WQ0035049_Monitoring - 12-2023_20240124

Monitoring Report Submittal
Permit Number#* WQ0035049
Name of Facility:* Maple Hill Wastewater Treatment Facility
Month: * December Year: * 2023
Report Information
Type* Upload Document*
NDMR, NDAR-1, NDAR-2, NDMLR Maple Hill December2023 NDMR, NDAR-1.pdf 2.09MB
PDF Only
Please upload one PDF containing all applicable monitoring reports
(i.e., NDMR, NDAR-1, NDAR-2, NDMLR, GW-59).
Confirmation Email Address: * [e-mail]
Name of Submitter: * Anthony Colon
Signature:
Date of submittal: 1/24/2024
This will be filled in automatically
Initial Review
Reviewer: Wanda.Gerald

Is the project number correct?* WQ0035049
Is the monitoring report accepted?* Yes No
Regional Office* Wilmington
Reviewer: _anonymous
Review Date: 2/20/2024

FORM: NDMR 10-13 NON -DISCHARGE MONITORING REPORT (NDMR) Page _1_ of -2-
Permit No.: WQ0035049
Facility Name: Maple Hill WWTF
County: Pencier
Month: December
Year: 2023
PPk 001
Flow Measuring Point: a]InHuent El Effluent ❑ No flow generated
Parameter Monitoring Point: ❑ influent O Effluent El Groundwater Lowering 17 Surface Water
Parameter Code -i
$0050
00400
J00310
00530
00610
00620
00620,
31616
00600
00665
00940
70300
<6
�F
O
c
O
U
W
O
m
C
;fn
N
Z
L
14
Y."+`+
o
!i O
U
Y«
N
7
F 0
L
a.
.r
U
a
H yN
p
24-hr
hrs
GPD
su
mg/L
mg/L
mg/L
mg/L
mg/L
#/100 mL
mg/L
I mg/L
mg1L
mg1L
1
09:30
6
9,165
7.4
2
9,333
3
8,632
4
07:30
6
9,399
7.2
5
10:00
7
8,854
7.2
6
07:30
5
7,235
7.4
7
07:30
6
9,946
7.5
8
07:30
6
8,810
7.2
9
11,444
10
13,574
11
07:30
6
14,681
7.4
12
07:30
7
1 a,011
7.4
13
07:30
7
10,138
7.4
14
07:30
5
10,270
7.4
11
4.9
3.9
12.7
3.3
<1
13.2
7,67
15
07:30
6
10,331
7.5
16
12,368
17
37,1.74
18
07:30
6
25,596.
7.9
19
07:30
7
13, 60
7.8
20
07:30
7
10,7611
7.6
21
09:00
6
9,952
7.8
22
07:30
5
10,864
7.4
23
11,448
24
12,848
251
09:00
2
10,774
7.4
261
09:00
4
12,158
7.5
27
09:00
4
88,919
7.5
28
07:30
7
17.638
7.5
29
07:30
7
11,958
7.3
30
10,468
31
10,353
Average:
14,797
11.00
4.90
3.90
12.70
3.30
1.00
13,20
7.67
Daily Maximum:
887919
7.90
11.00
4.90
3.+90
12.70
3..30
1.00
13.20
7.67
Daily Minimum:
7,235
7,20
11.00
4.90
3.90
12.70
3.30
1.00
13.21)
7.67
Sampling Type:
Recorder
Grab
Composite
Composite
Composite
Composite
Composite
Grab
Composite
Grab
Composite
Composite
Monthly Avg. Limit:
42,000
nla
30
30
15
n/a
r1la
200
n/a
nla
n1a
nla
Daily Limit:
n/a
6 to 9
n/a
n/a
nla
n/a
tila
n/a
pla
n/a
nfa
n/a
Sample Frequency:
Continous
5XWK
Weekly
Weekly
Weekly
Weekly
W-e'ekly
Weekly
Monthly
Montly I
3XYR
3XYR

FORM: NDMR 10-13 NON -DISCHARGE MONITORING REPORT (NDMR) Page _2_of 2_
Sampling Persons) Certified Laboratories
Name: Samples were collected by the Certified Laboratory Name: Environmental Chemists, Inc.
Name: Name: Jay Baker
Does all monitoring data and sampling frequencies meet the requirements in Attachment A of your permit? n compliant ❑ Non-Compliart
If the facility is non -compliant, please explain in the space below the reasons) the facility was not in compliance. Provide in your explanation the date(s) of the non-compliance and describe the corrective actions)
taken. Attach additional sheets if necessary.
Operator in Responsible Charge (ORC) Certification Permittee Certification
ORC: Christopher Pickett Permittee: Pender County Utilities
Certification No.: 995432 Signing Official: Anthony Colon
Grade: WW2 Phone Number: 910-259-1570 Signing Official's Title: Director
Has the ORC changed since the previous NDMR? o Yes CI No Phone Number: 910-259-1570 Permit Expiration: 8/31/2026
Signature Date Signature Date
By this signature. I certify that this report is accurrate and complete to the best of my knowledge [ certify, under penalty of Iar: that this document and all attachments were prepared under my direction or supervision in
accordance with a system designed to assure that all qualified personnel properly gathered and evaluated the information
submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for
gathering the information, the information submitted !s to the best of my knowledge and belief, true. accurate, and complete I am
aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for
knowing violations.
Mail Original and Two Copies to:
Division of Water Resources
Information Processing Unit
1617 Mail Service Center
Raleigh, North Carolina 27699-1617

F"O"W 747
Environmental Chemists, Inc.
envirochem 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab ° 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 - 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 + 910.347-5843 Lab;'Fax
ANALYTICAL & CONSULTING CHEMISTS ini'o,11 env ironmentalchemists.com
Pender County Utility Operations
Date of Report: Jan 10, 2024
Post Office Box 995
Customer PO #:
Burgaw NC 28425
Customer ID: 08100095
Attention:
Report M 2023-29338
Project ID: Maple Hill WWTP
Lab ID Sample ID:
Collect DatefTime Matrix Sampled by
23-71022 Site: Effluent
12/14/2023
9:30 AM Water JCB/Envirochem
Test
Method
Results
Date Analyzed
Ammonia Nitrogen
EPA 350.1, Rev. 2.0, 1993
3.9 mg/L
12/1912023
Total Kjeldahl Nitrogen (TKN)
EPA 351.2. Rev. 2.0, 1S93
3.3 mg/L
12/20/2023
Residue Suspended (TSS)
SM 2640 D-2015
4.9 mg/L
12/15/2023
BOD
SM 5210 B-2016
11 mg/L
12/14/2023
Sample estimated. Did not meet quality control requirements: Blank= 0.27mgfL,
above acceptable limit of 0. mg/L.
Nitrate Nitrogen (Calc)
Nitrite Nitrogen
EPA 353.2. Rev. 2.0. 1993
0.52 mg/L
12/14/2023
Nitrate+Nitrite-Nitrogen
EPA 353,2, Rev. 2.0. 1993
13.2 mg/L
12/18/2023
Nitrate Nitrogen
subtraction Method
12.7 mg/L
01/03/2024
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
23-71023 Site: Effluent - Grab
12/14/2023
11:30 AM Water JCB/Envirochem
Test
Method
Results
Date Analyzed
Fecal Coliform
1dexxColilert•18
<1 MPN/100ml
12/1412023
Temperature
SM 2550 8-2010
11.4 C
12/14/2023
pH
SM 4500 H 8-2011
7.3 units
12/14/2023
Total Phosphorus
SM 4500 P (F-H)-2011
7.67 mg/L
12/20/2023
Comment: ;
w
Reviewed by:
j%
ReportX. 2aD-29338 PagA 1 01 1

Date.. 123
Analyst., _ Jay Baker
Certification it 94
Facility Name: i s��l �� Itil • j-1
Permit M:
PH
Reference.. Methr l• GMdSnn 14+R -9M 1 In RTA R AT)I • K,1610C
Calibration Time
Cal Buffer 4.0 s.u.
Cal Buffer 10.0 s.u.
Check Buffer 7 0 sm,
Comments
�• 00
o- . ()
1�.(:)2 ()
Z Eli ( )
'pH check butler must read within t 0.1 pH units of the buffer's true value.
4 su buffer Lot#/: Rim 1304N,61 E21 7 su buffer LotlN: Ricci U 10G40 Exp. 1=4 10 su buffer Loth __ RICCA 13041'74 Eisi l� W4
Sample location
Sample Collection
Time
Sample Analysis
Time®
pH Result
s u
* Post -analysts Buffer
Check value s u
Comments/Data Qualifiers
t
1 (�
► Post analysis buffer check is required when performing analyses at multiple sampling locations and must be within+ 0.1 units of the buffer's true value
Afl pH values in pH units (i.e., sm.). Record all data to the nearest 0.01 sxu and rcpon to the nearest 0.1 sm
Total Residual Chlorine (TRC)
Reference Method: Stet 4500 CI-G2011: Hach 8167 FIR: f Please circle annlicable Methnril Insimmem in MACH ('ninrimpter 1511WIFIRgtlt)f
Daily Check
Post -analysis
Time check
Check Std.
Sample
Sample
Sample
TRC Result
Standard Result
(when analyzing Standard
Location
Collection
Analysis
pg/L or mg/L
Comments/Data Qualifiers
pglL or mg/L
Analyzed
at multi le sites
Time
Time
I KC Daily Check Standard true value pg/L or mg/L acceptance range pg/L or mg/L GEL STDS HACH A0038
Check standards must recover within t10"/o of the cheek standard's true value
Annual Calibration Curve Verification Date: 11J25/23 IDEXX (Free) 230901 Exp. Date:10/31/24 IDEXX fTotW1230757 Exo. Date:08/31/24
Reagent Blank Value: (When applicable- Analyze and document a reagent blank when standards, sample dilutions or PT Samples are prepared)
Dissolved Oxygen (DO)
Reference Method:SM 4500 0 G -2016 Instrument ID YSI PRO 20 22D100065
Calibration/ Calibration variable
Verification
Time Temp Barometric Salinity,
cC pressure
_Lh, I PPt
e Post -analysis calibration
Meier reading verification (when necessary)
or % efficiency
after calibration Theoretical Calculated
Value Value mg/L
Comments
Use this row when performing a verification instead of
__.�alibratiittt
Sample Location
P
Sample Collection
Time
'SampteAnalysis
Time
DO reading
U-IL
Comments/DataQualifiiers
e when performing analyses at multiple locations, the meter must be recalibrated at each site before analysis or a post -analysis calibration venfication must be performed
• Irsample is measured directly in the stream and/or onsite, only time analyzed would be recorded with a nose that they are measured in situ or immediately
Temperature
Reference Melhod $MISSri i4-?n10 Incrn,meni in S.TARA21, - WA6195
Sample Location
Sample
Collection
Time
*Sample
Analysis
Time
Temperature
°C
Comments/DataQualifiers
30
u�
ifsample is measured directly in the stream and/or on site, only time analyzed would be recorded, with a note that they are measured in situ or immediately
Annual Verification Date 11-25-23
Field Personnel Note:
QA.001 12i01122
Rev 1-2022

Environmental Chemist, Inc,, Wilmington, NC Lab #94
Sample Receipt Checklist
6602 Windmill Way
Wilmington, NC 28405
910 392 0223
Ciient:1('1t'
Date: Id `t T
Report Number: O 3-
Receipt of sample:
❑ YES ❑ NO
ECHEM Pickup Client Delivery ❑ UPS O FedEx ❑ Other 0
O N/A
❑ YES ❑ NO
1. Were custody seals present on the cooler?
p
Original temperature upon
N/A 2. If custody seals were present, were they intact/unbroken?
receipt °C
Corrected temperature upon receipt
How temperature taken: ❑ Temperature Blank ® — C
Against Bottles
IR Gun ID: Thomas Traceable S/N 210886869 IR Gun Correction Factor °C: 0.0
OO YES
0 YES
❑ NOtemperature
❑
of cooler exceeded 6°C, was Project Mgr./QA notified?
2 YES
N0
❑ NO
4. Were proper custody procedures (relinquished/received) followed?
5. Were sample ID's listed on the COC?
59 YES
13 NO
5. Were samples ID's listed on sample containers?
U YES
❑ NO
7. Were collection date and time listed on the COC?
IZ YES
❑ NO
8. Were tests to be performed listed on the COC?
0 YES
O
❑ NO
9. Did samples arrive in proper containers for each test?
YES
9
❑ NO
f0, Did samples arrive in good condition for each test?
YES
O NO
11. Was adequate sample volume available?'
❑x YES
YES
❑ NO
❑
12. Were samples received within proper holding time for requested tests?
❑
NO
13. Were acid preserved samples received at a pH of <27
YES
❑ NO
14. Were cyanide samples received at a pH >12?
❑ YES
❑ NO
1S, Were sulfide samples received at a pH >9?
YES
❑ YES
❑ NO
❑
16. Were NH3/TKN/Phenol received at a chlorine residual of <0,5 m/L? **
❑ YES
NO
❑
17. Were Sulfide/Cyanide received at a chlorine residual of <0.5 m/L?
NO
18. Were orthophosphate samples filtered in the field within 15 minutes?
* TOC/Volatiles are pH checked at time of analysis and recorded on the benchsheet.
Bacteria samples are checked for Chlorine at time of analysis and recorded on the benchsheet.
Sample Preservation:
(Must be completed for any sample(s) incorrectly y preserved or with headspace)
by adding (circle one):
were received incorrectly preserved and were adjusted accordingly
H2504 HNO3
Time of preservation:
HCI NaOH
If more than one preservative is needed, notate in
Note: Notify customer service immediately
comments below
for incorrectly preserved samples. Obtain a new sa rple or
notify the state lab if directed to analyzed by the customer. Who was notified, date and time:
Volatiles Sample(s)
were received with headspace
COMMENTS,
DOC. QA.002 Rev 1

44W ENVIRONMENTAL CHEMISTS, INC
Analytical & Consulting Chemists NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729
COLLECTION AND CHAIN OF CUSTODY
6602 Windmill Way Wilmington, NC 28405
OFFICE: 910-392-0223 FAX [phone]
info@e nvi ronmentalchem ists.com
Client: Pender County Utilities (Wastewater)
PROJECT NAME: Maple Hill WWTP (PPI 001)
REPORT NO: LsL 3 Zit 3
ADDRESS:
CONTACT NAME: Chris Pickett, ORC
PO NO:
REPORT TO: ORC
PHONE/FAX:
COPY TO:
email:
Sampled By: SAMPLE TYPE: I = Influent, E = Effluent, W = Well, ST = Stream, SO = Soil, SL = Sludge, Other:
Sample identification
Collection
m
E
�~
_s
N s
n o R
o
c
g
m
8`
o m
E
W
m m
_
PRESERVATION
ANALYSIS REQUESTED
Date
Time
Temp
z
o=
U i
_ 1
z
o
W
r
o
WWTP PPI 001 (composit
d �-
C
p
a �Q
X
-
113013, TSS, NO2
L �{
% s 7
C
P
�U y
La
X
NO3, NH3. TKN
WWTP PPI 001
(composite) Triannuals
C
P
X
Chloride, TDS (March, Jul,),, Nov)
C
P
G
G
WWTP Effluent (grab)
`A.
!Al-)f
P
��
4�
X
Total Phos
G
pH (field): -
C
P
X
Fecal Coliform
G
G
C
P
G
G
Samples due 1/month
C
P
G
G
C
P
G
G
_
Omits: BOD 30 mg1L, TSS 30 mg1L, NH3 15 mg/L, Fecal 200 colonles1100 ml
Transfer
Relinquished By:
DatelTime
Received By:
DatelTime
1.
2.
p
Temperature When Received: tr
Delivered By: IArl-I
Com
Accepted: --Rejected: Resampie Re u ted:
Received By:l���i'l_� CQ 4�- Date: i� s .�
_ � Time:��C(Z_
_____ TURNAROUND: !

FORM: NDAR-1 10-13 NON -DISCHARGE APPLICATION REPORT (NDAR-1) ?age _1_ of_4_
Permit No.: WQ0035049
Facility Name: 41
County: Pender
Month: December
Year: 2023
Did irrigation occur
Field Name:
1
Field Name:
2
Field Name:
3
Field Name:
4
at this facility?
Area (acres):
172
Area (acres):
1.72
Area (acres):
132
Area (acres):
1.72
Cover Crop:
Bermuda
Cover Crop:
Bermuda
Cover Crop:
Bermuda
Cover Crop:
Bermuda
o YES ❑ NC
Hourly Rate (in):
0.41
Hourly Rate (in):
0.41
Hourly Rate (in):
0,41
Hourly Rate (in):
0.41
58
Annual Rate (in):
29.71
Annual Rate (in):
29.71
Annual Rate (in):
29.71
Annual Rate (in):
29.71
Weather
Freeboard
Field Irrigated?
0 YES ❑ NO
Field Irrigated?
M YES © No
Field irrigated?
C YES C NO
Field Irrigated?
2 YES d No
d
�
o
U
�
r
CL
o
:9
y
� v
En�+
.E
CQ
a
0 CL
>
II.
o
a
m
s
d a
a
>
v
E
w
c
v
J
E a m
om
x�
m a
E 2
w
c
v
oE
E
3am
o�
m_m
E
a
c
Jao
ca J
3�ow
_°E
'F
in
It
ft
gal
min
in
in
gal
min
in
in
gal
min
in
in
gal
min
in
in
1
CL
51
0
3.9
2
3
4
CL
55
0.1
3-9
5
CL
56
0
3.9
7,000
20
0.16
0.15
6,880
20
0.15
0.15
6,280
20
0.13
0.13
6,180
20
0.13
0.13
6
CL
42
0
3.9
11
7
C
28
0
3.9
8
C
38
0
3.9
9
10
11
R
44
1.4
3.9
12
C
31
0
3.9
13
PC
30
0
3.9
14
C
36 1
0
3.9
15
C
37
0
3.9
16
17
18
C
53
2,7
3.8
19
C
37
0
3.8
201
C
33
0
3.8
21
C
44
0
3.8
22
C
30
0
3.8
23
24
25
PC
53
0
3.3,8
261
CL 1
58
0
3-8
27
R
64
2.7
3.7
28
CL
52
2.2
3,6
29
C
38
0
3.6
30
31
Monthly Loading:
7,000
0.15
y �.:�;z:
6,880
0.15
6,28D
4.13
..
6,180
0.13
12 Month Floating Total (in):
-_'-� t^�
10.97
`_-
10.71
�``= ='�
10.13
10.70

FORM: NDAR-1 10-13 NON -DISCHARGE APPLICATION REPORT (NDAR-1) Page _2_ of _4_
Permit No.: WQ0035049
Facility Name: Maple Hill WWTF
County: Pender
Month: December
Year: 2023
Did irrigation occur
Field Name:
5
Field Name:
6
Field Name:
7
Field Name:
8
this facility?
Area (acres):
1.72
Area (acres):
1.72
Area (acres):
1.74
Area (acres):
1.71
at
Cover Crop:
Bermuda
Cover Crop:
Bermuda
Cover Crop:
Bermuda
Cover Crop:
Bermuda
O YES p NO
Hourly Rate (in):
GA1
Hourly Rate (in):
0.41
Hourly Rate (in):
0.41
Hourly Rate (in):
0,41
Annual Rate (in):
29,71
Annual Rate (in):
29.71
Annual Rate (in);
29.71
Annual Rate (in):
29.71
Weather
Freeboard
Field Irrigated?
0 YE5 ❑ NO
Field Irrigated?
O YES ❑ NO
Field Irrigated?
Cl YES ❑ NO
Field Irrigated?
O YES ❑ No
d!
a
U
s
i
.=i
R
0
E
00
i+
°
0.
y
ILp
C�
m
co
v
y
d
a m
_ .V
a
d Z7
E v
7
> `'.
'Cf
a '.�',
_
a
C
V
r"i
J
?�'
a,
7 i
_
E a
7 G
> Q CL
d
E
F W
rn
c
J
>.
Q
L
7 v
R 2 J
a
3 Q
J� 6 CL
d
E
r
a
i
c
J
Cam]
;E 3>
m
v
3&
0.
d
E
H
Im
C
o L c
J ,E 7 '0
T w S 0
p
°F
in
ft
ft
gal
min
in
in
gal
min
in
in
gal
min
in
in
gal
min
in
in
1
CL
51
0
3,9
2
3
4
CL
55
0.1
3.9
5
CL
56
0
3.9
'6,880
20
0.15
0,15
6,800
20
0.15
0.15
6,920
20
0.15
0.15
6,960
20
0.15
0.15
6
CL
42
0
3.9
7
C
28
0
3.9
8
C
38
0
3.9
9
10
11
R
44
1.4
3.9
12
C
31
0
3.9
13
PC
30
0
3.9
14
C
36
0
3.9
15
C
37
0
3.9
16
17
18
C
53
2.7
3.8
19
C
37
0
3.8
20
C
33
0
3.8
21
C
44
0
3.8
22
C
30
0
38
23
24
25
PC
53
0
3.3.8
26
CL
58
0
3.8
27
R
64
2.7
37
28
CL
52
2.2
3.6
291
C
38
0
3.6
30
311
1
1
1--
Monthly Loading:
12 Month Floating Total (in):
6,880
0.15
10.72
6,800
0.15
11.56
6,920
ZZ
~`
Q.15
11.7Q
6,960
0.15
11.77

FORM: NDAR-1 10-13 NON -DISCHARGE APPLICATION REPORT (NDAR-1) Page 3_ of _4`
Permit No.: W00035049
Facility Name: MAPLE HILLWWTF
County: Pender
Month: December
Year: 2023
Did irrigation occur
Field Name:
9
Field Name:
10
Field Name:
11
Field Name:
this facility?
Area (acres):
1.75
Area (acres):
1.77
Area (acres):
1.72
Area (acres):
at
Cover Crop:
:Bermuda
Cover Crop:
Bermuda
Cover Crop,:
Bermuda
Cover Crop:
U1 YES E NO
Hourly Rate (ln):
0.41
Hourly Rate (in):
0.41
Hourly Rate (in):
0.41
Hourly Rate (in):
0
Afrnual Rate (in):
29.71
Annual Rate (in):
29.71
Annual bate (in):
29.71
Annual Rate (in):
Weather
Freeboard
Field irrigated?
21 YES El ND
Field Irrigated?
0 YES © NO
Field Irrigated?
-Z YES NO
Field Irrigated?
❑ YES n NO
❑
a
U
t
y
c
~
y
Q
W
`o
Cr v
CL 11 M
Ln
WE is
i
"a
2.
E p>
o
N 'p
E.9
o°
'O
d
E .m
'6
O
E
o
E
a
O
'
y'
E a
O
°F
in
ft
ft
gal
min
in
in
gal
min
in
in
gal
min
in
in
gal
min
in in
1
CL
51
0
3.9
2
3
4
CL
55
0.1
3.9
5
CL
56
0
3.9
6,720
20
0.14
0.14
6,780
20
0.14
0.14
6,340
20
0.14
0.14
6
CL
42
0
3.9
7
C
28
0
3.9
8
C
38
0
3.9
9
10
11
R
44
1 A
3.9
12
C
31
0
3.9
13
PC
30
0
3.9
14
C
36
0
3.9
15
C 1
37
0
3.9
16
17
18
C
53
2.7
3.8
19
C
37
0
3.8
20
C
33
0
3.8
211
C
44
0
3.8
22
C
30
0
3.8
23
24
25
PC
53
0
3.3.8
26
CL
58
0
3.8
27
R
64
2.7
3.7
28
CL
52
2,2
3.6
291
C
38
0
3.6
30
31
6,340
Monthly Loading:
12 Month Floating Total (in):
6.720
0.14
10.89
6,780
1
1
0.14
10 63
0.14
9.91
0
000

FORM NDAR-110-13 NON -DISCHARGE APPLICATION REPORT(NDAR-1) Page _4_of_4--__
Did the application rates exceed the limits in Attachment B of your permit?
Were adequate measures taken to prevent effluent ponding in or runoff from the sites?
Was a suitable vegetative cover maintained on all sites as specified in your permit?
Were all setbacks listed in your permit maintained for every application to each permitted site?
Were all freeboards maintained in accordance with the specified freeboard heights in your permit?
O Compliant ❑ Non -Compliant
O Compliant ❑ Non -Con iaN
0 Compliant ❑ Non -Compliant
0 Compliant ❑ Non-Compliart
O Compliant 0 Non-Compliart
If the facility is non -compliant, please explain in the space below the reason(s) the facility was not in compliance. Provide in your explanation the date(s) of the non-compliance and describe the corrective
action(s) taken. Attach additional sheets if necessary.
Operator in Responsible Charge (ORC) Certification
Permittee Certification
ORC: Christopher Pickett
Permittee:
Pender County Utilities
Certification No.: 1010919
Signing Official: Anthony Colon
Grade: WW-SI Phone Number: 910-259-1570
Signing Official's Title: Director
Has the ORC changed since the previous NDAR-1? ❑ Yes n No
Phone Number: 910-259-1570 Permit Exp.: 8/31/26
-
61 i 0
Signature Date
Signature Date
By this signature, 1 certify that this report is accunate and complete to the best of my knowledge
I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance
with a system designed to assure that all qualified personnel properly gathered and evaluated the information submitted, Based on my
inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the
information submitted is, ID the best of my knowledge and belief, true, accurate, and complete : am aware that there are significant
penalties for submitting false information, including the possibility of fines and imprisonment for knowing vielabons,
Mail Original and Two Copies to:
Division of Water Resources
Information Processing Unit
1617 Mail Service Center
Raleigh, North Carolina 27699-1617

Environmental Chemists, Inc,
o
il
tr
6602Windmill Way, Wilmington, NC 28405 .. 910.392.0223 Lab M 910.392.4424 Fax
710 6owsertown Road, Manteo, NC 27954 . 252.473.5702LabiFax
255 A Wilmington Highway, Jacksonville, NC 28540 * 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS infoacrenvironmentalchemists.com
Pender County Utility Operations Date of Report: Dec 21, 2023
Post Office Box 995 Customer PO #:
Burgaw NC 28425 Customer ID: 08100095
Attention: Report #: 2023-26818
Project ID: Maple Hill WWTP
Lab ID Sample ID: Collect DaterTime Matrix Sampled by
23-64998 Site: 001 11113/2023 11:30 AM Solid/Sludge Client
Test
Method
Results
Date Analyzed
Soil Fertility
Calcium
EPA200.7
2810mg/kg
11121/2023
Copper
EPA 2007
3.80mg/kg
11/21/2023
Magnesium
EPA200 7
820 mg/kg
11/21/2023
Manganese
EPA 200.7
24.9 mg/kg
11/21/2023
Potassium
EPA 200 7
413 mg/kg
11/21/2023
Sodium
EPA 200 7
1280 mg/kg
11 /27/2023
Zinc
EPA200.7
148 mg/kg
11/21/2023
Acidity (Soil Fertility)
NCDA-Agronomic Division
2 meq/100g
11 /28/2023
Base Saturation
NCDA Agronomic Division
90.7 %
12/12/2023
Cation Exchange Capacity
NCDA-Agronomic Division
24.1 meq/100g
12/12/2023
Exchangeable Sodium Percentage
NCDA-Agronomic Division
23.2 %
12/1212023
Humic Matter
NCDA-Agronomic Division
3.36 %
1211412023
Total Solids (%)
sM 2540 a
48.9 %
11 /1712023
Total Phosphorus
SM 4500 P F
239 mg/kg
11 /30/2023
pH
SW a4s Method 9045D
6.71 units
1112912023
Result estimated. Analyzed out of 15 minutes hold time.
Renort 4 2023-25818

Environmental Chemists, Inc.
envirochem
ANALYTICAL 8 CONSULTING CHEMISTS
6602 Windmill Way, Wilmington, NC 28405 . 910.392.0223 Lab . 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 a 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 . 910.347.5843 Lab,/Fax
infori.,environmentalchemists.com
Pender County Utility Operations Date of Report: Dec 21, 2023
Post Otrice Box 995 Customer PO #:
Burgaw NC 28425 Customer 10: 08100095
Attention: Report #: 2023-26818
Project ID: Maple Hill WWTP
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
23-64999 Site: 002 11/13/2023 11:34 AM Solid/Sludge Client
Test
Method
Results
Date Analyzed
Soil Fertility
Calcium
EPA 200.7
1180 mg/kg
11/21/2023
Copper
EPA 200.7
<2.99mg/kg
11/21/2023
Magnesium
EPA 200.7
290mg/kg
11/2112023
Manganese
EPA 200.7
3.73 mg/kg
11/21/2023
Potassium
EPA200.7
190 mg/kg
11/21/2023
Sodium
EPA 200.7
405mg/kg
11/27/2023
Zinc
EPA 200.7
34.1 mgikg
11/21/2023
Acidity (Soli Fertility)
NCDA-Agronomic Division
3 meq/100g
11/28/2023
Base Saturation
NCDA-Agronomic Divisatn
75.5 %
12/12/2023
Cation Exchange Capacity
NCDA-Agronomic Division
11.6 meq/100g
12/12/2023
Exchangeable Sodium Percentage
NCDA-Agronomic Division
15.1 %
12/12/2023
Humlc Matter
NCDA-Agronomic Division
2.28 %
12/14/2023
Total Solids (%)
$M 2540 8
73.7 %
11/17/2023
Total Phosphorus
SM 4500 P F
155 mg/kg
11 /30/2023
pH
SW 846 Method 9046D
5.67 units
11/28/2023
Result estimated. Analyzed out of 15 minutes hold time
Report #- 2023.2681$ Pane 2 of 11

•
nvirochem
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 * 910.392.0223 Lab * 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 . 910.347.5843 Lab/Fax
inro?a environmentalcliemists.corn
Ponder County Utility Operations Date of Report: Dec 21, 2023
Post Office Box 995 Customer PO #:
Burgaw NC 28425 Customer ID: 08100095
Attention: Report #: 2023-26818
Project ID: Maple Hill WWTP
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
23-65000 Site: 003 11/13/2023 11:38 AM Solid/Sludge Client
Test
Method
Results
Date Analyzed
Soil Fertility
Calcium
EPA 200.7
935 mg/kg
11/21/2023
Copper
EPA 200.7
<2.07 mg/kg
11/21/2023
Magnesium
EPA 200.7
162 mg/kg
11/21/2023
Manganese
EPA200.7
<2.07 mg/kg
11121/2023
Potassium
EPA 200J
132 mg/kg
11/21/2023
Sodium
EPA 200.7
329mg/kg
11/21/2023
Zinc
EPA 200.7
15.9 mg/kg
11/21/2023
Acidity (Soil Fertility)
NCDA-Agronomic Division
2 meq/100g
11/28/2023
Base Saturation
NCDA-Agronomic Division
73.8 %
12/12/2023
Cation Exchange Capacity
NCDA Agronomic Division
9.30 meq/100g
12112/2023
Exchangeable Sodium Percentage
NCDA-Agronomic Division
15.4 %
12/12/2023
Humic Matter
NCDA•Agronomic Division
3.48 %
12/14/2023
Total Solids (%)
5M 2540 B
71.6 %
11/17/2023
Total Phosphorus
SM 4600 P F
149 mg/kg
11/30/2023
pH
SW 846 Method 9045D
6.47 units
1 1/28/2023
Result estimated. Analyzed out of 15 minutes hold time.
Rand !P 7071-99AIA Penn o nt 7 i

-77
Anviranmental Chemists, Inc.
envirochem 6602 Windmill Way, Wilmington, NC 28405 « 910.392.0223 Lab . 910.392.4424 Fax
r . 710 Bowsertown Road, Manteo, NC 27954 . 252.473.5702 Lab/Fax
255 A Wilmington Highway, Jacksonville, NC 28540 * 910.347.5843 Lab/Fax
ANALYTICAL &CONSULTING CHEMISTS inforaenvironmentalchemists com
Pender County Utility Operations Date of Report: Dec 21, 2023
Post Office Box 995 Customer PO #•
Burgaw NC 28425 Customer ID: 08100095
Attention: Report #: 2023-26818
Project ID: Maple Hill WVVTP
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
23-66001 Site: 004 11/13/2023 11:43 AM Solid/Sludge Client
Test
Method
Results
Date Analyzed
Soil Fertility
Calcium
EPA 200 7
1610 mg/kg
11 /21 /2023
Copper
EPA 200.7
<2.56 mg/kg
11 /21 /2023
Magnesium
EPA200-7282mg/kg
11/21/2023
Manganese
EPA20Q7
8.85 mg/kg
11121/2023
Potassium
EPA 200.7
153mg/kg
11/21/2023
Sodium
EPA 200.7
200 mg/kg
11121/2023
Zinc
EPA200.7
9.64mg/kg
11121/2023
Acidity (Soil Fertility)
NCDA-Agronomic Division
0.7 meq/100g
11128/2023
Base Saturation
NCDA-Agronomic Division
93.7 %
12/12/2023
Cation Exchange Capacity
NCDA-Agronomic Division
11.5 meq/100g
12112/2023
Exchangeable Sodium Percentage
NCDA-Agronomic Division
7.60 %
12112/2023
Humic Matter
NCDA-AgronomfcDivision
1.32 %
12/14/2023
Total Solids (%)
SM 2540 B
73.0 %
11117/2023
Total Phosphorus
SM 4500 P F
281 mg/kg
11/30/2023
pH
SW 846 Method 9046D
6.47 units
11/28/2023
Result estimated. Analyzed out of 15
minutes hold time.
Reoort #:: 2023-26818 Pang d nr 11

Environmental Chemists, Inc.
envirochem 6602 Windmill Way, Wilmington, NC 28405 * 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 . 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 . 910.347.5843 Lab/Fax
ANALYTICAL R CONSULTING CHEMISTS infoia environmentaichemists.com
Ponder County Utility Operations
Post Office Box 995
Burgaw NC 28425
Attention:
Date of Report: Dec 21, 2023
Customer PO #:
Customer ID: 08100095
Report #: 2023-26818
Project ID: Maple Hill WWTP
Lab ID Sample ID-
Collect Date/Time Matrix Sampled by
23-65002 Site: 005
11/13/2023
11:49 AM Solid/Sludge Client
Test
Method
Results
Date Analyzed
Soil Fertility
-
Calcium
EPA 200 7
336 mg/kg
11/21/2023
Copper
EPA 200.7
<2.21 mg/kg
11/21/2023
Magnesium
EPA 200.7
119mg/kg
11/21/2023
Manganese
EPA 200.7
<2.21 mg/kg
11/21/2023
Potassium
EPA200.7
<110mg/kg
11/21/2023
Sodium
EPA 200,7
219 mg/kg
11121 /2023
Zinc
EPA 200.7
<2.21 mg/kg
11/21/2023
Acidity (Soil Fertility)
NCDA-Agronomic Division
2 meq/100g
11/28/2023
Base Saturation
NCDA-Agronomic Division
65 3 %
12/1212023
Cation Exchange Capacity
NCDA-Agronomic Division
4.50 meq/100g
12/12/2023
Exchangeable Sodium Percentage
NCDA-Agronomic Division
21.2 %
12/12/2023
Humic Matter
NCDA-Agronomic Division
1.28 %
12/14/2023
Total Solids (%)
sM 2W a
75.2 %
11 /17/2023
Total Phosphorus
SM 4500 P F
96.0 mg/kg
11 /30/2023
pH SW 846 Method 8045U
Result estimated. Analyzed out of 15 minutes hold time.
6.26 units
11 /28/2023
Report V 20M.76818 Pan. 5 of 1 i

ANALYTICAL & CONSULTING CHEMISTS
F"00" -- q9
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 - 910.392,0223 Lab * 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 , 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 * 910.3475843 Lab/Fax
info 4�environmentalchemists.com
Pender County Utility Operations Date of Report: Dec 21, 2023
Post Office Box 995 Customer PO #•
Burgaw NC 28425 Customer ID: 08100095
Attention: Report #: 2023-26818
Project ID: Maple Hill WWTP
Lab ID Sample ID: Collect DatelTime Matrix Sampled by
23-65003 Site: 006 11/13/2023 12:00 PM Solid/Sludge Client
Test
Method
Results
Date Analyzed
Soil Fertility
Calcium
EPA 200.7
1530 mg/kg
11/21 /2023
Capper
EPA 20D 7
<3.26 mg/kg
11/21/2023
Magnesium
EPA 2007
338 mg/kg
11/21/2023
Manganese
EPA 200 7
6.48 mg/kg
11 /21/2023
Potassium
EPA 200.7
<163 mg/kg
11/21/2023
Sodium
EPA 200.7
280mg/kg
11/21/2023
Zinc
EPA 200.7
25.1 mg/kg
11/21/2023
Acidity (Soil Fertility)
NCDA-Agronomic Division
1 meq/100g
11 /28/2023
Base Saturation
NCDA-Agronomic Division
88.0 %
12/12/2023
Cation Exchange Capacity
NCDA-Agronomic Division
12.3 meq/100g
12/12/2023
Exchangeable Sodium Percentage
NCDA-Agronomic Division
9.90 %
12/12/2023
Humic Matter
NCDA-Agronomic Division
1.60 %
12/14/2023
Total Solids (%)
SM 2540 8
71.8 %
11/17/2023
Total Phosphorus
SM4500P F
281 mg/kg
11/30/2023
pH
SW 846 Method 13045D
6.52 units
11 /28/2023
Result estimated. Analyzed out of 15 minutes hold time.
Reoort # 2023-2f:818 Paae 6 of 11

r7-71 Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 - 910.392.0223 Lab * 910.392,4424 Fax
710 Bowsertown Road, Manteo, NC 27954 . 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 . 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS infofr4 environmentaicheniists.com
Pender County Utility Operations Date of Report: Dec 21, 2023
Post Office Box 995 Customer PO #:
BurgaW NC 28425 Customer ID: 08100095
Attention: Report #: 2023-26818
Project ID: Maple Hill WWTP
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
23-65004 Site: 007 11/13/2023 12:05 PM Solid/Sludge Client
Test
Method
Results
Date Analyzed
Soil Fertility
Calcium
EPA 200.7
295mg/kg
11/21/2023
Copper
EPA 200.7
<2.53 mg/kg
11 /21/2023
Magnesium
EPA 200.7
<126 mg/kg
11/21/2023
Manganese
EPA 200.7
<2.53 mg/kg
11 /21 /2023
Potassium
EPA 200.7
<126mg/kg
11/21/2023
Sodium
EPA 200.7
<126 mg/kg
11/21/2023
Zinc
EPA 200.7
<2.53 mg/kg
11/21 /2023
Acidity (Soil Fertility)
NCDA-Agronomic Division
0.2 meq/100g
11/28/2023
Base Saturation
NCDA Agronomic Division
92.2 %
12/12/2023
Cation Exchange Capacity
NCDA-Agronomic Division
3.10 meq/100g
12/12/2023
Exchangeable Sodium Percentage
NCDA-Agronomic Division
17.8 %
12/12/2023
Humic Matter
NCDA-Agronomic Division
0.42 %
12/14/2023
Total Solids (%)
SM 2540 E
75.2 %
11/17/2023
Total Phosphorus
SM 4500 P F
169 mg/kg
11 /3012023
pH
SW 846 Method 90450
7.25 units
11 /28/2023
Result estimated. Analyzed out of 15 minutes hold time.
ReDOrt 4 2023.26818 Pan. 7 rtt I

F"007 -:"qql Environmental Chemists, Inc,
' 1 b602 Windmill Way, Wilmington, NC 28405 . 910.392.0223 Lab ■ 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 - 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS info!p�environmentalchemists.coln
Pender County Utility Operations Date of Report: Dec 21, 2023
Post Office Box 995 Customer PO #:
Burgaw NC 28425 Customer ID: 08100095
Attention: Report ##: 2023-26818
Project ID: Maple Hill WWTP
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
23-65005 Site: 008 11/13/2023 12:00 PM Solid/Sludge Client
Test
Method
Results
Date Analyzed
Soil Fertility
Calcium
EPA 200.7
635 mg/kg
11 /2112023
Copper
EPA 200.7
<2.72mg/kg
11/21/2023
Magnesium
EPA 2003
188 mg/kg
11 /21/2023
Manganese
EPA 200.7
5.80 mg/kg
11 /2112023
Potassium
EPA 200.7
<136 mg/kg
11 /21/2023
Sodium
EPA 200.7
248 mg/kg
11 /21 /2023
Zinc
EPA 200.7
6.21 mg/kg
11 /21/2023
Acidity (Soil Fertility)
NCDA-Agronomic Division
3 meq/100g
11 /28/2023
Base Saturation
NCDA-Agronomic Division
61.0 %
12/1212023
Cation Exchange Capacity
NCDA-Agronomic Division
8.30 meq/100g
12/12/2023
Exchangeable Sodium Percentage
NCDA-Agronomic Division
13.0 %
12/1212023
Humic Matter
NCDA-Agronomic Division
1.99 %
12/14/2023
Total Solids (%)
SM 2540 B
72.4 %
11/17/2023
Total Phosphorus
SM 4500 P F
123 mg/kg
11/30/2023
pH
SW 846 Method 9045D
5.97 units
11/28/2023
Result estimated. Analyzed out of 15 minutes hold time.
Report #-, 2023-26818 Paw 8 at 11

e
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 , 910.392.0223 Lab a 910.392.4424 Fax
710 8owsertown Road, Manteo, NC 27954 * 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 a 910.347.5843 Lab/Fax
info,a environmentalchemists.com
Pender County Utility Operations Date of Report: Dec 21, 2023
Post Office Box 995 Customer PO #:
Burgaw NC 28425 Customer ID: 08100095
Attention: Report #: 2023-26818
Project ID: Maple Hill WWTP
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
23-65006 Site: 009 11/13/2023 12:17 PM Solid/Sludge Client
Test
Method
Results
Date Analyzed
Soil Fertility
Calcium
EPA 200 7
598 mg/kg
11/21/2023
Copper
EPA200.7
<2.51 mg/kg
11/21/2023
Magnesium
EPA200.7
194mg/kg
11/21/2023
Manganese
EPA200.7
<2.51 mg/kg
11/21/2023
Potassium
EPA200.7
<125mglkg
11/21/2023
Sodium
EPA 2D0.7
<125 mg/kg
11 /2112023
Zinc
EPA200.7
5.32mg/kg
11/21/2023
Acidity (Soil Fertility)
NCDA-Agronomic Division
2 meq/100g
11/28/2023
Base Saturation
NCDA-Agronomic Division
74.5 %
12/12/2023
Cation Exchange Capacity
NCDA-Agronomic Division
6.60 meq/100g
12/12/2023
Exchangeable Sodium Percentage
NCDA-Agronomic Division
8.20 %
12/12/2023
Humic Matter
NCDA-Agronomic Division
0.73 %
12/1412023
Total Solids (%)
SM 2540 a
80.8 %
11 /17/2023
Total Phosphorus
SM4500 P F
95.1 mg/kg
11/30/2023
pH
SW 846 Method 9045D
5.69 units
11/2812023
Result estimated. Analyzed out of 15 minutes hold time.
Revert*' 2023-26818 Pace 9 of i 9

Environmental Chemists, Inc.
9 6602 Windmill Way, Wilmington, NC 28405 . 910.392.0223 Lab ■ 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 ■ 252.473.5702 Lab/Fax
- 255-A Wilmington Highway, Jacksonville, NC 28540 . 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS [e-mail]
Pender County Utility Operations Date of Report: Dec 21, 2023
Post Office Box 995 Customer PO #:
Burgaw NC 28425 Customer ID: 08100095
Attention: Report #: 2023-26818
Project ID: Maple Hill WWTP
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
23-65007 Site: 010 11/13/2023 12:24 PM Solid/Sludge Client
Test
Method
Results
Date Analyzed
Soil Fertility
Calcium
EPA 200.7
977mg/kg
11/21/2023
Copper
EPA 200.7
<2.59 mg/kg
11/21/2023
Magnesium
EPA 200.7
268 mglkg
11/21/2023
Manganese
EPA 200.7
<2.59 mg/kg
11/21/2023
Potassium
EPA 200.7
<129mglkg
11/21/2023
Sodium
EPA 200.7
<129 mg/kg
11/21/2023
Zinc
EPA 200.7
13.2 mg/kg
11/21/2023
Acidity (Soil Fertility)
NCDA-Agronomic Division
2 meq/100g
11/28/2023
Base Saturation
NCDA-Agronomic Division
78.4 %
12/12/2023
Cation Exchange Capacity
NCDA-Agronomic Division
9.40 meq/100g
12/12/2023
Exchangeable Sodium Percentage
NCDA-Agronomic Division
5.90 %
12/12/2023
Humic Matter
NCDA-Agronomic Division
2.81 %
12114/2023
Total Solids (%)
SM 2540 D
77.4 %
11/17/2023
Total Phosphorus
SM4500 P F
126 mg/kg
11/30/2023
pH
SW $46 Method 9045D
5.24 units
11 /28/2023
Result estimated. Analyzed out of 15 minutes hold time.
Report # 2023.26818 �� �— Pace 10 of 11

Environmental Chemists, Inc.
envirochem 6602 Windmill Way, Wilmington, NC 28405 a 910.392.0223 Lab a, 910.392.4424 Fax
w
710 Bowsertown Road, Manteo, NC 27954 e 252.473.5702 Lab/Fax
255 A Wilmington Highway, Jacksonville, NC 28540 - 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS info: a environmentalchemists.com
Pender County Utility Operations
Date of Report: Dec 21, 2023
Post Office Box 995
Customer PO #:
Burgaw NC 28425
Customer ID: 08100095
Attention:
Report #: 2023-26818
Project ID: Maple Hill WWTP
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
23-65008 Site: 011
11/13/2023
12:35 PM Solid/Sludge Client
Test
Method
Results Date Analyzed
Soil Fertility
Calcium
EPA200.7
528mg/kg
11/21/2023
Copper
EPA200.7
<2.68 mg/kg
11/21/2023
Magnesium
EPA200.7
184mg/kg
11/21/2023
Manganese
EPA200.7
<2.68mg/kg
11/21/2023
Potassium
EPA 200 7
<134 mg/kg
11 /2112023
Sodium
EPA 2007
8.74 mg/kg
11/21/2023
Zinc
EPA 200 7
<134 mg/kg
11/21/2023
Acidity (Soil Fertility)
NCDA-Agronomic Division
2 meq/100g
11/28/2023
Base Saturation
NCDA-Agronomic Division
58.8 %
12/12/2023
Cation Exchange Capacity
NCDA-Agronomic Division
6.50 meq/100g
12/12/2023
Exchangeable Sodium Percentage
NCDA-Agronomic Division
0.600 %
12/12/2023
Humic Matter
NCDA-Agronomic Division
1.57 %
12/14/2023
Total Solids (%)
SM 254a s
79.9 %
11 /17/2023
Total Phosphorus
SM 4600 P F
117 mg/kg
11 /30/2023
pH
5W a46 Method 9045D
4.42 units
11/28/2023
Result estimated. Analyzed out of 15 minutes hold time.
Comment: Results, except pH, reported on a dry weight basis. pH reported on an as received basis.
�1-
Reviewed by: �
`�
d
s
Report #:- 2023-MIS Page 71 of 11

-<<r'f vafrlfen[as Lnenllst, Inc., Wilmington, NC Lab #94
6602 Windmill '
Wilmington, NC 28
Sample Receipt Checklist 910.392.0
Client:
Date. Report Number: 2023-ljli
Receipt of sample: ECHEN1 Picku ❑
❑ YES ❑ NO � N p Client Deliver}' UPS ❑
/A 1. Were custody seals present on the cooler?
Cl YES ❑ Pl0 x N/A 2 If
FedEx ❑
Other El
custody seals were present, were they intact/unbroken?
Original temperature upon receipt
How temperature taken: O Temp oC Corrected temperature upon receipt
Temperature Blank O Against Bottles
lR Gun 1D: Thomas Traceable S/N 210886869
Cx1 YES IR Gun Correction Factor °C: 0.0
❑ NO 3. If temperature of cooler exceeded 6 C, was Project higr./QA notified?
O YES ❑ NO 4. Were proper custod
p Y procedures {relinquished/received) follov✓ed?
DX YES ❑ NO
$• Were sample ID s listed on the COC?
O YES ❑ NO 6. Were samples ID's listed on sample containers?
® YES ❑ NO i. Were collection date and time listed on the C©C?
LO YES C) NO 8. Were tests to be performed listed on the COC?
G YES ❑ NO 9. Did samples arrive in proper containers for each test?
O YES ❑ NO 10. Did samples arrive in good condition for each test?
O YES ❑ NO 11. Was adequate sample volume available?'
C YES ❑ NO 12. Were samples received within proper holding time for i
D YES ❑ NO 13. Were acid preserved samples received at a pH of <2?
CJ YES ❑ NO 1Q. Were cyanide samples received at a pH s12?
❑ YES ❑ NO 15- Were sulfide samples received at a pH >9?
❑ YES ❑ NO 16. Were NH.3 KN/phenol received at a chlorine residua` of <C 5 m; L,�
D YES ❑ NO 17. Were YES ® NO Sulfide/Cyanide received at a chlorine residual of <0 5 m/L?
❑ 18. Were orthophosphate samples filtered in the field within 15 m n,,tmc,?
* TOC/volat•les are pH checked at t;nte of anal, sis and recorded on the ben-hsheet
** Bacteria samples are checked for Chlorine at time of analysis and recorded on the bench_heet.
nested tests?
Sample Preservation: (Must be completed for any sample(s) incorrectly preserved or with headspace)
Sample{sj were received incorrectf
by adding (circle one): HSO H Y Preserved and were adjusted accordingly
` N0; HC1 NaOH
Time of preservation: If more than one p a
reservative is needed, notate n comments below
11C"? %:Ct ry C�S;C-re• S?.. `e r---23 3: CO
''f --zxro__t r (Jr�52^J�a Sd'T7
t-e i_a:e aC 'f d P ,2i Ob'a " a f e. SdTF e
."e C'_>`CSN3i (' :` `?� Q?i^.` s3-
volatiles u - "' Sample(s)
- were receitied with headspace
COMMENTS:
DOC. QA.002 Rev 1

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