2. Barium PPM
3-23-88
<0.20
3. Cadmium PPM
3-23-88
<0.01
4. Chromium PPM
3-23-88
<0.02
5. Lead PPri
3-23-88
0.02
6. Mercury PF11
3-15-88
0.002
7. Selenium PPM
3-I;-88
<0.01
S. Silver Ppji
3-23-88
<0.01
9. Endrin

Date Finished
11.
Methoxychlor
12.
Toxaphene
13.
2, 4-D
14.
2,495-TP
Results
All tests performed according to specifications contained in "Test Methods
for Evaluating Solid Waste - USEPA S.W. 846)
Certification/Signature:
I have personally examined and am familiar with the information submitted
in this certification. and I hereby certify under•penalty of law that this in-
formation is true, accurate and complete. I am aware that there are significant
penalties for submitting false information. including the possibility of tine
and imprisonment.
Law and Company of Wilmington, Inc.
Comments:

Main Office
1711 Castle St.
Wilmington, N. C. 28402
919-762 7082
TWX 510-937.0280
G�orrsri�ls9 c1sd.�'rtalyfscc�G'�.�vrrs.:sls
UTAeusNFo :ow
RICHARD CAiLIN 6 ASSOCIATE'S
POST OFFICE BO:: 557
WRIGHiSVULE BEACH, N.C. 28480
Branch Office
4736 Spruill A ve.
North Charleston, S.C.
803-747.1589
CERTIFICATION OF HAZARDOUS WASTR ANALYSIS
DEMONSTRATION FOR: E =01i USA TANK BOT:GMS 1ANK #4
Date b Time Date b Time Sample
Waste Sampled: 3-08-88 Received in Lab: _3 08-88 2!45
Date Finished Results
Ignitability:
I.
Flash Point (*F)
3-10-88
Corrosivity:
V.
pH
2.
Corrosion
rate
Reactivity:
I.
Cyanide
Y.
Sulfide
Extraction (Toxicity)
I.
Arsenic
PPM
3-21-88
2.
Barium
PPM
3-23-88
3.
Cadmium
PPH
3-23-8§
4.
Chromium
PPM
3-2S-88
5.
Lead
PPM
3-23-88
6.
Mercury
PPM
3-15-88
7.
Selenium
PPM
3-17-88
8.
Silver
PPM
3-23-88
NONE
<0.05
0.21
0.04
<0.02
0.18
<0.002
<0.01
0.02
9. End r in

f
11.'Methoxychlor ~
12. Toxaphene
13. 2 o 4-D
14. 29495-TP
All tests performed according to specifications contained in "Test Methods
for Evaluating Solid Waste - USEPA S.W. 846)
Certification/Signature:
I have personally examined and am familiar with the information submitted
in this certification, and I hereby certify under -penalty of law that this in-
formation is true, accurate and complete. I am aware that there are significant
penalties for submitting false information, including the possibility of fine
and imprisonment.
Law and Company of Wilmington, Inc. UL
Comments:
r

Main Office
1711 Castle St.
Wilmington, N.C. 28402
919-762-7082
TWX 5la937-0280
rr On
60'ffsSim y anar.
EsrAsuSHEo 19W
RICHARD CATLIN b ASSOCIATES
POST OFFICE BOX' 557
WRICHTSVILLE BEACH, N.C. 28480
CERTIFICATION OF HAZARDOUS WASTE ANALYSIS
Branch Office
4736 Spruill Ave.
Norrh Charleston, S. C.
803 747.1569
DEMONSTRATION FOR:
E XON USA TANK
BO AOMS :ANK 3
Dote 6 Time
Date & Time Sample
' . Waste Sampled:
3-OS-88
3-08-88 2:
Received in Lab: 45
Date Finished
Results
Ignitability:
1. Flash Point ('F)
3-10-88
NONE
Corrosivity:
�i
I. pH
2. Corrosion rate
Reactivity:
1. Cyanide
2. Sulfide
'
Extraction (Toxicity)
.
1. Arsenic PPM
3-21-88
<0.05
2. Barium FPM
3-23-88
<0.20
3. Cadmium PPM
3-23-88
0.01
4. Chromium PPM
3-23=88
<0.02
5. Lead PPM
3-23-88
0.98
6. Mercury PPM
3-15-88
<0.002
7. Selenium PPM
3- 17-88
< 1 .00
8. Silver PPM
3-23-88
<0.01
9. Endrin

Date Finished
11.
Methoxychlor
12.
Toxaphene
13.
2. 4-D
14.
2.495-TP
Results
All tests performed according to specifications contained in "Test Methods
for Evaluating Solid Waste - USEPA S.W. 846)
Certification/Signature:
I have personally examined and am familiar with the information submitted
in this certification. and I hereby certify under penalty of law that this in-
formation is true, accurate and complete. I am aware that there are significant
penalties for submitting false information. including the possibility of fine
and imprisonment.
Law and Company of Wilmington. Inc.QP
Comments:

Main Office
1711 Castle St.
Wilmington, N.C. 28402
919-762-7082
TWX 510-937-0280
��rsr��rr9 alra�.�r�a�l'ca���mf�-ls
WAeusH60 19M •
RiCHARD CA:LiN 6 ASSOCIATE'S Branch Office
POST OFFICE BO:: 557 4736 Spruill A ve.
WRIGH S�':LLE DEACIi • N . C . 284 AO North Charleston, S. C.
803 747.1589
CERTIFICATION OF HAZARDOUS WASTE ANALYSIS
DEMONSTRATION FOR: EX"OkPON USA ,ANK B0:7011S TANK # 1 (PARACYLF.NE )
Date 6 Time Date b Time Sample
Waste Sampled. 3-OS-88 Received in Lab:
Date Finished Results
Ignitability:
1. Flash Point (*F)
3-10-88
-:.
Corros ivi ty :
1. pH
2. Corrosion rate
Reactivity:
•
1. Cyanide
2. Sulfide
'
Extraction (Toxicity)
.
1. Arsenic PPM
3-21-88
2. Barium FPM
3-23-88
3. Cadmium ppli
3-23-88
4. Chromium ppM
3-23 88
'
5. Lead ppM
3-23-88
6. Mercury PPt1
3-15-88
7. Selenium FP!!
3- 17-88
8. Silver PPl1
3-23-88
9. End r in
NONE
3 wers.
<0.20
0.09
0.03
0.47
<0.002
<1.00
0.U5
3-08-88 2:45

` Date Finished
Results
11. Methoxychlor
j� 12. Toxaphene
I
13. 2, 4-D
14. 2 , 4 , 5-TP
i All tests performed according to specifications contained in 'lest
for Evaluating Solid Waste" - t Methods
USEPA S.N. 846)
Certifi
cation/Signature:
I have personally examined and am familiar with the information submitted
in this certification, and I hereby ce{tify under penalty of law that
formation is true, accurate and complete. I am aware that there this in-
formation'
penalties for submitting false information, including the are significant
and imprisonment. 8 possibility of fine
Law and Company of Wilmington, Inc.
Comments: