NCG210444_2024 DMR_20240220

NCDEQ Division of Energy, Mineral and Land Resources
Stormwater Discharge Monitoring Report (DMR) Form for NCG080000
Transit and Transportation
Click here for instructions
Complete,sign,scan and submit the DMR via the Stormwater NPDES Permit Data Monitoring Report(DMR) Upload form within
30 days of receiving sampling results. Mail the original,signed hard copy of the DMR to the appropriate DEMLR Regional Office.
Certificate of Coverage No. NCGO8 NCG210444 Person Collecting Samples:Connor Jarvis
Facility Name:Wyeth LLC. Laboratory Name: Eurofins Environmental Testing
Facility County:Lee Laboratory Cert. No.:591 (TSS)&269(O&G)
Discharge during this period:a Yes No (if no,skip to signature and date)
Has your facility implemented mandatory Tier response actions this sample period for any benchmark exceedances?❑Yes El No
If so,which Tier(I, II,or III)?N/A
A copy of this DMR has been uploaded electronically via https://edocs.deq.nc.gov/Forms/SW-DMR El Yes El No
Date Uploaded:N/A
Analytical Monitoring Requirements for Vehicle&Equipment Maintenance Areas—Benchmarks in(Red)
Parameter
Code Parameter Outfall 07 Outfall Outfall Outfall Outfall
N/A Receiving Stream Class C
N/A Date Sample Collected MM/DD/YYYY 01/16/2024
46529 24-Hour Rainfall in inches 0.2
C0530 TSS in mg/L(100 or 501 N/A
00552 Non-Polar Oil&Grease in mg/L(15) < 0.15 mg/L
00400 pH in standard units(6.0—9.0 FW, N/A
6.8—8.5 SW)
NCOIL Estimated New Motor/Hydraulic Oil
Usage in gal/month 58
*Outfalls to Outstanding Resource Waters(ORW),High Quality Waters(HQW),Trout Waters(Tr)and Primary Nursery Areas(PNA)
have a benchmark TSS limit of 50 mg/L.All other water classifications have a benchmark of 100 mg/L
FW(Freshwater)SW(Saltwater)
Notes(optional):Rainfall measurements were recorded from a region rain gauge.efforts were made to grab the DMR sample within the first 30 mins of the signifigant rain event.
"I certify by my signature below,under penalty of law,that this document and all attachments were prepared under my direction or supervision in
accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted.Based on my
inquiry of the person or persons who manage the system,or those persons directly responsible for gathering the information,the information
submitted is,to the best of my knowledge and belief,true,accurate,and complete.I am aware that there are significant penalties for submitting
false information,including the possibility of fines and imprisonment for knowing violations."
20FEB2024
Signature of Permittee or D g ed Authorized Individual Date
[e-mail] 919-566-5210
Email Address Phone Number

•
ti•. eurofins
Environment Testing
ANALYTICAL REPORT
PREPARED FOR
Attn: Connor Jarvis
Pfizer Inc.
4300 Oak Park
Sanford, North Carolina 27330
Generated 2/3/2024 12:18:10 PM
JOB DESCRIPTION
Stormwater
JOB NUMBER
752-15925-1
Eurofins Raleigh
102-A Woodwinds Industrial Court
Cary NC 27511
m
See page two for job notes and contact information. Page 1 of 17 �C • EyO L

EUrofins Raleigh
9
Job Notes
This report may not be reproduced except in full, and with written approval from the laboratory. The results relate only to the
samples tested. For questions please contact the Project Manager at the e-mail address or telephone number listed on this
page.
The test results in this report relate only to the samples as received by the laboratory and will meet all requirements of the
methodology,with any exceptions noted. This report shall not be reproduced except in full, without the express written
approval of the laboratory.All questions should be directed to the Eurofins Environment Testing Southeast, LLC Project
Manager.
Authorization
Generated
)\I `- 2/3/2024 12:18:10 PM
Authorized for release by
Noel Savoie,Project Manager I
[e-mail]
[phone]
Eurofins Raleigh is a laboratory within Eurofins Environment Testing Southeast,LLC,a company within Eurofins Environment Testing Group of Companies
Page 2 of 17 2/3/2024

Client: Pfizer Inc. Laboratory Job ID: 752-15925-1
Project/Site:Stormwater
Table of Contents
Cover Page 1
Table of Contents 3
Definitions/Glossary 4
Case Narrative 5
Detection Summary 6
Client Sample Results 7
QC Sample Results 8
QC Association Summary 9
Lab Chronicle 10
Certification Summary 11
Method Summary 12
Sample Summary 13
Chain of Custody 14
Receipt Checklists 16
Eurofins Raleigh
Page 3 of 17 2/3/2024

Definitions/Glossary
Client:Pfizer Inc. Job ID:752-15925-1
Project/Site:Stormwater
Glossary
El
Abbreviation These commonly used abbreviations may or may not be present in this report.
Listed under the"D"column to designate that the result is reported on a dry weight basis
%R Percent Recovery
CFL Contains Free Liquid
CFU Colony Forming Unit
CNF Contains No Free Liquid
DER Duplicate Error Ratio(normalized absolute difference)
Dil Fac Dilution Factor
DL Detection Limit(DoD/DOE)
DL,RA,RE,IN Indicates a Dilution,Re-analysis,Re-extraction,or additional Initial metals/anion analysis of the sample
DLC Decision Level Concentration(Radiochemistry)
EDL Estimated Detection Limit(Dioxin)
LOD Limit of Detection(DoD/DOE)
LOQ Limit of Quantitation(DoD/DOE)
MCL EPA recommended"Maximum Contaminant Level"
MDA Minimum Detectable Activity(Radiochemistry)
MDC Minimum Detectable Concentration(Radiochemistry)
MDL Method Detection Limit
ML Minimum Level(Dioxin)
MPN Most Probable Number
MQL Method Quantitation Limit
NC Not Calculated
ND Not Detected at the reporting limit(or MDL or EDL if shown)
NEG Negative/Absent
POS Positive/Present
PQL Practical Quantitation Limit
PRES Presumptive
QC Quality Control
RER Relative Error Ratio(Radiochemistry)
RL Reporting Limit or Requested Limit(Radiochemistry)
RPD Relative Percent Difference,a measure of the relative difference between two points
TEF Toxicity Equivalent Factor(Dioxin)
TEQ Toxicity Equivalent Quotient(Dioxin)
TNTC Too Numerous To Count
Eurofins Raleigh
Page 4 of 17 2/3/2024

Case Narrative
Client: Pfizer Inc. Job ID: 752-15925-1
Project: Stormwater
Job ID: 752-15925-1 Eurofins Raleigh
Job Narrative
752-15925-1 4
Analytical test results meet all requirements of the associated regulatory program listed on the Accreditation/Certification Summary
Page unless otherwise noted under the individual analysis. Data qualifiers are applied to indicate exceptions. Noncompliant
quality control(QC)is further explained in narrative comments.
• Matrix QC may not be reported if insufficient sample or site-specific QC samples were not submitted.In these situations,to
demonstrate precision and accuracy at a batch level,a LCS/LCSD may be performed,unless otherwise specified in the
method.
• Surrogate and/or isotope dilution analyte recoveries(if applicable)which are outside of the QC window are confirmed
unless attributed to a dilution or otherwise noted in the narrative.
Regulated compliance samples(e.g.SDWA, NPDES)must comply with the associated agency requirements/permits.
Receipt
The sample was received on 1/25/2024 11:30 AM. Unless otherwise noted below,the sample arrived in good condition,and,
where required, properly preserved and on ice. The temperature of the cooler at receipt time was 2.1°C
General Chemistry
No additional analytical or quality issues were noted,other than those described above or in the Definitions/Glossary page.
Eurofins Raleigh
Page 5 of 17 2/3/2024

Detection Summary
Client:Pfizer Inc. Job ID:752-15925-1
Project/Site:Stormwater
Client Sample ID: Stormwater Lab Sample ID: 752-15925-1
No Detections.
This Detection Summary does not include radiochemical test results.
Eurofins Raleigh
Page 6 of 17 2/3/2024

Client Sample Results
Client:Pfizer Inc. Job ID:752-15925-1
Project/Site:Stormwater
Client Sample ID: Stormwater Lab Sample ID: 752-15925-1
Date Collected: 01/16/24 11:54 Matrix:Water
Date Received:01/25/24 11:30
General Chemistry
Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac
TPH(1664B) <1.5 5.3 1.5 mg/L 02/02124 15:36 02/02/24 20:18 1
6
Eurofins Raleigh
Page 7 of 17 2/3/2024

QC Sample Results
Client: Pfizer Inc. Job ID:752-15925-1
Project/Site:Stormwater
Method: 1664E -HEM and SGT-HEM
Lab Sample ID:MB 680-820864/1-A Client Sample ID: Method Blank
Matrix:Water Prep Type:Total/NA
Analysis Batch:820894 Prep Batch:820864
MB MB
Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac
TPH <1.4 5.0 1.4 mg/L 02/02/24 15:36 02/02/24 20:18 1
Lab Sample ID:LCS 680-820864/2-A Client Sample ID: Lab Control Sample Ei
Matrix:Water Prep Type:Total/NA
Analysis Batch:820894 Prep Batch:820864
Spike LCS LCS %Rec
Analyte Added Result Qualifier Unit D %Rec Limits
TPH 20.0 14.60 mg/L 73 64_132
Lab Sample ID: LCSD 680-820864/3-A Client Sample ID: Lab Control Sample Dup
Matrix:Water Prep Type:Total/NA
Analysis Batch:820894 Prep Batch:820864
Spike LCSD LCSD %Rec RPD
Analyte Added Result Qualifier Unit D %Ree Limits RPD Limit
TPH 20.0 16.00 mg/L 80 64.132 9 34
Eurofins Raleigh
Page 8 of 17 2/3/2024

QC Association Summary
Client: Pfizer Inc. Job ID: 752-15925-1
Project/Site: Stormwater
General Chemistry
Prep Batch: 820864
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
752-15925-1 Stormwater Total/NA Water 1664B
MB 680-820864/1-A Method Blank Total/NA Water 1664E
LCS 680-820864/2-A Lab Control Sample Total/NA Water 1664B
LCSD 680-820864/3-A Lab Control Sample Dup Total/NA Water 1664E
Analysis Batch: 820894
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
752-15925-1 Stormwater TotaUNA Water 1664B 820864 8
MB 680-820864/1-A Method Blank Total/NA Water 1664E 820864
LCS 680-820864/2-A Lab Control Sample Total/NA Water 1664B 820864
LCSD 680-820864/3-A Lab Control Sample Dup Total/NA Water 1664E 820864
Eurofins Raleigh
Page 9 of 17 2/3/2024

Lab Chronicle
Client: Pfizer Inc. Job ID:752-15925-1
Project/Site:Stormwater
Client Sample ID: Stormwater Lab Sample ID: 752-15925-1
Date Collected: 01/16/24 11:54 Matrix:Water
Date Received: 01/25/24 11:30
Batch Batch Dilution Batch Prepared
Prep Type Type Method Run Factor Number Analyst Lab or Analyzed
Total/NA Prep 16648 820864 TD EET SAV 02/02/24 15:36
Total/NA Analysis 1664E 1 820894 TD EET SAV 02/02/24 20:18
Laboratory References:
EET SAV=Eurofins Savannah,5102 LaRoche Avenue,Savannah,GA 31404,TEL[phone]
9
Eurofins Raleigh
Page 10 of 17 2/3/2024

Accreditation/Certification Summary
Client: Pfizer Inc. Job ID:752-15925-1
Project/Site:Stormwater
Laboratory: Eurofins Savannah
The accreddations/certifications listed below are applicable to this report.
Authority Program Identification Number Expiration Date
North Carolina(WW/SW) State 269 12-31-24
Eurofins Raleigh
Page 11 of 17 2/3/2024

Method Summary
Client: Pfizer Inc. Job ID:752-15925-1
Project/Site:Stormwater
Method Method Description Protocol Laboratory
1664B HEM and SGT-HEM 1664E EET SAV
1664E HEM and SGT-HEM (Aqueous) 1664B EET SAV
Protocol References:
1664E=EPA-821-98-002
Laboratory References:
EET SAV=Eurofins Savannah,5102 LaRoche Avenue,Savannah,GA 31404,TEL[phone]
Eurofins Raleigh
Page 12 of 17 2/3/2024

Sample Summary
Client:Pfizer Inc. Job ID:752-15925-1
Project/Site:Stormwater
Lab Sample ID Client Sample ID Matrix Collected Received
752-15925-1 Stormwater Water 01/16/2411.54 01/25/2411.30
E
Eurofins
Page 13 of 17 2/3/2024

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Login Sample Receipt Checklist
Client:Pfizer Inc. Job Number:752-15925-1
Login Number:15925 List Source:Eurofins Raleigh
List Number:1
Creator:Yonish,Rachel
Question Answer Comment
Radioactivity wasn't checked or is</=background as measurer]by a survey True
meter.
The cooler's custody seal,if present,is intact. True
Sample custody seals,if present,are intact. True
The cooler or samples do not appear to have been compromised or True
tampered with.
Samples were received on ice. True
Cooler Temperature is acceptable. True
Cooler Temperature is recorded. True
COC is present. True
COC is filled out in ink and legible. True
COC is filled out with all pertinent information. True
Is the Field Sampler's name present on COC? True
There are no discrepancies between the containers received and the COC. True
Samples are received within Holding Time(excluding tests with immediate True HTs)
Sample containers have legible labels. True
Containers are not broken or leaking. True
Sample collection date/times are provided. True
Appropriate sample containers are used. True
Sample bottles are completely filled. True
Sample Preservation Verified. True
There is sufficient vol.for all requested analyses,incl.any requested True
MS/MSDs
Containers requiring zero headspace have no headspace or bubble is True
<6mm(1/4").
Multiphasic samples are not present. True
Samples do not require splitting or compositing. True
Residual Chlorine Checked. True
Eurofins Raleigh
Page 16 of 17 2/3/2024

Login Sample Receipt Checklist
Client:Pfizer Inc. Job Number:752-15925-1
Login Number:15925 List Source:Eurofins Savannah
List Number:2 List Creation:01/27/24 02:03 PM
Creator:Sims,Robert D
Question Answer Comment
Radioactivity wasn't checked or is</=background as measured by a survey N/A
meter.
The cooler's custody seal,if present,is intact. True
Sample custody seals,if present,are intact. True
The cooler or samples do not appear to have been compromised or True
tampered with.
Samples were received on ice. True
Cooler Temperature is acceptable. True
Cooler Temperature is recorded. True
COC is present. True
COC is filled out in ink and legible. True
COC is filled out with all pertinent information. True
Is the Field Sampler's name present on COC? True
There are no discrepancies between the containers received and the COC. True
Samples are received within Holding Time(excluding tests with immediate True
HTs)
Sample containers have legible labels. True
Containers are not broken or leaking. True
Sample collection date/times are provided. True
Appropriate sample containers are used. True
Sample bottles are completely filled. True
Sample Preservation Verified. N/A
There is sufficient vol.for all requested analyses,incl.any requested True
MS/MSDs
Containers requiring zero headspace have no headspace or bubble is N/A
<6mm(1/4").
Multiphasic samples are not present. True
Samples do not require splitting or compositing. True
Residual Chlorine Checked. N/A
Eurofins Raleigh 2/3/2024
Page 17 of 17