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Home My WebLink AboutNCG550336_Lab Analysis Data_20240221#=CL# February 13, 2024 LIMS USE: FR - ONE CLIENT LIMS OBJECT ID: 92711767 92711767 Project: Pace Project No.: RE: One Time Client Private Small Jobs Huntersville, NC 28078 STUART SAMPLING EVENT Dear One Client: Enclosed are the analytical results for sample(s) received by the laboratory on February 06, 2024. The results relate only to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report. The test results provided in this final report were generated by each of the following laboratories within the Pace Network: • Pace Analytical Services - Asheville • Pace Analytical Services - Charlotte • Pace Analytical Services - Ormond Beach If you have any questions concerning this report, please feel free to contact me. Sincerely, Ashari Taylor-Watson ashari.taylor-watson@pacelabs.com Project Manager 704-977-0939 Enclosures REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 1 of 11 #=CP# CERTIFICATIONS Pace Project No.: Project: 92711767 STUART SAMPLING EVENT Pace Analytical Services Ormond Beach 8 East Tower Circle, Ormond Beach, FL 32174 Alaska DEC- CS/UST/LUST Alabama Certification #: 41320 California Certification# 3096 Colorado Certification: FL NELAC Reciprocity Connecticut Certification #: PH-0216 Delaware Certification: FL NELAC Reciprocity DoD-ANAB #:ADE-3199 Florida Certification #: E83079 Georgia Certification #: 955 Guam Certification: FL NELAC Reciprocity Hawaii Certification: FL NELAC Reciprocity Illinois Certification #: 200068 Indiana Certification: FL NELAC Reciprocity Kansas Certification #: E-10383 Kentucky Certification #: 90050 Louisiana Certification #: FL NELAC Reciprocity Louisiana Environmental Certificate #: 05007 Maine Certification #: FL01264 Maryland Certification: #346 Massachusetts Certification #: M-FL1264 Michigan Certification #: 9911 Mississippi Certification: FL NELAC Reciprocity Missouri Certification #: 236 Montana Certification #: Cert 0074 Nebraska Certification: NE-OS-28-14 New Hampshire Certification #: 2958 New Jersey Certification #: FL022 New York Certification #: 11608 North Carolina Environmental Certificate #: 667 North Carolina Certification #: 12710 North Dakota Certification #: R-216 Ohio DEP 87780 Oklahoma Certification #: D9947 Pennsylvania Certification #: 68-00547 Puerto Rico Certification #: FL01264 South Carolina Certification: #96042001 Tennessee Certification #: TN02974 Texas Certification: FL NELAC Reciprocity US Virgin Islands Certification: FL NELAC Reciprocity Virginia Environmental Certification #: 460165 West Virginia Certification #: 9962C Wisconsin Certification #: 399079670 Wyoming (EPA Region 8): FL NELAC Reciprocity Pace Analytical Services Charlotte South Carolina Laboratory ID: 99006 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 North Carolina Drinking Water Certification #: 37706 North Carolina Field Services Certification #: 5342 North Carolina Wastewater Certification #: 12 South Carolina Laboratory ID: 99006 South Carolina Certification #: 99006001 South Carolina Drinking Water Cert. #: 99006003 Florida/NELAP Certification #: E87627 Kentucky UST Certification #: 84 Louisiana DoH Drinking Water #: LA029 Virginia/VELAP Certification #: 460221 Pace Analytical Services Asheville 2225 Riverside Drive, Asheville, NC 28804 Florida/NELAP Certification #: E87648 North Carolina Drinking Water Certification #: 37712 North Carolina Wastewater Certification #: 40 South Carolina Laboratory ID: 99030 South Carolina Certification #: 99030001 Virginia/VELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 2 of 11 #=SA# SAMPLE ANALYTE COUNT Pace Project No.: Project: 92711767 STUART SAMPLING EVENT Lab ID Sample ID Method Analytes Reported LaboratoryAnalysts 92711767001 001 EPA 200.8 1 PASI-OBSL Colisure 2 PASI-CKDF EPA 353.2 Rev 2.0 1993 2 PASI-ANCF PASI-A = Pace Analytical Services - Asheville PASI-C = Pace Analytical Services - Charlotte PASI-O = Pace Analytical Services - Ormond Beach REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 3 of 11 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92711767 STUART SAMPLING EVENT Sample:001 Lab ID:92711767001 Collected:02/05/24 11:25 Received:02/06/24 09:50 Matrix:Drinking Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit Analytical Method: EPA 200.8 Pace Analytical Services - Ormond Beach 200.8 MET ICPMS Drinking Water Lead ND ug/L 02/13/24 11:54 7439-92-11.0 1 Analytical Method: Colisure Preparation Method: Colisure Pace Analytical Services - Charlotte Total Coliform (P/A) CHT Total Coliforms PRESENT 02/07/24 17:3102/06/24 17:141 E.coli ABSENT 02/07/24 17:3102/06/24 17:141 Analytical Method: EPA 353.2 Rev 2.0 1993 Pace Analytical Services - Asheville 353.2 Nitrogen, NO2/NO3 DW Nitrogen, Nitrate 3.5 mg/L 02/07/24 01:04 14797-55-80.040 1 Nitrogen, Nitrite ND mg/L 02/07/24 01:04 14797-65-00.040 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 02/13/2024 05:35 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 4 of 11 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92711767 STUART SAMPLING EVENT Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. QC Batch: QC Batch Method: Analysis Method: Analysis Description: 988711 EPA 200.8 EPA 200.8 200.8 MET No Prep Drinking Water Laboratory:Pace Analytical Services - Ormond Beach Associated Lab Samples:92711767001 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:5436357 Associated Lab Samples:92711767001 Matrix:Water Analyzed Lead ug/L ND 1.0 02/13/24 12:00 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 5436358LABORATORY CONTROL SAMPLE: LCSSpike Lead ug/L 46.550 93 85-115 Parameter Units MS Result % Rec Limits Qual% RecConc. 5436353MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 35857432001 5436354 MSD Result MSD % Rec RPD MSDMS Spike Conc. Lead ug/L 50 92 70-13093 1500.00025 U mg/L 46.1 46.5 Parameter Units MS Result % Rec Limits Qual% RecConc. 5436355MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 60446497001 5436356 MSD Result MSD % Rec RPD MSDMS Spike Conc. Lead ug/L 50 92 70-13092 1502.3 48.5 48.1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 02/13/2024 05:35 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 5 of 11 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92711767 STUART SAMPLING EVENT Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. QC Batch: QC Batch Method: Analysis Method: Analysis Description: 830490 EPA 353.2 Rev 2.0 1993 EPA 353.2 Rev 2.0 1993 353.2 Nitrogen, NO2/NO3 DW Laboratory:Pace Analytical Services - Asheville Associated Lab Samples:92711767001 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:4292521 Associated Lab Samples:92711767001 Matrix:Water Analyzed Nitrogen, Nitrate mg/L ND 0.040 02/07/24 01:02 Nitrogen, Nitrite mg/L ND 0.040 02/07/24 01:02 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 4292522LABORATORY CONTROL SAMPLE: LCSSpike Nitrogen, Nitrate mg/L 1.51.5 102 90-110 Nitrogen, Nitrite mg/L 1.01 104 90-110 Parameter Units MS Result % Rec Limits Qual% RecConc. 4292523MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 92711767001 4292524 MSD Result MSD % Rec RPD MSDMS Spike Conc. Nitrogen, Nitrate mg/L 1.5 110 90-11094 51.53.5 5.1 4.9 Nitrogen, Nitrite mg/L 1 103 90-110104 11ND1.0 1.0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 02/13/2024 05:35 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 6 of 11 #=QL# QUALIFIERS Pace Project No.: Project: 92711767 STUART SAMPLING EVENT DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL - Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean-Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as "Total" may vary slightly from the sum of the reported component parameters. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 02/13/2024 05:35 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 7 of 11 #=CR# QUALITY CONTROL DATA CROSS REFERENCE TABLE Pace Project No.: Project: 92711767 STUART SAMPLING EVENT Lab ID Sample ID QC Batch Method QC Batch Analytical Method Analytical Batch 92711767001 988711001EPA 200.8 92711767001 830784 830785001ColisureColisure 92711767001 830490001EPA 353.2 Rev 2.0 1993 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 02/13/2024 05:35 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 8 of 11 Page 9 of 11 Page 10 of 11 Page 11 of 11