WQ0001953_2023 Residual Annual Report_20240212 (2)

Initial Review
Reviewer
nathaniel.thornburg
Is this submittal an application? (Excluding additional information.) *
Yes No
If not an application what is the submittal type?* Annual Report
Residual Annual Report
Additional Information
Other
Annual Report Year* 2023
Permit Number (IR) * WQ0001953
Applicant/Permittee Town of Spindale
Email Notifications
Does this need review by the hydrogeologist? * Yes No
Regional Office Asheville
CO Reviewer
Admin Reviewer Wanda Gerald

Submittal Form
Project Contact Information
Please provide information on the person to be contacted by NDB Staff regarding electronic submittal, confirmation of receipt, and other correspondence.
Name* Guy O'Connor
Email Address*
[e-mail]
Project Information
.........................
Application/Document Type*
New (Fee Required)
Modification - Major (Fee Required)
Renewal with Major Modification (Fee
Required)
Annual Report
Additional Information
Other
Phone Number*
8282863407
Modification - Minor
Renewal
GW-59, NDMR, NDMLR, NDAR-1,
N DAR-2
Residual Annual Report
Change of Ownership
We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form.
https://edoes.deq.nc.gov/Forms/NonDischarge_Monitoring_Report
Permit Type:*
Wastewater Irrigation
High -Rate Infiltration
Other Wastewater
Reclaimed Water
Closed -Loop Recycle
Residuals
Single -Family Residence Wastewater
Other
Irrigation
Permit Number:*
WQ0001953
Has Current Existing permit number
Applicant/Permittee Address*
327 Ecology Street Spindale NC 28160
Facility Name*
Town of Spindale Class B Residuals Program
Please provide comments/notes on your current submittal below.
At this time, paper copies are no longer required. If you have any questions about what is required, please contact Nathaniel Thornburg
at [e-mail].
Please attach all information required or requested for this submittal to be reviewed here.
(Application Form, Engineering Plans, Specifications, Calculations, Etc.)
2023 land app report.pdf 18.98MB
Upload only 1 PDF document (less than 250 MB). Multiple documents must be combined into one PDF file unless file is larger
than upload limit.
* By checking this box, I acknowledge that I understand the application will not be accepted for pre -review until the fee (if required) has
been received by the Non -Discharge Branch. Application fees must be submitted by check or money order and made payable to the
North Carolina Department of Environmental Quality (NCDEQ). I also confirm that the uploaded document is a single PDF with all parts
of the application in correct order (as specified by the application).
Mail payment to:
NCDEQ — Division of Water Resources
Attn: Non -Discharge Branch
1617 Mail Service Center
Raleigh, NC 27699-1617
Signature
Submission Date 2/12/2024

ANNUAL LAND APPLICATION CERTIFICATION FORM
WQ Permit#: WQ0001953 County:
Facility Name (as shown on permit):
Land Application Operator:
Rutherford
Year: 2023
Town of Spindale
U.S. Biosolids, Inc. Phone: [phone]
Land application of residuals as allowed by the permit occurred during the past calendar year?
® Yes 0 No - If No, skip Part A, and Part B and proceed to Part C. Also, If residuals were
generated but not land applied, please attach an explanation on how the residuals were handled.
Part A - Residuals Application Summarv:
Total number of application fields in thepermit:
6
Total number of fields utilized for land application during the year:
5
Total amount of dry tons applied during the year for all application sites:
162.97
Total number of acres utilizes for land application during the year:
64.4
Part B - Annual Compiance Statement:
Facility was compliant during calendar year 2023 with all conditions of the land application permit
(including but not limited to items 1-13 below) issued by the Division of Water Resources. 0 Yes 0 Na
If no please, provide a written description why the facility was not compliant, the dates, and explain corrective action
taken.
1) Only residuals approved for this permit were applied to the permitted sites.
2) Soil pH was adjusted as specified in the permit and'iime was applied (if needed) to achieve a soil pH of at least 6.0 or the
limit specified in the permit. • .
3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies of
laboratory results are attached.
4) Annual TCLP analysis (if required) was. performed and three (3) copies of certified laboratory results are attached.
5) All other monitoring was performed in accordance -with the permit and reported during the year as required and three (3)
copies of certified laboratory results are attached.
6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T. 1105(a) or the Pollutant Loading
Rates in 15A NCAC 02T .1105(b) (applicable to 40 CFR Part 503 regulated facilities).
7) All general requirements in as specified in the Land ApplicatiodPermit were complied with (applicable to 40 CFR Part
503 regulated facilities).
8) All monitoring and reporting requirements in 15A NCAC 02T .1111 were complied with (applicable to 40 CFR Part 503
regulated facilities).
9) All operations and maintenance requirements in the pen -nit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Resources.
10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
11) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as specified
in the permit.
12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13) All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C - Certification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate,
and complete. I am aware that there are significant penalties for submitting false information, including the possibility
of fines and imprisonment for knowing violations."
Ec o % T IJalp ec - k we,, Motpw5.
Permittee Name and Title (type or print)
2 /9/
Signature of Preparer* Date
(if different from Permittee)
* Preparer is defined in 40 CFR Part 503.9 (r) and 15A NCAC 02T
Signature of Permittee Date
of
1-23-2024
Date
(if different from Permittee and Preparer)
1102 (26) DENR FORM ACF (12/2006)

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ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Town of Spindale Total Dry Tons Applied (Annual):
Permit #: WQ00010953 Cation Exchange Capacity (non 503 only):
Operator: John McFadden Owner: John McFadden Predominant Soil Series:
Acres Used: 15.1 Acres Permitted: 15.1 Site #: M1 Field #:
28.42
PaC2
M1
RPcidnal Annlvcic Data (Fleavv 'Metals and Total Phosnhorus use miA2. % Solids use Raw Percent #):
Sample
or Com-
posite
Date
6/7/23
3..
41
51
6 !
7-;
8
_9
10.
% Solids 1
2.14
Arsenic
23.8
Cadmium
4.76
Copper
729
bromiurr
106
Lead
71.4
Mercury
7.67
Molyb
denum
11.9
Nickel
37.2
Selenium
23.8
Zinc
1830
Total
Phos-
horus
19100
Annual Npavv Metal lipid I.narlinocl('g1vn1atf,(1 in iwC/a(`rt'1:
Total
1
2
j
5
6
7
8
9
10;
1':
12
-
DT/Ac./
_3
_4
..
o
App.
a
Event
1.88
Arsenic.
0.090
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.090
Cadmium
0,018
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.018
Copper
2.744
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
2.744
011-0miun
0.399
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.399
Lead
0.269
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0269
Mercury
0.029
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.029
Molyb-
0.045
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.045
denum
Nickel
0.140
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.140
Selenium
0.090
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.090
Zinc
6.888
0.000
4.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
6.888
Total
" Phos-
71.891
0.000
0.000
0.060
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
71.892
horus
"I eertlty, unaer penalty of taw, tnat tors aoeument was preparea unaer my ulrecuo❑ or supe,-,-Mon Hi accoluance wail a
system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am
aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
C /1 1-23-2024
Signature of Land A plier Date
DENR FORM MFLSF (12/2006)

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ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Town of Spindale Total Dry Tons Applied (Annual):
Permit #: WQ00010953 Cation Exchange Capacity (non 503 only):
Operator: John McFadden Owner: John McFadden Predominant Soil Series:
Acres Used: 15.5 Acres Permitted: 15.5 Site #: M3 Field #:
24.37
PaC2
M3
_ _. . �._V_...t.. r�..... I Ul,..,.,., A4.,+-]1 .-A Tntot Phacnhnrnc iiCP Mo/ku_ n/n Solids use Raw Percent #):
1\C.JIUNL�I
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a
9_
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Sample
.._L...
3._i
4_1
or Com-
posite
Date
6/7/23
% Solids
2.14
Arsenic
23.8
R.
Cadmium
4.76
Copper
729
hrorniurr
106
Lead
71.4
Mercury
7.67
Molyb-
11.9
denum
Nickel
372
Selenium
23.8
Zinc
1830
Total
Phos-
19100
horus
M■/1�lR ESW1 MA ..1r= H
Total
1
2`
3
4
5
6i
7
8�
-
9!
-
10'
11,
-
12?
-
DT/Ac,/
m
App.
Event
1.57
Arsenic
0.075
0.000
0,000
0.000
0.000
0.000
0.000
0.000
0,000
0.000
0.000
0.000
0.075
CadiniLlnl
0.015
0.000
0.000
0.000
0.000
0,000
0.000
0.000
0.000
0.000
0.000
0.000
0.015
Copper
2.292
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
2.292
111-Omint
0.333
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0,000
0.000
0.000
0.000
0.333
Lead
0.224
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.224
Mercury
0.024
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.024
Motyb-
0.037
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.037
denum
Nickel
0.117
0.000
0.000
0.000
0,000
0.000
1 0.000
0.000
0.000
0.000
0.000
0.000
0.117
Selenium
0.075
1 0.000
0,000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.075
Zinc
5.754
1 0.000
0,000
0.000
1 0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
5.754
Total
- Phos-
60.050f
0.000
0.000
0.000
0,000
0,000
0.000
0.000
0.000
0,000
0.000
0.000
60.050
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aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
�&4 /lam 1-23-2024
Signature of Land Appli r Date
DENR FORM MFLSF (12/2006)

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ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
Town of Spindale Total Dry Tons Applied (Annual):
WQ00010953 Cation Exchange Capacity (non 503 only):
John McFadden Owner: John McFadden Predominant Soil Series:
Field #:
17.1 Acres Permitted:
17.1 Site #:
M4
57.40
PaC2
M4
Rocirinal Annlvsis data (Neavv Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Anneal Heavy Metal Field loadings (Calculated in lbs/acre):
Total
1
2
3 1
4
_5
6`
7
8
9`
10
11
12
DT/Ac./
a:
App.
Event
3.36
Arsenic
0.160
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.160
Cadmium
0.032
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0,000
0.000
0.032
Copper
4.895
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
4.895
hromiui
0.712
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.712
Lead
0.479
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.479
Mercury
0.051
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.051
Molyb-
0.080
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.080
denum
Nickel
0.250
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.250
Selenium
0.160
0.000
0M00
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.160
Zinc
12.287
0.000
Q000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
12.287
Total
,
Phos-
128.231
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a
system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am
aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Signature of Land A plier
1-23-2024
Date
DENR FORM MFLSF (12/2006)

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ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
Town of Spindale Total Dry Tons Applied (Annual):
WQ00010953 Cation Exchange Capacity (non 503 only):
John McFadden Owner: John McFadden Predominant Soil Series:
10.6 Acres Permitted:
10.6 Site #:
M5 Field #:
46.40
CaB2
M5
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, `% Solids use Raw Percent #):
Sample
or Com-
posite
Date
_.?....
6/7/23
.2. !
3_
41
5I
6_
7
$
Solids
2.14
-
Arsenic
23.8
Cadmium
4.76
Copper
729
Chromiurr
106
Lead
71.4
Mercury
7.67
Molyb-
denum
11.9
Nickel
37.2
Selenium
23.8
Zinc
1830
Total
Phos-
horus
19100
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
1
2
3
4
5j
6j
71
8,
9
10 !
11
12 )
DT/Ac./
-
-
c
App.
Event
4.38
Arsenic
0.208
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.208
Cadmium
0,042
0.000
0.000
0-000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.042
Copper
6,382
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
6.382
hromiun
0.928
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.928
Lead
1 0.625
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.625
Mercury
0.067
0.000
0.000
0.000
0.000
0.000
1 0.000
0.000
0.000
1 0.000
0.000
1 0.000
0.067
Molyb-
den um
0.104
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.104
Nickel
0.326
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.326
Selenium
0.208
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.208
Zinc
16.020
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
16.020
Total
"Phos-
167.201
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
######
horus
"t certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a
system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am
aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
.. k�� n�� -_
Signature of Land Applier
1-23-2024
Date
DENR FORM MFLSF (12/2006)

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ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
Town of Spindale Total Dry Tons Applied (Annual):
WQ00010953 Cation Exchange Capacity (non 503 only):
John McFadden Owner: John McFadden Predominant Soil Series
6.1 Acres Permitted: 6.1 Site #: M6 Field #:
6.38
CaB2
M6
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample
IIIor Com-
posite
DateTotal
BUM
Phos-
Annual Heavy Metal Field Loadings (Calculated in Ibs/acre):
Total
111
2
3
4
51
6
7
8
9
10
11
12
DT/Ac./
o
App.
Event
1.05
Arsenic
0.050
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.050
Cadmium
0.010
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.010
Copper
1.525
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1.525
Chromiurn
0.222
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.222
Lead
0.149
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1 0.000
0.000
0.000
0.000
0.149
Mercury
0.016
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.016
Molyb-
0.025
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.025
denum
Nickel
0.078
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.078
Selenium
0.050
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.050
Zinc
3.828
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
3.828
Total
,
Phos-
39.957
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
39.957
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a
system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am
aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
-4 />
Signature of Land A plicr
1-23-2024
Date
DENR FORM MFLSF (12/2006)

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ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Town of Spindale
WWTP Name: Town of Spindale WWTP
Monitoring Period: From 1/1/2023 To
WQ Permit Number: WQ0001953
NPDES Number: NCO020664
12-31-20232
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. A (time/temp) ❑ I
Alt B (Alk Treatment) ❑
Alt. C (Prior Testing)❑
Alt.D (No Prior Test) ❑
Process to Further Reduce Pathogengs ❑
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost 01
Heat Drying ❑
Heat Treatment ❑
Thermophilic ❑
Beta Ray ❑
Gamma Ray ❑
Pasteurization ❑
Class B:
I Alt. (1) Fecal Density R1
Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Paii(iogens":
Lime Stabilization ❑
1 Air Drying ❑
Composting ❑
Aerobic Digestion ❑
Anaerobic Digestion ❑
If applicable to alternative performed (Class A or Class B) complete the following monitoring data:
Parameter
Allowable Level
in Sludge
Pathogen Density
Number of
Fxcee-
ences
Frequency
of Analysis
Sample
Type
Analytical
Tech-
moue
inimu
Geo. Mean
aximu
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
45709
64932
-
87437
MPN/g
0
7
grab
sm9221
CFU
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per 4 grams
total solid (dry
I weight)
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed:
Alt.1 (VS reduction) ❑
Alt. 2 (40-day bench) ❑
Alt. 3 (30-day bench) ®
Alt. 4 (Spec. Oz uptake) ❑
Alt. 5 (14-Day Aerobic) ❑
Alt. 6 (Alk. Stabilization ❑
Alt 7 (Drying - Stable) ❑Alt.
8 (Drying - Unstable) ❑
Alt. 9 (Injection) ❑
Alt. 10 (Incorporation) ❑
No vector attraction reduction alternatives were performed ❑
CERTIFICATION STATEMENT (please check the appropriate statement)
® "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
❑ "1 certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note
if you check this statement attach an explanation why ,you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Preparer Name and Title (type or print)
Signature of Preparer*
Date
Zach Key U.S. Biosolids, Inc.
Land Applier Name and Title (if applicable)(type or print)
24 X 1-23-2024
Signature of Land Ap ter (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 02T (12/2006)

(2)
WayPAoi nt .
NALYTICAL
6/21 /2023
US Biosolids Inc
Dennis Key
958 Hoots Road
Roaring River, NC, 28669
Ref: Analytical Testing
Report Number: 23-159-0008
Project Description: Spindale
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° fax [phone]
www.waypointanalytical.com
Dear Dennis Key:
Waypoint Analytical Virginia, Inc. received sample(s) on 6/8/2023 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Anaiysis(s).,Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Brandi Watson
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 1 of 7

Wav 0 ,•
POI.,
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743.9401 ° Fax [phone]
wwmwaypointanalyti cal. com
Sample Summary Table
Report Number: 23-159-0008
Client Project Description: Spindale
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
62192
Spindale
Solids
06/07/2023 10:35
06/08/2023
62192
Spindale
Solids
06/07/2023 10:35
06/08/2023
rt.
SM-4500-NH3C
WP MTN
62192
Spindale
Solids
06/07/2023 10:35
06/08/2023
9045D
WP MTN
62192
Spindale
Solids
06/07/2023 10:35
06/08/2023
4500NO3F-2011
WP MTN
62192
Spindale
Solids
06/07/2023 10:35
06/08/2023
6010D
WP MTN
62192
Spindale
Solids
06/07/2023 10:35
06/08/2023
SW-74716
WP MTN
62192
Spindale
Solids
06/07/2023 10:35
06/08/2023
SM-4500-NH3C-TKN
WP MTN
62192
Spindale
Solids
06/07/2023 10:35
06/08/2023
SM-2540G
WP MTN
WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN
Page 2 of 7

Waypoint.
7621 Whitepine Road, Richmond,
VA 23237
Main 904-743-9401 ° Fax [phone]"6
ANALYTICAL
www.waypointanstocal.com
46381
US Biosolids Inc
Project
Spindale
Dennis Key
Report Date : 06/21/2023
958 Hoots Road
Information :
Received : 06/08/2023
Roaring River , NC 28669
Brandi Watson
Report Number: 23-159-0008
REPORTOFANALYSIS
Lab No : 62192
Matrix: Solids
Sample ID : Spindale
Sampled: 6/7/2023 10:35
Test
Results
Units
MOL
DF
Date / Time
By
Analytical
Analyzed
Method
Moisture
97.9
%
0.010
1
06/14/2317:55
TKM
SM-2540G
Potassium
4600
mg/Kg - dry
476
1
06/12/23 19:44
JTR
6010D
Sulfur
14800
mg/Kg - dry
476
1
06/12/23 19:44
JTR
6010D
Calcium
18100
mg/Kg - dry
2380
1
06/12/23 19:44
JTR
6010D
Magnesium
3800
mg/Kg - dry
238
1
06/12/23 19:44
JTR
6010D
Sodium
10400
mg/Kg - dry
1190
1
06/12/23 19:44
JTR
6010D
Iron
25300
mg/Kg - dry
476
1
06/12/23 19:44
JTR
6010D
Aluminum
30900
mg/Kg - dry
238
1
06/12/23 19:44
TJS
6010D
Manganese
557
mg/Kg - dry
23.8
1
06/12/23 19:44
JTR
6010D
Copper
729
mg/Kg - dry
23.8
1
06/12/23 19:44
JTR
6010D
Zinc
1830
mg/Kg - dry
59.5
1
06/12/23 19:44
JTR
6010D
Cadmium
<4.76
mg/Kg - dry
4.76
1
06/12/23 19:44
JTR
6010D
Chromium
106
mg/Kg - dry
11.9
1
06/12/23 19:44
JTR
6010D
Nickel
37.2
mg/Kg - dry
11.9
1
06/12/23 19:44
JTR
6010D
Lead
71.4
mg/Kg - dry
14.3
1
06/12/23 19:44
JTR
6010D
Arsenic
<23.8
mg/Kg - dry
23.8
1
06/12/23 19:44
JTR
6010D
Mercury
<7.67
mg/Kg - dry
7.67
1
06/12/23 11:29
FDS
SW-7471B
Selenium
<23.8
mg/Kg - dry
23.8
1
06/12/23 19:44
JTR
6010D
Molybdenum
<11.9
mg/Kg - dry
11.9
1
06/12/23 19:44
JTR
6010D
Qualifiers/ DF Dilution Factor
MQL Method Quantitation
Limit
Definitions
Page 3 of 7

Waypointo
ANALYTICAL
46381
US Biosolids Inc Project Spindale
Dennis Key
958 Hoots Road Information
Roaring River , NC 28669
Report Number : 23-159-0008 REPORTOFA
Lab No : 62192
Sample ID : Spindale
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytiCal.cam
Report Date : 06/21/2023
Received : 06/08/2023
Brandi Watson
NA YSIS
Matrix:: Solids
Sampled: 6/ 7/ 2023 10:35
Test
Results
Units
MQL
DF
Date / Time
Analyzed
By
Analytical
Method
Ammonia Nitrogen
10900
mg/Kg - dry
4760
1
06/21/23 07:00
JPJ
SM-4500-NH3C
Nitrate+Nitrite-N
<238
mg/Kg - dry
238
1
06/13/23 15:50
CLP
4500NO3F-2011
Organic N
51520
mg/Kg - dry
11900
1
06/20/23 13:45
CALCULATION
pH
&9
s.u.
1
06/12/2316:00
CNB
9045D
Total Solids
2.14
%
0.010
1
06/14/23 17:55
TKM
SM-2540G
Total Kjeldahl Nitrogen
62400
mg/Kg - dry
11900
1
06/20/23 13:45
JPJ
>M-4500-NH3C-TKP
Phosphorus
19100
mg/Kg - dry
238
1
06/12/23 19:44
JTR
6010D
Qualifiers/ DF Dilution Factor
Definitions
MQL Method Quantitation Limit
Page 4 of 7

Wav 0 (D
POI� .
ANALYTICAL
7621 whitepine Road, Richmond, VA 23237
Main 804-743-9401 Q Fax [phone]
w ww.wa y poi n to n a l yti ca 1. c o m
Client: US Biosolids Inc CASE NARRATIVE
Project: Spindale
Lab Report Number: 23-159-0008
Date: 6/21 /2023
Metals Analysis Method 6010D
Sample 85530
Analyte: Aluminum
QC Batch No: 1-687321 /L686988
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 85530
Analyte: Iron
QC Batch No: L687321/L686988
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 85530
Analyte: Potassium
QC Batch No: 1-687321/1-686988
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 85530
Analyte: Magnesium
QC Batch No: 1-687321 /L686988
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 85530
Analyte: Lead
QC Batch No: 1-687321/1-686988
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Page 5 of 7

(2)
Wayp►�►
7621 Whitepine Road, Richmond, VA 23237
■ S i�
Main 804-743-9401 ° Fax [phone]
ANALYTICAL
www.waypointanalytical.com
Shipment
Receipt Form
Customer Number: 46381
Customer Name: US Biosolids Inc
Report Number: 23-159-0008
Shipping Method
Fed Ex US Postal Lab
Other
• UPS Client Courier
Thermometer ID: -
Shipping container/cooler uncompromised?
• Yes
No
Number of coolers/boxes received
1
Custody seals intact on shipping container/cooler?
Yes
No • Not Present
Custody seals intact on sample bottles?
Yes
No • Not Present
Chain of Custody (COC) present?
• Yes
No
COC agrees with sample label(s)?
• Yes
(`; No
COC properly completed
• Yes
No
Samples in proper containers?
• Yes
( No _
Sample containers intact?
• Yes
% No
Sufficient sample volume for indicated test(s)?
• Yes
') No
All samples received within holding time?
• Yes
No
Cooler temperature in compliance?
• Yes
L. No
Cooler/Samples arrived at the laboratory on ice.
• Yes
No
Samples were considered acceptable as cooling
process had begun.
Water - Sample containers properly preserved
Yes
No N/A
Water - VOA vials free of headspace
Yes
No • N/A
Trip Blanks received with VOAs
Yes
No • N/A
Soil VOA method 5035 — compliance criteria met
Yes
No • N/A
High concentration container (48 hr)
Low concentration EnCore samplers (48 hr)
High concentration pre -weighed (methanol -14 d) Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included?
Yes
No
Comments:
Signature: Brandi Watson Date & Time: 06/08/2023 09:56:16
Page 6 of 7

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Page 7 of 7

AM
R&
PROM PT-AOCU RATE- RELtAMLE
EADOItATORIFS, INC:
WWWYARLAB&C0,4
REPORT OF ANALYSES
Attn: ZACH KEY
U,S. BIOSOLIDS, INC.
Po Box 146
RONDA, NC 28670-
SAMPLE NUMBER- 147351 SAMPLE ID- SPINDALE
DATE SAMPLED- 06/07/23
DATE RECEIVED- 66/07/23 SAMPLER- ZK
TIME RECEIVED- 1235 DELIVERED BY- ZK
Page 1 of I
PROJECT NAME: JUN 23
DATE: 07/1.2/23
ANALYSIS
ANALYSIS METHOD DATE TIME BY
FECAL COLIFORM (GEOM. MEAN) SM 9221 E 06/07/23 1630 RE
LABORATORY DIRECTOR
SAMPLE MATRIX- WW
TIME SAMPLED- 10315
RECEIVED BY- DJ
TYPE SAMPLE- Grab
RESULT UNITS
64,932 MPN/g
0 rpm
22 17 Graham Park Drive - Charlotte, NC 28273
Phone: [phone] - Fax: [phone]

Ask
PAF;Z
EABOR-A'rORI
CLIENT NAME. U.S. BIOSOLIDS
SAMPLE 10, OUT �Zf T
SAMPLE DATE: 011711URM
ANALYSIS.- INIAMOM,
ANALYSIS METHOD: ERIADWSER
2217 Graham Park Drive
PO Box 411483
Charlotte, NC 28241-1483
NC Cert # 20; SC Cert # 99003001
LAB ID #:
147351
Sample #
1
F. Colliform
1,493
T. Solids
2.37%
gram
62,951,68
2
2,003
2.29%
87,437.05
3
2,084
2.45%
85,07542
4
1,374
2.38%
57,830.70
5
1,444
2,24%
64,438.99
6
1,024
214%
45,709,18
7
1,431
1 2,35%
61,006.81,
i
Fecal Coliform
Geometric Mean= •

PpCi M IsT.A Ut+LR •i4KLSAaIil4
LABORATORIES, INC
CHAIN OF CUSTODY
Phone [phone]
Fax [phone]
Shipping It Mailing:
2217 Graham park Drive
Charlotte, NC 28273
R 4s essential that all mfonnaOon he rewfdect on ttus Chain of Custody document for acceptance oy PAR Laboratories, ,nc and the WOO
Carolina Department of Environmental and Natural Resources
Company Name (bititng)
Comments/ Spatial Instructions
_ U.S. Biosolids, Inc.
PO Box 146
City, State & zip code
Ronda, NC 28670
Point of Contact & Telephone Number
Zach Key 336-467-3550
Sample
;?'ti L K
Taken By: SIGNATURE
PRINTED NAME
ARE SAMPLES FOR STATE ch EPA REPORTING? YES NO
`Sample Type: ow __..._.._._....... ww. _ ___ -_ GWMW _._ HW sDil _ oqt
Sample Temp at time of sampling: C Sample Temp upon receipt: _° C
"Field Preserved: Yes No Teflon Liner(Zero Headspace: Yes No nfa
Residual Chlorine checked at time of —sampling {YIN): Dechlorination Necessary (YIN):
atyt�pie i.D
Ssnv% Localtumi ) comp
grab,
Sibi~.tz�t ....
Presewie . oatarriciv
�titir+
Daltlerrkm
I
f +---
e
"erinqumneo Dy Uaw i Mne Y4awiver 4Dy.
A r�l/ K �`1•'�3 JX i Qt*
Relinquished by Daie[Tvme Received by.
vale+ I trrM /
oatentme
' C=Composite G-Grab 0W=0nnking Water WW-Wastewater GWMW=Groundwater Monitonnp Well tiUV Maaarclrws Waste

LABORATORIES, IN-C
WWWYARLAWCOM
REPORT OF ANALYSES
Attn: ZACK KEY
U.S. BIOSOLIDS, INC.
PO BOX 146
RONDA, NC 28670-
PROJECT NAME: JUN 23
DATE: 07/12/23
SAMPLE NUMBER- 147353
SAMPLE ID- SPTNDALE
SAMPLE MATRIX- WW
DATE SAMPLED- 06/07/23
TIME SAMPLED- 1035
DATE RECEIVED- 06/07/23
SAMPLER- ZK
RECEIVED BY- DJ
TIME RECEIVED- 1235
DELIVERED BY--ZK-
TYPE SAMPLE- Grab
Page 1 of 2
ANALYSTS
ANALYSIS
METHOD
DATE
TIME
BY
RESULT
UNITS
TCLP CHARACTERISTICS
TCLP,
06/20/23
1248
CS
pH VALUE
TCLP
06/20/23
1248
CB
7.5
S.U.
CORROSIVITY
TCLP
06/20/23
1248
CB
NON
REACTIVITY
TCLP
06/20/23
1248
CB
NON
FLASH POINT
TCLP
06/20/23
1249
CB
> 200
degrees F
IGNITARTLITY
TCLP
06/,?0/23
1248
Ca
NON
PAINT FILTER TEST
TCLP
06/20/23
1248
CB
FL
TCLP METALS
'CLP
06/15/23
1917
BN
ARSENIC
TCLP
06/15/23
1917
BN
< 0.5
ppm
BARIUM
TCLP
06/15/23
1917
BN
< 10
ppm
CADMIUM
TCLP
06/15/23
1917
BN
< 0.1
ppm
CHROMIUM
TCLP
06/15/23
1917
BN
< 0,5
ppm
LEAD
TCLP
06/15/23
1917
BN
< 0.5
ppm
MERCURY
TCLP
06/15/23
1917
BN
< 0.02
ppm
SELENIUM
TCLP
06/15/23
1917
BN
< 0.1
ppm
SILVER
TCLP
06/15/23
1917
BN
< 0.5
ppm
TCLP PESTICIDES
TCLP
06/16/23
2046
VC
ENDRIN
TCLP
06/16/23
2046
VC
< 0.002
ppm
LINDANE
TCLP
06/16/23
2046
VC
< 0.04
ppro
METHOXYCHLOR
TCLP
06/16/23
2046
VC
< 1
ppm
TOXAPqENE
TCLT-:,
06/16/23
2046
VC
< 0.05
ppm
2217 Graham Park Drive - Charlotte, NC' 28273
Phone: [phone] -.Fax. [phone]

Aft
PA
PRC,MPT,ACCURATE* RELIABLE
LABOPLA'rOPLIESi INC
%"A8,'.PARl.,A8S.00M
Page 2 of 2
CONTINUATION OF DATA FOP,
SAMPLE NUMBER
147353
ANALYSIS
ANALYSIS
METHOD
DATE
TIME
BY
RESULT
UNITS
CHLORDANE
TCLP
06/16/23
2046
VC
< 0.003
ppm
HEPTACHLOR (AND ITS EPDXIDE) TCLP
06/16/23
2046
VC
< 0.0008
PPM
TCLP HERBICIDES
TCLP
-06/19/23
2037
VC
2,4-D
TCLP
06/19/23
2037
VC
< I
ppm
2,4,5-TP(SILVEX)
TCLP-
06,,"19/23
2037
VC
< 0.1
ppm
TCLP ORGANICS
TCTIQ
061109/23
202`J
MS
BENZENE
TCLP
06/09/23
2027
MS
< 0.05
ppm
CARBON TETRACHLORIDE
TCLP
06/09/23
2027
MS
< 0.05
ppm
CHLOROBENZENE
TCLP
CLp
06/091123
2027
MS
< 10
ppm
CHLOROFORM
TCLP
06/09/23
2027
MS
0.6
ppm
o-CRESOL
TCLP
06/09/23
2027
ms
< 20
ppm
p-CRESOL
TCLP
06/09/23
202'7
MS
< 20
ppm
m-CRESOL
TCLP
0()/C9/*,"3
2027
MS
< 20
ppm
1, 4-DTCHLOROBE-P,,!ZENE
TCLP
06/09/23
202'7
MS
< C. .'; 5
ppm
1,2-DICELOROETHANE
TCLP
06/C-9/23
202-1
MS
< 0.05
ppm
l,I-DICHLOROETHYLENE
TCLP
06/09/23
2021
MS
< 0.07
ppm
2,4-DTNITRoTLUENE
TCLP
06/09/23
202-7
MS
< 0.013
ppm
HEXACHLOROBENZENE
TCLP
06/09/23
2027
MS
< 0.01.3
ppm
HEXACHLOROBUTDIENE
TCLP
06/09/23
2027
MS
< 0.0-5
ppm
HEXACHLOROETRANE
TCLP
0C/09/23
202'7
ms
< 0.3
ppm
METHYL ETHYL KETONE
TCLP
06/09/23
2027
MS
< 20
ppm
NITROBENZENE
TCLP
06/09/23
2C27
MS
< 0.2
ppm
PENTACHLOROPHENOL
TCLP
06/09/23
2027
MS
< 110
ppm.
PYRIDINE
TCLP
06/091/23
2027
MS
< 0.5
ppm
TETRACHLORETHYLENE
TCLP
06/09/23
2027
MIS
< 0.07
ppm
TRICHLOROETHYTENE
TCLP
06/09/23
2027
MS
< 0.05
ppm
2,4,5-TRTCHLOROPHENOL
TCLP
06/09/23
2027
MS
< 40
ppm
2,4,6-TRICHLORPRENOL
TCLP
06/09/23
2027
MS
< 0.2
ppm
VINYL CHLORIDE
TCLP
06/09/23
2027
ms
< 0.02 ppm
LABORATORY DIRECTOR
2217 Cirraham Park Drive - Charlotte, NC-28273
Phone: [phone], Fax: [phone]

M.
LABORATORIES, INC
CHAIN OF CUSTODY
Rhme MAC SUATki
Fax [phone]
Shipping ft Mailing:
2217 Graham Park Drive
Charlotte, NC 28273
"is eswx viat as information toe recorded On M* CAam of Custody document for aKxeptance 1)y PAR La"atcfftes, Im and the North
Carofiria Department of Environmentai and Natural Resourufs
COMP" Name (billing) Commentsi Smial Instructions
U.S. Biosolids, Inc,
Adcliress
PO Box 146
City, State ft zip code
Ronda, NC 28670
. . ........
Point of Contact Ei Teteph(,ine Number
Zach Key 336-467-3550
Taken
; ... V. "111'&A V -, -
ken8y: _SIGNATURE PRINTED NAME:.t
ARE SAMPLES FOR STATE or EPA REPORTING? YES jE NO
'Sample Type: ow Ww J----GWMW — --, HW --- 561 Other
Sample Temp at time of sampling: 0C Sample Temp upon receipt: ^ C
"'Field Preserved: Yes No -Teflon Ci—neifzero Headspace: Yes No nj . a
Residual Chlorine checked at time ofsampling(YIN): D"blorination Necessary (YIN):
C=Cofrfposfte G-Grab DW�r Drinking Water WVV=Wastewater GWkft-Gfoundwatef Monitoring Well HW=HazardcKjsWaWe

pLL PR. III - A... RATE- RELIABLE
1,ADOPLA-170PLIES, INC
WWW.PAR1ABS.C'0M
REPORT OF ANALYSES
Attn: ZACH KEY
U.S. BIOSOLIDS, INC.
PO BOX 146
RONDA, NC 28670-
SAMPLE NUMBER- 147352 SAMPLE ID SPINDALE
DATE SAMPLED- 06/07/23
DATE RECEIVED- 06/07/23 SAMPLER- ZK
TIME RECEIVED- 1235 DELIVERED BY- ZK
Page 1 of 1
ANALYSIS
30 DAY BENCH SCALE TEST
PROJECT NAME: JUN 23
DATE: 08/18/23
ANALYSIS
METHOT5 DATE TIME BY
VAR 06/07/23 1530 RE
LABORATORY DIRECTOR
2217 Graham Park. Drive - Charlotte, NC 28273
Phone: [phone] - Fax: [phone]
SAMPLE MATRIX- WW
TIME SAMPLED- 1035
RECEIVED BY- DJ
TYPE SAMPLE- Grab
RESULT UNITS
4.78 %

Z
EA-BOP—A,IrOR.IES, irqc
WWW. PAR LASS. COM
30 Day Bench Scale Extended Aeration Test
Percent Volatile Solids Reduction
Stark: End:
TS (9)
0.2030
0.1986
TS%
1,95%
1.92%
VS (9)
01386
0.1311
Vs%
68,28%
66.01%
y Mass Fraction of Volatile Solids in Liquid Sludge
0.0133176,
0.0126790
x Mass Fraction of Fixed Solids in Liquid Sludge
0,0061880
0,0065281
FSVR (Mass Balance)
4,82%
FSVR (Van Kleeck)
FSVR (Mass Balance < 15 %
—4,78%
YES
IFSVR (Van Kleeck) <15%
YES
RO. Box411483 * Charlotte, NC 28241-1483
Phone: (704) W-8333 *Fax; t?04) 588-8335

P Am
LABORATOFUES, INC
WWW.PARLASS.COM
30 Day Bench Scale Extended Ae*ration Test
Collected
D.O.
Crucible
Tare W1 (g)
Sample Wt +
Tare Wit (g)
Liquid Sludge Wl
(g)
Oven Temp 'C
DateMme In
Date/Time Out
Dried Sample Wl
+ Tare Wt (9)
Dried Sludge Wt (9
Fixed solids Wt (�
Furnace Temp *C
Date/Time In
Date/Time Out
Burned Sample
Wt + Tare Wit (9)
Volatile Solids Wt
TS%
VS%
VAR Option 3, Percent Volatile Solids Keduction
CLIEN I NAME •
SAMPLE ID: SPINDALE
SAMPLE #:
START DATE,:
END DATF°
As Received Day 0 Day 7 Day 14 Day 21 Day 28
IrIA107121 Ofi,`07121 06118/23 06123123 06130123 07107123
W" I W 1
224
165
3.92
4.33
4,96
X10
X10
X13
X 3
X17
X24
227105
22,7105
21,8743
16.6088
16,9959
22.0138
331178
311178
.32-2246
27,1268
274396
32-1537
10.4073
10.4073
10.3503
10.5180
10.4437
10.3399
106
106
107
107
106
106
06/07,'23 1530
06107!23 16:00
N/16/23 09:45
06/23/23 08:50
06/30/23 09:20
07107/23 09,40
06/08123 15:20
06108/23 16.05
06117!23 10:00
06/24/23 09,00
07/01/23 09-30
07/081123 11100
229135
22,9135
22.0740
16.8058
171972
222124
012030
01030
0,1997
'01970
0,2013
0,1986
0,0644
0,0643
0,0660
0,0677
0.0675
550
550
550
550
550
06109123 17:15
06/17/23 15:00
06/24/23 14A5
07/01123 15405
071011123 15:50
06109/23 18:20
06117/23 16:05
06i24123 1600
07/01123 16-10
07108123 17:05
22.7749
21,9386
16.6748
17.0636
22,0813
0,1386
0.1354
0.1310
0.1336
0.1311
jg
1,95%
1 1,93%
1-87%
1.93%
i 1.92%
68.28%
6780%
66.50%
5637%
1 66 01 %
Yf Mass FIVCWn Of Veiiatifel SeihdS in I.dUld (Faed)
I Sludge a! Start of Test
0.0133176
YO Masts Fraction of Volatile Solids In Lid" (Bottom)
Sli.idge at End of Test
0,0126790
Xf Mass Fraction of Fixed Sollds in t.lquld {feed)
sludge w Start of Test
0.0061880
Xb Mass FractIor, of Feed Solids it Liquid (Bottom)
Sludge at End of 'act
0,0065281
TS (9)l
0 2033
`j
TS (9)
0,19861
VS (g)
013861
VS (g)
0.1311
Volatile Fraction In: 0,350175 Volatile Fraction Out]—
P.O. Box 411483 0 Charlotte, NC 282,41-1483
Phone: [phone] Fax: [phone]$

CHAIN OF CUSTODY
Phone (704) 5W8333
Fax [phone]
LADOPLATOPUV,S, INC
Shipping it Mailing:
2217 Graham Park Drive
Charlotte, HC 28273
It is essential that all iritarmation be recorded an it%$ Chain of Custody document for axeplance oy PAR Laocxatories, Inc " the Nom
Caroiina Denarlment of Environmental and Natural Resources
Company Name (billing)
U.S. Biosolids, Inc.
Address
PO Box 146
City. State ra Zip Code
Ronda, NC 28670
Paint of Contact ri Teteoone Number
Zach Key 336-467-3550
Comments/ Special Instructions
Sample
Taken By: SIGNATURE PRINTED NAME kf
ARE SAMPLES FOR STATE/orEPA REPORTING? YES NO
'Sample Type: ow WW -l""'
GWMW Sal 0thqr
Sample Temp at time of sampling: C Sample Temp upon receipt, a C
"Field Preserved, Yes No Teflon LinerrZero Headspace: Yes No n1a
Residual Chlorine checked at time of sampling (YIN). Dechlorination Necessary (YIN):
C=Compotifte GmGrao DW=0rinkjnqWalet WW-Wastewater GWMW=GroundwaterMonitcnngWell HW=Hazardous Waste

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