WQ0013263_2023 Residual Annual Report_20240201 (2)

Initial Review
Reviewer
nathaniel.thorn burg
Is this submittal an application? (Excluding additional information.) *
Yes No
If not an application what is the submittal type?* Annual Report
Residual Annual Report
Additional Information
Other
Annual Report Year* 2023
Permit Number (IR) * WQ0013263
Applicant/Permittee Town of Boone
Email Notifications
Does this need review by the hydrogeologist? * Yes U No
Regional Office Winston-Salem
CO Reviewer
Admin Reviewer [e-mail]

Submittal Form
Project Contact Information
Please provide information on the person to be contacted by NDB Staff regarding electronic submittal, confirmation of receipt, and other correspondence.
Name* Kenneth Howell
Email Address*
Kenneth. [e-mail]
Project Information
.........................
Application/Document Type*
New (Fee Required)
Modification - Major (Fee Required)
Renewal with Major Modification (Fee
Required)
Annual Report
Additional Information
Other
Phone Number*
828-268-6270
Modification - Minor
Renewal
GW-59, NDMR, NDMLR, NDAR-1,
N DAR-2
Residual Annual Report
Change of Ownership
We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form.
https://edoes.deq.nc.gov/Forms/NonDischarge_Monitoring_Report
Permit Type:*
Wastewater Irrigation
High -Rate Infiltration
Other Wastewater
Reclaimed Water
Closed -Loop Recycle
Residuals
Single -Family Residence Wastewater
Other
Irrigation
Permit Number:*
WQ0013263
Has Current Existing permit number
Applicant/Permittee Address*
201 Casey LAner Boone, NC 28605
Facility Name*
Town of Boone Class A Residuals Program
Please provide comments/notes on your current submittal below.
At this time, paper copies are no longer required. If you have any questions about what is required, please contact Nathaniel Thornburg
at [e-mail].
Please attach all information required or requested for this submittal to be reviewed here.
(Application Form, Engineering Plans, Specifications, Calculations, Etc.)
2023 Annual Report.pdf 2.86MB
Upload only 1 PDF document (less than 250 MB). Multiple documents must be combined into one PDF file unless file is larger
than upload limit.
* By checking this box, I acknowledge that I understand the application will not be accepted for pre -review until the fee (if required) has
been received by the Non -Discharge Branch. Application fees must be submitted by check or money order and made payable to the
North Carolina Department of Environmental Quality (NCDEQ). I also confirm that the uploaded document is a single PDF with all parts
of the application in correct order (as specified by the application).
Mail payment to:
NCDEQ — Division of Water Resources
Attn: Non -Discharge Branch
1617 Mail Service Center
Raleigh, NC 27699-1617
Signature
Submission Date 2/1/2024

1/31/23
Land Application Unit
1636 Mail Service Center
Raleigh, NC 27699-1636
Attached is the Town of Boone's 2023 Class A residuals program annual report.
Our system employs a thermal drier by a natural gas steam generator. Heat is transferred
to the residuals through a hollow rotor via a series of concentric disks in the drier. The
system is manufactured by Atlas-Stord, Inc. The enclosed report includes a technical
specifications section for your reference.
To assist your review, we have included summaries on production volume, the quantity
distributed, and information on each recipient.
We tested for quarterly for metals and fecal coliform . All of our test results were within
our permitted requirements.
We will promptly provide any additional records you may request to verify compliance
of this system with the regulations for Class A residuals distribution. If there is any need,
please contact me at [phone].
Sincerely,
Kenneth Howell
Senior Operator
cc: Rudy Broschinski, Wastewater Treatment Superintendent
Todd Moody, Director of Public Utilities

ANNUAL DISTRIBUTION AND MARKETING/SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM
FACILITY NAME: Town of Boone Jimmy Smith WWTP PERMIT #: WQ0013263 COUNTY: Watauga
FACILITY TYPE(please check one): = Surface Disposal (complete Part A (Sources(s) and "Residual IN" Volume Only) and Part C)
Distribution and Marketing (complete Parts A,B, and C)
WAS THE FACILITY IN OPERATION DURING THE PAST CALENDAR YEAR? YES X NO If NO, skip Parts A,13,and C and certify form below.
Part A*
Part B*
Month
Sources
(Include NPDES # if applicable)
Volume
Recipient Information
Amendment/
Balding Agent IN
Residual IN
Product OUT
Name(s) Volume Intended Use(s)
(dry tons)
January
Town of Boone Permit # NCO020621
None
***
83.87
36.0
February
Town of Boone Permit # NCO020621
None
69.56
Please see attachment for
163.8
Please see attachment
March
Town of Boone Permit # NCO020621
None
61.45
recipient information on
196.50
April
Town of Boone Permit # NCO020621
None
77.50
a monthly basis.
0.0
May
Town of Boone Permit # NCO020621
None
63.86
128.75
June
Town of Boone Permit # NCO020621
None
35.70
0.0
July
Town of Boone Permit # NCO020621
None
85.99
0.0
August
Town of Boone Permit # NCO020621
None
57.85
0.0
September
Town of Boone Permit # NCO020621
None
108.83
62.8
October
Town of Boone Permit # NCO020621
None
105.39
0.00
November
Town of Boone Permit # NCO020621
None
70.52
39.5
December
Town of Boone Permit # NCO020621
None
44.98
1
15.0
Totals:
Annual (dry tons)
865.50
642.4
Amendment(s) used: None Bulking Agent(s) used: None
*If more space is required than geiven, please use the comment space provided below or attach additional sheet(s).
Comments:
Part C
Facility was compliant during calendar year 2023 with all conditions of the permit (including but not limited to items 1-3 below) issued by the
Division of Water Quality x YES NO. If NO, please provide a written description of why the facility was not compliant.
1. All monitoring was performed in accordance with the permit and reported during the year as required and three (3) copies of certified lab results are attached.
2. All operations and maintenance requirements were compiled with or, in the case of deviation, prior to authorization was received from the Division of Water Quality.
3. No contravention of Ground Water Quality Standards occurred at a monitoring well.
"I CERmT, UNDER PENALTY OF LAW, THAT THE ABOVE INFORMATION IS, TO THE BEST OF MY H1i0WLEDGE AND BELIEF, THE, ACCURATE
AND COMPLETE. I AM AWARE THAT THERE ARE SIGNIFICANT PENALTIES FOR SUBMFPFING FALSE INFORMATION, INCLUDING THE POSSIBILITY OF FINES
AND WESONMENTS FOR HNO G VIOLATIONS." c3, 24-
�--a -z
SIGNATUR PER ITTEE DATE SIGNATURE OF P EPARER DATE
(If different from Permittee) *Preparer is defined in 40 CM Part 503.90

BACKGOUND INFORMATION
1. NAME AND ADDRESS OF FACILITY
Facility Name Town of Boone Jimmy Smith Wastewater Treatment Plant
Address 201 Casey Lane
City Boone State NC Zip 28607
Facility Contact Kenneth Hows Phone [phone]
Signatory
2. NAME AND ADDRESS OF FACILITY OWNER
Facility owner's Name Town of Boone
Address P.O. Box 192
City Boone
State NC Zip 28607
3. REPORTING PERIOD �4. NPDES PERMIT NUMBER
YEAR I MO I DAY IYEARI MO DAY NCO020621
FROM 23 1 1 1 1 TO 23 1 12 31
6. FACILITY STATUS 7. TOTAL ANNUAL VOLUME OF SEWAGE SLUDGE
X Preparer of sewage sludge
Land applier 11 36-0 1 163.8 196.5 2[0.0 1128.81 0.0
Owner/operator of surface disposal site
Owner/operator of incinerator 31 0.0 1 0.0 62.8 41 0.0 1 39.5 15.0
Units: (metric tons; dry weight)
EjOther: drytons
5. SLUDGE PERMIT NUMBER
WQ0013263
8. FINAL USE AND DISPOSAL METHOD
Land application
Surface disposal
Unlined or Lined
Incineration
X Other, explain Bulk Distribution
See cover letter
9. Name and address of persons performing final use or disposal (attach additional sheets if necessary)
Same as preparer
Facility Name
Facility Name
Address
Address
City State Zip
City State Zip
Facility Contact Phone
Facility Contact Phone
Volume of sludge received from preparer
Volume of sludge received from preparer
Final use/disposal method for sludge
Final use/disposal method for sludge
Facility Name
Facility Name
Address
Address
City State Zip
City State Zip
Facility Contact Phone
Facility Contact Phone
Volume of sludge received from preparer
Volume of sludge received from preparer
Final use/disposal method for sludge
Final use/disposal method for sludge
10. CERTIFICATION
I certify under penalty of law that this document and all attachments were prepared umder my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gather and evaluate the information submitted.
Based on my inquiry of the person or persons directly responsible for gathering the information
submitted, it is to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information.
Name and Official Title (type or print)
Area Code and Phone
Kenneth Howell Senior Operator
828 268-6270
Signature
4,� 4L Z:�dz
Date Signed
1-0) -z

CLASS A RESIDUALS POLLUTANT LIMITS
1. NAME AND ADDRESS OF FACILITY
Facility Name Town of Boone Jimmy Smith Wastewater Treatment Plant
Address 201 Casey Lane
T P,O. Box 192
City Boone
Facility Contact
Signatory
State NC Zip 28607
Kenneth Howell Phone [phone]
2. NAME AND ADDRESS OF FACILITY OWNER
Facility owner's Name Town of Boone
Address P.O. Box 192
City Boone
State NC Zip 28607
3. MONITORING PERIOD 4. NPDES PERMIT NUMBER 5. SLUDGE PERMIT NUMBER
YEAR MO DAY F23
EAR MO DAY NCO020621 WQ0013263 (Class A)
FROM 23 1 1 TO 3 31
6. INSTRUCTIONS: Complete the form based on the results of all analyses performed during the monitoring period using approved analytical method.
Complete a separate sheet for each monitoring period during the reporting period.
Parameter
Pollutant Concentration
(dry weight)
Frequency of
Analysis
Sample Type
(Grab or Composite)
Analytical
Method
Avg.
Reg Limit
Units
Potassium
Selenium
Sodium
Zinc
% Total Solids
Ammonia Nitrogen
Nitrate -Nitrite Nitrogen
Total Phosphorous
Total Kjeldahl Nitrogen
pH
PAN
SAR
Sample Measurement
2580
-
MG/KG
1
Grab
EPA 200.7
Sample Measurement
5.6
100
MG/KG
1
Grab
EPA 200.7
Sample Measurement
775
-
MG/KG
1
Grab
EPA 200.7
Sample Measurement
724
2800
MG/KG
1
Grab
EPA 200.7
Sample Measurement
91.5
-
MG/KG
1
Grab
EPA 160.3
Sample Measurement
1470
-
MG/KG
1
Grab
EPA 350.1
Sample Measurement
ND
-
MG/KG
1
Grab
EPA 353.2
Sample Measurement
16100
-
MG/KG
1
Grab
EPA 200.7
Sample Measurement
65000
-
MG/KG
1
Grab
EPA 351.1
Sample Measurement
5.9
-
su
1
Grab
EPA 150.1
NA
19800
-
MG/KG
NA
NA
Calculation
1.7
9.99
NA
1
Grab
EPA-6010
10. CERTIFICATION
I certify under penalty of law that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons directly responsible for gathering the information
submitted, it is to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information.
Name and Official Title (type or print) Area Code and Phone
Kenneth Howell, Senior Operator _1(828)268-6270
Signature 4�- , j 4� jDate Signed pof - 2 y

r:l ASS A RFsinUALS POLLUTANT LIMITS
1. NAME AND ADDRESS OF FACILITY
Facility Name Town of Boone Jimmy Smith Wastewater Treatment Plant
Address 201 Casey Lane
P.O. Box 192
City Boone State NC Zip 28607
Facility Contact Kenneth Howell Phone [phone]
Signatory
2. NAME AND ADDRESS OF FACILITY OWNER
Facility owner's Name Town of Boone
Address P.O. Box 192
City Boone
State NC Zip 28607
3, MONITORING PERIOD 4. NPDES PERMIT NUMBER 5. SLUDGE PERMIT NUMBER
YEARI MO IDAY YEAR MO DAY NCO020621 WQ0013263 (Class A)
FROM 23 1 1 TO 23 1 3 31
6. INSTRUCTIONS: Complete the form based on the results of a[[ analyses performed during the monitoring period using approved analytical method.
Complete a separate sheet for each monitoring period during the reporting period.
Parameter
Pollutant Concentration
(dry wei ht)
Frequency of
Analysis
Sample Type
(Grab or Composite)
Analytical
Method
Avg.
Reg Limit
Units
Aluminum
Arsenic
Cadmium
Calcium
Copper
Lead
Magnesium
Mercury
Molybdenum
Nickel
Sample Measurement
12300
-
MG/KG
1
Grab
EPA 200.7
Sample Measurement
ND
41
MG/KG
1
Grab
EPA 200.7
Sample Measurement
1.2
39
MG/KG
1
Grab
EPA 200.7
Sample Measurement
14000
-
MG/KG
1
Grab
EPA 200.7
Sample Measurement
350
1500
MG/KG
1
Grab
EPA 200.7
Sample Measurement
13.6
300
MG/KG
1
Grab
EPA 200.7
Sample Measurement
2230
-
MG/KG
1
Grab
EPA 200.7
Sample Measurement
0.390
17
MG/KG
1
Grab
EPA 1631
Sample Measurement
4.80
75
MG/KG
1
Grab
EPA 200.7
Sample Measurement
10.9
420
MG/KG
1
Grab
EPA 200.7
10. CERTIFICATION
I certify under penalty of law that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons directly responsible for gathering the information
submitted, it is to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information.
Name and Official Title (type or print)
Kenneth Howell, Senior Operator
Area Code and Phone
828 268-6270
Signature
d
Date Signed (-31-Ly

CLASS A RESIDUALS POLLUTANT LIMITS
1. NAME AND ADDRESS OF FACILITY
Facility Name Town of Boone Jimmy Smith Wastewater Treatment Plant
Address 201 Casey Lane
P.O. Box 192
City Boone State NC
Facility Contact Kenneth Howell
Signatory
Zip 28607
Phone [phone]
2. NAME AND ADDRESS OF FACILITY OWNER
Facility owner's Name Town of Boone
Address
P.O. Box 192
City Boone
State NC Zip
28607
3. MONITORING PERIOD 1 4, NPDES PERMIT NUMBER 5. SLUDGE PERMIT NUMBER
YEARI MO DAY EARI MO DAY I NCO020621 WQ0013263 (Class A)
FROM 23 1 4 1 TO 231 6 30
6. INSTRUCTIONS: Complete the form based on the results of all analyses performed during the monitoring period using approved analytical method.
Complete a separate sheet for each monitoring period during the reporting period.
Parameter
Pollutant Concentration
(dry wei ht)
Frequency of
Analysis
Sample Type
(Grab or Composite)
Analytical
Method
Avg.
Reg Limit
Units
Potassium
Selenium
Sodium
Zinc
% Total Solids
Ammonia Nitrogen
Nitrate -Nitrite Nitrogen
Total Phosphorous
Total Kjeldahl Nitrogen
pH
PAN
SAR
Sample Measurement
2610
-
MG/KG
1
Grab
EPA 2000.7
Sample Measurement
3.80
100
MG/KG
1
Grab
EPA 200.7
Sample Measurement
891
-
MG/KG
1
Grab
EPA 200.7
Sample Measurement
616
2800
MG/KG
1
Grab
EPA 200.7
Sample Measurement
91.7
-
MG/KG
1
Grab
EPA 160.3
Sample Measurement
1900
-
MG/KG
1
Grab
EPA 350.1
Sample Measurement
ND
-
MG/KG
1
Grab
EPA 353.2
Sample Measurement
7320
-
MG/KG
1
Grab
EPA 200.7
Sample Measurement
59800
-
MG/KG
1
Grab
EPA 351.1
Sample Measurement
6.1
-
su
1
Grab
EPA 150.1
NA
18300
-
MG/KG
NA
NA
Calculation
NA
1.81
9.99
NA
1
Grab
EPA 60100
10. CERTIFICATION
I certify under penalty of law that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons directly responsible for gathering the information
submitted, it is to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information.
Name and Official Title (type or print) Area Code and Phone
Kenneth Howell, Senior Operator][phone]
Date Signed 1_31- ZY

CI ASS A RESIDUALS POLLUTANT LIMITS
1. NAME AND ADDRESS OF FACILITY
Facility Name Town of Boone Jimmy Smith Wastewater Treatment Plant
Address 201 Casey Lane
P.O. Box 192
City Boone
Facility Contact
Signatory
State NC Zip 28607
Kenneth Howell Phone [phone]
2. NAME AND ADDRESS OF FACILITY OWNER
Facility owners Name Town of Boone
Address P.O. Box 192
City Boone
State NC
Zip
28607
3. MONITORING PERIOD E4. NPDES PERMIT NUMBER 5. SLUDGE PERMIT NUMBER
YEARI MO I DAY YEAR MO DAY NCO020621 WQ0013263 (Class A)
FROM 23 4 1 TO 1 23 1 6 1 30
6. INSTRUCTIONS: Complete the form based on the results of all analyses performed during the monitoring period using approved analytical method.
Complete a separate sheet for each monitoring period during the reporting period.
Parameter
Pollutant Concentration
(dry weight)
Frequency of
Analysis
Sample Type
(Grab or Composite)
Analytical
Method
Avg,
Reg Limit
Units
Aluminum
Arsenic
Cadmium
Calcium
Copper
Lead
Magnesium
Mercury
Molybdenum
Nickel
Sample Measurement
14300
-
MG/KG
1
Grab
EPA 200.7
Sample Measurement
2.60
41
MG/KG
1
Grab
EPA 200.7
Sample Measurement
1.1
39
MG/KG
1
Grab
EPA 200.7
Sample Measurement
16300
-
MG/KG
1
Grab
EPA 200.7
Sample Measurement
330
1500
MG/KG
1
Grab
EPA 200.7
Sample Measurement
12.0
300
MG/KG
1
Grab
EPA 200.7
Sample Measurement
2470
-
MG/KG
1
Grab
EPA 200.7
Sample Measurement
0.170
17
MG/KG
1
Grab
EPA 1631
Sample Measurement
ND
75
MG/KG
1
Grab
EPA 200.7
Sample Measurement
12.9
420
MG/KG
1
Grab
EPA 200.7
10. CERTIFICATION
I certify under penalty of law that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons directly responsible for gathering the information
submitted, it is to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information.
Name and Official Title (type or print)
Kenneth Howell, Senior Operator
Area Code and Phone
828 268-6270
Signature I
I
Date Signed
1-31"211

N ASS A RF.q1nl1Al S P01 I.LITANT LIMITS
1. NAME AND ADDRESS OF FACILITY
Facility Name Town of Boone Jimmy Smith Wastewater Treatment Plant
Address 201 Casey Lane
P.O. Box 192
City Boone State NC
Facility Contact Kenneth Howell
Signatory
Zip 28607
Phone [phone]
2. NAME AND ADDRESS OF FACILITY OWNER
Facility owner's Name Town of Boone
Address P.O. Box 192
City Boone
State NC Zip 28607
3. MONITORING PERIOD 1 4. NPDES PERMIT NUMBER 5. SLUDGE PERMIT NUMBER
YEAR MO DAY YEAR MO DAY _ NCO020621 WQ0013263 (Class A)
FROM 23 7 1 TO 23 1 9 30
6. INSTRUCTIONS: Complete the form based on the results of all analyses performed during the monitoring period using approved analytical method.
Complete a separate sheet for each monitoring period during the reporting period.
Parameter
Pollutant Concentration
(dry weight)
Frequency of
Analysis
Sample Type
(Grab or Composite)
Analytical
Method
Avg.
Reg Limit
Units
Aluminum
Arsenic
Cadmium
Calcium
Copper
Lead
Magnesium
Mercury
Molybdenum
Nickel
Sample Measurement
18600
-
MG/KG
1
Grab
EPA 200.7
Sample Measurement
3.4
41
MGIKG
i
Grab
EPA 200.7
Sample Measurement
1.20
39
MGIKG
1
Grab
EPA 200.7
Sample Measurement
19300
-
MGIKG
1
Grab
EPA 200.7
Sample Measurement
492
1500
MGIKG
1
Grab
EPA 200.7
Sample Measurement
17.4
300
MGIKG
1
Grab
EPA 200.7
Sample Measurement
2760
-
MGIKG
1
Grab
EPA 200.7
Sample Measurement
0.36
17
MG/KG
1
Grab
EPA 1631
Sample Measurement
ND
75
MGIKG
1
Grab
EPA 200.7
Sample Measurement
14.9
420
MG/KG
1
Grab
EPA 200.7
10. CERTIFICATION
I certify under penalty of law that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons directly responsible for gathering the information
submitted, it is to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information.
Name and Official Title (type or print)
Kenneth Howell, Senior Operator
Area Code and Phone
828 268-6270
Signature
Date Signed
:3(—Zc

r`I ASS A RFSInIIALS POLLUTANT LIMITS
1. NAME AND ADDRESS OF FACILITY
Facility Name Town of Boone Jimmy Smith Wastewater Treatment Plant
Address 201 Casey Lane
P.O. Box 192
City Boone
Facility Contact
Signatory
State NC Zip 28607
Kenneth Howell Phone [phone]
2. NAME AND ADDRESS OF FACILITY OWNER
Facility owner's Name Town of Boone
Address P.O. Box 192
City
State
Boone
NC Zip
28607
3. MONITORING PERIOD 4. NPDES PERMIT NUMBER 5. SLUDGE PERMIT NUMBER
YEAR MO DAY YEAR MO DAY NCO020621 WQ0013263 (Class A)
FROM 23 7 1 TO 23 9 30
6. INSTRUCTIONS: Complete the form based on the results of all analyses performed during the monitoring period using approved analytical method.
Complete a separate sheet for each monitoring period during the reporting period.
Parameter
Pollutant Concentration
(dry weight)
Frequency of
Analysis
Sample Type
(Grab or Composite)
Analytical
Method
Avg.
Reg Limit
Units
Potassium
Selenium
Sodium
Zinc
% Total Solids
Ammonia Nitrogen
Nitrate -Nitrite Nitrogen
Total Phosphorous
Total Kjeldahl Nitrogen
pH
PAN
SAR
Sample Measurement
2770
-
MG/KG
1
Grab
EPA 200.7
Sample Measurement
5.30
100
MG/KG
1
Grab
EPA 200.7
Sample Measurement
789
-
MG/KG
1
Grab
EPA 200.7
Sample Measurement
822
2800
MG/KG
1
Grab
EPA 200.7
Sample Measurement
93.1
-
MG/KG
1
Grab
EPA 160.3
Sample Measurement
1370
-
MG/KG
1
Grab
EPA 350.1
Sample Measurement
ND
-
MG/KG
1
Grab
EPA 353.2
Sample Measurement
15700
-
MG/KG
1
Grab
EPA 200.7
Sample Measurement
34800
-
MG/KG
1
Grab
EPA 351.1
Sample Measurement
6.0
-
su
1
Grab
EPA 150.1
NA
10700
-
MG/KG
NA
NA
Calculation
NA
2.1
9.99
1 NA
NA
Grab
EPA601OD
10. CERTIFICATION
I certify under penalty of law that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons directly responsible for gathering the information
submitted, it is to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information.
Name and Official Title (type or print) Area Code and Phone
Kenneth Howell, Senior Operator 828 268-6270
Signature L d 1 4t� Date Signed 1 3 I-Z I/

CLASS A RESIDUALS POLLUTANT LIMITS
1. NAME AND ADDRESS OF FACILITY
Facility Name Town of Boone Jimmy Smith Wastewater Treatment Plant
Address 201 Casey Lane
P.O. Box 192
City Boone State NC Zip 28607
Facility Contact Kenneth Howell Phone [phone]
Signatory
2. NAME AND ADDRESS OF FACILITY OWNER
Facility owner's Name Town of Boone
Address P.O. Box 192
City Boone
State NC Zip 28607
3. MONITORING PERIOD 14. NPDES PERMIT NUMBER 5. SLUDGE PERMIT NUMBER
YEAR MO DAY I YEAR MO DAY NCO020621 WQ0013263 (Class A)
FROM 23 10 1 1 TO 1 3 12 1 31
6. INSTRUCTIONS: Complete the form based on the results of all analyses performed during the monitoring period using approved analytical method.
Complete a separate sheet for each monitoring period during the reporting period.
Parameter
Pollutant Concentration
(dry weight)
Frequency of
Analysis
Sample Type
(Grab or Composite)
Analytical
Method
Avg.
I Reg Limit
Units
Aluminum
Arsenic
Cadmium
Calcium
Copper
Lead
Magnesium
Mercury
Molybdenum
Nickel
Sample Measurement
17000
-
MG/KG
1
Grab
EPA6010D
Sample Measurement
2.80
75
MG/KG
1
Grab
EPA6010D
Sample Measurement
1.4
85
MG/KG
1
Grab
EPA601 OD
Sample Measurement
16,700
-
MG/KG
1
Grab
EPA6010D
Sample Measurement
486
4300
MG/KG
1
Grab
EPA601 OD
Sample Measurement
17.8
840
MG/KG
1
Grab
EPA6010D
Sample Measurement
2460
-
MG/KG
1
Grab
EPA601 OD
Sample Measurement
0.4400
57
MG/KG
1
Grab
EPA7471 B
Sample Measurement
ND
75
MG/KG
1
Grab
EPA6010D
Sample Measurement
15.6
420
MG/KG
1
Grab
EPA6010D
10. CERTIFICATION
I certify under penalty of law that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons directly responsible for gathering the information
submitted, it is to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information.
Name and Official Title (type or print)
Kenneth Howell, Senior Operator
Area Code and Phone
828 268-6270
Signature
Date Signed

CLASS A RESIDUALS POLLUTANT LIMITS
1. NAME AND ADDRESS OF FACILITY
Facility Name Town of Boone Jimmy Smith Wastewater Treatment Plant
Address 201 Casey Lane _
P.O. Box 192
City Boone State NC Zip 28607
Facility Contact Kenneth Howell Phone [phone]
Signatory
2. NAME AND ADDRESS OF FACILITY OWNER
Facility owner's Name Town of Boone
Address P.O. Box 192
City Boone
State NC
Zip 28607
3. MONITORING PERIOD 1 4. NPDES PERMIT NUMBER 5. SLUDGE PERMIT NUMBER
YEAR MO D IYEARI MO I DAY I NCO020621 WQ0013263 (Class A)
FROM 23 10 1 TO 1 2 1 12 1 31
6. INSTRUCTIONS; Complete the form based on the results of all analyses performed during the monitoring period using approved analytical method.
Complete a separate sheet for each monitoring period during the reporting period.
Parameter
Pollutant Concentration
(dry wei ht)
Frequency of
Analysis
Sample Type
(Grab or Composite)
Analytical
Method
Avg.
Reg Limit
Units
Potassium
Selenium
Sodium
Zinc
% Total Solids
Ammonia Nitrogen
Nitrate -Nitrite Nitrogen
Total Phosphorous
Total Kjeldahl Nitrogen
pH
PAN
SAR
Sample Measurement
2240
-
MG/KG
1
Grab
EPA6010D
Sample Measurement
5
100
MG/KG
1
Grab
EPA6010D
Sample Measurement
1070
-
MG/KG
1
Grab
EPA6010D
Sample Measurement
885
7500
MG/KG
1
Grab
EPA6010D
Sample Measurement
91.2
-
MG/KG
1
Grab
SM2540G
Sample Measurement
1,490
-
MG/KG
1
Grab
EPA350.1
Sample Measurement
ND
-
MG/KG
1
Grab
EPA353.2
Sample Measurement
16,000
-
MG/KG
1
Grab
EPA365.1
Sample Measurement
35800
-
MG/KG
1
Grab
EPA351.2
Sample Measurement
6.2
-
su
1
Grab
EPA9045D
NA
11000
-
NA
1
Grab
NONE
NA
2.1
9.99
NA
1
Grab
EPA-6010D
10. CERTIFICATION
I certify under penalty of law that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons directly responsible for gathering the information
submitted, it is to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information.
Name and Official Title (type or print) Area Code and Phone
Kenneth Howell, Senior Operator1(828)268-6270
Signature �- jDate Signed `_31- L V

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Attach this form to the corresponding laboratory analysis.
Please note that your permit may contain additional parameters to be analyzed than thise requred to be summarized on this form.
Permit Number WQ0013263 Laboratory 1) Pace Analytical Servnces LLC
Facility Name Town of Boone 2) Water Quality Services, Inc.
NPDES # NCO020621
or WQ # (residual only facilities)
WWTP Name Town of Boone Jimmy Smith Wastewater Treatment Plant
Residual Analvsis Data
Date Sampled Grab Ceiling Con 2/14/2023 5/5/2023 8/2/2023 10/24/2023
p (Grab) 9
Quarter ILimit malkal 1st I 2nd 3rd 4th
weiclht)
Aluminum
NA 12,300
14300
18,600
17,000
Arsenic
75 ND
2.6
3A
2.8
Cadmium
85 1.20
1.1
1.20
1.4
Calcium
NA 14,000
16300
19,300
16,700
Copper
4300 350
330
492
486
Lead
840 13.6
12
17.4
17.8
Magnesium
NA 2,230
2,470
2,760
2,460
Mercwy
57 0.3900
0.1700
0.36
0.4400
Molybdenum
75 4.80
ND
ND
ND
Nickel
420 10.9
12.9
14.9
15.6
Potassium
NA 2,580
2,610
2,770
2,240
Selenium
100 5.60
3.80
5.30
5.00
Sodium
NA 775
891
789
1,070
Zinc
7500 724
616
822
885
Ammonia Nitrogen
NA 1470
1,900
1,370
1,490
Nitrate -Nitrite Nitrogen
NA ND
ND
ND
ND
Total Phosphorous
NA 16100
7,320
15,700
16,000
Total Keldahl Nitrogen
NA 65000
59800
34,800
35800
H
NA 5.9
6.1
6
6.2
PAN
NA 19800
18,300
10,700
11000
SAR
9.99
1.70
1 1.80
1.50
2.10
% Total Solids
NA
91.5
1 91.7
93.1
91.2
X
j. Z
(SIGNATURE OF PREPARER) DATE
I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
Significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (503 Rules)
Facility Name: Town of Boone
WQ0013263
WWTP Name: Town of Boone Jimmy Smith Wastewater Plant NPDES Number: NCO020621
Monitoring Period: From 1/l/2023 To 3/31/2023
Pathogen Reduction (40 CFR 503.32) - Please indicate level achieved and alternative performed:
WQ Permit Number:
Class A;
Alternative 1 D
Alternative 2 ❑
Alternative 3 ❑
Alternative 4 ❑
Alternative 5 0
Alternative 6 ❑
If applicable to alternative performed (Class A only) indicate "Process to Further
Reduce Pathogens":
Compost ❑
Heat Drying Q
Heat Treatment ❑
Thermophilic ❑
Beta Ray ❑
Gamma Ray ❑
Pasteurization ❑
Class B:
Alternative 1 ❑
Alternative 2 ❑
.
If applicable to alternative performed (Class B only) indicate "Process to Significantly
Reduce Pathogens":
Lime Stabilization ❑
Air Drying❑
Composting ❑ I
Aerobic Digestion ❑
Anaerobic Digestior. ❑
If applicable to alternative performed (Class A or Class B) complete the following monitoring data:
Parameter
Allowable Level
in Sludge
Pathogen Density
Numbera
Excee-
denc
Frequency
yis
of Analysis
Sample
Type
Analytical
Tech -
moue
Minimum
Geo. Mean
Maximus
Units
Fecal Coliform
2 x 10 to the
6th power
Per grain of
total solids
MPN
CFU
1000 rnpn per gram
of total solid (dry
weight)
228
331
454
MPN/g
Quarterly
grab
9221-E
Salmonella bacteria
(in lien of fecal
coliform)
3 MPN per 4 grams
total solid (dry
wei ht
Vector Attraction Reduction (40 CFR 503.33) - Please indicate option performed:
Alt.l (VS reduction) ❑
Alt. 2 (40-day bench) ❑
Alt. 3 (30-day bench) ❑
Alt. 4 (Spec. OZ uptake) ❑
Alt. 5 (14-Day Aerobic) ❑
Alt. 6 (Alk. Stabilization ❑
Alt 7 (Drying - Stable) d
Alt. 8 (Drying - Unstable) ❑
Alt. 9 (Injection) ❑
Alt. 10 (Incorporation) ❑
iNo vector attraction reduction alternatives were performed ❑
CERTIFICATION STATEMENT (please check the appropriate statement)
R1 "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector
attraction reduction requirement in 40 CFR 503.33 have been met."
❑ "I certify, tinder penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector
attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check
this statement attach an explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Kenneth Howell Senior Operator
Preparer Name and Title (type or print)
L.,4/ 9,6a#
Signature of Preparer* Date
NA
Land Applier Name and Title (if applicable)(type or print)
Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Pail 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 503 (12/2006)

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (503 Rules)
Facility Name: Town of Boone WQ Permit Number:
W WTP Name: Town of Boone Jimmy Smith Wastewater Plant NPDES Number:
Monitoring Period: From 4/l/2023 To 6/30/2023
WQ0013263
NCO020621
Pathogen Reduction (40 CFR 503.32) - Please indicate level achieved and alternative performed:
Class A:
Alternative 1 ❑
Alternative 2 ❑
Alternative 3 El
..................
Alternative 4 ElAlternative
5 21
Alternative 6 ❑
If applicable to alternative performed (Class A only indicate "Process to Further Reduce Pathogens":
Compost ❑
Heat Drying 17
Heat Treatment ❑
Thermoplvlic ❑
Beta Ray ❑
Gamma Ray ❑
Pasteurization C
Class B:
Alternative 1 ❑
Alternative 2 ❑
.,..............
If applicable to alternative
performed (Class
B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization ®
Air Drying❑ I
Composting ® jAerobic
Digestion ❑
Anaerobic Digestior ❑
:.: >;: s»<:::::
If applicable to alternative performed (Class A or Class B) complete the following monitoring data:
Parameter
Allowable Level
in Sludge
Pathogen Density
Number o
Excee-
Frequency
of
of Analysis
Y
Sample
Type
Analytical
Tech -
nioue
Minimun
Geo. Mean
Maximo
Units
Fecal Coliforni
2 x l0 to the
6th power
per gram of
total solids
MPN
CFU
318
370
444
MPN/G
Quarterly
grab
9221 E
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
(in lieu of fecal
coliforin)
3 MPN per 4 grams
total solid (dry
weight)
Vector Attraction Reduction (40 CFR 503.33) - Please indicate option performed:
Alt.1 (VS reduction)
❑ I
Alt. 2 (40-day bench)
❑
Alt. 3 (30-day bench) ❑
Alt. 4 (Spec. OZ uptake)
❑
Alt. 5 (14-Day Aerobic)
❑
Alt. 6 (Alk. Stabilization
❑
Alt 7 (Drying - Stable) 211
Alt, 8 (Drying - Unstable)
❑
Alt. 9 (Injection)
[I
Alt. 10 (Incorporation)
❑
No vector attraction reduction alternatives were performed
❑
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector
attraction reduction requirement in 40 CFR 503.33 have been met."
❑ "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector
attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check
this statement attach an explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Kenneth Howell Senior Operator
Preparer Name and Title (type or print)
&..d 41,m�
Signature of Preparer*
NA
Land Applier Name and Title (if applicable)(type or print)
Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 503 (1212006)

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (503 Rules)
Facility Name: Town of Boone
WQ Permit Number: WQ0013263
WWTP Name: Town of Bootie Jimmy Smith Wastewater Plant NPDFS Number: NCO020621
Monitoring Period: From 7/l/2023 To 9/31/2023
Pathogen Reduction (40 CFR 503.32) - Please indicate level achieved and alternative performed:
Class A:
Alternative 1 ❑
Alternative 2 ❑
Alternative 3 ❑
Alternative 4 ElAlternative
5 0
Alternative 6 ❑
If applicable to alternative performed (Class A only) indicate "Process to Further
Reduce Pathogens":
Compost ❑
Heat Drying R1
Heat Treatment ❑
Thennophilic ❑
Beta Ray ❑
Gamma Ray ❑
Pasteurization ❑
........•::.:.::.:.:.:: :
."... •"." "...".". .
Class B:
Alternative 1 ❑
Alternative 2 ❑
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization ❑
Air Drying❑
Composting ❑
Aerobic Digestion ❑
Anaerobic Digestion: ❑
- .. ,........". ,.... .
If applicable to alternative performed (Class A or Class B) complete the following monitoring data:
Parameter
Allowable Lever
in Sludge
Pathogen Density
Number of
Excee-
Frequency
of Analogesysis
Sample
Type
Analytical
Tech -
nioue
Minimu
Geo. Mean
Maximun
Units
Fecal Coliform
2 x 10 to the
6th power
per grain of
total solids
MPN
CFU
1000 mpn per gram
of total solid (dry
weight)
280
380
464
MPN/G
Quarterly
grab
9221 E
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per 4 grains
total solid (dry
Weight)
Vector Attraction Reduction (40 CFR 503.33) - Please indicate option performed:
Alt.] (VS reduction) ❑
Alt. 2 (40-day bench) ❑
Alt. 3 (30-day bench) [❑
I Alt. 4 (Spec. OZ uptake) ❑
Alt. 5 (14-Day Aerobic) ®
Alt. 6 (Alk. Stabilization ❑
Alt 7 (Drying - Stable) El
jAlt. 8 (Drying - Unstable) ❑
Alt. 9 (Injection) ❑
Alt. 10 (Incorporation) ❑
No vector attraction reduction alternatives were performed ❑
CERTIFICATION STATEMENT (please check the appropriate statement)
21 "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector
attraction reduction reauir•ement in 40 CFR 503.33 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector
attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check
this statement attach an explanation why you have not met one or• both of the requirements.)
"This determination has been made tinder my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Kenneth Howell Senior Operator NA
Preparer Name and Title (type or print) Land Applier Name and Title (if applicable)(type or print)
Signature of Preparer* Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 503 (12/2006)

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (503 Rules)
Facility Name: Town of Boone
WQ Permit Number: WQ0013263
WWTP Name: Town of Boone Jimmy Smith Wastewater Plant NPDES Number: NCO020621
Monitoring Period: From 10/1/2023 To 12/31/2023
Pathogen Reduction (40 CFR 503.32) - Please indicate level achieved and alternative performed:
Class A:
Alternative 1 ❑
Alternative 2 ❑
Alternative 3 ❑
Alternative 4 ❑
Alternative 5 0
Alternative 6 ❑
If applicable to alternative performed (Class A only indicate "Process to Further Reduce Pathogens":
Compost ❑
Heat Drying 21
Heat Treatment ❑
Thermophilic ❑
Beta Ray ❑
Gamma Ray ❑
Pasteurization ❑
Class B.
Alternative 1 ❑
Alternative 2 ❑
If applicable to alternative
performed (Class
B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization ❑
Air Drying[]
Composting ❑
Aerobic Digestion ❑
Anaerobic Digestior. ❑
If applicable to alternative erformed (Class A or Class B) complete the following monitoring data:
Parameter
Allowable Level
in Sludge
Pathogen Density
g ty
Number o
Excee-
dences
Frequency
of Analysis
Sample
na ytjca
Tech -
ni u
Minimum
Geo. Mean
MaximurUnits
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
CFU
1000 inpn per gram
of total solid (dry
weight)
44
90
156
MPN/G
Quarterly
grab
9221 E
Salmonella bacteria
(in lieu of fecal
Coliform
3 MPN per 4 grams
total solid (dry
weight)
Vector Attraction Reduction (40 CFR 503.33) - Please indicate option performed:
Alt.1 (VS reduction) ❑
Alt. 2 (40-day bench) ❑
JAR. 3 (30-day bench) ❑
I Alt. 4 (Spec. 02 uptake) ❑
Alt. 5 (14-Day Aerobic) ®
Alt. 6 (Alk. Stabilization ❑
JAR 7 (Drying - Stable) d
JAIt. 8 (Drying - Unstable) ❑
Alt. 9 (Injection) ❑
Alt. 10 (Incorporation) ❑
INo vector attraction reduction alternatives were performed ❑
CERTIFICATION STATEMENT (please check the appropriate statement)
0 "1 certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector
attraction reduction requirement in 40 CFR 503.33 have been met."
El "I certify, tinder penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector
attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check
this statement attach an explanation why you have not met one or both of the requirements.)
"This determination has been trade under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Kenneth Howell Senior Operator
Preparer Name and Title (type or print)
4 4,.,g
Signature of Preparer*
NA
Land Applier Name and Title (if app I icable) (type or print)
W)-0
Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 503 (12/2006)

e
rw
��
cn
.00
F-I
I
4-4
i
I
ti

. .
.
. . .
` ~".n"w rnPoK UUDJET
.
-~LE~ "^^cao COVER
INLET.
�ox�
. .. . ��LK
. ' -
.
'
. . ` '
.. .
�
� VmruK DOME
|
� DISC'
����� /
. .` ' —^-�'�n^E ro-c
. . . ..
-BAFFLE PLATE
�
.
. u|A|VR
..
' SUPPORT SADDLE
..
. . �
.
' MATERIAL
. .
. .OUTLET.
. . FOUNOATIOIj
.
. / . . . . . .
. . . .
. Ek][) -VIEW.
...
. '
. ^
. .
. . . .. .
'
. .
� . .
. . .
EXHAUST VAPOR ^
� �
. � VAPOR DOME
MATERIAL INLET
Li
`
j
DISCS
SEAL . .
ROTD�.
BEARING . ..
SIPHON-* -TUBE
' ROTOR AIR VENT
CONDENSATE OUTLET
'HOLLOW �
STEAM JOINT'
'
--...'_`
. '
.^ . .
� ���`
.
. .
' r'= ' ~-"
r"
'
P/PE3' �
PADDLES
. . ~~"~""w` ' ``-_-_-_--3UPpORT
MATERIAL OUTLET
.
SADDLE'
. E' VIEW
.SECTION
. .
. . .
� . .
) . .
Atl8s.Sf{}/ ' ��/�7~� ��k�/�/�\
. . -�.-_.,^^-^~`'`~
. . .
. . .
INO|F{EQTHE/TE[] 0 'C DRIER
. � . .
Figb[o I
�

•_; ®R
tV"Aligg gk.
j(l
"T
�lj
za
o
r U3
0 (a . .
C-5
. . LL
ECI
E: LQ
cl
cq
(13
Ul
9

Drier Log
--DATE
Date/Ti
me
;
H p
"' *'cq 4-5
2
0
s
"-
so
;a
as
`—
.cn
?oo l.2 t
o
roe 4
l7
a
15,6—
®�S.S
o
S
,s, .SD
-
l/7Uo `!
2ua / uy
D
p
(vl
(� /
S�
5, jS
J D
/ 19w 4q
2w /Vf5
o
rn
73
Co 2
�-
lzz$
�--
�17
0
s
°
D
i�r irS
d
2
Lo
9
/zr
in6
s��
ss
���
6 4
1-
S- J
l 1210
aqq 1gs
/24-
MO
G L
SST
j �
S"�
��—..�
lC0 6r
�t
z o
/ �/
r �
- /1)J00 /2!�
2 -r zs /0i0o h� /16 12.12
/Wo., /,21
Notes; .,,
HC114
12/2S/98
N

Drier Log
Date/Ti
El
E
CL)
(j)
, cl
me
cz
cd
'm
cu cl
r
4j
P.
P
%11.74
3,0
3Dd-43- /10 12L
-A,
S-Y
2-t
Lfq 110 / v
�v
Z-0
2-
J20
qt
'50 ZO
9s sz
1.70
121q,()
-
�5
'0
5-0
Zlcv tq s
0•
> Iwo via
0-0
rd
I-"
gtA
to
/Z4 G
3
J-3
:(VIA
oo /ur,
AL
;. 3
2,(
2-0
3 d.
gay
z z
/k �LQ
7
22 L2-22
W7 1231 -
2
1160
IC114
zlW91

)Drier Log
1�
Ali
DATE 11- G -L 3
C7
�
bate/Ti
ice. �
lCi
E-4
�
lZ
•-� .•
Ln 4-
[d
cl 0
.�
) cz
p
.�
¢
� L �
41 �CCcl
+ _
�
q 4-1
rn a
vi •E
iu A-s �,
a � -!-•
� ,�
11.E /otioa S'
41 /ytg
—Z
/la.?lcpr�-
/a l i I
N /x z
— `!
S' 2
,f'�3
�s"
j- 1
s�6
6 G y J
z
k41f
l a� Z
/7� 5�
ids / 21q
.3
H�.
uO
gu
So
5�
Gg �.a
—
K. 5
�a
Sq
t4S /Z{g
70 D
9569
3b
qQ
I YZ
HL?
-7
7 2-
/ yz i
llqo / 1fl
-3
s Z
.2
-
r
_-
-z� / j(p S`�
/t2E
L(. G
'
?0
2L,
Sg'
';b o
r
/
- 2
sr
57
70
0-&
s6
7
47
qDd
s 7
l-( D
l 7 O
24
Et�
110 1?21
h h
`+ 3
70
y
/010 1
1$1 /27.1
-
'y
5
70
,3s'
S''r
gv ) 3.q
i1, 74
KC L 14
12128/9S

Drier Log
.BATES-�L"L� � -
_ I
Date/Ti aH Iq
„ + o
me
A A pi A. o a s 60 J P-(
t C
"ZL. d7JJ s' r S
d t /1Z
17
� y
S Z14e- 3 `{ S p S c7` R9 64
55 /$S / 2/S 3 S {,s9 �
/ � Y '3y sa �s s s � •
VI 3 S - S �� SD
3 z 3 Z Sv 2 s (S S• d
/2tc,u 60'Y5 3 2 3 z
�r�rwS 5 3S�
3 Lf
Z ZS 7o
a O S- q /1- b to
/ I b /2 2 5 3 r7 _
LI
/ 7 LI, v
/�aoo y J �j /4211 J.6 r s► z
s 5— 7)-
Notes.
HC 114
12/28/93

r
€high country 6..1-g 135C)Salids s
.Produced by the Town of Boone
P.O. Drawer 192, Boone, NC 2BG07
ti
High Country 6-1-0 (HC 610) Is a high organic content fertilizer manufactured by the Town of Boone
Wastewater Treatment Facility. This product produces superior results on lawns, flower beds and
shrubs providing nutrients at the rates indicated below:
Guaranteed Analysis
Total Nitrogen ...............................
WaterInsoluble Nitrogen
..........................................3.5%
Available Phosphoric Acid
........................
Soluble Potash
°
1/o
...................
Iron...
0%
Recommended Application Rates
Lawn -Sod Establishment: Apply HC 610 at rate of 3b lbs per 1000 sq feet.
Turf Mailitenance: 'Apply HC 610 at a rate of 10'-15 lbs per !DOD -sq feet.
Plant Bed Establishment: Apply HC 610 at a rate of 2 lbs per ipo sq feet Into soil,
Planting Bed Maintenance: Apply HC 610 at a rate of 2 lbs per 100 sq feet in Spring/Fall
Warnings: HC 610. is environmentally safe when used as directed, but can become a hazard if
mismanaged. This product should not be used bn soils lntended for food crop production.
Cover HC 610 w)th a tarp or plastic during transportation. Store HC 610 in a dry area away from wells
or surface water where it could be washed into streams; keep product away from children's play
areas.
Limited Warranty and Discialmer: The Town of Bbone warrants that HC 610 meets the specifications
stated above, and that the heavy metal content is less than or equal to the limitations specified in the
EPA and NC Dept of Environmental and Natural Resources sludge quality criteria for land application.
If HC 610 falls to meet its specificbtlon, the buyer's sole remedy shall be the recovery of the purchase
price. Under no circumstances shall the Town of Boone be liable for any other 'damages, including
direct, Indirect, consequential or special damages.
The undersigned Buyer agrees to abide by the following Restrictions:
HC 610 shall not be applied to land except In accordance with the Instructions contained herein,
HC 610 shall not be applied to any site that is flooded, frozen, or snow-covered.
HC 610 shall not be applied within 100 feet of any water supply, stream.. river, or lake.
Adequate measures shall be provided to prevent surface runoff from carrying this product into any
surface waters.
Buyer Signature Date
Name (Print): Quantity:
lbs/tons
Street/Route: Intended Use:.
j Clty/State/Zip:
Amount Collected:
Telephone: Loaded By:
i
c

Town of Boone Wastewater Treatment Plant
2022 Class Residuals Production
Run
Gallons
Digester
Total
No.
Run Date
Processed
% Solids
Dry Tons Notes
1
1-/3/2023
137,404
2.86
16.39
2
1/9/2023
143,745
2.54
15.23
3
1/17/2023
112,037
2.62
14.68
4
1/23/2023
162,770
2.70
18.33
5
1 / 30/ 2023
175,454
2063.00
19.24
6
2/6/2023
162,770
2.39
16.22
7
2/23/2023
183,909
2.28
17.49
8
2/ 202/ 2023
202,934
2.32
19.63
9
2/27/2023
162,770
2.39
16.22
10
3/6/2023
164,884
2.38
16.36
11
3/13/2023
143,745
2.52
15.11
12
3/202/2023
188,137
2.56
20.08
13
3/ 27/ 2023
86,670
2.74
9.90
14
4/3/2023
181,796
2.81
21.30
15
4/10/2023
147,973
2.82
17.40
16
4/ 17/ 2023
90,898
2.80
10.61
17
4/20/2023
84,556
2.63
9.27
18
4/24/2023
171,226
2.65
18.92
19
5/1/2023
169,112
2.81
19.82
20
5/8/2023
181,795
2.80
2-1.23
21
5/ 22/ 2023
124,720
2.86
14.87
22
5/30/2023
69,759
2.73
7.94
23
6/ 5/ 2023
175,454
2.62
19.17
24
6/12/2023
93,012
2.94
11.40
25
6/26/2023
40,164
3.06
5.13
26
7/5/2023
122,606
2.88
14.72
27
7/10/2023
152,201
2.69
17.07
28
7/ 17/ 2023
147,973
3.04
18.70
29
7/24/2023
97,239
3.31
13.42
30
7/31/2023
150,087
3.52
22.03
31
8/7/2023
109,923
3.00
13.75
32
8/14/2023
103,581
3.32
14.34
33
8/21/2023
2,000,821
3.19
26.71
34
8/28/2023
23,259
3.15
3.05
35
9/11/2023
378,388
2.80
44.18
36
9/18/2023
228,301
2.96
28.18

37
9/25/2023
289,604
3.02
36.47
38
10/2/2023
236,757
2.56
25.27
39
10/9/2023
147,973
3.26
20.11
40
10/16/2023
137,404
3.26
18.68
41
10/23/2023
162,770
3.09
20.97
42
10/30/2023
162,277
3.00
20.36
43
11/6/2023
145,859
2.76
16.78
44
11/20/2023
186,023
2.47
19.16
45
11/14/2023
179,681
2.60
19.48
46
11/27/2023
118,378
3.06
15.10
47
12/4/2023
171,226
2.50
17.85
48
12/11/2023
61,303
2.75
7.03
49
12/18/2023
169,112
2.85
20.10
Totals
9,240,440
865.00

N
D)
P4
a
rncD
tn+
O Q;
�e
a
s
Q1
a
s
Q7
a
�
m
i�
ca
o
oD
LA
o0
00
el
CD
CR
Iq
o
�Mn
ON
to
✓-a,`ii t
N
to
'�•+
%
a
Lnz
00
cq
z
coV
00l
z
CIAo�0
Zo
A
00
fo
ifs
V
z
�.
N
V
i-
d
cy
y
V
z
w
a
o
W
abt
o
m
p�
fpa
ca
C)
C�
�o
V'
M
'eN
00
Ln
t r-^ Hr ti
rr
1-I
t'
Cd

(�Ia'cieAnalXical'
www.pecelatitcam
Laboratory Report
Karen Reece
Town of Boone WWTP
PO Drawer 192
Boone, NC 28607
Project: Town of Boone -Blosolids
Pace Project No.: 92648926
Pace Analytical Services, LLC
1377 South Park Drive
Kemersvitle, NC 27284
[phone]
Page 1 of 2
Report Date: 02/14/2023
Date Received: 01/26/2023
Sample: Biosolids
Lab ID: 92648926001 Collected: 01/2612308:40 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Method
Parameters
Results
Units
Report Limit
Analyzed
Qualifiers
EPA6010
Aluminum
12300
mg/kg
65.1
02/01/2311:19
EPA6010
Arsenic
NO
mg/kg
3.3
02/01/2311:19
D3
EPA6010
Cadmium
1.2
mg/kg
0.33
02101/2311:19
EPA 6010
Calcium
14000
mg/kg
326
02/01/23 11:19
EPA6010
Copper
350
mg/kg
3.3
02/02/23 03:10
EPA 6010
Lead
13.6
mg/kg
3.3
02/01/23 11:19
EPA6010
Magnesium
2230
mg/kg
163
02/01/2311:19
EPA 6010
Molybdenum
4.8
mg/kg
3.3
02/01/23 11:19
EPA 6010
Nickel
10.9
mg/kg
1.6
02/01/23 11:19
EPA6010
Potassium
2580
mg/kg
326
02/01/23 11:19
EPA 6010
Selenium
5.6
mg/kg
4.9
02/01/23 11:19
EPA6010
Sodium
775
mg/kg
326
02/01/2311:19
EPA6010
Zinc
724
mg/kg
32.6
02/01/2311:19
EPA 6010D
Sodium Adsorption Ratio
1.7
meq/L
02/13/23 18:04
N2
EPA 7471
Mercury
0.39
mg/kg
0.068
02/06/23 10:36
MI
SM 254OG-2011
Total Solids
91.5
%
0A0
01/27/23 15:18
SW-846
Percent Moisture
8.5
%
0.10
01/27/23 15:09
N2
EPA 90450
pH at 25 Degrees C
5.9
Sid. Units
0.10
02108/23 15:50
H3
None
Plant Available Nitrogen
19800
mg/kg
02/10/23 14:17
N2
TKN+NO3+NO2
Nitrogen
65000
mg/kg
40.0
02/0612314:58
Calculation
EPA 350.1 Rev 2.0 1993
Nitrogen, Ammonia
1470
mg/kg
21.4
02/09/23 12:02
Mod.
EPA 351.2 Rev 2.0 1993
Nitrogen, Kjeldahl, Total
65000
mg/kg
2600
02103/23 05:38
EPA 353.2 Rev 2.0 1993
Nitrogen, NO2 plus NO3
NO
mg/kg
4.3
01/27/23 23:37
M1
EPA 353.2 Rev 2.0 1993
Nitrogen, Nitrate
NO
mglkg
4.3
01/27/23 23:37
EPA 353.2 Rev 2.0 1993
Nitrogen, Nitrite
NO
mg/kg
4.3
01/27/23 23:37
Mi
EPA 365.1 Rev 2.0 1993
Phosphorus
16100
mg/kg
248
02/03/23 13:39
ANALYTE QUALIFIERS
D3 Sample was diluted due to the presence of high levels of non -target analytes or other matrix interference.
H3 Sample was received or analysis requested beyond the recognized method holding time.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
N2 The lab does not hold NELAC/TNI accreditation for this parameter but other accredliations/certifications may apply. A
complete list of accreditations/certifications is available upon request.
Page 1 of 5

aceAnalytical
www.pacotabs.com
Reviewed by: CDclk�
Stephanie Knott
704-977-0981
stephanie.knott@pacelabs,com
Pace Analytical Services Ormond Beach
8 East Tower Circle, Ormond Beach, FL 32174
Alaska DEC- CSIUSTILUST
Alabama Certification #: 41320
Colorado Certification: FL NELAC Reciprocity
Connecticut Certification #: PH-0216
Delaware Certification: FL NELAC Reciprocity
Florida Certification #: E83079
Georgia Certification #: 955
Guam Certification: FL NELAC Reciprocity
Hawaii Certification: FL NELAC Reciprocity
Illinois Certification #: 200068
Indiana Certification: FL NELAC Reciprocity
Kansas Certification #: E-10383
Kentucky Certification #: 90050
Louisiana Certification M FL NELAC Reciprocity
Louisiana Environmental Certificate #: 05007
Maine Certification #: FLO1264
Maryland Certification: #346
Massachusetts Certification #: M-FL1264
Michigan Certification #: 9911
Mississippi Certification: FL NELAC Reciprocity
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification M 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Laboratory ID: 99006
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
FloddalNELAP Certification #: E87648
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
Pace Analytical Services, LLC
1377 South Park Drive
Kemersville, NC 27284
[phone]
Missouri Certification #: 236
Montana Certification M Cert 0074
Nebraska Certification: NE-OS-28-14
New Hampshire Certification #: 2958
New Jersey Certification #: FL022
New York Certification #: 11608
North Carolina Environmental Certificate #: 667
North Carolina Certification #: 12710
North Dakota Certification #: R-216
Ohio DEP 87780
Oklahoma Certification #: D9947
Pennsylvania Certification #: 68-00547
Puerto Rico Certification #: FLO1264
South Carolina Certification: #96042001
Tennessee Certification #: TN02974
Texas Certification: FL NELAC Reciprocity
US Virgin Islands Certification: FL NELAC Reciprocity
Virginla Environmental Certification M 460165
West Virginia Certification #: 9962C
Wisconsin Certification #: 399079670
Wyoming (EPA Region 8): FL NELAC Reciprocity
South Carolina Certification #: 99006001
South Carolina Drinking Water Cert, #: 99006003
FloddalNELAP Certification #: E87627
Kentucky UST Certification #: 84
Louisiana DoH Drinking Water #: LA029
VirginiaNELAP Certification #: 460221
South Carolina Laboratory ID: 99030
South Carolina Certification #: 99030001
MrginlaNELAP Certification #: 460222
Page 2 of 2
Page 2 of 5

VVtl r ILiG. C.rY V "rrMyl-rILJVd 1-uuo,r vv i_i er-r7 Jpec Jam pie t�oticnxion
?GE- Lpon Receipt
.,nCkLA YM Effective Date: 05/12/2022
Laboratory receiving Samples:
Asheville ❑ Eden ❑ Greenwood ❑ Huntersville ❑ Raleigh❑ Mechanicsville❑ Atlanta[] Kernersvil)e ff
• H Client Name:
7•o iV h o A b ; y\ e, Project #;
ICI DJOi I'd J
Courier. [:]Fed Ex ❑UPS ❑USPS ❑Client 1
❑ Commercial [—]Pace ❑Other: Q tit Ct- t-
CarderTracking Number:
Custody Seal Present? ❑Yes ff No Seals Intact? ❑Yes ❑No
Packing Material: ❑Bubble Wrap ❑Bubble Bags ffNonee ❑ Other
Thermometer: ❑ IR Gun ID: 16- --T Q 0 Z— Type of Ice: [Jwet ❑Blue
Cooler Temp ('C): Correction Factor. Add /Subtract ('C) '
Corrected Cooler Temp ('C): Zr - S
USDA Regulated Sall (❑ N/A, water sample)
old samples originate In a quarantine zone within the United States: CA, NY, or SC (check maps)?
❑Yes gNo
Date/Initials Person Examining Contents: f+S
Biological Tissue Frozen?
❑Yes []No ❑N/A-
❑ None
Temp should be above freezing to 6'C
❑Samples out of temp criteria, Samples on ice, cooling proce
has begun
Did samples originate from a foreign source (internationally,
— u•
Comments/Discrepancy:
Chain of Custody Present?
(�TYes
❑No
l]N/A
1.
Samples Arrived within Hold Time?
Yes
❑No
❑N/A
2.
short Hold Time Analysts (<72 hr.)?
❑Yes
RJNo
❑N/A
3.
Rush Turn Around Time Requested?
[]Yes
ErNa,
❑N/A
4.
Sufficient Volume?
9Yes
I]No
❑N/A
S.
Correct Containers Used?
-Pace Containers Used?
(lYes
Qsres
I]No
❑Na
❑N/A
❑N/A
6.
Containers Intact?
[TYes
EJNo
❑N/A
7.
Dissolved analysis: Samples Field Filtered?
[]Yes
[]No
nN/A
a,
Sample Labels Match COO
-includes Date/rime/ID/Analysis Matrix:
r (']Yes
U L
[]No❑N/A
9.
iieadspace In VOA Vials (>S-6mm)?
❑Yes
❑No
iUN/A
10.
Trip Blank Present?
Trip Blank Custody Seals Present?
[]Yes
I]Yes
❑No
[]Na
IW/A
NJA
11.
COMMkNI.-)/]AMi'Lt UF11:HtNANr.Y
Temp Log: Temp must be maintained
at <5 C during login, record temp
every 20 minutes.
Time opened: I q I G7 Temp:
Time: I Z ,C put in cooler
Time: Temp:
Person Contacted: _
Project Manager SCURF Review:
Project Manager SRF Review:
Qualtrax Document ID: 70677
Field Data Required? ❑Yes ❑No
Lot ID of split containers:
CLIENT NOTIFICATIONJRESOLUTION
Date/Time:
Date:
Date:
Page 1 of 2
Page 4 of 5

Hat:le Identification Form (8
P3,e 1 C i
t NJ.:
f-CAR•CS-C«3-P,ev.Cl
'Check mark tzp half of box if pH and/or dechlor2in3tion is
verified and within the acceptance range for preservation
samples,
Ex._• .crs:'i �-, C�li,�rn, Tyr, t;i: � ;� Cr_.�_, r>.'`!3:'S (,' _ __-) Cn-, {,� �,
*#8ot.om half of box is to ljst number of bottles
FciB ird: Clln3i CSJ3i � �-Ira
Proles t l
1owt� a F
J
1
4
C
?
Ll
V
Vej
lam+
u
c
C.
_
-
_
C
N
V
O
U
a
y
O
n
a
(�`
Q
N
r
G
rt
N
r+
k
N
W
c.
O
=
r
W1
N
rr
E
ry
ra
<
U
,-,
C
rK
C
�i
<
—
J
N
l3
0
>
o
>
c
>
Q
v
}
N
e
C
E
C
n
U
L
L
L
G
L
L
C
C
C7
C^
l7
.
<
<
N
U'
<
t2
<
U
c
0
>
V
>
toQ
G
>
`
iJ
7
n
t
v
N
N
N
ah
La
IZI\III
\\III\I\\\IIIlllll
I
I31\
III
\
I I\
I
I
I I
I
I
I
I
I\
NI
II
1\1
\1
I
1\1
I\
I
I
I
I
I
I
I\\
I51\III\
\
I
I
I\
I
III
1
1\
I\
1
1 1\\
\I
I
1\1
I\
I1
1
1
II\
\N
I
I I\ \\\
I
I......
I
\\
1
I
1
1
1
1
1
I\\
181
I
I I
N\1
F
I
\
I
I
I
III
I
I
I\I.
I\III
l
i
91
I"N
II
\\11
I
\kllk
1
11I\
I\1
I
I
I\\
I
-IN
N1`I\
\
k
I
I
I
I
I
I
1-1
NNNL\1
I
I
\I
\I
II
I
pi I iAuju5Lment Lo. for Freserved Samples
Sample Ifl
Type of Preservative
pH upon receipt
Data preser"dan aejustzd
Time preserrat on Amount of Pra5e040tive
adjusted added
Lot 9
Apr— WhaoaV�r
thora is .l diSr K+^.lnry —F—.1—
M—h r ..1:na
Out of hold, incorrect pre;erva vz, out of temp, Incorrect containers,
- --- - rrr •-...••a ��•„ ••,,. =•n w u,c raw us �a:wana utti�ii; Gerjr1catlon Off re (I.e,
Page 6 of 5

CD
a)
OD
It
N
aaa)
'th
O
3
U�
Fo,_
-
v_
Welul
_.-
(NIA)
_ =�='a
{N1A1cu4�aS401�P?�FJ
�
Z
:�
tiA
_
o
O-u? dVi3J.
ea7
Y
v
(09"6 Vd3) Hd
x
-
a3
z
:iu (f3UYLVd3)1Gnnsaµl
cA
U I 123
uogdi-qy
x
�'
_
—
(WS) aley uuipaS
!
tV 5
� �
_ 'Wnlsae=od're�plp!'wnuaR9RloW
x
_�
YunJsaudeN Pea-1'JaddzWnple�
'wrgwpeo jm!uV wnulwnlV
!
;=
ID
..
o�
(eonz YES) SmRs ieloi lueamd
x
` �
o
(VOC Vd3) sntoydsagd Ishii
¢ voyaynleo
= (NVd)ua_&VMQigaUeAV]uefd
a�i
(ZeSCVd3J'ZON EON {z lye
x
? y
Co
'+ dM NNJ. OM: Vd3) N-eHN
w
c
o
w C
'c
pueylaw
-
=_
tOlSZaN
o
ca
x
J
HOeN
-
_
N V
a
m
m
IOH
u� u�
m
m
o
'
a
6oszH
=`
=
d
penmmdufl
F
o a& y
o
G.
a
Z.
h e U
a
ei
a
='"
3i 171V1Naa j09
'�
—
.NOl1.o3"11c7JlY
dltc�l3biWV5
c
—"=�
�
�
m
f r F
O
y
Lil
o
C
D
Q
3, "
-�C
a'
ak
5 v
q
ti
�
a
G
�
O
c i Acn
(dWQ 96flFJ=JJ-3d.11.31dY1b9
U`
j
(u-]alSap=PJ ass) =-aooYJAL"
rJil
a
m
iq u F o
Q
a
o tea.
F
u
gg
$4�33a«o3gai_"
'
rn K o_ U
a
a`
a.
3 a
3$ 9
�033���s�$o�
::
N
co
1
t
m
-
IL
o
#
u
Q
C2 5
0
0
uj
c
e O
co
o
J
�S O o
m
a
G 12 4
m
p
�
_
a m
u U O
W
a
Page
tt IN0.l.I
1
ff
PIN?.
ac cL 4
E
w
.9G
a
cc
_
3of5

aceAnapieal
WWW.yacelabs.cam
Laboratory Report
Karen Reece
Town of Boone WWTP
PO Drawer 192
Boone, NC 28607
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 1 of 2
Report Date: 05/05/2023
Date Received: 04/20/2023
Project: Biosolids - Quarterly
Pace Project No.: 92663377
Sample: Biosolids tab ID: 92663377001 Collected: 04/20/23 08:55 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Method
EPA 6010D
EPA 6010D
EPA 6010D
EPA 60100
EPA 6010D
EPA 6010D
EPA 6010D
EPA 6010D
EPA 601 OD
EPA 6010D
EPA 6010D
EPA 6010D
EPA 60100
EPA 6010D
EPA 7471 B
SM 2540G-201i
SW-846
EPA 9045D
None
TKN+NO3+NO2
Calculation
EPA 350.1 Rev 2.0 1993
Mod.
EPA 351.2 Rev 2.0 1993
EPA 353.2 Rev 2.0 1993
EPA 353.2 Rev 2.0 i 993
EPA 353.2 Rev 2.0 1993
EPA 365.1 Rev 2.0 1993
ANALYTE QUALIFIERS
Parameters Results Units Report Limit Analyzed Qualifiers
Aluminum
Arsenic
Cadmium
Calcium
Copper
Lead
Magnesium
Molybdenum
Nickel
Potassium
Selenium
Sodium
Zinc
Sodium Adsorption Ratio
Mercury
Total Solids
Percent Moisture
pH at 25 Degrees C
Plant Available Nitrogen
Nitrogen
Nitrogen, Ammonia
Nitrogen, Kjeldahl, Total
Nitrogen, NO2 plus NO3
Nitrogen, Nitrate
Nitrogen, Nitrite
Phosphorus
14300
mgikg
105
05/0312318:25
Mi
2.6
mg/kg
2.6
04/26/23 01:21
1.1
mgikg
0.10
04/26/23 01:21
16300
mgikg
262
05/03/2318:25
M1
330
mg/kg
52.4
05103/2318:25
M1
12.0
mgikg
1.0
04/26/23 01:21
2470
mg/kg
W5
05103/2318:25
Mi
ND
mgikg
5.2
04/26/23 01:21
12.9
mg/kg
0.52
04/26/23 01:21
2610
mgikg
524
04/26/23 01:21
3.8
mg/kg
1.0
04/26/23 01:21
891
mgikg
524
04/26/23 01:21
616
mg/kg
1.0
04/26/23 01:21
M1
1.8
meq/L
05/0512311:40
N2
0.17
mgikg
0.011
0510112312:39
91.7
%
0.10
04/22/23 00:27
8.3
%
0.10
04/22/23 00:20
N2
6.1
Sid. Units
0.10
04/25/23 13:49
H3
18300
mg/kg
05/0412313:15
N2
59800
mg/kg
40.0
05/04/231317
1900
mg/kg
37.0
04/27/2312:38
59800
mg/kg
5450
05/04/23 08:02
ND
mgikg
4.3
04/22/23 04:15
M1
ND
mglkg
4.3
04/22/23 04:15
ND
mglkg
4.3
04122/23 04:15
M1
7320
mgikg
214
04124/2312:26
H3 Sample was received or analysis requested beyond the recognized method holding time.
Mi Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
N2 The lab does not hold NELAC/TNI accreditation for this parameter but other accredltations/certifications may apply. A
complete list of accreditationslcertiflcations is available upon request,
Reviewed by:
Stephanie Knott
704-977-0981
[e-mail]
Page 1 of 5

Iac
eAnalytical
www.pactiabs.tom
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Laboratory ID: 99006
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
FloridalNELAP Certification #: E87648
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification M 99006001
South Carolina Drinking Water Cert, #: 99006003
FloridalNELAP Certification M. E87627
Kentucky UST Certification #: 84
Louisiana DoH Drinking Water #: LA029
VirginiaNELAP Certification #: 460221
South Carolina Laboratory ID: 99030
South Carolina Certification #: 99030001
VirginiaNELAP Certification #: 460222
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 2 of 2
Page 2 of 5

F
4r-
ji
I
-I
kA1
"N
Ll
(MA)
RE
z
MVIOU
0
Ut dVI;U
V6
(Gom yda) -M WWPOS vinluolfs
1410"
WDKZ 44S) VPNOS PRO), IUQILMd
(wa)
ZOWWN ��Iv
tit
IL
=
Vdal WA,(L,m Y.13) N-CNN
rr
MAO
ro
con
o
kogN
MH
ji
tONN
0
cl
24
WSW
P--AlUn
0
tip
A'
SU3AY"4W A'Q 0
RM33MO LY dMM TWOS
LL
v-
'CP
It.
6m .1 VNM pw- -4 wcrj mly"
4-A
to
eq
W 20
9
IL
2
#
I
IN,
-1;�"i,
SN
a
Page 3 of 5

/� I3G#_Tit1e,. ENV-FRNI-HUNI-0084 vOl Tech Spec Sample condition
r�� t'ace- Upon Receipt
u.:•.c"r�..�l Effeotivo Data, 0511212022
aboratory receiving samples;
,Sheville Q Eden Q Greenwood ❑ Huntersvilte Q Raleigh❑ Mechanicsville❑ AtlantaQ KernersviileV
Client Name:
Project q:
:Dueler; []Fed Ex []UPS U ❑LISPS QClient
I Commercial [ Pace ❑Other:_
:arrier Tracking Number
�ustody Seal Present? QYes Seals Intact? QYas []NO Date/Initials Person Examining Contents:
asking Material: ❑Oubble Wrap ubbie gags ❑None ❑ otner Biological Tissue, —F.r��ozen?
QYes QNo ram. tv/A
hermameter. Cl iR Gun in a Type or t__ceff at ❑ aiuc ❑?la«e
Toler Temp (•C ):�+ ,� _ Correction factor; Add / Subtract ('C ) `V ' _ Temp should be above freezing to 6'C
� ❑p 5amp!es out of tamc<Oeria. Samples on lce. coo sng pro
orrected Cooler Tpmp ("C 1: J `-� has begHn
SDA Regulated Soil (Q NJA, water sample)
Id sampl�es or irate ;n a quarantine tone within the United 5ta es: CA, NY, or SC (check maps)? Did samotes otleirate film a foreign source ltrterna; ova ly.
]Yes t`xi'+o _ lrc:sding 93wail and Puerto Rico)? QYes
Chain of Custody Present? wet l_1No ]N/A I 1-
Samples Arrived within Hold Time? Yes [_—)No ❑NJA 2, _
Short Hold Time Analysis (<72 hr.)? es []No� ❑NJAA 3 _
Rush Turn Around Time Requested? `(]Yes I4o ❑NJA tt a
rDisscilhmd
?ent Vo:ume' T CiKes ONO QNJA 15:
ct Cartaners Used? IQ+" �s j]No QN/A 6.
ac? Containers Used? es ❑No _❑N/A
ainers tritact? Yes ONO ❑N/A 7.
analysis: Samples field_ Filtered? Oyes QNo . /A 6.
1 Sample Labels klatch COC? WI -es ONo QN/A J 9.
L -includes Date/Time/ID/Analysis Matrix:_ I h+ ( i
HeadspaceInVOAVialsl>5-6mm)? Qlei ❑No A 10.
Trip Blank Presanl? QYes ON. CaWA 11.
Trip Blank Custody Seals Present? ❑Yet []NO QRKA
COMMENTS/SAMPLE D15CREPANCY field Data Required? Oyes ONO
Temp Log: Temp must be maintained
at <6 C during login, record temp
every 2D minutes,
Time opined: Temp. ,
p put in coot et r�
Time: Temp:
Person Contacted, —
Project Manager SCURF Review,
Project Manager SRF Review:
Quallrax Document ID: 70677
Lot 10 of split containers:
CLIENT NOTIFICATION/RE50LU7ION
Date;
Date:
Page 1 of 2
Page 4 of 5

DC#_Title: ENV-pRM-HUN1-0084 v01_Tech Spec Sample Condition
' -t'CB Upon Receipt
r-J•,otst—ts I Effective Date: 0511212022
*Check mark top half of box if pH and/or dechlorination Project #
is verified and within the acceptance range for
preservation samples,
Exceptions,. VOA, Collform, TOC, Oil and Grease, DRO/8015 (water) DOC, UHg
"Bottom half of box is to fist number of bottles
***Check all unpreserved Nitrates for chlorine
z
4
a
aS
a
N O
ti
V
2
x
N
N
`
M
Z
�Z
S
wW
N
4.
.qw
n
ro
a
.ro.
`
a
v
n
n,
CL
a
a
O
d
a
=
?
¢
Z
M�`
�
2
N
a a
V
7
V
5
V
C
7
N
=
V
Z
V
b
V
C
7
tJ
=
y
0
i
..
tj
N
G
M
N
..'.
z
n
O
C
V
.iJ
a
£
11/y�
o
E
pO
w
N
Vryf
N
=
G E
,On
N
E
O
E
tl
E
O
�T
b
a_
}
J
E
N
E
tl
f
N
o
O
E
obf
J.
E
t=
a
rl
�
V
N
7
M
U1
�
N
.d
�
ei
.it
4
�.'
M
N
V
H
�
•t
W
V•
3
�-I
r�
rl
rl
M
t9
rt
l7
N
M
(D U'
4T
L�
0
q
tl1
U'
Of
cl
Of
.Mn
t:)
H
N
F•
N
M
O
a
(J
>
Ot
o
m
m
m
m
m
61
R1
m
¢
a
a
a
x G
a
>
>
n
o
>
v�
w
as
1
�
—
2
3
4
5
N
I
\\N\
6
9
1D
11
12
_FF,
pH Adjustment
Log for preserved Samples _
Sample to Type of Preservative
pH upon recelpt
Date preservation adjusted
Time preservation I Amount of Preservative
adjusted added
lot 11
Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification 011ice lLe.
Out of hold, Incorrect preservative, out of temp, incorrect containers)
Qualtrax Document ID: 70677
Page 2 of 2
Page 5 of 5

�41ace,
Laboratory Report
Karen Reece
Town of Boone WWTP
PO Drawer 192
Boone, NC 28607
Project: Town of Boone - Blosollds
Pace Project No.: 92677254
Pace Analytical Services, LLC
1377 South Park Drive
Kernersviite, NC 27284
(704)977-098t
Page 1 of 2
Report Date: 08/02/2023
Date Received: 07/13/2023
Sample: Blosolids
Lab ID: 92677254001 Collected: 07/13/23 10:30 Matrix: Solid
Results reported on a "dry weight' basis and are adjusted for percent moisture, sample size and any dilutions.
Method
Parameters
Results
Units
Report Limit
Analyzed
Qualifiers
EPA6010D
Aluminum
18600
mg/kg
100
07/31/23 12:04
EPA6010D
Arsenic
3.4
mg/kg
2.5
07/24/23 18:25
EPA6010D
Cadmium
1.2
mg/kg
0.10
07124/23 18:25
EPA 601OD
Calcium
19300
mg/k9
251
0713112312:04
EPA6010D
Copper
492
mg/kg
5.0
07/24/23 18,25
EPA6010D
Lead
17.4
mg/kg
1.0
07/24/23 18:25
EPA6010D
Magnesium
2760
mg/kg
10.0
07/24/23 18:25
EPA6010D
Molybdenum
ND
mg/kg
5.0
07/2412318:25
EPA60100
Nickel
14.9
mg/kg
0,50
07124/23 18:25
EPA6010D
Potassium
2770
mg/kg
502
07124/23 18:25
EPA6010D
Selenium
5.3
mg/kg
1.0
07124/23 18:25
EPA 601 OD
Sodium
789
mg/kg
502
07/24/23 18:25
EPA6010D
Zinc
822
mg/kg
1.0
07/2412318:25
EPA6010D
Sodium Adsorption Ratio
1.5
meq/L
08/02/23 16:05
N2
EPA7471B
Mercury
0.36
mg/kg
0,030
0712812313:11
M1,R1
SM 2540G-2011
Total Solids
83.0
%
0.10
07/17/23 16:17
SW-846
Percent Moisture
17.0
%
0.10
07117/23 16:10
N2
EPA 9045D
pH at 25 Degrees C
6.0
Sid, Units
0.10
07/20/23 13:06
H3
None
Plant Available Nitrogen
10700
mg/kg
07/22/23 11:51
N2
TKN+NO3+NO2
Nitrogen
34800
mg/kg
40.0
0712212311:58
Calculation
EPA 360.1 Rev 2.0 1993
Nitrogen, Ammonia
1370
mg/kg
21.1
07/20/23 12:46
Mod.
EPA 351.2 Rev 2.01993
Nitrogen, Kjeldahl, Total
34800
mg/kg
2410
07/22123 06:05
M1
EPA 353.2 Rev 2.0 1993
Nitrogen, NO2 plus NO3
NO
mg/kg
4.7
07/14/23 23:56
EPA 353.2 Rev 2.0 1993
Nitrogen, Nitrate
NO
mg/kg
4.7
07/14/23 23:56
EPA 353.2 Rev 2.01993
Nitrogen, Nitrite
NO
mg/kg
4.7
07/14/23 23:56
EPA 365.1 Rev 2.0 1993
Phosphorus
15700
mg/kg
269
07/27/23 12:20
M1
ANALYTE QUALIFIERS
H3 Sample was received or analysis requested beyond the recognized method holding time.
M1 Matrix spike recovery exceeded QC limits, Batch accepted based on laboratory control sample (LCS) recovery.
N2 The tab does not hold NEt.AC/TNI accreditation for this parameter but other accreditations/certifications may apply. A
complete list of accreditations/certifications is available upon request.
R1 RPD value was outside control limits.
Page 1 of 5

(��Flaca'
Reviewed by:
Stephanie Knott
704-977-0981
[e-mail]
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Laboratory ID: 99006
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
FloddalNELAP Certification #: E87648
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99006001
South Carolina Drinking Water Cert. #: 99006003
FloddalNELAP Certification #: E87627
Kentucky UST Certification M 84
Louisiana DoH Drinking Water #: LA029
VirginlaNELAP Certification #: 460221
South Carolina Laboratory ID: 99030
South Carolina Certification #: 99030001
VirginlaNELAP Certification #: 460222
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 2 of 2
Page 2 of 5

a
z
H
�
m
q
roa
� g
m
-w
go
R
� q
a�
y
9
V
� N
LL (
1
4
1
1
1
R
al
m
Ri (WA) -POM3 "It.d z
.(UWM Vd�) Nd x
(Ht4l'LVda)Ao—A x
(ilVS)Q wauogdj" 'PQS
ae vdd) � '�!Po5 '4O1F1°IaS
'Iwnngod'I�MI''�nwPa�pMl
nauboy( `Prtll'��ddo'J tiutPitl'J
LInpW wJ'�uauy'umvlulPN
(JO zws)+PIItl31 pLPww*d x
( 9K Yd3) snwydca(d IQWi
U04tlMglp x
(NWd) U46MV Q?gsil-'Y MW
(Z'tStVdq)ZQN•GON'(Z'(S£ x
vd3) NNI'Won wal N-"
i9U10
puapeyy
COZSZtlN
N N
EON
u tow
POSZN
Panasad�ft `
9y3NrylltO�dC1� '
2
F
W
O
(dY1QY.14YNOW% iidFl 3'idW1S
(09101ggt� OW �) iIQ(YJ XIHiVMI
8$"s�C.:�iiSE
3
O
fi e
N
0 WBII
(wA)
KIoIUE
-Idwws
(wA)
)9mo
PBIeaS
n
(wA)
uo pw{o�a,y
s
z`
Page 3 of 5

v �.. n- $ LM. "I• V -1 Novo —I I%Jft 1"VVV^r V V I —I rst.11 Qvvq.: Jd IIIPIV Lrullu It IV II
ace, Upon Receipt
M.Itr.$4 ras Eftective Date; 0511212022
Laboratory receiving samples:
Asheville ❑ Eden ❑ Greenwood ❑ Huntersviile ❑ Raleigh❑ Mechanicsville[] Atlanta❑ Kernersviile
Sample Condition Upon Client Name:
Recelpt T o W y� p { (,� D 0 YvQ Project ff: 0 ,
f� l
Courler: ❑F d Ex ❑UPS ❑USPS ❑Client
❑ Commercial rPaPace [—]other:
—
Carrier Tracking Number:
Custody Seal Present? ❑Yes E3No Seals Intact? []Yes ONO Data/Inittals Person ExaminingContents:
Packing Material: [:]Bubble Wrap / Bubble gags ❑None ❑ other Biological Tissue Frozen?
[]Yes ONO ❑N/A
Thermometer; El III Gun 14: K4 T D 0 2 Type of Ice; d Wet []Blue❑ Node
:ooler Temp ('C )- -? Correction Factor. Add /Subtract ('C) ' 1 Temp should be above freezing to 6'C
Corrected Cooler Temp ('C ): 3' U ❑Samples out of temp criteria. Samples on ice, cooling proce
has begun
USDA Regulated Sall (❑ N/A, water sample)
Did samples originate in a quarantine zone within the United States: CA, NY, or SC (check maps)? Did samples originate from a foreign source (internationally,
❑Yes ONO Including Hawaii and Puerto Rico)? []Yes ONO
Comments/Olscrepanty:
Chain of Custody Present?
es
No
ONJA
1.
Samples Arrived within Hold Time?
Yes
[]NO
❑N/A
2.
Short Hold Time Analysis (<72 hr.)?
[]Yes
OiNa
❑N/A
3.
Rush Turn Around Time Requesled7
[]Yes
QNo
NIA
4.
SuMclent Volume?
cryes
No
N/A
S.
Correct Containers Used?
-Pace Containers Used?
[ Yes
Yes
❑No
No
❑N/A
N/A
6.
Containers Intact?
Yes
❑No
❑N/A
7.
Dissolved analysis: Samples Field Filtered?
❑Yes
❑No
UNJA
8.
Sample Labels Match COO
-Includes Date/Time/ID/Analysis Matrix:
[3Ies
u I-
[]No
❑NIA
9.
Headspace In VOA Vials (>5-6mm)7
Yes
No
JA
lo.
Trip Blank Present?
Trip Blank Custody Seals Present?
❑Yes
Yes
❑No
QNo
3-N/A
ONJA
it.
COMMENTS15AMPLE DISCREPANCY
Temp togs Temp must be maintained
at <6 C during login, record tamp
every 20 minutes.
Time openedP-1 LJ J Temp: 3,1
Time;ic( 4 ' T put in cooler
Time: Temp;
Person Contacted:
Project Manager SCURF Review:
Project Manager SRF Review:
Qualtrax Document ID: 70677
CLIENT
Field Data Requlrad7 ❑Yes ❑No
ID of sDIlt conta
Date/Time:
Date:
Date:
Page 1 of 2 Page 4 of 5

Document Name;
Document Issued: November 15, 2021
Bottle Identificatlon Form (DIF)
Page 1 of 1
Document No.:
Issuing Authority:
/ _.- ace�ralyticall
F
F•CAR•CS•043•Rev.01
pace Carolinas Quality Office
*Check mark top half of box if pH and/or dechlorination is
verified and within the acceptance range for preservation
samples.
Exceptions: VOA, Coliform, TOC, Oil and Grease, ORO/8015 (water) DOC, LLHg
"Bottom half of box is to list number of bottles
Project #
m
a£r
U
SSZ
'U
d
$
E
y
m
a
E
�
y
m
V
N
a
S
LL
m
4
u
L
o
j
I
.yu.
A
m
D
V
O
o
J
£
aA3
V
?
p
n
J
£
d
m
x
2
di
1�
4
a.
J
E
'
'a
N
A
a
x0
n.
J
E
d
m'
yy
O
ro
ro
E
v
M
T]
E
K
5
a
V
V
E
Q
.�
t'l
4
Z
£
q
J
E
0
1n
47
4
_
O
£
q
.emu
J�
t�
4
N
vOi
d
J
E
4
Z
�'
Q
ld.1
47
a
O
J
E
x
L�7
o
O
O
5
E
?
`
O
J
E
>
a
4
E
in
0
o
a
'�
^
O
7
Z
N
°
7
A
V
Yn
J
E
vt
N
u
.J
E
d
In
M
NN
x
£
a
m
>
c
£
E
MEE
l�tl
¢
T
c
c
J
r�i,
}
N
n
J
l7
o
1
2
3
4
\N
NN6
7
e
9
10
11
12
pH Adjustment
Log for Preserved Samples
Sample ID
Type of Preservative
pH upon receipt
Date preservation adjusted
Ttma preservation
adjusted
Amount of Preservative
added
Lot A
Mote: Whenever there Is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the Norm Larouna ucnnn Lenurcauon untce Ilm.
Out of hold, incorrect preservative, Out of temp, Incorrect containers,
Page 5 of 5

ace°
Welcome, Kenneth Howell
Change Password Provide us Feedback bout
Home Container0rders Results EDOS Data Notifications Resources Help
Project information
client Project: Town of Boo ne Blosollds TS
Profectstalus: Complete
1.
Pam "act Nbr: 92680924
Matrix: Saud
Sample: Blosolids
CotiectedDate: 08103/2023
Labid• 92680924001
Received Data: 0810412023
Methods
Anatysra
Method Casa
254OG Total Percent Solids SM25400-2011
- Complete
Percent Moisture SW-846
complete
Shaw Hits Only
Ouory by 1�tothod
Result List
_
RL=Report Limit, MDL-Method Detection Limit, DF=Dilution Factor, Bas=Basis, Oual-Qualifiers
. Method Des¢
Parammors Results
UnIN
RL
MOL
DF
Anatymd Dato
Dos
Qual
SM25:- 0111 Total Solids 93.1 91, 0.10 0.000010
1 08/071202314:30
Wet.
SW-848 PercentMoislure 6.9 °!0 010 0.10
1 0810712023tA:22
Wet
Comment List
No Resuhs Found
Last login: Wed Aug 09 OS:26.42 CDT 2023 Terms of Service Copyright © 2023. Ali Rights Reserved.

Yace-
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Laboratory Report
Karen Reece
Town of Boone WWTP
PO Drawer 192
Boone, NC 28607
Project: Town of Boone - Biosolids
Pace Project No.: 92691715
Page 1 of 2
Report Date: 10/24/2023
Date Received: 10/05/2023
Sample: Biosollds Lab ID: 92691715001 Collected: 10/05/23 10:00 Matrix: Solid
Results reported on a 'dry weight' basis and are adjusted for percent moisture, sample size and any dilutfons.
Method
EPA 6010D
EPA 601 OD
EPA 601 OD
EPA 601 OD
EPA 601 OD
EPA 601 OD
EPA 601 OD
EPA 6010D
EPA 6010D
EPA 6010D
EPA 601100,
EPA 6010D
EPA 60100
EPA 601 OD
EPA 7471 B
SM 254OG-2011
SW-846
EPA 9045D
None
TKN+NO3+NO2
Calculation
EPA 350.1 Rev 2.0 1993
Mod.
EPA 351.2 Rev 2.0 1993
EPA 353.2 Rev 2.0 1993
EPA 353.2 Rev 2.0 1993
EPA 3531 Rev 2.01993
EPA 365.1 Rev 2.0 1993
ANALYTE QUALIFIERS
Parameters
Aluminum
Arsenic
Cadmium
Calcium
Copper
Lead
Magnesium
Molybdenum
Nickel
Potassium
Selenium
Sodium
Zinc
Sodium Adsorption Ratio
Mercury
Total Solids
Percent Moisture
pH at 25 Degrees C
Plant Available Nitrogen
Nitrogen
Results
Units
17000
mg/kg
2.8
mg/kg
1.4
mgtkg
16700
mg/kg
486
mg/kg
17.8
mglkg
2460
mglkg
NO
mg/kg
15.6
mg/kg
2240
mg/kg
5.0
mg/kg
1070
mg/kg
885
mg/kg
2.1
meg1L
o.44
mg/kg
91.2
%
8.8
%
6.2
Std. Units
11000
mglkg
35800
mg/kg
Report Limit
Analyzed
Qualifiers
102
10/18/2317:45
M1
2.6
10117/23 16:00
0.10
10/17/23 15:00
256
10/18/2317:45
M1
5.1
10/17/23 15:00
1.0
W117123 15:00
10,2
10/17/23 15:00
5.1
10/17/23 15:00
0.51
10/17123 15:00
512
10117/23 15:00
1.0
10117/23 15:00
512
10/17/23 15:00
1.0
10/1712315:00
M1
10119/2317:00
N2
0.021
10/10/23 13:35
0,10
1010012316:45
0,10
10109/2316:38
N2
0.10
10/19/2316:19
H3
10/18123 13:41
N2
40.0
10/18123 13:35
Nitrogen, Ammonia
1490
mg/kg
52.7
1 Oil1123 09:40
Nitrogen, Kjeldahl, Total
35800
mg/kg
4980
10/18123 06:49
Nitrogen, NO2 plus NO3
NO
mg/kg
4.3
10107/23 03:03
Nitrogen, Nitrate
ND
mglkg
4.3
10107/23 03:03
Nitrogen, Nitrite
ND
mglkg
4.3
10/07/23 03:03 M1
Phosphorus
16000
mg/kg
274
10/10/2312:04
H3 Sample was received or analysis requested beyond the recognized method holding time.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
N2 The lab does not hold NELAC/TNI accreditation for this parameter but other accreditations/certifications may apply. A
complete list of accreditations/certifications is available upon request.
Reviewed by:
Arnie Ferguson for
Stephanie Knott
704-977-0981
stephanie,[e-mail]
Page 1 of 5

(�V'aCeo
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification M 37706
North Carolina Field Services Certificatlon #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Laboratory ID: 99006
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
FloridalNELAP Certification M E87648
North Carolina Drinking Water Certification M. 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99006001
South Carolina Drinking Water Cert. #: 99006003
FloridalNELAP Certification #: E87627
Kentucky UST Certification #: 84
Louisiana DoH Drinking Water #: LA029
VirginiaNELAP Certification #: 460221
South Carolina Laboratory ID: 99030
South Carolina Certification #: 99030001
VrginiaNELAP Certification #: 460222
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 2 of 2
Page 2 of 5

'�'
3{'r
1wlJxwa�u�teat�4saa z
�..�
f z
(aerilYd3)+oY+ x
r�
u°A�lm x
.-CD wr��
(tlYSloloauoadrosm'uln�og
i' �•,
�i".
((0309Yd3)gW'wn!M'tUnFn s
'AulYs9e�ai'IaSpIN'wlluspq/aoy; x.
w4
,� 'wnpRu4aW'Mol'��°'J'�olaJ
jfumy,—"ry
CD
+'
T M/owN
(DOKZ rAS) tows Mai Nam!
WSK Yd3) <nloWMWd MOO
E $
-
WpVItrJ1V� x
(NYd)«a6°�INORIO NvAld
Q.�
(ZCSCYd3) ZON LON'(Z tSC x
w E
a
0. >c
Yd91 NSU.' VOSC Yd3) N-CHN
v c
Q�
m
IOyIQ
N�RAnYI
m
N C$ �
mzwm
)aj O
m
HOON
RSi
C: Z)
c m� � N
7 V F'
� MH
m
LON1i
Q Q pC
tOSZH
�
v � z .� � •
pwlwwduh v
SN3MYl1to0 dD
4 a
?Oi1 moo 1Y mu TUVVVS
(� o?
U�
U-
S
—
a
o
r
wwo aYu�) eaiu 31dMW
az
Qp49'�mm-4 Raco ml1YW
Q
O
C f
a
S
Y
a°e c'S
a
a
v`A oe
j
3gg �
14
a
14
e
Cl
W
14
t
IL
c
> a
g
rn
t
� r
Av o fl W3J1
ar _-
{wik)
Wgtvl.
eobwag
Guu
Npa�
Paw�S
4w�1
�I
uo pc�vww)3
ouldW31
M
Y
a
Z
Page 3 of 5

L Document Name:
Document Revised: November 15, 2021
aceAI)31y 1Gai
Sample Condition Upon Receipt ISCUR)
Document Na.:
Page 1 of 2
_ issuing Authority:
F-CAR•CS•033-Rev.08
Pace Carolinas Quality Office
Laboratory receiving samples:
Asheville ❑ Eden❑ Greenwood ❑ Huntersville [] Raleigh❑
Mechanicsville❑ Atlanta❑ Kernersville❑
5ample Condition Client Name:
Upon Receipt Project q: O d r e
1
Courier; ❑Fed Ex []Ups ❑USPS ❑Client
1
❑ Commercial (Apace ❑Other:
Custody Seal Present? []Yes dNo Seats Intact? []Yes ❑No
S
Date/Initials Person Examining Contents:
Packing Material; []Bubble Wrap ❑Bubble Bags [None ❑ other
Biological Tissue Frozen?
Thermometer: �/
r o 7 L1Wet ❑Blue
[]Yes ❑No ❑N/A
❑None
❑ tR Gun 10: O
_ Type of Ice:
Correction Factor:
Cooler Temp: AddAubtract ('C) r i
Temp should be above freezing to 6'C
[]samples out of temp criteria. Samples an ice, cooling process
Cooler Temp Corrected ('C),
has begun
USDA Regulated Soll (�/A, water sample)
Did samples ( i ' ate In a quarantine zone within the United States; CA, NY, or $C Icheck maps)?
Did samples originate from a foreign source Ilnternationally,
rt,.,.. t 7fni,,
inctudina Hawaii and Puerto Ricol? ❑Yes [?�a
Chain
Samples Arrived within Hold Time?
(3Yes
❑No
❑N/A
2.
She,,,Hold Time Analysis (02 hr.)?
[$Yes
❑No
❑N/A
3.
Rush Turn Around Time Requested? r
Oyes
Dfio
❑NIA
4.
Sufficient Volume?
E]Yes
❑No
ON/A
S.
Correct Containers Used?
-pace Containers Used?
dYes
ClYes
[)No
❑No
❑NJA
N/A
6.
Ict?
[Yes
❑No
QN/A
7,
sis: Samples Field f iitered?
❑Yes
❑No
EjNJA
8.
Match COO
atefTime/IDJAnalysis Matrix:
r,.-ln,1,des
[4Yes
kp1rr
❑No
❑NJA
9.
VOA Vials (>5-6mm)?
Yes
[]No
NJA
10.
Trip Blank Present?
[]Yes
❑No
EEah/A
I 11.
Trip Blank Custody Seals Present?
COMMENTS/SAMPLE DISCREPANCY
Lot t0 of split containers;
CLIENT NOTIF ICATION f RESOLUTION
Person contacted:
project Manager SCURf Review;
Project Manager SRF Review:
Date/Time:
Date:
Date:
Field Data Required? ❑Yes ON.
Page 4 of 5

'' ;aceftlylical
Document Name: Document issued: November t5, 2021
Bottle Identification Form (BIF) Page 1 of 1
Document No.:
F-CAR•CS-043-Rev
"Check mark top half of box if pH and/or dechlorination is
verified and within the acceptance range for preservation
samples.
Exceptions: VOA, coliform, TOC, Oil and Grease, ORGISO15 (water) DOC, LLHg
"Bottom half of box is to list number of bottles
Project q
Issuing Authority'
Pace Carolinas Quality Office
u
d
a y
Oi 0!
4
CLUE
c c
�u n
E E
.n o
.N-t N
�
n� d
ru rD
Q
Z
C3 O w
2 N
u V v V y �' _
V O u 2 ,e
c a Z O
2 U
.o ee a
a J J J V
E ? E E E E v
v ._ ,n o ,n to ?
H ,N.i NN., .N.1 ?
7 7 of Z N m u�.
a a a A a
to co m to m 3
v
d
u
IL
>
E
d
_
r1
7
ri
C%
Q
U —u
fV V f. i
n q O a
'� S = Q
it a N
E -, E Q ri
Q C d .1 Q
C v E n
� ,9i .- o '�
N f� ,.., N
S 7 N
.-� M m
lh t9 h t7
d 4 d 4
`
Q p U
U N g
O O Q
} j
E E >
o 0
7 q `r
m ai u+
l7 l7 t9
'a } >
_
Z �e
d O a
O
j p y
E y m
0
m 4 c7
t7 O r
A > 7
= a
`� ✓.
E E
'^ v
N N
r1 a
N h
z
r1 U
= c
a vC
v
m
n tq9
eo 4
z
`
U
:e
c 4
Q
E E
o 0
m Q
> 4
1
�
2
3
\N
I
5
NN
\d
N
\N
I
I
\N
6
1
N
—
\N
1
7N\N
—
N
I
N
�\M
8
11
1\\
N;��\N
I
-
I
-
--L\N—LL
::��
-
I
[-\[��N
I
-]
I
I
I-
NNJJ
pH Adjustment
Log for Preserved Samples _
Sample 10 Type of Preservative pH upon receipt
bate preservation adiusted Time preservation Amount of Preservarive Lot it
adiusted added
Notes whenever there is a discrepancy affect ng North Carolina compliance samples, a copy of this form will be sent to the North Carolina 0£HNR Certification office p.e.
Out of hold, incorrect preservative, out of temp, incorrect containers
Page 5 of 5

• 1 211M IT, mill 1 1•• • o,:Town Of :•• rlI pa
MAR/01/202ARD 12:38 Ph PAR No. P, 002/002
WATER (QUALITY LAB & OPERATIONS, INC.
P.O. BOX 1167
BANNER ELK, NO 28604
[phone]
CLIENT: TOWN OF BOONE WWTP
ADDRESS: P.O. BOX 192
CITY: 130ONE RECEIVED DATE: 19-Jan-23
STATE: NO ZIP 28607 REPORTED DATE: 27-Feb-23
ID#: NCO020621
ANALYSIS
LSID #
ANALYSIS
MQL's
UNITS
SAMPLE
ANALYSIS
INT
RESULTS
LOCATION
COMPLETED
TOTAL. SOLIDS
1
90.6
%
SLUDGE
FECAL COLIFORM
228
MPN/q
SLUDGE
20-Jan-23
PI
TOTAL SOLIDS
2
91 A
%
SLUDGE
FECAL COLIFORM
440
MPN/p
SLUDGE
20-Jan-23
PI
TOTAL SOLIDS
3
90.6
%
SLUDGE
FECAL COLIFORM
318
MPNIg
SLUDGE
20-Jan-23
Pi
TOTAL SOLIDS
4
92.1
%
SLUDGE
FECAL COLIFORM
454
MPN/g
SLUDGE
20-Jan-23
PI
TOTAL SOLIDS
5
92.4
%
SLUDGE
Fr -CAI. COLIFORM
280
MPNIg
SLUDGE
20-Jan-23
PI
TOTAL SOLIDS
6
91.6
%
SLUDGE
FECAL COLIFORM
266
MPNIg
SLUDGE
20-Jan-23
PI
TOTAL SOLIDS
7
91.4
%
SLUDGE
FECAL COLIFORM
410
MPNIg
SLUDGE
20-Jan-23
PI
REPORTED BY: NO CERTIFIED LAB # 544
PAUL ISENHOUR, SUPERVISOR

.• A. 1•• • • :•• •tin P .
MAR/01/2023/WED 12:37 PM FAX 110. P, 001/002
WATER QUALITY SERVICES, INC.
P.O, 'E3OX 1102, BANNER ELK, NC 26604
(828) B98-6277
fax (828) 898r6255
TYPE SAMPLE; WAS CHAIN OF CUSTODY
LOCATION; f
CI, � � S�p I?F�ESERVATION CODE '
FACILITY ID #: I - H2SO4, 2 - HNO3, 3 - HCL,
.SAMPLER NAME: pw 0 - obtij _. 4 - NAOH, 5 - NONE, 6 - COOL ICI=
:OMPOSITE SAMPLE; START rrne __ 7 NA2S203, 8 ` OTI^IER
containers leaving the lab, unless otherwise noted.�asC�vazroes error to sarnpie
CL2-0-CL2= Chlorine check and dechlortrfation verification: `*
RESERVATION:
I COOL, 4C.: BOD, RESIDUE, CONDUCTIVITY, WAS, COLOR, ALKALINITY, CR, VI, TURBIDITY
I COOL 4C, PH<2 H2s04 : NH3, NO2-NO3, TKN, O&G, TOC, COB, HARDNESS, PHF-NOLS, TOT PHOS,
I COOL 4C, PH<2 HNO3 :.METALS except CR, VI
) NONE: CHLORIDE, PH, FLUORIDE rHP-R: SAMPLE DEVIATION:
j,VCOOL 4C, NA28203 : COLI)"ORM BACTERIA
NOTIFICATION;

•• �. 1 1� -• � • • .•• fTTT � •.•-
MAY/15/2023/MON 02:33 PM FAX No, P.002/002
WATER QUALITY LAB & OPERATIONS, INC.
P,Q. SOX 1167
BANNER ELK, NO 28604
[phone]
CLIENT: TOWN OF BOONE WWTP
ADDRESS: P.O. SOX 192
CITY: BOONE RECEIVED DATE: 20-Apr-23
STATE: NO, ZIP 28607 REPORTED DATE: 15-May-23
ID#: NCOU20621
ANALYSIS
LSID #
ANALYSIS
MQL's
UNITS
SAMPLE
ANALYSIS
INT
RESULT$
LOCATION
COMPLETED
TOTAL SOLIDS
1
90.1
%
SLUDGE
FECAL COUFORM
444
MPN/
SLUDGE
21-A r-23
PI
TOTAL SOLIDS
2
91.1
%
SLUDGE
FECAL COLIFORM
350
MPNlg i
SLUDGE
21-Apr-23
PI
TOTAL SOLIDS
3
90.5
%
SLUDGE
FECAL COLIFORM
412
MPN/
SLUDGE
21-Apr-23
PI
TOTAL SOLIDS
4
91.6
°/a
SLUDGE
FECAL COLIFORM
388
MPN/
SLUDGE
21-A r-23
PI
TOTAL SOLIDS
5
91.8
%
SLUDGE
FECAL COLIFORM
322
MPN/g
SLUDGE
21-A r-23
PI
TOTAL SOLIDS
B
903
%
SLUDGE
FECAL COLIFORM
370
MPNIg
SLUQGF,
21-Apr-23
I PI
TOTAL SOLIDS
7
90.4
%
SLUDGE
FECAL COLIFORM
L 318
MpNq
SLUDGE
1 21-A r-23
REPORTED BY: NO CERTIFIED LAB # 544
PAUL ISENHOUR, SUPERVISOR

MAY/15/2023/MON 02:32 PM FAX No, P,001/002
WATER QUALITY SERVICFS, INC.
P.O. BOX 1102, BANNER I=LK, NC 28604
(828) 89B..6277
fax [phone]
CHAIN OF CUSTODY
TYPE SAMPLE: WASTEWATER " PRESERVATION CODE
LOCATION: CL 5'rbKAGF- jgA 1 - H2504, 2 - HNO3, 3 - HCL,
FACILITY It) # C 6a 4 - NAOH, 5 -NONE*, 6 - COAL ICESAMPLER NAME: QW rJ p - BDa�.11~ 7 - NA2S203, 8 - OTHER
:OMPOSITE SAMPLE; START TIME: ; STOP TIME' le
rt"1Nk-2U15rik1J BY: I DATE I TIME ( R=CEIVEQ BYE naTPTIf nG
DATE I TIME I a n av I r- rG I "K
-- '.aoorazory preservation Is ensured by addition of preservatives prior
conttainers leaving the lab, unless otherwise noted.
CL2-P-CL2= Chlorine check and dechloririation verification. -4
RESERVATION;
I COOL 4C. BOD, RESIDUE, CONDUCTIVITY, M13AS, COLOR,.ALKALINITY, CR, VI, TURBIDITY
I COOL 4C, PH<2 H2SO4: NH3, NO2-NO3, TKN, 0&0, TOO, COD, HARDNESS, PHENOLS, TOT PHOS.
I COOL 4C, PH<2 HNO3 : METALS except OR, VI
I NONE: CHLORIDE., PH, FLUORIDE SAMPLE DEVIATION:
rHER:
-jkQOL 4C, NA2S203 ; COLIFORM 13ACTE.RIA
NOTIFICATION:

AU6/03/2023/THU I I : I I AM FAX No. P.002/002
WATER QUALITY LAS S OPERATIONS, INC.
P.O. BOX 1167
BANNER ELK, NC 28604
[phone]
CLIENT. TOWN OF BOONE WWTP
ADDRESS: P.O. BOX 102
CITY: BOONE RECEIVED DATE: 20-Jul-23
STATE: NC ZIP 28607 REPORTED DATE: 3-Aug-23
ID#: NCO020621
ANALYSIS
LSID #
ANALYSIS
MQ129
UNITS
SAMPLE
ANALYSIS
INT
RESULTS
LOCATION
COMPLETED
TOTAL SOLIDS
1
92.1
%
SLUDGE
FECAL COLIFORM
338
MPN/g
SLUDGE
21-Jul-23
PI
TOTAL SOLIDS
2
90.8
%
SLUDGE
FECAL COLIFORM
380
MPN/p
SLUDGE
21-Jul-23
PI
TOTAL SOLIDS
3
91.2
%
SLUDGE
FECAL COLIFORM
442
MPNIq
SLUDGE
21-Jul-23
PI
TOTAL SOLIDS
4
91.7
%
SLUDGE
FECAL COLIFORM
280
MPNIg
SLUDGE
21-Jul-23
PI
TOTAL SOLIDS
5
92.0
%
SLUDGE
FECAL COLIFORM
402
MPN/n
SLUDGI=
21-Jul-23
PI
TOTAL SOLIDS
6
90,6
%
SLUDGE
FECAL COLIFORM
404
MPN/g
SLUDGE
21-Jul-23
PI
TOTAL SOLIDS
7
90.7
%
SLUDGE.
FECAL COLIFORM
300
MPNIg
SLUDGE
21-Jul-23
PI
REPORTED BY: NC CERTIFIED LAB # 544
PAUL ISENHOUR, SUPERVISOR

Emmmumliamm. i • • • ••• rrrr - •
AOG/03/2023/THU 11:10 AM FAX No. P, 001/002
WATER QUALITY SERVICES, INN.
P.O. •HOX'1102, BANNER ELK, NC 2.
8604
_ [phone]
fax [phone]
TYPE SAMPLE: WASTEWATER CHAIN OF CUSTOI]Y
L-OCATION: C S ,5T0P, Gl~ " PRESERVATION CODS
FACILITY ID � t] A 1 - H2SO4, 2 - HNO3, 3 - HCL,
,WViPLER NAME: oW _ O� 4 - NAOH, 5 - NONE, e -COOL ICE
:OMPOSITE SAMPLE: START nmr 7 " NA2$203, 8 "OTHER
N
htt;tlVED BY:
� .z.,o-�>+—A7T,—MPE�
7
DATi~
I-e•uoralory preservation is ensured by adon of preservatives prior to sample
containers leaving the lab, unless otherwise noted,
CL2-D-CL2ge Chlorine check and dechipririation verlficaliort:
RESERVATION:
I COOL 40: SOD, RESIDUE, CONDUCTIVITY, WAS, CQLOR, ALKALINITY, CR, VI, TURBIDITY
I COOL 4C, PH<2 H2SO4: NH3, N0e-1403, TKN, O&C, TOC, COD, HARDNESS, PHENOLS, TOT PHOS,
I COOL 4C, Phi<2 HNO3 :.METALS except CR, Vl
} NONE: CHLORIDE, PH, FLUORIDE SAMPLE DEVIATION:
!"HER:
xktOOL 4C, NA2S203 : COLIFORM BACTERIA
NOTIFICATION:

WATER QUALITY LAB & OPERATIONS, INC.
P.O. BOX 1167
BANNER ELK, NC 28604
[phone]
CLIENT: TOWN OF BOONE WWTP
ADDRESS: P.O. BOX 192
CITY: BOONE RECEIVED DATE:
STATE. NC ZIP 28607 REPORTED DATE:
ID##: NCO020621
ANALYSES :=
LSID #
ANA1YSfS
MQL's :
UNITS
"SAMPLE
TOTAL SOLIDS
1
RESULTS
-
1.00AYION
FECAL COLIFORM
90,8
103
%
SLUDGE
TOTAL SOLIDS
2
91.1
MPN/g
SLUDGE
FECAL COLIFORM
44
%
MPN/g
SLUDGE
SLUDGE.
TOTAL SOLIDS
3
92.1
%
SLUDGE
FECAL COLIFORM
77
MPN/g
SLUDGE
TOTAL SOLIDS
4
91.8
%
SLUDGE
FECAL COLIFORM
118
MPN/g
SLUDGE
TOTAL SOLIDS
5
91.6
%
SLUDGE
FECAL COLIFORM
156
MPN/g
SLUDGE
TOTAL SOLIDS
6
90.9
%
SLUDGE
FECAL COLIFORM
83
MPN/g
SLUDGE
TOTAL SOLIDS
7
91.5
%
SLUDGE
FECAL COLIFORM
91
MPN/g
SLUDGE
REPORTED BY: NC CERTIFIED LAB ## 544
r
PAUL ISENHOUR, SUPERVISOR
19-Oct-23
7-Nov-23
ANALYSIS -INT
COMPLETED
20-Oct-23 PI
20-Oct-23 I PI
20-Oct-23 I PI
20-Oct-23 I PI
20-Oct-23 I pI
20-Oct-23 I Pl
20-Oct-23 pi

AUG/03/2023/THU 11:10 AM FAX No, P,001/002
WATER QUALITY SERVICES, INC.
P.0.'BOK1102, BANNER ELK, NC 2.
8604
(828) 898•-6277
fax (828) 898�'6255
1'YP� SAMPLE: WASTEWATER CHAIN OF CUSTOpY
LOCATION: CLA�� A_5-rop Aqt A� ` PRESERVATION CODS '
FACILITY ID' p 6a � 1 - H2SO4, 2 - HNO3, 3 - HCL,
SAMPLER NAME: qW 0 . o� 4 - NAOH, 5 -NONE, 6 - COOL ICE
'OMPOSITE SAMPLE: START 'r]Mr;• . r-- T•. _ 7 ` NA2S2o3, 8 -OTHER
" •, ~- �'��n� RECEIVED BY: DATE
TIME
;t=LINQUISHlED BY: PATE .TIME REC BY: DATE TIME
Laporatory preservation is ensured by addition of preservatives prior to sample
containers leaving the lab, unless otherwise noted.
CL2�D-CL2tt C131011ine check and dechlOrldption verification: -+
RESERVATION:
I COOL 4C : $OD, RESIDUE, CONDUCTIVITY, MBAS, CQLOR, ALKALINITY, CR, Vi, TURBIDITY
I COOL 4C, PH<2 H2SO4: NH3, NO2-1103, TKN, O&O, TOC, COD, HARDNESS, PHENOLS, TOT PROS.
I COOL 40, PH<2 HNO3 ;.METALS except CR, VI
1 NONE: CHLORIDE, PH, FLUORIDE SAMPLE DEVIATION:
4kOOL 4C, NA2S203 : COL.IFORM BACTERIA
NOTIFICATION: