WQ0033677_Groundwater Monitoring Report November 2023_20231228

Enter date monRorrng resulla Were due. g -fA WilWill Viis rnoniioring ropori (GVV-59 and GVU a9A)
YES
IV®
be submitted after the established due date?
Was any required information missing on the GIY-59 report Yarn?
YES
Ro
IF fhe answer to question l or 2 is "YES, list in the space provided below the well identification number(s) and
explain the problems encountered in obtaining the required information.
Arc any of the monitor wcils in need of repair or maintenance (damaged casing, unlocked or missing cap, missing
YES
NO
identification plate, area overgrown, etc.)? Ifthe answer is "Yes', contact the Regional Ofee forg idance.
Are any monitored constituents equal to or above the established standards?
vs
o
lfthe answer to question 9 is WO', skip to sectfon B.
tf fhe answer to question 4 is "YES" list the affected wells individually with constituents) and canaeatration(s)
exceeding standards in the space provided below.
y
ror the constituents identified in question 4 above, have standards been exceeded previously for the
YES
NO
same constituents) in the same well(s) in the lost two years?
Iffhe answer to question 5is "AU', skip to section &.
It the answer to ques'rfon 5 is "YES", fist in the space provided below, each welt with consfifuent(sJ exceeding
standards, concentralion(s) reported, and sample collection date for each occutrence (for the last two years).
Are the knonitoving wells listed In section h located at ®r beyond the Veview boundary?
YE9
NO
If the onswor is " %fCS , a arovfodwater c;uatifyArrebforn may bo occarrring, CCJAIMCi THE REG[CA f
0 l=f=11EIHAP:ED dEf ifP0 P G,UT AAlC-7. N2he answer'is "All'; r tanikorlrT, wells mat/heimp rmperly
Me Re"ji0rF-i O five,
.. Cn t ,'.11 (• _ I ...lii ct`t t �•Lirf I.-i,=. �.I E...-'... s-. ]. fnllx �7: i'11ig __-.._�
1.
...•
(�,t -

r,C)U iDWATER QQAL1TY 1}t1ONITOPJNG:
PmPUANCE REPORT FORM'
or
Dame:
Name Of different}:
Address: 5,8 �,,
NC
act PBr5on: 0 9 9 r i.
Location/Site Name:n�
Li 1D NUMlER (from Permit):
Well Depth:
Depth to Water Level: ' fL below mansur g Point
Measuring Point is ft. above land su •ace
Volume of water pumped)bailed:befar sampling: . ; L f
7.
'
;lVan-Discharge
I
!NPDES
TYPE OF PLC
_ - County r
©i aoAo�
� ❑''Spr�Y em i�
I
-T'elephoneg: 44�--�421 4 ado
©�nEary
No. of wells to be sam led: -
- P
❑ Wa't2r 5oL Ce:�.
Dafe sarnple'aoilected: `l, ➢
FIELD .. EZ..
ff i.PJD.r
U
Well Djameter• in.
p
.vim.
V DR' aL
Screened Interval: " ft, to' ft. Spey. con
°n?
Relative M.P. 1_lavation: ft..
Odor
same rng.
ins �
a�d field acidltied: • ❑ YEs I-1 rvn
lnpea[ ar,c�
.......
_ ham.
=aEe sample analyzed: ` ' E rr n e,
Laboratory
Name: us rC f ,-, A
_ �-
AF�P flRFTi R5 FIO7: Values shoui�l r ecl+diso[vred atg<t col;ardl
cnncentratio' "
COD it rrtgll
CnItform: MF Fec41 IiCl0lnl
Nitrite
Pikrate (&C� as
CQliform:MFTot
. {Nora: Usa MPN
DOm
Ph SbF crus: Total as P �3, n rrwll
' --�
N
-
meihad for hi�ry WrDia spmplet}
j'togEiasphaie
DiSSQIved Solids: Total i
'.
' r• ..-:
mall
Ot er (S,,
�-ign
,I i k - AI rnlnum Il
PH (when analyzed) r units
m
9.
as.-18erium
r
ell, P
:.I
Te7C-—_ �1n511
Ca' Calcium mgl€
—
Chloride ! f j r 1
.,Cd-C�drnium `
_
�
I 191
Arsenic 1 o.fi m Il
9 I
mgI!
Carom€u;
m: Total
_
Grease and Offs. j I '
rrtgli .
9
;)-,u'CoppeY V mg!]
Phenol ': lhgli
Su fate i :
Fe -Eton ri
I
�l
itri.
!1
SPeciifG C9nductan� ; J. i4lhns
Hs ..M:t cu��
_ery I mgA
XI_ PotaS5IUM - ° I I
fccYo
1fOC
Total Ammonia I rri l[
farnmonla Ntrngen; NH,- N;AMIAenia 9
r ' _mg
. . N{� ",, i5iE8gflesittm ' m�l
4 uw.ry Fofia6 i :
1 "
TKN as N d
i .
j AAn - Manganese t"
-
q�` ;rn9Ji
Ni --Nickel
licltel g'I
—_ ---
t'or
Ta......
m 'v O
5
a
LPI^a+S
-
.. ",
�Ld
PeFrprt?@e( Elu{horiaedAg�nt}Narne,andTdle.Ple sr�GBntorigpr=
Sig ,lure of Pe[m{g {orAuihcr¢edna,r,,,
Rev. t12oo7.

�OMPLIAHGE REPORT -FORM
cility Name: U4
rmit Flame (if different):
cili y Address: 5-6 (�
act Person:
LocationlSjte Nam�_ 5't
WELL ID NUMBER (from P§grmlt)-
ell Reptlt; �� : ft.
DepEh to Water Level:dA.j ft. below measu
Measuring Point is ft. above land sl
Volume ofwater pumped)bailed:before sampling:.
COcnty
y� s. Telephone* 90o'
No, of wells to be sampled:
point.
:e
7ats sample analyaed:n , t� � �
�ARAt'diEmRS NOTE: 'J 4aiues shouE ! re€t CIdlSsatu
cob i {I rngll
COIHOMm: MF FeCal 7. 1701p!
CQllform: 1�9F Total
(Note: Use MPN =Md tdr _. �OIYIi
- I><9hlYi�rFrids�mples]
Dissolved Solids: Total
pH (when analyzed} I nits
TOC
Chloride mgli
Arse*4p� ai mgll
Grease and Oils, Ii it g1[
Phenol m�
Sulfate i ' ltngll
6p�cific Conductance I yMhn
TotalAmmonia C3 ';• 1'ni�l
(Ammonla Nkr4gw NHsas N: ". onla ISErogenj ow) i :
T•KN as N i4k i`: _mg11
For s'amadiation Systems
M
Date ;am ple'collected:_._P�`�� � � —
Well D7j meter ° in.
Screened Interval: 'C� ft, to 4.
Ralative M.P. Elevation: eft,.
gallons ''
td0'. zrdSeldacidified: -❑YES No
on-DischerQ�• -
_�._�
PDES
-
I'FE OF PERYJJl . 7
Lagocn
❑ Vlrafer S curt= - _
._... .... ,
or�v�r
lir
Spa van .�
i lme O
G'dor
- ISampE�7W
chock ;
Apnear2nce
La�oratpry
s
Name:
e¢Ialid coiioid3.Goncentrataons.
Nitrite
(NO,) as N€ melt
Pb - Laau
(hips)
as'N :.as A4 m91I,
w
�F vlr
I •
Phbs o
Pn 't'us: TO
--
al as P ��,.� � �_mgll •
`.
.OMthophsphate
AI--Al�minum
_ mgll
5
mgli
mail
Ca =
Cd - Ckdmium
Caiclurn _---mgl1
�_�.� __.
-- -
mgllT
Crorrium:
Total mgll
-,_-11
W, _
Cu .,Copper::. _rrgR •
Cp i l: -
Fe', fron nigGl
(5fne f r f ,-
i.i Hg Mercury mgll
i
RSpc tEz: _
Kj= Potassium .�'�.�. ri]glj
lJCC
M .Ma spium 'MCI[
Mn - Man arAse m9!
I. Ei - �
=iniiu�t To, 1,14Cs
_.f ._ � Fs•w v+ hYNY � •f
�w:es Rsv, �rzoa7
f I
Qaztur! f�� (orAutnor�,od�9En., �,•
.........

AWD-fill j LjMEVU:
;OMPUANG� REPORT FOR �M
-A9,jLljyjNJEQ-RMATJMFYease P int rj6my or Type
"SO RY Name: r
lermit Name (if different): . . ......................
72cillityAddress:
Contact Person:
n
4
VV LL �IWM�SER
Well Depth: -LE(2 1---
ft.
:2
Depth to Water Level: ft• below mpasu
Mt�asuring Pcint is ft. above land St
Volume of wafe
r pump edibajjid'beforg sampling:.'
VAKAM57ERS NOTE VALies-i
cot)
Coliform: MF Fecal
CPlIfOrm: MTotal 1
.{Nate: use MAN methptl for raghly twb
Dissulved Solids: Total r
PH (when analyzed')
TO C 76
Chloride
Arsenio 40
Grease and 01
Phenol
Sulfate
specific Condurtance, - 1
T021 Arnmonla
[A-112 MW690n; NH,&s
TKN as N
For Rarnadiatlan qvtt— n.,11, P
Rev. 112OC7
County
Te lephonet!-.
No. of wells to be sampled:
Pate sample, collected:
Well Dlimeter:
paint Screened CreeneJnteTVa]:,
. I 't-,to ft
Relative M.P. Elevatlor;
ft.
D.ES.
...........
:C'
VfaiBrS0UFO j
.. ........ . .. ... . ......... ...
PH
Spec.
Oda:
MPEM;j
'Chick
Entilterad:• ICES
LJ N 6. field acidiN�d: ❑E3YES Q NO
bare
it
Lob' qfato.r - Name:
y L
- ----------------
Jf
is
.d !—L
....... ...
.1
-:1 mg
OOrniil
Writs (1� 12) as N
mg f[
-b! i
Nitrate (N a) as N rng&
Zn, t
PhPsp,6-0 rUs: To i1i as P
units
M,
Inum mgll
. .......
_
6:
Ba. Barium MM
Qa�
-zz
MR,
!Cd - cidmium Mg1l
C�rcmlum! Total
rlgll
MO
I' ICU -�Cnnper
wil
Iron 311 rngfl
fsQ%-- . .....
E
HO.,marcury
Kk-Pofasiium
Mg/I
-,;man 2nesd
Q
a Ni Nickel Frig
itachil
U voc�: .. ..... .... -
EMpnt
i a! VOCO:
512**re of Perrhi qpa Or AU�Ihortze

POST OFFICE BOX 1056 • 85 PINEWOOD PLAZA DR.
GRANITE FALLS, NORTH CAROLINA 28630
[phone]
SAMPLE: Case Farms -Hatchery COLLECTION DATE: 1111512023
PERMITA- COLLECTION TIME: 14:15
ADDRESS: Case Farms Hatchery RECEIVED DATE: 11/15/2023
RECEIVED TIME: 14:55
REPORTED: 12114/2023
ANALYSIS
ANALYSIS
EFFLUENT
UNITS
DATE
ANALYST
BOD
552
mg/L
11/16/23
jdg
TSS
430
mg/L
11/17/23
jrg
NH3
22.64
mg/L
11/17/23
jrg
Fecal Coliform
52
/100mL
11/15/13
jsg
Conductivity
870
umhos/cm
11/17123
jsg
NO3-N
4.07
mg/L
11/20/23
jsg
TKN
87.00
mg/L
11/16/23
jdg
T. Nitrogen
91.07
mg/L
11/20/23
jdg
T. Phosphorus
9.39
mg/L
11/17/23
jdg
Chloride
meritech
TDS
meritech
LOG ID: 2311-244 REPORTED BY: NC CERTIFIED LAB # 50
Tony Gragg, Lab Supervisor

Meritech, Inc.
Environmental Laboratory
Laboratory Certification No.165
Contact: Cathy Gragg
Client: Water Tech Labs, Inc
5 Pinewood Plaza Drive
Granite Falls, NC 28630
Page 1
Report Date: 12/12/2023
Date Sample Rcvd: 11/16/2023
Meritech Work Order # 11162399 Sample: Case Farms -Effluent Grab 11/15/23
Parameters Resul Analysis DateReporting Limit Method
Total Dissolved Solids 494 mg/L 11/21/23 10 mg/L SM 2540C
Chloride 27.9 mg/L 11/21/23 0.5 mg/L SM 4500 Cl B
Meritech Work Order # 111623100 Sample: Case Farms-MW #3 Grab 11/15/23
parameters Result Analysis 12ate Reporting 1( unit Method
Total Dissolved Solids
109 mg/L
11/21/23
10 mg/L
SM 2540C
Chloride
24.1 mg/L
11/21/23
0.5 mg/L
SM 4500 Cl B
MBAS (as LAS 340)
<1.00 mg/L
11/17/23
1.00 mg/L
SM 5540 C
TOC
Attached
-
Formaldehyde*
<0.25 mg/L
11/28/23
0.25 mg/L
N3500
Arsenic, total
<0.010 mg/L
11/22/23
0.010 mg/L
EPA 200.7
Barium, total
0.153 mg/L
11/22/23
0.002 mg/L
EPA 200.7
Copper, total
<0.002 mg/L
11/22/23
0.002 mg/L
EPA 200.7
Iron, total
3.05 mg/L
11/22/23
0.010 mg/L
EPA 200.7
Manganese, total
0.074 mg/L
11/22/23
0.005 mg/L
EPA 200.7
Sodium, total
10.4 mg/L
11/22/23
0.200 mg/L
EPA 200.7
Potassium, total
2.64 mg/L
11/22/23
0.200 mg/L
EPA 200.7
Zinc, total
<0.010 mg/L
11/22/23
0.010 mg/L
EPA 200.7
EPA 8260
Attached
11/21/23
-
EPA 8260
642 Tamco Road, Reidsville, forth Carolina 27320
tel.[phone] fax.[phone]

Water Tech Labs
Method SM 20 Ed 4500-H-201 I
PH BENCHSHEET
Analysis
Date Time
Sample ID
Collection
Date Time
Results SU's
Analyst
-3-2
L) E'W
Buffer 4.00
*****
*****
of O L
Buffer 10.00
*****
*****
p
Ug D
Buffer 7.00 QC
*****
*****
�, UD
*****
Slope Efficiency
0 S
CASE FARMS
- 3- Z3
O/D
d
"Duplicate
o i9
Buffer 7.00 QC
3o
Buffer 4.00
*****
*****
6b
v Z
Buffer 10.00
*****
*****
d. GD
;V"
p 7-3
Buffer 7.00 QC
*****
*****
V-D
*****
Slope Efficiency
*****
*****
0�
CASE FARMS
_ o_
0 a o
. 6
7
" "Duplicate
0 U
Buffer 7.00 QC
z3
p 6D
Buffer 4.00
O702-
Buffer 10.00
*****
*****
6,ob
070
Buffer 7.00 QC
*****
*****
*****
Slope Efficiency
*****
*****
p 5—D
CASE FARMS
—Z -23
Q z
" Duplicate
a�
„
7-
r)9 j
Buffer 7.00 QC
7, o /
Buffer 4.00
*****
*****
Buffer 10.00
*****
*****
Buffer 7.00 QC
*****
*****
*****
Slope Efficiency
*****
*****
CASE FARMS
Duplicate
Buffer 7.00 QC
Buffer 4.00
*****
*****
Buffer 10.00
*****
*****
Buffer 7.00 QC
*****
*****
*****
Slope Efficiency
*****
*****
CASE FARMS
" " Duplicate
Buffer 7.00 QC
BUFFERS:
4.00 LOT # 8208112 EXP AUG 2024 WATER TECH LABS
7.00 LOT # 8210229 EXP OCT 2024 NCO50
10.00 LOT # 8206193 EXP JUN 2024

WATER TECH LARS,; INC
5 Pinewood Plaza Drive • P.O. Box 1056
Granite Falls, NC 28630
Phone [phone]
CLIENT: Case Farms Hatchery
PHONE M 828-438-6900
CHAIN OF CUSTODY
PERMIT #:
TYPE SAMPLE: II I
SAMPLERNAME:�c1�k G/ ��hl En(
Sample Collection Information
TYPE
CONTAINERS
ANALYSIS REQUIRED
Sample Location
FacilityName
DATE
TIME
TEMP. °C
Grab/
Composite
No
Plastic/
Glass
Effluent
I I �S�a
14 ; I S
I I
Grab
8
P
BOD, TSS, TDS, Fecal
I i
Cond, Cl, NO3, NH3, TKN
M. Well #3
Grab
12
PIG
TDS, Cl, MBAS, Formalde
I i
It
1
As,Cu,K,Zn,Na,Ba,Fe,Mn
I
It
I,
NH3, NO3, TP, Fecal, TOC
l i
i
It
VOC (Annual Nov.)
M. Well #4
��j�a�
`�.�S
I B
Grab
12
PIG
Same as#3
M. Well #5
�'I i�a3
I S
I b
Grab
12
PIG
Same as #3
S
elfin wished y:
D te:
Time:
Rec rved
Date:
Time:
Relinquished By:
Date:
Time:
eived By:
Dat :
ime:
PRESERVATION.
t5d'Cool 60C HNO3
Ji(( H2SO4 Dechlorinating Agent
(J NaOH (J Other
SAMPLE TEMP. @ LAB (°C) .q 0
1 - Chlorine Residual <(). f mg/I
NC CERTIFIED LAB # 50

wormirvCH MINSI.C.
POST OFFICE 80X 1056 • #5 PINEWOOD PLAZA DR.
GRANITE FALLS, NORTH CAROLINA 28630
[phone]
SAMPLE: Case Farms-Hatchery-MW#3 COLLECTION DATE: 11/15/2023
PERMITA- COLLECTION TIME., 12:45
ADDRESS: Case Farms Hatchery RECEIVED DATE: 11/1512023
RECEIVED TIME: 14:55
REPORTED: 12/14/2023
ANALYSIS
ANALYSIS
RESULTS
UNITS
DATE
ANALYST
NH3
<1.0
mg/L
11/17/23
jrg
Fecal Coliform
<1
/100ml-
11/16/13
jsg
Metals
meritech
NO3-N
2.79
mg/L
11/20/23
jsg
TKN
5.60
mg/L
11/16/23
jdg
T. Nitrogen
8.39
mg/L
11/20/23
jdg
T. Phosphorus
0.49
mg/L
11/17/23
jdg
Chloride
meritech
TDS
meritech
LOG ID: 2311-245 REPORTED BY: NC CERTIFIED LAB # 50
Tony Gragg, Lab Supervisor

Meritech, Inc.
Environmental Laboratory
Laboratory Certification No.165
Contact: Cathy Gragg
Client: Water Tech Labs, Inc
5 Pinewood Plaza Drive
Granite Falls, NC 28630
Page 1
Report Date: 12/12/2023
Date Sample Rcvd: 11/16/2023
Meritech Work Order #
Parameters
11162399 Sample: Case Farms -Effluent Grab
Result Analysis ate
Reporting Limit
11/15/23
Method
Total Dissolved Solids
494 mg/L
11/21/23
10 mg/L
SM 2540C
Chloride
27.9 mg/L
11/21/23
0,5 mg/L
SM 4500 Cl B
Meritech Work Order #
111623100 Sample: Case Farms-MW #3 Grab
11/15/23
Parameters
Result
Analysis Date
Reporting Limit
Method
Total Dissolved Solids
109 mg/L
11/21/23
10 mg/L
SM 2540C
Chloride
24.1 mg/L
11/21/23
0.5 mg/L
SM 4500 Cl B
MBAS (as LAS 340)
<1,00 mg/L
11/17/23
1.00 mg/L
SM 5540 C
TOC
Attached
-
Formaldehyde*
<0.25 mg/L
11/28/23
0.25 mg/L
N3500
Arsenic, total
<0.010 mg/L
11/22/23
0.010 mg/L
EPA 200.7
Barium, total
0.153 mg/L
11/22/23
0,002 mg/L
EPA 200.7
Copper, total
<0.002 mg/L
11/22/23
0.002 mg/L
EPA 200.7
Iron, total
3.05 mg/L
11/22/23
0.010 mg/L
EPA 2003
Manganese, total
0.074 mg/L
11/22/23
0,005 mg/L
EPA 200.7
Sodium, total
10.4 mg/L
11/22/23
0.200 mg/L
EPA 200.7
Potassium, total
2.64 mg/L
11/22/23
0,200 mg/L
EPA 200.7
Zinc, total
<0.010 mg/L
11/22/23
0.010 mg/L
EPA 200.7
EPA 8260
Attached
11/21/23
EPA 8260
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

M RI TECH, INC.
Environmental Laboratories
Laboratory Certification #165
;..
Client:
Water Tech Labs, Inc. Mcritecb ID#:
111623100
Project:
8260D
Analysis:
1 1/21/23
Client Sample ID:
Case Farms - MW #3 Analyst:
VWV
Sample Collection:
1 1/15/23
Dilution Factor:
1
Report Date:
11 /30/23
SW-846-8260D VOLATILE ORGANICS -Water
Acetone
<5.00 ug/L,
cis-1,3-Dichloropropene
<0,500 ug/L
Benzene
<0500 ug/L
trans-1,3-Dichloropropene
<0.500 ug/L
Bromobenzene
<0.500 ug/L
Ethanol
<50.0 ug/L
Bromodichloromethane
<0,500 ug/L
Ethyl benzene
<0,500 ug/L
Bromoehloromethane
<0,500 ug/L
Hoxachlorobutadiene
<0.500 ug/l,
Bromoform
<0.500 ug/L,
2-Hexanone
<1,00 ug/L
Bromomethane
<0.500 ug/L
I'sopropylbenzene
<0.500 ug/L
2-Butanone (MF.K)
< 3.00 ug/L
p-lsopropyltoluene
< 0.500 ug/L
n-Butylbenzene
<0,500 ug/L
Methylene chloride
<MOO ug/L
sec-Butylbenzene
<0.500 ug/L
Methly Isobutyl Ketone (MIBK)
< 0.500 ug/L
tort-Butylbenzene
<0.500 ug/L,
Naphthalene
<0,500 ug/L
Carbon Tetrachloride
<0.500 ug/L
n-Propylbenzene
<0.500 ug/L
Chlorobenzene
<0,500 ug/L
Styrene
<0,500 ug/L,
Chloroethane
<0.500 ug/L
1, 1, 1,2-Tetrachloroethane
<0.500 ug/L
Chloroform
<0,500 ug/L,
1,1,2,2-Tetrachloroethane
<0,500 ug/L
Chloromethane
<0,500 ug/L
Tetrachloroethane (PCE)
<0,500 ug/L
2-Chlorotohtene
<0,500 ug/L
Toluene
<0.500 ug/L
4-Clilorotoluene
<0,500 ug/L
1, 1, 1 -Trichloroethane
<0.500 ug/L
Dibromochloromethane
<0,500 ug/L
I,1,2»Trichloroethane
<0,500 ug/L
1,2-Dibromo-3-chloropropane
<0.500 ug/L
Trichloroethene(TCE)
<0.500 ug/L
1,2-Dibromoethane(ET3B)
<0,500 ug/L
1,2,3-Trichlorobenzene
<0.500 ug/L
Dibromomethane
<0,500 ug/L.
1,2,4-Trichlorobenzene
<0.500 ug/L
Dichlorodifluoromethane
<0.500 ug/L
1,2,3-Trichloropropane
<0.500 ug/L
l,l-Dichloroethane
<0.500 ug/L
Trichlorofluoromethane
<0.500 ug/L
1,2-Dichloroethane
< 0,500 ug/L
1,2,4-Trimethylbenzene
< 0.500 ug/L
1,4-Dichlorobenzene
<0.500 ug/L
1,3,5-T'rhnethylbenzene
<0.500 ug/L
1,2-Dichlorobenzeno
<0,500 ug/L
Vinyl acetate
< 1.00 ug/L
1,3-Dichlorohenzene
<0.500ug/L
Vinyl chloride
<0,500ug/L
l,l-Dichloroethene
<0.500 ug/L
m/p-Xylenes
< 1.00 ug/L
cis-1,2-Dichloroethane
<0.500 ug/L
o-Xylene
<0.500 ug/l,
trans-1,2-Dichloroethane
< 0.500 ug/L
1,2-Dichloropropane
<0.500 ug/L
Additional Compounds
1,3-Dichloropropane
< 0,500 ug/L
Methyl-tert-butyl ether (MTBE)
< 0.500 ug/L
2,2-Dichloropropane
<0.500 ug/L
Isopropyl ether(IPE)
<0,500 ug/L
1,1-Dichloropropene
< 0,500 ug/L
1,2-Dichloropropene
<0.500 ug/L
�\
I hereby certify that I have reviewed and approve these data. Laboratory Representative
642 Tamco Road * Reidsville, NC 27320
[phone] Ph " [e-mail]

ANALYTICAL SERVICES
Pace Analytical Services, LLC
P,O. Box 907
Madisonville, KY 42431
270.821.7375
www.pacelabs.corn
ANALYTICAL RESULTS
Lab Sample ID: 3114277-16 Sample Collection Date Time: 11/09/2023 08:02
Description: North Carolina SDWA 92699344016 111023 37 MW6 Sample Received Date Time: 11/21/2023 10:52
Conventional ChemistryAnalyses Madisonville
Analyto Result Flag Units MRL MDL Method Prepared Analyzed Analyst
Tula] Organic Carbon 0.6 mg/L 0.5 0.4 5310 C-2014 1112912023 11:30 12/01/2023 06:12 HMF
ANALYTICAL RESULTS
Lab Sample ID: 3114277-17 Sample Collection Date Time: 11/16/2023 08:30
Description: North Carolina SDWA 92699344017 111623 197 W4 Sample Received Date Time: 11/21/2023 10:52
Conventional Chemistry Analyses Madisonville
Analyto Result Flag Units MRL MDL Method Prepared Analyzed Anatyst
Total Organic Carbon 2.0 mg1 0.5 0.4 5310 C-2014 11/2912023 11:30 12/0112023 06:35 HMF
ANALYTICAL RESULTS
Lab Sample ID: 3114277-18 Sample Collection Date Time: 11/16/2023 08:15
Description: North Carolina SDWA 92699344018 111623 198 W5 Sample Received Date Time: 11/21/2023 10:52
Conventional Chemistry Analyses Madisonville
Analyte Result Flag Units MRL MDL Method Prepared Analyzed Analyst
Total Organic Carbon 4.9 mglL 0.5 0.4 5310 C-2014 11/29/2023 11:30 12J01r2023 06:52 HMF
ANALYTICAL RESULTS
Lab Sample ID: 3114277-19 Sample Collection Date Time: 1111512023 12:45
Description: North Carolina SDWA 92699 44019 111623 100 MW3 Sample Received Date Time: 11121/2 r 023 10:52
Conventional Chemistry Analyses Madisonville
Analyte Result Flag Units MRL MDL Method Prepared Analyzed Analyst
Total Organic Carbon 0.5 mg1L 0.5 0.4 5310 C-2014 11129/2023 11:30 12/0112023 08:02 HMF

Water Tech Labs
Method SM 20 Ed 4500-H-2011
Wastewater
PH BENCHSHEET
Analysis
Date Time
Sample ID
Collection
Date Time
Results SU's
Analyst
Buffer4.00
*****
*****
p z
Buffer 10.00
*****
*****
gt>
Buffer 7.00 QC
*****
*****
-7. ao
*****
Slope Efficiency
*****
*****
2 56
(lG2 r
/ -1 -2
/2Y-
13 zo
% uJ S
x
131
Jr.
3 S-V
Al W
/ S
7
-7•
K z
c • bZ>
--
. a
BUFFERS:
4.00 LOT # 8208112 EXP AUG 2024
7.00 LOT # 8210229 EXP OCT 2024
10.00 LOT # 8206193 EXP JUN 2024
* NON REPORTABLE FOR NPDES COMPLIANCE MONITORING
EXCEEDS HOLD TIME
DUPLICATE/S f 0.1 SU'S ✓

unrmii! lire Lfillgmc.
POST OFFICE BOX 1056 • N5 PINEWOOD PLAZA DR.
GRANITE FALLS, NORTH CAROLINA 28630
[phone]
SAMPLE: CaseFarms-Hatchery-MW#4 COLLECTION DATE: 11115/2023
PERMIT M COLLECTION TIME: 13:45
ADDRESS: Case Farms Hatchery RECEIVED DATE: 11/16/2023
RECEIVED TIME., 14:55
REPORTED: 12/14/2023
ANALYSIS
ANALYSIS
RESULTS
UNITS
DATE
ANALYST
NH3
<1.0
mg/L
11/17/23
jrg
Fecal Coliform
<1
/100ml-
11/15/13
jsg
Metals
meritech
NO3-N
3.94
mg/L
1211123
jsg
TKN
<1.0
mg/L
12/4123
jdg
T. Nitrogen
3.94
mg/L
12/4/23
jdg
T. Phosphorus
<0.16
mg/L
1211/23
jdg
Chloride
meritech
TDS
meritech
LOG ID: 2311-246 REPORTED BY:
yJ�N�'yC, CERTIFIED LAB # 50
oli
Tony Gragg, Lab Supervisor

Meritech, Inc,
Environmental Laboratory
Laboratory Certification No. 165
Page 2
Contact: Cathy Gragg
Report Date:
12/12/2023
Client: Water Tech Labs,
Inc
S Pinewood Plaza
Drive
Granite Falls, NC 28630
Date Sample Rcvd:
11/16/2023
Meritech Work Order #
111623101 Sample: Case
Farms-MW #4 Grab
11/15/23
Parameter
Result
Aj a his Date )ate
Reporting Lind
Metho
Total Dissolved Solids
97 mg/L
11/21/23
10 mg/L
SM 2540C
Chloride
18.1 mg/L
11/21/23
0.5 mg/L
SM 4500 Cl B
MEAS (as LAS 340)
<1.00 mg/L
11/17/23
1.00 mg/L
SM 5540 C
TOC
Attached
-
Formaldehyde*
<0.25 mg/L
11/28/23
0.25 mg/L
N3500
Arsenic, total
<0..010 mg/L
11/22/23
0.010 mg/L
EPA 200.7
Barium, total
0,205 mg/l.
11/22/23
0.002 mg/L
EPA 200.7
Copper, total
0.005 mg/L
11/22/23
0.002 mg/L
EPA 200.7
Iron, total
5.92 mg/L
11/22/23
OA10 rng/L
EPA 200.7
Manganese, total
0.146 mg/L
11/22/23
0.005 mg/L
EPA 200.7
Sodium, total
9.31 tog/L
11/22/23
0.200 mg/L
EPA 2003
Potassium, total
3.28 mg/L
11/22/23
0,200 mg/L
EPA 200.7
Zinc, total
0.025 mg/L
11/22/23
0.010 mg/L
EPA 200.7
EPA 8260
Attached
11/21/23
EPA 8260
Meritech Work Order #
111623102 Sample: Case Farms-MW #5 Grab
11/15/23
Parameters
r$�5
Analysis Date
Reporting Litnit
Method
Total Dissolved Solids
103 rng/L
11/21/23
10 mg/L
SM 2540C
Chloride
18.1 mg/L
11/21/23
0.5 mg/L
SM 4500 Cl B
MBAS (as LAS 340)
<1.00 mg/L
11/17/23
1.00 mg/L
SM 5540 C
TUC
Attached
-
Fortnaldehyde*
<0.25 mg/l.
11/28/23
0.25 mg/I.
N3500
Arsenic, total
<0.010 mg/L
11/22/23
0,010 mg/L
EPA 200.7
Barium, total
0.207 mg/L
11/22/23
0.002 mg/L
EPA 200.7
Copper, total
0.003 mg/L
11/22/23
0,002 mg/L
EPA 200.7
Iron, total
5.84 mg/L
11/22/23
0.010 mg/L
EPA 200.7
Manganese, total
0.142 mg/L
11/22/23
0,005 mg/L
EPA 200.7
Sodium, total
9.09 mg/L
11/22/23
0.200 mg/L
EPA 200.7
Potassium, total
2.87 mg/L
11/22/23
0.200 mg/L
EPA 200.7
Zinc, total
0.017 mg/L
11/22/23
0.010 mg/L
EPA 200.7
EPA 8260
Attached
;1/21/23
EPA 8260
hereby certify that I have reviewed and approve these data. 1 &qC wG1,(Y'1C Q(�
Laboratory Representative
642 Tainco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

NiERITtECH, INC.
Environmental Laboratories
" t ..
M y4.n
Laboratory Certification #165
eClient:
Water Tech Labs, Inc. Meritech IDO;
Project:
8260D Analysis:
Client Sample ID:
Case Farms - MW #4 Analyst:
Sample Collection:
11/15/23 Dilation Factor:
Report Date:
SW-846-8260D 'VOLATILE ORGANICS -Water
Acetone
< 5.00 ug/L
cis-1,3-Dichloropropene
Benzene
<0.500 ug/L
trans-1,3-Dichloropropene
Brornobenzene
< 0.500 ug/L
Ethanol
Bromodichloromethane
<0.500 ug1L
Ethyl benzene
Bromochloromethane
< 0,500 ug/L
Elexachlorobutadiene
Bromoform
<0.500 ug/L
2-I3exanone
Bromomethane
<0.500 ug/L
Isopropylbenzene
2-Butanone (MEK)
< 5.00 ug/L
p-Isopropyltoluene
n-Butylbenzene
<0,500 ug/L
Methylene chloride
sec-Butylbenzene
< 0,500 ug/L
Methly Isobutyl Ketone (MIRK)
tent-Butylbenzene
<0.500 ug/L
Naphthalene
Carbon Tetrachloride
< 0.500 ug/L
n-Propylbenzene
Chlorobenzene
< 0,500 ug/L
Styrene
Chloroethane
< 0.500 ug/L
1,1,1,2-Tetrachtcroethane
Chloroform
<0,500 ug/L
1,1,2,24'et'rachloroethane
Chloromethane
<0.500 ug/L,
Tetrachloroethene(PCE)
2-Ch1orotoluene
< 0.500 ug/L
Toluene
4-Chlorotoluene
< 0.500 ug/L
1, 1, I-Trichloroethane,
Dibromochloromethane
<0,500 ug/L
1,t,2-Trlchloroothanc
1,2-Dibromo-3-chloropropane
< 0.500 ug/L
Trichloroethene (TCE)
1,2-Dibromoethane(EDB)
< 0.500 ug/L
1,2,3-Trichlorobenzene
Dibromoutethane
< 0,500 ug/L
1,2,4-Trichlorobenzene
Dichloroditluoromethane
< 0.500 ug/L
1,2,3-Trichloroprropane
1, t -Dichloroethane
<0,500ug/L
Trichiorofluoromethane
1,2-Dichloroethane
< 0.500 ug/L
1,2,4-Trimethylbenzene
1,4-Dichlorobenzone
<0.500 ug/L
1,3,5-Trimethylbenzene
1,2-Dichlorobenzene
< 0.500 ug/L
Vinyl acetate
1,3-Dichlorobenzene
<0.500 ug/L
Vinyl chloride
1,1-Dichloroethene
< 0,500 ug/L
m/p-Xylenes
cis-1,2-Dichloroethene
<0.500 ug/L
o-Xylene
trans-1,2-Dichloroethene
< 0.500 ug/L
1,2-Dichloropropatie
<0.500ug/L
AddltionalComnotugis
1,3-Dichloropropane
< 0.500 ug/L
Mothyl-tert-butyl ether (MTBE)
2,2-Dichloropropatie
< 0.500 ug/L
Isopropyl ether (LPE)
1, 1 -Dichloropropene
< 0.500 ug/L
1,2-Dichloropropene
<0,500 ug/L
I hereby certify that I have reviewed and approve these data.
642 Tamco Road * Reidsville, NC 27320
[phone] Ph * [e-mail]
111623101
11/21/23
VWV
11 /30/23
0.500 ug/L
< 0.500 ug/L
< 50.0 ug/L
<0,500 ug/L
< 0.500 ug/L
< 1.00 ug/L
<0.500 ug/L
<0.500 ug/L
<0.500 ug/L
< 0.500 ug/L
< 0.500 ug/L
< 0.500 ug/L
0.500 ug/L
0.500 ug/L
<0,500 ug/L
<0.500 ug/L
< 0,500 ug/L
< 0.500 ug/L
< 0.500 ug/L,
< 0.500 ug/L
0.500 ug/L
<0,500 ug/L
< 0.500 ug/L
<0.500 ug/I',
<0.500 ug/L
< 0,500 ug/L
< 1.00 ug/l,
<0,500 ug/L
< 1.00 ug/L
<0,500 ug/L
< 0,500 ug/L
< 0.500 ug/L
Laboratory Representative

ANALYTICAL SERVICES
Pace Analytical Services, LLC
P.O. Box 907
Madisonville, KY 42431
270.821.7375
www.parelabs.corn
l---AM4,YTICAL RESULTS
Lab Sample ID: 3114277-20 Sample Collection Date Time: 11/15/2023 13A5
description: North Carolina SDWA 92699 020:111623 101 MW4 r Sample Received Date Time: 11/21/2023 10:52
Conventional Chemistry Analyses Madisonville
Analyse Result Flag Units MRL MDL Method Prepared Analyzed Analyst
Total Organic Carbon 0.5 mglL 0.5 0.4 5310 C-2014 11/29/2023 11:30 12/0112023 08:16 HMF
ANALYTICAL RESULTS
Lab Sample ID: 3114277-21 Sample Collection Date Time: 11/15/2023 13:15
Description: North Carolina SDWA 92699344021 111623102 MW5 Sample Received Date Time: 11121/2023 10:52
Conventional Chemistry Analyses Madisonville
Analyte Result Flag Unlls MRL MDL Method Prepared Analyzed Analyst
Total Organic Carbon 0.6 mglL 0.5 0.4 5310 C-2014 11/29/2023 11;30 12/01/2023 08:29 HMF
ANALYTICAL RESULTS
Lab Sample ID: 3114277-22 Sample Collection Date Time: 11/13/2023 10:35
Description: North Carolina SDWA 92699344022 111423 36 FIELD Sample Received Date Time: 11/21/2023 10:52
BLANK
Conventional Chemistry Analyses Madisonville
Analyte Result Flag Units MRL MDL Method Prepared Analyzed Analyst
Dissolved Organic Carbon ND u mg1L 0.5 0.3 5310 C-2014 11/13/2023 10:35 11/2212023 07:11 HMF
ANALYTICAL RESULTS
Lab Sample ID: 3114277-23 Sample Collection Date Time: 11/13/2023 10A0
Description: North Carolina SDWA 92699344023 111423 37 LIT4 Sample Received Date Time: 11/21/2023 10:52
Conventional chemistry Analyses Madisonville
Analyte Result Flag Units MRL MDL Method Prepared Analyzed Analyst
Dissolved Organic Carbon 6.3 mg1L 0.5 0.3 5310 C-2014 11/1312023 10:40 11/22/2023 07:34 HMF

Water Tech Labs
Method SM 20 Ed 4500-H-2011
Wastewater
PH BENCHSHEET
Analysis
Date Time
Sam le ID
Collection
Date Time
Results SU's
Analyst
Buffer 4.00
*****
*****
oft 2_,
Buffer 10.00
*****
*****
. OD
ga
Buffer 7.00 QC
*****
*****
7 "
*****
Slope Efficiency
*****
*****
t 3 Z0
guJ.S
1/31
S-
S-
3 S—D
a/
/3 S
5. 7
n E-
s-
7.
KZ
C 6U
—7z.A
BUFFERS:
4.00 LOT # 8208112 EXP AUG 2024
7.00 LOT # 8210229 EXP OCT 2024
10.00 LOT # 8206193 EXP JUN 2024
* NON REPORTABLE FOR NPDES COMPLIANCE MONITORING
EXCEEDS HOLD TIME
DUPLICATE/S f 0.1 SU'S._

mrsPROrcH Lfigg.inc.
POST OFFICE BOX 1056 - #5 PINEWOOD PLAZA DR.
GRANITE FALLS, NORTH CAROLINA 28630
[phone]
SAMPLE., Case Farms-Hatchery-MW#5 COLLECTION DATE: 11/15/2023
PERMIT A, COLLECTION TIME: 13:15
ADDRESS: Case Farms Hatchery RECEIVEDDATE: 11/15/2023
RECEIVED TIME: 14:55
REPORTED: 12114/2023
ANALYSIS
ANALYSIS
RESULTS
UNITS
DATE
ANALYST
NH3
<1.0
mg/L
11/17/23
jrg
Fecal Coliform
<1
/100mL
11/15/13
jsg
Metals
meritech
NO3-N
4.51
mg/L
12/1123
jsg
TKN
<1.0
mg/L
12/4123
jdg
T. Nitrogen
4.51
mg/L
1214/23
jdg
T. Phosphorus
<0.16
mg/L
12/1/23
jdg
Chloride
meritech
TDS
meritech
LOG 1D: 2311-247 REPORTED BY: NC CERTIFIED LAB # 50
foll ER
Tony Gragg, Lab Supervisor

Meritech, Inc.
Environmental Laboratory
Laboratory Certification No. 165
Page 2
Contact: Cathy Gragg
Report Date:
12/12/2023
Client: Water Tech Labs,
Inc
5 Pinewood Plaza
Drive
Granite Falls, NC 28630
Date Sample Rcvd:
11/16/2023
Meritech Work Order #
111623101 Sample:
Case Farms-MW #4 Grab
11/15/23
Parameters
Result
Analysis Date
Reporting Urnt
Method
Total Dissolved Solids
97 mg/L
11/21/23
10 mg/L
SM 2540C
Chloride
18.1 mg/L
11/21/23
0.5 mg/L
SM 4500 Cl B
MBAS (as LAS 340)
<1.00 mg/L
11/17/23
1,00 mg/L
SM 5540 C
TOC
Attached
-
Formaldehyde*
<0.25 mg/L
11/28/23
0.25 mg/L
N3500
Arsenic, total
<0.01.0 mg/L
11/22/23
0.010 rng/L
EPA 200.7
Barium, total
0.205 mg/L
11/22/23
0.002 mg/L
EPA 200.7
Copper, total
0.005 rng/L
11/22/23
0.002 mg/L
EPA 200.7
Iron, total
5.92 mg/L
11/22/23
0,010 mg/L
EPA 200.7
Manganese, total
0,146 mg/L
11/22/23
0.005 mg/L
EPA 200.7
Sodium, total
9.31 mg/L
11/22/23
0.200 mg/L
EPA 200.7
Potassium, total
3.28 mg/L
11/22/23
0.200 mg/L
EPA 200.7
Zinc; total
0.025 mg/L
11/22/23
0.010 mg/L
EPA 200.7
EPA 8260
Attached
11/21/23
EPA 8260
Meritech Work Order #
111623102 Sample: Case Farms-MW #5 Grab
11/15/23
Parameters
Result
Analysis Date
Reporting Lhnit
Method
Total Dissolved Solids
103 rng/L
11/21/23
10 mg/L
SM 2540C
Chloride
181 mg/L
11/21/23
0.5 mg/L
SM 4500 Cl B
MBAS (as LAS 340)
<1.00 mg/L
11/17/23
1.00 mg/L
SM SS40 C
TOC
Attached
-
Formaldehyde*
<0.25 mg/L
11/28/23
0.25 mg/L
N3500
Arsenic, total
<0.010 rng/L
11/22/23
0.010 mg/L
EPA 200.7
Barium, total
0.207 mg/L
11/22/23
0.002 mg/L
EPA 200.7
Copper, total
0.003 mg/L
11/22/23
0.002 mg/L
EPA 200.7
Iron, total
5.84 mg/L
11/22/23
0,010 mg/L
EPA 200.7
Manganese, total
0142 mg/L
11/22/23
0.005 mg/L
EPA 200.7
Sodium, total
9.09 mg/L
11/22/23
0.200 mg/L
EPA 200.7
Potassium, total
2.87 mg/L
11/22/23
0.200 mg/L
EPA 2003
Zinc, total
0.017 mg/L
11/22/23
0.010 mg/L
EPA 200.7
EPA 8260
Attached
;11/21/23
EPA 8260
* Results not for regulatory purposes
1 hereby certify that 1 have reviewed and approve these data.
Laboratory Representative
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

M RI TECH, INC.
Environmental Laboratories
+
Laboratory Certification #165
p ,
Client:
Water Tech Labs, Inc. Meritech ip#:
Project:
8260D Analysis:
Client Sample ID:
Case Farms - MW #5 Analyst:
Sample Collection:
11/15/23 Dilation Factor:
Repot Date:
SW-846-8260D VOLATILE ORGANICS - Water
Acetone
<5.00 ug/L
cis-1,3-Dichloropropene
Benzene
< 0,500 ug/L
trans-1,3-Dichloropropene
Brornobenzene
< 0.500 ug/L
Ethanol
Bromodichloromethane
<0,500 ug/L
Ethyl benzene
Bromochloromethane
<0.500 ug/L
I-Iexachlorobutadiene
Bronaform
<0,500 ug/L
2-1-lexanone
Bromomethane
<0,500 ug/L
Isopropylbenzene
2-Butanone(MEK)
<5.00 ug/L
p-lsopropyltoluene
n-Butylbenzene
<0.500 ug/L
Methylene chloride
sec-Butylbenzene
< 0.500 ug/L
Methly Isobutyl Ketone (MIBK)
tort-Butylbenzene
< 0.500 ug/L
Naphthalene
Carbon Tetrachloride
< 0.500 ug/L
n-Propylbenzene
Chlorobenzene
<0,500 ug/L
Styrene
Chloroethane
<0.500 ug/L
1,1,1,2-Tetrachloroethane
Chloroform
<0,500 ug/L
1,1,2,2-Tetrachloroethane
Chloromethane
< 0.500 ug/L
Tetracbloroethane (PCB)
2-Chlootoluene
< 0,500 ug/L
Toluene
4-Chlorotoluene
<OS00 ug/L
1, 1, t-Trichloroethane
Dibromochlorotilethane
< 0,500 ug/L
1,1,2-Trichloroethane
1,2-Dibrono-3-chloroproparte
< MOO ug/L
Trichloroethene(Tep
1,2-Dibromoethane (EDB)
< 0.500 ug/L
1,2,3-Trichlorobenzene
Dibromomethane
<0.500 ug/L
1,2,4-Trichlorobenzene
Dichlorodifluoromethane
<0,500 ug/L
1,2,3-Trichloropropane,
l,l-Dichloroethane
<0.500 ug/L
TriChlorofluo•omethane
1,2-Dichloroethane
<0.500 ug/L
1,2,4-Trimethylbenzene
1,4-Diehlorobenzene
< 0.500 ug/L
1,3,5-Trimethylbenzeno
1,2-Dichlorobenzone
<0.500 ug/L
Vinyl acetate
1,3-Dichlorobenzene
<0.500 ug/L
Vinyl chloride
1,1-Dichloroethane
<0,500 ug/L
m/p-Xylenes
cis-1,2-Dichloroethene
<0.500 ug/L
o-Xylene
trans-1,2-Dichloroethene
<0,500 ug/L
1,2-Dichloropropane
<0.500 trg/L
AdditionalConpounds
1,3-Dichloropropane
< 0,500 ug/L
Mothyl-test-butyl ether (MTBE)
2,2-Dichloropropene
<0.500 ug/I,
Isopropyl ether (IPE)
1, 1 -Dich loropropene
<0.500 ug/L
1,2-Dichloropropene
<0,500 ug/L
L hereby certify that I have reviewed and approve these data.
642 Tamco Road * Reidsville, NC 27320
[phone] Ph * [e-mail]
111623102
11/21/23
VWV
11/30/23
< 0.500 ug/L
<0,500 ug/L
< 50.0 ug/L
<0,500 ug/L
< 0.500 ug/L
< 1.00 ug/L
< 0.500 ug/L
<0.500 ug/L
<0,500 ug/L
< 0.500 ug/L
<0.500 ug/L
< 0,500 ug/L
< 0.500 ug/L
<0,500 ug/I,
< 0.500 ug/L
< 0.500 ug/l,
< 0.500 ug/L
<0,500 ug/L,
<0,500 ug/L
<0,500 ug/L
< 0.500 ug/L
< 0.500 uO,
< 0.500 ug/L
< 0,500 ug/L
<0.500 ug/L
<0.500 ug/L
< 1.00 uWL,
< 0.500 ug/L
< 1.00 ug/L
<0,500 ug/L
<0,500 ug/L
< 0.500 ug/L
Laboratory Representative

ANALYTICAL 57 RVICES
Pace Analytical Services, LLC
P.O. Box 907
Madisonville, KY 42431
270.821.7375
www.pacelabs.corn
ANALYTICAL RESULTS
Lab Sample ID: 3114277-20 Sample Collection Date Time: 11/15/2023 13:45
Description: North Carolina SOWA 92699344020:111623 101 MW4 Sample Received Date Time: 11/21/2023 10:52
Conventional Chemistry Analyses Madisonville
Analyte Result Flag Units h1RL MDL Method Prepared Analyzed Analyst
Total Organic Carbon 0.5 mg1L 0.5 0.4 5310 C-2014 1112012023 11:30 12/0112023 08:16 HNIF
r —" N LY_ ICAL RESULTS
Lab Sample ID: 3114277-21 Sample Collection Date Time: 11/15/2023 13:15
Description: North Carolina SDWA 926 9344021 111623102 MW5 Sample Received Date Time: 11121/2023 10:52
Conventional Chemistry Analyses Madisonville
Analyte Result Flag Units MRL MDL Method Prepared Analyzed Analyst
Total Organic Carbon 0.6 mg/L 0.5 0.4 5310 C-2014 1112912023 1130 12101I2023 W29 HMF
ANALYTICAL RESULTS
Lab Sample ID: 3114277-22 Sample Collection Date Time: 11/13/2023 10:35
Description: North Carolina SDWA 92699344022 111423 36 FIELD Sample Received Date Time: 11/21/2023 10:52
BLANK
Conventional Chemistry Analyses Madisonville
Analyte Result Flag Units MftL MDL Method Prepared Analyzed Analyst
Dissolved Organic Carbon ND u mg1L 0.5 0.3 5310 C-2014 11/13/2023 10:35 11/22/2023 07:11 HMF
ANALYTICAL RESULTS
Lab Sample ID: 3114277-23 Sample Collection Date Time: 11/13/2023 10:40
Description: North Carolina SDWA 92699344023 111423 37 UT4 Sample Received Date Time: 11/21/2023 10:52
Conventional Chemistry Analyses Madisonville
Analyte Result Flag Units MRL MDL Method Prepared Analyzed Anafysl
Dissolved Organic Carbon 6.3 mg1L 0.5 0.3 5310 C-2014 11113/2023 10:40 11/2212023 07:34 HMF

Water Tech Labs
Method SM 20 Ed 4500-H-2011
Wastewater
PH BENCHSHEET
Analysis
Date Time
Sample ID
Collection
Date Time
Results SU's
Analyst
3
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ANALYTICAL G)
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Sample Summary Table
Report Number: 23-325-0004
Client Project Description: Case Farms Hatchery
11-15-23
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
63990
Zone 1
Solids
11/21/2023
6010D
WP MTN
63990
Zone 1
Solids
11/21/2023
SW-7471B
WP MTN
63991
Zone 2
Solids
11/21/2023
SW-7471B
WP MTN
63991
Zone 2
Solids
11/21/2023
6010D
WP MTN
63992
Zone 3
Solids
11/21/2023
SW-7471B
WP MTN
63992
Zone 3
Solids
11/21/2023
6010D
WP MTN
63993
Zone 4
Solids
11/21/2023
6010D
WP MTN
63993
Zone 4
Solids
11/21/2023
SW-7471B
WP MTN
WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN
Page 2 of 9

e
Waypoi nt,. 7621 ain 804-7 Road, Richmond, 27 -6446
w r✓Y N V/ Main 804-743-9901 °Fax [phone]
ANALYTICAL www.waypointanalytical.com
15506
Water Tech Labs Inc Project Case Farms Hatchery
Tony Gragg
PC Box 1056 Information : I1-15-23
5 Pinewood Plaza Dr
Granite Falls , NC 28630
Report Number : 23-325-0004
REPORT OFANAL YSIS
Report Date : 12/04/2023
Received : 11/21/2023
Brand! Watson
Lab No : 63990 Matrix: Solids
Sample ID : Zone 1 Sampled:
Test Results Units MQL DF Date/Time By Analytical
Analyzed Method
Copper
11.6
mg/Kg
0.500
1
11/30/23
20:37
BKN
6010D
Zinc
27.4
mg/Kg
1.25
1
11/30/23
20:37
BKN
6010D
Cadmium
0.415
mg/Kg
0.100
1
11/30/23
20:37
BKN
6010D
Chromium
11.8
mg/Kg
0.250
1
11/30/23
20:37
BKN
6010D
Nickel
5.35
mg/Kg
0.250
1
11/30/23
20:37
BKN
6010D
Lead
12.2
mg/Kg
0.300
1
11/30/23
20:37
BKN
6010D
Arsenic
1.62
mg/Kg
0.500
1
11/30/23
20:37
BKN
6010D
Mercury
<0.167
mg/Kg
0.167
1
12/01/2311:32
FDS
SW-7471B
Selenium
<0.500
mg/Kg
0.500
1
11/30/23
20:37
BKN
6010D
Molybdenum
0.488
mg/Kg
0.250
1
11/30/23
20:37
BKN
6010D
Qualifiers/ DF Dilution Factor
Definitions
MQL Method Quantitation Limit
Page 3 of 9

Waypoint_
ANALYTICAL
15506
Water Tech Labs Inc
Tony Gragg
PO Box 1056
5 Pinewood Plaza Dr
Granite Falls , NC 28630
Report Number:23-325-0004
Lab No : 63991
Sample ID : Zone 2
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.way poi n to nal ytical.com
Project Case Farms Hatchery
Information : 11-15-23
REPORTOFANAL YSIS
Report Date : 12/04/2023
Received : 11/21/2023
Brand! Watson
Matrix: Solids
Sampled:
Test
Results
Units
MDL
DF
Date/Time
Analyzed
By
Analytical
Method
Copper
7.66
mg/Kg
0.500
1
11/30/23 20:42
BKN
6010D
Zinc
19.3
mg/Kg
1.25
1
11/30/23 20:42
BKN
6010D
Cadmium
0.242
mg/Kg
0.100
1
11/30/23 20:42
BKN
6010D
Chromium
8.37
mg/Kg
0.250
1
11/30/23 20:42
BKN
6010D
Nickel
4.06
mg/Kg
0.250
1
11/30/23 20:42
BKN
6010D
Lead
12.7
mg/Kg
0.300
1
11/30/23 20:42
BKN
6010D
Arsenic
1.28
mg/Kg
0.500
1
11/30/23 20:42
BKN
6010D
Mercury
<0.179
mg/Kg
0.179
1
12/01/2311:33
FDS
SW-7471B
Selenium
<0.500
mg/Kg
0.500
1
11/30/23 20:42
BKN
6010D
Molybdenum
0.320
mg/Kg
0.250
1
11/30/23 20:42
BKN
6010D
Qualifiers/ DF Dilution Factor
Definitions
MQL Method Quantitation Limit
Page 4 of 9

s
•
WaypoIntu
7621 Win
ne Road, Richmond, 3237
�j
27 -6446
Main 804-743-9401 °Fax [phone]
80
ANALYTICAL
www.waypointanalytical.com
15506
Water Tech Labs Inc
Project
Case Farms
Hatchery
Tony Gragg
Report Date : 12/04/2023
PO Box 1056
Information: 11-15-23
Received : 11/21/2023
5 Pinewood Plaza Dr
Granite Falls , NC 28630
&`ts
Report Number :23.325.0004
REPORTOFANALYSIS
Brands Watson
Lab No : 63992
Matrix: Solids
Sample ID : Zone 3
Sampled:
Test
Results
Units
MQL
DF
Date ITime
By Analytical
Analyzed
Method
Copper
14.1
mg/Kg
0.500
1
11/30/23 20:58
BKN 6010D
Zinc
32.0
mg/Kg
1.25
1
11/30/23 20:58
BKN 6010D
Cadmium
0.575
mg/Kg
0.100
1
11/30/23 20:58
BKN 6010D
Chromium
13.1
mg/Kg
0.250
1
11/30/23 20:58
BKN 6010D
Nickel
6.02
mg/Kg
0.250
1
11/30/23 20:58
BKN 6010D
Lead
11.7
mg/Kg
0,300
1
11/30/23 20:58
BKN 6010D
Arsenic
1.93
mg/Kg
0.500
1
11/30/23 20:58
BKN 6010D
Mercury
<0.177
mg/Kg
0.177
1
12/01/2311:35
FDS SW-7471B
Selenium
<0.500
mg/Kg
0.500
1
11/30/23 20:58
BKN 6010D
Molybdenum
0.506
mg/Kg
0.250
1
11/30/23 20:58
BKN 6010D
Qualifiers/ DF Dilution Factor
Definitions
MQL Method Quantitation Limit
Page 5 of 9

yyLL
0.
Wayp®A n�_ 7621 ain 80 -7 Road, Richmond, 27 -6446
Main 804-743.9401 0Fax 804-27i-6446
ANALYTICAL www.waypointanalytical.com
15506
Water Tech Labs Inc Project Case Farms Hatchery
Tony Gragg
PO Box 1056 Information: 11-15-23
5 Pinewood Plaza Dr
Granite Falls , NC 28630
Report Number: 23-325-0004
REPORT OFANAL YSIS
Report Date : 12/04/2023
Received : 11/21/2023
(�/W�✓�L testy
Brand! Watson
Lab No : 63993 Matrix: Solids
Sample ID : Zone 4 Sampled:
Test Results Units MOIL DF Date l Time By Analytical
Analyzed Method
Copper
10.5
mg/Kg
0.500
1
11/30/23 21:04
BKN
6010D
Zinc
35.7
mg/Kg
1.25
1
11/30/23 21:04
BKN
6010D
Cadmium
0.658
mg/Kg
0.100
1
11/30/23 21:04
BKN
6010D
Chromium
9.54
mg/Kg
0.250
1
11/30/23 21:04
BKN
6010D
Nickel
4.99
mg/Kg
0.250
1
11/30/23 21:04
BKN
6010D
Lead
13.4
mg/Kg
0.300
1
I1/30/23 21:04
BKN
6010D
Arsenic
1.96
mg/Kg
0.500
1
11/30/23 21:04
BKN
6010D
Mercury
<0.180
mg/Kg
0.180
1
12/01/2311:36
FDS
SW-7471B
Selenium
<0.500
mg/Kg
0.500
1
11/30/23 21:04
BKN
6010D
Molybdenum
_ 0.468
mg/Kg
0.250
1
11/30/23 21:04
BKN
6010D
Qualifiers/ DF Dilution Factor
Definitions
MQL Method Quantitation Limit
Page 6 of 9