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HomeMy WebLinkAboutNC0006033_Staff Comments_1989110641 DIVISION OF ENVIRONMENTAL MANAGENIENT Monday, November 6, 1989 MEMORANDUM TO: Richard Bridgeman�� THROUGH: Ken Eagleson FROM: Larry Ausley SUBJECT: JPS Autoproducts Corp. NC0006033 Gaston Co. Basin 030836 In response to your letter concerning the referenced facility,we have decided that the chronic toxicity test performed by the facility in September 1989 at a concentration of 7% should be accepted as a good faith effort by the facility to continue monitoring by the administrative letter in effect prior to issuance of the permit. We agree that the first testing required by the permit should be performed in December 1989. To answer you specific questions on this matter, the following is offered: Q-1. Given the above, was the permittee in error for conducting the test at an effluent concentration of 7% A-1. Ideally this should have been performed at the correct IWC of 4.7% although the facility has the right to perform any additional monitoring not required by the permit. Q-2. Should a second (consecutive) failure precipitate an NOV." A-2. As we are accepting this as part of the administrative letter monitoring requirement information, essentially before the presence of a pen -nit imitation, no. Should the test have been performed correctly, under permit requirements, a second failure should instigate an NOV. If we were to accept this test as submittal under permit limitation, it would have received a "bad test" letter and required retesting within 30 days. Q-3. Should the failure precipitate monthly monitoring? A-3. As the September test is being accepted as an administrative letter data point we don't feel that it should instigate required monthly testing, essentially prior to the existence of a permit requirement Q-4. If so, prior to December 1959? A-4. See 3. With regard to your comment on making a coordination in testing months on transition from a letter requirement to a permit requirement or from quarterly to monthly, it is agreed that this would be a helpful practice. I intend to discuss this with Tom Stockton to see if a logical way of doing it can be placed into the limits development process. If you have further questions on this matter, please contact me at (919) 733-2136 cc:Dennis Ramsey Michael L. Parker, MRO Tom Stockton State of North Carolina Department of Natural Resources and Community Development Division of Environmental Management 512 North Salisbury Street • Raleigh, North Carolina 27611 James G. Martin, Governor William W. Cobey, Jr., Secretary Mr. Sam Griggs JPS Autoproducts Corporation PO Box 208 Greenville, SC 29602 Dear Mr. Griggs: October 18, 1989 R. Paul Wilms Director 0 0 T 13 1989 HRArcH Subject: Modificatio o NPDES Permit No.WIC0006033 JPS AutoprIpducts Corporation Gaston County In accordance with your request for permit modification, the Division of Environmental Management is forwarding herewith a modification to the subject permit. This modification is to require monthly instead of weekly monitoring requirements for total chromium, sulfides, and ammonia as nitrogen. A revised effluent sheet is attached and should be inserted into your permit. The old effluent sheet should be discarded. All other terms and conditions contained in the original permit remain unchanged and in full effect. This modification is issued pursuant to the requirements of North Carolina General Statute 143-215.1 and the Memorandum of Agreement between North Carolina and the U.S. Environmental Protection Agency dated December 6, 1983. This permit modification becomes effective immediately. If this decision is unacceptable to you, you have the right to an adjudicatory hearing upon written request within thirty (30) days following receipt of this letter. This request must be in the form of a written petition, conforming to Chapter 150B of the North Carolina General Statutes, and filed with the Office of Administrative Hearings, Post Office Drawer 11666, Raleigh, North Carolina, 27604. Unless such a demand is made, this decision shall be final and binding. Pollution Prevention Pays P.O. Box 27687, Raleigh, North Carolina 27611-7687 Telephone 919-733-7015 An Equal Opportunity Affirmative Action Employer If you have any questions concerning this permit, please contact Mr. Dale Overcash at telephone number (919) 733-5083. Sincerely, ` / R. Paul Wilms Enclosure cc: Central Files Mooresville Regional Office Technical Support Branch Mr. Jim Patrick, EPA A. M . EFFLUENT LIMITATIONS AND MONITORING REQUIREMENTS Final NPDES No. NC0006033 During the period beginning on the effective date of the Permit and lasting until expiration, the Permittee is authorized to discharge from outfall(s) serial number(s) 001. Such discharges shall be limited and monitored by the Permittee as specified below: Effluent Characteristics Discharge Limitations Lbs da Monthly Avg. Daily Max. Flow BOD, 5Day, 20 Degrees C 304.0 532.0 Total Suspended Residue 809.0 1618.0 COD 3474.0 7399.0 Sulfide 8.9 17.8 Phenols 0.7 Total Chromium 4.5 8.9 Temperature Dissolved Oxygen Conductivity NH3 as N Total Residual Chlorine Fecal Coliform (geometric mean) Total Nitrogen (NO2 + NO3 + TKN) Total Phosphorus Chronic Toxicity **** Pollutant Analysis ***** Monitoring Requirements Other Units (Specify) **Measurement Sample Monthly Avg. Daily Max. Frequency Type 4.0 MGD Continuous Recording Daily Composite Daily Composite Weekly Composite Monthly Grab 21.0 ug/1 Weekly Grab Monthly Composite ** Daily Grab Grab Grab Monthly Composite Daily Grab 1000.001/100 ml 2000./100 ml Daily Grab Monthly Composite Monthly Composite Quarterly Composite Annually Sample i Or t E E E E E E E, U, U, D U, D E E E, U, E E E E Vol 1. I - Influent, E - Effluent, U - Upstream at bridge just above outfall, D - Downstream at upper Armstrong Bridge. All stream samples shall be grab samples. Daily stream sampling frequency may. be reduced at each sampling station to one time per week except during the months of June, July, August, and September when the frequency must be no less that three times per week at each sampling station. ** Daily means every day on which a wastewater discharge occurs except Saturdays, Sundays, and legal holidays. *** The temperature of the effluent shall be such as not to cause an increase in the temperature of the receiving stream of more that 2.8 Degrees C and in no case cause the ambient water temperature to exceed 32 Degrees C. **** Chronic Toxicity (Ceriadophnia) P/F at 4.7%, March, June, September, December, See Part III, Condition No. G. ***** See Part III, Condition No. H. The pH shall not be less than 6.0 standard units nor greater than 9.0 standard units and shall be monitored daily at the effluent. There shall be no discharge of floating solids or visible foam in other than trace amounts. State of North Carolina r Department of Natural Resources and Community Development Division of Environmental Management 512 North Salisbury Street • Raleigh, North Carolina 27611 James G. Martin, Governor R. Paul Wilms William W. Cobey, Jr., Secretary Director October 10, 1989 Mr. Samuel H. Griggs Director of.Environmental Affairs JPS Converter and Industrial Corp. P.O. Box 208 Greenville, SC 29602 Subject: JPS Automotive Products Corp. Cramerton Plant Monitoring Frequencies NPDES No. NC0006033 Gaston County Dear Mr. Griggs: I am writing in response to your letter of August 31 concern- ing the NPDES permit monitoring frequencies for phenols, chromium, sulfides, ammonia, total phosphorus, and total nitrogen. The data you submitted indicate that the monitoring frequency for chromium, sulfides, and ammonia can be reduced to monthly. However, the monitoring frequency for phenols will remain as weekly. The phenols data submitted for March, 1988 and July, 1989 indicated concentrations of 30 ug/1 and 21 ug/1 respectively which are at or above the permitted level of 21 ug/l. The total nitrogen and total phosphorus monitoring require- ments will remain as monthly. 15 NCAC 2B.0508(d)2(B) requires all facilities in the Catawba River Basin which have a design capacity greater than 1 mgd to monitor for these parameters monthly. In addition, the receiving stream, South Fork of the Catawba River, flows into Lake Wylie which the Division of Environmental Manage- ment is currently monitoring for nutrient sensitivity. Therefore, I will not reduce these monitoring requirements at this time. If you have any further questions, please contact Trevor Clements or Dale Overcash of my Water Quality staff at ( 919) 733-5083 . I hope that the Division's response is satisfactory to the company. However, if this letter does not adequately address your concerns, you have the right to an adjudicatory hearing upon Pollution Prevention Pays P.O Box 27687, Raleigh, North Carolina 27611-7687 Telephone 919-733-7015 An Equal Opportunity Affirmative Action Employer written request within thirty (30) days following issuance of the final NPDES permit. This request must be in the form of a written petition, conforming to Chapter 150B of the North Carolina General Statutes, and filed with the Office of Administrative Hearings, Post Office Drawer 11666, Raleigh, North Carolina, 27604. Unless such a request is received by this Division, the requirement con- tained in the issued permit shall be final and binding. Sincerely, R. Paul Wilms cc: Dale Overcash Trevor Clements Rex Gleason Central Files JPS Converter And Industrial Corp. R O. Box 2118 Gi-cenville. S.C. 29602 80 3.2.`39-4818 7rCO&I IWO •� 1989 Corporate A/0 31 August 1989 ;A U� Mr. Paul Wilms NC Division of Environmental Management '•r.:r;;; P.O. Box 27687 Raleigh, NC 27611-7687 Re: JPS Automotive Products Group�, �� yj Cramerton Plant NPDES No. NC0006033 Dear Mr. Wilms: As expressed in your transmittal letter for the above referenced permit, I am requsting a waiver or modification to the monitoring requirements. I am enclosing a summary of data for each of the parameters from August 1987 thru July 1989. Specifically I request that analyses for phenols, chromium, sulfides and ammonia - nitrogen be reduced from weekly to monthly. I also request that total nitrogen and total phosphorous analyses be reduced from monthly to quarterly. If the analyses for any of these parameters should show a significant in- crease we would increase the frequency of the analyses. My contention is not to continue to look for low level values when history has shown them not to be a problem. If you have any questions concerning this please let me know. Sincerely, Y Samuel H. Griggs Director Environmental Affairs SHG/mmr Enclosure cc: B.L. Childress ' CRAMERTON EFFLUENT PHENOLS CHROMIUM SULFIDE ' DATE ug/l ug/l mg/l 8/1/IF: 9 11 30 <0.05 7/l1/�9 21 25 <0.05 6/13/89 ::520 <0.05 5/9/89 <5 20 <0.05 4/11/89 3/14/89 14 15 2/14/89 8 5 <0"05 1/10/89 <5 5 12/13/88 <5 15 <0.05 11/15/88 <5 10 <0.05 10/11/88 <5 15 <0.05 9/20/88 6.6 10 <0.05 8/16/88 <5 10 X'0.05 7/19/88 <5 10 <0.05 6/14/88 <5 <5 <0.05 5/24/88 (5 10 <0.05 4/19/88 <5 10 <0.05 3/22/88 30 15 <0.05 2/16/88 <5 15 <0.05 1/19/88 6 15 12/15/87 <5 20 <0.05 11�10/87 <5 30 �0.05 10/13/87 <5 25 <0.05 40 <0.05 8/18/87 <5 35 <0.05 NH3-N mg/l <0.10 <0.10 0.17 0.17 0.36 0.43 0.29 0.33 0.34 0.34 1.17 0.27 0.59 0.43 0.24 C. 0.16 k)c 000\e o33 J?5 5. F. colc rrx. Q o3o8bu -row Cr - !JQ alloro3 Yll us/ Llnt, (EL) � 02tAml %0 Ovp„ l v> F�re n data 5ubb�rxkd h�k_ ma. 2c� _ 0n /y Mon . IX Imo, CoLdd 6L v mofAly 8.91 Ibld = a-2D ujIt IV, i(a lald = /30 Alf 4/0 zj? a ,;OC-S (vCti ✓ YO&) bm,0.-7 I bld = zI u5( p �h5h value of SIP - onit� moo. ma,ilt,.y /Jao aAIS O cox ) = C A�h (al"L t < 50 -161R {5it-6�t{oZ dd-Ehe� CW(P-41 n rfvn. onlu .lyc jMor4h 11+13 A(O 6- n, { th5h value of I. n r �k - Currcylf(y Hon. ovn(y 13,/lffzn6) > I m jd - mm*ly ma•,, fDaj y .(D go$ Cd ) z (S ) State of North Carolina Department of Natural Resources and Community Development Division of Environmental Management 512 North Salisbury Street • Raleigh, North Carolina 27611 James G. Martin, Governor R. Paul Wilms William W. Cobey, Jr., Secretary Director ,7uly 26, l 84. Mr. Samuel H. Griggs Director of Environmental Affairs JPS Converter and Industrial Corp. P.O. Box 208 Greenville, SC 29602 Subject: JPS Automotive Products Corp. Cramerton Plant Draft Permit Limits NPDES No. NC0006033 Gaston County Dear Mr. Griggs: I am writing in response to your letter of July 6 concerning your draft NPDES permit. Your comments are addressed by item as follows: (1) Monitoring Frequency The instream conductivity monitoring requirement will remain in the permit. Conductivity values help the State evaluate the level of pollution instream. The sulfide, phe- nols, chromium, and ammonia monitoring frequencies were det- ermined from standard procedure for pollutants not listed in the monitoring regulations. The company may request the Division of Environmental Management (DEM) to reevaluate the weekly monitoring frequency after one year of data have been submitted. The State will consider changing the monitoring frequency provided the data indicate that low levels of the pollutants exist. The total nitrogen and total phosphorus monitoring requirements are needed per 15.NCAC 2B.0508 which requires facilities in the Catawba River Basin to monitor these nutrients monthly. Your particular receiving stream flows into Lake Wylie which DEM is currently studying for its sen- sitivity to nutrient inputs. Therefore, I will not modify this requirement at this time. P.O. Box 27687, Raleigh, North Carolina 27611-7687 Telephone 919-733-7015 An Equal Opportunity Affirmative Action Employer Priority pollutant analyses must be performed annually per DEM's administrative procedure that is applied to all major NPDES permits. (2) Phenols Limit Per 15 NCAC 2B.0206, the flow used to set limits for parameters which have a water quality standard is the 7Q10. If you have any further questions about the draft permit, please contact Trevor Clements or Dale Overcash of my staff at (919) 733-5083. I hope that the Division's response is satisfactory to the company. However, if this letter does not adequately address your concerns, you have the right to an adjudicatory hearing upon written request within thirty (30) days following receipt of the issued permit. This request must be in the form of a written petition, conforming to Chapter 150B of the North Carolina General Statutes, and filed with the Office of Administrative Hearings, Post Office Drawer 11666, Raleigh, North Carolina 27604. Unless such a request is received by this Division, the requirements contained in the issued permit shall be final and binding. nc rely, R. Paul Wilms cc: Dale Overcash Trevor Clements Mike Parker Central Files (T5 J-L'11� �) JPS Converter And Industrial Corp. P.O. Box 208 Greenville, S.C. 29602 - Corporate A/0 808-2.99-4818 .,. RECEIVED JUL v 1989 PERMITS h �;, :ih'EkifVG 6 July 1989 Mr. Arthur Mouberry NC Division of Environmental Management P.O. Box 27687 Raleigh, NC 27611-7687 Re: JPS Automotive Products Corp. Cramerton Plant NPDES No. NC 0006033 Dear Mr. Mouberry: We have received and reviewed the draft permit for the Cramerton Plant of JPS Automotive Products Corp. Several comments need to be made. 1. I have previously written Ms. Lulu Harris concerning the frequency of sampling (copy attached) and again request that the original sampling frequency be maintained and that conductivity be deleted. The requested changes in the sampling frequencies are: 1 Sulfide to monthly ) Phenols to monthly T. Chromium to monthly r.- NH3-N - doMe,Hc to monthly Total nitrogen to quarterly Total phosphorus to quarterly "Pollutant Analyses" to every three (3) years 2. Request that the concentration limit for phenols be eliminated in that the mass limitations have been calculated on "worst conditions" of 7Q10 flows. With higher flows in the stream the dilution factor is greater and a lessor harm would come to the stream. B Mr. Arthur Mouberry 6 July 1989 Page two AL101989 PEilf�R�r: � r If you have any questions about these reports please let me know. Sincerely, S Samuel H. Griggs Director Environmental Affairs SHG/mmr Attachment cc: Mr. B.L. Childress JPS Converter And Industrial Corp. P.O. Box 208 (;,,,nvi((r. S.C. 29602 803-239-4818 31 May 1989 y 4 Ms. Lulq M. Harris NC Division of Environmental Management P.O. Box 27687 Raleigh, NC 27611 7687 Subject: JPS Automotive Products Corp. Cramerton Plant NPDES No. NC 0006033 Dear Ms. Harris: 1989 I am enclosing the results of the priority pollutant analyses to complete the NPDES application for the Cramerton plant. The frequency of sampling in the draft permit for the Cramerton plant has been changed from the earlier permit and I request that the original sam- pling frequences be maintained. They are: Sulfide Phenols from weekly to monthly (as previous) T-Chromium NH3N Conductivity from daily to weekly Your attention to this request would be appreciated. If you have any questions concerning the analytical results or the sample analyses frequency change, please let me know. Sincerely, 'I 1�( Seamuel H. Griggs Director Environmental Affairs Attachment cc: Mr. B.L. Childress 0 GENERAL ENGINEERING LABORATORIES 198Q Environmental Engineering and Analytical Services, MAY Laboratory Certifications: lolly F.Greene FL E571561S7294 Presidcnt \C 233 George C. Grccrc. P.E. Ph.D. sC 101:0 Vice ilresldcnt VA 1001 j l SCRcgistration No. 9lG= NACIP Approved May 29, 1989T �. Mr. Sam Griggs 1989 JPS PO Box 208' Greenville, SC 29602 Dear Mr. Griggs: Enclosed are the results from the JPS Autoproducts, Cramerton Plant for your requested parameters. Although we were to identify and quantify ten significant peaks using a GC/MS library search, page five of the attached results lists only six compounds. All of the tentatively identified compounds (TIC) reported are less than 10% of the nearest internal standard. Therefore they do not qualify as TIC compounds by CLP requirements. Quantitative analyses cannot be performed due to the trace levels of these compounds which would give values of less than 4 ppb on all six compounds. I am happy to inform you that I am serving as your Project Manager as of today. It is my responsibility to ensure your projects run smoothly and to communicate the status of your project to you. For example, i understand that with this project we did not meet our promised turnaround and tharyou had to call us. Please call me for future projects and pricing. If you have any problems with our services, please talk with me first and I'll be pleased to follow-up on them. I look forward to serving as your Project Manager. Yours very truly, �-G Cherie Pittillo Customer Relations encl jpsg052989 ti P. O. Box 30712 - Charleston. SC 29417 - - - - Phone (803) 556-8171 FAX (803) 766-1178 n I GENERAL ENGINEERING LABORATORIES Environmental Engineering and Analytical Services rccnc Laboratory Certifications: ns: " FL E37156/37294 137294 ,NC 233 233 Grccne, P.E. Ph.D. SC 10120 10120 Acne VA 00151 00151 ::!;::n No. 9103 NACIi' Arproved rroved CERTIFICATE OF ANALYSIS Cl lent: .JPS CONVERTER AND INDUSTRIAL CORP. P.O. BOX 2oe Gate : 0 `5/29/89 .9 GREENV I LLE , SC 296 iC _ Contact: 1 MR. SAM GRIGGS Released by: OC/ .A Oft icer cc/fc: .JPSG/.JPSG 1 Page No.: 1 2 - - - - - - - - - - - - - - - - - - - - - - ------------------------------------ Samp 1 e ID CRAMERTOfJ-�-� EFF . COMP i i .- �� 04/27/89 j+_:�' Lab ID ., 8904149 Sample Type 12:�j:;��.�L. Date Received: o4/28/89 t Parameter -------------------------------------------------------------------------------- Collected by .JPSG CHLORIDES CYANIDE, TOTAL FLUORIDE SULFATE (as SO4) ALUMINUM ANTIMONY BERYLLIUM BARIUM CADMIUM CHROMIUM COPPER LEAD MERCURY NICKEL SELENIUM SILVER ZINC ACID DIGESTION DIGESTION FOR MERCURY ACID COMPOUNDS -14-DIMETHYLPHENOL 4,b-DINITRO-o-CRESOL 2,4-DINITROPHENOL 2-NITROPHENOL 4-NITROPHENOL p-CHLORO-m-CRESOL PENTACHLOROPHENOL PHENOL 214,6-TRICHLOROPHENOL 2-CHLOROPHENOL 2,4-DICHLOROPHENOL 842 ppm 0.01 ppm 0.60 ppir, 63 ppm 0 .28 ppm o .0 2 ppm 0 •()1() ppm <0 .03 ppm :'0.01cj ppm %.'0 •(:)3 ppin 0.21 ppm 0.0)9 ppm ;�i •2 ppb <0.03 ppm :;ry •i?c-ice ppm 0 ,03 ppm �J •��� ppm YES ANALYSIS YES <1(') ppb ppb ::4`, ppb <10 ppb < 10 ppb <10 ppb < 10 ppb < 10 ppb < 10 ppb ::10 ppb 1 i ppb I 2040 Savage Road - Charleston, SC 29414 / P. O. Box 30712 • Charleston, SC 29417 .._. _ _._ . ... nrC (803) =c5-?171 P X IRA?) 766-1 i.7? . fL_� ' GENERAL ENGINEERING LABORATORIES y.� Environmental Engineering and Analytical Services MoII}' F. Greene Laboratory Certifications: President FL E871561,g7294 \ C 233 George C. Greene. P.E., Ph.D. SC 10120 Vice President VA 00151 SC Registration No. 91TZ NAC:P Approved CEn*rIFICATE OF ANALYSIS Cl i ent : •JPS CONVERTER AND INDUSTRIAL CORP. P.O. EllX 208 GREENVILLE SC 29602 Contact: MR. SAM GRIGGS Date : 05/29/89 cc/f c : JF'SG/ .JPSG1 Page No.: 3 -------------------------------------------------------------------------------- Sainp l e ID CRAMERTON EFF . COMP 04/27/89 -Lab ID 89041499 Date Received: -------------------------------------------------------------------------------- 04/28/89 HEXACHLOROBENZENE 10 ppb HEXACHLOROBUTADIENE ::1y ppb HEXACHLOROPENTAD I EIAE 1 C1 ppb HE�,i.HL�]F;uETHHhdE 1tJ ppb I NDENO (1 , 2 , 3-cd) PYRENE <1(:) ppb I SOPHORONE < 10 1 ppb NrIPHTHALENE <10 ppb NITRODENZENE � 1�1 ppb N-NITROSODIMETHYLAriINE 1".1() ppb N-NITROSODIPROPYLAMINE <10 ppb N-NITROSODIPHENYLAMINE %1t1 ppb F'IIENANTHRENE •1 ppb PYRENE <lppb 1 , 2 , 4-TR I CHLOROBEN ZENE <10 ppb & I S (2-CHLOROETHOX Y) METHANE •::1(.) ppb SAMPLE PREP - H/N COMPOUNDS YES PESTICIDES ALDRIN :.10 ppb a-BHC ` 111 pob b-BHC °:10 ppb g-EHC (L I NDANE) c: I ppb d-IHC ::1ppb CHLORDANE l() ppb 4 , 4' -DDT I O ppb 4 , 4' -DDE <10 ppb 414' -DDD •: 1t1 ppb D I ELDR I N < 10 ppb ENDOSULFHAN I <10 ppb ENDOSULFAN II ` 1 i 1 ppb ENDOSULFAN SULFATE '.10 ppb ENDR I N < 10 ppb ENDRIN ALDEHYDE <10 ppb HEPTACHLOR < 1 i � ppb 200 Savage Road • Charleston, SC 29414. / P. O. Box 30712 • Charleston, SC 29417- Pl nnn (Pn %N 171 FA' C (RMN ?.rl,_? 1.72 GENERAL ENGINEERING LABORATORIES '1, c\ r0. Environmental Enbineerinb and AnalvticaI Services . 4olly F. Greene President George C. Grccnc, P.E., Ph.D. Vice President SC Rcgistrttion No. 9103 CERTIFICATE OF ANALYSIS Client: •JPS CONVERTER AND INDUSTRIAL CORP. P.O. BOX 2208 GREENV I LLE , SC ?9bi �2. Contact: MR. SAM GRIGGS cc/fc: •JPSG/•JPSG1 Sample ID CRAMERTON EFF . COMP 04/27/89 - Lab ID 89� �41499 ----------------------------------------------- Gate Received: 04/228/89 HEPTACHLOR EPDXIDE <1t► ppb F'C6—lti16 <1510 ppb PCB-14�1 1510 ppb PCB-12C-' :1=0 ppb PCB-1242 ppb F'CB-12I46 :1 00 ppb PCB-12154 ;150 ppb F'CE�-1?Gt� ::1`0 ppb TOXAPHENE 10 ppb SAMPLE PREP - PESTICIDES YES 4—D ::ltfci ppb �,4,5—TP (SILVEX) ,:1( ppb 1,4 ,C-T ;.10 ppb SAMPLE PREP - HERBICIDES YES Laboratory Certifications: FL E37156/87294 NC 233 SC 10120 VA 00151 \,1C:11' Arprovedi Date: 1)51/ 29/89 Page No.: 4 ------------------------------- 2040 Savage Road • Charleston, SC 29414 / P. O. Box 30712 • Charleston. SC 29417 _ - _n�:r;:c (Qnz� rc�-4171 .•_.F.AX {$Q3.� 755-1173.._.�..__�.._ _.......__ • _....---- ..__ ..: ___ .__.._.....' -.. -- : . i GENERAL ENGINEERING LABORATORIES ;/ y® Environmental Engineering and Analytical Services Greene Laboratory Certifications: �1o11y F. Nf ollyPresidF. FL E37156i8729.3 NC '_'33 George C. Greene, P.E., Ph.D. SC 101:0 Vice President VA C0151 SC Registration No. 9103 N,\C;P Approved CERTIFICATE OF ANALYSIS CLIENT: JPS CONVERTER AND INDUSTRIAL CORP. DATE: 05/26/89 P. O. BOX 208 GREENVILLE, SC 29602 CONTACT: MR. SAM GRIGGS CC/FC: JPSG/JPSG1 PAGE NO.: 5 SAMPLE I.D.& LOCATION: CRAMERTON EFF. COMP DATE & TIME SAMPLED: 04/27/89 LAB l.D.: 89041499 DATE RECEIVED: 04/28/89 The following compounds were selected from a search of the NBS library of 45,000 compounds as those with the b&g fit when matched against unidentified chromatographic peaks from the GC/MS analyses of the Cramerton Eff. Comp. sample. PARAMETER 1,3-DIOXOLANE, 2-CYCLOHEXYL-4,5-DIMETHYL- CYCLOPENTASILOXANE, DECAMETHYL- 1 H-IM I DAZOLE, 1-(1-OXOPENTYL)- BENZENE, 1,4-BIS(1-METHYLETHYL)- 1 H-BENZOTRIAZOLE, 1-ETHENYL- NAPHTHALENE, 1,1'-(1,2-ETHANEDIYL) BIS- CAN Bi 372 791 769 878 1065 902 1933 859 2047 822 2261 775 _. 2040 Savage Road - Charleston, SC 29414 P. O: Box 30712 Charleston, SC 29417 I GENERAL ENGINEERING LABORATORIES Environmental Engineering and :analytical Services ..jolly R Greene Laboratory Certifications: Presidcnt rL E371 56; 37294 \C 233 George C. Greene, P.E., l'h.D. SC 101=0 Vice President VA GOi- 1 SC Registr Lion No. 910 5 3 NACTIP CERTIFICATE OF AtiALYSIS Client: -JPS CONVERTER AND INDUSTRIAL CORP. P.O. BOX 208 Date: 05/" /on9 GREENV I LLE SC 1296i i2 Contact: MR. SAM GRIGGS Released by: OC/OA OTficcr cc/fc: •JPSG/.JPSG 1 Page No.: 1 Sample ID CRAMERTON TRIP EFF . GRAB BLANK 04/27/89 .. Lab 10 89t i41 Sc it.i 8904150 1 Sample Type 12 12 Date Received: 04/28/89 04/.28/89 Parameter Collected by ----------------------------------------------------------------- .JPSG -JPSG PHENOLS, TOTAL 14 ppb VOLATILE COMPOUNDS ACROLEIN <20 ppb <;20 ppb ACRYLONITRILE <20 ppb ppb BENZENE <2 ppb <2 ppb EIS—CHLOROMETHYL ETHER <2 ppb <2 ppb BROMOFORM <2 ppb <2 ppb CARBON TETRACHLORIDE 2' ppb <:2 ppb CHLOROBENZENE <2 ppb <2 ppb CHLORODIBROMOMETHANE '.2 ppb <2 ppb CHLOROETHANE <..? ppb ppb 2—CHLOROETHYLVINYL ETHER <2 ppb %2 ppb CHLOROFORM 6 ppb ppb DICHLOROBROMOMETHANE 2 ppb <2 ppb DICHLORODIFLUOROMETHANE <2 ppb ,n ppb 111—DICHLOROETHANE <2 ppb •<2 ppb 112—DICHLOROETHANE ppb <2 ppb 171—DICHLOROETHYLENE <2 ppb <2 ppb 112—DICHLOROF-ROPANE :2 ppb <2 ppb • •= 1 ,2—D-'r7" nf.-; �-.-r. YLENE ., �.:. ppb 2 �.� ppb ETHYLBENZENE ,-'2 ppb :.2 ppb METHYL BROMIDE ppb <2 ppb METHYL CHLGRIDE <2 ppb <2 ppb METHYLENE CHLORIDE <:2 ppb 2 ppb 1 ,1 ,2,2—TETRACHLOROETHANE? ppb <2 ppb TETRACHLOROETHYLENE <2 ppb ;2 ppb TOLUENE <? ppb <2 ppb 112—TRANS—DICHLOROETHYLENE <;2 ppb <2 ppb 11111—TRICHLOROETHANE <:2 ppb <2 ppb 1 ,1 ,2—TRICHLOROETHANE <:2 ppb <;2 ppb TRICHLOROETHYLENE <2 ppb :; ppb 204.0 Savage Road • Charleston, SC 29414 / P. O. Box 30712 • Charleston, SC 29417 nl.wic (Qn2) 556-1172 F.4s: (803) 766-1173 t GENERAL ENGINEERING ]LABORATORIES rl��w Environmental Engineering and :analytical Services ,dolly F. Greene President Gcor,c C. Greene, P.E., Ph. D. Vice President SC RC-,1Str3[lon No. 9103 CE?ETIFICA T OF . NAL i SIS Laboratory Certifications: FL E871 156iS 7 294 INC 233 SC 10120 VA 001C1 NAC1 ' arrrc%*t!d Client: JPS CONVERTER AND INDUSTRIAL CORP. P.O. BOX 'M. Date: 05/29/89 GREENVILLE SC �9662 Contact: MR. SAM GRIGGS cc/'fc: •JF'SG/.JF'SG 1 Page No.: 2 -------------------------------------------------------------------------------- Samp l e ID CRAMERTON TRIP EFF , GRAB BLANK: 04/?7/89 - Lab ID : 890415� 0 89041501 Date Received: 04/'?8/89 04/'28/89 -------------------------------------------------------------------------------- TRICHLOROFLUOROMETHANE <22 ppb `42 ppb VINYL CHLORIDE <;? ppb ppb _2040 Savage Road_ Charleston, SC 29414 / P. O., Box 30712 Charleston, SC 29417 —• ---- •-•— ----. __... _ _..._. �'�...:;C`n{j^.1 <��_41^t r,_�v �o{1'tl ^G(.; !'1� - - _. -