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HomeMy WebLinkAboutWQ0004972_Monitoring - 12-2023_20240130Monitoring Report Submittal Permit Number#* Name of Facility:* Month: * December Report Information WQ0004972 Forest Lake RV WWTP Type * NDMR, NDAR-1, NDAR-2, NDMLR Confirmation Email Address: * Name of Submitter: * Signature: Date of submittal: Initial Review Year:* 2023 Upload Document* 2023_December_Monthly_Report_WQ004972 1.55M B complete.pdf PDF Only Please upload one PDF containing all applicable monitoring reports (i.e., NDMR, NDAR-1, NDAR-2, NDMLR, GW-59). agrenier@greenerehssolutions.com Amanda Grenier ollow ada e*Aw t 1 /30/2024 This will be filled in automatically Reviewer: Wanda.Gerald Is the project number correct?* W00004972 Is the monitoring report accepted?* Yes NO Regional Office* Winston-Salem Reviewer: _anonymous Review Date: 2/26/2024 DocuSign Envelope ID: 84-7C2B-4F01-AFB9-9D154DCFD7B2 I Uo-IniON-DISCHARGE APPLICATION REPORT (NDAR-1) Page of Permit No.: Q11149 • - D. December irrigation • occur at this facility? . .. . ..Cover Crop:. .. NO 1Hourly Rate (in): Hourly Rate (in):, Hourly Rate (in): Annual Rate (in):.:Annual Rate (in): Annual Rate (in): Annual Rate (in): Field Irrigated? Field Irrigated? Field Irrigated? Field Irrigated? in Monthly Loading:12 Month Floating Total (in): DocuSign Envelope ID: 84-7C2B-4F01-AFB9-9D154DCFD7B2 I uo-IniON-DISCHARGE APPLICATION REPORT (NDAR-1) Page of DocuSign Envelope ID: FOAF6A84-7C2B-4F01-AFB9-9D154DCFD7B2 Did the application rates exceed the limits in Attachment B of your permit? O Compliant ❑ Non -Compliant Were adequate measures taken to prevent effluent ponding in or runoff from the sites? O Compliant ❑ Non -Compliant Was a suitable vegetative cover maintained on all sites as specified in your permit? O Compliant ❑ Non -Compliant Were all setbacks listed in your permit maintained for every application to each permitted site? O Compliant ❑ Non -Compliant Were all freeboards maintained in accordance with the specified freeboard heights in your permit? ❑ Compliant O Non -Compliant If the facility is non -compliant, please explain in the space below the reason(s) the facility was not in compliance. Provide in your explanation the date(s) of the non-compliance and describe the corrective action(s) taken. Attach additional sheets if necessary. Freeboard was 1.5 ft on 12/28/2023 and 1.2 ft on 12/29/23 due to high flows and rainfall. The permit owner was notified and irrigation was done once the fields dried out to bring the freeboard back to above 2 ft. Operator in Responsible Charge (ORC) Certification Permittee Certification ORC: Sam Perry Permittee: MHC TT, LP Certification No.: 1014038 Signing Official: George Gudgeon Grade: SI Phone Number: 919-548-2381 Signing Officials Title: Sr. Vice President Has the ORC changed since the previous NDAR-1? ❑ Yes 0 No Phone Number: 312-279-1400 Permit Exp.: 10/31/27 1/30/2024r�t. CAJepv, 1/30/2024 1 2 Signature Date Signature Date By this signature, I certify that this report is accurrate and complete to the best of my knowledge. I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that all qualified personnel properly gathered and evaluated the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations. Mail Original and Two Copies to: Division of Water Resources Information Processing Unit 1617 Mail Service Center Raleigh, North Carolina 27699-1617 M DocuSign Envelope ID: FOAF6A84-7C2B-4F01-AFB9-9D154DCFD7B2 Permit No.: WQ0004972 Facility Name: Forest Lake Preserve ELS County: Davie Month: December Year: 2023 PPI: 001 Flow Measuring Point: ❑ Influent 0 Effluent El No flow generated Parameter Monitoring Point: Influent O Effluent El Groundwater Lowering El Surface Water Parameter Code - 0 50050 00400 50060 70300 00530 00310 31616 00600 00610 00625 00630 00620 00615 00665 00940 Q V6 ~m ~OO E a 0 LLCL h U y Z a 2 Lnn f a cc a c N <n p CO _ LL U Z 0 E Q t ° aa Y Z o F- R _ Z m ° �Oac NVl sO a ULd 24-hr hrs GPD su mg/L mg/L mg/L mg/L #/100 mL mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L 1 08:00 5 21,564 6.2 1.8 2 28,771 3 23,778 4 07:00 5 33,248 6.45 1.6 5 08:00 5 18,226 6.21 0.6 6 08:00 5 30,746 6.43 0.5 7 08:00 5 26,357 6.11 0.6 8 08:00 5 22,680 6.14 1.2 9 17,507 10 25,638 11 08:00 5 70,243 6.25 0.6 12 08:00 5 31,603 6.16 1.9 13 08:00 5 25,991 6.18 1.2 14 08:00 5 27,930 6.15 1.4 15 08:00 5 28,971 6.05 0.2 16 23,337 17 28,888 18 08:00 5 59,442 6.27 0.2 19 08:00 5 6,539 6.34 1.4 20 08:00 5 25,562 6.11 0.3 21 08:00 5 31,564 6.26 1.8 269 115 23.5 10 52.8 14 24.4 28.4 7.3 22 08:00 5 23,805 6.24 2.1 23 23,718 24 17,384 25 Holiday 31,070 Holiday 26 Holiday 23,011 Holiday 27 Holiday 76,019 Holiday 28 08:00 5 50,521 6.69 1.6 29 08:00 5 29,570 6.35 1.4 30 25,239 31 31,370 Average: 30,332 1.13 269.00 115.00 23.50 10.00 52.80 14.00 24.40 28.40 7.30 Daily Maximum: 76,019 6.69 2.10 269.00 115.00 23.50 10.00 52.80 14.00 24.40 28.40 7.30 Daily Minimum: 6,539 6.05 0.20 269.00 115.00 23.50 10.00 52.80 14.00 24.40 28.40 7.30 Sampling Type: Monthly Avg. Limit: Daily Limit: Sample Frequency: Continuous 5x/Week 5X/Week Monthly Monthly Monthly Monthly Monthly Monthly Monthly Monthly Monthly Monthly Monthly 3X/year DocuSign Envelope ID: FOAF6A84-7C2B-4F01-AFB9-9D154DCFD7B2 Sampling Person(s) Certified Laboratories Name: Amanda Grenier Name: Sam Perry Name: Greener EHS Solutions, LLC Name: Pace Analytical Does all monitoring data and sampling frequencies meet the requirements in Attachment A of your permit? ❑ Compliant El Non -Compliant If the facility is non -compliant, please explain in the space below the reason(s) the facility was not in compliance. Provide in your explanation the date(s) of the non-compliance and describe the corrective action(s) taken. Attach additional sheets if necessary. The Monthly average flow exceeded the permitted flow of 24,400 gpd. The permitted application rate was not exceeded. The flow meter was calibrated on June 27, 2023 and the meter was reading significantly low before the calibration. This was noted on the June 2023 NDMR. The plant is in the process of an upgrade to increase the capacity as well as investigating extraneous flow for 1/1 and leaking fixtures. Lab Qualifiers, December 21 , 2023 - Phosphorus, TKN, and Ammonia, M1 - Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.TSS, D6 - The precision between the sample and sample duplicate exceeded laboratory control limits. Operator in Responsible Charge (ORC) Certification Permittee Certification ORC: Sam Perry Permittee: MHC TT, LP Certification No.: 1014038 Signing Official: George Gudgeon Grade: SI Phone Number: 919-548-2381 Signing Officials Title: Sr. Vice President Has the ORC changed since the previous NDMR? ❑ Yes El No Phone Number: 312-279-1400 Permit Expiration: 10/31/2027 fir' t. �w 4 1/30/2024 1/30/2024 Signature Date Signature Date By this signature, I certify that this report is accurrate and complete to the best of my knowledge. I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that all qualified personnel properly gathered and evaluated the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations. Mail Original and Two Copies to: Division of Water Resources Information Processing Unit 1617 Mail Service Center Raleigh, North Carolina 27699-1617 DocuSign Envelope ID: FOAF6A84-7C2B-4F01-AFB9-9D154DCFD7B2 aceo Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 January 09, 2024 Amanda D. Grenier Greener EHS Solutions 21 Selby Ct. Holly Springs, NC 27540 RE: Project: FOREST LAKE -MONTHLY Pace Project No.: 92705282 Dear Amanda Grenier: Enclosed are the analytical results for sample(s) received by the laboratory on December 21, 2023. The results relate only to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report. The test results provided in this final report were generated by each of the following laboratories within the Pace Network: • Pace Analytical Services - Asheville • Pace Analytical Services - Charlotte If you have any questions concerning this report, please feel free to contact me. Sincerely, Matthew Brainard matthew.brainard@pacelabs.com 704-977-0942 Project Manager Enclosures REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 of 17 DocuSign Envelope ID: FOAF6A84-7C2B-4F01-AFB9-9D154DCFD7B2 aceo Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: FOREST LAKE -MONTHLY Pace Project No.: 92705282 Pace Analytical Services Charlotte South Carolina Laboratory ID: 99006 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 North Carolina Drinking Water Certification #: 37706 North Carolina Field Services Certification #: 5342 North Carolina Wastewater Certification #: 12 South Carolina Laboratory ID: 99006 Pace Analytical Services Asheville 2225 Riverside Drive, Asheville, NC 28804 Florida/NELAP Certification #: E87648 North Carolina Drinking Water Certification #: 37712 North Carolina Wastewater Certification #: 40 CERTIFICATIONS South Carolina Certification #: 99006001 South Carolina Drinking Water Cert. #: 99006003 Florida/NELAP Certification #: E87627 Kentucky UST Certification #: 84 Louisiana DoH Drinking Water #: LA029 VirginiaNELAP Certification #: 460221 South Carolina Laboratory ID: 99030 South Carolina Certification #: 99030001 VirginiaNELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 2 of 17 DocuSign Envelope ID: FOAF6A84-7C2B-4F01-AFB9-9D154DCFD7B2 Pace Analytical Services, LLC �aceo 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 SAMPLE ANALYTE COUNT Project: FOREST LAKE -MONTHLY Pace Project No.: 92705282 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92705282001 EFFLUENT GRAB SM 9222D-2015 KDF 1 PASI-C SM 2540C-2015 JAY 1 PASI-A SM 2540D-2015 JAY 1 PASI-A SM 521OB-2016 KO 1 PASI-A TKN+NO3+NO2 Calculation KDF1 1 PASI-A EPA 350.1 Rev 2.0 1993 NCF 1 PASI-A EPA 351.2 Rev 2.0 1993 MFO 1 PASI-A EPA 353.2 Rev 2.0 1993 NCF 1 PASI-A EPA 365.1 Rev 2.0 1993 Zip 1 PASI-A PASI-A = Pace Analytical Services - Asheville PASI-C = Pace Analytical Services - Charlotte REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 3 of 17 DocuSign Envelope ID: FOAF6A84-7C2B-4F01-AFB9-9D154DCFD7B2 aceo Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: FOREST LAKE -MONTHLY Pace Project No.: 92705282 Sample: EFFLUENT GRAB Lab ID: 92705282001 Collected: 12/21/23 12:35 Received: 12/21/23 14:55 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual MBIO 9222D Fecal Coliform CHT Analytical Method: SM 9222D-2015 Preparation Method: SM 9222D-2015 Pace Analytical Services - Charlotte Fecal Coliforms 10.0 CFU/100 mL 1.0 1 12/21/23 15:57 12/22/23 14:08 2540C Total Dissolved Solids Analytical Method: SM 2540C-2015 Pace Analytical Services -Asheville Total Dissolved Solids 269 mg/L 25.0 1 12/22/23 10:38 2540D Total Suspended Solids Analytical Method: SM 2540D-2015 Pace Analytical Services -Asheville Total Suspended Solids 115 mg/L 31.2 1 12/27/23 12:08 5210B BOD, 5 day Analytical Method: SM 521OB-2016 Pace Analytical Services -Asheville BOD, 5 day 23.5 mg/L 2.0 1 12/22/23 14:37 12/27/23 11:40 Total Nitrogen Calculation Analytical Method: TKN+NO3+NO2 Calculation Pace Analytical Services -Asheville Total Nitrogen 52.8 mg/L 0.040 1 01/09/24 08:20 350.1 Ammonia Analytical Method: EPA 350.1 Rev 2.0 1993 Pace Analytical Services -Asheville Nitrogen, Ammonia 14.0 mg/L 0.50 5 01/06/24 06:19 7664-41-7 351.2 Total Kjeldahl Nitrogen Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993 Pace Analytical Services -Asheville Nitrogen, Kjeldahl, Total 24.4 mg/L 2.5 5 01/08/24 14:51 01/09/24 05:25 7727-37-9 353.2 Nitrogen, NO2/NO3 unpres Analytical Method: EPA 353.2 Rev 2.0 1993 Pace Analytical Services -Asheville Nitrogen, Nitrate 28.4 mg/L 0.40 10 12/21/23 23:29 14797-55-8 365.1 Phosphorus, Total Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation Method: EPA 365.1 Rev 2.0 1993 Pace Analytical Services -Asheville Phosphorus 7.3 mg/L 0.15 3 01/05/2413:40 01/08/2411:01 7723-14-0 Date: 01/09/2024 08:22 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 4 of 17 DocuSign Envelope ID: FOAF6A84-7C2B-4F01-AFB9-9D154DCFD7B2 Pace Analytical Services, LLC �aceo 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: FOREST LAKE -MONTHLY Pace Project No.: 92705282 QC Batch: 821311 Analysis Method: SM 9222D-2015 QC Batch Method: SM 9222D-2015 Analysis Description: 9222D Fecal Coliform(MF) - CHT Laboratory: Pace Analytical Services - Charlotte Associated Lab Samples: 92705282001 METHOD BLANK: 4250844 Matrix: Water Associated Lab Samples: 92705282001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Fecal Coliforms CFU/100 mL ND 1.0 12/22/23 14:08 SAMPLE DUPLICATE: 4250845 Parameter Fecal Coliforms 92705282001 Dup Units Result Result RPD Qualifiers CFU/100 mL 10.0 ND Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01 /09/2024 08:22 AM without the written consent of Pace Analytical Services, LLC. Page 5 of 17 DocuSign Envelope ID: FOAF6A84-7C2B-4F01-AFB9-9D154DCFD7B2 Pace Analytical Services, LLC �aceo 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: FOREST LAKE -MONTHLY Pace Project No.: 92705282 QC Batch: 821398 Analysis Method: SM 2540C-2015 QC Batch Method: SM 2540C-2015 Analysis Description: 2540C Total Dissolved Solids Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92705282001 METHOD BLANK: 4251194 Associated Lab Samples: 92705282001 Parameter Units Total Dissolved Solids mg/L LABORATORY CONTROL SAMPLE: 4251195 Parameter Units Total Dissolved Solids mg/L SAMPLE DUPLICATE: 4251341 Parameter Units Total Dissolved Solids mg/L Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 25.0 12/22/23 10:36 Spike LCS LCS % Rec Conc. Result % Rec Limits Qualifiers 250 262 105 90-110 92705156001 Dup Result Result RPD Qualifiers 61.0 56.0 9 SAMPLE DUPLICATE: 4251342 92705282001 Dup Parameter Units Result Result Total Dissolved Solids mg/L 269 269 RPD Qualifiers 0 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01 /09/2024 08:22 AM without the written consent of Pace Analytical Services, LLC. Page 6 of 17 DocuSign Envelope ID: FOAF6A84-7C2B-4F01-AFB9-9D154DCFD7B2 Pace Analytical Services, LLC �aceo 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: FOREST LAKE -MONTHLY Pace Project No.: 92705282 QC Batch: 821952 Analysis Method: SM 2540D-2015 QC Batch Method: SM 2540D-2015 Analysis Description: 2540D Total Suspended Solids Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92705282001 METHOD BLANK: 4253573 Associated Lab Samples: 92705282001 Parameter Units Total Suspended Solids mg/L LABORATORY CONTROL SAMPLE: 4253574 Parameter Units Total Suspended Solids mg/L SAMPLE DUPLICATE: 4253691 Parameter Units Total Suspended Solids mg/L Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 2.5 12/27/23 11:55 Spike LCS LCS % Rec Conc. Result % Rec Limits Qualifiers 250 226 90 90-110 92705218003 Dup Result Result RPD Qualifiers 2960 2980 1 SAMPLE DUPLICATE: 4253692 92705227001 Dup Parameter Units Result Result Total Suspended Solids mg/L 1050 585 RPD Qualifiers 57 D6 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01 /09/2024 08:22 AM without the written consent of Pace Analytical Services, LLC. Page 7 of 17 DocuSign Envelope ID: FOAF6A84-7C2B-4F01-AFB9-9D154DCFD7B2 Pace Analytical Services, LLC �aceo 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: FOREST LAKE -MONTHLY Pace Project No.: 92705282 QC Batch: 821467 Analysis Method: SM 521 OB-2016 QC Batch Method: SM 521OB-2016 Analysis Description: 5210E BOD, 5 day Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92705282001 METHOD BLANK: 4251449 Associated Lab Samples: 92705282001 Parameter Units BOD, 5 day mg/L LABORATORY CONTROL SAMPLE: 4251451 Parameter Units BOD, 5 day mg/L Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 2.0 12/27/23 11:09 Spike LCS LCS % Rec Conc. Result % Rec Limits Qualifiers 198 210 106 84.6-115 SAMPLE DUPLICATE: 4251452 92705305002 Dup Parameter Units Result Result BOD, 5 day mg/L ND ND RPD Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01 /09/2024 08:22 AM without the written consent of Pace Analytical Services, LLC. Page 8 of 17 DocuSign Envelope ID: FOAF6A84-7C2B-4F01-AFB9-9D154DCFD7B2 Pace Analytical Services, LLC �aceo 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: FOREST LAKE -MONTHLY Pace Project No.: 92705282 QC Batch: 823864 Analysis Method: EPA 350.1 Rev 2.0 1993 QC Batch Method: EPA 350.1 Rev 2.0 1993 Analysis Description: 350.1 Ammonia Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92705282001 METHOD BLANK: 4262034 Associated Lab Samples: 92705282001 Parameter Units Nitrogen, Ammonia mg/L LABORATORY CONTROL SAMPLE: 4262035 Parameter Units Nitrogen, Ammonia mg/L Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 0.10 01 /06/24 04:12 Spike LCS LCS % Rec Conc. Result % Rec Limits Qualifiers 5 4.9 98 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4262036 4262037 MS MSD 92706635001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, Ammonia mg/L 38.5 5 5 43.0 43.4 89 97 90-110 1 M1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4262038 4262039 MS MSD 92706635002 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, Ammonia mg/L 27.2 5 5 31.8 31.9 92 94 90-110 0 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01 /09/2024 08:22 AM without the written consent of Pace Analytical Services, LLC. Page 9 of 17 DocuSign Envelope ID: FOAF6A84-7C2B-4F01-AFB9-9D154DCFD7B2 Pace Analytical Services, LLC �aceo 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: FOREST LAKE -MONTHLY Pace Project No.: 92705282 QC Batch: 824033 Analysis Method: EPA 351.2 Rev 2.0 1993 QC Batch Method: EPA 351.2 Rev 2.0 1993 Analysis Description: 351.2 TKN Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92705282001 METHOD BLANK: 4262523 Associated Lab Samples: 92705282001 Parameter Units Nitrogen, Kjeldahl, Total mg/L LABORATORY CONTROL SAMPLE: 4262524 Parameter Units Nitrogen, Kjeldahl, Total mg/L Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 0.50 01 /09/24 03:54 Spike LCS LCS % Rec Conc. Result % Rec Limits Qualifiers 10 9.5 95 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4262525 4262526 MS MSD 92705349001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, Kjeldahl, Total mg/L 24.3 10 10 36.4 34.2 121 99 90-110 6 M1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4262527 4262528 MS MSD 92705351001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, Kjeldahl, Total mg/L 2.5 10 10 12.9 13.2 104 108 90-110 3 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01 /09/2024 08:22 AM without the written consent of Pace Analytical Services, LLC. Page 10 of 17 DocuSign Envelope ID: FOAF6A84-7C2B-4F01-AFB9-9D154DCFD7B2 Pace Analytical Services, LLC �aceo 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: FOREST LAKE -MONTHLY Pace Project No.: 92705282 QC Batch: 821342 Analysis Method: EPA 353.2 Rev 2.0 1993 QC Batch Method: EPA 353.2 Rev 2.0 1993 Analysis Description: 353.2 Nitrate + Nitrite, Unpres. Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92705282001 METHOD BLANK: 4251049 Associated Lab Samples: 92705282001 Parameter Units Nitrogen, Nitrate mg/L LABORATORY CONTROL SAMPLE: 4251050 Parameter Units Nitrogen, Nitrate mg/L Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 0.040 12/21 /23 23:04 Spike LCS LCS % Rec Conc. Result % Rec Limits Qualifiers 1.5 1.5 98 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4251051 4251052 MS MSD 92705238001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, Nitrate mg/L 23.7 1.5 1.5 25.6 26.3 124 175 90-110 3 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01 /09/2024 08:22 AM without the written consent of Pace Analytical Services, LLC. Page 11 of 17 DocuSign Envelope ID: FOAF6A84-7C2B-4F01-AFB9-9D154DCFD7B2 Pace Analytical Services, LLC �aceo 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: FOREST LAKE -MONTHLY Pace Project No.: 92705282 QC Batch: 823702 Analysis Method: EPA 365.1 Rev 2.0 1993 QC Batch Method: EPA 365.1 Rev 2.0 1993 Analysis Description: 365.1 Phosphorus, Total Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92705282001 METHOD BLANK: 4260934 Associated Lab Samples: 92705282001 Parameter Units Phosphorus mg/L LABORATORY CONTROL SAMPLE: 4260935 Parameter Units Phosphorus mg/L Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 0.050 01 /08/24 10:40 Spike LCS LCS % Rec Conc. Result % Rec Limits Qualifiers 2.5 2.6 103 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4260936 4260937 MS MSD 92704967001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Phosphorus mg/L 7.8 2.5 2.5 10.3 10.3 98 99 90-110 0 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4260938 4260939 MS MSD 92705130001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Phosphorus mg/L 6.7 2.5 2.5 8.3 8.8 65 83 90-110 5 M1 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01 /09/2024 08:22 AM without the written consent of Pace Analytical Services, LLC. Page 12 of 17 DocuSign Envelope ID: FOAF6A84-7C2B-4F01-AFB9-9D154DCFD7B2 aceo Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALIFIERS Project: FOREST LAKE -MONTHLY Pace Project No.: 92705282 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as "Total" may vary slightly from the sum of the reported component parameters. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TN -The NELAC Institute. ANALYTE QUALIFIERS D6 The precision between the sample and sample duplicate exceeded laboratory control limits. M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01 /09/2024 08:22 AM without the written consent of Pace Analytical Services, LLC. Page 13 of 17 DocuSign Envelope ID: FOAF6A84-7C2B-4F01-AFB9-9D154DCFD7B2 aceo Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: Pace Project No.: FOREST LAKE -MONTHLY 92705282 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92705282001 EFFLUENT GRAB SM 9222D-2015 821311 SM 9222D-2015 821312 92705282001 EFFLUENT GRAB SM 254OC-2015 821398 92705282001 EFFLUENT GRAB SM 2540D-2015 821952 92705282001 EFFLUENT GRAB SM 521 OB-2016 821467 SM 521 OB-2016 821563 92705282001 EFFLUENT GRAB TKN+NO3+NO2 824212 Calculation 92705282001 EFFLUENT GRAB EPA 350.1 Rev 2.0 1993 823864 92705282001 EFFLUENT GRAB EPA 351.2 Rev 2.0 1993 824033 EPA 351.2 Rev 2.0 1993 824187 92705282001 EFFLUENT GRAB EPA 353.2 Rev 2.0 1993 821342 92705282001 EFFLUENT GRAB EPA 365.1 Rev 2.0 1993 823702 EPA 365.1 Rev 2.0 1993 823767 Date: 01/09/2024 08:22 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 14 of 17 �J I DG#_Title: ENV-PRIM-HUN1-UU83 vU3_5ample Condition Upon Kecelpt DocuSign Envelope ID: FOAF6A84-7C2B-4F01-AFB9-9D154DCFD7B2 NvvI Effective Date: 11/29/2023 4:16:30 PM Laboratory receiving samples: Asheville ❑ Eden❑ Greenwood ❑ Huntersville Raleigh❑ Mechanicsville❑ Atlanta) —I kor..o-�••;�I^n ConditionSample Client LC NamWO#:92705282 Upon Receipt U-\e'�A� ������(�S Project #: Courier. LJ Fed Ex Li UPS U USPS Client III II' II III II I IIIII III ❑ Commercial DPace ❑ Other: 92705282 I Custody Seal Present? ❑Yes '23No Seals Intact? ❑Yes [SNo ❑N/A 1 Date/Initials Person Examining Contents: Packing Material: Bubble Wrap ❑ Bubble Bags ❑ None ❑ Other Biologi 1 Tissue Frozen? Thermometer: ( ❑Yes KNo ❑N/A ❑ IR Gun ID: ' ZIvo Type of Ice: [ .Net ❑Blue ❑None Correction Factor: Cooler Temp: �O Add/Subtract (°C) —� ,� Temp should be above freezing to 6°C ❑ Samples out of temp criteria. Samples on ice, cooling process Cooler Temp Corrected (°C): �� has begun USDA Regulated Soil ( 09 N/A, water sample) Did samples originate in a quarantine zone within the United States: CA, NY, or SC Did samples originate from a foreign source (internationally, Irhrrk man%1?F— YPc Fa No includine Hawaii and Puerto Ricol? ❑Yes �iINo Comments/Discrepancy: Chain of Custody Present? 'SYes ❑ No 3 N/A 1. Samples Arrived within Hold Time? 13Yes ❑ No ❑ N/A 2. Short Hold Time Analysis (<72 hr.)? Yes ❑ No ❑ N/A 3. Rush Turn Around Time Requested? ❑ Yes Q)No ❑ N/A 4. Sufficient Volume? I&Yes ❑ No ❑ N/A 5. Correct Containers Used? -Pace Containers Used? 0Yes Yes ❑No ❑ No ❑N/A ❑ N/A 6. Containers Intact? B-Nes ❑ No ❑ N/A 7. Dissolved analysis: Samples Field Filtered? ❑Yes [I No /A 8. Sample Labels Match COC? -Includes Date/-rime/ID/Analysis Matrix: `'F3Yes W ❑No [I N/A 9. Headspace in VOA Vials (>5-6mm)? ❑ Yes ❑ No N/A 10. Trip Blank Present? Trip Blank Custody Seals Present? ❑Yes ❑ Yes El No ❑ No TN/A /A 11. COMMENTS/SAMPLE DISCREPANCY CLIENT NOTIFICATION/RESOLUTION Person contacted: Project Manager SCURF Review: Project Manager SRF Review: Lot ID of split containers: Date/Time: Date: Date: Field Data Required? U Yes U No Qualtrax ID: 69614 Paae 1 of 2 Page 15 of 17 DocuSign Envelope ID: FOAF6A84-7C2B-4F01-AFB9-9D154DCFD7B2 I I `Check mark top half of box if pH and/or dechlorination is verified and within the acceptance range for preservation samples. Exceptions: VOA, Coliform, TOC, Oil and Grease, DRO/8015 (water) DOC. LLHg "Bottom half of box is to list number of bottles • "Check all unpreserved Nitrates for chlorine Prniact9 WO# : 92705282 PM: MWB Due Date: 01/09/24 CLIENT: 92—Greener Z u W Z v V 1 Z v 0 a 1' u _ v a O v C O *a r7 u iu � ` I ! v �_ Z V Z W v G v — Z v Z 2 J -_ r r7 Z 12 r ZVVvim. � Z Z Z n � ' y Z v ii 7 a. a O o c 0. E C N E O 2 a E ¢ Z N E O Z�� 7 E 10 v C D ? V D E C O O E .O Q E ,, N x C E S 17 Z D E ? i,J Q O > £ O N m q O c 6 c C O > E O m C O > E = 7 x > q a m y a yr `° S a ry Z = aJr E Q o A -E O E E .NiN as a m V1 a m ,`a, eiN 7 a m In a m Z a m N s m r0 a m W 3 :: (-NVI t.7 ¢ °: = r7 a p a! 7 N .i t7 t? a a Vf rn t0 a E O M l9 o OO = Cr L9 o !- � t7 > 7 M > O >jrn M o E O a x E a > In [-E Nej a m ID Q E vvii�m > E n � `\ 2 N\N 3 5 I \ N 1: \\- _VN6 � N\NN \ I \j E Nv i - - -\ N I I I Nj I 10 11 t� \\ Nil `.-_I L\ I \ _ NN .. - 5ample ID I Type of Preservative pH Adjustment Log for Preserved Samples eceipt Date preservation adjusted Time preservalicn Amount of Preservative Lot p adjusted I added T — Note whenever there Is a discrepancy affecting ?forth Carolina consoliance samples, a copy of this form will be sent to the North Carolina DENR Certification Office (i e. Out of hold, incorrect preservative, out of temp, incorrect containers. Qualtrax ID 69,314 Page 2 of 2 Page 16 of 17 Doc uSic S' d a O n n 0 a a m z 5 3 O A 0 0 I� to o N W O n Envelope ID: FOAF6A84-7C2B-4F01-AFB9-9D154DCFD7B2 " o I 'o w O o -+ n p o A n 3 n 3 n 3 3 3. = n M - _ .. 0 3 oCb n N v .�. g x D v n o g a 2 f < < _ F a G1 °c $ n ti C • • r F o a 5 - c goo v o v v \ v o _ o_ _ m 3 3 3 3 c � = _ a >v m m = D m m D �p O —_ = .. 9p S z 1 3 0 - ° m w "- o a c • O C — e g 71 c N n D n S 1Cn 4 ° - > v D 0 7 A R _ 2 n ° ° °fu s z O i o n 3 n 3 3 3 3 71 o o o Ol _ _ n 3 0 ii a z ` _ " 3 m S I Ammonia/ T. Phos r a �a BOD 5-day D n Fecal Coliform MF, M-FC NitrateQ. i p TDS d q n N3 m .ma TSS 3 N - Co m Total Nitrogen & TKN C rt a _ y > lS g `S1 0 0 o N � O O ro n O. z m ^1 3 Lab Use Only g K 3° o- O 3 V ? v 1 3 y ,°., m o ` Preservation non.c°nformance identirted for - -_ sample. 2023_December Monthly_Report_WQ004972 for signature Final Audit Report 2024-01-30 Created: 2024-01-30 By: Amanda Grenier (agrenier@greenerehssolutions.com) Status: Signed Transaction ID: CBJCHBCAABAAz1xhC2rQalc_68X581OUjgXOgzNdQmmh "2023_December_Monthly_Report_WQ004972 for signature" Hi story Document created by Amanda Grenier (agrenier@greenerehssolutions.com) 2024-01-30 - 10:37:54 PM GMT Document emailed to Sam Perry (sperry@greenerehssolutions.com) for signature 2024-01-30 - 10:38:00 PM GMT Email viewed by Sam Perry (sperry@greenerehssolutions.com) 2024-01-30 - 10:39:54 PM GMT Document e-signed by Sam Perry (sperry@greenerehssolutions.com) Signature Date: 2024-01-30 - 10:43:52 PM GMT - Time Source: server Agreement completed. 2024-01-30 - 10:43:52 PM GMT a Adobe Acrobat Sign