NCG060184_2024 DMR_20240209

NCDEQ Division of Energy,Mineral and Land Resources
Stormwater Discharge Monitoring Report(DMR) Form for NCGO60000
Food and Kindred
Click here for instructions
Complete,sign,scan and submit the DMR via the Stormwater NPDES Permit Data Monitoring Report(DMR)Upload form within
30 days of receiving sampling results. Mail the original,signed hard copy of the DMR to the appropriate DEMLR Regional Office.
Certificate of Coverage No. NCG060184 Person Collecting Samples:Jeremy Spencer
Facility Name: Pilgrim's Pride Corp.,Wingate Feed Mill/Truck Shop Laboratory Name: Environmental Chemists, Inc.
Facility County:Union Laboratory Cert. No.: 94
Discharge during this period:❑✓ Yes ❑ No (if no,skip to signature and date)
Has your facility implemented mandatory Tier response actions this sample period for any benchmark exceedances?❑Yes ❑,/ No
If so,which Tier(I, II,or III)?
A copy of this DMR has been uploaded electronically via https://edocs.deq.nc.gov/Farms/SW•DMR ❑/ Yes ❑ No
Date Uploaded: February 9,2024
Analytical Monitoring Requirements for Outfalls with Industrial Activities—Benchmarks in(Red)
Parameter Parameter Outfall#001A Outfall#002A Outfall#003A Outfall Outfall
Code
N/A Receiving Stream Class Rays Fork Creek Rays Fork Creek Rays Fork Creek
N/A Date Sample Collected MM/DD/YYYY 1/9/2024 1/9/2024 1/9/2024
46529 24-Hour Rainfall in inches 1.82 1.82 1.82
C0530 TSS in mg/L(100 or 50*) 21.1 12.8 19.5
00400 pH in standard units(6.0--9.0) 7.0 7.5 6.9
00556 Oil&Grease in mg/L(30) <5.0 <5.26 <5.10
31616 Fecal Coliform per 100 ml of
freshwater(if required)(1000)
61211 Enterococci per 100 ml of saltwater
(if required)(500)
00340 Chemical Oxygen Demand in mg/L 27.0 34.0 30.0
Additional parameters for outfalls in drainage areas that use>55 gallons per month of new hydraulic oil on average
NCOIL Estimated New Motor/Hydraulic Oil
Usage in gal/month 71 71 71
00552 Non-Polar Oil&Grease in mg/L(15) ??? ??? ???
Outfalls to Outstanding Resource Waters(ORW),High Quality Waters(HQW),Trout Waters(Tr)and Primary Nursery Areas(PNA)
have a benchmark TSS limit of S0 mg/L.All other water classifications have a benchmark of 100 mg/L
Notes(optional):
"I certify by my signature below,under penalty of law,that this document and all attachments were prepared under my direction or supervision in
accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted.Based on my
inquiry of the person or persons who manage the system,or those persons directly responsible for gathering the information,the information
submitted is,to the best of my knowledge and belief,true,accurate,and complete.I am aware that there are significant penalties for submitting
false information,including the possibility of fines and imprisonment for knowing violations."
.2- -.zy
Signature of Permittee or Delegated Auth zed Individual Date
Email Address [e-mail] Phone Number [phone]

Environmental Chemists, Inc.
envirochem 6602 Windmill Way,Wilmington,NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road,Manteo,NC 27954 • 252.473.5702 Lab/Fax
w 255-A Wilmington Highway,Jacksonville,NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL&CONSULTING CHEMISTS [e-mail]
Pilgrim's Pride-Wingate Feed Mill Date of Report. Jan 19,2024
205 Edgewater Dr. Customer PO#:
Wingate NC 28174 Customer ID: 18020004
Attention: Report#: 2024-00665
Project ID: Wingate Feed Mill-Stormwater
Lab ID Sample ID: Pilgrim's Pride-Wingate Collect Date/Time Matrix Sampled by
Feed Mill
24-01621 Site: Outfall #001A 1/9/2024 9:25 AM Water client
Test Method Results Date Analyzed
Oil& Grease(O&G) EPA 1884 Rev B <5.00 mg/L 01/16/2024
Residue Suspended(TSS) SM 2540 0.2015 21.1 mg/L 01/10/2024
pH SM4500HB2011 7.0units 01/16/2024
Result estimated Analyzed out of 15 minutes hold time
COD SM 5220 D-2011 27.0 mg/L 01/11/2024
Lab ID Sample ID: Pilgrim's Pride-Wingate Collect DatefTime Matrix Sampled by
Feed Mill
24-01623 Site: Outfall#002A 1/9/2024 9:15 AM Water client
Test Method Results Date Analyzed
Oil&Grease(O&G) EPA 1684 Rev B <5.26 mg/L 01/16/2024
Residue Suspended (TSS) sat 2540 0.2015 12.8 mg/L 01/10/2024
pH SM 4500 H B-2011 7.5 units 01/16/2024
Result estimated. Analyzed out of 15 minutes hold time
COD sM 5220 D-2011 34.0 mg/L 01/11/2024
Lab ID Sample ID: Pilgrim's Pride-Wingate Collect DatefTime Matrix Sampled by
Feed Mill
24-01624 Site: Outfall#003A 1/9/2024 8 55 AM Water client
Test Method Results Date Analyzed
Oil& Grease(O&G) EPA 1664 Rev B <5.10 mg/L 01/16/2024
Residue Suspended (TSS) SM 2540 D-2015 19.5 mg/L 01/10/2024
pH SM 450011 B-2011 6.9 units 01/16/2024
Result estimated. Analyzed out of 15 minutes hold time.
COD SM 5220 D-2011 30.0 mg/L 01/11/2024
Comment:
Reviewed by: N\liCad'I CY! O4-
Report it: 2024.00685 Page I of I

Environmental Chemists, Inc.
envirochem 6602 Windmill Way,Wilmington,NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
90 710 Bowsertown Road,Manteo,NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway,Jacksonville,NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL&CONSULTING CHEMISTS infoOpenvironmentalchemists.com
Pilgrim's QC - 2024-00665
LCS
Parameter True Value Result % True Value Limits
mg/L mg/L %
COD 1000 983 98 90-110
TSS 94.6 91.0 96 82.4-1 18
pH _ 10.0 9.9 99 90.110
OIL&GREASE 40.0 35.8 90 78-1 14
MS/MSD
True Value Recovery %Recovery % Limits % Limits %
Parameter
mg mg/L Difference Recovery Difference
COD 45.0 46/49 102/109 7 80-120 <20
TSS N/A NA N/A N/A N/A N/A
pH N/A N A NA N?A N/A N/A
OIL& GREASE 40.0 33.3 83 NJA 78-114 S. 18
DUPLICATE SAMPLES
Results
Parameter m /L %Difference Limits %
g
COD N/A N/A N/A <10
TSS 276.7 260.0 6 <10
pH N/A N/A N/A <10
OIL& GREASE <5.0 <5.0 0 <_ 18
BLANK
Results Limit
Parameter
mg/L mg/L
COD <10 10
TSS <2.5 2.5
pH N/A N/A
OIL&GREASE <5.0 5.0

Environmental Chemist, Inc., Wilmington, NC Lab#94
6602 Windmill Way
Wilmington, NC 28405
Sample Receipt Checklist 9�0'392'0223
Client: p1 ‘ar k 'MS VI' i � Date:
7Report Number: 2024-
Receipt of sample: ECHEM Pickup 11 Client Delivery 0 UPS 0 FedEx 0❑ YES 0 NO O N/A 1. Were custody seals present on the cooler? Other 0
❑ YES 0 NO 18 N/A 2. If custody seals were present, were they intact/unbroken?
Original temperature upon receipt MO 'C Corrected temperature upon receipt
How temperature taken: ElTemperature Blank 0 Against Bottles OC
IR Gun ID: Thomas Traceable S/N 210886869 IR Gun Correction Factor°C: 0.0
© YES ❑ NO 3. If temperature of cooler exceeded 6°C, was Project Mgr./QA notified?
0 YES ❑ NO 4. Were proper custody procedures(relinquished/received)followed?
S. Were sample ID's listed on the COC?
O YES ❑ NO 6. Were samples ID's listed on sample containers?
N YES ❑ NO 7. Were collection date and time listed on the COC?
E YES ❑ NO 8. Were tests to be performed listed on the COC?
!] YES 0 NO 9. Did samples arrive in proper containers for each test?
D YES ❑ NO 10. Did samples arrive in good condition for each test?
© YES ❑ NO 11. Was adequate sample volume available?'
0 YES 0 NO 12. Were samples received within proper holding time for requested tests?
YES ❑ NO 13. Were acid preserved samples received at a pH of<2? *
❑ YES ❑ NO 14. Were cyanide samples received at a pH>12?
O YES ❑ NO 15. Were sulfide samples received at a pH>9?
❑ YES 0 NO 16. Were NH3/TKN/Phenol received at a chlorine residual of<0.5 m/L?**
0 YES ❑ NO 17. Were Sulfide/Cyanide received at a chlorine residual of<0.5 m/L?
❑ YES 0 NO 18. Were orthophosphate samples filtered in the field within 15 minutes?
* TOC/Volatiles are pH checked at time of analysis and recorded on the benchsheet.
** Bacteria samples are checked for Chlorine at time of analysis and recorded on the benchsheet.
Sample Preservation: (Must be completed for any sample(s) incorrectly preserved or with headspace)
Sample(s) were received incorrectly preserved and were adjusted accordingly
by adding(circle one): H2SO4 HNO3 HCI NaOH
Time of preservation: If more than one preservative is needed, notate in comments below
Note:Notify customer service immediately for incorrectly preserved samples.Obtain a new sample or
notify the state lab if directed to analyzed by the customer.Who was notified,date and time
Volatiles Samples)
were received with headspace
COMMENTS:
DOC.QA,002 Rev 1

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