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WQ0006101_2023 Residual Annual Report_20240212 (2)
Initial Review Reviewer nathaniel.thornburg Is this submittal an application? (Excluding additional information.) * Yes No If not an application what is the submittal type?* Annual Report Residual Annual Report Additional Information Other Annual Report Year* 2023 Permit Number (IR) * WQ0006101 Applicant/Permittee City of Dunn Email Notifications Does this need review by the hydrogeologist? * Yes No Regional Office Fayetteville CO Reviewer Wanda GeraId:Wanda.Gerald@deq.nc.gov Admin Reviewer Wanda Gerald Submittal Form Project Contact Information Please provide information on the person to be contacted by NDB Staff regarding electronic submittal, confirmation of receipt, and other correspondence. Name* Drew Matthews Email Address* dmatthews@soilplus.net Project Information ......................... Application/Document Type* New (Fee Required) Modification - Major (Fee Required) Renewal with Major Modification (Fee Required) Annual Report Additional Information Other Phone Number* 2528839301 Modification - Minor Renewal GW-59, NDMR, NDMLR, NDAR-1, N DAR-2 Residual Annual Report Change of Ownership We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form. https://edoes.deq.nc.gov/Forms/NonDischarge_Monitoring_Report Permit Type:* Wastewater Irrigation High -Rate Infiltration Other Wastewater Reclaimed Water Closed -Loop Recycle Residuals Single -Family Residence Wastewater Other Irrigation Permit Number:* WQ0006101 Has Current Existing permit number Applicant/Permittee Address* PO Box 1065, Dunn, NC 28335 Facility Name* City of Dunn Class B Residuals Program Please provide comments/notes on your current submittal below. At this time, paper copies are no longer required. If you have any questions about what is required, please contact Nathaniel Thornburg at nathaniel.thornburg@ncdenr.gov. Please attach all information required or requested for this submittal to be reviewed here. (Application Form, Engineering Plans, Specifications, Calculations, Etc.) 2023 Dunn Annual Report.pdf 3.47MB Upload only 1 PDF document (less than 250 MB). Multiple documents must be combined into one PDF file unless file is larger than upload limit. * By checking this box, I acknowledge that I understand the application will not be accepted for pre -review until the fee (if required) has been received by the Non -Discharge Branch. Application fees must be submitted by check or money order and made payable to the North Carolina Department of Environmental Quality (NCDEQ). I also confirm that the uploaded document is a single PDF with all parts of the application in correct order (as specified by the application). Mail payment to: NCDEQ — Division of Water Resources Attn: Non -Discharge Branch 1617 Mail Service Center Raleigh, NC 27699-1617 Signature 01f1 i �4e*A~ Submission Date 2/12/2024 CITY OF DUNN 2023 ANNUAL LAND APPLICATION OF RESIDUAL BIOSOLIDS REPORT CLASS B PROGRAM WQ0006101 Submitted by: Soil Plus PO Box 1396 Oxford, North Carolina 27565 February 12, 2024 SOIL PLUS SOIL PLUS February 12, 2024 NCDEQ-DWR Information Processing Unit 1617 Mail Service Center Raleigh, North Carolina 27699-1617 Re: 2023 LAND APPLICATION ANNUAL REPORT City of Dunn "Class B" Program NC Permit No.: WQ0006101 Soil Plus Project No. 202009 Information Processing Unit: Soil Plus, LLC (Soil Plus) is submitting all monitoring and reporting requirements as specified in the above referenced permit for the City of Dunn on behalf of Granville Farms, Inc. Soil Plus compiled this report using data gathered during the compliance year. This data includes (1) certification form, (2) residual sampling, (3) field loading calculations, (4) pathogen and vector attraction reduction documentation, (5) standard soil fertility nutrient analysis. The City of Dunn conducted application events on permitted fields in Cumberland and Harnett counties during 2023. A total of 1,456,000 gallons or 154.22 dry tons of permitted residual biosolids were land applied to the City of Dunn's permitted fields. If there is any further information required or questions regarding this report, please do not hesitate to contact me or the City of Dunn (910-766-0997) for further assistance. Respectfully, Drew Matthews, Soil Plus cc: Donrie Dukes, City of Dunn Jason Smith, Granville Farms PO Box 1396 Oxford, NC 27565 (252) 883-9301 dmatthews @s oilplus.net www.soilplusllc.com City of Dunn 2023 Annual Land Application of Residual Biosolids Report WQ0006101 Dunn, NC Annual Land Application Certification Form Annual Residual Sampling Summary Form Field Loading Summary Forms Pathogen & Vector Attraction Reduction Form 2023 Soil Samples City of Dunn 2023 Class B Annual Report WQ Permit# WQ0006101 Annual Certification Form Source Summary Field Loading Summary ANNUAL 1AND. APPLICATION CERTIFICATION FORM' PermitNumber FacilityNwne Umd.Appfic-20on Operator County Phone Numbtr Yi wQff-161 01 City of Dunn G.-='TMC FUMS, Inc. 1-12M.at M.0)-166-0997, .lAiW-stp.plicatioa.ofresiduals; as allowcd by pct=dt.-oc=ed.du%jngt1ne post calendar tar? lf No, 2" skip P AandP= ye 4 s No B a3d proceed to Part C. Adso, Ifresidwals W= ga zed hart -toot lwid..:ippfiedplease a:ttAch:a�txP1 nanatioonhowthe residva.4 were handled. Application S urrunar, Total numbcr of Application: fields in the. permit Total number .offield s utilized: for lind APP*Adqn duri-9 the yean* 6 T%21.amoantof dry tons appkd during the Yffitall -0pplicItiOn Site$-, 154-22 To—W number of acres udilizes for I=d 4pplka6.n during the Year 573 Y Na M M9 I R n pe.rrait? r%CiETYW" CQ P Xi AAkOdiO -4-COTKIld fts-Offlitland-ap pa Ldudingbut o&A Bwittd to kedis 1-131Aaw)UsneA.-by thc.,Di,Won a . 0 'hc facMty w 4: nqt z-4impliantthe. dates, and expL* Omxtive: action takm., .If please, pro -vine a written deslaiption-vi* t A. Onlyfesidugh: approved fair this pegqowerttppaed ttilt Putted' sae$ vu - I Soil pli vu adjusted as Spcdfierl in d%L aniflime i* top PROCat l st6. i 3, Annual sods arsalysig oft cacih.site: too"ag feSIdjalla during the P-t estterst ar.vm. and hies Co W. of Isbot2tory 4. AAnual TCLP aiudysis (if. "Wred.) vns petforrata: and: du . tZ (3) copict of ccrdficd Wbmtorjr resulis are a=chr-d 5. All other monkoxiog was pexfo=od in iccordanccvith the per-ruit and reported duringlhe year as required: =d Hires (3)ampler of rrsulct Ate attached 6.11w fkffity did wt exCeed any of &g.Pollummat Cbidcentratlon.Unuts, in i5A NCAC 02T 7, as..sp4d6ed in the Und.Application Ptnritwre comPud th lipplible.to 40CFR Paa 503 regulatd far lhies 6. All -me MMM mplied v tutomgw. repoving*=q%d * ts1nt5A.NCJkC 02T.111.1 were co kh (apor-a -to 40 CFX Put.50*3.regulatvd ficilides) 9, AR 0 6 pmd In the permttwcTcwmphed:-wit1a or, in the -caic-df.adci iafiorn, ptibrauthoriiat onwm rectiveJ froM the Drvision of Watcr Quality 10, No cono2vendolAi of Ground.Witei Quality. Standar& bdrutred at a inonkma bk Wil ar explimations of violationd are attached -to, include 2ppropnatc actions and Pt!0P*Cr,CrDP MIna_O-Went W" Ptt formed. on. mM reach =vg residuals, As specified in. the Poxmit 12.N,o =noffvf=SiC1u2lq from the a*pocadon%siLaunw.adi-acentproperty orneaxby surfacewatersh2a accurrett jj.jAj.hit ffcrrap&ime= 2s.syecified on the permit were maim aineddiu-ingeach app]1catiork of rcsiduals, Pgri:C - terfification; .y,i.mder penalty.eflaw, that the aban 106nuation is, to the heloinfiny-kno eii accurate, and venawes for submitting Use infb=` ZT2 Complete. I aM avrAft OlAt 01M aXIM Significant :ioa possibility of fines and ixaptisonment for knowing vriolatinns." Steirert Neusebafer, OW .«lUazger 2/12/24 Signatum of Populace Dare a=1 ittee Nam. a�ATjdc (type or vAn* q 2/8/24 W8124 signatutcorprepatc;r* Date (if different fi-om Permittee) *.Przpa=riS defimedla 40 CFR Paz* 563.9 (r) and M.NCAC=.1102(26) Signature of Land Applip-T (if different from Permittet) ... ......... .......... I ............... ........... . ........... .............. Source Summary Report Dunn WWrP 1,456,000 154.22 Total 1,456,000 154.22 Site# CU-34 Site# FIA-08 YEAR TO DATE FIELD LOADING SUMMARY CROPS USED AND VOLUME APPLIED PERMITTED CROPS AND LOADING RATES Acres Volume Crop 1 PAN Crop 2 PAN Crop 1 PAN 1 Crop 2 PAN 2 Field Used Avvlied Total DT lbs/Ac. lbs/Ac. Crop 1 Name PAN Used Crop 2 Name PAN Used 1 4.8 65,000 6.88 40.00 Annual Ryegrass - 136 29.4% Hay 2 4 58,500 6.20 43.20 Annual Ryegrass - 136 31.8% Hay 3 4.3 58,500 6.20 40.18 Annual Ryegrass - 136 29.5% Hay 4 6.2 71,500 7.57 34.06 Annual Ryegrass - 123 27.7% Hay 8 18.3 611,000 64.72 98.61 Common 225 43.8% Bermudagrass Hay 9 19.7 591,500 62.65 88.68 Common 225 39.4% Bermudagrass Hay Total 1,456,000 City of Dunn 2023 Class B Annual Report WQ Permit# WQ0006101 Residual Sampling Summary Forms Dunn WWTP Field Loading Calculations 2023 Analytical 2023 TCLP Oa N c 0 V 1 71 O,w qu '� La q Z U U m N T .Ci m u lu o � ^ u O .y •C Q y d � O Gs -� ..0.. � w m • IV.• O y V �a q � � m 3 •O �' i� dl \ni N1 � � .. � � : N ' � � h � � I N W O i �. .� c^ a �4^ 0. � �" v�i '�G �p .%yV•' N � i _...._._.l o.© ,� ' o C? d d 41 d d g d d c c ro m j .� z n v 'z Z Z z Z z Z ZIs n °" U i v U z z I z '•" '� ''�` �Z, z z z Z Iz z z :z 00 cf A a Y 4j on i•' N i+ � V q7 ! � G•� �,.. y/I i Y i T V � V � G� � � :l iSi M v x W I I J.-..__ _lz.._ .._._.......__....:. _..... _..... A,,AGMAN FIELD LOADING ESTIMATES Facility Dunn WWTP Sample Date 5/3/2023 % Solids 2.54 Mineralization Rate 0.3 Gallons per DT 9,441.27 pH 6 Sodium Absorpotion 0.66 <5.0 Safe Ratio NITROGEN APPLICATION 5.0 - 10.0 Careful Management >15.0 Do Not Land Apply TKN (mg/kg) 44,900 lbs./1,000 gal 9.51 Ammonia Nitrogen (mg/kg 394.00 lbs./1,000 gal 0.08 Nitrate -Nitrite (mg/kg) 394.00 lbs./1,000 gal 0.08 PLANT AVAILABLE NITROGEN SURFACE APPLIED PAN (mg/kg) 13,943 lbs./1,000 gal 2.95 PLANT AVAILABLE NITROGEN INJECTED/INCORPORATED APPLIED PAN (mg/kg) 14,140 lbs./1,000 gal 3.00 Volatization Rate= 0.5 Surface Application 1.0 Injection/Incorporation EPA METAL LIMITS 1 st Year 2nd Year 3rd Year 4th Year 5th Year Ceiling Conc. Limit (mg/kg) 75 85 4,300 840 57 420 100 7,500 HEAVY METAL CONCENTRATION NUTRIENT APPLICATION Potassium lbs./1,000 gal 1.30 Phosphorus lbs./1,000 gal 4.24 Calcium lbs./1,000 gal 1.85 Magnesium lbs./1,000 gal 0.68 Manganese lbs./1,000 gal Sulfur lbs./1,000 gal Molybdenum lbs./1,000 gal 0.00 HEAVY METAL LOADING Arsenic (mg/kg) 3.77 Arsenic lbs./1,000 gal 0.00 Cadmium (mg/kg) 1.56 Cadmium lbs./1,000 gal 0.00 Copper (mg/kg) 269.00 Copper lbs./1,000 gal 0.06 Lead (mg/kg) 29.90 Lead lbs./1,000 gal 0.01 Mercury (mg/kg) 0.43 Mercury lbs./1,000 gal 0.00 Nickel (mg/kg) 14.30 Nickel lbs./1,000 gal 0.00 Selenium (mg/kg) 1.97 Selenium lbs./1,000 gal 0.00 Zinc (mg/kg) 579.00 Zinc lbs./1,000 gal 0.12 RESIDUAL NITROGEN CALCULATION Surface Application Injection/Incorporation Application Remaining Remaining Organic Organic PAN PAN Nitrogen PAN PAN Nitrogen TKN (mg/kg) (lbs/DT) (mg/kg) TKN (mg/kg) (lbs/DT) (mg/kg) 44,900 13,943 27.89 30,957 44,900 14,140 28.28 30,760 30,957 4,644 9.29 26,314 30,760 4,614 9.23 26,146 26,314 1,974 3.95 24,340 26,146 1,961 3.92 24,185 24,340 913 1.83 23,427 24,185 907 1.81 23,278 23,427 439 0.88 22,988 23,278 436 0.87 22,842 Equations 1st Yr. PAN (mg/kg)=(MR x (TKN-NH3))+(VR x NH3)+NOx 2nd Yr PAN (mg/kg)= 2nd Yr. TKN x (MR/2) 3rd Yr PAN (mg/kg)= 3rd Yr. TKN x (MR/4) 4th Yr PAN (mg/kg)= 4th Yr. TKN x (MR/8) 5th Yr PAN (mg/kg)= 5th Yr. TKN x (MR/16) Total 21,912 43.82 Total 22,058 44.12 Contact: Drew Matthews Client: Soil Plus P.O. Box 1396 Oxford, NC 27565 Meritech Work Order # 05032394 Parameters % Total Solids Ammonia, Nitrogen TKN Nitrate/Nitrite, Nitrogen Aluminum, total Arsenic, total Cadmium, total Calcium, total Copper, total Lead, total Magnesium, total Mercury, total Molybdenum, total Nickel, total Phosphorus, total Potassium, total Selenium, total Sodium, total Zinc, total pH Meritech, Inc. Environmental Laboratory Laboratory Certification No. 165 Sample: DN 050323 Grab Results 2.54 <394 mg/kg 44,900 mg/kg <394 mg/kg 8,980 mg/kg 3.77 mg/kg 1.56 mg/kg 8,740 mg/kg 269 mg/kg 29.9 mg/kg 3,200 mg/kg 0.433 mg/kg 7.99 mg/kg 14.3 mg/kg 20,000 mg/kg 6,140 mg/kg <1.97 mg/kg 1,800 mg/kg 579 mg/kg 6.0 S.U. Analysis Date 5/4/23 5/4/23 5/10/23 5/5/23 5/5/23 5/5/23 5/5/23 5/8/23 5/5/23 5/5/23 5/5/23 5/9/23 5/5/23 5/5/23 5/8/23 5/8/23 5/5/23 5/5/23 5/8/23 5/4/23 Report Date: 5/12/2023 Project: Dunn WWTP Date Sample Rcvd: 5/3/2023 Reporting Limit 0-100 % 394 mg/kg 20 mg/kg 394 mg/kg 2.50 mg/kg 1.40 mg/kg 0.200 mg/kg 10.0 mg/kg 1.00 mg/kg 0.500 mg/kg 10.0 mg/kg 0.02 mg/kg 0.500 mg/kg 2.0 mg/kg 2.00 mg/kg 20.0 mg/kg 1.97 mg/kg 20.0 mg/kg 0.500 mg/kg 1.0 - 14.0 S.U. 5/3/23 Method SM 2540B EPA 350.1 EPA 351.2 EPA 353.2 EPA 200.7 EPA 200.7 EPA 200.7 EPA 200.7 EPA 200.7 EPA 200.7 EPA 200.7 EPA 245.1 EPA 200.7 EPA 200.7 EPA 200.7 EPA 200.7 EPA 200.7 EPA 200.7 EPA 200.7 SM 4500-HB I hereby certify that I have reviewed and approve these data. ,(NAa�a UJU k) Laboratory Representative 642 Tamco Road, Reidsville, North Carolina 27320 tel.(336)342-4748 fax.(336)342-1522 2 Y Y c o v a O p _ a }•� •v _ � y a CA- a o` ZO CL a E v 0 0� 3 o n �. _ o Lo in 3 o M �> I � M � c � � 3 ~ ti n- N nn Y 00 O N x cn a o X _ U Q, ' O Q iF z iQ Y o n LO N cn J (U -a V) LU Q nae J bp �. O X O O cc@ n LL Q o C Q •� 0 v N T '� N z tr_ .E i LO >- v E° cn �, _- C: ° n. CO N Y w c c z c c % r� V o Q N o f, �-- x z a a ° = t;, z r o -a o z CL m p ra r a m c0 v v v. U S E � z v Cl z=- O O o N m C= O v L o p 'u v M ro - C N � O U F cc Y ~ _ L N a °i E 'o V c U Q Q a u 0 c v � E E E E v E a i } c Q1 r D ) Q aQj ' rtS E m o0 M • N oo w v=i Lr l C 1 C Ln V+ O N ci Q �/ f^' d' t!1 O >, 0- O O Q in a U Q M m s N Q O (0 O i M _ c X u a O p Jo u O f0 u C a E - V p W ,- '� `O cl)W O c� O1 � F, Q rru O m 'ro s (n v W cD > o U LU ° "" 1 o n n i ,- Z E w f0 p * } V) L i- - �- a _O .O m It E -C .L -C U1D v ° ro E � c > ccr O U Of O M t '' -�,• O �' 4- O > U. 61 NLn �, �yi U' ❑. Meritech, Inc. Environmental Laboratory Laboratory Certification No. 165 Contact: Drew Matthews Client: Soil Plus Page 1 Report Date: 5/25/2023 P.O. Box 1396 Project: Dunn WWTP Oxford, NC 27565 Date Sample Rcvd: 5/3/2023 Meritech Work Order # OS032395 Sample: DN050323 Grab 5/3/2023 1311 - TCLP Metals Parameter Results Analysis Date Det. Limit Reg. Limit Method Arsenic <0.100 mg/L 5/10/23 0.100 5.0 EPA 200.7 Barium 0.072 mg/L 5/10/23 0.050 100.0 EPA 200.7 Cadmium <0.020 mg/L 5/10/23 0.020 1.0 EPA 200.7 Chromium <0.050 mg/L 5/10/23 0.050 5.0 EPA 200.7 Lead <0.100 mg/L 5/10/23 0.100 S.0 EPA 200.7 Mercury <0.020 mg/L 5/9/23 0.020 0.2 EPA 245.1 Selenium <0.100 mg/L 5/10/23 0.100 1.0 EPA 200.7 Silver <0.050 mg/L 5/10/23 0.050 5.0 EPA 200.7 TCLP Organics Parameter Results Analysis Date Reporting Limi Method Volatiles 8260 Attached 5/12/23 - 8260 Semi Vol. 8270 Attached 5/23/23 - 8270 Other Tests Parameter Results Analysis Date Reporting Limit Method Cyanide, total 0.252 mg/kg 5/9/23 0.050 mg/kg EPA 335.4 Sulfide <10.0 mg/kg 5/9/23 10.0 mg/kg SM4500S2D Ignitability Will Not Ignite 5/9/23 - EPA 1030 Corrositivity (pH) 6.3 S.U. 5/9/23 1.0 - 14.0 S.U. SM 4500 HB 642 Tamco Road, Reidsville, North Carolina 27320 tel.(336)342-4748 fax.(336)342-1522 Meritech, Inc. Environmental Laboratory Laboratory Certification No. 165 ,i Page 2 Contact. !;;atthews Report Date: 5/25/2023 Client: Soil Plus P.O. Box 1396 Project: Dunn WWTP Oxford, NC 27565 Date Sample Rcvd: 5/3/2023 Meritech Work Order # 05032395 Sample: DN050323 Grab 5/3/2023 1311- TCLP Pesticides & Herbicides Pesticide - SW-846 8081A Parameter Results Analysis Date Det. Limit Reg. Limit Dilution Factor Endrin Attached - - - Chlordane Attached - - - Toxaphene Attached - - - Methoxychlor Attached - - - Heptachlor Attached - - - Lindane Attached - - - Herbicides - SW-846 8151A Parameter 2,4-D 2,4,5-TP (Silvex) Results Analysis Date Det. Limit Reg. Limit Dilution Factor Attached Attached 1 hereby certify that I have reviewed and approve these data. A (AhO� a k2 Laboratory Representative 642 Tamco Road, Reidsville, North Carolina 27320 tel.(336)342-4748 fax.(336)342-1522 3310 Summit Win StSt. . summist ENVIRONMENTAL TECHNOLOGIES, INC Cuyahoga Falls, Ohio 44223 Arralytical Laboratories TEL: (330) 253-8211 FAX (330) 253-4489 Website: http://W-ww.setiek.com Analytical Report (consolidated) WU#: 23050523 Date Reported: 5/19/2023 Lab ID: 23050523-004 Collection Date: 5/3/2023 8:25:00 AM Client Sample ID 050323-95 Matrix: SOLID Analysis Result MDL PQL Qual Units Dilution Batch Date Analyzed TCLP PESTICIDES EPA 8081 B EPA 3510 Analyst: PGP Chlordane, total ND 0.380 25.0 U µg/L 10 64962 5/11/2023 L2:24:00 AM Toxaphene ND 1.60 50.0 U µg/L 10 64962 5/11/2023 12:24:00 AM Endrin ND 0.0634 5.00 U µg/L 10 64962 5/11/2023 12:24:00 AM gamma-BHC ND 0.0429 5.00 U µg/L 10 64962 5/11/2023 12:24:00 AM Heptachlor ND 0.0336 5.00 U µg/L 10 64962 5/11/2023 12:24:00 AM Heptachlor epoxide ND 0.0676 5.00 U µg/L 10 64962 5/11/2023 12:24:00 AM Methoxvchlor ND 0.0509 5.00 U µg/L 10 64962 5/11/2023 12:24:00 AM TCLP HERBICIDES EPA 8321E Analyst: JDB 2,4-D ND 0.500 0.500 U mg/L 50 R 163408 5/9/2023 2:00:00 PM 2,4,5-TP ND 0.500 0.500 U mg/L 50 R163408 5/9/2023 2:00:00 PM Qualifiers: B Analyte detected in the associated Method Blank H Holding times for preparation or analysis exceeded MC Value is below Minimum Compound Limit. ND Not Detected P Second column confirmation exceeds E Value above quantitation range M Manual Integration used to detennine area response N Tentatively identified compounds OG1 PL Permit Limit Page 9 of 18 MERITECH, INC. Alp Environmental Laboratories • Laboratory Certificate #165 Client: Soil Plus Project: Dunn WWTP Client Sample ID: DNO50323 Sample Collection: 05/03/23 Meritech Sample ID: 05032395 1311 - TCLP Organics Volatiles: SW-846 8260 Analysis: 05/ 12/23 Extraction: 05/08/23 Analyst: VWV Report Date: 05/16/23 Parameter Result Units Det. Limit Ree. Limit Dilution Factor Benzene < 0.0100 mg/L 0.0100 0.50 10 Carbon Tetrachloride < 0.0100 mg/L 0.0100 0.50 10 Chlorobenzene < 0.0100 mg/L 0.0100 100 10 Chloroform < 0.0100 mg/L 0.0100 6.0 10 1,2-Dichloroethane < 0.0100 mg/L 0.0100 0.50 10 1,1-Dichloroethene <0.0100 mg/L 0.0100 0.70 10 Methyl Ethyl Ketone <0.100 mg/L 0.100 200 10 Tetrachloroethylene <0.0100 mg/L 0.0100 0.70 10 Trichloroethene < 0.0100 mg/L 0.0100 0.50 10 Vinyl Chloride <0.0200 mg/L 0.020 0.20 10 Semi-Volatiles: SW-846 8270 Analysis: 05/23/23 Extraction: 05/08/23 Analyst: PM Report Date: 05/24/23 Parameter Result Units Det. Limit Rem. Limit Dilution Factor 1,4-Dichlorobenzene <0.100 mg/L 0.100 7.5 10 Hexachlorobenzene <0.100 mg/L 0.100 0.13 10 Hexachloro-1,3-butadiene <0.100 mg/L 0.100 0.5 10 Hexachloroethane <0.100 mg/L 0.100 3.00 10 o-cresol <0.100 mg/L 0.100 200 10 m&p-cresol <0.200 mg/L 0.200 200 10 Total cresols <0.300 mg/L 0.300 200 10 Nitrobenzene <0.100 mg/L 0.100 2.00 10 Pentachlorophenol <0.500 mg/L 0.500 100 10 Pyridine <0.100 mg/L 0.100 5.0 10 2,4,5-Trichlorophenol <0.100 mg/L 0.100 400 10 2,4,6-Trichlorophenol <0.100 mg/L 0.100 2.00 10 2,4-Dinitrotoluene <0.100 mg/L 0.100 0.13 10 I hereby certify that I have reviewed and approve these data. f/ ,g t /, 14"(" Laboratory Representative 642 Tamco Road * Reidsville, NC 27320 (336) 342-4748 * info@meritechlabs.com > a p U a O d _ F- a E E E 0 z � Q � v n to c O� >' � U � MU-) oOOO O U)3 Y : Y E' -0 cm)X IJ t� o N 0-) LLl •� E a t Z n L.L E w a. 0- fO v Cl cam. Lf O O a i w U a -oZi- v O O T 4) \/ 4-J -6 N N -y c i Q CO [I - N Y ELO w E ~ c v o c' U 0 ' a v x O m O v 3 u a v °i v v� — O x _ E V) C w v Q E a � '�O/) _ o N El _ aQ1 N O C oN v t1 0 - E m U O Ur .° ro O z -� U Q Q a o C w c c W E N E O E Q) a ui 7 r1 • oor*T U v J (�Nl �l �i Ln E O W 4� dam' �-{ f0 O O W p O E C ,D_ E 0 O n O r' Ll +-' C: m r9 • fD a o .`�° cn Q O m m Obp <( c x v E (5 a d w J : U V.7 O o j= �n u) ° a LLJ z Q uw O Q E N vi Y O C ^r1 2 U Qx m c O V N a N @ O in `J ai U o u w • F v Y 4- Z L E G * * .. N T T T C N O � w _0 a1 s s > s U (D O Q Q C M o v u ^1 �r$�0 v 0 O E > �yCL �, Q LE_ IDIC1.0'E City of Dunn 2023 Class B Annual Report WQ Permit# WQ0006101 Land Application Field Summary Forms PermitNumber WQ0006101 Facility Name City of Dunn LandOwner Harold Lee Eldridge Operator ANNUAL LAND APPLICATION FIELD SUMMARY FORM Site# CU-34 County Harnett Crop 1 Annual Ryegrass - Hay Field Name 1 SoilSeries Goldsboro Crop 1 Pan 136 Acres Permited 4.80 Soil Abbrevation: GoA Crop 2 Crop 2 Pan Volume Acres Dry Soil Application Total Nitrate- Crop 1 Crop 2 Date Measurement Applied % Solids Used DT/Ac. Tons Source Condition Precip Method P Volatilization Mineralization TKN Ammonia Nitrite PAN PAN Crop 01/10/2023 Gallons 19,500 2.54 4.80 0.43 2.07 Dunn WWTP Moist < 0.5" Surface 17.21 0.50 0.3 44,900 394.00 394.00 12.00 Crop 1 01/11/2023 Gallons 45,500 2.54 4.80 1.00 4.82 Dunn WWTP Moist < 0.5" Surface 40.16 0.50 0.3 44,900 394.00 394.00 28.00 Crop 1 Total Volume Applied 65,000 Total Dry Tons 6.88 Sum Total P 57.37 Total 40.00 Total Reported in Gallons Arsenic Cadmium Copper Chromium Lead Mercury Molybdenum Nickel Selenium Zinc Crop 1 Crop 2 PAN PAN Current Year 0.011 0.004 0.772 0.086 0.001 0.023 0.041 0.006 1.661 (lbs./Ac.) (lbs./Ac.) Lime (T/Ac.) Date Prior Year 0.441 0.107 12.633 1.837 1.818 0.067 0.463 1.017 0.386 23.119 Cumulative Total 0.452 0.112 13.404 1.903 0.069 0.486 1.058 0.392 24.780 N/A Permitted CPLR 36 34 1338 267 15 374 89 2498 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, S�4L Jou **Volatilization Rate: Surface - 0.5, Injection/Incorporation -1.0 aerobically digested -0.3, raw sludge -0.4 1/23/2024 ****C.P.L.R.: Cumulative Pollutant Loading Rate Signature of Land Applier Date ANNUAL LAND APPLICATION FIELD SUMMARY FORM PermitNumber WQ0006101 Site# CU-34 County Harnett Crop 1 Annual Ryegrass - Hay Facility Name City of Dunn Field Name 2 SoilSeries Goldsboro Crop 1 Pan 136 LandOwner Harold Lee Eldridge Acres Permited 4.00 Soil Abbrevation: GoA Crop 2 Operator Crop 2 Pan Volume Acres Dry Date Measurement Applied % Solids Used DT/Ac. Tons 01/12/2023 Gallons 58,500 2.54 4.00 1.55 6.20 Source Dunn WWTP Soil Application Condition Precip Method Moist < 0.51, Surface Total P 61.96 Nitrate- Crop 1 Volatilization Mineralization TKN Ammonia Nitrite PAN 0.50 0.3 44,900 394.00 394.00 43.20 Crop 2 PAN Crop Crop 1 Total Volume Applied 58,500 Total Dry Tons 6.20 Sum Total P 61.96 Total 43.20 Total Reported in Gallons Arsenic Cadmium Copper Chromium Lead Mercury Molybdenum Nickel Selenium Zinc Crop 1 Crop 2 PAN PAN Current Year 0.012 0.005 0.833 0.093 0.001 0.025 0.044 0.006 1.794 (lbs./Ac.) (lbs./Ac.) Lime (T/Ac.) Date Prior Year 0.426 0.101 11.232 1.588 1.618 0.061 0.414 0.870 0.379 20.738 Cumulative Total 0.438 0.106 12.065 1.711 0.062 0.439 0.914 0.385 22.531 N/A Permitted CPLR 36 34 1338 267 15 374 89 2498 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, **Volatilization Rate: Surface - 0.5, Injection/Incorporation -1.0 aerobically digested -0.3, raw sludge -0.4 1 /23/2024 ****C.P.L.R.: Cumulative Pollutant Loading Rate Signature of Land Applier Date ANNUAL LAND APPLICATION FIELD SUMMARY FORM PermitNumber WQ0006101 Site# CU-34 County Harnett Crop 1 Annual Ryegrass - Hay Facility Name City of Dunn Field Name 3 SoilSeries Goldsboro Crop 1 Pan 136 LandOwner Harold Lee Eldridge Acres Permited 4.30 Soil Abbrevation: GoA Crop 2 Operator Crop 2 Pan Volume Acres Dry Date Measurement Applied % Solids Used DT/Ac. Tons 01/10/2023 Gallons 58,500 2.54 4.30 1.44 6.20 Source Dunn WWTP Soil Application Condition Precip Method Moist < 0.51, Surface Total P 57.64 Nitrate- Crop 1 Volatilization Mineralization TKN Ammonia Nitrite PAN 0.50 0.3 44,900 394.00 394.00 40.18 Crop 2 PAN Crop Crop 1 Total Volume Applied 58,500 Total Dry Tons 6.20 Sum Total P 57.64 Total 40.18 Total Reported in Gallons Arsenic Cadmium Copper Chromium Lead Mercury Molybdenum Nickel Selenium Zinc Crop 1 Crop 2 PAN PAN Current Year 0.011 0.004 0.775 0.086 0.001 0.023 0.041 0.006 1.669 (lbs./Ac.) (lbs./Ac.) Lime (T/Ac.) Date Prior Year 0.474 0.111 12.760 1.939 1.846 0.069 0.485 1.116 0.396 23.371 Cumulative Total 0.485 0.116 13.535 1.932 0.071 0.508 1.157 0.402 25.040 N/A Permitted CPLR 36 34 1338 267 15 374 89 2498 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, **Volatilization Rate: Surface - 0.5, Injection/Incorporation -1.0 aerobically digested -0.3, raw sludge -0.4 1 /23/2024 ****C.P.L.R.: Cumulative Pollutant Loading Rate Signature of Land Applier Date ANNUAL LAND APPLICATION FIELD SUMMARY FORM PermitNumber WQ0006101 Site# CU-34 County Harnett Crop 1 Annual Ryegrass - Hay Facility Name City of Dunn Field Name 4 SoilSeries Norfolk Crop 1 Pan 123 LandOwner Harold Lee Eldridge Acres Permited 6.20 Soil Abbrevation: NoB Crop 2 Operator Crop 2 Pan Volume Acres Dry Date Measurement Applied % Solids Used DT/Ac. Tons 01/09/2023 Gallons 71,500 2.54 6.20 1.22 7.57 Source Dunn WWTP Soil Application Condition Precip Method Moist < 0.51, Surface Total P 48.86 Nitrate- Crop 1 Volatilization Mineralization TKN Ammonia Nitrite PAN 0.50 0.3 44,900 394.00 394.00 34.06 Crop 2 PAN Crop Crop 1 Total Volume Applied 71,500 Total Dry Tons 7.57 Sum Total P 48.86 Total 34.06 Total Reported in Gallons Arsenic Cadmium Copper Chromium Lead Mercury Molybdenum Nickel Selenium Zinc Crop 1 Crop 2 PAN PAN Current Year 0.009 0.004 0.657 0.073 0.001 0.020 0.035 0.005 1.414 (lbs./Ac.) (lbs./Ac.) Lime (T/Ac.) Date Prior Year 0.532 0.121 13.746 2.065 2.099 0.069 0.516 1.209 0.418 25.741 Cumulative Total 0.541 0.125 14.403 2.172 0.070 0.536 1.244 0.422 27.156 N/A Permitted CPLR 36 34 1338 267 15 374 89 2498 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, **Volatilization Rate: Surface - 0.5, Injection/Incorporation -1.0 aerobically digested -0.3, raw sludge -0.4 1 /23/2024 ****C.P.L.R.: Cumulative Pollutant Loading Rate Signature of Land Applier Date ANNUAL LAND APPLICATION FIELD SUMMARY FORM PermitNumber WQ0006101 Site# HA-08 County Harnett Crop 1 Common Bermudagrass Hay Facility Name City of Dunn Field Name 8 SoilSeries Norfolk Crop 1 Pan 225 LandOwner R. Harold Dixon Acres Permited 18.30 Soil Abbrevation: NoB Crop 2 Operator Crop 2 Pan Volume Acres Dry Soil Application Total Nitrate- Crop 1 Crop 2 Date Measurement Applied % Solids Used DT/Ac. Tons Source Condition Precip Method P Volatilization Mineralization TKN Ammonia Nitrite PAN PAN Crop 05/15/2023 Gallons 110,500 2.54 18.30 0.64 11.70 Dunn WWTP Dry < 0.5" Surface 25.58 0.50 0.3 44,900 394.00 394.00 17.83 Crop 1 05/16/2023 Gallons 84,500 2.54 18.30 0.49 8.95 Dunn WWTP Dry < 0.5" Surface 19.56 0.50 0.3 44,900 394.00 394.00 13.64 Crop 1 05/17/2023 Gallons 130,000 2.54 18.30 0.75 13.77 Dunn WWTP Dry < 0.5" Surface 30.10 0.50 0.3 44,900 394.00 394.00 20.98 Crop 1 05/18/2023 Gallons 19,500 2.54 18.30 0.11 2.07 Dunn WWTP Dry < 0.5" Surface 4.51 0.50 0.3 44,900 394.00 394.00 3.15 Crop 1 07/05/2023 Gallons 19,500 2.54 18.30 0.11 2.07 Dunn WWTP Dry < 0.5" Surface 4.51 0.50 0.3 44,900 394.00 394.00 3.15 Crop 1 07/07/2023 Gallons 19,500 2.54 18.30 0.11 2.07 Dunn WWTP Dry < 0.5" Surface 4.51 0.50 0.3 44,900 394.00 394.00 3.15 Crop 1 07/11/2023 Gallons 19,500 2.54 18.30 0.11 2.07 Dunn WWTP Dry < 0.5" Surface 4.51 0.50 0.3 44,900 394.00 394.00 3.15 Crop 1 07/12/2023 Gallons 32,500 2.54 18.30 0.19 3.44 Dunn WWTP Dry < 0.5" Surface 7.52 0.50 0.3 44,900 394.00 394.00 5.25 Crop 1 07/13/2023 Gallons 32,500 2.54 18.30 0.19 3.44 Dunn WWTP Dry < 0.5" Surface 7.52 0.50 0.3 44,900 394.00 394.00 5.25 Crop 1 07/27/2023 Gallons 45,500 2.54 18.30 0.26 4.82 Dunn WWTP Dry < 0.5" Surface 10.53 0.50 0.3 44,900 394.00 394.00 7.34 Crop 1 07/31/2023 Gallons 97,500 2.54 18.30 0.56 10.33 Dunn WWTP Dry < 0.5" Surface 22.57 0.50 0.3 44,900 394.00 394.00 15.74 Crop 1 Total Volume Applied 611,000 Total Dry Tons 64.72 Sum Total P 141.46 Total 98.61 Total Reported in Gallons Arsenic Cadmium Copper Chromium Lead Mercury Molybdenum Nickel Selenium Zinc Crop 1 Crop 2 PAN PAN Current Year 0.027 0.011 1.903 0.211 0.003 0.057 0.101 0.014 4.095 (lbs./Ac.) (lbs./Ac.) Lime (T/Ac.) Date Prior Year 0.384 0.252 21.060 2.762 2.129 0.074 0.871 2.246 0.346 53.271 Cumulative Total 0.411 0.263 22.962 2.341 0.077 0.928 2.348 0.360 57.366 N/A Permitted CPLR 36 34 1338 267 15 374 89 2498 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, JaU4 **Volatilization Rate: Surface - 0.5, Injection/Incorporation -1.0 aerobically digested -0.3, raw sludge -0.4 S�4L 1 /23/2024 ****C.P.L.R: Cumulative Pollutant Loading Rate Signature of Land Applier Date ANNUAL LAND APPLICATION FIELD SUMMARY FORM PermitNumber WQ0006101 Site# HA-08 County Harnett Crop 1 Common Bermudagrass Hay Facility Name City of Dunn Field Name 9 SoilSeries Norfolk Crop 1 Pan 225 LandOwner R. Harold Dixon Acres Permited 19.70 Soil Abbrevation: NoB Crop 2 Operator Crop 2 Pan Volume Acres Dry Soil Application Total Nitrate- Crop 1 Crop 2 Date Measurement Applied % Solids Used DT/Ac. Tons Source Condition Precip Method P Volatilization Mineralization TKN Ammonia Nitrite PAN PAN Crop 04/26/2023 Gallons 13,000 2.54 19.70 0.07 1.38 Dunn WWTP Dry < 0.5" Surface 2.80 0.50 0.3 44,900 394.00 394.00 1.95 Crop 1 05/02/2023 Gallons 26,000 2.54 19.70 0.14 2.75 Dunn WWTP Dry < 0.5" Surface 5.59 0.50 0.3 44,900 394.00 394.00 3.90 Crop 1 05/03/2023 Gallons 52,000 2.54 19.70 0.28 5.51 Dunn WWTP Dry < 0.5" Surface 11.18 0.50 0.3 44,900 394.00 394.00 7.80 Crop 1 05/04/2023 Gallons 39,000 2.54 19.70 0.21 4.13 Dunn WWTP Dry < 0.5" Surface 8.39 0.50 0.3 44,900 394.00 394.00 5.85 Crop 1 05/05/2023 Gallons 39,000 2.54 19.70 0.21 4.13 Dunn WWTP Dry < 0.5" Surface 8.39 0.50 0.3 44,900 394.00 394.00 5.85 Crop 1 05/08/2023 Gallons 39,000 2.54 19.70 0.21 4.13 Dunn WWTP Dry < 0.5" Surface 8.39 0.50 0.3 44,900 394.00 394.00 5.85 Crop 1 05/09/2023 Gallons 32,500 2.54 19.70 0.17 3.44 Dunn WWTP Dry < 0.5" Surface 6.99 0.50 0.3 44,900 394.00 394.00 4.87 Crop 1 05/10/2023 Gallons 26,000 2.54 19.70 0.14 2.75 Dunn WWTP Dry < 0.5" Surface 5.59 0.50 0.3 44,900 394.00 394.00 3.90 Crop 1 05/11/2023 Gallons 39,000 2.54 19.70 0.21 4.13 Dunn WWTP Dry < 0.5" Surface 8.39 0.50 0.3 44,900 394.00 394.00 5.85 Crop 1 05/12/2023 Gallons 84,500 2.54 19.70 0.45 8.95 Dunn WWTP Dry < 0.5" Surface 18.17 0.50 0.3 44,900 394.00 394.00 12.67 Crop 1 07/18/2023 Gallons 19,500 2.54 19.70 0.10 2.07 Dunn WWTP Dry < 0.5" Surface 4.19 0.50 0.3 44,900 394.00 394.00 2.92 Crop 1 07/19/2023 Gallons 32,500 2.54 19.70 0.17 3.44 Dunn WWTP Dry < 0.5" Surface 6.99 0.50 0.3 44,900 394.00 394.00 4.87 Crop 1 07/25/2023 Gallons 39,000 2.54 19.70 0.21 4.13 Dunn WWTP Dry < 0.5" Surface 8.39 0.50 0.3 44,900 394.00 394.00 5.85 Crop 1 07/26/2023 Gallons 52,000 2.54 19.70 0.28 5.51 Dunn WWTP Dry < 0.5" Surface 11.18 0.50 0.3 44,900 394.00 394.00 7.80 Crop 1 08/01/2023 Gallons 58,500 2.54 19.70 0.31 6.20 Dunn WWTP Dry < 0.5" Surface 12.58 0.50 0.3 44,900 394.00 394.00 8.77 Crop 1 Total Volume Applied 591,500 Total Dry Tons 62.65 Sum Total P 127.21 Total 88.68 Total Reported in Gallons Arsenic Cadmium Copper Chromium Lead Mercury Molybdenum Nickel Selenium Zinc Crop 1 Crop 2 PAN PAN Current Year 0.024 0.010 1.711 0.190 0.003 0.051 0.091 0.013 3.683 (lbs./Ac.) (lbs./Ac.) Lime (T/Ac.) Date Prior Year 0.309 0.177 16.534 2.115 1.867 0.057 0.663 1.771 0.280 40.049 Cumulative Total 0.333 0.187 18.245 2.057 0.060 0.714 1.862 0.293 43.732 N/A Permitted CPLR 36 34 1338 267 15 374 89 2498 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, 'n **Volatilization Rate: Surface - 0.5, Injection/Incorporation -1.0 aerobically digested -0.3, raw sludge -0.4 +� 1 /23/2024 ****C.P.L.R.: Cumulative Pollutant Loading Rate Signature of Land Applier Date City of Dunn 2023 Class B Annual Report WQ Permit# WQ0006101 Pathogen & Vector Attraction Reduction Form Dunn WWTP Fecal Coliform Data 38% Volatile Solids Reduction ANNU.M.., PATHOGEN .AND VECTOR ATTRACTION .REDUCTION FORM (02T Rules) Facility Nance: City of Dunn WQ Permit Nutnber: WQ0006101 WWTP.Nsunc: Dunn WWTP NPDESNu.mbe.r. NCO043176 MonitoringPeriod: 01 /01 /2023 to 12/31 /2023 Pathogen .Reduction (15A NCAC 02T .1106) - Please Indicate level achieved and alternative performed: r "Class A" Alternative: Not Applicable If applicable to alternative performed ("Class A" only) indicate "Process to Further Reduce Pathogens": Not Applicable "Class B" Alternative: Alternative 1 If applicable to alternative performed ("Class B" only) indicate "Process to Further Reduce Pathogens": Not Applicable Fecal Coliform CFU Minimum Geo. Mean Maximum # of Exceedences Frequency Sample Type (Dry Weight) 5,530 7,322 8,462 0 Annually Grab Samples Technique SM 9222 D Vector Attraction Reduction Performed (15A NCAC 02T .1107): Alt. 1 (VS reduction) "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have been met." "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explatiation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Donne Dukes, ORC Jason Smith, VP Preparer Nance and Title (type or print) Land Applier Name and Title (if applicable)(type or print) 2/8/24 Signature of Preparer* Dace Signature of Land Applier (if applicable) Date ;s *Preparer is defined in 40 CPR Part 503.9(r) and 15A NCAC 2T .1102 (26) M Meritech, Inc. Environmental Laboratory Laboratory Certification No. 165 Page 1 Contact: Drew Matthews Report Date: 5/12/2023 Client: Soil Plus P.O. Box 1396 Project: Dunn WWTP Oxford, NC 27565 Date Sample Rcvd: 5/3/2023 Meritech Work Order # 05032387 Sample: DNO50323 (001) Grab 5/3/23 Parameters Results Analysis Date Reporting Limit Method % Total Solids 2.60 % 5/4/23 0-100 % SM 2540B Fecal Coliform (Sludge) 8,462 CFU/g dry wt 5/3/23 130 CFU/g dry wt SM 9222D Meritech Work Order # 05032388 Parameters Sample: DNO50323 (002) Grab Results Analysis Date 5/3/23 Reporting Limit Method % Total Solids 2.63 % 5/4/23 0-100 % SM 2540B Fecal Coliform (Sludge) 7,605 CFU/g dry wt 5/3/23 130 CFU/g dry wt SM 9222D Meritech Work Order # 05032389 Sample: DN050323 (003) Grab 5/3/23 Parameters Results Analysis Date Reporting Limit Method % Total Solids 2.63 % 5/4/23 0-100 % SM 2540B Fecal Coliform (Sludge) 5,530 CFU/g dry wt 5/3/23 130 CFU/g dry wt SM 9222D Meritech Work Order # 05032390 Sample: DN050323 (004) Grab 5/3/23 Parameters Results Analysis Date Reporting Limit Method % Total Solids 2.59 % 5/4/23 0-100 % SM 2540B Fecal Coliform (Sludge) 7,722 CFU/g dry wt 5/3/23 130 CFU/g dry wt SM 9222D 642 Tamco Road, Reidsville, North Carolina 27320 tel.(336)342-4748 fax.(336)342-1522 Meritech, Inc. Environmental Laboratory Laboratory Certification No. 165 4 Page 2 Contact: Drew Matthews Report Date: 5/12/2023 Client: Soil Plus P.O. Box 1396 Project: Dunn WWTP Oxford, NC 27565 Date Sample Rcvd: 5/3/2023 Meritech Work Order # 05032391 Parameters Sample: DN050323 (005) Grab Results Analysis Date 5/3/23 Reporting Limit Method % Total Solids 2.57 % 5/4/23 0-100 % SM 2540B Fecal Coliform (Sludge) 8,171 CFU/g dry wt 5/3/23 130 CFU/g dry wt SM 9222D Meritech Work Order # 05032392 Parameters Sample: DN050323 (006) Grab Results Analysis Date 5/3/23 Reporting Limit Method % Total Solids 2.62 % 5/4/23 0-100 % SM 2540B Fecal Coliform (Sludge) 6,246 CFU/g dry wt 5/3/23 130 CFU/g dry wt SM 9222D Meritech Work Order # 05032393 Parameters Sample: DN050323 (007) Grab Results Analysis Date 5/3/23 Reporting Limit Method % Total Solids 2.61 % 5/4/23 0-100 % SM 2540B Fecal Coliform (Sludge) 8,046 CFU/g dry wt 5/3/23 130 CFU/g dry wt SM 9222D 1 hereby certify that 1 have reviewed and approve these data. (2� Laboratory Representative 642 Tamco Road, Reidsville, North Carolina 27320 tel.(336)342-4748 fax.(336)342-1522 a 0U O a Q CC v, m d S (, a 3t W ro — - - rt = Z a K O v o u �' a E E E O c _ E v0 cti r E O fl u rn LO M O 3 u d \ �- au co (n Lo „ v x- 1 E o o 0 Q LO v u N 0)LU ro (6 H E o Z a w w CL Q: r,• a ,-C37f iz X w fn w (n (n U) d Gii T) -O 'O -6 'n "i7 o C to w 0 (n w 0`o_ - OCL_ _ _ cu (n O O O O 0 Fp- a �. o ♦- I- f- F- CL ai �C ( cc w [ C CC c X G Y \ C c - \. N = co U p T - p O O O O O a U U U U U U o a v U U U U U U Q' 0 Y E LL- LL LL LL LL LL _ _ m n O n OLXO p i " -- o V z m Ln lJ F N0 0O fO V V V V V V V Z V Q Q n- U Oc N ui ai ui = c E E E w E b Q a, ^'1 ^S • W 00 � Nr1i w U c- CD � ~ m ~ �i V1 E W C N N t0 f0 N O E Q o 0 0 0 z O Q O m N u U ¢ Q 1 OC m m o p ` O OfI v m u ('1 bO a a ~ tw rrr Q w � 'Q. � o� v W z ' m N v rMis s el'�'t o E o p z va A v CD O -O m •N N cc U ui > 0u U C ~ � � O N � s c N 0 � _ n v D Z L3 _ C U t0 O O O O O O p E- c C O O O O O O Op U +M M C- M M N1 r6 r5 r6 r6 0 '- > M M c� 'p v w a iA a O O O 4 O O O Ln Qs 41 Black River Wastewater Treatment Plant City of Dunn 2023 January 2023 Vector Attraction Rec.—.77 Holding Tank—.66 .77 - .66 = 42 77 - (.77x.66) July 2023 Vector Attraction Rec.--.80 Holding Tank--.68 .80 - .68 = 46.9% City of Dunn 2023 Class B Annual Report WQ Permit# WQ0006101 Soil Samples Page 1 of 1 Report No: 23-354-0600 Account No: 04596 Advisor: Soil Plus, LLC Joyce Barrette P.O. Box 1396 Oxford NC 27565 Waypointo ANALYTICAL Client: GRANVILLE FARMS INC 2850 Daisy Lane, Wilson, NC 27896 Main 252-206-1721 ° Fax 252-206-9973 www.waypointanalytical.com Farm: CU-34 Date Received: 12/20/2023 Date of Report: 12/21/2023 Lab No Field ID Sample ID Soil Class HM% W/V pH Ac P-1 K-1 S-1 Mn-I Mn-All Mn-Al2 Zn-1 Zn-AI Cu-1 CEC BS % Ca % Mg % ESP Na 19817 1 MIN 0.9 6.0 1.4 187 24 48 44 43 0 245 245 190 6.3 78 53 22 1.5 0.1 Crop Recommendations: 1- Bermudagrass Hay Rec Uom lb/acre Lime (t/acre) 0.5 N 200 P2 05 0 K2 0 178 S 0 Mn 0 Zn 0 Cu 0 B Mg 0 Last Crop 19818 2 MIN 0.1 6.2 1.0 221 31 48 63 52 0 268 268 160 5.8 82 53 24 1.3 0.1 Crop Recommendations: 1- Bermudagrass Hay Rec Uom lb/acre Lime (Vacre) 0.0 N 200 P2 OS 0 K2 0 159 S 0 Mn 0 Zn 0 Cu 0 B Mg 0 Last Crop 19819 3 MIN 0.8 6.1 1.2 187 34 44 44 42 0 200 200 165 5.5 78 51 23 1.4 0.1 Crop Recommendations: 1- Bermudagrass Hay Rec Uom lb/acre Lime (t/acre) 0.5 N 200 P2 05 0 K2 0 151 S 0 Mn 0 Zn 0 Cu 0 B Mg 0 Last Crop 19820 4 MIN 0.3 6.1 1.0 234 32 50 56 49 0 205 205 210 4.9 77 49 24 1.4 0.1 Crop Recommendations: 1- Bermudagrass Hay Rec Uom lb/acre Lime (Vacre) 0.5 N 200 P2 OS 0 K2 0 156 S 0 Mn 0 Zn 0 Cu 0 B Mg 0 Last Crop 19821 5 MIN 0.9 6.4 1.0 198 18 33 56 44 0 240 240 200 6.5 85 55 28 1.1 0.1 Crop Recommendations: 1- Bermudagrass Hay Rec Uom lb/acre Lime (Vacre) 0.0 N 200 P2 05 0 K2 0 195 S 0 Mn 0 Zn 0 Cu 0 B Mg 0 Last Crop Comment: Test result units = CEC and Na in meq/100cm3; NO3 N in mg/dm3; WN in g/cm3 North Carolina Division of Water Quality Certification #257, Analysis and fertility recommendations shown on this report are performed in accordance within NCDA guidelines, Analysis prepared by: Waypoint Analytical Carolina, Inc. Page 1 of 1 Report No: 23-354-0591 Account No: 04596 Advisor: Soil Plus, LLC Joyce Barrette P.O. Box 1396 Oxford NC 27565 Waypoint ANALYTICAL Client: GRANVILLE FARMS INC 2850 Daisy Lane, Wilson, NC 27896 Main 252-206-1721 0 Fax 252-206-9973 www.waypointanalytical.com Farm: HA-08 Date Received: 12/20/2023 Date of Report: 12/21/2023 Lab No Field ID Sample ID Soil Class HM% W/V pH Ac P-1 K-1 S-1 Mn-I Mn-All Mn-Al2 Zn-I Zn-AI Cu-1 CEC BS % Ca % Mg % ESP Na 19795 8 MIN 0.2 5.5 1.6 489 15 44 88 77 0 373 373 195 4.7 65 55 7 1.0 0 Crop Recommendations: 1- Bermudagrass Hay Rec Uom lb/acre Lime (t/acre) 0.7 N 200 P2 05 0 K2 0 204 S 0 Mn 0 Zn 0 Cu 0 B Mg 0 Last Crop 19796 9 MIN 0.2 5.7 1.4 477 18 44 81 70 0 393 393 190 4.5 69 57 9 1.6 0.1 Crop Recommendations: 1- Bermudagrass Hay Rec Uom lb/acre Lime (Vacre) 0.5 N 200 P2 OS 0 K2 0 195 S 0 Mn 0 Zn 0 Cu 0 B Mg 0 Last Crop Comment Test result units = CEC and Na in meq/100cm3; NO3 N in mg/dm3; WN in g/cm3 North Carolina Division of Water Quality Certification #257, Analysis and fertility recommendations shown on this report are performed in accordance within NCDA guidelines, Analysis prepared by: Waypoint Analytical Carolina, Inc.