WQ0034806_2023 Residual Annual Report_20240207 (2)

Initial Review
Reviewer
nathaniel.thorn burg
Is this submittal an application? (Excluding additional information.) *
Yes No
If not an application what is the submittal type?* Annual Report
Residual Annual Report
Additional Information
Other
Annual Report Year* 2023
Permit Number (IR) * WQ0034806
Applicant/Permittee Coastal Farms and Residuals, LLC
Email Notifications
Does this need review by the hydrogeologist? * Yes QQ No
Regional Office Wilmington
CO Reviewer
Admin Reviewer [e-mail]

Submittal Form
Project Contact Information
Please provide information on the person to be contacted by NDB Staff regarding electronic submittal, confirmation of receipt, and other correspondence.
Name* Martin Mabe
Email Address*
[e-mail]
Project Information
.........................
Application/Document Type*
New (Fee Required)
Modification - Major (Fee Required)
Renewal with Major Modification (Fee
Required)
Annual Report
Additional Information
Other
Phone Number*
3363121396
Modification - Minor
Renewal
GW-59, NDMR, NDMLR, NDAR-1,
N DAR-2
Residual Annual Report
Change of Ownership
We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form.
https://edoes.deq.nc.gov/Forms/NonDischarge_Monitoring_Report
Permit Type:*
Wastewater Irrigation
High -Rate Infiltration
Other Wastewater
Reclaimed Water
Closed -Loop Recycle
Residuals
Single -Family Residence Wastewater
Other
Irrigation
Permit Number:*
WQ0034806
Has Current Existing permit number
Applicant/Permittee Address*
8155 Malpass Corner Road, Currie, NC 28435
Facility Name*
Coastal Farms and Residuals Class B Residuals
Program
Please provide comments/notes on your current submittal below.
At this time, paper copies are no longer required. If you have any questions about what is required, please contact Nathaniel Thornburg
at [e-mail].
Please attach all information required or requested for this submittal to be reviewed here.
(Application Form, Engineering Plans, Specifications, Calculations, Etc.)
Coastal Farms 2023 Annual Report WQ0034806
12.26MB
(NCDEQ).pdf
Upload only 1 PDF document (less than 250 MB). Multiple documents must be combined into one PDF file unless file is larger
than upload limit.
* By checking this box, I acknowledge that I understand the application will not be accepted for pre -review until the fee (if required) has
been received by the Non -Discharge Branch. Application fees must be submitted by check or money order and made payable to the
North Carolina Department of Environmental Quality (NCDEQ). I also confirm that the uploaded document is a single PDF with all parts
of the application in correct order (as specified by the application).
Mail payment to:
NCDEQ — Division of Water Resources
Attn: Non -Discharge Branch
1617 Mail Service Center
Raleigh, NC 27699-1617
Signature
Submission Date 2/7/2024

2023 ANNUAL REPORT
LAND APPLICATION PROGRAM
COASTAL FARMS AND RESIDUALS, LLC
PERMIT #WQ0034806
Prepared For:
Coastal Farms and Residuals, LLC
8155 Malpass Corner Road
Currie, North Carolina 28435
Compiled By:
Willcox & Mabe Soil Solutions, PLLC
7231B Summerfield Road
Summerfield, North Carolina 27358
February 2024

��_
willcox&mate
SOIL SOLUTIONS
February 7, 2024
NCDEQ-DWR Non -Discharge Compliance Unit
512 North Salisbury Street
V' Floor Office# 942X
Raleigh, North Carolina 27604
Attention: Non -Discharge Compliance Unit
Reference: 2023 LAND APPLICATION ANNUAL REPORT
Coastal Farms and Residuals, LLC
Permit No. WQ0034806
WMSS Project No. 15-19 Ph:01
Non -Discharge Compliance Unit:
Willcox & Mabe Soil Solutions, PLLC (WMSS) is submitting all monitoring and reporting
requirements as specified in the above referenced permit on behalf of Coastal Farms and
Residuals, LLC. WMSS compiled this report using data gathered during the compliance
year by Coastal Farms and Residuals, LLC. This data includes: 1) certification form, 2)
residuals analyses and pathogen / vector data, 3) application summaries and field loading
rate reports, 4) soil analyses.
If there is any further information required or questions regarding this annual report please
do not hesitate to contact Coastal Farms and Residuals, LLC or WMSS for further
assistance.
Sincerely,
Willcox & Mabe Soil Solutions, PLLC
/& 1?,1.4
Martin Mabe
NC Land Application/Residuals Operator
#22753
Enclosures
Shared\WMSS Projects\2015\15-19 Coastal Residuals\2023 Annual Report\2023 ANNUAL REPORT - COASTAL FARMS.doc
Willcox 8, Mabe Soil Solutions, PLLC / 7231 B Summerfield Road / Summerfield, NC 27358 / Rob 336.339.9128 or Martin
336.312.1396 / www.wilicoxmabesoil.com

TABLE OF CONTENTS
SECTION NO. TITLE
Certification Form
II Residuals Analyses & Pathogen / Vector Attraction Data
III 2023 Application Summary and Field Loading Rate Reports
IV Soil Analysis

CERTIFICATION FORM

ANNUAL LAND APPLICATION CERTIFICATION FORM
WQ Permit#: WQ0034806 County: Pender Year: 2023
Facility Name (as shown on permit):
Coastal Farms and Residuals, LLC
Land Application Operator: Mr. Wesley Wooten Phone:
910-283-5444
Land application of residuals as allowed by the permit occurred during the past calendar year?
0 Yes ❑ No - If No, skip Part A, and Part B and proceed to Part C. Also, If residuals were
generated but not land applied, please attach an explanation on how the residuals were handled.
Part A - Residuals Application Summary:
Total number of application fields in thepermit:
12
Total number of fields utilized for land application during the year:
2
Total amount of dry tons applied during the year for all application sites:
501.85
Total number of acres utilized for land application during the year:
175.3
Part B - Annual Compiance Statement:
Facility was compliant during calendar year 2023 with all conditions of the land application permit
(including but not limited to items 1-13 below) issued by the Division of Water Quality. El Yes ❑ No
If no please, provide a written description why the facility was not compliant, the dates, and explain corrective
action taken.
1) Only residuals approved for this permit were applied to the permitted sites.
2) Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least
6.0 or the limit specified in the permit.
3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3)
copies of laboratory results are attached.
4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are
5) All other monitoring was performed in accordance with the permit and reported during the year as required and
three (3) copies of certified laboratory results are attached.
6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .1105(a) or the Pollutant
Loading Rates in 15A NCAC 02T .1105(b) (applicable to 40 CFR Part 503 regulated facilities).
7) All general requirements in as specified in the Land Application Permit were complied with (applicable to 40
CFR Part 503 regulated facilities).
8) All monitoring and reporting requirements in 15A NCAC 02T .1111 were complied with (applicable to 40 CFR
Part 503 regulated facilities).
9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation,
prior authorization was received from the Division of Water Quality.
10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations
are attached to include appropriate actions and remediations.
11) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as
specified in the permit.
12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13) All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C - Certification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true,
accurate, and complete. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations."
Mr. Wesley W000ten, President
Permittee Name and Title (type or print)
1/26/2024
Signature o Permittee Date
Signature of Preparer* Date Signature of Land Applier Date
(if different from Permittee) (if different from Permittee and Preparer)
* Preparer is defined in 40 CFR Part 503.9 (r) and 15A NCAC 02T .1102 (26)
DENR FORM ACF (12/2006)

RESIDUAL ANALYSES
TCLP ANALYSES IF REQUIRED
AND PATHOGEN AND VECTOR ATTRACTION REDUCTION

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COASTAL RESIDUALS
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: September 22, 2023
Avendale WWTP
3.42 % Solids
7.02 PH
Permit No. WQ0030775
Parameter
%
JMg/Kg Dry Weight
x 10,000)
Pounds/Dry Ton
(Mg/Kg(MgfKg x 0.002)
Nitrogen (TKN)
7.830
78,300.000
156.600
Phosphorus
0.854
8,540.000
17.080
Potassium
0.307
3,070.000
6.140
PAN injected)*
2.608
26,075.000
52.150
PAN surface)*
2.439
24,385.000
48.770
Ammonia Nitrogen
0.338
3,380.000
6.760
Calcium
1.320
13,200.000
26.400
Calcium Carbonate E .
---
---
---
Magnesium
---
4,040.000
8.080
Sodium
3,600.000
7.200
Sulfur
---
---
Nitrate N / Nitrite N
---
219.000
0.438
Barium
Chloride
---
---
---
---
SAR
1.30
Iron
---
---
---
Ceiling Concen.
Aluminum
---
2,640.00
5.280
(M /IC )
Arsenic
---
29.80
0.060
75
Cadmium
---
30.10
0.060
85
Chromium
---
30.100
0.060
---
Copper
---
142.00
0.284
4,300
Lead
---
30.10
0.060
840
Mercury
---
0.488
0.001
57
Molybdenum
---
30.10
0.060
75
Nickel
---
30.10
0.060
420
Selenium
---
30.10
0.060
100
Zinc
---
1,040.00
2.080
7,500
Environmental Chemists €l 2023-22071
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits
for calculation purposes.

COASTAL FARMS AND RESIDUALS, LLC
WQ0034806
Avendale WWTP
at ?'
€F a1 o ift zir .
-'
09/22/23
454,546
5.6576
09/22/23
65,218
4.8144
09/22/23
462,428
5.6650
09/22/23
109,375
5.0389
09/22/23
78,476
4.8947
09/22/23
428,955
5.6324
09/22/23
427,808
5.6312
Total 1 37.3343
Average 1 5.3335
Geometric Mean L$il Fecal Coliform MPN / gram
Geometric Mean of Less than 2,000,000 meets Class B - Alternative 1 Pathogen Reduction
requirement.

:enviroehemn].
ANALYTICAL & CONSULTING CHEMISTS
Lewis Farms & Liquid Waste, INC.
8155 Malpass Corner Road
Currie NC 28435
Attention:
Lab ID Sample ID:
23-53785 Site: Sludge
Test
Sludge Residuals
Aluminum
Arsenic
Cadmium
Calcium
Chromium
Copper
Lead
Magnesium
Molybdenum
Nickel
Potassium
Selenium
Sodium
Zinc
Nitrate+Nitrite-Nitrogen
Total Solids (%)
Ammonia Nitrogen
Total Kjeldahl Nitrogen (TKN)
Total Phosphorus
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910,392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 - 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 a 910.347.5843 Lab/Fax
info(aenvironmentalchemists. com
Date of Report: Oct 24, 2023
Customer PO #:
Customer ID: 14020008
Report #: 2023-22074
Project ID: AquaNC-Avendale
Collect Date/Time Matrix
9/22/2023 9:15 AM Solid/Sludge
Method
EPA 200.7, Rev. 4.4, 1994
EPA 200.7. Rev. 4.4, 1994
EPA 200.7, Rev. 4.4, 1994
EPA 200.7, Rev. 4.4, 1994
EPA 200.7. Rev. 4.4, 1994
EPA 200.7. Rev. 4.4, 1994
EPA 200.7, Rev. 4.4, 1994
EPA 200.7, Rev. 4.4, 1994
EPA 200.7, Rev. 4.4. 1994
EPA 200.7, Rev. 4.4, 1994
EPA 200.7, Rev. 4.4, 1994
EPA 200.7, Rev. 4.4. 1994
EPA 200.7, Rev, 4.4, 1994
EPA 200.7, Rev 4.4, 1994
EPA 353.2
SM 2540 B
SM 4500 NH3 C-2011
SM 4500 Norg B-2011
SM 4500 P (F-H)-2011
pH SW 846 Method 90450
Result estimated. Analyzed out of 15 minutes hold time.
Mercury
SW-846 7471 B
Results
Sampled by
Client
Date Analyzed
2640 mg/kg
10/17/2023
<29.8 mg/kg
10/17/2023
<30.1 mg/kg
10/09/2023
13200 mg/kg
10/09/2023
<30.1 mg/kg
10/09/2023
142 mg/kg
10/09/2023
<30.1 mg/kg
10/09/2023
4040 mg/kg
10/09/2023
<30.1 mg/kg
10/09/2023
<30.1 mg/kg
10/09/2023
3070 mg/kg
10/09/2023
<30.1 mg/kg
10/09/2023
3600 mg/kg
10/09/2023
1040 mg/kg
10/09/2023
219 mg/kg
09/27/2023
3,42 %
09/26/2023
3380 mg/kg
09/26/2023
78300 mg/kg
09/26/2023
8540 mg/kg
09/29/2023
7,02 units
10/09/2023
<0.488 mg/kg 10/11/2023
Report N. • 2023.22074 Pape 1 of 3

Environmental Chemists, Inc.
envirochem
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab 4 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 * 910.347.5843 Lab/Fax
ANALYTICAL R CONSULTING CHEMISTS
[e-mail]
Lewis Farms & Liquid Waste, INC. Date of Report: Oct 24, 2023
8155 Malpass Corner Road
Customer PO #:
Currie NC 28435
Customer ID: 14020008
Attention:
Report #-. 2023-22074
Project ID: AquaNC-Avendale
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
23-53786 Site: 1
9/22/2023 9:15 AM Solid/Sludge Client
Test
Method Results Date Analyzed
Total Solids {%)
SM 2540 B 3.52 % 09/26/2023
Fecal Density
SM 9221C E-2014 454546 MPN/g 09/22/2023
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
23-53787 Site: 2
9/22/2023 9:15 AM Solid/Sludge Client
Test
Method Results Date Analyzed
Total Solids (%)
SM 2540 B 3.68 % 09126/2023
Fecal Density
SM 9221C E-2014 65218 MPN/g 09/22/2023
Lab ID Sample 1D:
Collect Date/Time Matrix Sampled by
23-53788 Site: 3
9/22/2023 9:15 AM Solid/Sludge Client
Test
Method Results Date Analyzed
Total Solids (%)
SM 2540 B 3.46 % 09/26/2023
Fecal Density
SM 9221C E-2014 462428 MPN/g 09/22/2023
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
23-53789 Site: 4
9/22/2023 9:15 AM Solid/Sludge Client
Test
Method Results Date Analyzed
Total Solids (%)
SM 2540 B 3.20 % 09/26/2023
Fecal Density
SM 9221C E-2014 109375 MPN/g 09/22/2023
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
23-53790 Site: 5
9/22/2023 9:15 AM Solid/Sludge Client
Test
Method Results Date Analyzed
Total Solids (%)
SM 2540 B 4.46 % 09/26/2023
Fecal Density
SM 9221C E-2014 78476 MPN/g 09/22/2023
Report #:: 2023.22074
Page 2 of 3

FFI'". -- --"qql
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS [e-mail]
Lewis Farms & Liquid Waste, INC.
8155 Malpass Corner Road
Currie NC 28435
Attention:
Lab ID Sample ID:
23-53791 Site:6
Test
Total Solids (%)
Fecal Density
Lab ID Sample ID:
23-53792 Site:7
Test
Date of Report: Oct 24, 2023
Customer PO #:
Customer ID: 14020008
Report #: 2023-22074
Project ID: AquaNC-Avendale
Collect Date/Time Matrix Sampled by
9/22/2023 9:15 AM Solid/Sludge Client
Method Results Date Analyzed
SM 2540 a 3.73 % 09/26/2023
SM 9221C E-2014 428955 MPN/g 09/22/2023
Collect Date/Time Matrix Sampled by
9/22/2023 9:15 AM Solid/Sludge Client
Method
Results Date Analyzed
Total Solids (%) SM 2540 e 3 74 %
Fecal Density SM 9221c E-2014 427808 MPN/g
Comment: Results, except pH, reported on a dry weight basis. pH reported on an as received basis.
n
Reviewed by:
09/26/2023
09/22/2023
Report #:: 2023.22074 Page 3 of 3

V iln"inton
oal, NC
Sample Receipt Checklist 010•391
Cl•en `:_ o
' Date:
-- � Report Number: /
0.
i -C-�` N%fi-
�` t.i i�•.i Lj ���/� 1 al; N sent O1 tR_ conic-?
.�.',�h^i?i a n• z frCUstrJCl�==a1s+%rie ( n , ,.—..__—
t_•rIp nature upon receipt P es_Rt, were ti;a'
• :C _y intacVunbroken?
- �- - Corrected
m eratlro to _n: ❑ temperature orG
'�� Tem(`ra'�•-e �r- .. f upon r_.._ip,
a _ _ .
±D: Tl omas Trace b� N 21 �,-arr;st B t� -_ _ -
a •e S/ 0885859 Ip r_, C J o :les
-;Factor `C: 0.0
�- pi2ratureorcv ;fir
-;-•;__eu�r1 -Project- -
. 4 1 ❑ (JO 4. 1., u C, :vas , -
- ere proper custody pro'e ures r-! • fAsr./Qq notified?
'c5 ` ❑ NO - { e mquished rece t, - ---
5. Were sample f0`s iiste(l 0n th_ ? i ed) foNo:'red?
I NO 6. Were samples US listed on s: ~` YES ❑ NO mPle containers?
7• Were collection date and tim= listed on the S C1 NO COC?
` 8• UJere tests to be a
� YES ❑ PJO 9. Did samples arrive infProperolisted on the COC?
YES O NO containers for each test?
10. Did samples arrive in good condition for each test?
YES ❑ NO 11. Was adequate sample volume available?*
YES O NO 12. Were s
YES
❑
NO
a -pies received within proper holding time for requested tests?
13. Were acid
G YES
G
❑
NO
preserved samples received at a pH of <2?
lei. Were cyanide samples
YES
❑
NO
received at a pH >12?
15• Were sulfide
❑ -iC
samples received at a PH>g?
116. Were tJH3,rTKN/P;;e,:o'r
iG YES
C
No
17• 'Here Sulfide/C anid� r�;idual OF <J.5-
Y received
❑
NO
at a chlorine residual of <0.5 m/E?l'
18. Were ortho hosphate sam ie
P
i
p s filtered in the field within 15 minutes;)
.rtes.
1= r o�;
a-e
PH checked at tirr.2 o; an,r, an
al' / c
_ , recard!d -he b n
ar_ r� _ _fo, 0-1 e cf;sh e:
Sample Preservation; t
�amPle(s)
(Must be comP ►eted for any sample(s) incorrectly preserved or with he
Dy adding (circle one): H SO_ were received incorrect) r adspace)
Y pre and were adjusted acr_ordincrIv
Time of preservation: HNO, HCI NaOH
If more than one- pserrai
reti-
- a is needed notate in comments o., ,�., _,. • - -- i.. ?�_�. SST _. bel
pl_Y �? t�= =;i: _ . v'•^� :',3i' .'?' date-
i ^1=
v ere received �';ith headspace
COMMENTS:
DOC. QA.002 Rev 1
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T: 1N

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Coastal Farms and Residuals, LLC
WWTP Name: Avendale WWTP
Monitoring Period:
From 1/1/2023
To
WQ Permit Number: WQ0034806
NPDES Number: WQ0030775
12/31 /2023
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level arh►Pvar1 and alfnrnor;vn
Class A: Alt. A (time/temp) ❑ Alt B (Alk Treatment) ❑ Alt. C (Prior Testing) ❑
A1t.D (No Prior Test} ❑ Process to Further Reduce Pathogengs ❑
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost ❑ Heat Drying ❑ Heat Treatment ❑ Thermophilic ❑
Beta Ray ❑
Gatnma Ray ❑
Pasteurization ❑
.Q
Class B:
Alt. (1) Fecal DensityI].1. Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization ❑ Air Drying ❑ Col"Posting
❑ Aerobic Digestion El-Anaerob
,Anaerobic es ton
If applicable to alternative performed (Class A ot•Class B) complete the
_
following .monitorin...data:
Parameter
Allowable Level
Pathogen Density
Number ot
Frequency
Sample
Analytical
in Sludge
Excee-
s
of Analysis
Type
Tech-
niclue
Minimu
Geo. Mean
Maximu
Units
2 x 10 to the
6th power
MPN
65,218
215,512
462,428
MPN/g
0
Annual
Grab
SM92210E
per gram of
Fecal Coliform
total solids
CFU
1000 mpn per gram
oftoW solid (dry
weight)
Salmonella bacteria
3 MPN per 4 grams
(in lieu of fecal
total solid (dry
coliform)
wei lit)
va --& wuwiA A%,--UUCLtvtl k JLDA 1-iUak, 06 1 .110 / t - Please indicate a{rerrinfivP nArfnrmnrl-
Alt.1 (VS reduction) ❑
Alt. 2 (40-day bench) ❑
Alt. 3 (30-day bench) ❑ jAlt, 4 (Spec. 0, uptake) ❑
Alt. 5 (14-Day Aerobic) ❑
Alt. 6 (Alk. Stabilization ❑
Alt 7 (Drying - Stable) ❑ 1 Alt. 8 (Drying - Unstable) ❑
Alt. 9 (Injection) El
iTTTTT. Tl', ♦ Mr— r.
Alt. 10 (Incorporation) []
No vector attraction reduction alternatives were performed ❑
>✓A�ALA•Av.tiIAvlv31AIElviLlvl(pteasecheck the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if
you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
/11 LAY/�6 EDtQc{ 1'd 5 - QRC Wesley Wooten, President
Pre arer Name an Title (type or print) Land Applier Name and Title (if applicable)(type or print)
a�3 +t/ 12/1/23
Signature of Preparer* Date Signature of La d Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .l 102 (26)
DENR FORM PVRF 02T (12/2006)

COASTAL FARMS
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: March 14, 2023
Morehead City
23.90 % Solids
7.17. n74
Permit No. NC0026611
Parameter
%
Mg/Kg Dry Weight
(% x 10,000)
Pounds/Dry—Ton
(M,-/Kg x 0.002)
Nitrogen (TKN)
5.100
51,000.000
102.000
Phosphorus
3.520
35,200.000
70.400
Potassium
0.382
3,820.000
7.640
PAN (injected)*
1,694
3,869.500
7.739
PAN (surface)*
1.662
1 3,777.000
7.554
Ammonia Nitrogen
0.062
622,000
1,244
Calcium
5.770
57,700.000
115.400
Calcium Carbonate E .
---
___
---
Magnesium
0.443
4,430.000
8.860
Sodium
0.447
4,470.000
8.940
Sulfur
__-
___
Nitrate N /Nitrite N
---
1,200.000
2.400
Barium
.-_
___
-_-
Chloride
---
___
Iron
___
--_
Aluminum
---
16,900.00
33.800
Arsenic
---
10.90
0.022
Cadmium
---
6.19
0.012
Chromium
---
14.500
---
Copper
---
807.00
1.614
Lead
---
15.80
0.032
Mercury
---
0.988
0.002
Molybdenum
—
6.19
0.012
Nickel
--
13.50
0.027
Selenium
---
6.19
0.012
Zinc
---
1,240.00
2.480
Environmental Chemists, Inc. 2023-05103
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
SAR
2.36
Ceiling Concen.
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits
for calculation purposes.
75
85
840
57
75
420
100
7,501

COASTAL FARMS AND RESIDUALS, LLC
WQ0034806
Morehead City W WTP
03/14/23
65
1.8129
03/14/23
10
1.0000
03/14/23
10
1.0000
03/14/23
8
0.9031
03/14/23
9
0.9542
03/14/23
38
1.5798
03/14/23
9
0.9542
Total 8.2043
Average 1.1720
------------------
Geometric Mean )!S ` € Fecal Coli�form MPN / gram
Geometric Mean of Less than 2,000,000 meets Class B - Alternative I Pathogen Reduction
requirement.

[en:vlroehem
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowser -town Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
info`r environmentalchemists.com
Town Of Morehead City
Date of Report: Apr 17, 2023
1100 Bridges Street
Customer PO M
Morehead City NC 28557
Customer ID: 09020011
Attention:
Report M 2023-05103
Project ID: Sludge
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
23-12698 Site: Sludge
3/14/2023
10:10 AM Solid/Sludge Nate Johnson
Test
Method
Results
Date Analyzed
CCE
AOAc 1,005
0.0%
04/13/2023
Paint Filter Test
SW 846 Method 9095 A
pass
04/14/2023
Chlordane (TCLP)
SW-846 8081 B
<0.005 mg/L
03/20/2023
Endrin (TCLP)
SW-846 8081 B
<0.00005 mg/L
03/20/2023
Heptachlor (TCLP)
SW-846 8081 B
<0.00005 mg/L
03/20/2023
Heptachlor epoxide (TCLP)
SW-846 8081 8
<0.00005 mg/L
03/20/2023
Lindane (TCLP)
SW-846 8081 8
<0.00005 mg/L
03/20/2023
Methoxychlor (TCLP)
SW-846 8081 B
<0.00005 mg/L
03/20/2023
Toxaphene (TCLP)
SW-846 8081 B
<0.005 mg/L
03/20/2023
2,4,5-TP (TCLP)
SW-846 8151 A
<0.003 mg/L
03/17/2023
2,4-D (TCLP)
SW446 8151 A
<0.003 mg/L
03/17/2023
1,4-Dichlorobenzene (TCLP)
SW-846 8270 E
<0.050 mg/L
03/20/3023
2,4,5-Trichlorophenol (TCLP)
SW-846 8270 E
<0.050 mg/L
03/20/3023
2,4,6-Trichlorophenol (TCLP)
SW-846 8270 E
<0.050 mg/L
03/20/3023
2,4-Dinitrotoluene (TCLP)
SW-846 8270 E
<0.050 mg/L
03/20/3023
Cresol (TCLP)
SW-846 8270 E
<0.050 mg/L
03/20/3023
Hexachloro-1,3-butadiene (TCLP)
SW.8468270E
<0.050mg/L
03/20/3023
Hexachlorobenzene (TCLP)
SW-845 8270 E
<0.050 mg/L
03/20/3023
Hexachloroethane (TCLP)
SW-846 8270 E
<0.050 mg/L
03/20/3023
m + p-Cresol (TCLP)
SW-846 8270 E
<0.050 mg/L
03/20/3023
Nitrobenzene (TCLP)
SW-846 8270 E
<0.050 mg/L
03/20/3023
o-Cresol (TCLP)
SW-846 8270 E
<0.050 mg/L
03/20/3023
Pentachlorophenol (TCLP)
SW-8468270E
<0.250mg/L
03/20/3023
Pyridine (TCLP)
SW-046 6270 E
<0.050 mg/L
03/20/3023
1, 1 -Dichloroethylene (TCLP)
SW-846 Method8260D
<0.01 mg/L
3/21/2023
1,2-Dichloroethane (TCLP)
SW-846 Method6260D
< 0.01 mg/L
3/21/2023
Report #:: 2023.05103
Page 1 of 5

Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS info`tgenvironmenlalchemists.com
Town Of Morehead City
Date of Report: Apr 17, 2023
1100 Bridges Street
Customer PO #:
Morehead City NC
28557
Customer ID: 09020011
Attention:
Report #: 2023-05103
Project ID: Sludge
Benzene (TCLP)
SW-846 Method6260D
< 0.01 mg/L
3/21/2023
Carbon Tetrachloride (TCLP)
SW-846 Method 8260D
< 0.01 mg/L
3/21/2023
Chlorobenzene (TCLP)
SW-846 Method82600
< 0.01 mg/L
3/21/2023
Chloroform (TCLP)
SW-846 Method 8260D
< 0.01 mg/L
3/21/2023
Methyl ethyl ketone (TCLP)
SW-846 Method 8260D
0.05 mg/L
3/21/2023
Tetrachloroethylene (TCLP)
SW.848 Method 8260D
< 0.01 mg/L
3/21/2023
Trichloroethylene (TCLP)
SW-846 Method 8260D
< 0.01 mg/L
3/21/2023
Vinyl Chloride (TCLP)
SW-846 Method 8260D
< 0.01 mg/L
3/21/2023
RCI
Ignitability
EPA 1030
<0.8 mm/sec
03/21/2023
Cyanide
SM 4500 CN D-2016
2.99 mg/kg
03121 /2023
Sulfide
SM 4500 S D
<0.37 mg/kg
03/24/2023
Sludge Residuals
Aluminum
EPA 200.7.Rev 4.4. 1994
16900mg/kg
03/22/2023
Arsenic
EPA 200.7, Rev 4.4, 1994
10.9 mg/kg
03/22/2023
Cadmium
EPA 200.7, Rev. 4.4, 1994
<6.19 mg/kg
03/22/2023
Calcium
EPA 200.7. Rev 4.4, 1994
57700 mg/kg
03/22/2023
Chromium
EPA 20D.7, Rev. 4.4, 1994
14.5 mg/kg
03/22/2023
Copper
EPA 200.7, Rev, 4.4. 1994
807 mg/kg
03/22/2023
Lead
EPA 200.7, Rev. 4 4, 1994
15.8 mg/kg
03/22/2023
Magnesium
EPA 200.7, Rev. 4 4, 1994
4430 mg/kg
03/22/2023
Molybdenum
EPA 200.7, Rev. 4 4, 1994
<6.19 mg/kg
03/22/2023
Nickel
EPA 200.7, Rev. 4 4. 1994
13.5 mg/kg
03/22/2023
Potassium
EPA 200.7. Rev. 4.4, 1994
3820 mg/kg
03/22/2023
Selenium
EPA 200.7, Rev. 4.4, 1994
<6.19 mg/kg
03/22/2023
Sodium
EPA 200.7, Rev. 4.4, 1994
4470 mg/kg
03/22/2023
Zinc
EPA 200.7, Rev. 4.4, 1994
1240 mg/kg
03/22/2023
Nitrate+Nitrite-Nitrogen
EPA353.2
1200mg/kg
03/17/2023
Total Solids (%)
SM 2540 8
23.9 %
03/15/2023
Ammonia Nitrogen
SM 4500 NH3 C-2011
622 mg/kg
03/15/2023
Report #.' 2023.05103
Page 2 of 5

ANALYTICAL & CONSULTING CHEMISTS
Town Of Morehead City
1100 Bridges Street
Morehead City NC
Attention:
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 29405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
[e-mail]
Date of Report: Apr 17, 2023
Customer PO #:
28557 Customer ID: 09020011
Report #: 2023-05103
Project ID: Sludge
Total Kjeldahl Nitrogen (TKN) SM 4500 Norg B-2011
Total Phosphorus SM 4500 P (F-H)-2011
pH SW 846 Method 9045D
Result estimated. Analyzed out or 15 minutes hold time.
Mercury
TCLP Metals
Arsenic (TCLP)
Barium (TCLP)
Cadmium (TCLP)
Chromium (TCLP)
Lead (TCLP)
Selenium (TCLP)
Silver (TCLP)
Mercury (TCLP)
Lab ID Sample ID:
23-12699 Site: Sludge 1
SW-846 7471 B
EPA 200.7. Rev. 4.4, 1994
EPA 200.7. Rev. 4.4, 1994
EPA 200.7, Rev. 4.4, 1994
EPA 2007, Rev. 4.4, 1994
EPA 200.7, Rev. 4.4, 1994
EPA 2003, Rev. 4.4. 1994
EPA 200.7, Rev. 4.4. 1994
EPA 245A
51000 mg/kg
35200 mg/kg
7.12 units
0.988 mg/kg
<1.0 mg/L
<1.0 mg/L
<1.0 mg/L
<1.0 mg/L
<1.0 mg/L
<1.0 mg/L
<1.0 mg/L
<0.0002 mg/L
Collect Date/Time Matrix Sampled by
3/14/2023 10:11 AM Solid/Sludge Nate Johnson
03/15/2023
03/23/2023
03/31 /2023
03/17/2023
03/22/2023
03/22/2023
03/22/2023
03/22/2023
03/22/2023
03/22/2023
03/24/2023
03/30/2023
Test Method Results Date Analyzed
Total Solids (%)
SM 2540 B
20.2 %
03/15/2023
Fecal Density
SM 9221C E-2014
65 MPN/g
03/14/2023
Lab ID Sample ID:
Collect DatefTime
Matrix Sampled by
23-12700 Site: Sludge 2
3/14/2023 10:12 AM
Solid/Sludge Nate Johnson
Test
Method
Results Date Analyzed
Total Solids (%)
SM 254013
20.0 %
03/15/2023
Fecal Density
SM 9221C E-2014
10 MPN/q
03/14/2023
Report #.: 2023.05103
Page 3 of 5

ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 ' 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 ' 910.347.5843 Lab/Fax
info(aenvironmentalchemists.com
Town Of Morehead City Date of Report: Apr 17, 2023
1100 Bridges Street Customer PO #:
Morehead City NC 28557 Customer ID: 09020011
Attention: Report #: 2023-05103
Project ID: Sludge
Lab ID Sample ID: Collect DatelTime Matrix Sampled by
23-12701 Site: Sludge 3 3/14/2023 10:13 AM Solid/Sludge Nate Johnson
Test Method Results Date Analyzed
Total Solids (%)
Fecal Density
Lab ID Sample ID:
23-12702 Site: Sludge 4
Test
SM 2540 B
SM 9221C E-2014
20.8 % 03/15/2023
10 MPN/g 03/14/2023
Collect DatefTime Matrix Sampled by
3/14/2023 10:14 AM Solid/Sludge Nate Johnson
Method Results Date Analyzed
Total Solids (%)
SM 2540 B
23.1 % 03/15/2023
Fecal Density
SM 9221C E-2014
<8 MPN/g 03/14/2023
Lab ID Sample ID:
Collect DatelTime
Matrix Sampled by
23-12703 Site: Sludge 5
3/14/2023 10:15 AM
Solid/Sludge Nate Johnson
Test
Method
Results Date Analyzed
Total Solids (%)
SM 2540 B
20.5 % 03/15/2023
Fecal Density
SM 9221C E-2014
<9 MPN/g 03/14/2023
Lab ID Sample ID:
Collect DaterTime
Matrix Sampled by
23-12704 Site: Sludge 6
3/14/2023 10:16 AM
Solid/Sludge Nate Johnson
Test
Method
Results Date Analyzed
Total Solids (%)
SM 2540 B
20.7 % 03/15/2023
Fecal Density
SM 9221C E-2014
38 MPN/g 03/14/2023
Lab ID Sample ID:
Collect DaterTime
Matrix Sampled by
23-12705 Site: Sludge 7
3/14/2023 10:17 AM
Solid/Sludge Nate Johnson
Test
Method
Results Date Analyzed
Total Solids (%}
SM 2540 B
20.6 % 03/15/2023
Fecal Density
SM 9221C E•2014
<9 MPN/g 03/14/2023
Report #:: 2023.05103
Page 4 of 5

Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab ' 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 ' 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 ' 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS [e-mail]
Town Of Morehead City Date of Report: Apr 17, 2023
1100 Bridges Street Customer PO #:
Morehead City NC 28557 Customer ID: 09020011
Attention: Report #: 2023-05103
Project ID: Sludge
Comment: Sludge residuals, except pH, reported on a dry weight basis. pH reported on an as received basis
Reviewed by: / 9--�
{
teport C 2023.05103 Page 5 of 5

Environmental Chemist, Inc., Wilmington, NC Lab 494
6602 Windmill Way
Wilmington, NC 28405
910.392.0223
Sample Receipt Checklist
Date: 1 - Report Number: 20230
Receipt of sample:
ECHEM Pickup Client Delivery ❑ UPS ❑ FedEx ❑ Other ❑
E
ES
]GSV
A
1, Were custody seals present on the cooler?
ES
A
2. !f custody seals were present, were they intact/unbroken?
Original temperature upon receipt
°C Corrected temperature upon receipt
How temperature taken:
❑ Temperature Blank 14 Against Bottles
IR Gun ID: Thomas Traceable 5/N 210886869 IR Gun Correction Factor `C: 0.0
YES
❑
NO
3. If temperature of cooler exceeded 6°C, was Project Mgr./QA notified?
YES
❑
NO
4. Were proper custody procedures (relinquished/received) followed?
YES
❑
NO
5. Were sample ID's listed on the COC?
YES
❑
NO
6. Were samples ID's listed on sample containers?
YES
❑
NO
7. Were collection date and time listed on the COC?
YES
❑
NO
8. Were tests to be performed listed on the COO
YES
❑
NO
9. Did samples arrive in proper containers for each test?
)l
YES
❑
NO
10. Did samples arrive in good condition for each test?
YES
O
NO
11. Was adequate sample volume available?'
YES
❑
NO
12. Were samples received within proper holding time for requested tests?
❑
YES
❑
NO
13. Were acid preserved samples received at a pH of <2?
❑
YES
❑
NO
14. Were cyanide samples received at a pH >12?
❑
YES
❑
NO
15. Were sulfide samples received at a pH >9?
❑
YES
❑
NO
16. Were NH3/TKN/Phenol received at a chlorine residual of <0.5 m/L? **
❑
YES
❑
NO
117. Were Sulfide/Cyanide received at a chlorine residual of <0.5 m/L?
❑
YES
❑
NO
18. Were orthophosphate samples filtered in the field within 15 minutes?
* TOC/Volatiles are pH checked at time of analysis and recorded on the benchsheet.
* * Bacteria samples are checked for Chlorine at time of analysis and recorded on the benchsheet.
Sample Preservation: (Must be completed for any sample(s) incorrectly preserved or with headspace)
Sample(s) were received incorrectly preserved and were adjusted accord ngly
by adding (circle one): HiSO-' HNO3 HCl NaOH
Time of preservation: If more than one preservative is needed, notate in comments below
Note: Notify customer service immed ate'y for Sncorrectly preserved samp es Obtain a new sample or
notify the state lab if d,rected to a-ia yzed by the customer. who was not{fied, date and tme
Volatiles Samples) were received with headspace
COMMENTS:
DOC. QA.002 Rev 1
°c

Ici

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (503 Rules)
Facility Name: Coastal Farms and Residuals, LLC WQ Permit Number: WQ0034806
WWTP Name: Town of Morehead City NPDES Number: NCO026611
Monitoring Period: From l/l/2023 To 12/31/2023
Pathogen Reduction (40 CFR 503.32) - Please indicate ]evPl nehiPvarl a,,] Latta rno4ivn ne.fn. me 7.
Class A:
Alternative 1 ❑
Alterative 2 ❑
Altemativ e 3 ❑
Alternative 4 ❑
Alternative 5 ❑
Alternative 6 ❑
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost ❑ Heat Drying ❑ Heat Treatment ❑ Thennophilic El
Beta Ray El
Gamma Ray ❑
Pasteurization ❑
Class B: Alternative I El Alt-mative 2 ❑
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization ❑ Air Drying❑ Com ostin ❑ Aerobic Digestion ❑
Anaerobic
btc Digestion
sh n o ❑
-Class .the .fo[lo—wing •monitoring
If applicable to alternative performed (Class A or B). complete
.data:
Parameter
Allowable Level
Pathogen Density
um er of
Frequency
Sample
Analytical
in Slud,-e
b
Excees
of AnalysisType
Tech-
ninue
Minimum
Geo. Mean
Maximum
Units
2 x 10 to the
6th power
MPN
8
15
65
MPN/g
0
Annual
Grab
SM9221C;
per gram of
Fecal Coliform
total solids
CPU
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
3 MPN per 4 grams
(in lieu of fecal
total solid (dry
coliform)
weight)
V
ector Attraction Reduction (40 CFR 503.33) - Please indicate nntinn nerfnrrn,-d-
Alt. I (VS reduction) ❑
Alt. 2 (40-day bench) ❑
Alt. 3 (30-day bench) ❑
Alt. 4 (Spec. O, uptake) Cl
Alt. 5 (14-Day Aerobic) ❑
Alt. 6 (Alk. Stabilization ❑
Alt 7 (Drying - Stable) ❑
I Alt. 8 (Drying - Unstable) ❑
Alt. 9 (Injection) ❑
Alt. 10 (Incorporation) El
No vector attraction reduction alternatives were performed ❑
CER1 IFICA ION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector
attraction reduction requirement in 40 CFR 503.33 have been met."
❑ "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector
attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check
this statement attach an explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Chad Sutton, WWTP Superintendent Wesley Wooten, President
Pr r
print) Land Applier Name and Title (if appIicable)(type or print)
1 10/31 /23
Signature of Preparer* Date Signature of Land pplier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .l 102 (26)
DENR FORM PVRF 503 (12/2006)

COASTAL RESIDUALS
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: November 20, 2023
Pluris Hampstead WWTF Permit No. WQ0037287
3.48 % Solids
7.37 pH
Parameter
%
Mg/Kg Dry Weight
(% x 10,000)
Pounds/Dry Ton
(Mg/Kg(Mg/Kg x 0.002)
Nitrogen (TKN)
5.780
57,800.000
115.600
Phosphorus
3.180
31,800.000
63.600
Potassium
0.848
8,480.000
16.960
PAN (injected)*
2.123
21,234.000
42.468
PAN (surface)*
1.866
18,664.000
37.328
Ammonia Nitrogen
0.514
5,140.000
10.280
Calcium
2.440
24,400.000
48.800
Calcium Carbonate E .
---
---
---
Magnesium
---
5,230,000
10.460
Sodium
---
3,330.000
6.660
Sulfur
--
--_
Nitrate N / Nitrite N
---
296.000
0.592
Barium
---
---
---
SAR
0.94
Chloride
---
---
---
Iron
---
---
---
Ceiling Concen.
(Mg/Kg)
Aluminum
---
10,900.00
21.800
Arsenic
---
21.20
0.042
75
Cadmium
---
16.10
0.032
85
Chromium
---
30.500
0.061
---
Copper
---
185.00
0.370
4,300
Lead
---
16.10
0.032
840
Mercury
---
0.53
0.001
57
Molybdenum
---
16.10
0.032
75
Nickel
---
16.10
0.032
420
Selenium
---
16.10
0.032
100
Zinc
---
787.00
1.574
7,500
Environmental Chemists # 2023-27165
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits
for calculation purposes.

COASTAL FARMS AND RESIDUALS, LLC
WQ0034806
Pluris Hampstead WWTF
MP
11/20/23
153,410
5.1859
11/20/23
259,888
5.4148
11/20/23
479,042
5.6804
11/20/23
507,937
5.7058
11/20/23
501,568
5.7003
11/20/23
162,651
5.2113
11/20/23
437,159
5.6406
Total 1 38.5390
Average 5.5056--1
Geometric Mean ..4 !;11�jj Fecal Coliform MPN / gram
j1
Geometric Mean of Less than 2,000,000 meets Class B - Alternative I Pathogen Reduction
requirement.

:envirochem
ANALYTICAL & CONSULTING CHEMISTS
Lewis Farms & Liquid Waste, INC.
8155 Malpass Corner Road
Currie NC 28435
Attention:
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
info(2environmentalchemisls.com
Date of Report: Dec 21, 2023
Customer PO #:
Customer ID: 14020008
Report #: 2023-27165
Project ID: Hampstead
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
23-65816 Site: Sludge 11/20/2023 10:40 AM Solid/Sludge Kris King
Test Method Results Date Analyzed
Chlordane (TCLP)
SW-846 8081 B
<0.02 mg/L
11/28/2023
Endrin (TCLP)
SW-846 80816
<0.0005 mg/L
11/28/2023
Heptachlor (TCLP)
SW-846 8081 B
<0.0005 mg/L
11/28/2023
Heptachlor epoxide (TCLP)
SW-846 8081 B
<0.0005 mg/L
11/28/2023
Lindane (TCLP)
SW-846 8081 B
<0.0005 mg/L
11/28/2023
Methoxych►or (TCLP)
SW-846 8081 B
<0.0005 mg/L
11/28/2023
Toxaphene (TCLP)
SW-846 8081 B
<0.05 mg/L
11/28/2023
2,4,5-TP (TCLP)
SW-846 8151 A
<0.003 mg/L
11/29/2023
2,4-D (TCLP)
SW-846 8151 A
<0.003 mg/L
11/29/2023
1,4-Dichlorobenzene (TCLP)
SW-846 8270 E
<0.050 mg/L
11/30/2023
2.4,5-Trichlorophenol (TCLP)
SW-846 8270 E
<0.050 mg/L
11/30/2023
2,4,6-Trichlorophenol (TCLP)
SW 846 8270 E
<0.050 mg/L
11/30/2023
2.4-Dinitrotoluene (TCLP)
SW-846 8270 E
<0.050 mg/L
11/30/2023
Cresol (TCLP)
SW-846 8270 E
<0.050 mg/L
11/30/2023
Hexachloro-1,3-butadiene(TCLP)
SW-8468270E
<0,050mg/L
11/30/2023
Hexachlorobenzene (TCLP)
SW-846 8270 E
<0.050 mg/L
11/30/2023
Hexachloroethane (TCLP)
SW-846 8270 E
<0,050 mg/L
11/30/2023
m + p-Cresol (TCLP)
SW-846 8270 E
<0.050 mg/L
11/30/2023
Nitrobenzene (TCLP)
Sw-846 8270 E
<0.050 mg/L
11/30/2023
o-Cresol (TCLP)
SW-846 8270 E
<0.050 mg/L
11/30/2023
Pentachlorophenol (TCLP)
SW-846 8270 E
<0.250 mg/L
11/30/2023
Pyridine (TCLP)
SW-846 8270 E
<0.050 mg/L
11/30/2023
1,1-Dichloroethylene (TCLP)
SW-846 Method 8260D
< 0.01 mg/L
12/5/2023
1,2-Dichloroethane (TCLP)
SW-846 Method 8260D
< 0.01 mg/L
12/5/2023
Benzene (TCLP)
SW 846 Method 8260D
< 0.01 mg/L
12/5/2023
Carbon Tetrachloride (TCLP)
SW 846 Method 8260D
< 0.01 mg/L
12/5/2023
Report #.; 2023.27165 Page 1 of 4

Environmental Chemists, Inc.
L. envirlthem6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 1 910,347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS info((�environmentalchemists.eoln
Lewis Farms & Liquid Waste, INC.
8155 Malpass Corner Road
Currie NC 28435
Attention:
Date of Report: Dec 21, 2023
Customer PO #:
Customer ID: 14020008
Report #: 2023-27165
Project ID: Hampstead
Chlorobenzene (TCLP)
SW-846 Method 8260D
< 0.01 mg/L
12/5/2023
Chloroform (TCLP)
SW-846 Method 82600
< 0.01 mg/L
12/5/2023
Methyl ethyl ketone (TCLP)
SW-846 Method 8260D
< 0.05 mg/L
12/5/2023
Tetrachloroethylene (TCLP)
SW-846 Method 82601)
< 0.01 mg/L
12/512023
Trichloroethylene (TCLP)
SW-846 Method 8260D
< 0.01 mg/L
12/5/2023
Vinyl Chloride (TCLP)
SW-846 Method 8260D
< 0.01 mg/L
12/5/2023
RCI
Cyanide
SM 4500 CN 0-2016
1.85 mg/kg
12/04/2023
Sulfide
SM 4500 S D-2011
13.3 mglkg
12/06/2023
Ignitability
SW 846 method 1010
>157 °F
11/29/2023
Sludge Residuals
Aluminum
EPA 200.7, Rev 4.4, 1994
10900 mg/kg
11/29/2023
Arsenic
EPA 200.7. Rev. 4.4,1994
21.2 mg/kg
11/29/2023
Cadmium
EPA 200.7, Rev. 4.4,1994
<16.1 mg/kg
11/29/2023
Calcium
EPA 200.7, Rev 4.4,1994
24400 mg/kg
11/29/2023
Chromium
EPA 200.7, Rev 4.4.1994
30.5 mg/kg
11/29/2023
Copper
EPA 200.7, Rev 4.4, 1994
185 mg/kg
11/29/2023
Lead
EPA 200.7, Rev 4.4,1994
<16.1 mg/kg
11/29/2023
Magnesium
EPA 200.7. Rev 4A. 1994
5230 mg/kg
11/29/2023
Molybdenum
EPA 200.7, Rev 4.4. 1994
<16.1 mg/kg
11/29/2023
Nickel
EPA 200.7, Rev. 4.4.1994
<16.1 mg/kg
11/29/2023
Potassium
EPA 200.7. Rev. 4.4, 1994
8480 mg/kg
11/29/2023
Selenium
EPA 200.7. Rev 4A,1994
<16.1 mg/kg
11/29/2023
Sodium
EPA 200.7. Rev 4.4. 1994
3330 mg/kg
11/29/2023
Zinc
EPA 200.7. Rev, 4.4, 1994
787 mg/kg
11/29/2023
Nitrate+Nitrite-Nitrogen
EPA353.2
296mg/kg
11/22/2023
Total Solids (%)
SM 2540 B
3.48 %
11/21/2023
Ammonia Nitrogen
SM 4500 NF13 C-2011
5140 mg/kg
11/21/2023
Total Kjeldahl Nitrogen (TKN)
SM 4500 Norg B-2011
57800 mg/kg
11/21/2023
Total Phosphorus
SM 4500 P (F-H)-2011
31800 m /k9
- -
12/01/2023
Report p: 2023.27165
Page 2 of 4

ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392-0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
[e-mail]
Lewis Farms & Liquid Waste, INC. Date of Report: Dec 21, 2023
8155 Malpass Corner Road Customer PO #:
Currie NC 28435 Customer ID: 14020008
Attention: Report #: 2023-27165
Project ID: Hampstead
pH SW a46 Method 90451) 7.37 units 12/08/2023
Result estimated. Analyzed out of 15 minutes hold time.
Mercury
SW.846 74718
<0.526 mg/kg
11/30/2023
TCLP Metals
Arsenic (TCLP)
EPA 200.7, Rev 4.4, 1994
<1.0 mg/L
11/29/2023
Barium (TCLP)
EPA 2007, Rev 4.4, 1994
<1.0 mg/L
11/29/2023
Cadmium (TCLP)
EPA 200.7, Rev 4.4. 1994
<1.0 mg/L
11/29/2023
Chromium (TCLP)
EPA 200.7, Rev 4.4, 1994
<1.0 mg/L
11/29/2023
Lead (TCLP)
EPA 200.7, Rev 4.4. 1994
<1.0 mg/L
11/29/2023
Selenium (TCLP)
EPA 200.7, Rev 4.4. 1994
<1.0 mg/L
11/29/2023
Silver (TCLP)
EPA 200.7, Rev. 4.4, 1994
<1.0 mg/L
11/29/2023
Mercury (TCLP)
EPA 245.1
<0.0002 mg/L
11/29/2023
Lab ID Sample ID:
Collect DatelTime
Matrix Sampled by
23-65817 Site: Sludge
11/20/2023 10:40 AM
Solid/Sludge Kris King
Test
Method
Results Date Analyzed
Total Solids (%)
SM 2540 B
3.52 %
11/21/2023
Fecal Density
SM9221C E-2014
153410 MPN/g
11/20/2023
Lab ID Sample ID:
Collect Date/Time
Matrix Sampled by
23-65818 Site: Sludge
11/20/2023 10,40 AM
Solid/Sludge Kris King
Test
Method
Results Date Analyzed
Total Solids (%)
SM 2540 B
3.54 %
11/21/2023
Fecal Density
SM9221C E-2014
259888 MPN/g
11/20/2023
Lab ID Sample ID:
Collect Date/Time
Matrix Sampled by
23-65819 Site: Sludge
11/20/2023 10:40 AM
Solid/Sludge Kris King
Test
Method
Results Date Analyzed
Total Solids (%)
SM 2540 B
3.34 %
11 /21/2023
Fecal Density
SM 9221C E-2014
479042 MPN/g
11/20/2023
Report #.: 2023-27165 Page 3 of 4

Environmental Chemists, Inc.
(W-i—K40 41AWTI 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
V 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
!�
255-A Wilmington Highway, Jacksonville, NC 28540 - 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS infotbenvironmentalchemists.com
Lewis Farms & Liquid Waste, INC. Date of Report: Dec 21, 2023
8155 Malpass Corner Road Customer PO #:
Currie NC
28435 Customer ID: 14020008
Attention.
Report #: 2023-27165
Project ID: Hampstead
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
23-65820 Site: Sludge
11/20/2023 10:40 AM Solid/Sludge Kris King
Test
Method Results Date Analyzed
Total Solids (%)
SM 2540 8 3.15 % 11/21/2023
Fecal Density
SM 9221C E-2014 507937 MPN/g 11/20/2023
Lab ID Sample ID:
Collect DaterTime Matrix Sampled by
23-65821 Site: Sludge
11/20/2023 10:40 AM Solid/Sludge Kris King
Test
Method Results Date Analyzed
Total Solids (%)
SM 2540 B 3.19 % 11/21/2023
Fecal Density
SM 9221C E-2014 501568 MPN/g 11/20/2023
Lab ID Sample ID:
Collect DatelTime Matrix Sampled by
23-65822 Site: Sludge
11/20/2023 10:40 AM Solid/Sludge Kris King
Test
Method Results Date Analyzed
Total Solids (%)
SM 2540 a 3.32 % 11/21/2023
Fecal Density
SM9221C E-2014 162651 MPN/g 11/20/2023
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
23-65823 Site: Sludge
11/20/2023 10A0 AM Solid/Sludge Kris King
Test
Method Results Date Analyzed
Total Solids (%)
SM 2540 B 3.66 % 11/21/2023
Fecal Density
SM 0221C E-2014 437159 MPN/g 11/20/2023
Comment: Results, e
pt pH, reported on a dry weight basis. pH reported on an as received basis.
Reviewed by:
°
Report p:: 2023-27165 Page 4 of 4

.­­. �„c„iibt, inc., Wilmington, NC Lab #94
Sample Receipt Checklist
6602 Windmill t
Wilmington, NC 28
910.392.0
Client: to � \ t/t l 1 1 1��__ Date.A _ Report Number. _ 2023- 3:1 1 ug—
Receipt of sample: ECHEM Pickup ( Client Delivery ❑
UPS D Fe�IEx ❑ Other ❑
D YES
❑ NO
C N/A
_
Were custody seals present on the cooler?
❑ YES I0
NO
I r, N/A
2. If custody seals were present, were they intact/unbroken?
Original temperature upon receipt ___°C Corrected temperature upon receipt
Ho.o., temperature taken: ❑ Temperature Blank L Against Bottles
IR Gun ID. Thomas Traceable S/N 210886869 IR Gun Correction Factor °C: 0.0
1J. YES
❑ NO
_
3. If temperature of cooler exceeded 6-C, was Project Mgr./QA notified?
s✓' YES
❑ NO
4. Were proper custody procedures (relinquished/received) followed?
r YES 10
NO
5. Were sample ID's listed on the COC?
p YES
10 NO
6. Were samples ID's listed on sample containers?
121 YES 10
NO
7. Were collection date and time listed on the COC?
O YES
10 NO
_
8. Were tests to be performed listed on the COC?
9 YES
I ❑ NO
9. Did samples arrive in proper containers for each test?
O YES
10 NO
10. Did samples arrive in good condition for each test?
C YES
10 NO
_
11. Was adequate sample volume available?'
L, YES
10 NO
12. Were samples received within proper holding time for requested tests?
❑ YES
10 NO
13. Were acid preserved samples received at a pH of <2?
❑ YES
10 NO
J 14. Were cyanide samples received at a pH >12?
❑ YES
❑ NO
J 15. Were sulfide samples received at a pH >9?
❑ YES
❑ NO
116. Were NH3/TKN/Pheno► received at a chlorine residual of <0.5 n-.IL?
❑ YES
10 NO
117. Were Sulfide/Cyanide received at a chlorine residua( of <0.5 m/L?
❑ YES
10 NO
118. Were orthophosphate samples filtered in the field within 15 minutes?
* TOC/Volat.les are pH checked at time of analyse and recorded on the ben:hsheet
** Bacteria samples are checked for Chlorine at time of analysis and recorded on the benchsheet.
Sample Preservation: (Must be completed for any sample(s) incorrectly preserved or with headspace)
Sample(s) were received incorrectly preserved and were adjusted accordingly
by adding (circle one). H;SO_ HNO; HCI NaOH
Time of preservation: If more than one preservative is needed, notate in comments belov,
:C .r_2A 3-2 f °_ :0'r?: q 0-e3e :'e7 S3-ip es Octa - a re.. ia'rC'2 C'
t-2 i:a:e a: f d rc--"t---3'%=-. cy z V. _ ..3; . .'e j Ca!_ a-_ ! —=-
Volatiles Sampte(s) _ were received with headspace
COMMENTS:
DOC. QA.002 Rev 1

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ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Coastal Farins and Residuals, LLC WQ Permit Number: WQ0034806
WWTP Name: Pluris I-Iampstead WWTF NPDES Number: WQ0037287
Monitoring Period: From l/I/2023 To 12/31/2023
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. A (tiute/tent) ❑ Alt B (Allc Treatment) ❑ I Alt. C (Prior Testing)❑
Alt.D (No Prior Test) 1 Process to Further Reduce Pathoeengs ❑
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost ❑
Hcat Dlying ❑
Heat Treatment ❑
Thenno hilic ❑
Beta Ray ❑
Gatunra Ray ❑
Pasteurization ❑
Class B:
Alt. (])Fecal Density -El
Alt. (2) Process to Significantly Reduce Pathogens ❑
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Litne Stabilization ❑ Air Drying ❑
Composting ❑ jAerobic Digestion ❑
Anaerobic Digestion ❑
If applicable to alternative performed (Class A or Class B) complete the
following monitoring data:
Parameter
Allowable Level
in Sludge
Pathogen Density
D y
um er o
Excee-
dences
Frequency
ofAnalysis
Sample
Type
na ynca
Tech -
ninite
Millimurr
Geo. Mean
Maximuni
Units
Fecal Colifortn
2 x 10 to the
6th power
per gram of
total solids
MPN
153,410
320,316
507,937
MPN/g
0
Annual
Grab
SM92210E
CFU
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
(in lieu of fecal
coliform) I
3 MPN per 4 grams
total solid (dry
weight)
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed:
Alt.1 (VS reduction)
❑
Alt. 2 (40-day bench) ❑
Alt. 3 (30-day bench) ❑ lAlt. 4 (Spec. 0, uptake)
❑
Alt. 5 (14-Day Aerobic)
❑
Alt. 6 (Alk. Stabilization ❑
Alt 7 (Drying- Stable) ❑ 1 Alt. 8 (Drying - Unstable)
❑
All. 9 (injection)
[]
Alt. 10 (Incorporation) El
No vector attraction redaction alternatives were performed
❑
CERTIFICATION STATEMENT (please check the appropriate statement)
El "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note
if you check this statement attach an explanation wliy you have not met one or both of the
requirements.)
"This determination has been made tinder my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Kris King, ORC Wesley Wooten, President
Preparer Na1nc and Title_ type o Land Applier Name and Title (if applicable)(type or print)
1 /2/24
Signature of Si nature ofLa APPlier (if applicable) Dat
e
*Preparer is defined in 40 CFR Part 503.9(r) and I SA NCAC 2T . 1102 (26)
DENR FORM PVRF 02T (12/2006)

COASTAL RESIDUALS
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: April 18, 2023
Southeast Brunswick Sanitary District WWTP Permit No. WQ0013200
1.79 % Solids
7.25 pH
Parameter
%
JMg/KgDryWeightE(Mg/Kj
(% x 10,000)
Pounds/Dry Ton
x0.002)
Nitrogen (TKN)
6.730
67,300.000
134.600
Phosphorus
3.730
37,300.000
74.600
Potassium
0.517
5,170.000
10.340
PAN (injected)*
2.503
25,028,200
50.056
PAN (surface)*
2.164
21,638.200
43.276
Ammonia Nitrogen
0.678
6,780.000
13.560
Calcium
2.170
21,700.000
43.400
Calcium Carbonate E .
---
---
---
Magnesium
---
4,300.000
8.600
Sodium
---
2,540.000
5.080
Sulfur
---
---
---
Nitrate N / Nitrite N
---
92.200
0.184
Barium
---
---
---
SAR
1 0.55
Chloride
---
---
---
Iron
---
---
---
Ceiling Conceit.
(Mg/Kg)
Aluminum
---
16,400.00
32.800
Arsenic
---
47.00
0.094
75
Cadmium
---
47.00
0.094
85
Chromium
---
47.000
---
--
Copper
---
216.00
0.432
4,300
Lead
---
47.00
0.094
840
Mercury
---
1.020
0.002
57
Molybdenum
---
47.00
0.094
75
Nickel
---
47.00
0.094
420
Selenium
---
47.00
0.094
100
Zinc
---
804.00
1.608
7,500
Environmental Chemists # 2023-07463
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits
for calculation purposes.

COASTAL FARMS AND RESIDUALS, LLC
WQ0034806
Southeast Brunswick Sanitary District WWTF
04/18/23
89,190
4.9503
04/18/23
41,146
4.6143
04/18/23
68,750
4.8373
04/18/23
28,000
4.4472
04/18/23
40,000
4.6021
04/18/23
72,223 1
4.8587
04/18/23
60,440 1
4.7813
Total 1 33.0911
Average 4.7273
Geometric Mean s53'1 Fecal Coliform MPN / gram
Geometric Mean of Less than 2,000,000 meets Class B - Alternative 1 Pathogen Reduction
requirement.

F"1007-71
%.u,
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 . 910.392,0223 Lab . 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 . 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 . 910.347.5843 Lab/Fax
info c environnlentalchemists.com
Envirolink, Inc. Revised Report: May 12, 2023
PO Box 670 Original Report Date: May 11, 2023
Bailey NC 27807 Report #: 2023-07463
Attention: Customer ID: 16040014
Project ID: SE Brunswick Sanitary
Lab ID Sample ID:
23-18981 Site: SE Bruns Sanitary
Test
Collect Date/Time
4/18/2023 12:00 PM
Method
Matrix Sampled by
Solid/Sludge Stephanie Moore
Results Date Analyzed
Total Organic Carbon (TOC)
e060
321000 mg/kg
04/27/2023
Chlordane (TCLP)
SW-846 8081 e
<0.02 mg/L
04/24/2023
Endrin (TCLP)
SW-846 8081 8
<0.0005 mg/L
04/24/2023
Heptachlor (TCLP)
SW-848 80818
<0.0005 mg/L
04/24/2023
Heptachlor epoxide (TCLP)
SW-846 8081 8
<0.0005 mg/L
04/24/2023
Lindane (TCLP)
SW-846 8081 8
<0.0005 mg/L
04/24/2023
Methoxychlor (TCLP)
SW-846 8081 8
<0.0005 mg/L
04/24/2023
Toxaphene (TCLP)
SW-846 80818
<0.05 mg/L
04/24/2023
2,4,5-TP (TCLP)
SW-846 8151 A
<0.003 mg/L
04/25/2023
2,4-D (TCLP)
SW-846 8151 A
<0.003 mg/L
04/25/2023
1,4-Dichlorobenzene (TCLP)
SW-846 8270 E
<0.050 mg/L
04/26/2023
2,4,5-Trichlorophenol (TCLP)
SW-846 8270 E
<0.050 mg/L
04/26/2023
2,4,6-Trichlorophenol (TCLP)
SW-846 8270 E
<0.050 mg/L
04/26/2023
2,4-Dinitrotoluene (TCLP)
SW-846 8270 E
<0.050 mg/L
04/26/2023
Cresol (TCLP)
SW-846 8270 E
<0.050 mg/L
04/26/2023
Hexachloro-1,3-butadiene (TCLP)
SW446 8270 E
<0.050 mg/L
04/26/2023
Hexachlorobenzene (TCLP)
SW-848 8270 E
<0.050 mg/L
04/26/2023
Hexachloroethane (TCLP)
SW848 $270 E
<0.050 mg/L
04/26/2023
m + p-Cresol (TCLP)
SW-646 8270 E
<0.050 mg/L
04/26/2023
Nitrobenzene (TCLP)
SW-846 8270 E
<0.050 mg/L
04/26/2023
o-Cresol (TCLP)
SW-846 6270 E
<0.050 mg/L
04/26/2023
Pentachlorophenol (TCLP)
SW-846 8270 E
<0.250 mg/L
04/26/2023
Pyridine (TCLP)
SW-846 8270 E
<0.050 mg/L
04/26/2023
1,1-Dichloroethylene (TCLP)
SW-846 Method8260D
<0.01 mg/L
04/28/2023
1,2-Dichloroethane (TCLP)
SW-646 Method 8260D
<0.01 mg/L
04/28/2023
Benzene (TCLP)
SW-846 Method 8260D
<0.01 mg/L
04/28/2023
Report #:: 2023-07463
Page 1 of 5

Environmental Chemists, Inc.
envirochem 6602 Windmill Way, Wilmington, NC 28405 v 910.392.0223 Lab • 910.392.4424 Fax
f? 710 Bowsertown Road, Manteo, NC 27954 . 252.473.5702 Lab,/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS info(genvironmentalchemists.com
Envirolink, Inc. Revised Report: May 12, 2023
PO Box 670 Original Report Date: May 11, 2023
Bailey NC 27807 Report ##: 2023-07463
Attention: Customer ID: 16040014
Project ID: SE Brunswick Sanitary
Carbon Tetrachloride (TCLP)
SW-846 Method 8260D
<0.01 mg/L
04/28/2023
Chlorobenzene (TCLP)
SW-846 Method 8260D
<0.01 mg/L
04/28/2023
Chloroform (TCLP)
SW-84e Method 8260D
<0.01 mg/L
04/28/2023
Methyl ethyl ketone (TCLP)
SW-846 Method 8260D
<0.05 mg1L
04/28/2023
Tetrachloroethylene (TCLP)
SW-846 Method 8260D
<0.01 mg/L
04/28/2023
Trichloroethylene (TCLP)
SW-846 Method 8260D
<0.01 mg/L
04/28/2023
Vinyl Chloride (TCLP)
SW-846 Method 82600
<0.01 mg/L
04/28/2023
RCI
Cyanide
SM 4500 ctv 0-2016
1.60 mg/kg
04/19/2023
Sulfide
SM 4500 s D
4.30 mg/kg
04/24/2023
Ignitability
SW 846 method 1010
>158 °F
04/18/2023
pH
SW 846 Method 9045D
7.25 units
04/24/2023
Sludge Residuals
Aluminum
EPA 200.7, Rev. 4.4. 1994
16400 mg/kg
04/26/2023
Arsenic
EPA 200.7, Rev. 4.4, 1994
<47.0 mg/kg
04/26/2023
Cadmium
EPA 200.7. Rev. 4.4, 1994
<47.0 mg/kg
04/26/2023
Calcium
EPA 200.7. Rev. 4.4, 1994
21700 mg/kg
04/26/2023
Chromium
EPA 200.7. Rev. 4.4, 1994
<47.0 mg/kg
04/26/2023
Copper
EPA 200.7, Rev. 4.4,1094
216 mg/kg
04/26/2023
Lead
EPA 200.7, Rev. 4.4, 1994
<47.0 mg/kg
04/26/2023
Magnesium
EPA 200.7, Rev. 4.4, 1994
4300 mg/kg
04/26/2023
Molybdenum
EPA 200.7, Rev. 4.4. 1994
<47.0 mg/kg
04/26/2023
Nickel
EPA 200.7, Rev. 4.4. 1994
<47.0 mg/kg
04/26/2023
Potassium
EPA 200.7, Rev. 4.4, 1994
5170 mg/kg
04/26/2023
Selenium
EPA 200.7, Rev. 4.4, 1994
<47.0 mg/kg
04/26/2023
Sodium
EPA 200.7. Rev. 4.4. 1994
2540 mg/kg
04/26/2023
Zinc
EPA 200.7, Rev. 4.4. 1994
804 mg/kg
04/26/2023
Nitrate+Nitrite-Nitrogen
EPA 353.2
92.2 mg/kg
04/20/2023
Total Solids (%)
SM 2540 8
1.79 %
04/18/2023
Report #:: 2023-07463
Page 2 of 5

ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 - 910.347.5843 Lab/Fax
info(41.environmentalchemists.com
Envirolink, Inc.
PO Box 670
Bailey NC
Attention:
27807
Revised Report: May 12, 2023
Original Report Date: May 11, 2023
Report #: 2023-07463
Customer ID: 16040014
Project ID: SE Brunswick Sanitary
Ammonia Nitrogen
SM 4500 NH3 C-2011
6780 mg/kg
04/20/2023
Total Kieldahl Nitrogen (TKN)
SM 4500 Norg 8-2011
67300 mg/kg
04/20/2023
Total Phosphorus
SM 4500 P (F-H).2011
37300 mg/kg
04/27/2023
Mercury
SW-846 7471 B
<1.02 mg/kg
04/27/2023
TCLP Metals
Arsenic (TCLP)
EPA 200.7, Rev 4.4, 1994
<1.0 mg/L
04/26/2023
Barium (TCLP)
EPA 200.7, Rev 4.4, 1994
<1.0 mg/L
04/26/2023
Cadmium (TCLP)
EPA 200.7, Rev. 4.4, 1994
<1.0 mg/L
04/26/2023
Chromium (TCLP)
EPA 200.7, Rev. 4.4, 1994
<1.0 mg/L
04/26/2023
Lead (TCLP)
EPA 200.7, Rev. 4.4, 1994
<1.0 mg/L
04/26/2023
Selenium (TCLP)
EPA 200.7. Rev 4 4,1994
<1.0 mg/L
04/26/2023
Silver (TCLP)
EPA 200.7. Rev 4.4. 1994
<1.0 mg/L
04/26/2023
Mercury (TCLP)
EPA 245 1
<0.0002 mg/L
04/27/2023
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
23-18986 Site: 1
4/18/2023
12:05 PM Solid/Sludge Stephanie Moore
Test
Method
Results Date Analyzed
Total Solids (%)
Fecal Density
Lab ID Sample ID:
23-18987 Site:2
Test
Total Solids (%)
Fecal Density
SM 2540 B
SM 9221C E-2014
1.85 % 04/18/2023
89190 MPN/g 04/18/2023
Collect DatelTime Matrix Sampled by
4/18/2023 12:06 PM Solid/Sludge Stephanie Moore
Method Results Date Analvzed
SM 2540 B
SM 9221C E-2014
1.92 % 04/18/2023
41146 MPN/g 04/18/2023
Report a:: 2023-07463 Page 3 of 5

envirochem
NMi
ANALYTICAL & CONSULTING CHEMISTS
F"007 —:,oq7
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab . 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 . 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
[e-mail]
Envirolink, Inc.
Revised Report: May 12, 2023
PO Box 670
Original Report Date: May 11, 2023
Bailey NC
27807 Report #:
2023-07463
Attention:
Customer ID: 16040014
Project ID:
SE Brunswick Sanitary
Lab ID Sample ID:
Collect Date/Time
Matrix Sampled by
23-18988 Site: 3
4/18/2023 12:07 PM
Solid/Sludge Stephanie Moore
Test
Method
Results Date Analyzed
Total Solids (%)
SM 2540 B
1.60 % 04/18/2023
Fecal Density
SM 9221C E-2014
68750 MPN/g 04/18/2023
Lab ID Sample ID:
Collect Date/Time
Matrix Sampled by
23-18989 Site: 4
4/18/2023 12:08 PM
Solid/Sludge Stephanie Moore
Test
Method
Results Date Analyzed
Total Solids (%)
SM 2540 B
1.75 % 04/18/2023
Fecal Density
SM 9221C E-2014
28000 MPN/g 04/18/2023
Lab ID Sample ID:
Collect Date/Time
Matrix Sampled by
23-18990 Site: 5
4/18/2023 12.-09 PM
Solid/Sludge Stephanie Moore
Test
Method
Results Date Analyzed
Total Solids (%)
SM 2540 B
1.75 % 04/18/2023
Fecal Density
SM 9221C E-2014
40000 MPN/g 04/18/2023
Lab ID Sample ID:
Collect Date/Time
Matrix Sampled by
23-18991 Site: 6
4/18/2023 12:10 PM
Solid/Sludge Stephanie Moore
Test
Method
Results Date Analyzed
Total Solids (%)
SM 2540 B
1.80 % 04/18/2023
Fecal Density
SM 9221C E-2014
72223 MPN/g 04/18/2023
Lab ID Sample ID:
Collect Date/Time
Matrix Sampled by
23-18992 Site: 7
4/18/2023 12:11 PM
Solid/Sludge Stephanie Moore
Test
Method
Results Date Analyzed
Total Solids (%)
SM 2540 B
1.82 % 04/18/2023
Fecal Density
SM 9221C E-2014
60440 MPN/g 04/18/2023
Report #:: 2023.07463
Page 4 or 5

ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
[e-mail]
Envirolink, Inc. Revised Report: May 12, 2023
PO Box 670 Original Report Date: May 11, 2023
Bailey NC 27807 Report #: 2023-07463
Attention: Customer ID: 16040014
Project ID: SE Brunswick Sanitary
Comment:
Reviewed by:
Sludge residuals, TOC, and Fecal Density - reported on a dry weight basis. Revised to amend
project ID.
Report #:: 2023.07463 Page 5 of 5

Analytical Environmental Services, Inc
Date: 27-Apr-23
Client: Environmental Chemists, Inc. Client Sample ID: 23.18981
ProJect Name: 23.18981 Collection Date: 4r1912023 12:00:00 PM
Lab ID: 2304M92-001 Matrix: Sludgc
Analyses Result mvpurung Qual Units BatchlD Dilution Date Analyzed Analyst
Limit Factor
Total Organic Carbon In Soil SW9060 (SW9060 Modified)
Total Organic Carbon (TOQ 321000 2000 mg Ka -dry 355192 1 047712023 11.23 AY
Qrlllfknl V"W cactedf tuaur cwunww kVd
SRL e�{mc rcyvntryt htret
It Holdmr lia" C. prrpvuwn a anilyar ercetdcd
N' AnUyk not \LLAC cen,R d
a Arulyh dt«ted to Iha a ,wd mcdwd W.,
' Grvartr than A -A •�1w
k Lu-m d0.kh abocc 9oortt�atwn nnYcl
S Spkc aawn o"- hmai doe to rtutnx
lean 5cttoon wnt
h A-4zed m tlk bb iwkh a a d,.t— hom the method
• Lot rhrn R"Wr blue
1 Lrum dIII- &-Wcwd bebw ltmonrr L~
Page 4 of 7

Environmental Chemist, Inc., Wilmington, NC Lab #94
Sample Receipt Checklist
6602 Windmill Way
Wilmington, NC 28405
910,392.0223
Client:_ Fhb% + I n K Date: ( Ci(Z3 Report Number: Z3 ~ a ��V
Receipt of sample: Echem Pick up ❑ Client Delivery UPS ❑ FeclEx ❑ Other ❑
❑ YES
10 NO
JJ& N/Al
11. Were custody seals present on the cooler?
O YES
10 NO
115 N/Al
12. If custody seals were present, were they Intact/unbroken?
Original temperature upon receipt X'C Corrected temperature upon receipt 'C
How temperature taken: ❑ Temperature Blank Against Bottles
IR Gun ID:
Thomas Traceable S/N 192511657 IR Gun Correction Factor'C: 0.0
❑ YES
❑ NO
3. If temperature of cooler exceeded 6'C, was Project Mgr./CIA notified?
O NO
4. Were proper custody procedures (relinquished/received) followed?
VY
❑ NO
S. Were sample ID's listed on the COC?
❑ NO
6. Were samples ID's listed on sample containers?
51 YES
O NO
7. Were collection date and time listed on the COC?
YES
❑ NO
8. Were tests to be performed listed on the COC?
YES
❑ NO
9. Did samples arrive In proper containers for each test?
YES
O NO
10. Did samples arrive in good condition for each test?
fil YES
❑ NO
11. Was adequate sample volume available?'
14 YES
❑ NO
12. Were samples received within proper holding time for requested tests?
❑ YES
❑ NO
13. Were acid preserved samples received at a pH of <2?
❑ YES
❑ NO
14. Were cyanide samples received at a pH >12?
❑ YES
❑ NO
15. Were sulfide samples received at a pH >9?
❑ YES
❑ NO
16. Were NH3/TKN/Phenol received at a chlorine residual of <0.5 m/L? ••
❑ YES
❑ NO
17. Were Sulfide/Cyanide received at a chlorine residual of <0.5 m/L?
O YES
❑ NO
18. Were orthophosphate samples filtered in field within 15 minutes?
TOC/Volatiles are pH checked at time of analysis and recorded on the benchsheet.
•* Bacteria samples are checked for Chlorine at time of analysis and recorded on the benchsheet.
Sample Preservation (Must be completed for any sample(s) incorrectly preserved or with headspace)
Sample(s) were received incorrectly preserved and were adjusted accordingly
by adding (circle one): H2SO4 HNO3 HCI NaOH
Time of preservation: If more than one preservative is needed, notate in comments below
Note: Notify customer service immediately for incorrectly preserved samples. Obtain a new sample or
notify the state lab If directed to analyzed by the customer. Who was notified, date and time:
Volatiles Sample(s) were received with headspace
COMMENTS:
DOC.OA.002 Rev 1

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ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Coastal Fauns and Residuals, LLC WQ Permit Number: 1VQ0034806
WWTP Name: Southeast Brunswick Sanitary District W VTP NPDES Number: WQ0013200
Monitoring Period: From 1/1/2023 Ta 12/31/2023
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level nrhtwrrt nna nitwrn"tiasw nwrfnrmn`i•
Class A:
Alt. A (time/temp) ❑ Alt B (Alk Treatment) ❑ Alt. C (Prior Testing) ❑
AILD (No Prior Test) ❑ Process to Further Reduce Pathogengs ❑
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost ❑
Heat Drying ❑
Heat Treatment ❑
Thennophilic ❑
Beta Ray ❑
Gamma Ray ❑
Pasteurization ❑
Class B:
jAlt. (1) Fecal Density p
Alt_ (2) Process to Siganificantly Reduce Pathogens ❑
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization ❑ Air Drying ❑ Composting ❑ jAerobic Digestion ❑
Anaerobic Digestion ❑
If applicable to alternative performed (Class A or Class B) complete the
following monitoring data:
Parameter
Allowable Level
in Sludge
Pathogen)
Density
Number ot
'
dene q
Frequency
of Analysis
Sample
Type
Analytical
ytica
nich-
cue
Minimurr
Geo. Mean
Maximu
Units
Fecal Colifonn
2 x 10 to the
6th power
per gram of
total solids
MPN
25,000
53,371
59,190
MPN/g
0
Annual
Grab
SM92210E
CFU
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
(in lieu of fecal
coliform)
r
3 NIPN per 4 grams
total solid (dry
weight)
v ector Attraction Reduction (15A NCAC U21 .1107) -Please indicate alternative nerformed:
Alt.l (VS reduction) ❑
Alt. 2 (40-day bench) ❑
JAR. 3 (3aybench) ❑
JAR. 4 (Spec. 0, uptake) ❑
Alt. 5 (14-Day Aerobic) ❑
Alt. 6 (Alk. Stabilization ❑
jAlt 7 (Drying - Stable) ❑
I Alt. 8 (Drying - Uns(able) ❑
Alt. 9 (Injection) Ej
Alt. 10 (Incorporation) p
INo vector attraction reduction alteniatives were performed ❑
%-nis r tl x%-&jL WN S i Ai L, IWE N 1 (please ciiectc ttie appropriate statement)
0 "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if
you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the systeni
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Stephanie Moore, ORC Wesley Wooten, President
Preparer Nan.Ae and Title (type or print) Land Applier Name and
%Title (if applicable)(type or print)
Signature of Preparer' Date Signature of Land pplier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .l 102 (26)
DENR FORM PVRF 02T (12/2006)

COASTAL RESIDUALS
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: July 26, 2023
Surf Citv WWTP
2.04 % Solids
7.30 pH
Permit No. WQ0000795
Parameter
%
Mg/Kg Dry Weight
(% x 10,000)
Pounds/Dry Ton
(Mg/Kg x 0.002)
Nitrogen (TKN)
6.820
68,200.000
136.400
Phosphorus
1.470
14,700.000
29.400
Potassium
0.410
4,100.000
8.200
PAN (injected)*
2.175
21,753.100
43.506
PAN (surface)*
2.087
20,868.100
41.736
Ammonia Nitrogen
0.177
1,770.000
3.540
Calcium
3.410
34,100.000
68.200
Calcium Carbonate E .
---
---
Magnesium
---
4,060.000
8.120
Sodium
---
9,120.000
18.240
Sulfur
---
_--
---
Nitrate N / Nitrite N
---
54.100
0.108
Barium
---
---
---
SAR
Chloride
---
---
1.77
Iron
---
---
Cg eilin Concen.
Aluminum
---
3,090.00
6.180
(M-/I()
Arsenic
---
40.30
0.081
75
Cadmium
---
31.70
0.063
85
Chromium
---
31.700
0.063
---
Copper
---
348.00
0.696
4,300
Lead
---
31.70
0.063
840
Mercury
- -
0.824
0.002
57
Molybdenum
---
31.70
0.063
75
Nickel
---
31.70
0.063
420
Selenium
---
31.70
0.063
100
Zinc
---
3,380.00
6.760
7,500
Environmental Chemists # 2023-16252
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits
for calculation purposes.

LEWIS FARMS
WQ0000455
Surf City WWTP
07/26/23
16,130
4.2076
07/26/23
15,766
4.1977
07/26/23
23,377
4.3688
07/26/23
15,766
4.1977
07/26/23
11,595
4.0643
07/26/23
14,958
4.1749
07/26/23
10,910
4.0378
Total 29.2488
Average 4.1784
Geometric Mean 15i84 Fecal Coliform MPN / gram
Geometric Mean of Less than 2,000,000 meets Class B - Alternative 1 Pathogen Reduction
requirement.

Environmental Chemists,
Inc.
6602 Windmill Way,
Wilmington, NC 28405 • 910.392.0223 Lab • 910,392.4424
Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5643 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS
[e-mail]
Lewis Farms & Liquid Waste, INC.
Date of Report: Aug 30, 2023
8155 Malpass Corner Road
Customer PO #:
Currie NC 28435
Customer ID: 14020008
Attention:
Report #: 2023-16252
Project ID: Surf City
Lab ID Sample ID:
Collect DatefTime Matrix Sampled by
2340141 Site: Sludge
7/26/2023
7:05 AM Solid/Sludge Mike Hash
Test
Method
Results Date Analyzed
Chlordane (TCLP)
SW-846 8081 8
<0.02 mg/L
08/03/2023
Endrin (TCLP)
SW-846 80818
<0.0005 mg/L
08/03/2023
Heptachlor (TCLP)
SW-846 8081 B
<0.0005 mg/L
08/03/2023
Heptachlor epoxide (TCLP)
SW-846 8081 B
<0.0005 mg/L
08/03/2023
Lindane (TCLP)
SW-846 8081 B
<0.0005mg/L
08/03/2023
Methoxychlor (TCLP)
SW-846 8081 8
<0.0005 mg/L
08/03/2023
Toxaphene (TCLP)
SW-846 8081 B
<0.05 mg/L
08/03/2023
2,4,5-TP (TCLP)
SW-845 6151 A
<0.003 mg/L
08/07/2023
2,4-0 (TCLP)
SW-846 8151 A
<0.003 mg/L
08/07/2023
1,4-Dichlorobenzene (TCLP)
SW-846 8270 E
<0.050 mg/L
08/04/2023
2,4,5-Trichlorophenol (TCLP)
SW-846 8270 E
<0.050 mg/L
08/04/2023
2,4,6-Trich lorophenol (TCLP)
SW-845 6270 E
<0.050 mg/L
08/04/2023
2,4-Dinitrotoluene (TCLP)
SW-846 8270 E
<0.050 mg/L
08/04/2023
Cresol (TCLP)
SW-846 8270 E
<0.050 mg/L
08/04/2023
Hexachloro-1,3-butadiene (TCLP)
SW-848 8270 E
<0.050 mg/L
08/04/2023
Hexachlorobenzene (TCLP)
SW-846 8270 E
<0.050 mg/L
08/04/2023
Hexachloroethane (TCLP)
SW-846 8270 E
<0.050 mg/L
08/04/2023
m + p-Cresol (TCLP)
SW-846 8270 E
<0.050 mg/L
08/04/2023
Nitrobenzene (TCLP)
SW-846 8270 E
<0.050 mg/L
08/04/2023
o-Cresol (TCLP)
SW-646 8270 E
<0.050 mg/L
08/04/2023
Pentachlorophenol (TCLP)
SW-846 8270 E
<0.250 mg/L
08/04/2023
Pyridine (TCLP)
SW-846 8270 E
<0.050 mg/L
08/04/2023
1, 1 -Dichlorcethylene (TCLP)
SW-846 Method 8260D
< 0.01 mg/L
8/15/2023
1,2-Dichloroethane (TCLP)
SW-846 Method8250D
<0.01 mg/L
8/15/2023
Benzene (TCLP)
SW-846 Method 8260D
< 0.01 mg/L
8/15/2023
Carbon Tetrachloride (TCLP)
SW-846 Method 8260D
< 0.01 mg/L
8/15/2023
Report #.: 2023-16252
Page 1 of 5

Environmental Chemists, Inc.
envirochem 1 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab a 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
P 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS [e-mail]
Lewis Farms & Liquid Waste, INC.
Date of Report: Aug 30, 2023
8155 Malpass Corner Road
Customer PO #:
Currie NC 28435
Customer ID: 14020008
Attention:
Report #: 2023-16252
Project ID: Surf City
Chlorobenzene (TCLP)
SW-846 Method 8260D
< 0.01 mg/L
8/15/2023
Chloroform (TCLP)
SW-846 Method 8260D
< 0.01 mg/L
8/15/2023
Methyl ethyl ketone (TCLP)
SW-846 Method 8260D
< 0.05 mg/L
8/15/2023
Tetrachloroethylene (TCLP)
SW-846 Method 8260D
< 0.01 mg/L
8/15/2023
Trichloroethylene (TCLP)
SW-846 Method 8260D
< 0.01 mg/L
8/15/2023
Vinyl Chloride (TCLP)
SW-846 Method 82600
< 0.01 mg/L
8/15/2023
RCI
Cyanide
SM 4500 CN D-2016
2.15 mg/kg
08/09/2023
Sulfide
Analyzed outside of hold time.
SM 4500 S D
1.69 mg/kg
08/12/2023
Ignitability
SW 846 method 1010
>158 °F
08/01/2023
pH
Result estimated. Analyzed out of
SW 846 Method 9045D
15 minutes hold time.
7.30 units
08/23/2023
Sludge Residuals
Aluminum
EPA 200.7, Rev, 4.4,1994
3090 mg/kg
08/02/2023
Arsenic
EPA 200.7, Rev. 4.4, 1994
40.3 mg/kg
08/02/2023
Cadmium
EPA 200.7, Rev. 4.4, 1994
<31.7 mg/kg
08/02/2023
Calcium
EPA 200.7, Rev. 4.4. 1994
34100 mg/kg
08/02/2023
Chromium
EPA 200.7, Rev. 4.4, 1994
<31.7 mg/kg
08/02/2023
Copper
EPA 200.7. Rev. 4.4, 1994
348 mg/kg
08/02/2023
Lead
EPA 200.7. Rev. 4.4, 1994
<31.7 mg/kg
08/02/2023
Magnesium
EPA 200.7. Rev. 4.4, 1994
4060 mg/kg
08/02/2023
Molybdenum
EPA 200.7, Rev. 4.4. 1994
<31.7 mg/kg
08/02/2023
Nickel
EPA 200.7, Rev. 4.4, 1994
<31.7 mg/kg
08/02/2023
Potassium
EPA 200.7. Rev, 4.4, 1994
4100 mg/kg
08/02/2023
Selenium
EPA 200.7, Rev. 4.4, 1994
<31.7 mg/kg
08/02/2023
Sodium
EPA 200.7, Rev. 4.4. 1994
9120 mg/kg
08/02/2023
Zinc
EPA 200.7. Rev. 4.4. 1994
3380 mg/kg
08/02/2023
Nitrate+Nitrite-Nitrogen
EPA353.2
54.1 mg/kg
08/02/2023
Total Solids (%)
SM 2540 s
2.04 %
07/27/2023
Report a:: 2023.16252 Page 2 of 6

Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
L.u, 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
' 255-A Wilmington Highway, Jacksonville, NC 28540 , 910.347.5%M3 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS info`a)environmentalchemists com
Lewis Farms & Liquid Waste, INC.
Date of Report: Aug 30, 2023
8155 Malpass Corner Road
Customer PO #:
Currie NC 28435
Customer ID: 14020008
Attention:
Report #: 2023-16252
Project ID: Surf City
Ammonia Nitrogen
SM 4500 NH3 C-2011
1770 mg/kg
07/30/2023
Total Kjeldahl Nitrogen (TKN)
SM 4500 Norg B-2011
68200 mg/kg
08/01/2023
Total Phosphorus
SM 4500 P (F-H)-2011
14700 mg/kg
08/10/2023
Mercury
SW-e46 7471 B
<0.824 mg/kg
07/31/2023
TCLP Metals
Arsenic (TCLP)
EPA 200.7, Rev. 4.4, 1994
<1.0 mg/L
08/09/2023
Barium (TCLP)
EPA 200.7, Rev, 4.4. 1994
<1.0 mg/L
03/09/2023
Cadmium (TCLP)
EPA 2003, Rev. 4.4, 1994
<1.0 mg/L
08/09/2023
Chromium (TCLP)
EPA 200.7, Rev 44, 1994
<1.0 mg/L
08/09/2023
Lead (TCLP)
EPA 2007, Rev 4.4, 1994
<1.0 mg/L
08/09/2023
Selenium (TCLP)
EPA 200.7, Rev 4,4, 1994
<1.0 mg/L
08/09/2023
Silver (TCLP)
EPA 200.7. Rev 4.4, 1994
<1.0 mg/L
08/09/2023
Mercury (TCLP)
EPA 245.1
<0.0002 mg/L
08/03/2023
Lab ID Sample ID:
Collect Date/Time
Matrix Sampled by
23-40142 Site: Sludge 1
7/26/2023 T10 AM
Solid/Sludge Mike Hash
Test
Method
Results Date Analyzed
Total Solids (%)
SM 2540 5
2.17 % 07/27/2023
Fecal Density
SM 9221C E-2014
16130 MPN/g 07/26/2023
Lab ID Sample ID:
Collect Date/Time
Matrix Sampled by
23-40143 Site: Sludge 2
7/26/2023 7:10 AM
Solid/Sludge Mike Hash
Test
Method
Results Date Analyzed
Total Solids (%)
SM 2540 B
2.22 % 07/27/2023
Fecal Density
SM 9221C E-2014
15766 MPN/g 07/26/2023
Report #:: 2023-16252 Page 3 of 5

Environmental Chemists, Inc.
' i 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS [e-mail]
Lewis Farms & Liquid Waste, INC. Date of Report: Aug 30, 2023
8155 Malpass Corner Road
Customer PO #:
Currie NC 28435
Customer ID: 14020008
Attention:
Report #: 2023-16252
Project ID: Surf City
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
23-40144 Site: Sludge 3
7/26/2023 7:10 AM Solid/Sludge Mike Hash
Test
Method Results Date Analyzed
Total Solids (%)
SM 2540 B 2.31 % 07/27/2023
Fecal Density
SM 9221C E-2014 23377 MPN/g 07/26/2023
Lab ID Sample ID:
Collect DatelTime Matrix Sampled by
23-40145 Site: Sludge 4
7/26/2023 7:10 AM Solid/Sludge Mike Hash
Test
Method Results Date Analyzed
Total Solids (%)
SM 2540 B 2.22 % 07/27/2023
Fecal Density
SM 9221C E-2014 15766 MPN/g 07/26/2023
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
23-40146 Site: Sludge 5
7/26/2023 7:10 AM Solid/Sludge Mike Hash
Test
Method Results Date Analyzed
Total Solids (%)
SM 2540 B 2_07 % 07/27/2023
Fecal Density
SM 9221C E-2014 11595 MPN/g 07/26/2023
Lab ID Sample ID:
Collect DatelTime Matrix Sampled by
23-40147 Site: Sludge 6
7/2612023 7:10 AM Solid/Sludge Mike Hash
Test
Method Results Date Analyzed
Total Solids (%)
SM 2540 B 2.34 % 07/27/2023
Fecal Density
SM 9221C E-2014 14958 MPN/g 07/26/2023
Lab ID Sample ID:
Collect DatelTime Matrix Sampled by
23-40148 Site: Sludge 7
7/26/2023 7:10 AM Solid/Sludge Mike Hash
Test
Method Results Date Analyzed
Total Solids (%)
SM 2540 B 2.20 % 07/27/2023
Fecal Density
SM 9221C E-2014 10910 MPN/g 07/26/2023
Report k: 2023-165252
Page 4 of 5

6e�nvirochem
ANALYTICAL & CONSULTING CHEMISTS
Lewis Farms & Liquid Waste, INC.
8155 Malpass Corner Road
Currie NC 28435
Attention:
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
Comment: Sludge residuals reported on a dry weight basis.
Reviewed by: i
[e-mail]
Date of Report: Aug 30, 2023
Customer PO #:
Customer ID: 14020008
Report #: 2023-16252
Project ID: Surf City
teport #:: 2023-16252
Page 5 of 5

Environmental Chemist, Inc., Wilmington, NC Lab #94
Client: Sample Receipt Checklist
�-f_�J
- —,� Date: Report Number
6602 Windmill Way
Wilmington, NC 2840S
910.392.0223
_ 2023- I�L a
Receipt of sample: ECHEM Picku Client Delivery O UPS ❑ FedEx ❑ Other ❑
❑ YES ❑ NO D N/A 1. Were custody seals present on the cooler?
❑ YES ❑ NO ❑D N/A 2. If custody seals were present, were they intact/unbroken?
Original temperature upon receipt
w
°C Corrected temperature upon receipt °C
How temperature taken:
❑ Temperature Blank D Against Bottles
IR Gun ID: Thomas Traceable S/N 210886869 IR Gun Correction Factor °C: 0.0
D
YES
❑
NO
3. If temperature of cooler exceeded 6°C, was Project Mgr./QA notified?
�
YES
❑
NO
4. Were proper custody procedures (relinquished/received) followed?
D
YES
❑
NO
S. Were sample ID's listed on the COC?
D
YES
❑
NO
6. Were samples ID's listed on sample containers?
CJ
YES
❑
NO
7. Were collection date and time listed on the COC?
D
YES
❑
NO
8. Were tests to be performed listed on the COC?
❑D
YES
❑
NO
9. Did samples arrive in proper containers for each test?
D
YES
❑
NO
10. Did samples arrive in good condition for each test?
D
YES
❑
NO
11. Was adequate sample volume available?'
D
Y
O
NO
12. Were samples received ;4
NO
proper holding time for requested tests?
13. Were acid preserved samples received at a pH of <27
❑
❑ NO
14. Were cyanide samples received at a pH >12?
❑ YES
❑ NO
15. Were sulfide samples received at a pH >9?
❑ YES
❑ NO
16. Were NH3/TKN/Phenol received at a chlorine residual of <0.5 m/L? **
❑ YES
❑ NO
17. Were Sulfide/Cyanide received at a chlorine residual of <0.5 m/L?
❑ YES
❑ NO
18. Were orthophosphate samples filtered in the field within 15 minutes?
* TOC/Volatiles are pH checked at time of analysis and recorded on the benchsheet.
** Bacteria samples are checked for Chlorine at time of analysis and recorded on the benchsheet
Sample Preservation: (Must be completed for any sample(s) incorrectly preserved or with headspace)
Sample(s) were received incorrectly preserved and were adjusted accordingly
by adding (circle one): H2SO4 HNO3 HCl NaOH
Time of preservation: If more than one preservative is needed, notate in comments below
Note: Notify customer service immediately for incorrectly preserved samples. Obtain a new sample or
notify the state lab if directed to analyzed by the customer. Who was notified, date and time:
Volatiles Sample(s) were received with headspace
COMMENTS:
DOC. QA.002 Rev 1

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ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Coastal Farms and Residuals, LLC WQ Permit Number: WQ0034806
WWTP Name: SurfCity WWTP NPDES Number: WQ0000795
Monitoring Period: From 1/1/2023 To 12/31/2023
Pathogen Reduction (15A NCAC 02T .1106) - Please inrlionta Invnl .,,.t,mat-4 ,,.,a ,p� . , 4 _r_ _ .r-
Class A:
Alt. A (time/temp) ❑
�+ nauvc �Jcllul r"cu.
Alt B (Alk Treatment) ❑ Alt. C (Prior Testing) El
AIt.D (No Prior Test) Elgs Process to Further Reduce Pathogen ❑
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost 01 Heat Drying ❑ Heat Treatment ❑ Thennophilic ❑
Beta Ray 01 Gamma Ray ❑ Pasteurization ❑
'
Class B: JAR. (1) Fecal Density p Alt. (2) Process to Si tificantly Reduce Pathogens ❑
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization ❑ Air Di ing ❑ Composting ❑ Aerobic Digestion El,
Anaerobic Digestion .....................................
If apica ble to
plicable
pp alternative performed (Class A or Class B) complete the
following monitoring data:
Parameter
Allowable Level
Pathogen Density
um er o
Frequency
Sample
Analytical
in
in Sludge
Minimu
Geo. Mean
Maximu
Units
Excee-
dences
of Analysis
Type
Tech -
i otie
2 x 10 to the
6th power
MPN
10,910
15,080
23,377
MPN/g
0
Annual
Grab
sM92210E
per gram of
Fecal Coliform
total solids
CFU
1000 mpn per gram
oftotal solid (dry
weight)
Salmonella bacteria
3 MPN per 4 grams
(in lieu of fecal
total solid (dry
coliform)
weialit)
VPrtnr Aftr7rfinn
T2 n.lnnt: flCA
Ar/1Arl A.m
Lynn.
ram.
Alt. I (VS reduction) ❑
Alt. 2 (40-day bench) ❑
Alt. 3 (30-day bench) ❑Alt. 4 (Spec. O, uptake) ❑
Alt. 5 (14-Day Aerobic) ❑
Alt. 6 (Alk. Stabilization ❑
Alt 7 (Drying - Stable) ❑ Alt. 8 (Drying - Unstable) ❑
Alt. 9 (Injection) l7
Alt. 10 (Incorporation) Q
No vector attraction reduction alternatives were perfornied ❑
Or DTf Pff- A mrllAr c1111 ♦ minn,r,r,,.,.r
.
—U 111'1\..L111V 1 o 1 A I L' 1YIEN J. tprease check the appropriate statement)
El "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vec
tor attraction reduction requirement in 15A NCAC 02T .1107 have been met."
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if
you check this statement attach an explanation why you have not met one or bout of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Zachary Butler, ORC Wesley Wooten, President
Preparer Name and Title (type or print) Land Applier Name and Title (if applicable)(type or print)
�� l�cd�eti 9/8/23 9/5/23
Sigri'dture of P parer* Date Signature of Lan Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 02T (12/2006)

2023 APPLICATION SUMMARY

COASTAL FARMS AND RESIDUALS, LLC
Permit # WQ 0034806
2023
RESIDUALS APPLICATIONS
Metric Tons 455.18

FIELD LOADING RATE REPORTS

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