WQ0013419_Groundwater Monitoring Report November 2023_20231120

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November 20, 2023
LIMS USE: FR - MIKE CODY
LIMS OBJECT ID: 92696513
92696513
Project:
Pace Project No.:
RE:
Mr. Mike Cody
Glatfelter Corp.
228 South Main Street
Spring Grove, PA 17362
Sludge LF November 2023
Dear Mr. Cody:
Enclosed are the analytical results for sample(s) received by the laboratory between November 01, 2023 and November
02, 2023. The results relate only to the samples included in this report. Results reported herein conform to the applicable
TNI/NELAC Standards and the laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the
report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Asheville
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Lorri Patton
[e-mail]
Project Manager
828-417-6055
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 1 of 99
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CERTIFICATIONS
Pace Project No.:
Project:
92696513
Sludge LF November 2023
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Laboratory ID: 99006
South Carolina Certification #: 99006001
South Carolina Drinking Water Cert. #: 99006003
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Louisiana DoH Drinking Water #: LA029
Virginia/VELAP Certification #: 460221
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Laboratory ID: 99030
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 2 of 99
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SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92696513
Sludge LF November 2023
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92696513001 SWP-1 EPA 6010D 18 PASI-ADBB1, SBW
EPA 8270E 74 PASI-CPKS
EPA 8260D 63 PASI-CLMB
EPA 8260D Mod.3 PASI-CTEG
SM 2320B-2011 1 PASI-ASMS
SM 2540C-2015 1 PASI-AJMH1
EPA 300.0 Rev 2.1 1993 1 PASI-ACDC
SM 4500-Cl-E-2011 1 PASI-AZJP
SM 5310B-2014 1 PASI-AMJP
92696513002 SWP-2 EPA 6010D 18 PASI-ASBW
EPA 8270E 74 PASI-CPKS
EPA 8260D 63 PASI-CLMB
EPA 8260D Mod.3 PASI-CTEG
SM 2320B-2011 1 PASI-ASMS
SM 2540C-2015 1 PASI-AJMH1
EPA 300.0 Rev 2.1 1993 1 PASI-ACDC
SM 4500-Cl-E-2011 1 PASI-AZJP
SM 5310B-2014 1 PASI-AMJP
92696513003 Q06V09 EPA 6010D 18 PASI-ADBB1, SBW
EPA 8270E 74 PASI-CPKS
EPA 8260D 63 PASI-CTMH
EPA 8260D Mod.3 PASI-CTEG
SM 2320B-2011 1 PASI-ASMS
SM 2540C-2015 1 PASI-AJMH1
EPA 300.0 Rev 2.1 1993 1 PASI-ACDC
SM 4500-Cl-E-2011 1 PASI-AZJP
SM 5310B-2014 1 PASI-AMJP
92696513004 Q06V10 EPA 6010D 18 PASI-ASBW
EPA 8270E 74 PASI-CPKS
EPA 8260D 63 PASI-CTMH
EPA 8260D Mod.3 PASI-CTEG
SM 2320B-2011 1 PASI-ASMS
SM 2540C-2015 1 PASI-AJMH1
EPA 300.0 Rev 2.1 1993 1 PASI-ACDC
SM 4500-Cl-E-2011 1 PASI-AZJP
SM 5310B-2014 1 PASI-AMJP
92696513005 Q06V11 EPA 6010D 18 PASI-ASBW
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 3 of 99
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SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92696513
Sludge LF November 2023
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
EPA 8270E 74 PASI-CPKS
EPA 8260D 63 PASI-CTMH
EPA 8260D Mod.3 PASI-CTEG
SM 2320B-2011 1 PASI-ASMS
SM 2540C-2015 1 PASI-AJMH1
EPA 300.0 Rev 2.1 1993 1 PASI-ACDC
SM 4500-Cl-E-2011 1 PASI-AZJP
SM 5310B-2014 1 PASI-AMJP
92696513007 TRIP BLANK EPA 8260D 63 PASI-CTMH
EPA 8260D Mod.3 PASI-CTEG
PASI-A = Pace Analytical Services - Asheville
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 4 of 99
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SUMMARY OF DETECTION
Pace Project No.:
Project:
92696513
Sludge LF November 2023
Parameters AnalyzedResult
Lab Sample ID
Report Limit QualifiersUnitsMethod
Client Sample ID
92696513001 SWP-1
Performed by Pace 11/01/23 14:30
Collected By Mark
Swann
11/01/23 14:30
Collected Date 11/1/23 11/01/23 14:30
Collected Time 14:30 11/01/23 14:30
pH 7.21 Std. Units 11/01/23 14:30
Temperature 16.7 deg C 11/01/23 14:30
Specific Conductance 1227 umhos/cm 11/01/23 14:30
Oxygen, Dissolved 7.73 mg/L 11/01/23 14:30
REDOX 35.7 mV 11/01/23 14:30
Turbidity 177.4 NTU 11/01/23 14:30
Odor No odor 11/01/23 14:30
Appearance Hazy,rusty
tint
11/01/23 14:30
Arsenic 6.1J ug/L 11/04/23 20:4910.0EPA 6010D
Barium 289 ug/L 11/04/23 20:495.0EPA 6010D
Calcium 143000 ug/L 11/05/23 20:27500EPA 6010D
Cobalt 11.9 ug/L 11/04/23 20:495.0EPA 6010D
Magnesium 62300 ug/L 11/04/23 20:49100EPA 6010D
Potassium 15000 ug/L 11/04/23 20:495000EPA 6010D
Sodium 22500 ug/L 11/04/23 20:495000EPA 6010D
Zinc 31.9 ug/L 11/04/23 20:4910.0EPA 6010D
Alkalinity, Total as CaCO3 719 mg/L 11/08/23 19:085.0SM 2320B-2011
Total Dissolved Solids 626 mg/L 11/04/23 13:0050.0SM 2540C-2015
Sulfate 1.1 mg/L 11/03/23 17:371.0EPA 300.0 Rev 2.1 1993
Chloride 26.5 mg/L 11/17/23 14:181.0SM 4500-Cl-E-2011
Total Organic Carbon 9.1 mg/L 11/06/23 18:231.0SM 5310B-2014
92696513002 SWP-2
Performed by Pace 11/01/23 15:15
Collected By Mark
Swann
11/01/23 15:15
Collected Date 11/1/23 11/01/23 15:15
Collected Time 15:15 11/01/23 15:15
pH 7.82 Std. Units 11/01/23 15:15
Temperature 12.3 deg C 11/01/23 15:15
Specific Conductance 192 umhos/cm 11/01/23 15:15
Oxygen, Dissolved 9.21 mg/L 11/01/23 15:15
REDOX 109.3 mV 11/01/23 15:15
Turbidity 52.22 NTU 11/01/23 15:15
Odor No odor 11/01/23 15:15
Appearance Clear with
rusty
sediment
11/01/23 15:15
Barium 72.0 ug/L 11/04/23 20:525.0EPA 6010D
Calcium 20500 ug/L 11/04/23 20:52100EPA 6010D
Cobalt 10.3 ug/L 11/04/23 20:525.0EPA 6010D
Magnesium 4860 ug/L 11/04/23 20:52100EPA 6010D
Sodium 9480 ug/L 11/04/23 20:525000EPA 6010D
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 5 of 99
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SUMMARY OF DETECTION
Pace Project No.:
Project:
92696513
Sludge LF November 2023
Parameters AnalyzedResult
Lab Sample ID
Report Limit QualifiersUnitsMethod
Client Sample ID
92696513002 SWP-2
Alkalinity, Total as CaCO3 96.4 mg/L 11/08/23 19:175.0SM 2320B-2011
Total Dissolved Solids 115 mg/L 11/04/23 13:0125.0SM 2540C-2015
Sulfate 2.5 mg/L 11/03/23 17:521.0EPA 300.0 Rev 2.1 1993
Chloride 3.0 mg/L 11/17/23 13:121.0SM 4500-Cl-E-2011
92696513003 Q06V09
Performed by Pace 11/02/23 11:40
Collected By Mark
Swann
11/02/23 11:40
Collected Date 11/2/23 11/02/23 11:40
Collected Time 11:40 11/02/23 11:40
pH 6.38 Std. Units 11/02/23 11:40
Temperature 16.9 deg C 11/02/23 11:40
Static Water Level 30.05 feet 11/02/23 11:40
Specific Conductance 1243 umhos/cm 11/02/23 11:40
Oxygen, Dissolved 2.40 mg/L 11/02/23 11:40
Total Well Depth 69.80 feet 11/02/23 11:40
REDOX Missed mV 11/02/23 11:40
Turbidity 48.11 NTU 11/02/23 11:40
Odor No odor 11/02/23 11:40
Appearance Cloudy 11/02/23 11:40
Barium 285 ug/L 11/04/23 20:545.0EPA 6010D
Calcium 173000 ug/L 11/05/23 20:35500EPA 6010D
Cobalt 14.4 ug/L 11/04/23 20:545.0EPA 6010D
Magnesium 80200 ug/L 11/04/23 20:54100EPA 6010D
Nickel 15.8 ug/L 11/04/23 20:545.0EPA 6010D
Potassium 5020 ug/L 11/04/23 20:545000EPA 6010D
Sodium 31800 ug/L 11/04/23 20:545000EPA 6010D
Zinc 24.2 ug/L 11/04/23 20:5410.0EPA 6010D
Alkalinity, Total as CaCO3 749 mg/L 11/08/23 21:045.0SM 2320B-2011
Total Dissolved Solids 776 mg/L 11/07/23 11:0250.0SM 2540C-2015
Sulfate 1.9 mg/L 11/03/23 21:401.0EPA 300.0 Rev 2.1 1993
Chloride 45.7 mg/L 11/17/23 13:292.0SM 4500-Cl-E-2011
Total Organic Carbon 3.7 mg/L 11/14/23 20:031.0SM 5310B-2014
92696513004 Q06V10
Performed by Pace 11/02/23 10:05
Collected By Mark
Swann
11/02/23 10:05
Collected Date 11/2/23 11/02/23 10:05
Collected Time 10:05 11/02/23 10:05
pH 5.32 Std. Units 11/02/23 10:05
Temperature 12.1 deg C 11/02/23 10:05
Static Water Level 28.72 feet 11/02/23 10:05
Specific Conductance 29.3 umhos/cm 11/02/23 10:05
Oxygen, Dissolved 3.88 mg/L 11/02/23 10:05
Total Well Depth 32.50 feet 11/02/23 10:05
REDOX 157.9 mV 11/02/23 10:05
Turbidity 1.86 NTU 11/02/23 10:05
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 6 of 99
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SUMMARY OF DETECTION
Pace Project No.:
Project:
92696513
Sludge LF November 2023
Parameters AnalyzedResult
Lab Sample ID
Report Limit QualifiersUnitsMethod
Client Sample ID
92696513004 Q06V10
Odor No odor 11/02/23 10:05
Appearance Clear 11/02/23 10:05
Barium 5.0 ug/L 11/04/23 20:575.0EPA 6010D
Calcium 2100 ug/L 11/04/23 20:57100EPA 6010D
Magnesium 846 ug/L 11/04/23 20:57100EPA 6010D
Sodium 2090J ug/L 11/04/23 20:575000EPA 6010D
Alkalinity, Total as CaCO3 10.5 mg/L 11/08/23 21:145.0SM 2320B-2011
Total Dissolved Solids 28.0 mg/L 11/07/23 11:0225.0SM 2540C-2015
Sulfate 0.83J mg/L 11/03/23 22:251.0EPA 300.0 Rev 2.1 1993
Chloride 1.6 mg/L 11/17/23 13:301.0SM 4500-Cl-E-2011
92696513005 Q06V11
Performed by Pace 11/02/23 10:30
Collected By Mark
Swann
11/02/23 10:30
Collected Date 11/2/23 11/02/23 10:30
Collected Time 10:30 11/02/23 10:30
pH 5.57 Std. Units 11/02/23 10:30
Temperature 12.7 deg C 11/02/23 10:30
Static Water Level 41.66 feet 11/02/23 10:30
Specific Conductance 70.8 umhos/cm 11/02/23 10:30
Oxygen, Dissolved 3.25 mg/L 11/02/23 10:30
Total Well Depth 56.91 feet 11/02/23 10:30
REDOX 155.7 mV 11/02/23 10:30
Turbidity 9.62 NTU 11/02/23 10:30
Odor No odor 11/02/23 10:30
Appearance Clear 11/02/23 10:30
Barium 7.0 ug/L 11/04/23 21:005.0EPA 6010D
Calcium 6200 ug/L 11/04/23 21:00100EPA 6010D
Magnesium 2720 ug/L 11/04/23 21:00100EPA 6010D
Sodium 4170J ug/L 11/04/23 21:005000EPA 6010D
Alkalinity, Total as CaCO3 29.7 mg/L 11/08/23 21:195.0SM 2320B-2011
Total Dissolved Solids 48.0 mg/L 11/07/23 11:0225.0SM 2540C-2015
Sulfate 4.6 mg/L 11/03/23 22:401.0EPA 300.0 Rev 2.1 1993
Chloride 1.5 mg/L 11/17/23 13:311.0SM 4500-Cl-E-2011
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 7 of 99
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ANALYTICAL RESULTS
Pace Project No.:
Project:
92696513
Sludge LF November 2023
Sample:SWP-1 Lab ID:92696513001 Collected:11/01/23 14:30 Received:11/01/23 17:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualPQL
Analytical Method:
Pace Analytical Services - Charlotte
Monitoring Well Data
Performed by Pace 11/01/23 14:301
Collected By Mark
Swann
11/01/23 14:301
Collected Date 11/1/23 11/01/23 14:301
Collected Time 14:30 11/01/23 14:301
pH 7.21 Std. Units 11/01/23 14:301
Temperature 16.7 deg C 11/01/23 14:301
Specific Conductance 1227 umhos/cm 11/01/23 14:301
Oxygen, Dissolved 7.73 mg/L 11/01/23 14:30 7782-44-71
REDOX 35.7 mV 11/01/23 14:301
Turbidity 177.4 NTU 11/01/23 14:301
Odor No odor 11/01/23 14:301
Appearance Hazy,rusty
tint
11/01/23 14:301
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Pace Analytical Services - Asheville
6010 MET ICP
Antimony ND ug/L 11/04/23 20:49 7440-36-011/03/23 15:205.0 1
Arsenic 6.1J ug/L 11/04/23 20:49 7440-38-211/03/23 15:2010.0 1
Barium 289 ug/L 11/04/23 20:49 7440-39-311/03/23 15:205.0 1
Cadmium ND ug/L 11/04/23 20:49 7440-43-911/03/23 15:201.0 1
Calcium 143000 ug/L 11/05/23 20:27 7440-70-211/03/23 15:205005
Chromium ND ug/L 11/04/23 20:49 7440-47-311/03/23 15:205.0 1
Cobalt 11.9 ug/L 11/04/23 20:49 7440-48-411/03/23 15:205.0 1
Copper ND ug/L 11/04/23 20:49 7440-50-811/03/23 15:205.0 1
Lead ND ug/L 11/04/23 20:49 7439-92-111/03/23 15:205.0 1
Magnesium 62300 ug/L 11/04/23 20:49 7439-95-411/03/23 15:201001
Nickel ND ug/L 11/04/23 20:49 7440-02-011/03/23 15:205.0 1
Potassium 15000 ug/L 11/04/23 20:49 7440-09-711/03/23 15:2050001
Selenium ND ug/L 11/04/23 20:49 7782-49-211/03/23 15:2010.0 1
Silver ND ug/L 11/04/23 20:49 7440-22-411/03/23 15:205.0 1
Sodium 22500 ug/L 11/04/23 20:49 7440-23-511/03/23 15:2050001
Thallium ND ug/L 11/04/23 20:49 7440-28-011/03/23 15:2010.0 1
Vanadium ND ug/L 11/04/23 20:49 7440-62-211/03/23 15:205.0 1
Zinc 31.9 ug/L 11/04/23 20:49 7440-66-611/03/23 15:2010.0 1
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Acenaphthene ND ug/L 11/08/23 12:38 83-32-911/06/23 12:508.3 1
Acenaphthylene ND ug/L 11/08/23 12:38 208-96-811/06/23 12:508.3 1
Aniline ND ug/L 11/08/23 12:38 62-53-311/06/23 12:508.3 1
Anthracene ND ug/L 11/08/23 12:38 120-12-711/06/23 12:508.3 1
Benzo(a)anthracene ND ug/L 11/08/23 12:38 56-55-311/06/23 12:508.3 1
Benzo(a)pyrene ND ug/L 11/08/23 12:38 50-32-811/06/23 12:508.3 1
Benzo(b)fluoranthene ND ug/L 11/08/23 12:38 205-99-211/06/23 12:508.3 1
Benzo(g,h,i)perylene ND ug/L 11/08/23 12:38 191-24-211/06/23 12:508.3 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/20/2023 08:39 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 8 of 99
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ANALYTICAL RESULTS
Pace Project No.:
Project:
92696513
Sludge LF November 2023
Sample:SWP-1 Lab ID:92696513001 Collected:11/01/23 14:30 Received:11/01/23 17:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualPQL
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Benzo(k)fluoranthene ND ug/L 11/08/23 12:38 207-08-911/06/23 12:508.3 1
Benzoic Acid ND ug/L 11/08/23 12:38 65-85-011/06/23 12:5041.7 1
Benzyl alcohol ND ug/L 11/08/23 12:38 100-51-611/06/23 12:5016.7 1
4-Bromophenylphenyl ether ND ug/L 11/08/23 12:38 101-55-311/06/23 12:508.3 1
Butylbenzylphthalate ND ug/L 11/08/23 12:38 85-68-711/06/23 12:508.3 1
4-Chloro-3-methylphenol ND ug/L 11/08/23 12:38 59-50-711/06/23 12:508.3 1
4-Chloroaniline ND ug/L 11/08/23 12:38 106-47-811/06/23 12:5016.7 1
bis(2-Chloroethoxy)methane ND ug/L 11/08/23 12:38 111-91-111/06/23 12:508.3 1
bis(2-Chloroethyl) ether ND ug/L 11/08/23 12:38 111-44-411/06/23 12:508.3 1
2-Chloronaphthalene ND ug/L 11/08/23 12:38 91-58-711/06/23 12:508.3 1
2-Chlorophenol ND ug/L 11/08/23 12:38 95-57-811/06/23 12:508.3 1
4-Chlorophenylphenyl ether ND ug/L 11/08/23 12:38 7005-72-311/06/23 12:508.3 1
Chrysene ND ug/L 11/08/23 12:38 218-01-911/06/23 12:508.3 1
Dibenz(a,h)anthracene ND ug/L 11/08/23 12:38 53-70-311/06/23 12:508.3 1
Dibenzofuran ND ug/L 11/08/23 12:38 132-64-911/06/23 12:508.3 1
1,2-Dichlorobenzene ND ug/L 11/08/23 12:38 95-50-111/06/23 12:508.3 1
1,3-Dichlorobenzene ND ug/L 11/08/23 12:38 541-73-111/06/23 12:508.3 1
1,4-Dichlorobenzene ND ug/L 11/08/23 12:38 106-46-711/06/23 12:508.3 1
3,3'-Dichlorobenzidine ND ug/L 11/08/23 12:38 91-94-111/06/23 12:5016.7 1
2,4-Dichlorophenol ND ug/L 11/08/23 12:38 120-83-211/06/23 12:508.3 1
Diethylphthalate ND ug/L 11/08/23 12:38 84-66-211/06/23 12:508.3 1
2,4-Dimethylphenol ND ug/L 11/08/23 12:38 105-67-911/06/23 12:508.3 1
Dimethylphthalate ND ug/L 11/08/23 12:38 131-11-311/06/23 12:508.3 1
Di-n-butylphthalate ND ug/L 11/08/23 12:38 84-74-211/06/23 12:508.3 1
4,6-Dinitro-2-methylphenol ND ug/L 11/08/23 12:38 534-52-111/06/23 12:5016.7 1
2,4-Dinitrophenol ND ug/L 11/08/23 12:38 51-28-511/06/23 12:5041.7 1
2,4-Dinitrotoluene ND ug/L 11/08/23 12:38 121-14-211/06/23 12:508.3 1
2,6-Dinitrotoluene ND ug/L 11/08/23 12:38 606-20-211/06/23 12:508.3 1
Di-n-octylphthalate ND ug/L 11/08/23 12:38 117-84-011/06/23 12:508.3 1
bis(2-Ethylhexyl)phthalate ND ug/L 11/08/23 12:38 117-81-711/06/23 12:505.0 1
Fluoranthene ND ug/L 11/08/23 12:38 206-44-011/06/23 12:508.3 1
Fluorene ND ug/L 11/08/23 12:38 86-73-711/06/23 12:508.3 1
Hexachloro-1,3-butadiene ND ug/L 11/08/23 12:38 87-68-311/06/23 12:508.3 1
Hexachlorobenzene ND ug/L 11/08/23 12:38 118-74-111/06/23 12:508.3 1
Hexachlorocyclopentadiene ND ug/L 11/08/23 12:38 77-47-411/06/23 12:508.3 1
Hexachloroethane ND ug/L 11/08/23 12:38 67-72-111/06/23 12:508.3 1
Indeno(1,2,3-cd)pyrene ND ug/L 11/08/23 12:38 193-39-511/06/23 12:508.3 1
Isophorone ND ug/L 11/08/23 12:38 78-59-111/06/23 12:508.3 1
1-Methylnaphthalene ND ug/L 11/08/23 12:38 90-12-011/06/23 12:508.3 1
2-Methylnaphthalene ND ug/L 11/08/23 12:38 91-57-611/06/23 12:508.3 1
2-Methylphenol(o-Cresol)ND ug/L 11/08/23 12:38 95-48-711/06/23 12:508.3 1
3&4-Methylphenol(m&p Cresol)ND ug/L 11/08/23 12:38 15831-10-411/06/23 12:508.3 1
Naphthalene ND ug/L 11/08/23 12:38 91-20-311/06/23 12:508.3 1
2-Nitroaniline ND ug/L 11/08/23 12:38 88-74-411/06/23 12:5016.7 1
3-Nitroaniline ND ug/L 11/08/23 12:38 99-09-211/06/23 12:5016.7 1
4-Nitroaniline ND ug/L 11/08/23 12:38 100-01-611/06/23 12:5016.7 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/20/2023 08:39 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 9 of 99
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ANALYTICAL RESULTS
Pace Project No.:
Project:
92696513
Sludge LF November 2023
Sample:SWP-1 Lab ID:92696513001 Collected:11/01/23 14:30 Received:11/01/23 17:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualPQL
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Nitrobenzene ND ug/L 11/08/23 12:38 98-95-311/06/23 12:508.3 1
2-Nitrophenol ND ug/L 11/08/23 12:38 88-75-511/06/23 12:508.3 1
4-Nitrophenol ND ug/L 11/08/23 12:38 100-02-711/06/23 12:5041.7 1
N-Nitrosodimethylamine ND ug/L 11/08/23 12:38 62-75-911/06/23 12:508.3 1
N-Nitroso-di-n-propylamine ND ug/L 11/08/23 12:38 621-64-711/06/23 12:508.3 1
N-Nitrosodiphenylamine ND ug/L 11/08/23 12:38 86-30-611/06/23 12:508.3 1
2,2'-Oxybis(1-chloropropane)ND ug/L 11/08/23 12:38 108-60-111/06/23 12:508.3 1
Pentachlorophenol ND ug/L 11/08/23 12:38 87-86-511/06/23 12:5016.7 1
Phenanthrene ND ug/L 11/08/23 12:38 85-01-811/06/23 12:508.3 1
Phenol ND ug/L 11/08/23 12:38 108-95-211/06/23 12:508.3 1
Pyrene ND ug/L 11/08/23 12:38 129-00-011/06/23 12:508.3 1
1,2,4-Trichlorobenzene ND ug/L 11/08/23 12:38 120-82-111/06/23 12:508.3 1
2,4,5-Trichlorophenol ND ug/L 11/08/23 12:38 95-95-411/06/23 12:508.3 1
2,4,6-Trichlorophenol ND ug/L 11/08/23 12:38 88-06-211/06/23 12:508.3 1
Surrogates
Nitrobenzene-d5 (S)56 %11/08/23 12:38 4165-60-011/06/23 12:5010-133 1
2-Fluorobiphenyl (S)47 %11/08/23 12:38 321-60-811/06/23 12:5010-130 1
Terphenyl-d14 (S)97 %11/08/23 12:38 1718-51-011/06/23 12:5010-193 1
Phenol-d6 (S)24 %11/08/23 12:38 13127-88-311/06/23 12:5010-130 1
2-Fluorophenol (S)40 %11/08/23 12:38 367-12-411/06/23 12:5010-130 1
2,4,6-Tribromophenol (S)68 %11/08/23 12:38 118-79-611/06/23 12:5010-166 1
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level Landfill
Acetone ND ug/L 11/07/23 05:02 67-64-125.0 1
Benzene ND ug/L 11/07/23 05:02 71-43-21.0 1
Bromobenzene ND ug/L 11/07/23 05:02 108-86-11.0 1
Bromochloromethane ND ug/L 11/07/23 05:02 74-97-51.0 1
Bromodichloromethane ND ug/L 11/07/23 05:02 75-27-41.0 1
Bromoform ND ug/L 11/07/23 05:02 75-25-21.0 1
Bromomethane ND ug/L 11/07/23 05:02 74-83-92.0 1
2-Butanone (MEK)ND ug/L 11/07/23 05:02 78-93-35.0 1
Carbon tetrachloride ND ug/L 11/07/23 05:02 56-23-51.0 1
Chlorobenzene ND ug/L 11/07/23 05:02 108-90-71.0 1
Chloroethane ND ug/L 11/07/23 05:02 75-00-31.0 1
Chloroform ND ug/L 11/07/23 05:02 67-66-31.0 1
Chloromethane ND ug/L 11/07/23 05:02 74-87-31.0 1
2-Chlorotoluene ND ug/L 11/07/23 05:02 95-49-81.0 1
4-Chlorotoluene ND ug/L 11/07/23 05:02 106-43-41.0 1
1,2-Dibromo-3-chloropropane ND ug/L 11/07/23 05:02 96-12-82.0 1
Dibromochloromethane ND ug/L 11/07/23 05:02 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 11/07/23 05:02 106-93-41.0 1
Dibromomethane ND ug/L 11/07/23 05:02 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 11/07/23 05:02 95-50-11.0 1
1,3-Dichlorobenzene ND ug/L 11/07/23 05:02 541-73-11.0 1
1,4-Dichlorobenzene ND ug/L 11/07/23 05:02 106-46-71.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/20/2023 08:39 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 10 of 99
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92696513
Sludge LF November 2023
Sample:SWP-1 Lab ID:92696513001 Collected:11/01/23 14:30 Received:11/01/23 17:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualPQL
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level Landfill
Dichlorodifluoromethane ND ug/L 11/07/23 05:02 75-71-81.0 1
1,1-Dichloroethane ND ug/L 11/07/23 05:02 75-34-31.0 1
1,2-Dichloroethane ND ug/L 11/07/23 05:02 107-06-21.0 1
1,1-Dichloroethene ND ug/L 11/07/23 05:02 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 11/07/23 05:02 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 11/07/23 05:02 156-60-51.0 1
1,2-Dichloropropane ND ug/L 11/07/23 05:02 78-87-51.0 1
1,3-Dichloropropane ND ug/L 11/07/23 05:02 142-28-91.0 1
2,2-Dichloropropane ND ug/L 11/07/23 05:02 594-20-71.0 1
1,1-Dichloropropene ND ug/L 11/07/23 05:02 563-58-61.0 1
cis-1,3-Dichloropropene ND ug/L 11/07/23 05:02 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 11/07/23 05:02 10061-02-61.0 1
Diisopropyl ether ND ug/L 11/07/23 05:02 108-20-31.0 1
Ethylbenzene ND ug/L 11/07/23 05:02 100-41-41.0 1
Hexachloro-1,3-butadiene ND ug/L 11/07/23 05:02 87-68-32.0 1
2-Hexanone ND ug/L 11/07/23 05:02 591-78-65.0 1
p-Isopropyltoluene ND ug/L 11/07/23 05:02 99-87-61.0 1
Methylene Chloride ND ug/L 11/07/23 05:02 75-09-25.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 11/07/23 05:02 108-10-15.0 1
Methyl-tert-butyl ether ND ug/L 11/07/23 05:02 1634-04-41.0 1
Naphthalene ND ug/L 11/07/23 05:02 91-20-31.0 1
Styrene ND ug/L 11/07/23 05:02 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 11/07/23 05:02 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 11/07/23 05:02 79-34-51.0 1
Tetrachloroethene ND ug/L 11/07/23 05:02 127-18-41.0 1
Toluene ND ug/L 11/07/23 05:02 108-88-31.0 1
1,2,3-Trichlorobenzene ND ug/L 11/07/23 05:02 87-61-61.0 1
1,2,4-Trichlorobenzene ND ug/L 11/07/23 05:02 120-82-11.0 1
1,1,1-Trichloroethane ND ug/L 11/07/23 05:02 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 11/07/23 05:02 79-00-51.0 1
Trichloroethene ND ug/L 11/07/23 05:02 79-01-61.0 1
Trichlorofluoromethane ND ug/L 11/07/23 05:02 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 11/07/23 05:02 96-18-41.0 1
Vinyl acetate ND ug/L 11/07/23 05:02 108-05-42.0 1
Vinyl chloride ND ug/L 11/07/23 05:02 75-01-41.0 1
Xylene (Total)ND ug/L 11/07/23 05:02 1330-20-71.0 1
m&p-Xylene ND ug/L 11/07/23 05:02 179601-23-12.0 1
o-Xylene ND ug/L 11/07/23 05:02 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)99 %11/07/23 05:02 460-00-470-130 1
1,2-Dichloroethane-d4 (S)108 %11/07/23 05:02 17060-07-070-130 1
Toluene-d8 (S)102 %11/07/23 05:02 2037-26-570-130 1
Analytical Method: EPA 8260D Mod.
Pace Analytical Services - Charlotte
8260D MSV SIM
1,4-Dioxane (p-Dioxane)ND ug/L 11/03/23 23:03 123-91-12.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/20/2023 08:39 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 11 of 99
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92696513
Sludge LF November 2023
Sample:SWP-1 Lab ID:92696513001 Collected:11/01/23 14:30 Received:11/01/23 17:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualPQL
Analytical Method: EPA 8260D Mod.
Pace Analytical Services - Charlotte
8260D MSV SIM
Surrogates
1,2-Dichloroethane-d4 (S)95 %11/03/23 23:03 17060-07-067-130 1
Toluene-d8 (S)95 %11/03/23 23:03 2037-26-570-130 1
Analytical Method: SM 2320B-2011
Pace Analytical Services - Asheville
2320B Alkalinity
Alkalinity, Total as CaCO3 719 mg/L 11/08/23 19:085.0 1
Analytical Method: SM 2540C-2015
Pace Analytical Services - Asheville
2540C Total Dissolved Solids
Total Dissolved Solids 626 mg/L 11/04/23 13:0050.0 1
Analytical Method: EPA 300.0 Rev 2.1 1993
Pace Analytical Services - Asheville
300.0 IC Anions 28 Days
Sulfate 1.1 mg/L 11/03/23 17:37 14808-79-81.0 1
Analytical Method: SM 4500-Cl-E-2011
Pace Analytical Services - Asheville
4500 Chloride
Chloride 26.5 mg/L 11/17/23 14:18 16887-00-61.0 1
Analytical Method: SM 5310B-2014
Pace Analytical Services - Asheville
5310B TOC
Total Organic Carbon 9.1 mg/L 11/06/23 18:23 7440-44-01.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/20/2023 08:39 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 12 of 99
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92696513
Sludge LF November 2023
Sample:SWP-2 Lab ID:92696513002 Collected:11/01/23 15:15 Received:11/01/23 17:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualPQL
Analytical Method:
Pace Analytical Services - Charlotte
Monitoring Well Data
Performed by Pace 11/01/23 15:151
Collected By Mark
Swann
11/01/23 15:151
Collected Date 11/1/23 11/01/23 15:151
Collected Time 15:15 11/01/23 15:151
pH 7.82 Std. Units 11/01/23 15:151
Temperature 12.3 deg C 11/01/23 15:151
Specific Conductance 192 umhos/cm 11/01/23 15:151
Oxygen, Dissolved 9.21 mg/L 11/01/23 15:15 7782-44-71
REDOX 109.3 mV 11/01/23 15:151
Turbidity 52.22 NTU 11/01/23 15:151
Odor No odor 11/01/23 15:151
Appearance Clear with
rusty
sediment
11/01/23 15:151
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Pace Analytical Services - Asheville
6010 MET ICP
Antimony ND ug/L 11/04/23 20:52 7440-36-011/03/23 15:205.0 1
Arsenic ND ug/L 11/04/23 20:52 7440-38-211/03/23 15:2010.0 1
Barium 72.0 ug/L 11/04/23 20:52 7440-39-311/03/23 15:205.0 1
Cadmium ND ug/L 11/04/23 20:52 7440-43-911/03/23 15:201.0 1
Calcium 20500 ug/L 11/04/23 20:52 7440-70-211/03/23 15:201001
Chromium ND ug/L 11/04/23 20:52 7440-47-311/03/23 15:205.0 1
Cobalt 10.3 ug/L 11/04/23 20:52 7440-48-411/03/23 15:205.0 1
Copper ND ug/L 11/04/23 20:52 7440-50-811/03/23 15:205.0 1
Lead ND ug/L 11/04/23 20:52 7439-92-111/03/23 15:205.0 1
Magnesium 4860 ug/L 11/04/23 20:52 7439-95-411/03/23 15:201001
Nickel ND ug/L 11/04/23 20:52 7440-02-011/03/23 15:205.0 1
Potassium ND ug/L 11/04/23 20:52 7440-09-711/03/23 15:2050001
Selenium ND ug/L 11/04/23 20:52 7782-49-211/03/23 15:2010.0 1
Silver ND ug/L 11/04/23 20:52 7440-22-411/03/23 15:205.0 1
Sodium 9480 ug/L 11/04/23 20:52 7440-23-511/03/23 15:2050001
Thallium ND ug/L 11/04/23 20:52 7440-28-011/03/23 15:2010.0 1
Vanadium ND ug/L 11/04/23 20:52 7440-62-211/03/23 15:205.0 1
Zinc ND ug/L 11/04/23 20:52 7440-66-611/03/23 15:2010.0 1
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Acenaphthene ND ug/L 11/08/23 13:04 83-32-911/06/23 12:508.3 1
Acenaphthylene ND ug/L 11/08/23 13:04 208-96-811/06/23 12:508.3 1
Aniline ND ug/L 11/08/23 13:04 62-53-311/06/23 12:508.3 1
Anthracene ND ug/L 11/08/23 13:04 120-12-711/06/23 12:508.3 1
Benzo(a)anthracene ND ug/L 11/08/23 13:04 56-55-311/06/23 12:508.3 1
Benzo(a)pyrene ND ug/L 11/08/23 13:04 50-32-811/06/23 12:508.3 1
Benzo(b)fluoranthene ND ug/L 11/08/23 13:04 205-99-211/06/23 12:508.3 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/20/2023 08:39 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 13 of 99
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92696513
Sludge LF November 2023
Sample:SWP-2 Lab ID:92696513002 Collected:11/01/23 15:15 Received:11/01/23 17:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualPQL
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Benzo(g,h,i)perylene ND ug/L 11/08/23 13:04 191-24-211/06/23 12:508.3 1
Benzo(k)fluoranthene ND ug/L 11/08/23 13:04 207-08-911/06/23 12:508.3 1
Benzoic Acid ND ug/L 11/08/23 13:04 65-85-011/06/23 12:5041.7 1
Benzyl alcohol ND ug/L 11/08/23 13:04 100-51-611/06/23 12:5016.7 1
4-Bromophenylphenyl ether ND ug/L 11/08/23 13:04 101-55-311/06/23 12:508.3 1
Butylbenzylphthalate ND ug/L 11/08/23 13:04 85-68-711/06/23 12:508.3 1
4-Chloro-3-methylphenol ND ug/L 11/08/23 13:04 59-50-711/06/23 12:508.3 1
4-Chloroaniline ND ug/L 11/08/23 13:04 106-47-811/06/23 12:5016.7 1
bis(2-Chloroethoxy)methane ND ug/L 11/08/23 13:04 111-91-111/06/23 12:508.3 1
bis(2-Chloroethyl) ether ND ug/L 11/08/23 13:04 111-44-411/06/23 12:508.3 1
2-Chloronaphthalene ND ug/L 11/08/23 13:04 91-58-711/06/23 12:508.3 1
2-Chlorophenol ND ug/L 11/08/23 13:04 95-57-811/06/23 12:508.3 1
4-Chlorophenylphenyl ether ND ug/L 11/08/23 13:04 7005-72-311/06/23 12:508.3 1
Chrysene ND ug/L 11/08/23 13:04 218-01-911/06/23 12:508.3 1
Dibenz(a,h)anthracene ND ug/L 11/08/23 13:04 53-70-311/06/23 12:508.3 1
Dibenzofuran ND ug/L 11/08/23 13:04 132-64-911/06/23 12:508.3 1
1,2-Dichlorobenzene ND ug/L 11/08/23 13:04 95-50-111/06/23 12:508.3 1
1,3-Dichlorobenzene ND ug/L 11/08/23 13:04 541-73-111/06/23 12:508.3 1
1,4-Dichlorobenzene ND ug/L 11/08/23 13:04 106-46-711/06/23 12:508.3 1
3,3'-Dichlorobenzidine ND ug/L 11/08/23 13:04 91-94-111/06/23 12:5016.7 1
2,4-Dichlorophenol ND ug/L 11/08/23 13:04 120-83-211/06/23 12:508.3 1
Diethylphthalate ND ug/L 11/08/23 13:04 84-66-211/06/23 12:508.3 1
2,4-Dimethylphenol ND ug/L 11/08/23 13:04 105-67-911/06/23 12:508.3 1
Dimethylphthalate ND ug/L 11/08/23 13:04 131-11-311/06/23 12:508.3 1
Di-n-butylphthalate ND ug/L 11/08/23 13:04 84-74-211/06/23 12:508.3 1
4,6-Dinitro-2-methylphenol ND ug/L 11/08/23 13:04 534-52-111/06/23 12:5016.7 1
2,4-Dinitrophenol ND ug/L 11/08/23 13:04 51-28-511/06/23 12:5041.7 1
2,4-Dinitrotoluene ND ug/L 11/08/23 13:04 121-14-211/06/23 12:508.3 1
2,6-Dinitrotoluene ND ug/L 11/08/23 13:04 606-20-211/06/23 12:508.3 1
Di-n-octylphthalate ND ug/L 11/08/23 13:04 117-84-011/06/23 12:508.3 1
bis(2-Ethylhexyl)phthalate ND ug/L 11/08/23 13:04 117-81-711/06/23 12:505.0 1
Fluoranthene ND ug/L 11/08/23 13:04 206-44-011/06/23 12:508.3 1
Fluorene ND ug/L 11/08/23 13:04 86-73-711/06/23 12:508.3 1
Hexachloro-1,3-butadiene ND ug/L 11/08/23 13:04 87-68-311/06/23 12:508.3 1
Hexachlorobenzene ND ug/L 11/08/23 13:04 118-74-111/06/23 12:508.3 1
Hexachlorocyclopentadiene ND ug/L 11/08/23 13:04 77-47-411/06/23 12:508.3 1
Hexachloroethane ND ug/L 11/08/23 13:04 67-72-111/06/23 12:508.3 1
Indeno(1,2,3-cd)pyrene ND ug/L 11/08/23 13:04 193-39-511/06/23 12:508.3 1
Isophorone ND ug/L 11/08/23 13:04 78-59-111/06/23 12:508.3 1
1-Methylnaphthalene ND ug/L 11/08/23 13:04 90-12-011/06/23 12:508.3 1
2-Methylnaphthalene ND ug/L 11/08/23 13:04 91-57-611/06/23 12:508.3 1
2-Methylphenol(o-Cresol)ND ug/L 11/08/23 13:04 95-48-711/06/23 12:508.3 1
3&4-Methylphenol(m&p Cresol)ND ug/L 11/08/23 13:04 15831-10-411/06/23 12:508.3 1
Naphthalene ND ug/L 11/08/23 13:04 91-20-311/06/23 12:508.3 1
2-Nitroaniline ND ug/L 11/08/23 13:04 88-74-411/06/23 12:5016.7 1
3-Nitroaniline ND ug/L 11/08/23 13:04 99-09-211/06/23 12:5016.7 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/20/2023 08:39 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 14 of 99
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92696513
Sludge LF November 2023
Sample:SWP-2 Lab ID:92696513002 Collected:11/01/23 15:15 Received:11/01/23 17:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualPQL
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
4-Nitroaniline ND ug/L 11/08/23 13:04 100-01-611/06/23 12:5016.7 1
Nitrobenzene ND ug/L 11/08/23 13:04 98-95-311/06/23 12:508.3 1
2-Nitrophenol ND ug/L 11/08/23 13:04 88-75-511/06/23 12:508.3 1
4-Nitrophenol ND ug/L 11/08/23 13:04 100-02-711/06/23 12:5041.7 1
N-Nitrosodimethylamine ND ug/L 11/08/23 13:04 62-75-911/06/23 12:508.3 1
N-Nitroso-di-n-propylamine ND ug/L 11/08/23 13:04 621-64-711/06/23 12:508.3 1
N-Nitrosodiphenylamine ND ug/L 11/08/23 13:04 86-30-611/06/23 12:508.3 1
2,2'-Oxybis(1-chloropropane)ND ug/L 11/08/23 13:04 108-60-111/06/23 12:508.3 1
Pentachlorophenol ND ug/L 11/08/23 13:04 87-86-511/06/23 12:5016.7 1
Phenanthrene ND ug/L 11/08/23 13:04 85-01-811/06/23 12:508.3 1
Phenol ND ug/L 11/08/23 13:04 108-95-211/06/23 12:508.3 1
Pyrene ND ug/L 11/08/23 13:04 129-00-011/06/23 12:508.3 1
1,2,4-Trichlorobenzene ND ug/L 11/08/23 13:04 120-82-111/06/23 12:508.3 1
2,4,5-Trichlorophenol ND ug/L 11/08/23 13:04 95-95-411/06/23 12:508.3 1
2,4,6-Trichlorophenol ND ug/L 11/08/23 13:04 88-06-211/06/23 12:508.3 1
Surrogates
Nitrobenzene-d5 (S)95 %11/08/23 13:04 4165-60-011/06/23 12:5010-133 1
2-Fluorobiphenyl (S)86 %11/08/23 13:04 321-60-811/06/23 12:5010-130 1
Terphenyl-d14 (S)120 %11/08/23 13:04 1718-51-011/06/23 12:5010-193 1
Phenol-d6 (S)37 %11/08/23 13:04 13127-88-311/06/23 12:5010-130 1
2-Fluorophenol (S)63 %11/08/23 13:04 367-12-411/06/23 12:5010-130 1
2,4,6-Tribromophenol (S)92 %11/08/23 13:04 118-79-611/06/23 12:5010-166 1
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level Landfill
Acetone ND ug/L 11/07/23 05:20 67-64-125.0 1
Benzene ND ug/L 11/07/23 05:20 71-43-21.0 1
Bromobenzene ND ug/L 11/07/23 05:20 108-86-11.0 1
Bromochloromethane ND ug/L 11/07/23 05:20 74-97-51.0 1
Bromodichloromethane ND ug/L 11/07/23 05:20 75-27-41.0 1
Bromoform ND ug/L 11/07/23 05:20 75-25-21.0 1
Bromomethane ND ug/L 11/07/23 05:20 74-83-92.0 1
2-Butanone (MEK)ND ug/L 11/07/23 05:20 78-93-35.0 1
Carbon tetrachloride ND ug/L 11/07/23 05:20 56-23-51.0 1
Chlorobenzene ND ug/L 11/07/23 05:20 108-90-71.0 1
Chloroethane ND ug/L 11/07/23 05:20 75-00-31.0 1
Chloroform ND ug/L 11/07/23 05:20 67-66-31.0 1
Chloromethane ND ug/L 11/07/23 05:20 74-87-31.0 1
2-Chlorotoluene ND ug/L 11/07/23 05:20 95-49-81.0 1
4-Chlorotoluene ND ug/L 11/07/23 05:20 106-43-41.0 1
1,2-Dibromo-3-chloropropane ND ug/L 11/07/23 05:20 96-12-82.0 1
Dibromochloromethane ND ug/L 11/07/23 05:20 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 11/07/23 05:20 106-93-41.0 1
Dibromomethane ND ug/L 11/07/23 05:20 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 11/07/23 05:20 95-50-11.0 1
1,3-Dichlorobenzene ND ug/L 11/07/23 05:20 541-73-11.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/20/2023 08:39 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 15 of 99
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92696513
Sludge LF November 2023
Sample:SWP-2 Lab ID:92696513002 Collected:11/01/23 15:15 Received:11/01/23 17:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualPQL
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level Landfill
1,4-Dichlorobenzene ND ug/L 11/07/23 05:20 106-46-71.0 1
Dichlorodifluoromethane ND ug/L 11/07/23 05:20 75-71-81.0 1
1,1-Dichloroethane ND ug/L 11/07/23 05:20 75-34-31.0 1
1,2-Dichloroethane ND ug/L 11/07/23 05:20 107-06-21.0 1
1,1-Dichloroethene ND ug/L 11/07/23 05:20 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 11/07/23 05:20 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 11/07/23 05:20 156-60-51.0 1
1,2-Dichloropropane ND ug/L 11/07/23 05:20 78-87-51.0 1
1,3-Dichloropropane ND ug/L 11/07/23 05:20 142-28-91.0 1
2,2-Dichloropropane ND ug/L 11/07/23 05:20 594-20-71.0 1
1,1-Dichloropropene ND ug/L 11/07/23 05:20 563-58-61.0 1
cis-1,3-Dichloropropene ND ug/L 11/07/23 05:20 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 11/07/23 05:20 10061-02-61.0 1
Diisopropyl ether ND ug/L 11/07/23 05:20 108-20-31.0 1
Ethylbenzene ND ug/L 11/07/23 05:20 100-41-41.0 1
Hexachloro-1,3-butadiene ND ug/L 11/07/23 05:20 87-68-32.0 1
2-Hexanone ND ug/L 11/07/23 05:20 591-78-65.0 1
p-Isopropyltoluene ND ug/L 11/07/23 05:20 99-87-61.0 1
Methylene Chloride ND ug/L 11/07/23 05:20 75-09-25.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 11/07/23 05:20 108-10-15.0 1
Methyl-tert-butyl ether ND ug/L 11/07/23 05:20 1634-04-41.0 1
Naphthalene ND ug/L 11/07/23 05:20 91-20-31.0 1
Styrene ND ug/L 11/07/23 05:20 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 11/07/23 05:20 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 11/07/23 05:20 79-34-51.0 1
Tetrachloroethene ND ug/L 11/07/23 05:20 127-18-41.0 1
Toluene ND ug/L 11/07/23 05:20 108-88-31.0 1
1,2,3-Trichlorobenzene ND ug/L 11/07/23 05:20 87-61-61.0 1
1,2,4-Trichlorobenzene ND ug/L 11/07/23 05:20 120-82-11.0 1
1,1,1-Trichloroethane ND ug/L 11/07/23 05:20 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 11/07/23 05:20 79-00-51.0 1
Trichloroethene ND ug/L 11/07/23 05:20 79-01-61.0 1
Trichlorofluoromethane ND ug/L 11/07/23 05:20 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 11/07/23 05:20 96-18-41.0 1
Vinyl acetate ND ug/L 11/07/23 05:20 108-05-42.0 1
Vinyl chloride ND ug/L 11/07/23 05:20 75-01-41.0 1
Xylene (Total)ND ug/L 11/07/23 05:20 1330-20-71.0 1
m&p-Xylene ND ug/L 11/07/23 05:20 179601-23-12.0 1
o-Xylene ND ug/L 11/07/23 05:20 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)99 %11/07/23 05:20 460-00-470-130 1
1,2-Dichloroethane-d4 (S)109 %11/07/23 05:20 17060-07-070-130 1
Toluene-d8 (S)104 %11/07/23 05:20 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/20/2023 08:39 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 16 of 99
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92696513
Sludge LF November 2023
Sample:SWP-2 Lab ID:92696513002 Collected:11/01/23 15:15 Received:11/01/23 17:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualPQL
Analytical Method: EPA 8260D Mod.
Pace Analytical Services - Charlotte
8260D MSV SIM
1,4-Dioxane (p-Dioxane)ND ug/L 11/03/23 23:24 123-91-12.0 1
Surrogates
1,2-Dichloroethane-d4 (S)93 %11/03/23 23:24 17060-07-067-130 1
Toluene-d8 (S)95 %11/03/23 23:24 2037-26-570-130 1
Analytical Method: SM 2320B-2011
Pace Analytical Services - Asheville
2320B Alkalinity
Alkalinity, Total as CaCO3 96.4 mg/L 11/08/23 19:175.0 1
Analytical Method: SM 2540C-2015
Pace Analytical Services - Asheville
2540C Total Dissolved Solids
Total Dissolved Solids 115 mg/L 11/04/23 13:0125.0 1
Analytical Method: EPA 300.0 Rev 2.1 1993
Pace Analytical Services - Asheville
300.0 IC Anions 28 Days
Sulfate 2.5 mg/L 11/03/23 17:52 14808-79-81.0 1
Analytical Method: SM 4500-Cl-E-2011
Pace Analytical Services - Asheville
4500 Chloride
Chloride 3.0 mg/L 11/17/23 13:12 16887-00-61.0 1
Analytical Method: SM 5310B-2014
Pace Analytical Services - Asheville
5310B TOC
Total Organic Carbon ND mg/L 11/06/23 18:42 7440-44-01.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/20/2023 08:39 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 17 of 99
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92696513
Sludge LF November 2023
Sample:Q06V09 Lab ID:92696513003 Collected:11/02/23 11:40 Received:11/02/23 16:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualPQL
Analytical Method:
Pace Analytical Services - Charlotte
Monitoring Well Data
Performed by Pace 11/02/23 11:401
Collected By Mark
Swann
11/02/23 11:401
Collected Date 11/2/23 11/02/23 11:401
Collected Time 11:40 11/02/23 11:401
pH 6.38 Std. Units 11/02/23 11:401
Temperature 16.9 deg C 11/02/23 11:401
Static Water Level 30.05 feet 11/02/23 11:401
Specific Conductance 1243 umhos/cm 11/02/23 11:401
Oxygen, Dissolved 2.40 mg/L 11/02/23 11:40 7782-44-71
Total Well Depth 69.80 feet 11/02/23 11:401
REDOX Missed mV 11/02/23 11:401
Turbidity 48.11 NTU 11/02/23 11:401
Odor No odor 11/02/23 11:401
Appearance Cloudy 11/02/23 11:401
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Pace Analytical Services - Asheville
6010 MET ICP
Antimony ND ug/L 11/04/23 20:54 7440-36-011/03/23 15:205.0 1
Arsenic ND ug/L 11/04/23 20:54 7440-38-211/03/23 15:2010.0 1
Barium 285 ug/L 11/04/23 20:54 7440-39-311/03/23 15:205.0 1
Cadmium ND ug/L 11/04/23 20:54 7440-43-911/03/23 15:201.0 1
Calcium 173000 ug/L 11/05/23 20:35 7440-70-211/03/23 15:205005
Chromium ND ug/L 11/04/23 20:54 7440-47-311/03/23 15:205.0 1
Cobalt 14.4 ug/L 11/04/23 20:54 7440-48-411/03/23 15:205.0 1
Copper ND ug/L 11/04/23 20:54 7440-50-811/03/23 15:205.0 1
Lead ND ug/L 11/04/23 20:54 7439-92-111/03/23 15:205.0 1
Magnesium 80200 ug/L 11/04/23 20:54 7439-95-411/03/23 15:201001
Nickel 15.8 ug/L 11/04/23 20:54 7440-02-011/03/23 15:205.0 1
Potassium 5020 ug/L 11/04/23 20:54 7440-09-711/03/23 15:2050001
Selenium ND ug/L 11/04/23 20:54 7782-49-211/03/23 15:2010.0 1
Silver ND ug/L 11/04/23 20:54 7440-22-411/03/23 15:205.0 1
Sodium 31800 ug/L 11/04/23 20:54 7440-23-511/03/23 15:2050001
Thallium ND ug/L 11/04/23 20:54 7440-28-011/03/23 15:2010.0 1
Vanadium ND ug/L 11/04/23 20:54 7440-62-211/03/23 15:205.0 1
Zinc 24.2 ug/L 11/04/23 20:54 7440-66-611/03/23 15:2010.0 1
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Acenaphthene ND ug/L 11/08/23 13:29 83-32-911/06/23 12:508.3 1
Acenaphthylene ND ug/L 11/08/23 13:29 208-96-811/06/23 12:508.3 1
Aniline ND ug/L 11/08/23 13:29 62-53-311/06/23 12:508.3 1
Anthracene ND ug/L 11/08/23 13:29 120-12-711/06/23 12:508.3 1
Benzo(a)anthracene ND ug/L 11/08/23 13:29 56-55-311/06/23 12:508.3 1
Benzo(a)pyrene ND ug/L 11/08/23 13:29 50-32-811/06/23 12:508.3 1
Benzo(b)fluoranthene ND ug/L 11/08/23 13:29 205-99-211/06/23 12:508.3 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/20/2023 08:39 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 18 of 99
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92696513
Sludge LF November 2023
Sample:Q06V09 Lab ID:92696513003 Collected:11/02/23 11:40 Received:11/02/23 16:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualPQL
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Benzo(g,h,i)perylene ND ug/L 11/08/23 13:29 191-24-211/06/23 12:508.3 1
Benzo(k)fluoranthene ND ug/L 11/08/23 13:29 207-08-911/06/23 12:508.3 1
Benzoic Acid ND ug/L 11/08/23 13:29 65-85-011/06/23 12:5041.7 1
Benzyl alcohol ND ug/L 11/08/23 13:29 100-51-611/06/23 12:5016.7 1
4-Bromophenylphenyl ether ND ug/L 11/08/23 13:29 101-55-311/06/23 12:508.3 1
Butylbenzylphthalate ND ug/L 11/08/23 13:29 85-68-711/06/23 12:508.3 1
4-Chloro-3-methylphenol ND ug/L 11/08/23 13:29 59-50-711/06/23 12:508.3 1
4-Chloroaniline ND ug/L 11/08/23 13:29 106-47-811/06/23 12:5016.7 1
bis(2-Chloroethoxy)methane ND ug/L 11/08/23 13:29 111-91-111/06/23 12:508.3 1
bis(2-Chloroethyl) ether ND ug/L 11/08/23 13:29 111-44-411/06/23 12:508.3 1
2-Chloronaphthalene ND ug/L 11/08/23 13:29 91-58-711/06/23 12:508.3 1
2-Chlorophenol ND ug/L 11/08/23 13:29 95-57-811/06/23 12:508.3 1
4-Chlorophenylphenyl ether ND ug/L 11/08/23 13:29 7005-72-311/06/23 12:508.3 1
Chrysene ND ug/L 11/08/23 13:29 218-01-911/06/23 12:508.3 1
Dibenz(a,h)anthracene ND ug/L 11/08/23 13:29 53-70-311/06/23 12:508.3 1
Dibenzofuran ND ug/L 11/08/23 13:29 132-64-911/06/23 12:508.3 1
1,2-Dichlorobenzene ND ug/L 11/08/23 13:29 95-50-111/06/23 12:508.3 1
1,3-Dichlorobenzene ND ug/L 11/08/23 13:29 541-73-111/06/23 12:508.3 1
1,4-Dichlorobenzene ND ug/L 11/08/23 13:29 106-46-711/06/23 12:508.3 1
3,3'-Dichlorobenzidine ND ug/L 11/08/23 13:29 91-94-111/06/23 12:5016.7 1
2,4-Dichlorophenol ND ug/L 11/08/23 13:29 120-83-211/06/23 12:508.3 1
Diethylphthalate ND ug/L 11/08/23 13:29 84-66-211/06/23 12:508.3 1
2,4-Dimethylphenol ND ug/L 11/08/23 13:29 105-67-911/06/23 12:508.3 1
Dimethylphthalate ND ug/L 11/08/23 13:29 131-11-311/06/23 12:508.3 1
Di-n-butylphthalate ND ug/L 11/08/23 13:29 84-74-211/06/23 12:508.3 1
4,6-Dinitro-2-methylphenol ND ug/L 11/08/23 13:29 534-52-111/06/23 12:5016.7 1
2,4-Dinitrophenol ND ug/L 11/08/23 13:29 51-28-511/06/23 12:5041.7 1
2,4-Dinitrotoluene ND ug/L 11/08/23 13:29 121-14-211/06/23 12:508.3 1
2,6-Dinitrotoluene ND ug/L 11/08/23 13:29 606-20-211/06/23 12:508.3 1
Di-n-octylphthalate ND ug/L 11/08/23 13:29 117-84-011/06/23 12:508.3 1
bis(2-Ethylhexyl)phthalate ND ug/L 11/08/23 13:29 117-81-711/06/23 12:505.0 1
Fluoranthene ND ug/L 11/08/23 13:29 206-44-011/06/23 12:508.3 1
Fluorene ND ug/L 11/08/23 13:29 86-73-711/06/23 12:508.3 1
Hexachloro-1,3-butadiene ND ug/L 11/08/23 13:29 87-68-311/06/23 12:508.3 1
Hexachlorobenzene ND ug/L 11/08/23 13:29 118-74-111/06/23 12:508.3 1
Hexachlorocyclopentadiene ND ug/L 11/08/23 13:29 77-47-411/06/23 12:508.3 1
Hexachloroethane ND ug/L 11/08/23 13:29 67-72-111/06/23 12:508.3 1
Indeno(1,2,3-cd)pyrene ND ug/L 11/08/23 13:29 193-39-511/06/23 12:508.3 1
Isophorone ND ug/L 11/08/23 13:29 78-59-111/06/23 12:508.3 1
1-Methylnaphthalene ND ug/L 11/08/23 13:29 90-12-011/06/23 12:508.3 1
2-Methylnaphthalene ND ug/L 11/08/23 13:29 91-57-611/06/23 12:508.3 1
2-Methylphenol(o-Cresol)ND ug/L 11/08/23 13:29 95-48-711/06/23 12:508.3 1
3&4-Methylphenol(m&p Cresol)ND ug/L 11/08/23 13:29 15831-10-411/06/23 12:508.3 1
Naphthalene ND ug/L 11/08/23 13:29 91-20-311/06/23 12:508.3 1
2-Nitroaniline ND ug/L 11/08/23 13:29 88-74-411/06/23 12:5016.7 1
3-Nitroaniline ND ug/L 11/08/23 13:29 99-09-211/06/23 12:5016.7 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/20/2023 08:39 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 19 of 99
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92696513
Sludge LF November 2023
Sample:Q06V09 Lab ID:92696513003 Collected:11/02/23 11:40 Received:11/02/23 16:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualPQL
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
4-Nitroaniline ND ug/L 11/08/23 13:29 100-01-611/06/23 12:5016.7 1
Nitrobenzene ND ug/L 11/08/23 13:29 98-95-311/06/23 12:508.3 1
2-Nitrophenol ND ug/L 11/08/23 13:29 88-75-511/06/23 12:508.3 1
4-Nitrophenol ND ug/L 11/08/23 13:29 100-02-711/06/23 12:5041.7 1
N-Nitrosodimethylamine ND ug/L 11/08/23 13:29 62-75-911/06/23 12:508.3 1
N-Nitroso-di-n-propylamine ND ug/L 11/08/23 13:29 621-64-711/06/23 12:508.3 1
N-Nitrosodiphenylamine ND ug/L 11/08/23 13:29 86-30-611/06/23 12:508.3 1
2,2'-Oxybis(1-chloropropane)ND ug/L 11/08/23 13:29 108-60-111/06/23 12:508.3 1
Pentachlorophenol ND ug/L 11/08/23 13:29 87-86-511/06/23 12:5016.7 1
Phenanthrene ND ug/L 11/08/23 13:29 85-01-811/06/23 12:508.3 1
Phenol ND ug/L 11/08/23 13:29 108-95-211/06/23 12:508.3 1
Pyrene ND ug/L 11/08/23 13:29 129-00-011/06/23 12:508.3 1
1,2,4-Trichlorobenzene ND ug/L 11/08/23 13:29 120-82-111/06/23 12:508.3 1
2,4,5-Trichlorophenol ND ug/L 11/08/23 13:29 95-95-411/06/23 12:508.3 1
2,4,6-Trichlorophenol ND ug/L 11/08/23 13:29 88-06-211/06/23 12:508.3 1
Surrogates
Nitrobenzene-d5 (S)80 %11/08/23 13:29 4165-60-011/06/23 12:5010-133 1
2-Fluorobiphenyl (S)73 %11/08/23 13:29 321-60-811/06/23 12:5010-130 1
Terphenyl-d14 (S)93 %11/08/23 13:29 1718-51-011/06/23 12:5010-193 1
Phenol-d6 (S)31 %11/08/23 13:29 13127-88-311/06/23 12:5010-130 1
2-Fluorophenol (S)52 %11/08/23 13:29 367-12-411/06/23 12:5010-130 1
2,4,6-Tribromophenol (S)92 %11/08/23 13:29 118-79-611/06/23 12:5010-166 1
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level Landfill
Acetone ND ug/L 11/08/23 18:36 67-64-125.0 1
Benzene ND ug/L 11/08/23 18:36 71-43-21.0 1
Bromobenzene ND ug/L 11/08/23 18:36 108-86-11.0 1
Bromochloromethane ND ug/L 11/08/23 18:36 74-97-51.0 1
Bromodichloromethane ND ug/L 11/08/23 18:36 75-27-41.0 1
Bromoform ND ug/L 11/08/23 18:36 75-25-21.0 1
Bromomethane ND ug/L 11/08/23 18:36 74-83-92.0 1
2-Butanone (MEK)ND ug/L 11/08/23 18:36 78-93-35.0 1
Carbon tetrachloride ND ug/L 11/08/23 18:36 56-23-51.0 1
Chlorobenzene ND ug/L 11/08/23 18:36 108-90-71.0 1
Chloroethane ND ug/L 11/08/23 18:36 75-00-31.0 1
Chloroform ND ug/L 11/08/23 18:36 67-66-31.0 1
Chloromethane ND ug/L 11/08/23 18:36 74-87-31.0 1
2-Chlorotoluene ND ug/L 11/08/23 18:36 95-49-81.0 1
4-Chlorotoluene ND ug/L 11/08/23 18:36 106-43-41.0 1
1,2-Dibromo-3-chloropropane ND ug/L 11/08/23 18:36 96-12-82.0 1
Dibromochloromethane ND ug/L 11/08/23 18:36 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 11/08/23 18:36 106-93-41.0 1
Dibromomethane ND ug/L 11/08/23 18:36 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 11/08/23 18:36 95-50-11.0 1
1,3-Dichlorobenzene ND ug/L 11/08/23 18:36 541-73-11.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/20/2023 08:39 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 20 of 99
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92696513
Sludge LF November 2023
Sample:Q06V09 Lab ID:92696513003 Collected:11/02/23 11:40 Received:11/02/23 16:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualPQL
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level Landfill
1,4-Dichlorobenzene ND ug/L 11/08/23 18:36 106-46-71.0 1
Dichlorodifluoromethane ND ug/L 11/08/23 18:36 75-71-8 v21.0 1
1,1-Dichloroethane ND ug/L 11/08/23 18:36 75-34-31.0 1
1,2-Dichloroethane ND ug/L 11/08/23 18:36 107-06-21.0 1
1,1-Dichloroethene ND ug/L 11/08/23 18:36 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 11/08/23 18:36 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 11/08/23 18:36 156-60-51.0 1
1,2-Dichloropropane ND ug/L 11/08/23 18:36 78-87-51.0 1
1,3-Dichloropropane ND ug/L 11/08/23 18:36 142-28-91.0 1
2,2-Dichloropropane ND ug/L 11/08/23 18:36 594-20-71.0 1
1,1-Dichloropropene ND ug/L 11/08/23 18:36 563-58-61.0 1
cis-1,3-Dichloropropene ND ug/L 11/08/23 18:36 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 11/08/23 18:36 10061-02-61.0 1
Diisopropyl ether ND ug/L 11/08/23 18:36 108-20-31.0 1
Ethylbenzene ND ug/L 11/08/23 18:36 100-41-41.0 1
Hexachloro-1,3-butadiene ND ug/L 11/08/23 18:36 87-68-32.0 1
2-Hexanone ND ug/L 11/08/23 18:36 591-78-65.0 1
p-Isopropyltoluene ND ug/L 11/08/23 18:36 99-87-61.0 1
Methylene Chloride ND ug/L 11/08/23 18:36 75-09-25.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 11/08/23 18:36 108-10-15.0 1
Methyl-tert-butyl ether ND ug/L 11/08/23 18:36 1634-04-41.0 1
Naphthalene ND ug/L 11/08/23 18:36 91-20-31.0 1
Styrene ND ug/L 11/08/23 18:36 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 11/08/23 18:36 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 11/08/23 18:36 79-34-51.0 1
Tetrachloroethene ND ug/L 11/08/23 18:36 127-18-41.0 1
Toluene ND ug/L 11/08/23 18:36 108-88-31.0 1
1,2,3-Trichlorobenzene ND ug/L 11/08/23 18:36 87-61-61.0 1
1,2,4-Trichlorobenzene ND ug/L 11/08/23 18:36 120-82-11.0 1
1,1,1-Trichloroethane ND ug/L 11/08/23 18:36 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 11/08/23 18:36 79-00-51.0 1
Trichloroethene ND ug/L 11/08/23 18:36 79-01-61.0 1
Trichlorofluoromethane ND ug/L 11/08/23 18:36 75-69-4 v21.0 1
1,2,3-Trichloropropane ND ug/L 11/08/23 18:36 96-18-41.0 1
Vinyl acetate ND ug/L 11/08/23 18:36 108-05-42.0 1
Vinyl chloride ND ug/L 11/08/23 18:36 75-01-41.0 1
Xylene (Total)ND ug/L 11/08/23 18:36 1330-20-71.0 1
m&p-Xylene ND ug/L 11/08/23 18:36 179601-23-12.0 1
o-Xylene ND ug/L 11/08/23 18:36 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)96 %11/08/23 18:36 460-00-470-130 1
1,2-Dichloroethane-d4 (S)107 %11/08/23 18:36 17060-07-070-130 1
Toluene-d8 (S)96 %11/08/23 18:36 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/20/2023 08:39 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 21 of 99
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92696513
Sludge LF November 2023
Sample:Q06V09 Lab ID:92696513003 Collected:11/02/23 11:40 Received:11/02/23 16:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualPQL
Analytical Method: EPA 8260D Mod.
Pace Analytical Services - Charlotte
8260D MSV SIM
1,4-Dioxane (p-Dioxane)ND ug/L 11/06/23 15:48 123-91-12.0 1
Surrogates
1,2-Dichloroethane-d4 (S)96 %11/06/23 15:48 17060-07-067-130 1
Toluene-d8 (S)98 %11/06/23 15:48 2037-26-570-130 1
Analytical Method: SM 2320B-2011
Pace Analytical Services - Asheville
2320B Alkalinity
Alkalinity, Total as CaCO3 749 mg/L 11/08/23 21:045.0 1
Analytical Method: SM 2540C-2015
Pace Analytical Services - Asheville
2540C Total Dissolved Solids
Total Dissolved Solids 776 mg/L 11/07/23 11:0250.0 1
Analytical Method: EPA 300.0 Rev 2.1 1993
Pace Analytical Services - Asheville
300.0 IC Anions 28 Days
Sulfate 1.9 mg/L 11/03/23 21:40 14808-79-81.0 1
Analytical Method: SM 4500-Cl-E-2011
Pace Analytical Services - Asheville
4500 Chloride
Chloride 45.7 mg/L 11/17/23 13:29 16887-00-62.0 2
Analytical Method: SM 5310B-2014
Pace Analytical Services - Asheville
5310B TOC
Total Organic Carbon 3.7 mg/L 11/14/23 20:03 7440-44-01.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/20/2023 08:39 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 22 of 99
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92696513
Sludge LF November 2023
Sample:Q06V10 Lab ID:92696513004 Collected:11/02/23 10:05 Received:11/02/23 16:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualPQL
Analytical Method:
Pace Analytical Services - Charlotte
Monitoring Well Data
Performed by Pace 11/02/23 10:051
Collected By Mark
Swann
11/02/23 10:051
Collected Date 11/2/23 11/02/23 10:051
Collected Time 10:05 11/02/23 10:051
pH 5.32 Std. Units 11/02/23 10:051
Temperature 12.1 deg C 11/02/23 10:051
Static Water Level 28.72 feet 11/02/23 10:051
Specific Conductance 29.3 umhos/cm 11/02/23 10:051
Oxygen, Dissolved 3.88 mg/L 11/02/23 10:05 7782-44-71
Total Well Depth 32.50 feet 11/02/23 10:051
REDOX 157.9 mV 11/02/23 10:051
Turbidity 1.86 NTU 11/02/23 10:051
Odor No odor 11/02/23 10:051
Appearance Clear 11/02/23 10:051
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Pace Analytical Services - Asheville
6010 MET ICP
Antimony ND ug/L 11/04/23 20:57 7440-36-011/03/23 15:205.0 1
Arsenic ND ug/L 11/04/23 20:57 7440-38-211/03/23 15:2010.0 1
Barium 5.0 ug/L 11/04/23 20:57 7440-39-311/03/23 15:205.0 1
Cadmium ND ug/L 11/04/23 20:57 7440-43-911/03/23 15:201.0 1
Calcium 2100 ug/L 11/04/23 20:57 7440-70-211/03/23 15:201001
Chromium ND ug/L 11/04/23 20:57 7440-47-311/03/23 15:205.0 1
Cobalt ND ug/L 11/04/23 20:57 7440-48-411/03/23 15:205.0 1
Copper ND ug/L 11/04/23 20:57 7440-50-811/03/23 15:205.0 1
Lead ND ug/L 11/04/23 20:57 7439-92-111/03/23 15:205.0 1
Magnesium 846 ug/L 11/04/23 20:57 7439-95-411/03/23 15:201001
Nickel ND ug/L 11/04/23 20:57 7440-02-011/03/23 15:205.0 1
Potassium ND ug/L 11/04/23 20:57 7440-09-711/03/23 15:2050001
Selenium ND ug/L 11/04/23 20:57 7782-49-211/03/23 15:2010.0 1
Silver ND ug/L 11/04/23 20:57 7440-22-411/03/23 15:205.0 1
Sodium 2090J ug/L 11/04/23 20:57 7440-23-511/03/23 15:2050001
Thallium ND ug/L 11/04/23 20:57 7440-28-011/03/23 15:2010.0 1
Vanadium ND ug/L 11/04/23 20:57 7440-62-211/03/23 15:205.0 1
Zinc ND ug/L 11/04/23 20:57 7440-66-611/03/23 15:2010.0 1
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Acenaphthene ND ug/L 11/08/23 13:55 83-32-911/06/23 12:508.3 1
Acenaphthylene ND ug/L 11/08/23 13:55 208-96-811/06/23 12:508.3 1
Aniline ND ug/L 11/08/23 13:55 62-53-311/06/23 12:508.3 1
Anthracene ND ug/L 11/08/23 13:55 120-12-711/06/23 12:508.3 1
Benzo(a)anthracene ND ug/L 11/08/23 13:55 56-55-311/06/23 12:508.3 1
Benzo(a)pyrene ND ug/L 11/08/23 13:55 50-32-811/06/23 12:508.3 1
Benzo(b)fluoranthene ND ug/L 11/08/23 13:55 205-99-211/06/23 12:508.3 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/20/2023 08:39 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 23 of 99
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92696513
Sludge LF November 2023
Sample:Q06V10 Lab ID:92696513004 Collected:11/02/23 10:05 Received:11/02/23 16:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualPQL
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Benzo(g,h,i)perylene ND ug/L 11/08/23 13:55 191-24-211/06/23 12:508.3 1
Benzo(k)fluoranthene ND ug/L 11/08/23 13:55 207-08-911/06/23 12:508.3 1
Benzoic Acid ND ug/L 11/08/23 13:55 65-85-011/06/23 12:5041.7 1
Benzyl alcohol ND ug/L 11/08/23 13:55 100-51-611/06/23 12:5016.7 1
4-Bromophenylphenyl ether ND ug/L 11/08/23 13:55 101-55-311/06/23 12:508.3 1
Butylbenzylphthalate ND ug/L 11/08/23 13:55 85-68-711/06/23 12:508.3 1
4-Chloro-3-methylphenol ND ug/L 11/08/23 13:55 59-50-711/06/23 12:508.3 1
4-Chloroaniline ND ug/L 11/08/23 13:55 106-47-811/06/23 12:5016.7 1
bis(2-Chloroethoxy)methane ND ug/L 11/08/23 13:55 111-91-111/06/23 12:508.3 1
bis(2-Chloroethyl) ether ND ug/L 11/08/23 13:55 111-44-411/06/23 12:508.3 1
2-Chloronaphthalene ND ug/L 11/08/23 13:55 91-58-711/06/23 12:508.3 1
2-Chlorophenol ND ug/L 11/08/23 13:55 95-57-811/06/23 12:508.3 1
4-Chlorophenylphenyl ether ND ug/L 11/08/23 13:55 7005-72-311/06/23 12:508.3 1
Chrysene ND ug/L 11/08/23 13:55 218-01-911/06/23 12:508.3 1
Dibenz(a,h)anthracene ND ug/L 11/08/23 13:55 53-70-311/06/23 12:508.3 1
Dibenzofuran ND ug/L 11/08/23 13:55 132-64-911/06/23 12:508.3 1
1,2-Dichlorobenzene ND ug/L 11/08/23 13:55 95-50-111/06/23 12:508.3 1
1,3-Dichlorobenzene ND ug/L 11/08/23 13:55 541-73-111/06/23 12:508.3 1
1,4-Dichlorobenzene ND ug/L 11/08/23 13:55 106-46-711/06/23 12:508.3 1
3,3'-Dichlorobenzidine ND ug/L 11/08/23 13:55 91-94-111/06/23 12:5016.7 1
2,4-Dichlorophenol ND ug/L 11/08/23 13:55 120-83-211/06/23 12:508.3 1
Diethylphthalate ND ug/L 11/08/23 13:55 84-66-211/06/23 12:508.3 1
2,4-Dimethylphenol ND ug/L 11/08/23 13:55 105-67-911/06/23 12:508.3 1
Dimethylphthalate ND ug/L 11/08/23 13:55 131-11-311/06/23 12:508.3 1
Di-n-butylphthalate ND ug/L 11/08/23 13:55 84-74-211/06/23 12:508.3 1
4,6-Dinitro-2-methylphenol ND ug/L 11/08/23 13:55 534-52-111/06/23 12:5016.7 1
2,4-Dinitrophenol ND ug/L 11/08/23 13:55 51-28-511/06/23 12:5041.7 1
2,4-Dinitrotoluene ND ug/L 11/08/23 13:55 121-14-211/06/23 12:508.3 1
2,6-Dinitrotoluene ND ug/L 11/08/23 13:55 606-20-211/06/23 12:508.3 1
Di-n-octylphthalate ND ug/L 11/08/23 13:55 117-84-011/06/23 12:508.3 1
bis(2-Ethylhexyl)phthalate ND ug/L 11/08/23 13:55 117-81-711/06/23 12:505.0 1
Fluoranthene ND ug/L 11/08/23 13:55 206-44-011/06/23 12:508.3 1
Fluorene ND ug/L 11/08/23 13:55 86-73-711/06/23 12:508.3 1
Hexachloro-1,3-butadiene ND ug/L 11/08/23 13:55 87-68-311/06/23 12:508.3 1
Hexachlorobenzene ND ug/L 11/08/23 13:55 118-74-111/06/23 12:508.3 1
Hexachlorocyclopentadiene ND ug/L 11/08/23 13:55 77-47-411/06/23 12:508.3 1
Hexachloroethane ND ug/L 11/08/23 13:55 67-72-111/06/23 12:508.3 1
Indeno(1,2,3-cd)pyrene ND ug/L 11/08/23 13:55 193-39-511/06/23 12:508.3 1
Isophorone ND ug/L 11/08/23 13:55 78-59-111/06/23 12:508.3 1
1-Methylnaphthalene ND ug/L 11/08/23 13:55 90-12-011/06/23 12:508.3 1
2-Methylnaphthalene ND ug/L 11/08/23 13:55 91-57-611/06/23 12:508.3 1
2-Methylphenol(o-Cresol)ND ug/L 11/08/23 13:55 95-48-711/06/23 12:508.3 1
3&4-Methylphenol(m&p Cresol)ND ug/L 11/08/23 13:55 15831-10-411/06/23 12:508.3 1
Naphthalene ND ug/L 11/08/23 13:55 91-20-311/06/23 12:508.3 1
2-Nitroaniline ND ug/L 11/08/23 13:55 88-74-411/06/23 12:5016.7 1
3-Nitroaniline ND ug/L 11/08/23 13:55 99-09-211/06/23 12:5016.7 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/20/2023 08:39 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 24 of 99
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92696513
Sludge LF November 2023
Sample:Q06V10 Lab ID:92696513004 Collected:11/02/23 10:05 Received:11/02/23 16:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualPQL
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
4-Nitroaniline ND ug/L 11/08/23 13:55 100-01-611/06/23 12:5016.7 1
Nitrobenzene ND ug/L 11/08/23 13:55 98-95-311/06/23 12:508.3 1
2-Nitrophenol ND ug/L 11/08/23 13:55 88-75-511/06/23 12:508.3 1
4-Nitrophenol ND ug/L 11/08/23 13:55 100-02-711/06/23 12:5041.7 1
N-Nitrosodimethylamine ND ug/L 11/08/23 13:55 62-75-911/06/23 12:508.3 1
N-Nitroso-di-n-propylamine ND ug/L 11/08/23 13:55 621-64-711/06/23 12:508.3 1
N-Nitrosodiphenylamine ND ug/L 11/08/23 13:55 86-30-611/06/23 12:508.3 1
2,2'-Oxybis(1-chloropropane)ND ug/L 11/08/23 13:55 108-60-111/06/23 12:508.3 1
Pentachlorophenol ND ug/L 11/08/23 13:55 87-86-511/06/23 12:5016.7 1
Phenanthrene ND ug/L 11/08/23 13:55 85-01-811/06/23 12:508.3 1
Phenol ND ug/L 11/08/23 13:55 108-95-211/06/23 12:508.3 1
Pyrene ND ug/L 11/08/23 13:55 129-00-011/06/23 12:508.3 1
1,2,4-Trichlorobenzene ND ug/L 11/08/23 13:55 120-82-111/06/23 12:508.3 1
2,4,5-Trichlorophenol ND ug/L 11/08/23 13:55 95-95-411/06/23 12:508.3 1
2,4,6-Trichlorophenol ND ug/L 11/08/23 13:55 88-06-211/06/23 12:508.3 1
Surrogates
Nitrobenzene-d5 (S)98 %11/08/23 13:55 4165-60-011/06/23 12:5010-133 1
2-Fluorobiphenyl (S)86 %11/08/23 13:55 321-60-811/06/23 12:5010-130 1
Terphenyl-d14 (S)125 %11/08/23 13:55 1718-51-011/06/23 12:5010-193 1
Phenol-d6 (S)40 %11/08/23 13:55 13127-88-311/06/23 12:5010-130 1
2-Fluorophenol (S)64 %11/08/23 13:55 367-12-411/06/23 12:5010-130 1
2,4,6-Tribromophenol (S)105 %11/08/23 13:55 118-79-611/06/23 12:5010-166 1
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level Landfill
Acetone ND ug/L 11/08/23 18:53 67-64-125.0 1
Benzene ND ug/L 11/08/23 18:53 71-43-21.0 1
Bromobenzene ND ug/L 11/08/23 18:53 108-86-11.0 1
Bromochloromethane ND ug/L 11/08/23 18:53 74-97-51.0 1
Bromodichloromethane ND ug/L 11/08/23 18:53 75-27-41.0 1
Bromoform ND ug/L 11/08/23 18:53 75-25-21.0 1
Bromomethane ND ug/L 11/08/23 18:53 74-83-92.0 1
2-Butanone (MEK)ND ug/L 11/08/23 18:53 78-93-35.0 1
Carbon tetrachloride ND ug/L 11/08/23 18:53 56-23-51.0 1
Chlorobenzene ND ug/L 11/08/23 18:53 108-90-71.0 1
Chloroethane ND ug/L 11/08/23 18:53 75-00-31.0 1
Chloroform ND ug/L 11/08/23 18:53 67-66-31.0 1
Chloromethane ND ug/L 11/08/23 18:53 74-87-31.0 1
2-Chlorotoluene ND ug/L 11/08/23 18:53 95-49-81.0 1
4-Chlorotoluene ND ug/L 11/08/23 18:53 106-43-41.0 1
1,2-Dibromo-3-chloropropane ND ug/L 11/08/23 18:53 96-12-82.0 1
Dibromochloromethane ND ug/L 11/08/23 18:53 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 11/08/23 18:53 106-93-41.0 1
Dibromomethane ND ug/L 11/08/23 18:53 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 11/08/23 18:53 95-50-11.0 1
1,3-Dichlorobenzene ND ug/L 11/08/23 18:53 541-73-11.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/20/2023 08:39 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 25 of 99
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92696513
Sludge LF November 2023
Sample:Q06V10 Lab ID:92696513004 Collected:11/02/23 10:05 Received:11/02/23 16:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualPQL
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level Landfill
1,4-Dichlorobenzene ND ug/L 11/08/23 18:53 106-46-71.0 1
Dichlorodifluoromethane ND ug/L 11/08/23 18:53 75-71-8 v21.0 1
1,1-Dichloroethane ND ug/L 11/08/23 18:53 75-34-31.0 1
1,2-Dichloroethane ND ug/L 11/08/23 18:53 107-06-21.0 1
1,1-Dichloroethene ND ug/L 11/08/23 18:53 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 11/08/23 18:53 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 11/08/23 18:53 156-60-51.0 1
1,2-Dichloropropane ND ug/L 11/08/23 18:53 78-87-51.0 1
1,3-Dichloropropane ND ug/L 11/08/23 18:53 142-28-91.0 1
2,2-Dichloropropane ND ug/L 11/08/23 18:53 594-20-71.0 1
1,1-Dichloropropene ND ug/L 11/08/23 18:53 563-58-61.0 1
cis-1,3-Dichloropropene ND ug/L 11/08/23 18:53 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 11/08/23 18:53 10061-02-61.0 1
Diisopropyl ether ND ug/L 11/08/23 18:53 108-20-31.0 1
Ethylbenzene ND ug/L 11/08/23 18:53 100-41-41.0 1
Hexachloro-1,3-butadiene ND ug/L 11/08/23 18:53 87-68-32.0 1
2-Hexanone ND ug/L 11/08/23 18:53 591-78-65.0 1
p-Isopropyltoluene ND ug/L 11/08/23 18:53 99-87-61.0 1
Methylene Chloride ND ug/L 11/08/23 18:53 75-09-25.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 11/08/23 18:53 108-10-15.0 1
Methyl-tert-butyl ether ND ug/L 11/08/23 18:53 1634-04-41.0 1
Naphthalene ND ug/L 11/08/23 18:53 91-20-31.0 1
Styrene ND ug/L 11/08/23 18:53 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 11/08/23 18:53 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 11/08/23 18:53 79-34-51.0 1
Tetrachloroethene ND ug/L 11/08/23 18:53 127-18-41.0 1
Toluene ND ug/L 11/08/23 18:53 108-88-31.0 1
1,2,3-Trichlorobenzene ND ug/L 11/08/23 18:53 87-61-61.0 1
1,2,4-Trichlorobenzene ND ug/L 11/08/23 18:53 120-82-11.0 1
1,1,1-Trichloroethane ND ug/L 11/08/23 18:53 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 11/08/23 18:53 79-00-51.0 1
Trichloroethene ND ug/L 11/08/23 18:53 79-01-61.0 1
Trichlorofluoromethane ND ug/L 11/08/23 18:53 75-69-4 v21.0 1
1,2,3-Trichloropropane ND ug/L 11/08/23 18:53 96-18-41.0 1
Vinyl acetate ND ug/L 11/08/23 18:53 108-05-42.0 1
Vinyl chloride ND ug/L 11/08/23 18:53 75-01-41.0 1
Xylene (Total)ND ug/L 11/08/23 18:53 1330-20-71.0 1
m&p-Xylene ND ug/L 11/08/23 18:53 179601-23-12.0 1
o-Xylene ND ug/L 11/08/23 18:53 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)97 %11/08/23 18:53 460-00-470-130 1
1,2-Dichloroethane-d4 (S)109 %11/08/23 18:53 17060-07-070-130 1
Toluene-d8 (S)96 %11/08/23 18:53 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/20/2023 08:39 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 26 of 99
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92696513
Sludge LF November 2023
Sample:Q06V10 Lab ID:92696513004 Collected:11/02/23 10:05 Received:11/02/23 16:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualPQL
Analytical Method: EPA 8260D Mod.
Pace Analytical Services - Charlotte
8260D MSV SIM
1,4-Dioxane (p-Dioxane)ND ug/L 11/06/23 16:10 123-91-12.0 1
Surrogates
1,2-Dichloroethane-d4 (S)93 %11/06/23 16:10 17060-07-067-130 1
Toluene-d8 (S)97 %11/06/23 16:10 2037-26-570-130 1
Analytical Method: SM 2320B-2011
Pace Analytical Services - Asheville
2320B Alkalinity
Alkalinity, Total as CaCO3 10.5 mg/L 11/08/23 21:145.0 1
Analytical Method: SM 2540C-2015
Pace Analytical Services - Asheville
2540C Total Dissolved Solids
Total Dissolved Solids 28.0 mg/L 11/07/23 11:0225.0 1
Analytical Method: EPA 300.0 Rev 2.1 1993
Pace Analytical Services - Asheville
300.0 IC Anions 28 Days
Sulfate 0.83J mg/L 11/03/23 22:25 14808-79-81.0 1
Analytical Method: SM 4500-Cl-E-2011
Pace Analytical Services - Asheville
4500 Chloride
Chloride 1.6 mg/L 11/17/23 13:30 16887-00-61.0 1
Analytical Method: SM 5310B-2014
Pace Analytical Services - Asheville
5310B TOC
Total Organic Carbon ND mg/L 11/14/23 20:23 7440-44-01.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/20/2023 08:39 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 27 of 99
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92696513
Sludge LF November 2023
Sample:Q06V11 Lab ID:92696513005 Collected:11/02/23 10:30 Received:11/02/23 16:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualPQL
Analytical Method:
Pace Analytical Services - Charlotte
Monitoring Well Data
Performed by Pace 11/02/23 10:301
Collected By Mark
Swann
11/02/23 10:301
Collected Date 11/2/23 11/02/23 10:301
Collected Time 10:30 11/02/23 10:301
pH 5.57 Std. Units 11/02/23 10:301
Temperature 12.7 deg C 11/02/23 10:301
Static Water Level 41.66 feet 11/02/23 10:301
Specific Conductance 70.8 umhos/cm 11/02/23 10:301
Oxygen, Dissolved 3.25 mg/L 11/02/23 10:30 7782-44-71
Total Well Depth 56.91 feet 11/02/23 10:301
REDOX 155.7 mV 11/02/23 10:301
Turbidity 9.62 NTU 11/02/23 10:301
Odor No odor 11/02/23 10:301
Appearance Clear 11/02/23 10:301
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Pace Analytical Services - Asheville
6010 MET ICP
Antimony ND ug/L 11/04/23 21:00 7440-36-011/03/23 15:205.0 1
Arsenic ND ug/L 11/04/23 21:00 7440-38-211/03/23 15:2010.0 1
Barium 7.0 ug/L 11/04/23 21:00 7440-39-311/03/23 15:205.0 1
Cadmium ND ug/L 11/04/23 21:00 7440-43-911/03/23 15:201.0 1
Calcium 6200 ug/L 11/04/23 21:00 7440-70-211/03/23 15:201001
Chromium ND ug/L 11/04/23 21:00 7440-47-311/03/23 15:205.0 1
Cobalt ND ug/L 11/04/23 21:00 7440-48-411/03/23 15:205.0 1
Copper ND ug/L 11/04/23 21:00 7440-50-811/03/23 15:205.0 1
Lead ND ug/L 11/04/23 21:00 7439-92-111/03/23 15:205.0 1
Magnesium 2720 ug/L 11/04/23 21:00 7439-95-411/03/23 15:201001
Nickel ND ug/L 11/04/23 21:00 7440-02-011/03/23 15:205.0 1
Potassium ND ug/L 11/04/23 21:00 7440-09-711/03/23 15:2050001
Selenium ND ug/L 11/04/23 21:00 7782-49-211/03/23 15:2010.0 1
Silver ND ug/L 11/04/23 21:00 7440-22-411/03/23 15:205.0 1
Sodium 4170J ug/L 11/04/23 21:00 7440-23-511/03/23 15:2050001
Thallium ND ug/L 11/04/23 21:00 7440-28-011/03/23 15:2010.0 1
Vanadium ND ug/L 11/04/23 21:00 7440-62-211/03/23 15:205.0 1
Zinc ND ug/L 11/04/23 21:00 7440-66-611/03/23 15:2010.0 1
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Acenaphthene ND ug/L 11/08/23 14:21 83-32-911/06/23 12:5010.0 1
Acenaphthylene ND ug/L 11/08/23 14:21 208-96-811/06/23 12:5010.0 1
Aniline ND ug/L 11/08/23 14:21 62-53-311/06/23 12:5010.0 1
Anthracene ND ug/L 11/08/23 14:21 120-12-711/06/23 12:5010.0 1
Benzo(a)anthracene ND ug/L 11/08/23 14:21 56-55-311/06/23 12:5010.0 1
Benzo(a)pyrene ND ug/L 11/08/23 14:21 50-32-811/06/23 12:5010.0 1
Benzo(b)fluoranthene ND ug/L 11/08/23 14:21 205-99-211/06/23 12:5010.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/20/2023 08:39 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 28 of 99
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92696513
Sludge LF November 2023
Sample:Q06V11 Lab ID:92696513005 Collected:11/02/23 10:30 Received:11/02/23 16:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualPQL
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Benzo(g,h,i)perylene ND ug/L 11/08/23 14:21 191-24-211/06/23 12:5010.0 1
Benzo(k)fluoranthene ND ug/L 11/08/23 14:21 207-08-911/06/23 12:5010.0 1
Benzoic Acid ND ug/L 11/08/23 14:21 65-85-011/06/23 12:5050.0 1
Benzyl alcohol ND ug/L 11/08/23 14:21 100-51-611/06/23 12:5020.0 1
4-Bromophenylphenyl ether ND ug/L 11/08/23 14:21 101-55-311/06/23 12:5010.0 1
Butylbenzylphthalate ND ug/L 11/08/23 14:21 85-68-711/06/23 12:5010.0 1
4-Chloro-3-methylphenol ND ug/L 11/08/23 14:21 59-50-711/06/23 12:5010.0 1
4-Chloroaniline ND ug/L 11/08/23 14:21 106-47-811/06/23 12:5020.0 1
bis(2-Chloroethoxy)methane ND ug/L 11/08/23 14:21 111-91-111/06/23 12:5010.0 1
bis(2-Chloroethyl) ether ND ug/L 11/08/23 14:21 111-44-411/06/23 12:5010.0 1
2-Chloronaphthalene ND ug/L 11/08/23 14:21 91-58-711/06/23 12:5010.0 1
2-Chlorophenol ND ug/L 11/08/23 14:21 95-57-811/06/23 12:5010.0 1
4-Chlorophenylphenyl ether ND ug/L 11/08/23 14:21 7005-72-311/06/23 12:5010.0 1
Chrysene ND ug/L 11/08/23 14:21 218-01-911/06/23 12:5010.0 1
Dibenz(a,h)anthracene ND ug/L 11/08/23 14:21 53-70-311/06/23 12:5010.0 1
Dibenzofuran ND ug/L 11/08/23 14:21 132-64-911/06/23 12:5010.0 1
1,2-Dichlorobenzene ND ug/L 11/08/23 14:21 95-50-111/06/23 12:5010.0 1
1,3-Dichlorobenzene ND ug/L 11/08/23 14:21 541-73-111/06/23 12:5010.0 1
1,4-Dichlorobenzene ND ug/L 11/08/23 14:21 106-46-711/06/23 12:5010.0 1
3,3'-Dichlorobenzidine ND ug/L 11/08/23 14:21 91-94-111/06/23 12:5020.0 1
2,4-Dichlorophenol ND ug/L 11/08/23 14:21 120-83-211/06/23 12:5010.0 1
Diethylphthalate ND ug/L 11/08/23 14:21 84-66-211/06/23 12:5010.0 1
2,4-Dimethylphenol ND ug/L 11/08/23 14:21 105-67-911/06/23 12:5010.0 1
Dimethylphthalate ND ug/L 11/08/23 14:21 131-11-311/06/23 12:5010.0 1
Di-n-butylphthalate ND ug/L 11/08/23 14:21 84-74-211/06/23 12:5010.0 1
4,6-Dinitro-2-methylphenol ND ug/L 11/08/23 14:21 534-52-111/06/23 12:5020.0 1
2,4-Dinitrophenol ND ug/L 11/08/23 14:21 51-28-511/06/23 12:5050.0 1
2,4-Dinitrotoluene ND ug/L 11/08/23 14:21 121-14-211/06/23 12:5010.0 1
2,6-Dinitrotoluene ND ug/L 11/08/23 14:21 606-20-211/06/23 12:5010.0 1
Di-n-octylphthalate ND ug/L 11/08/23 14:21 117-84-011/06/23 12:5010.0 1
bis(2-Ethylhexyl)phthalate ND ug/L 11/08/23 14:21 117-81-711/06/23 12:506.0 1
Fluoranthene ND ug/L 11/08/23 14:21 206-44-011/06/23 12:5010.0 1
Fluorene ND ug/L 11/08/23 14:21 86-73-711/06/23 12:5010.0 1
Hexachloro-1,3-butadiene ND ug/L 11/08/23 14:21 87-68-311/06/23 12:5010.0 1
Hexachlorobenzene ND ug/L 11/08/23 14:21 118-74-111/06/23 12:5010.0 1
Hexachlorocyclopentadiene ND ug/L 11/08/23 14:21 77-47-411/06/23 12:5010.0 1
Hexachloroethane ND ug/L 11/08/23 14:21 67-72-111/06/23 12:5010.0 1
Indeno(1,2,3-cd)pyrene ND ug/L 11/08/23 14:21 193-39-511/06/23 12:5010.0 1
Isophorone ND ug/L 11/08/23 14:21 78-59-111/06/23 12:5010.0 1
1-Methylnaphthalene ND ug/L 11/08/23 14:21 90-12-011/06/23 12:5010.0 1
2-Methylnaphthalene ND ug/L 11/08/23 14:21 91-57-611/06/23 12:5010.0 1
2-Methylphenol(o-Cresol)ND ug/L 11/08/23 14:21 95-48-711/06/23 12:5010.0 1
3&4-Methylphenol(m&p Cresol)ND ug/L 11/08/23 14:21 15831-10-411/06/23 12:5010.0 1
Naphthalene ND ug/L 11/08/23 14:21 91-20-311/06/23 12:5010.0 1
2-Nitroaniline ND ug/L 11/08/23 14:21 88-74-411/06/23 12:5020.0 1
3-Nitroaniline ND ug/L 11/08/23 14:21 99-09-211/06/23 12:5020.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/20/2023 08:39 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 29 of 99
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92696513
Sludge LF November 2023
Sample:Q06V11 Lab ID:92696513005 Collected:11/02/23 10:30 Received:11/02/23 16:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualPQL
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
4-Nitroaniline ND ug/L 11/08/23 14:21 100-01-611/06/23 12:5020.0 1
Nitrobenzene ND ug/L 11/08/23 14:21 98-95-311/06/23 12:5010.0 1
2-Nitrophenol ND ug/L 11/08/23 14:21 88-75-511/06/23 12:5010.0 1
4-Nitrophenol ND ug/L 11/08/23 14:21 100-02-711/06/23 12:5050.0 1
N-Nitrosodimethylamine ND ug/L 11/08/23 14:21 62-75-911/06/23 12:5010.0 1
N-Nitroso-di-n-propylamine ND ug/L 11/08/23 14:21 621-64-711/06/23 12:5010.0 1
N-Nitrosodiphenylamine ND ug/L 11/08/23 14:21 86-30-611/06/23 12:5010.0 1
2,2'-Oxybis(1-chloropropane)ND ug/L 11/08/23 14:21 108-60-111/06/23 12:5010.0 1
Pentachlorophenol ND ug/L 11/08/23 14:21 87-86-511/06/23 12:5020.0 1
Phenanthrene ND ug/L 11/08/23 14:21 85-01-811/06/23 12:5010.0 1
Phenol ND ug/L 11/08/23 14:21 108-95-211/06/23 12:5010.0 1
Pyrene ND ug/L 11/08/23 14:21 129-00-011/06/23 12:5010.0 1
1,2,4-Trichlorobenzene ND ug/L 11/08/23 14:21 120-82-111/06/23 12:5010.0 1
2,4,5-Trichlorophenol ND ug/L 11/08/23 14:21 95-95-411/06/23 12:5010.0 1
2,4,6-Trichlorophenol ND ug/L 11/08/23 14:21 88-06-211/06/23 12:5010.0 1
Surrogates
Nitrobenzene-d5 (S)80 %11/08/23 14:21 4165-60-011/06/23 12:5010-133 1
2-Fluorobiphenyl (S)77 %11/08/23 14:21 321-60-811/06/23 12:5010-130 1
Terphenyl-d14 (S)111 %11/08/23 14:21 1718-51-011/06/23 12:5010-193 1
Phenol-d6 (S)32 %11/08/23 14:21 13127-88-311/06/23 12:5010-130 1
2-Fluorophenol (S)50 %11/08/23 14:21 367-12-411/06/23 12:5010-130 1
2,4,6-Tribromophenol (S)83 %11/08/23 14:21 118-79-611/06/23 12:5010-166 1
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level Landfill
Acetone ND ug/L 11/08/23 19:11 67-64-125.0 1
Benzene ND ug/L 11/08/23 19:11 71-43-21.0 1
Bromobenzene ND ug/L 11/08/23 19:11 108-86-11.0 1
Bromochloromethane ND ug/L 11/08/23 19:11 74-97-51.0 1
Bromodichloromethane ND ug/L 11/08/23 19:11 75-27-41.0 1
Bromoform ND ug/L 11/08/23 19:11 75-25-21.0 1
Bromomethane ND ug/L 11/08/23 19:11 74-83-92.0 1
2-Butanone (MEK)ND ug/L 11/08/23 19:11 78-93-35.0 1
Carbon tetrachloride ND ug/L 11/08/23 19:11 56-23-51.0 1
Chlorobenzene ND ug/L 11/08/23 19:11 108-90-71.0 1
Chloroethane ND ug/L 11/08/23 19:11 75-00-31.0 1
Chloroform ND ug/L 11/08/23 19:11 67-66-31.0 1
Chloromethane ND ug/L 11/08/23 19:11 74-87-31.0 1
2-Chlorotoluene ND ug/L 11/08/23 19:11 95-49-81.0 1
4-Chlorotoluene ND ug/L 11/08/23 19:11 106-43-41.0 1
1,2-Dibromo-3-chloropropane ND ug/L 11/08/23 19:11 96-12-82.0 1
Dibromochloromethane ND ug/L 11/08/23 19:11 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 11/08/23 19:11 106-93-41.0 1
Dibromomethane ND ug/L 11/08/23 19:11 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 11/08/23 19:11 95-50-11.0 1
1,3-Dichlorobenzene ND ug/L 11/08/23 19:11 541-73-11.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/20/2023 08:39 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 30 of 99
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92696513
Sludge LF November 2023
Sample:Q06V11 Lab ID:92696513005 Collected:11/02/23 10:30 Received:11/02/23 16:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualPQL
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level Landfill
1,4-Dichlorobenzene ND ug/L 11/08/23 19:11 106-46-71.0 1
Dichlorodifluoromethane ND ug/L 11/08/23 19:11 75-71-8 v21.0 1
1,1-Dichloroethane ND ug/L 11/08/23 19:11 75-34-31.0 1
1,2-Dichloroethane ND ug/L 11/08/23 19:11 107-06-21.0 1
1,1-Dichloroethene ND ug/L 11/08/23 19:11 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 11/08/23 19:11 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 11/08/23 19:11 156-60-51.0 1
1,2-Dichloropropane ND ug/L 11/08/23 19:11 78-87-51.0 1
1,3-Dichloropropane ND ug/L 11/08/23 19:11 142-28-91.0 1
2,2-Dichloropropane ND ug/L 11/08/23 19:11 594-20-71.0 1
1,1-Dichloropropene ND ug/L 11/08/23 19:11 563-58-61.0 1
cis-1,3-Dichloropropene ND ug/L 11/08/23 19:11 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 11/08/23 19:11 10061-02-61.0 1
Diisopropyl ether ND ug/L 11/08/23 19:11 108-20-31.0 1
Ethylbenzene ND ug/L 11/08/23 19:11 100-41-41.0 1
Hexachloro-1,3-butadiene ND ug/L 11/08/23 19:11 87-68-32.0 1
2-Hexanone ND ug/L 11/08/23 19:11 591-78-65.0 1
p-Isopropyltoluene ND ug/L 11/08/23 19:11 99-87-61.0 1
Methylene Chloride ND ug/L 11/08/23 19:11 75-09-25.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 11/08/23 19:11 108-10-15.0 1
Methyl-tert-butyl ether ND ug/L 11/08/23 19:11 1634-04-41.0 1
Naphthalene ND ug/L 11/08/23 19:11 91-20-31.0 1
Styrene ND ug/L 11/08/23 19:11 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 11/08/23 19:11 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 11/08/23 19:11 79-34-51.0 1
Tetrachloroethene ND ug/L 11/08/23 19:11 127-18-41.0 1
Toluene ND ug/L 11/08/23 19:11 108-88-31.0 1
1,2,3-Trichlorobenzene ND ug/L 11/08/23 19:11 87-61-61.0 1
1,2,4-Trichlorobenzene ND ug/L 11/08/23 19:11 120-82-11.0 1
1,1,1-Trichloroethane ND ug/L 11/08/23 19:11 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 11/08/23 19:11 79-00-51.0 1
Trichloroethene ND ug/L 11/08/23 19:11 79-01-61.0 1
Trichlorofluoromethane ND ug/L 11/08/23 19:11 75-69-4 v21.0 1
1,2,3-Trichloropropane ND ug/L 11/08/23 19:11 96-18-41.0 1
Vinyl acetate ND ug/L 11/08/23 19:11 108-05-42.0 1
Vinyl chloride ND ug/L 11/08/23 19:11 75-01-41.0 1
Xylene (Total)ND ug/L 11/08/23 19:11 1330-20-71.0 1
m&p-Xylene ND ug/L 11/08/23 19:11 179601-23-12.0 1
o-Xylene ND ug/L 11/08/23 19:11 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)99 %11/08/23 19:11 460-00-470-130 1
1,2-Dichloroethane-d4 (S)108 %11/08/23 19:11 17060-07-070-130 1
Toluene-d8 (S)98 %11/08/23 19:11 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/20/2023 08:39 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 31 of 99
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92696513
Sludge LF November 2023
Sample:Q06V11 Lab ID:92696513005 Collected:11/02/23 10:30 Received:11/02/23 16:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualPQL
Analytical Method: EPA 8260D Mod.
Pace Analytical Services - Charlotte
8260D MSV SIM
1,4-Dioxane (p-Dioxane)ND ug/L 11/06/23 16:31 123-91-12.0 1
Surrogates
1,2-Dichloroethane-d4 (S)92 %11/06/23 16:31 17060-07-067-130 1
Toluene-d8 (S)97 %11/06/23 16:31 2037-26-570-130 1
Analytical Method: SM 2320B-2011
Pace Analytical Services - Asheville
2320B Alkalinity
Alkalinity, Total as CaCO3 29.7 mg/L 11/08/23 21:195.0 1
Analytical Method: SM 2540C-2015
Pace Analytical Services - Asheville
2540C Total Dissolved Solids
Total Dissolved Solids 48.0 mg/L 11/07/23 11:0225.0 1
Analytical Method: EPA 300.0 Rev 2.1 1993
Pace Analytical Services - Asheville
300.0 IC Anions 28 Days
Sulfate 4.6 mg/L 11/03/23 22:40 14808-79-81.0 1
Analytical Method: SM 4500-Cl-E-2011
Pace Analytical Services - Asheville
4500 Chloride
Chloride 1.5 mg/L 11/17/23 13:31 16887-00-61.0 1
Analytical Method: SM 5310B-2014
Pace Analytical Services - Asheville
5310B TOC
Total Organic Carbon ND mg/L 11/14/23 21:14 7440-44-01.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/20/2023 08:39 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 32 of 99
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92696513
Sludge LF November 2023
Sample:TRIP BLANK Lab ID:92696513007 Collected:11/02/23 09:00 Received:11/02/23 16:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualPQL
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level Landfill
Acetone ND ug/L 11/08/23 15:58 67-64-125.0 1
Benzene ND ug/L 11/08/23 15:58 71-43-21.0 1
Bromobenzene ND ug/L 11/08/23 15:58 108-86-11.0 1
Bromochloromethane ND ug/L 11/08/23 15:58 74-97-51.0 1
Bromodichloromethane ND ug/L 11/08/23 15:58 75-27-41.0 1
Bromoform ND ug/L 11/08/23 15:58 75-25-21.0 1
Bromomethane ND ug/L 11/08/23 15:58 74-83-92.0 1
2-Butanone (MEK)ND ug/L 11/08/23 15:58 78-93-35.0 1
Carbon tetrachloride ND ug/L 11/08/23 15:58 56-23-51.0 1
Chlorobenzene ND ug/L 11/08/23 15:58 108-90-71.0 1
Chloroethane ND ug/L 11/08/23 15:58 75-00-31.0 1
Chloroform ND ug/L 11/08/23 15:58 67-66-31.0 1
Chloromethane ND ug/L 11/08/23 15:58 74-87-31.0 1
2-Chlorotoluene ND ug/L 11/08/23 15:58 95-49-81.0 1
4-Chlorotoluene ND ug/L 11/08/23 15:58 106-43-41.0 1
1,2-Dibromo-3-chloropropane ND ug/L 11/08/23 15:58 96-12-82.0 1
Dibromochloromethane ND ug/L 11/08/23 15:58 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 11/08/23 15:58 106-93-41.0 1
Dibromomethane ND ug/L 11/08/23 15:58 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 11/08/23 15:58 95-50-11.0 1
1,3-Dichlorobenzene ND ug/L 11/08/23 15:58 541-73-11.0 1
1,4-Dichlorobenzene ND ug/L 11/08/23 15:58 106-46-71.0 1
Dichlorodifluoromethane ND ug/L 11/08/23 15:58 75-71-8 v21.0 1
1,1-Dichloroethane ND ug/L 11/08/23 15:58 75-34-31.0 1
1,2-Dichloroethane ND ug/L 11/08/23 15:58 107-06-21.0 1
1,1-Dichloroethene ND ug/L 11/08/23 15:58 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 11/08/23 15:58 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 11/08/23 15:58 156-60-51.0 1
1,2-Dichloropropane ND ug/L 11/08/23 15:58 78-87-51.0 1
1,3-Dichloropropane ND ug/L 11/08/23 15:58 142-28-91.0 1
2,2-Dichloropropane ND ug/L 11/08/23 15:58 594-20-71.0 1
1,1-Dichloropropene ND ug/L 11/08/23 15:58 563-58-61.0 1
cis-1,3-Dichloropropene ND ug/L 11/08/23 15:58 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 11/08/23 15:58 10061-02-61.0 1
Diisopropyl ether ND ug/L 11/08/23 15:58 108-20-31.0 1
Ethylbenzene ND ug/L 11/08/23 15:58 100-41-41.0 1
Hexachloro-1,3-butadiene ND ug/L 11/08/23 15:58 87-68-32.0 1
2-Hexanone ND ug/L 11/08/23 15:58 591-78-65.0 1
p-Isopropyltoluene ND ug/L 11/08/23 15:58 99-87-61.0 1
Methylene Chloride ND ug/L 11/08/23 15:58 75-09-25.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 11/08/23 15:58 108-10-15.0 1
Methyl-tert-butyl ether ND ug/L 11/08/23 15:58 1634-04-41.0 1
Naphthalene ND ug/L 11/08/23 15:58 91-20-31.0 1
Styrene ND ug/L 11/08/23 15:58 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 11/08/23 15:58 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 11/08/23 15:58 79-34-51.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/20/2023 08:39 AM
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2225 Riverside Dr.
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Page 33 of 99
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92696513
Sludge LF November 2023
Sample:TRIP BLANK Lab ID:92696513007 Collected:11/02/23 09:00 Received:11/02/23 16:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualPQL
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level Landfill
Tetrachloroethene ND ug/L 11/08/23 15:58 127-18-41.0 1
Toluene ND ug/L 11/08/23 15:58 108-88-31.0 1
1,2,3-Trichlorobenzene ND ug/L 11/08/23 15:58 87-61-61.0 1
1,2,4-Trichlorobenzene ND ug/L 11/08/23 15:58 120-82-11.0 1
1,1,1-Trichloroethane ND ug/L 11/08/23 15:58 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 11/08/23 15:58 79-00-51.0 1
Trichloroethene ND ug/L 11/08/23 15:58 79-01-61.0 1
Trichlorofluoromethane ND ug/L 11/08/23 15:58 75-69-4 v21.0 1
1,2,3-Trichloropropane ND ug/L 11/08/23 15:58 96-18-41.0 1
Vinyl acetate ND ug/L 11/08/23 15:58 108-05-42.0 1
Vinyl chloride ND ug/L 11/08/23 15:58 75-01-41.0 1
Xylene (Total)ND ug/L 11/08/23 15:58 1330-20-71.0 1
m&p-Xylene ND ug/L 11/08/23 15:58 179601-23-12.0 1
o-Xylene ND ug/L 11/08/23 15:58 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)94 %11/08/23 15:58 460-00-470-130 1
1,2-Dichloroethane-d4 (S)107 %11/08/23 15:58 17060-07-070-130 1
Toluene-d8 (S)95 %11/08/23 15:58 2037-26-570-130 1
Analytical Method: EPA 8260D Mod.
Pace Analytical Services - Charlotte
8260D MSV SIM
1,4-Dioxane (p-Dioxane)ND ug/L 11/06/23 09:28 123-91-12.0 1
Surrogates
1,2-Dichloroethane-d4 (S)87 %11/06/23 09:28 17060-07-067-130 1
Toluene-d8 (S)122 %11/06/23 09:28 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/20/2023 08:39 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 34 of 99
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92696513
Sludge LF November 2023
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
810885
EPA 3010A
EPA 6010D
6010 MET
Laboratory:Pace Analytical Services - Asheville
Associated Lab Samples:92696513001, 92696513002, 92696513003, 92696513004, 92696513005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4198298
Associated Lab Samples:92696513001, 92696513002, 92696513003, 92696513004, 92696513005
Matrix:Water
Analyzed
Antimony ug/L ND 5.0 11/04/23 19:50
Arsenic ug/L ND 10.0 11/04/23 19:50
Barium ug/L ND 5.0 11/04/23 19:50
Cadmium ug/L ND 1.0 11/04/23 19:50
Calcium ug/L ND 100 11/04/23 19:50
Chromium ug/L ND 5.0 11/04/23 19:50
Cobalt ug/L ND 5.0 11/04/23 19:50
Copper ug/L ND 5.0 11/04/23 19:50
Lead ug/L ND 5.0 11/04/23 19:50
Magnesium ug/L ND 100 11/04/23 19:50
Nickel ug/L ND 5.0 11/04/23 19:50
Potassium ug/L ND 5000 11/04/23 19:50
Selenium ug/L ND 10.0 11/04/23 19:50
Silver ug/L ND 5.0 11/04/23 19:50
Sodium ug/L ND 5000 11/04/23 19:50
Thallium ug/L ND 10.0 11/04/23 19:50
Vanadium ug/L ND 5.0 11/04/23 19:50
Zinc ug/L ND 10.0 11/04/23 19:50
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4198299LABORATORY CONTROL SAMPLE:
LCSSpike
Antimony ug/L 516500 103 80-120
Arsenic ug/L 515500 103 80-120
Barium ug/L 517500 103 80-120
Cadmium ug/L 539500 108 80-120
Calcium ug/L 54205000 108 80-120
Chromium ug/L 510500 102 80-120
Cobalt ug/L 534500 107 80-120
Copper ug/L 523500 105 80-120
Lead ug/L 530500 106 80-120
Magnesium ug/L 51605000 103 80-120
Nickel ug/L 528500 106 80-120
Potassium ug/L 54005000 108 80-120
Selenium ug/L 513500 103 80-120
Silver ug/L 257250 103 80-120
Sodium ug/L 53805000 108 80-120
Thallium ug/L 518500 104 80-120
Vanadium ug/L 519500 104 80-120
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/20/2023 08:39 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 35 of 99
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92696513
Sludge LF November 2023
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4198299LABORATORY CONTROL SAMPLE:
LCSSpike
Zinc ug/L 546500 109 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4198300MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92696481001
4198301
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Antimony ug/L 500 107 75-125107 0500ND534536
Arsenic ug/L 500 106 75-125106 05006.3J 536 537
Barium ug/L 500 102 75-125103 150081.1 590 597
Cadmium ug/L 500 107 75-125106 1500ND536531
Calcium ug/L M150004375-125100 35000103000105000108000
Chromium ug/L 500 101 75-125101 0500ND506507
Cobalt ug/L 500 105 75-125105 0500ND527527
Copper ug/L 500 107 75-125108 0500ND537539
Lead ug/L 500 105 75-125104 0500ND524522
Magnesium ug/L 5000 97 75-125112 35000214002620027000
Nickel ug/L 500 103 75-125103 0500ND517515
Potassium ug/L 5000 102 75-125109 2500085201360014000
Selenium ug/L 500 108 75-125108 0500ND542541
Silver ug/L 250 106 75-125106 0250ND264265
Sodium ug/L 5000 81 75-12595 25000241002820028900
Thallium ug/L 500 103 75-125102 1500ND517512
Vanadium ug/L 500 105 75-125105 0500ND524525
Zinc ug/L 500 108 75-125107 0500ND538537
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/20/2023 08:39 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 36 of 99
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92696513
Sludge LF November 2023
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
811264
EPA 8260D
EPA 8260D
8260D MSV Low Level Landfill
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92696513001, 92696513002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4200215
Associated Lab Samples:92696513001, 92696513002
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 1.0 11/06/23 21:59
1,1,1-Trichloroethane ug/L ND 1.0 11/06/23 21:59
1,1,2,2-Tetrachloroethane ug/L ND 1.0 11/06/23 21:59
1,1,2-Trichloroethane ug/L ND 1.0 11/06/23 21:59
1,1-Dichloroethane ug/L ND 1.0 11/06/23 21:59
1,1-Dichloroethene ug/L ND 1.0 11/06/23 21:59
1,1-Dichloropropene ug/L ND 1.0 11/06/23 21:59
1,2,3-Trichlorobenzene ug/L ND 1.0 11/06/23 21:59
1,2,3-Trichloropropane ug/L ND 1.0 11/06/23 21:59
1,2,4-Trichlorobenzene ug/L ND 1.0 11/06/23 21:59
1,2-Dibromo-3-chloropropane ug/L ND 2.0 11/06/23 21:59
1,2-Dibromoethane (EDB)ug/L ND 1.0 11/06/23 21:59
1,2-Dichlorobenzene ug/L ND 1.0 11/06/23 21:59
1,2-Dichloroethane ug/L ND 1.0 11/06/23 21:59
1,2-Dichloropropane ug/L ND 1.0 11/06/23 21:59
1,3-Dichlorobenzene ug/L ND 1.0 11/06/23 21:59
1,3-Dichloropropane ug/L ND 1.0 11/06/23 21:59
1,4-Dichlorobenzene ug/L ND 1.0 11/06/23 21:59
2,2-Dichloropropane ug/L ND 1.0 11/06/23 21:59
2-Butanone (MEK)ug/L ND 5.0 11/06/23 21:59
2-Chlorotoluene ug/L ND 1.0 11/06/23 21:59
2-Hexanone ug/L ND 5.0 11/06/23 21:59
4-Chlorotoluene ug/L ND 1.0 11/06/23 21:59
4-Methyl-2-pentanone (MIBK)ug/L ND 5.0 11/06/23 21:59
Acetone ug/L ND 25.0 11/06/23 21:59
Benzene ug/L ND 1.0 11/06/23 21:59
Bromobenzene ug/L ND 1.0 11/06/23 21:59
Bromochloromethane ug/L ND 1.0 11/06/23 21:59
Bromodichloromethane ug/L ND 1.0 11/06/23 21:59
Bromoform ug/L ND 1.0 11/06/23 21:59
Bromomethane ug/L ND 2.0 11/06/23 21:59
Carbon tetrachloride ug/L ND 1.0 11/06/23 21:59
Chlorobenzene ug/L ND 1.0 11/06/23 21:59
Chloroethane ug/L ND 1.0 11/06/23 21:59
Chloroform ug/L ND 1.0 11/06/23 21:59
Chloromethane ug/L ND 1.0 11/06/23 21:59
cis-1,2-Dichloroethene ug/L ND 1.0 11/06/23 21:59
cis-1,3-Dichloropropene ug/L ND 1.0 11/06/23 21:59
Dibromochloromethane ug/L ND 1.0 11/06/23 21:59
Dibromomethane ug/L ND 1.0 11/06/23 21:59
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/20/2023 08:39 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 37 of 99
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92696513
Sludge LF November 2023
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4200215
Associated Lab Samples:92696513001, 92696513002
Matrix:Water
Analyzed
Dichlorodifluoromethane ug/L ND 1.0 11/06/23 21:59
Diisopropyl ether ug/L ND 1.0 11/06/23 21:59
Ethylbenzene ug/L ND 1.0 11/06/23 21:59
Hexachloro-1,3-butadiene ug/L ND 2.0 11/06/23 21:59
m&p-Xylene ug/L ND 2.0 11/06/23 21:59
Methyl-tert-butyl ether ug/L ND 1.0 11/06/23 21:59
Methylene Chloride ug/L ND 5.0 11/06/23 21:59
Naphthalene ug/L ND 1.0 11/06/23 21:59
o-Xylene ug/L ND 1.0 11/06/23 21:59
p-Isopropyltoluene ug/L ND 1.0 11/06/23 21:59
Styrene ug/L ND 1.0 11/06/23 21:59
Tetrachloroethene ug/L ND 1.0 11/06/23 21:59
Toluene ug/L ND 1.0 11/06/23 21:59
trans-1,2-Dichloroethene ug/L ND 1.0 11/06/23 21:59
trans-1,3-Dichloropropene ug/L ND 1.0 11/06/23 21:59
Trichloroethene ug/L ND 1.0 11/06/23 21:59
Trichlorofluoromethane ug/L ND 1.0 11/06/23 21:59
Vinyl acetate ug/L ND 2.0 11/06/23 21:59
Vinyl chloride ug/L ND 1.0 11/06/23 21:59
Xylene (Total)ug/L ND 1.0 11/06/23 21:59
1,2-Dichloroethane-d4 (S)%107 70-130 11/06/23 21:59
4-Bromofluorobenzene (S)%100 70-130 11/06/23 21:59
Toluene-d8 (S)%101 70-130 11/06/23 21:59
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4200216LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 20.720 103 70-130
1,1,1-Trichloroethane ug/L 20.920 105 70-130
1,1,2,2-Tetrachloroethane ug/L 20.020 100 70-130
1,1,2-Trichloroethane ug/L 19.120 95 70-130
1,1-Dichloroethane ug/L 20.520 102 70-130
1,1-Dichloroethene ug/L 21.220 106 69-131
1,1-Dichloropropene ug/L 21.920 109 70-132
1,2,3-Trichlorobenzene ug/L 19.520 97 70-132
1,2,3-Trichloropropane ug/L 19.620 98 70-130
1,2,4-Trichlorobenzene ug/L 19.520 97 70-130
1,2-Dibromo-3-chloropropane ug/L 17.320 86 70-130
1,2-Dibromoethane (EDB)ug/L 19.220 96 70-130
1,2-Dichlorobenzene ug/L 19.820 99 70-130
1,2-Dichloroethane ug/L 19.720 99 70-130
1,2-Dichloropropane ug/L 19.920 99 70-130
1,3-Dichlorobenzene ug/L 20.320 102 70-130
1,3-Dichloropropane ug/L 18.720 93 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/20/2023 08:39 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 38 of 99
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92696513
Sludge LF November 2023
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4200216LABORATORY CONTROL SAMPLE:
LCSSpike
1,4-Dichlorobenzene ug/L 19.920 100 70-130
2,2-Dichloropropane ug/L 19.620 98 69-130
2-Butanone (MEK)ug/L 36.940 92 67-133
2-Chlorotoluene ug/L 19.920 99 70-130
2-Hexanone ug/L 36.240 90 70-133
4-Chlorotoluene ug/L 20.020 100 70-130
4-Methyl-2-pentanone (MIBK)ug/L 35.940 90 70-130
Acetone ug/L 35.640 89 67-130
Benzene ug/L 19.920 99 70-130
Bromobenzene ug/L 19.520 97 70-130
Bromochloromethane ug/L 19.720 98 70-130
Bromodichloromethane ug/L 20.020 100 70-130
Bromoform ug/L 19.620 98 70-133
Bromomethane ug/L 21.920 109 41-148
Carbon tetrachloride ug/L 21.120 106 70-130
Chlorobenzene ug/L 20.220 101 70-130
Chloroethane ug/L 24.020 120 41-157
Chloroform ug/L 20.520 102 70-130
Chloromethane ug/L 23.220 116 59-141
cis-1,2-Dichloroethene ug/L 20.720 103 70-130
cis-1,3-Dichloropropene ug/L 19.520 98 70-130
Dibromochloromethane ug/L 20.020 100 70-130
Dibromomethane ug/L 18.520 92 70-130
Dichlorodifluoromethane ug/L 23.720 118 54-147
Diisopropyl ether ug/L 19.120 96 70-130
Ethylbenzene ug/L 20.220 101 70-130
Hexachloro-1,3-butadiene ug/L 20.120 101 70-134
m&p-Xylene ug/L 40.740 102 70-130
Methyl-tert-butyl ether ug/L 18.220 91 70-130
Methylene Chloride ug/L 20.620 103 62-130
Naphthalene ug/L 19.820 99 70-135
o-Xylene ug/L 20.020 100 70-130
p-Isopropyltoluene ug/L 20.720 103 70-130
Styrene ug/L 20.320 101 70-130
Tetrachloroethene ug/L 18.820 94 70-130
Toluene ug/L 19.720 98 70-130
trans-1,2-Dichloroethene ug/L 20.420 102 70-130
trans-1,3-Dichloropropene ug/L 19.020 95 70-130
Trichloroethene ug/L 19.820 99 70-130
Trichlorofluoromethane ug/L 21.420 107 57-130
Vinyl acetate ug/L 39.840 100 70-141
Vinyl chloride ug/L 21.520 107 66-140
Xylene (Total)ug/L 60.660 101 70-130
1,2-Dichloroethane-d4 (S)%107 70-130
4-Bromofluorobenzene (S)%102 70-130
Toluene-d8 (S)%101 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/20/2023 08:39 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 39 of 99
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92696513
Sludge LF November 2023
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
4200218MATRIX SPIKE SAMPLE:
MSSpike
Result
92696513002
1,1,1,2-Tetrachloroethane ug/L 22.920 115 70-146ND
1,1,1-Trichloroethane ug/L 25.020 125 70-150ND
1,1,2,2-Tetrachloroethane ug/L 21.420 107 66-144ND
1,1,2-Trichloroethane ug/L 21.020 105 70-142ND
1,1-Dichloroethane ug/L 24.120 121 68-150ND
1,1-Dichloroethene ug/L 25.120 125 64-162ND
1,1-Dichloropropene ug/L 25.020 125 70-160ND
1,2,3-Trichlorobenzene ug/L 22.120 111 66-151ND
1,2,3-Trichloropropane ug/L 20.220 101 66-144ND
1,2,4-Trichlorobenzene ug/L 22.320 111 69-147ND
1,2-Dibromo-3-chloropropane ug/L 18.020 90 62-146ND
1,2-Dibromoethane (EDB)ug/L 21.120 105 70-143ND
1,2-Dichlorobenzene ug/L 22.220 111 70-142ND
1,2-Dichloroethane ug/L 22.220 111 68-145ND
1,2-Dichloropropane ug/L 22.320 112 70-144ND
1,3-Dichlorobenzene ug/L 22.620 113 70-142ND
1,3-Dichloropropane ug/L 20.720 104 70-141ND
1,4-Dichlorobenzene ug/L 22.620 113 70-140ND
2,2-Dichloropropane ug/L 25.520 127 58-160ND
2-Butanone (MEK)ug/L 36.040 90 57-156ND
2-Chlorotoluene ug/L 23.020 115 70-148ND
2-Hexanone ug/L 36.340 91 62-153ND
4-Chlorotoluene ug/L 22.720 113 70-144ND
4-Methyl-2-pentanone (MIBK)ug/L 36.440 91 65-144ND
Acetone ug/L 35.740 89 49-162ND
Benzene ug/L 23.020 115 68-144ND
Bromobenzene ug/L 21.620 108 70-144ND
Bromochloromethane ug/L 21.620 108 70-148ND
Bromodichloromethane ug/L 22.820 114 70-141ND
Bromoform ug/L 20.620 103 59-144ND
Bromomethane ug/L 29.520 147 23-190ND
Carbon tetrachloride ug/L 24.620 123 70-147ND
Chlorobenzene ug/L 22.820 114 70-143ND
Chloroethane ug/L 27.620 138 55-190ND
Chloroform ug/L 23.720 118 67-148ND
Chloromethane ug/L 28.0 v32014038-180ND
cis-1,2-Dichloroethene ug/L 23.620 118 67-151ND
cis-1,3-Dichloropropene ug/L 22.020 110 70-142ND
Dibromochloromethane ug/L 22.020 110 68-140ND
Dibromomethane ug/L 20.120 101 70-142ND
Dichlorodifluoromethane ug/L 28.9 v32014515-200ND
Diisopropyl ether ug/L 21.620 108 62-149ND
Ethylbenzene ug/L 22.920 114 70-145ND
Hexachloro-1,3-butadiene ug/L 24.120 120 64-164ND
m&p-Xylene ug/L 46.040 115 70-148ND
Methyl-tert-butyl ether ug/L 19.920 100 64-146ND
Methylene Chloride ug/L 23.120 115 54-149ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/20/2023 08:39 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 40 of 99
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92696513
Sludge LF November 2023
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
4200218MATRIX SPIKE SAMPLE:
MSSpike
Result
92696513002
Naphthalene ug/L 21.320 107 62-154ND
o-Xylene ug/L 22.520 112 70-145ND
p-Isopropyltoluene ug/L 24.220 121 70-153ND
Styrene ug/L 22.220 111 70-147ND
Tetrachloroethene ug/L 21.420 107 70-145ND
Toluene ug/L 22.220 111 65-146ND
trans-1,2-Dichloroethene ug/L 25.420 127 69-155ND
trans-1,3-Dichloropropene ug/L 21.920 109 70-142ND
Trichloroethene ug/L 23.220 116 70-152ND
Trichlorofluoromethane ug/L 25.820 129 60-158ND
Vinyl acetate ug/L 43.840 110 56-157ND
Vinyl chloride ug/L 25.4 v32012751-178ND
Xylene (Total)ug/L 68.560 114 70-146ND
1,2-Dichloroethane-d4 (S)%103 70-130
4-Bromofluorobenzene (S)%101 70-130
Toluene-d8 (S)%102 70-130
Parameter Units
Dup
Result QualifiersRPDResult
92696585014
4200217SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/L NDND
1,1,1-Trichloroethane ug/L NDND
1,1,2,2-Tetrachloroethane ug/L NDND
1,1,2-Trichloroethane ug/L NDND
1,1-Dichloroethane ug/L NDND
1,1-Dichloroethene ug/L NDND
1,1-Dichloropropene ug/L NDND
1,2,3-Trichlorobenzene ug/L NDND
1,2,3-Trichloropropane ug/L NDND
1,2,4-Trichlorobenzene ug/L NDND
1,2-Dibromo-3-chloropropane ug/L NDND
1,2-Dibromoethane (EDB)ug/L NDND
1,2-Dichlorobenzene ug/L NDND
1,2-Dichloroethane ug/L NDND
1,2-Dichloropropane ug/L NDND
1,3-Dichlorobenzene ug/L NDND
1,3-Dichloropropane ug/L NDND
1,4-Dichlorobenzene ug/L NDND
2,2-Dichloropropane ug/L NDND
2-Butanone (MEK)ug/L NDND
2-Chlorotoluene ug/L NDND
2-Hexanone ug/L NDND
4-Chlorotoluene ug/L NDND
4-Methyl-2-pentanone (MIBK)ug/L NDND
Acetone ug/L NDND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/20/2023 08:39 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 41 of 99
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92696513
Sludge LF November 2023
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92696585014
4200217SAMPLE DUPLICATE:
Benzene ug/L NDND
Bromobenzene ug/L NDND
Bromochloromethane ug/L NDND
Bromodichloromethane ug/L NDND
Bromoform ug/L NDND
Bromomethane ug/L NDND
Carbon tetrachloride ug/L NDND
Chlorobenzene ug/L NDND
Chloroethane ug/L NDND
Chloroform ug/L NDND
Chloromethane ug/L NDND
cis-1,2-Dichloroethene ug/L NDND
cis-1,3-Dichloropropene ug/L NDND
Dibromochloromethane ug/L NDND
Dibromomethane ug/L NDND
Dichlorodifluoromethane ug/L NDND
Diisopropyl ether ug/L NDND
Ethylbenzene ug/L NDND
Hexachloro-1,3-butadiene ug/L NDND
m&p-Xylene ug/L NDND
Methyl-tert-butyl ether ug/L NDND
Methylene Chloride ug/L NDND
Naphthalene ug/L NDND
o-Xylene ug/L NDND
p-Isopropyltoluene ug/L NDND
Styrene ug/L NDND
Tetrachloroethene ug/L NDND
Toluene ug/L NDND
trans-1,2-Dichloroethene ug/L NDND
trans-1,3-Dichloropropene ug/L NDND
Trichloroethene ug/L NDND
Trichlorofluoromethane ug/L NDND
Vinyl acetate ug/L NDND
Vinyl chloride ug/L NDND
Xylene (Total)ug/L NDND
1,2-Dichloroethane-d4 (S)%103114
4-Bromofluorobenzene (S)%101101
Toluene-d8 (S)%102104
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/20/2023 08:39 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 42 of 99
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92696513
Sludge LF November 2023
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
811863
EPA 8260D
EPA 8260D
8260D MSV Low Level Landfill
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92696513003, 92696513004, 92696513005, 92696513007
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4203421
Associated Lab Samples:92696513003, 92696513004, 92696513005, 92696513007
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 1.0 11/08/23 15:23
1,1,1-Trichloroethane ug/L ND 1.0 11/08/23 15:23
1,1,2,2-Tetrachloroethane ug/L ND 1.0 11/08/23 15:23
1,1,2-Trichloroethane ug/L ND 1.0 11/08/23 15:23
1,1-Dichloroethane ug/L ND 1.0 11/08/23 15:23
1,1-Dichloroethene ug/L ND 1.0 11/08/23 15:23
1,1-Dichloropropene ug/L ND 1.0 11/08/23 15:23
1,2,3-Trichlorobenzene ug/L ND 1.0 11/08/23 15:23
1,2,3-Trichloropropane ug/L ND 1.0 11/08/23 15:23
1,2,4-Trichlorobenzene ug/L ND 1.0 11/08/23 15:23
1,2-Dibromo-3-chloropropane ug/L ND 2.0 11/08/23 15:23
1,2-Dibromoethane (EDB)ug/L ND 1.0 11/08/23 15:23
1,2-Dichlorobenzene ug/L ND 1.0 11/08/23 15:23
1,2-Dichloroethane ug/L ND 1.0 11/08/23 15:23
1,2-Dichloropropane ug/L ND 1.0 11/08/23 15:23
1,3-Dichlorobenzene ug/L ND 1.0 11/08/23 15:23
1,3-Dichloropropane ug/L ND 1.0 11/08/23 15:23
1,4-Dichlorobenzene ug/L ND 1.0 11/08/23 15:23
2,2-Dichloropropane ug/L ND 1.0 11/08/23 15:23
2-Butanone (MEK)ug/L ND 5.0 11/08/23 15:23
2-Chlorotoluene ug/L ND 1.0 11/08/23 15:23
2-Hexanone ug/L ND 5.0 11/08/23 15:23
4-Chlorotoluene ug/L ND 1.0 11/08/23 15:23
4-Methyl-2-pentanone (MIBK)ug/L ND 5.0 11/08/23 15:23
Acetone ug/L ND 25.0 11/08/23 15:23
Benzene ug/L ND 1.0 11/08/23 15:23
Bromobenzene ug/L ND 1.0 11/08/23 15:23
Bromochloromethane ug/L ND 1.0 11/08/23 15:23
Bromodichloromethane ug/L ND 1.0 11/08/23 15:23
Bromoform ug/L ND 1.0 11/08/23 15:23
Bromomethane ug/L ND 2.0 11/08/23 15:23
Carbon tetrachloride ug/L ND 1.0 11/08/23 15:23
Chlorobenzene ug/L ND 1.0 11/08/23 15:23
Chloroethane ug/L ND 1.0 11/08/23 15:23
Chloroform ug/L ND 1.0 11/08/23 15:23
Chloromethane ug/L ND 1.0 11/08/23 15:23
cis-1,2-Dichloroethene ug/L ND 1.0 11/08/23 15:23
cis-1,3-Dichloropropene ug/L ND 1.0 11/08/23 15:23
Dibromochloromethane ug/L ND 1.0 11/08/23 15:23
Dibromomethane ug/L ND 1.0 11/08/23 15:23
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/20/2023 08:39 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 43 of 99
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92696513
Sludge LF November 2023
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4203421
Associated Lab Samples:92696513003, 92696513004, 92696513005, 92696513007
Matrix:Water
Analyzed
Dichlorodifluoromethane ug/L ND 1.0 v211/08/23 15:23
Diisopropyl ether ug/L ND 1.0 11/08/23 15:23
Ethylbenzene ug/L ND 1.0 11/08/23 15:23
Hexachloro-1,3-butadiene ug/L ND 2.0 11/08/23 15:23
m&p-Xylene ug/L ND 2.0 11/08/23 15:23
Methyl-tert-butyl ether ug/L ND 1.0 11/08/23 15:23
Methylene Chloride ug/L ND 5.0 11/08/23 15:23
Naphthalene ug/L ND 1.0 11/08/23 15:23
o-Xylene ug/L ND 1.0 11/08/23 15:23
p-Isopropyltoluene ug/L ND 1.0 11/08/23 15:23
Styrene ug/L ND 1.0 11/08/23 15:23
Tetrachloroethene ug/L ND 1.0 11/08/23 15:23
Toluene ug/L ND 1.0 11/08/23 15:23
trans-1,2-Dichloroethene ug/L ND 1.0 11/08/23 15:23
trans-1,3-Dichloropropene ug/L ND 1.0 11/08/23 15:23
Trichloroethene ug/L ND 1.0 11/08/23 15:23
Trichlorofluoromethane ug/L ND 1.0 v211/08/23 15:23
Vinyl acetate ug/L ND 2.0 11/08/23 15:23
Vinyl chloride ug/L ND 1.0 11/08/23 15:23
Xylene (Total)ug/L ND 1.0 11/08/23 15:23
1,2-Dichloroethane-d4 (S)%107 70-130 11/08/23 15:23
4-Bromofluorobenzene (S)%95 70-130 11/08/23 15:23
Toluene-d8 (S)%95 70-130 11/08/23 15:23
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4203422LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 18.920 95 70-130
1,1,1-Trichloroethane ug/L 17.920 90 70-130
1,1,2,2-Tetrachloroethane ug/L 20.720 104 70-130
1,1,2-Trichloroethane ug/L 19.620 98 70-130
1,1-Dichloroethane ug/L 18.120 90 70-130
1,1-Dichloroethene ug/L 18.120 90 69-131
1,1-Dichloropropene ug/L 18.920 94 70-132
1,2,3-Trichlorobenzene ug/L 18.620 93 70-132
1,2,3-Trichloropropane ug/L 19.620 98 70-130
1,2,4-Trichlorobenzene ug/L 19.420 97 70-130
1,2-Dibromo-3-chloropropane ug/L 19.020 95 70-130
1,2-Dibromoethane (EDB)ug/L 18.820 94 70-130
1,2-Dichlorobenzene ug/L 20.020 100 70-130
1,2-Dichloroethane ug/L 18.520 93 70-130
1,2-Dichloropropane ug/L 18.620 93 70-130
1,3-Dichlorobenzene ug/L 19.720 99 70-130
1,3-Dichloropropane ug/L 18.120 90 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/20/2023 08:39 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 44 of 99
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92696513
Sludge LF November 2023
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4203422LABORATORY CONTROL SAMPLE:
LCSSpike
1,4-Dichlorobenzene ug/L 19.920 99 70-130
2,2-Dichloropropane ug/L 18.220 91 69-130
2-Butanone (MEK)ug/L 34.740 87 67-133
2-Chlorotoluene ug/L 19.320 96 70-130
2-Hexanone ug/L 37.540 94 70-133
4-Chlorotoluene ug/L 19.420 97 70-130
4-Methyl-2-pentanone (MIBK)ug/L 37.240 93 70-130
Acetone ug/L 37.040 92 67-130
Benzene ug/L 18.420 92 70-130
Bromobenzene ug/L 18.520 93 70-130
Bromochloromethane ug/L 19.420 97 70-130
Bromodichloromethane ug/L 17.820 89 70-130
Bromoform ug/L 18.620 93 70-133
Bromomethane ug/L 13.120 66 41-148
Carbon tetrachloride ug/L 17.420 87 70-130
Chlorobenzene ug/L 19.120 96 70-130
Chloroethane ug/L 19.720 99 41-157
Chloroform ug/L 16.620 83 70-130
Chloromethane ug/L 25.320 127 59-141
cis-1,2-Dichloroethene ug/L 18.120 90 70-130
cis-1,3-Dichloropropene ug/L 19.020 95 70-130
Dibromochloromethane ug/L 18.320 92 70-130
Dibromomethane ug/L 19.020 95 70-130
Dichlorodifluoromethane ug/L 22.4 v32011254-147
Diisopropyl ether ug/L 17.920 90 70-130
Ethylbenzene ug/L 18.620 93 70-130
Hexachloro-1,3-butadiene ug/L 20.320 102 70-134
m&p-Xylene ug/L 38.040 95 70-130
Methyl-tert-butyl ether ug/L 17.220 86 70-130
Methylene Chloride ug/L 20.120 101 62-130
Naphthalene ug/L 18.720 93 70-135
o-Xylene ug/L 20.120 101 70-130
p-Isopropyltoluene ug/L 20.120 100 70-130
Styrene ug/L 19.920 99 70-130
Tetrachloroethene ug/L 17.520 87 70-130
Toluene ug/L 18.920 94 70-130
trans-1,2-Dichloroethene ug/L 17.820 89 70-130
trans-1,3-Dichloropropene ug/L 19.420 97 70-130
Trichloroethene ug/L 18.320 92 70-130
Trichlorofluoromethane ug/L 19.6 v3209857-130
Vinyl acetate ug/L 37.940 95 70-141
Vinyl chloride ug/L 19.020 95 66-140
Xylene (Total)ug/L 58.160 97 70-130
1,2-Dichloroethane-d4 (S)%101 70-130
4-Bromofluorobenzene (S)%102 70-130
Toluene-d8 (S)%104 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/20/2023 08:39 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 45 of 99
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92696513
Sludge LF November 2023
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
4203424MATRIX SPIKE SAMPLE:
MSSpike
Result
92696890003
1,1,1,2-Tetrachloroethane ug/L 21.420 107 70-146ND
1,1,1-Trichloroethane ug/L 24.120 121 70-150ND
1,1,2,2-Tetrachloroethane ug/L 21.920 110 66-144ND
1,1,2-Trichloroethane ug/L 21.420 107 70-142ND
1,1-Dichloroethane ug/L 23.620 118 68-150ND
1,1-Dichloroethene ug/L 25.420 127 64-162ND
1,1-Dichloropropene ug/L 24.520 122 70-160ND
1,2,3-Trichlorobenzene ug/L 20.520 103 66-151ND
1,2,3-Trichloropropane ug/L 21.020 105 66-144ND
1,2,4-Trichlorobenzene ug/L 21.220 106 69-147ND
1,2-Dibromo-3-chloropropane ug/L 20.120 101 62-146ND
1,2-Dibromoethane (EDB)ug/L 20.820 104 70-143ND
1,2-Dichlorobenzene ug/L 22.320 112 70-142ND
1,2-Dichloroethane ug/L 22.720 113 68-145ND
1,2-Dichloropropane ug/L 23.020 115 70-144ND
1,3-Dichlorobenzene ug/L 22.420 112 70-142ND
1,3-Dichloropropane ug/L 21.120 105 70-141ND
1,4-Dichlorobenzene ug/L 21.620 108 70-140ND
2,2-Dichloropropane ug/L 23.120 115 58-160ND
2-Butanone (MEK)ug/L 46.140 115 57-156ND
2-Chlorotoluene ug/L 22.520 112 70-148ND
2-Hexanone ug/L 45.840 115 62-153ND
4-Chlorotoluene ug/L 22.720 114 70-144ND
4-Methyl-2-pentanone (MIBK)ug/L 45.140 113 65-144ND
Acetone ug/L 44.840 112 49-162ND
Benzene ug/L 23.320 116 68-144ND
Bromobenzene ug/L 21.920 109 70-144ND
Bromochloromethane ug/L 22.620 113 70-148ND
Bromodichloromethane ug/L 21.820 109 70-141ND
Bromoform ug/L 20.220 101 59-144ND
Bromomethane ug/L 16.020 80 23-190ND
Carbon tetrachloride ug/L 23.820 119 70-147ND
Chlorobenzene ug/L 22.320 111 70-143ND
Chloroethane ug/L 25.220 126 55-190ND
Chloroform ug/L 22.620 113 67-148ND
Chloromethane ug/L 29.7 v12014838-180ND
cis-1,2-Dichloroethene ug/L 23.520 117 67-151ND
cis-1,3-Dichloropropene ug/L 21.220 106 70-142ND
Dibromochloromethane ug/L 20.020 100 68-140ND
Dibromomethane ug/L 21.220 106 70-142ND
Dichlorodifluoromethane ug/L 25.920 129 15-200ND
Diisopropyl ether ug/L 23.020 115 62-149ND
Ethylbenzene ug/L 22.720 114 70-145ND
Hexachloro-1,3-butadiene ug/L 22.120 111 64-164ND
m&p-Xylene ug/L 44.940 112 70-148ND
Methyl-tert-butyl ether ug/L 19.220 96 64-146ND
Methylene Chloride ug/L 25.720 128 54-149ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/20/2023 08:39 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 46 of 99
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92696513
Sludge LF November 2023
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
4203424MATRIX SPIKE SAMPLE:
MSSpike
Result
92696890003
Naphthalene ug/L 22.420 112 62-154ND
o-Xylene ug/L 21.920 110 70-145ND
p-Isopropyltoluene ug/L 23.620 118 70-153ND
Styrene ug/L 22.120 110 70-147ND
Tetrachloroethene ug/L 22.820 114 70-145ND
Toluene ug/L 22.320 111 65-146ND
trans-1,2-Dichloroethene ug/L 23.920 120 69-155ND
trans-1,3-Dichloropropene ug/L 21.720 108 70-142ND
Trichloroethene ug/L 21.520 108 70-152ND
Trichlorofluoromethane ug/L 25.720 129 60-158ND
Vinyl acetate ug/L 38.340 96 56-157ND
Vinyl chloride ug/L 23.820 119 51-178ND
Xylene (Total)ug/L 66.960 111 70-146ND
1,2-Dichloroethane-d4 (S)%104 70-130
4-Bromofluorobenzene (S)%99 70-130
Toluene-d8 (S)%101 70-130
Parameter Units
Dup
Result QualifiersRPDResult
92696890001
4203423SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/L NDND
1,1,1-Trichloroethane ug/L NDND
1,1,2,2-Tetrachloroethane ug/L NDND
1,1,2-Trichloroethane ug/L NDND
1,1-Dichloroethane ug/L NDND
1,1-Dichloroethene ug/L NDND
1,1-Dichloropropene ug/L NDND
1,2,3-Trichlorobenzene ug/L NDND
1,2,3-Trichloropropane ug/L NDND
1,2,4-Trichlorobenzene ug/L NDND
1,2-Dibromo-3-chloropropane ug/L NDND
1,2-Dibromoethane (EDB)ug/L NDND
1,2-Dichlorobenzene ug/L NDND
1,2-Dichloroethane ug/L NDND
1,2-Dichloropropane ug/L NDND
1,3-Dichlorobenzene ug/L NDND
1,3-Dichloropropane ug/L NDND
1,4-Dichlorobenzene ug/L NDND
2,2-Dichloropropane ug/L NDND
2-Butanone (MEK)ug/L NDND
2-Chlorotoluene ug/L NDND
2-Hexanone ug/L NDND
4-Chlorotoluene ug/L NDND
4-Methyl-2-pentanone (MIBK)ug/L NDND
Acetone ug/L NDND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/20/2023 08:39 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 47 of 99
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92696513
Sludge LF November 2023
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92696890001
4203423SAMPLE DUPLICATE:
Benzene ug/L NDND
Bromobenzene ug/L NDND
Bromochloromethane ug/L NDND
Bromodichloromethane ug/L NDND
Bromoform ug/L NDND
Bromomethane ug/L NDND
Carbon tetrachloride ug/L NDND
Chlorobenzene ug/L NDND
Chloroethane ug/L NDND
Chloroform ug/L NDND
Chloromethane ug/L ND v1ND
cis-1,2-Dichloroethene ug/L NDND
cis-1,3-Dichloropropene ug/L NDND
Dibromochloromethane ug/L NDND
Dibromomethane ug/L NDND
Dichlorodifluoromethane ug/L NDND
Diisopropyl ether ug/L NDND
Ethylbenzene ug/L NDND
Hexachloro-1,3-butadiene ug/L NDND
m&p-Xylene ug/L NDND
Methyl-tert-butyl ether ug/L NDND
Methylene Chloride ug/L NDND
Naphthalene ug/L NDND
o-Xylene ug/L NDND
p-Isopropyltoluene ug/L NDND
Styrene ug/L NDND
Tetrachloroethene ug/L NDND
Toluene ug/L NDND
trans-1,2-Dichloroethene ug/L NDND
trans-1,3-Dichloropropene ug/L NDND
Trichloroethene ug/L NDND
Trichlorofluoromethane ug/L NDND
Vinyl acetate ug/L NDND
Vinyl chloride ug/L NDND
Xylene (Total)ug/L NDND
1,2-Dichloroethane-d4 (S)%100105
4-Bromofluorobenzene (S)%10196
Toluene-d8 (S)%10696
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/20/2023 08:39 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 48 of 99
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92696513
Sludge LF November 2023
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
810909
EPA 8260D Mod.
EPA 8260D Mod.
8260D MSV SIM
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92696513001, 92696513002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4198471
Associated Lab Samples:92696513001, 92696513002
Matrix:Water
Analyzed
1,4-Dioxane (p-Dioxane)ug/L ND 2.0 11/03/23 17:00
1,2-Dichloroethane-d4 (S)%88 67-130 11/03/23 17:00
Toluene-d8 (S)%93 70-130 11/03/23 17:00
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4198472LABORATORY CONTROL SAMPLE:
LCSSpike
1,4-Dioxane (p-Dioxane)ug/L 21.720 109 70-130
1,2-Dichloroethane-d4 (S)%89 67-130
Toluene-d8 (S)%93 70-130
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4198473MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92696449001
4198474
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
1,4-Dioxane (p-Dioxane)ug/L 20 100 55-13798 220ND19.9 19.6
1,2-Dichloroethane-d4 (S)%90 67-13091
Toluene-d8 (S)%117 70-130100
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/20/2023 08:39 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 49 of 99
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92696513
Sludge LF November 2023
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
811131
EPA 8260D Mod.
EPA 8260D Mod.
8260D MSV SIM
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92696513007
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4199518
Associated Lab Samples:92696513007
Matrix:Water
Analyzed
1,4-Dioxane (p-Dioxane)ug/L ND 2.0 11/06/23 08:11
1,2-Dichloroethane-d4 (S)%85 67-130 11/06/23 08:11
Toluene-d8 (S)%111 70-130 11/06/23 08:11
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4199519LABORATORY CONTROL SAMPLE:
LCSSpike
1,4-Dioxane (p-Dioxane)ug/L 22.520 112 70-130
1,2-Dichloroethane-d4 (S)%90 67-130
Toluene-d8 (S)%117 70-130
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4199520MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92696756002
4199521
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
1,4-Dioxane (p-Dioxane)ug/L 20 103 55-137102 1204.8 25.4 25.1
1,2-Dichloroethane-d4 (S)%91 67-13093
Toluene-d8 (S)%112 70-130121
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/20/2023 08:39 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 50 of 99
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92696513
Sludge LF November 2023
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
811148
EPA 8260D Mod.
EPA 8260D Mod.
8260D MSV SIM
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92696513003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4199562
Associated Lab Samples:92696513003
Matrix:Water
Analyzed
1,4-Dioxane (p-Dioxane)ug/L ND 2.0 11/06/23 08:20
1,2-Dichloroethane-d4 (S)%90 67-130 11/06/23 08:20
Toluene-d8 (S)%95 70-130 11/06/23 08:20
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4199563LABORATORY CONTROL SAMPLE:
LCSSpike
1,4-Dioxane (p-Dioxane)ug/L 21.220 106 70-130
1,2-Dichloroethane-d4 (S)%89 67-130
Toluene-d8 (S)%95 70-130
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4199564MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92696795010
4199565
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
1,4-Dioxane (p-Dioxane)ug/L 20 107 55-137102 520ND21.3 20.4
1,2-Dichloroethane-d4 (S)%93 67-13091
Toluene-d8 (S)%95 70-13094
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/20/2023 08:39 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 51 of 99
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92696513
Sludge LF November 2023
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
811197
EPA 8260D Mod.
EPA 8260D Mod.
8260D MSV SIM
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92696513004, 92696513005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4199862
Associated Lab Samples:92696513004, 92696513005
Matrix:Water
Analyzed
1,4-Dioxane (p-Dioxane)ug/L ND 2.0 11/06/23 08:41
1,2-Dichloroethane-d4 (S)%90 67-130 11/06/23 08:41
Toluene-d8 (S)%96 70-130 11/06/23 08:41
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4199863LABORATORY CONTROL SAMPLE:
LCSSpike
1,4-Dioxane (p-Dioxane)ug/L 19.820 99 70-130
1,2-Dichloroethane-d4 (S)%89 67-130
Toluene-d8 (S)%96 70-130
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4199864MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92696513004
4199865
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
1,4-Dioxane (p-Dioxane)ug/L 20 112 55-137113 120ND22.4 22.5
1,2-Dichloroethane-d4 (S)%92 67-13088
Toluene-d8 (S)%96 70-13094
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/20/2023 08:39 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 52 of 99
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92696513
Sludge LF November 2023
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
811142
EPA 3510C
EPA 8270E
8270E Water MSSV RVE
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92696513001, 92696513002, 92696513003, 92696513004, 92696513005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4199550
Associated Lab Samples:92696513001, 92696513002, 92696513003, 92696513004, 92696513005
Matrix:Water
Analyzed
1,2,4-Trichlorobenzene ug/L ND 10.0 11/07/23 20:20
1,2-Dichlorobenzene ug/L ND 10.0 11/07/23 20:20
1,3-Dichlorobenzene ug/L ND 10.0 11/07/23 20:20
1,4-Dichlorobenzene ug/L ND 10.0 11/07/23 20:20
1-Methylnaphthalene ug/L ND 10.0 11/07/23 20:20
2,2'-Oxybis(1-chloropropane)ug/L ND 10.0 11/07/23 20:20
2,4,5-Trichlorophenol ug/L ND 10.0 11/07/23 20:20
2,4,6-Trichlorophenol ug/L ND 10.0 11/07/23 20:20
2,4-Dichlorophenol ug/L ND 10.0 11/07/23 20:20
2,4-Dimethylphenol ug/L ND 10.0 11/07/23 20:20
2,4-Dinitrophenol ug/L ND 50.0 11/07/23 20:20
2,4-Dinitrotoluene ug/L ND 10.0 11/07/23 20:20
2,6-Dinitrotoluene ug/L ND 10.0 11/07/23 20:20
2-Chloronaphthalene ug/L ND 10.0 11/07/23 20:20
2-Chlorophenol ug/L ND 10.0 11/07/23 20:20
2-Methylnaphthalene ug/L ND 10.0 11/07/23 20:20
2-Methylphenol(o-Cresol)ug/L ND 10.0 11/07/23 20:20
2-Nitroaniline ug/L ND 20.0 11/07/23 20:20
2-Nitrophenol ug/L ND 10.0 11/07/23 20:20
3&4-Methylphenol(m&p Cresol)ug/L ND 10.0 11/07/23 20:20
3,3'-Dichlorobenzidine ug/L ND 20.0 11/07/23 20:20
3-Nitroaniline ug/L ND 20.0 11/07/23 20:20
4,6-Dinitro-2-methylphenol ug/L ND 20.0 11/07/23 20:20
4-Bromophenylphenyl ether ug/L ND 10.0 11/07/23 20:20
4-Chloro-3-methylphenol ug/L ND 10.0 11/07/23 20:20
4-Chloroaniline ug/L ND 20.0 11/07/23 20:20
4-Chlorophenylphenyl ether ug/L ND 10.0 11/07/23 20:20
4-Nitroaniline ug/L ND 20.0 11/07/23 20:20
4-Nitrophenol ug/L ND 50.0 11/07/23 20:20
Acenaphthene ug/L ND 10.0 11/07/23 20:20
Acenaphthylene ug/L ND 10.0 11/07/23 20:20
Aniline ug/L ND 10.0 11/07/23 20:20
Anthracene ug/L ND 10.0 11/07/23 20:20
Benzo(a)anthracene ug/L ND 10.0 11/07/23 20:20
Benzo(a)pyrene ug/L ND 10.0 11/07/23 20:20
Benzo(b)fluoranthene ug/L ND 10.0 11/07/23 20:20
Benzo(g,h,i)perylene ug/L ND 10.0 11/07/23 20:20
Benzo(k)fluoranthene ug/L ND 10.0 11/07/23 20:20
Benzoic Acid ug/L ND 50.0 11/07/23 20:20
Benzyl alcohol ug/L ND 20.0 11/07/23 20:20
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/20/2023 08:39 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 53 of 99
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92696513
Sludge LF November 2023
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4199550
Associated Lab Samples:92696513001, 92696513002, 92696513003, 92696513004, 92696513005
Matrix:Water
Analyzed
bis(2-Chloroethoxy)methane ug/L ND 10.0 11/07/23 20:20
bis(2-Chloroethyl) ether ug/L ND 10.0 11/07/23 20:20
bis(2-Ethylhexyl)phthalate ug/L ND 6.0 11/07/23 20:20
Butylbenzylphthalate ug/L ND 10.0 11/07/23 20:20
Chrysene ug/L ND 10.0 11/07/23 20:20
Di-n-butylphthalate ug/L ND 10.0 11/07/23 20:20
Di-n-octylphthalate ug/L ND 10.0 11/07/23 20:20
Dibenz(a,h)anthracene ug/L ND 10.0 11/07/23 20:20
Dibenzofuran ug/L ND 10.0 11/07/23 20:20
Diethylphthalate ug/L ND 10.0 11/07/23 20:20
Dimethylphthalate ug/L ND 10.0 11/07/23 20:20
Fluoranthene ug/L ND 10.0 11/07/23 20:20
Fluorene ug/L ND 10.0 11/07/23 20:20
Hexachloro-1,3-butadiene ug/L ND 10.0 11/07/23 20:20
Hexachlorobenzene ug/L ND 10.0 11/07/23 20:20
Hexachlorocyclopentadiene ug/L ND 10.0 11/07/23 20:20
Hexachloroethane ug/L ND 10.0 11/07/23 20:20
Indeno(1,2,3-cd)pyrene ug/L ND 10.0 11/07/23 20:20
Isophorone ug/L ND 10.0 11/07/23 20:20
N-Nitroso-di-n-propylamine ug/L ND 10.0 11/07/23 20:20
N-Nitrosodimethylamine ug/L ND 10.0 11/07/23 20:20
N-Nitrosodiphenylamine ug/L ND 10.0 11/07/23 20:20
Naphthalene ug/L ND 10.0 11/07/23 20:20
Nitrobenzene ug/L ND 10.0 11/07/23 20:20
Pentachlorophenol ug/L ND 20.0 11/07/23 20:20
Phenanthrene ug/L ND 10.0 11/07/23 20:20
Phenol ug/L ND 10.0 11/07/23 20:20
Pyrene ug/L ND 10.0 11/07/23 20:20
2,4,6-Tribromophenol (S)%8 10-166 S011/07/23 20:20
2-Fluorobiphenyl (S)%74 10-130 11/07/23 20:20
2-Fluorophenol (S)%4 10-130 S011/07/23 20:20
Nitrobenzene-d5 (S)%92 10-133 11/07/23 20:20
Phenol-d6 (S)%16 10-130 11/07/23 20:20
Terphenyl-d14 (S)%114 10-193 11/07/23 20:20
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4199551LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene ug/L 31.350 63 14-130
1,2-Dichlorobenzene ug/L 27.650 55 10-130
1,3-Dichlorobenzene ug/L 26.650 53 10-130
1,4-Dichlorobenzene ug/L 26.750 53 10-130
1-Methylnaphthalene ug/L 44.750 89 26-131
2,2'-Oxybis(1-chloropropane)ug/L 42.650 85 23-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/20/2023 08:39 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 54 of 99
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92696513
Sludge LF November 2023
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4199551LABORATORY CONTROL SAMPLE:
LCSSpike
2,4,5-Trichlorophenol ug/L 46.850 94 36-150
2,4,6-Trichlorophenol ug/L 45.350 91 30-151
2,4-Dichlorophenol ug/L 47.350 95 36-140
2,4-Dimethylphenol ug/L 50.850 102 36-155
2,4-Dinitrophenol ug/L 261250 104 10-169
2,4-Dinitrotoluene ug/L 54.650 109 46-160
2,6-Dinitrotoluene ug/L 48.750 97 47-161
2-Chloronaphthalene ug/L 42.250 84 29-134
2-Chlorophenol ug/L 45.150 90 29-130
2-Methylnaphthalene ug/L 44.050 88 26-130
2-Methylphenol(o-Cresol)ug/L 42.950 86 32-130
2-Nitroaniline ug/L 99.7100 100 41-150
2-Nitrophenol ug/L 46.250 92 31-145
3&4-Methylphenol(m&p Cresol)ug/L 41.150 82 29-130
3,3'-Dichlorobenzidine ug/L 122100 122 46-153
3-Nitroaniline ug/L 97.4100 97 47-156
4,6-Dinitro-2-methylphenol ug/L 120100 120 23-161
4-Bromophenylphenyl ether ug/L 50.950 102 45-143
4-Chloro-3-methylphenol ug/L 96.9100 97 42-143
4-Chloroaniline ug/L 90.3100 90 37-135
4-Chlorophenylphenyl ether ug/L 49.050 98 43-140
4-Nitroaniline ug/L 116100 116 47-157
4-Nitrophenol ug/L 171250 68 10-130
Acenaphthene ug/L 46.950 94 38-138
Acenaphthylene ug/L 46.650 93 39-139
Aniline ug/L 32.250 64 16-130
Anthracene ug/L 55.550 111 45-136
Benzo(a)anthracene ug/L 66.750 133 52-151
Benzo(a)pyrene ug/L 69.650 139 46-165
Benzo(b)fluoranthene ug/L 69.850 140 44-170
Benzo(g,h,i)perylene ug/L 70.750 141 39-171
Benzo(k)fluoranthene ug/L 67.850 136 43-168
Benzoic Acid ug/L 152250 61 10-130
Benzyl alcohol ug/L 96.3100 96 33-134
bis(2-Chloroethoxy)methane ug/L 49.350 99 37-140
bis(2-Chloroethyl) ether ug/L 46.650 93 33-136
bis(2-Ethylhexyl)phthalate ug/L 66.250 132 50-169
Butylbenzylphthalate ug/L 65.450 131 50-174
Chrysene ug/L 67.450 135 52-148
Di-n-butylphthalate ug/L 64.550 129 51-154
Di-n-octylphthalate ug/L 67.250 134 44-170
Dibenz(a,h)anthracene ug/L 71.750 143 41-171
Dibenzofuran ug/L 46.850 94 42-157
Diethylphthalate ug/L 52.650 105 50-149
Dimethylphthalate ug/L 49.050 98 47-146
Fluoranthene ug/L 65.350 131 51-152
Fluorene ug/L 49.450 99 46-143
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/20/2023 08:39 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 55 of 99
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92696513
Sludge LF November 2023
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4199551LABORATORY CONTROL SAMPLE:
LCSSpike
Hexachloro-1,3-butadiene ug/L 27.050 54 10-130
Hexachlorobenzene ug/L 52.050 104 40-139
Hexachlorocyclopentadiene ug/L 32.950 66 10-130
Hexachloroethane ug/L 24.450 49 10-130
Indeno(1,2,3-cd)pyrene ug/L 68.950 138 40-172
Isophorone ug/L 50.850 102 37-143
N-Nitroso-di-n-propylamine ug/L 50.750 101 38-145
N-Nitrosodimethylamine ug/L 39.850 80 30-130
N-Nitrosodiphenylamine ug/L 52.650 105 46-144
Naphthalene ug/L 36.850 74 21-130
Nitrobenzene ug/L 45.750 91 33-136
Pentachlorophenol ug/L 121100 121 19-156
Phenanthrene ug/L 57.850 116 49-143
Phenol ug/L 28.050 56 18-130
Pyrene ug/L 66.050 132 48-156
2,4,6-Tribromophenol (S)%104 10-166
2-Fluorobiphenyl (S)%84 10-130
2-Fluorophenol (S)%68 10-130
Nitrobenzene-d5 (S)%95 10-133
Phenol-d6 (S)%54 10-130
Terphenyl-d14 (S)%129 10-193
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4199552MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92696779007
4199553
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
1,2,4-Trichlorobenzene ug/L R183.3 61 10-13043 3583.3ND 50.7 35.6
1,2-Dichlorobenzene ug/L R183.3 54 10-13034 4683.3ND 44.9 28.1
1,3-Dichlorobenzene ug/L R183.3 52 10-13031 4983.3ND 43.0 26.1
1,4-Dichlorobenzene ug/L R183.3 53 10-13033 4683.3ND 44.0 27.5
1-Methylnaphthalene ug/L R183.3 81 10-13053 4283.3ND 67.7 44.4
2,2'-Oxybis(1-chloropropane)ug/L R183.3 78 10-13251 4283.3ND 64.8 42.4
2,4,5-Trichlorophenol ug/L R183.3 93 10-17459 4583.3ND 77.9 49.1
2,4,6-Trichlorophenol ug/L R183.3 94 10-17356 5183.3ND 78.4 46.6
2,4-Dichlorophenol ug/L R183.3 90 10-15356 4783.3ND 75.3 46.9
2,4-Dimethylphenol ug/L R183.3 103 12-15763 4883.3ND 85.9 52.6
2,4-Dinitrophenol ug/L R14177510-16547 46417ND312196
2,4-Dinitrotoluene ug/L 83.3 99 29-16882 1983.3ND 82.7 68.7
2,6-Dinitrotoluene ug/L R183.3 90 28-16864 3383.3ND 74.7 53.4
2-Chloronaphthalene ug/L R183.3 82 11-13652 4583.3ND 68.4 43.2
2-Chlorophenol ug/L R183.3 91 10-13459 4383.3ND 76.2 49.5
2-Methylnaphthalene ug/L R183.3 80 10-13154 3983.3ND 66.7 44.7
2-Methylphenol(o-Cresol)ug/L R183.3 89 10-13058 4283.3ND 74.2 48.6
2-Nitroaniline ug/L R11679519-15664 38167ND158107
2-Nitrophenol ug/L R183.3 96 10-16059 4883.3ND 80.3 49.4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/20/2023 08:39 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 56 of 99
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92696513
Sludge LF November 2023
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4199552MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92696779007
4199553
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
3&4-Methylphenol(m&p
Cresol)
ug/L R183.3 80 10-13253 4183.3ND 66.8 44.0
3,3'-Dichlorobenzidine ug/L 167 87 10-17393 7167ND145155
3-Nitroaniline ug/L 167 87 19-16973 17167ND145122
4,6-Dinitro-2-methylphenol ug/L 167 106 10-17888 19167ND177146
4-Bromophenylphenyl ether ug/L R183.3 91 28-14966 3183.3ND 75.7 55.4
4-Chloro-3-methylphenol ug/L R11679618-14862 44167ND161103
4-Chloroaniline ug/L R11677710-14153 36167ND12888.6
4-Chlorophenylphenyl ether ug/L R183.3 88 24-14455 4683.3ND 73.1 45.8
4-Nitroaniline ug/L 167 83 18-17080 3167ND138134
4-Nitrophenol ug/L 417 65 10-13060 9417ND273248
Acenaphthene ug/L R183.3 86 18-14253 4883.3ND 71.9 44.2
Acenaphthylene ug/L R183.3 87 18-14355 4583.3ND 72.7 46.0
Aniline ug/L 83.3 73 10-13055 2983.3ND 60.9 45.7
Anthracene ug/L 83.3 100 32-13884 1883.3ND 83.5 69.7
Benzo(a)anthracene ug/L 83.3 114 41-155104 883.3ND 94.7 87.0
Benzo(a)pyrene ug/L 83.3 116 10-167104 1083.3ND 96.4 86.8
Benzo(b)fluoranthene ug/L 83.3 110 31-172107 383.3ND 92.0 89.6
Benzo(g,h,i)perylene ug/L 83.3 125 26-177119 583.3ND 104 99.5
Benzo(k)fluoranthene ug/L 83.3 112 31-168103 983.3ND 93.4 85.6
Benzoic Acid ug/L 417 55 10-13011417ND22747.0J
Benzyl alcohol ug/L R11679210-13662 39167ND153103
bis(2-Chloroethoxy)methane ug/L R183.3 107 12-14367 4583.3ND 89.0 56.0
bis(2-Chloroethyl) ether ug/L R183.3 104 10-13967 4383.3ND 86.5 55.8
bis(2-Ethylhexyl)phthalate ug/L 83.3 112 41-173108 483.3ND 93.5 89.7
Butylbenzylphthalate ug/L 83.3 107 38-182106 183.3ND 89.1 88.1
Chrysene ug/L 83.3 117 41-152105 1083.3ND 97.4 87.8
Di-n-butylphthalate ug/L 83.3 106 37-16299 783.3ND 88.2 82.6
Di-n-octylphthalate ug/L 83.3 119 36-176115 383.3ND 98.8 95.6
Dibenz(a,h)anthracene ug/L 83.3 123 29-175115 783.3ND 102 95.6
Dibenzofuran ug/L R183.3 84 23-14452 4883.3ND 70.0 43.1
Diethylphthalate ug/L 83.3 94 33-15477 2083.3ND 78.1 63.8
Dimethylphthalate ug/L R183.3 88 29-15063 3383.3ND 73.2 52.5
Fluoranthene ug/L 83.3 112 40-15699 1283.3ND 93.6 82.7
Fluorene ug/L R183.3 90 26-14857 4483.3ND 74.9 47.7
Hexachloro-1,3-butadiene ug/L R183.3 52 10-13034 4083.3ND 42.9 28.6
Hexachlorobenzene ug/L 83.3 91 27-14569 2883.3ND 75.8 57.4
Hexachlorocyclopentadiene ug/L R183.3 64 10-13041 4583.3ND 53.5 34.0
Hexachloroethane ug/L R183.3 48 10-13025 6383.3ND 39.8 20.7
Indeno(1,2,3-cd)pyrene ug/L 83.3 120 28-176109 1083.3ND 100 91.0
Isophorone ug/L R183.3 105 14-14565 4783.3ND 87.2 54.2
N-Nitroso-di-n-propylamine ug/L R183.3 99 12-14967 3883.3ND 82.4 56.1
N-Nitrosodimethylamine ug/L R183.3 101 10-13067 4183.3ND 84.4 55.6
N-Nitrosodiphenylamine ug/L 83.3 97 29-14976 2583.3ND 81.1 63.0
Naphthalene ug/L R183.3 73 10-13050 3883.3ND 60.6 41.4
Nitrobenzene ug/L R183.3 105 10-14566 4583.3ND 87.1 55.2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/20/2023 08:39 AM
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2225 Riverside Dr.
Asheville, NC 28804
[phone]
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#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92696513
Sludge LF November 2023
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4199552MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92696779007
4199553
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Pentachlorophenol ug/L 167 102 10-17889 13167ND170149
Phenanthrene ug/L 83.3 102 36-14682 2283.3ND 85.4 68.7
Phenol ug/L R183.3 70 10-13048 3783.3ND 58.5 40.2
Pyrene ug/L 83.3 111 42-156105 683.3ND 92.7 87.5
2,4,6-Tribromophenol (S)%81 10-16667
2-Fluorobiphenyl (S)%72 10-13046
2-Fluorophenol (S)%66 10-13047
Nitrobenzene-d5 (S)%93 10-13363
Phenol-d6 (S)%53 10-13038
Terphenyl-d14 (S)%84 10-19391
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/20/2023 08:39 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 58 of 99
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92696513
Sludge LF November 2023
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
811742
SM 2320B-2011
SM 2320B-2011
2320B Alkalinity
Laboratory:Pace Analytical Services - Asheville
Associated Lab Samples:92696513001, 92696513002, 92696513003, 92696513004, 92696513005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4202710
Associated Lab Samples:92696513001, 92696513002, 92696513003, 92696513004, 92696513005
Matrix:Water
Analyzed
Alkalinity, Total as CaCO3 mg/L ND 5.0 11/08/23 17:40
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4202711LABORATORY CONTROL SAMPLE:
LCSSpike
Alkalinity, Total as CaCO3 mg/L 51.750 103 80-120
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4202712LABORATORY CONTROL SAMPLE:
LCSSpike
Alkalinity, Total as CaCO3 mg/L 50.250 100 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4202713MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92697037009
4202714
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Alkalinity, Total as CaCO3 mg/L 50 102 80-120103 05076.5 127 128
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4202715MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92697037010
4202716
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Alkalinity, Total as CaCO3 mg/L 50 99 80-120106 35062.4 112 116
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/20/2023 08:39 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 59 of 99
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92696513
Sludge LF November 2023
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
811041
SM 2540C-2015
SM 2540C-2015
2540C Total Dissolved Solids
Laboratory:Pace Analytical Services - Asheville
Associated Lab Samples:92696513001, 92696513002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4199280
Associated Lab Samples:92696513001, 92696513002
Matrix:Water
Analyzed
Total Dissolved Solids mg/L ND 25.0 11/04/23 13:00
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4199281LABORATORY CONTROL SAMPLE:
LCSSpike
Total Dissolved Solids mg/L 254250 101 90-110
Parameter Units
Dup
Result QualifiersRPDResult
92696489003
4199282SAMPLE DUPLICATE:
Total Dissolved Solids mg/L 367 0367
Parameter Units
Dup
Result QualifiersRPDResult
92696655001
4199283SAMPLE DUPLICATE:
Total Dissolved Solids mg/L 240 0240
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/20/2023 08:39 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 60 of 99
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92696513
Sludge LF November 2023
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
811437
SM 2540C-2015
SM 2540C-2015
2540C Total Dissolved Solids
Laboratory:Pace Analytical Services - Asheville
Associated Lab Samples:92696513003, 92696513004, 92696513005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4201022
Associated Lab Samples:92696513003, 92696513004, 92696513005
Matrix:Water
Analyzed
Total Dissolved Solids mg/L ND 25.0 11/07/23 10:59
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4201023LABORATORY CONTROL SAMPLE:
LCSSpike
Total Dissolved Solids mg/L 268250 107 90-110
Parameter Units
Dup
Result QualifiersRPDResult
92696521008
4201024SAMPLE DUPLICATE:
Total Dissolved Solids mg/L 188 15218
Parameter Units
Dup
Result QualifiersRPDResult
92696737001
4201025SAMPLE DUPLICATE:
Total Dissolved Solids mg/L 761 1765
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/20/2023 08:39 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 61 of 99
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92696513
Sludge LF November 2023
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
810773
EPA 300.0 Rev 2.1 1993
EPA 300.0 Rev 2.1 1993
300.0 IC Anions
Laboratory:Pace Analytical Services - Asheville
Associated Lab Samples:92696513001, 92696513002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4197586
Associated Lab Samples:92696513001, 92696513002
Matrix:Water
Analyzed
Sulfate mg/L ND 1.0 11/03/23 10:51
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4197587LABORATORY CONTROL SAMPLE:
LCSSpike
Sulfate mg/L 51.050 102 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4197588MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92696201001
4197589
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Sulfate mg/L 50 102 90-110105 15093.6 145 146
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4197590MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92696449004
4197591
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Sulfate mg/L 50 99 90-110103 15092.7 142 144
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/20/2023 08:39 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 62 of 99
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92696513
Sludge LF November 2023
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
810904
EPA 300.0 Rev 2.1 1993
EPA 300.0 Rev 2.1 1993
300.0 IC Anions
Laboratory:Pace Analytical Services - Asheville
Associated Lab Samples:92696513003, 92696513004, 92696513005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4198439
Associated Lab Samples:92696513003, 92696513004, 92696513005
Matrix:Water
Analyzed
Sulfate mg/L ND 1.0 11/03/23 17:14
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4198440LABORATORY CONTROL SAMPLE:
LCSSpike
Sulfate mg/L 53.350 107 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4198441MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92696521004
4198442
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Sulfate mg/L 50 100 90-110104 450ND50.3 52.6
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4198443MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92696513003
4198444
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Sulfate mg/L 50 101 90-110102 1501.9 52.4 53.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/20/2023 08:39 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 63 of 99
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92696513
Sludge LF November 2023
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
813868
SM 4500-Cl-E-2011
SM 4500-Cl-E-2011
4500 Chloride
Laboratory:Pace Analytical Services - Asheville
Associated Lab Samples:92696513001, 92696513002, 92696513003, 92696513004, 92696513005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4213738
Associated Lab Samples:92696513001, 92696513002, 92696513003, 92696513004, 92696513005
Matrix:Water
Analyzed
Chloride mg/L ND 1.0 11/17/23 13:08
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4213739LABORATORY CONTROL SAMPLE:
LCSSpike
Chloride mg/L 20.820 104 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4213742MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92696513002
4213743
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Chloride mg/L 10 103 90-110101 2103.0 13.4 13.1
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4213760MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92696528001
4213761
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Chloride mg/L 10 98 90-11098 0100.86J 10.7 10.7
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/20/2023 08:39 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 64 of 99
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92696513
Sludge LF November 2023
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
811188
SM 5310B-2014
SM 5310B-2014
5310B TOC
Laboratory:Pace Analytical Services - Asheville
Associated Lab Samples:92696513001, 92696513002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4199748
Associated Lab Samples:92696513001, 92696513002
Matrix:Water
Analyzed
Total Organic Carbon mg/L ND 1.0 11/06/23 13:12
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4199749LABORATORY CONTROL SAMPLE:
LCSSpike
Total Organic Carbon mg/L 23.525 94 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4199750MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92696725001
4199751
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Total Organic Carbon mg/L 25 98 90-11098 0253.1 27.6 27.6
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4199752MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92696725002
4199753
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Total Organic Carbon mg/L 25 97 90-11098 1253.0 27.2 27.5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/20/2023 08:39 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 65 of 99
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92696513
Sludge LF November 2023
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
813070
SM 5310B-2014
SM 5310B-2014
5310B TOC
Laboratory:Pace Analytical Services - Asheville
Associated Lab Samples:92696513003, 92696513004, 92696513005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4209685
Associated Lab Samples:92696513003, 92696513004, 92696513005
Matrix:Water
Analyzed
Total Organic Carbon mg/L ND 1.0 11/14/23 13:15
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4209686LABORATORY CONTROL SAMPLE:
LCSSpike
Total Organic Carbon mg/L 23.925 96 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4209687MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92697397007
4209688
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Total Organic Carbon mg/L 25 95 90-11096 125ND23.6 24.0
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4209689MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92697473001
4209690
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Total Organic Carbon mg/L 25 99 90-11099 0253.7 28.5 28.4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/20/2023 08:39 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 66 of 99
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92696513
Sludge LF November 2023
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
RPD value was outside control limits.R1
Surrogate recovery outside laboratory control limits.S0
The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in the
associated samples may have a high bias.v1
The continuing calibration verification was below the method acceptance limit. The analyte was not detected in the
associated samples and the sensitivity of the instrument was verified with a reporting limit check standard.v2
The continuing calibration verification was below the method acceptance limit. Any detection for the analyte in the
associated samples may have low bias.v3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/20/2023 08:39 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 67 of 99
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92696513
Sludge LF November 2023
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92696513001 SWP-1
92696513002 SWP-2
92696513003 Q06V09
92696513004 Q06V10
92696513005 Q06V11
92696513001 810885 811002SWP-1 EPA 3010A EPA 6010D
92696513002 810885 811002SWP-2 EPA 3010A EPA 6010D
92696513003 810885 811002Q06V09EPA 3010A EPA 6010D
92696513004 810885 811002Q06V10EPA 3010A EPA 6010D
92696513005 810885 811002Q06V11EPA 3010A EPA 6010D
92696513001 811142 811565SWP-1 EPA 3510C EPA 8270E
92696513002 811142 811565SWP-2 EPA 3510C EPA 8270E
92696513003 811142 811565Q06V09EPA 3510C EPA 8270E
92696513004 811142 811565Q06V10EPA 3510C EPA 8270E
92696513005 811142 811565Q06V11EPA 3510C EPA 8270E
92696513001 811264SWP-1 EPA 8260D
92696513002 811264SWP-2 EPA 8260D
92696513003 811863Q06V09EPA 8260D
92696513004 811863Q06V10EPA 8260D
92696513005 811863Q06V11EPA 8260D
92696513007 811863TRIP BLANK EPA 8260D
92696513001 810909SWP-1 EPA 8260D Mod.
92696513002 810909SWP-2 EPA 8260D Mod.
92696513003 811148Q06V09EPA 8260D Mod.
92696513004 811197Q06V10EPA 8260D Mod.
92696513005 811197Q06V11EPA 8260D Mod.
92696513007 811131TRIP BLANK EPA 8260D Mod.
92696513001 811742SWP-1 SM 2320B-2011
92696513002 811742SWP-2 SM 2320B-2011
92696513003 811742Q06V09SM 2320B-2011
92696513004 811742Q06V10SM 2320B-2011
92696513005 811742Q06V11SM 2320B-2011
92696513001 811041SWP-1 SM 2540C-2015
92696513002 811041SWP-2 SM 2540C-2015
92696513003 811437Q06V09SM 2540C-2015
92696513004 811437Q06V10SM 2540C-2015
92696513005 811437Q06V11SM 2540C-2015
92696513001 810773SWP-1 EPA 300.0 Rev 2.1 1993
92696513002 810773SWP-2 EPA 300.0 Rev 2.1 1993
92696513003 810904Q06V09EPA 300.0 Rev 2.1 1993
92696513004 810904Q06V10EPA 300.0 Rev 2.1 1993
92696513005 810904Q06V11EPA 300.0 Rev 2.1 1993
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/20/2023 08:39 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 68 of 99
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92696513
Sludge LF November 2023
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92696513001 813868SWP-1 SM 4500-Cl-E-2011
92696513002 813868SWP-2 SM 4500-Cl-E-2011
92696513003 813868Q06V09SM 4500-Cl-E-2011
92696513004 813868Q06V10SM 4500-Cl-E-2011
92696513005 813868Q06V11SM 4500-Cl-E-2011
92696513001 811188SWP-1 SM 5310B-2014
92696513002 811188SWP-2 SM 5310B-2014
92696513003 813070Q06V09SM 5310B-2014
92696513004 813070Q06V10SM 5310B-2014
92696513005 813070Q06V11SM 5310B-2014
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/20/2023 08:39 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
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The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced,except in its entirety,without the written approval of Pace Analytical Services,LLC.
Pace Analytical Services,LLC (formerly Shealy Environmental Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172
Tel:[phone] Fax:[phone] www.pacelabs.com
Report of Analysis
Pace Analytical Services,LLC
2225 Riverside Drive
Asheville,NC 28804
Attention:Lorri Patton
Project Name:Sludge Landfill 11-1
Project Number:92696513
Lot Number:YK04013
Date Completed:11/15/2023
11/17/2023 4:25 PM
Approved and released by:
Project Coordinator 1:Jenna S.Holliday
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PACE ANALYTICAL SERVICES,LLC
SC DHEC No:32010001 NELAC No:E87653 NC DENR No:329 NC Field Parameters No:5639
Pace Analytical Services,LLC (formerly Shealy Environmetal Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax [phone] www.pacelabs.com
Case Narrative
Pace Analytical Services,LLC
Lot Number:YK04013
This Report of Analysis contains the analytical result(s)for the sample(s)listed on the Sample Summary
following this Case Narrative.The sample receiving date is documented in the header information
associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.Where
sampling is conducted by the client,results relate to the accuracy of the information provided,and as the
samples are received.
Sample receipt,sample analysis,and data review have been performed in accordance with the most
current approved The NELAC Institute (TNI)standards,the Pace Analytical Services,LLC ("Pace")
Laboratory Quality Manual,standard operating procedures (SOPs),and Pace policies.Any exceptions to
the TNI standards,the Laboratory Quality Manual,SOPs or policies are qualified on the results page or
discussed below.
Pace is a TNI accredited laboratory;however,the following analyses are currently not listed on our TNI
scope of accreditation:E.coli and Total coliforms SM 9223 B-2004,Solid Chemical Material:TOC
Walkley-Black,Biological Tissue:All,Non-Potable Water:SGT-HEM EPA 1664B,Silica EPA 200.7,
Boron,Calcium,Silicon,Strontium EPA 200.8,Bicarbonate,Carbonate,and Hydroxide Alkalinity SM
2320 B-2011,SM 9221 C E-2006 &SM 9222D-2006,Strontium SW-846 6010D,VOC SM 6200 B-2011,
Fecal Coliform Colilert-18.If you have any questions regarding this report,please contact the Pace
Project Manager listed on the cover page.
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PACE ANALYTICAL SERVICES, LLC
Sample Summary
Pace Analytical Services, LLC
Lot Number: YK04013

Project Name: Sludge Landfill 11-1
Project Number: 92696513
Sample Number Sample ID Matrix Date Sampled Date Received
001 11/01/2023 1430SWP-1 Aqueous 11/07/2023
002 11/01/2023 1515SWP-2 Aqueous 11/04/2023
003 11/02/2023 1140Q06V09Aqueous 11/04/2023
004 11/02/2023 1005Q06V10Aqueous 11/04/2023
005 11/02/2023 1030Q06V11Aqueous 11/04/2023
006 11/02/2023 1145FIELD BLANK Aqueous 11/04/2023
(6 samples)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

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PACE ANALYTICAL SERVICES, LLC
Detection Summary
Pace Analytical Services, LLC
Lot Number: YK04013

Project Name: Sludge Landfill 11-1
Project Number: 92696513
Sample Sample ID Matrix Parameter Method Result Q Units Page
004 Q06V10 Aqueous Mercury (CVAFS)1631E 9.71 ng/L 8
005 Q06V11 Aqueous Mercury (CVAFS)1631E 0.742 ng/L 9
(2 detections)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

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Mercury (CVAFS)
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Pace Analytical Services, LLC
SWP-1
YK04013-001
11/01/2023 1430
11/07/2023
Aqueous
Project Name: Sludge Landfill 11-1
Project Number: 92696513
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 1631E 1 11/15/2023 0923 KAJ 11/14/2023 1454 89948
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run
Mercury (CVAFS)7439-97-6 1631E ND 1ng/L0.500
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the LOQ N = Recovery is out of criteria
H = Out of holding time
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failureW = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 5 of 18
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Mercury (CVAFS)
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Pace Analytical Services, LLC
SWP-2
YK04013-002
11/01/2023 1515
11/04/2023
Aqueous
Project Name: Sludge Landfill 11-1
Project Number: 92696513
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 1631E 1 11/15/2023 0929 KAJ 11/14/2023 1454 89948
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run
Mercury (CVAFS)7439-97-6 1631E ND 1ng/L0.500
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the LOQ N = Recovery is out of criteria
H = Out of holding time
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failureW = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

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Mercury (CVAFS)
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Pace Analytical Services, LLC
Q06V09
YK04013-003
11/02/2023 1140
11/04/2023
Aqueous
Project Name: Sludge Landfill 11-1
Project Number: 92696513
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 1631E 1 11/15/2023 0934 KAJ 11/14/2023 1454 89948
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run
Mercury (CVAFS)7439-97-6 1631E ND 1ng/L0.500
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the LOQ N = Recovery is out of criteria
H = Out of holding time
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failureW = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

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Mercury (CVAFS)
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Pace Analytical Services, LLC
Q06V10
YK04013-004
11/02/2023 1005
11/04/2023
Aqueous
Project Name: Sludge Landfill 11-1
Project Number: 92696513
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 1631E 1 11/15/2023 0940 KAJ 11/14/2023 1454 89948
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run
Mercury (CVAFS)7439-97-6 1631E 9.71 1ng/L0.500
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the LOQ N = Recovery is out of criteria
H = Out of holding time
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failureW = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 8 of 18
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Mercury (CVAFS)
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Pace Analytical Services, LLC
Q06V11
YK04013-005
11/02/2023 1030
11/04/2023
Aqueous
Project Name: Sludge Landfill 11-1
Project Number: 92696513
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 1631E 1 11/15/2023 0945 KAJ 11/14/2023 1454 89948
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run
Mercury (CVAFS)7439-97-6 1631E 0.742 1ng/L0.500
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the LOQ N = Recovery is out of criteria
H = Out of holding time
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failureW = Reported on wet weight basis
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Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

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Mercury (CVAFS)
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Pace Analytical Services, LLC
FIELD BLANK
YK04013-006
11/02/2023 1145
11/04/2023
Aqueous
Project Name: Sludge Landfill 11-1
Project Number: 92696513
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 1631E 1 11/15/2023 0951 KAJ 11/14/2023 1454 89948
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run
Mercury (CVAFS)7439-97-6 1631E ND 1ng/L0.500
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the LOQ N = Recovery is out of criteria
H = Out of holding time
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failureW = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

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QC Summary
QC Data for Lot Number: YK04013
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

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Mercury (CVAFS) - MB
Batch:Prep Method:
Prep Date:
Sample ID:YQ89948-001
89948
11/14/2023 1454Analytical Method:1631E
Matrix:Aqueous
Parameter Result Q LOQ Units Analysis DateDil
Mercury (CVAFS)ND 11/15/2023 08560.500 ng/L1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation ND = Not detected at or above the LOQ N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria* = RSD is out of criteria
QC Data for Lot Number: YK04013
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Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

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Mercury (CVAFS) - LCS
Batch:Prep Method:
Prep Date:
Sample ID:YQ89948-002
89948
11/14/2023 1454Analytical Method:1631E
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
%Rec
LimitDil(ng/L)(ng/L)
Mercury (CVAFS)5.00 11/15/2023 09071005.00 75-1251
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation ND = Not detected at or above the LOQ N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria* = RSD is out of criteria
QC Data for Lot Number: YK04013
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Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

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Chain of Custody
and
Miscellaneous Documents
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Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

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PACE ANALYTICAL SERVICES, LLC

106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

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PACE ANALYTICAL SERVICES, LLC

106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

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PACE ANALYTICAL SERVICES, LLC

106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

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