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WQ0001489_2023 Residual Annual Report_20240130 (2)
Initial Review Reviewer nathaniel.thorn burg Is this submittal an application? (Excluding additional information.) * Yes No If not an application what is the submittal type?* Annual Report Residual Annual Report Additional Information Other Annual Report Year* 2023 Permit Number (IR) * WQ0001489 Applicant/Permittee US MCAS Cherry Point Email Notifications Does this need review by the hydrogeologist? * Yes QQ No Regional Office Washington CO Reviewer Admin Reviewer wanda.gerald@deq.nc.gov Submittal Form Project Contact Information Please provide information on the person to be contacted by NDB Staff regarding electronic submittal, confirmation of receipt, and other correspondence. Name* Richard Weaver Email Address* richard.weaver@usmc.mil Project Information ......................... Application/Document Type* New (Fee Required) Modification - Major (Fee Required) Renewal with Major Modification (Fee Required) Annual Report Additional Information Other Phone Number* 252-466-5917 Modification - Minor Renewal GW-59, NDMR, NDMLR, NDAR-1, N DAR-2 Residual Annual Report Change of Ownership We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form. https://edoes.deq.nc.gov/Forms/NonDischarge_Monitoring_Report Permit Type:* Wastewater Irrigation High -Rate Infiltration Other Wastewater Reclaimed Water Closed -Loop Recycle Residuals Single -Family Residence Wastewater Other Irrigation Permit Number:* WQ0001489 Has Current Existing permit number Applicant/Permittee Address* MCAS Cherry Point, PSC Box 8006, Cherry Point, NC 28533 Facility Name* US MCAS Cherry Point Class B Residuals Program Please provide comments/notes on your current submittal below. Marine Corps Air Station (MCAS) Cherry Point submits the enclosed 2023 Treatment and Land Application of Residuals Report for permit WQ0001489. For the calendar year of 2023, MCAS Cherry Point was in compliance with all conditions of the land application permit. At this time, paper copies are no longer required. If you have any questions about what is required, please contact Nathaniel Thornburg at nathaniel.thornburg@ncdenr.gov. Please attach all information required or requested for this submittal to be reviewed here. (Application Form, Engineering Plans, Specifications, Calculations, Etc.) Final 2023 Annual Sludge Report WQ0001489.pdf 6.03MB Upload only 1 PDF document (less than 250 MB). Multiple documents must be combined into one PDF file unless file is larger than upload limit. * By checking this box, I acknowledge that I understand the application will not be accepted for pre -review until the fee (if required) has been received by the Non -Discharge Branch. Application fees must be submitted by check or money order and made payable to the North Carolina Department of Environmental Quality (NCDEQ). I also confirm that the uploaded document is a single PDF with all parts of the application in correct order (as specified by the application). Mail payment to: NCDEQ — Division of Water Resources Attn: Non -Discharge Branch 1617 Mail Service Center Raleigh, NC 27699-1617 Signature Submission Date 1/30/2024 UNITED STATES MARINE CORPS MARINE CORPS AIR STATION POSTAL SERVICE CENTER BOX 8003 CHERRY POINT, NORTH CAROLINA 28533-0003 IN REPLY REFER TO: 5090/07202 LN January 16, 2023 North Carolina Department of Environment Quality Division of Water Resources Information Processing Center 1617 Mail Service Center Raleigh, NC 27699-1617 SUBJECT: TREATMENT AND LAND APPLICATION OF RESIDUALS Marine Corps Air Station (MCAS) Cherry Point submits the enclosed 2023 Treatment and Land Application of Residuals Report for permit WQ0001489 as enclosure (1). For the calendar year of 2023, MCAS Cherry Point was in compliance with all conditions of the land application permit. During the 2023 reporting year, 105.95 dry tons were land applied on 37.50 acres on Sites 1 and 2 of our nine permitted application sites that encompass 389.24 total acres. The residual source was the MCAS Cherry Point's Wastewater Treatment Plant (WWTP). The 105.95 dry tons is a reduction in the total volume of sludge land applied from the previous year (141.80) for the primary source, Cherry Point's WWTP. As documented in enclosure (2), the annual data submitted herein was submitted to the Environmental Protection Agency's Biosolids Section via the NPDES eReporting Tool under identification number NCL003 816. For additional information, please contact Mr. Rich Weaver of the Environmental Affairs Department at (252) 466-5917. Sincerely, (A6TH N A. FERENCE Deputy Facilities Director By direction of the Commanding Officer Enclosures: 1. 2023 Annual Land Application of Residuals Report 2.2023 EPA Biosolids Report 2023 ANNUAL SLUDGE REPORT PACKAGE ORDER 1. ACF 2. RSSF a. MCAS Cherry Point 3. MFLSF 4. FSF 5. PVRF and Supporting Documents for MCAS Cherry Point 6. Laboratory Reports for MCAS Cherry Point a. Residuals lab report (general chemistry) b. TCLP lab report c. Soils fertility lab report 7. Triennial Groundwater Monitoring Enclosure (1) ANNUAL LAND APPLICATION CERTIFICATION FORM Enclosure (1) ANNUAL LAND APPLICATION CERTIFICATION FORM Permit#: WQ0001489 County: Craven Year: 2023 Facility Name (as shown on permit): US Marine Corps - Cherry Point Land Application Operator: Jeffery Clayton Phone: (252) 466-6787 Land application of residual solids as allowed by the permit occurred during the past calendar year? X Yes ❑ No If No, skip Part A, and Part B and proceed to the certification. Also, if residuals were generated but not land applied, please attach an explanation on how the residuals were handled. Part A: Total number of application fields in permit: 9 Total number of fields land application occurred during the year: 2 Total amount of dry tons applied during the year for all application sites: 105.95 Total number of acres land application occurred during the year: 37.50 Part B: Facility was compliant during calendar year 2023 with all conditions of the land application permit (including but not limited to items 1-12 below) issued by the Division of Water Quality. x Yes ❑ No If no please, provide a written description why the facility was not compliant, the dates, and explain corrective action taken. 1. Only residuals approved for this permit were applied to the permitted sites. 2. Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or the limit specified in the permit. 3. Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies of laboratory results are attached. 4. Annual TCLP analysis was performed and three (3) copies of certified laboratory results are attached. 5. All other monitoring was performed in accordance with the permit and reported during the year as required and three (3) copies of certified laboratory results are attached. 6. The facility did not exceed any of the Pollutant Concentration Limits in Table 1 of 40 CFR Part 503.13 or the Pollutant Loading Rates in Table 2 of 40 CFR part 503.13 (applicable to 40 CFR Part 503 regulated facilities). 7. All general requirements in 40 CFR Part 503.12 and management practices in 40 CFR Part 503.14 were complied with (applicable to 40 CFR Part 503 regulated facilities). 8. All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior authorization was received from the Division of Water Quality. 9. No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are attached to include appropriate actions and remediations. 10. Vegetative cover as specified in the permit was maintained on this site and the crops grown were removed in accordance with the crop management plan. 11. No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred. 12. All buffer requirements as specified on the permit were maintained during each application of residuals. "I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Anthony A. Ference, Deputy Facilites Director / 7 ` goa- Permittee Name and Title (type or print) SignatLkdf &rmittee by Direction 1 Date of the Comi n i fficer IL Signature of Preparer* Date Signature of and Applier Date (if different from Permittee) (if different from Permittee and Preparer) " Preparer is defined in 40 CFR Part 503.9 (r) DENR FORM ACF (5/2003) RESIDUAL SAMPLING SUMMARY FORMS 1) MCAS Cherry Point Enclosure (1) W � N M AM +-a C� in 0 a p 00 M O O O IV kn 1 O O 000 N 00 NN- O N00N O O N kn N N N O N N N 000 D\ z C/I��� Parameters mgkg 0 0 � N M � tI in 0 a 0 PLO 00 U 00 � O E� M O O C U U z :Ji N O - O N O -- O 't ct NcM O� M "o N O� vn N 000 O O t- I CD_ C1 a H H Q6�D o Parameters mo,/k M 0 0 N m LL U) cn 0 LL Z w 0 METALS FIELD LOADING SUMMARY FORM Enclosure (1) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Permit #: USMCAS - Cherry Point WWTP Total Dry Tons Applied (Annual): WQ0001489 Cation Exchange Capacity (non 503 only): Operator: Jeffery Clayton Owner: US Marine Corps - Cherry Point Acres Used: 30.63 Acres Permitted: 44.94 Site #: 1 Field #: 84.2474691 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Sample or Com- posite Date 11 9/28/22 21111 2/14/23 3 2/14/23 4 2/14/23 5 2/14/23 6 2/14/23 71 2/14/23 8 2/14/23 9 LO 11 12 % Solids 14.2 1.79 1.79 1.79 1.79 1.79 1.79 1.79 Arsenic 5.12 49.7 49.7 49.7 49.7 49.7 49.7 49.7 Cadmium 2.04 49.7 49.7 49.7 49.7 49.7 49.7 49.7 Chromium 49.9 161 161 161 161 161 161 161 Copper 56.2 449 449 449 449 449 449 449 Lead 2.68 49.7 49.7 49.7 49.7 49.7 49.7 49.7 Mercury 0.121 1.03 1.03 1.03 1.03 1.03 1.03 1.03 Molyb- denum 2.04 49.7 49.7 49.7 49.7 49.7 49.7 49.7 Nickel 2.92 49.7 49.7 49.7 49.7 49.7 49.7 49.7 Selenium 2.04 49.7 49.7 49.7 49.7 49.7 49.7 49.7 Zinc 84.7 754 754 754 754 754 754 754 Total Phos- chorus 143 31500 31500 31500 31500 31500 31500 31500 Annual Heavy Metal Field Loadings (Calculated in lbs/acre): 0 1 2 3 4 5 6 7 8 9_1 10 12' CD r1o p 5, 0.3186 0.2784 0.349 0.3925 0.3652 0.2999 0.3568 0.3901 0 0 0 Arsenic 0.0033 0.0277 0.0347 0.039 0.0363 0.0298 0.0355 0.0388 0 0 0 0 0.245 Cadmium 0.0013 0.0277 0.0347 0.039 0.0363 0.0298 0.0355 0.0388 0 0 0 0 0.243 Chromiuir 0.0318 0.0896 0.1124 0.1264 0.1176 0.0966 0.1149 0.1256 0 0 0 0 0.8149 Copper 0.0358 0.25 0.3134 0.3524 0.328 0.2694 0.3204 0.3503 0 0 0 0 2.2197 Lead 0.0017 0.0277 0.0347 0.039 1 0.0363 0.02981 0.0355 0.0388 0 0 0 1 0 0.2434 Mercury 8E-05 0.0006 0.0007 0.0008 0.0008 0.00061 0.0007 0.0008 0 0 0 0 0.0051 Molyb- 0.0013 0.0277 0.0347 0.039 0.0363 0.0298 0.0355 0.0388 0 0 0 0 0.243 denum Nickel 0.0019 0.0277 0.0347 0.039 0.0363 0.0298 0.0355 0.0388 0 0 0 0 0.2436 Selenium 0.0013 0.0277 0.0347 0.039 0.0363 0.0298 0.0355 0.0388 0 0 0 0 0.243 Zinc 0.054 0.4198 0.5262 0.5919 0.5508 0.4523 0.5381 0.5883 0 1 0 0 0 3.7213 Total Phos- 0.0911 17.538 21.984 24.726 23.01 18.897 22.478 24.578 0 0 0 0 153.3 phorus "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibili of fines and imprisonment for knowing violations" lv 1- Signature of Laid Ap ier D to * See bottom of FSF Form for helpful instructions for this MFLSF Form and the mathematica j WWnF (5/2003) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: USMCAS - Cherry Point WWTP Total Dry Tons Applied (Annual): 21.71 Permit #: WQ0001489 Cation Exchange Capacity (non 503 only): Operator: Jeffery Clayton Owner: US Marine Corps - Cherry Point Acres Used: 6.87 Acres Permitted: 23.40 Site #: 2 Field #: Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Sample or Com- posite Date _j_l 2/14/23 21 2/14/23 3_ 41 4' 6 7 81 9 101 11 12 % Solids 1.79 1.79 Arsenic 49.7 49.7 Cadmium 49.7 49.7 Chromium 161 161 Copper 449 449 Lead 49.7 49.7 Mercury 1.03 1.03 Molyb- denum 49.7 49.7 Nickel 49.7 49.7 Selenium 49.7 49.7 Zinc 754 754 Total Phos- horus 31500 31500 Annual Heavy Metal Field Loadings (Calculated in lbs/acre): 0 11 21 3 4 5 6 71 81 9 10 11 12 cn H p o' 1.6661 1.4955 0 0 0 0 0 0 0 0 0 Arsenic 0.16561 0.1487 0 0 0 0 0 0 0 0 0 0 0.3143 Cadmium 0.1656 0.1487 0 0 0 0 0 0 0 0 0 0 0.3143 'hromiun 0.5365 0.4816 0 0 0 0 0 0 0 0 0 0 1.018 Copper 1.4961 1.343 0 0 0 0 0 0 0 0 0 0 2.8391 Lead 0.1656 0.1487 0 0 0 0 0 0 0 0 0 0 0.3143 Mercury 0.00341 0.0031 0 0 0 0 0 0 0 0 0 0 0.0065 Molyb- 0.1656 0.1487 0 0 0 0 0 0 0 0 0 0 0.3143 denum Nickel 0.1656 0.1487 0 0 0 0 0 0 0 0 0 0 0.3143 Selenium 0.1656 0.1487 0 0 0 0 0 1 0 0 0 0 0 0.3143 Zinc 2.5124 2.2552 0 0 0 1 0 0 0 1 0 0 0 0 4.7677 Total Phos- 104.96 94.217 0 0 0 0 0 0 0 0 0 0 199.18 phorus "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possib it of fu►es and imprisonment for knowing violations" tv Signature of Lan Appli' Ddte * See bottom of FSF Form for helpful instructions for this MFLSF Form and the mathematical YM L%F (5/2003) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Permit #: Operator: Acres Used: USMCAS - Cherry Point WWTP Total Dry Tons Applied (Annual): #DIV/0! WQ0001489 Cation Exchange Capacity (non 503 only): Jeffery Clayton Owner: US Marine Corps - Cherry Point 0.00 Acres Permitted: 16.80 Site #: 3 Field #: Residual Analvsis Data (Heave Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Sample or Com- posite Date 1 1 21 31 4 j 5 61 71 8 9 10 ' 11 12 % Solids Arsenic Cadmium Chromium Copper Lead Mercury Molyb- denum Nickel Selenium Zinc Total Phos- phorus Annual Heavy Metal Field Loadings (Calculated in Ibs/acre): icy 1' 21 3 4 5 6 71 8] 9 10' 11 12 m t7 m a a ; 0 0 0 0 ###### ###### ###### ###### ###### ###### Arsenic 0 0 0 0 ###### ###### ###### ###### ###### ###### 0 0 1###### Cadmium 0 0 0 0 ###### ###### ###### ###### ###### ###### 0 0 ###### 'hromiun 0 0 0 0 ###### ###### ###### ###### ###### ###### 0 0 ###### Copper 0 0 0 0 ###### ###### ###### ###### ###### ###### 0 0 ###### Lead 0 0 0 0 ###### ###### ###### ###### ###### ###### 0 1 0 ###### Mercury 0 0 0 0 ###### ###### ###### ###### ###### ###### 0 0 1###### Molyb- 0 0 0 0 ###### ###### ###### ###### ###### ###### 0 0 ###### denum Nickel 0 0 0 0 ###### ###### ###### ###### ###### ###### 0 0 ###### Selenium 0 0 0 0 ###### ###### ###### ###### ###### ###### 0 0 ###### Zinc 0 0 0 0 ###### ###### ###### ###### ###### ###### 0 0 ###### Total Phos- 0 0 0 0 ###### ###### ###### ###### ###### ###### 0 0 ###### phorus "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility 'ty of fines and imprisonment for knowing violations" /17//" Signature of La d A 1plier Dale * See bottom of FSF Form for helpful instructions for this MFLSF Form and the mathematica EW96F (5/2003) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Permit #: Operator: Acres Used: USMCAS - Cherry Point WWTP Total Dry Tons Applied (Annual): #DIV/0! WQ0001489 Cation Exchange Capacity (non 503 only): Jeffery Clayton Owner: US Marine Corps - Cherry Point 0.00 Acres Permitted: 8.00 Site #: 4 Field #: Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent ft Sample or Com- posite Date 1 1 21 21 21 5 6 7 8 91 10 11 12_ % Solids Arsenic Cadmium Chromium Copper Lead Mercury Molyb- denum Nickel Selenium Zinc Total Phos- phorus Annual Heavy Metal Field Loadings (Calculated in lbs/acre): 0 1 2' 3 4 5� 6 7' 8 9 10 11 12 CD �P a o. ; ###### ###### ###### ###### Arsenic ###### ###### ###### ###### 0 0 0 0 0 0 0 0 ###### Cadmium ###### ###### ###### ###### 0 0 0 0 0 0 0 0 ###### hromiun ###### ###### ###### ###### 0 0 0 0 0 0 0 0 ###### Copper ###### ###### ###### ###### 0 0 0 0 0 1 0 0 0 ###### Lead ###### ###### ###### ###### 0 0 0 0 0 0 0 0 ###### Mercury ###### ###### ###### ###### 0 0 0 0 0 0 0 0 ###### Molyb- ###### ###### ###### ###### 0 0 0 0 0 0 0 0 ###### denum Nickel ###### ###### ###### ###### 0 0 0 0 0 1 0 0 0 ###### selenium ###### ###### ###### ###### 0 0 0 0 0 0 0 0 ###### Zinc ###### ###### ###### ###### 0 0 0 0 0 0 0 0 ###### Total Phos- ###### ###### ###### ###### 0 0 0 0 0 0 0 0 ###### phorus "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the ossibi ' y of fines and imprisonment for knowing violations" Signature of Lai 1 App er Da * See bottom of FSF Form for helpful instructions for this MFLSF Form and the mathematical TWMF (5/2003) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: USMCAS - Cherry Point WWTP Total Dry Tons Applied (Annual): 0 Permit #: WQ0001489 Cation Exchange Capacity (non 503 only): Operator: Jeffery Clayton Owner: US Marine Corps - Cherry Point Acres Used: 0.00 Acres Permitted: 24.00 Site #: 5 Field #: Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Sample or Com- posite Date 1 21 3 4 5' 61 7 8 9 10 11 12 % Solids Arsenic Cadmium Chromium Copper Lead Mercury Molyb- denum Nickel Selenium Zinc Total Phos- phorus Annual Heavy Metal Field Loadings (Calculated in lbs/acre): �■�000000000000 .. , 000000�■000000 o000000�n■000�■o ... - o0000000000■�0 �0000�■000000■�o �0000000000000 �0000000000000 �0000000000000 �0000000000 o0 Total . . , . . "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations" I IY Signature of L id. )plier Date * See bottom of FSF Form for helpful instructions for this MFLSF Form and the mathematically linked FSF Form DENR FORM MFLSF (5/2003) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: USMCAS - Cherry Point WWTP Total Dry Tons Applied (Annual): 0 Permit #: WQ0001489 Cation Exchange Capacity (non 503 only): Operator: Jeffery Clayton Owner: US Marine Corps - Cherry Point Acres Used: 0.00 Acres Permitted: 8.10 Site #: 6 Field #: Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Sample or Com- posite Date 1 2 3 4 5 61 7 8 91 101 111 12 % Solids Arsenic Cadmium Chromium Copper Lead Mercury Molyb- denum Nickel Selenium Zinc Total Phos- phorus Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Boom 1111111 0. .. 00000�'�00�000 ��0�00�000 000 �00000�'000�� � QO �00000 � �000000 �00000��000�'QO ®00000��000�00 .. Phos- .. rus.000MENEENEENE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the ,ss' ility of fines and imprisonment for knowing violations" IA 7/ L Signature o anc : pplier D e See bottom of FSF Form for helpful instructions for this MFLSF Form and the mathematically linked FSF Form DENR FORM MFLSF (5/2003) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Permit #: Operator: Acres Used: USMCAS - Cherry Point WWTP Total Dry Tons Applied (Annual): #DIV/0! WQ0001489 Cation Exchange Capacity (non 503 only): Jeffery Clayton Owner: US Marine Corps - Cherry Point 0.00 Acres Permitted: 35.00 Site #: 7 Field #: Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Sample or Com- posite Date 1 2 1 31 4. 51 6 71 8 9 101 11 12 % Solids Arsenic Cadmium Chromium Copper Lead Mercury Molyb- denum Nickel Selenium Zinc Total Phos- phorus Annual Heavy Metal Field Loadings (Calculated in lbs/acre): M o 1 2 3 4 5 61 7 8 9 10 11 12 rn H � m Y o' ###### Arsenic ###### 0 0 0 0 0 0 0 0 0 0 0 ###### Cadmium ###### 0 0 0 0 0 0 0 0 0 0 0 ###### 'hromiun ###### 0 0 0 0 0 0 0 0 0 0 0 ###### Copper ###### 0 0 0 0 0 0 0 0 0 0 0 1###### Lead ######1 0 0 0 0 0 0 0 0 0 0 0 ###### Mercury ###### 0 0 0 0 0 0 0 0 0 0 0 ###### Molyb- ###### 0 0 0 0 0 0 0 0 0 0 0 ###### denum Nickel ###### 0 0 0 0 0 0 0 0 1 0 0 1 0 ###### Selenium ######1 0 0 0 0 0 0 0 0 0 0 0 ###### Zinc ###### 0 0 0 1 0 0 1 0 0 0 0 0 0 ###### Total Phos- ###### 0 0 0 0 0 0 0 0 0 0 0 ###### phorus "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including thA-sibility of fines and imprisonment for knowing violations" Signature ofier Dale * See bottom of FSF Form for helpful instructions for this MFLSF Form and the mathematically linked FSF Form DENR FORM MFLSF (5/2003) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: USMCAS - Cherry Point WWTP Total Dry Tons Applied (Annual): 0 Permit #: WQ0001489 Cation Exchange Capacity (non 503 only): Operator: Jeffery Clayton Owner: US Marine Corps - Cherry Point Acres Used: 0.00 Acres Permitted: 110.00 Site #: 8 Field #: Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Sample or Com- posite Date 1 #REF! 2 3 41 5 6 7 8 9 10 11 12 % Solids #REF! Arsenic #REF! Cadmium #REF! Chromium #REF! Copper #REF! Lead #REF! Mercury #REF! Molyb- denum #REF! Nickel #REF! selenium #REF! Zinc #REF! Total Phos- chorus #REF! Annual Heavy Metal Field Loadings (Calculated in lbs/acre): i��oo�■oo■�00000� .. ,�0000000000■�� , . ,�000000�■0000� ...-�o■�0000■00000 -. ��0000000�■000� ��o�■o■�0000 , ■■�o� ', '�00000000000� . � -�00000■�00000 - - ��00000000000� ® -�00000000000� Total �. . . "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the ibility of fines and imprisonment for knowing violations" Signature of Land Applier * See bottom of FSF Form for helpful instructions for this MFLSF Form and the mathematically linked FSF Form DENR FORM MFLSF (5/2003) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: USMCAS - Cherry Point WWTP Total Dry Tons Applied (Annual): 0 Permit #: WQ0001489 Cation Exchange Capacity (non 503 only): Operator: Jeffery Clayton Owner: US Marine Corps - Cherry Point Acres Used: 0.00 Acres Permitted: 119.00 Site #: 10 Field #: Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Sample or Com- posite Date 1_ 21 31 41 5j 7 8 9 10 11 12 % Solids Arsenic Cadmium Chromium Copper Lead Mercury Molyb- denum Nickel Selenium Zinc Total Phos- phorus Annual Heavy Metal Field Loadings (Calculated in lbs/acre): �s-�0000�0�000000 p 0000 000000 �00000000000 �00�1' � 000�0�000 �0000000�0�000 ®0�'�1'000��0�000 Total .. "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations" l Iy L Signature o anY Applier I D, e * See bottom of FSF Form for helpful instructions for this MFLSF Form and the mathematically linked FSF Form DENR FORM MFLSF (5/2003) FIELD SUMMARY FORMS Enclosure (1) N 00 00 M, W a a O L u I M O M Lrl y a� M. 4 •IF iE iE iF •--� N M 'IT h r- 00 O\ O '� O O i yUj 0 O N � U u w w w w w w w w J N N a •r O W) 00 00 �O Cl) N N •--� (ONO N M � O O "'q: O D1 O �O •--� N O O� N a - a 00 M .�•� tn DO 00 00 OO 00 00 00 a O Q 0 M 0 enM 0 0 0 M 0 M 0 M L." 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N�N O LL w z W O LABORATORY REPORTS FOR MCAS CHERRY POINT 1) GENERAL CHEMISTRY 2) TCLP 3) SOILS FERTILITY Enclosure (1) Environmental Chemists, Inc. envirochem 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax s 710 Bowsertown Road, Manteo, NC 27954 • 252-473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 23540 • 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS infoCaenvironmentalchemists com MCAS Cherry Point Revised Report: Feb 02, 2023 PSC Box 8006 Original Report Date: Sep 28, 2022 Cherry Point NC 28533 Report #: 2022-16488 Attention: Customer ID: 09110093 Project ID: MCAS 001 Sludge Lab ID Sample ID: Collect Date/Time Matrix Sampled by 22-40321 Site: WAS 001 Sludge 8/23/2022 8:00 AM Solid/Sludge Fread Shimmel Test Method Results Date Analyzed PAN Used 3t)%Mineralization Rate. calculation 2150 mg/kg 02l02l2023 Chlordane (TCLP) SW-846 8081 B <0.02 mg/L 09/14/2022 Endrin (TCLP) SW-846 8081 B <0.0005 mg/L 09/14/2022 Heptachlor (TCLP) SW-846 6081 B <0.0005 mg/L 09/14/2022 Heptachlor epoxide (TCLP) SW-846 8081 B <0.0005 mg/L 09/14/2022 Lindane (TCLP) SW-846 8081 8 <0.0005 mg/L 09/14/2022 Methoxychlor (TCLP) SW-846 8081 B <0.0005 mg/L 09/14/2022 Toxaphene (TCLP) SW-846 8081 B <0.05 mg/L 09/14/2022 2,4,5-TP (TCLP) SW-646 8151 A <0.003 mg/L 09/13/2022 2,4-D (TCLP) SW-846 8151 A <0.003 mg/L 09/13/2022 1,4-Dichlorobenzene (TCLP) SW-846 8270 E <0.050 mg/L 09/15/2022 2,4,5-Trichiorophenol (TCLP) SW-846 8270 E <0.050 mg/L 09/15/2022 2,4,6-Trichlorophenol (TCLP) SW-848 8270 E <0.050 mg/L 09/15/2022 2,4-Dinitrotoluene (TCLP) SW-8468270E <0.050mg/L 09/15/2022 Cresol (TCLP) SW-846 8270 E <0.050 mg/L 09/15/2022 Hexachloro-1,3-butadiene (TCLP) SW-846 8270 E <0.050 mg/L 09/15/2022 Hexachlorobenzene (TCLP) SW-846 8270 E <0.050 mg/L 09/15/2022 Hexachloroethane (TCLP) SW-846 8270 E <0.050 mg/L 09/15/2022 rn + p-Cresol (TCLP) SW-846 8270 E <0.050 mg/L 09/15/2022 Nitrobenzene (TCLP) SW-846 8270 E <0.050 mg/L 09/15/2022 o-Cresol (TCLP) SW-846 8270 E <0.050 mg/L 09/15/2022 Pentachlorophenol (TCLP) SW-846 8270 E <0.250 mg/L 09/15/2022 Pyridine (TCLP) SW-846 8270 E <0.050 mg/L 09/15/2022 1,1-Dichloroethylene (TCLP) SW-846 Method8260D <0.01 mg/L 08/31/2022 1,2-Dichloroethane (TCLP) SW-846 Method 8260D <0.01 mg/L 08/31/2022 RannO 9 9n72AAARR ' Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 - 910.392.0223 Lab - 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 - 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 - 910.347.5843 Lab/Fax ANALYTICAL 8 CONSULTING CHEMISTS infoCa�environmentalchemists com MCAS Cherry Point PSC Box 8006 Cherry Point NC Attention: 28533 Revised Report: Feb 02, 2023 Original Report Date: Sep 28, 2022 Report #: 2022-16488 Customer ID: 09110093 Project ID: MICAS 001 Sludge Benzene (TCLP) SW-846 Method 8260D <0.01 mg/L 08/31/2022 Carbon Tetrachloride (TCLP) SW-846 Method 8260D <0.01 mg/L 08/31/2022 Chlorobenzene (TCLP) SW-846 Method 8260D <0.01 mg/L 08/31/2022 Chloroform (TCLP) SW-846 Method 8260D <0.01 mg/L 08/31/2022 Methyl ethyl ketone (TCLP) SW-846 Method 8260D <0.05 mg/L 08/31/2022 Tetrachloroethylene (TCLP) SW-846 Method 8260D <0.01 mg/L 08/31/2022 Trichloroethylene (TCLP) SW-846 Method 8260D <0.01 mg/L 08/31/2022 Vinyl Chloride (TCLP) SW-846 Method 8260D <0.01 mg/L 08/31/2022 RCI Cyanide SM 4500 CN D-2016 <1.0 mg/kg 08/29/2022 Sulfide SM4500 S D 0.06 mg/kg 08/31/2022 Ignitability SW 846 method 1010 >158 °F 09/15/2022 Sludge Residuals Aluminum EPA 200 7 Rev 4 4 1994 2660 mg/kg 09/07/2022 Arsenic EPA 200 7, Rev 4 4, 1994 5.12 mg/kg 09/14/2022 Cadmium EPA 200 7, Rev 4 4, 1994 <2.04 mg/kg 09/07/2022 Calcium EPA 200 7 Rev 4 4, 1994 2770 mg/kg 09/07/2022 Chromium EPA 200 7, Rev 4 4. 1994 49.9 mg/kg 09/07/2022 Copper EPA 200 7, Rev 4 4, 1994 56.2 mg/kg 09/07/2022 Lead EPA 200 7, Rev 4 4, 1994 2.68 mg/kg 09/07/2022 Magnesium EPA 20D 7. Rev 4 4, 1994 341 mg/kg 09/07/2022 Molybdenum EPA 200 7, Rev 4 4, 1994 <2.04 mg/kg 09/07/2022 Nickel EPA 200 7, Rev 4 4, 1994 2.92 mg/kg 09/07/2022 Potassium EPA 200 7. Rev. 4 4, 1994 370 mg/kg 09/07/2022 Selenium EPA 200 7, Rev 4 4 1994 <2.04 mg/kg 09/07/2022 Sodium EPA 200 7, Rev 4 4 1994 591 mg/kg 09/07/2022 Zinc EPA 200 7. Rev 4 4 1994 84.7 mg/kg 09/07/2022 Nitrate+Nitrite-Nitrogen EPA 353 2 754 mg/kg 08/29/2022 Total Solids (%) SM 2540 a 14.2 % 08/24/2022 Reoort# 2022-18488 9 MR -.. ANALYTICAL & CONSULTING CHEMISTS MCAS Cherry Point PSC Box 8006 Cherry Point NC 28533 Attention: Environments Chemists, Earn 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax infola environmentalchemists.com Ammonia Nitrogen SM 4500 NH3 C-2011 Total KJeldahl Nitrogen (TKN) SM 4500 Norg B-2011 Total Phosphorus SM 4500 P (F-H)•2011 pH SW 846 Method 9045D Result estimated. Analyzed out of 15 minutes hold time. Revised Report: Feb 02, 2023 Original Report Date: Sep 28, 2022 Report M 2022-16488 Customer ID: 09110093 Project ID: MCAS 001 Sludge 145 mg/kg 08/24/2022 4570 mg/kg 08/24/2022 143mg/kg 08/31/2022 6.21 units 08/31/2022 Mercury SW-846 7471 B <0.121 mg/kg 09/09/2022 TCLP Metals Arsenic EPA 200 7, Rev 4.4, 1994 <1.0 09/08/2022 Barium EPA 2007 Rev 4.4, 1994 <1.0 09/08/2022 Cadmium EPA 2007, Rev 44, 1994 <1.0 09/08/2022 Chromium EPA 200 7, Rev 4 4,1994 <1.0 09/08/2022 Lead EPA 200 7, Rev 4.4, 1994 <1.0 09/08/2022 Selenium EPA 200 7, Rev 4,4, 1994 <1.0 09/08/2022 Silver EPA 200 7, Rev 4 4, 1994 <1.0 09/08/2022 Mercury EPA 245 1 <0.0002 09/17/2022 Comment: Results, except pH, reports on a dry Weight basis. pH reported on an as received basis. sa Reviewed by: Rennd !! 9099-imas 93... 1 nF v envirochem h• C 7 Environmental Chemists, Inc. 66M Windmill Way, Wilmington, NC 2NO + 910.392.0223 Lab . 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 . 910.347.5M Lab/Fax Wfo@emironmentalchemist&com WAS Cherry Point Date of Report: Mar 09, 2023 PSC Box 8006 Customer PO #: M301463261797 Cherry Point NC 28533 Customer ID: 09110093 Attention: Report 0: 2023-03093 Project ID: Sludge Lab ID Sample ID: Collect DateITime Matrix Sampled by 23-07666 Site: 001 Sludge 2/14/2023 7:40 AM Solid/Sludge J. France Test Method Results Date Analyzed PAN CBWB* r 20900mg/kg 03/06/2023 Used 30% Minerallzatlon Rate. Chlordane (TCLP) SW4MO 80818 <0.02 mg/L 02/16/2023 Endrin (TCLP) SW446 W81 B <0.0005 mg/L 02/16/2023 Heptachlor (TCLP) SW44e Mal <0.0005 mg/L 02/16/2023 Heptachlor epoxide (TCLP) svi-m owl B <0.0005 mg/L 02/16/2023 Lindane (TCLP) SV4 446 awl B <0.0005 mg/L 02/16/2023 Methoxyoldor (TCLP) SW W W81 B <0.0005 mg/L 02/162023 Toxaphene (TCLP) sw•446 W81 B <0.05 mg/L 02/16/2023 2,4,5-TP (TCLP) SW446 8151 A <0.003 mg/L 02/16/2023 2,4-13 (TCLP) SW4446 8161 A <0.003 mg/L 02/16/2023 1,4-Dichlorobenzene (TCLP) SW446 8270 E <0.050 mg/L 02/22/2023 2,4,5-Trichlomphenol (TCLP) sW-444 8270 E <0.050 mg/L 02/22/2023 2,4,6 Trichlomphenol (TCLP) SW-444 W70 E <0.050 mg/L 02/22/2023 2,4-Dinitrotoluene (TCLP) SW-W 8270 E <0.050 mg/L 02/22/2023 Cresol (TCLP) SW-4444270E <0.050mg/L 02/22/2023 Hexachloro-1,3-butadiene (TCLP) SWe466270E <0.050mg/L 02/22/2023 Hexachlorobenzene(TCLP) SW-646OVOE <0.050mg/L 02/22/2023 Hexachloroethane (TCLP) SW-846 $270 E <0.050mg/L 02/22/2023 m + p-Cresol (TCLP) SW.440 8270 E <0.050 mg/L 02/22/2023 Nitrobenzene (TCLP) SW446 070 E <0.050 mg/L 02/22/2023 o-Cresol (TCLP) SWa46 8270 E <0.050 mg/L 02rM023 Pentachlorophenol (TCLP) SW-64e C70 E 40.250 mg/L 02/22/2023 Pyridine (TCLP) SW 80 U70 E <0.050mg/L 02/22/2023 1. 1 -Dichloroethylene (TCLP) SW -NO MOOM WOOD < 0.01 mg/L 2/18/2023 1,2-Dichloroethane (TCLP) SW.e46 Me4aa 8280D < 0.01 mg/L 2/18/2023 Report E:: 20234=3 Page 1 of 3 envirochem Environmental Chemists, Inc. 6602 WmdmM way, Wilmington, NC 28M . 910.392.0223 Lab * 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 . 252.473.5702 Lab/Fax 255-A Wilmington Highway, jacksonville, NC 28540 • 910.347.5W Lab/Fax info@envimnmentaId=dsts.com MCAS Cherry Point Date of Report: Mar 09, 2023 PSC Box 8006 Customer PO #: M301463261797 Cherry Point NC 28533 Customer ID: 09110093 Attention: Report #: 2023-03093 Project ID: Sludge Benzene (TCLP) sw-84e MWW OMI) < 0.01 mg/L 2/18/2023 Carbon Tetrachloride (TCLP) SW-84e Method OMD < 0.01 mg/L 2/18/2023 Chlorobenzene (TCLP) sw-m method em!) < 0.01 mg/L 2/18/2023 Chloroform (TCLP) sw-m Menroa am!) < 0.01 mg/L 2/18/2023 Methyl ethyl ketone (TCLP) SW4M Mew 92son < 0.05 mg/L 2/18/2023 Tetrachloroethylene (TCLP) WON Method 82601) < 0.01 mg/L 2/18/2023 Trichloroethylene (TCLP) SW-848 Method s2s0u < 0.01 mg/L 2/18/2023 Vinyl Chloride (TCLP) SW-846 Method SO= < 0.01 mg/L 2/18/2023 RCI Cyanide SM 4500 CN 0-2018 <1 mg/kg 02/15/2023 Sulfide SM 4500 S o 0.50 mglkg 02/15/2023 ignitability SW 846Method 1010 >158 °F 02/16/2023 pH SW 848 Method 0045D 6.30 units 02/24/2023 ResuR estimated. Analyzed out or 15 minutes hold time. Sludge Residuals Aluminum EPA 200.7, Rev. 4.4,1994 9110 mg/kg 02/20/2023 Arsenic EPA 2007, Rev. 4A.1994 <49.7 mg/kg 02/20/2023 Cadmium EPA 200.7, Rev. 4.4,19" <49.7 mg/kg 02/20/2023 Calcium EPA 200.7, Rev. 4.4. 1994 21800 mg/kg 02/20/2023 Chromium EPA 200.7. Rev. 4.4.1094 161 mg/kg 02/20/2023 Copper EPA 200.7, Rev. 4.4.1904 449 mg/kg 02/20/2023 Lead EPA 200.7, Pev. 4.4.104 <49.7 mg/kg 02/20/2023 Magnesium EPA 200.7, Rev. 4A,1994 2620 mg/kg 02/20/2023 Molybdenum EPA 200.7• Rev. 4A.1904 <49.7 mg/kg 02/20/2023 Nickel EPA 200.7, Rev. 4 4.1994 <49.7 mg/kg 02120/2023 Potassium EPA 200.7. Rev. 4.4, 1994 3340 mg/kg 02/20/2023 Selenium EPA 200.7• Rev. 4.4.19e4 <49.7 mg/kg 02120/2023 Sodium EPA 200.7. Rev. 4A.19" W40 mg/kg 0=012023 Zinc EPA 200.7. Rev. 4A.19" 754 mg/kg 02/20/2023 Nitrate+Nitrite-Nitrogen EPA 353.2 7180 mg/kg 02/21/2023 Report g:: 20234=3 Page 2 013 F"007 -77 Environmental Chemists, Inc. envirochem"M Windmill Way, Wilmington, NC 28405 + 910.392.0223 Lab 9 910.392.4424 Fax 710 Bowsertown 1%ad, Manteo, NC 27954 ° 252.4733M Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 910.3473843 Lab/Fax ANALYTICAL S OCNWLTING CHEMISTS infooenviwnawntalchemismcom MCAS Cherry Point Date of Report: Mar 09, 2023 PSC Box 8006 Customer PO #: M301463261797 Cherry Point NC 28533 Customer ID: 09110093 Attention: Report P 2023-03093 Project ID: Sludge Total Solids sM 2540 B 1.79 % 02/16/2023 Ammonia Nitrogen SM 4500 NH3 C-2011 2330 mglkg 02/17/2023 Total Kjeldahl Nitrogen (TKN) sM 4500 Norio "11 44200 mg/kg 02/18/2023 Total Phosphorus sM 46M P (F-H)-2011 31500 mg/kg 02/23/2023 Mercury sw44e 74716 <1.03 mg/kg 02/20/2023 TCLP Metals Arsenic (TCLP) EPA 200.7, Rev. 4-4,1994 <1.0 mg/L 02/20/2023 Barium (TCLP) EPA 200 7, Rev. 44.1994 <1.0 mg1L 02/20/2023 Cadmium (TCLP) EPA 2007. Rev. 4.4, 1994 <1.0 mg1L 02/20/2023 Chromium (TCLP) EPA 200 7. Rev. 4 4.1994 <1.0 mg/L 02I20/2023 Lead (TCLP) EPA 200.7, Rev. 4.4, 1994 <1.0 mglL 02/20/2023 Selenium (TCLP) EPA 200.7, Rev. 4.4,1994 <1.0 mg/L 02/20/2023 Silver (TCLP) EPA 200.7. Rev. 4.4,1994 <1.0 mg1L 02/20/2023 Mercury (TCLP) EPA 2451 <0.0002 mg1L 02/20/2023 Comment: Sludge residuals reported on a dry vrei ht basis, Reviewed by: Report A. 2023.03093 Page 3 of 3 Environmental Chemist, Inc., Wilmington, NC Lab #94 Sample Receipt Checklist 6602 Windmill Way Wilmington, NC 28405 910.392.0223 Client:kC AS-- Date: a+ tT Report Number:_ 2023- j9ZOJ3 Receipt of sample: ECHEM Pickup X Client Delivery ❑ UPS ❑ FeclEx ❑ Other ❑ ❑ YES 113 NO IR N/A 11. Were custody seals present on the cooler? ❑ YES ❑ NO q N/A 12. If custody seals were present, were they intact/unbroken? Original temperature upon receipt "C Corrected temperature upon receipt °C How temperature taken: ❑ Temperature Blank Q Against Bottles IR Gun ID: Thomas Traceable S/N 210886869 IR Gun Correction Factor °C: 0.0 10 YES ❑ NO 3. If temperature of cooler exceeded 6'C, was Project Mgr./QA notified? PO YES ❑ NO 4. Were proper custody procedures (relinquished/received} followed? 0 YES ❑ NO 5. Were sample ID's listed on the COC? Od YES ❑ NO 6. Were samples ID's listed on sample containers? YES ❑ NO 7. Were collection date and time listed on the COC? YES ❑ NO B. Were tests to be performed listed on the COU YES ❑ NO 9. Did samples arrive in proper containers for each test? IW YES ❑ NO 10. Did samples arrive in good condition for each test? YES 17 NO 11. Was adequate sample volume available?' YES ❑ NO 12. Were samples received within proper holding time for requested tests? D YES ❑ NO 13. Were acid preserved samples received at a pH of <2? ❑ YES ❑ NO 14. Were cyanide samples received at a pH >12? ❑ YES ❑ NO 25. Were sulfide samples received at a pH >9? ❑ YES ❑ NO 16. Were NH3/TKN/Phenol received at a chlorine residual of <0.5 m/L? ** ❑ YES 113 NO 117. Were Sulfide/Cyanide received at a chlorine residual of <0.5 m/L? ❑ YES J ❑ NO 118. Were orthophosphate samples filtered in the field within 15 minutes? * TOC/Volatiles are pH checked at time of analysis and recorded on the benchsheet. ** Bacteria samples are checked for Chlorine at time of analysis and recorded on the benchsheet. Sample Preservation: (Must be completed for any sample(s) incorrectly preserved or with headspace) Sample(s) _ were received incorrectly preserved and were adjusted accordingly by adding (circle one): H2SO4 HNO3 HCl NaOH Time of preservation: __ If more than one preservative is needed, notate in comments below Note: Notify customer service immediately for incorrectly preserved samples. Obtain a new sample or notify the state lab if directed to analyzed by the customer. Who was notified, date and time:__ Volatiles Sample(s) were received with headspace COMMENTS: DnC_ nn nm Row 7 IT 4 116111111111�8 Z 0 z c z n r 0 m x z iln m Environmental Chemists, Inc. enviroc6602 Windmill Way, Wilmington, NC 28405 a 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax sM 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS infoirtenvironmentalchemists com MCAS Cherry Point Date of Report: Jan 10, 2023 PSC Box 8006 Customer PO #: Cherry Point NC 28533 Customer ID: 09110093 Attention: Steve Reavis Report #: 2022-25444 Project ID: Soil Sampling Lab ID Sample ID: Collect Date/Time Matrix Sampled by 22-62593 Site: MCAS FIELD #1 12/20/2022 10:30 AM Solid/Sludge Steve Reavis Test Method Results Date Analyzed Soil Fertility Calcium EPA 200.7 2010 mg/kg 01/04/2023 Copper EPA 200.7 2.74 mg/kg 01/04/2023 Magnesium EPA 200.7 158 mg/kg 01/04/2023 Manganese EPA 200.7 14.5 mg/kg 01/04/2023 Potassium EPA 200.7 101 mg/kg 01/04/2023 Sodium EPA 200.7 <26.2mg/kg 01/04/2023 Zinc EPA 200.7 7.14 mg/kg 01/04/2023 Acidity (Soil Fertility) NCDA-Agronomic Division 1 meq/100g 01/03/2023 Base Saturation NCDA-Agronomic Division 92.0 % 01/10/2023 Cation Exchange Capacity NCDA-Agronomic Division 12.6 meq/100g 01/10/2023 Exchangeable Sodium Percentage NCDA-Agronomic Division 0.900 % 01/10/2023 Humic Matter NCDA-Agronomic Division 0.87 % 01/03/2023 Total Solids (%) SM 2540 B 80.2 % 12/22/2022 Total Phosphorus SM 4500 P F 152 mg/kg 01/04/2023 pH SW 846 Method 9046D 6.81 units 01/03/2023 Result estimated. Analyzed out of 15 minutes hold time. Report fit;: 2022-25444 0--- , ..r In 7envirochem ANALYTICAL S CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 + 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax infora environmentalchemists.com MCAS Cherry Point Date of Report: Jan 10, 2023 PSC Box 8006 Customer PO #: Cherry Point NC 28533 Customer ID: 09110093 Attention: Steve Reavis Report #: 2022-25444 Project ID: Soil Sampling Lab ID Sample ID: Collect Date/Time Matrix Sampled by 22-62594 Site: MCAS FIELD #2 12/20/2022 10:45 AM Solid/Sludge Steve Reavis Test Method Results Date Analyzed Soil Fertility Calcium EPA 200.7 578mg/kg 01/04/2023 Copper EPA 200.7 2.52 mg/kg 01/04/2023 Magnesium EPA 200.7 153mg/kg 01/04/2023 Manganese EPA 200.7 18.3mg/kg 01/04/2023 Potassium EPA 200.7 115 mg/kg 01/04/2023 Sodium EPA 200.7 <29.3mg/kg 01/04/2023 Zinc EPA 200.7 6.58 mg/kg 01/04/2023 Acidity (Soil Fertility) NCDA-Agronomic Division 1 meq/100g 01/03/2023 Base Saturation NCDA-Agronomic Division 79.3 % 01/10/2023 Cation Exchange Capacity NCDA-Agronomic Division 5.60 meq/100g 01/10/2023 Exchangeable Sodium Percentage NCDA-Agronomic Division 2.30 % 01/10/2023 Humic Matter NCDA-Agronomic Division 0.40 % 01 /03/2023 Total Solids (%) SM 2540 B 87.3 % 12/22/2022 Total Phosphorus SM 4500 P F 120 mg/kg 01/04/2023 pH SW 845 Method 9045D 6.60 units 01 /03/2023 Result estimated. Analyzed out of 15 minutes hold time. Report #:: 2022-25444 Fr- VFW- -7 Environmental Chemists, Inc. envirochem 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473,5702 Lab/Fax sM 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS infora environmentalchemists.com MCAS Cherry Point Date of Report: Jan 10, 2023 PSC Box 8006 Customer PO #: Cherry Point NC 28533 Customer ID: 09110093 Attention: Steve Reavis Report #: 2022-25444 Project ID: Soil Sampling Lab ID Sample ID: Collect Date/Time Matrix Sampled by 22-62595 Site: MCAS FIELD #3 12/20/2022 11:05 AM Solid/Sludge Steve Reavis Test Method Results Date Analyzed Soil Fertility Calcium EPA 200.7 777 mg/kg 01/04/2023 Copper EPA 200.7 1.47 mg/kg 01/04/2023 Magnesium EPA 200.7 89.5mg/kg 01/04/2023 Manganese EPA 200.7 5.43 mg/kg 01/04/2023 Potassium EPA 200.7 86.7 mg/kg 01/04/2023 Sodium EPA 200.7 <27.6 mg/kg 01/04/2023 Zinc EPA 200.7 2.95 mg/kg 01/04/2023 Acidity (Soil Fertility) NCDA-Agronomic Division 1 meq/100g 01/03/2023 Base Saturation NCDA-Agronomic Division 82.9% 01/10/2023 Cation Exchange Capacity NCDA-Agronomic Division 5.80 meq/100g 01/10/2023 Exchangeable Sodium Percentage NCDA-Agronomic Division 2.00 % 01/10/2023 Humic Matter NCDA-Agronomic Division 0.40 % 01/03/2023 Total Solids (%) SM 2540 8 85.0 % 12/22/2022 Total Phosphorus SM 4500 P F 84.5 mg/kg 01 /04/2023 pH SW 846 Method 9045D 6.54 units 01 /03/2023 Result estimated. Analyzed out of 15 minutes hold time. Report #;: 2022.25444 0 —1 • 7 Environmental Chemists, Inc. ,7envi-rochem A 6602 Windmill Way, Wilmington, NC 28405 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 ' 252A73.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS infout environmentalchemists.com MCAS Cherry Point Date of Report: Jan 10, 2023 PSC Box 8006 Customer PO #: Cherry Point NC 28533 Customer ID: 09110093 Attention: Steve Reavis Report #: 2022-25444 Project ID: Soil Sampling Lab ID Sample ID: Collect Date/Time Matrix Sampled by 22-62596 Site: MCAS FIELD #4 12/20/2022 11:22 AM Solid/Sludge Steve Reavis Test Method Results Date Analyzed Soil Fertility Calcium EPA 200.7 579 mg/kg 01/04/2023 Copper EPA 200.7 2.75mg/kg 01/04/2023 Magnesium EPA 200.7 94.6 mg/kg 01/04/2023 Manganese EPA 200.7 7.68 mg/kg 01/04/2023 Potassium EPA 200.7 82.6 mg/kg 01/04/2023 Sodium EPA 200.7 <23.4 mg/kg 01/04/2023 Zinc EPA 200.7 3.95 mg/kg 01/04/2023 Acidity (Soil Fertility) NCDA-Agronomic Division 0.5 meq/100g 01/03/2023 Base Saturation NCDA-Agronomic Division 88.9 % 01/10/2023 Cation Exchange Capacity NCDA-Agronomic Division 4.40 meq/100g 01/10/2023 Exchangeable Sodium Percentage NCDA-Agronomic Division 2.30 % 01/10/2023 Humic Matter NCDA-Agronomic Division 0.10 % 01/03/2023 Total Solids (%) SM 2540 B 90.6 % 12122/2022 Total Phosphorus SM 4500 P F 172 mg/kg 01/04/2023 pH SW 846 Method 9045D 8.25 units 01/03/2023 Result estimated. Analyzed out of 15 minutes hold time. Report #:: 2022-25444 0--- . -. - r- ppop, Environmental Chemists, Inc. envirochem 6602 Windmill Way, Wilmington, NC 28405 ' 910.392.0223 Lab • 910.392.4424 Fax +SM 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS info�ti•em+ironmentalchemists.com MCAS Cherry Point PSC Box 8006 Cherry Point NC 28533 Attention: Steve Reavis Date of Report: Jan 10, 2023 Customer PO #: Customer ID: 09110093 Report #: 2022-25444 Project ID: Soil Sampling Lab ID Sample ID: Collect DatelTime Matrix Sampled by 22-62597 Site: MCAS FIELD #5 12/20/2022 11:35 AM Solid/Sludge Steve Reavis Test Method Results Date Analyzed Soil Fertility Calcium EPA 200 7 720 mg/kg 01/04/2023 Copper EPA 200 7 5.78 mg/kg 01/04/2023 Magnesium EPA 2007 133 mg/kg 01/04/2023 Manganese EPA 200 7 8.44 mg/kg 01/04/2023 Potassium EPA 200 7 107 mg/kg 01/04/2023 Sodium EPA 200 7 <24.9 mg/kg 01/04/2023 Zinc EPA 200.7 8.05 mg/kg 01/04/2023 Acidity (Soil Fertility) NCDA-Agronomic Division 0.2 meq/100g 01/03/2023 Base Saturation NCDA-Agronomic Division 96.1 % 01/10/2023 Cation Exchange Capacity NCDA-Agronomic Division 5.20 meq/100g 01/10/2023 Exchangeable Sodium Percentage NCDA-Agronomic Division 2.10 % 01/10/2023 Humic Matter NCDA-Agronomic Division 0.29 % 01/03/2023 Total Solids (%) SM 2540 B 89.6 % 12/22/2022 Total Phosphorus SM 4500 P F 322 mg/kg 01/04/2023 pH SW 846 Method 90451) 7.01 units 01/03/2023 Result estimated. Analyzed out of 15 minutes hold time. Report #.. 2022-25444 P2— 9 „r 4 n . FPP Environmental Chemists, Inc. envirochem 6602 Windmill Way, Wilmington, NC 28405 a 910.392.0223 Lab + 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax sM 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS info(aenvironmentalchemists.com MCAS Cherry Point Date of Report: Jan 10, 2023 PSC Box 8006 Customer PO #: Cherry Point NC 28533 Customer 1D: 09110093 Attention: Steve Reavis Report #: 2022-25444 Project ID: Soil Sampling Lab ID Sample ID: Collect Date/Time Matrix Sampled by 22-62598 Site: MCAS FIELD #7 12/20/2022 11:56 AM Solid/Sludge Steve Reavis Test Method Results Date Analyzed Soil Fertility Calcium EPA 200.7 1560 mg/kg 01/04/2023 Copper EPA 200.7 7.07 mg/kg 01/04/2023 Magnesium EPA 200.7 214 mg/kg 01/04/2023 Manganese EPA 200.7 18.7 mg/kg 01/04/2023 Potassium EPA 200.7 156 mg/kg 01/04/2023 Sodium EPA 200.7 <29.1 mg/kg 01/04/2023 Zinc EPA 200.7 11.3 mg/kg 01/04/2023 Acidity (Soil Fertility) NCDA-Agronomic Division 0.9 meq/100g 01 /03/2023 Base Saturation NCDA-Agronomic Division 91.5 % 01 /10/2023 Cation Exchange Capacity NCDA-Agronomic Division 10.8 meq/100g 01 /10/2023 Exchangeable Sodium Percentage NCDA-Agronomic Division 1.20 % 01 /10/2023 Humic Matter NCDA Agronomic Division 0.42 % 01 /03/2023 Total Solids (%) SM 2540 B 85.1 % 12/22/2022 Total Phosphorus SM 4500 P F 350 mg/kg 01/04/2023 pH SW 846 Method 9045D 6.66 units 01/03/2023 Result estimated. Analyzed out of 15 minutes hold time. Environmental Chemist, Inc., Wilmington, NC Lab #94 6602 Windmill Way Wilmington, NC 28405 910.392.0223 ii Sample Receipt Checklist Client: NBC- 016 1 Date:q;U lao Report Number: _ 2022- D S�j y Receipt o!sample: ECHEM Pickup Client Delivery ❑ UPS ❑ FedEx ❑ ❑ YES❑ NO N/A 1. Were custody seals present on the cooler? ❑ YES ❑ NO N/A 2 If t d Other ❑ Original temperature upon cus o y seals were present, were they intact/unbroken? receipt `J °C , Corrected temperature upon receipt cc How temperature taken: ❑ Temperature Blank T Against Bottles IR Gun ID: Thomas Traceable S/N 210886869 IR Gun Correction Factor °C: 0.0 YES ❑ NO 3. If temperature of cooler exceeded 6°C, was Project Mgr./QA notified? YES ❑ NO 4. Were proper custody procedures (relinquished/received) followed? YES ❑ NO 5. Were sample ID's listed on the COC? YES ❑ NO 6. Were samples ID's listed on sample containers? YES ❑ NO 7. Were collection date and time listed on the COC? YES ❑ NO 8. Were tests to be performed listed on the COC? YES ❑Did samples arrive in proper containers for each test? YES ❑ NO 10. Did samples arrive in good condition for each test? YES ❑ NO 11. Was adequate sample volume available?' YES ❑ NO 12. Were samples received within proper holding time for requested tests? ❑ YES ❑ NO 13. Were acid preserved samples received at a pH of <2? ❑ YES ❑ NO 14. Were cyanide samples received at a pH >12? ❑ YES ❑ NO 15. Were sulfide samples received at a pH >9? ❑ YES ❑ NO 16. Were NH3/TKN/Phenol received at a chlorine residual of <0.5 m/L? ** ❑ YES ❑ NO 17. Were Sulfide/Cyanide received at a chlorine residual of <0.5 m/L? ❑ YES ❑ NO 18. Were orthophosphate samples filtered in the field within 15 minutes? * TOC/Volatiles are pH checked at time of analysis and recorded on the benchsheet. ** Bacteria samples are checked for Chlorine at time of analysis and recorded on the benchsheet. Sample Preservation: (Must be completed for any samples) incorrectly preserved or with headspace) Sample(s) were received incorrectly preserved and were adjusted accordingly by adding (circle one): H2SO4 HNO3 HCl NaOH Time of preservation: If more than one preservative is needed, notate in comments below Note: Notify customer service immediately for incorrectly preserved samples. Obtain a new sample or notify the state lab if directed to analyzed by the customer. Who was notified, date and time: Volatiles Sample(s) were received with headspace COMMENTS: DOC. QA.002 Rev 1 CL c A a c X z a O c O N j 6 0) D D D D colow) n TI -n 'n M ?1 •O jp m 'm m c� cc cD' eo c a v a a a W a N a ii 3 O C�fl W E a i i i i i �.► Fa m N N N N N N N N N A N N N O i i i i i i i i i Q i O � C77 CA CJ CT IV N O w 4 CA 6 O C4 �+ m c D co Sample 0 0 0 0 0 0 Type Composite 0 0 0 0 0 0 or Grab D 3 T hi 0 0 00 0 0 Container rn (P or G) N T NChlorine mglL m •11 ® N 3 V) N s+ LAB ID C 7 j . C NUMBER m " X x x x x x NONE HCL C� H2SW N M J. ;101 HNOI C 11 NAOH O a cn THIO z -4 w u OTHER q d � m 0 2za, u �7 0 c a w > cn r .� 7 y y II = o N y Cn 99 p C t O fDITI C Ye C U1 N 0 3 M v oni 0 C Cfl A n m z N Z C CO) Q 0 � n � (a O c � o �9 i a O m O -t O -1 m o D a ca 3 c mFA m � a cas so w a C c M T X 0 O O H m o to Z w o O d A. jQj N j C 0 m z X 0 Z E M Z r 0 M E ♦� Y z (01, PATHOGEN/VECTOR ATTRACTION REDUCTION FORM AND SUPPORTING DOCUMENTATION FOR MCAS CHERRY POINT Enclosure (1) ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM Facility Name: US Marine Corps - Cherry Point Permit Number: WWTP Name: USMCAS - Cherry Point WWTP NPDES Number: Monitoring Period: From l/l/2023 To 12/31/2023 WQ0001489 NC0003 816 Pathogen Reduction (40 CFR 503.32) - Please indicate level achieved and alternative performed: Class A: Alternative 1 ❑ Alternative 2 p Alternative 3 C3 Alternative 4 ❑ Alternative 5 ❑ Alternative 6 p If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost 01 Heat Drying ❑ Heat Treatment p Thermophilic p Beta Ray Ell Gamma Ray Pasteurization Class B: Alternative 1 ❑ Alternative 2 X Alternative 3 ❑ If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization X Air Drying ❑ Composting ❑ jAerobic Digestion p Anaerobic Digestion i n es o g .................................................................. ... If applicable to alternative performed (Class A or Class B) complete the following monito, ing data: Parameter Allowable Level in Sludge Pathogen Density Number of Excee- deuces Frequency of Anal vsis Sample Type Analytical ytica Tech - ni ue inimun Geo. Mean aximu Units Fecal Coliform 2 x 10 to the 6th power MPN per gram of total solids or 2 x 10 to the 6th power CFU per gram of 1000 mpn per gram of total solid (dry weight) Salmonella bacteria (in lieu of fecal coliform) 3 MPN per 4 grams total solid (dry weight) Vector Attraction Reduction (40 CFR 503.33) - Please indicate option performed: Option 1 ❑ Option 2 [11 Option 3 ❑ I Option 4 ❑ 13ption 5 ❑ Option 6 X Option 7 [31 Option 8 p Option 9 ❑ Option 10 C3 No vector attraction reduction formed er were options p P ❑ CERTIFICATION STATEMENT (please check the appropriate statement) X "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have been met." ® "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Richard Weaver, Env. Eng. Pre er Name and Ti e (type or print) Signature of Preparer Date Jeffery Clayton - ORC Land Applier Name and Title (if applicable)(type or print) Q)QY - Signature o an pplier (if applicable) D e DENR FORM RF (5/2003) TRIENNIAL GROUNDWATER MONITORING REPORTS Enclosure (1) 3/28/23, 6:29 AM Submission Completed Permit #: * Name of Facility:'' Month: February Report Information WQ0001489 MCAS Cherry Point Year:* 2023 4D NORTH CAROLINA Eft*Ww@Wmf qwft Type Upload Document' GW-59 Feb 2023 Triennual GW-59.pdf 547.89KB PDF Only Please upload one PDF containing all applicable monitoring reports (i.e., NDMR, NDAR-1, NDAR-2, NDMLR, GW-59). Confirmation Email Address:* Name of Submitter: Signature: * -Stubmittal Date:- richard.weaver@usmc.mil Richard Weaver an InalwIt 3/28/2023 Will be filled out automatically. https:Hedocs.deq.nc.gov/Forms/Form/Submit 1/1 UNITED STATES MARINE CORPS MARINE CORPS AIR STATION POSTAL SERVICE CENTER BOX 8003 CHERRY POINT, NORTH CAROLINA 28533-0003 IN REPLY REFER TO: 5090/071009 IN March 22, 2023 North Carolina Department of Environment Quality Division of Water Resources Information Processing Center 1617 Mail Service Center Raleigh, NC 27699-1617 SUBJECT: TRIENNIAL GROUNDWATER MONITORING In accordance with the groundwater monitoring and reporting requirements of MCAS Cherry Point's Non-NPDES permit WQ0001489 for Land Application of Wastewater Residuals, enclosed are the GW-59-A report and the three GW-59 reports (one each for monitoring wells 2, 3, and 5) for the triennial reporting for February 2023. Monitoring well 1 could not be tested because it was damaged during a land clearing process. We are currently examining locations for new monitoring wells and will request a permit modification as soon as new locations are determined. Should you have any questions, please contact Mr. Richard Weaver of the Environmental Affairs Department at your earliest convenience at (252) 466-5917. Sincerely, ANTH N A. FERENCE acilities Director By direction of the Commanding Officer Enclosures: 1. GW-59-A 2. GW-59 for MW-2 3. GW-59 for MW-3 4. GW-59 for MW-5 GW-59A COMPLIANCE REPORT FORM Permit # WQ0001489 (Submit one each monitoringperiod with GW-59forms) Enter date monitoring results were due. 3/31/2023 Will this monitoring report (GW-59 and GW-59A) be YES NO 1 submitted after the established due date? X Was any required information missing on the GW-59 report forms? YES NO 2 X IF the answer to question 1 or 2 is "YES", list in the space provided below the well identification number(s) and explain the problems encountered in obtaining the required information. Well MW-01 was not able to be tested. The well was damaged during a field clearing process. Are any of the monitor wells in need of repair or maintenance (damaged casing, unlocked or missing cap, YES NO 3 missing identification plate, area overgrown, etc.)? If the answer is "Yes", contact the Regional Office for guidance. X Are any monitored constituents equal to or above the established standards? YES NO 4 X If the answer to question 4 is "NO", skip to section 8. If the answer to question 4 is "YES" list the affected wells individually with constituent(s) and concentration(s) exceeding standards in the space provided below: MW-2 NH3: 2.8 MW-3 NH3: 7.7 MW-5 NH3: 2.0 For the constituents identified in question 4 above, have standards been exceeded previously for the same YES NO 5 constituent(s) in the same well(s) in the last two years? X If the answer to question 5 is "NO", skip to section 8. If the answer to question 5 is "YES", list in the space provided below, each well with constituent(s) exceeding standards, concentration(s) reported, and sample collection date for each occurrence (for the last two years). MW-2 NH3: 10/15/214.4 mg/l, 2116122 3.1 mg/l, 6/21/22 3.4 mg/1, 10/25/22 5.9 mg/1 MW-5 NH3: 10/15/214.1 mg/l, 2116/22 3.5 mg/4 6/21/22 2.6 mg/l, 10/25/22 4.0 mg/1 Are the monitoring wells listed in section 5 located at or beyond the review boundary? YES NO 6 X If the answer is "YES", a groundwater quality problem may be occurring. CONTACT THE REGIONAL OFFICE IMMEDIATELY FOR GUIDANCE. If the answer is "NO", monitoring wells may be improperly located; contact the Regional Office. Is the permittee implementing previously approved actions required by the Division involving this groundwater YES NO 7 quality problem? X If the answer to question 7 is "YES", describe those actions in the space provided below. If the answer to question 7 is "NO", contact the Regional Office within 90 dacs• an evaluation may be required to determine the impact the waste disposal s%stem is having at the review and compliance boundaries surrounding this facilitN. Failure to do so maN subject the permittee to a Notice of Violation, fines. and/or penalties. The person completing this portion (GW-59A) of the monitoring report should sign below and submit this form with 8 GW-59 forms for required wells to the address provided at the top of the current GW-59 form. 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O O ao v 0 Lo M V O a- E N M O Ln E M CO O) O Ln ti O O fD E W O t L �' Z € M M :: a y 0 W 0 0 0 Co Cl N O O O a O O F .20 ch m t t` O O O O O M O O O y O CY W A� ..0 ai O a °'2 �vn m m U m_� a a; cam z F Q m a ' E a E a > O a�i C$ o v 0 aci O aci w c o z W QU �U as g o a�i �'O44))LU LLF� F �-o E2'D m E iF F- W N 0 � � E �S Z� C LL� za v Q U a m a N 5 E m Y QV a Orr Z Z ca Q ZO LL W azJ O LL o E o m U 9 Ena o Om o FEZJ ai F _ N E a o a cn _ CL J t O Q co € m o m Q �L J! aL aai ami o E Q a O C7 C% LL LL d LL U� N$: O > rn J 0 LL 0 E O n m Z m c rn r5 m d Z, Lo C .a m y la m a m c c N m E m �z . C m O N s m ¢ o) L ffLO 'S. QL V a 7/IVU3, /:43AM Submission Completed ,i r k NonDischarge Monitoring Report + ram! Permit #: W00001489 Name of Facility:* US MCAS Cherry Point RLAP Month: * June 2023 Report Information ` Upload Document* GW-59 G W-59-A_Ju ne_2023. pdf 562.65KB PDF Only Please upload one PDF containing all applicable monitoring reports (i.e., NDMR, NDAR-1, NDAR-2, NDMLR, GW-59). Confirmation Email Address:* Name of Submitter: Signature: * Submittal Date: richard.weaver@usmc.mil Richard Weaver 7/19/2023 Will be filled out automatically. https://edocs.deq.nc.gov/Forms/Form/Submit 1/1 UNITED STATES MARINE CORPS MARINE CORPS AIR STATION POSTAL SERVICE CENTER BOX 8003 CHERRY POINT, NORTH CAROLINA 28533-0003 IN REPLY REFER TO: 5090/071009 LN July 17, 2023 North Carolina Department of Environment Quality Division of Water Resources Information Processing Center 1617 Mail Service Center Raleigh, NC 27699-1617 SUBJECT: TRIENNIAL GROUNDWATER MONITORING In accordance with the groundwater monitoring and reporting requirements of MCAS Cherry Point's Non-NPDES permit WQ0001489 for Land Application of Wastewater Residuals, enclosed are the GW-59-A report and the three GW-59 reports (one each for monitoring wells 2, 3, and 5) for the triennial reporting for June 2023. Monitoring well 1 could not be tested because it was damaged during a land clearing process. We are currently examining locations for new monitoring wells and will request a permit modification as soon as new locations are determined. Should you have any questions, please contact Mr. Richard Weaver of the Environmental Affairs Department at your earliest convenience at (252) 466-5917. Sincerely, fNY FERENCE acilities Director By direction of the Commanding Officer Enclosures: 1. GW-59-A 2. GW-59 for MW-2 3. GW-59 for MW-3 4. GW-59 for MW-5 GW-59A COMPLIANCE REPORT FORM WQ0001489 (Submit one each monitoring period with GW-59 forms) Enter date monitoring results were due. 7/31/2023 Will this monitoring report (GW-59 and GW-59A) be YES NO 1 submitted after the established due date? X Was any required information missing on the GW-59 report forms? YES NO 2 X IF the answer to question 1 or 2 is "YES", list in the space provided below the well identification number(s) and explain the problems encountered in obtaining the required information. Well MW-01 was not able to be tested. The well was damaged during a field clearing process. Are any of the monitor wells in need of repair or maintenance (damaged casing, unlocked or missing cap, YES NO 3 missing identification plate, area overgrown, etc.)? Ifthe answer is "Yes", contact the Regional OA'ice forguidance. X Are any monitored constituents equal to or above the established standards? YES NO 4 X If the answer to question 4 is "NO", skip to section 8. If the answer to question 4 is "YES" list the affected wells individually with constituent(s) and concentration(s) exceeding standards in the space provided below: MW-2 NH3: 5.9 MW-3 NH3: 5.3mg/l, TDS: 1256 mg/1, TOC: 10.8mg/1 MW-5 NH3: 4.1 For the constituents identified in question 4 above, have standards been exceeded previously for the same YES NO 5 constituent(s) in the same well(s) in the last two years? X If the answer to question 5 is "NO", skip to section 8. If the answer to question 5 is "YES", list in the space provided below, each well with constituent(s) exceeding standards, concentration(s) reported, and sample collection date for each occurrence (for the last two years). MW-2 NH3: 2/16/22 3.1 mg/l, 6/21/22 3.4 mg/l,10/25/22 5.9 mg/l, 2/6/23 2.8 mg/1 MW-3 NH3: 2/7/23 7.7mg/1 MW-5 NH3: 2/16/22 3.5 mg/l, 6/21/22 2.6 mg/l, 10/25/22 4.0 mg/1, 2/6/23 2.0mg/1 Are the monitoring wells listed in section 5 located at or beyond the review boundary? YES NO 6 X If the answer is "YES", a groundwater quality problem may be occurring. CONTACT THE REGIONAL OFFICE IMMEDIATELY FOR GUIDANCE. If the answer is "NO", monitoring wells may be improperly located; contact the Regional Office. Is the permittee implementing previously approved actions required by the Division involving this groundwater YES NO 7 quality problem? X If the answer to question 7 is "YES", describe those actions in the space provided below. If the answer to question 7 is "NO", contact the Regional Office within 90 da%s: an evaluation mar be required to determine the impact the waste disposal st stem is havine at the review and compliance boundaries surrounding this facilih. Failure to do so mar subject the permittee to a Notice of Violation, flues, and/or penalties. The person completing this portion (GW-59A) of the monitoring report should sign below and submit this form with 8 GW-59 forms for required wells to the address provided at the top of the current GW-59 form. I hereby acknowledge that the above information was evaluated and the information submitted in this report (Compliance Report GW-59A) is true and complete to the best of my knowledge. Anthony A Ference Deputy Facilities Director (b, Direction of Commanding Officer) Signature of Permittee (or Authorized Agent) Date / 7 y M W °pax ❑ 3a9EE� w3o:�Mut .. j H e wS M Z H q N 8 N NO .� Q❑ O N O t 3LLI C ` N J K r c O E U J a y o 0 0 0 Cc m :.i _ p �Z G c O N a� w8 0m oE'-' a m � d w ea isCCLL m _ ❑ O ga 0 C7 a�i aqi 9 d aEi F" c m E o3 w.0 0 Q ��pp o o 00 -Z d U 3 C a O E W w J �l .c ° r N U 'O Do X wCD O . 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NORTH CAROLINA &VW6l MWftIV1QWft Permit #: * Name of Facility: Month: October Report Information G W-59 WQ0001489 MCAS Cherry Point RLAP Year:* 2023 Upload Document* GW-59 Triennial groundwater monito. 1.23MB PDF Only Please upload one PDF containing all applicable monitoring reports (i.e., NDMR, NDAR-1. NDAR-2, NDMLR, GW-59). Confirmation Email Address:* richard.weaver@usmc.mil Name of Submitter: J Richard Weaver Signature: Submittal Date: 12/1 /2023 Will be filled out automatically. https:/Iedocs.deq.nc.gov/Forms/Form/Submit ill UNITED STATES MARINE CORPS MARINE CORPS AIR STATION POSTAL SERVICE CENTER BOX 8003 CHERRY POINT, NORTH CAROLINA 28533-0003 IN REPLY REFER TO: 5090/071009 LN November 27, 2023 North Carolina Department of Environment Quality Division of Water Resources Information Processing Center 1617 Mail Service Center Raleigh, NC 27699-1617 SUBJECT: TRIENNIAL GROUNDWATER MONITORING In accordance with the groundwater monitoring and reporting requirements of MCAS Cherry Point's Non-NPDES permit WQ0001489 for Land Application of Wastewater Residuals, enclosed are the GW-59-A report and the three GW-59 reports (one each for monitoring wells 2, 3, and 5) for the triennial reporting for October 2023. Monitoring well 1 could not be tested because it was damaged during a land clearing process. We are currently examining locations for new monitoring wells and will request a permit modification as soon as new locations are determined. Should you have any questions, please contact Mr. Richard Weaver of the Environmental Affairs Department at your earliest convenience at (252) 466-5917. Sincerely, ANTH Y , . FER$NCE Dep Facilities Director By direction of the Commanding Officer Enclosures: 1. GW-59-A 2. GW-59 for MW-2 3. GW-59 for MW-3 4. GW-59 for MW-5 GW-59A COMPLIANCE REPORT FORM Permit # WQ0001489 (Submit one each monitoring period with GW-59 forms) Enter date monitoring results were due. 11/30/2023 Will this monitoring report (GW-59 and GW-59A) be YES NO I submitted after the established due date? X 2 Was any required information missing on the GW-59 report forms? YES NO X IF the answer to question 1 or 2 is "YES", list in the space provided below the well identification number(s) and explain the problems encountered in obtaining the required information. Well MW-01 was not able to be tested. The well was damaged during a field clearing process Are any of the monitor wells in need of repair or maintenance (damaged casing, unlocked or missing cap, YES NO 3 missing identification plate, area overgrown, etc.)? lfthe answer is "Yes", contact the Regional Ofceforguidance. X YES NO 4 Are any monitored constituents equal to or above the established standards? X If the answer to question 4 is 'NO", skip to section 8. If the answer to question 4 is "YES" list the affected wells individually with constituent(s) and concentration(s) exceeding standards in the space provided below: MW-2 NH3: 3.5mg/l, TDS: 664mg/I MW-3 NH3: 2.8mg/I, TDS: 608mg/l MW-5 NH3: 2.9m /1 TOC: 12.2 ,/I For the constituents identified in question 4 above, have standards been exceeded previously for the same YES NO 5 constituent(s) in the same well(s) in the last two years? X If the answer to question 5 is "NO", skip to section 8. If the answer to question 5 is "YES", list in the space provided below, each well with constituent(s) exceeding standards, concentration(s) reported, and sample collection date for each occurrence (for the last two years). MW-2 NH3: 6/21/22 3.4mg/I, 10/25/22 5.9mg/l, 2/6/23 2.8mg/l, 6/12/23 5.9mg/I MW-3 NH3: 2/7/23 7.7mg/l, 6/13/23 5.3mg/I, TDS: 6/13/23 1256mg/1 MW-5 NH3: 6/21/22 2.6mg/l, 10/25/22 4.Omg/1, 2/6/23 2.Omgfl, 6/12/23 4.1 mg/l 6 Are the monitoring wells listed in section 5 located at or beyond the review boundary? YES NO X If the answer is "YES", a groundwater quality problem may be occurring. CONTACT THE REGIONAL OFFICE IMMEDIATELY FOR GUIDANCE. If the answer is "NO", monitoring wells may be improperly located; contact the Regional Office. Is the permittee implementing previously approved actions required by the Division involving this groundwater YES NO 7 quality problem? X If the answer to question 7 is "YES", describe those actions in the space provided below. If the answer to question 7 is "NO", contact the Regional Office within 90 da%s: an evaluation ma% be required to determine the impact the waste disposal sr stem is having at the review and compliance boundaries surrounding this facility Failure to do so ma% subject the permittee to a Notice of Violation. fines, and/or penalties. The person completing this portion (GW-59A) of the monitoring report should sign below and submit this form with 8 GW-59 forms for required wells to the address provided at the top of the current GW-59 form. I hereby acknowledge that the above information was evaluated and the information submitted in this report (Compliance Report GW-59A) is true and complete to the best of my knowledge. 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UI V a�i z U Q V z ® v v N r �' C .N_ Q O LL W J vi 7 CL N? a) �' C Z a, o G N ° Q o U) C G a z E E °o z :: o m E 0 T� € o' v E v o 0 E° Z 0 . d N O IL Z Z Q n. v z a ?� m o w g E W o o z U v o O J�� m J ) r .N E n 0 y Z U o _n 0 0 IQilia0 co .LL U� w am 0-joa e 0 E !V ff) 0 O c m 7 W L R 0 a N a N L c R U Eto LL N wO © ¢ N N ° V N N N N O N N L LL 3 Qa� .0 ANALYTICAL 8 CONSULTING CHEMISTS F"00--. -, -"7 Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 . 910.392.0223 Lab + 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 � 910.347.5843 Lab/Fax info@envimnmentalchemists.com MCAS Cherry Point Date of Report: Nov 21, 2023 PSC Box 8006 Customer PO #: Cherry Point NC 28533 Customer ID: 09110093 Attention: Report #: 2023 24498 Project ID: MCAS MW Lab ID Sample ID: Collect Date/Time Matrix Sampled by 23-59486 Site: MW 2 10/19/2023 10:20 AM Water Susan Leary Test Method Results Date Analyzed 1. 1, 1,2-Tetrachloroethane SW "0 Me" SMD/5030B <0.5 pg/L 10/28/2023 1,1,1-Trichlomethane SW 8" MWW OMDr5030B <0.5 pg/L 10/28/2023 1,1,2,2-Tetrachloroethane SW 848 Memod 8280D150308 <0.5 pg/L 10/28/2023 1,1,2-Trichloroethane SW Wfi4e0wd CMD/W3OB <0.5 pg/L 10/28/2023 1,1-Dichloroethane SW 80 Memod MOD150 0B <0.5 pg/L 10/28/2023 1,1-Dichloroethene SW 848 Memod 8280D=30B <0.5 pg/L 10/28/2023 1,1-Dichloropropene SW 848 McOwd 8MD=308 <0.5 pg/L 10/28/2023 1,2,3-Trichlorobenzene SW 848 Memed 8MD/50MB <0.5 pg/L 10/28/2023 1,2,3-Trichloropropane SW 80 MemOd 8260DI5 M <0.5 pg/L 10/28/2023 1,2,4-Trichlorobenzene SW 848 Method 82MISOM <0.5 pg/L 10/28/2023 1,2,4-Trimethylbenzene SW 846 Memos e280D/5030B <0.5 pg/L 10/28/2023 1,2-Dibromo-3-Chloropropane SW 846 r+ WW e280D/5030B <0.5 pg/L 10/28/2023 1,2-Dibromoethane SW 848 MW*d 8280D/5030B <0.5 pg/L 10/28/2023 1, 2-Dichlorobenzene SW 846 Memod 828oD/5030B <0.5 pg/L 10/28r2023 1,2-Dichloroethane SW 848 Memos 8280D/50306 <0.5 pg/L 10/28/2023 1,2-Dichloropropane SW 848 Method MOM030B <0.5 pg/L 10/28/2023 1,3,5-Trimethylbenzene SW 846 MethW 828oD/503oB <0.5 pg/L I U2812023 1,3-Dichlorobenzene SW 848 Method 8Z8oD/503o8 <0.5 pg/L 10/28/2023 1,3-Dichloropropane SW 846 L%Uwd 8280D/5030B <0.5 pg/L 10/28/2023 1,4-Dichlorobenzene SW 046 Memos 8280D/5030S <0.5 pg/L 10/28/2023 2,2-Dichloropropane SW 80 Memos 82ND150M <0.5 pg/L 10/28/2023 2-Chlorotoluene sw So Memod 82M5030B <0.5 pg/L 10/28/2023 4-Chlorotoluene SW 848 Memos e2M50N08 <0.5 pg/L 10/28/2023 Benzene SW 848 Meawd 826MM308 <0.5 pg/L 10/282023 Bromobenzene SW $46 Memos 82NMO308 <0.5 pg/L 10/28/2023 Bromochloromethane SW 846 Memos 8280D/5030B <0.5 pg/L 10/28a023 Repot M. 2023.24488 Page 1 of 9 envirochem -I ANALYTICAL & CONSULTING CHEMISTS MCAS Cherry Point PSC Box 8006 Cherry Point Attention: Environmental Chemists, Inc.. 6602 Windmill Way, Wilmington, NC 28405 = 910.392A223 Lab , 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 w 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 F• 910.347.5843 Lab/Fax info@environmentalchemistscom Date of Report: Nov 21, 2023 Customer PO #: NC 28533 Customer ID: 09110093 Report #: 2023-24498 Project ID: WAS MW Bromod ihloromethane SW NO M99M WW W WS <0.5 pg/L 10/28/2023 Bromoform SW e46 McMW 82NDW308 <0.5 pg/L 10/28/2023 Bromomethane SW 846 Memos 82NDUMS <0.5 pg/L 10/28/2023 Carbon tetrachloride SW 646 Memod 8280D15030B <0.5 pg/L 10/28t2023 Chlorobenzene SW 846 Me#wd BMIV5=B <0.5 pg/L 10/28/2023 Chloroethane SW 846 Medwa 82OW5030D <0.5 pg/L 10/28/2023 Chloroform SW 846 Meewd 8260D150308 <0.5 pg/L 10/28/2023 Chloromethane SW 846 Memos 828ODMO30B <0.5 pg/L 10/28/2023 cis-1,2-Dichloroethene SW Sae Memod 82so SGWB <0.5 pg/L 10/28/2023 cis-1,3-Dichloropropene SW 046 Method 6260D1503M <0.5 pg/L 10/28/2023 Dibromochloromethane SW 846 Memos e26oD15o308 <0.5 pg/L 10/28/2023 Dibromomethane sw 8" Memos 82WD15MB <0.5 pg/L 10/28/2023 Dichlorodifluoromethane SW 846 Menwa 626OW50306 <0.5 pg/L 10/28/2023 Ethylbenzene SW a46 Method 6260DI5030B <0.5 PA 10/28/2023 Hexachlorobutadiene SW 846 Memos 626011 MS <0.5 pg/L 10/28/2023 lsopropylbenzene SW $46 Memod 8260D150308 <0.5 pg/L 10/28/2023 M+P Xylene SW US Memos 82800/50308 <1.0 pg/L 10/28/2023 Methylene chloride SW 846 Me9wd 8260015OWS <0.5 pg/L 10/28/2023 Naphthalene SW 846 Memos 826ODr50WO <0.5 pg/L 10/28/2023 n-Butylbenzene SW 846 Memos 826ODMO308 <0.5 pg/L 10/28/2023 n-Propylbenzene SW 646 Memos e260D15030s <0.5 pg/L 10/28/2023 ortho-Xylene SW 848 Memos e2s0D/5WOB <0.5 pg/L 10/28/2023 p-lsopropyltoluene SW 848 Memos 826OD150308 <0.5 pg/L 10/28/2023 sec-Butylbenzene SW 8" %*wd 828=5030B <0.5 pg/L 10/28/2023 Styrene SW 8" Method e260D15030B <0.5 pg/L 10/28/2023 tert-Butylbenzene SW e48 Method 8260D/5W08 <0.5 pg/L 10/28/2023 Tetrachloroethene SW a46 Method OMD1503oB <0.5 pg/L 10/28/2023 Toluene SW a" Memos 8260DI50308 <0.5 pg/L 10/28/2023 Trans-1,2-Dichloroethene SW a46 Memos 826OD15MOS <0.5 pg/L 10I28/2023 Trans-1, 3-dichloropropene SW 848 Memos 625=5=8 <0.5 pg/L 10/28/2023 Report a: 2023.24498 Page 2 019 ANALYTICAL & CONSULTING CHEMISTS MCAS Cherry Point PSC Box 80D6 Cherry Point NC 28533 Attention: Trichloroethene Tdchlomfluoromethane Vinyl chloride Environmc n tal Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 & 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 % 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 * 910.347.5843 Lab/Fax infog'environmentalchemists.com Date of Report: Nov 21, 2023 Customer PO N: Customer ID: 09110093 Report #: 2023-24498 Project ID: MCAS MW sw Ns Wuxi aze DW3oe <0.5 lig/L 10/28/2023 SW 80 Method e200D/603os <0.5 lig/L 10/28/2023 sw 048 Method SMOD15030B <0.5 lig/L 10/28/2023 Report a:: 2023-24488 Page 3 of 9 envirochem ANALYTICAL A CONSULTING CHEMISTS EnvirmnmentW Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab e 910.392.4424 Fax 710 Bowsertown (toad, Manteo, NC 27954 • 252.4735702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax info(&; environmenta tchemists.00m MCAS Chevy Point Date of Report: Nov 21, 2023 PSC Box 8006 Customer PO #: Cherry Point NC 28533 Customer ID: 09110093 Attention: Report #: 2023-24498 Project ID: MCAS MW Lab ID Sample ID: Collect Datemme Matrix Sampled by 23-59490 Site: MW-3 10/19/2023 11:05 AM Water Susan Leary Test Method Results Date Analyzed 1,1,1,2-Tetrachloroethane sw 046 MethW SZOI) soaoe <0.5 Vg/L 10128/2023 1,1,1-Trichloroethane sw 645 Method 826OD15MB <0.5 pg/L 10/28/2023 1,1,2,2-Tetrachloroethane SW846LWVd8260Dl5 M <0.5ug/L 10/28/2023 1,1,2-Tdchloroethane SW $45 Method 8260MMB <0.5 pg/L 10/28/2023 1,1-Dichloroethane SW 046 Method 628OD15MB <0.5 Ng/L 10/28/2023 1, 1 -Dichloroethene SW e46 Meewd e260DJ50= <0.5 pg/L 10/28/2023 1,1-Dichloropropene SW 846 memos 82GOD150M <0.5 Ng/L 10/28/2023 1,2,3-Trichlorobenzene SW846Meeiode260DAMS <0.5 pg/L 10/28/2023 1,2,3-Trichloropropane SW 846 Method 826ODMMS <0.5 Ng/L 10/28/2023 1,2,4-Trichlorobenzene SW 846 Method 826=5o3011 <0.5 pg/L 10/28/2023 1,2,4-Trimethylbenzens sw 846 McOwd $260I) "11 <0.5 pg/L 10/28/2023 1,2-Dibromo-3-Chloropropane SW 046 McOwd 8260Drs MB <0.5 pg/L 10/28/2023 1,2-Dibromoethane SW 846 Method MOD/503o13 <0.5 pg/L 10/28=23 1,2-Dichlorobenzene SW $46 Method MOD/et = <0.5 Ng/L 10/28/2023 1,2-Dichloroethane swea Method 826op1 MB <0.5 pg/L 10/28/2023 1,2-Dichloropropane SW 80Idedwd BMDW300 <0.5 Ng/L 10/28/2023 1,3,5-Tdmethylbenzene SW e46 Method 8260D15030B <0.5 pg/L 10/28/2023 1, 3-Dichlorobenzene SW 646 Method 8280DUMB <0.5 pg/L 10/28/2023 1,3-Dichloropropane SW 646 Method 82sooMWB <0.5 pg/L 10/28/2023 1,4-Dichlorobenzene SW e46 Memos e29 D=30e <0.5 pg/L 10/28/2023 2,2-Dichloropropane SW e46 Memos 6MDM30B <0.5 pg/L 10/28/2023 2-Chlorotoluene Sw646 Memod 528W5030B <0.5 pg/L 10/28/2023 4-Chlorotoluene SW "a Method 82600/50308 <0.5 pg/L 10/28/2023 Benzene S^+848 MeuW 8280DW308 <0.5 pg/L 10/28/2023 Bromobenzene SW $46 Method 826ODMO30B <0.5 pg/L 10/28/2023 Bromochloromethane SW 846 Method S2600150308 <0.5 pg/L 10/28/2023 Repot M: 2023-24498 - - - — Page 4 of 9 i ANALYTICAL d CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 910.392.0223 Lab 910392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 * 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 . 910347SM Lab/Fax info(aenvironmentalchemists.com MCAS Cherry Point Date of Report: Nov 21, 2023 PSC Box 8008 Customer PO #: Cherry Point NC 28533 Customer ID: 09110093 Attention: Report #: 2023 24498 Project ID: MCAS MW Bromodichloromethane SW 0" Method 8260=30B <0.5 pg/L 10/28/2023 Bromoform SW s46 Method 8280D=308 <0.5 pg/L 10,08/2023 Bromomethane SW e4s Method 8260MO30B <0.5 pg/L 10/28/2023 Carbon tetrachloride SW 8" Method SMEW5030B <0.5 pg/L 10/28/2023 Chlorobenzene SW 80 AAethod a460D=30B <0.5 pg/L 10/28/2023 Chloroethene SW ers Method 8280D/50306 <0.5 pg/L 10/28QO23 Chloroform SW 0" Method 8260D15030B <0.5 pg/L 10/28/2023 Chloromethane sw 848 Method 826OW030B <0.5 pg/L 10/28/2023 cis-1,2-Dichloroethene SW 846Method 8280DW30B <0.5 pg/L 10/28/2023 cis-1,3-Dichlompropene SW 8" Method 826000030B <0.5 pg/L 10/28/2023 Dibromochloromethane SW 8" Method 82SOM5030B <0.5 pg/L 10/28/2023 Dibromomethane SW 948 Method W60/5030e <0.5 pg/L 10/28/2023 Dichiorodifluommethane SW e46 Method 8260w5030B <0.5 pg/L 10/28/2023 Ethylbenzene SW 846 Method U60DW308 <0.5 pg/L 10/2W023 Hexaehlorobutadiene SW 646 Method 828ae,50306 <0.5 pg/L 10/28/2023 Isopropylbenzene sw 846 Method &MDvso30B <0.5 pg/L 10/28/2023 M+P Xylene SW 845 Method 82ND/5030B <1.0 pg/L 10/28/2023 Methylene chloride SW 846 Method 8260D/5030 <0.5 pg/L 10/28/2023 Naphthalene SW 846 Method 8260DM03M <0.5 pg/L 10/28/2023 n-Butylbenzene SW 846 Method 8280D/50309 <0.5 pg/L 10/28/2023 n-Propylbenzene SW 846 Method 8260015030E <0.5 pg/L 10/2812023 ortho-Xylene sw $46 Method tt2600/5030e <0.5 pg/L 10/28/2023 p-Isopropyltoluene sw 848 Method 82OD1503M <0.5 pg/L 10/28/2023 sec-Butylbenzene SW 848 Method 8=D/5 = <0.5 pg/L 10/28/2023 Styrene sw $46 Method e280DI5=8 <0.5 pg/L 10/28/2023 tert-Butylbenzene sW 84e Method 828aD/sosoB <0.5 pg/L 10/28/2023 Tetrachloroethene SW "S Method 82M5o3OB <0.5 pg/L 10/28f2023 Toluene sw 0" Method 8260015030E <0.5 pg/L 10/28/2023 Trans-1 ,2-Dichioroethene sw 0" Method 82SWI5030B <0.5 pg/L 10/28/2023 Trans-1,3-dichloropropene SW $48 Method 826=5030B <0.5 pg/L 10/28/2023 Report c 2023.24498 Pace s a e Lenviroehem ANALYTICAL & OONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 ; 910.392.0223 Lab , 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 5- 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 910.347.5843 Lab/Fax info@environmentalchemists.com MCAS Cherry Point Date of Report: Nov 21, 2023 PSC Box 8006 Customer PO M Cherry Point NC 28533 Customer ID: 09110093 Attention: Report M 2023-24498 Project ID: MCAS MW Trichloroethene Sw so Meow FAUDIS0308 <0.5 pWL 10/28/2023 Trichlorofluoromethane SW M 6 McMod e26oDM306 <0.5 pWL 10/28/2023 Vinyl chloride Sw me Klemm MMDM306 <0.5 I.tg/L 10/28/2023 Report # . 2023-24498 Page 6 of 9 -1707 Environmental Chemists, Inc. envirochem 6602 Windmill Way, Wilmington, NC 28405 is 910.39Z0223 Lab a 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 ■ 252A73.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax ANALYTICAL 3 CONSULTING CHEMISTS info@environmentalchemistscom MCAS Cherry Point Date of Report: Nov 21, 2023 PSC Box 8006 Customer PO #: Cherry Point NC 28533 Customer ID: 09110093 Attention: Report #: 2023-24498 Project ID: MCAS MW Lab ID Sample ID: Collect Date/Time Matrix Sampled by 23-59491 Site: MW-5 10/19/2023 9:35 AM Water Susan Leary Test Method Results Date Analyzed 1.1,1,2-Tetrachioroethane SwsaeWmoa825O soeoB <0.5pg/L 10/28/2023 1,1,1-Trichloroethane SW 80 WWthW SMM <0.5 pg/L 10/28/2023 1,1,2,2-Tetrachioroethane SW B46 Mes+od 92BODl5 M <0.5 pg/L 10/28/2023 1,12-Trichloroethane sw e46 AWMW ers M030B cO.5 pg/L 10/28/2023 1,1-Dichioroethane sw sae Memos OMDM306 <0.5 pg/L 10/28/2023 1,1-Dichloroethene SW 0" WOW MQD(5=B <0,5 pg/L 10/28/2023 1,1-Dichloropropene SW 84e Meaad SMOM030B <0.5 pg/L 10/28/2023 1,2,3-Trichlorobenzene sw eae Meuwa 8zsoD"08 <0.5 pg/L 10/28/2023 1,2,3-Trichloropropane sw64eMW4dszsowsoso6 <0.5 pg/L 10/28/2023 VA-Trichlorobenzene SW eas Memos 828ot/5030B <0.5 pg/L 10/28/2023 1,2,4-Trimethylbenzene SW B4e Memod 8200MOSOB <0.5 pg/L 10/28/2023 1,2-Dibromo-3-Chloropropane SW 846 Memos 82eoo/50308 <0.5 pg/L 10/28/2023 1,2-Dibromoethane SW e46 Memod 82soor5030 <0,5 pg/L 10/28/2023 1,2-Dichlorobenzene SW 84e Method 828o ONO <0.5 pg/L 10/28/2023 1,2-Dichloroethane SW Bae McMod s2eoMONG <0.5 pg/L 10/28/2023 1, 2-Dichloropropane SW 8" Memos 826ODMO308 <0.5 pg/L 10/28/2023 1,3,5-Trimethyibenzene SW84BMeVW82wisom <0.5pg/L 10/28/2023 1,3-Dichlorobenzene SW 846 Memod 82M6030B <0.5 pg/L 10/28/2023 1,3-Dichloropropane SW sae Mamod 6260DW3013 <0.5 pg/L 10/28/2023 1,4-Dichlorobenzene sw w Memos MOIX5030B <0.5 pg/L 10/28/2023 2,2-Dichloropropans sw e46 Memod 6260DW30B <0.5 pg/L 10/28/2023 2-Chlorotoiuene sw 8" Memod BMDMWoB <0.5 pg/L 10/2W023 4-Chlorotoluene SW On Mettwd BMDUMB <0.5 pg/L 10/28/2023 Benzene Sw e4e Memos e201)15=B <0.5 pg/L 10/28/2023 Bromobenzene sw e4e Memos 8260o150308 <0.5 pg/L 10/28/2023 Bromochioromethane SW 84e Memos 8260015OUS <0.5 pg/L 10/28/2023 Report 2023-24498 Pape 7 ae Environmental Chemists, Inc. envirochem 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab 1, 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252A73.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.3475843 Lab/Fax ANALYTICAL 8 CONSULTING CHEMISTS infolatnvironmentalchemist&com MCAS Cherry Point Date of Report: Nov 21, 2023 PSC Box 8006 Customer PO 0: Cherry Point NC 28533 Customer ID: 09110093 Attention: Report 0: 2023-24498 Project ID: WAS MW Bromodichloromethane sw 80 MW%od 8P80DISMS <0.5 pg/L 10/28/2023 Bromoform SW NO Memod 8280Dl50308 <0.5 pg/L 10/28/2023 Bromomethane SW 848 "%1W MODI °0B <0.5 pg/L 10/28/2023 Carbon tetrachloride SW 848 Method 6200DMMB <0.5 pg/L 10/28/2023 Chlorobenzene sw B48 Mettmd 826OD150 B <0.5 pg/L 10/28/2023 Chloroethane sw 846 Mew 8280D=DB <0.5 pg/L 10/28/2023 Chloroform SW 846 Method SMODM308 <0.5 pg/L 10/28/2023 Chloromethane sw 80 Monad ONODW30B <0.5 pg/L 10/28/2023 cis-1,2-Dichloroethene SW B48 Memod 8280DJ5030e <0,5 pg/L 10/28/2023 cis-1, 3-Dichlompropene SW 840 Method 828oDffi=B <0.5 pg/L 10/28/2023 Dibromochloromethane SW 846 Memos 82WO150308 <0.5 pg/L 10/28/2023 Dibromomethane SW 848 Memos e2eoDmuo <0.5 pg/L 10/28/2023 Dichlorodifluoromethane SW 846 Medmd 8280DMUS <0.5 pg/L 10/28/2023 Ethylbenzene SW 846 Memos 8280D UMB <0.5 pg/L 10/28/2023 Hexachlorobutadiene SW 8" Memos 8280Dl5030B <0.5 pg/L 10/28/2023 lsopropyibenzene SW 848 Monad 82ND15030B <0.5 pg/L 10/28/2023 M+P Xylene SW 846 Memos BMODM30B <1.0 pg/L 10/28/2023 Methylene chloride SW 848 Method BMM5030B <0.5 pg/L 10/28/2023 Naphthalene sw 848 MOW 826OW5030B <0.5 pg/L 10/28/2023 n-Butylbenzene SW Us Memos 826017a503os <0.5 pg/L 10/28/2023 n-Propylbenzene SW 846 Memos 828oD/5WOB <0.5 pg/L 10/28/2023 ortho-Xylene SW 80 Method 828oDMUS <0.5 pg/L 10/28/2023 p-isopropyltoluene sw 848 Method BMOMOMB <0.5 pg/L 10/28/2023 sec-Butylbenzene SW 846 Memos 9MDMWB <0,5 pg/L 10/28/2023 Styrene SW 046 Method 8280 =30B <0.5 pg/L 10/28/2023 tort-Butylbenzene SW 048 Method 82BODW30B <0.5 pg/L 10/28/2023 Tetrachioroethene sw 846 Method 8260DW308 <0.5 pg/L 10/28/2023 Toluene sw 848 Memos 828O0MMB <0.5 pg/L 10/28/2023 Trans-1 ,2-Dichloroethene SW e+e MORW 82sOwsMB <0.5 pg/L 10/28/2023 Trans-1,3-dic hloropropene SW 848Meumd 828oa503o8 <0.5 pg/L 10/28/2023 Report Y : 2023-24498 - - Pegs 8 of 9 IL envirochem ANALYTICAL & CONSULTING CHEMISTS F00,057 41 Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 #, 910.392.0223 Lab P 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 c 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 * 910.347.5543 Lab/Fax info@environmentalchemismoom MCAS Cherry Point Date of Report: Nov 21, 2023 PSC Box 8006 Customer PO M Cherry Point NC 28533 Customer ID: 09110093 Attention: Report #: 2023 24496 Project ID: MCAS MW Trichloroethene sw US Method 8260D15 M8 <0.5 Ng/L 10/28/2023 Tdchlorofluoromethane sw US Method SM00/303M <0.5 pg/L 10/26/2023 Vinyl chloride SW 8" McOwd 8200DW3M <0.5 pg/L 10/26/2023 Comment_ t Reviewed by: Repent C 2023-24498 — - - - Peke 9 019 Environmental Chemist, Inc., Wilmington, NC Lab #94 6602 Windmill Way Wilmington, NC 28405 Sample Receipt Checklist 910.392.0223 Client: IM Date: Q Report Number:_ 2023- ay q8 Receipt of sample: O YES ❑ NO ECHEM Pickup Client Delivery ❑ UPS ❑ FedEx ❑ Other ❑ ® N/A 1. ❑ Were custody seals present on the cooler? YES Original temperature ❑ NO upon ®N/A 2. If custody seals were present, were they intact/unbroken7 receipt *C Corrected temperature upon receipt C How temperature taken: ❑ Temperature Blank ® Against Bottles IR Gun ID: Thomas Traceable S/N 210886869 IR Gun Correction Factor *C: 0.0 © YES 0 ❑ NO 3. If temperature of cooler exceeded 6*C, was Project Mgr./QA notified? YES © ❑ NO 4. Were proper custody procedures (relinquished/received) followed? YES ❑ NO 5. Were sample ID's listed on the COC? ® YES ❑ NO 6. Were samples ID's listed on sample containers? ® YES ❑ NO 7. Were collection date and time listed on the COC? ® YES ❑ NO B. Were tests to be performed listed on the COC? ® YES ❑ NO 9. Did samples arrive in proper containers for each test? © YES ❑ NO 10. Did samples arrive in good condition for each test? © YES ❑ NO 11. Was adequate sample volume available?' ® YES ❑ NO 12. Were samples received within proper holding time for requested tests? ❑ YES ❑ NO 13. Were acid preserved samples received at a pH of <2? • ❑ YES ❑ NO 14. Were cyanide samples received at a pH >12? ❑ YES ❑ENO O 15. Were sulfide samples received at a pH >9? ❑ YES ❑ ❑O 16. Were NH3/TKN/Phenol received at a chlorine residual of <0.5 m/L) ** YES ❑ 13 17. Were Sulfide/Cyanide received at a chlorine residual of <0.5 m/L? YES 113 NO 18. Were orthophosphate samples filtered in the field within 15 minutes? * TOC/Volatiles are pH checked at time of analysis and recorded on the benchsheet. *' Bacteria samples are checked for Chlorine at time of analysis and recorded on the benchsheet Sample Preservation: (Must be completed for any sample(s) incorrectly preserved or with headspace) Sample(s) were received incorrectly preserved and were adjusted accordingly by adding (circle one): H2SO4 HNO3 HCI NaOH Time of preservation: If more than one preservative is needed, notate in comments below Note: Notify customer service immediately for incorrectly preserved samples. Obtain a new sample or notify the state lab if directed to analyzed by the customer. who was notified. date and time. olatiles Samples) COMMENTS: were received with DOC. QA.002 Rev 1 N r iF �71 �ii N a 3 N N � W O C _ = O oz x 3 Type c•4• or P C Co I* r jPorGj N G, N W Chkua I M91L •�� LAO ID � NUMBER NOW NCB -v �e K X #am � Nu MACH O Tf10 z OT M w � � c m z 0 z z m z n r g m c FA V zA � I EPA BIOSOLIDS REPORT ID# NCL003186 Enclosure (2) NPDES & UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Form Approved. FORM WASHINGTON, DC 20460 OMB No. 2040-0004. 6100.035 BIOSOLIDS ANNUAL REPORT Exp. 07/31/2026 EPA's sewage sludge regulations require certain publicly owned treatment works (POTWs) and Class I sewage sludge management facilities to submit to a Sewage Sludge (Biosolids) Annual Report (see 40 CFR 503.18 (https:/Avww.ecfr.gov/cgi-binitext-idx? node=pt40.32.503&rgn=div5#se40.32.503_118), 503.28 (https://www.ecfr.gov/cgi-bin/text-idx?node=pt40.32.503&rgn=div5#se40.32.503_128), 503.48 (https://www.ecfr.govtcgi-bin/text-idx?node=pt40.32.503&rgn=div5#se40.32.503_148)). Facilities that must submit a Sewage Sludge (Biosolids) Annual Report include POTWs with a design flow rate equal to or greater than one million gallons per day, POTWs that serve 10,000 people or more, Class I Sludge Management Facilities (as defined by 40 CFR 503.9 (https://www.eefr.gov/cgi-bin/text-idx? node=pt40.32.503&rgn=div5#se40.32.503_19)), and facilities otherwise required to file this report (e.g., permit condition, enforcement action, state law). This is the electronic form for Sewage Sludge (Biosolids) Annual Report filers to use if they are located in one of the states, tribes, or territories (https://www.epa.gov/npdes/npdes-state-program-information) where EPA administers the Federal biosolids program. For the purposes of this form, the term 'sewage sludge (httpsJ/www.ecfr.gov/ogi-bin/text-idx?node=pt40.32.503&rgn=div5#se40.32.503_19)' also refers to the material that is commonly referred to as 'biosolids'. EPA does not have a regulatory definition for biosolids but this material is commonly referred to as sewage sludge that is placed on, or applied to the land to use the beneficial properties of the material as a soil amendment, conditioner, or fertilizer. EPA's use of the term'biosolids' in this forth is to confirm that information about beneficially used sewage sludge (a.k.a. biosolids) should be reported on this forth. Public Availability of Information Submitted on and with this Program Report EPA may make all the information submitted through this form (including all attachments) available to the public without further notice to you. Do not use this online form to submit personal information (e.g., non -business cell phone number or non -business email address), confidential business information (CBI), or if you intend to assert a CBI claim on any of the submitted information. Pursuant to 40 CFR 2.203(a), EPA is providing you with notice that all CBI claims must be asserted at the time of submission. EPA cannot accommodate a late CBI claim to cover previously submitted information because efforts to protect the information are not administratively practicable since it may already be disclosed to the public. Although we do not foresee a need for persons to assert a claim of CBI based on the types of information requested in this form, if persons wish to assert a CBI claim we direct submitters to contact the NPDES eReporting Help Desk (NPDESeReporting@epa.gov (mailto:NPDESereporting@epa.gov)) for further guidance. Please note that EPA may contact you after you submit this report for more information regarding your sewage sludge management program. Burden Statement This collection of information is approved by OMB under the Paperwork Reduction Act, 44 U.S.C. 3501 et seq. (OMB Control No. 2040-0004). Responses to this collection of information are mandatory in accordance with EPA NPDES regulations (40 CFR 503.18, 503.28, and 503.48). An agency may not conduct or sponsor, and a person is not required to respond to, a collection of information unless it displays a currently valid OMB control number. The public reporting and recordkeeping burden for this collection of information are estimated to average one to five hours per response. Send comments on the Agency's need for this information, the accuracy of the provided burden estimates and any suggested methods for minimizing respondent burden to the Regulatory Support Division Director, U.S. Environmental Protection Agency (2821T), 1200 Pennsylvania Ave., NW, Washington, D.C. 20460. Include the OMB control number In any correspondence. Do not send the completed form to this address. Facility Information Facility Name: US MCAS CHERRY POINT NPDES ID: NCL003816 Program Information Please select all of the following that apply to your obligation to submit a Sewage Sludge (Blosollds) Annual Report in compliance with 40 CFR part 503. The facility is: • a POTW that serves 10,000 people or more In the reporting period, did you manage your sewage sludge or biosolids using any of the following management practices: land application, surface disposal, or Incineration? & YES O NO If your facility Is a POTW, please provide the estimated total amount of sewage sludge produced at your facility for the reporting period (in dry metric tons). If your facility is not a POTW, please provide the estimated total amount of biosolids produced at your facility for the reporting period (in dry metric tons). 105.95 Reporting Period Start Date:01/0112023 Reporting Period End Date:12/31/2023 Treatment Processes Processes to Significantly Reduce Pathogens (PSRP): Lime Stabilization Page 1 of 6 Processes to Further Reduce Pathogens (PFRP): Physical Treatment Options: Thickening (e.g., Gravity and/or Flotation Thickening, Centrifugation, Belt Filter Press, Vacuum Fitter, Screw press) Other Processes to Manage Sewage Sludge: Analytical Methods Did you or your facility collect sewage sludge or biosolids samples for laboratory analysis? L' YES ONO Analytical Methods • Standard Method 4500-N - Nitrogen • Standard Method 4500-NH3 - Ammonia Nitrogen • Standard Method 2540 - Total Solids • EPA Method 9040 - pH (— 7% solids) Other Analytical Methods • Other Total Kjeldahl Nitrogen Analytical Method Other Analytical Methods Text Area: SM 4500 Norg B-2011 • Other Metals Analytical Method Other Analytical Methods Text Area: 200_.7 . Other TCLP Analytical Method Other Analytical Methods Text Area: 200.7 846 Method 8260D . Other Mercury Analytical Method Other Analytical Methods Text Area: 846 7471 B . Other Copper Analytical Method Other Analytical Methods Text Area: 200.7 . Other Molybdenum Analytical Method Other Analytical Methods Text Area: 200.7 • Other Nickel Analytical Method Other Analytical Methods Text Area: zoo.7 • Other Zinc Analytical Method Other Analytical Methods Text Area: 200.7 • Other Nitrate Nitrogen Analytical Method Other Analytical Methods Text Area: 353.2 Sludge Management - Land Application ID: 001 Page 2 of 6 Amount: 84.2 Handler, Preparer, or Applier Type: On -Site Owner or Operator Management Practice Detail: Other Other Management Practice Detail Description: Land Application of Class B Residuals Bulk or Bag/Container: Bulk Pathogen Class: Class B Sewage Sludge or Biosolids Pathogen Reduction Options: " Class B-Altemative 2 PSRP 5: Lime Stabilization Sewage Sludge or Biosolids Vector Attraction Reduction Options: " Option 6 -Alkaline Treatment Did the facility land apply bulk sewage sludge when one or more pollutants In the sewage sludge exceeded 90 percent or more of any of the cumulative pollutant loading rates in Table 2 of 40 CFR 503.13? OYES & NO O UNKNOWN Monitoring Data INSTRUCTIONS: Pollutants, pathogen densities, and vector attraction reduction must be monitored when sewage sludge or biosolids are applied to the land. Please use the following section to report monitoring data for the land application conducted by you or your facility in the reporting period for this SSUID. These monitoring data should be representative of the sewage sludge or biosolids that was applied to land during the compliance monitoring period for this SSUID (40 CFR 503.8(a) (http:/Avww.ecfr.gov/cgi-bin/text-idx? node=pt4D.32.503&rgn=div5#se40.32.503_18)). All pollutant monitoring data should be reported In milligrams per kilogram (mg/kg), dry weight basis. EPA will be using these data to demonstrate compliance with EPA's land application requirements (40 CFR 503, Subpart B). Compliance Monitoring Periods INSTRUCTIONS: Please use the table below to identify the start date and end date for each compliance monitoring period. You can adjust the start and end dates as needed. Please note that the compliance monitoring periods cannot overlap and that each compliance monitoring period must have a start date that is equal to or less than the end date. The number of compliance monitoring periods is based on the number of metric tons (dry weight basis) of sewage sludge or biosolids land applied in the reporting period (summed across all land application SSUIDs). For example, you will need to provide monitoring data for 12 compliance monitoring periods for each land application SSUID when you land apply 15,000 or more metric tons (dry weight basis) of sewage sludge or biosolids (summed across all land application SSUIDs) in the reporting period (see 40 CFR 503.16(http://www.ecfr.gov/cgi-bin/text-idx? node=pt4D.32.503&rgn=div5#se40.32.503_116)). Compliance Monitoring Event No. 1 Compliance Monitoring Period Start Compliance Monitoring Period End Date: Date: 12/31/2023 01/01/2023 Do you have analytical results to report for this monitoring period? B YES O NO Are you reporting maximum pollutant concentrations that are equivalent to the monthly average pollutant concentrations for this compliance monitoring event? [For example, this will be the case If you only collected and analyzed one sample of sewage sludge or blosolids for this compliance monitoring period.] G YES O NO Maximum Concentration Data for All Sewage Sludge or Biosolids Applied to Land This section summarizes the maximum pollutant concentrations In the biosolids or sewage sludge that was applied to land during the compliance monitoring period for this SSUID. In accordance with 40 CFR 503.13(a) (http:/Avww.ecrr.gov/cgi-binftext-idx? node=pt40.32.503&rgn=div5#se40.32.503_113). EPA's regulations prohibit land application of bulk sewage sludge or sewage sludge sold or gave away sewage sludge in a bag or other container when one or more sewage sludge pollutant concentrations in the sewage sludge exceed a land application ceiling pollutant limit (Table 1 of 40 CFR 503.13 (httpJ/www.ecfr.gov/cgi-bin/text-idx? node=pt40.32.503&rgn=div5#se40.32.503_113)). EPA will compare the pollutant concentrations in this section against the ceiling concentration limits in Table 1 of 40 CFR 503.13 (hftp://www.ecfr.gov/cgi-bin/text-idx?node=pt4O.32.503&rgn=div5#se4O.32.503_113) to identify noncompliance events. All pollutant monitoring data should be reported in milligrams per kilogram (mg/kg), dry weight basis. Please only select a "No Data Indicator Code" if you are reporting no data for the sampling period or particular parameter. Sewage Sludge or Biosolids Value Parameter Concentration (mg/kg, dry -weight If No Data, Select One Of The Parameter Qualifier basis or Pass/Fall) Following Arsenic = 49.7 Cadmium = 49.7 Copper = 449 Page 3 of 6 Sewage Sludge or Blosolids Value Parameter Concentration (mglkg, dry -weight If No Data, Select One Of The Parameter Qualifier basis or Pass/Fall) Following Lead = 49.7 Mercury = 1.03 Molybdenum = 49.7 Nickel = 49.7 Selenium = 49.7 Zinc = 754 Monthly Average Pollutant Concentration Data for All Sewage Sludge or Blosolids Applied to Land This section summarizes the monthly average pollutant concentrations in the biosolids or sewage sludge that was applied to land during the compliance monitoring period for this SSUID. All pollutant monitoring data should be reported in milligrams per kilogram (mglkg), dry weight basis. Sewage Sludge or Biosolids Value Parameter Concentration (mglkg, dry -weight If No Data, Select One Of The Parameter Qualifier basis or Pass/Fail) Following Arsenic = 49.7 Cadmium = 49.7 Copper = 449 Lead = 49.7 Mercury = 1.03 Nickel = 49.7 Selenium = 49.7 Zinc = 754 Report the average concentration (mg/kg, dry weight basis) of Total Nitrogen (TKN plus Nitrate -Nitrite, as N) in the sewage sludge or biosolids that was applied to land during the compliance monitoring period for this SSUID. Sewage Sludge or Blosolids Value Parameter Concentration (mglkg, dry- If No Data, Select One Of The Parameter Qualifier weight basis) Following Total Nitrogen (TKN plus Nitrate- = 44200 Nitrite) ID: 002 Amount: 21.7 Handler, Preparer, or Applier Type: On -Site Owner or Operator Management Practice Detail: Other Other Management Practice Detail Description: Land Application of Class B Residuals Bulk or Bag/Container: Bulk Pathogen Class: Class B Sewage Sludge or Blosolids Pathogen Reduction Options: Class B-Altemative 2 PSRP 5: Lime Stabilization Sewage Sludge or Blosolids Vector Attraction Reduction Options: Option 6 -Alkaline Treatment Did the facility land apply bulk sewage sludge when one or more pollutants in the sewage sludge exceeded 90 percent or more of any of the cumulative pollutant loading rates In Table 2 of 40 CFR 503.13? O YES 1 NO O UNKNOWN Monitoring Data Page 4 of 6 Compliance Monitoring Periods INSTRUCTIONS: Pollutants, pathogen densities, and vector attraction reduction must be monitored when sewage sludge or biosolids are applied to the land. Please use the following section to report monitoring data for the land application conducted by you or your facility in the reporting period for this SSUID. These monitoring data should be representative of the sewage sludge or biosolids that was applied to land during the compliance monitoring period for this SSUID (40 CFR 503.8(a) (http:/AwAv.ecfr.gov/cgi-bin/text-idx? node=pt40.32.503&rgn=div5#se40.32.503_18)). All pollutant monitoring data should be reported in milligrams per kilogram (mg/kg), dry weight basis. EPA will be using these data to demonstrate compliance with EPA's land application requirements (40 CFR 503, Subpart B). INSTRUCTIONS: Please use the table below to identify the start date and end date for each compliance monitoring period. You can adjust the start and end dates as needed. Please note that the compliance monitoring periods cannot overlap and that each compliance monitoring period must have a start date that is equal to or less than the end date. The number of compliance monitoring periods is based on the number of metric tons (dry weight basis) of sewage sludge or biosolids land applied in the reporting period (summed across all land application SSUIDs). For example, you will need to provide monitoring data for 12 compliance monitoring periods for each land application SSUID when you land apply 15,000 or more metric tons (dry weight basis) of sewage sludge or biosolids (summed across all land application SSUIDs) in the reporting period (see 40 CFR 503.16 (http:/Avww.ecfr.gov/cgi-binftext-idx? node=pt40.32.503&rgn=div5#se40.32.503_116)). Compliance Monitoring Event No. 1 Compliance Monitoring Period Start Compliance Monitoring Period End Date: Date: 12/31/2023 01 /01/2023 Do you have analytical results to report for this monitoring period? E YES O NO Are you reporting maximum pollutant concentrations that are equivalent to the monthly average pollutant concentrations for this compliance monitoring event? [For example, this will be the case if you only collected and analyzed one sample of sewage sludge or biosolids for this compliance monitoring period.] G YES O NO Maximum Concentration Data for All Sewage Sludge or Blosollds Applied to Land This section summarizes the maximum pollutant concentrations in the biosolids or sewage sludge that was applied to land during the compliance monitoring period for this SSUID. In accordance with 40 CFR 503.13(a) (http://www.ecfr.gov/cgi-bin/text-idx? node=pt40.32.503&rgn=div5#se40.32.503_113), EPA's regulations prohibit land application of bulk sewage sludge or sewage sludge sold or gave away sewage sludge in a bag or other container when one or more sewage sludge pollutant concentrations in the sewage sludge exceed a land application ceiling pollutant limit (Table 1 of 40 CFR 503.13 (httpJAvww.ecfr.gov/cgi-bin/text-idx? node=pt40.32.503&rgn=div5#se40.32.503_113)). EPA will compare the pollutant concentrations in this section against the ceiling concentration limits in Table 1 of 40 CFR 503.13 (http://www.ecfr.gov/cgi-binttext4dx?node=pt4O.32.503&rgn=div5#se4O.32.503_113) to identify noncompliance events. All pollutant monitoring data should be reported in milligrams per kilogram (mg/kg), dry weight basis. Please only select a "No Data Indicator Code" if you are reporting no data for the sampling period or particular parameter. Sewage Sludge or Blosollds Value Parameter Concentration (mg/kg, dry -weight If No Data, Select One Of The Parameter Qualifier basis or Pass/Fail) Following Arsenic = 49.7 Cadmium = 49.7 Copper = 449 Lead = 49.7 Mercury = 1.03 Molybdenum = 49.7 Nickel = 49.7 Selenium = 49.7 Zinc = 754 Monthly Average Pollutant Concentration Data for All Sewage Sludge or Blosollds Applied to Land This section summarizes the monthly average pollutant concentrations in the biosolids or sewage sludge that was applied to land during the compliance monitoring period for this SSUID. All pollutant monitoring data should be reported in milligrams per kilogram (mg/kg), dry weight basis. Sewage Sludge or Biosolids Value Parameter Concentration (mg/kg, dry -weight If No Data, Select One Of The Parameter Qualifier basis or Pass/Fail) Following Arsenic = 49.7 Cadmium = 49.7 Copper = 449 Lead = 49.7 Mercury = 1.03 Page 5 of 6 Sewage Sludge or Blosolids Value Parameter Concentration (mg/kg, dry -weight If No Data, Select One Of The Parameter Qualifier basis or Pass/Fail) Following Nickel = 49.7 Selenium = 49.7 Zinc = 754 Report the average concentration (mg/kg, dry weight basis) of Total Nitrogen (TKN plus Nitrate -Nitrite, as N) in the sewage sludge or biosolids that was applied to land during the compliance monitoring period for this SSUID. Sewage Sludge or Blosolids Value Parameter Concentration (mg/kg, dry- If No Data, Select One Of The Parameter Qualifier weight basis) Following Total Nitrogen (TKN plus Nitrate- = 44200 Nitrite) Sludge Management - Surface Disposal Sludge Management - Incineration Sludge Management - Other Management Practice Additional Information Please enter any additional information that you would like to provide in the comment box below. The attached files are the completed annual sludge report for CY2023 for permit WQ0001489 to be provided to NCDEQ. Additional Attachments Name 2023 Annual Sludge report 3.pdf 2023 Annual Sludge report 4.pdf 2023 Annual Sludge report 1.pdf 2023 Annual Sludge report 2.pdf Certification Information Created Date 01 /22/2024 4:21 PM 01 /22/2024 4:21 PM 01/22/2024 4:21 PM 01 /22/2024 4:21 PM Size 1.19 MB 2.43 MB 1.13 MB 1018.97 KB I certify under penalty of law that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the Information, the Information submitted Is, to the best of my knowledge and belief, true, accurate, and complete. I have no personal knowledge that the information submitted is other than true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fine and Imprisonment for knowing violations. Signing an electronic document on behalf of another person is subject to criminal, civil, administrative, or other lawful action. Certified By: Dale A. McFarland (MCFARLANDMCASCHERRYPOINT) Certified On: 01/30/2024 8:20 AM ET Page 6 of 6