DRAFT PHASE II Hickory NE Flood Mitigation Measures Waste Characterization (1)

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G ro u p by Nova Group
WASTE CHARACTERIZATION REPORT
HICKORY NE WWTP FLOOD MITIGATION
MEASURES SITE CHARACTERIZATION
310 CLONINGER MILL ROAD
HICKORY, NORTH CAROLINA
REPORT DATE: NOVEMBER 7, 2022
NOVA PROJECT NO. J22-8073
PREPARED FOR
KCI ASSOICATES OF NC
4505 FALLS OF NUESE ROAD
RALEIGH, NORTH CAROLINA 27604
PREPARED BY
NOVA GROUP, GBC
5320 West 23rd STREET, SUITE 270
ST. LOUIS PARK, MN 55416
L-1

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7A* Group
TABLE OF CONTENTS
1.0 INTRODUCTION.......................................................................................................... 1
1.1 Authorization......................................................................................................................1
1.2 Background.........................................................................................................................1
1.3 Objective.............................................................................................................................1
1.4 Scope of Services................................................................................................................1
2.0 METHODS AND PROCEDURES..................................................................................... 3
2.1 Geophysical Survey.............................................................. Error! Bookmark not defined.
2.2 Soil Boring Sampling Locations...........................................................................................3
2.3 Soil Boring Advancement Procedures.................................................................................3
2.4 Field Screening....................................................................................................................3
2.5 Laboratory Chemical Analyses............................................................................................4
3.0 RESULTS.............:AW....:.........................................................................................5
3.1 Geology and Site Conditions...............................................................................................5
3.2 Field Screening....................................................................................................................5
3.3 Chemical Analyses...............................................................................................................5
4.0 CUNLLUSIUNS ANu RELUmMENDATIONS.................................................................. 8
5.0 STANDARD OF CARE .... W................................................................................ 9
FIGURES
1. Site Location Map
2. Topographic Map
3. Site Plan
4. Sample Location Map
T
1. Summary of Soil Sample Analytical Results Metals
2. Summary of Soil Sample Analytical Results Organics and Cyanide
/_1]:"L10110 V
A. Photographic Documentation
B. Soil Boring Logs
C. Laboratory Chemical Analysis Report
WASTE CHARACTERIZATION i 310 CLONINGER MILL ROAD, HICKORY, NC
HICKORY NE WWTP FLOOD MITIGATION MEASURES SITE PROJECT NO. J22-8073

AWS N ova
7A* Group
1.0 INTRODUCTION
Authorization
In accordance with the written authorization received from KCl Associates of NC (KCI), Nova
Group, GBC (Nova) has conducted a Site Characterization at the property located near 310
Cloninger Mill Road NE, Hickory, NC ("the Site"). A Site Location Map (Figure 1), Topographic
Map and Basin Location Map (Figure 2), and Sample Location Map (Figure 3) are attached as
Figure 1, Figure 2, and Figure 3, respectively.
Background
The Site is within an irregular -shaped parcel and consists of a portion of a larger 45.83-acre
tract owned by the City of Hickory. The Site, for the purposes of this report, is a portion of
land south of the Hickory NE waste -water treatment plant (WWTP) and is bordered to the
north by Falling Creek (and the Hickory NE WWTP beyond), to the south by undeveloped
land, to the east by Cloninger Mill Road NE and undeveloped land, and west by undeveloped
land (Figure 1).
Available historical information indicates the Site was utilized as WWTP sludge
drying/dewatering beds for the adjacent WWTP. Available information provided indicated
the period of operation was generally from the 1970's and 1980's, although the precise date
of use is not documented. The Site was excavated and graded to configure four (4) sludge
drying basins along the south side of Falling Creek south of the Hickory NE WWTP. For the
purposes of this report the basins will be identified as Basin 1 through 4, in an east to west
orientation. The basins were apparently excavated in native soil which appears to have been
used as earthen berms for the basins. The locations of each basin are shown on Figure 2,
basins are numbered east to west (Basinl through 4).
Currently, the Site is currently undeveloped, and has overgrown since being taken out of
service.
Objective
The objective of this waste characterization was to conduct a preliminary sampling for
sludge, focusing on the presence or absence of noticeable remaining WWTP sludge
preliminary site characteristics, and the collection of samples of WWTP sludges. Chemical
analysis is for waste characterization in preparation for implementation of the Hickory NE
WWTP Flood Mitigation Measures Plan, prepared by KCI, and proposed for this location,
which will require the excavation of the former settling basin areas
Scope of Services
As part of this study, Nova completed the following scope of services:
WASTE CHARACTERIZATION 1 310 CLONINGER MILL ROAD, HICKORY, NC
HICKORY NE WWTP FLOOD MITIGATION MEASURES SITE PROJECT NO. J22-8073

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- Cleared public underground utilities through the State one call system (NC One Call 811)
prior to initiating any subsurface investigation activities;
- Advanced 10 soil borings (GP-1 through GP-8, HA-1, and HA-2) using a direct push drill
rig and hand augers to depths of up to 15 feet below ground surface (bgs), or refusal.
Field screened soil samples collected from the soil borings for organic vapors at
continuous intervals with a photoionization detector (PID), as well as recorded a detailed
description of subsurface lithology and documented any indications of unusual odors or
staining;
- Collected and submitted one (1) soil sample from each of the ten (10) soil sampling
locations for OP Pesticides using United States Environmental Protection Agency
(USEPA) Method 814113, GSC Pesticides using USEPA Method 808113, GCS PCBs using
USEPA Method 8082A, tin using USEPA Method 6010, metals using USEPA Methods
6020/7471, Semi -Volatile Organic Compounds (SVOCs) using USEPA 8270E-MSSV,
Flashpoint using USEPA 101013, pH using USEPA Method SM90451), Sulfide soil using
Method 4500-S2D-2011, and total cyanide using USEPA Method 9012;
- Additionally, four (4) locations were selected (one in each basin) and laboratory analyzed
for volatile organic compounds (VOCs) using United States Environmental Protection
Agency (USEPA) Method SW 8260D;
- Analysis of four (4) composite samples (one (1) from each basin) for metals by the
Toxicity Characteristic Leachate Procedure (TCLP) using USEPA Methods 6010D/7470A
with TCLP extraction Method 3010A, and speciation of chromium (Cr+3 - trivalent, and
Cr+6 - hexavalent) using USEPA Method 7196A; and
Prepared this report detailing the investigation methods and procedures, summarizing
the field and analytical results to date, and providing appropriate conclusions and
recommendations.
WASTE CHARACTERIZATION 2 310 CLONINGER MILL ROAD, HICKORY, NC
HICKORY NE WWTP FLOOD MITIGATION MEASURES SITE PROJECT NO. J22-8073

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7A* Group
2.0 METHODS AND PROCEDURES
Soil Boring Sampling Locations
On August 16, 2022, land clearing was conducted by City of Hickory personnel to provide
access to the suspected sludge basins, which were identifiable in the field based on elevation
changes and the presence of man-made earthen berms around each basin area. Upon
completion of limited land clearing activities soil borings (GP-1-1 through GP-7) were
advanced by JG Drilling at the Site using a direct push drill rig. Due to physical constraints,
Basin 1 and Basin 2 were sampled using a hand auger, and an additional surficial sample was
collected from Basin 3 using hand equipment due to the absence of soil cover at this location.
A map depicting the soil boring locations is included as Figure 3 Photographs showing the
general sampling locations are included in Appendix A.
Soil goring Advancement Procedures
Soil borings GP-1 through GP-7 were completed using a track -mounted Geoprobe° drill rig.
A Geoprobe° Macro -Core sampler was used to collect the soil samples from the borings at
continuous five-foot intervals to depths to feet bgs. The Macro -Core sampler consists of a
2.25-inch outside diameter, nickel -plated alloy -steel sampling tube with an inserted
polyvinyl chloride (PVC) liner that is continuously filled with soil as it is pushed and/or
hammered to a depth of drilling refusal. The liners were removed from the sampler after
each sampling interval and a new liner was inserted into the sampler for the next sampling
interval.
Soil samples from each boring were typically selected for submittal to the laboratory for
chemical analysis from the depth interval exhibiting the highest PID reading or other field
indicators of contamination. If the field screening did not identify any evidence of
contamination, the soil samples were collected where there was a change in lithology. Soil
samples chosen for laboratory analyses were placed into clean, laboratory -supplied glass
sample jars, labeled, and placed on wet ice in a cooler.
Field Screening
An environmental scientist recorded a physical description of the soils encountered at each
boring location on a field -boring log. Visual classification of soil was generally based on
American Society of Testing and Materials (ASTM) Methods 2487 and 2488, Soil
Conservation Service, and American standards. The soil sample descriptions generally
included type, color, grain size, texture, and moisture. The descriptions were recorded on
the soil boring logs included in Appendix B.
In addition to recording the physical description of the soils encountered at each boring
location on a field -boring log, the on -site environmental scientist screened the soil samples
for indications of environmental impacts. Each of the soil samples retrieved from the
borehole was screened for organic vapors using a PID. The PID was equipped with a 11.7 eV
WASTE CHARACTERIZATION 3 310 CLONINGER MILL ROAD, HICKORY, NC
HICKORY NE WWTP FLOOD MITIGATION MEASURES SITE PROJECT NO. J22-8073

AWS N ova
7 jh* Group
lamp and was calibrated to an isobutylene standard prior to being used at the Site. Physical
evidence of any unusual odors or staining was also recorded on the sol boring log (as no
indications of the presence of VOCs were detected in the field screening, this data was not
included on the soil boring logs).
Laboratory Chemical Analyses
A total of ten (10) soil samples were collected from soil boring locations GP-1 through GP-7,
HA-1, HA-2 and SB-3 (Surface Basin 3). The soil samples collected were laboratory analyzed
for OP Pesticides using USEPA Method 8141B, GSC Pesticides using USEPA Method 8081B,
GCS PCBs using USEPA Method 8082A, tin using USEPA Method 6010, metals using USEPA
Methods 6020/7471, Semi -Volatile Organic Compounds (SVOCs) using USEPA 8270E-MSSV,
Flashpoint using USEPA 1010B, pH using USEPA Method SM90451), Sulfide soil using Method
4500-S2D-2011, and total cyanide using USEPA Method 9012. The soil samples collected
from the four (4) basins were additionally analyzed for volatile organic compounds (VOCs)
using (USEPA) Method SW 8260D.
Additionally, four (4) composite samples (one (1) from each basin) were analyzed for metals
by the Toxicity Characteristic Leachate Procedure (TCLP) using USEPA Methods
6010D/7470A with TCLP extraction Method 3010A, and speciation of chromium (Cr+3 -
trivalent, and Cr+6 - hexavalent) using USEPA Method 7196A.
The collected samples were placed in laboratory -supplied containers, stored in a cooler with
wet ice, and transported to Pace in Raleigh, NC. Pace is certified to analyze environmental
samples collected in the State of North Carolain. A copy of the completed analytical report in
included as Appendix D.
WASTE CHARACTERIZATION 4 310 CLONINGER MILL ROAD, HICKORY, NC
HICKORY NE WWTP FLOOD MITIGATION MEASURES SITE PROJECT NO. J22-8073

AWS N ova
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3.0 RESULTS
Geology and Site Conditions
Conditions within each basin encountered at the Site consisted of an uncompacted soil cover
on Basinl, Basin 2, and Basin 4. Basin 3 did not appear to have a soil cover. Cover material
at Basin 3 appeared to consist of native soils which were clayey sandy silts. In Basins 1, 2 and
4 a layer of dark gray/black material was visually identified as WWTP sludge at
approximately 2 to 3 feet bgs.
Basin 3 did not have a soil cover, and the depth of the suspected sludge material extended
from ground surface to a depth of approximately 3 feet bgs. Basins 1 and 2 are smaller in
aerial extent than Basins 3 and 4. Basins 1 and 2 appeared to have been clay lined at about
3.5 feet bgs. Basins 3 and 4 appeared to have native soils beneath the sludge layer. These
soils appeared to be tan/yellow brown in color and were mostly clayey, sandy silts.
Refusal was encountered at a depth of approximately 10 feet bgs in partially weathered rock.
Groundwater was encountered at a relatively shallow depth of 5 to 7 feet bgs. Considering
the basins are located abutting Falling Creek, it is assumed that groundwater flow and
discharge would be to the north where the rock was observed to be cropping out along the
creek bed.
Soil boring logs with descriptions of the encountered materials are contained in Appendix
C.
Field Screening
Field screening of the soil samples collected from the soil borings did not detect significant
organic vapors when screened with a PID. The complete organic vapor screening results are
not included on the soil boring logs, as no field indications of the presence of VOCs were
detected. The soil boring logs are attached in Appendix C.
Chemical Analyses
Nova compared the detected contaminants to the North Carolina Department of
Environmental Quality (NCDEQ) Preliminary Soil Remediation Goals (PSRGs) dated January
2021.
Metals were detected above the laboratory RLs in all soil samples as shown in the following
table:
WASTE CHARACTERIZATION 5 310 CLONINGER MILL ROAD, HICKORY, NC
HICKORY NE WWTP FLOOD MITIGATION MEASURES SITE PROJECT NO. J22-8073

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FALLING CREEK SLUDGE CHARACTERIZATION
TABLE 1 - METALS
Sample ID
Units
Barium
Be Ilium
CadmiumChromiu
Cobalt
Copper
Lead
Nickel
Seleniu
Silver
Vanadiu
Zinc
Mercur
GP-1 2-3'
m Ik
129
5.6
757
065
6.8
612
62
252
193
18
7.2
527
41.3
353
4.2
GP-22-3'
mglkg
317
7.6
1760
051
11
182C
63
553
394
18.2
72
128
42
184
13.7GP32-3'
m /k
rinAntimonyArsenic
339
4.9
1770
032
11
1940
5,2
558
388
13.9
5.7
130
33.9
174
14
GP-4 2-3'
m /k
210
3.4
1310
NA*
61
296D
55 5
405
2510
76
73
159
279
143
9
GP-5 2-3'
m 1k
106
59
1780
038
132
152D
373
787
6150
61
81
175
31.1
6660
96
GP-62-3'
m !k
255
7.2
1640
0,38
15
2240
11,4
687
3860
14.5
8.1
165
34.8
449
6.7
GP-7 2-3'
mqikq
214
429
5.7
2600
055
303
2850
94
652
903
137
6 3
260
44.7
207
182
HA-12-3'
mglkg
127
244
5.1
1620
0,26
8.1
3120
7,1
403
359c
9.2
7.9
175
32
180
6.7
HA-2 2-3'
m Ik
189
258
8.6
1710
0.75
9.1
3160
10.5
500
2870
21.7
8
163
53.4
177
12.5
SB-3
m lk
101
176
NA*
820
NA*
4.3
1090
NA`
185
269
5.8
3.9
106
17.9
NA`
5.7
NO PSRGs
mg/kg
NL
63
0 68
3100
31
14
23000
47
NL
270
0.76
78
78
78
NL
1
The data show that generally the sludge has elevated metals concentrations in particular
interest area the metals lead, chromium, mercury and detectable levels of the other metals
(except thallium) at concentrations above typically expected background concentrations in
native soils, but below regulatory limits. While other metals were detected at levels
considered above background, lead, chromium and mercury appear to be the most
problematic due to the potential to extract above the regulatory limit as determined by the
RCRA Toxicity Characteristic Leachate Procedure (TCLP). Table 1 also includes the
Preliminary Soil Remediation Goals (PSRGs) for the associated constituent. Due to the
naturally occurring levels of chromium the PSRG is relatively high, but it should be noted
that the chromium present in the sludge is not naturally occurring as it is within a solid
waste. Speciation is necessary to determine the character of the chromium if it is in its
trivalent state (Cr+3), or if it is present in its hexavalent state (Cr+6). The associated PSRG for
hexavalent chromium is 0.31 mg/kg.
Concentrations of lead and chromium that extract under the TCLP are considered to be
hazardous by toxicity characteristic at a concentration of 5 mg/L for both lead (D008) and
chromium (D007). A typical rule of thumb is that when total concentrations in soil exceed
the TCLP by a factor of 20, the material is likely to fail the TCLP. To assess this potential the
remaining soils retained by the laboratory were therefore composited for each basin and
analyzed for TCLP Metals.
TCLP results are as follows:
TCLP FALLING CREEK BASINS 1 - BASIN 4
Location
As
m L
Ba
m L
Cd
m L
Cr
m L
Pb
m L
Se
m L
Ag
m L
Hg
u L
Il
m L
Basin 1
ND
ND
ND
ND
ND
ND
ND
ND
ND
Basin 2
ND
ND
ND
0.58
0.87
ND
ND
1.4
ND
Basin 3
ND
3.5
0.052
1.5
13.5
ND
0.27
10.6
ND
Basin 4
ND
ND
ND
ND
ND
ND
ND
ND
ND
WASTE CHARACTERIZATION 6 310 CLONINGER MILL ROAD, HICKORY, NC
HICKORY NE WWTP FLOOD MITIGATION MEASURES SITE PROJECT NO. J22-8073

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The results of the TCLP analysis show that only Basin 3 has an exceedance of the TCLP
regulatory concentration for lead (Ph) of 13.5 milligrams per liter (mg/L). The Resource
Conservation Recovery Act (RCRA) limit for lead is 5.0 mg/L. This data shows that while
there are elevated total metal concentrations in all of the samples, only Basin 3 exceeds the
regulatory limit for lead, characterizing the sludge as a RCRA hazardous waste.
Soil Sample laboratory analytical results, show low concentrations of several VOCs (toluene,
styrene, and carbon tetrachloride), low concentrations of pesticides (DDT, DDE, Dieldrin,
Endrin, ), PCB 1245, and Bis-2 ethylhexelphthalate detected above the laboratory reporting
limits (RLs) in the soil samples collected. Table 2 summarizes the results of the analysis:
FALLING CREEK SLUDGE CHARACTERIZATION
TABLE 2 ORGANICS AND CYANIDE
Sample ID lunits IChlordane 4,4"-DDE 4,4"-DDT IDieldrin lEndrin I PCB-12541 Carbon I Styrene IToluene bis 2-Eth the I C anide
aldehyde terachloride phthalate
GP-1 2-3' ug+kg NA* 1 255 NA* I NA* NA* 6690 NA* 33.5 1 108 NA* 5.1
GP-22-3'
uglkg
583
236
147
NA*
NA*
NA*
NA*
NA*
NA*
NA*
18.6
GP-32-3'
uglkg
610
212
NA*
NA*
NA*
4810
NA*
NA*
NA*
NA*
21.6
GP42-3'
uglkg
549
NA*
NA*
NA*
NA*
NA*
NA*
NA*
NA*
8470
13.6
GP-52-3'
uglkg
694
NA*
NA*
NA*
NA*
NA*
NA*
NA*
NA*
79DO
12.4
GP-62-3'
uglkg
958
NA*
NA*
NA*
NA*
2020
NA*
NA*
34.6
NA*
12.3
GP-72-3'
uglkg
NA*
NA*
NA*
NA*
NA*
1450
NA*
NA*
NA*
NA*
16.8
HA-12-T
uglkg
1420
NA*
NA*
79.7
NA*
1310
NA*
NA*
NA*
14100
7.3
HA-2 2-3'
uglkg
1060
NA*
NA*
NA*
NA*
2390
41
NA*
24.9
27900
12
SB-3
uglkg
1 D80
NA*
NA*
NA*
73.4
1360
NA*
NA*
NA*
NA*
19.3
NC PSRGs
uglkg
1700
2000
1900
34
3800
230
690
12DO
99D
Not Listed
4700
In summary, the table lists the constituents detected at concentrations above the laboratory
RLs with the associated human health based PSRGs. Chemical analysis shows low levels of
the PCB Aroclor 1254 in the range of 1 to 6 parts per million (ppm), chlorodane at
approximately 0.5 to 1.5 ppm, DDE (DDT degradation product), DDT, dieldrin at a
concentration of 0.0797 ppm, endrin aldehyde at low concentrations, and bis-2-
ethylhexelphthalate (plastisizer) 8 to 27 ppm (which was the only BN 8270 constituent
detected). Of the constituents identified, PCB Aroclor 1254 and dieldrin were detected at
concentrations above the associated PSRG values. A copy of the North Carolina PSRG tables
have been included in the report appendix for reference.
The complete laboratory analytical report which includes the soil sample results is attached
as Appendix D.
WASTE CHARACTERIZATION 7 310 CLONINGER MILL ROAD, HICKORY, NC
HICKORY NE WWTP FLOOD MITIGATION MEASURES SITE PROJECT NO. J22-8073

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4.0 CONCLUSIONS
The Site is within an irregular -shaped parcel and consists of a portion of a larger 45.83-acre
tract owned by the City of Hickory. The Site, for the purposes of this report, is a portion of
land south of the Hickory NE waste -water treatment plant (WWTP) and is bordered to the
north by Falling Creek (and the Hickory NE WWTP beyond), to the south by undeveloped
land, to the east by Cloninger Mill Road NE and undeveloped land, and west by undeveloped
land.
Available historical information indicates the Site was utilized as WWTP sludge
drying/ dewatering beds for the adjacent WWTP. Available information provided indicated
the period of operation was generally from the 1970's and 1980's, although the precise date
of use is not documented. The Site was excavated and graded to configure four (4) sludge
drying basins along the south side of Falling Creek south of the Hickory NE WWTP. For the
purposes of this report the basins will be identified as Basin 1 through 4, in an east to west
orientation. The basins were apparently excavated in native soil which appears to have been
used as earthen berms for the basins.
In general, native soil encountered at the Site consisted mainly of clayey, sandy Silt, with
partially weathered bedrock at approximately 10 feet bgs. Soils beneath the sludge layer
were moist to wet, with noticeable groundwater present between 6 and 7 feet bgs. The
sludge layer is easily identified in the field based on color, cohesion and grain size. Based on
the approximate aerial extent of the basins which cover approximately one acre, and the
estimated depth and extent of the sludge, it is estimated that approximately 1600 cubic yards
of sludge material are present, based on the preliminary data. Excavation would likely
include surficial and basal soils bringing the preliminary estimated volume to approximately
5,000 cubic yards. Based on an average weight of 1.5 tons/cubic yard, the estimated total
tonnage is approximately 7,500 tons.
The results of the TCLP analysis show that only Basin 3 has an exceedance of the TCLP
regulatory concentration for lead (Pb) of 13.5 mg/L (RCRA Toxicity characteristic for lead is
5.0 mg/L). This data shows that while there are elevated total metal concentrations in all of
the samples, only Basin 3 exceeds the regulatory limit for lead, characterizing the sludge
layer from this basin as a RCRA hazardous waste.
The next step is to complete a waste characterization for landfilling and conducting a
treatability test for the Basin 3 sludge. Lead containing soils should be treatable to render
them non -hazardous and suitable disposal in a Subtitle D landfill locally (based on the
acceptance of the completed profile with the landfill.
WASTE CHARACTERIZATION 8 310 CLONINGER MILL ROAD, HICKORY, NC
HICKORY NE WWTP FLOOD MITIGATION MEASURES SITE PROJECT NO. J22-8073

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5.0 STANDARD OF CARE
The services performed by Nova on this project have been conducted with that level of care
and skill ordinarily exercised by reputable members of the profession, practicing in the same
locality, under similar budget and time constraints. No other warranty is expressed or
intended.
This document was prepared exclusively for the use or benefit of those listed on the Title
page of this report. Reliance or use by any other third party without explicit written
authorization from Nova will be at the third party's own risk. No warranties or
representations, express or implied, are made to any such third party.
We appreciate the opportunity to provide this service. If you have any questions regarding
this report, please contact us.
NOVA GROUP, GBC
Report Completed By:
David Brewster
Senior Project Manager
Report Review By:
Wil King
Senior Project Manager
WASTE CHARACTERIZATION 9
HICKORY NE WWTP FLOOD MITIGATION MEASURES SITE
310 CLONINGER MILL ROAD, HICKORY, NC
PROJECT NO. J22-8073

FIGURES

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Topographic Map
Hickory NE Flood Mitigation Measures Site
Basin Locations
810 Cloninger Mill Road NE
Hickory, NC 28601
Figure
Project # J -8703
410* Nova
Group

Hickory NE WWTP
O
t-"
Basin 2
GP4
GP6 HA2
�
GP7
GP5
■� GP-1 Basin 3 HAi
GP2 Basin
Basin 4
GP3
M
Scale Not Provided
Hickory NE WWTP Flood Mitigation Measures Site - Catawba County, N
Approximate Sampling Locations
A Sludge Basing Lida Imagery - Sample Locations
310 CIoninger MITI Road Nova
Hickory, N8801 Group
Figure 3
Project # J22-807

APPENDIX A
PHOTOGRAPHIC DOCUMENTATION
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APPENDIX B
SOIL BORING LOGS

NOVA GROUP GBC
LOG OF BORING GP-1
Raleigh, North Carolina
Environmental Services
(Page 1 of 1)
Date 08/16/2022 Weather : Cloudy, 75 deg. F, It. wind
Cloninger MITI Road
Drilling Company : JG Drilling Temporary Well Type : Not Applicable
Hickory, NC
Hole Diameter : 2-inches
Drilling Method : Geoprobe Survey By
Sampling Method : Macro Core Logged By : DCB
Project NO. J22-8073
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DESCRIPTION
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REMARKS
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SOII
Soil
Micacious, silty Clay, red brown, dry, slightly moist
1
CL
2
Sludge, black, very fine grained, slightly moist
FB
3
GP-1
clayey, sandy SILT, tan/yellowish brown,
4-
5-
6—
Water at 6 - 7 feet
SM
7
8
9
10
Rock at 10 feet

NOVA GROUP GBC
LOG OF BORING GP-2
Raleigh, North Carolina
Environmental Services
(Page 1 of 1)
Date 08/16/2022 Weather : Cloudy, 75 deg. F, It. wind
Cloninger MITI Road
Drilling Company : JG Drilling Temporary Well Type : Not Applicable
Hickory, NC
Hole Diameter : 2-inches
Drilling Method : Geoprobe Survey By
Sampling Method : Macro Core Logged By : DCB
Project NO. J22-8073
a
u-
c
0-
E
U
_
E
m
=
o
Q
n
DESCRIPTION
�,
REMARKS
Q
J
0
U
Z)
0
o-
m
0
SOII
Soil
Micacious, silty Clay, red brown, dry, slightly moist
1
CL
2
Sludge, black, very fine grained, slightly moist
FB
3
GP-1
clayey., sandy SILT, tan/yellowish brown,
4-
5-
6—
Water at 6 - 7 feet
SM
7
8
9
10
Rock at 10 feet

NOVA GROUP GBC
LOG OF BORING GP-3
Raleigh, North Carolina
Environmental Services
(Page 1 of 1)
Date 08/16/2022 Weather : Cloudy, 75 deg. F, It. wind
Cloninger MITI Road
Drilling Company : JG Drilling Temporary Well Type : Not Applicable
Hickory, NC
Hole Diameter : 2-inches
Drilling Method : Geoprobe Survey By
Sampling Method : Macro Core Logged By : DCB
Project NO. J22-8073
a
u-
c
0-
E
U
_
E
m
=
o
Q
n
DESCRIPTION
�,
REMARKS
Q
J
0
U
Z)
0
o-
m
0
SOII
Soil
Micacious, silty Clay, red brown, dry, slightly moist
1
CL
2
Sludge, black, very fine grained, slightly moist
FB
3
GP-1
clayey, sandy SILT, tan/yellowish brown,
4-
5-
6—
Water at 6 - 7 feet
SM
7
8
9
10
Rock at 10 feet

NOVA GROUP GBC
LOG OF BORING GP-4
Raleigh, North Carolina
Environmental Services
(Page 1 of 1)
Date 08/16/2022 Weather : Cloudy, 75 deg. F, It. wind
Cloninger MITI Road
Drilling Company : JG Drilling Temporary Well Type : Not Applicable
Hickory, NC
Hole Diameter : 2-inches
Drilling Method : Geoprobe Survey By
Sampling Method : Macro Core Logged By : DCB
Project No. J22-8073
a
u_
c
0-
E
U
_
E
m
>
cn
=
a
Q
n
DESCRIPTION
�,
REMARKS
Q
0
J
0
U
Z)
0
0-
m
0—Soil
Highly organic soil
Highly organic soil grading into residual fine-grained sludge
1
CL
2
Sludge, black, very fine grained, slightly moist
FB
3
GP-1
I
clayey, sandy SILT, tan/yellowish brown,
4-
5-
6—
Water at 6 -7 feet
SM
7
8
9
10
Rock at 10 feet

NOVA GROUP GBC
LOG OF BORING GP-5
Raleigh, North Carolina
Environmental Services
(Page 1 of 1)
Date 08/16/2022 Weather : Cloudy, 75 deg. F, It. wind
Cloninger MITI Road
Drilling Company : JG Drilling Temporary Well Type : Not Applicable
Hickory, NC
Hole Diameter : 2-inches
Drilling Method : Geoprobe Survey By
Sampling Method : Macro Core Logged By : DCB
Project No. J22-8073
a
u_
c
0-
E
U
_
E
m
>
cn
=
a
Q
n
DESCRIPTION
�,
REMARKS
Q
0
J
0
U
Z)
0
0-
m
0—Soil
Highly organic soil
Highly organic soil grading into residual fine-grained sludge
1
CL
2
Sludge, black, very fine grained, slightly moist
FB
3
GP-1
I
clayey sandy SILT, tan/yellowish brown,
4-
5-
6—
Water at 6 -7 feet
SM
7
8
9
10
Rock at 10 feet

NOVA GROUP GBC
LOG OF BORING GP-6
Raleigh, North Carolina
Environmental Services
(Page 1 of 1)
Date 08/16/2022 Weather : Cloudy, 75 deg. F, It. wind
Cloninger MITI Road
Drilling Company : JG Drilling Temporary Well Type : Not Applicable
Hickory, NC
Hole Diameter : 2-inches
Drilling Method : Geoprobe Survey By
Sampling Method : Macro Core Logged By : DCB
Project No. J22-8073
a
u_
c
0-
E
U
_
E
m
>
cn
=
a
Q
n
DESCRIPTION
�,
REMARKS
Q
0
J
0
U
Z)
0
0-
m
0—Soil
Highly organic soil
Highly organic soil grading into residual fine-grained sludge
1
CL
2
Sludge, black, very fine grained, slightly moist
FB
3
GP-1
I
clayey, sandy SILT, tan/yellowish brown
4-
5-
6—
Water 6 - 7 feet
SM
7
8
9
10
Rock at 10 feet

NOVA GROUP GBC
LOG OF BORING GP-7
Raleigh, North Carolina
Environmental Services
(Page 1 of 1)
Date 08/16/2022 Weather : Cloudy, 75 deg. F, It. wind
Cloninger MITI Road
Drilling Company : JG Drilling Temporary Well Type : Not Applicable
Hickory, NC
Hole Diameter : 2-inches
Drilling Method : Geoprobe Survey By
Sampling Method : Macro Core Logged By : DCB
Project No. J22-8073
a
u_
c
0-
E
U
_
E
m
>
cn
=
a
Q
n
DESCRIPTION
�,
REMARKS
Q
0
J
0
U
Z)
0
0-
m
0—Soil
Highly organic soil
Highly organic soil grading into residual fine-grained sludge
1
CL
2
Sludge, black, very fine grained, slightly moist
FB
3
GP-1
I
clayey, sandy, SILT, tan/yellowish brown
4-
5-
6—
Water at 6 -7 feet
SM
7
8
9
10
Rock at 10 feet

APPENDIX C
LABORATORY CHEMICAL ANALYSIS REPORT
I

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
October 25, 2022
Mike Minett
Nova Consulting Group, Inc.
442 South Main Street
Suite #7
Davidson, NC 28036
RE: Project: WASTE CHARACTERIZATION
Pace Project No.: 92621331
Dear Mike Minett:
Enclosed are the analytical results for sample(s) received by the laboratory between August 17, 2022 and September 13,
2022. The results relate only to the samples included in this report. Results reported herein conform to the applicable
TNI/NELAC Standards and the laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the
report.
Some analyses were subcontracted outside of the Pace Network. The test report from the external subcontractor is
attached to this report in its entirety.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace National - Mt. Juliet
• Pace Analytical Services - Asheville
• Pace Analytical Services - Charlotte
• Pace Analytical Services - Minneapolis
• Pace Analytical Services - Ormond Beach
Report revision 1: On 10/19/22, client requested to composite and break samples into Basin 1,2,3,4. For those four
samples, we ran and reported Metals and Hex Chrome.
Report revision 2: On 10/25/22, the lab completed and reported the missing RCRA Metals for Basin 3 & 4.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
�'ft.w
Bonnie Vang
[e-mail]
[phone]
Project Manager
A� ...
REPORT OF LABORATORY ANALYSIS
r
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 165

lceAnalyircal
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
October 25, 2022
Page 2
Enclosures
kc
r
to
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 2 of 165

laneAnalytical
www,pacelabs.com
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Project: WASTE CHARACTERIZATION
Pace Project No.: 92621331
Pace Analytical Services, LLC - Minneapolis MN
1700 Elm Street SE, Minneapolis, MN 55414
1800 Elm Street SE, Minneapolis, MN 55414--Satellite Air
Lab
A21-A Certification #: 2926.01
Alabama Certification #: 40770
Alaska Contaminated Sites Certification #: 17-009*
Alaska DW Certification #: MN00064
Arizona Certification #: AZ0014*
Arkansas DW Certification #: MN00064
Arkansas WW Certification #: 88-0680
California Certification #: 2929
Colorado Certification #: MN00064
Connecticut Certification #: PH-0256
EPA Region 8 Tribal Water Systems+Wyoming DW
Certification #: via MN 027-053-137
Florida Certification #: E87605*
Georgia Certification #: 959
Hawaii Certification #: MN00064
Idaho Certification #: MN00064
Illinois Certification #: 200011
Indiana Certification #: C-MN-01
Iowa Certification #: 368
Kansas Certification M E-10167
Kentucky DW Certification #: 90062
Kentucky WW Certification #: 90062
Louisiana DEQ Certification #: AI-03086*
Louisiana DW Certification #: MN00064
Maine Certification #: MN00064*
Maryland Certification #: 322
Michigan Certification #: 9909
Minnesota Certification #: 027-053-137*
Minnesota Dept ofAg Approval: via MN 027-053-137
Minnesota Petrofund Registration #: 1240*
Mississippi Certification #: MN00064
Pace Analytical Services Ormond Beach
8 East Tower Circle, Ormond Beach, FL 32174
Alaska DEC- CS/UST/LUST
Alabama Certification #: 41320
Colorado Certification: FL NELAC Reciprocity
Connecticut Certification #: PH-0216
Delaware Certification: FL NELAC Reciprocity
Florida Certification #: E83079
Georgia Certification #: 955
Guam Certification: FL NELAC Reciprocity
Hawaii Certification: FL NELAC Reciprocity
Illinois Certification #: 200068
Indiana Certification: FL NELAC Reciprocity
Kansas Certification #: E-10383
Kentucky Certification #: 90050
Louisiana Certification #: FL NELAC Reciprocity
Louisiana Environmental Certificate #: 05007
CERTIFICATIONS
Missouri Certification #: 10100
Montana Certification #: CERT0092
Nebraska Certification #: NE-OS-18-06
Nevada Certification #: MN00064
New Hampshire Certification #: 2081*
New Jersey Certification #: MN002
New York Certification #: 11647*
North Carolina DW Certification #: 27700
North Carolina WW Certification #: 530
North Dakota Certification (A2LA) #: R-036
North Dakota Certification (MN) #: R-036
Ohio DW Certification #: 41244
Ohio VAP Certification (1700) #: CL101
Ohio VAP Certification (1800) #: CL110*
Oklahoma Certification #: 9507*
Oregon Primary Certification #: MN300001
Oregon Secondary Certification #: MN200001*
Pennsylvania Certification #: 68-00563*
Puerto Rico Certification #: MN00064
South Carolina Certification #:74003001
Tennessee Certification #: TN02818
Texas Certification #: T104704192*
Utah Certification #: MN00064*
Vermont Certification #: VT-027053137
Virginia Certification #: 460163*
Washington Certification #: C486*
West Virginia DEP Certification #: 382
West Virginia DW Certification #: 9952 C
Wisconsin Certification #: 999407970
Wyoming UST Certification #: via A21-A 2926.01
USDA Permit #: P330-19-00208
*Please Note: Applicable air certifications are denoted with
an asterisk (*).
Maine Certification #: FL01264
Maryland Certification: #346
Massachusetts Certification #: M-FL1264
Michigan Certification #: 9911
Mississippi Certification: FL NELAC Reciprocity
Missouri Certification #: 236
Montana Certification M Cert 0074
Nebraska Certification: NE-OS-28-14
New Hampshire Certification #: 2958
New Jersey Certification M FL022
New York Certification #: 11608
North Carolina Environmental Certificate #: 667
North Carolina Certification M 12710
North Dakota Certification M R-216
Ohio DEP 87780
Oklahoma Certification #: D9947
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 3 of 165

laneAnalytical
www,pacelabs.com
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Project: WASTE CHARACTERIZATION
Pace Project No.: 92621331
Pace Analytical Services Ormond Beach
Pennsylvania Certification #: 68-00547
Puerto Rico Certification #: FLO1264
South Carolina Certification: #96042001
Tennessee Certification #: TN02974
Texas Certification: FL NELAC Reciprocity
Pace Analytical Services National
12065 Lebanon Road, Mt. Juliet, TN 37122
Alabama Certification #: 40660
Alaska Certification 17-026
Arizona Certification #: AZ0612
Arkansas Certification #: 88-0469
California Certification #: 2932
Canada Certification #: 1461.01
Colorado Certification #: TN00003
Connecticut Certification #: PH-0197
DOD Certification: #1461.01
EPA# TN00003
Florida Certification #: E87487
Georgia DW Certification #: 923
Georgia Certification: NELAP
Idaho Certification #: TN00003
Illinois Certification #: 200008
Indiana Certification #: C-TN-01
Iowa Certification #: 364
Kansas Certification #: E-10277
Kentucky UST Certification #: 16
Kentucky Certification #: 90010
Louisiana Certification #: A130792
Louisiana DW Certification #: LA180010
Maine Certification #: TN0002
Maryland Certification #: 324
Massachusetts Certification #: M-TNO03
Michigan Certification #: 9958
Minnesota Certification #: 047-999-395
Mississippi Certification #: TN00003
Missouri Certification #: 340
Montana Certification #: CERT0086
Nebraska Certification #: NE-OS-15-05
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Laboratory ID: 99006
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
CERTIFICATIONS
US Virgin Islands Certification: FL NELAC Reciprocity
Virginia Environmental Certification #: 460165
West Virginia Certification #: 9962C
Wisconsin Certification #: 399079670
Wyoming (EPA Region 8): FL NELAC Reciprocity
Nevada Certification #: TN-03-2002-34
New Hampshire Certification #: 2975
New Jersey Certification #: TNO02
New Mexico DW Certification
New York Certification #: 11742
North Carolina Aquatic Toxicity Certification #: 41
North Carolina Drinking Water Certification #: 21704
North Carolina Environmental Certificate #: 375
North Dakota Certification #: R-140
Ohio VAP Certification #: CL0069
Oklahoma Certification #: 9915
Oregon Certification M TN200002
Pennsylvania Certification #: 68-02979
Rhode Island Certification #: LA000356
South Carolina Certification #: 84004
South Dakota Certification
Tennessee DW/Chem/Micro Certification #: 2006
Texas Certification #: T 104704245-17-14
Texas Mold Certification #: LABO152
USDA Soil Permit #: P330-15-00234
Utah Certification #: TN00003
Vermont Dept. of Health: ID# VT-2006
Virginia Certification #: VT2006
Virginia Certification #: 460132
Washington Certification #: C847
West Virginia Certification #: 233
Wisconsin Certification #: 998093910
Wyoming UST Certification #: via A21-A 2926.01
A2LA-ISO 17025 Certification M 1461.01
A2LA-ISO 17025 Certification #: 1461.02
AIHA-LAP/LLC EMLAP Certification #:100789
South Carolina Certification #: 99006001
South Carolina Drinking Water Cert. #: 99006003
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Louisiana DoH Drinking Water #: LA029
Virginia/VELAP Certification #: 460221
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 4 of 165

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: WASTE CHARACTERIZATION
Pace Project No.: 92621331
Pace Analytical Services Asheville
South Carolina Laboratory ID: 99030
South Carolina Certification #: 99030001
CERTIFICATIONS
VirginiaNELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 5 of 165

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE ANALYTE COUNT
Project: WASTE CHARACTERIZATION
Pace Project No.: 92621331
Lab ID
Sample ID
Method
Analysts
Analytes
Reported
Laboratory
92621331001
GP-1 2-3'
EPA 8141 B
AMM
27
PAN
EPA 8081 B
SEM
24
PASI-C
EPA 8082A
BAJ
8
PASI-C
EPA 6010
KC2
1
PASI-O
EPA 6020
BSL, LEC
15
PASI-O
EPA 7471
JNK
1
PASI-O
EPA 8270E
BPJ
134
PASI-C
SW-846
KDF
1
PASI-C
EPA 1010E
MJP
1
PASI-A
SM 2540G
CMK
1
PAN
SM 4500-S2D-2011 Modified
JP1
1
PASI-A
EPA 9045D
YEG
1
PASI-A
EPA 9012
JH2
1
PASI-O
92621331002
GP-2 2-3'
EPA 8141 B
AMM
27
PAN
EPA 8081 B
SEM
24
PASI-C
EPA 8082A
BAJ
8
PASI-C
EPA 6010
AME
1
PASI-O
EPA 6020
BSL, LEC
15
PASI-O
EPA 7471
JNK
1
PASI-O
EPA 8270E
BPJ
134
PASI-C
SW-846
KDF
1
PASI-C
EPA 1010E
MJP
1
PASI-A
SM 2540G
CMK
1
PAN
SM 4500-S2D-2011 Modified
JP1
1
PASI-A
EPA 9045D
YEG
1
PASI-A
EPA 9012
JH2
1
PASI-O
92621331003
GP-3 2-3'
EPA 8141 B
AMM
27
PAN
EPA 8081 B
SEM
24
PASI-C
EPA 8082A
BAJ
8
PASI-C
EPA 6010
AME
1
PASI-O
EPA 6020
BSL, LEC
15
PASI-O
EPA 7471
JNK
1
PASI-O
EPA 8270E
BPJ
134
PASI-C
SW-846
KDF
1
PASI-C
EPA 1010E
MJP
1
PASI-A
SM 2540G
CMK
1
PAN
SM 4500-S2D-2011 Modified
JP1
1
PASI-A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 6 of 165

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE ANALYTE COUNT
Project: WASTE CHARACTERIZATION
Pace Project No.: 92621331
Lab ID
Sample ID
Method
Analysts
Analytes
Reported
Laboratory
EPA 9045D
YEG
1
PASI-A
EPA 9012
JH2
1
PASI-O
92621331004
GP-4 2-3'
EPA 8141 B
AMM
27
PAN
EPA 8081 B
SEM
24
PASI-C
EPA 8082A
BAJ
8
PASI-C
EPA 6010
AME
1
PASI-O
EPA 6020
BSL, LEC
15
PASI-O
EPA 7471
JNK
1
PASI-O
EPA 8270E
BPJ
134
PASI-C
SW-846
KDF
1
PASI-C
EPA 1010E
MJP
1
PASI-A
SM 2540G
CMK
1
PAN
SM 4500-S2D-2011 Modified
JP1
1
PASI-A
EPA 9045D
YEG
1
PASI-A
EPA 9012
JH2
1
PASI-O
92621331005
GP-5 2-3'
, EPA 8141 B
AMM
27
PAN
EPA 8081 B
SEM
24
PASI-C
EPA 8082A
BAJ
8
PASI-C
EPA 6010
AME
1
PASI-O
EPA 6020
LEC
15
PASI-O
EPA 7471
JNK
1
PASI-O
EPA 8270E
BPJ
134
PASI-C
SW-846
KDF
1
PASI-C
EPA 1010E
MJP
1
PASI-A
SM 2540G
CMK
1
PAN
SM 4500-S2D-2011 Modified
JP1
1
PASI-A
EPA 9045D
YEG
1
PASI-A
EPA 9012
JH2
1
PASI-O
92621331006
GP-6 2-3'
EPA 8141 B
AMM
27
PAN
EPA 8081 B
SEM
24
PASI-C
EPA 8082A
BAJ
8
PASI-C
EPA 6010
AME
1
PASI-O
EPA 6020
LEC
15
PASI-O
EPA 7471
JNK
1
PASI-O
EPA 8270E
BPJ
134
PASI-C
SW-846
KDF
1
PASI-C
EPA 1010E
MJP
1
PASI-A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 7 of 165

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE ANALYTE COUNT
Project: WASTE CHARACTERIZATION
Pace Project No.: 92621331
Analytes
Lab ID Sample ID Method Analysts Reported Laboratory
SM 2540G CMK 1 PAN
SM 4500-S2D-2011 Modified JP1 1 PASI-A
EPA 9045D YEG 1 PASI-A
EPA 9012 JH2 1 PASI-O
92621331007 GP-7 2-3' EPA 8141 B AMM 27 PAN
EPA 8081 B SEM 24 PASI-C
EPA 8082A BAJ 8 PASI-C
EPA6010 AME 1 PASI-O
EPA 6020 LEC 15 PASI-O
EPA 7471 JNK 1 PASI-O
EPA 8270E BPJ 134 PASI-C
SW-846 KDF 1 PASI-C
EPA 1010E MJP 1 PASI-A
SM 2540G CMK 1 PAN
SM 4500-S2D-2011 Modified JP1 1 PASI-A
EPA 9045D YEG 1 PASI-A
EPA 9012 JH2 1 PASI-O
92621331008 HA-12-3' EPA 8141B AMM 27 PAN
EPA 8081 B SEM 24 PASI-C
EPA 8082A BAJ 8 PASI-C
EPA6010 AME 1 PASI-O
EPA 6020 LEC 15 PASI-O
EPA 7471 JNK 1 PASI-O
EPA 8270E BPJ 134 PASI-C
SW-846 KDF 1 PASI-C
EPA 1010E MJP 1 PASI-A
SM 2540G CMK 1 PAN
SM 4500-S2D-2011 Modified JP1 1 PASI-A
EPA 9045D YEG 1 PASI-A
EPA 9012 JH2 1 PASI-O
92621331009 HA-2 2-3' EPA 8141 B AMM 27 PAN
EPA 8081 B SEM 24 PASI-C
EPA 8082A BAJ 8 PASI-C
EPA 6010 AME 1 PASI-O
EPA 6020 BSL, LEC 15 PASI-O
EPA 7471 JNK 1 PASI-O
EPA 8270E BPJ 134 PASI-C
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 8 of 165

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE ANALYTE COUNT
Project: WASTE CHARACTERIZATION
Pace Project No.: 92621331
Analytes
Lab ID Sample ID Method Analysts Reported Laboratory
SW-846 KDF 1 PASI-C
EPA 1010E MJP 1 PASI-A
SM 2540G CMK 1 PAN
SM 4500-S2D-2011 Modified JP1 1 PASI-A
EPA 9045D YEG 1 PASI-A
EPA 9012 JH2 1 PASI-O
92621331010 SURFACE BASIN 3 EPA 8141B AMM 27 PAN
EPA 8081 B SEM 24 PASI-C
EPA 8082A BAJ 8 PASI-C
EPA 6010 AME 1 PASI-O
EPA 6020 LEC 15 PASI-O
EPA 7471 JNK 1 PASI-O
EPA 8270E BPJ 134 PASI-C
SW-846 KDF 1 PASI-C
EPA 1010E MJP 1 PASI-A
SM 2540G CMK 1 PAN
SM 4500-S2D-2011 Modified JP1 1 PASI-A
EPA 9045D YEG 1 PASI-A
EPA 9012 JH2 1 PASI-O
92621331011 GP-1 2-3' EPA 8260D SAS 67 PASI-C
SW-846 KDF 1 PASI-C
92621331012 GP-6 2-3' EPA 8260D SAS 67 PASI-C
SW-846 KDF 1 PASI-C
92621331013 HA-1 2-3' EPA 8260D SAS 67 PASI-C
SW-846 KDF 1 PASI-C
92621331014 HA-2 2-3' EPA 8260D SAS 67 PASI-C
SW-846 KDF 1 PASI-C
92621331015 Basin 1 EPA 601 OD DM 7 PASI-M
EPA 7470A LMW 1 PASI-M
EPA 7196A JMH 1 PASI-A
92621331016 Basin 2 EPA 601 OD DM 7 PASI-M
EPA 7470A LMW 1 PASI-M
EPA 7196A JMH 1 PASI-A
92621331017 Basin 3 EPA 601 OD DM 7 PASI-M
EPA 7470A LMW 1 PASI-M
EPA 7196A JMH 1 PASI-A
92621331018 Basin 4 EPA 601 OD DM 7 PASI-M
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 9 of 165

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9800 Kincey Ave. Suite 100
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SAMPLE ANALYTE COUNT
Project: WASTE CHARACTERIZATION
Pace Project No.: 92621331
Analytes
Lab ID Sample ID Method Analysts Reported Laboratory
EPA 7470A LMW 1 PASI-M
EPA 7196A JMH 1 PASI-A
PAN = Pace National - Mt. Juliet
PASI-A = Pace Analytical Services - Asheville
PASI-C = Pace Analytical Services - Charlotte
PASI-M = Pace Analytical Services - Minneapolis
PASI-O = Pace Analytical Services - Ormond Beach
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 10 of 165

lceAnalyircal
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: WASTE CHARACTERIZATION
Pace Project No.: 92621331
Sample: GP-1 2-3' Lab ID: 92621331001 Collected: 08/16/22 10:45 Received: 08/17/22 16:15 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
OP Pesticides 8141 B
Analytical Method: EPA 8141 B Preparation Method: 3546
Pace National
- Mt. Juliet
Azinphos, methyl (Guthion)
ND
mg/kg
0.185
1
08/21/22 16:12
08/22/22 01:29
86-50-0
Bolstar
ND
mg/kg
0.185
1
08/21/22 16:12
08/22/22 01:29
35400-43-2
Chlorpyrifos
ND
mg/kg
0.185
1
08/21/22 16:12
08/22/22 01:29
2921-88-2
Coumaphos
ND
mg/kg
0.185
1
08/21/22 16:12
08/22/22 01:29
56-72-4
Total Demeton
ND
mg/kg
0.130
1
08/21/22 16:12
08/22/22 01:29
8065-48-3
Diazinon
ND
mg/kg
0.185
1
08/21/22 16:12
08/22/22 01:29
333-41-5
Dichlorvos
ND
mg/kg
0.185
1
08/21/22 16:12
08/22/22 01:29
62-73-7
Dimethoate
ND
mg/kg
0.185
1
08/21/22 16:12
08/22/22 01:29
60-51-5
Disulfoton
ND
mg/kg
0.185
1
08/21/22 16:12
08/22/22 01:29
298-04-4
EPN (ENT)
ND
mg/kg
0.185
1
08/21/22 16:12
08/22/22 01:29
2104-64-5
Ethoprop
ND
mg/kg
0.185
1
08/21/22 16:12
08/22/22 01:29
13194-48-4
Parathion (Ethyl parathion)
ND
mg/kg
0.185
1
08/21/22 16:12
08/22/22 01:29
56-38-2
Fensulfothion
ND
mg/kg
0.185
1
08/21/22 16:12
08/22/22 01:29
115-90-2
Fenthion
ND
mg/kg
0.185
1
08/21/22 16:12
08/22/22 01:29
55-38-9
Malathion
ND
mg/kg
0.185
1
08/21/22 16:12
08/22/22 01:29
121-75-5
Merphos
ND
mg/kg
0.185
1
08/21/22 16:12
08/22/22 01:29
150-50-5
Methyl parathion
ND
mg/kg
0.185
1
08/21/22 16:12
08/22/22 01:29
298-00-0
Mevinphos
ND
mg/kg
0.185
1
08/21/22 16:12
08/22/22 01:29
7786-34-7
Naled
ND
mg/kg
0.185
1
08/21/22 16:12
08/22/22 01:29
300-76-5
Phorate
ND
mg/kg
0.185
1
08/21/22 16:12
08/22/22 01:29
298-02-2
Ronnel
ND
mg/kg
0.185
1
08/21/22 16:12
08/22/22 01:29
299-84-3
Stirophos (Tetrachlorvinphos)
ND
mg/kg
0.185
1
08/21/22 16:12
08/22/22 01:29
22248-79-9
Sulfotepp (ThiodiphosphoricAc
ND
mg/kg
0.185
1
08/21/22 16:12
08/22/22 01:29
3689-24-5
TEPP
ND
mg/kg
1.85
1
08/21/22 16:12
08/22/22 01:29
107-49-3
Tokuthion (Prothiofos)
ND
mg/kg
0.185
1
08/21/22 16:12
08/22/22 01:29
34643-46-4
Trichloronate
ND
mg/kg
0.185
1
08/21/22 16:12
08/22/22 01:29
327-98-0
Surrogates
Triphenyl phosphate (S)
41.3
%
36.0-121
1
08/21/22 16:12
08/22/22 01:29
115-86-6
8081 GCS Pesticides
Analytical Method: EPA 8081 B Preparation Method: EPA 3546
Pace Analytical
Services - Charlotte
alpha-BHC
ND
ug/kg
41.5
10
08/24/22 07:17
08/26/22 17:52
319-84-6
gamma-BHC (Lindane)
ND
ug/kg
41.5
10
08/24/22 07:17
08/26/22 17:52
58-89-9
beta-BHC
ND
ug/kg
41.5
10
08/24/22 07:17
08/26/22 17:52
319-85-7
Heptachlor
ND
ug/kg
41.5
10
08/24/22 07:17
08/26/22 17:52
76-44-8
delta-BHC
ND
ug/kg
41.5
10
08/24/22 07:17
08/26/22 17:52
319-86-8
Aldrin
ND
ug/kg
41.5
10
08/24/22 07:17
08/26/22 17:52
309-00-2
Heptachlor epoxide
ND
ug/kg
41.5
10
08/24/22 07:17
08/26/22 17:52
1024-57-3
Endosulfan I
ND
ug/kg
41.5
10
08/24/22 07:17
08/26/22 17:52
959-98-8
4,4'-DDE
255
ug/kg
41.5
10
08/24/22 07:17
08/26/22 17:52
72-55-9
Dieldrin
ND
ug/kg
41.5
10
08/24/22 07:17
08/26/22 17:52
60-57-1
Endrin
ND
ug/kg
41.5
10
08/24/22 07:17
08/26/22 17:52
72-20-8
4,4'-DDD
ND
ug/kg
41.5
10
08/24/22 07:17
08/26/22 17:52
72-54-8
Endosulfan II
ND
ug/kg
41.5
10
08/24/22 07:17
08/26/22 17:52
33213-65-9
4,4'-DDT
ND
ug/kg
41.5
10
08/24/22 07:17
08/26/22 17:52
50-29-3
REPORT OF LABORATORY ANALYSIS
LO
This report shall not be reproduced, except in full,
Date: 10/25/2022 02:36 PM without the written consent of Pace Analytical Services, LLC. Page 11 of 165

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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: WASTE CHARACTERIZATION
Pace Project No.: 92621331
Sample: GP-1 2-3' Lab ID: 92621331001 Collected: 08/16/22 10:45 Received: 08/17/22 16:15 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8081 GCS Pesticides
Endrin aldehyde
Endosulfan sulfate
Methoxychlor
Endrin ketone
Chlordane (Technical)
Toxaphene
Mirex
Hexachlorobenzene
Surrogates
Tetrachloro-m-xylene (S)
Decachlorobiphenyl (S)
8082 GCS PCB
PCB-1016 (Aroclor 1016)
PCB-1221 (Aroclor 1221)
PCB-1232 (Aroclor 1232)
PCB-1242 (Aroclor 1242)
PCB-1248 (Aroclor 1248)
PCB-1254 (Aroclor 1254)
PCB-1260 (Aroclor 1260)
Surrogates
Decachlorobiphenyl (S)
Analytical Method: EPA 8081 B Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
ND
ug/kg
41.5
10
08/24/22 07:17
08/26/22 17:52
7421-93-4
ND
ug/kg
41.5
10
08/24/22 07:17
08/26/22 17:52
1031-07-8
ND
ug/kg
104
10
08/24/22 07:17
08/26/22 17:52
72-43-5
ND
ug/kg
41.5
10
08/24/22 07:17
08/26/22 17:52
53494-70-5
ND
ug/kg
207
10
08/24/22 07:17
08/26/22 17:52
57-74-9
ND
ug/kg
145
10
08/24/22 07:17
08/26/22 17:52
8001-35-2
ND
ug/kg
104
10
08/24/22 07:17
08/26/22 17:52
2385-85-5
ND
ug/kg
41.5
10
08/24/22 07:17
08/26/22 17:52
118-74-1
0
%
10-133
10
08/24/22 07:17
08/26/22 17:52
877-09-8 D3,S4
0
%
10-146
10
08/24/22 07:17
08/26/22 17:52
2051-24-3 S4
Analytical Method: EPA 8082A Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
ND
ug/kg
1230
20
08/19/22 15:53
08/24/22 05:50
12674-11-2
ND
ug/kg
1230
20
08/19/22 15:53
08/24/22 05:50
11104-28-2
ND
ug/kg
1230
20
08/19/22 15:53
08/24/22 05:50
11141-16-5
ND
ug/kg
1230
20
08/19/22 15:53
08/24/22 05:50
53469-21-9
ND
ug/kg
1230
20
08/19/22 15:53
08/24/22 05:50
12672-29-6
6690
ug/kg
1230
20
08/19/22 15:53
08/24/22 05:50
11097-69-1
ND
ug/kg
1230
20
08/19/22 15:53
08/24/22 05:50
11096-82-5
0
%
10-160
20
08/19/22 15:53
08/24/22 05:50
2051-24-3 D3,S4
6010 MET ICP
Analytical Method: EPA 6010 Preparation Method: EPA 3050
Pace Analytical
Services - Ormond Beach
Tin
67.9
mg/kg
5.5
1
08/31/22 00:58
09/02/22 21:18
7440-31-5
6020 MET ICPMS
Analytical Method: EPA 6020 Preparation Method:
EPA 3050
Pace Analytical
Services - Ormond Beach
Antimony
129
mg/kg
4.1
20
08/27/22 00:15
08/29/22 09:59
7440-36-0
1g,N2
Arsenic
5.6
mg/kg
2.1
20
08/27/22 00:15
08/29/22 09:59
7440-38-2
1g
Barium
757
mg/kg
2.1
20
08/27/22 00:15
08/29/22 09:59
7440-39-3
1g
Beryllium
0.65
mg/kg
0.25
20
08/27/22 00:15
08/29/22 09:59
7440-41-7
1g
Cadmium
6.8
mg/kg
0.25
20
08/27/22 00:15
08/31/22 13:52
7440-43-9
1g
Chromium
612
mg/kg
2.1
20
08/27/22 00:15
08/29/22 09:59
7440-47-3
1g
Cobalt
6.2
mg/kg
2.1
20
08/27/22 00:15
08/29/22 09:59
7440-48-4
1g
Copper
252
mg/kg
4.1
20
08/27/22 00:15
08/31/22 13:52
7440-50-8
1g
Lead
193
mg/kg
2.1
20
08/27/22 00:15
08/31/22 13:52
7439-92-1
1g
Nickel
18.0
mg/kg
2.1
20
08/27/22 00:15
08/29/22 09:59
7440-02-0
1g
Selenium
7.2
mg/kg
2.1
20
08/27/22 00:15
08/31/22 13:52
7782-49-2
1g
Silver
52.7
mg/kg
0.25
20
08/27/22 00:15
08/29/22 09:59
7440-22-4
1g
Thallium
ND
mg/kg
2.1
20
08/27/22 00:15
08/29/22 09:59
7440-28-0
1g
Vanadium
41.3
mg/kg
2.1
20
08/27/22 00:15
08/29/22 09:59
7440-62-2
1g
Zinc
353
mg/kg
82.3
20
08/27/22 00:15
08/31/22 13:52
7440-66-6
1g
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/25/2022 02:36 PM without the written consent of Pace Analytical Services, LLC. Page 12 of 165

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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: WASTE CHARACTERIZATION
Pace Project No.: 92621331
Sample: GP-1 2-3' Lab ID: 92621331001 Collected: 08/16/22 10:45 Received: 08/17/22 16:15 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
7471 Mercury Analytical Method: EPA 7471 Preparation Method: EPA 7471
Pace Analytical Services - Ormond Beach
Mercury 4.2 mg/kg 0.17 10 08/24/22 07:26 08/24/22 12:08 7439-97-6
8270E MSSV Microwave
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical
Services - Charlotte
Acenaphthene
ND
ug/kg
6220
10
08/29/22 10:52
08/30/22 14:38
83-32-9
Acenaphthylene
ND
ug/kg
6220
10
08/29/22 10:52
08/30/22 14:38
208-96-8
Acetophenone
ND
ug/kg
6220
10
08/29/22 10:52
08/30/22 14:38
98-86-2
2-Acetylaminofluorene
ND
ug/kg
12400
10
08/29/22 10:52
08/30/22 14:38
53-96-3
4-Aminobiphenyl
ND
ug/kg
6220
10
08/29/22 10:52
08/30/22 14:38
92-67-1
Anthracene
ND
ug/kg
6220
10
08/29/22 10:52
08/30/22 14:38
120-12-7
Benzo(a)anthracene
ND
ug/kg
6220
10
08/29/22 10:52
08/30/22 14:38
56-55-3
Benzo(a)pyrene
ND
ug/kg
6220
10
08/29/22 10:52
08/30/22 14:38
50-32-8
Benzo(b)fluoranthene
ND
ug/kg
6220
10
08/29/22 10:52
08/30/22 14:38
205-99-2
Benzo(g,h,i)perylene
ND
ug/kg
6220
10
08/29/22 10:52
08/30/22 14:38
191-24-2
Benzo(k)fluoranthene
ND
ug/kg
6220
10
08/29/22 10:52
08/30/22 14:38
207-08-9
Benzyl alcohol
ND
ug/kg
12400
10
08/29/22 10:52
08/30/22 14:38
100-51-6
bis(2-Chloroethoxy)methane
ND
ug/kg
6220
10
08/29/22 10:52
08/30/22 14:38
111-91-1
bis(2-Chloroethyl) ether
ND
ug/kg
6220
10
08/29/22 10:52
08/30/22 14:38
111-44-4
2-Chloronaphthalene
ND
ug/kg
6220
10
08/29/22 10:52
08/30/22 14:38
91-58-7
2-Chlorophenol
ND
ug/kg
6220
10
08/29/22 10:52
08/30/22 14:38
95-57-8
4-Chlorophenylphenyl ether
ND
ug/kg
6220
10
08/29/22 10:52
08/30/22 14:38
7005-72-3
Chrysene
ND
ug/kg
6220
10
08/29/22 10:52
08/30/22 14:38
218-01-9
n-Decane
ND
ug/kg
6220
10
08/29/22 10:52
08/30/22 14:38
124-18-5
Diallate
ND
ug/kg
6220
10
08/29/22 10:52
08/30/22 14:38
2303-16-4
Dibenz(a,h)anthracene
ND
ug/kg
6220
10
08/29/22 10:52
08/30/22 14:38
53-70-3
Dibenzo(a,e)pyrene
ND
ug/kg
18900
10
08/29/22 10:52
08/30/22 14:38
192-65-4
Dibenzofuran
ND
ug/kg
6220
10
08/29/22 10:52
08/30/22 14:38
132-64-9
2,3-Dibromo-1-propanol phosph
ND
ug/kg
31100
10
08/29/22 10:52
08/30/22 14:38
126-72-7
1,2-Dichlorobenzene
ND
ug/kg
6220
10
08/29/22 10:52
08/30/22 14:38
95-50-1
1,3-Dichlorobenzene
ND
ug/kg
6220
10
08/29/22 10:52
08/30/22 14:38
541-73-1
1,4-Dichlorobenzene
ND
ug/kg
6220
10
08/29/22 10:52
08/30/22 14:38
106-46-7
3,3'-Dichlorobenzidine
ND
ug/kg
12400
10
08/29/22 10:52
08/30/22 14:38
91-94-1
2,4-Dichlorophenol
ND
ug/kg
6220
10
08/29/22 10:52
08/30/22 14:38
120-83-2
2,6-Dichlorophenol
ND
ug/kg
6220
10
08/29/22 10:52
08/30/22 14:38
87-65-0
2,3-Dichloroaniline
ND
ug/kg
6220
10
08/29/22 10:52
08/30/22 14:38
608-27-5
Diethylphthalate
ND
ug/kg
6220
10
08/29/22 10:52
08/30/22 14:38
84-66-2
Dimethoate
ND
ug/kg
12400
10
08/29/22 10:52
08/30/22 14:38
60-51-5
P-Dimethylaminoazobenzene
ND
ug/kg
6220
10
08/29/22 10:52
08/30/22 14:38
60-11-7
7,12-Dimethylbenz(a)anthracene
ND
ug/kg
6220
10
08/29/22 10:52
08/30/22 14:38
57-97-6
3,3'-Dimethylbenzidine
ND
ug/kg
12400
10
08/29/22 10:52
08/30/22 14:38
119-93-7
2,4-Dimethylphenol
ND
ug/kg
6220
10
08/29/22 10:52
08/30/22 14:38
105-67-9
a,a-Dimethylphenylethylamine
ND
ug/kg
31100
10
08/29/22 10:52
08/30/22 14:38
122-09-8
Dimethylphthalate
ND
ug/kg
6220
10
08/29/22 10:52
08/30/22 14:38
131-11-3
Di-n-butylphthalate
ND
ug/kg
6220
10
08/29/22 10:52
08/30/22 14:38
84-74-2
4,6-Dinitro-2-methyl phenol
ND
ug/kg
12400
10
08/29/22 10:52
08/30/22 14:38
534-52-1
REPORT OF LABORATORY ANALYSIS
v1
IL
IL
IH
v1
This report shall not be reproduced, except in full,
Date: 10/25/2022 02:36 PM without the written consent of Pace Analytical Services, LLC. Page 13 of 165

lceAnalyircal
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: WASTE CHARACTERIZATION
Pace Project No.: 92621331
Sample: GP-1 2-3' Lab ID: 92621331001 Collected: 08/16/22 10:45 Received: 08/17/22 16:15 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No
8270E MSSV Microwave
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical
Services - Charlotte
1,3-Dinitrobenzene
ND
ug/kg
6220
10
08/29/22 10:52
08/30/22 14:38
99-65-0
1,4-Dinitrobenzene
ND
ug/kg
6220
10
08/29/22 10:52
08/30/22 14:38
100-25-4
2,4-Dinitrophenol
ND
ug/kg
31100
10
08/29/22 10:52
08/30/22 14:38
51-28-5
2,4-Dinitrotoluene
ND
ug/kg
6220
10
08/29/22 10:52
08/30/22 14:38
121-14-2
2,6-Dinitrotoluene
ND
ug/kg
6220
10
08/29/22 10:52
08/30/22 14:38
606-20-2
Di-n-octylphthalate
ND
ug/kg
6220
10
08/29/22 10:52
08/30/22 14:38
117-84-0
Dinoseb
ND
ug/kg
12400
10
08/29/22 10:52
08/30/22 14:38
88-85-7
Diphenylamine
ND
ug/kg
6220
10
08/29/22 10:52
08/30/22 14:38
122-39-4
Diphenyl ether (Phenyl ether)
ND
ug/kg
9430
10
08/29/22 10:52
08/30/22 14:38
101-84-8
1,2-Diphenylhydrazine
ND
ug/kg
6220
10
08/29/22 10:52
08/30/22 14:38
122-66-7
Disulfoton
ND
ug/kg
6220
10
08/29/22 10:52
08/30/22 14:38
298-04-4
bis(2- Ethyl hexyl)phthalate
ND
ug/kg
6220
10
08/29/22 10:52
08/30/22 14:38
117-81-7
Ethyl methanesulfonate
ND
ug/kg
12400
10
08/29/22 10:52
08/30/22 14:38
62-50-0
Famphur
ND
ug/kg
12400
10
08/29/22 10:52
08/30/22 14:38
52-85-7
Fluoranthene
ND
ug/kg
6220
10
08/29/22 10:52
08/30/22 14:38
206-44-0
Fluorene
ND
ug/kg
6220
10
08/29/22 10:52
08/30/22 14:38
86-73-7
Hexachloro-1,3-butadiene
ND
ug/kg
6220
10
08/29/22 10:52
08/30/22 14:38
87-68-3
Hexachlorobenzene
ND
ug/kg
6220
10
08/29/22 10:52
08/30/22 14:38
118-74-1
Hexachlorocyclopentadiene
ND
ug/kg
6220
10
08/29/22 10:52
08/30/22 14:38
77-47-4
Hexachloroethane
ND
ug/kg
6220
10
08/29/22 10:52
08/30/22 14:38
67-72-1
Hexachlorophene
ND
ug/kg
62200
10
08/29/22 10:52
08/30/22 14:38
70-30-4
Hexachloropropene
ND
ug/kg
6220
10
08/29/22 10:52
08/30/22 14:38
1888-71-7
Indeno(1,2,3-cd)pyrene
ND
ug/kg
6220
10
08/29/22 10:52
08/30/22 14:38
193-39-5
Isodrin
ND
ug/kg
6220
10
08/29/22 10:52
08/30/22 14:38
465-73-6
Isophorone
ND
ug/kg
6220
10
08/29/22 10:52
08/30/22 14:38
78-59-1
Isosafrole
ND
ug/kg
6220
10
08/29/22 10:52
08/30/22 14:38
120-58-1
Kepone
ND
ug/kg
12400
10
08/29/22 10:52
08/30/22 14:38
143-50-0
Methapyrilene
ND
ug/kg
31100
10
08/29/22 10:52
08/30/22 14:38
91-80-5
3-Methylcholanthrene
ND
ug/kg
6220
10
08/29/22 10:52
08/30/22 14:38
56-49-5
4,4'-Methylene-bis(2-chloroani
ND
ug/kg
12400
10
08/29/22 10:52
08/30/22 14:38
101-14-4
Methyl methanesulfonate
ND
ug/kg
12400
10
08/29/22 10:52
08/30/22 14:38
66-27-3
1-Methylnaphthalene
ND
ug/kg
6220
10
08/29/22 10:52
08/30/22 14:38
90-12-0
2-Methylnaphthalene
ND
ug/kg
6220
10
08/29/22 10:52
08/30/22 14:38
91-57-6
2-Methyl-5-nitroaniline
ND
ug/kg
6220
10
08/29/22 10:52
08/30/22 14:38
99-55-8
Methyl parathion
ND
ug/kg
6220
10
08/29/22 10:52
08/30/22 14:38
298-00-0
2-Methylphenol(o-Cresol)
ND
ug/kg
6220
10
08/29/22 10:52
08/30/22 14:38
95-48-7
3&4-Methyl phenol (m&p Cresol)
ND
ug/kg
6220
10
08/29/22 10:52
08/30/22 14:38
15831-10-4
1-Naphthalenamine
ND
ug/kg
12400
10
08/29/22 10:52
08/30/22 14:38
134-32-7
2-Naphthalenamine
ND
ug/kg
12400
10
08/29/22 10:52
08/30/22 14:38
91-59-8
Naphthalene
ND
ug/kg
6220
10
08/29/22 10:52
08/30/22 14:38
91-20-3
1,4-Naphthoquinone
ND
ug/kg
31100
10
08/29/22 10:52
08/30/22 14:38
130-15-4
2-Nitroaniline
ND
ug/kg
31100
10
08/29/22 10:52
08/30/22 14:38
88-74-4
3-Nitroaniline
ND
ug/kg
31100
10
08/29/22 10:52
08/30/22 14:38
99-09-2
4-Nitroaniline
ND
ug/kg
12400
10
08/29/22 10:52
08/30/22 14:38
100-01-6
Nitrobenzene
ND
ug/kg
6220
10
08/29/22 10:52
08/30/22 14:38
98-95-3
REPORT OF LABORATORY ANALYSIS
Qual
IH,L2
IH
This report shall not be reproduced, except in full,
Date: 10/25/2022 02:36 PM without the written consent of Pace Analytical Services, LLC. Page 14 of 165

lceAnalyircal
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: WASTE CHARACTERIZATION
Pace Project No.: 92621331
Sample: GP-1 2-3' Lab ID: 92621331001 Collected: 08/16/22 10:45 Received: 08/17/22 16:15 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters
8270E MSSV Microwave
2-Nitrophenol
4-Nitrophenol
4-Nitroquinoline-n-oxide
5-Nitro-o-toluidine
N-Nitrosodiethylamine
N-Nitrosodimethylamine
N-Nitroso-di-n-butylamine
N-Nitroso-di-n-propylamine
N-Nitrosodiphenylamine
N-Nitrosomethylethylamine
N-Nitrosomorpholine
N-Nitrosopiperidine
N-Nitrosopyrrolidine
n-Octadecane
O,O,O-Triethylphosphorothioate
2,2'-Oxybis(1-chloropropane)
Parathion (Ethyl parathion)
Pentachlorobenzene
Pentachloroethane
Pentachloronitrobenzene
Pentachlorophenol
Phenacetin
Phenanthrene
Phenol
p-Phenylenediamine
Phorate
Phthalic anhydride
2-Picoline
Pronamide
Pyrene
Pyridine
Safrole
Sulfotepp (ThiodiphosphoricAc
Terpineol
1,2,4,5-Tetrachlorobenzene
2,3,4,6-Tetrachlorophenol
Thionazin
O-Toluidine
1,2,4-Trichlorobenzene
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
1,3,5-Trinitrobenzene
Surrogates
2-Fluorobiphenyl (S)
Terphenyl-d14 (S)
Results Units Report Limit DF Prepared Analyzed CAS No. Qual
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
ND
ug/kg
6220
10
08/29/2210:52
08/30/2214:38
88-75-5
ND
ug/kg
31100
10
08/29/2210:52
08/30/2214:38
100-02-7
ND
ug/kg
31100
10
08/29/2210:52
08/30/2214:38
56-57-5
v2
ND
ug/kg
6220
10
08/29/2210:52
08/30/2214:38
99-55-8
ND
ug/kg
6220
10
08/29/2210:52
08/30/2214:38
55-18-5
ND
ug/kg
6220
10
08/29/2210:52
08/30/2214:38
62-75-9
ND
ug/kg
6220
10
08/29/2210:52
08/30/2214:38
924-16-3
ND
ug/kg
6220
10
08/29/2210:52
08/30/2214:38
621-64-7
ND
ug/kg
6220
10
08/29/2210:52
08/30/2214:38
86-30-6
ND
ug/kg
6220
10
08/29/2210:52
08/30/2214:38
10595-95-6
ND
ug/kg
6220
10
08/29/2210:52
08/30/2214:38
59-89-2
ND
ug/kg
12400
10
08/29/2210:52
08/30/2214:38
100-75-4
ND
ug/kg
12400
10
08/29/2210:52
08/30/2214:38
930-55-2
ND
ug/kg
6220
10
08/29/2210:52
08/30/2214:38
593-45-3
ND
ug/kg
6220
10
08/29/2210:52
08/30/2214:38
126-68-1
ND
ug/kg
6220
10
08/29/2210:52
08/30/2214:38
108-60-1
ND
ug/kg
6220
10
08/29/2210:52
08/30/2214:38
56-38-2
ND
ug/kg
6220
10
08/29/2210:52
08/30/2214:38
608-93-5
ND
ug/kg
6220
10
08/29/2210:52
08/30/2214:38
76-01-7
ND
ug/kg
6220
10
08/29/2210:52
08/30/2214:38
82-68-8
ND
ug/kg
12400
10
08/29/2210:52
08/30/2214:38
87-86-5
ND
ug/kg
12400
10
08/29/2210:52
08/30/2214:38
62-44-2
ND
ug/kg
6220
10
08/29/2210:52
08/30/2214:38
85-01-8
ND
ug/kg
6220
10
08/29/2210:52
08/30/2214:38
108-95-2
ND
ug/kg
12400
10
08/29/2210:52
08/30/2214:38
106-50-3
IL
ND
ug/kg
6220
10
08/29/2210:52
08/30/2214:38
298-02-2
L2
ND
ug/kg
47100
10
08/29/2210:52
08/30/2214:38
85-44-9
ND
ug/kg
6220
10
08/29/2210:52
08/30/2214:38
109-06-8
ND
ug/kg
12400
10
08/29/2210:52
08/30/2214:38
23950-58-5
ND
ug/kg
6220
10
08/29/2210:52
08/30/2214:38
129-00-0
ND
ug/kg
6220
10
08/29/2210:52
08/30/2214:38
110-86-1
ND
ug/kg
12400
10
08/29/2210:52
08/30/2214:38
94-59-7
ND
ug/kg
6220
10
08/29/2210:52
08/30/2214:38
3689-24-5
ND
ug/kg
6220
10
08/29/2210:52
08/30/2214:38
98-55-5
ND
ug/kg
6220
10
08/29/2210:52
08/30/2214:38
95-94-3
ND
ug/kg
6220
10
08/29/2210:52
08/30/2214:38
58-90-2
ND
ug/kg
6220
10
08/29/2210:52
08/30/2214:38
297-97-2
ND
ug/kg
6220
10
08/29/2210:52
08/30/2214:38
95-53-4
ND
ug/kg
6220
10
08/29/2210:52
08/30/2214:38
120-82-1
ND
ug/kg
6220
10
08/29/2210:52
08/30/2214:38
95-95-4
ND
ug/kg
6220
10
08/29/2210:52
08/30/2214:38
88-06-2
ND
ug/kg
6220
10
08/29/2210:52
08/30/2214:38
99-35-4
0
%
19-130
10
08/29/2210:52
08/30/2214:38
321-60-8
D3,S4
0
%
15-130
10
08/29/2210:52
08/30/2214:38
1718-51-0
S4
REPORT
OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/25/2022 02:36 PM without the written consent of Pace Analytical Services, LLC. Page 15 of 165

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: WASTE CHARACTERIZATION
Pace Project No.: 92621331
Sample: GP-1 2-3'
Lab ID: 92621331001 Collected: 08/16/22 10:45 Received: 08/17/22 16:15 Matrix: Solid
Results reported on a "dry weight"
basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters
Results Units Report Limit DF Prepared
Analyzed
CAS No. Qual
8270E MSSV Microwave
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
Surrogates
Phenol-d6 (S)
0 % 18-130 10 08/29/22 10:52
08/30/22 14:38
13127-88-3 S4
2-Fluorophenol (S)
0 % 18-130 10 08/29/22 10:52
08/30/22 14:38
367-12-4 S4
2,4,6-Tribromophenol (S)
0 % 18-130 10 08/29/22 10:52
08/30/22 14:38
118-79-6 S4
Nitrobenzene-d5 (S)
0 % 21-130 10 08/29/22 10:52
08/30/22 14:38
4165-60-0 S4
Percent Moisture
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
46.2 % 0.10 1
08/22/22 15:39
N2
1010 Flash poi nt,Closed Cup
Analytical Method: EPA 1010B
Pace Analytical Services -Asheville
Flashpoint
>200 deg F 70.0 1
08/22/22 11:23
Total Solids 2540 G-2011
Analytical Method: SM 2540G Preparation Method: SM 2540 G
Pace National - Mt. Juliet
Total Solids
54.1 % 1 08/23/22 10:37
08/23/22 10:58
4500S21) Sulfide Soil
Analytical Method: SM 4500-S2D-2011 Modified Preparation Method: SM
4500-S2D-2011 Modified
Pace Analytical Services -Asheville
Sulfide
ND mg/kg 9.0 1 08/20/22 02:37
08/20/22 06:37
18496-25-8
9045 pH Soil
Analytical Method: EPA 9045D
Pace Analytical Services -Asheville
pH at 25 Degrees C
6.4 Std. Units 0.10 1
08/23/22 18:01
H3
9012 Cyanide, Total
Analytical Method: EPA 9012 Preparation Method: EPA 9012
Pace Analytical Services - Ormond Beach
Cyanide
5.1 mg/kg 4.6 10 08/29/2209:41
08/29/2215:14
57-12-5 M1,R1
Date: 10/25/2022 02:36 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 16 of 165

lceAnalyircal
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: WASTE CHARACTERIZATION
Pace Project No.: 92621331
Sample: GP-2 2-3' Lab ID: 92621331002 Collected: 08/16/22 10:55 Received: 08/17/22 16:15 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
OP Pesticides 8141 B
Analytical Method: EPA 8141 B Preparation Method: 3546
Pace National
- Mt. Juliet
Azinphos, methyl (Guthion)
ND
mg/kg
0.195
1
08/21/22 16:12
08/22/22 02:03
86-50-0
Bolstar
ND
mg/kg
0.195
1
08/21/22 16:12
08/22/22 02:03
35400-43-2
Chlorpyrifos
ND
mg/kg
0.195
1
08/21/22 16:12
08/22/22 02:03
2921-88-2
Coumaphos
ND
mg/kg
0.195
1
08/21/22 16:12
08/22/22 02:03
56-72-4
Total Demeton
ND
mg/kg
0.137
1
08/21/22 16:12
08/22/22 02:03
8065-48-3
Diazinon
ND
mg/kg
0.195
1
08/21/22 16:12
08/22/22 02:03
333-41-5
Dichlorvos
ND
mg/kg
0.195
1
08/21/22 16:12
08/22/22 02:03
62-73-7
Dimethoate
ND
mg/kg
0.195
1
08/21/22 16:12
08/22/22 02:03
60-51-5
Disulfoton
ND
mg/kg
0.195
1
08/21/22 16:12
08/22/22 02:03
298-04-4
EPN (ENT)
ND
mg/kg
0.195
1
08/21/22 16:12
08/22/22 02:03
2104-64-5
Ethoprop
ND
mg/kg
0.195
1
08/21/22 16:12
08/22/22 02:03
13194-48-4
Parathion (Ethyl parathion)
ND
mg/kg
0.195
1
08/21/22 16:12
08/22/22 02:03
56-38-2
Fensulfothion
ND
mg/kg
0.195
1
08/21/22 16:12
08/22/22 02:03
115-90-2
Fenthion
ND
mg/kg
0.195
1
08/21/22 16:12
08/22/22 02:03
55-38-9
Malathion
ND
mg/kg
0.195
1
08/21/22 16:12
08/22/22 02:03
121-75-5
Merphos
ND
mg/kg
0.195
1
08/21/22 16:12
08/22/22 02:03
150-50-5
Methyl parathion
ND
mg/kg
0.195
1
08/21/22 16:12
08/22/22 02:03
298-00-0
Mevinphos
ND
mg/kg
0.195
1
08/21/22 16:12
08/22/22 02:03
7786-34-7
Naled
ND
mg/kg
0.195
1
08/21/22 16:12
08/22/22 02:03
300-76-5
Phorate
ND
mg/kg
0.195
1
08/21/22 16:12
08/22/22 02:03
298-02-2
Ronnel
ND
mg/kg
0.195
1
08/21/22 16:12
08/22/22 02:03
299-84-3
Stirophos (Tetrachlorvinphos)
ND
mg/kg
0.195
1
08/21/22 16:12
08/22/22 02:03
22248-79-9
Sulfotepp (ThiodiphosphoricAc
ND
mg/kg
0.195
1
08/21/22 16:12
08/22/22 02:03
3689-24-5
TEPP
ND
mg/kg
1.95
1
08/21/22 16:12
08/22/22 02:03
107-49-3
Tokuthion (Prothiofos)
ND
mg/kg
0.195
1
08/21/22 16:12
08/22/22 02:03
34643-46-4
Trichloronate
ND
mg/kg
0.195
1
08/21/22 16:12
08/22/22 02:03
327-98-0
Surrogates
Triphenyl phosphate (S)
58.7
%
36.0-121
1
08/21/22 16:12
08/22/22 02:03
115-86-6
8081 GCS Pesticides
Analytical Method: EPA 8081 B Preparation Method: EPA 3546
Pace Analytical
Services - Charlotte
Aldrin
ND
ug/kg
36.4
10
08/24/22 07:17
08/26/22 18:04
309-00-2
alpha-BHC
ND
ug/kg
36.4
10
08/24/22 07:17
08/26/22 18:04
319-84-6
beta-BHC
ND
ug/kg
36.4
10
08/24/22 07:17
08/26/22 18:04
319-85-7
delta-BHC
ND
ug/kg
36.4
10
08/24/22 07:17
08/26/22 18:04
319-86-8
gamma-BHC (Lindane)
ND
ug/kg
36.4
10
08/24/22 07:17
08/26/22 18:04
58-89-9
Chlordane (Technical)
583
ug/kg
182
10
08/24/22 07:17
08/26/22 18:04
57-74-9
4,4'-DDD
ND
ug/kg
36.4
10
08/24/22 07:17
08/26/22 18:04
72-54-8
4,4'-DDE
236
ug/kg
36.4
10
08/24/22 07:17
08/26/22 18:04
72-55-9
4,4'-DDT
147
ug/kg
36.4
10
08/24/22 07:17
08/26/22 18:04
50-29-3
Dieldrin
ND
ug/kg
36.4
10
08/24/22 07:17
08/26/22 18:04
60-57-1
Endosulfan I
ND
ug/kg
36.4
10
08/24/22 07:17
08/26/22 18:04
959-98-8
Endosulfan II
ND
ug/kg
36.4
10
08/24/22 07:17
08/26/22 18:04
33213-65-9
Endosulfan sulfate
ND
ug/kg
36.4
10
08/24/22 07:17
08/26/22 18:04
1031-07-8
Endrin
ND
ug/kg
36.4
10
08/24/22 07:17
08/26/22 18:04
72-20-8
REPORT OF LABORATORY ANALYSIS
LO
This report shall not be reproduced, except in full,
Date: 10/25/2022 02:36 PM without the written consent of Pace Analytical Services, LLC. Page 17 of 165

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: WASTE CHARACTERIZATION
Pace Project No.: 92621331
Sample: GP-2 2-3' Lab ID: 92621331002 Collected: 08/16/22 10:55 Received: 08/17/22 16:15 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8081 GCS Pesticides
Endrin aldehyde
Endrin ketone
Heptachlor
Heptachlor epoxide
Hexachlorobenzene
Methoxychlor
Mirex
Toxaphene
Surrogates
Tetrachloro-m-xylene (S)
Decachlorobiphenyl (S)
8082 GCS PCB
PCB-1016 (Aroclor 1016)
PCB-1221 (Aroclor 1221)
PCB-1232 (Aroclor 1232)
PCB-1242 (Aroclor 1242)
PCB-1248 (Aroclor 1248)
PCB-1254 (Aroclor 1254)
PCB-1260 (Aroclor 1260)
Surrogates
Decachlorobiphenyl (S)
Analytical Method: EPA 8081 B Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
ND
ug/kg
36.4
10
08/24/22 07:17
08/26/22 18:04
7421-93-4
ND
ug/kg
36.4
10
08/24/22 07:17
08/26/22 18:04
53494-70-5
ND
ug/kg
36.4
10
08/24/22 07:17
08/26/22 18:04
76-44-8
ND
ug/kg
36.4
10
08/24/22 07:17
08/26/22 18:04
1024-57-3
ND
ug/kg
36.4
10
08/24/22 07:17
08/26/22 18:04
118-74-1
ND
ug/kg
91.0
10
08/24/22 07:17
08/26/22 18:04
72-43-5
ND
ug/kg
91.0
10
08/24/22 07:17
08/26/22 18:04
2385-85-5
ND
ug/kg
127
10
08/24/22 07:17
08/26/22 18:04
8001-35-2
0
%
10-133
10
08/24/22 07:17
08/26/22 18:04
877-09-8 D3,S4
0
%
10-146
10
08/24/22 07:17
08/26/22 18:04
2051-24-3 S4
Analytical Method: EPA 8082A Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
ND
ug/kg
60.1
1
08/19/22 15:53
08/24/22 06:05
12674-11-2
ND
ug/kg
60.1
1
08/19/22 15:53
08/24/22 06:05
11104-28-2
ND
ug/kg
60.1
1
08/19/22 15:53
08/24/22 06:05
11141-16-5
ND
ug/kg
60.1
1
08/19/22 15:53
08/24/22 06:05
53469-21-9
ND
ug/kg
60.1
1
08/19/22 15:53
08/24/22 06:05
12672-29-6
ND
ug/kg
60.1
1
08/19/22 15:53
08/24/22 06:05
11097-69-1
ND
ug/kg
60.1
1
08/19/22 15:53
08/24/22 06:05
11096-82-5
656
%
10-160
1
08/19/22 15:53
08/24/22 06:05
2051-24-3 S5
6010 MET ICP
Analytical Method: EPA 6010 Preparation Method: EPA 3050
Pace Analytical
Services - Ormond Beach
Tin
168
mg/kg
4.9
1
08/30/2219:03
08/31/2218:12
7440-31-5
6020 MET ICPMS
Analytical Method: EPA 6020 Preparation Method: EPA 3050
Pace Analytical
Services - Ormond Beach
Antimony
317
mg/kg
4.3
20
08/27/22 00:15
08/29/22 10:02
7440-36-0
1g,N2
Arsenic
7.6
mg/kg
2.1
20
08/27/22 00:15
08/29/22 10:02
7440-38-2
1g
Barium
1760
mg/kg
10.7
100
08/27/22 00:15
08/31/22 13:57
7440-39-3
1g
Beryllium
0.51
mg/kg
0.26
20
08/27/22 00:15
08/29/22 10:02
7440-41-7
1g
Cadmium
11.0
mg/kg
0.26
20
08/27/22 00:15
08/31/22 13:55
7440-43-9
1g
Chromium
1820
mg/kg
10.7
100
08/27/22 00:15
08/31/22 13:57
7440-47-3
1g
Cobalt
6.3
mg/kg
2.1
20
08/27/22 00:15
08/29/22 10:02
7440-48-4
1g
Copper
553
mg/kg
4.3
20
08/27/22 00:15
08/31/22 13:55
7440-50-8
1g
Lead
394
mg/kg
2.1
20
08/27/22 00:15
08/31/22 13:55
7439-92-1
1g
Nickel
18.2
mg/kg
2.1
20
08/27/22 00:15
08/29/22 10:02
7440-02-0
1g
Selenium
7.2
mg/kg
2.1
20
08/27/22 00:15
08/31/22 13:55
7782-49-2
1g
Silver
128
mg/kg
1.3
100
08/27/22 00:15
08/31/22 13:57
7440-22-4
1g
Thallium
ND
mg/kg
2.1
20
08/27/22 00:15
08/29/22 10:02
7440-28-0
1g
Vanadium
42.0
mg/kg
2.1
20
08/27/22 00:15
08/29/22 10:02
7440-62-2
1g
Zinc
184
mg/kg
85.8
20
08/27/22 00:15
08/31/22 13:55
7440-66-6
1g
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/25/2022 02:36 PM without the written consent of Pace Analytical Services, LLC. Page 18 of 165

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: WASTE CHARACTERIZATION
Pace Project No.: 92621331
Sample: GP-2 2-3' Lab ID: 92621331002 Collected: 08/16/22 10:55 Received: 08/17/22 16:15 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No
7471 Mercury
Analytical Method: EPA 7471
Preparation Method: EPA 7471
Pace Analytical
Services - Ormond Beach
Mercury
13.7
mg/kg
0.33
20
08/24/22 07:26
08/24/22 12:10
7439-97-6
8270E MSSV Microwave
Analytical Method: EPA 8270E Preparation Method:
EPA 3546
Pace Analytical
Services - Charlotte
Acenaphthene
ND
ug/kg
6110
10
08/29/22 10:52
08/30/22 15:08
83-32-9
Acenaphthylene
ND
ug/kg
6110
10
08/29/22 10:52
08/30/22 15:08
208-96-8
Acetophenone
ND
ug/kg
6110
10
08/29/22 10:52
08/30/22 15:08
98-86-2
2-Acetylaminofluorene
ND
ug/kg
12200
10
08/29/22 10:52
08/30/22 15:08
53-96-3
4-Aminobiphenyl
ND
ug/kg
6110
10
08/29/22 10:52
08/30/22 15:08
92-67-1
Anthracene
ND
ug/kg
6110
10
08/29/22 10:52
08/30/22 15:08
120-12-7
Benzo(a)anthracene
ND
ug/kg
6110
10
08/29/22 10:52
08/30/22 15:08
56-55-3
Benzo(a)pyrene
ND
ug/kg
6110
10
08/29/22 10:52
08/30/22 15:08
50-32-8
Benzo(b)fluoranthene
ND
ug/kg
6110
10
08/29/22 10:52
08/30/22 15:08
205-99-2
Benzo(g,h,i)perylene
ND
ug/kg
6110
10
08/29/22 10:52
08/30/22 15:08
191-24-2
Benzo(k)fluoranthene
ND
ug/kg
6110
10
08/29/22 10:52
08/30/22 15:08
207-08-9
Benzyl alcohol
ND
ug/kg
12200
10
08/29/22 10:52
08/30/22 15:08
100-51-6
bis(2-Chloroethoxy)methane
ND
ug/kg
6110
10
08/29/22 10:52
08/30/22 15:08
111-91-1
bis(2-Chloroethyl) ether
ND
ug/kg
6110
10
08/29/22 10:52
08/30/22 15:08
111-44-4
2-Chloronaphthalene
ND
ug/kg
6110
10
08/29/22 10:52
08/30/22 15:08
91-58-7
2-Chlorophenol
ND
ug/kg
6110
10
08/29/22 10:52
08/30/22 15:08
95-57-8
4-Chlorophenylphenyl ether
ND
ug/kg
6110
10
08/29/22 10:52
08/30/22 15:08
7005-72-3
Chrysene
ND
ug/kg
6110
10
08/29/22 10:52
08/30/22 15:08
218-01-9
n-Decane
ND
ug/kg
6110
10
08/29/22 10:52
08/30/22 15:08
124-18-5
Diallate
ND
ug/kg
6110
10
08/29/22 10:52
08/30/22 15:08
2303-16-4
Dibenz(a,h)anthracene
ND
ug/kg
6110
10
08/29/22 10:52
08/30/22 15:08
53-70-3
Dibenzo(a,e)pyrene
ND
ug/kg
18500
10
08/29/22 10:52
08/30/22 15:08
192-65-4
Dibenzofuran
ND
ug/kg
6110
10
08/29/22 10:52
08/30/22 15:08
132-64-9
2,3-Dibromo-1-propanol phosph
ND
ug/kg
30500
10
08/29/22 10:52
08/30/22 15:08
126-72-7
1,2-Dichlorobenzene
ND
ug/kg
6110
10
08/29/22 10:52
08/30/22 15:08
95-50-1
1,3-Dichlorobenzene
ND
ug/kg
6110
10
08/29/22 10:52
08/30/22 15:08
541-73-1
1,4-Dichlorobenzene
ND
ug/kg
6110
10
08/29/22 10:52
08/30/22 15:08
106-46-7
3,3'-Dichlorobenzidine
ND
ug/kg
12200
10
08/29/22 10:52
08/30/22 15:08
91-94-1
2,4-Dichlorophenol
ND
ug/kg
6110
10
08/29/22 10:52
08/30/22 15:08
120-83-2
2,6-Dichlorophenol
ND
ug/kg
6110
10
08/29/22 10:52
08/30/22 15:08
87-65-0
2,3-Dichloroaniline
ND
ug/kg
6110
10
08/29/22 10:52
08/30/22 15:08
608-27-5
Diethylphthalate
ND
ug/kg
6110
10
08/29/22 10:52
08/30/22 15:08
84-66-2
Dimethoate
ND
ug/kg
12200
10
08/29/22 10:52
08/30/22 15:08
60-51-5
P-Dimethylaminoazobenzene
ND
ug/kg
6110
10
08/29/22 10:52
08/30/22 15:08
60-11-7
7,12-Dimethylbenz(a)anthracene
ND
ug/kg
6110
10
08/29/22 10:52
08/30/22 15:08
57-97-6
3,3'-Dimethylbenzidine
ND
ug/kg
12200
10
08/29/22 10:52
08/30/22 15:08
119-93-7
2,4-Dimethylphenol
ND
ug/kg
6110
10
08/29/22 10:52
08/30/22 15:08
105-67-9
a,a-Dimethylphenylethylamine
ND
ug/kg
30500
10
08/29/22 10:52
08/30/22 15:08
122-09-8
Dimethylphthalate
ND
ug/kg
6110
10
08/29/22 10:52
08/30/22 15:08
131-11-3
Di-n-butylphthalate
ND
ug/kg
6110
10
08/29/22 10:52
08/30/22 15:08
84-74-2
4,6-Dinitro-2-methyl phenol
ND
ug/kg
12200
10
08/29/22 10:52
08/30/22 15:08
534-52-1
REPORT OF LABORATORY ANALYSIS
v1
IL
IL
IH
v1
Qual
This report shall not be reproduced, except in full,
Date: 10/25/2022 02:36 PM without the written consent of Pace Analytical Services, LLC. Page 19 of 165

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: WASTE CHARACTERIZATION
Pace Project No.: 92621331
Sample: GP-2 2-3' Lab ID: 92621331002 Collected: 08/16/22 10:55 Received: 08/17/22 16:15 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No
8270E MSSV Microwave
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical
Services - Charlotte
1,3-Dinitrobenzene
ND
ug/kg
6110
10
08/29/22 10:52
08/30/22 15:08
99-65-0
1,4-Dinitrobenzene
ND
ug/kg
6110
10
08/29/22 10:52
08/30/22 15:08
100-25-4
2,4-Dinitrophenol
ND
ug/kg
30500
10
08/29/22 10:52
08/30/22 15:08
51-28-5
2,4-Dinitrotoluene
ND
ug/kg
6110
10
08/29/22 10:52
08/30/22 15:08
121-14-2
2,6-Dinitrotoluene
ND
ug/kg
6110
10
08/29/22 10:52
08/30/22 15:08
606-20-2
Di-n-octylphthalate
ND
ug/kg
6110
10
08/29/22 10:52
08/30/22 15:08
117-84-0
Dinoseb
ND
ug/kg
12200
10
08/29/22 10:52
08/30/22 15:08
88-85-7
Diphenylamine
ND
ug/kg
6110
10
08/29/22 10:52
08/30/22 15:08
122-39-4
Diphenyl ether (Phenyl ether)
ND
ug/kg
9250
10
08/29/22 10:52
08/30/22 15:08
101-84-8
1,2-Diphenylhydrazine
ND
ug/kg
6110
10
08/29/22 10:52
08/30/22 15:08
122-66-7
Disulfoton
ND
ug/kg
6110
10
08/29/22 10:52
08/30/22 15:08
298-04-4
bis(2- Ethyl hexyl)phthalate
ND
ug/kg
6110
10
08/29/22 10:52
08/30/22 15:08
117-81-7
Ethyl methanesulfonate
ND
ug/kg
12200
10
08/29/22 10:52
08/30/22 15:08
62-50-0
Famphur
ND
ug/kg
12200
10
08/29/22 10:52
08/30/22 15:08
52-85-7
Fluoranthene
ND
ug/kg
6110
10
08/29/22 10:52
08/30/22 15:08
206-44-0
Fluorene
ND
ug/kg
6110
10
08/29/22 10:52
08/30/22 15:08
86-73-7
Hexachloro-1,3-butadiene
ND
ug/kg
6110
10
08/29/22 10:52
08/30/22 15:08
87-68-3
Hexachlorobenzene
ND
ug/kg
6110
10
08/29/22 10:52
08/30/22 15:08
118-74-1
Hexachlorocyclopentadiene
ND
ug/kg
6110
10
08/29/22 10:52
08/30/22 15:08
77-47-4
Hexachloroethane
ND
ug/kg
6110
10
08/29/22 10:52
08/30/22 15:08
67-72-1
Hexachlorophene
ND
ug/kg
61100
10
08/29/22 10:52
08/30/22 15:08
70-30-4
Hexachloropropene
ND
ug/kg
6110
10
08/29/22 10:52
08/30/22 15:08
1888-71-7
Indeno(1,2,3-cd)pyrene
ND
ug/kg
6110
10
08/29/22 10:52
08/30/22 15:08
193-39-5
Isodrin
ND
ug/kg
6110
10
08/29/22 10:52
08/30/22 15:08
465-73-6
Isophorone
ND
ug/kg
6110
10
08/29/22 10:52
08/30/22 15:08
78-59-1
Isosafrole
ND
ug/kg
6110
10
08/29/22 10:52
08/30/22 15:08
120-58-1
Kepone
ND
ug/kg
12200
10
08/29/22 10:52
08/30/22 15:08
143-50-0
Methapyrilene
ND
ug/kg
30500
10
08/29/22 10:52
08/30/22 15:08
91-80-5
3-Methylcholanthrene
ND
ug/kg
6110
10
08/29/22 10:52
08/30/22 15:08
56-49-5
4,4'-Methylene-bis(2-chloroani
ND
ug/kg
12200
10
08/29/22 10:52
08/30/22 15:08
101-14-4
Methyl methanesulfonate
ND
ug/kg
12200
10
08/29/22 10:52
08/30/22 15:08
66-27-3
1-Methylnaphthalene
ND
ug/kg
6110
10
08/29/22 10:52
08/30/22 15:08
90-12-0
2-Methylnaphthalene
ND
ug/kg
6110
10
08/29/22 10:52
08/30/22 15:08
91-57-6
2-Methyl-5-nitroaniline
ND
ug/kg
6110
10
08/29/22 10:52
08/30/22 15:08
99-55-8
Methyl parathion
ND
ug/kg
6110
10
08/29/22 10:52
08/30/22 15:08
298-00-0
2-Methylphenol(o-Cresol)
ND
ug/kg
6110
10
08/29/22 10:52
08/30/22 15:08
95-48-7
3&4-Methyl phenol (m&p Cresol)
ND
ug/kg
6110
10
08/29/22 10:52
08/30/22 15:08
15831-10-4
1-Naphthalenamine
ND
ug/kg
12200
10
08/29/22 10:52
08/30/22 15:08
134-32-7
2-Naphthalenamine
ND
ug/kg
12200
10
08/29/22 10:52
08/30/22 15:08
91-59-8
Naphthalene
ND
ug/kg
6110
10
08/29/22 10:52
08/30/22 15:08
91-20-3
1,4-Naphthoquinone
ND
ug/kg
30500
10
08/29/22 10:52
08/30/22 15:08
130-15-4
2-Nitroaniline
ND
ug/kg
30500
10
08/29/22 10:52
08/30/22 15:08
88-74-4
3-Nitroaniline
ND
ug/kg
30500
10
08/29/22 10:52
08/30/22 15:08
99-09-2
4-Nitroaniline
ND
ug/kg
12200
10
08/29/22 10:52
08/30/22 15:08
100-01-6
Nitrobenzene
ND
ug/kg
6110
10
08/29/22 10:52
08/30/22 15:08
98-95-3
REPORT OF LABORATORY ANALYSIS
Qual
IH,L2
IH
This report shall not be reproduced, except in full,
Date: 10/25/2022 02:36 PM without the written consent of Pace Analytical Services, LLC. Page 20 of 165

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: WASTE CHARACTERIZATION
Pace Project No.: 92621331
Sample: GP-2 2-3' Lab ID: 92621331002 Collected: 08/16/22 10:55 Received: 08/17/22 16:15 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters
8270E MSSV Microwave
2-Nitrophenol
4-Nitrophenol
4-Nitroquinoline-n-oxide
5-Nitro-o-toluidine
N-Nitrosodiethylamine
N-Nitrosodimethylamine
N-Nitroso-di-n-butylamine
N-Nitroso-di-n-propylamine
N-Nitrosodiphenylamine
N-Nitrosomethylethylamine
N-Nitrosomorpholine
N-Nitrosopiperidine
N-Nitrosopyrrolidine
n-Octadecane
O,O,O-Triethylphosphorothioate
2,2'-Oxybis(1-chloropropane)
Parathion (Ethyl parathion)
Pentachlorobenzene
Pentachloroethane
Pentachloronitrobenzene
Pentachlorophenol
Phenacetin
Phenanthrene
Phenol
p-Phenylenediamine
Phorate
Phthalic anhydride
2-Picoline
Pronamide
Pyrene
Pyridine
Safrole
Sulfotepp (ThiodiphosphoricAc
Terpineol
1,2,4,5-Tetrachlorobenzene
2,3,4,6-Tetrachlorophenol
Thionazin
O-Toluidine
1,2,4-Trichlorobenzene
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
1,3,5-Trinitrobenzene
Surrogates
2-Fluorobiphenyl (S)
Terphenyl-d14 (S)
Results Units Report Limit DF Prepared Analyzed CAS No. Qual
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
ND
ug/kg
6110
10
08/29/2210:52
08/30/2215:08
88-75-5
ND
ug/kg
30500
10
08/29/2210:52
08/30/2215:08
100-02-7
ND
ug/kg
30500
10
08/29/2210:52
08/30/2215:08
56-57-5
v2
ND
ug/kg
6110
10
08/29/2210:52
08/30/2215:08
99-55-8
ND
ug/kg
6110
10
08/29/2210:52
08/30/2215:08
55-18-5
ND
ug/kg
6110
10
08/29/2210:52
08/30/2215:08
62-75-9
ND
ug/kg
6110
10
08/29/2210:52
08/30/2215:08
924-16-3
ND
ug/kg
6110
10
08/29/2210:52
08/30/2215:08
621-64-7
ND
ug/kg
6110
10
08/29/2210:52
08/30/2215:08
86-30-6
ND
ug/kg
6110
10
08/29/2210:52
08/30/2215:08
10595-95-6
ND
ug/kg
6110
10
08/29/2210:52
08/30/2215:08
59-89-2
ND
ug/kg
12200
10
08/29/2210:52
08/30/2215:08
100-75-4
ND
ug/kg
12200
10
08/29/2210:52
08/30/2215:08
930-55-2
ND
ug/kg
6110
10
08/29/2210:52
08/30/2215:08
593-45-3
ND
ug/kg
6110
10
08/29/2210:52
08/30/2215:08
126-68-1
ND
ug/kg
6110
10
08/29/2210:52
08/30/2215:08
108-60-1
ND
ug/kg
6110
10
08/29/2210:52
08/30/2215:08
56-38-2
ND
ug/kg
6110
10
08/29/2210:52
08/30/2215:08
608-93-5
ND
ug/kg
6110
10
08/29/2210:52
08/30/2215:08
76-01-7
ND
ug/kg
6110
10
08/29/2210:52
08/30/2215:08
82-68-8
ND
ug/kg
12200
10
08/29/2210:52
08/30/2215:08
87-86-5
ND
ug/kg
12200
10
08/29/2210:52
08/30/2215:08
62-44-2
ND
ug/kg
6110
10
08/29/2210:52
08/30/2215:08
85-01-8
ND
ug/kg
6110
10
08/29/2210:52
08/30/2215:08
108-95-2
ND
ug/kg
12200
10
08/29/2210:52
08/30/2215:08
106-50-3
IL
ND
ug/kg
6110
10
08/29/2210:52
08/30/2215:08
298-02-2
L2
ND
ug/kg
46300
10
08/29/2210:52
08/30/2215:08
85-44-9
ND
ug/kg
6110
10
08/29/2210:52
08/30/2215:08
109-06-8
ND
ug/kg
12200
10
08/29/2210:52
08/30/2215:08
23950-58-5
ND
ug/kg
6110
10
08/29/2210:52
08/30/2215:08
129-00-0
ND
ug/kg
6110
10
08/29/2210:52
08/30/2215:08
110-86-1
ND
ug/kg
12200
10
08/29/2210:52
08/30/2215:08
94-59-7
ND
ug/kg
6110
10
08/29/2210:52
08/30/2215:08
3689-24-5
ND
ug/kg
6110
10
08/29/2210:52
08/30/2215:08
98-55-5
ND
ug/kg
6110
10
08/29/2210:52
08/30/2215:08
95-94-3
ND
ug/kg
6110
10
08/29/2210:52
08/30/2215:08
58-90-2
ND
ug/kg
6110
10
08/29/2210:52
08/30/2215:08
297-97-2
ND
ug/kg
6110
10
08/29/2210:52
08/30/2215:08
95-53-4
ND
ug/kg
6110
10
08/29/2210:52
08/30/2215:08
120-82-1
ND
ug/kg
6110
10
08/29/2210:52
08/30/2215:08
95-95-4
ND
ug/kg
6110
10
08/29/2210:52
08/30/2215:08
88-06-2
ND
ug/kg
6110
10
08/29/2210:52
08/30/2215:08
99-35-4
0
%
19-130
10
08/29/2210:52
08/30/2215:08
321-60-8
D3,S4
0
%
15-130
10
08/29/2210:52
08/30/2215:08
1718-51-0
S4
REPORT
OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/25/2022 02:36 PM without the written consent of Pace Analytical Services, LLC. Page 21 of 165

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: WASTE CHARACTERIZATION
Pace Project No.: 92621331
Sample: GP-2 2-3'
Lab ID: 92621331002 Collected: 08/16/22 10:55 Received: 08/17/22 16:15 Matrix: Solid
Results reported on a "dry weight"
basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters
Results Units Report Limit DF Prepared
Analyzed
CAS No. Qual
8270E MSSV Microwave
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
Surrogates
Phenol-d6 (S)
0 % 18-130 10 08/29/22 10:52
08/30/22 15:08
13127-88-3 S4
2-Fluorophenol (S)
0 % 18-130 10 08/29/22 10:52
08/30/22 15:08
367-12-4 S4
2,4,6-Tribromophenol (S)
0 % 18-130 10 08/29/22 10:52
08/30/22 15:08
118-79-6 S4
Nitrobenzene-d5 (S)
0 % 21-130 10 08/29/22 10:52
08/30/22 15:08
4165-60-0 S4
Percent Moisture
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
45.2 % 0.10 1
08/22/22 15:39
N2
1010 Flash poi nt,Closed Cup
Analytical Method: EPA 1010B
Pace Analytical Services -Asheville
Flashpoint
>200 deg F 70.0 1
08/22/22 11:53
Total Solids 2540 G-2011
Analytical Method: SM 2540G Preparation Method: SM 2540 G
Pace National - Mt. Juliet
Total Solids
51.2 % 1 08/23/22 10:15
08/23/22 10:31
4500S21) Sulfide Soil
Analytical Method: SM 4500-S2D-2011 Modified Preparation Method: SM
4500-S2D-2011 Modified
Pace Analytical Services -Asheville
Sulfide
ND mg/kg 9.0 1 08/20/22 02:37
08/20/22 06:37
18496-25-8
9045 pH Soil
Analytical Method: EPA 9045D
Pace Analytical Services -Asheville
pH at 25 Degrees C
5.2 Std. Units 0.10 1
08/23/22 18:03
H3
9012 Cyanide, Total
Analytical Method: EPA 9012 Preparation Method: EPA 9012
Pace Analytical Services - Ormond Beach
Cyanide
18.6 mg/kg 4.7 10 08/29/22 09:41
08/29/22 15:16
57-12-5
Date: 10/25/2022 02:36 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 22 of 165

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: WASTE CHARACTERIZATION
Pace Project No.: 92621331
Sample: GP-3 2-3' Lab ID: 92621331003 Collected: 08/16/22 11:05 Received: 08/17/22 16:15 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
OP Pesticides 8141 B
Analytical Method: EPA 8141 B Preparation Method: 3546
Pace National
- Mt. Juliet
Azinphos, methyl (Guthion)
ND
mg/kg
0.139
1
08/21/22 16:12
08/22/22 02:37
86-50-0
Bolstar
ND
mg/kg
0.139
1
08/21/22 16:12
08/22/22 02:37
35400-43-2
Chlorpyrifos
ND
mg/kg
0.139
1
08/21/22 16:12
08/22/22 02:37
2921-88-2
Coumaphos
ND
mg/kg
0.139
1
08/21/22 16:12
08/22/22 02:37
56-72-4
Total Demeton
ND
mg/kg
0.0975
1
08/21/22 16:12
08/22/22 02:37
8065-48-3
Diazinon
ND
mg/kg
0.139
1
08/21/22 16:12
08/22/22 02:37
333-41-5
Dichlorvos
ND
mg/kg
0.139
1
08/21/22 16:12
08/22/22 02:37
62-73-7
Dimethoate
ND
mg/kg
0.139
1
08/21/22 16:12
08/22/22 02:37
60-51-5
Disulfoton
ND
mg/kg
0.139
1
08/21/22 16:12
08/22/22 02:37
298-04-4
EPN (ENT)
ND
mg/kg
0.139
1
08/21/22 16:12
08/22/22 02:37
2104-64-5
Ethoprop
ND
mg/kg
0.139
1
08/21/22 16:12
08/22/22 02:37
13194-48-4
Parathion (Ethyl parathion)
ND
mg/kg
0.139
1
08/21/22 16:12
08/22/22 02:37
56-38-2
Fensulfothion
ND
mg/kg
0.139
1
08/21/22 16:12
08/22/22 02:37
115-90-2
Fenthion
ND
mg/kg
0.139
1
08/21/22 16:12
08/22/22 02:37
55-38-9
Malathion
ND
mg/kg
0.139
1
08/21/22 16:12
08/22/22 02:37
121-75-5
Merphos
ND
mg/kg
0.139
1
08/21/22 16:12
08/22/22 02:37
150-50-5
Methyl parathion
ND
mg/kg
0.139
1
08/21/22 16:12
08/22/22 02:37
298-00-0
Mevinphos
ND
mg/kg
0.139
1
08/21/22 16:12
08/22/22 02:37
7786-34-7
Naled
ND
mg/kg
0.139
1
08/21/22 16:12
08/22/22 02:37
300-76-5
Phorate
ND
mg/kg
0.139
1
08/21/22 16:12
08/22/22 02:37
298-02-2
Ronnel
ND
mg/kg
0.139
1
08/21/22 16:12
08/22/22 02:37
299-84-3
Stirophos (Tetrachlorvinphos)
ND
mg/kg
0.139
1
08/21/22 16:12
08/22/22 02:37
22248-79-9
Sulfotepp (ThiodiphosphoricAc
ND
mg/kg
0.139
1
08/21/22 16:12
08/22/22 02:37
3689-24-5
TEPP
ND
mg/kg
1.39
1
08/21/22 16:12
08/22/22 02:37
107-49-3
Tokuthion (Prothiofos)
ND
mg/kg
0.139
1
08/21/22 16:12
08/22/22 02:37
34643-46-4
Trichloronate
ND
mg/kg
0.139
1
08/21/22 16:12
08/22/22 02:37
327-98-0
Surrogates
Triphenyl phosphate (S)
79.6
%
36.0-121
1
08/21/22 16:12
08/22/22 02:37
115-86-6
8081 GCS Pesticides
Analytical Method: EPA 8081 B Preparation Method: EPA 3546
Pace Analytical
Services - Charlotte
alpha-BHC
ND
ug/kg
77.3
20
08/24/22 07:17
08/26/22 18:15
319-84-6
gamma-BHC (Lindane)
ND
ug/kg
77.3
20
08/24/22 07:17
08/26/22 18:15
58-89-9
beta-BHC
ND
ug/kg
77.3
20
08/24/22 07:17
08/26/22 18:15
319-85-7
Heptachlor
ND
ug/kg
77.3
20
08/24/22 07:17
08/26/22 18:15
76-44-8
delta-BHC
ND
ug/kg
77.3
20
08/24/22 07:17
08/26/22 18:15
319-86-8
Aldrin
ND
ug/kg
77.3
20
08/24/22 07:17
08/26/22 18:15
309-00-2
Heptachlor epoxide
ND
ug/kg
77.3
20
08/24/22 07:17
08/26/22 18:15
1024-57-3
Endosulfan I
ND
ug/kg
77.3
20
08/24/22 07:17
08/26/22 18:15
959-98-8
4,4'-DDE
212
ug/kg
77.3
20
08/24/22 07:17
08/26/22 18:15
72-55-9
Dieldrin
ND
ug/kg
77.3
20
08/24/22 07:17
08/26/22 18:15
60-57-1
Endrin
ND
ug/kg
77.3
20
08/24/22 07:17
08/26/22 18:15
72-20-8
4,4'-DDD
ND
ug/kg
77.3
20
08/24/22 07:17
08/26/22 18:15
72-54-8
Endosulfan II
ND
ug/kg
77.3
20
08/24/22 07:17
08/26/22 18:15
33213-65-9
4,4'-DDT
ND
ug/kg
77.3
20
08/24/22 07:17
08/26/22 18:15
50-29-3
REPORT OF LABORATORY ANALYSIS
LO
This report shall not be reproduced, except in full,
Date: 10/25/2022 02:36 PM without the written consent of Pace Analytical Services, LLC. Page 23 of 165

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: WASTE CHARACTERIZATION
Pace Project No.: 92621331
Sample: GP-3 2-3' Lab ID: 92621331003 Collected: 08/16/22 11:05 Received: 08/17/22 16:15 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8081 GCS Pesticides
Endrin aldehyde
Endosulfan sulfate
Methoxychlor
Endrin ketone
Chlordane (Technical)
Toxaphene
Mirex
Hexachlorobenzene
Surrogates
Tetrachloro-m-xylene (S)
Decachlorobiphenyl (S)
8082 GCS PCB
PCB-1016 (Aroclor 1016)
PCB-1221 (Aroclor 1221)
PCB-1232 (Aroclor 1232)
PCB-1242 (Aroclor 1242)
PCB-1248 (Aroclor 1248)
PCB-1254 (Aroclor 1254)
PCB-1260 (Aroclor 1260)
Surrogates
Decachlorobiphenyl (S)
Analytical Method: EPA 8081 B Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
ND
ug/kg
77.3
20
08/24/22 07:17
08/26/22 18:15
7421-93-4
ND
ug/kg
77.3
20
08/24/22 07:17
08/26/22 18:15
1031-07-8
ND
ug/kg
193
20
08/24/22 07:17
08/26/22 18:15
72-43-5
ND
ug/kg
77.3
20
08/24/22 07:17
08/26/22 18:15
53494-70-5
610
ug/kg
386
20
08/24/22 07:17
08/26/22 18:15
57-74-9
ND
ug/kg
270
20
08/24/22 07:17
08/26/22 18:15
8001-35-2
ND
ug/kg
193
20
08/24/22 07:17
08/26/22 18:15
2385-85-5
ND
ug/kg
77.3
20
08/24/22 07:17
08/26/22 18:15
118-74-1
0
%
10-133
20
08/24/22 07:17
08/26/22 18:15
877-09-8 D3,S4
0
%
10-146
20
08/24/22 07:17
08/26/22 18:15
2051-24-3 S4
Analytical Method: EPA 8082A Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
ND
ug/kg
1250
20
08/19/22 15:53
08/24/22 06:19
12674-11-2
ND
ug/kg
1250
20
08/19/22 15:53
08/24/22 06:19
11104-28-2
ND
ug/kg
1250
20
08/19/22 15:53
08/24/22 06:19
11141-16-5
ND
ug/kg
1250
20
08/19/22 15:53
08/24/22 06:19
53469-21-9
ND
ug/kg
1250
20
08/19/22 15:53
08/24/22 06:19
12672-29-6
4810
ug/kg
1250
20
08/19/22 15:53
08/24/22 06:19
11097-69-1
ND
ug/kg
1250
20
08/19/22 15:53
08/24/22 06:19
11096-82-5
0
%
10-160
20
08/19/22 15:53
08/24/22 06:19
2051-24-3 D3,S4
6010 MET ICP
Analytical Method: EPA 6010 Preparation Method: EPA 3050
Pace Analytical
Services - Ormond Beach
Tin
181
mg/kg
5.4
1
08/30/2219:03
08/31/22 18:15
7440-31-5
6020 MET ICPMS
Analytical Method: EPA 6020 Preparation Method: EPA 3050
Pace Analytical
Services - Ormond Beach
Antimony
339
mg/kg
4.1
20
08/27/22 00:15
08/29/22 10:05
7440-36-0
1g,N2
Arsenic
4.9
mg/kg
2.0
20
08/27/22 00:15
08/31/22 14:00
7440-38-2
1g
Barium
1770
mg/kg
10.1
100
08/27/22 00:15
08/31/22 14:02
7440-39-3
1g
Beryllium
0.32
mg/kg
0.24
20
08/27/22 00:15
08/29/22 10:05
7440-41-7
1g
Cadmium
11.0
mg/kg
0.24
20
08/27/22 00:15
08/31/22 14:00
7440-43-9
1g
Chromium
1940
mg/kg
10.1
100
08/27/22 00:15
08/31/22 14:02
7440-47-3
1g
Cobalt
5.2
mg/kg
2.0
20
08/27/22 00:15
08/29/22 10:05
7440-48-4
1g
Copper
558
mg/kg
4.1
20
08/27/22 00:15
08/31/22 14:00
7440-50-8
1g
Lead
388
mg/kg
2.0
20
08/27/22 00:15
08/31/22 14:00
7439-92-1
1g
Nickel
13.9
mg/kg
2.0
20
08/27/22 00:15
08/29/22 10:05
7440-02-0
1g
Selenium
5.7
mg/kg
2.0
20
08/27/22 00:15
08/31/22 14:00
7782-49-2
1g
Silver
130
mg/kg
1.2
100
08/27/22 00:15
08/31/22 14:02
7440-22-4
1g
Thallium
ND
mg/kg
2.0
20
08/27/22 00:15
08/29/22 10:05
7440-28-0
1g
Vanadium
33.9
mg/kg
2.0
20
08/27/22 00:15
08/29/22 10:05
7440-62-2
1g
Zinc
174
mg/kg
81.0
20
08/27/22 00:15
08/31/22 14:00
7440-66-6
1g
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/25/2022 02:36 PM without the written consent of Pace Analytical Services, LLC. Page 24 of 165

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: WASTE CHARACTERIZATION
Pace Project No.: 92621331
Sample: GP-3 2-3' Lab ID: 92621331003 Collected: 08/16/22 11:05 Received: 08/17/22 16:15 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
7471 Mercury Analytical Method: EPA 7471 Preparation Method: EPA 7471
Pace Analytical Services - Ormond Beach
Mercury 14.0 mg/kg 0.37 20 08/24/22 07:26 08/24/22 11:25 7439-97-6
8270E MSSV Microwave
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical
Services - Charlotte
Acenaphthene
ND
ug/kg
6370
10
08/29/22 10:52
08/30/22 15:38
83-32-9
Acenaphthylene
ND
ug/kg
6370
10
08/29/22 10:52
08/30/22 15:38
208-96-8
Acetophenone
ND
ug/kg
6370
10
08/29/22 10:52
08/30/22 15:38
98-86-2
2-Acetylaminofluorene
ND
ug/kg
12700
10
08/29/22 10:52
08/30/22 15:38
53-96-3
4-Aminobiphenyl
ND
ug/kg
6370
10
08/29/22 10:52
08/30/22 15:38
92-67-1
Anthracene
ND
ug/kg
6370
10
08/29/22 10:52
08/30/22 15:38
120-12-7
Benzo(a)anthracene
ND
ug/kg
6370
10
08/29/22 10:52
08/30/22 15:38
56-55-3
Benzo(a)pyrene
ND
ug/kg
6370
10
08/29/22 10:52
08/30/22 15:38
50-32-8
Benzo(b)fluoranthene
ND
ug/kg
6370
10
08/29/22 10:52
08/30/22 15:38
205-99-2
Benzo(g,h,i)perylene
ND
ug/kg
6370
10
08/29/22 10:52
08/30/22 15:38
191-24-2
Benzo(k)fluoranthene
ND
ug/kg
6370
10
08/29/22 10:52
08/30/22 15:38
207-08-9
Benzyl alcohol
ND
ug/kg
12700
10
08/29/22 10:52
08/30/22 15:38
100-51-6
bis(2-Chloroethoxy)methane
ND
ug/kg
6370
10
08/29/22 10:52
08/30/22 15:38
111-91-1
bis(2-Chloroethyl) ether
ND
ug/kg
6370
10
08/29/22 10:52
08/30/22 15:38
111-44-4
2-Chloronaphthalene
ND
ug/kg
6370
10
08/29/22 10:52
08/30/22 15:38
91-58-7
2-Chlorophenol
ND
ug/kg
6370
10
08/29/22 10:52
08/30/22 15:38
95-57-8
4-Chlorophenylphenyl ether
ND
ug/kg
6370
10
08/29/22 10:52
08/30/22 15:38
7005-72-3
Chrysene
ND
ug/kg
6370
10
08/29/22 10:52
08/30/22 15:38
218-01-9
n-Decane
ND
ug/kg
6370
10
08/29/22 10:52
08/30/22 15:38
124-18-5
Diallate
ND
ug/kg
6370
10
08/29/22 10:52
08/30/22 15:38
2303-16-4
Dibenz(a,h)anthracene
ND
ug/kg
6370
10
08/29/22 10:52
08/30/22 15:38
53-70-3
Dibenzo(a,e)pyrene
ND
ug/kg
19300
10
08/29/22 10:52
08/30/22 15:38
192-65-4
Dibenzofuran
ND
ug/kg
6370
10
08/29/22 10:52
08/30/22 15:38
132-64-9
2,3-Dibromo-1-propanol phosph
ND
ug/kg
31900
10
08/29/22 10:52
08/30/22 15:38
126-72-7
1,2-Dichlorobenzene
ND
ug/kg
6370
10
08/29/22 10:52
08/30/22 15:38
95-50-1
1,3-Dichlorobenzene
ND
ug/kg
6370
10
08/29/22 10:52
08/30/22 15:38
541-73-1
1,4-Dichlorobenzene
ND
ug/kg
6370
10
08/29/22 10:52
08/30/22 15:38
106-46-7
3,3'-Dichlorobenzidine
ND
ug/kg
12700
10
08/29/22 10:52
08/30/22 15:38
91-94-1
2,4-Dichlorophenol
ND
ug/kg
6370
10
08/29/22 10:52
08/30/22 15:38
120-83-2
2,6-Dichlorophenol
ND
ug/kg
6370
10
08/29/22 10:52
08/30/22 15:38
87-65-0
2,3-Dichloroaniline
ND
ug/kg
6370
10
08/29/22 10:52
08/30/22 15:38
608-27-5
Diethylphthalate
ND
ug/kg
6370
10
08/29/22 10:52
08/30/22 15:38
84-66-2
Dimethoate
ND
ug/kg
12700
10
08/29/22 10:52
08/30/22 15:38
60-51-5
P-Dimethylaminoazobenzene
ND
ug/kg
6370
10
08/29/22 10:52
08/30/22 15:38
60-11-7
7,12-Dimethylbenz(a)anthracene
ND
ug/kg
6370
10
08/29/22 10:52
08/30/22 15:38
57-97-6
3,3'-Dimethylbenzidine
ND
ug/kg
12700
10
08/29/22 10:52
08/30/22 15:38
119-93-7
2,4-Dimethylphenol
ND
ug/kg
6370
10
08/29/22 10:52
08/30/22 15:38
105-67-9
a,a-Dimethylphenylethylamine
ND
ug/kg
31900
10
08/29/22 10:52
08/30/22 15:38
122-09-8
Dimethylphthalate
ND
ug/kg
6370
10
08/29/22 10:52
08/30/22 15:38
131-11-3
Di-n-butylphthalate
ND
ug/kg
6370
10
08/29/22 10:52
08/30/22 15:38
84-74-2
4,6-Dinitro-2-methyl phenol
ND
ug/kg
12700
10
08/29/22 10:52
08/30/22 15:38
534-52-1
REPORT OF LABORATORY ANALYSIS
v1
IL
IL
IH
v1
This report shall not be reproduced, except in full,
Date: 10/25/2022 02:36 PM without the written consent of Pace Analytical Services, LLC. Page 25 of 165

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: WASTE CHARACTERIZATION
Pace Project No.: 92621331
Sample: GP-3 2-3' Lab ID: 92621331003 Collected: 08/16/22 11:05 Received: 08/17/22 16:15 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No
8270E MSSV Microwave
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical
Services - Charlotte
1,3-Dinitrobenzene
ND
ug/kg
6370
10
08/29/22 10:52
08/30/22 15:38
99-65-0
1,4-Dinitrobenzene
ND
ug/kg
6370
10
08/29/22 10:52
08/30/22 15:38
100-25-4
2,4-Dinitrophenol
ND
ug/kg
31900
10
08/29/22 10:52
08/30/22 15:38
51-28-5
2,4-Dinitrotoluene
ND
ug/kg
6370
10
08/29/22 10:52
08/30/22 15:38
121-14-2
2,6-Dinitrotoluene
ND
ug/kg
6370
10
08/29/22 10:52
08/30/22 15:38
606-20-2
Di-n-octylphthalate
ND
ug/kg
6370
10
08/29/22 10:52
08/30/22 15:38
117-84-0
Dinoseb
ND
ug/kg
12700
10
08/29/22 10:52
08/30/22 15:38
88-85-7
Diphenylamine
ND
ug/kg
6370
10
08/29/22 10:52
08/30/22 15:38
122-39-4
Diphenyl ether (Phenyl ether)
ND
ug/kg
9660
10
08/29/22 10:52
08/30/22 15:38
101-84-8
1,2-Diphenylhydrazine
ND
ug/kg
6370
10
08/29/22 10:52
08/30/22 15:38
122-66-7
Disulfoton
ND
ug/kg
6370
10
08/29/22 10:52
08/30/22 15:38
298-04-4
bis(2- Ethyl hexyl)phthalate
ND
ug/kg
6370
10
08/29/22 10:52
08/30/22 15:38
117-81-7
Ethyl methanesulfonate
ND
ug/kg
12700
10
08/29/22 10:52
08/30/22 15:38
62-50-0
Famphur
ND
ug/kg
12700
10
08/29/22 10:52
08/30/22 15:38
52-85-7
Fluoranthene
ND
ug/kg
6370
10
08/29/22 10:52
08/30/22 15:38
206-44-0
Fluorene
ND
ug/kg
6370
10
08/29/22 10:52
08/30/22 15:38
86-73-7
Hexachloro-1,3-butadiene
ND
ug/kg
6370
10
08/29/22 10:52
08/30/22 15:38
87-68-3
Hexachlorobenzene
ND
ug/kg
6370
10
08/29/22 10:52
08/30/22 15:38
118-74-1
Hexachlorocyclopentadiene
ND
ug/kg
6370
10
08/29/22 10:52
08/30/22 15:38
77-47-4
Hexachloroethane
ND
ug/kg
6370
10
08/29/22 10:52
08/30/22 15:38
67-72-1
Hexachlorophene
ND
ug/kg
63700
10
08/29/22 10:52
08/30/22 15:38
70-30-4
Hexachloropropene
ND
ug/kg
6370
10
08/29/22 10:52
08/30/22 15:38
1888-71-7
Indeno(1,2,3-cd)pyrene
ND
ug/kg
6370
10
08/29/22 10:52
08/30/22 15:38
193-39-5
Isodrin
ND
ug/kg
6370
10
08/29/22 10:52
08/30/22 15:38
465-73-6
Isophorone
ND
ug/kg
6370
10
08/29/22 10:52
08/30/22 15:38
78-59-1
Isosafrole
ND
ug/kg
6370
10
08/29/22 10:52
08/30/22 15:38
120-58-1
Kepone
ND
ug/kg
12700
10
08/29/22 10:52
08/30/22 15:38
143-50-0
Methapyrilene
ND
ug/kg
31900
10
08/29/22 10:52
08/30/22 15:38
91-80-5
3-Methylcholanthrene
ND
ug/kg
6370
10
08/29/22 10:52
08/30/22 15:38
56-49-5
4,4'-Methylene-bis(2-chloroani
ND
ug/kg
12700
10
08/29/22 10:52
08/30/22 15:38
101-14-4
Methyl methanesulfonate
ND
ug/kg
12700
10
08/29/22 10:52
08/30/22 15:38
66-27-3
1-Methylnaphthalene
ND
ug/kg
6370
10
08/29/22 10:52
08/30/22 15:38
90-12-0
2-Methylnaphthalene
ND
ug/kg
6370
10
08/29/22 10:52
08/30/22 15:38
91-57-6
2-Methyl-5-nitroaniline
ND
ug/kg
6370
10
08/29/22 10:52
08/30/22 15:38
99-55-8
Methyl parathion
ND
ug/kg
6370
10
08/29/22 10:52
08/30/22 15:38
298-00-0
2-Methylphenol(o-Cresol)
ND
ug/kg
6370
10
08/29/22 10:52
08/30/22 15:38
95-48-7
3&4-Methyl phenol (m&p Cresol)
ND
ug/kg
6370
10
08/29/22 10:52
08/30/22 15:38
15831-10-4
1-Naphthalenamine
ND
ug/kg
12700
10
08/29/22 10:52
08/30/22 15:38
134-32-7
2-Naphthalenamine
ND
ug/kg
12700
10
08/29/22 10:52
08/30/22 15:38
91-59-8
Naphthalene
ND
ug/kg
6370
10
08/29/22 10:52
08/30/22 15:38
91-20-3
1,4-Naphthoquinone
ND
ug/kg
31900
10
08/29/22 10:52
08/30/22 15:38
130-15-4
2-Nitroaniline
ND
ug/kg
31900
10
08/29/22 10:52
08/30/22 15:38
88-74-4
3-Nitroaniline
ND
ug/kg
31900
10
08/29/22 10:52
08/30/22 15:38
99-09-2
4-Nitroaniline
ND
ug/kg
12700
10
08/29/22 10:52
08/30/22 15:38
100-01-6
Nitrobenzene
ND
ug/kg
6370
10
08/29/22 10:52
08/30/22 15:38
98-95-3
REPORT OF LABORATORY ANALYSIS
Qual
IH,L2
IH
This report shall not be reproduced, except in full,
Date: 10/25/2022 02:36 PM without the written consent of Pace Analytical Services, LLC. Page 26 of 165

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: WASTE CHARACTERIZATION
Pace Project No.: 92621331
Sample: GP-3 2-3' Lab ID: 92621331003 Collected: 08/16/22 11:05 Received: 08/17/22 16:15 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters
8270E MSSV Microwave
2-Nitrophenol
4-Nitrophenol
4-Nitroquinoline-n-oxide
5-Nitro-o-toluidine
N-Nitrosodiethylamine
N-Nitrosodimethylamine
N-Nitroso-di-n-butylamine
N-Nitroso-di-n-propylamine
N-Nitrosodiphenylamine
N-Nitrosomethylethylamine
N-Nitrosomorpholine
N-Nitrosopiperidine
N-Nitrosopyrrolidine
n-Octadecane
O,O,O-Triethylphosphorothioate
2,2'-Oxybis(1-chloropropane)
Parathion (Ethyl parathion)
Pentachlorobenzene
Pentachloroethane
Pentachloronitrobenzene
Pentachlorophenol
Phenacetin
Phenanthrene
Phenol
p-Phenylenediamine
Phorate
Phthalic anhydride
2-Picoline
Pronamide
Pyrene
Pyridine
Safrole
Sulfotepp (ThiodiphosphoricAc
Terpineol
1,2,4,5-Tetrachlorobenzene
2,3,4,6-Tetrachlorophenol
Thionazin
O-Toluidine
1,2,4-Trichlorobenzene
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
1,3,5-Trinitrobenzene
Surrogates
2-Fluorobiphenyl (S)
Terphenyl-d14 (S)
Results Units Report Limit DF Prepared Analyzed CAS No. Qual
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
ND
ug/kg
6370
10
08/29/2210:52
08/30/2215:38
88-75-5
ND
ug/kg
31900
10
08/29/2210:52
08/30/2215:38
100-02-7
ND
ug/kg
31900
10
08/29/2210:52
08/30/2215:38
56-57-5
v2
ND
ug/kg
6370
10
08/29/2210:52
08/30/2215:38
99-55-8
ND
ug/kg
6370
10
08/29/2210:52
08/30/2215:38
55-18-5
ND
ug/kg
6370
10
08/29/2210:52
08/30/2215:38
62-75-9
ND
ug/kg
6370
10
08/29/2210:52
08/30/2215:38
924-16-3
ND
ug/kg
6370
10
08/29/2210:52
08/30/2215:38
621-64-7
ND
ug/kg
6370
10
08/29/2210:52
08/30/2215:38
86-30-6
ND
ug/kg
6370
10
08/29/2210:52
08/30/2215:38
10595-95-6
ND
ug/kg
6370
10
08/29/2210:52
08/30/2215:38
59-89-2
ND
ug/kg
12700
10
08/29/2210:52
08/30/2215:38
100-75-4
ND
ug/kg
12700
10
08/29/2210:52
08/30/2215:38
930-55-2
ND
ug/kg
6370
10
08/29/2210:52
08/30/2215:38
593-45-3
ND
ug/kg
6370
10
08/29/2210:52
08/30/2215:38
126-68-1
ND
ug/kg
6370
10
08/29/2210:52
08/30/2215:38
108-60-1
ND
ug/kg
6370
10
08/29/2210:52
08/30/2215:38
56-38-2
ND
ug/kg
6370
10
08/29/2210:52
08/30/2215:38
608-93-5
ND
ug/kg
6370
10
08/29/2210:52
08/30/2215:38
76-01-7
ND
ug/kg
6370
10
08/29/2210:52
08/30/2215:38
82-68-8
ND
ug/kg
12700
10
08/29/2210:52
08/30/2215:38
87-86-5
ND
ug/kg
12700
10
08/29/2210:52
08/30/2215:38
62-44-2
ND
ug/kg
6370
10
08/29/2210:52
08/30/2215:38
85-01-8
ND
ug/kg
6370
10
08/29/2210:52
08/30/2215:38
108-95-2
ND
ug/kg
12700
10
08/29/2210:52
08/30/2215:38
106-50-3
IL
ND
ug/kg
6370
10
08/29/2210:52
08/30/2215:38
298-02-2
L2
ND
ug/kg
48300
10
08/29/2210:52
08/30/2215:38
85-44-9
ND
ug/kg
6370
10
08/29/2210:52
08/30/2215:38
109-06-8
ND
ug/kg
12700
10
08/29/2210:52
08/30/2215:38
23950-58-5
ND
ug/kg
6370
10
08/29/2210:52
08/30/2215:38
129-00-0
ND
ug/kg
6370
10
08/29/2210:52
08/30/2215:38
110-86-1
ND
ug/kg
12700
10
08/29/2210:52
08/30/2215:38
94-59-7
ND
ug/kg
6370
10
08/29/2210:52
08/30/2215:38
3689-24-5
ND
ug/kg
6370
10
08/29/2210:52
08/30/2215:38
98-55-5
ND
ug/kg
6370
10
08/29/2210:52
08/30/2215:38
95-94-3
ND
ug/kg
6370
10
08/29/2210:52
08/30/2215:38
58-90-2
ND
ug/kg
6370
10
08/29/2210:52
08/30/2215:38
297-97-2
ND
ug/kg
6370
10
08/29/2210:52
08/30/2215:38
95-53-4
ND
ug/kg
6370
10
08/29/2210:52
08/30/2215:38
120-82-1
ND
ug/kg
6370
10
08/29/2210:52
08/30/2215:38
95-95-4
ND
ug/kg
6370
10
08/29/2210:52
08/30/2215:38
88-06-2
ND
ug/kg
6370
10
08/29/2210:52
08/30/2215:38
99-35-4
0
%
19-130
10
08/29/2210:52
08/30/2215:38
321-60-8
D3,S4
0
%
15-130
10
08/29/2210:52
08/30/2215:38
1718-51-0
S4
REPORT
OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/25/2022 02:36 PM without the written consent of Pace Analytical Services, LLC. Page 27 of 165

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: WASTE CHARACTERIZATION
Pace Project No.: 92621331
Sample: GP-3 2-3'
Lab ID: 92621331003 Collected: 08/16/22 11:05 Received: 08/17/22 16:15 Matrix: Solid
Results reported on a "dry weight"
basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters
Results Units Report Limit DF Prepared
Analyzed
CAS No. Qual
8270E MSSV Microwave
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
Surrogates
Phenol-d6 (S)
0 % 18-130 10 08/29/22 10:52
08/30/22 15:38
13127-88-3 S4
2-Fluorophenol (S)
0 % 18-130 10 08/29/22 10:52
08/30/22 15:38
367-12-4 S4
2,4,6-Tribromophenol (S)
0 % 18-130 10 08/29/22 10:52
08/30/22 15:38
118-79-6 S4
Nitrobenzene-d5 (S)
0 % 21-130 10 08/29/22 10:52
08/30/22 15:38
4165-60-0 S4
Percent Moisture
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
47.9 % 0.10 1
08/22/22 15:39
N2
1010 Flash poi nt,Closed Cup
Analytical Method: EPA 1010B
Pace Analytical Services -Asheville
Flashpoint
>200 deg F 70.0 1
08/22/22 12:22
Total Solids 2540 G-2011
Analytical Method: SM 2540G Preparation Method: SM 2540 G
Pace National - Mt. Juliet
Total Solids
71.8 % 1 08/23/22 10:15
08/23/22 10:31
4500S21) Sulfide Soil
Analytical Method: SM 4500-S2D-2011 Modified Preparation Method: SM
4500-S2D-2011 Modified
Pace Analytical Services -Asheville
Sulfide
ND mg/kg 9.6 1 08/20/22 02:37
08/20/22 06:38
18496-25-8
9045 pH Soil
Analytical Method: EPA 9045D
Pace Analytical Services -Asheville
pH at 25 Degrees C
4.5 Std. Units 0.10 1
08/23/22 18:04
H3
9012 Cyanide, Total
Analytical Method: EPA 9012 Preparation Method: EPA 9012
Pace Analytical Services - Ormond Beach
Cyanide
21.6 mg/kg 4.8 10 08/29/22 09:41
08/29/22 15:17
57-12-5
Date: 10/25/2022 02:36 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 28 of 165

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: WASTE CHARACTERIZATION
Pace Project No.: 92621331
Sample: GP-4 2-3'
Lab ID: 92621331004
Collected: 08/16/22 11:30
Received: 08/17/22 16:15 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters
Results
Units
Report Limit
DF
Prepared
Analyzed
CAS No. Qual
OP Pesticides 8141 B
Analytical Method:
EPA 8141
B Preparation Method:
3546
Pace National
- Mt. Juliet
Azinphos, methyl (Guthion)
ND
mg/kg
4.58
20
08/21/22 16:12
08/22/22 06:32
86-50-0
Bolstar
ND
mg/kg
4.58
20
08/21/22 16:12
08/22/22 06:32
35400-43-2
Chlorpyrifos
ND
mg/kg
4.58
20
08/21/22 16:12
08/22/22 06:32
2921-88-2
Coumaphos
ND
mg/kg
4.58
20
08/21/22 16:12
08/22/22 06:32
56-72-4
Total Demeton
ND
mg/kg
3.21
20
08/21/22 16:12
08/22/22 06:32
8065-48-3
Diazinon
ND
mg/kg
4.58
20
08/21/22 16:12
08/22/22 06:32
333-41-5
Dichlorvos
ND
mg/kg
4.58
20
08/21/22 16:12
08/22/22 06:32
62-73-7
Dimethoate
ND
mg/kg
4.58
20
08/21/22 16:12
08/22/22 06:32
60-51-5
Disulfoton
ND
mg/kg
4.58
20
08/21/22 16:12
08/22/22 06:32
298-04-4
EPN (ENT)
ND
mg/kg
4.58
20
08/21/22 16:12
08/22/22 06:32
2104-64-5
Ethoprop
ND
mg/kg
4.58
20
08/21/22 16:12
08/22/22 06:32
13194-48-4
Parathion (Ethyl parathion)
ND
mg/kg
4.58
20
08/21/22 16:12
08/22/22 06:32
56-38-2
Fensulfothion
ND
mg/kg
4.58
20
08/21/22 16:12
08/22/22 06:32
115-90-2
Fenthion
ND
mg/kg
4.58
20
08/21/22 16:12
08/22/22 06:32
55-38-9
Malathion
ND
mg/kg
4.58
20
08/21/22 16:12
08/22/22 06:32
121-75-5
Merphos
ND
mg/kg
4.58
20
08/21/22 16:12
08/22/22 06:32
150-50-5
Methyl parathion
ND
mg/kg
4.58
20
08/21/22 16:12
08/22/22 06:32
298-00-0
Mevinphos
ND
mg/kg
4.58
20
08/21/22 16:12
08/22/22 06:32
7786-34-7
Naled
ND
mg/kg
4.58
20
08/21/22 16:12
08/22/22 06:32
300-76-5
Phorate
ND
mg/kg
4.58
20
08/21/22 16:12
08/22/22 06:32
298-02-2
Ronnel
ND
mg/kg
4.58
20
08/21/22 16:12
08/22/22 06:32
299-84-3
Stirophos (Tetrachlorvinphos)
ND
mg/kg
4.58
20
08/21/22 16:12
08/22/22 06:32
22248-79-9
Sulfotepp (ThiodiphosphoricAc
ND
mg/kg
4.58
20
08/21/22 16:12
08/22/22 06:32
3689-24-5
TEPP
ND
mg/kg
45.8
20
08/21/22 16:12
08/22/22 06:32
107-49-3 LO
Tokuthion (Prothiofos)
ND
mg/kg
4.58
20
08/21/22 16:12
08/22/22 06:32
34643-46-4
Trichloronate
ND
mg/kg
4.58
20
08/21/22 16:12
08/22/22 06:32
327-98-0
Surrogates
Triphenyl phosphate (S)
58.1
%
36.0-121
20
08/21/22 16:12
08/22/22 06:32
115-86-6 S4
8081 GCS Pesticides
Analytical Method: EPA 8081
B Preparation Method:
EPA 3546
Pace Analytical
Services -
Charlotte
Aldrin
ND
ug/kg
43.4
10
08/29/22 10:46
08/29/22 15:07
309-00-2
alpha-BHC
ND
ug/kg
43.4
10
08/29/22 10:46
08/29/22 15:07
319-84-6
beta-BHC
ND
ug/kg
43.4
10
08/29/22 10:46
08/29/22 15:07
319-85-7
delta-BHC
ND
ug/kg
43.4
10
08/29/22 10:46
08/29/22 15:07
319-86-8
gamma-BHC (Lindane)
ND
ug/kg
43.4
10
08/29/22 10:46
08/29/22 15:07
58-89-9
Chlordane (Technical)
549
ug/kg
217
10
08/29/22 10:46
08/29/22 15:07
57-74-9
4,4'-DDD
ND
ug/kg
43.4
10
08/29/22 10:46
08/29/22 15:07
72-54-8
4,4'-DDE
ND
ug/kg
43.4
10
08/29/22 10:46
08/29/22 15:07
72-55-9
4,4'-DDT
ND
ug/kg
43.4
10
08/29/22 10:46
08/29/22 15:07
50-29-3
Dieldrin
ND
ug/kg
43.4
10
08/29/22 10:46
08/29/22 15:07
60-57-1
Endosulfan I
ND
ug/kg
43.4
10
08/29/22 10:46
08/29/22 15:07
959-98-8
Endosulfan II
ND
ug/kg
43.4
10
08/29/22 10:46
08/29/22 15:07
33213-65-9
Endosulfan sulfate
ND
ug/kg
43.4
10
08/29/22 10:46
08/29/22 15:07
1031-07-8
Endrin
ND
ug/kg
43.4
10
08/29/22 10:46
08/29/22 15:07
72-20-8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/25/2022 02:36 PM without the written consent of Pace Analytical Services, LLC. Page 29 of 165

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: WASTE CHARACTERIZATION
Pace Project No.: 92621331
Sample: GP-4 2-3' Lab ID: 92621331004 Collected: 08/16/22 11:30 Received: 08/17/22 16:15 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8081 GCS Pesticides
Endrin aldehyde
Endrin ketone
Heptachlor
Heptachlor epoxide
Hexachlorobenzene
Methoxychlor
Mirex
Toxaphene
Surrogates
Tetrachloro-m-xylene (S)
Decachlorobiphenyl (S)
8082 GCS PCB
PCB-1016 (Aroclor 1016)
PCB-1221 (Aroclor 1221)
PCB-1232 (Aroclor 1232)
PCB-1242 (Aroclor 1242)
PCB-1248 (Aroclor 1248)
PCB-1254 (Aroclor 1254)
PCB-1260 (Aroclor 1260)
Surrogates
Decachlorobiphenyl (S)
Analytical Method: EPA 8081 B Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
ND
ug/kg
43.4
10
08/29/2210:46
08/29/2215:07
7421-93-4
ND
ug/kg
43.4
10
08/29/2210:46
08/29/2215:07
53494-70-5
ND
ug/kg
43.4
10
08/29/2210:46
08/29/2215:07
76-44-8
ND
ug/kg
43.4
10
08/29/2210:46
08/29/2215:07
1024-57-3
ND
ug/kg
43.4
10
08/29/2210:46
08/29/2215:07
118-74-1
ND
ug/kg
109
10
08/29/2210:46
08/29/2215:07
72-43-5
ND
ug/kg
109
10
08/29/2210:46
08/29/2215:07
2385-85-5
ND
ug/kg
152
10
08/29/2210:46
08/29/2215:07
8001-35-2
0
%
10-133
10
08/29/2210:46
08/29/2215:07
877-09-8 D3,S4
0
%
10-146
10
08/29/2210:46
08/29/2215:07
2051-24-3 S4
Analytical Method: EPA 8082A Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
ND
ug/kg
90.3
1
08/19/22 15:53
08/24/22 06:34
12674-11-2
ND
ug/kg
90.3
1
08/19/22 15:53
08/24/22 06:34
11104-28-2
ND
ug/kg
90.3
1
08/19/22 15:53
08/24/22 06:34
11141-16-5
ND
ug/kg
90.3
1
08/19/22 15:53
08/24/22 06:34
53469-21-9
ND
ug/kg
90.3
1
08/19/22 15:53
08/24/22 06:34
12672-29-6
ND
ug/kg
90.3
1
08/19/22 15:53
08/24/22 06:34
11097-69-1
ND
ug/kg
90.3
1
08/19/22 15:53
08/24/22 06:34
11096-82-5
174
%
10-160
1
08/19/22 15:53
08/24/22 06:34
2051-24-3 S5
6010 MET ICP
Analytical Method: EPA 6010 Preparation Method: EPA 3050
Pace Analytical
Services - Ormond Beach
Tin
188
mg/kg
6.4
1
08/30/2219:03
08/31/2218:19
7440-31-5
6020 MET ICPMS
Analytical Method: EPA 6020 Preparation Method: EPA 3050
Pace Analytical
Services - Ormond Beach
Antimony
210
mg/kg
5.0
20
08/27/22 00:15
08/29/22 10:08
7440-36-0
1g,N2
Arsenic
3.4
mg/kg
2.5
20
08/27/22 00:15
08/31/22 14:04
7440-38-2
1g
Barium
1310
mg/kg
12.6
100
08/27/22 00:15
08/31/22 14:07
7440-39-3
1g
Beryllium
ND
mg/kg
0.30
20
08/27/22 00:15
08/29/22 10:08
7440-41-7
1g
Cadmium
6.1
mg/kg
0.30
20
08/27/22 00:15
08/31/22 14:04
7440-43-9
1g
Chromium
2960
mg/kg
12.6
100
08/27/22 00:15
08/31/22 14:07
7440-47-3
1g
Cobalt
5.5
mg/kg
2.5
20
08/27/22 00:15
08/29/22 10:08
7440-48-4
1g
Copper
405
mg/kg
5.0
20
08/27/22 00:15
08/31/22 14:04
7440-50-8
1g
Lead
2510
mg/kg
12.6
100
08/27/22 00:15
08/31/22 14:07
7439-92-1
1g
Nickel
7.6
mg/kg
2.5
20
08/27/22 00:15
08/29/22 10:08
7440-02-0
1g
Selenium
7.3
mg/kg
2.5
20
08/27/22 00:15
08/31/22 14:04
7782-49-2
1g
Silver
159
mg/kg
1.5
100
08/27/22 00:15
08/31/22 14:07
7440-22-4
1g
Thallium
ND
mg/kg
2.5
20
08/27/22 00:15
08/29/22 10:08
7440-28-0
1g
Vanadium
27.9
mg/kg
2.5
20
08/27/22 00:15
08/29/22 10:08
7440-62-2
1g
Zinc
143
mg/kg
101
20
08/27/22 00:15
08/31/22 14:04
7440-66-6
1g
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/25/2022 02:36 PM without the written consent of Pace Analytical Services, LLC. Page 30 of 165

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: WASTE CHARACTERIZATION
Pace Project No.: 92621331
Sample: GP-4 2-3' Lab ID: 92621331004 Collected: 08/16/22 11:30 Received: 08/17/22 16:15 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
7471 Mercury Analytical Method: EPA 7471 Preparation Method: EPA 7471
Pace Analytical Services - Ormond Beach
Mercury 9.0 mg/kg 0.19 10 08/24/22 07:26 08/24/22 11:28 7439-97-6
8270E MSSV Microwave
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical
Services - Charlotte
Acenaphthene
ND
ug/kg
7070
10
08/29/22 10:52
08/30/22 16:09
83-32-9
Acenaphthylene
ND
ug/kg
7070
10
08/29/22 10:52
08/30/22 16:09
208-96-8
Acetophenone
ND
ug/kg
7070
10
08/29/22 10:52
08/30/22 16:09
98-86-2
2-Acetylaminofluorene
ND
ug/kg
14100
10
08/29/22 10:52
08/30/22 16:09
53-96-3
4-Aminobiphenyl
ND
ug/kg
7070
10
08/29/22 10:52
08/30/22 16:09
92-67-1
Anthracene
ND
ug/kg
7070
10
08/29/22 10:52
08/30/22 16:09
120-12-7
Benzo(a)anthracene
ND
ug/kg
7070
10
08/29/22 10:52
08/30/22 16:09
56-55-3
Benzo(a)pyrene
ND
ug/kg
7070
10
08/29/22 10:52
08/30/22 16:09
50-32-8
Benzo(b)fluoranthene
ND
ug/kg
7070
10
08/29/22 10:52
08/30/22 16:09
205-99-2
Benzo(g,h,i)perylene
ND
ug/kg
7070
10
08/29/22 10:52
08/30/22 16:09
191-24-2
Benzo(k)fluoranthene
ND
ug/kg
7070
10
08/29/22 10:52
08/30/22 16:09
207-08-9
Benzyl alcohol
ND
ug/kg
14100
10
08/29/22 10:52
08/30/22 16:09
100-51-6
bis(2-Chloroethoxy)methane
ND
ug/kg
7070
10
08/29/22 10:52
08/30/22 16:09
111-91-1
bis(2-Chloroethyl) ether
ND
ug/kg
7070
10
08/29/22 10:52
08/30/22 16:09
111-44-4
2-Chloronaphthalene
ND
ug/kg
7070
10
08/29/22 10:52
08/30/22 16:09
91-58-7
2-Chlorophenol
ND
ug/kg
7070
10
08/29/22 10:52
08/30/22 16:09
95-57-8
4-Chlorophenylphenyl ether
ND
ug/kg
7070
10
08/29/22 10:52
08/30/22 16:09
7005-72-3
Chrysene
ND
ug/kg
7070
10
08/29/22 10:52
08/30/22 16:09
218-01-9
n-Decane
ND
ug/kg
7070
10
08/29/22 10:52
08/30/22 16:09
124-18-5
Diallate
ND
ug/kg
7070
10
08/29/22 10:52
08/30/22 16:09
2303-16-4
Dibenz(a,h)anthracene
ND
ug/kg
7070
10
08/29/22 10:52
08/30/22 16:09
53-70-3
Dibenzo(a,e)pyrene
ND
ug/kg
21400
10
08/29/22 10:52
08/30/22 16:09
192-65-4
Dibenzofuran
ND
ug/kg
7070
10
08/29/22 10:52
08/30/22 16:09
132-64-9
2,3-Dibromo-1-propanol phosph
ND
ug/kg
35300
10
08/29/22 10:52
08/30/22 16:09
126-72-7
1,2-Dichlorobenzene
ND
ug/kg
7070
10
08/29/22 10:52
08/30/22 16:09
95-50-1
1,3-Dichlorobenzene
ND
ug/kg
7070
10
08/29/22 10:52
08/30/22 16:09
541-73-1
1,4-Dichlorobenzene
ND
ug/kg
7070
10
08/29/22 10:52
08/30/22 16:09
106-46-7
3,3'-Dichlorobenzidine
ND
ug/kg
14100
10
08/29/22 10:52
08/30/22 16:09
91-94-1
2,4-Dichlorophenol
ND
ug/kg
7070
10
08/29/22 10:52
08/30/22 16:09
120-83-2
2,6-Dichlorophenol
ND
ug/kg
7070
10
08/29/22 10:52
08/30/22 16:09
87-65-0
2,3-Dichloroaniline
ND
ug/kg
7070
10
08/29/22 10:52
08/30/22 16:09
608-27-5
Diethylphthalate
ND
ug/kg
7070
10
08/29/22 10:52
08/30/22 16:09
84-66-2
Dimethoate
ND
ug/kg
14100
10
08/29/22 10:52
08/30/22 16:09
60-51-5
P-Dimethylaminoazobenzene
ND
ug/kg
7070
10
08/29/22 10:52
08/30/22 16:09
60-11-7
7,12-Dimethylbenz(a)anthracene
ND
ug/kg
7070
10
08/29/22 10:52
08/30/22 16:09
57-97-6
3,3'-Dimethylbenzidine
ND
ug/kg
14100
10
08/29/22 10:52
08/30/22 16:09
119-93-7
2,4-Dimethylphenol
ND
ug/kg
7070
10
08/29/22 10:52
08/30/22 16:09
105-67-9
a,a-Dimethylphenylethylamine
ND
ug/kg
35300
10
08/29/22 10:52
08/30/22 16:09
122-09-8
Dimethylphthalate
ND
ug/kg
7070
10
08/29/22 10:52
08/30/22 16:09
131-11-3
Di-n-butylphthalate
ND
ug/kg
7070
10
08/29/22 10:52
08/30/22 16:09
84-74-2
4,6-Dinitro-2-methyl phenol
ND
ug/kg
14100
10
08/29/22 10:52
08/30/22 16:09
534-52-1
REPORT OF LABORATORY ANALYSIS
v1
IL
IL
IH
v1
This report shall not be reproduced, except in full,
Date: 10/25/2022 02:36 PM without the written consent of Pace Analytical Services, LLC. Page 31 of 165

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: WASTE CHARACTERIZATION
Pace Project No.: 92621331
Sample: GP-4 2-3' Lab ID: 92621331004 Collected: 08/16/22 11:30 Received: 08/17/22 16:15 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No
8270E MSSV Microwave
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical
Services - Charlotte
1,3-Dinitrobenzene
ND
ug/kg
7070
10
08/29/22 10:52
08/30/22 16:09
99-65-0
1,4-Dinitrobenzene
ND
ug/kg
7070
10
08/29/22 10:52
08/30/22 16:09
100-25-4
2,4-Dinitrophenol
ND
ug/kg
35300
10
08/29/22 10:52
08/30/22 16:09
51-28-5
2,4-Dinitrotoluene
ND
ug/kg
7070
10
08/29/22 10:52
08/30/22 16:09
121-14-2
2,6-Dinitrotoluene
ND
ug/kg
7070
10
08/29/22 10:52
08/30/22 16:09
606-20-2
Di-n-octylphthalate
ND
ug/kg
7070
10
08/29/22 10:52
08/30/22 16:09
117-84-0
Dinoseb
ND
ug/kg
14100
10
08/29/22 10:52
08/30/22 16:09
88-85-7
Diphenylamine
ND
ug/kg
7070
10
08/29/22 10:52
08/30/22 16:09
122-39-4
Diphenyl ether (Phenyl ether)
ND
ug/kg
10700
10
08/29/22 10:52
08/30/22 16:09
101-84-8
1,2-Diphenylhydrazine
ND
ug/kg
7070
10
08/29/22 10:52
08/30/22 16:09
122-66-7
Disulfoton
ND
ug/kg
7070
10
08/29/22 10:52
08/30/22 16:09
298-04-4
bis(2- Ethyl hexyl)phthalate
8470
ug/kg
7070
10
08/29/22 10:52
08/30/22 16:09
117-81-7
Ethyl methanesulfonate
ND
ug/kg
14100
10
08/29/22 10:52
08/30/22 16:09
62-50-0
Famphur
ND
ug/kg
14100
10
08/29/22 10:52
08/30/22 16:09
52-85-7
Fluoranthene
ND
ug/kg
7070
10
08/29/22 10:52
08/30/22 16:09
206-44-0
Fluorene
ND
ug/kg
7070
10
08/29/22 10:52
08/30/22 16:09
86-73-7
Hexachloro-1,3-butadiene
ND
ug/kg
7070
10
08/29/22 10:52
08/30/22 16:09
87-68-3
Hexachlorobenzene
ND
ug/kg
7070
10
08/29/22 10:52
08/30/22 16:09
118-74-1
Hexachlorocyclopentadiene
ND
ug/kg
7070
10
08/29/22 10:52
08/30/22 16:09
77-47-4
Hexachloroethane
ND
ug/kg
7070
10
08/29/22 10:52
08/30/22 16:09
67-72-1
Hexachlorophene
ND
ug/kg
70700
10
08/29/22 10:52
08/30/22 16:09
70-30-4
Hexachloropropene
ND
ug/kg
7070
10
08/29/22 10:52
08/30/22 16:09
1888-71-7
Indeno(1,2,3-cd)pyrene
ND
ug/kg
7070
10
08/29/22 10:52
08/30/22 16:09
193-39-5
Isodrin
ND
ug/kg
7070
10
08/29/22 10:52
08/30/22 16:09
465-73-6
Isophorone
ND
ug/kg
7070
10
08/29/22 10:52
08/30/22 16:09
78-59-1
Isosafrole
ND
ug/kg
7070
10
08/29/22 10:52
08/30/22 16:09
120-58-1
Kepone
ND
ug/kg
14100
10
08/29/22 10:52
08/30/22 16:09
143-50-0
Methapyrilene
ND
ug/kg
35300
10
08/29/22 10:52
08/30/22 16:09
91-80-5
3-Methylcholanthrene
ND
ug/kg
7070
10
08/29/22 10:52
08/30/22 16:09
56-49-5
4,4'-Methylene-bis(2-chloroani
ND
ug/kg
14100
10
08/29/22 10:52
08/30/22 16:09
101-14-4
Methyl methanesulfonate
ND
ug/kg
14100
10
08/29/22 10:52
08/30/22 16:09
66-27-3
1-Methylnaphthalene
ND
ug/kg
7070
10
08/29/22 10:52
08/30/22 16:09
90-12-0
2-Methylnaphthalene
ND
ug/kg
7070
10
08/29/22 10:52
08/30/22 16:09
91-57-6
2-Methyl-5-nitroaniline
ND
ug/kg
7070
10
08/29/22 10:52
08/30/22 16:09
99-55-8
Methyl parathion
ND
ug/kg
7070
10
08/29/22 10:52
08/30/22 16:09
298-00-0
2-Methylphenol(o-Cresol)
ND
ug/kg
7070
10
08/29/22 10:52
08/30/22 16:09
95-48-7
3&4-Methyl phenol (m&p Cresol)
ND
ug/kg
7070
10
08/29/22 10:52
08/30/22 16:09
15831-10-4
1-Naphthalenamine
ND
ug/kg
14100
10
08/29/22 10:52
08/30/22 16:09
134-32-7
2-Naphthalenamine
ND
ug/kg
14100
10
08/29/22 10:52
08/30/22 16:09
91-59-8
Naphthalene
ND
ug/kg
7070
10
08/29/22 10:52
08/30/22 16:09
91-20-3
1,4-Naphthoquinone
ND
ug/kg
35300
10
08/29/22 10:52
08/30/22 16:09
130-15-4
2-Nitroaniline
ND
ug/kg
35300
10
08/29/22 10:52
08/30/22 16:09
88-74-4
3-Nitroaniline
ND
ug/kg
35300
10
08/29/22 10:52
08/30/22 16:09
99-09-2
4-Nitroaniline
ND
ug/kg
14100
10
08/29/22 10:52
08/30/22 16:09
100-01-6
Nitrobenzene
ND
ug/kg
7070
10
08/29/22 10:52
08/30/22 16:09
98-95-3
REPORT OF LABORATORY ANALYSIS
Qual
IH,L2
IH
This report shall not be reproduced, except in full,
Date: 10/25/2022 02:36 PM without the written consent of Pace Analytical Services, LLC. Page 32 of 165

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: WASTE CHARACTERIZATION
Pace Project No.: 92621331
Sample: GP-4 2-3' Lab ID: 92621331004 Collected: 08/16/22 11:30 Received: 08/17/22 16:15 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters
8270E MSSV Microwave
2-Nitrophenol
4-Nitrophenol
4-Nitroquinoline-n-oxide
5-Nitro-o-toluidine
N-Nitrosodiethylamine
N-Nitrosodimethylamine
N-Nitroso-di-n-butylamine
N-Nitroso-di-n-propylamine
N-Nitrosodiphenylamine
N-Nitrosomethylethylamine
N-Nitrosomorpholine
N-Nitrosopiperidine
N-Nitrosopyrrolidine
n-Octadecane
O,O,O-Triethylphosphorothioate
2,2'-Oxybis(1-chloropropane)
Parathion (Ethyl parathion)
Pentachlorobenzene
Pentachloroethane
Pentachloronitrobenzene
Pentachlorophenol
Phenacetin
Phenanthrene
Phenol
p-Phenylenediamine
Phorate
Phthalic anhydride
2-Picoline
Pronamide
Pyrene
Pyridine
Safrole
Sulfotepp (ThiodiphosphoricAc
Terpineol
1,2,4,5-Tetrachlorobenzene
2,3,4,6-Tetrachlorophenol
Thionazin
O-Toluidine
1,2,4-Trichlorobenzene
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
1,3,5-Trinitrobenzene
Surrogates
2-Fluorobiphenyl (S)
Terphenyl-d14 (S)
Results Units Report Limit DF Prepared Analyzed CAS No. Qual
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
ND
ug/kg
7070
10
08/29/2210:52
08/30/2216:09
88-75-5
ND
ug/kg
35300
10
08/29/2210:52
08/30/2216:09
100-02-7
ND
ug/kg
35300
10
08/29/2210:52
08/30/2216:09
56-57-5
v2
ND
ug/kg
7070
10
08/29/2210:52
08/30/2216:09
99-55-8
ND
ug/kg
7070
10
08/29/2210:52
08/30/2216:09
55-18-5
ND
ug/kg
7070
10
08/29/2210:52
08/30/2216:09
62-75-9
ND
ug/kg
7070
10
08/29/2210:52
08/30/2216:09
924-16-3
ND
ug/kg
7070
10
08/29/2210:52
08/30/2216:09
621-64-7
ND
ug/kg
7070
10
08/29/2210:52
08/30/2216:09
86-30-6
ND
ug/kg
7070
10
08/29/2210:52
08/30/2216:09
10595-95-6
ND
ug/kg
7070
10
08/29/2210:52
08/30/2216:09
59-89-2
ND
ug/kg
14100
10
08/29/2210:52
08/30/2216:09
100-75-4
ND
ug/kg
14100
10
08/29/2210:52
08/30/2216:09
930-55-2
ND
ug/kg
7070
10
08/29/2210:52
08/30/2216:09
593-45-3
ND
ug/kg
7070
10
08/29/2210:52
08/30/2216:09
126-68-1
ND
ug/kg
7070
10
08/29/2210:52
08/30/2216:09
108-60-1
ND
ug/kg
7070
10
08/29/2210:52
08/30/2216:09
56-38-2
ND
ug/kg
7070
10
08/29/2210:52
08/30/2216:09
608-93-5
ND
ug/kg
7070
10
08/29/2210:52
08/30/2216:09
76-01-7
ND
ug/kg
7070
10
08/29/2210:52
08/30/2216:09
82-68-8
ND
ug/kg
14100
10
08/29/2210:52
08/30/2216:09
87-86-5
ND
ug/kg
14100
10
08/29/2210:52
08/30/2216:09
62-44-2
ND
ug/kg
7070
10
08/29/2210:52
08/30/2216:09
85-01-8
ND
ug/kg
7070
10
08/29/2210:52
08/30/2216:09
108-95-2
ND
ug/kg
14100
10
08/29/2210:52
08/30/2216:09
106-50-3
IL
ND
ug/kg
7070
10
08/29/2210:52
08/30/2216:09
298-02-2
L2
ND
ug/kg
53600
10
08/29/2210:52
08/30/2216:09
85-44-9
ND
ug/kg
7070
10
08/29/2210:52
08/30/2216:09
109-06-8
ND
ug/kg
14100
10
08/29/2210:52
08/30/2216:09
23950-58-5
ND
ug/kg
7070
10
08/29/2210:52
08/30/2216:09
129-00-0
ND
ug/kg
7070
10
08/29/2210:52
08/30/2216:09
110-86-1
ND
ug/kg
14100
10
08/29/2210:52
08/30/2216:09
94-59-7
ND
ug/kg
7070
10
08/29/2210:52
08/30/2216:09
3689-24-5
ND
ug/kg
7070
10
08/29/2210:52
08/30/2216:09
98-55-5
ND
ug/kg
7070
10
08/29/2210:52
08/30/2216:09
95-94-3
ND
ug/kg
7070
10
08/29/2210:52
08/30/2216:09
58-90-2
ND
ug/kg
7070
10
08/29/2210:52
08/30/2216:09
297-97-2
ND
ug/kg
7070
10
08/29/2210:52
08/30/2216:09
95-53-4
ND
ug/kg
7070
10
08/29/2210:52
08/30/2216:09
120-82-1
ND
ug/kg
7070
10
08/29/2210:52
08/30/2216:09
95-95-4
ND
ug/kg
7070
10
08/29/2210:52
08/30/2216:09
88-06-2
ND
ug/kg
7070
10
08/29/2210:52
08/30/2216:09
99-35-4
0
%
19-130
10
08/29/2210:52
08/30/2216:09
321-60-8
D3,S4
0
%
15-130
10
08/29/2210:52
08/30/2216:09
1718-51-0
S4
REPORT
OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/25/2022 02:36 PM without the written consent of Pace Analytical Services, LLC. Page 33 of 165

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: WASTE CHARACTERIZATION
Pace Project No.: 92621331
Sample: GP-4 2-3'
Lab ID: 92621331004 Collected: 08/16/22 11:30 Received: 08/17/22 16:15 Matrix: Solid
Results reported on a "dry weight"
basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters
Results Units Report Limit DF Prepared
Analyzed
CAS No. Qual
8270E MSSV Microwave
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
Surrogates
Phenol-d6 (S)
0 % 18-130 10 08/29/22 10:52
08/30/22 16:09
13127-88-3 S4
2-Fluorophenol (S)
0 % 18-130 10 08/29/22 10:52
08/30/22 16:09
367-12-4 S4
2,4,6-Tribromophenol (S)
0 % 18-130 10 08/29/22 10:52
08/30/22 16:09
118-79-6 S4
Nitrobenzene-d5 (S)
0 % 21-130 10 08/29/22 10:52
08/30/22 16:09
4165-60-0 S4
Percent Moisture
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
53.3 % 0.10 1
08/22/22 15:39
N2
1010 Flash poi nt,Closed Cup
Analytical Method: EPA 1010B
Pace Analytical Services -Asheville
Flashpoint
>200 deg F 70.0 1
08/22/22 12:51
Total Solids 2540 G-2011
Analytical Method: SM 2540G Preparation Method: SM 2540 G
Pace National - Mt. Juliet
Total Solids
43.6 % 1 08/23/22 10:15
08/23/22 10:31
4500S21) Sulfide Soil
Analytical Method: SM 4500-S2D-2011 Modified Preparation Method: SM
4500-S2D-2011 Modified
Pace Analytical Services -Asheville
Sulfide
ND mg/kg 10.5 1 08/20/22 02:37
08/20/22 06:39
18496-25-8
9045 pH Soil
Analytical Method: EPA 9045D
Pace Analytical Services -Asheville
pH at 25 Degrees C
5.2 Std. Units 0.10 1
08/23/22 18:09
H3
9012 Cyanide, Total
Analytical Method: EPA 9012 Preparation Method: EPA 9012
Pace Analytical Services - Ormond Beach
Cyanide
13.6 mg/kg 5.4 10 08/29/22 09:41
08/29/22 15:18
57-12-5
Date: 10/25/2022 02:36 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 34 of 165

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: WASTE CHARACTERIZATION
Pace Project No.: 92621331
Sample: GP-5 2-3' Lab ID: 92621331005 Collected: 08/16/22 12:00 Received: 08/17/22 16:15 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
OP Pesticides 8141 B
Analytical Method: EPA 8141 B Preparation Method: 3546
Pace National
- Mt. Juliet
Azinphos, methyl (Guthion)
ND
mg/kg
0.209
1
08/21/22 16:12
08/22/22 03:10
86-50-0
Bolstar
ND
mg/kg
0.209
1
08/21/22 16:12
08/22/22 03:10
35400-43-2
Chlorpyrifos
ND
mg/kg
0.209
1
08/21/22 16:12
08/22/22 03:10
2921-88-2
Coumaphos
ND
mg/kg
0.209
1
08/21/22 16:12
08/22/22 03:10
56-72-4
Total Demeton
ND
mg/kg
0.146
1
08/21/22 16:12
08/22/22 03:10
8065-48-3
Diazinon
ND
mg/kg
0.209
1
08/21/22 16:12
08/22/22 03:10
333-41-5
Dichlorvos
ND
mg/kg
0.209
1
08/21/22 16:12
08/22/22 03:10
62-73-7
Dimethoate
ND
mg/kg
0.209
1
08/21/22 16:12
08/22/22 03:10
60-51-5
Disulfoton
ND
mg/kg
0.209
1
08/21/22 16:12
08/22/22 03:10
298-04-4
EPN (ENT)
ND
mg/kg
0.209
1
08/21/22 16:12
08/22/22 03:10
2104-64-5
Ethoprop
ND
mg/kg
0.209
1
08/21/22 16:12
08/22/22 03:10
13194-48-4
Parathion (Ethyl parathion)
ND
mg/kg
0.209
1
08/21/22 16:12
08/22/22 03:10
56-38-2
Fensulfothion
ND
mg/kg
0.209
1
08/21/22 16:12
08/22/22 03:10
115-90-2
Fenthion
ND
mg/kg
0.209
1
08/21/22 16:12
08/22/22 03:10
55-38-9
Malathion
ND
mg/kg
0.209
1
08/21/22 16:12
08/22/22 03:10
121-75-5
Merphos
ND
mg/kg
0.209
1
08/21/22 16:12
08/22/22 03:10
150-50-5
Methyl parathion
ND
mg/kg
0.209
1
08/21/22 16:12
08/22/22 03:10
298-00-0
Mevinphos
ND
mg/kg
0.209
1
08/21/22 16:12
08/22/22 03:10
7786-34-7
Naled
ND
mg/kg
0.209
1
08/21/22 16:12
08/22/22 03:10
300-76-5
Phorate
ND
mg/kg
0.209
1
08/21/22 16:12
08/22/22 03:10
298-02-2
Ronnel
ND
mg/kg
0.209
1
08/21/22 16:12
08/22/22 03:10
299-84-3
Stirophos (Tetrachlorvinphos)
ND
mg/kg
0.209
1
08/21/22 16:12
08/22/22 03:10
22248-79-9
Sulfotepp (ThiodiphosphoricAc
ND
mg/kg
0.209
1
08/21/22 16:12
08/22/22 03:10
3689-24-5
TEPP
ND
mg/kg
2.09
1
08/21/22 16:12
08/22/22 03:10
107-49-3
Tokuthion (Prothiofos)
ND
mg/kg
0.209
1
08/21/22 16:12
08/22/22 03:10
34643-46-4
Trichloronate
ND
mg/kg
0.209
1
08/21/22 16:12
08/22/22 03:10
327-98-0
Surrogates
Triphenyl phosphate (S)
63.4
%
36.0-121
1
08/21/22 16:12
08/22/22 03:10
115-86-6
8081 GCS Pesticides
Analytical Method: EPA 8081 B Preparation Method: EPA 3546
Pace Analytical
Services - Charlotte
alpha-BHC
ND
ug/kg
41.8
10
08/29/22 10:46
08/29/22 15:18
319-84-6
gamma-BHC (Lindane)
ND
ug/kg
41.8
10
08/29/22 10:46
08/29/22 15:18
58-89-9
beta-BHC
ND
ug/kg
41.8
10
08/29/22 10:46
08/29/22 15:18
319-85-7
Heptachlor
ND
ug/kg
41.8
10
08/29/22 10:46
08/29/22 15:18
76-44-8
delta-BHC
ND
ug/kg
41.8
10
08/29/22 10:46
08/29/22 15:18
319-86-8
Aldrin
ND
ug/kg
41.8
10
08/29/22 10:46
08/29/22 15:18
309-00-2
Heptachlor epoxide
ND
ug/kg
41.8
10
08/29/22 10:46
08/29/22 15:18
1024-57-3
Endosulfan I
ND
ug/kg
41.8
10
08/29/22 10:46
08/29/22 15:18
959-98-8
4,4'-DDE
ND
ug/kg
41.8
10
08/29/22 10:46
08/29/22 15:18
72-55-9
Dieldrin
ND
ug/kg
41.8
10
08/29/22 10:46
08/29/22 15:18
60-57-1
Endrin
ND
ug/kg
41.8
10
08/29/22 10:46
08/29/22 15:18
72-20-8
4,4'-DDD
ND
ug/kg
41.8
10
08/29/22 10:46
08/29/22 15:18
72-54-8
Endosulfan II
ND
ug/kg
41.8
10
08/29/22 10:46
08/29/22 15:18
33213-65-9
4,4'-DDT
ND
ug/kg
41.8
10
08/29/22 10:46
08/29/22 15:18
50-29-3
REPORT OF LABORATORY ANALYSIS
LO
This report shall not be reproduced, except in full,
Date: 10/25/2022 02:36 PM without the written consent of Pace Analytical Services, LLC. Page 35 of 165

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: WASTE CHARACTERIZATION
Pace Project No.: 92621331
Sample: GP-5 2-3' Lab ID: 92621331005 Collected: 08/16/22 12:00 Received: 08/17/22 16:15 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8081 GCS Pesticides
Endrin aldehyde
Endosulfan sulfate
Methoxychlor
Endrin ketone
Chlordane (Technical)
Toxaphene
Mirex
Hexachlorobenzene
Surrogates
Tetrachloro-m-xylene (S)
Decachlorobiphenyl (S)
8082 GCS PCB
PCB-1016 (Aroclor 1016)
PCB-1221 (Aroclor 1221)
PCB-1232 (Aroclor 1232)
PCB-1242 (Aroclor 1242)
PCB-1248 (Aroclor 1248)
PCB-1254 (Aroclor 1254)
PCB-1260 (Aroclor 1260)
Surrogates
Decachlorobiphenyl (S)
Analytical Method: EPA 8081 B Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
ND
ug/kg
41.8
10
08/29/2210:46
08/29/2215:18
7421-93-4
ND
ug/kg
41.8
10
08/29/2210:46
08/29/2215:18
1031-07-8
ND
ug/kg
105
10
08/29/2210:46
08/29/2215:18
72-43-5
ND
ug/kg
41.8
10
08/29/2210:46
08/29/2215:18
53494-70-5
694
ug/kg
209
10
08/29/2210:46
08/29/2215:18
57-74-9
ND
ug/kg
146
10
08/29/2210:46
08/29/2215:18
8001-35-2
ND
ug/kg
105
10
08/29/2210:46
08/29/2215:18
2385-85-5
ND
ug/kg
41.8
10
08/29/2210:46
08/29/2215:18
118-74-1
0
%
10-133
10
08/29/2210:46
08/29/2215:18
877-09-8 D3,S4
0
%
10-146
10
08/29/2210:46
08/29/2215:18
2051-24-3 S4
Analytical Method: EPA 8082A Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
ND
ug/kg
1350
20
08/19/22 15:53
08/24/22 06:48
12674-11-2
ND
ug/kg
1350
20
08/19/22 15:53
08/24/22 06:48
11104-28-2
ND
ug/kg
1350
20
08/19/22 15:53
08/24/22 06:48
11141-16-5
ND
ug/kg
1350
20
08/19/22 15:53
08/24/22 06:48
53469-21-9
ND
ug/kg
1350
20
08/19/22 15:53
08/24/22 06:48
12672-29-6
ND
ug/kg
1350
20
08/19/22 15:53
08/24/22 06:48
11097-69-1
ND
ug/kg
1350
20
08/19/22 15:53
08/24/22 06:48
11096-82-5
0
%
10-160
20
08/19/22 15:53
08/24/22 06:48
2051-24-3 D3,S4
6010 MET ICP
Analytical Method: EPA 6010 Preparation Method: EPA 3050
Pace Analytical
Services - Ormond Beach
Tin
128
mg/kg
6.1
1
08/30/2219:03
08/31/2218:23
7440-31-5
6020 MET ICPMS
Analytical Method: EPA 6020 Preparation Method: EPA 3050
Pace Analytical
Services - Ormond Beach
Antimony
106
mg/kg
4.4
20
08/27/22 00:15
08/29/22 19:31
7440-36-0
1g,N2
Arsenic
5.9
mg/kg
2.2
20
08/27/22 00:15
08/29/22 19:31
7440-38-2
1g
Barium
1760
mg/kg
11.1
100
08/27/22 00:15
08/31/22 14:09
7440-39-3
1g
Beryllium
0.38
mg/kg
0.27
20
08/27/22 00:15
08/29/22 19:31
7440-41-7
1g
Cadmium
13.2
mg/kg
0.27
20
08/27/22 00:15
08/29/22 19:31
7440-43-9
1g
Chromium
1520
mg/kg
11.1
100
08/27/22 00:15
08/31/22 14:09
7440-47-3
1g
Cobalt
37.3
mg/kg
2.2
20
08/27/22 00:15
08/29/22 19:31
7440-48-4
1g
Copper
787
mg/kg
4.4
20
08/27/22 00:15
08/29/22 19:31
7440-50-8
1g
Lead
6150
mg/kg
111
1000
08/27/22 00:15
09/01 /22 09:09
7439-92-1
1g
Nickel
61.0
mg/kg
2.2
20
08/27/22 00:15
08/29/22 19:31
7440-02-0
1g
Selenium
8.1
mg/kg
2.2
20
08/27/22 00:15
08/29/22 19:31
7782-49-2
1g
Silver
175
mg/kg
1.3
100
08/27/22 00:15
08/31/22 14:09
7440-22-4
1g
Thallium
ND
mg/kg
2.2
20
08/27/22 00:15
08/29/22 19:31
7440-28-0
1g
Vanadium
31.1
mg/kg
2.2
20
08/27/22 00:15
08/29/22 19:31
7440-62-2
1g
Zinc
6660
mg/kg
443
100
08/27/22 00:15
08/31/22 14:09
7440-66-6
1g
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/25/2022 02:36 PM without the written consent of Pace Analytical Services, LLC. Page 36 of 165

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: WASTE CHARACTERIZATION
Pace Project No.: 92621331
Sample: GP-5 2-3' Lab ID: 92621331005 Collected: 08/16/22 12:00 Received: 08/17/22 16:15 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
7471 Mercury Analytical Method: EPA 7471 Preparation Method: EPA 7471
Pace Analytical Services - Ormond Beach
Mercury 9.6 mg/kg 0.20 10 08/24/22 07:26 08/24/22 11:30 7439-97-6
8270E MSSV Microwave
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical
Services - Charlotte
Acenaphthene
ND
ug/kg
6790
10
08/29/22 10:52
08/30/22 16:39
83-32-9
Acenaphthylene
ND
ug/kg
6790
10
08/29/22 10:52
08/30/22 16:39
208-96-8
Acetophenone
ND
ug/kg
6790
10
08/29/22 10:52
08/30/22 16:39
98-86-2
2-Acetylaminofluorene
ND
ug/kg
13600
10
08/29/22 10:52
08/30/22 16:39
53-96-3
4-Aminobiphenyl
ND
ug/kg
6790
10
08/29/22 10:52
08/30/22 16:39
92-67-1
Anthracene
ND
ug/kg
6790
10
08/29/22 10:52
08/30/22 16:39
120-12-7
Benzo(a)anthracene
ND
ug/kg
6790
10
08/29/22 10:52
08/30/22 16:39
56-55-3
Benzo(a)pyrene
ND
ug/kg
6790
10
08/29/22 10:52
08/30/22 16:39
50-32-8
Benzo(b)fluoranthene
ND
ug/kg
6790
10
08/29/22 10:52
08/30/22 16:39
205-99-2
Benzo(g,h,i)perylene
ND
ug/kg
6790
10
08/29/22 10:52
08/30/22 16:39
191-24-2
Benzo(k)fluoranthene
ND
ug/kg
6790
10
08/29/22 10:52
08/30/22 16:39
207-08-9
Benzyl alcohol
ND
ug/kg
13600
10
08/29/22 10:52
08/30/22 16:39
100-51-6
bis(2-Chloroethoxy)methane
ND
ug/kg
6790
10
08/29/22 10:52
08/30/22 16:39
111-91-1
bis(2-Chloroethyl) ether
ND
ug/kg
6790
10
08/29/22 10:52
08/30/22 16:39
111-44-4
2-Chloronaphthalene
ND
ug/kg
6790
10
08/29/22 10:52
08/30/22 16:39
91-58-7
2-Chlorophenol
ND
ug/kg
6790
10
08/29/22 10:52
08/30/22 16:39
95-57-8
4-Chlorophenylphenyl ether
ND
ug/kg
6790
10
08/29/22 10:52
08/30/22 16:39
7005-72-3
Chrysene
ND
ug/kg
6790
10
08/29/22 10:52
08/30/22 16:39
218-01-9
n-Decane
ND
ug/kg
6790
10
08/29/22 10:52
08/30/22 16:39
124-18-5
Diallate
ND
ug/kg
6790
10
08/29/22 10:52
08/30/22 16:39
2303-16-4
Dibenz(a,h)anthracene
ND
ug/kg
6790
10
08/29/22 10:52
08/30/22 16:39
53-70-3
Dibenzo(a,e)pyrene
ND
ug/kg
20600
10
08/29/22 10:52
08/30/22 16:39
192-65-4
Dibenzofuran
ND
ug/kg
6790
10
08/29/22 10:52
08/30/22 16:39
132-64-9
2,3-Dibromo-1-propanol phosph
ND
ug/kg
33900
10
08/29/22 10:52
08/30/22 16:39
126-72-7
1,2-Dichlorobenzene
ND
ug/kg
6790
10
08/29/22 10:52
08/30/22 16:39
95-50-1
1,3-Dichlorobenzene
ND
ug/kg
6790
10
08/29/22 10:52
08/30/22 16:39
541-73-1
1,4-Dichlorobenzene
ND
ug/kg
6790
10
08/29/22 10:52
08/30/22 16:39
106-46-7
3,3'-Dichlorobenzidine
ND
ug/kg
13600
10
08/29/22 10:52
08/30/22 16:39
91-94-1
2,4-Dichlorophenol
ND
ug/kg
6790
10
08/29/22 10:52
08/30/22 16:39
120-83-2
2,6-Dichlorophenol
ND
ug/kg
6790
10
08/29/22 10:52
08/30/22 16:39
87-65-0
2,3-Dichloroaniline
ND
ug/kg
6790
10
08/29/22 10:52
08/30/22 16:39
608-27-5
Diethylphthalate
ND
ug/kg
6790
10
08/29/22 10:52
08/30/22 16:39
84-66-2
Dimethoate
ND
ug/kg
13600
10
08/29/22 10:52
08/30/22 16:39
60-51-5
P-Dimethylaminoazobenzene
ND
ug/kg
6790
10
08/29/22 10:52
08/30/22 16:39
60-11-7
7,12-Dimethylbenz(a)anthracene
ND
ug/kg
6790
10
08/29/22 10:52
08/30/22 16:39
57-97-6
3,3'-Dimethylbenzidine
ND
ug/kg
13600
10
08/29/22 10:52
08/30/22 16:39
119-93-7
2,4-Dimethylphenol
ND
ug/kg
6790
10
08/29/22 10:52
08/30/22 16:39
105-67-9
a,a-Dimethylphenylethylamine
ND
ug/kg
33900
10
08/29/22 10:52
08/30/22 16:39
122-09-8
Dimethylphthalate
ND
ug/kg
6790
10
08/29/22 10:52
08/30/22 16:39
131-11-3
Di-n-butylphthalate
ND
ug/kg
6790
10
08/29/22 10:52
08/30/22 16:39
84-74-2
4,6-Dinitro-2-methyl phenol
ND
ug/kg
13600
10
08/29/22 10:52
08/30/22 16:39
534-52-1
REPORT OF LABORATORY ANALYSIS
v1
IL
IL
IH
v1
This report shall not be reproduced, except in full,
Date: 10/25/2022 02:36 PM without the written consent of Pace Analytical Services, LLC. Page 37 of 165

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: WASTE CHARACTERIZATION
Pace Project No.: 92621331
Sample: GP-5 2-3' Lab ID: 92621331005 Collected: 08/16/22 12:00 Received: 08/17/22 16:15 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No
8270E MSSV Microwave
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical
Services - Charlotte
1,3-Dinitrobenzene
ND
ug/kg
6790
10
08/29/22 10:52
08/30/22 16:39
99-65-0
1,4-Dinitrobenzene
ND
ug/kg
6790
10
08/29/22 10:52
08/30/22 16:39
100-25-4
2,4-Dinitrophenol
ND
ug/kg
33900
10
08/29/22 10:52
08/30/22 16:39
51-28-5
2,4-Dinitrotoluene
ND
ug/kg
6790
10
08/29/22 10:52
08/30/22 16:39
121-14-2
2,6-Dinitrotoluene
ND
ug/kg
6790
10
08/29/22 10:52
08/30/22 16:39
606-20-2
Di-n-octylphthalate
ND
ug/kg
6790
10
08/29/22 10:52
08/30/22 16:39
117-84-0
Dinoseb
ND
ug/kg
13600
10
08/29/22 10:52
08/30/22 16:39
88-85-7
Diphenylamine
ND
ug/kg
6790
10
08/29/22 10:52
08/30/22 16:39
122-39-4
Diphenyl ether (Phenyl ether)
ND
ug/kg
10300
10
08/29/22 10:52
08/30/22 16:39
101-84-8
1,2-Diphenylhydrazine
ND
ug/kg
6790
10
08/29/22 10:52
08/30/22 16:39
122-66-7
Disulfoton
ND
ug/kg
6790
10
08/29/22 10:52
08/30/22 16:39
298-04-4
bis(2- Ethyl hexyl)phthalate
7900
ug/kg
6790
10
08/29/22 10:52
08/30/22 16:39
117-81-7
Ethyl methanesulfonate
ND
ug/kg
13600
10
08/29/22 10:52
08/30/22 16:39
62-50-0
Famphur
ND
ug/kg
13600
10
08/29/22 10:52
08/30/22 16:39
52-85-7
Fluoranthene
ND
ug/kg
6790
10
08/29/22 10:52
08/30/22 16:39
206-44-0
Fluorene
ND
ug/kg
6790
10
08/29/22 10:52
08/30/22 16:39
86-73-7
Hexachloro-1,3-butadiene
ND
ug/kg
6790
10
08/29/22 10:52
08/30/22 16:39
87-68-3
Hexachlorobenzene
ND
ug/kg
6790
10
08/29/22 10:52
08/30/22 16:39
118-74-1
Hexachlorocyclopentadiene
ND
ug/kg
6790
10
08/29/22 10:52
08/30/22 16:39
77-47-4
Hexachloroethane
ND
ug/kg
6790
10
08/29/22 10:52
08/30/22 16:39
67-72-1
Hexachlorophene
ND
ug/kg
67900
10
08/29/22 10:52
08/30/22 16:39
70-30-4
Hexachloropropene
ND
ug/kg
6790
10
08/29/22 10:52
08/30/22 16:39
1888-71-7
Indeno(1,2,3-cd)pyrene
ND
ug/kg
6790
10
08/29/22 10:52
08/30/22 16:39
193-39-5
Isodrin
ND
ug/kg
6790
10
08/29/22 10:52
08/30/22 16:39
465-73-6
Isophorone
ND
ug/kg
6790
10
08/29/22 10:52
08/30/22 16:39
78-59-1
Isosafrole
ND
ug/kg
6790
10
08/29/22 10:52
08/30/22 16:39
120-58-1
Kepone
ND
ug/kg
13600
10
08/29/22 10:52
08/30/22 16:39
143-50-0
Methapyrilene
ND
ug/kg
33900
10
08/29/22 10:52
08/30/22 16:39
91-80-5
3-Methylcholanthrene
ND
ug/kg
6790
10
08/29/22 10:52
08/30/22 16:39
56-49-5
4,4'-Methylene-bis(2-chloroani
ND
ug/kg
13600
10
08/29/22 10:52
08/30/22 16:39
101-14-4
Methyl methanesulfonate
ND
ug/kg
13600
10
08/29/22 10:52
08/30/22 16:39
66-27-3
1-Methylnaphthalene
ND
ug/kg
6790
10
08/29/22 10:52
08/30/22 16:39
90-12-0
2-Methylnaphthalene
ND
ug/kg
6790
10
08/29/22 10:52
08/30/22 16:39
91-57-6
2-Methyl-5-nitroaniline
ND
ug/kg
6790
10
08/29/22 10:52
08/30/22 16:39
99-55-8
Methyl parathion
ND
ug/kg
6790
10
08/29/22 10:52
08/30/22 16:39
298-00-0
2-Methylphenol(o-Cresol)
ND
ug/kg
6790
10
08/29/22 10:52
08/30/22 16:39
95-48-7
3&4-Methyl phenol (m&p Cresol)
ND
ug/kg
6790
10
08/29/22 10:52
08/30/22 16:39
15831-10-4
1-Naphthalenamine
ND
ug/kg
13600
10
08/29/22 10:52
08/30/22 16:39
134-32-7
2-Naphthalenamine
ND
ug/kg
13600
10
08/29/22 10:52
08/30/22 16:39
91-59-8
Naphthalene
ND
ug/kg
6790
10
08/29/22 10:52
08/30/22 16:39
91-20-3
1,4-Naphthoquinone
ND
ug/kg
33900
10
08/29/22 10:52
08/30/22 16:39
130-15-4
2-Nitroaniline
ND
ug/kg
33900
10
08/29/22 10:52
08/30/22 16:39
88-74-4
3-Nitroaniline
ND
ug/kg
33900
10
08/29/22 10:52
08/30/22 16:39
99-09-2
4-Nitroaniline
ND
ug/kg
13600
10
08/29/22 10:52
08/30/22 16:39
100-01-6
Nitrobenzene
ND
ug/kg
6790
10
08/29/22 10:52
08/30/22 16:39
98-95-3
REPORT OF LABORATORY ANALYSIS
Qual
IH,L2
IH
This report shall not be reproduced, except in full,
Date: 10/25/2022 02:36 PM without the written consent of Pace Analytical Services, LLC. Page 38 of 165

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: WASTE CHARACTERIZATION
Pace Project No.: 92621331
Sample: GP-5 2-3' Lab ID: 92621331005 Collected: 08/16/22 12:00 Received: 08/17/22 16:15 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters
8270E MSSV Microwave
2-Nitrophenol
4-Nitrophenol
4-Nitroquinoline-n-oxide
5-Nitro-o-toluidine
N-Nitrosodiethylamine
N-Nitrosodimethylamine
N-Nitroso-di-n-butylamine
N-Nitroso-di-n-propylamine
N-Nitrosodiphenylamine
N-Nitrosomethylethylamine
N-Nitrosomorpholine
N-Nitrosopiperidine
N-Nitrosopyrrolidine
n-Octadecane
O,O,O-Triethylphosphorothioate
2,2'-Oxybis(1-chloropropane)
Parathion (Ethyl parathion)
Pentachlorobenzene
Pentachloroethane
Pentachloronitrobenzene
Pentachlorophenol
Phenacetin
Phenanthrene
Phenol
p-Phenylenediamine
Phorate
Phthalic anhydride
2-Picoline
Pronamide
Pyrene
Pyridine
Safrole
Sulfotepp (ThiodiphosphoricAc
Terpineol
1,2,4,5-Tetrachlorobenzene
2,3,4,6-Tetrachlorophenol
Thionazin
O-Toluidine
1,2,4-Trichlorobenzene
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
1,3,5-Trinitrobenzene
Surrogates
2-Fluorobiphenyl (S)
Terphenyl-d14 (S)
Results Units Report Limit DF Prepared Analyzed CAS No. Qual
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
ND
ug/kg
6790
10
08/29/2210:52
08/30/2216:39
88-75-5
ND
ug/kg
33900
10
08/29/2210:52
08/30/2216:39
100-02-7
ND
ug/kg
33900
10
08/29/2210:52
08/30/2216:39
56-57-5
v2
ND
ug/kg
6790
10
08/29/2210:52
08/30/2216:39
99-55-8
ND
ug/kg
6790
10
08/29/2210:52
08/30/2216:39
55-18-5
ND
ug/kg
6790
10
08/29/2210:52
08/30/2216:39
62-75-9
ND
ug/kg
6790
10
08/29/2210:52
08/30/2216:39
924-16-3
ND
ug/kg
6790
10
08/29/2210:52
08/30/2216:39
621-64-7
ND
ug/kg
6790
10
08/29/2210:52
08/30/2216:39
86-30-6
ND
ug/kg
6790
10
08/29/2210:52
08/30/2216:39
10595-95-6
ND
ug/kg
6790
10
08/29/2210:52
08/30/2216:39
59-89-2
ND
ug/kg
13600
10
08/29/2210:52
08/30/2216:39
100-75-4
ND
ug/kg
13600
10
08/29/2210:52
08/30/2216:39
930-55-2
ND
ug/kg
6790
10
08/29/2210:52
08/30/2216:39
593-45-3
ND
ug/kg
6790
10
08/29/2210:52
08/30/2216:39
126-68-1
ND
ug/kg
6790
10
08/29/2210:52
08/30/2216:39
108-60-1
ND
ug/kg
6790
10
08/29/2210:52
08/30/2216:39
56-38-2
ND
ug/kg
6790
10
08/29/2210:52
08/30/2216:39
608-93-5
ND
ug/kg
6790
10
08/29/2210:52
08/30/2216:39
76-01-7
ND
ug/kg
6790
10
08/29/2210:52
08/30/2216:39
82-68-8
ND
ug/kg
13600
10
08/29/2210:52
08/30/2216:39
87-86-5
ND
ug/kg
13600
10
08/29/2210:52
08/30/2216:39
62-44-2
ND
ug/kg
6790
10
08/29/2210:52
08/30/2216:39
85-01-8
ND
ug/kg
6790
10
08/29/2210:52
08/30/2216:39
108-95-2
ND
ug/kg
13600
10
08/29/2210:52
08/30/2216:39
106-50-3
IL
ND
ug/kg
6790
10
08/29/2210:52
08/30/2216:39
298-02-2
L2
ND
ug/kg
51400
10
08/29/2210:52
08/30/2216:39
85-44-9
ND
ug/kg
6790
10
08/29/2210:52
08/30/2216:39
109-06-8
ND
ug/kg
13600
10
08/29/2210:52
08/30/2216:39
23950-58-5
ND
ug/kg
6790
10
08/29/2210:52
08/30/2216:39
129-00-0
ND
ug/kg
6790
10
08/29/2210:52
08/30/2216:39
110-86-1
ND
ug/kg
13600
10
08/29/2210:52
08/30/2216:39
94-59-7
ND
ug/kg
6790
10
08/29/2210:52
08/30/2216:39
3689-24-5
ND
ug/kg
6790
10
08/29/2210:52
08/30/2216:39
98-55-5
ND
ug/kg
6790
10
08/29/2210:52
08/30/2216:39
95-94-3
ND
ug/kg
6790
10
08/29/2210:52
08/30/2216:39
58-90-2
ND
ug/kg
6790
10
08/29/2210:52
08/30/2216:39
297-97-2
ND
ug/kg
6790
10
08/29/2210:52
08/30/2216:39
95-53-4
ND
ug/kg
6790
10
08/29/2210:52
08/30/2216:39
120-82-1
ND
ug/kg
6790
10
08/29/2210:52
08/30/2216:39
95-95-4
ND
ug/kg
6790
10
08/29/2210:52
08/30/2216:39
88-06-2
ND
ug/kg
6790
10
08/29/2210:52
08/30/2216:39
99-35-4
0
%
19-130
10
08/29/2210:52
08/30/2216:39
321-60-8
D3,S4
0
%
15-130
10
08/29/2210:52
08/30/2216:39
1718-51-0
S4
REPORT
OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/25/2022 02:36 PM without the written consent of Pace Analytical Services, LLC. Page 39 of 165

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: WASTE CHARACTERIZATION
Pace Project No.: 92621331
Sample: GP-5 2-3'
Lab ID: 92621331005 Collected: 08/16/22 12:00 Received: 08/17/22 16:15 Matrix: Solid
Results reported on a "dry weight"
basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters
Results Units Report Limit DF Prepared
Analyzed
CAS No. Qual
8270E MSSV Microwave
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
Surrogates
Phenol-d6 (S)
0 % 18-130 10 08/29/22 10:52
08/30/22 16:39
13127-88-3 S4
2-Fluorophenol (S)
0 % 18-130 10 08/29/22 10:52
08/30/22 16:39
367-12-4 S4
2,4,6-Tribromophenol (S)
0 % 18-130 10 08/29/22 10:52
08/30/22 16:39
118-79-6 S4
Nitrobenzene-d5 (S)
0 % 21-130 10 08/29/22 10:52
08/30/22 16:39
4165-60-0 S4
Percent Moisture
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
51.9 % 0.10 1
08/22/22 15:39
N2
1010 Flash poi nt,Closed Cup
Analytical Method: EPA 1010B
Pace Analytical Services -Asheville
Flashpoint
>200 deg F 70.0 1
08/22/22 13:52
Total Solids 2540 G-2011
Analytical Method: SM 2540G Preparation Method: SM 2540 G
Pace National - Mt. Juliet
Total Solids
47.9 % 1 08/23/22 10:15
08/23/22 10:31
4500S21) Sulfide Soil
Analytical Method: SM 4500-S2D-2011 Modified Preparation Method: SM
4500-S2D-2011 Modified
Pace Analytical Services -Asheville
Sulfide
ND mg/kg 10.1 1 08/20/22 02:37
08/20/22 06:39
18496-25-8
9045 pH Soil
Analytical Method: EPA 9045D
Pace Analytical Services -Asheville
pH at 25 Degrees C
4.3 Std. Units 0.10 1
08/23/22 18:10
H3
9012 Cyanide, Total
Analytical Method: EPA 9012 Preparation Method: EPA 9012
Pace Analytical Services - Ormond Beach
Cyanide
12.4 mg/kg 5.3 10 08/29/22 09:41
08/29/22 15:19
57-12-5
Date: 10/25/2022 02:36 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 40 of 165

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: WASTE CHARACTERIZATION
Pace Project No.: 92621331
Sample: GP-6 2-3' Lab ID: 92621331006 Collected: 08/16/22 12:30 Received: 08/17/22 16:15 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
OP Pesticides 8141 B
Analytical Method: EPA 8141 B Preparation Method: 3546
Pace National
- Mt. Juliet
Azinphos, methyl (Guthion)
ND
mg/kg
0.242
1
08/21/22 16:12
08/22/22 03:44
86-50-0
Bolstar
ND
mg/kg
0.242
1
08/21/22 16:12
08/22/22 03:44
35400-43-2
Chlorpyrifos
ND
mg/kg
0.242
1
08/21/22 16:12
08/22/22 03:44
2921-88-2
Coumaphos
ND
mg/kg
0.242
1
08/21/22 16:12
08/22/22 03:44
56-72-4
Total Demeton
ND
mg/kg
0.169
1
08/21/22 16:12
08/22/22 03:44
8065-48-3
Diazinon
ND
mg/kg
0.242
1
08/21/22 16:12
08/22/22 03:44
333-41-5
Dichlorvos
ND
mg/kg
0.242
1
08/21/22 16:12
08/22/22 03:44
62-73-7
Dimethoate
ND
mg/kg
0.242
1
08/21/22 16:12
08/22/22 03:44
60-51-5
Disulfoton
ND
mg/kg
0.242
1
08/21/22 16:12
08/22/22 03:44
298-04-4
EPN (ENT)
ND
mg/kg
0.242
1
08/21/22 16:12
08/22/22 03:44
2104-64-5
Ethoprop
ND
mg/kg
0.242
1
08/21/22 16:12
08/22/22 03:44
13194-48-4
Parathion (Ethyl parathion)
ND
mg/kg
0.242
1
08/21/22 16:12
08/22/22 03:44
56-38-2
Fensulfothion
ND
mg/kg
0.242
1
08/21/22 16:12
08/22/22 03:44
115-90-2
Fenthion
ND
mg/kg
0.242
1
08/21/22 16:12
08/22/22 03:44
55-38-9
Malathion
ND
mg/kg
0.242
1
08/21/22 16:12
08/22/22 03:44
121-75-5
Merphos
ND
mg/kg
0.242
1
08/21/22 16:12
08/22/22 03:44
150-50-5
Methyl parathion
ND
mg/kg
0.242
1
08/21/22 16:12
08/22/22 03:44
298-00-0
Mevinphos
ND
mg/kg
0.242
1
08/21/22 16:12
08/22/22 03:44
7786-34-7
Naled
ND
mg/kg
0.242
1
08/21/22 16:12
08/22/22 03:44
300-76-5
Phorate
ND
mg/kg
0.242
1
08/21/22 16:12
08/22/22 03:44
298-02-2
Ronnel
ND
mg/kg
0.242
1
08/21/22 16:12
08/22/22 03:44
299-84-3
Stirophos (Tetrachlorvinphos)
ND
mg/kg
0.242
1
08/21/22 16:12
08/22/22 03:44
22248-79-9
Sulfotepp (ThiodiphosphoricAc
ND
mg/kg
0.242
1
08/21/22 16:12
08/22/22 03:44
3689-24-5
TEPP
ND
mg/kg
2.42
1
08/21/22 16:12
08/22/22 03:44
107-49-3
Tokuthion (Prothiofos)
ND
mg/kg
0.242
1
08/21/22 16:12
08/22/22 03:44
34643-46-4
Trichloronate
ND
mg/kg
0.242
1
08/21/22 16:12
08/22/22 03:44
327-98-0
Surrogates
Triphenyl phosphate (S)
64.1
%
36.0-121
1
08/21/22 16:12
08/22/22 03:44
115-86-6
8081 GCS Pesticides
Analytical Method: EPA 8081 B Preparation Method: EPA 3546
Pace Analytical
Services - Charlotte
alpha-BHC
ND
ug/kg
115
10
08/24/22 07:17
08/26/22 18:27
319-84-6
gamma-BHC (Lindane)
ND
ug/kg
115
10
08/24/22 07:17
08/26/22 18:27
58-89-9
beta-BHC
ND
ug/kg
115
10
08/24/22 07:17
08/26/22 18:27
319-85-7
Heptachlor
ND
ug/kg
115
10
08/24/22 07:17
08/26/22 18:27
76-44-8
delta-BHC
ND
ug/kg
115
10
08/24/22 07:17
08/26/22 18:27
319-86-8
Aldrin
ND
ug/kg
115
10
08/24/22 07:17
08/26/22 18:27
309-00-2
Heptachlor epoxide
ND
ug/kg
115
10
08/24/22 07:17
08/26/22 18:27
1024-57-3
Endosulfan I
ND
ug/kg
115
10
08/24/22 07:17
08/26/22 18:27
959-98-8
4,4'-DDE
ND
ug/kg
115
10
08/24/22 07:17
08/26/22 18:27
72-55-9
Dieldrin
ND
ug/kg
115
10
08/24/22 07:17
08/26/22 18:27
60-57-1
Endrin
ND
ug/kg
115
10
08/24/22 07:17
08/26/22 18:27
72-20-8
4,4'-DDD
ND
ug/kg
115
10
08/24/22 07:17
08/26/22 18:27
72-54-8
Endosulfan II
ND
ug/kg
115
10
08/24/22 07:17
08/26/22 18:27
33213-65-9
4,4'-DDT
ND
ug/kg
115
10
08/24/22 07:17
08/26/22 18:27
50-29-3
REPORT OF LABORATORY ANALYSIS
LO
This report shall not be reproduced, except in full,
Date: 10/25/2022 02:36 PM without the written consent of Pace Analytical Services, LLC. Page 41 of 165

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: WASTE CHARACTERIZATION
Pace Project No.: 92621331
Sample: GP-6 2-3' Lab ID: 92621331006 Collected: 08/16/22 12:30 Received: 08/17/22 16:15 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8081 GCS Pesticides
Endrin aldehyde
Endosulfan sulfate
Methoxychlor
Endrin ketone
Chlordane (Technical)
Toxaphene
Mirex
Hexachlorobenzene
Surrogates
Tetrachloro-m-xylene (S)
Decachlorobiphenyl (S)
8082 GCS PCB
PCB-1016 (Aroclor 1016)
PCB-1221 (Aroclor 1221)
PCB-1232 (Aroclor 1232)
PCB-1242 (Aroclor 1242)
PCB-1248 (Aroclor 1248)
PCB-1254 (Aroclor 1254)
PCB-1260 (Aroclor 1260)
Surrogates
Decachlorobiphenyl (S)
Analytical Method: EPA 8081 B Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
ND
ug/kg
115
10
08/24/22 07:17
08/26/22 18:27
7421-93-4
ND
ug/kg
115
10
08/24/22 07:17
08/26/22 18:27
1031-07-8
ND
ug/kg
288
10
08/24/22 07:17
08/26/22 18:27
72-43-5
ND
ug/kg
115
10
08/24/22 07:17
08/26/22 18:27
53494-70-5
958
ug/kg
576
10
08/24/22 07:17
08/26/22 18:27
57-74-9
ND
ug/kg
403
10
08/24/22 07:17
08/26/22 18:27
8001-35-2
ND
ug/kg
288
10
08/24/22 07:17
08/26/22 18:27
2385-85-5
ND
ug/kg
115
10
08/24/22 07:17
08/26/22 18:27
118-74-1
0
%
10-133
10
08/24/22 07:17
08/26/22 18:27
877-09-8 D3,S4
0
%
10-146
10
08/24/22 07:17
08/26/22 18:27
2051-24-3 S4
Analytical Method: EPA 8082A Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
ND
ug/kg
1430
20
08/19/22 15:53
08/24/22 07:03
12674-11-2
ND
ug/kg
1430
20
08/19/22 15:53
08/24/22 07:03
11104-28-2
ND
ug/kg
1430
20
08/19/22 15:53
08/24/22 07:03
11141-16-5
ND
ug/kg
1430
20
08/19/22 15:53
08/24/22 07:03
53469-21-9
ND
ug/kg
1430
20
08/19/22 15:53
08/24/22 07:03
12672-29-6
2020
ug/kg
1430
20
08/19/22 15:53
08/24/22 07:03
11097-69-1
ND
ug/kg
1430
20
08/19/22 15:53
08/24/22 07:03
11096-82-5
0
%
10-160
20
08/19/22 15:53
08/24/22 07:03
2051-24-3 D3,S4
6010 MET ICP
Analytical Method: EPA 6010 Preparation Method: EPA 3050
Pace Analytical
Services - Ormond Beach
Tin
161
mg/kg
6.1
1
08/30/2219:03
08/31/22 18:27
7440-31-5
6020 MET ICPMS
Analytical Method: EPA 6020 Preparation Method: EPA 3050
Pace Analytical
Services - Ormond Beach
Antimony
255
mg/kg
4.9
20
08/27/22 00:15
08/29/22 19:44
7440-36-0
1g,N2
Arsenic
7.2
mg/kg
2.4
20
08/27/22 00:15
08/29/22 19:44
7440-38-2
1g
Barium
1640
mg/kg
24.3
200
08/27/22 00:15
08/31/22 14:12
7440-39-3
1g
Beryllium
0.38
mg/kg
0.29
20
08/27/22 00:15
08/29/22 19:44
7440-41-7
1g
Cadmium
15.0
mg/kg
0.29
20
08/27/22 00:15
08/29/22 19:44
7440-43-9
1g
Chromium
2240
mg/kg
24.3
200
08/27/22 00:15
08/31/22 14:12
7440-47-3
1g
Cobalt
11.4
mg/kg
2.4
20
08/27/22 00:15
08/29/22 19:44
7440-48-4
1g
Copper
687
mg/kg
4.9
20
08/27/22 00:15
08/29/22 19:44
7440-50-8
1g
Lead
3860
mg/kg
24.3
200
08/27/22 00:15
08/31/22 14:12
7439-92-1
1g
Nickel
14.5
mg/kg
2.4
20
08/27/22 00:15
08/29/22 19:44
7440-02-0
1g
Selenium
8.1
mg/kg
2.4
20
08/27/22 00:15
08/29/22 19:44
7782-49-2
1g
Silver
165
mg/kg
2.9
200
08/27/22 00:15
08/31/22 14:12
7440-22-4
1g
Thallium
ND
mg/kg
2.4
20
08/27/22 00:15
08/29/22 19:44
7440-28-0
1g
Vanadium
34.8
mg/kg
2.4
20
08/27/22 00:15
08/29/22 19:44
7440-62-2
1g
Zinc
449
mg/kg
97.1
20
08/27/22 00:15
08/29/22 19:44
7440-66-6
1g
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/25/2022 02:36 PM without the written consent of Pace Analytical Services, LLC. Page 42 of 165

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: WASTE CHARACTERIZATION
Pace Project No.: 92621331
Sample: GP-6 2-3' Lab ID: 92621331006 Collected: 08/16/22 12:30 Received: 08/17/22 16:15 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
7471 Mercury Analytical Method: EPA 7471 Preparation Method: EPA 7471
Pace Analytical Services - Ormond Beach
Mercury 6.7 mg/kg 0.41 20 08/24/22 07:26 08/24/22 11:36 7439-97-6
8270E MSSV Microwave
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical
Services - Charlotte
Acenaphthene
ND
ug/kg
7320
10
08/29/22 10:52
08/30/22 17:09
83-32-9
Acenaphthylene
ND
ug/kg
7320
10
08/29/22 10:52
08/30/22 17:09
208-96-8
Acetophenone
ND
ug/kg
7320
10
08/29/22 10:52
08/30/22 17:09
98-86-2
2-Acetylaminofluorene
ND
ug/kg
14600
10
08/29/22 10:52
08/30/22 17:09
53-96-3
4-Aminobiphenyl
ND
ug/kg
7320
10
08/29/22 10:52
08/30/22 17:09
92-67-1
Anthracene
ND
ug/kg
7320
10
08/29/22 10:52
08/30/22 17:09
120-12-7
Benzo(a)anthracene
ND
ug/kg
7320
10
08/29/22 10:52
08/30/22 17:09
56-55-3
Benzo(a)pyrene
ND
ug/kg
7320
10
08/29/22 10:52
08/30/22 17:09
50-32-8
Benzo(b)fluoranthene
ND
ug/kg
7320
10
08/29/22 10:52
08/30/22 17:09
205-99-2
Benzo(g,h,i)perylene
ND
ug/kg
7320
10
08/29/22 10:52
08/30/22 17:09
191-24-2
Benzo(k)fluoranthene
ND
ug/kg
7320
10
08/29/22 10:52
08/30/22 17:09
207-08-9
Benzyl alcohol
ND
ug/kg
14600
10
08/29/22 10:52
08/30/22 17:09
100-51-6
bis(2-Chloroethoxy)methane
ND
ug/kg
7320
10
08/29/22 10:52
08/30/22 17:09
111-91-1
bis(2-Chloroethyl) ether
ND
ug/kg
7320
10
08/29/22 10:52
08/30/22 17:09
111-44-4
2-Chloronaphthalene
ND
ug/kg
7320
10
08/29/22 10:52
08/30/22 17:09
91-58-7
2-Chlorophenol
ND
ug/kg
7320
10
08/29/22 10:52
08/30/22 17:09
95-57-8
4-Chlorophenylphenyl ether
ND
ug/kg
7320
10
08/29/22 10:52
08/30/22 17:09
7005-72-3
Chrysene
ND
ug/kg
7320
10
08/29/22 10:52
08/30/22 17:09
218-01-9
n-Decane
ND
ug/kg
7320
10
08/29/22 10:52
08/30/22 17:09
124-18-5
Diallate
ND
ug/kg
7320
10
08/29/22 10:52
08/30/22 17:09
2303-16-4
Dibenz(a,h)anthracene
ND
ug/kg
7320
10
08/29/22 10:52
08/30/22 17:09
53-70-3
Dibenzo(a,e)pyrene
ND
ug/kg
22200
10
08/29/22 10:52
08/30/22 17:09
192-65-4
Dibenzofuran
ND
ug/kg
7320
10
08/29/22 10:52
08/30/22 17:09
132-64-9
2,3-Dibromo-1-propanol phosph
ND
ug/kg
36600
10
08/29/22 10:52
08/30/22 17:09
126-72-7
1,2-Dichlorobenzene
ND
ug/kg
7320
10
08/29/22 10:52
08/30/22 17:09
95-50-1
1,3-Dichlorobenzene
ND
ug/kg
7320
10
08/29/22 10:52
08/30/22 17:09
541-73-1
1,4-Dichlorobenzene
ND
ug/kg
7320
10
08/29/22 10:52
08/30/22 17:09
106-46-7
3,3'-Dichlorobenzidine
ND
ug/kg
14600
10
08/29/22 10:52
08/30/22 17:09
91-94-1
2,4-Dichlorophenol
ND
ug/kg
7320
10
08/29/22 10:52
08/30/22 17:09
120-83-2
2,6-Dichlorophenol
ND
ug/kg
7320
10
08/29/22 10:52
08/30/22 17:09
87-65-0
2,3-Dichloroaniline
ND
ug/kg
7320
10
08/29/22 10:52
08/30/22 17:09
608-27-5
Diethylphthalate
ND
ug/kg
7320
10
08/29/22 10:52
08/30/22 17:09
84-66-2
Dimethoate
ND
ug/kg
14600
10
08/29/22 10:52
08/30/22 17:09
60-51-5
P-Dimethylaminoazobenzene
ND
ug/kg
7320
10
08/29/22 10:52
08/30/22 17:09
60-11-7
7,12-Dimethylbenz(a)anthracene
ND
ug/kg
7320
10
08/29/22 10:52
08/30/22 17:09
57-97-6
3,3'-Dimethylbenzidine
ND
ug/kg
14600
10
08/29/22 10:52
08/30/22 17:09
119-93-7
2,4-Dimethylphenol
ND
ug/kg
7320
10
08/29/22 10:52
08/30/22 17:09
105-67-9
a,a-Dimethylphenylethylamine
ND
ug/kg
36600
10
08/29/22 10:52
08/30/22 17:09
122-09-8
Dimethylphthalate
ND
ug/kg
7320
10
08/29/22 10:52
08/30/22 17:09
131-11-3
Di-n-butylphthalate
ND
ug/kg
7320
10
08/29/22 10:52
08/30/22 17:09
84-74-2
4,6-Dinitro-2-methyl phenol
ND
ug/kg
14600
10
08/29/22 10:52
08/30/22 17:09
534-52-1
REPORT OF LABORATORY ANALYSIS
v1
IL
IL
IH
v1
This report shall not be reproduced, except in full,
Date: 10/25/2022 02:36 PM without the written consent of Pace Analytical Services, LLC. Page 43 of 165

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: WASTE CHARACTERIZATION
Pace Project No.: 92621331
Sample: GP-6 2-3' Lab ID: 92621331006 Collected: 08/16/22 12:30 Received: 08/17/22 16:15 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No
8270E MSSV Microwave
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical
Services - Charlotte
1,3-Dinitrobenzene
ND
ug/kg
7320
10
08/29/22 10:52
08/30/22 17:09
99-65-0
1,4-Dinitrobenzene
ND
ug/kg
7320
10
08/29/22 10:52
08/30/22 17:09
100-25-4
2,4-Dinitrophenol
ND
ug/kg
36600
10
08/29/22 10:52
08/30/22 17:09
51-28-5
2,4-Dinitrotoluene
ND
ug/kg
7320
10
08/29/22 10:52
08/30/22 17:09
121-14-2
2,6-Dinitrotoluene
ND
ug/kg
7320
10
08/29/22 10:52
08/30/22 17:09
606-20-2
Di-n-octylphthalate
ND
ug/kg
7320
10
08/29/22 10:52
08/30/22 17:09
117-84-0
Dinoseb
ND
ug/kg
14600
10
08/29/22 10:52
08/30/22 17:09
88-85-7
Diphenylamine
ND
ug/kg
7320
10
08/29/22 10:52
08/30/22 17:09
122-39-4
Diphenyl ether (Phenyl ether)
ND
ug/kg
11100
10
08/29/22 10:52
08/30/22 17:09
101-84-8
1,2-Diphenylhydrazine
ND
ug/kg
7320
10
08/29/22 10:52
08/30/22 17:09
122-66-7
Disulfoton
ND
ug/kg
7320
10
08/29/22 10:52
08/30/22 17:09
298-04-4
bis(2- Ethyl hexyl)phthalate
ND
ug/kg
7320
10
08/29/22 10:52
08/30/22 17:09
117-81-7
Ethyl methanesulfonate
ND
ug/kg
14600
10
08/29/22 10:52
08/30/22 17:09
62-50-0
Famphur
ND
ug/kg
14600
10
08/29/22 10:52
08/30/22 17:09
52-85-7
Fluoranthene
ND
ug/kg
7320
10
08/29/22 10:52
08/30/22 17:09
206-44-0
Fluorene
ND
ug/kg
7320
10
08/29/22 10:52
08/30/22 17:09
86-73-7
Hexachloro-1,3-butadiene
ND
ug/kg
7320
10
08/29/22 10:52
08/30/22 17:09
87-68-3
Hexachlorobenzene
ND
ug/kg
7320
10
08/29/22 10:52
08/30/22 17:09
118-74-1
Hexachlorocyclopentadiene
ND
ug/kg
7320
10
08/29/22 10:52
08/30/22 17:09
77-47-4
Hexachloroethane
ND
ug/kg
7320
10
08/29/22 10:52
08/30/22 17:09
67-72-1
Hexachlorophene
ND
ug/kg
73200
10
08/29/22 10:52
08/30/22 17:09
70-30-4
Hexachloropropene
ND
ug/kg
7320
10
08/29/22 10:52
08/30/22 17:09
1888-71-7
Indeno(1,2,3-cd)pyrene
ND
ug/kg
7320
10
08/29/22 10:52
08/30/22 17:09
193-39-5
Isodrin
ND
ug/kg
7320
10
08/29/22 10:52
08/30/22 17:09
465-73-6
Isophorone
ND
ug/kg
7320
10
08/29/22 10:52
08/30/22 17:09
78-59-1
Isosafrole
ND
ug/kg
7320
10
08/29/22 10:52
08/30/22 17:09
120-58-1
Kepone
ND
ug/kg
14600
10
08/29/22 10:52
08/30/22 17:09
143-50-0
Methapyrilene
ND
ug/kg
36600
10
08/29/22 10:52
08/30/22 17:09
91-80-5
3-Methylcholanthrene
ND
ug/kg
7320
10
08/29/22 10:52
08/30/22 17:09
56-49-5
4,4'-Methylene-bis(2-chloroani
ND
ug/kg
14600
10
08/29/22 10:52
08/30/22 17:09
101-14-4
Methyl methanesulfonate
ND
ug/kg
14600
10
08/29/22 10:52
08/30/22 17:09
66-27-3
1-Methylnaphthalene
ND
ug/kg
7320
10
08/29/22 10:52
08/30/22 17:09
90-12-0
2-Methylnaphthalene
ND
ug/kg
7320
10
08/29/22 10:52
08/30/22 17:09
91-57-6
2-Methyl-5-nitroaniline
ND
ug/kg
7320
10
08/29/22 10:52
08/30/22 17:09
99-55-8
Methyl parathion
ND
ug/kg
7320
10
08/29/22 10:52
08/30/22 17:09
298-00-0
2-Methylphenol(o-Cresol)
ND
ug/kg
7320
10
08/29/22 10:52
08/30/22 17:09
95-48-7
3&4-Methyl phenol (m&p Cresol)
ND
ug/kg
7320
10
08/29/22 10:52
08/30/22 17:09
15831-10-4
1-Naphthalenamine
ND
ug/kg
14600
10
08/29/22 10:52
08/30/22 17:09
134-32-7
2-Naphthalenamine
ND
ug/kg
14600
10
08/29/22 10:52
08/30/22 17:09
91-59-8
Naphthalene
ND
ug/kg
7320
10
08/29/22 10:52
08/30/22 17:09
91-20-3
1,4-Naphthoquinone
ND
ug/kg
36600
10
08/29/22 10:52
08/30/22 17:09
130-15-4
2-Nitroaniline
ND
ug/kg
36600
10
08/29/22 10:52
08/30/22 17:09
88-74-4
3-Nitroaniline
ND
ug/kg
36600
10
08/29/22 10:52
08/30/22 17:09
99-09-2
4-Nitroaniline
ND
ug/kg
14600
10
08/29/22 10:52
08/30/22 17:09
100-01-6
Nitrobenzene
ND
ug/kg
7320
10
08/29/22 10:52
08/30/22 17:09
98-95-3
REPORT OF LABORATORY ANALYSIS
Qual
IH,L2
IH
This report shall not be reproduced, except in full,
Date: 10/25/2022 02:36 PM without the written consent of Pace Analytical Services, LLC. Page 44 of 165

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: WASTE CHARACTERIZATION
Pace Project No.: 92621331
Sample: GP-6 2-3' Lab ID: 92621331006 Collected: 08/16/22 12:30 Received: 08/17/22 16:15 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters
8270E MSSV Microwave
2-Nitrophenol
4-Nitrophenol
4-Nitroquinoline-n-oxide
5-Nitro-o-toluidine
N-Nitrosodiethylamine
N-Nitrosodimethylamine
N-Nitroso-di-n-butylamine
N-Nitroso-di-n-propylamine
N-Nitrosodiphenylamine
N-Nitrosomethylethylamine
N-Nitrosomorpholine
N-Nitrosopiperidine
N-Nitrosopyrrolidine
n-Octadecane
O,O,O-Triethylphosphorothioate
2,2'-Oxybis(1-chloropropane)
Parathion (Ethyl parathion)
Pentachlorobenzene
Pentachloroethane
Pentachloronitrobenzene
Pentachlorophenol
Phenacetin
Phenanthrene
Phenol
p-Phenylenediamine
Phorate
Phthalic anhydride
2-Picoline
Pronamide
Pyrene
Pyridine
Safrole
Sulfotepp (ThiodiphosphoricAc
Terpineol
1,2,4,5-Tetrachlorobenzene
2,3,4,6-Tetrachlorophenol
Thionazin
O-Toluidine
1,2,4-Trichlorobenzene
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
1,3,5-Trinitrobenzene
Surrogates
2-Fluorobiphenyl (S)
Terphenyl-d14 (S)
Results Units Report Limit DF Prepared Analyzed CAS No. Qual
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
ND
ug/kg
7320
10
08/29/2210:52
08/30/2217:09
88-75-5
ND
ug/kg
36600
10
08/29/2210:52
08/30/2217:09
100-02-7
ND
ug/kg
36600
10
08/29/2210:52
08/30/2217:09
56-57-5
v2
ND
ug/kg
7320
10
08/29/2210:52
08/30/2217:09
99-55-8
ND
ug/kg
7320
10
08/29/2210:52
08/30/2217:09
55-18-5
ND
ug/kg
7320
10
08/29/2210:52
08/30/2217:09
62-75-9
ND
ug/kg
7320
10
08/29/2210:52
08/30/2217:09
924-16-3
ND
ug/kg
7320
10
08/29/2210:52
08/30/2217:09
621-64-7
ND
ug/kg
7320
10
08/29/2210:52
08/30/2217:09
86-30-6
ND
ug/kg
7320
10
08/29/2210:52
08/30/2217:09
10595-95-6
ND
ug/kg
7320
10
08/29/2210:52
08/30/2217:09
59-89-2
ND
ug/kg
14600
10
08/29/2210:52
08/30/2217:09
100-75-4
ND
ug/kg
14600
10
08/29/2210:52
08/30/2217:09
930-55-2
ND
ug/kg
7320
10
08/29/2210:52
08/30/2217:09
593-45-3
ND
ug/kg
7320
10
08/29/2210:52
08/30/2217:09
126-68-1
ND
ug/kg
7320
10
08/29/2210:52
08/30/2217:09
108-60-1
ND
ug/kg
7320
10
08/29/2210:52
08/30/2217:09
56-38-2
ND
ug/kg
7320
10
08/29/2210:52
08/30/2217:09
608-93-5
ND
ug/kg
7320
10
08/29/2210:52
08/30/2217:09
76-01-7
ND
ug/kg
7320
10
08/29/2210:52
08/30/2217:09
82-68-8
ND
ug/kg
14600
10
08/29/2210:52
08/30/2217:09
87-86-5
ND
ug/kg
14600
10
08/29/2210:52
08/30/2217:09
62-44-2
ND
ug/kg
7320
10
08/29/2210:52
08/30/2217:09
85-01-8
ND
ug/kg
7320
10
08/29/2210:52
08/30/2217:09
108-95-2
ND
ug/kg
14600
10
08/29/2210:52
08/30/2217:09
106-50-3
IL
ND
ug/kg
7320
10
08/29/2210:52
08/30/2217:09
298-02-2
L2
ND
ug/kg
55500
10
08/29/2210:52
08/30/2217:09
85-44-9
ND
ug/kg
7320
10
08/29/2210:52
08/30/2217:09
109-06-8
ND
ug/kg
14600
10
08/29/2210:52
08/30/2217:09
23950-58-5
ND
ug/kg
7320
10
08/29/2210:52
08/30/2217:09
129-00-0
ND
ug/kg
7320
10
08/29/2210:52
08/30/2217:09
110-86-1
ND
ug/kg
14600
10
08/29/2210:52
08/30/2217:09
94-59-7
ND
ug/kg
7320
10
08/29/2210:52
08/30/2217:09
3689-24-5
ND
ug/kg
7320
10
08/29/2210:52
08/30/2217:09
98-55-5
ND
ug/kg
7320
10
08/29/2210:52
08/30/2217:09
95-94-3
ND
ug/kg
7320
10
08/29/2210:52
08/30/2217:09
58-90-2
ND
ug/kg
7320
10
08/29/2210:52
08/30/2217:09
297-97-2
ND
ug/kg
7320
10
08/29/2210:52
08/30/2217:09
95-53-4
ND
ug/kg
7320
10
08/29/2210:52
08/30/2217:09
120-82-1
ND
ug/kg
7320
10
08/29/2210:52
08/30/2217:09
95-95-4
ND
ug/kg
7320
10
08/29/2210:52
08/30/2217:09
88-06-2
ND
ug/kg
7320
10
08/29/2210:52
08/30/2217:09
99-35-4
0
%
19-130
10
08/29/2210:52
08/30/2217:09
321-60-8
D3,S4
0
%
15-130
10
08/29/2210:52
08/30/2217:09
1718-51-0
S4
REPORT
OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/25/2022 02:36 PM without the written consent of Pace Analytical Services, LLC. Page 45 of 165

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: WASTE CHARACTERIZATION
Pace Project No.: 92621331
Sample: GP-6 2-3'
Lab ID: 92621331006 Collected: 08/16/22 12:30 Received: 08/17/22 16:15 Matrix: Solid
Results reported on a "dry weight"
basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters
Results Units Report Limit DF Prepared
Analyzed
CAS No. Qual
8270E MSSV Microwave
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
Surrogates
Phenol-d6 (S)
0 % 18-130 10 08/29/22 10:52
08/30/22 17:09
13127-88-3 S4
2-Fluorophenol (S)
0 % 18-130 10 08/29/22 10:52
08/30/22 17:09
367-12-4 S4
2,4,6-Tribromophenol (S)
0 % 18-130 10 08/29/22 10:52
08/30/22 17:09
118-79-6 S4
Nitrobenzene-d5 (S)
0 % 21-130 10 08/29/22 10:52
08/30/22 17:09
4165-60-0 S4
Percent Moisture
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
54.3 % 0.10 1
08/22/22 15:39
N2
1010 Flash poi nt,Closed Cup
Analytical Method: EPA 1010B
Pace Analytical Services -Asheville
Flashpoint
>200 deg F 70.0 1
08/22/22 14:20
Total Solids 2540 G-2011
Analytical Method: SM 2540G Preparation Method: SM 2540 G
Pace National - Mt. Juliet
Total Solids
41.4 % 1 08/23/22 10:15
08/23/22 10:31
4500S21) Sulfide Soil
Analytical Method: SM 4500-S2D-2011 Modified Preparation Method: SM
4500-S2D-2011 Modified
Pace Analytical Services -Asheville
Sulfide
ND mg/kg 10.5 1 08/20/22 02:37
08/20/22 06:39
18496-25-8
9045 pH Soil
Analytical Method: EPA 9045D
Pace Analytical Services -Asheville
pH at 25 Degrees C
4.2 Std. Units 0.10 1
08/23/22 18:13
H3
9012 Cyanide, Total
Analytical Method: EPA 9012 Preparation Method: EPA 9012
Pace Analytical Services - Ormond Beach
Cyanide
12.3 mg/kg 5.5 10 08/29/22 09:41
08/29/22 15:20
57-12-5
Date: 10/25/2022 02:36 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 46 of 165

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: WASTE CHARACTERIZATION
Pace Project No.: 92621331
Sample: GP-7 2-3' Lab ID: 92621331007 Collected: 08/16/22 12:40 Received: 08/17/22 16:15 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
OP Pesticides 8141 B
Analytical Method: EPA 8141 B Preparation Method: 3546
Pace National
- Mt. Juliet
Azinphos, methyl (Guthion)
ND
mg/kg
0.222
1
08/21/22 16:12
08/22/22 04:18
86-50-0
Bolstar
ND
mg/kg
0.222
1
08/21/22 16:12
08/22/22 04:18
35400-43-2
Chlorpyrifos
ND
mg/kg
0.222
1
08/21/22 16:12
08/22/22 04:18
2921-88-2
Coumaphos
ND
mg/kg
0.222
1
08/21/22 16:12
08/22/22 04:18
56-72-4
Total Demeton
ND
mg/kg
0.155
1
08/21/22 16:12
08/22/22 04:18
8065-48-3
Diazinon
ND
mg/kg
0.222
1
08/21/22 16:12
08/22/22 04:18
333-41-5
Dichlorvos
ND
mg/kg
0.222
1
08/21/22 16:12
08/22/22 04:18
62-73-7
Dimethoate
ND
mg/kg
0.222
1
08/21/22 16:12
08/22/22 04:18
60-51-5
Disulfoton
ND
mg/kg
0.222
1
08/21/22 16:12
08/22/22 04:18
298-04-4
EPN (ENT)
ND
mg/kg
0.222
1
08/21/22 16:12
08/22/22 04:18
2104-64-5
Ethoprop
ND
mg/kg
0.222
1
08/21/22 16:12
08/22/22 04:18
13194-48-4
Parathion (Ethyl parathion)
ND
mg/kg
0.222
1
08/21/22 16:12
08/22/22 04:18
56-38-2
Fensulfothion
ND
mg/kg
0.222
1
08/21/22 16:12
08/22/22 04:18
115-90-2
Fenthion
ND
mg/kg
0.222
1
08/21/22 16:12
08/22/22 04:18
55-38-9
Malathion
ND
mg/kg
0.222
1
08/21/22 16:12
08/22/22 04:18
121-75-5
Merphos
ND
mg/kg
0.222
1
08/21/22 16:12
08/22/22 04:18
150-50-5
Methyl parathion
ND
mg/kg
0.222
1
08/21/22 16:12
08/22/22 04:18
298-00-0
Mevinphos
ND
mg/kg
0.222
1
08/21/22 16:12
08/22/22 04:18
7786-34-7
Naled
ND
mg/kg
0.222
1
08/21/22 16:12
08/22/22 04:18
300-76-5
Phorate
ND
mg/kg
0.222
1
08/21/22 16:12
08/22/22 04:18
298-02-2
Ronnel
ND
mg/kg
0.222
1
08/21/22 16:12
08/22/22 04:18
299-84-3
Stirophos (Tetrachlorvinphos)
ND
mg/kg
0.222
1
08/21/22 16:12
08/22/22 04:18
22248-79-9
Sulfotepp (ThiodiphosphoricAc
ND
mg/kg
0.222
1
08/21/22 16:12
08/22/22 04:18
3689-24-5
TEPP
ND
mg/kg
2.22
1
08/21/22 16:12
08/22/22 04:18
107-49-3
Tokuthion (Prothiofos)
ND
mg/kg
0.222
1
08/21/22 16:12
08/22/22 04:18
34643-46-4
Trichloronate
ND
mg/kg
0.222
1
08/21/22 16:12
08/22/22 04:18
327-98-0
Surrogates
Triphenyl phosphate (S)
60.4
%
36.0-121
1
08/21/22 16:12
08/22/22 04:18
115-86-6
8081 GCS Pesticides
Analytical Method: EPA 8081 B Preparation Method: EPA 3546
Pace Analytical
Services - Charlotte
Aldrin
ND
ug/kg
297
10
08/24/22 07:17
08/26/22 18:39
309-00-2
alpha-BHC
ND
ug/kg
297
10
08/24/22 07:17
08/26/22 18:39
319-84-6
beta-BHC
ND
ug/kg
297
10
08/24/22 07:17
08/26/22 18:39
319-85-7
delta-BHC
ND
ug/kg
297
10
08/24/22 07:17
08/26/22 18:39
319-86-8
gamma-BHC (Lindane)
ND
ug/kg
297
10
08/24/22 07:17
08/26/22 18:39
58-89-9
Chlordane (Technical)
ND
ug/kg
1480
10
08/24/22 07:17
08/26/22 18:39
57-74-9
4,4'-DDD
ND
ug/kg
297
10
08/24/22 07:17
08/26/22 18:39
72-54-8
4,4'-DDE
ND
ug/kg
297
10
08/24/22 07:17
08/26/22 18:39
72-55-9
4,4'-DDT
ND
ug/kg
297
10
08/24/22 07:17
08/26/22 18:39
50-29-3
Dieldrin
ND
ug/kg
297
10
08/24/22 07:17
08/26/22 18:39
60-57-1
Endosulfan I
ND
ug/kg
297
10
08/24/22 07:17
08/26/22 18:39
959-98-8
Endosulfan II
ND
ug/kg
297
10
08/24/22 07:17
08/26/22 18:39
33213-65-9
Endosulfan sulfate
ND
ug/kg
297
10
08/24/22 07:17
08/26/22 18:39
1031-07-8
Endrin
ND
ug/kg
297
10
08/24/22 07:17
08/26/22 18:39
72-20-8
REPORT OF LABORATORY ANALYSIS
LO
This report shall not be reproduced, except in full,
Date: 10/25/2022 02:36 PM without the written consent of Pace Analytical Services, LLC. Page 47 of 165

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: WASTE CHARACTERIZATION
Pace Project No.: 92621331
Sample: GP-7 2-3' Lab ID: 92621331007 Collected: 08/16/22 12:40 Received: 08/17/22 16:15 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8081 GCS Pesticides
Endrin aldehyde
Endrin ketone
Heptachlor
Heptachlor epoxide
Hexachlorobenzene
Methoxychlor
Mirex
Toxaphene
Surrogates
Tetrachloro-m-xylene (S)
Decachlorobiphenyl (S)
8082 GCS PCB
PCB-1016 (Aroclor 1016)
PCB-1221 (Aroclor 1221)
PCB-1232 (Aroclor 1232)
PCB-1242 (Aroclor 1242)
PCB-1248 (Aroclor 1248)
PCB-1254 (Aroclor 1254)
PCB-1260 (Aroclor 1260)
Surrogates
Decachlorobiphenyl (S)
Analytical Method: EPA 8081 B Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
ND
ug/kg
297
10
08/24/22 07:17
08/26/22 18:39
7421-93-4
ND
ug/kg
297
10
08/24/22 07:17
08/26/22 18:39
53494-70-5
ND
ug/kg
297
10
08/24/22 07:17
08/26/22 18:39
76-44-8
ND
ug/kg
297
10
08/24/22 07:17
08/26/22 18:39
1024-57-3
ND
ug/kg
297
10
08/24/22 07:17
08/26/22 18:39
118-74-1
ND
ug/kg
742
10
08/24/22 07:17
08/26/22 18:39
72-43-5
ND
ug/kg
742
10
08/24/22 07:17
08/26/22 18:39
2385-85-5
ND
ug/kg
1040
10
08/24/22 07:17
08/26/22 18:39
8001-35-2
0
%
10-133
10
08/24/22 07:17
08/26/22 18:39
877-09-8 D3,S4
0
%
10-146
10
08/24/22 07:17
08/26/22 18:39
2051-24-3 S4
Analytical Method: EPA 8082A Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
ND
ug/kg
1410
20
08/19/22 15:53
08/24/22 07:18
12674-11-2
ND
ug/kg
1410
20
08/19/22 15:53
08/24/22 07:18
11104-28-2
ND
ug/kg
1410
20
08/19/22 15:53
08/24/22 07:18
11141-16-5
ND
ug/kg
1410
20
08/19/22 15:53
08/24/22 07:18
53469-21-9
ND
ug/kg
1410
20
08/19/22 15:53
08/24/22 07:18
12672-29-6
1450
ug/kg
1410
20
08/19/22 15:53
08/24/22 07:18
11097-69-1
ND
ug/kg
1410
20
08/19/22 15:53
08/24/22 07:18
11096-82-5
0
%
10-160
20
08/19/22 15:53
08/24/22 07:18
2051-24-3 D3,S4
6010 MET ICP
Analytical Method: EPA 6010 Preparation Method: EPA 3050
Pace Analytical
Services - Ormond Beach
Tin
214
mg/kg
6.7
1
08/30/2219:03
08/31/2218:30
7440-31-5
6020 MET ICPMS
Analytical Method: EPA 6020 Preparation Method: EPA 3050
Pace Analytical
Services - Ormond Beach
Antimony
429
mg/kg
4.9
20
08/27/22 00:15
08/29/22 19:47
7440-36-0
1g,N2
Arsenic
5.7
mg/kg
2.4
20
08/27/22 00:15
08/29/22 19:47
7440-38-2
1g
Barium
2600
mg/kg
24.4
200
08/27/22 00:15
08/31/22 14:14
7440-39-3
1g
Beryllium
0.55
mg/kg
0.29
20
08/27/22 00:15
08/29/22 19:47
7440-41-7
1g
Cadmium
30.3
mg/kg
0.29
20
08/27/22 00:15
08/29/22 19:47
7440-43-9
1g
Chromium
2850
mg/kg
24.4
200
08/27/22 00:15
08/31/22 14:14
7440-47-3
1g
Cobalt
9.4
mg/kg
2.4
20
08/27/22 00:15
08/29/22 19:47
7440-48-4
1g
Copper
652
mg/kg
4.9
20
08/27/22 00:15
08/29/22 19:47
7440-50-8
1g
Lead
903
mg/kg
24.4
200
08/27/22 00:15
08/31/22 14:14
7439-92-1
1g
Nickel
13.7
mg/kg
2.4
20
08/27/22 00:15
08/29/22 19:47
7440-02-0
1g
Selenium
6.3
mg/kg
2.4
20
08/27/22 00:15
08/29/22 19:47
7782-49-2
1g
Silver
260
mg/kg
2.9
200
08/27/22 00:15
08/31/22 14:14
7440-22-4
1g
Thallium
ND
mg/kg
2.4
20
08/27/22 00:15
08/29/22 19:47
7440-28-0
1g
Vanadium
44.7
mg/kg
2.4
20
08/27/22 00:15
08/29/22 19:47
7440-62-2
1g
Zinc
207
mg/kg
97.4
20
08/27/22 00:15
08/29/22 19:47
7440-66-6
1g
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/25/2022 02:36 PM without the written consent of Pace Analytical Services, LLC. Page 48 of 165

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: WASTE CHARACTERIZATION
Pace Project No.: 92621331
Sample: GP-7 2-3' Lab ID: 92621331007 Collected: 08/16/22 12:40 Received: 08/17/22 16:15 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
7471 Mercury Analytical Method: EPA 7471 Preparation Method: EPA 7471
Pace Analytical Services - Ormond Beach
Mercury 18.2 mg/kg 0.42 20 08/24/22 07:26 08/24/22 11:54 7439-97-6
8270E MSSV Microwave
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical
Services - Charlotte
Acenaphthene
ND
ug/kg
7130
10
08/29/22 10:52
08/30/22 12:23
83-32-9
Acenaphthylene
ND
ug/kg
7130
10
08/29/22 10:52
08/30/22 12:23
208-96-8
Acetophenone
ND
ug/kg
7130
10
08/29/22 10:52
08/30/22 12:23
98-86-2
2-Acetylaminofluorene
ND
ug/kg
14300
10
08/29/22 10:52
08/30/22 12:23
53-96-3
4-Aminobiphenyl
ND
ug/kg
7130
10
08/29/22 10:52
08/30/22 12:23
92-67-1
Anthracene
ND
ug/kg
7130
10
08/29/22 10:52
08/30/22 12:23
120-12-7
Benzo(a)anthracene
ND
ug/kg
7130
10
08/29/22 10:52
08/30/22 12:23
56-55-3
Benzo(a)pyrene
ND
ug/kg
7130
10
08/29/22 10:52
08/30/22 12:23
50-32-8
Benzo(b)fluoranthene
ND
ug/kg
7130
10
08/29/22 10:52
08/30/22 12:23
205-99-2
Benzo(g,h,i)perylene
ND
ug/kg
7130
10
08/29/22 10:52
08/30/22 12:23
191-24-2
Benzo(k)fluoranthene
ND
ug/kg
7130
10
08/29/22 10:52
08/30/22 12:23
207-08-9
Benzyl alcohol
ND
ug/kg
14300
10
08/29/22 10:52
08/30/22 12:23
100-51-6
bis(2-Chloroethoxy)methane
ND
ug/kg
7130
10
08/29/22 10:52
08/30/22 12:23
111-91-1
bis(2-Chloroethyl) ether
ND
ug/kg
7130
10
08/29/22 10:52
08/30/22 12:23
111-44-4
2-Chloronaphthalene
ND
ug/kg
7130
10
08/29/22 10:52
08/30/22 12:23
91-58-7
2-Chlorophenol
ND
ug/kg
7130
10
08/29/22 10:52
08/30/22 12:23
95-57-8
4-Chlorophenylphenyl ether
ND
ug/kg
7130
10
08/29/22 10:52
08/30/22 12:23
7005-72-3
Chrysene
ND
ug/kg
7130
10
08/29/22 10:52
08/30/22 12:23
218-01-9
n-Decane
ND
ug/kg
7130
10
08/29/22 10:52
08/30/22 12:23
124-18-5
Diallate
ND
ug/kg
7130
10
08/29/22 10:52
08/30/22 12:23
2303-16-4
Dibenz(a,h)anthracene
ND
ug/kg
7130
10
08/29/22 10:52
08/30/22 12:23
53-70-3
Dibenzo(a,e)pyrene
ND
ug/kg
21600
10
08/29/22 10:52
08/30/22 12:23
192-65-4
Dibenzofuran
ND
ug/kg
7130
10
08/29/22 10:52
08/30/22 12:23
132-64-9
2,3-Dibromo-1-propanol phosph
ND
ug/kg
35700
10
08/29/22 10:52
08/30/22 12:23
126-72-7
1,2-Dichlorobenzene
ND
ug/kg
7130
10
08/29/22 10:52
08/30/22 12:23
95-50-1
1,3-Dichlorobenzene
ND
ug/kg
7130
10
08/29/22 10:52
08/30/22 12:23
541-73-1
1,4-Dichlorobenzene
ND
ug/kg
7130
10
08/29/22 10:52
08/30/22 12:23
106-46-7
3,3'-Dichlorobenzidine
ND
ug/kg
14300
10
08/29/22 10:52
08/30/22 12:23
91-94-1
2,4-Dichlorophenol
ND
ug/kg
7130
10
08/29/22 10:52
08/30/22 12:23
120-83-2
2,6-Dichlorophenol
ND
ug/kg
7130
10
08/29/22 10:52
08/30/22 12:23
87-65-0
2,3-Dichloroaniline
ND
ug/kg
7130
10
08/29/22 10:52
08/30/22 12:23
608-27-5
Diethylphthalate
ND
ug/kg
7130
10
08/29/22 10:52
08/30/22 12:23
84-66-2
Dimethoate
ND
ug/kg
14300
10
08/29/22 10:52
08/30/22 12:23
60-51-5
P-Dimethylaminoazobenzene
ND
ug/kg
7130
10
08/29/22 10:52
08/30/22 12:23
60-11-7
7,12-Dimethylbenz(a)anthracene
ND
ug/kg
7130
10
08/29/22 10:52
08/30/22 12:23
57-97-6
3,3'-Dimethylbenzidine
ND
ug/kg
14300
10
08/29/22 10:52
08/30/22 12:23
119-93-7
2,4-Dimethylphenol
ND
ug/kg
7130
10
08/29/22 10:52
08/30/22 12:23
105-67-9
a,a-Dimethylphenylethylamine
ND
ug/kg
35700
10
08/29/22 10:52
08/30/22 12:23
122-09-8
Dimethylphthalate
ND
ug/kg
7130
10
08/29/22 10:52
08/30/22 12:23
131-11-3
Di-n-butylphthalate
ND
ug/kg
7130
10
08/29/22 10:52
08/30/22 12:23
84-74-2
4,6-Dinitro-2-methyl phenol
ND
ug/kg
14300
10
08/29/22 10:52
08/30/22 12:23
534-52-1
REPORT OF LABORATORY ANALYSIS
v1
IL
IL
IH
v1
This report shall not be reproduced, except in full,
Date: 10/25/2022 02:36 PM without the written consent of Pace Analytical Services, LLC. Page 49 of 165

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: WASTE CHARACTERIZATION
Pace Project No.: 92621331
Sample: GP-7 2-3' Lab ID: 92621331007 Collected: 08/16/22 12:40 Received: 08/17/22 16:15 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No
8270E MSSV Microwave
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical
Services - Charlotte
1,3-Dinitrobenzene
ND
ug/kg
7130
10
08/29/22 10:52
08/30/22 12:23
99-65-0
1,4-Dinitrobenzene
ND
ug/kg
7130
10
08/29/22 10:52
08/30/22 12:23
100-25-4
2,4-Dinitrophenol
ND
ug/kg
35700
10
08/29/22 10:52
08/30/22 12:23
51-28-5
2,4-Dinitrotoluene
ND
ug/kg
7130
10
08/29/22 10:52
08/30/22 12:23
121-14-2
2,6-Dinitrotoluene
ND
ug/kg
7130
10
08/29/22 10:52
08/30/22 12:23
606-20-2
Di-n-octylphthalate
ND
ug/kg
7130
10
08/29/22 10:52
08/30/22 12:23
117-84-0
Dinoseb
ND
ug/kg
14300
10
08/29/22 10:52
08/30/22 12:23
88-85-7
Diphenylamine
ND
ug/kg
7130
10
08/29/22 10:52
08/30/22 12:23
122-39-4
Diphenyl ether (Phenyl ether)
ND
ug/kg
10800
10
08/29/22 10:52
08/30/22 12:23
101-84-8
1,2-Diphenylhydrazine
ND
ug/kg
7130
10
08/29/22 10:52
08/30/22 12:23
122-66-7
Disulfoton
ND
ug/kg
7130
10
08/29/22 10:52
08/30/22 12:23
298-04-4
bis(2- Ethyl hexyl)phthalate
ND
ug/kg
7130
10
08/29/22 10:52
08/30/22 12:23
117-81-7
Ethyl methanesulfonate
ND
ug/kg
14300
10
08/29/22 10:52
08/30/22 12:23
62-50-0
Famphur
ND
ug/kg
14300
10
08/29/22 10:52
08/30/22 12:23
52-85-7
Fluoranthene
ND
ug/kg
7130
10
08/29/22 10:52
08/30/22 12:23
206-44-0
Fluorene
ND
ug/kg
7130
10
08/29/22 10:52
08/30/22 12:23
86-73-7
Hexachloro-1,3-butadiene
ND
ug/kg
7130
10
08/29/22 10:52
08/30/22 12:23
87-68-3
Hexachlorobenzene
ND
ug/kg
7130
10
08/29/22 10:52
08/30/22 12:23
118-74-1
Hexachlorocyclopentadiene
ND
ug/kg
7130
10
08/29/22 10:52
08/30/22 12:23
77-47-4
Hexachloroethane
ND
ug/kg
7130
10
08/29/22 10:52
08/30/22 12:23
67-72-1
Hexachlorophene
ND
ug/kg
71300
10
08/29/22 10:52
08/30/22 12:23
70-30-4
Hexachloropropene
ND
ug/kg
7130
10
08/29/22 10:52
08/30/22 12:23
1888-71-7
Indeno(1,2,3-cd)pyrene
ND
ug/kg
7130
10
08/29/22 10:52
08/30/22 12:23
193-39-5
Isodrin
ND
ug/kg
7130
10
08/29/22 10:52
08/30/22 12:23
465-73-6
Isophorone
ND
ug/kg
7130
10
08/29/22 10:52
08/30/22 12:23
78-59-1
Isosafrole
ND
ug/kg
7130
10
08/29/22 10:52
08/30/22 12:23
120-58-1
Kepone
ND
ug/kg
14300
10
08/29/22 10:52
08/30/22 12:23
143-50-0
Methapyrilene
ND
ug/kg
35700
10
08/29/22 10:52
08/30/22 12:23
91-80-5
3-Methylcholanthrene
ND
ug/kg
7130
10
08/29/22 10:52
08/30/22 12:23
56-49-5
4,4'-Methylene-bis(2-chloroani
ND
ug/kg
14300
10
08/29/22 10:52
08/30/22 12:23
101-14-4
Methyl methanesulfonate
ND
ug/kg
14300
10
08/29/22 10:52
08/30/22 12:23
66-27-3
1-Methylnaphthalene
ND
ug/kg
7130
10
08/29/22 10:52
08/30/22 12:23
90-12-0
2-Methylnaphthalene
ND
ug/kg
7130
10
08/29/22 10:52
08/30/22 12:23
91-57-6
2-Methyl-5-nitroaniline
ND
ug/kg
7130
10
08/29/22 10:52
08/30/22 12:23
99-55-8
Methyl parathion
ND
ug/kg
7130
10
08/29/22 10:52
08/30/22 12:23
298-00-0
2-Methylphenol(o-Cresol)
ND
ug/kg
7130
10
08/29/22 10:52
08/30/22 12:23
95-48-7
3&4-Methyl phenol (m&p Cresol)
ND
ug/kg
7130
10
08/29/22 10:52
08/30/22 12:23
15831-10-4
1-Naphthalenamine
ND
ug/kg
14300
10
08/29/22 10:52
08/30/22 12:23
134-32-7
2-Naphthalenamine
ND
ug/kg
14300
10
08/29/22 10:52
08/30/22 12:23
91-59-8
Naphthalene
ND
ug/kg
7130
10
08/29/22 10:52
08/30/22 12:23
91-20-3
1,4-Naphthoquinone
ND
ug/kg
35700
10
08/29/22 10:52
08/30/22 12:23
130-15-4
2-Nitroaniline
ND
ug/kg
35700
10
08/29/22 10:52
08/30/22 12:23
88-74-4
3-Nitroaniline
ND
ug/kg
35700
10
08/29/22 10:52
08/30/22 12:23
99-09-2
4-Nitroaniline
ND
ug/kg
14300
10
08/29/22 10:52
08/30/22 12:23
100-01-6
Nitrobenzene
ND
ug/kg
7130
10
08/29/22 10:52
08/30/22 12:23
98-95-3
REPORT OF LABORATORY ANALYSIS
Qual
IH,L2
IH
This report shall not be reproduced, except in full,
Date: 10/25/2022 02:36 PM without the written consent of Pace Analytical Services, LLC. Page 50 of 165

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: WASTE CHARACTERIZATION
Pace Project No.: 92621331
Sample: GP-7 2-3' Lab ID: 92621331007 Collected: 08/16/22 12:40 Received: 08/17/22 16:15 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters
8270E MSSV Microwave
2-Nitrophenol
4-Nitrophenol
4-Nitroquinoline-n-oxide
5-Nitro-o-toluidine
N-Nitrosodiethylamine
N-Nitrosodimethylamine
N-Nitroso-di-n-butylamine
N-Nitroso-di-n-propylamine
N-Nitrosodiphenylamine
N-Nitrosomethylethylamine
N-Nitrosomorpholine
N-Nitrosopiperidine
N-Nitrosopyrrolidine
n-Octadecane
O,O,O-Triethylphosphorothioate
2,2'-Oxybis(1-chloropropane)
Parathion (Ethyl parathion)
Pentachlorobenzene
Pentachloroethane
Pentachloronitrobenzene
Pentachlorophenol
Phenacetin
Phenanthrene
Phenol
p-Phenylenediamine
Phorate
Phthalic anhydride
2-Picoline
Pronamide
Pyrene
Pyridine
Safrole
Sulfotepp (ThiodiphosphoricAc
Terpineol
1,2,4,5-Tetrachlorobenzene
2,3,4,6-Tetrachlorophenol
Thionazin
O-Toluidine
1,2,4-Trichlorobenzene
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
1,3,5-Trinitrobenzene
Surrogates
2-Fluorobiphenyl (S)
Terphenyl-d14 (S)
Results Units Report Limit DF Prepared Analyzed CAS No. Qual
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
ND
ug/kg
7130
10
08/29/2210:52
08/30/2212:23
88-75-5
ND
ug/kg
35700
10
08/29/2210:52
08/30/2212:23
100-02-7
ND
ug/kg
35700
10
08/29/2210:52
08/30/2212:23
56-57-5
v2
ND
ug/kg
7130
10
08/29/2210:52
08/30/2212:23
99-55-8
ND
ug/kg
7130
10
08/29/2210:52
08/30/2212:23
55-18-5
ND
ug/kg
7130
10
08/29/2210:52
08/30/2212:23
62-75-9
ND
ug/kg
7130
10
08/29/2210:52
08/30/2212:23
924-16-3
ND
ug/kg
7130
10
08/29/2210:52
08/30/2212:23
621-64-7
ND
ug/kg
7130
10
08/29/2210:52
08/30/2212:23
86-30-6
ND
ug/kg
7130
10
08/29/2210:52
08/30/2212:23
10595-95-6
ND
ug/kg
7130
10
08/29/2210:52
08/30/2212:23
59-89-2
ND
ug/kg
14300
10
08/29/2210:52
08/30/2212:23
100-75-4
ND
ug/kg
14300
10
08/29/2210:52
08/30/2212:23
930-55-2
ND
ug/kg
7130
10
08/29/2210:52
08/30/2212:23
593-45-3
ND
ug/kg
7130
10
08/29/2210:52
08/30/2212:23
126-68-1
ND
ug/kg
7130
10
08/29/2210:52
08/30/2212:23
108-60-1
ND
ug/kg
7130
10
08/29/2210:52
08/30/2212:23
56-38-2
ND
ug/kg
7130
10
08/29/2210:52
08/30/2212:23
608-93-5
ND
ug/kg
7130
10
08/29/2210:52
08/30/2212:23
76-01-7
ND
ug/kg
7130
10
08/29/2210:52
08/30/2212:23
82-68-8
ND
ug/kg
14300
10
08/29/2210:52
08/30/2212:23
87-86-5
ND
ug/kg
14300
10
08/29/2210:52
08/30/2212:23
62-44-2
ND
ug/kg
7130
10
08/29/2210:52
08/30/2212:23
85-01-8
ND
ug/kg
7130
10
08/29/2210:52
08/30/2212:23
108-95-2
ND
ug/kg
14300
10
08/29/2210:52
08/30/2212:23
106-50-3
IL
ND
ug/kg
7130
10
08/29/2210:52
08/30/2212:23
298-02-2
L2
ND
ug/kg
54000
10
08/29/2210:52
08/30/2212:23
85-44-9
ND
ug/kg
7130
10
08/29/2210:52
08/30/2212:23
109-06-8
ND
ug/kg
14300
10
08/29/2210:52
08/30/2212:23
23950-58-5
ND
ug/kg
7130
10
08/29/2210:52
08/30/2212:23
129-00-0
ND
ug/kg
7130
10
08/29/2210:52
08/30/2212:23
110-86-1
ND
ug/kg
14300
10
08/29/2210:52
08/30/2212:23
94-59-7
ND
ug/kg
7130
10
08/29/2210:52
08/30/2212:23
3689-24-5
ND
ug/kg
7130
10
08/29/2210:52
08/30/2212:23
98-55-5
ND
ug/kg
7130
10
08/29/2210:52
08/30/2212:23
95-94-3
ND
ug/kg
7130
10
08/29/2210:52
08/30/2212:23
58-90-2
ND
ug/kg
7130
10
08/29/2210:52
08/30/2212:23
297-97-2
ND
ug/kg
7130
10
08/29/2210:52
08/30/2212:23
95-53-4
ND
ug/kg
7130
10
08/29/2210:52
08/30/2212:23
120-82-1
ND
ug/kg
7130
10
08/29/2210:52
08/30/2212:23
95-95-4
ND
ug/kg
7130
10
08/29/2210:52
08/30/2212:23
88-06-2
ND
ug/kg
7130
10
08/29/2210:52
08/30/2212:23
99-35-4
0
%
19-130
10
08/29/2210:52
08/30/2212:23
321-60-8
D3,S4
0
%
15-130
10
08/29/2210:52
08/30/2212:23
1718-51-0
S4
REPORT
OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/25/2022 02:36 PM without the written consent of Pace Analytical Services, LLC. Page 51 of 165

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: WASTE CHARACTERIZATION
Pace Project No.: 92621331
Sample: GP-7 2-3'
Lab ID: 92621331007 Collected: 08/16/22 12:40 Received: 08/17/22 16:15 Matrix: Solid
Results reported on a "dry weight"
basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters
Results Units Report Limit DF Prepared
Analyzed
CAS No. Qual
8270E MSSV Microwave
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
Surrogates
Phenol-d6 (S)
0 % 18-130 10 08/29/22 10:52
08/30/22 12:23
13127-88-3 S4
2-Fluorophenol (S)
0 % 18-130 10 08/29/22 10:52
08/30/22 12:23
367-12-4 S4
2,4,6-Tribromophenol (S)
0 % 18-130 10 08/29/22 10:52
08/30/22 12:23
118-79-6 S4
Nitrobenzene-d5 (S)
0 % 21-130 10 08/29/22 10:52
08/30/22 12:23
4165-60-0 S4
Percent Moisture
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
54.0 % 0.10 1
08/22/22 15:39
N2
1010 Flash poi nt,Closed Cup
Analytical Method: EPA 1010B
Pace Analytical Services -Asheville
Flashpoint
>200 deg F 70.0 1
08/22/22 14:50
Total Solids 2540 G-2011
Analytical Method: SM 2540G Preparation Method: SM 2540 G
Pace National - Mt. Juliet
Total Solids
45.1 % 1 08/23/22 10:15
08/23/22 10:31
4500S21) Sulfide Soil
Analytical Method: SM 4500-S2D-2011 Modified Preparation Method: SM
4500-S2D-2011 Modified
Pace Analytical Services -Asheville
Sulfide
ND mg/kg 10.6 1 08/20/22 02:37
08/20/22 06:40
18496-25-8
9045 pH Soil
Analytical Method: EPA 9045D
Pace Analytical Services -Asheville
pH at 25 Degrees C
3.8 Std. Units 0.10 1
08/23/22 18:15
H3
9012 Cyanide, Total
Analytical Method: EPA 9012 Preparation Method: EPA 9012
Pace Analytical Services - Ormond Beach
Cyanide
16.8 mg/kg 5.6 10 08/29/22 09:41
08/29/22 15:21
57-12-5
Date: 10/25/2022 02:36 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 52 of 165

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: WASTE CHARACTERIZATION
Pace Project No.: 92621331
Sample: HA-1 2-3' Lab ID: 92621331008 Collected: 08/16/22 13:00 Received: 08/17/22 16:15 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
OP Pesticides 8141 B
Analytical Method: EPA 8141 B Preparation Method: 3546
Pace National
- Mt. Juliet
Azinphos, methyl (Guthion)
ND
mg/kg
0.204
1
08/21/22 16:12
08/22/22 04:51
86-50-0
Bolstar
ND
mg/kg
0.204
1
08/21/22 16:12
08/22/22 04:51
35400-43-2
Chlorpyrifos
ND
mg/kg
0.204
1
08/21/22 16:12
08/22/22 04:51
2921-88-2
Coumaphos
ND
mg/kg
0.204
1
08/21/22 16:12
08/22/22 04:51
56-72-4
Total Demeton
ND
mg/kg
0.143
1
08/21/22 16:12
08/22/22 04:51
8065-48-3
Diazinon
ND
mg/kg
0.204
1
08/21/22 16:12
08/22/22 04:51
333-41-5
Dichlorvos
ND
mg/kg
0.204
1
08/21/22 16:12
08/22/22 04:51
62-73-7
Dimethoate
ND
mg/kg
0.204
1
08/21/22 16:12
08/22/22 04:51
60-51-5
Disulfoton
ND
mg/kg
0.204
1
08/21/22 16:12
08/22/22 04:51
298-04-4
EPN (ENT)
ND
mg/kg
0.204
1
08/21/22 16:12
08/22/22 04:51
2104-64-5
Ethoprop
ND
mg/kg
0.204
1
08/21/22 16:12
08/22/22 04:51
13194-48-4
Parathion (Ethyl parathion)
ND
mg/kg
0.204
1
08/21/22 16:12
08/22/22 04:51
56-38-2
Fensulfothion
ND
mg/kg
0.204
1
08/21/22 16:12
08/22/22 04:51
115-90-2
Fenthion
ND
mg/kg
0.204
1
08/21/22 16:12
08/22/22 04:51
55-38-9
Malathion
ND
mg/kg
0.204
1
08/21/22 16:12
08/22/22 04:51
121-75-5
Merphos
ND
mg/kg
0.204
1
08/21/22 16:12
08/22/22 04:51
150-50-5
Methyl parathion
ND
mg/kg
0.204
1
08/21/22 16:12
08/22/22 04:51
298-00-0
Mevinphos
ND
mg/kg
0.204
1
08/21/22 16:12
08/22/22 04:51
7786-34-7
Naled
ND
mg/kg
0.204
1
08/21/22 16:12
08/22/22 04:51
300-76-5
Phorate
ND
mg/kg
0.204
1
08/21/22 16:12
08/22/22 04:51
298-02-2
Ronnel
ND
mg/kg
0.204
1
08/21/22 16:12
08/22/22 04:51
299-84-3
Stirophos (Tetrachlorvinphos)
ND
mg/kg
0.204
1
08/21/22 16:12
08/22/22 04:51
22248-79-9
Sulfotepp (ThiodiphosphoricAc
ND
mg/kg
0.204
1
08/21/22 16:12
08/22/22 04:51
3689-24-5
TEPP
ND
mg/kg
2.04
1
08/21/22 16:12
08/22/22 04:51
107-49-3
Tokuthion (Prothiofos)
ND
mg/kg
0.204
1
08/21/22 16:12
08/22/22 04:51
34643-46-4
Trichloronate
ND
mg/kg
0.204
1
08/21/22 16:12
08/22/22 04:51
327-98-0
Surrogates
Triphenyl phosphate (S)
51.7
%
36.0-121
1
08/21/22 16:12
08/22/22 04:51
115-86-6
8081 GCS Pesticides
Analytical Method: EPA 8081 B Preparation Method: EPA 3546
Pace Analytical
Services - Charlotte
Aldrin
ND
ug/kg
73.5
20
08/24/22 07:17
08/26/22 18:50
309-00-2
alpha-BHC
ND
ug/kg
73.5
20
08/24/22 07:17
08/26/22 18:50
319-84-6
beta-BHC
ND
ug/kg
73.5
20
08/24/22 07:17
08/26/22 18:50
319-85-7
delta-BHC
ND
ug/kg
73.5
20
08/24/22 07:17
08/26/22 18:50
319-86-8
gamma-BHC (Lindane)
ND
ug/kg
73.5
20
08/24/22 07:17
08/26/22 18:50
58-89-9
Chlordane (Technical)
1420
ug/kg
368
20
08/24/22 07:17
08/26/22 18:50
57-74-9
4,4'-DDD
ND
ug/kg
73.5
20
08/24/22 07:17
08/26/22 18:50
72-54-8
4,4'-DDE
ND
ug/kg
73.5
20
08/24/22 07:17
08/26/22 18:50
72-55-9
4,4'-DDT
ND
ug/kg
73.5
20
08/24/22 07:17
08/26/22 18:50
50-29-3
Dieldrin
79.7
ug/kg
73.5
20
08/24/22 07:17
08/26/22 18:50
60-57-1
Endosulfan I
ND
ug/kg
73.5
20
08/24/22 07:17
08/26/22 18:50
959-98-8
Endosulfan II
ND
ug/kg
73.5
20
08/24/22 07:17
08/26/22 18:50
33213-65-9
Endosulfan sulfate
ND
ug/kg
73.5
20
08/24/22 07:17
08/26/22 18:50
1031-07-8
Endrin
ND
ug/kg
73.5
20
08/24/22 07:17
08/26/22 18:50
72-20-8
REPORT OF LABORATORY ANALYSIS
LO
This report shall not be reproduced, except in full,
Date: 10/25/2022 02:36 PM without the written consent of Pace Analytical Services, LLC. Page 53 of 165

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: WASTE CHARACTERIZATION
Pace Project No.: 92621331
Sample: HA-1 2-3' Lab ID: 92621331008 Collected: 08/16/22 13:00 Received: 08/17/22 16:15 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8081 GCS Pesticides
Endrin aldehyde
Endrin ketone
Heptachlor
Heptachlor epoxide
Hexachlorobenzene
Methoxychlor
Mirex
Toxaphene
Surrogates
Tetrachloro-m-xylene (S)
Decachlorobiphenyl (S)
8082 GCS PCB
PCB-1016 (Aroclor 1016)
PCB-1221 (Aroclor 1221)
PCB-1232 (Aroclor 1232)
PCB-1242 (Aroclor 1242)
PCB-1248 (Aroclor 1248)
PCB-1254 (Aroclor 1254)
PCB-1260 (Aroclor 1260)
Surrogates
Decachlorobiphenyl (S)
Analytical Method: EPA 8081 B Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
ND
ug/kg
73.5
20
08/24/22 07:17
08/26/22 18:50
7421-93-4
ND
ug/kg
73.5
20
08/24/22 07:17
08/26/22 18:50
53494-70-5
ND
ug/kg
73.5
20
08/24/22 07:17
08/26/22 18:50
76-44-8
ND
ug/kg
73.5
20
08/24/22 07:17
08/26/22 18:50
1024-57-3
ND
ug/kg
73.5
20
08/24/22 07:17
08/26/22 18:50
118-74-1
ND
ug/kg
184
20
08/24/22 07:17
08/26/22 18:50
72-43-5
ND
ug/kg
184
20
08/24/22 07:17
08/26/22 18:50
2385-85-5
ND
ug/kg
257
20
08/24/22 07:17
08/26/22 18:50
8001-35-2
0
%
10-133
20
08/24/22 07:17
08/26/22 18:50
877-09-8 D3,S4
0
%
10-146
20
08/24/22 07:17
08/26/22 18:50
2051-24-3 S4
Analytical Method: EPA 8082A Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
ND
ug/kg
1220
20
08/19/22 15:53
08/24/22 07:32
12674-11-2
ND
ug/kg
1220
20
08/19/22 15:53
08/24/22 07:32
11104-28-2
ND
ug/kg
1220
20
08/19/22 15:53
08/24/22 07:32
11141-16-5
ND
ug/kg
1220
20
08/19/22 15:53
08/24/22 07:32
53469-21-9
ND
ug/kg
1220
20
08/19/22 15:53
08/24/22 07:32
12672-29-6
1310
ug/kg
1220
20
08/19/22 15:53
08/24/22 07:32
11097-69-1
ND
ug/kg
1220
20
08/19/22 15:53
08/24/22 07:32
11096-82-5
0
%
10-160
20
08/19/22 15:53
08/24/22 07:32
2051-24-3 D3,S4
6010 MET ICP
Analytical Method: EPA 6010 Preparation Method: EPA 3050
Pace Analytical
Services - Ormond Beach
Tin
127
mg/kg
4.6
1
08/30/2219:03
08/31/2218:34
7440-31-5
6020 MET ICPMS
Analytical Method: EPA 6020 Preparation Method: EPA 3050
Pace Analytical
Services - Ormond Beach
Antimony
244
mg/kg
4.3
20
08/27/22 00:15
08/29/22 19:50
7440-36-0
1g,N2
Arsenic
5.1
mg/kg
2.2
20
08/27/22 00:15
08/29/22 19:50
7440-38-2
1g
Barium
1620
mg/kg
21.7
200
08/27/22 00:15
08/31/22 14:22
7440-39-3
1g
Beryllium
0.26
mg/kg
0.26
20
08/27/22 00:15
08/29/22 19:50
7440-41-7
1g
Cadmium
8.1
mg/kg
0.26
20
08/27/22 00:15
08/29/22 19:50
7440-43-9
1g
Chromium
3120
mg/kg
21.7
200
08/27/22 00:15
08/31/22 14:22
7440-47-3
1g
Cobalt
7.1
mg/kg
2.2
20
08/27/22 00:15
08/29/22 19:50
7440-48-4
1g
Copper
403
mg/kg
4.3
20
08/27/22 00:15
08/29/22 19:50
7440-50-8
1g
Lead
3590
mg/kg
21.7
200
08/27/22 00:15
08/31/22 14:22
7439-92-1
1g
Nickel
9.2
mg/kg
2.2
20
08/27/22 00:15
08/29/22 19:50
7440-02-0
1g
Selenium
7.9
mg/kg
2.2
20
08/27/22 00:15
08/29/22 19:50
7782-49-2
1g
Silver
175
mg/kg
2.6
200
08/27/22 00:15
08/31/22 14:22
7440-22-4
1g
Thallium
ND
mg/kg
2.2
20
08/27/22 00:15
08/29/22 19:50
7440-28-0
1g
Vanadium
32.0
mg/kg
2.2
20
08/27/22 00:15
08/29/22 19:50
7440-62-2
1g
Zinc
180
mg/kg
87.0
20
08/27/22 00:15
08/29/22 19:50
7440-66-6
1g
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/25/2022 02:36 PM without the written consent of Pace Analytical Services, LLC. Page 54 of 165

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: WASTE CHARACTERIZATION
Pace Project No.: 92621331
Sample: HA-1 2-3' Lab ID: 92621331008 Collected: 08/16/22 13:00 Received: 08/17/22 16:15 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
7471 Mercury Analytical Method: EPA 7471 Preparation Method: EPA 7471
Pace Analytical Services - Ormond Beach
Mercury 6.7 mg/kg 0.18 10 08/24/22 07:26 08/24/22 11:57 7439-97-6
8270E MSSV Microwave
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical
Services - Charlotte
Acenaphthene
ND
ug/kg
9740
10
08/25/22 05:38
08/26/22 13:38
83-32-9
Acenaphthylene
ND
ug/kg
9740
10
08/25/22 05:38
08/26/22 13:38
208-96-8
Acetophenone
ND
ug/kg
9740
10
08/25/22 05:38
08/26/22 13:38
98-86-2
2-Acetylaminofluorene
ND
ug/kg
19500
10
08/25/22 05:38
08/26/22 13:38
53-96-3
4-Aminobiphenyl
ND
ug/kg
9740
10
08/25/22 05:38
08/26/22 13:38
92-67-1
Anthracene
ND
ug/kg
9740
10
08/25/22 05:38
08/26/22 13:38
120-12-7
Benzo(a)anthracene
ND
ug/kg
9740
10
08/25/22 05:38
08/26/22 13:38
56-55-3
Benzo(a)pyrene
ND
ug/kg
9740
10
08/25/22 05:38
08/26/22 13:38
50-32-8
Benzo(b)fluoranthene
ND
ug/kg
9740
10
08/25/22 05:38
08/26/22 13:38
205-99-2
Benzo(g,h,i)perylene
ND
ug/kg
9740
10
08/25/22 05:38
08/26/22 13:38
191-24-2
Benzo(k)fluoranthene
ND
ug/kg
9740
10
08/25/22 05:38
08/26/22 13:38
207-08-9
Benzyl alcohol
ND
ug/kg
19500
10
08/25/22 05:38
08/26/22 13:38
100-51-6
bis(2-Chloroethoxy)methane
ND
ug/kg
9740
10
08/25/22 05:38
08/26/22 13:38
111-91-1
bis(2-Chloroethyl) ether
ND
ug/kg
9740
10
08/25/22 05:38
08/26/22 13:38
111-44-4
2-Chloronaphthalene
ND
ug/kg
9740
10
08/25/22 05:38
08/26/22 13:38
91-58-7
2-Chlorophenol
ND
ug/kg
9740
10
08/25/22 05:38
08/26/22 13:38
95-57-8
4-Chlorophenylphenyl ether
ND
ug/kg
9740
10
08/25/22 05:38
08/26/22 13:38
7005-72-3
Chrysene
ND
ug/kg
9740
10
08/25/22 05:38
08/26/22 13:38
218-01-9
n-Decane
ND
ug/kg
9740
10
08/25/22 05:38
08/26/22 13:38
124-18-5
Diallate
ND
ug/kg
9740
10
08/25/22 05:38
08/26/22 13:38
2303-16-4
Dibenz(a,h)anthracene
ND
ug/kg
9740
10
08/25/22 05:38
08/26/22 13:38
53-70-3
Dibenzo(a,e)pyrene
ND
ug/kg
29500
10
08/25/22 05:38
08/26/22 13:38
192-65-4
Dibenzofuran
ND
ug/kg
9740
10
08/25/22 05:38
08/26/22 13:38
132-64-9
2,3-Dibromo-1-propanol phosph
ND
ug/kg
48700
10
08/25/22 05:38
08/26/22 13:38
126-72-7
1,2-Dichlorobenzene
ND
ug/kg
9740
10
08/25/22 05:38
08/26/22 13:38
95-50-1
1,3-Dichlorobenzene
ND
ug/kg
9740
10
08/25/22 05:38
08/26/22 13:38
541-73-1
1,4-Dichlorobenzene
ND
ug/kg
9740
10
08/25/22 05:38
08/26/22 13:38
106-46-7
3,3'-Dichlorobenzidine
ND
ug/kg
19500
10
08/25/22 05:38
08/26/22 13:38
91-94-1
2,4-Dichlorophenol
ND
ug/kg
9740
10
08/25/22 05:38
08/26/22 13:38
120-83-2
2,6-Dichlorophenol
ND
ug/kg
9740
10
08/25/22 05:38
08/26/22 13:38
87-65-0
2,3-Dichloroaniline
ND
ug/kg
9740
10
08/25/22 05:38
08/26/22 13:38
608-27-5
Diethylphthalate
ND
ug/kg
9740
10
08/25/22 05:38
08/26/22 13:38
84-66-2
Dimethoate
ND
ug/kg
19500
10
08/25/22 05:38
08/26/22 13:38
60-51-5
P-Dimethylaminoazobenzene
ND
ug/kg
9740
10
08/25/22 05:38
08/26/22 13:38
60-11-7
7,12-Dimethylbenz(a)anthracene
ND
ug/kg
9740
10
08/25/22 05:38
08/26/22 13:38
57-97-6
3,3'-Dimethylbenzidine
ND
ug/kg
19500
10
08/25/22 05:38
08/26/22 13:38
119-93-7
2,4-Dimethylphenol
ND
ug/kg
9740
10
08/25/22 05:38
08/26/22 13:38
105-67-9
a,a-Dimethylphenylethylamine
ND
ug/kg
48700
10
08/25/22 05:38
08/26/22 13:38
122-09-8
Dimethylphthalate
ND
ug/kg
9740
10
08/25/22 05:38
08/26/22 13:38
131-11-3
Di-n-butylphthalate
ND
ug/kg
9740
10
08/25/22 05:38
08/26/22 13:38
84-74-2
4,6-Dinitro-2-methyl phenol
ND
ug/kg
19500
10
08/25/22 05:38
08/26/22 13:38
534-52-1
REPORT OF LABORATORY ANALYSIS
IL
IL
IH
This report shall not be reproduced, except in full,
Date: 10/25/2022 02:36 PM without the written consent of Pace Analytical Services, LLC. Page 55 of 165

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: WASTE CHARACTERIZATION
Pace Project No.: 92621331
Sample: HA-1 2-3' Lab ID: 92621331008 Collected: 08/16/22 13:00 Received: 08/17/22 16:15 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No
8270E MSSV Microwave
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical
Services - Charlotte
1,3-Dinitrobenzene
ND
ug/kg
9740
10
08/25/22 05:38
08/26/22 13:38
99-65-0
1,4-Dinitrobenzene
ND
ug/kg
9740
10
08/25/22 05:38
08/26/22 13:38
100-25-4
2,4-Dinitrophenol
ND
ug/kg
48700
10
08/25/22 05:38
08/26/22 13:38
51-28-5
2,4-Dinitrotoluene
ND
ug/kg
9740
10
08/25/22 05:38
08/26/22 13:38
121-14-2
2,6-Dinitrotoluene
ND
ug/kg
9740
10
08/25/22 05:38
08/26/22 13:38
606-20-2
Di-n-octylphthalate
ND
ug/kg
9740
10
08/25/22 05:38
08/26/22 13:38
117-84-0
Dinoseb
ND
ug/kg
19500
10
08/25/22 05:38
08/26/22 13:38
88-85-7
Diphenylamine
ND
ug/kg
9740
10
08/25/22 05:38
08/26/22 13:38
122-39-4
Diphenyl ether (Phenyl ether)
ND
ug/kg
14800
10
08/25/22 05:38
08/26/22 13:38
101-84-8
1,2-Diphenylhydrazine
ND
ug/kg
9740
10
08/25/22 05:38
08/26/22 13:38
122-66-7
Disulfoton
ND
ug/kg
9740
10
08/25/22 05:38
08/26/22 13:38
298-04-4
bis(2- Ethyl hexyl)phthalate
14100
ug/kg
9740
10
08/25/22 05:38
08/26/22 13:38
117-81-7
Ethyl methanesulfonate
ND
ug/kg
19500
10
08/25/22 05:38
08/26/22 13:38
62-50-0
Famphur
ND
ug/kg
19500
10
08/25/22 05:38
08/26/22 13:38
52-85-7
Fluoranthene
ND
ug/kg
9740
10
08/25/22 05:38
08/26/22 13:38
206-44-0
Fluorene
ND
ug/kg
9740
10
08/25/22 05:38
08/26/22 13:38
86-73-7
Hexachloro-1,3-butadiene
ND
ug/kg
9740
10
08/25/22 05:38
08/26/22 13:38
87-68-3
Hexachlorobenzene
ND
ug/kg
9740
10
08/25/22 05:38
08/26/22 13:38
118-74-1
Hexachlorocyclopentadiene
ND
ug/kg
9740
10
08/25/22 05:38
08/26/22 13:38
77-47-4
Hexachloroethane
ND
ug/kg
9740
10
08/25/22 05:38
08/26/22 13:38
67-72-1
Hexachlorophene
ND
ug/kg
97400
10
08/25/22 05:38
08/26/22 13:38
70-30-4
Hexachloropropene
ND
ug/kg
9740
10
08/25/22 05:38
08/26/22 13:38
1888-71-7
Indeno(1,2,3-cd)pyrene
ND
ug/kg
9740
10
08/25/22 05:38
08/26/22 13:38
193-39-5
Isodrin
ND
ug/kg
9740
10
08/25/22 05:38
08/26/22 13:38
465-73-6
Isophorone
ND
ug/kg
9740
10
08/25/22 05:38
08/26/22 13:38
78-59-1
Isosafrole
ND
ug/kg
9740
10
08/25/22 05:38
08/26/22 13:38
120-58-1
Kepone
ND
ug/kg
19500
10
08/25/22 05:38
08/26/22 13:38
143-50-0
Methapyrilene
ND
ug/kg
48700
10
08/25/22 05:38
08/26/22 13:38
91-80-5
3-Methylcholanthrene
ND
ug/kg
9740
10
08/25/22 05:38
08/26/22 13:38
56-49-5
4,4'-Methylene-bis(2-chloroani
ND
ug/kg
19500
10
08/25/22 05:38
08/26/22 13:38
101-14-4
Methyl methanesulfonate
ND
ug/kg
19500
10
08/25/22 05:38
08/26/22 13:38
66-27-3
1-Methylnaphthalene
ND
ug/kg
9740
10
08/25/22 05:38
08/26/22 13:38
90-12-0
2-Methylnaphthalene
ND
ug/kg
9740
10
08/25/22 05:38
08/26/22 13:38
91-57-6
2-Methyl-5-nitroaniline
ND
ug/kg
9740
10
08/25/22 05:38
08/26/22 13:38
99-55-8
Methyl parathion
ND
ug/kg
9740
10
08/25/22 05:38
08/26/22 13:38
298-00-0
2-Methylphenol(o-Cresol)
ND
ug/kg
9740
10
08/25/22 05:38
08/26/22 13:38
95-48-7
3&4-Methyl phenol (m&p Cresol)
ND
ug/kg
9740
10
08/25/22 05:38
08/26/22 13:38
15831-10-4
1-Naphthalenamine
ND
ug/kg
19500
10
08/25/22 05:38
08/26/22 13:38
134-32-7
2-Naphthalenamine
ND
ug/kg
19500
10
08/25/22 05:38
08/26/22 13:38
91-59-8
Naphthalene
ND
ug/kg
9740
10
08/25/22 05:38
08/26/22 13:38
91-20-3
1,4-Naphthoquinone
ND
ug/kg
48700
10
08/25/22 05:38
08/26/22 13:38
130-15-4
2-Nitroaniline
ND
ug/kg
48700
10
08/25/22 05:38
08/26/22 13:38
88-74-4
3-Nitroaniline
ND
ug/kg
48700
10
08/25/22 05:38
08/26/22 13:38
99-09-2
4-Nitroaniline
ND
ug/kg
19500
10
08/25/22 05:38
08/26/22 13:38
100-01-6
Nitrobenzene
ND
ug/kg
9740
10
08/25/22 05:38
08/26/22 13:38
98-95-3
REPORT OF LABORATORY ANALYSIS
IH
IH
Qual
This report shall not be reproduced, except in full,
Date: 10/25/2022 02:36 PM without the written consent of Pace Analytical Services, LLC. Page 56 of 165

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: WASTE CHARACTERIZATION
Pace Project No.: 92621331
Sample: HA-1 2-3' Lab ID: 92621331008 Collected: 08/16/22 13:00 Received: 08/17/22 16:15 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters
8270E MSSV Microwave
2-Nitrophenol
4-Nitrophenol
4-Nitroquinoline-n-oxide
5-Nitro-o-toluidine
N-Nitrosodiethylamine
N-Nitrosodimethylamine
N-Nitroso-di-n-butylamine
N-Nitroso-di-n-propylamine
N-Nitrosodiphenylamine
N-Nitrosomethylethylamine
N-Nitrosomorpholine
N-Nitrosopiperidine
N-Nitrosopyrrolidine
n-Octadecane
O,O,O-Triethylphosphorothioate
2,2'-Oxybis(1-chloropropane)
Parathion (Ethyl parathion)
Pentachlorobenzene
Pentachloroethane
Pentachloronitrobenzene
Pentachlorophenol
Phenacetin
Phenanthrene
Phenol
p-Phenylenediamine
Phorate
Phthalic anhydride
2-Picoline
Pronamide
Pyrene
Pyridine
Safrole
Sulfotepp (ThiodiphosphoricAc
Terpineol
1,2,4,5-Tetrachlorobenzene
2,3,4,6-Tetrachlorophenol
Thionazin
O-Toluidine
1,2,4-Trichlorobenzene
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
1,3,5-Trinitrobenzene
Surrogates
2-Fluorobiphenyl (S)
Terphenyl-d14 (S)
Results Units Report Limit DF Prepared Analyzed CAS No. Qual
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
ND
ug/kg
9740
10
08/25/22 05:38
08/26/22 13:38
88-75-5
ND
ug/kg
48700
10
08/25/22 05:38
08/26/22 13:38
100-02-7
ND
ug/kg
48700
10
08/25/22 05:38
08/26/22 13:38
56-57-5
ND
ug/kg
9740
10
08/25/22 05:38
08/26/22 13:38
99-55-8
ND
ug/kg
9740
10
08/25/22 05:38
08/26/22 13:38
55-18-5
ND
ug/kg
9740
10
08/25/22 05:38
08/26/22 13:38
62-75-9
ND
ug/kg
9740
10
08/25/22 05:38
08/26/22 13:38
924-16-3
ND
ug/kg
9740
10
08/25/22 05:38
08/26/22 13:38
621-64-7
ND
ug/kg
9740
10
08/25/22 05:38
08/26/22 13:38
86-30-6
ND
ug/kg
9740
10
08/25/22 05:38
08/26/22 13:38
10595-95-6
ND
ug/kg
9740
10
08/25/22 05:38
08/26/22 13:38
59-89-2
ND
ug/kg
19500
10
08/25/22 05:38
08/26/22 13:38
100-75-4
ND
ug/kg
19500
10
08/25/22 05:38
08/26/22 13:38
930-55-2
ND
ug/kg
9740
10
08/25/22 05:38
08/26/22 13:38
593-45-3
ND
ug/kg
9740
10
08/25/22 05:38
08/26/22 13:38
126-68-1
ND
ug/kg
9740
10
08/25/22 05:38
08/26/22 13:38
108-60-1
ND
ug/kg
9740
10
08/25/22 05:38
08/26/22 13:38
56-38-2
ND
ug/kg
9740
10
08/25/22 05:38
08/26/22 13:38
608-93-5
ND
ug/kg
9740
10
08/25/22 05:38
08/26/22 13:38
76-01-7
ND
ug/kg
9740
10
08/25/22 05:38
08/26/22 13:38
82-68-8
ND
ug/kg
19500
10
08/25/22 05:38
08/26/22 13:38
87-86-5
ND
ug/kg
19500
10
08/25/22 05:38
08/26/22 13:38
62-44-2
ND
ug/kg
9740
10
08/25/22 05:38
08/26/22 13:38
85-01-8
ND
ug/kg
9740
10
08/25/22 05:38
08/26/22 13:38
108-95-2
ND
ug/kg
19500
10
08/25/22 05:38
08/26/22 13:38
106-50-3 IL
ND
ug/kg
9740
10
08/25/22 05:38
08/26/22 13:38
298-02-2
ND
ug/kg
73800
10
08/25/22 05:38
08/26/22 13:38
85-44-9
ND
ug/kg
9740
10
08/25/22 05:38
08/26/22 13:38
109-06-8
ND
ug/kg
19500
10
08/25/22 05:38
08/26/22 13:38
23950-58-5
ND
ug/kg
9740
10
08/25/22 05:38
08/26/22 13:38
129-00-0
ND
ug/kg
9740
10
08/25/22 05:38
08/26/22 13:38
110-86-1
ND
ug/kg
19500
10
08/25/22 05:38
08/26/22 13:38
94-59-7
ND
ug/kg
9740
10
08/25/22 05:38
08/26/22 13:38
3689-24-5
ND
ug/kg
9740
10
08/25/22 05:38
08/26/22 13:38
98-55-5
ND
ug/kg
9740
10
08/25/22 05:38
08/26/22 13:38
95-94-3
ND
ug/kg
9740
10
08/25/22 05:38
08/26/22 13:38
58-90-2
ND
ug/kg
9740
10
08/25/22 05:38
08/26/22 13:38
297-97-2
ND
ug/kg
9740
10
08/25/22 05:38
08/26/22 13:38
95-53-4
ND
ug/kg
9740
10
08/25/22 05:38
08/26/22 13:38
120-82-1
ND
ug/kg
9740
10
08/25/22 05:38
08/26/22 13:38
95-95-4
ND
ug/kg
9740
10
08/25/22 05:38
08/26/22 13:38
88-06-2
ND
ug/kg
9740
10
08/25/22 05:38
08/26/22 13:38
99-35-4
0
%
19-130
10
08/25/22 05:38
08/26/22 13:38
321-60-8 D3,S4
0
%
15-130
10
08/25/22 05:38
08/26/22 13:38
1718-51-0 S4
REPORT
OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/25/2022 02:36 PM without the written consent of Pace Analytical Services, LLC. Page 57 of 165

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: WASTE CHARACTERIZATION
Pace Project No.: 92621331
Sample: HA-1 2-3'
Lab ID: 92621331008 Collected: 08/16/22 13:00 Received: 08/17/22 16:15 Matrix: Solid
Results reported on a "dry weight"
basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters
Results Units Report Limit DF Prepared
Analyzed
CAS No. Qual
8270E MSSV Microwave
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
Surrogates
Phenol-d6 (S)
0 % 18-130 10 08/25/22 05:38
08/26/22 13:38
13127-88-3 S4
2-Fluorophenol (S)
0 % 18-130 10 08/25/22 05:38
08/26/22 13:38
367-12-4 S4
2,4,6-Tribromophenol (S)
0 % 18-130 10 08/25/22 05:38
08/26/22 13:38
118-79-6 S4
Nitrobenzene-d5 (S)
0 % 21-130 10 08/25/22 05:38
08/26/22 13:38
4165-60-0 S4
Percent Moisture
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
46.0 % 0.10 1
08/22/22 15:40
N2
1010 Flash poi nt,Closed Cup
Analytical Method: EPA 1010B
Pace Analytical Services -Asheville
Flashpoint
>200 deg F 70.0 1
08/22/22 15:20
Total Solids 2540 G-2011
Analytical Method: SM 2540G Preparation Method: SM 2540 G
Pace National - Mt. Juliet
Total Solids
48.9 % 1 08/23/22 10:15
08/23/22 10:31
4500S21) Sulfide Soil
Analytical Method: SM 4500-S2D-2011 Modified Preparation Method: SM
4500-S2D-2011 Modified
Pace Analytical Services -Asheville
Sulfide
ND mg/kg 8.9 1 08/20/22 02:37
08/20/22 06:40
18496-25-8
9045 pH Soil
Analytical Method: EPA 9045D
Pace Analytical Services -Asheville
pH at 25 Degrees C
3.8 Std. Units 0.10 1
08/23/22 18:17
H3
9012 Cyanide, Total
Analytical Method: EPA 9012 Preparation Method: EPA 9012
Pace Analytical Services - Ormond Beach
Cyanide
7.3 mg/kg 4.5 10 08/29/22 09:41
08/29/22 15:22
57-12-5
Date: 10/25/2022 02:36 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 58 of 165

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: WASTE CHARACTERIZATION
Pace Project No.: 92621331
Sample: HA-2 2-3' Lab ID: 92621331009 Collected: 08/16/22 13:15 Received: 08/17/22 16:15 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
OP Pesticides 8141 B
Analytical Method: EPA 8141 B Preparation Method: 3546
Pace National
- Mt. Juliet
Azinphos, methyl (Guthion)
ND
mg/kg
0.198
1
08/21/22 16:12
08/22/22 05:25
86-50-0
Bolstar
ND
mg/kg
0.198
1
08/21/22 16:12
08/22/22 05:25
35400-43-2
Chlorpyrifos
ND
mg/kg
0.198
1
08/21/22 16:12
08/22/22 05:25
2921-88-2
Coumaphos
ND
mg/kg
0.198
1
08/21/22 16:12
08/22/22 05:25
56-72-4
Total Demeton
ND
mg/kg
0.138
1
08/21/22 16:12
08/22/22 05:25
8065-48-3
Diazinon
ND
mg/kg
0.198
1
08/21/22 16:12
08/22/22 05:25
333-41-5
Dichlorvos
ND
mg/kg
0.198
1
08/21/22 16:12
08/22/22 05:25
62-73-7
Dimethoate
ND
mg/kg
0.198
1
08/21/22 16:12
08/22/22 05:25
60-51-5
Disulfoton
ND
mg/kg
0.198
1
08/21/22 16:12
08/22/22 05:25
298-04-4
EPN (ENT)
ND
mg/kg
0.198
1
08/21/22 16:12
08/22/22 05:25
2104-64-5
Ethoprop
ND
mg/kg
0.198
1
08/21/22 16:12
08/22/22 05:25
13194-48-4
Parathion (Ethyl parathion)
ND
mg/kg
0.198
1
08/21/22 16:12
08/22/22 05:25
56-38-2
Fensulfothion
ND
mg/kg
0.198
1
08/21/22 16:12
08/22/22 05:25
115-90-2
Fenthion
ND
mg/kg
0.198
1
08/21/22 16:12
08/22/22 05:25
55-38-9
Malathion
ND
mg/kg
0.198
1
08/21/22 16:12
08/22/22 05:25
121-75-5
Merphos
ND
mg/kg
0.198
1
08/21/22 16:12
08/22/22 05:25
150-50-5
Methyl parathion
ND
mg/kg
0.198
1
08/21/22 16:12
08/22/22 05:25
298-00-0
Mevinphos
ND
mg/kg
0.198
1
08/21/22 16:12
08/22/22 05:25
7786-34-7
Naled
ND
mg/kg
0.198
1
08/21/22 16:12
08/22/22 05:25
300-76-5
Phorate
ND
mg/kg
0.198
1
08/21/22 16:12
08/22/22 05:25
298-02-2
Ronnel
ND
mg/kg
0.198
1
08/21/22 16:12
08/22/22 05:25
299-84-3
Stirophos (Tetrachlorvinphos)
ND
mg/kg
0.198
1
08/21/22 16:12
08/22/22 05:25
22248-79-9
Sulfotepp (ThiodiphosphoricAc
ND
mg/kg
0.198
1
08/21/22 16:12
08/22/22 05:25
3689-24-5
TEPP
ND
mg/kg
1.98
1
08/21/22 16:12
08/22/22 05:25
107-49-3
Tokuthion (Prothiofos)
ND
mg/kg
0.198
1
08/21/22 16:12
08/22/22 05:25
34643-46-4
Trichloronate
ND
mg/kg
0.198
1
08/21/22 16:12
08/22/22 05:25
327-98-0
Surrogates
Triphenyl phosphate (S)
49.1
%
36.0-121
1
08/21/22 16:12
08/22/22 05:25
115-86-6
8081 GCS Pesticides
Analytical Method: EPA 8081 B Preparation Method: EPA 3546
Pace Analytical
Services - Charlotte
Aldrin
ND
ug/kg
94.0
20
08/24/22 07:17
08/26/22 19:02
309-00-2
alpha-BHC
ND
ug/kg
94.0
20
08/24/22 07:17
08/26/22 19:02
319-84-6
beta-BHC
ND
ug/kg
94.0
20
08/24/22 07:17
08/26/22 19:02
319-85-7
delta-BHC
ND
ug/kg
94.0
20
08/24/22 07:17
08/26/22 19:02
319-86-8
gamma-BHC (Lindane)
ND
ug/kg
94.0
20
08/24/22 07:17
08/26/22 19:02
58-89-9
Chlordane (Technical)
1060
ug/kg
470
20
08/24/22 07:17
08/26/22 19:02
57-74-9
4,4'-DDD
ND
ug/kg
94.0
20
08/24/22 07:17
08/26/22 19:02
72-54-8
4,4'-DDE
ND
ug/kg
94.0
20
08/24/22 07:17
08/26/22 19:02
72-55-9
4,4'-DDT
ND
ug/kg
94.0
20
08/24/22 07:17
08/26/22 19:02
50-29-3
Dieldrin
ND
ug/kg
94.0
20
08/24/22 07:17
08/26/22 19:02
60-57-1
Endosulfan I
ND
ug/kg
94.0
20
08/24/22 07:17
08/26/22 19:02
959-98-8
Endosulfan II
ND
ug/kg
94.0
20
08/24/22 07:17
08/26/22 19:02
33213-65-9
Endosulfan sulfate
ND
ug/kg
94.0
20
08/24/22 07:17
08/26/22 19:02
1031-07-8
Endrin
ND
ug/kg
94.0
20
08/24/22 07:17
08/26/22 19:02
72-20-8
REPORT OF LABORATORY ANALYSIS
LO
This report shall not be reproduced, except in full,
Date: 10/25/2022 02:36 PM without the written consent of Pace Analytical Services, LLC. Page 59 of 165

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: WASTE CHARACTERIZATION
Pace Project No.: 92621331
Sample: HA-2 2-3' Lab ID: 92621331009 Collected: 08/16/22 13:15 Received: 08/17/22 16:15 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8081 GCS Pesticides
Endrin aldehyde
Endrin ketone
Heptachlor
Heptachlor epoxide
Hexachlorobenzene
Methoxychlor
Mirex
Toxaphene
Surrogates
Tetrachloro-m-xylene (S)
Decachlorobiphenyl (S)
8082 GCS PCB
PCB-1016 (Aroclor 1016)
PCB-1221 (Aroclor 1221)
PCB-1232 (Aroclor 1232)
PCB-1242 (Aroclor 1242)
PCB-1248 (Aroclor 1248)
PCB-1254 (Aroclor 1254)
PCB-1260 (Aroclor 1260)
Surrogates
Decachlorobiphenyl (S)
Analytical Method: EPA 8081 B Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
ND
ug/kg
94.0
20
08/24/22 07:17
08/26/22 19:02
7421-93-4
ND
ug/kg
94.0
20
08/24/22 07:17
08/26/22 19:02
53494-70-5
ND
ug/kg
94.0
20
08/24/22 07:17
08/26/22 19:02
76-44-8
ND
ug/kg
94.0
20
08/24/22 07:17
08/26/22 19:02
1024-57-3
ND
ug/kg
94.0
20
08/24/22 07:17
08/26/22 19:02
118-74-1
ND
ug/kg
235
20
08/24/22 07:17
08/26/22 19:02
72-43-5
ND
ug/kg
235
20
08/24/22 07:17
08/26/22 19:02
2385-85-5
ND
ug/kg
329
20
08/24/22 07:17
08/26/22 19:02
8001-35-2
0
%
10-133
20
08/24/22 07:17
08/26/22 19:02
877-09-8 D3,S4
0
%
10-146
20
08/24/22 07:17
08/26/22 19:02
2051-24-3 S4
Analytical Method: EPA 8082A Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
ND
ug/kg
1530
20
08/19/22 15:53
08/24/22 07:47
12674-11-2
ND
ug/kg
1530
20
08/19/22 15:53
08/24/22 07:47
11104-28-2
ND
ug/kg
1530
20
08/19/22 15:53
08/24/22 07:47
11141-16-5
ND
ug/kg
1530
20
08/19/22 15:53
08/24/22 07:47
53469-21-9
ND
ug/kg
1530
20
08/19/22 15:53
08/24/22 07:47
12672-29-6
2390
ug/kg
1530
20
08/19/22 15:53
08/24/22 07:47
11097-69-1
ND
ug/kg
1530
20
08/19/22 15:53
08/24/22 07:47
11096-82-5
0
%
10-160
20
08/19/22 15:53
08/24/22 07:47
2051-24-3 D3,S4
6010 MET ICP
Analytical Method: EPA 6010 Preparation Method: EPA 3050
Pace Analytical
Services - Ormond Beach
Tin
189
mg/kg
7.0
1
08/30/2219:03
08/31/2218:38
7440-31-5
6020 MET ICPMS
Analytical Method: EPA 6020 Preparation Method: EPA 3050
Pace Analytical
Services - Ormond Beach
Antimony
256
mg/kg
5.0
20
08/27/22 00:15
08/29/22 19:53
7440-36-0
1g,N2
Arsenic
8.6
mg/kg
2.5
20
08/27/22 00:15
08/29/22 19:53
7440-38-2
1g
Barium
1710
mg/kg
24.9
200
08/27/22 00:15
08/31/22 14:25
7440-39-3
1g
Beryllium
0.75
mg/kg
0.30
20
08/27/22 00:15
08/29/22 19:53
7440-41-7
1g
Cadmium
9.1
mg/kg
0.30
20
08/27/22 00:15
08/29/22 19:53
7440-43-9
1g
Chromium
3160
mg/kg
24.9
200
08/27/22 00:15
08/31/22 14:25
7440-47-3
1g
Cobalt
10.5
mg/kg
2.5
20
08/27/22 00:15
08/29/22 19:53
7440-48-4
1g
Copper
500
mg/kg
5.0
20
08/27/22 00:15
08/29/22 10:30
7440-50-8
1g
Lead
2870
mg/kg
24.9
200
08/27/22 00:15
08/31/22 14:25
7439-92-1
1g
Nickel
21.7
mg/kg
2.5
20
08/27/22 00:15
08/29/22 19:53
7440-02-0
1g
Selenium
8.0
mg/kg
2.5
20
08/27/22 00:15
08/29/22 19:53
7782-49-2
1g
Silver
163
mg/kg
3.0
200
08/27/22 00:15
08/31/22 14:25
7440-22-4
1g
Thallium
ND
mg/kg
2.5
20
08/27/22 00:15
08/29/22 19:53
7440-28-0
1g
Vanadium
53.4
mg/kg
2.5
20
08/27/22 00:15
08/29/22 19:53
7440-62-2
1g
Zinc
177
mg/kg
99.4
20
08/27/22 00:15
08/29/22 19:53
7440-66-6
1g
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/25/2022 02:36 PM without the written consent of Pace Analytical Services, LLC. Page 60 of 165

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: WASTE CHARACTERIZATION
Pace Project No.: 92621331
Sample: HA-2 2-3' Lab ID: 92621331009 Collected: 08/16/22 13:15 Received: 08/17/22 16:15 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No
7471 Mercury
Analytical Method: EPA 7471
Preparation Method: EPA 7471
Pace Analytical
Services - Ormond Beach
Mercury
12.5
mg/kg
0.43
20
08/24/22 07:26
08/24/22 12:02
7439-97-6
8270E MSSV Microwave
Analytical Method: EPA 8270E Preparation Method:
EPA 3546
Pace Analytical
Services - Charlotte
Acenaphthene
ND
ug/kg
10200
10
08/25/22 05:38
08/26/22 14:08
83-32-9
Acenaphthylene
ND
ug/kg
10200
10
08/25/22 05:38
08/26/22 14:08
208-96-8
Acetophenone
ND
ug/kg
10200
10
08/25/22 05:38
08/26/22 14:08
98-86-2
2-Acetylaminofluorene
ND
ug/kg
20300
10
08/25/22 05:38
08/26/22 14:08
53-96-3
4-Aminobiphenyl
ND
ug/kg
10200
10
08/25/22 05:38
08/26/22 14:08
92-67-1
Anthracene
ND
ug/kg
10200
10
08/25/22 05:38
08/26/22 14:08
120-12-7
Benzo(a)anthracene
ND
ug/kg
10200
10
08/25/22 05:38
08/26/22 14:08
56-55-3
Benzo(a)pyrene
ND
ug/kg
10200
10
08/25/22 05:38
08/26/22 14:08
50-32-8
Benzo(b)fluoranthene
ND
ug/kg
10200
10
08/25/22 05:38
08/26/22 14:08
205-99-2
Benzo(g,h,i)perylene
ND
ug/kg
10200
10
08/25/22 05:38
08/26/22 14:08
191-24-2
Benzo(k)fluoranthene
ND
ug/kg
10200
10
08/25/22 05:38
08/26/22 14:08
207-08-9
Benzyl alcohol
ND
ug/kg
20300
10
08/25/22 05:38
08/26/22 14:08
100-51-6
bis(2-Chloroethoxy)methane
ND
ug/kg
10200
10
08/25/22 05:38
08/26/22 14:08
111-91-1
bis(2-Chloroethyl) ether
ND
ug/kg
10200
10
08/25/22 05:38
08/26/22 14:08
111-44-4
2-Chloronaphthalene
ND
ug/kg
10200
10
08/25/22 05:38
08/26/22 14:08
91-58-7
2-Chlorophenol
ND
ug/kg
10200
10
08/25/22 05:38
08/26/22 14:08
95-57-8
4-Chlorophenylphenyl ether
ND
ug/kg
10200
10
08/25/22 05:38
08/26/22 14:08
7005-72-3
Chrysene
ND
ug/kg
10200
10
08/25/22 05:38
08/26/22 14:08
218-01-9
n-Decane
ND
ug/kg
10200
10
08/25/22 05:38
08/26/22 14:08
124-18-5
Diallate
ND
ug/kg
10200
10
08/25/22 05:38
08/26/22 14:08
2303-16-4
Dibenz(a,h)anthracene
ND
ug/kg
10200
10
08/25/22 05:38
08/26/22 14:08
53-70-3
Dibenzo(a,e)pyrene
ND
ug/kg
30800
10
08/25/22 05:38
08/26/22 14:08
192-65-4
Dibenzofuran
ND
ug/kg
10200
10
08/25/22 05:38
08/26/22 14:08
132-64-9
2,3-Dibromo-1-propanol phosph
ND
ug/kg
50900
10
08/25/22 05:38
08/26/22 14:08
126-72-7
1,2-Dichlorobenzene
ND
ug/kg
10200
10
08/25/22 05:38
08/26/22 14:08
95-50-1
1,3-Dichlorobenzene
ND
ug/kg
10200
10
08/25/22 05:38
08/26/22 14:08
541-73-1
1,4-Dichlorobenzene
ND
ug/kg
10200
10
08/25/22 05:38
08/26/22 14:08
106-46-7
3,3'-Dichlorobenzidine
ND
ug/kg
20300
10
08/25/22 05:38
08/26/22 14:08
91-94-1
2,4-Dichlorophenol
ND
ug/kg
10200
10
08/25/22 05:38
08/26/22 14:08
120-83-2
2,6-Dichlorophenol
ND
ug/kg
10200
10
08/25/22 05:38
08/26/22 14:08
87-65-0
2,3-Dichloroaniline
ND
ug/kg
10200
10
08/25/22 05:38
08/26/22 14:08
608-27-5
Diethylphthalate
ND
ug/kg
10200
10
08/25/22 05:38
08/26/22 14:08
84-66-2
Dimethoate
ND
ug/kg
20300
10
08/25/22 05:38
08/26/22 14:08
60-51-5
P-Dimethylaminoazobenzene
ND
ug/kg
10200
10
08/25/22 05:38
08/26/22 14:08
60-11-7
7,12-Dimethylbenz(a)anthracene
ND
ug/kg
10200
10
08/25/22 05:38
08/26/22 14:08
57-97-6
3,3'-Dimethylbenzidine
ND
ug/kg
20300
10
08/25/22 05:38
08/26/22 14:08
119-93-7
2,4-Dimethylphenol
ND
ug/kg
10200
10
08/25/22 05:38
08/26/22 14:08
105-67-9
a,a-Dimethylphenylethylamine
ND
ug/kg
50900
10
08/25/22 05:38
08/26/22 14:08
122-09-8
Dimethylphthalate
ND
ug/kg
10200
10
08/25/22 05:38
08/26/22 14:08
131-11-3
Di-n-butylphthalate
ND
ug/kg
10200
10
08/25/22 05:38
08/26/22 14:08
84-74-2
4,6-Dinitro-2-methyl phenol
ND
ug/kg
20300
10
08/25/22 05:38
08/26/22 14:08
534-52-1
REPORT OF LABORATORY ANALYSIS
IL
IL
IH
Qual
This report shall not be reproduced, except in full,
Date: 10/25/2022 02:36 PM without the written consent of Pace Analytical Services, LLC. Page 61 of 165

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: WASTE CHARACTERIZATION
Pace Project No.: 92621331
Sample: HA-2 2-3' Lab ID: 92621331009 Collected: 08/16/22 13:15 Received: 08/17/22 16:15 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No
8270E MSSV Microwave
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical
Services - Charlotte
1,3-Dinitrobenzene
ND
ug/kg
10200
10
08/25/22 05:38
08/26/22 14:08
99-65-0
1,4-Dinitrobenzene
ND
ug/kg
10200
10
08/25/22 05:38
08/26/22 14:08
100-25-4
2,4-Dinitrophenol
ND
ug/kg
50900
10
08/25/22 05:38
08/26/22 14:08
51-28-5
2,4-Dinitrotoluene
ND
ug/kg
10200
10
08/25/22 05:38
08/26/22 14:08
121-14-2
2,6-Dinitrotoluene
ND
ug/kg
10200
10
08/25/22 05:38
08/26/22 14:08
606-20-2
Di-n-octylphthalate
ND
ug/kg
10200
10
08/25/22 05:38
08/26/22 14:08
117-84-0
Dinoseb
ND
ug/kg
20300
10
08/25/22 05:38
08/26/22 14:08
88-85-7
Diphenylamine
ND
ug/kg
10200
10
08/25/22 05:38
08/26/22 14:08
122-39-4
Diphenyl ether (Phenyl ether)
ND
ug/kg
15400
10
08/25/22 05:38
08/26/22 14:08
101-84-8
1,2-Diphenylhydrazine
ND
ug/kg
10200
10
08/25/22 05:38
08/26/22 14:08
122-66-7
Disulfoton
ND
ug/kg
10200
10
08/25/22 05:38
08/26/22 14:08
298-04-4
bis(2- Ethyl hexyl)phthalate
27900
ug/kg
10200
10
08/25/22 05:38
08/26/22 14:08
117-81-7
Ethyl methanesulfonate
ND
ug/kg
20300
10
08/25/22 05:38
08/26/22 14:08
62-50-0
Famphur
ND
ug/kg
20300
10
08/25/22 05:38
08/26/22 14:08
52-85-7
Fluoranthene
ND
ug/kg
10200
10
08/25/22 05:38
08/26/22 14:08
206-44-0
Fluorene
ND
ug/kg
10200
10
08/25/22 05:38
08/26/22 14:08
86-73-7
Hexachloro-1,3-butadiene
ND
ug/kg
10200
10
08/25/22 05:38
08/26/22 14:08
87-68-3
Hexachlorobenzene
ND
ug/kg
10200
10
08/25/22 05:38
08/26/22 14:08
118-74-1
Hexachlorocyclopentadiene
ND
ug/kg
10200
10
08/25/22 05:38
08/26/22 14:08
77-47-4
Hexachloroethane
ND
ug/kg
10200
10
08/25/22 05:38
08/26/22 14:08
67-72-1
Hexachlorophene
ND
ug/kg
102000
10
08/25/22 05:38
08/26/22 14:08
70-30-4
Hexachloropropene
ND
ug/kg
10200
10
08/25/22 05:38
08/26/22 14:08
1888-71-7
Indeno(1,2,3-cd)pyrene
ND
ug/kg
10200
10
08/25/22 05:38
08/26/22 14:08
193-39-5
Isodrin
ND
ug/kg
10200
10
08/25/22 05:38
08/26/22 14:08
465-73-6
Isophorone
ND
ug/kg
10200
10
08/25/22 05:38
08/26/22 14:08
78-59-1
Isosafrole
ND
ug/kg
10200
10
08/25/22 05:38
08/26/22 14:08
120-58-1
Kepone
ND
ug/kg
20300
10
08/25/22 05:38
08/26/22 14:08
143-50-0
Methapyrilene
ND
ug/kg
50900
10
08/25/22 05:38
08/26/22 14:08
91-80-5
3-Methylcholanthrene
ND
ug/kg
10200
10
08/25/22 05:38
08/26/22 14:08
56-49-5
4,4'-Methylene-bis(2-chloroani
ND
ug/kg
20300
10
08/25/22 05:38
08/26/22 14:08
101-14-4
Methyl methanesulfonate
ND
ug/kg
20300
10
08/25/22 05:38
08/26/22 14:08
66-27-3
1-Methylnaphthalene
ND
ug/kg
10200
10
08/25/22 05:38
08/26/22 14:08
90-12-0
2-Methylnaphthalene
ND
ug/kg
10200
10
08/25/22 05:38
08/26/22 14:08
91-57-6
2-Methyl-5-nitroaniline
ND
ug/kg
10200
10
08/25/22 05:38
08/26/22 14:08
99-55-8
Methyl parathion
ND
ug/kg
10200
10
08/25/22 05:38
08/26/22 14:08
298-00-0
2-Methylphenol(o-Cresol)
ND
ug/kg
10200
10
08/25/22 05:38
08/26/22 14:08
95-48-7
3&4-Methyl phenol (m&p Cresol)
ND
ug/kg
10200
10
08/25/22 05:38
08/26/22 14:08
15831-10-4
1-Naphthalenamine
ND
ug/kg
20300
10
08/25/22 05:38
08/26/22 14:08
134-32-7
2-Naphthalenamine
ND
ug/kg
20300
10
08/25/22 05:38
08/26/22 14:08
91-59-8
Naphthalene
ND
ug/kg
10200
10
08/25/22 05:38
08/26/22 14:08
91-20-3
1,4-Naphthoquinone
ND
ug/kg
50900
10
08/25/22 05:38
08/26/22 14:08
130-15-4
2-Nitroaniline
ND
ug/kg
50900
10
08/25/22 05:38
08/26/22 14:08
88-74-4
3-Nitroaniline
ND
ug/kg
50900
10
08/25/22 05:38
08/26/22 14:08
99-09-2
4-Nitroaniline
ND
ug/kg
20300
10
08/25/22 05:38
08/26/22 14:08
100-01-6
Nitrobenzene
ND
ug/kg
10200
10
08/25/22 05:38
08/26/22 14:08
98-95-3
REPORT OF LABORATORY ANALYSIS
IH
IH
Qual
This report shall not be reproduced, except in full,
Date: 10/25/2022 02:36 PM without the written consent of Pace Analytical Services, LLC. Page 62 of 165

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: WASTE CHARACTERIZATION
Pace Project No.: 92621331
Sample: HA-2 2-3' Lab ID: 92621331009 Collected: 08/16/22 13:15 Received: 08/17/22 16:15 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters
8270E MSSV Microwave
2-Nitrophenol
4-Nitrophenol
4-Nitroquinoline-n-oxide
5-Nitro-o-toluidine
N-Nitrosodiethylamine
N-Nitrosodimethylamine
N-Nitroso-di-n-butylamine
N-Nitroso-di-n-propylamine
N-Nitrosodiphenylamine
N-Nitrosomethylethylamine
N-Nitrosomorpholine
N-Nitrosopiperidine
N-Nitrosopyrrolidine
n-Octadecane
O,O,O-Triethylphosphorothioate
2,2'-Oxybis(1-chloropropane)
Parathion (Ethyl parathion)
Pentachlorobenzene
Pentachloroethane
Pentachloronitrobenzene
Pentachlorophenol
Phenacetin
Phenanthrene
Phenol
p-Phenylenediamine
Phorate
Phthalic anhydride
2-Picoline
Pronamide
Pyrene
Pyridine
Safrole
Sulfotepp (ThiodiphosphoricAc
Terpineol
1,2,4,5-Tetrachlorobenzene
2,3,4,6-Tetrachlorophenol
Thionazin
O-Toluidine
1,2,4-Trichlorobenzene
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
1,3,5-Trinitrobenzene
Surrogates
2-Fluorobiphenyl (S)
Terphenyl-d14 (S)
Results Units Report Limit DF Prepared Analyzed CAS No. Qual
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
ND
ug/kg
10200
10
08/25/22 05:38
08/26/22 14:08
88-75-5
ND
ug/kg
50900
10
08/25/22 05:38
08/26/22 14:08
100-02-7
ND
ug/kg
50900
10
08/25/22 05:38
08/26/22 14:08
56-57-5
ND
ug/kg
10200
10
08/25/22 05:38
08/26/22 14:08
99-55-8
ND
ug/kg
10200
10
08/25/22 05:38
08/26/22 14:08
55-18-5
ND
ug/kg
10200
10
08/25/22 05:38
08/26/22 14:08
62-75-9
ND
ug/kg
10200
10
08/25/22 05:38
08/26/22 14:08
924-16-3
ND
ug/kg
10200
10
08/25/22 05:38
08/26/22 14:08
621-64-7
ND
ug/kg
10200
10
08/25/22 05:38
08/26/22 14:08
86-30-6
ND
ug/kg
10200
10
08/25/22 05:38
08/26/22 14:08
10595-95-6
ND
ug/kg
10200
10
08/25/22 05:38
08/26/22 14:08
59-89-2
ND
ug/kg
20300
10
08/25/22 05:38
08/26/22 14:08
100-75-4
ND
ug/kg
20300
10
08/25/22 05:38
08/26/22 14:08
930-55-2
ND
ug/kg
10200
10
08/25/22 05:38
08/26/22 14:08
593-45-3
ND
ug/kg
10200
10
08/25/22 05:38
08/26/22 14:08
126-68-1
ND
ug/kg
10200
10
08/25/22 05:38
08/26/22 14:08
108-60-1
ND
ug/kg
10200
10
08/25/22 05:38
08/26/22 14:08
56-38-2
ND
ug/kg
10200
10
08/25/22 05:38
08/26/22 14:08
608-93-5
ND
ug/kg
10200
10
08/25/22 05:38
08/26/22 14:08
76-01-7
ND
ug/kg
10200
10
08/25/22 05:38
08/26/22 14:08
82-68-8
ND
ug/kg
20300
10
08/25/22 05:38
08/26/22 14:08
87-86-5
ND
ug/kg
20300
10
08/25/22 05:38
08/26/22 14:08
62-44-2
ND
ug/kg
10200
10
08/25/22 05:38
08/26/22 14:08
85-01-8
ND
ug/kg
10200
10
08/25/22 05:38
08/26/22 14:08
108-95-2
ND
ug/kg
20300
10
08/25/22 05:38
08/26/22 14:08
106-50-3 IL
ND
ug/kg
10200
10
08/25/22 05:38
08/26/22 14:08
298-02-2
ND
ug/kg
77100
10
08/25/22 05:38
08/26/22 14:08
85-44-9
ND
ug/kg
10200
10
08/25/22 05:38
08/26/22 14:08
109-06-8
ND
ug/kg
20300
10
08/25/22 05:38
08/26/22 14:08
23950-58-5
ND
ug/kg
10200
10
08/25/22 05:38
08/26/22 14:08
129-00-0
ND
ug/kg
10200
10
08/25/22 05:38
08/26/22 14:08
110-86-1
ND
ug/kg
20300
10
08/25/22 05:38
08/26/22 14:08
94-59-7
ND
ug/kg
10200
10
08/25/22 05:38
08/26/22 14:08
3689-24-5
ND
ug/kg
10200
10
08/25/22 05:38
08/26/22 14:08
98-55-5
ND
ug/kg
10200
10
08/25/22 05:38
08/26/22 14:08
95-94-3
ND
ug/kg
10200
10
08/25/22 05:38
08/26/22 14:08
58-90-2
ND
ug/kg
10200
10
08/25/22 05:38
08/26/22 14:08
297-97-2
ND
ug/kg
10200
10
08/25/22 05:38
08/26/22 14:08
95-53-4
ND
ug/kg
10200
10
08/25/22 05:38
08/26/22 14:08
120-82-1
ND
ug/kg
10200
10
08/25/22 05:38
08/26/22 14:08
95-95-4
ND
ug/kg
10200
10
08/25/22 05:38
08/26/22 14:08
88-06-2
ND
ug/kg
10200
10
08/25/22 05:38
08/26/22 14:08
99-35-4
0
%
19-130
10
08/25/22 05:38
08/26/22 14:08
321-60-8 D3,S4
0
%
15-130
10
08/25/22 05:38
08/26/22 14:08
1718-51-0 S4
REPORT
OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/25/2022 02:36 PM without the written consent of Pace Analytical Services, LLC. Page 63 of 165

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: WASTE CHARACTERIZATION
Pace Project No.: 92621331
Sample: HA-2 2-3'
Lab ID: 92621331009 Collected: 08/16/22 13:15 Received: 08/17/22 16:15 Matrix: Solid
Results reported on a "dry weight"
basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters
Results Units Report Limit DF Prepared
Analyzed
CAS No. Qual
8270E MSSV Microwave
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
Surrogates
Phenol-d6 (S)
0 % 18-130 10 08/25/22 05:38
08/26/22 14:08
13127-88-3 S4
2-Fluorophenol (S)
0 % 18-130 10 08/25/22 05:38
08/26/22 14:08
367-12-4 S4
2,4,6-Tribromophenol (S)
0 % 18-130 10 08/25/22 05:38
08/26/22 14:08
118-79-6 S4
Nitrobenzene-d5 (S)
0 % 21-130 10 08/25/22 05:38
08/26/22 14:08
4165-60-0 S4
Percent Moisture
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
57.3 % 0.10 1
08/22/22 15:40
N2
1010 Flash poi nt,Closed Cup
Analytical Method: EPA 1010B
Pace Analytical Services -Asheville
Flashpoint
>200 deg F 70.0 1
08/23/22 11:03
Total Solids 2540 G-2011
Analytical Method: SM 2540G Preparation Method: SM 2540 G
Pace National - Mt. Juliet
Total Solids
50.6 % 1 08/23/22 10:15
08/23/22 10:31
4500S21) Sulfide Soil
Analytical Method: SM 4500-S2D-2011 Modified Preparation Method: SM
4500-S2D-2011 Modified
Pace Analytical Services -Asheville
Sulfide
ND mg/kg 11.2 1 08/20/22 02:37
08/20/22 06:41
18496-25-8
9045 pH Soil
Analytical Method: EPA 9045D
Pace Analytical Services -Asheville
pH at 25 Degrees C
3.9 Std. Units 0.10 1
08/23/22 18:18
H3
9012 Cyanide, Total
Analytical Method: EPA 9012 Preparation Method: EPA 9012
Pace Analytical Services - Ormond Beach
Cyanide
12.0 mg/kg 5.9 10 08/29/22 09:41
08/29/22 15:25
57-12-5
Date: 10/25/2022 02:36 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 64 of 165

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: WASTE CHARACTERIZATION
Pace Project No.: 92621331
Sample: SURFACE BASIN 3 Lab ID: 92621331010 Collected: 08/16/22 13:30 Received: 08/17/22 16:15 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
OP Pesticides 8141 B
Analytical Method: EPA 8141 B Preparation Method: 3546
Pace National
- Mt. Juliet
Azinphos, methyl (Guthion)
ND
mg/kg
0.201
1
08/21/22 16:12
08/22/22 05:58
86-50-0
Bolstar
ND
mg/kg
0.201
1
08/21/22 16:12
08/22/22 05:58
35400-43-2
Chlorpyrifos
ND
mg/kg
0.201
1
08/21/22 16:12
08/22/22 05:58
2921-88-2
Coumaphos
ND
mg/kg
0.201
1
08/21/22 16:12
08/22/22 05:58
56-72-4
Total Demeton
ND
mg/kg
0.141
1
08/21/22 16:12
08/22/22 05:58
8065-48-3
Diazinon
ND
mg/kg
0.201
1
08/21/22 16:12
08/22/22 05:58
333-41-5
Dichlorvos
ND
mg/kg
0.201
1
08/21/22 16:12
08/22/22 05:58
62-73-7
Dimethoate
ND
mg/kg
0.201
1
08/21/22 16:12
08/22/22 05:58
60-51-5
Disulfoton
ND
mg/kg
0.201
1
08/21/22 16:12
08/22/22 05:58
298-04-4
EPN (ENT)
ND
mg/kg
0.201
1
08/21/22 16:12
08/22/22 05:58
2104-64-5
Ethoprop
ND
mg/kg
0.201
1
08/21/22 16:12
08/22/22 05:58
13194-48-4
Parathion (Ethyl parathion)
ND
mg/kg
0.201
1
08/21/22 16:12
08/22/22 05:58
56-38-2
Fensulfothion
ND
mg/kg
0.201
1
08/21/22 16:12
08/22/22 05:58
115-90-2
Fenthion
ND
mg/kg
0.201
1
08/21/22 16:12
08/22/22 05:58
55-38-9
Malathion
ND
mg/kg
0.201
1
08/21/22 16:12
08/22/22 05:58
121-75-5
Merphos
ND
mg/kg
0.201
1
08/21/22 16:12
08/22/22 05:58
150-50-5
Methyl parathion
ND
mg/kg
0.201
1
08/21/22 16:12
08/22/22 05:58
298-00-0
Mevinphos
ND
mg/kg
0.201
1
08/21/22 16:12
08/22/22 05:58
7786-34-7
Naled
ND
mg/kg
0.201
1
08/21/22 16:12
08/22/22 05:58
300-76-5
Phorate
ND
mg/kg
0.201
1
08/21/22 16:12
08/22/22 05:58
298-02-2
Ronnel
ND
mg/kg
0.201
1
08/21/22 16:12
08/22/22 05:58
299-84-3
Stirophos (Tetrachlorvinphos)
ND
mg/kg
0.201
1
08/21/22 16:12
08/22/22 05:58
22248-79-9
Sulfotepp (ThiodiphosphoricAc
ND
mg/kg
0.201
1
08/21/22 16:12
08/22/22 05:58
3689-24-5
TEPP
ND
mg/kg
2.01
1
08/21/22 16:12
08/22/22 05:58
107-49-3
Tokuthion (Prothiofos)
ND
mg/kg
0.201
1
08/21/22 16:12
08/22/22 05:58
34643-46-4
Trichloronate
ND
mg/kg
0.201
1
08/21/22 16:12
08/22/22 05:58
327-98-0
Surrogates
Triphenyl phosphate (S)
51.7
%
36.0-121
1
08/21/22 16:12
08/22/22 05:58
115-86-6
8081 GCS Pesticides
Analytical Method: EPA 8081 B Preparation Method: EPA 3546
Pace Analytical
Services - Charlotte
Aldrin
ND
ug/kg
45.1
10
08/24/22 07:17
08/26/22 19:13
309-00-2
alpha-BHC
ND
ug/kg
45.1
10
08/24/22 07:17
08/26/22 19:13
319-84-6
beta-BHC
ND
ug/kg
45.1
10
08/24/22 07:17
08/26/22 19:13
319-85-7
delta-BHC
ND
ug/kg
45.1
10
08/24/22 07:17
08/26/22 19:13
319-86-8
gamma-BHC (Lindane)
ND
ug/kg
45.1
10
08/24/22 07:17
08/26/22 19:13
58-89-9
Chlordane (Technical)
1080
ug/kg
226
10
08/24/22 07:17
08/26/22 19:13
57-74-9
4,4'-DDD
ND
ug/kg
45.1
10
08/24/22 07:17
08/26/22 19:13
72-54-8
4,4'-DDE
ND
ug/kg
45.1
10
08/24/22 07:17
08/26/22 19:13
72-55-9
4,4'-DDT
ND
ug/kg
45.1
10
08/24/22 07:17
08/26/22 19:13
50-29-3
Dieldrin
ND
ug/kg
45.1
10
08/24/22 07:17
08/26/22 19:13
60-57-1
Endosulfan I
ND
ug/kg
45.1
10
08/24/22 07:17
08/26/22 19:13
959-98-8
Endosulfan II
ND
ug/kg
45.1
10
08/24/22 07:17
08/26/22 19:13
33213-65-9
Endosulfan sulfate
ND
ug/kg
45.1
10
08/24/22 07:17
08/26/22 19:13
1031-07-8
Endrin
ND
ug/kg
45.1
10
08/24/22 07:17
08/26/22 19:13
72-20-8
REPORT OF LABORATORY ANALYSIS
LO
This report shall not be reproduced, except in full,
Date: 10/25/2022 02:36 PM without the written consent of Pace Analytical Services, LLC. Page 65 of 165

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: WASTE CHARACTERIZATION
Pace Project No.: 92621331
Sample: SURFACE BASIN 3 Lab ID: 92621331010 Collected: 08/16/22 13:30 Received: 08/17/22 16:15 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8081 GCS Pesticides
Endrin aldehyde
Endrin ketone
Heptachlor
Heptachlor epoxide
Hexachlorobenzene
Methoxychlor
Mirex
Toxaphene
Surrogates
Tetrachloro-m-xylene (S)
Decachlorobiphenyl (S)
8082 GCS PCB
PCB-1016 (Aroclor 1016)
PCB-1221 (Aroclor 1221)
PCB-1232 (Aroclor 1232)
PCB-1242 (Aroclor 1242)
PCB-1248 (Aroclor 1248)
PCB-1254 (Aroclor 1254)
PCB-1260 (Aroclor 1260)
Surrogates
Decachlorobiphenyl (S)
Analytical Method: EPA 8081 B Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
73.4
ug/kg
45.1
10
08/24/22 07:17
08/26/22 19:13
7421-93-4
ND
ug/kg
45.1
10
08/24/22 07:17
08/26/22 19:13
53494-70-5
ND
ug/kg
45.1
10
08/24/22 07:17
08/26/22 19:13
76-44-8
ND
ug/kg
45.1
10
08/24/22 07:17
08/26/22 19:13
1024-57-3
ND
ug/kg
45.1
10
08/24/22 07:17
08/26/22 19:13
118-74-1
ND
ug/kg
113
10
08/24/22 07:17
08/26/22 19:13
72-43-5
ND
ug/kg
113
10
08/24/22 07:17
08/26/22 19:13
2385-85-5
ND
ug/kg
158
10
08/24/22 07:17
08/26/22 19:13
8001-35-2
0
%
10-133
10
08/24/22 07:17
08/26/22 19:13
877-09-8 D3,S4
0
%
10-146
10
08/24/22 07:17
08/26/22 19:13
2051-24-3 S4
Analytical Method: EPA 8082A Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
ND
ug/kg
1320
20
08/19/22 15:53
08/24/22 08:01
12674-11-2
ND
ug/kg
1320
20
08/19/22 15:53
08/24/22 08:01
11104-28-2
ND
ug/kg
1320
20
08/19/22 15:53
08/24/22 08:01
11141-16-5
ND
ug/kg
1320
20
08/19/22 15:53
08/24/22 08:01
53469-21-9
ND
ug/kg
1320
20
08/19/22 15:53
08/24/22 08:01
12672-29-6
1360
ug/kg
1320
20
08/19/22 15:53
08/24/22 08:01
11097-69-1
ND
ug/kg
1320
20
08/19/22 15:53
08/24/22 08:01
11096-82-5
0
%
10-160
20
08/19/22 15:53
08/24/22 08:01
2051-24-3 D3,S4
6010 MET ICP
Analytical Method: EPA 6010 Preparation Method: EPA 3050
Pace Analytical
Services - Ormond Beach
Tin
101
mg/kg
5.3
1
08/30/2219:03
08/31/2218:42
7440-31-5
6020 MET ICPMS
Analytical Method: EPA 6020 Preparation Method:
EPA 3050
Pace Analytical
Services - Ormond Beach
Antimony
176
mg/kg
4.7
20
08/27/22 00:15
08/29/22 19:56
7440-36-0
1g,N2
Arsenic
ND
mg/kg
2.4
20
08/27/22 00:15
08/29/22 19:56
7440-38-2
1g
Barium
810
mg/kg
2.4
20
08/27/22 00:15
08/29/22 19:56
7440-39-3
1g
Beryllium
ND
mg/kg
0.28
20
08/27/22 00:15
08/29/22 19:56
7440-41-7
1g
Cadmium
4.3
mg/kg
0.28
20
08/27/22 00:15
08/29/22 19:56
7440-43-9
1g
Chromium
1090
mg/kg
2.4
20
08/27/22 00:15
08/29/22 19:56
7440-47-3
1g
Cobalt
ND
mg/kg
2.4
20
08/27/22 00:15
08/29/22 19:56
7440-48-4
1g
Copper
185
mg/kg
4.7
20
08/27/22 00:15
08/29/22 19:56
7440-50-8
1g
Lead
269
mg/kg
2.4
20
08/27/22 00:15
08/29/22 19:56
7439-92-1
1g
Nickel
5.8
mg/kg
2.4
20
08/27/22 00:15
08/29/22 19:56
7440-02-0
1g
Selenium
3.9
mg/kg
2.4
20
08/27/22 00:15
08/29/22 19:56
7782-49-2
1g
Silver
106
mg/kg
0.28
20
08/27/22 00:15
08/29/22 19:56
7440-22-4
1g
Thallium
ND
mg/kg
2.4
20
08/27/22 00:15
08/29/22 19:56
7440-28-0
1g
Vanadium
17.9
mg/kg
2.4
20
08/27/22 00:15
08/29/22 19:56
7440-62-2
1g
Zinc
ND
mg/kg
95.0
20
08/27/22 00:15
08/29/22 19:56
7440-66-6
1g
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/25/2022 02:36 PM without the written consent of Pace Analytical Services, LLC. Page 66 of 165

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: WASTE CHARACTERIZATION
Pace Project No.: 92621331
Sample: SURFACE BASIN 3 Lab ID: 92621331010 Collected: 08/16/22 13:30 Received: 08/17/22 16:15 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
7471 Mercury Analytical Method: EPA 7471 Preparation Method: EPA 7471
Pace Analytical Services - Ormond Beach
Mercury 5.7 mg/kg 0.18 10 08/24/22 07:26 08/24/22 12:04 7439-97-6
8270E MSSV Microwave
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical
Services - Charlotte
Acenaphthene
ND
ug/kg
6790
10
08/29/22 10:52
08/30/22 17:39
83-32-9
Acenaphthylene
ND
ug/kg
6790
10
08/29/22 10:52
08/30/22 17:39
208-96-8
Acetophenone
ND
ug/kg
6790
10
08/29/22 10:52
08/30/22 17:39
98-86-2
2-Acetylaminofluorene
ND
ug/kg
13600
10
08/29/22 10:52
08/30/22 17:39
53-96-3
4-Aminobiphenyl
ND
ug/kg
6790
10
08/29/22 10:52
08/30/22 17:39
92-67-1
Anthracene
ND
ug/kg
6790
10
08/29/22 10:52
08/30/22 17:39
120-12-7
Benzo(a)anthracene
ND
ug/kg
6790
10
08/29/22 10:52
08/30/22 17:39
56-55-3
Benzo(a)pyrene
ND
ug/kg
6790
10
08/29/22 10:52
08/30/22 17:39
50-32-8
Benzo(b)fluoranthene
ND
ug/kg
6790
10
08/29/22 10:52
08/30/22 17:39
205-99-2
Benzo(g,h,i)perylene
ND
ug/kg
6790
10
08/29/22 10:52
08/30/22 17:39
191-24-2
Benzo(k)fluoranthene
ND
ug/kg
6790
10
08/29/22 10:52
08/30/22 17:39
207-08-9
Benzyl alcohol
ND
ug/kg
13600
10
08/29/22 10:52
08/30/22 17:39
100-51-6
bis(2-Chloroethoxy)methane
ND
ug/kg
6790
10
08/29/22 10:52
08/30/22 17:39
111-91-1
bis(2-Chloroethyl) ether
ND
ug/kg
6790
10
08/29/22 10:52
08/30/22 17:39
111-44-4
2-Chloronaphthalene
ND
ug/kg
6790
10
08/29/22 10:52
08/30/22 17:39
91-58-7
2-Chlorophenol
ND
ug/kg
6790
10
08/29/22 10:52
08/30/22 17:39
95-57-8
4-Chlorophenylphenyl ether
ND
ug/kg
6790
10
08/29/22 10:52
08/30/22 17:39
7005-72-3
Chrysene
ND
ug/kg
6790
10
08/29/22 10:52
08/30/22 17:39
218-01-9
n-Decane
ND
ug/kg
6790
10
08/29/22 10:52
08/30/22 17:39
124-18-5
Diallate
ND
ug/kg
6790
10
08/29/22 10:52
08/30/22 17:39
2303-16-4
Dibenz(a,h)anthracene
ND
ug/kg
6790
10
08/29/22 10:52
08/30/22 17:39
53-70-3
Dibenzo(a,e)pyrene
ND
ug/kg
20600
10
08/29/22 10:52
08/30/22 17:39
192-65-4
Dibenzofuran
ND
ug/kg
6790
10
08/29/22 10:52
08/30/22 17:39
132-64-9
2,3-Dibromo-1-propanol phosph
ND
ug/kg
34000
10
08/29/22 10:52
08/30/22 17:39
126-72-7
1,2-Dichlorobenzene
ND
ug/kg
6790
10
08/29/22 10:52
08/30/22 17:39
95-50-1
1,3-Dichlorobenzene
ND
ug/kg
6790
10
08/29/22 10:52
08/30/22 17:39
541-73-1
1,4-Dichlorobenzene
ND
ug/kg
6790
10
08/29/22 10:52
08/30/22 17:39
106-46-7
3,3'-Dichlorobenzidine
ND
ug/kg
13600
10
08/29/22 10:52
08/30/22 17:39
91-94-1
2,4-Dichlorophenol
ND
ug/kg
6790
10
08/29/22 10:52
08/30/22 17:39
120-83-2
2,6-Dichlorophenol
ND
ug/kg
6790
10
08/29/22 10:52
08/30/22 17:39
87-65-0
2,3-Dichloroaniline
ND
ug/kg
6790
10
08/29/22 10:52
08/30/22 17:39
608-27-5
Diethylphthalate
ND
ug/kg
6790
10
08/29/22 10:52
08/30/22 17:39
84-66-2
Dimethoate
ND
ug/kg
13600
10
08/29/22 10:52
08/30/22 17:39
60-51-5
P-Dimethylaminoazobenzene
ND
ug/kg
6790
10
08/29/22 10:52
08/30/22 17:39
60-11-7
7,12-Dimethylbenz(a)anthracene
ND
ug/kg
6790
10
08/29/22 10:52
08/30/22 17:39
57-97-6
3,3'-Dimethylbenzidine
ND
ug/kg
13600
10
08/29/22 10:52
08/30/22 17:39
119-93-7
2,4-Dimethylphenol
ND
ug/kg
6790
10
08/29/22 10:52
08/30/22 17:39
105-67-9
a,a-Dimethylphenylethylamine
ND
ug/kg
34000
10
08/29/22 10:52
08/30/22 17:39
122-09-8
Dimethylphthalate
ND
ug/kg
6790
10
08/29/22 10:52
08/30/22 17:39
131-11-3
Di-n-butylphthalate
ND
ug/kg
6790
10
08/29/22 10:52
08/30/22 17:39
84-74-2
4,6-Dinitro-2-methyl phenol
ND
ug/kg
13600
10
08/29/22 10:52
08/30/22 17:39
534-52-1
REPORT OF LABORATORY ANALYSIS
v1
IL
IL
IH
v1
This report shall not be reproduced, except in full,
Date: 10/25/2022 02:36 PM without the written consent of Pace Analytical Services, LLC. Page 67 of 165

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: WASTE CHARACTERIZATION
Pace Project No.: 92621331
Sample: SURFACE BASIN 3 Lab ID: 92621331010 Collected: 08/16/22 13:30 Received: 08/17/22 16:15 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No
8270E MSSV Microwave
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical
Services - Charlotte
1,3-Dinitrobenzene
ND
ug/kg
6790
10
08/29/22 10:52
08/30/22 17:39
99-65-0
1,4-Dinitrobenzene
ND
ug/kg
6790
10
08/29/22 10:52
08/30/22 17:39
100-25-4
2,4-Dinitrophenol
ND
ug/kg
34000
10
08/29/22 10:52
08/30/22 17:39
51-28-5
2,4-Dinitrotoluene
ND
ug/kg
6790
10
08/29/22 10:52
08/30/22 17:39
121-14-2
2,6-Dinitrotoluene
ND
ug/kg
6790
10
08/29/22 10:52
08/30/22 17:39
606-20-2
Di-n-octylphthalate
ND
ug/kg
6790
10
08/29/22 10:52
08/30/22 17:39
117-84-0
Dinoseb
ND
ug/kg
13600
10
08/29/22 10:52
08/30/22 17:39
88-85-7
Diphenylamine
ND
ug/kg
6790
10
08/29/22 10:52
08/30/22 17:39
122-39-4
Diphenyl ether (Phenyl ether)
ND
ug/kg
10300
10
08/29/22 10:52
08/30/22 17:39
101-84-8
1,2-Diphenylhydrazine
ND
ug/kg
6790
10
08/29/22 10:52
08/30/22 17:39
122-66-7
Disulfoton
ND
ug/kg
6790
10
08/29/22 10:52
08/30/22 17:39
298-04-4
bis(2- Ethyl hexyl)phthalate
ND
ug/kg
6790
10
08/29/22 10:52
08/30/22 17:39
117-81-7
Ethyl methanesulfonate
ND
ug/kg
13600
10
08/29/22 10:52
08/30/22 17:39
62-50-0
Famphur
ND
ug/kg
13600
10
08/29/22 10:52
08/30/22 17:39
52-85-7
Fluoranthene
ND
ug/kg
6790
10
08/29/22 10:52
08/30/22 17:39
206-44-0
Fluorene
ND
ug/kg
6790
10
08/29/22 10:52
08/30/22 17:39
86-73-7
Hexachloro-1,3-butadiene
ND
ug/kg
6790
10
08/29/22 10:52
08/30/22 17:39
87-68-3
Hexachlorobenzene
ND
ug/kg
6790
10
08/29/22 10:52
08/30/22 17:39
118-74-1
Hexachlorocyclopentadiene
ND
ug/kg
6790
10
08/29/22 10:52
08/30/22 17:39
77-47-4
Hexachloroethane
ND
ug/kg
6790
10
08/29/22 10:52
08/30/22 17:39
67-72-1
Hexachlorophene
ND
ug/kg
67900
10
08/29/22 10:52
08/30/22 17:39
70-30-4
Hexachloropropene
ND
ug/kg
6790
10
08/29/22 10:52
08/30/22 17:39
1888-71-7
Indeno(1,2,3-cd)pyrene
ND
ug/kg
6790
10
08/29/22 10:52
08/30/22 17:39
193-39-5
Isodrin
ND
ug/kg
6790
10
08/29/22 10:52
08/30/22 17:39
465-73-6
Isophorone
ND
ug/kg
6790
10
08/29/22 10:52
08/30/22 17:39
78-59-1
Isosafrole
ND
ug/kg
6790
10
08/29/22 10:52
08/30/22 17:39
120-58-1
Kepone
ND
ug/kg
13600
10
08/29/22 10:52
08/30/22 17:39
143-50-0
Methapyrilene
ND
ug/kg
34000
10
08/29/22 10:52
08/30/22 17:39
91-80-5
3-Methylcholanthrene
ND
ug/kg
6790
10
08/29/22 10:52
08/30/22 17:39
56-49-5
4,4'-Methylene-bis(2-chloroani
ND
ug/kg
13600
10
08/29/22 10:52
08/30/22 17:39
101-14-4
Methyl methanesulfonate
ND
ug/kg
13600
10
08/29/22 10:52
08/30/22 17:39
66-27-3
1-Methylnaphthalene
ND
ug/kg
6790
10
08/29/22 10:52
08/30/22 17:39
90-12-0
2-Methylnaphthalene
ND
ug/kg
6790
10
08/29/22 10:52
08/30/22 17:39
91-57-6
2-Methyl-5-nitroaniline
ND
ug/kg
6790
10
08/29/22 10:52
08/30/22 17:39
99-55-8
Methyl parathion
ND
ug/kg
6790
10
08/29/22 10:52
08/30/22 17:39
298-00-0
2-Methylphenol(o-Cresol)
ND
ug/kg
6790
10
08/29/22 10:52
08/30/22 17:39
95-48-7
3&4-Methyl phenol (m&p Cresol)
ND
ug/kg
6790
10
08/29/22 10:52
08/30/22 17:39
15831-10-4
1-Naphthalenamine
ND
ug/kg
13600
10
08/29/22 10:52
08/30/22 17:39
134-32-7
2-Naphthalenamine
ND
ug/kg
13600
10
08/29/22 10:52
08/30/22 17:39
91-59-8
Naphthalene
ND
ug/kg
6790
10
08/29/22 10:52
08/30/22 17:39
91-20-3
1,4-Naphthoquinone
ND
ug/kg
34000
10
08/29/22 10:52
08/30/22 17:39
130-15-4
2-Nitroaniline
ND
ug/kg
34000
10
08/29/22 10:52
08/30/22 17:39
88-74-4
3-Nitroaniline
ND
ug/kg
34000
10
08/29/22 10:52
08/30/22 17:39
99-09-2
4-Nitroaniline
ND
ug/kg
13600
10
08/29/22 10:52
08/30/22 17:39
100-01-6
Nitrobenzene
ND
ug/kg
6790
10
08/29/22 10:52
08/30/22 17:39
98-95-3
REPORT OF LABORATORY ANALYSIS
Qual
IH,L2
IH
This report shall not be reproduced, except in full,
Date: 10/25/2022 02:36 PM without the written consent of Pace Analytical Services, LLC. Page 68 of 165

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: WASTE CHARACTERIZATION
Pace Project No.: 92621331
Sample: SURFACE BASIN 3 Lab ID: 92621331010 Collected: 08/16/22 13:30 Received: 08/17/22 16:15 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters
8270E MSSV Microwave
2-Nitrophenol
4-Nitrophenol
4-Nitroquinoline-n-oxide
5-Nitro-o-toluidine
N-Nitrosodiethylamine
N-Nitrosodimethylamine
N-Nitroso-di-n-butylamine
N-Nitroso-di-n-propylamine
N-Nitrosodiphenylamine
N-Nitrosomethylethylamine
N-Nitrosomorpholine
N-Nitrosopiperidine
N-Nitrosopyrrolidine
n-Octadecane
O,O,O-Triethylphosphorothioate
2,2'-Oxybis(1-chloropropane)
Parathion (Ethyl parathion)
Pentachlorobenzene
Pentachloroethane
Pentachloronitrobenzene
Pentachlorophenol
Phenacetin
Phenanthrene
Phenol
p-Phenylenediamine
Phorate
Phthalic anhydride
2-Picoline
Pronamide
Pyrene
Pyridine
Safrole
Sulfotepp (ThiodiphosphoricAc
Terpineol
1,2,4,5-Tetrachlorobenzene
2,3,4,6-Tetrachlorophenol
Thionazin
O-Toluidine
1,2,4-Trichlorobenzene
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
1,3,5-Trinitrobenzene
Surrogates
2-Fluorobiphenyl (S)
Terphenyl-d14 (S)
Results Units Report Limit DF Prepared Analyzed CAS No. Qual
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
ND
ug/kg
6790
10
08/29/2210:52
08/30/2217:39
88-75-5
ND
ug/kg
34000
10
08/29/2210:52
08/30/2217:39
100-02-7
ND
ug/kg
34000
10
08/29/2210:52
08/30/2217:39
56-57-5
v2
ND
ug/kg
6790
10
08/29/2210:52
08/30/2217:39
99-55-8
ND
ug/kg
6790
10
08/29/2210:52
08/30/2217:39
55-18-5
ND
ug/kg
6790
10
08/29/2210:52
08/30/2217:39
62-75-9
ND
ug/kg
6790
10
08/29/2210:52
08/30/2217:39
924-16-3
ND
ug/kg
6790
10
08/29/2210:52
08/30/2217:39
621-64-7
ND
ug/kg
6790
10
08/29/2210:52
08/30/2217:39
86-30-6
ND
ug/kg
6790
10
08/29/2210:52
08/30/2217:39
10595-95-6
ND
ug/kg
6790
10
08/29/2210:52
08/30/2217:39
59-89-2
ND
ug/kg
13600
10
08/29/2210:52
08/30/2217:39
100-75-4
ND
ug/kg
13600
10
08/29/2210:52
08/30/2217:39
930-55-2
ND
ug/kg
6790
10
08/29/2210:52
08/30/2217:39
593-45-3
ND
ug/kg
6790
10
08/29/2210:52
08/30/2217:39
126-68-1
ND
ug/kg
6790
10
08/29/2210:52
08/30/2217:39
108-60-1
ND
ug/kg
6790
10
08/29/2210:52
08/30/2217:39
56-38-2
ND
ug/kg
6790
10
08/29/2210:52
08/30/2217:39
608-93-5
ND
ug/kg
6790
10
08/29/2210:52
08/30/2217:39
76-01-7
ND
ug/kg
6790
10
08/29/2210:52
08/30/2217:39
82-68-8
ND
ug/kg
13600
10
08/29/2210:52
08/30/2217:39
87-86-5
ND
ug/kg
13600
10
08/29/2210:52
08/30/2217:39
62-44-2
ND
ug/kg
6790
10
08/29/2210:52
08/30/2217:39
85-01-8
ND
ug/kg
6790
10
08/29/2210:52
08/30/2217:39
108-95-2
ND
ug/kg
13600
10
08/29/2210:52
08/30/2217:39
106-50-3
IL
ND
ug/kg
6790
10
08/29/2210:52
08/30/2217:39
298-02-2
L2
ND
ug/kg
51400
10
08/29/2210:52
08/30/2217:39
85-44-9
ND
ug/kg
6790
10
08/29/2210:52
08/30/2217:39
109-06-8
ND
ug/kg
13600
10
08/29/2210:52
08/30/2217:39
23950-58-5
ND
ug/kg
6790
10
08/29/2210:52
08/30/2217:39
129-00-0
ND
ug/kg
6790
10
08/29/2210:52
08/30/2217:39
110-86-1
ND
ug/kg
13600
10
08/29/2210:52
08/30/2217:39
94-59-7
ND
ug/kg
6790
10
08/29/2210:52
08/30/2217:39
3689-24-5
ND
ug/kg
6790
10
08/29/2210:52
08/30/2217:39
98-55-5
ND
ug/kg
6790
10
08/29/2210:52
08/30/2217:39
95-94-3
ND
ug/kg
6790
10
08/29/2210:52
08/30/2217:39
58-90-2
ND
ug/kg
6790
10
08/29/2210:52
08/30/2217:39
297-97-2
ND
ug/kg
6790
10
08/29/2210:52
08/30/2217:39
95-53-4
ND
ug/kg
6790
10
08/29/2210:52
08/30/2217:39
120-82-1
ND
ug/kg
6790
10
08/29/2210:52
08/30/2217:39
95-95-4
ND
ug/kg
6790
10
08/29/2210:52
08/30/2217:39
88-06-2
ND
ug/kg
6790
10
08/29/2210:52
08/30/2217:39
99-35-4
0
%
19-130
10
08/29/2210:52
08/30/2217:39
321-60-8
D3,S4
0
%
15-130
10
08/29/2210:52
08/30/2217:39
1718-51-0
S4
REPORT
OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/25/2022 02:36 PM without the written consent of Pace Analytical Services, LLC. Page 69 of 165

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: WASTE CHARACTERIZATION
Pace Project No.: 92621331
Sample: SURFACE BASIN 3
Lab ID: 92621331010 Collected: 08/16/22 13:30 Received: 08/17/22 16:15 Matrix: Solid
Results reported on a "dry weight"
basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters
Results Units Report Limit DF Prepared
Analyzed
CAS No. Qual
8270E MSSV Microwave
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
Surrogates
Phenol-d6 (S)
0 % 18-130 10 08/29/22 10:52
08/30/22 17:39
13127-88-3 S4
2-Fluorophenol (S)
0 % 18-130 10 08/29/22 10:52
08/30/22 17:39
367-12-4 S4
2,4,6-Tribromophenol (S)
0 % 18-130 10 08/29/22 10:52
08/30/22 17:39
118-79-6 S4
Nitrobenzene-d5 (S)
0 % 21-130 10 08/29/22 10:52
08/30/22 17:39
4165-60-0 S4
Percent Moisture
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
50.9 % 0.10 1
08/22/22 15:40
N2
1010 Flash poi nt,Closed Cup
Analytical Method: EPA 1010B
Pace Analytical Services -Asheville
Flashpoint
>200 deg F 70.0 1
08/23/22 12:00
Total Solids 2540 G-2011
Analytical Method: SM 2540G Preparation Method: SM 2540 G
Pace National - Mt. Juliet
Total Solids
49.7 % 1 08/23/22 10:15
08/23/22 10:31
4500S21) Sulfide Soil
Analytical Method: SM 4500-S2D-2011 Modified Preparation Method: SM
4500-S2D-2011 Modified
Pace Analytical Services -Asheville
Sulfide
ND mg/kg 9.8 1 08/20/22 02:37
08/20/22 06:41
18496-25-8 M1
9045 pH Soil
Analytical Method: EPA 9045D
Pace Analytical Services -Asheville
pH at 25 Degrees C
3.7 Std. Units 0.10 1
08/23/22 18:21
H3
9012 Cyanide, Total
Analytical Method: EPA 9012 Preparation Method: EPA 9012
Pace Analytical Services - Ormond Beach
Cyanide
19.3 mg/kg 5.0 10 08/29/22 09:41
08/29/22 15:26
57-12-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/25/2022 02:36 PM without the written consent of Pace Analytical Services, LLC. Page 70 of 165

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: WASTE CHARACTERIZATION
Pace Project No.: 92621331
Sample: GP-1 2-3' Lab ID: 92621331011 Collected: 08/16/22 10:45 Received: 08/17/22 16:15 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No
8260D/5035A/5030B Volatiles
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical
Services - Charlotte
Acetone
ND
ug/kg
522
1
08/18/22 22:11
08/19/22 06:34
67-64-1
Acetonitrile
ND
ug/kg
522
1
08/18/22 22:11
08/19/22 06:34
75-05-8
Acrolein
ND
ug/kg
522
1
08/18/22 22:11
08/19/22 06:34
107-02-8
Acrylonitrile
ND
ug/kg
522
1
08/18/22 22:11
08/19/22 06:34
107-13-1
Allyl chloride
ND
ug/kg
261
1
08/18/22 22:11
08/19/22 06:34
107-05-1
Benzene
ND
ug/kg
26.1
1
08/18/22 22:11
08/19/22 06:34
71-43-2
Bromochloromethane
ND
ug/kg
26.1
1
08/18/22 22:11
08/19/22 06:34
74-97-5
Bromodichloromethane
ND
ug/kg
26.1
1
08/18/22 22:11
08/19/22 06:34
75-27-4
Bromoform
ND
ug/kg
26.1
1
08/18/22 22:11
08/19/22 06:34
75-25-2
Bromomethane
ND
ug/kg
52.2
1
08/18/22 22:11
08/19/22 06:34
74-83-9
2-Butanone (MEK)
ND
ug/kg
522
1
08/18/22 22:11
08/19/22 06:34
78-93-3
Carbon disulfide
ND
ug/kg
52.2
1
08/18/22 22:11
08/19/22 06:34
75-15-0
Carbon tetrachloride
ND
ug/kg
26.1
1
08/18/22 22:11
08/19/22 06:34
56-23-5
Chlorobenzene
ND
ug/kg
26.1
1
08/18/22 22:11
08/19/22 06:34
108-90-7
Chloroethane
ND
ug/kg
52.2
1
08/18/22 22:11
08/19/22 06:34
75-00-3
Chloroform
ND
ug/kg
26.1
1
08/18/22 22:11
08/19/22 06:34
67-66-3
Chloromethane
ND
ug/kg
52.2
1
08/18/22 22:11
08/19/22 06:34
74-87-3
Chloroprene
ND
ug/kg
52.2
1
08/18/22 22:11
08/19/22 06:34
126-99-8
Dibromochloromethane
ND
ug/kg
26.1
1
08/18/22 22:11
08/19/22 06:34
124-48-1
Dibromomethane
ND
ug/kg
26.1
1
08/18/22 22:11
08/19/22 06:34
74-95-3
1,2-Dichlorobenzene
ND
ug/kg
26.1
1
08/18/22 22:11
08/19/22 06:34
95-50-1
1,3-Dichlorobenzene
ND
ug/kg
26.1
1
08/18/22 22:11
08/19/22 06:34
541-73-1
1,4-Dichlorobenzene
ND
ug/kg
26.1
1
08/18/22 22:11
08/19/22 06:34
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/kg
52.2
1
08/18/22 22:11
08/19/22 06:34
110-57-6
Dichlorodifluoromethane
ND
ug/kg
52.2
1
08/18/22 22:11
08/19/22 06:34
75-71-8
1,1-Dichloroethane
ND
ug/kg
26.1
1
08/18/22 22:11
08/19/22 06:34
75-34-3
1,2-Dichloroethane
ND
ug/kg
26.1
1
08/18/22 22:11
08/19/22 06:34
107-06-2
1,1-Dichloroethene
ND
ug/kg
26.1
1
08/18/22 22:11
08/19/22 06:34
75-35-4
cis-1,2-Dichloroethene
ND
ug/kg
26.1
1
08/18/22 22:11
08/19/22 06:34
156-59-2
trans-1,2-Dichloroethene
ND
ug/kg
26.1
1
08/18/22 22:11
08/19/22 06:34
156-60-5
1,2-Dichloropropane
ND
ug/kg
26.1
1
08/18/22 22:11
08/19/22 06:34
78-87-5
1,3-Dichloropropane
ND
ug/kg
26.1
1
08/18/22 22:11
08/19/22 06:34
142-28-9
2,2-Dichloropropane
ND
ug/kg
26.1
1
08/18/22 22:11
08/19/22 06:34
594-20-7
1,1-Dichloropropene
ND
ug/kg
26.1
1
08/18/22 22:11
08/19/22 06:34
563-58-6
cis-1,3-Dichloropropene
ND
ug/kg
26.1
1
08/18/22 22:11
08/19/22 06:34
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/kg
26.1
1
08/18/22 22:11
08/19/22 06:34
10061-02-6
Ethylbenzene
ND
ug/kg
26.1
1
08/18/22 22:11
08/19/22 06:34
100-41-4
Ethyl methacrylate
ND
ug/kg
26.1
1
08/18/22 22:11
08/19/22 06:34
97-63-2
Hexachloro-1,3-butadiene
ND
ug/kg
52.2
1
08/18/22 22:11
08/19/22 06:34
87-68-3
2-Hexanone
ND
ug/kg
261
1
08/18/22 22:11
08/19/22 06:34
591-78-6
lodomethane
ND
ug/kg
261
1
08/18/22 22:11
08/19/22 06:34
74-88-4
Isobutanol
ND
ug/kg
522
1
08/18/22 22:11
08/19/22 06:34
78-83-1
Methacrylonitrile
ND
ug/kg
261
1
08/18/22 22:11
08/19/22 06:34
126-98-7
Methylene Chloride
ND
ug/kg
104
1
08/18/22 22:11
08/19/22 06:34
75-09-2
Methyl methacrylate
ND
ug/kg
26.1
1
08/18/22 22:11
08/19/22 06:34
80-62-6
REPORT OF LABORATORY ANALYSIS
Qual
IH,v1
This report shall not be reproduced, except in full,
Date: 10/25/2022 02:36 PM without the written consent of Pace Analytical Services, LLC. Page 71 of 165

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: WASTE CHARACTERIZATION
Pace Project No.: 92621331
Sample: GP-1 2-3'
Lab ID: 92621331011 Collected:
08/16/22
10:45
Received: 08/17/22 16:15 Matrix: Solid
Results reported on a "dry weight"
basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters
Results
Units Report
Limit
DF
Prepared
Analyzed
CAS No. Qual
8260D/5035A/5030B Volatiles
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical
Services - Charlotte
4-Methyl-2-pentanone (MIBK)
ND
ug/kg
261
1
08/18/22 22:11
08/19/22 06:34
108-10-1
Naphthalene
ND
ug/kg
26.1
1
08/18/22 22:11
08/19/22 06:34
91-20-3
Propionitrile
ND
ug/kg
261
1
08/18/22 22:11
08/19/22 06:34
107-12-0
Styrene
ND
ug/kg
26.1
1
08/18/22 22:11
08/19/22 06:34
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/kg
26.1
1
08/18/22 22:11
08/19/22 06:34
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/kg
26.1
1
08/18/22 22:11
08/19/22 06:34
79-34-5
Tetrachloroethene
ND
ug/kg
26.1
1
08/18/22 22:11
08/19/22 06:34
127-18-4
Toluene
108
ug/kg
26.1
1
08/18/22 22:11
08/19/22 06:34
108-88-3
1,2,4-Trichlorobenzene
ND
ug/kg
26.1
1
08/18/22 22:11
08/19/22 06:34
120-82-1
1,1,1-Trichloroethane
ND
ug/kg
26.1
1
08/18/22 22:11
08/19/22 06:34
71-55-6
1,1,2-Trichloroethane
ND
ug/kg
26.1
1
08/18/22 22:11
08/19/22 06:34
79-00-5
Trichloroethene
ND
ug/kg
26.1
1
08/18/22 22:11
08/19/22 06:34
79-01-6
Trichlorofluoromethane
ND
ug/kg
26.1
1
08/18/22 22:11
08/19/22 06:34
75-69-4
1,2,3-Trichloropropane
ND
ug/kg
26.1
1
08/18/22 22:11
08/19/22 06:34
96-18-4
Vinyl acetate
ND
ug/kg
261
1
08/18/22 22:11
08/19/22 06:34
108-05-4
Vinyl chloride
ND
ug/kg
52.2
1
08/18/22 22:11
08/19/22 06:34
75-01-4
Xylene (Total)
ND
ug/kg
52.2
1
08/18/22 22:11
08/19/22 06:34
1330-20-7
m&p-Xylene
ND
ug/kg
52.2
1
08/18/22 22:11
08/19/22 06:34
179601-23-1
o-Xylene
ND
ug/kg
26.1
1
08/18/22 22:11
08/19/22 06:34
95-47-6
Surrogates
Toluene-d8 (S)
100
%
70-130
1
08/18/22 22:11
08/19/22 06:34
2037-26-5
4-Bromofluorobenzene (S)
100
%
70-130
1
08/18/22 22:11
08/19/22 06:34
460-00-4
1,2-Dichloroethane-d4 (S)
96
%
70-130
1
08/18/22 22:11
08/19/22 06:34
17060-07-0
Percent Moisture
Analytical Method: SW-846
Pace Analytical
Services - Charlotte
Percent Moisture
47.0
%
0.10
1
08/22/22 15:40
N2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/25/2022 02:36 PM without the written consent of Pace Analytical Services, LLC. Page 72 of 165

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: WASTE CHARACTERIZATION
Pace Project No.: 92621331
Sample: GP-6 2-3' Lab ID: 92621331012 Collected: 08/16/22 12:30 Received: 08/17/22 16:15 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No
8260D/5035A/5030B Volatiles
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical
Services - Charlotte
Acetone
ND
ug/kg
557
1
08/18/22 22:11
08/19/22 06:52
67-64-1
Acetonitrile
ND
ug/kg
557
1
08/18/22 22:11
08/19/22 06:52
75-05-8
Acrolein
ND
ug/kg
557
1
08/18/22 22:11
08/19/22 06:52
107-02-8
Acrylonitrile
ND
ug/kg
557
1
08/18/22 22:11
08/19/22 06:52
107-13-1
Allyl chloride
ND
ug/kg
279
1
08/18/22 22:11
08/19/22 06:52
107-05-1
Benzene
ND
ug/kg
27.9
1
08/18/22 22:11
08/19/22 06:52
71-43-2
Bromochloromethane
ND
ug/kg
27.9
1
08/18/22 22:11
08/19/22 06:52
74-97-5
Bromodichloromethane
ND
ug/kg
27.9
1
08/18/22 22:11
08/19/22 06:52
75-27-4
Bromoform
ND
ug/kg
27.9
1
08/18/22 22:11
08/19/22 06:52
75-25-2
Bromomethane
ND
ug/kg
55.7
1
08/18/22 22:11
08/19/22 06:52
74-83-9
2-Butanone (MEK)
ND
ug/kg
557
1
08/18/22 22:11
08/19/22 06:52
78-93-3
Carbon disulfide
ND
ug/kg
55.7
1
08/18/22 22:11
08/19/22 06:52
75-15-0
Carbon tetrachloride
ND
ug/kg
27.9
1
08/18/22 22:11
08/19/22 06:52
56-23-5
Chlorobenzene
ND
ug/kg
27.9
1
08/18/22 22:11
08/19/22 06:52
108-90-7
Chloroethane
ND
ug/kg
55.7
1
08/18/22 22:11
08/19/22 06:52
75-00-3
Chloroform
ND
ug/kg
27.9
1
08/18/22 22:11
08/19/22 06:52
67-66-3
Chloromethane
ND
ug/kg
55.7
1
08/18/22 22:11
08/19/22 06:52
74-87-3
Chloroprene
ND
ug/kg
55.7
1
08/18/22 22:11
08/19/22 06:52
126-99-8
Dibromochloromethane
ND
ug/kg
27.9
1
08/18/22 22:11
08/19/22 06:52
124-48-1
Dibromomethane
ND
ug/kg
27.9
1
08/18/22 22:11
08/19/22 06:52
74-95-3
1,2-Dichlorobenzene
ND
ug/kg
27.9
1
08/18/22 22:11
08/19/22 06:52
95-50-1
1,3-Dichlorobenzene
ND
ug/kg
27.9
1
08/18/22 22:11
08/19/22 06:52
541-73-1
1,4-Dichlorobenzene
ND
ug/kg
27.9
1
08/18/22 22:11
08/19/22 06:52
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/kg
55.7
1
08/18/22 22:11
08/19/22 06:52
110-57-6
Dichlorodifluoromethane
ND
ug/kg
55.7
1
08/18/22 22:11
08/19/22 06:52
75-71-8
1,1-Dichloroethane
ND
ug/kg
27.9
1
08/18/22 22:11
08/19/22 06:52
75-34-3
1,2-Dichloroethane
ND
ug/kg
27.9
1
08/18/22 22:11
08/19/22 06:52
107-06-2
1,1-Dichloroethene
ND
ug/kg
27.9
1
08/18/22 22:11
08/19/22 06:52
75-35-4
cis-1,2-Dichloroethene
ND
ug/kg
27.9
1
08/18/22 22:11
08/19/22 06:52
156-59-2
trans-1,2-Dichloroethene
ND
ug/kg
27.9
1
08/18/22 22:11
08/19/22 06:52
156-60-5
1,2-Dichloropropane
ND
ug/kg
27.9
1
08/18/22 22:11
08/19/22 06:52
78-87-5
1,3-Dichloropropane
ND
ug/kg
27.9
1
08/18/22 22:11
08/19/22 06:52
142-28-9
2,2-Dichloropropane
ND
ug/kg
27.9
1
08/18/22 22:11
08/19/22 06:52
594-20-7
1,1-Dichloropropene
ND
ug/kg
27.9
1
08/18/22 22:11
08/19/22 06:52
563-58-6
cis-1,3-Dichloropropene
ND
ug/kg
27.9
1
08/18/22 22:11
08/19/22 06:52
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/kg
27.9
1
08/18/22 22:11
08/19/22 06:52
10061-02-6
Ethylbenzene
ND
ug/kg
27.9
1
08/18/22 22:11
08/19/22 06:52
100-41-4
Ethyl methacrylate
ND
ug/kg
27.9
1
08/18/22 22:11
08/19/22 06:52
97-63-2
Hexachloro-1,3-butadiene
ND
ug/kg
55.7
1
08/18/22 22:11
08/19/22 06:52
87-68-3
2-Hexanone
ND
ug/kg
279
1
08/18/22 22:11
08/19/22 06:52
591-78-6
lodomethane
ND
ug/kg
279
1
08/18/22 22:11
08/19/22 06:52
74-88-4
Isobutanol
ND
ug/kg
557
1
08/18/22 22:11
08/19/22 06:52
78-83-1
Methacrylonitrile
ND
ug/kg
279
1
08/18/22 22:11
08/19/22 06:52
126-98-7
Methylene Chloride
ND
ug/kg
ill
1
08/18/22 22:11
08/19/22 06:52
75-09-2
Methyl methacrylate
ND
ug/kg
27.9
1
08/18/22 22:11
08/19/22 06:52
80-62-6
REPORT OF LABORATORY ANALYSIS
Qual
IH,v1
This report shall not be reproduced, except in full,
Date: 10/25/2022 02:36 PM without the written consent of Pace Analytical Services, LLC. Page 73 of 165

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: WASTE CHARACTERIZATION
Pace Project No.: 92621331
Sample: GP-6 2-3'
Lab ID: 92621331012 Collected:
08/16/22
12:30
Received: 08/17/22 16:15 Matrix: Solid
Results reported on a "dry weight"
basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters
Results
Units Report
Limit
DF
Prepared
Analyzed
CAS No. Qual
8260D/5035A/5030B Volatiles
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical
Services - Charlotte
4-Methyl-2-pentanone (MIBK)
ND
ug/kg
279
1
08/18/22 22:11
08/19/22 06:52
108-10-1
Naphthalene
ND
ug/kg
27.9
1
08/18/22 22:11
08/19/22 06:52
91-20-3
Propionitrile
ND
ug/kg
279
1
08/18/22 22:11
08/19/22 06:52
107-12-0
Styrene
ND
ug/kg
27.9
1
08/18/22 22:11
08/19/22 06:52
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/kg
27.9
1
08/18/22 22:11
08/19/22 06:52
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/kg
27.9
1
08/18/22 22:11
08/19/22 06:52
79-34-5
Tetrachloroethene
ND
ug/kg
27.9
1
08/18/22 22:11
08/19/22 06:52
127-18-4
Toluene
34.6
ug/kg
27.9
1
08/18/22 22:11
08/19/22 06:52
108-88-3
1,2,4-Trichlorobenzene
ND
ug/kg
27.9
1
08/18/22 22:11
08/19/22 06:52
120-82-1
1,1,1-Trichloroethane
ND
ug/kg
27.9
1
08/18/22 22:11
08/19/22 06:52
71-55-6
1,1,2-Trichloroethane
ND
ug/kg
27.9
1
08/18/22 22:11
08/19/22 06:52
79-00-5
Trichloroethene
ND
ug/kg
27.9
1
08/18/22 22:11
08/19/22 06:52
79-01-6
Trichlorofluoromethane
ND
ug/kg
27.9
1
08/18/22 22:11
08/19/22 06:52
75-69-4
1,2,3-Trichloropropane
ND
ug/kg
27.9
1
08/18/22 22:11
08/19/22 06:52
96-18-4
Vinyl acetate
ND
ug/kg
279
1
08/18/22 22:11
08/19/22 06:52
108-05-4
Vinyl chloride
ND
ug/kg
55.7
1
08/18/22 22:11
08/19/22 06:52
75-01-4
Xylene (Total)
ND
ug/kg
55.7
1
08/18/22 22:11
08/19/22 06:52
1330-20-7
m&p-Xylene
ND
ug/kg
55.7
1
08/18/22 22:11
08/19/22 06:52
179601-23-1
o-Xylene
ND
ug/kg
27.9
1
08/18/22 22:11
08/19/22 06:52
95-47-6
Surrogates
Toluene-d8 (S)
100
%
70-130
1
08/18/22 22:11
08/19/22 06:52
2037-26-5
4-Bromofluorobenzene (S)
104
%
70-130
1
08/18/22 22:11
08/19/22 06:52
460-00-4
1,2-Dichloroethane-d4 (S)
96
%
70-130
1
08/18/22 22:11
08/19/22 06:52
17060-07-0
Percent Moisture
Analytical Method: SW-846
Pace Analytical
Services - Charlotte
Percent Moisture
58.8
%
0.10
1
08/22/22 15:40
N2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/25/2022 02:36 PM without the written consent of Pace Analytical Services, LLC. Page 74 of 165

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: WASTE CHARACTERIZATION
Pace Project No.: 92621331
Sample: HA-1 2-3' Lab ID: 92621331013 Collected: 08/16/22 13:00 Received: 08/17/22 16:15 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No
8260D/5035A/5030B Volatiles
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical
Services - Charlotte
Acetone
ND
ug/kg
421
1
08/18/22 22:11
08/19/22 07:10
67-64-1
Acetonitrile
ND
ug/kg
421
1
08/18/22 22:11
08/19/22 07:10
75-05-8
Acrolein
ND
ug/kg
421
1
08/18/22 22:11
08/19/22 07:10
107-02-8
Acrylonitrile
ND
ug/kg
421
1
08/18/22 22:11
08/19/22 07:10
107-13-1
Allyl chloride
ND
ug/kg
210
1
08/18/22 22:11
08/19/22 07:10
107-05-1
Benzene
ND
ug/kg
21.0
1
08/18/22 22:11
08/19/22 07:10
71-43-2
Bromochloromethane
ND
ug/kg
21.0
1
08/18/22 22:11
08/19/22 07:10
74-97-5
Bromodichloromethane
ND
ug/kg
21.0
1
08/18/22 22:11
08/19/22 07:10
75-27-4
Bromoform
ND
ug/kg
21.0
1
08/18/22 22:11
08/19/22 07:10
75-25-2
Bromomethane
ND
ug/kg
42.1
1
08/18/22 22:11
08/19/22 07:10
74-83-9
2-Butanone (MEK)
ND
ug/kg
421
1
08/18/22 22:11
08/19/22 07:10
78-93-3
Carbon disulfide
ND
ug/kg
42.1
1
08/18/22 22:11
08/19/22 07:10
75-15-0
Carbon tetrachloride
ND
ug/kg
21.0
1
08/18/22 22:11
08/19/22 07:10
56-23-5
Chlorobenzene
ND
ug/kg
21.0
1
08/18/22 22:11
08/19/22 07:10
108-90-7
Chloroethane
ND
ug/kg
42.1
1
08/18/22 22:11
08/19/22 07:10
75-00-3
Chloroform
ND
ug/kg
21.0
1
08/18/22 22:11
08/19/22 07:10
67-66-3
Chloromethane
ND
ug/kg
42.1
1
08/18/22 22:11
08/19/22 07:10
74-87-3
Chloroprene
ND
ug/kg
42.1
1
08/18/22 22:11
08/19/22 07:10
126-99-8
Dibromochloromethane
ND
ug/kg
21.0
1
08/18/22 22:11
08/19/22 07:10
124-48-1
Dibromomethane
ND
ug/kg
21.0
1
08/18/22 22:11
08/19/22 07:10
74-95-3
1,2-Dichlorobenzene
ND
ug/kg
21.0
1
08/18/22 22:11
08/19/22 07:10
95-50-1
1,3-Dichlorobenzene
ND
ug/kg
21.0
1
08/18/22 22:11
08/19/22 07:10
541-73-1
1,4-Dichlorobenzene
ND
ug/kg
21.0
1
08/18/22 22:11
08/19/22 07:10
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/kg
42.1
1
08/18/22 22:11
08/19/22 07:10
110-57-6
Dichlorodifluoromethane
ND
ug/kg
42.1
1
08/18/22 22:11
08/19/22 07:10
75-71-8
1,1-Dichloroethane
ND
ug/kg
21.0
1
08/18/22 22:11
08/19/22 07:10
75-34-3
1,2-Dichloroethane
ND
ug/kg
21.0
1
08/18/22 22:11
08/19/22 07:10
107-06-2
1,1-Dichloroethene
ND
ug/kg
21.0
1
08/18/22 22:11
08/19/22 07:10
75-35-4
cis-1,2-Dichloroethene
ND
ug/kg
21.0
1
08/18/22 22:11
08/19/22 07:10
156-59-2
trans-1,2-Dichloroethene
ND
ug/kg
21.0
1
08/18/22 22:11
08/19/22 07:10
156-60-5
1,2-Dichloropropane
ND
ug/kg
21.0
1
08/18/22 22:11
08/19/22 07:10
78-87-5
1,3-Dichloropropane
ND
ug/kg
21.0
1
08/18/22 22:11
08/19/22 07:10
142-28-9
2,2-Dichloropropane
ND
ug/kg
21.0
1
08/18/22 22:11
08/19/22 07:10
594-20-7
1,1-Dichloropropene
ND
ug/kg
21.0
1
08/18/22 22:11
08/19/22 07:10
563-58-6
cis-1,3-Dichloropropene
ND
ug/kg
21.0
1
08/18/22 22:11
08/19/22 07:10
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/kg
21.0
1
08/18/22 22:11
08/19/22 07:10
10061-02-6
Ethylbenzene
ND
ug/kg
21.0
1
08/18/22 22:11
08/19/22 07:10
100-41-4
Ethyl methacrylate
ND
ug/kg
21.0
1
08/18/22 22:11
08/19/22 07:10
97-63-2
Hexachloro-1,3-butadiene
ND
ug/kg
42.1
1
08/18/22 22:11
08/19/22 07:10
87-68-3
2-Hexanone
ND
ug/kg
210
1
08/18/22 22:11
08/19/22 07:10
591-78-6
lodomethane
ND
ug/kg
210
1
08/18/22 22:11
08/19/22 07:10
74-88-4
Isobutanol
ND
ug/kg
421
1
08/18/22 22:11
08/19/22 07:10
78-83-1
Methacrylonitrile
ND
ug/kg
210
1
08/18/22 22:11
08/19/22 07:10
126-98-7
Methylene Chloride
ND
ug/kg
84.1
1
08/18/22 22:11
08/19/22 07:10
75-09-2
Methyl methacrylate
ND
ug/kg
21.0
1
08/18/22 22:11
08/19/22 07:10
80-62-6
REPORT OF LABORATORY ANALYSIS
Qual
IH,v1
This report shall not be reproduced, except in full,
Date: 10/25/2022 02:36 PM without the written consent of Pace Analytical Services, LLC. Page 75 of 165

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: WASTE CHARACTERIZATION
Pace Project No.: 92621331
Sample: HA-1 2-3'
Lab ID: 92621331013 Collected:
08/16/22
13:00
Received: 08/17/22 16:15 Matrix: Solid
Results reported on a "dry weight"
basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters
Results
Units Report
Limit
DF
Prepared
Analyzed
CAS No. Qual
8260D/5035A/5030B Volatiles
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical
Services - Charlotte
4-Methyl-2-pentanone (MIBK)
ND
ug/kg
210
1
08/18/22 22:11
08/19/22 07:10
108-10-1
Naphthalene
ND
ug/kg
21.0
1
08/18/22 22:11
08/19/22 07:10
91-20-3
Propionitrile
ND
ug/kg
210
1
08/18/22 22:11
08/19/22 07:10
107-12-0
Styrene
ND
ug/kg
21.0
1
08/18/22 22:11
08/19/22 07:10
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/kg
21.0
1
08/18/22 22:11
08/19/22 07:10
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/kg
21.0
1
08/18/22 22:11
08/19/22 07:10
79-34-5
Tetrachloroethene
ND
ug/kg
21.0
1
08/18/22 22:11
08/19/22 07:10
127-18-4
Toluene
ND
ug/kg
21.0
1
08/18/22 22:11
08/19/22 07:10
108-88-3
1,2,4-Trichlorobenzene
ND
ug/kg
21.0
1
08/18/22 22:11
08/19/22 07:10
120-82-1
1,1,1-Trichloroethane
ND
ug/kg
21.0
1
08/18/22 22:11
08/19/22 07:10
71-55-6
1,1,2-Trichloroethane
ND
ug/kg
21.0
1
08/18/22 22:11
08/19/22 07:10
79-00-5
Trichloroethene
ND
ug/kg
21.0
1
08/18/22 22:11
08/19/22 07:10
79-01-6
Trichlorofluoromethane
ND
ug/kg
21.0
1
08/18/22 22:11
08/19/22 07:10
75-69-4
1,2,3-Trichloropropane
ND
ug/kg
21.0
1
08/18/22 22:11
08/19/22 07:10
96-18-4
Vinyl acetate
ND
ug/kg
210
1
08/18/22 22:11
08/19/22 07:10
108-05-4
Vinyl chloride
ND
ug/kg
42.1
1
08/18/22 22:11
08/19/22 07:10
75-01-4
Xylene (Total)
ND
ug/kg
42.1
1
08/18/22 22:11
08/19/22 07:10
1330-20-7
m&p-Xylene
ND
ug/kg
42.1
1
08/18/22 22:11
08/19/22 07:10
179601-23-1
o-Xylene
ND
ug/kg
21.0
1
08/18/22 22:11
08/19/22 07:10
95-47-6
Surrogates
Toluene-d8 (S)
99
%
70-130
1
08/18/22 22:11
08/19/22 07:10
2037-26-5
4-Bromofluorobenzene (S)
101
%
70-130
1
08/18/22 22:11
08/19/22 07:10
460-00-4
1,2-Dichloroethane-d4 (S)
96
%
70-130
1
08/18/22 22:11
08/19/22 07:10
17060-07-0
Percent Moisture
Analytical Method: SW-846
Pace Analytical
Services - Charlotte
Percent Moisture
51.0
%
0.10
1
08/22/22 15:40
N2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/25/2022 02:36 PM without the written consent of Pace Analytical Services, LLC. Page 76 of 165

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: WASTE CHARACTERIZATION
Pace Project No.: 92621331
Sample: HA-2 2-3' Lab ID: 92621331014 Collected: 08/16/22 13:15 Received: 08/17/22 16:15 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No
8260D/5035A/5030B Volatiles
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical
Services - Charlotte
Acetone
ND
ug/kg
470
1
08/18/22 22:11
08/19/22 07:28
67-64-1
Acetonitrile
ND
ug/kg
470
1
08/18/22 22:11
08/19/22 07:28
75-05-8
Acrolein
ND
ug/kg
470
1
08/18/22 22:11
08/19/22 07:28
107-02-8
Acrylonitrile
ND
ug/kg
470
1
08/18/22 22:11
08/19/22 07:28
107-13-1
Allyl chloride
ND
ug/kg
235
1
08/18/22 22:11
08/19/22 07:28
107-05-1
Benzene
ND
ug/kg
23.5
1
08/18/22 22:11
08/19/22 07:28
71-43-2
Bromochloromethane
ND
ug/kg
23.5
1
08/18/22 22:11
08/19/22 07:28
74-97-5
Bromodichloromethane
ND
ug/kg
23.5
1
08/18/22 22:11
08/19/22 07:28
75-27-4
Bromoform
ND
ug/kg
23.5
1
08/18/22 22:11
08/19/22 07:28
75-25-2
Bromomethane
ND
ug/kg
47.0
1
08/18/22 22:11
08/19/22 07:28
74-83-9
2-Butanone (MEK)
ND
ug/kg
470
1
08/18/22 22:11
08/19/22 07:28
78-93-3
Carbon disulfide
ND
ug/kg
47.0
1
08/18/22 22:11
08/19/22 07:28
75-15-0
Carbon tetrachloride
41.0
ug/kg
23.5
1
08/18/22 22:11
08/19/22 07:28
56-23-5
Chlorobenzene
ND
ug/kg
23.5
1
08/18/22 22:11
08/19/22 07:28
108-90-7
Chloroethane
ND
ug/kg
47.0
1
08/18/22 22:11
08/19/22 07:28
75-00-3
Chloroform
ND
ug/kg
23.5
1
08/18/22 22:11
08/19/22 07:28
67-66-3
Chloromethane
ND
ug/kg
47.0
1
08/18/22 22:11
08/19/22 07:28
74-87-3
Chloroprene
ND
ug/kg
47.0
1
08/18/22 22:11
08/19/22 07:28
126-99-8
Dibromochloromethane
ND
ug/kg
23.5
1
08/18/22 22:11
08/19/22 07:28
124-48-1
Dibromomethane
ND
ug/kg
23.5
1
08/18/22 22:11
08/19/22 07:28
74-95-3
1,2-Dichlorobenzene
ND
ug/kg
23.5
1
08/18/22 22:11
08/19/22 07:28
95-50-1
1,3-Dichlorobenzene
ND
ug/kg
23.5
1
08/18/22 22:11
08/19/22 07:28
541-73-1
1,4-Dichlorobenzene
ND
ug/kg
23.5
1
08/18/22 22:11
08/19/22 07:28
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/kg
47.0
1
08/18/22 22:11
08/19/22 07:28
110-57-6
Dichlorodifluoromethane
ND
ug/kg
47.0
1
08/18/22 22:11
08/19/22 07:28
75-71-8
1,1-Dichloroethane
ND
ug/kg
23.5
1
08/18/22 22:11
08/19/22 07:28
75-34-3
1,2-Dichloroethane
ND
ug/kg
23.5
1
08/18/22 22:11
08/19/22 07:28
107-06-2
1,1-Dichloroethene
ND
ug/kg
23.5
1
08/18/22 22:11
08/19/22 07:28
75-35-4
cis-1,2-Dichloroethene
ND
ug/kg
23.5
1
08/18/22 22:11
08/19/22 07:28
156-59-2
trans-1,2-Dichloroethene
ND
ug/kg
23.5
1
08/18/22 22:11
08/19/22 07:28
156-60-5
1,2-Dichloropropane
ND
ug/kg
23.5
1
08/18/22 22:11
08/19/22 07:28
78-87-5
1,3-Dichloropropane
ND
ug/kg
23.5
1
08/18/22 22:11
08/19/22 07:28
142-28-9
2,2-Dichloropropane
ND
ug/kg
23.5
1
08/18/22 22:11
08/19/22 07:28
594-20-7
1,1-Dichloropropene
ND
ug/kg
23.5
1
08/18/22 22:11
08/19/22 07:28
563-58-6
cis-1,3-Dichloropropene
ND
ug/kg
23.5
1
08/18/22 22:11
08/19/22 07:28
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/kg
23.5
1
08/18/22 22:11
08/19/22 07:28
10061-02-6
Ethylbenzene
ND
ug/kg
23.5
1
08/18/22 22:11
08/19/22 07:28
100-41-4
Ethyl methacrylate
ND
ug/kg
23.5
1
08/18/22 22:11
08/19/22 07:28
97-63-2
Hexachloro-1,3-butadiene
ND
ug/kg
47.0
1
08/18/22 22:11
08/19/22 07:28
87-68-3
2-Hexanone
ND
ug/kg
235
1
08/18/22 22:11
08/19/22 07:28
591-78-6
lodomethane
ND
ug/kg
235
1
08/18/22 22:11
08/19/22 07:28
74-88-4
Isobutanol
ND
ug/kg
470
1
08/18/22 22:11
08/19/22 07:28
78-83-1
Methacrylonitrile
ND
ug/kg
235
1
08/18/22 22:11
08/19/22 07:28
126-98-7
Methylene Chloride
ND
ug/kg
94.0
1
08/18/22 22:11
08/19/22 07:28
75-09-2
Methyl methacrylate
ND
ug/kg
23.5
1
08/18/22 22:11
08/19/22 07:28
80-62-6
REPORT OF LABORATORY ANALYSIS
Qual
IH,v1
This report shall not be reproduced, except in full,
Date: 10/25/2022 02:36 PM without the written consent of Pace Analytical Services, LLC. Page 77 of 165

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: WASTE CHARACTERIZATION
Pace Project No.: 92621331
Sample: HA-2 2-3'
Lab ID: 92621331014 Collected:
08/16/22
13:15
Received: 08/17/22 16:15 Matrix: Solid
Results reported on a "dry weight"
basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters
Results
Units Report
Limit
DF
Prepared
Analyzed
CAS No. Qual
8260D/5035A/5030B Volatiles
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical
Services - Charlotte
4-Methyl-2-pentanone (MIBK)
ND
ug/kg
235
1
08/18/22 22:11
08/19/22 07:28
108-10-1
Naphthalene
ND
ug/kg
23.5
1
08/18/22 22:11
08/19/22 07:28
91-20-3
Propionitrile
ND
ug/kg
235
1
08/18/22 22:11
08/19/22 07:28
107-12-0
Styrene
33.5
ug/kg
23.5
1
08/18/22 22:11
08/19/22 07:28
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/kg
23.5
1
08/18/22 22:11
08/19/22 07:28
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/kg
23.5
1
08/18/22 22:11
08/19/22 07:28
79-34-5
Tetrachloroethene
ND
ug/kg
23.5
1
08/18/22 22:11
08/19/22 07:28
127-18-4
Toluene
24.9
ug/kg
23.5
1
08/18/22 22:11
08/19/22 07:28
108-88-3
1,2,4-Trichlorobenzene
ND
ug/kg
23.5
1
08/18/22 22:11
08/19/22 07:28
120-82-1
1,1,1-Trichloroethane
ND
ug/kg
23.5
1
08/18/22 22:11
08/19/22 07:28
71-55-6
1,1,2-Trichloroethane
ND
ug/kg
23.5
1
08/18/22 22:11
08/19/22 07:28
79-00-5
Trichloroethene
ND
ug/kg
23.5
1
08/18/22 22:11
08/19/22 07:28
79-01-6
Trichlorofluoromethane
ND
ug/kg
23.5
1
08/18/22 22:11
08/19/22 07:28
75-69-4
1,2,3-Trichloropropane
ND
ug/kg
23.5
1
08/18/22 22:11
08/19/22 07:28
96-18-4
Vinyl acetate
ND
ug/kg
235
1
08/18/22 22:11
08/19/22 07:28
108-05-4
Vinyl chloride
ND
ug/kg
47.0
1
08/18/22 22:11
08/19/22 07:28
75-01-4
Xylene (Total)
ND
ug/kg
47.0
1
08/18/22 22:11
08/19/22 07:28
1330-20-7
m&p-Xylene
ND
ug/kg
47.0
1
08/18/22 22:11
08/19/22 07:28
179601-23-1
o-Xylene
ND
ug/kg
23.5
1
08/18/22 22:11
08/19/22 07:28
95-47-6
Surrogates
Toluene-d8 (S)
99
%
70-130
1
08/18/22 22:11
08/19/22 07:28
2037-26-5
4-Bromofluorobenzene (S)
94
%
70-130
1
08/18/22 22:11
08/19/22 07:28
460-00-4
1,2-Dichloroethane-d4 (S)
96
%
70-130
1
08/18/22 22:11
08/19/22 07:28
17060-07-0
Percent Moisture
Analytical Method: SW-846
Pace Analytical
Services - Charlotte
Percent Moisture
49.4
%
0.10
1
08/22/22 15:40
N2
REPORT OF LABORATORY ANALYSIS
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Date: 10/25/2022 02:36 PM without the written consent of Pace Analytical Services, LLC. Page 78 of 165

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: WASTE CHARACTERIZATION
Pace Project No.: 92621331
Sample: Basin 1 Lab ID: 92621331015 Collected: 08/16/22 13:00 Received: 09/13/22 09:44 Matrix: Solid
Results reported on a "wet -weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010D MET ICP, TCLP
Arsenic
Barium
Cadmium
Chromium
Lead
Selenium
Silver
7470A Mercury, TCLP
Mercury
7196 Chromium, Hexavalent
Chromium, Hexavalent
Date: 10/25/2022 02:36 PM
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Leachate Method/Date: EPA 1311; 10/05/22 14:17
Pace Analytical Services - Minneapolis
ND mg/L
0.50
1
10/13/2214:19
10/14/2210:36
7440-38-2
ND mg/L
1.0
1
10/13/2214:19
10/14/2210:36
7440-39-3
ND mg/L
0.050
1
10/13/2214:19
10/14/2210:36
7440-43-9
ND mg/L
0.50
1
10/13/2214:19
10/14/2210:36
7440-47-3
ND mg/L
0.50
1
10/13/2214:19
10/14/2210:36
7439-92-1
ND mg/L
0.10
1
10/13/2214:19
10/14/2210:36
7782-49-2
ND mg/L
0.10
1
10/13/2214:19
10/14/2210:36
7440-22-4
Analytical Method: EPA 7470A Preparation Method:
EPA 7470A
Leachate Method/Date: EPA 1311; 10/05/22
14:17
Pace Analytical Services - Minneapolis
ND ug/L
0.60
1
10/06/2211:30
10/06/2216:17
7439-97-6 H3
Analytical Method: EPA 7196A Preparation Method:
EPA 7196A Modified
Pace Analytical Services -Asheville
ND mg/kg
4.9
1
09/22/22 09:30
09/22/22 11:58
18540-29-9 H2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 79 of 165

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: WASTE CHARACTERIZATION
Pace Project No.: 92621331
Sample: Basin 2 Lab ID: 92621331016 Collected: 08/16/22 13:15 Received: 09/13/22 09:44 Matrix: Solid
Results reported on a "wet -weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010D MET ICP, TCLP
Arsenic
Barium
Cadmium
Chromium
Lead
Selenium
Silver
7470A Mercury, TCLP
Mercury
7196 Chromium, Hexavalent
Chromium, Hexavalent
Date: 10/25/2022 02:36 PM
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Leachate Method/Date: EPA 1311; 10/05/22 14:17
Pace Analytical Services - Minneapolis
ND mg/L
0.50
1
10/13/2214:19
10/14/2210:37
7440-38-2
ND mg/L
1.0
1
10/13/2214:19
10/14/2210:37
7440-39-3
ND mg/L
0.050
1
10/13/2214:19
10/14/2210:37
7440-43-9
0.58 mg/L
0.50
1
10/13/2214:19
10/14/2210:37
7440-47-3
0.87 mg/L
0.50
1
10/13/2214:19
10/14/2210:37
7439-92-1
ND mg/L
0.10
1
10/13/2214:19
10/14/2210:37
7782-49-2
ND mg/L
0.10
1
10/13/2214:19
10/14/2210:37
7440-22-4
Analytical Method: EPA 7470A Preparation Method:
EPA 7470A
Leachate Method/Date: EPA 1311; 10/05/22
14:17
Pace Analytical Services - Minneapolis
1.4 ug/L
0.60
1
10/06/2211:30
10/06/2216:22
7439-97-6 H3
Analytical Method: EPA 7196A Preparation Method:
EPA 7196A Modified
Pace Analytical Services -Asheville
ND mg/kg
2.5
1
09/22/22 09:30
09/22/22 11:58
18540-29-9 H2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 80 of 165

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: WASTE CHARACTERIZATION
Pace Project No.: 92621331
Sample: Basin 3 Lab ID: 92621331017 Collected: 08/16/22 11:30 Received: 09/13/22 09:44 Matrix: Solid
Results reported on a "wet -weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010D MET ICP, TCLP
Arsenic
Barium
Cadmium
Chromium
Lead
Selenium
Silver
7470A Mercury, TCLP
Mercury
7196 Chromium, Hexavalent
Chromium, Hexavalent
Date: 10/25/2022 02:36 PM
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Leachate Method/Date: EPA 1311; 10/10/22 14:21
Pace Analytical Services - Minneapolis
ND mg/L
0.50
1
10/24/22 06:21
10/24/22 12:55
7440-38-2
3.5 mg/L
1.0
1
10/24/22 06:21
10/24/22 12:55
7440-39-3
0.052 mg/L
0.050
1
10/24/22 06:21
10/24/22 12:55
7440-43-9
1.5 mg/L
0.50
1
10/24/22 06:21
10/24/22 12:55
7440-47-3
13.5 mg/L
0.50
1
10/24/22 06:21
10/24/22 12:55
7439-92-1 M1
ND mg/L
0.10
1
10/24/22 06:21
10/24/22 12:55
7782-49-2
0.27 mg/L
0.10
1
10/24/22 06:21
10/24/22 12:55
7440-22-4
Analytical Method: EPA 7470A Preparation Method:
EPA 7470A
Leachate Method/Date: EPA 1311; 10/10/22
14:21
Pace Analytical Services - Minneapolis
10.6 ug/L
0.60
1
10/11/22 08:58
10/11/22 12:20
7439-97-6 H3
Analytical Method: EPA 7196A Preparation Method:
EPA 7196A Modified
Pace Analytical Services -Asheville
ND mg/kg
2.8
1
09/22/22 09:30
09/22/22 11:59
18540-29-9 H2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 81 of 165

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: WASTE CHARACTERIZATION
Pace Project No.: 92621331
Sample: Basin 4 Lab ID: 92621331018 Collected: 08/16/22 10:45 Received: 09/13/22 09:44 Matrix: Solid
Results reported on a "wet -weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010D MET ICP, TCLP
Arsenic
Barium
Cadmium
Chromium
Lead
Selenium
Silver
7470A Mercury, TCLP
Mercury
7196 Chromium, Hexavalent
Chromium, Hexavalent
Date: 10/25/2022 02:36 PM
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Leachate Method/Date: EPA 1311; 10/10/22 14:21
Pace Analytical Services - Minneapolis
ND mg/L
0.50
1
10/24/22 06:21
10/24/22 13:03
7440-38-2
ND mg/L
1.0
1
10/24/22 06:21
10/24/22 13:03
7440-39-3
ND mg/L
0.050
1
10/24/22 06:21
10/24/22 13:03
7440-43-9
ND mg/L
0.50
1
10/24/22 06:21
10/24/22 13:03
7440-47-3
ND mg/L
0.50
1
10/24/22 06:21
10/24/22 13:03
7439-92-1
ND mg/L
0.10
1
10/24/22 06:21
10/24/22 13:03
7782-49-2
ND mg/L
0.10
1
10/24/22 06:21
10/24/22 13:03
7440-22-4
Analytical Method: EPA 7470A Preparation Method:
EPA 7470A
Leachate Method/Date: EPA 1311; 10/10/22
14:21
Pace Analytical Services - Minneapolis
ND ug/L
0.60
1
10/11/22 08:58
10/11/22 12:21
7439-97-6 H3
Analytical Method: EPA 7196A Preparation Method:
EPA 7196A Modified
Pace Analytical Services -Asheville
ND mg/kg
4.2
1
09/22/22 09:30
09/22/22 11:59
18540-29-9 H2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 82 of 165

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: WASTE CHARACTERIZATION
Pace Project No.: 92621331
QC Batch: 1914170 Analysis Method: EPA 8141 B
QC Batch Method: 3546 Analysis Description: OP Pesticides 8141 B
Laboratory: Pace National - Mt. Juliet
Associated Lab Samples: 92621331001, 92621331002, 92621331003, 92621331004, 92621331005, 92621331006, 92621331007,
92621331008,92621331009,92621331010
METHOD BLANK: R3828771-1 Matrix: Solid
Associated Lab Samples: 92621331001, 92621331002, 92621331003, 92621331004, 92621331005, 92621331006, 92621331007,
92621331008,92621331009,92621331010
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Azinphos, methyl (Guthion)
mg/kg
ND
0.100
08/21/22 22:07
Bolstar
mg/kg
ND
0.100
08/21/22 22:07
Chlorpyrifos
mg/kg
ND
0.100
08/21/22 22:07
Coumaphos
mg/kg
ND
0.100
08/21/22 22:07
Total Demeton
mg/kg
ND
0.0700
08/21/22 22:07
Diazinon
mg/kg
ND
0.100
08/21/22 22:07
Dichlorvos
mg/kg
ND
0.100
08/21/22 22:07
Dimethoate
mg/kg
ND
0.100
08/21/22 22:07
Disulfoton
mg/kg
ND
0.100
08/21/22 22:07
EPN (ENT)
mg/kg
ND
0.100
08/21/22 22:07
Ethoprop
mg/kg
ND
0.100
08/21/22 22:07
Parathion (Ethyl parathion)
mg/kg
ND
0.100
08/21/22 22:07
Fensulfothion
mg/kg
ND
0.100
08/21/22 22:07
Fenthion
mg/kg
ND
0.100
08/21/22 22:07
Malathion
mg/kg
ND
0.100
08/21/22 22:07
Merphos
mg/kg
ND
0.100
08/21/22 22:07
Methyl parathion
mg/kg
ND
0.100
08/21/22 22:07
Mevinphos
mg/kg
ND
0.100
08/21/22 22:07
Naled
mg/kg
ND
0.100
08/21/22 22:07
Phorate
mg/kg
ND
0.100
08/21/22 22:07
Ronnel
mg/kg
ND
0.100
08/21/22 22:07
Stirophos (Tetrachlorvinphos)
mg/kg
ND
0.100
08/21/22 22:07
Sulfotepp (ThiodiphosphoricAc
mg/kg
ND
0.100
08/21/22 22:07
TEPP
mg/kg
ND
1.00
08/21/22 22:07
Tokuthion (Prothiofos)
mg/kg
ND
0.100
08/21/22 22:07
Trichloronate
mg/kg
ND
0.100
08/21/22 22:07
Triphenylphosphate (S)
%
96.7
36.0-121
08/21/22 22:07
LABORATORY CONTROL SAMPLE:
R3828771-2
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits Qualifiers
Azinphos, methyl (Guthion)
mg/kg
0.333
0.361
108
58.0-125
Bolstar
mg/kg
0.333
0.322
96.7
64.0-120
Chlorpyrifos
mg/kg
0.333
0.297
89.2
62.0-120
Coumaphos
mg/kg
0.333
0.351
105
60.0-120
Total Demeton
mg/kg
0.167
0.145
86.8
59.0-120
Diazinon
mg/kg
0.333
0.281
84.4
49.0-120
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/25/2022 02:36 PM without the written consent of Pace Analytical Services, LLC. Page 83 of 165

Pace Analytical Services, LLC
9800
lCtaac,Analyfical ® Kiney Ave. Suite 100
Huntersville, NC 28078
0788
www.pacelabs.com [phone]
QUALITY CONTROL DATA
Project: WASTE CHARACTERIZATION
Pace Project No.: 92621331
LABORATORY CONTROL SAMPLE:
Parameter
R3828771-2
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
Dichlorvos
mg/kg
0.333
0.215
64.6
37.0-120
Dimethoate
mg/kg
0.333
0.294
88.3
46.0-127
Disulfoton
mg/kg
0.333
0.298
89.5
60.0-121
EPN (ENT)
mg/kg
0.333
0.373
112
60.0-121
Ethoprop
mg/kg
0.333
0.302
90.7
59.0-120
Parathion (Ethyl parathion)
mg/kg
0.333
0.321
96.4
62.0-120
Fensulfothion
mg/kg
0.333
0.343
103
58.0-123
Fenthion
mg/kg
0.333
0.317
95.2
61.0-121
Malathion
mg/kg
0.333
0.316
94.9
59.0-120
Merphos
mg/kg
0.333
0.292
87.7
59.0-120
Methyl parathion
mg/kg
0.333
0.314
94.3
63.0-120
Mevinphos
mg/kg
0.333
0.264
79.3
50.0-120
Naled
mg/kg
0.333
0.179
53.8
10.0-125
Phorate
mg/kg
0.333
0.289
86.8
60.0-120
Ronnel
mg/kg
0.333
0.320
96.1
62.0-120
Stirophos (Tetrachlorvinphos)
mg/kg
0.333
0.326
97.9
62.0-120
Sulfotepp (ThiodiphosphoricAc
mg/kg
0.333
0.307
92.2
62.0-122
TEPP
mg/kg
3.33
0.264
7.93
10.0-135 LO
Tokuthion (Prothiofos)
mg/kg
0.333
0.313
94.0
63.0-120
Trichloronate
mg/kg
0.333
0.288
86.5
62.0-120
Triphenyl phosphate (S)
%
95.8
36.0-121
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: R3828771-3
MS
L1527612-01 Spike
Parameter Units Result Conc.
MSD
Spike
Conc.
R3828771-4
MS MSD
Result Result
MS
% Rec
MSD
% Rec
% Rec
Limits
RPD Qual
Azinphos, methyl (Guthion)
mg/kg
ND
0.321
0.319
0.240
0.241
74.8
75.5
10.0-160
0.416
Bolstar
mg/kg
ND
0.321
0.319
0.213
0.230
66.4
72.1
10.0-151
7.67
Chlorpyrifos
mg/kg
ND
0.321
0.319
0.196
0.210
61.1
65.8
12.0-149
6.90
Coumaphos
mg/kg
ND
0.321
0.319
0.234
0.246
72.9
77.1
10.0-160
5.00
Total Demeton
mg/kg
ND
0.161
0.160
0.0996
0.0983
61.9
61.4
10.0-160
1.31
Diazinon
mg/kg
ND
0.321
0.319
0.197
0.208
61.4
65.2
11.0-157
5.43
Dichlorvos
mg/kg
ND
0.321
0.319
0.213
0.228
66.4
71.5
10.0-160
6.80
Dimethoate
mg/kg
ND
0.321
0.319
0.241
0.252
75.1
79.0
10.0-150
4.46
Disulfoton
mg/kg
ND
0.321
0.319
0.195
0.203
60.7
63.6
12.0-155
4.02
EPN (ENT)
mg/kg
ND
0.321
0.319
0.276
0.281
86.0
88.1
10.0-159
1.80
Ethoprop
mg/kg
ND
0.321
0.319
0.203
0.212
63.2
66.5
11.0-156
4.34
Parathion (Ethyl parathion)
mg/kg
ND
0.321
0.319
0.239
0.243
74.5
76.2
10.0-147
1.66
Fensulfothion
mg/kg
ND
0.321
0.319
0.243
0.248
75.7
77.7
10.0-157
2.04
Fenthion
mg/kg
ND
0.321
0.319
0.204
0.214
63.6
67.1
13.0-155
4.78
Malathion
mg/kg
ND
0.321
0.319
0.227
0.231
70.7
72.4
13.0-137
1.75
Merphos
mg/kg
ND
0.321
0.319
0.155
0.174
48.3
54.5
10.0-147
11.6
Methyl parathion
mg/kg
ND
0.321
0.319
0.215
0.218
67.0
68.3
10.0-150
1.39
Mevinphos
mg/kg
ND
0.321
0.319
0.208
0.213
64.8
66.8
10.0-158
2.38
Naled
mg/kg
ND
0.321
0.319
0.110
0.107
34.3
33.5
10.0-137
2.76
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/25/2022 02:36 PM without the written consent of Pace Analytical Services, LLC. Page 84 of 165

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: WASTE CHARACTERIZATION
Pace Project No.: 92621331
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: R3828771-3
MS
L1527612-01 Spike
Parameter Units Result Conc.
MSD
Spike
Conc.
R3828771-4
MS MSD
Result Result
MS
% Rec
MSD
% Rec
% Rec
Limits
RPD Qual
Phorate
mg/kg
ND
0.321
0.319
0.189
0.199
58.9
62.4
13.0-154
5.15
Ronnel
mg/kg
ND
0.321
0.319
0.213
0.224
66.4
70.2
14.0-149
5.03
Stirophos (Tetrachlorvinphos)
mg/kg
ND
0.321
0.319
0.220
0.228
68.5
71.5
10.0-150
3.57
Sulfotepp (Thiodiphosphoric
mg/kg
ND
0.321
0.319
0.221
0.226
68.8
70.8
10.0-160
2.24
Ac
TEPP
mg/kg
ND
3.21
3.19
2.65
2.41
82.6
75.5
10.0-142
9.49
Tokuthion (Prothiofos)
mg/kg
ND
0.321
0.319
0.206
0.222
64.2
69.6
12.0-153
7.48
Trichloronate
mg/kg
ND
0.321
0.319
0.193
0.211
60.1
66.1
12.0-152
8.91
Triphenylphosphate (S)
%
89.4
84.6
36.0-121
r
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/25/2022 02:36 PM without the written consent of Pace Analytical Services, LLC.
Page 85 of 165

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: WASTE CHARACTERIZATION
Pace Project No.: 92621331
QC Batch: 845066 Analysis Method: EPA 7470A
QC Batch Method: EPA 7470A Analysis Description: 7470A Mercury TCLP
Laboratory: Pace Analytical Services - Minneapolis
Associated Lab Samples: 92621331015, 92621331016
METHOD BLANK: 4471470 Matrix: Water
Associated Lab Samples: 92621331015, 92621331016
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Mercury ug/L ND 0.60 10/06/2216:14
METHOD BLANK: 4467618 Matrix: Water
Associated Lab Samples: 92621331015, 92621331016
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Mercury ug/L ND 0.60 10/06/2216:48
METHOD BLANK: 4471302 Matrix: Water
Associated Lab Samples: 92621331015, 92621331016
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Mercury ug/L ND 0.60 10/06/2216:49
LABORATORY CONTROL SAMPLE: 4471471
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Mercury ug/L 15 16.2 108 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4471472 4471473
MS MSD
92621331015 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Mercury ug/L ND 15 15 16.2 16.4 106 107 80-120 1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/25/2022 02:36 PM without the written consent of Pace Analytical Services, LLC.
Page 86 of 165

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: WASTE CHARACTERIZATION
Pace Project No.: 92621331
QC Batch: 845983 Analysis Method: EPA 7470A
QC Batch Method: EPA 7470A Analysis Description: 7470A Mercury TCLP
Laboratory: Pace Analytical Services - Minneapolis
Associated Lab Samples: 92621331017, 92621331018
METHOD BLANK: 4476136 Matrix: Water
Associated Lab Samples: 92621331017, 92621331018
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Mercury ug/L ND 0.60 10/11/2212:12
METHOD BLANK: 4475236
Matrix:
Water
Associated Lab Samples: 92621331017, 92621331018
Blank
Reporting
Parameter
Units
Result
Limit Analyzed Qualifiers
Mercury
ug/L
ND
0.60 10/11/2212:44
LABORATORY CONTROL SAMPLE:
4476137
Spike
LCS LCS % Rec
Parameter
Units
Conc.
Result % Rec Limits Qualifiers
Mercury
ug/L
15
15.7 104 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4476138 4476139
MS MSD
10626741001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Mercury ug/L ND 15 15 16.2 16.2 108 108 80-120 0
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/25/2022 02:36 PM without the written consent of Pace Analytical Services, LLC.
Page 87 of 165

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: WASTE CHARACTERIZATION
Pace Project No.: 92621331
QC Batch: 850454 Analysis Method: EPA 7471
QC Batch Method: EPA 7471 Analysis Description: 7471 Mercury
Laboratory: Pace Analytical Services - Ormond Beach
Associated Lab Samples: 92621331001, 92621331002, 92621331003, 92621331004, 92621331005, 92621331006, 92621331007,
92621331008,92621331009,92621331010
METHOD BLANK: 4679207 Matrix: Solid
Associated Lab Samples: 92621331001, 92621331002, 92621331003, 92621331004, 92621331005, 92621331006, 92621331007,
92621331008,92621331009,92621331010
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Mercury mg/kg ND 0.0092 08/24/2210:48
LABORATORY CONTROL SAMPLE: 4679208
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Mercury mg/kg 0.095 0.086 90 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4679209 4679210
MS MSD
35739359001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Mercury mg/kg 0.0077 0.153 0.155 0.13 0.13 83 82 80-120 1
U
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/25/2022 02:36 PM without the written consent of Pace Analytical Services, LLC.
Page 88 of 165

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: WASTE CHARACTERIZATION
Pace Project No.: 92621331
QC Batch: 852452 Analysis Method: EPA 6010
QC Batch Method: EPA 3050 Analysis Description: 6010 MET Solid
Laboratory: Pace Analytical Services - Ormond Beach
Associated Lab Samples: 92621331002, 92621331003, 92621331004, 92621331005, 92621331006, 92621331007, 92621331008,
92621331009,92621331010
METHOD BLANK: 4690207 Matrix: Solid
Associated Lab Samples: 92621331002, 92621331003, 92621331004, 92621331005, 92621331006, 92621331007, 92621331008,
92621331009,92621331010
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Tin mg/kg ND 2.9 08/31/2214:24
LABORATORY CONTROL SAMPLE: 4690208
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Tin mg/kg 63.4 65.8 104 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4690209 4690210
MS MSD
35742050002 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Tin mg/kg ND 67.4 62.9 57.8 55.3 84 86 75-125 4
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/25/2022 02:36 PM without the written consent of Pace Analytical Services, LLC.
Page 89 of 165

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: WASTE CHARACTERIZATION
Pace Project No.: 92621331
QC Batch: 852504 Analysis Method: EPA 6010
QC Batch Method: EPA 3050 Analysis Description: 6010 MET Solid
Laboratory: Pace Analytical Services - Ormond Beach
Associated Lab Samples: 92621331001
METHOD BLANK: 4690598
Associated Lab Samples: 92621331001
Parameter Units
Tin mg/kg
LABORATORY CONTROL SAMPLE: 4690599
Parameter Units
Tin mg/kg
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
Matrix: Solid
Blank Reporting
Result Limit Analyzed Qualifiers
ND 3.1 09/05/22 03:09
Spike LCS LCS % Rec
Conc. Result % Rec Limits Qualifiers
75.7 77.2 102 80-120
MS MSD
Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/25/2022 02:36 PM without the written consent of Pace Analytical Services, LLC. Page 90 of 165

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: WASTE CHARACTERIZATION
Pace Project No.: 92621331
QC Batch: 846729 Analysis Method: EPA 6010D
QC Batch Method: EPA 3010A Analysis Description: 601 OD TCLP
Laboratory: Pace Analytical Services - Minneapolis
Associated Lab Samples: 92621331015, 92621331016
METHOD BLANK: 4480073
Matrix:
Water
Associated Lab Samples:
92621331015, 92621331016
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed
Arsenic
mg/L
ND
0.50
10/14/2210:22
Barium
mg/L
ND
1.0
10/14/2210:22
Cadmium
mg/L
ND
0.050
10/14/2210:22
Chromium
mg/L
ND
0.50
10/14/2210:22
Lead
mg/L
ND
0.50
10/14/2210:22
Selenium
mg/L
ND
0.10
10/14/2210:22
Silver
mg/L
ND
0.10
10/14/2210:22
LABORATORY CONTROL SAMPLE:
4480074
Parameter
Units
Arsenic
mg/L
Barium
mg/L
Cadmium
mg/L
Chromium
mg/L
Lead
mg/L
Selenium
mg/L
Silver
mg/L
Qualifiers
Spike
LCS
LCS
% Rec
Conc.
Result
% Rec
Limits Qualifiers
5
4.9
98
80-120
5
4.9
97
80-120
5
5.0
101
80-120
5
4.9
97
80-120
5
4.9
98
80-120
5
5.2
104
80-120
2.5
2.5
100
80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
4480075
4480076
MS
MSD
10629543001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Arsenic
mg/L
ND
5
5
5.9
4.9
118
98
75-125
18
Barium
mg/L
ND
5
5
5.2
5.5
102
110
75-125
7
Cadmium
mg/L
ND
5
5
5.3
5.6
105
113
75-125
7
Chromium
mg/L
ND
5
5
5.2
5.6
103
110
75-125
7
Lead
mg/L
ND
5
5
5.2
5.5
103
111
75-125
7
Selenium
mg/L
ND
5
5
6.2
5.2
124
104
75-125
18
Silver
mg/L
ND
2.5
2.5
2.6
2.8
106
113
75-125
7
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/25/2022 02:36 PM without the written consent of Pace Analytical Services, LLC.
Page 91 of 165

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: WASTE CHARACTERIZATION
Pace Project No.: 92621331
QC Batch: 848727 Analysis Method: EPA 6010D
QC Batch Method: EPA 3010A Analysis Description: 601 OD TCLP
Laboratory: Pace Analytical Services - Minneapolis
Associated Lab Samples: 92621331017, 92621331018
METHOD BLANK: 4490096
Matrix:
Water
Associated Lab Samples:
92621331017, 92621331018
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Arsenic
mg/L
ND
0.50
10/24/2212:50
Barium
mg/L
ND
1.0
10/24/2212:50
Cadmium
mg/L
ND
0.050
10/24/2212:50
Chromium
mg/L
ND
0.50
10/24/2212:50
Lead
mg/L
ND
0.50
10/24/2212:50
Selenium
mg/L
ND
0.10
10/24/2212:50
Silver
mg/L
ND
0.10
10/24/2212:50
METHOD BLANK: 4475236
Matrix:
Water
Associated Lab Samples:
92621331017, 92621331018
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Arsenic
mg/L
ND
0.50
10/24/2212:51
Barium
mg/L
ND
1.0
10/24/2212:51
Cadmium
mg/L
ND
0.050
10/24/2212:51
Chromium
mg/L
ND
0.50
10/24/2212:51
Lead
mg/L
ND
0.50
10/24/2212:51
Selenium
mg/L
ND
0.10
10/24/2212:51
Silver
mg/L
ND
0.10
10/24/2212:51
LABORATORY CONTROL SAMPLE:
4490097
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits Qualifiers
Arsenic
mg/L
5
5.1
102
80-120
Barium
mg/L
5
5.0
101
80-120
Cadmium
mg/L
5
5.2
105
80-120
Chromium
mg/L
5
5.1
102
80-120
Lead
mg/L
5
5.1
102
80-120
Selenium
mg/L
5
5.5
109
80-120
Silver
mg/L
2.5
2.6
104
80-120
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/25/2022 02:36 PM without the written consent of Pace Analytical Services, LLC.
Page 92 of 165

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: WASTE CHARACTERIZATION
Pace Project No.: 92621331
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4490098
4490099
MS
MSD
92621331017 Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter Units Result Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Arsenic mg/L ND
5 5
5.2
4.9
103
99
75-125
4
Barium mg/L 3.5
5 5
8.4
8.1
97
90
75-125
4
Cadmium mg/L 0.052
5 5
5.3
5.1
104
100
75-125
4
Chromium mg/L 1.5
5 5
6.5
6.2
100
94
75-125
4
Lead mg/L 13.5
5 5
17.6
16.9
82
69
75-125
4 M1
Selenium mg/L ND
5 5
5.5
5.2
109
104
75-125
5
Silver mg/L 0.27 2.5
2.5
2.9
2.8
104
99
75-125
4
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/25/2022 02:36 PM without the written consent of Pace Analytical Services, LLC.
Page 93 of 165

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: WASTE CHARACTERIZATION
Pace Project No.: 92621331
QC Batch: 851671 Analysis Method: EPA 6020
QC Batch Method: EPA 3050 Analysis Description: 6020 MET SOLID
Laboratory: Pace Analytical Services - Ormond Beach
Associated Lab Samples: 92621331001, 92621331002, 92621331003, 92621331004, 92621331005, 92621331006, 92621331007,
92621331008,92621331009,92621331010
METHOD BLANK: 4686954 Matrix: Solid
Associated Lab Samples: 92621331001, 92621331002, 92621331003, 92621331004, 92621331005, 92621331006, 92621331007,
92621331008,92621331009,92621331010
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Arsenic
mg/kg
ND
1.2
08/29/22 09:40 1g
Barium
mg/kg
ND
1.2
08/29/22 09:40 1g
Beryllium
mg/kg
ND
0.15
08/29/22 09:40 1g
Cadmium
mg/kg
ND
0.15
08/29/22 09:40 1g
Chromium
mg/kg
ND
1.2
08/29/22 09:40 1g
Cobalt
mg/kg
ND
1.2
08/29/22 09:40 1g
Copper
mg/kg
ND
2.5
08/29/22 09:40 1g
Lead
mg/kg
ND
1.2
08/29/22 09:40 1g
Nickel
mg/kg
ND
1.2
08/29/22 09:40 1g
Selenium
mg/kg
ND
1.2
08/29/22 09:40 1g
Silver
mg/kg
ND
0.15
08/29/22 09:40 1g
Thallium
mg/kg
ND
1.2
08/29/22 09:40 1g
Vanadium
mg/kg
ND
1.2
08/29/22 09:40 1g
Zinc
mg/kg
ND
49.6
08/29/22 09:40 1g
LABORATORY CONTROL SAMPLE:
Parameter
4686955
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
Arsenic
mg/kg
30.7
31.6
103
80-120 1g
Barium
mg/kg
30.7
32.8
107
80-120 1g
Beryllium
mg/kg
3.1
3.2
105
80-120 1g
Cadmium
mg/kg
3.1
3.3
109
80-120 1g
Chromium
mg/kg
30.7
33.8
110
80-120 1g
Cobalt
mg/kg
30.7
33.6
109
80-120 1g
Copper
mg/kg
30.7
32.9
107
80-120 1g
Lead
mg/kg
30.7
31.1
101
80-120 1g
Nickel
mg/kg
30.7
33.6
110
80-120 1g
Selenium
mg/kg
30.7
32.6
106
80-120 1g
Silver
mg/kg
3.1
3.2
103
80-120 1g
Thallium
mg/kg
30.7
30.5
100
80-120 1g
Vanadium
mg/kg
30.7
34.0
111
80-120 1g
Zinc
mg/kg
153
162
106
80-120 1g
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/25/2022 02:36 PM without the written consent of Pace Analytical Services, LLC. Page 94 of 165

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project:
Pace Project No.:
WASTE CHARACTERIZATION
92621331
MATRIX SPIKE &
MATRIX SPIKE DUPLICATE:
4686956
4686957
MS
MSD
35741869007
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Arsenic
mg/kg
3.4
30.1
29.6
31.5
33.8
93
103
75-125
71g
Barium
mg/kg
15.6
30.1
29.6
47.5
49.9
106
116
75-125
51g
Beryllium
mg/kg
0.14J
3.05
2.93
4.3
4.4
138
143
75-125
2 1g,M1
Cadmium
mg/kg
0.20
3.05
2.93
3.2
3.2
98
102
75-125
31g
Chromium
mg/kg
11.8
30.1
29.6
38.8
43.5
89
107
75-125
12 1g
Cobalt
mg/kg
0.911
30.1
29.6
29.8
31.0
96
102
75-125
41g
Copper
mg/kg
13.1
30.1
29.6
37.8
39.0
82
87
75-125
31g
Lead
mg/kg
26.9
30.1
29.6
55.1
49.4
94
76
75-125
11 1g
Nickel
mg/kg
2.7
30.1
29.6
31.7
34.2
96
106
75-125
71g
Selenium
mg/kg
0.61U
30.1
29.6
29.5
32.2
96
107
75-125
91g
Silver
mg/kg
0.0451-1
3.05
2.93
3.0
3.2
99
107
75-125
61g
Thallium
mg/kg
0.21U
30.1
29.6
29.5
29.6
98
100
75-125
1 1g
Vanadium
mg/kg
7.6
30.1
29.6
36.5
39.7
96
108
75-125
81g
Zinc
mg/kg
45.9J
150
148
194
196
99
102
75-125
1 1g
?AA"
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/25/2022 02:36 PM without the written consent of Pace Analytical Services, LLC.
Page 95 of 165

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: WASTE CHARACTERIZATION
Pace Project No.: 92621331
QC Batch: 718270 Analysis Method: EPA 8260D
QC Batch Method: EPA 5035A/5030B Analysis Description: 8260D 5035A 5030E
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92621331011, 92621331012, 92621331013, 92621331014
METHOD BLANK: 3744381 Matrix: Solid
Associated Lab Samples: 92621331011, 92621331012, 92621331013, 92621331014
Blank Reporting
Parameter Units Result Limit
1,1,1,2-Tetrachloroethane
1,1,1-Trichloroethane
1,1,2,2-Tetrachloroethane
1,1,2-Trichloroethane
1,1-Dichloroethane
1,1-Dichloroethene
1,1-Dichloropropene
1,2,3-Trichloropropane
1,2,4-Trichlorobenzene
1,2-Dichlorobenzene
1,2-Dichloroethane
1,2-Dichloropropane
1,3-Dichlorobenzene
1,3-Dichloropropane
1,4-Dichlorobenzene
2,2-Dichloropropane
2-Butanone (MEK)
2-Hexanone
4-Methyl-2-pentanone (MIBK)
Acetone
Acetonitrile
Acrolein
Acrylonitrile
Allyl chloride
Benzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Chloroprene
cis-1,2-Dichloroethene
cis-1,3-Dichloropropene
Dibromochloromethane
Dibromomethane
ug/kg
ND
5.0
ug/kg
ND
5.0
ug/kg
ND
5.0
ug/kg
ND
5.0
ug/kg
ND
5.0
ug/kg
ND
5.0
ug/kg
ND
5.0
ug/kg
ND
5.0
ug/kg
ND
5.0
ug/kg
ND
5.0
ug/kg
ND
5.0
ug/kg
ND
5.0
ug/kg
ND
5.0
ug/kg
ND
5.0
ug/kg
ND
5.0
ug/kg
ND
5.0
ug/kg
ND
100
ug/kg
ND
50.0
ug/kg
ND
50.0
ug/kg
ND
100
ug/kg
ND
100
ug/kg
ND
100
ug/kg
ND
100
ug/kg
ND
50.0
ug/kg
ND
5.0
ug/kg
ND
5.0
ug/kg
ND
5.0
ug/kg
ND
5.0
ug/kg
ND
10.0
ug/kg
ND
10.0
ug/kg
ND
5.0
ug/kg
ND
5.0
ug/kg
ND
10.0
ug/kg
ND
5.0
ug/kg
ND
10.0
ug/kg
ND
10.0
ug/kg
ND
5.0
ug/kg
ND
5.0
ug/kg
ND
5.0
ug/kg
ND
5.0
Analyzed
08/19/22 03:55
08/19/22 03:55
08/19/22 03:55
08/19/22 03:55
08/19/22 03:55
08/19/22 03:55
08/19/22 03:55
08/19/22 03:55
08/19/22 03:55
08/19/22 03:55
08/19/22 03:55
08/19/22 03:55
08/19/22 03:55
08/19/22 03:55
08/19/22 03:55
08/19/22 03:55
08/19/22 03:55
08/19/22 03:55
08/19/22 03:55
08/19/22 03:55
08/19/22 03:55
08/19/22 03:55
08/19/22 03:55
08/19/22 03:55
08/19/22 03:55
08/19/22 03:55
08/19/22 03:55
08/19/22 03:55
08/19/22 03:55
08/19/22 03:55
08/19/22 03:55
08/19/22 03:55
08/19/22 03:55
08/19/22 03:55
08/19/22 03:55
08/19/22 03:55
08/19/22 03:55
08/19/22 03:55
08/19/22 03:55
08/19/22 03:55
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/25/2022 02:36 PM without the written consent of Pace Analytical Services, LLC. Page 96 of 165

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: WASTE CHARACTERIZATION
Pace Project No.: 92621331
METHOD BLANK: 3744381 Matrix: Solid
Associated Lab Samples: 92621331011, 92621331012, 92621331013, 92621331014
Blank Reporting
Parameter Units Result Limit
Analyzed
Dichlorodifluoromethane
ug/kg
ND
10.0
08/19/22 03:55
Ethyl methacrylate
ug/kg
ND
5.0
08/19/22 03:55
Ethylbenzene
ug/kg
ND
5.0
08/19/22 03:55
Hexachloro-1,3-butadiene
ug/kg
ND
10.0
08/19/22 03:55
lodomethane
ug/kg
ND
50.0
08/19/22 03:55
Isobutanol
ug/kg
ND
100
08/19/22 03:55
m&p-Xylene
ug/kg
ND
10.0
08/19/22 03:55
Methacrylonitrile
ug/kg
ND
50.0
08/19/22 03:55
Methyl methacrylate
ug/kg
ND
5.0
08/19/22 03:55
Methylene Chloride
ug/kg
ND
20.0
08/19/22 03:55
Naphthalene
ug/kg
ND
5.0
08/19/22 03:55
o-Xylene
ug/kg
ND
5.0
08/19/22 03:55
Propionitrile
ug/kg
ND
50.0
08/19/22 03:55
Styrene
ug/kg
ND
5.0
08/19/22 03:55
Tetrachloroethene
ug/kg
ND
5.0
08/19/22 03:55
Toluene
ug/kg
ND
5.0
08/19/22 03:55
trans-1,2-Dichloroethene
ug/kg
ND
5.0
08/19/22 03:55
trans- 1,3-Dichloropropene
ug/kg
ND
5.0
08/19/22 03:55
trans-1,4-Dichloro-2-butene
ug/kg
ND
10.0
08/19/22 03:55
Trichloroethene
ug/kg
ND
5.0
08/19/22 03:55
Trichlorofluoromethane
ug/kg
ND
5.0
08/19/22 03:55
Vinyl acetate
ug/kg
ND
50.0
08/19/22 03:55
Vinyl chloride
ug/kg
ND
10.0
08/19/22 03:55
Xylene (Total)
ug/kg
ND
10.0
08/19/22 03:55
1,2-Dichloroethane-d4 (S)
%
106
70-130
08/19/22 03:55
4-Bromofluorobenzene (S)
%
102
70-130
08/19/22 03:55
Toluene-d8 (S)
%
99
70-130
08/19/22 03:55
Qualifiers
IH.v1
LABORATORY CONTROL SAMPLE:
Parameter
3744382
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
1,1,1,2-Tetrachloroethane
ug/kg
1250
1290
103
70-130
1,1,1-Trichloroethane
ug/kg
1250
1290
103
70-130
1,1,2,2-Tetrachloroethane
ug/kg
1250
1130
90
70-130
1,1,2-Trichloroethane
ug/kg
1250
1210
97
70-130
1,1-Dichloroethane
ug/kg
1250
1250
100
70-130
1,1-Dichloroethene
ug/kg
1250
1390
111
70-130
1,1-Dichloropropene
ug/kg
1250
1310
105
70-130
1,2,3-Trichloropropane
ug/kg
1250
1120
90
70-130
1,2,4-Trichlorobenzene
ug/kg
1250
1250
100
70-130
1,2-Dichlorobenzene
ug/kg
1250
1270
102
70-130
1,2-Dichloroethane
ug/kg
1250
1180
94
70-130
1,2-Dichloropropane
ug/kg
1250
1260
101
70-130
1,3-Dichlorobenzene
ug/kg
1250
1250
100
70-130
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/25/2022 02:36 PM without the written consent of Pace Analytical Services, LLC. Page 97 of 165

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: WASTE CHARACTERIZATION
Pace Project No.: 92621331
LABORATORY CONTROL SAMPLE: 3744382
Parameter
QUALITY CONTROL DATA
Spike LCS LCS % Rec
Units Conc. Result % Rec Limits Qualifiers
1,3-Dichloropropane
ug/kg
1250
1210
97
70-130
1,4-Dichlorobenzene
ug/kg
1250
1280
102
70-130
2,2-Dichloropropane
ug/kg
1250
1250
100
67-130
2-Butanone (MEK)
ug/kg
2500
2150
86
66-130
2-Hexanone
ug/kg
2500
2370
95
70-130
4-Methyl-2-pentanone (MIBK)
ug/kg
2500
2360
94
70-130
Acetone
ug/kg
2500
2130
85
67-130
Acetonitrile
ug/kg
12500
10900
87
70-130
Acrolein
ug/kg
6250
7240
116
70-130
Acrylonitrile
ug/kg
6250
5840
93
70-130
Allyl chloride
ug/kg
1250
1310
105
70-130
Benzene
ug/kg
1250
1200
96
70-130
Bromochloromethane
ug/kg
1250
1250
100
70-130
Bromodichloromethane
ug/kg
1250
1240
100
70-130
Bromoform
ug/kg
1250
1200
96
70-130
Bromomethane
ug/kg
1250
1290
103
53-175
Carbon disulfide
ug/kg
1250
1270
101
70-130
Carbon tetrachloride
ug/kg
1250
1340
107
70-130
Chlorobenzene
ug/kg
1250
1240
99
70-130
Chloroethane
ug/kg
1250
1370
110
70-135
Chloroform
ug/kg
1250
1130
90
70-130
Chloromethane
ug/kg
1250
1420
114
64-130
Chloroprene
ug/kg
1250
1280
103
70-130
cis-1,2-Dichloroethene
ug/kg
1250
1280
102
70-130
cis-1,3-Dichloropropene
ug/kg
1250
1290
103
70-130
Dibromochloromethane
ug/kg
1250
1250
100
70-130
Dibromomethane
ug/kg
1250
1210
97
70-130
Dichlorodifluoromethane
ug/kg
1250
1720
137
63-1451H,v1
Ethyl methacrylate
ug/kg
1250
1260
101
70-130
Ethylbenzene
ug/kg
1250
1190
95
70-130
Hexachloro-1,3-butadiene
ug/kg
1250
1210
97
70-130
lodomethane
ug/kg
2500
2440
98
70-130
Isobutanol
ug/kg
25000
21700
87
70-130
m&p-Xylene
ug/kg
2500
2540
102
70-130
Methacrylonitrile
ug/kg
12500
10800
87
70-130
Methyl methacrylate
ug/kg
1250
1250
100
70-130
Methylene Chloride
ug/kg
1250
1170
94
67-130
Naphthalene
ug/kg
1250
1270
101
70-130
o-Xylene
ug/kg
1250
1290
103
70-130
Propionitrile
ug/kg
12500
10800
86
70-130
Styrene
ug/kg
1250
1320
105
70-130
Tetrachloroethene
ug/kg
1250
1180
94
70-130
Toluene
ug/kg
1250
1250
100
70-130
trans-1,2-Dichloroethene
ug/kg
1250
1320
106
70-130
trans- 1,3-Dichloropropene
ug/kg
1250
1290
103
70-130
trans-1,4-Dichloro-2-butene
ug/kg
1250
982
79
70-130
Trichloroethene
ug/kg
1250
1270
101
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/25/2022 02:36 PM without the written consent of Pace Analytical Services, LLC. Page 98 of 165

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: WASTE CHARACTERIZATION
Pace Project No.: 92621331
LABORATORY CONTROL SAMPLE:
3744382
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits Qualifiers
Trichlorofluoromethane
ug/kg
1250
1240
99
70-130
Vinyl acetate
ug/kg
2500
2340
94
70-134
Vinyl chloride
ug/kg
1250
1400
112
68-130
Xylene (Total)
ug/kg
3750
3840
102
70-130
1,2-Dichloroethane-d4 (S)
%
93
70-130
4-Bromofluorobenzene (S)
%
100
70-130
Toluene-d8 (S)
%
100
70-130
MATRIX SPIKE SAMPLE:
Parameter
3744383
Units
92621393001
Result
Spike
Conc.
MS
Result
MS
% Rec
% Rec
Limits Qualifiers
1,1,1,2-Tetrachloroethane
ug/kg
ND
727
867
119
58-140
1,1,1-Trichloroethane
ug/kg
ND
727
881
121
58-144
1,1,2,2-Tetrachloroethane
ug/kg
ND
727
696
96
52-139
1,1,2-Trichloroethane
ug/kg
ND
727
784
108
56-140
1,1-Dichloroethane
ug/kg
ND
727
778
107
58-145
1,1-Dichloroethene
ug/kg
ND
727
812
112
57-158
1,1-Dichloropropene
ug/kg
ND
727
909
125
58-151
1,2,3-Trichloropropane
ug/kg
ND
727
695
96
54-132
1,2,4-Trichlorobenzene
ug/kg
ND
727
403
56
51-151
1,2-Dichlorobenzene
ug/kg
ND
727
841
116
59-147
1,2-Dichloroethane
ug/kg
ND
727
759
104
57-139
1,2-Dichloropropane
ug/kg
ND
727
833
115
62-145
1,3-Dichlorobenzene
ug/kg
ND
727
866
119
58-144
1,3-Dichloropropane
ug/kg
ND
727
784
108
60-142
1,4-Dichlorobenzene
ug/kg
ND
727
905
125
57-143
2,2-Dichloropropane
ug/kg
ND
727
762
105
37-144
2-Butanone (MEK)
ug/kg
ND
1450
1250
85
28-146
2-Hexanone
ug/kg
ND
1450
1340
92
44-141
4-Methyl-2-pentanone (MIBK)
ug/kg
ND
1450
1470
101
50-138
Acetone
ug/kg
ND
1450
1150
79
20-136
Acetonitrile
ug/kg
ND
7270
4010
55
70-130 M1
Acrolein
ug/kg
ND
3640
3830
105
70-130
Acrylonitrile
ug/kg
ND
3640
3300
91
36-152
Allyl chloride
ug/kg
ND
727
718
99
70-130
Benzene
ug/kg
ND
727
854
118
60-145
Bromochloromethane
ug/kg
ND
727
775
107
57-143
Bromodichloromethane
ug/kg
ND
727
804
111
53-133
Bromoform
ug/kg
ND
727
747
103
48-133
Bromomethane
ug/kg
ND
727
967
133
10-167
Carbon disulfide
ug/kg
ND
727
731
101
55-147
Carbon tetrachloride
ug/kg
ND
727
942
130
57-147
Chlorobenzene
ug/kg
ND
727
854
118
61-144
Chloroethane
ug/kg
ND
727
565
78
10-153
Chloroform
ug/kg
ND
727
733
101
58-141
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/25/2022 02:36 PM without the written consent of Pace Analytical Services, LLC. Page 99 of 165

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: WASTE CHARACTERIZATION
Pace Project No.: 92621331
MATRIX SPIKE SAMPLE: 3744383
92621393001 Spike MS MS % Rec
Parameter Units Result Conc. Result % Rec Limits Qualifiers
Chloromethane
ug/kg
ND
727
1090
150
54-165
Chloroprene
ug/kg
ND
727
845
116
70-130
cis-1,2-Dichloroethene
ug/kg
ND
727
820
113
59-144
cis-1,3-Dichloropropene
ug/kg
ND
727
834
115
56-137
Dibromochloromethane
ug/kg
ND
727
779
107
53-139
Dibromomethane
ug/kg
ND
727
798
110
60-136
Dichlorodifluoromethane
ug/kg
ND
727
1360
187
49-1771H,M1
Ethyl methacrylate
ug/kg
ND
727
762
105
70-130
Ethylbenzene
ug/kg
3.9J
727
819
112
53-150
Hexachloro-1,3-butadiene
ug/kg
ND
727
735
101
42-186
lodomethane
ug/kg
ND
1450
783
54
70-130 M1
Isobutanol
ug/kg
ND
14500
7320
50
70-130 M1
m&p-Xylene
ug/kg
7.9J
1450
1770
121
49-156
Methacrylonitrile
ug/kg
ND
7270
7230
100
70-130
Methyl methacrylate
ug/kg
ND
727
796
110
70-130
Methylene Chloride
ug/kg
ND
727
652
90
50-153
Naphthalene
ug/kg
ND
727
184
25
37-150 M1
o-Xylene
ug/kg
7.6
727
888
121
54-150
Propionitrile
ug/kg
ND
7270
3900
54
70-130 M1
Styrene
ug/kg
ND
727
866
119
60-148
Tetrachloroethene
ug/kg
ND
727
817
112
53-151
Toluene
ug/kg
ND
727
871
120
52-148
trans-1,2-Dichloroethene
ug/kg
ND
727
827
114
60-148
trans- 1,3-Dichloropropene
ug/kg
ND
727
819
113
55-133
trans-1,4-Dichloro-2-butene
ug/kg
ND
727
790
109
70-130
Trichloroethene
ug/kg
ND
727
903
124
60-148
Trichlorofluoromethane
ug/kg
ND
727
577
79
10-154
Vinyl acetate
ug/kg
ND
1450
1420
98
50-149
Vinyl chloride
ug/kg
ND
727
1190
163
57-157 M1
Xylene (Total)
ug/kg
15.5
2170
2660
121
52-153
1,2-Dichloroethane-d4 (S)
%
91
70-130
4-Bromofluorobenzene (S)
%
97
70-130
Toluene-d8 (S)
%
100
70-130
SAMPLE DUPLICATE: 3744384
Parameter
Units
92621393002
Result
Dup
Result RPD Qualifiers
1,1,1,2-Tetrachloroethane
ug/kg
ND
ND
1,1,1-Trichloroethane
ug/kg
ND
ND
1,1,2,2-Tetrachloroethane
ug/kg
ND
ND
1,1,2-Trichloroethane
ug/kg
ND
ND
1,1-Dichloroethane
ug/kg
ND
ND
1,1-Dichloroethene
ug/kg
ND
ND
1,1-Dichloropropene
ug/kg
ND
ND
1,2,3-Trichloropropane
ug/kg
ND
ND
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/25/2022 02:36 PM without the written consent of Pace Analytical Services, LLC. Page 100 of 165

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: WASTE CHARACTERIZATION
Pace Project No.: 92621331
SAMPLE DUPLICATE: 3744384
Parameter
Units
92621393002 Dup
Result Result
1,2,4-Trichlorobenzene
ug/kg
ND
ND
1,2-Dichlorobenzene
ug/kg
ND
ND
1,2-Dichloroethane
ug/kg
ND
ND
1,2-Dichloropropane
ug/kg
ND
ND
1,3-Dichlorobenzene
ug/kg
ND
ND
1,3-Dichloropropane
ug/kg
ND
ND
1,4-Dichlorobenzene
ug/kg
ND
ND
2,2-Dichloropropane
ug/kg
ND
ND
2-Butanone (MEK)
ug/kg
ND
ND
2-Hexanone
ug/kg
ND
ND
4-Methyl-2-pentanone (MIBK)
ug/kg
ND
ND
Acetone
ug/kg
ND
ND
Acetonitrile
ug/kg
ND
ND
Acrolein
ug/kg
ND
ND
Acrylonitrile
ug/kg
ND
ND
Allyl chloride
ug/kg
ND
ND
Benzene
ug/kg
ND V
ND
Bromochloromethane
Bromodichloromethane
ug/kg
ug/kg
ND
ND
ND
ND
Bromoform
ug/kg
ND 1111111110
ND
Bromomethane
ug/kg
ND
ND
Carbon disulfide
ug/kg
ND
ND
Carbon tetrachloride
ug/kg
ND
ND
Chlorobenzene
ug/kg
ND
ND
Chloroethane
ug/kg
ND
ND
Chloroform
ug/kg
ND
ND
Chloromethane
ug/kg
ND
ND
Chloroprene
ug/kg
ND
ND
cis-1,2-Dichloroethene
ug/kg
ND
ND
cis-1,3-Dichloropropene
ug/kg
ND
ND
Dibromochloromethane
ug/kg
ND
ND
Dibromomethane
ug/kg
ND
ND
Dichlorodifluoromethane
ug/kg
ND
ND
Ethyl methacrylate
ug/kg
ND
ND
Ethylbenzene
ug/kg
4.8J
4AJ
Hexachloro-1,3-butadiene
ug/kg
ND
ND
lodomethane
ug/kg
ND
ND
Isobutanol
ug/kg
ND
ND
m&p-Xylene
ug/kg
ND
ND
Methacrylonitrile
ug/kg
ND
ND
Methyl methacrylate
ug/kg
ND
ND
Methylene Chloride
ug/kg
ND
ND
Naphthalene
ug/kg
ND
ND
o-Xylene
ug/kg
8.1
8.7
Propionitrile
ug/kg
ND
ND
Styrene
ug/kg
ND
ND
Tetrachloroethene
ug/kg
ND
ND
RPD Qualifiers
8
IH,v1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/25/2022 02:36 PM without the written consent of Pace Analytical Services, LLC. Page 101 of 165

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: WASTE CHARACTERIZATION
Pace Project No.: 92621331
SAMPLE DUPLICATE: 3744384
Parameter
Units
92621393002
Result
Dup
Result
Toluene
ug/kg
ND
ND
trans-1,2-Dichloroethene
ug/kg
ND
ND
trans- 1,3-Dichloropropene
ug/kg
ND
ND
trans-1,4-Dichloro-2-butene
ug/kg
ND
ND
Trichloroethene
ug/kg
ND
ND
Trichlorofluoromethane
ug/kg
ND
ND
Vinyl acetate
ug/kg
ND
ND
Vinyl chloride
ug/kg
ND
ND
Xylene (Total)
ug/kg
8.11
8.7J
1,2-Dichloroethane-d4 (S)
%
100
99
4-Bromofluorobenzene (S)
%
102
100
Toluene-d8(S)
%
99
100
RPD Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/25/2022 02:36 PM without the written consent of Pace Analytical Services, LLC.
Page 102 of 165

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: WASTE CHARACTERIZATION
Pace Project No.: 92621331
QC Batch: 719156 Analysis Method: EPA 8081 B
QC Batch Method: EPA 3546 Analysis Description: 8081 GCS Pesticides
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92621331001, 92621331002, 92621331003, 92621331006, 92621331007, 92621331008, 92621331009,
92621331010
METHOD BLANK: 3748500 Matrix: Solid
Associated Lab Samples: 92621331001, 92621331002, 92621331003, 92621331006, 92621331007, 92621331008, 92621331009,
92621331010
Parameter
Units
Blank
Result
Reporting
Limit
4,4'-DDD
ug/kg
ND
2.0
4,4'-DDE
ug/kg
ND
2.0
4,4'-DDT
ug/kg
ND
2.0
Aldrin
ug/kg
ND
2.0
alpha-BHC
ug/kg
ND
2.0
beta-BHC
ug/kg
ND
2.0
Chlordane (Technical)
ug/kg
ND
10.1
delta-BHC
ug/kg
ND
2.0
Dieldrin
ug/kg
ND
2.0
Endosulfan I
ug/kg
ND
2.0
Endosulfan II
ug/kg
ND
2.0
Endosulfan sulfate
ug/kg
ND
2.0
Endrin
ug/kg
ND
2.0
Endrin aldehyde
ug/kg
ND
2.0
Endrin ketone
ug/kg
ND
2.0
gamma-BHC (Lindane)
ug/kg
ND
2.0
Heptachlor
ug/kg
ND
2.0
Heptachlor epoxide
ug/kg
ND
2.0
Hexachlorobenzene
ug/kg
ND
2.0
Methoxychlor
ug/kg
ND
5.1
Mirex
ug/kg
ND
5.1
Toxaphene
ug/kg
ND
7.1
Decachlorobiphenyl (S)
%
71
10-146
Tetrachloro-m-xylene (S)
%
70
10-133
Analyzed Qualifiers
08/26/22 21:20
08/26/22 21:20
08/26/22 21:20
08/26/22 21:20
08/26/22 21:20
08/26/22 21:20
08/26/22 21:20
08/26/22 21:20
08/26/22 21:20
08/26/22 21:20
08/26/22 21:20
08/26/22 21:20
08/26/22 21:20
08/26/22 21:20
08/26/22 21:20
08/26/22 21:20
08/26/22 21:20
08/26/22 21:20
08/26/22 21:20
08/26/22 21:20
08/26/22 21:20
08/26/22 21:20
08/26/22 21:20
08/26/22 21:20
LABORATORY CONTROL SAMPLE:
3748501
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits Qualifiers
4,4'-DDD
ug/kg
8.4
10.3
122
40-160
4,4'-DDE
ug/kg
8.4
8.6
102
41-154
4,4'-DDT
ug/kg
8.4
5.4
64
34-163
Aldrin
ug/kg
8.4
6.0
72
39-144
alpha-BHC
ug/kg
8.4
6.1
73
36-145
beta-BHC
ug/kg
8.4
6.4
76
39-152
delta-BHC
ug/kg
8.4
6.9
82
41-147
Dieldrin
ug/kg
8.4
8.6
103
42-153
Endosulfan I
ug/kg
8.4
6.5
77
39-148
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/25/2022 02:36 PM without the written consent of Pace Analytical Services, LLC. Page 103 of 165

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: WASTE CHARACTERIZATION
Pace Project No.: 92621331
LABORATORY CONTROL SAMPLE:
Parameter
3748501
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
Endosulfan II
ug/kg
8.4
6.4
77
40-147
Endosulfan sulfate
ug/kg
8.4
6.6
79
40-148
Endrin
ug/kg
8.4
8.7
104
42-158
Endrin aldehyde
ug/kg
8.4
5.8
69
39-130
Endrin ketone
ug/kg
8.4
5.6
66
39-159
gamma-BHC (Lindane)
ug/kg
8.4
6.2
74
38-146
Heptachlor
ug/kg
8.4
5.9
70
39-144
Heptachlor epoxide
ug/kg
8.4
6.4
76
40-143
Hexachlorobenzene
ug/kg
8.4
5.8
69
33-139
Methoxychlor
ug/kg
25.2
12.0
48
32-146
Mirex
ug/kg
25.2
18.4
73
39-141
Decachlorobiphenyl (S)
%
85
10-146
Tetrachloro-m-xylene (S)
%
66
10-133
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3748546
MS
92621751001 Spike
Parameter Units Result Conc.
MSD
Spike
Conc.
3748547
MS
Result
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits
RPD Qual
4,4'-DDD
ug/kg
ND
9.2
9.1
8.6
9.3
94
103
10-160
8
4,4'-DDE
ug/kg
ND
9.2
9.1
5.8
6.0
63
66
10-170
4
4,4'-DDT
ug/kg
ND
9.2
9.1
5.6
5.5
62
60
10-194
3
Aldrin
ug/kg
ND
9.2
9.1
5.4
5.3
60
59
10-143
2
alpha-BHC
ug/kg
ND
9.2
9.1
5.7
5.4
62
59
10-144
5
beta-BHC
ug/kg
ND
9.2
9.1
5.7
5.7
62
63
10-152
0
delta-BHC
ug/kg
ND
9.2
9.1
6.2
6.4
68
71
10-147
3
Dieldrin
ug/kg
ND
9.2
9.1
7.7
7.9
84
87
10-181
3
Endosulfan I
ug/kg
ND
9.2
9.1
3.6
2.9
39
32
10-147
21
Endosulfan II
ug/kg
ND
9.2
9.1
5.7
5.9
62
65
11-149
4
Endosulfan sulfate
ug/kg
ND
9.2
9.1
8.5
7.3
93
80
10-153
16
Endrin
ug/kg
ND
9.2
9.1
8.1
8.1
88
89
10-160
0
Endrin aldehyde
ug/kg
ND
9.2
9.1
4.7
4.8
52
53
10-134
1
Endrin ketone
ug/kg
ND
9.2
9.1
5.7
5.9
62
65
11-155
3
gamma-BHC (Lindane)
ug/kg
ND
9.2
9.1
5.7
5.5
62
60
10-152
3
Heptachlor
ug/kg
ND
9.2
9.1
5.5
5.3
60
58
10-149
5
Heptachlor epoxide
ug/kg
ND
9.2
9.1
5.6
5.7
61
63
10-142
3
Hexachlorobenzene
ug/kg
ND
9.2
9.1
5.6
4.9
61
54
10-140
12
Methoxychlor
ug/kg
ND
27.5
27.2
29.7
37.6
108
138
10-147
24
Mirex
ug/kg
ND
27.5
27.2
17.8
18.5
65
68
11-139
4
Decachlorobiphenyl (S)
%
42
50
10-146
Tetrachloro-m-xylene (S)
%
51
50
10-133
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/25/2022 02:36 PM without the written consent of Pace Analytical Services, LLC.
Page 104 of 165

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: WASTE CHARACTERIZATION
Pace Project No.: 92621331
QC Batch: 720087 Analysis Method: EPA 8081 B
QC Batch Method: EPA 3546 Analysis Description: 8081 GCS Pesticides
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92621331004, 92621331005
METHOD BLANK: 3752578
Associated Lab Samples: 92621331004, 92621331005
Parameter Units
Matrix:
Blank
Result
Solid
Reporting
Limit
Analyzed
4,4'-DDD
ug/kg
ND
2.0
08/29/22 15:53
4,4'-DDE
ug/kg
ND
2.0
08/29/22 15:53
4,4'-DDT
ug/kg
ND
2.0
08/29/22 15:53
Aldrin
ug/kg
ND
2.0
08/29/22 15:53
alpha-BHC
ug/kg
ND
2.0
08/29/22 15:53
beta-BHC
ug/kg
ND
2.0
08/29/22 15:53
Chlordane (Technical)
ug/kg
ND
9.9
08/29/22 15:53
delta-BHC
ug/kg
ND
2.0
08/29/22 15:53
Dieldrin
ug/kg
ND
k 2.0
08/29/22 15:53
Endosulfan I
ug/kg
ND
2.0
08/29/22 15:53
Endosulfan II
ug/kg
ND
2.0
08/29/22 15:53
Endosulfan sulfate
ug/kg
ND
2.0
08/29/22 15:53
Endrin
ug/kg
ND
2.0
08/29/22 15:53
Endrin aldehyde
ug/kg
ND
2.0
08/29/22 15:53
Endrin ketone
ug/kg
ND
14 2.0
08/29/22 15:53
gamma-BHC (Lindane)
ug/kg
ND
2.0
08/29/22 15:53
Heptachlor
ug/kg
ND
2.0
08/29/22 15:53
Heptachlor epoxide
ug/kg
ND
2.0
08/29/22 15:53
Hexachlorobenzene
ug/kg
ND
2.0
08/29/22 15:53
Methoxychlor
ug/kg
ND
5.0
08/29/22 15:53
Mirex
ug/kg
ND
5.0
08/29/22 15:53
Toxaphene
ug/kg
ND
6.9
08/29/22 15:53
Decachlorobiphenyl (S)
%
81
10-146
08/29/22 15:53
Tetrachloro-m-xylene (S)
%
63
10-133
08/29/22 15:53
LABORATORY CONTROL SAMPLE: 3752579
Qualifiers
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits Qualifiers
4,4'-DDD
ug/kg
8.3
9.0
108
40-160
4,4'-DDE
ug/kg
8.3
8.8
106
41-154
4,4'-DDT
ug/kg
8.3
8.9
107
34-163
Aldrin
ug/kg
8.3
5.9
71
39-144
alpha-BHC
ug/kg
8.3
6.1
73
36-145
beta-BHC
ug/kg
8.3
6.3
76
39-152
delta-BHC
ug/kg
8.3
6.9
83
41-147
Dieldrin
ug/kg
8.3
8.7
104
42-153
Endosulfan I
ug/kg
8.3
6.7
80
39-148
Endosulfan II
ug/kg
8.3
6.8
81
40-147
Endosulfan sulfate
ug/kg
8.3
7.2
86
40-148
Results presented on
this page are in the units
indicated by the "Units"
column except
where an alternate unit
is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/25/2022 02:36 PM without the written consent of Pace Analytical Services, LLC.
Page 105 of 165

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: WASTE CHARACTERIZATION
Pace Project No.: 92621331
LABORATORY CONTROL SAMPLE:
Parameter
3752579
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
Endrin
ug/kg
8.3
9.1
109
42-158
Endrin aldehyde
ug/kg
8.3
6.9
82
39-130
Endrin ketone
ug/kg
8.3
6.5
78
39-159
gamma-BHC (Lindane)
ug/kg
8.3
6.2
75
38-146
Heptachlor
ug/kg
8.3
6.3
76
39-144
Heptachlor epoxide
ug/kg
8.3
6.4
77
40-143
Hexachlorobenzene
ug/kg
8.3
5.8
70
33-139
Methoxychlor
ug/kg
25
20.1
80
32-146
Mirex
ug/kg
25
19.1
76
39-141
Decachlorobiphenyl (S)
%
79
10-146
Tetrachloro-m-xylene (S)
%
65
10-133
SAMPLE DUPLICATE: 3752581
Parameter
Units
92621331005 Dup
Result Result
RPD Qualifiers
4,4'-DDD
ug/kg
ND
ND
4,4'-DDE
ug/kg
ND
ND
4,4'-DDT
ug/kg
ND
ND
Aldrin
ug/kg
ND
ND
alpha-BHC
ug/kg
ND
ND
beta-BHC
ug/kg
ND
ND
Chlordane (Technical)
ug/kg
694
790 13
delta-BHC
ug/kg
ND
ND
Dieldrin
ug/kg
ND
ND
Endosulfan I
ug/kg
ND
ND
Endosulfan II
ug/kg
ND
ND
Endosulfan sulfate
ug/kg
ND
ND
Endrin
ug/kg
ND
ND
Endrin aldehyde
ug/kg
ND
ND
Endrin ketone
ug/kg
ND
ND
gamma-BHC (Lindane)
ug/kg
ND
ND
Heptachlor
ug/kg
ND
ND
Heptachlor epoxide
ug/kg
ND
ND
Hexachlorobenzene
ug/kg
ND
ND
Methoxychlor
ug/kg
ND
ND
Mirex
ug/kg
ND
ND
Toxaphene
ug/kg
ND
ND
Decachlorobiphenyl (S)
%
0
0 S4
Tetrachloro-m-xylene (S)
%
0
0 D3,S4
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/25/2022 02:36 PM without the written consent of Pace Analytical Services, LLC.
Page 106 of 165

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: WASTE CHARACTERIZATION
Pace Project No.: 92621331
QC Batch: 718460 Analysis Method: EPA 8082A
QC Batch Method: EPA 3546 Analysis Description: 8082 GCS PCB
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92621331001, 92621331002, 92621331003, 92621331004, 92621331005, 92621331006, 92621331007,
92621331008,92621331009,92621331010
METHOD BLANK: 3745227
Matrix:
Solid
Associated Lab Samples:
92621331001, 92621331002, 92621331003, 92621331004, 92621331005,
92621331006, 92621331007,
92621331008,92621331009,92621331010
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
PCB-1016 (Aroclor 1016)
ug/kg
ND
33.2
08/23/22 14:45
PCB-1221 (Aroclor 1221)
ug/kg
ND
33.2
08/23/22 14:45
PCB-1232 (Aroclor 1232)
ug/kg
ND
33.2
08/23/22 14:45
PCB-1242 (Aroclor 1242)
ug/kg
ND
33.2
08/23/22 14:45
PCB-1248 (Aroclor 1248)
ug/kg
ND
33.2
08/23/22 14:45
PCB-1254 (Aroclor 1254)
ug/kg
ND
33.2
08/23/22 14:45
PCB-1260 (Aroclor 1260)
ug/kg
ND
33.2
08/23/22 14:45
Decachlorobiphenyl (S)
%
99
10-160
08/23/22 14:45
LABORATORY CONTROL SAMPLE:
3745228
Spike
LCS LCS % Rec
Parameter
Units
Conc.
Result % Rec Limits Qualifiers
PCB-1016 (Aroclor 1016)
ug/kg
164
140 85 34-143
PCB-1260 (Aroclor 1260)
ug/kg
164
146 89 31-146
Decachlorobiphenyl (S)
%
98 10-160
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
3745229
3745230
MS
MSD
92621463001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits RPD Qual
PCB-1016 (Aroclor 1016)
ug/kg
ND
1660
1650
2740
1540
165
93
10-184 56 R1
PCB-1260 (Aroclor 1260)
ug/kg
ND
1660
1650
1140
795
69
48
10-151 36 R1
Decachlorobiphenyl (S)
%
56
47
10-160
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/25/2022 02:36 PM without the written consent of Pace Analytical Services, LLC.
Page 107 of 165

laneAnalytical
www,pacelabs.com
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Project: WASTE CHARACTERIZATION
Pace Project No.: 92621331
QC Batch: 719449
QC Batch Method: EPA 3546
Associated Lab Samples: 92621331008, 92621331009
QUALITY CONTROL DATA
Analysis Method: EPA 8270E
Analysis Description: 8270E Solid MSSV Microwave
Laboratory: Pace Analytical Services - Charlotte
METHOD BLANK: 3749839
Associated Lab Samples: 92621331008, 92621331009
Parameter Units
Matrix: Solid
Blank Reporting
Result Limit
Analyzed
1,2,4,5-Tetrachlorobenzene
ug/kg
ND
325
08/26/22 11:08
1,2,4-Trichlorobenzene
ug/kg
ND
325
08/26/22 11:08
1,2-Dichlorobenzene
ug/kg
ND
325
08/26/22 11:08
1,2-Diphenylhydrazine
ug/kg
ND
325
08/26/22 11:08
1,3,5-Trinitrobenzene
ug/kg
ND
325
08/26/22 11:08
1,3-Dichlorobenzene
ug/kg
ND
325
08/26/22 11:08
1,3-Dinitrobenzene
ug/kg
ND
325
08/26/22 11:08
1,4-Dichlorobenzene
ug/kg
ND
325
08/26/22 11:08
1,4-Dinitrobenzene
ug/kg
ND
325
08/26/22 11:08
1,4-Naphthoquinone
ug/kg
ND
1620
08/26/22 11:08
1-Methyl naphthalene
ug/kg
ND
325
08/26/22 11:08
1-Naphthalenamine
ug/kg
ND
649
08/26/22 11:08
2,2'-Oxybis(1-chloropropane)
ug/kg
ND
325
08/26/22 11:08
2,3,4,6-Tetrachlorophenol
ug/kg
ND
325
08/26/22 11:08
2,3-Dibromo-1-propanol phosph
ug/kg
ND
1620
08/26/22 11:08
2,3-Dichloroaniline
ug/kg
ND
325
08/26/22 11:08
2,4,5-Trichlorophenol
ug/kg
ND
325
08/26/22 11:08
2,4,6-Trichlorophenol
ug/kg
ND
325
08/26/22 11:08
2,4-Dichlorophenol
ug/kg
ND
325
08/26/22 11:08
2,4-Dimethyl phenol
ug/kg
ND
325
08/26/22 11:08
2,4-Dinitrophenol
ug/kg
ND
1620
08/26/22 11:08
2,4-Dinitrotoluene
ug/kg
ND
325
08/26/22 11:08
2,6-Dichlorophenol
ug/kg
ND
325
08/26/22 11:08
2,6-Dinitrotoluene
ug/kg
ND
325
08/26/22 11:08
2-Acetylaminofluorene
ug/kg
ND
649
08/26/22 11:08
2-Chloronaphthalene
ug/kg
ND
325
08/26/22 11:08
2-Chlorophenol
ug/kg
ND
325
08/26/22 11:08
2-Methyl-5-nitroaniline
ug/kg
ND
325
08/26/22 11:08
2-Methyl naphthalene
ug/kg
ND
325
08/26/22 11:08
2-Methylphenol (o-Cresol)
ug/kg
ND
325
08/26/22 11:08
2-Naphthalenamine
ug/kg
ND
649
08/26/22 11:08
2-Nitroaniline
ug/kg
ND
1620
08/26/22 11:08
2-Nitrophenol
ug/kg
ND
325
08/26/22 11:08
2-Picoline
ug/kg
ND
325
08/26/22 11:08
3&4-Methylphenol(m&p Cresol)
ug/kg
ND
325
08/26/22 11:08
3,3'-Dichlorobenzidine
ug/kg
ND
649
08/26/22 11:08
3,3'-Dimethylbenzidine
ug/kg
ND
649
08/26/22 11:08
3-Methylcholanthrene
ug/kg
ND
325
08/26/22 11:08
3-Nitroaniline
ug/kg
ND
1620
08/26/22 11:08
4,4'-Methylene-bis(2-chloroani
ug/kg
ND
649
08/26/22 11:08
IL
IH
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/25/2022 02:36 PM without the written consent of Pace Analytical Services, LLC. Page 108 of 165

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: WASTE CHARACTERIZATION
Pace Project No.: 92621331
METHOD BLANK: 3749839
Associated Lab Samples: 92621331008, 92621331009
Parameter Units
Matrix:
Blank
Result
Solid
Reporting
Limit
Analyzed
4,6-Dinitro-2-methyl phenol
ug/kg
ND
649
08/26/22 11:08
4-Aminobiphenyl
ug/kg
ND
325
08/26/22 11:08
4-Chlorophenylphenyl ether
ug/kg
ND
325
08/26/22 11:08
4-Nitroaniline
ug/kg
ND
649
08/26/22 11:08
4-Nitrophenol
ug/kg
ND
1620
08/26/22 11:08
4-Nitroquinoline-n-oxide
ug/kg
ND
1620
08/26/22 11:08 v2
5-Nitro-o-toluidine
ug/kg
ND
325
08/26/22 11:08
7,12-Dimethylbenz(a)anthracene
ug/kg
ND
325
08/26/22 11:08
a,a-Dimethylphenylethylamine
ug/kg
ND
1620
08/26/22 11:08
Acenaphthene
ug/kg
ND
325
08/26/22 11:08
Acenaphthylene
ug/kg
ND
325
08/26/22 11:08
Acetophenone
ug/kg
ND
325
08/26/22 11:08
Anthracene
ug/kg
ND
325
08/26/22 11:08
Benzo(a)anthracene
ug/kg
ND
325
08/26/22 11:08
Benzo(a)pyrene
ug/kg
ND
325
08/26/22 11:08
Benzo(b)fluoranthene
ug/kg
ND
325
08/26/22 11:08
Benzo(g,h,i)perylene
ug/kg
ND
325
08/26/22 11:08
Benzo(k)fluoranthene
ug/kg
ND
325
08/26/22 11:08
Benzyl alcohol
ug/kg
ND
649
08/26/22 11:08
bis(2-Chloroethoxy)methane
ug/kg
ND
325
08/26/22 11:08
bis(2-Chloroethyl) ether
ug/kg
ND
325
08/26/22 11:08
bis(2-Ethylhexyl)phthalate
ug/kg
ND
325
08/26/22 11:08
Chrysene
ug/kg
ND
325
08/26/22 11:08
Di-n-butylphthalate
ug/kg
ND
325
08/26/22 11:08
Di-n-octylphthalate
ug/kg
ND
325
08/26/22 11:08
Diallate
ug/kg
ND
325
08/26/22 11:08
Dibenz(a,h)anthracene
ug/kg
ND
325
08/26/22 11:08
Dibenzo(a,e)pyrene
ug/kg
ND
984
08/26/22 11:08
Dibenzofuran
ug/kg
ND
325
08/26/22 11:08
Diethylphthalate
ug/kg
ND
325
08/26/22 11:08
Dimethoate
ug/kg
ND
649
08/26/22 11:08
Dimethylphthalate
ug/kg
ND
325
08/26/22 11:08
Dinoseb
ug/kg
ND
649
08/26/22 11:08
Diphenyl ether (Phenyl ether)
ug/kg
ND
492
08/26/22 11:08
Diphenylamine
ug/kg
ND
325
08/26/22 11:08
Disulfoton
ug/kg
ND
325
08/26/22 11:08
Ethyl methanesulfonate
ug/kg
ND
649
08/26/22 11:08
Famphur
ug/kg
ND
649
08/26/22 11:08 IH
Fluoranthene
ug/kg
ND
325
08/26/22 11:08
Fluorene
ug/kg
ND
325
08/26/22 11:08
Hexachloro-1,3-butadiene
ug/kg
ND
325
08/26/22 11:08
Hexachlorobenzene
ug/kg
ND
325
08/26/22 11:08
Hexachlorocyclopentadiene
ug/kg
ND
325
08/26/22 11:08
Hexachloroethane
ug/kg
ND
325
08/26/22 11:08
Hexachlorophene
ug/kg
ND
3250
08/26/22 11:08 IH
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/25/2022 02:36 PM without the written consent of Pace Analytical Services, LLC. Page 109 of 165

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: WASTE CHARACTERIZATION
Pace Project No.: 92621331
METHOD BLANK: 3749839
Associated Lab Samples: 92621331008, 92621331009
Parameter Units
Matrix:
Blank
Result
Solid
Reporting
Limit
Analyzed
Hexachloropropene
ug/kg
ND
325
08/26/22 11:08
Indeno(1,2,3-cd)pyrene
ug/kg
ND
325
08/26/22 11:08
Isodrin
ug/kg
ND
325
08/26/22 11:08
Isophorone
ug/kg
ND
325
08/26/22 11:08
Isosafrole
ug/kg
ND
325
08/26/22 11:08
Kepone
ug/kg
ND
649
08/26/22 11:08
Methapyrilene
ug/kg
ND
1620
08/26/22 11:08
Methyl methanesulfonate
ug/kg
ND
649
08/26/22 11:08
Methyl parathion
ug/kg
ND
325
08/26/22 11:08
n-Decane
ug/kg
ND
325
08/26/22 11:08
N-Nitroso-di-n-butylamine
ug/kg
ND
325
08/26/22 11:08
N-Nitroso-di-n-propylamine
ug/kg
ND
325
08/26/22 11:08
N-Nitrosodiethylamine
ug/kg
ND
325
08/26/22 11:08
N-Nitrosodimethylamine
ug/kg
ND
325
08/26/22 11:08
N-Nitrosodiphenylamine
ug/kg
ND
325
08/26/22 11:08
N-Nitrosomethylethylamine
ug/kg
ND
325
08/26/22 11:08
N-Nitrosomorpholine
ug/kg
ND
325
08/26/22 11:08
N-Nitrosopiperidine
ug/kg
ND
649
08/26/22 11:08
N-Nitrosopyrrolidine
ug/kg
ND
649
08/26/22 11:08
n-Octadecane
ug/kg
ND
325
08/26/22 11:08
Naphthalene
ug/kg
ND
325
08/26/22 11:08
Nitrobenzene
ug/kg
ND
325
08/26/22 11:08
O,O,O-Triethylphosphorothioate
ug/kg
ND
325
08/26/22 11:08
O-Toluidine
ug/kg
ND
325
08/26/22 11:08
P-Dimethylaminoazobenzene
ug/kg
ND
325
08/26/22 11:08
p-Phenylenediamine
ug/kg
ND
649
08/26/22 11:08
Parathion (Ethyl parathion)
ug/kg
ND
325
08/26/22 11:08
Pentachlorobenzene
ug/kg
ND
325
08/26/22 11:08
Pentachloroethane
ug/kg
ND
325
08/26/22 11:08
Pentachloronitrobenzene
ug/kg
ND
325
08/26/22 11:08
Pentachlorophenol
ug/kg
ND
649
08/26/22 11:08
Phenacetin
ug/kg
ND
649
08/26/22 11:08
Phenanthrene
ug/kg
ND
325
08/26/22 11:08
Phenol
ug/kg
ND
325
08/26/22 11:08
Phorate
ug/kg
ND
325
08/26/22 11:08
Phthalic anhydride
ug/kg
ND
2460
08/26/22 11:08
Pronamide
ug/kg
ND
649
08/26/22 11:08
Pyrene
ug/kg
ND
325
08/26/22 11:08
Pyridine
ug/kg
ND
325
08/26/22 11:08
Safrole
ug/kg
ND
649
08/26/22 11:08
Sulfotepp (ThiodiphosphoricAc
ug/kg
ND
325
08/26/22 11:08
Terpineol
ug/kg
ND
325
08/26/22 11:08
Thionazin
ug/kg
ND
325
08/26/22 11:08
2,4,6-Tribromophenol (S)
%
64
18-130
08/26/22 11:08
2-Fluorobiphenyl (S)
%
53
19-130
08/26/22 11:08
v1
IL
IL
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/25/2022 02:36 PM without the written consent of Pace Analytical Services, LLC. Page 110 of 165

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: WASTE CHARACTERIZATION
Pace Project No.: 92621331
METHOD BLANK: 3749839
Matrix:
Solid
Associated Lab Samples:
92621331008, 92621331009
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
2-Fluorophenol(S)
%
52
18-130
08/26/22 11:08
Nitrobenzene-d5 (S)
%
52
21-130
08/26/22 11:08
Phenol-d6 (S)
%
52
18-130
08/26/22 11:08
Terphenyl-d14 (S)
%
84
15-130
08/26/22 11:08
LABORATORY CONTROL SAMPLE:
Parameter
3749840
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
1,2,4,5-Tetrachlorobenzene
ug/kg
1640
1250
76
56-130
1,2,4-Trichlorobenzene
ug/kg
1640
1110
67
47-130
1,2-Dichlorobenzene
ug/kg
1640
991
60
49-130
1,2-Diphenylhydrazine
ug/kg
1640
1280
78
34-171
1,3,5-Trinitrobenzene
ug/kg
1640
1290
79
46-143
1,3-Dichlorobenzene
ug/kg
1640
972
59
48-130
1,3-Dinitrobenzene
ug/kg
1640
1270
77
66-130
1,4-Dichlorobenzene
ug/kg
1640
966
59
49-130
1,4-Dinitrobenzene
ug/kg
1640
1310
80
63-130
1,4-Naphthoquinone
ug/kg
1640
1040J
63
10-137
1-Methylnaphthalene
ug/kg
1640
1120
68
54-130
1-Naphthalenamine
ug/kg
1640
1110
67
45-130
2,2'-Oxybis(1-chloropropane)
ug/kg
1640
1070
65
38-130
2,3,4,6-Tetrachlorophenol
ug/kg
1640
1150
70
51-133
2,3-Dibromo-1-propanol phosph
ug/kg
6580
2710
41
10-160 IL
2,3-Dichloroaniline
ug/kg
1640
1130
68
46-145
2,4,5-Trichlorophenol
ug/kg
1640
1180
71
49-130
2,4,6-Trichlorophenol
ug/kg
1640
1170
71
50-130
2,4-Dichlorophenol
ug/kg
1640
1160
71
51-130
2,4-Dimethylphenol
ug/kg
1640
1300
79
53-130
2,4-Dinitrophenol
ug/kg
8220
5300
64
39-130
2,4-Dinitrotoluene
ug/kg
1640
1240
76
53-130
2,6-Dichlorophenol
ug/kg
1640
1390
85
55-130
2,6-Dinitrotoluene
ug/kg
1640
1230
75
55-130
2-Acetylaminofluorene
ug/kg
1640
1280
78
38-130
2-Chloronaphthalene
ug/kg
1640
1130
69
48-130
2-Chlorophenol
ug/kg
1640
1040
63
54-130
2-Methyl-5-nitroaniline
ug/kg
1640
1260
77
52-130
2-Methylnaphthalene
ug/kg
1640
1090
66
57-130
2-Methylphenol(o-Cresol)
ug/kg
1640
1040
63
50-130
2-Naphthalenamine
ug/kg
1640
963
59
25-130
2-Nitroaniline
ug/kg
3290
2480
75
49-130
2-Nitrophenol
ug/kg
1640
1100
67
50-130
2-Picoline
ug/kg
1640
978
59
10-130
3&4-Methyl phenol (m&p Cresol)
ug/kg
1640
1140
70
50-130
3,3'-Dichlorobenzidine
ug/kg
3290
2210
67
47-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/25/2022 02:36 PM without the written consent of Pace Analytical Services, LLC. Page 111 of 165

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: WASTE CHARACTERIZATION
Pace Project No.: 92621331
LABORATORY CONTROL SAMPLE:
Parameter
3749840
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
3,3'-Dimethylbenzidine
ug/kg
3290
3450
105
10-1301H
3-Methylcholanthrene
ug/kg
1640
1150
70
68-175
3-Nitroaniline
ug/kg
3290
2330
71
45-130
4,4'-Methylene-bis(2-chloroani
ug/kg
3290
2470
75
20-130
4,6-Dinitro-2-methyl phenol
ug/kg
3290
2400
73
50-142
4-Aminobiphenyl
ug/kg
1640
806
49
10-130
4-Chlorophenylphenyl ether
ug/kg
1640
1230
75
53-130
4-Nitroaniline
ug/kg
3290
2230
68
51-130
4-Nitrophenol
ug/kg
8220
6630
81
40-130
4-Nitroquinoline-n-oxide
ug/kg
3290
1290J
39
30-130 v3
5-Nitro-o-toluidine
ug/kg
1640
1260
77
35-130
7,12-Dimethylbenz(a)anthracene
ug/kg
1640
1110
67
62-130
a,a-Dimethylphenylethylamine
ug/kg
1640
447J
27
10-160
Acenaphthene
ug/kg
1640
1180
72
56-130
Acenaphthylene
ug/kg
1640
1250
76
58-130
Acetophenone
ug/kg
1640
1060
64
54-130
Anthracene
ug/kg
1640
1120
68
60-130
Benzo(a)anthracene
ug/kg
1640
1290
78
59-130
Benzo(a)pyrene
ug/kg
1640
1600
97
57-130
Benzo(b)fluoranthene
ug/kg
1640
1580
96
54-130
Benzo(g,h,i)perylene
ug/kg
1640
1340
81
59-130
Benzo(k)fluoranthene
ug/kg
1640
1440
88
54-130
Benzyl alcohol
ug/kg
3290
2140
65
50-130
bis(2-Chloroethoxy)methane
ug/kg
1640
1050
64
55-130
bis(2-Chloroethyl) ether
ug/kg
1640
976
59
53-130
bis(2-Ethylhexyl)phthalate
ug/kg
1640
1300
79
58-130
Chrysene
ug/kg
1640
1260
77
57-130
Di-n-butylphthalate
ug/kg
1640
1220
74
57-130
Di-n-octylphthalate
ug/kg
1640
1370
84
57-130
Diallate
ug/kg
1640
1190
72
48-130
Dibenz(a,h)anthracene
ug/kg
1640
1280
78
60-130
Dibenzo(a,e)pyrene
ug/kg
1640
1460
89
49-130
Dibenzofuran
ug/kg
1640
1250
76
54-130
Diethylphthalate
ug/kg
1640
1200
73
55-130
Dimethoate
ug/kg
1640
1380
84
67-133
Dimethylphthalate
ug/kg
1640
1190
73
57-130
Dinoseb
ug/kg
1640
1390
85
30-139
Diphenyl ether (Phenyl ether)
ug/kg
1640
1090
66
50-150
Diphenylamine
ug/kg
1640
1180
71
58-130
Disulfoton
ug/kg
1640
1130
69
55-139
Ethyl methanesulfonate
ug/kg
1640
1100
67
39-144
Famphur
ug/kg
3290
510J
15
10-200 IH
Fluoranthene
ug/kg
1640
1260
77
57-130
Fluorene
ug/kg
1640
1180
72
56-130
Hexachloro-1,3-butadiene
ug/kg
1640
1070
65
41-130
Hexachlorobenzene
ug/kg
1640
1240
76
53-130
Hexachlorocyclopentadiene
ug/kg
1640
1030
63
23-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/25/2022 02:36 PM without the written consent of Pace Analytical Services, LLC. Page 112 of 165

Pace Analytical Services, LLC
9800
lCtaac,Analyfical ® Kiney Ave. Suite 100
Huntersville, NC 28078
0788
www.pacelabs.com [phone]
QUALITY CONTROL DATA
Project: WASTE CHARACTERIZATION
Pace Project No.: 92621331
LABORATORY CONTROL SAMPLE:
Parameter
3749840
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
Hexachloroethane
ug/kg
1640
935
57
48-130
Hexachlorophene
ug/kg
16400
9380
57
10-131 IH
Hexachloropropene
ug/kg
1640
1200
73
29-130
Indeno(1,2,3-cd)pyrene
ug/kg
1640
1330
81
61-130
Isodrin
ug/kg
1640
1360
83
66-130
Isophorone
ug/kg
1640
1060
64
49-130
Isosafrole
ug/kg
1640
1100
67
33-130
Kepone
ug/kg
3290
1040
32
10-147 v1
Methapyrilene
ug/kg
1640
400J
24
10-130
Methyl methanesulfonate
ug/kg
1640
1290
79
23-138
Methyl parathion
ug/kg
1640
1460
89
57-130
n-Decane
ug/kg
1640
958
58
25-130
N-Nitroso-di-n-butylamine
ug/kg
1640
1290
79
19-130
N-Nitroso-di-n-propylamine
ug/kg
1640
1080
66
52-130
N-Nitrosodiethylamine
ug/kg
1640
1070
65
22-130
N-Nitrosodimethylamine
ug/kg
1640
924
56
45-130
N-Nitrosodiphenylamine
ug/kg
1640
1180
71
56-130
N-Nitrosomethylethylamine
ug/kg
1640
1030
62
16-130
N-Nitrosomorpholine
ug/kg
1640
1270
77
26-130
N-Nitrosopiperidine
ug/kg
1640
1190
72
37-130
N-Nitrosopyrrolidine
ug/kg
1640
1070
65
33-130
n-Octadecane
ug/kg
1640
1200
73
43-130
Naphthalene
ug/kg
1640
1080
66
56-130
Nitrobenzene
ug/kg
1640
1110
67
50-130
O,O,O-Triethylphosphorothioate
ug/kg
1640
1200
73
29-175
O-Toluidine
ug/kg
1640
1050
64
41-130
P-Dimethylaminoazobenzene
ug/kg
1640
676
41
14-130 IL
p-Phenylenediamine
ug/kg
ND
IL
Parathion (Ethyl parathion)
ug/kg
1640
1330
81
61-130
Pentachlorobenzene
ug/kg
1640
1320
80
57-130
Pentachloroethane
ug/kg
1640
1080
66
35-141
Pentachloronitrobenzene
ug/kg
1640
1760
107
67-130
Pentachlorophenol
ug/kg
3290
2780
84
33-130
Phenacetin
ug/kg
1640
1290
79
64-130
Phenanthrene
ug/kg
1640
1240
75
60-130
Phenol
ug/kg
1640
1050
64
54-130
Phorate
ug/kg
1640
1220
74
59-130
Phthalic anhydride
ug/kg
ND
Pronamide
ug/kg
1640
1400
85
68-130
Pyrene
ug/kg
1640
1330
81
61-130
Pyridine
ug/kg
1640
761
46
35-130
Safrole
ug/kg
1640
1200
73
57-130
Sulfotepp (ThiodiphosphoricAc
ug/kg
1640
1420
86
10-160
Terpineol
ug/kg
1640
1840
112
39-130
Thionazin
ug/kg
1640
1270
77
43-146
2,4,6-Tribromophenol (S)
%
80
18-130
2-Fluorobiphenyl (S)
%
64
19-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/25/2022 02:36 PM without the written consent of Pace Analytical Services, LLC. Page 113 of 165

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: WASTE CHARACTERIZATION
Pace Project No.: 92621331
LABORATORY CONTROL SAMPLE:
3749840
Spike LCS
LCS
% Rec
Parameter
Units Conc. Result
% Rec
Limits
2-Fluorophenol(S)
%
61
18-130
Nitrobenzene-d5 (S)
%
61
21-130
Phenol-d6 (S)
%
62
18-130
Terphenyl-d14 (S)
%
79
15-130
Qualifiers
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3749841
MS
92621241006 Spike
Parameter Units Result Conc.
MSD
Spike
Conc.
3749842
MS
Result
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits
RPD Qual
1,2,4,5-Tetrachlorobenzene
ug/kg
ND
1810
1810
1870
1700
103
94
16-130
9
1,2,4-Trichlorobenzene
ug/kg
ND
1810
1810
1610
1440
89
79
22-130
11
1,2-Dichlorobenzene
ug/kg
ND
1810
1810
1420
1260
78
70
23-130
12
1,2-Diphenylhydrazine
ug/kg
ND
1810
1810
1850
1810
102
100
23-130
2
1,3,5-Trinitrobenzene
ug/kg
ND
1810
1810
1870
1860
103
102
70-130
1
1,3-Dichlorobenzene
ug/kg
ND
1810
1810
1410
1210
78
67
26-130
15
1,3-Dinitrobenzene
ug/kg
ND
1810
1810
1790
1820
99
100
70-130
1
1,4-Dichlorobenzene
ug/kg
ND
1810
1810
1400
1220
77
68
27-130
14
1,4-Dinitrobenzene
ug/kg
ND
1810
1810
1830
1810
101
100
10-139
1
1,4-Naphthoquinone
ug/kg
ND
1810
1810
1570J
1530J
87
85
70-130
1-Methylnaphthalene
ug/kg
ND
1810
1810
1580
1460
87
80
30-130
8
1-Naphthalenamine
ug/kg
ND
1810
1810
869
821
48
45
70-130
6 M1
2,2'-Oxybis(1-chloropropane)
ug/kg
ND
1810
1810
1520
1360
84
75
30-130
11
2,3,4,6-Tetrachlorophenol
ug/kg
ND
1810
1810
1560
1570
86
87
10-200
0
2,3-Dibromo-1-propanol
ug/kg
ND
7250
7250
4260
3560
59
49
10-194
18IL
phosph
2,3-Dichloroaniline
ug/kg
0.01
1810
1810
1630
1560
90
86
70-130
5
2,4,5-Trichlorophenol
ug/kg
ND
1810
1810
1710
1670
95
92
26-130
3
2,4,6-Trichlorophenol
ug/kg
ND
1810
1810
1720
1640
95
91
23-130
5
2,4-Dichlorophenol
ug/kg
ND
1810
1810
1660
1530
92
85
29-130
8
2,4-Dimethylphenol
ug/kg
ND
1810
1810
1720
1610
95
89
13-130
6
2,4-Dinitrophenol
ug/kg
ND
9060
9060
4760
4890
53
54
10-131
3
2,4-Dinitrotoluene
ug/kg
ND
1810
1810
1750
1720
97
95
28-130
2
2,6-Dichlorophenol
ug/kg
ND
1810
1810
1900
1800
105
99
10-150
5
2,6-Dinitrotoluene
ug/kg
ND
1810
1810
1830
1760
101
97
36-130
4
2-Acetylaminofluorene
ug/kg
ND
1810
1810
1850
1820
102
101
10-130
2
2-Chloronaphthalene
ug/kg
ND
1810
1810
1650
1510
91
84
27-130
9
2-Chlorophenol
ug/kg
ND
1810
1810
1460
1310
81
72
29-130
11
2-Methyl-5-nitroaniline
ug/kg
ND
1810
1810
1670
1720
92
95
70-130
3
2-Methylnaphthalene
ug/kg
ND
1810
1810
1530
1420
84
78
29-130
8
2-Methylphenol(o-Cresol)
ug/kg
ND
1810
1810
1430
1340
79
74
20-130
6
2-Naphthalenamine
ug/kg
ND
1810
1810
495J
485J
27
27
70-130
M1
2-Nitroaniline
ug/kg
ND
3620
3620
3520
3440
97
95
29-130
2
2-Nitrophenol
ug/kg
ND
1810
1810
1560
1390
86
77
26-130
11
2-Picoline
ug/kg
ND
1810
1810
1410
1260
78
70
70-130
11
3&4-Methyl phenol (m&p
ug/kg
ND
1810
1810
1580
1500
87
83
10-176
5
Cresol)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/25/2022 02:36 PM without the written consent of Pace Analytical Services, LLC.
Page 114 of 165

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: WASTE CHARACTERIZATION
Pace Project No.: 92621331
MATRIX SPIKE & MATRIX SPIKE
DUPLICATE:
3749841
3749842
MS
MSD
92621241006
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
3,3'-Dichlorobenzidine
ug/kg
ND
3620
3620
3070
2750
85
76
15-130
11
3,3'-Dimethylbenzidine
ug/kg
ND
3620
3620
3030
1970
84
54
70-130
431H,M1,R1
3-Methylcholanthrene
ug/kg
ND
1810
1810
1480
1410
81
78
10-183
5
3-Nitroaniline
ug/kg
ND
3620
3620
3090
3100
85
86
28-130
0
4,4'-Methylene-bis(2-chloroani
ug/kg
ND
3620
3620
3520
3140
97
87
10-130
11
4,6-Dinitro-2-methyl phenol
ug/kg
ND
3620
3620
3450
3310
95
91
15-132
4
4-Aminobiphenyl
ug/kg
ND
1810
1810
896
793
49
44
70-130
12 M1
4-Chlorophenylphenyl ether
ug/kg
ND
1810
1810
1800
1710
99
94
32-130
5
4-Nitroaniline
ug/kg
ND
3620
3620
3000
2990
83
82
30-130
0
4-Nitrophenol
ug/kg
ND
9060
9060
8910
9030
98
100
17-130
1
4-Nitroquinoline-n-oxide
ug/kg
ND
3620
3620
2150
1970
59
54
70-130
9 M1,v3
5-Nitro-o-toluidine
ug/kg
ND
1810
1810
1670
1720
92
95
10-130
3
7,12-
ug/kg
ND
1810
1810
1510
1530
83
84
70-130
1
Dimethylbenz(a)anthracene
a,a-Dimethylphenylethylamine
ug/kg
ND
1810
1810
354J
474J
20
26
70-130
M1
Acenaphthene
ug/kg
ND
1810
1810
1650
1570
91
87
29-130
5
Acenaphthylene
ug/kg
ND
1810
1810
1740
1650
96
91
31-130
5
Acetophenone
ug/kg
ND
1810
1810
1530
1410
85
78
31-130
8
Anthracene
ug/kg
ND
1810
1810
1590
1520
88
84
33-130
5
Benzo(a)anthracene
ug/kg
ND
1810
1810
1780
1690
98
93
32-130
6
Benzo(a)pyrene
ug/kg
ND
1810
1810
2340
2240
129
124
32-130
4
Benzo(b)fluoranthene
ug/kg
ND
1810
1810
2190
2120
121
117
33-130
3
Benzo(g,h,i)perylene
ug/kg
ND
1810
1810
2100
1890
116
105
28-130
10
Benzo(k)fluoranthene
ug/kg
ND
1810
1810
2000
1940
110
107
31-130
3
Benzyl alcohol
ug/kg
ND
3620
3620
3000
2780
83
77
31-130
7
bis(2-Chloroethoxy)methane
ug/kg
ND
1810
1810
1490
1290
82
71
30-130
14
bis(2-Chloroethyl) ether
ug/kg
ND
1810
1810
1390
1240
77
69
68-130
11
bis(2-Ethylhexyl)phthalate
ug/kg
ND
1810
1810
1810
1730
100
95
40-130
5
Chrysene
ug/kg
ND
1810
1810
1820
1690
101
94
30-130
7
Di-n-butylphthalate
ug/kg
ND
1810
1810
1700
1610
94
89
41-130
5
Di-n-octylphthalate
ug/kg
ND
1810
1810
1690
1710
93
94
42-130
1
Diallate
ug/kg
ND
1810
1810
1780
1690
98
93
70-130
5
Dibenz(a,h)anthracene
ug/kg
ND
1810
1810
2050
1920
113
106
27-130
6
Dibenzo(a,e)pyrene
ug/kg
ND
1810
1810
2350
2230
130
123
70-130
5
Dibenzofuran
ug/kg
ND
1810
1810
1730
1640
95
90
32-130
6
Diethylphthalate
ug/kg
ND
1810
1810
1690
1660
93
92
40-130
1
Dimethoate
ug/kg
ND
1810
1810
2110
2040
116
112
70-130
3
Dimethylphthalate
ug/kg
ND
1810
1810
1710
1650
94
91
37-130
3
Dinoseb
ug/kg
ND
1810
1810
2090
2040
115
113
10-146
2
Diphenyl ether (Phenyl ether)
ug/kg
0.01
1810
1810
1620
1480
89
81
70-130
9
Diphenylamine
ug/kg
ND
1810
1810
1790
1690
99
93
10-134
6
Disulfoton
ug/kg
ND
1810
1810
1610
1570
89
87
70-130
2
Ethyl methanesulfonate
ug/kg
ND
1810
1810
1530
1420
84
78
70-130
8
Famphur
ug/kg
ND
3620
3620
1930
1620
53
45
10-200
181H
Fluoranthene
ug/kg
ND
1810
1810
1680
1630
93
90
26-130
3
Fluorene
ug/kg
ND
1810
1810
1650
1610
91
89
31-130
3
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/25/2022 02:36 PM without the written consent of Pace Analytical Services, LLC. Page 115 of 165

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: WASTE CHARACTERIZATION
Pace Project No.: 92621331
MATRIX SPIKE & MATRIX SPIKE
DUPLICATE:
3749841
3749842
MS
MSD
92621241006
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Hexachloro-1,3-butadiene
ug/kg
ND
1810
1810
1580
1410
87
78
20-130
12
Hexachlorobenzene
ug/kg
ND
1810
1810
1970
1840
109
101
29-130
7
Hexachlorocyclopentadiene
ug/kg
ND
1810
1810
1590
1310
88
72
10-130
19
Hexachloroethane
ug/kg
ND
1810
1810
1410
1230
78
68
21-130
14
Hexachlorophene
ug/kg
ND
18100
18100
14100
15000
78
83
70-130
61H
Hexachloropropene
ug/kg
ND
1810
1810
1760
1570
97
86
10-145
12
Indeno(1,2,3-cd)pyrene
ug/kg
ND
1810
1810
2030
1850
112
102
28-130
9
Isodrin
ug/kg
ND
1810
1810
1820
1750
100
97
70-130
4
Isophorone
ug/kg
ND
1810
1810
1490
1370
82
75
32-130
8
Isosafrole
ug/kg
ND
1810
1810
1580
1510
87
83
24-130
5
Kepone
ug/kg
ND
3620
3620
1690
1150
47
32
70-130
38 M1,R1,v1
Methapyrilene
ug/kg
ND
1810
1810
1480J
1530J
82
84
10-199
Methyl methanesulfonate
ug/kg
ND
1810
1810
1810
1680
100
93
70-130
7
Methyl parathion
ug/kg
ND
1810
1810
2020
2030
112
112
70-130
0
n-Decane
ug/kg
ND
1810
1810
1360
1100
75
61
70-130
21 M1
N-Nitroso-di-n-butylamine
ug/kg
ND
1810
1810
1820
1770
101
98
10-130
3
N-Nitroso-di-n-propylamine
ug/kg
ND
1810
1810
1530
1430
85
79
31-130
7
N-Nitrosodiethylamine
ug/kg
ND
1810
1810
1510
1390
84
77
10-130
9
N-Nitrosodimethylamine
ug/kg
ND
1810
1810
1270
1070
70
59
20-130
17
N-Nitrosodiphenylamine
ug/kg
ND
1810
1810
1790
1690
99
93
32-130
6
N-Nitrosomethylethylamine
ug/kg
ND
1810
1810
1420
1280
79
71
10-130
11
N-Nitrosomorpholine
ug/kg
ND
1810
1810
1810
1870
100
103
10-130
4
N-Nitrosopiperidine
ug/kg
ND
1810
1810
1660
1530
92
84
10-130
8
N-Nitrosopyrrolidine
ug/kg
ND
1810
1810
1520
1490
84
82
10-130
2
n-Octadecane
ug/kg
ND
1810
1810
1810
1690
100
93
70-130
7
Naphthalene
ug/kg
ND
1810
1810
1540
1370
85
76
30-130
11
Nitrobenzene
ug/kg
ND
1810
1810
1540
1350
85
75
25-130
13
0,0,0-
ug/kg
ND
1810
1810
1760
1570
97
87
70-130
11
Triethyl phosphorothioate
O-Toluidine
ug/kg
ND
1810
1810
1430
1370
79
76
70-130
4
P-Dimethylaminoazobenzene
ug/kg
ND
1810
1810
1060
1000
58
55
70-130
51L,M1
p-Phenylenediamine
ug/kg
ND
ND
ND
IL
Parathion (Ethyl parathion)
ug/kg
ND
1810
1810
1850
1830
102
101
70-130
1
Pentachlorobenzene
ug/kg
ND
1810
1810
1980
1910
109
106
10-130
3
Pentachloroethane
ug/kg
ND
1810
1810
1550
1350
86
74
70-130
14
Pentachloronitrobenzene
ug/kg
ND
1810
1810
2590
2440
143
134
24-130
6 M1
Pentachlorophenol
ug/kg
ND
3620
3620
3950
3850
109
106
10-130
3
Phenacetin
ug/kg
ND
1810
1810
1880
1870
104
103
10-137
1
Phenanthrene
ug/kg
ND
1810
1810
1760
1680
97
92
34-130
5
Phenol
ug/kg
ND
1810
1810
1520
1380
82
74
14-130
9
Phorate
ug/kg
ND
1810
1810
1790
1750
99
97
70-130
2
Phthalic anhydride
ug/kg
ND
ND
ND
Pronamide
ug/kg
ND
1810
1810
2060
2010
114
111
10-156
2
Pyrene
ug/kg
ND
1810
1810
1970
1770
109
98
31-130
11
Pyridine
ug/kg
ND
1810
1810
1090
892
60
49
10-130
20
Safrole
ug/kg
ND
1810
1810
1690
1570
93
87
10-132
7
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/25/2022 02:36 PM without the written consent of Pace Analytical Services, LLC. Page 116 of 165

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: WASTE CHARACTERIZATION
Pace Project No.: 92621331
MATRIX SPIKE & MATRIX SPIKE
DUPLICATE: 3749841
3749842
MS
MSD
92621241006
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits RPD Qual
Sulfotepp (Thiodiphosphoric
ug/kg ND
1810
1810
2210
2150
122
119
70-130 3
Ac
Terpineol
ug/kg 0.01
1810
1810
2580
2350
142
129
70-130 9 M1
Thionazin
ug/kg ND
1810
1810
1750
1720
97
95
70-130 2
2,4,6-Tribromophenol (S)
%
110
108
18-130
2-Fluorobiphenyl (S)
%
81
77
19-130
2-Fluorophenol(S)
%
74
68
18-130
Nitrobenzene-d5(S)
%
76
70
21-130
Phenol-d6 (S)
%
76
73
18-130
Terphenyl-d14(S)
%
107
98
15-130
k
to
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/25/2022 02:36 PM without the written consent of Pace Analytical Services, LLC.
Page 117 of 165

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: WASTE CHARACTERIZATION
Pace Project No.: 92621331
QC Batch: 720089 Analysis Method: EPA 8270E
QC Batch Method: EPA 3546 Analysis Description: 8270E Solid MSSV Microwave
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92621331001, 92621331002, 92621331003, 92621331004, 92621331005, 92621331006, 92621331007,
92621331010
METHOD BLANK: 3752586
Matrix: Solid
Associated Lab Samples: 92621331001, 92621331002, 92621331003, 92621331004, 92621331005, 92621331006, 92621331007,
92621331010
Parameter
Units
Blank
Result
Reporting
Limit
Analyzed
1,2,4,5-Tetrachlorobenzene
ug/kg
ND
328
08/30/22 11:23
1,2,4-Trichlorobenzene
ug/kg
ND
328
08/30/22 11:23
1,2-Dichlorobenzene
ug/kg
ND
328
08/30/22 11:23
1,2-Diphenylhydrazine
ug/kg
ND
328
08/30/22 11:23
1,3,5-Trinitrobenzene
ug/kg
ND
328
08/30/22 11:23
1,3-Dichlorobenzene
ug/kg
ND
328
08/30/22 11:23
1,3-Dinitrobenzene
ug/kg
ND
328
08/30/22 11:23
1,4-Dichlorobenzene
ug/kg
ND
328
08/30/22 11:23
1,4-Dinitrobenzene
ug/kg
ND
328
08/30/22 11:23
1,4-Naphthoquinone
ug/kg
ND
1640
08/30/22 11:23
1-Methylnaphthalene
ug/kg
ND
328
08/30/22 11:23
1-Naphthalenamine
ug/kg
ND
656
08/30/22 11:23
2,2'-Oxybis(1-chloropropane)
ug/kg
ND
328
08/30/22 11:23
2,3,4,6-Tetrachlorophenol
ug/kg
ND
328
08/30/22 11:23
2,3-Dibromo-1-propanol phosph
ug/kg
ND
1640
08/30/22 11:23
2,3-Dichloroaniline
ug/kg
ND
328
08/30/22 11:23
2,4,5-Trichlorophenol
ug/kg
ND
328
08/30/22 11:23
2,4,6-Trichlorophenol
ug/kg
ND
328
08/30/22 11:23
2,4-Dichlorophenol
ug/kg
ND
328
08/30/22 11:23
2,4-Dimethylphenol
ug/kg
ND
328
08/30/22 11:23
2,4-Dinitrophenol
ug/kg
ND
1640
08/30/22 11:23
2,4-Dinitrotoluene
ug/kg
ND
328
08/30/22 11:23
2,6-Dichlorophenol
ug/kg
ND
328
08/30/22 11:23
2,6-Dinitrotoluene
ug/kg
ND
328
08/30/22 11:23
2-Acetylaminofluorene
ug/kg
ND
656
08/30/22 11:23
2-Chloronaphthalene
ug/kg
ND
328
08/30/22 11:23
2-Chlorophenol
ug/kg
ND
328
08/30/22 11:23
2-Methyl-5-nitroaniline
ug/kg
ND
328
08/30/22 11:23
2-Methylnaphthalene
ug/kg
ND
328
08/30/22 11:23
2-Methylphenol(o-Cresol)
ug/kg
ND
328
08/30/22 11:23
2-Naphthalenamine
ug/kg
ND
656
08/30/22 11:23
2-Nitroaniline
ug/kg
ND
1640
08/30/22 11:23
2-Nitrophenol
ug/kg
ND
328
08/30/22 11:23
2-Picoline
ug/kg
ND
328
08/30/22 11:23
3&4-Methylphenol (m&p Cresol)
ug/kg
ND
328
08/30/22 11:23
3,3'-Dichlorobenzidine
ug/kg
ND
656
08/30/22 11:23
3,3'-Dimethylbenzidine
ug/kg
ND
656
08/30/22 11:23
3-Methylcholanthrene
ug/kg
ND
328
08/30/22 11:23
3-Nitroaniline
ug/kg
ND
1640
08/30/22 11:23
IL
v1
IH
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/25/2022 02:36 PM without the written consent of Pace Analytical Services, LLC. Page 118 of 165

laneAnalytical
www,pacelabs.com
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: WASTE CHARACTERIZATION
Pace Project No.: 92621331
METHOD BLANK: 3752586 Matrix: Solid
Associated Lab Samples: 92621331001, 92621331002, 92621331003, 92621331004, 92621331005, 92621331006, 92621331007,
92621331010
Parameter
Units
Blank
Result
Reporting
Limit
Analyzed
4,4'-Methylene-bis(2-chloroani
ug/kg
ND
656
08/30/22 11:23
4,6-Dinitro-2-methylphenol
ug/kg
ND
656
08/30/22 11:23
4-Aminobiphenyl
ug/kg
ND
328
08/30/22 11:23
4-Chlorophenylphenyl ether
ug/kg
ND
328
08/30/22 11:23
4-Nitroaniline
ug/kg
ND
656
08/30/22 11:23
4-Nitrophenol
ug/kg
ND
1640
08/30/22 11:23
4-Nitroquinoline-n-oxide
ug/kg
ND
1640
08/30/22 11:23
5-Nitro-o-toluidine
ug/kg
ND
328
08/30/22 11:23
7,12-Dimethylbenz(a)anthracene
ug/kg
ND
328
08/30/22 11:23
a,a-Dimethylphenylethylamine
ug/kg
ND
1640
08/30/22 11:23
Acenaphthene
ug/kg
ND
328
08/30/22 11:23
Acenaphthylene
ug/kg
ND
328
08/30/22 11:23
Acetophenone
ug/kg
ND
328
08/30/22 11:23
Anthracene
ug/kg
ND
328
08/30/22 11:23
Benzo(a)anthracene
ug/kg
ND
328
08/30/22 11:23
Benzo(a)pyrene
Benzo(b)fluoranthene
ug/kg
ug/kg
ND
ND
328
328
08/30/22 11:23
08/30/22 11:23
-OO
Benzo(g,h,i)perylene
ug/kg
ND
328
08/30/22 11:23
Benzo(k)fluoranthene
ug/kg
ND
328
08/30/22 11:23
Benzyl alcohol
ug/kg
ND
656
08/30/22 11:23
bis(2-Chloroethoxy)methane
ug/kg
ND
328
08/30/22 11:23
bis(2-Chloroethyl) ether
ug/kg
ND
328
08/30/22 11:23
bis(2-Ethylhexyl)phthalate
ug/kg
ND
328
08/30/22 11:23
Chrysene
ug/kg
ND
328
08/30/22 11:23
Di-n-butylphthalate
ug/kg
ND
328
08/30/22 11:23
Di-n-octylphthalate
ug/kg
ND
328
08/30/22 11:23
Diallate
ug/kg
ND
328
08/30/22 11:23
Dibenz(a,h)anthracene
ug/kg
ND
328
08/30/22 11:23
Dibenzo(a,e)pyrene
ug/kg
ND
993
08/30/22 11:23
Dibenzofuran
ug/kg
ND
328
08/30/22 11:23
Diethylphthalate
ug/kg
ND
328
08/30/22 11:23
Dimethoate
ug/kg
ND
656
08/30/22 11:23
Dimethylphthalate
ug/kg
ND
328
08/30/22 11:23
Dinoseb
ug/kg
ND
656
08/30/22 11:23
Diphenyl ether (Phenyl ether)
ug/kg
ND
497
08/30/22 11:23
Diphenylamine
ug/kg
ND
328
08/30/22 11:23
Disulfoton
ug/kg
ND
328
08/30/22 11:23
Ethyl methanesulfonate
ug/kg
ND
656
08/30/22 11:23
Famphur
ug/kg
ND
656
08/30/22 11:23
Fluoranthene
ug/kg
ND
328
08/30/22 11:23
Fluorene
ug/kg
ND
328
08/30/22 11:23
Hexachloro-1,3-butadiene
ug/kg
ND
328
08/30/22 11:23
Hexachlorobenzene
ug/kg
ND
328
08/30/22 11:23
Hexachlorocyclopentadiene
ug/kg
ND
328
08/30/22 11:23
Hexachloroethane
ug/kg
ND
328
08/30/22 11:23
v2
v1
IH
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/25/2022 02:36 PM without the written consent of Pace Analytical Services, LLC. Page 119 of 165

laneAnalytical
www,pacelabs.com
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: WASTE CHARACTERIZATION
Pace Project No.: 92621331
METHOD BLANK: 3752586 Matrix: Solid
Associated Lab Samples: 92621331001, 92621331002, 92621331003, 92621331004, 92621331005, 92621331006, 92621331007,
92621331010
Parameter
Units
Blank
Result
Reporting
Limit
Analyzed
Hexachlorophene
ug/kg
ND
3280
08/30/22 11:23
Hexachloropropene
ug/kg
ND
328
08/30/22 11:23
Indeno(1,2,3-cd)pyrene
ug/kg
ND
328
08/30/22 11:23
Isodrin
ug/kg
ND
328
08/30/22 11:23
Isophorone
ug/kg
ND
328
08/30/22 11:23
Isosafrole
ug/kg
ND
328
08/30/22 11:23
Kepone
ug/kg
ND
656
08/30/22 11:23
Methapyrilene
ug/kg
ND
1640
08/30/22 11:23
Methyl methanesulfonate
ug/kg
ND
656
08/30/22 11:23
Methyl parathion
ug/kg
ND
328
08/30/22 11:23
n-Decane
ug/kg
ND
328
08/30/22 11:23
N-Nitroso-di-n-butylamine
ug/kg
ND
328
08/30/22 11:23
N-Nitroso-di-n-propylamine
ug/kg
ND
328
08/30/22 11:23
N-Nitrosodiethylamine
ug/kg
ND
328
08/30/22 11:23
N-Nitrosodimethylamine
ug/kg
ND
328
08/30/22 11:23
N-Nitrosodiphenylamine
ug/kg
ND
328
08/30/22 11:23
N-Nitrosomethylethylamine
ug/kg
ND
328
08/30/22 11:23
N-Nitrosomorpholine
ug/kg
N
328
08/30/22 11:23
N-Nitrosopiperidine
ug/kg
ND
656
08/30/22 11:23
N-Nitrosopyrrolidine
ug/kg
ND
656
08/30/22 11:23
n-Octadecane
ug/kg
ND
328
08/30/22 11:23
Naphthalene
ug/kg
ND
328
08/30/22 11:23
Nitrobenzene
ug/kg
ND
328
08/30/22 11:23
O,O,O-Triethylphosphorothioate
ug/kg
ND
328
08/30/22 11:23
O-Toluidine
ug/kg
ND
328
08/30/22 11:23
P-Dimethylaminoazobenzene
ug/kg
ND
328
08/30/22 11:23
p-Phenylenediamine
ug/kg
ND
656
08/30/22 11:23
Parathion (Ethyl parathion)
ug/kg
ND
328
08/30/22 11:23
Pentachlorobenzene
ug/kg
ND
328
08/30/22 11:23
Pentachloroethane
ug/kg
ND
328
08/30/22 11:23
Pentachloronitrobenzene
ug/kg
ND
328
08/30/22 11:23
Pentachlorophenol
ug/kg
ND
656
08/30/22 11:23
Phenacetin
ug/kg
ND
656
08/30/22 11:23
Phenanthrene
ug/kg
ND
328
08/30/22 11:23
Phenol
ug/kg
ND
328
08/30/22 11:23
Phorate
ug/kg
ND
328
08/30/22 11:23
Phthalic anhydride
ug/kg
ND
2480
08/30/22 11:23
Pronamide
ug/kg
ND
656
08/30/22 11:23
Pyrene
ug/kg
ND
328
08/30/22 11:23
Pyridine
ug/kg
ND
328
08/30/22 11:23
Safrole
ug/kg
ND
656
08/30/22 11:23
Sulfotepp (Thiodiphosphoric Ac
ug/kg
ND
328
08/30/22 11:23
Terpineol
ug/kg
ND
328
08/30/22 11:23
Thionazin
ug/kg
ND
328
08/30/22 11:23
2,4,6-Tribromophenol (S)
%
48
18-130
08/30/22 11:23
IH
IL
IL
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/25/2022 02:36 PM without the written consent of Pace Analytical Services, LLC. Page 120 of 165

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: WASTE CHARACTERIZATION
Pace Project No.: 92621331
METHOD BLANK: 3752586 Matrix: Solid
Associated Lab Samples: 92621331001, 92621331002, 92621331003, 92621331004, 92621331005, 92621331006, 92621331007,
92621331010
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
2-Fluorobiphenyl (S)
%
49
19-130
08/30/22 11:23
2-Fluorophenol(S)
%
51
18-130
08/30/22 11:23
Nitrobenzene-d5 (S)
%
52
21-130
08/30/22 11:23
Phenol-d6 (S)
%
52
18-130
08/30/22 11:23
Terphenyl-d14 (S)
%
50
15-130
08/30/22 11:23
LABORATORY CONTROL SAMPLE:
Parameter
3752587
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
1,2,4,5-Tetrachlorobenzene
ug/kg
1650
1260
77
56-130
1,2,4-Trichlorobenzene
ug/kg
1650
1260
76
47-130
1,2-Dichlorobenzene
ug/kg
1650
1240
75
49-130
1,2-Diphenylhydrazine
ug/kg
1650
1370
83
34-171
1,3,5-Trinitrobenzene
ug/kg
1650
1280
78
46-143
1,3-Dichlorobenzene
ug/kg
1650
1220
74
48-130
1,3-Dinitrobenzene
ug/kg
1650
1420
86
66-130
1,4-Dichlorobenzene
ug/kg
1650
1200
73
49-130
1,4-Dinitrobenzene
ug/kg
1650
1450
88
63-130
1,4-Naphthoquinone
ug/kg
1650
1130J
68
10-137
1-Methylnaphthalene
ug/kg
1650
1280
78
54-130
1-Naphthalenamine
ug/kg
1650
1270
77
45-130
2,2'-Oxybis(1-chloropropane)
ug/kg
1650
1410
86
38-130
2,3,4,6-Tetrachlorophenol
ug/kg
1650
1160
70
51-133
2,3-Dibromo-1-propanol phosph
ug/kg
6600
3770
57
10-160 IL
2,3-Dichloroaniline
ug/kg
1650
1210
73
46-145
2,4,5-Trichlorophenol
ug/kg
1650
1220
74
49-130
2,4,6-Trichlorophenol
ug/kg
1650
1250
76
50-130
2,4-Dichlorophenol
ug/kg
1650
1320
80
51-130
2,4-Dimethylphenol
ug/kg
1650
1440
87
53-130
2,4-Dinitrophenol
ug/kg
8250
6810
83
39-130
2,4-Dinitrotoluene
ug/kg
1650
1350
82
53-130
2,6-Dichlorophenol
ug/kg
1650
1530
93
55-130
2,6-Dinitrotoluene
ug/kg
1650
1310
79
55-130
2-Acetylaminofluorene
ug/kg
1650
1640
100
38-130 v1
2-Chloronaphthalene
ug/kg
1650
1210
73
48-130
2-Chlorophenol
ug/kg
1650
1280
78
54-130
2-Methyl-5-nitroaniline
ug/kg
1650
1410
86
52-130
2-Methylnaphthalene
ug/kg
1650
1260
77
57-130
2-Methylphenol(o-Cresol)
ug/kg
1650
1240
75
50-130
2-Naphthalenamine
ug/kg
1650
1130
68
25-130
2-Nitroaniline
ug/kg
3300
2850
86
49-130
2-Nitrophenol
ug/kg
1650
1280
77
50-130
2-Picoline
ug/kg
1650
1160
70
10-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/25/2022 02:36 PM without the written consent of Pace Analytical Services, LLC. Page 121 of 165

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: WASTE CHARACTERIZATION
Pace Project No.: 92621331
LABORATORY CONTROL SAMPLE: 3752587
Parameter
QUALITY CONTROL DATA
Spike LCS LCS % Rec
Units Conc. Result % Rec Limits Qualifiers
3&4-Methyl phenol (m&p Cresol)
ug/kg
1650
1390
84
50-130
3,3'-Dichlorobenzidine
ug/kg
3300
2560
77
47-130
3,3'-Dimethylbenzidine
ug/kg
3300
3920
119
10-1301H
3-Methylcholanthrene
ug/kg
1650
1310
79
68-175
3-Nitroaniline
ug/kg
3300
2700
82
45-130
4,4'-Methylene-bis(2-chloroani
ug/kg
3300
2810
85
20-130
4,6-Dinitro-2-methyl phenol
ug/kg
3300
2660
80
50-142
4-Aminobiphenyl
ug/kg
1650
955
58
10-130
4-Chlorophenylphenyl ether
ug/kg
1650
1320
80
53-130
4-Nitroaniline
ug/kg
3300
2720
82
51-130
4-Nitrophenol
ug/kg
8250
7660
93
40-130
4-Nitroquinoline-n-oxide
ug/kg
3300
1850
56
30-130 v3
5-Nitro-o-toluidine
ug/kg
1650
1410
86
35-130
7,12-Dimethylbenz(a)anthracene
ug/kg
1650
1100
66
62-130
a,a-Dimethylphenylethylamine
ug/kg
1650
513J
31
10-160 v1
Acenaphthene
ug/kg
1650
1290
78
56-130
Acenaphthylene
ug/kg
1650
1350
82
58-130
Acetophenone
ug/kg
1650
1360
82
54-130
Anthracene
ug/kg
1650
1210
73
60-130
Benzo(a)anthracene
ug/kg
1650
1350
82
59-130
Benzo(a)pyrene
ug/kg
1650
1670
101
57-130
Benzo(b)fluoranthene
ug/kg
1650
1580
96
54-130
Benzo(g,h,i)perylene
ug/kg
1650
1470
89
59-130
Benzo(k)fluoranthene
ug/kg
1650
1440
88
54-130
Benzyl alcohol
ug/kg
3300
2630
80
50-130
bis(2-Chloroethoxy)methane
ug/kg
1650
1260
77
55-130
bis(2-Chloroethyl) ether
ug/kg
1650
1280
77
53-130
bis(2-Ethylhexyl)phthalate
ug/kg
1650
1320
80
58-130
Chrysene
ug/kg
1650
1310
79
57-130
Di-n-butylphthalate
ug/kg
1650
1280
78
57-130
Di-n-octylphthalate
ug/kg
1650
1440
87
57-130
Diallate
ug/kg
1650
1290
78
48-130
Dibenz(a,h)anthracene
ug/kg
1650
1520
92
60-130
Dibenzo(a,e)pyrene
ug/kg
1650
1580
96
49-130
Dibenzofuran
ug/kg
1650
1350
82
54-130
Diethylphthalate
ug/kg
1650
1290
78
55-130
Dimethoate
ug/kg
1650
1530
93
67-133
Dimethylphthalate
ug/kg
1650
1290
78
57-130
Dinoseb
ug/kg
1650
1490
90
30-139
Diphenyl ether (Phenyl ether)
ug/kg
1650
1170
71
50-150
Diphenylamine
ug/kg
1650
1250
76
58-130
Disulfoton
ug/kg
1650
1220
74
55-139
Ethyl methanesulfonate
ug/kg
1650
1380
84
39-144
Famphur
ug/kg
3300
248J
8
10-200 IH,L2
Fluoranthene
ug/kg
1650
1380
83
57-130
Fluorene
ug/kg
1650
1290
78
56-130
Hexachloro-1,3-butadiene
ug/kg
1650
1160
70
41-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/25/2022 02:36 PM without the written consent of Pace Analytical Services, LLC. Page 122 of 165

Pace Analytical Services, LLC
9800
lCtaac,Analyfical ® Kiney Ave. Suite 100
Huntersville, NC 28078
0788
www.pacelabs.com [phone]
QUALITY CONTROL DATA
Project: WASTE CHARACTERIZATION
Pace Project No.: 92621331
LABORATORY CONTROL SAMPLE:
Parameter
3752587
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
Hexachlorobenzene
ug/kg
1650
1240
75
53-130
Hexachlorocyclopentadiene
ug/kg
1650
1170
71
23-130
Hexachloroethane
ug/kg
1650
1250
76
48-130
Hexachlorophene
ug/kg
16500
12000
73
10-131 IH
Hexachloropropene
ug/kg
1650
1430
86
29-130
Indeno(1,2,3-cd)pyrene
ug/kg
1650
1500
91
61-130
Isodrin
ug/kg
1650
1360
83
66-130
Isophorone
ug/kg
1650
1190
72
49-130
Isosafrole
ug/kg
1650
1180
71
33-130
Kepone
ug/kg
3300
865
26
10-147
Methapyrilene
ug/kg
1650
562J
34
10-130
Methyl methanesulfonate
ug/kg
1650
1620
98
23-138
Methyl parathion
ug/kg
1650
1540
93
57-130
n-Decane
ug/kg
1650
1250
76
25-130
N-Nitroso-di-n-butylamine
ug/kg
1650
1440
87
19-130
N-Nitroso-di-n-propylamine
ug/kg
1650
1340
81
52-130
N-Nitrosodiethylamine
ug/kg
1650
1350
82
22-130
N-Nitrosodimethylamine
ug/kg
1650
1150
70
45-130
N-Nitrosodiphenylamine
ug/kg
1650
1250
76
56-130
N-Nitrosomethylethylamine
ug/kg
1650
1310
80
16-130
N-Nitrosomorpholine
ug/kg
1650
1510
92
26-130
N-Nitrosopiperidine
ug/kg
1650
1360
83
37-130
N-Nitrosopyrrolidine
ug/kg
1650
1350
82
33-130
n-Octadecane
ug/kg
1650
1220
74
43-130
Naphthalene
ug/kg
1650
1270
77
56-130
Nitrobenzene
ug/kg
1650
1300
79
50-130
O,O,O-Triethylphosphorothioate
ug/kg
1650
1320
80
29-175
O-Toluidine
ug/kg
1650
1290
78
41-130
P-Dimethylaminoazobenzene
ug/kg
1650
690
42
14-130IL
p-Phenylenediamine
ug/kg
ND
IL
Parathion (Ethyl parathion)
ug/kg
1650
1370
83
61-130
Pentachlorobenzene
ug/kg
1650
1340
81
57-130
Pentachloroethane
ug/kg
1650
1360
82
35-141
Pentachloronitrobenzene
ug/kg
1650
1680
102
67-130
Pentachlorophenol
ug/kg
3300
2710
82
33-130
Phenacetin
ug/kg
1650
1420
86
64-130
Phenanthrene
ug/kg
1650
1310
79
60-130
Phenol
ug/kg
1650
1290
78
54-130
Phorate
ug/kg
1650
910
55
59-130 L2
Phthalic anhydride
ug/kg
ND
Pronamide
ug/kg
1650
1460
88
68-130
Pyrene
ug/kg
1650
1420
86
61-130
Pyridine
ug/kg
1650
941
57
35-130
Safrole
ug/kg
1650
1350
82
57-130
Sulfotepp (ThiodiphosphoricAc
ug/kg
1650
1290
78
10-160
Terpineol
ug/kg
1650
2110
128
39-130
Thionazin
ug/kg
1650
1340
81
43-146
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/25/2022 02:36 PM without the written consent of Pace Analytical Services, LLC. Page 123 of 165

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: WASTE CHARACTERIZATION
Pace Project No.: 92621331
LABORATORY CONTROL SAMPLE:
3752587
Spike LCS LCS
% Rec
Parameter
Units
Conc. Result % Rec
Limits
2,4,6-Tribromophenol (S)
%
72
18-130
2-Fluorobiphenyl (S)
%
67
19-130
2-Fluorophenol(S)
%
74
18-130
Nitrobenzene-d5(S)
%
70
21-130
Phenol-d6 (S)
%
75
18-130
Terphenyl-d14 (S)
%
75
15-130
SAMPLE DUPLICATE: 3752589
Parameter
Units
92621331007
Result
Dup
Result
1,2,4,5-Tetrachlorobenzene
ug/kg
ND
ND
1,2,4-Trichlorobenzene
ug/kg
ND
ND
1,2-Dichlorobenzene
ug/kg
ND
ND
1,2-Diphenylhydrazine
ug/kg
ND
ND
1,3,5-Trinitrobenzene
ug/kg
ND
ND
1,3-Dichlorobenzene
ug/kg
ND
ND
1,3-Dinitrobenzene
ug/kg
ND
ND
1,4-Dichlorobenzene
ug/kg
ND
ND
1,4-Dinitrobenzene
ug/kg
ND
ND
1,4-Naphthoquinone
ug/kg
ND
ND
1-Methylnaphthalene
ug/kg
ND
ND
1-Naphthalenamine
ug/kg
ND
ND
2,2'-Oxybis(1-chloropropane)
ug/kg
ND
ND
2,3,4,6-Tetrachlorophenol
ug/kg
ND
ND
2,3-Dibromo-1-propanol phosph
ug/kg
ND
ND
2,3-Dichloroaniline
ug/kg
ND
ND
2,4,5-Trichlorophenol
ug/kg
ND
ND
2,4,6-Trichlorophenol
ug/kg
ND
ND
2,4-Dichlorophenol
ug/kg
ND
ND
2,4-Dimethylphenol
ug/kg
ND
ND
2,4-Dinitrophenol
ug/kg
ND
ND
2,4-Dinitrotoluene
ug/kg
ND
ND
2,6-Dichlorophenol
ug/kg
ND
ND
2,6-Dinitrotoluene
ug/kg
ND
ND
2-Acetylaminofluorene
ug/kg
ND
ND
2-Chloronaphthalene
ug/kg
ND
ND
2-Chlorophenol
ug/kg
ND
ND
2-Methyl-5-nitroaniline
ug/kg
ND
ND
2-Methylnaphthalene
ug/kg
ND
ND
2-Methylphenol(o-Cresol)
ug/kg
ND
ND
2-Naphthalenamine
ug/kg
ND
ND
2-Nitroaniline
ug/kg
ND
ND
2-Nitrophenol
ug/kg
ND
ND
2-Picoline
ug/kg
ND
ND
3&4-Methyl phenol (m&p Cresol)
ug/kg
ND
ND
RPD Qualifiers
IL
v1
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/25/2022 02:36 PM without the written consent of Pace Analytical Services, LLC. Page 124 of 165

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: WASTE CHARACTERIZATION
Pace Project No.: 92621331
SAMPLE DUPLICATE: 3752589
Parameter
Units
92621331007 Dup
Result Result
3,3'-Dichlorobenzidine
ug/kg
ND
ND
3,3'-Dimethylbenzidine
ug/kg
ND
ND
3-Methylcholanthrene
ug/kg
ND
ND
3-Nitroaniline
ug/kg
ND
ND
4,4'-Methylene-bis(2-chloroani
ug/kg
ND
ND
4,6-Dinitro-2-methyl phenol
ug/kg
ND
ND
4-Aminobiphenyl
ug/kg
ND
ND
4-Chlorophenylphenyl ether
ug/kg
ND
ND
4-Nitroaniline
ug/kg
ND
ND
4-Nitrophenol
ug/kg
ND
ND
4-Nitroquinoline-n-oxide
ug/kg
ND
ND
5-Nitro-o-toluidine
ug/kg
ND
ND
7,12-Dimethylbenz(a)anthracene
ug/kg
ND
ND
a,a-Dimethylphenylethylamine
ug/kg
ND
ND
Acenaphthene
ug/kg
ND
ND
Acenaphthylene
ug/kg
ND
ND
Acetophenone
ug/kg
ND V
ND
Anthracene
Benzo(a)anthracene
ug/kg
ug/kg
ND
ND
ND
ND
Benzo(a)pyrene
ug/kg
ND 1111111110
ND
Benzo(b)fluoranthene
ug/kg
ND
ND
Benzo(g,h,i)perylene
ug/kg
ND
ND
Benzo(k)fluoranthene
ug/kg
ND
ND
Benzyl alcohol
ug/kg
ND
ND
bis(2-Chloroethoxy)methane
ug/kg
ND
ND
bis(2-Chloroethyl) ether
ug/kg
ND
ND
bis(2-Ethylhexyl)phthalate
ug/kg
ND 5760J
Chrysene
ug/kg
ND
ND
Di-n-butylphthalate
ug/kg
ND
ND
Di-n-octylphthalate
ug/kg
ND
ND
Diallate
ug/kg
ND
ND
Dibenz(a,h)anthracene
ug/kg
ND
ND
Dibenzo(a,e)pyrene
ug/kg
ND
ND
Dibenzofuran
ug/kg
ND
ND
Diethylphthalate
ug/kg
ND
ND
Dimethoate
ug/kg
ND
ND
Dimethylphthalate
ug/kg
ND
ND
Dinoseb
ug/kg
ND
ND
Diphenyl ether (Phenyl ether)
ug/kg
ND
ND
Diphenylamine
ug/kg
ND
ND
Disulfoton
ug/kg
ND
ND
Ethyl methanesulfonate
ug/kg
ND
ND
Famphur
ug/kg
ND
ND
Fluoranthene
ug/kg
ND
ND
Fluorene
ug/kg
ND
ND
Hexachloro-1,3-butadiene
ug/kg
ND
ND
Hexachlorobenzene
ug/kg
ND
ND
RPD Qualifiers
v2
v1
IH
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/25/2022 02:36 PM without the written consent of Pace Analytical Services, LLC. Page 125 of 165

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: WASTE CHARACTERIZATION
Pace Project No.: 92621331
SAMPLE DUPLICATE: 3752589
Parameter
Units
92621331007 Dup
Result Result
Hexachlorocyclopentadiene
ug/kg
ND
ND
Hexachloroethane
ug/kg
ND
ND
Hexachlorophene
ug/kg
ND
ND
Hexachloropropene
ug/kg
ND
ND
Indeno(1,2,3-cd)pyrene
ug/kg
ND
ND
Isodrin
ug/kg
ND
ND
Isophorone
ug/kg
ND
ND
Isosafrole
ug/kg
ND
ND
Kepone
ug/kg
ND
ND
Methapyrilene
ug/kg
ND
ND
Methyl methanesulfonate
ug/kg
ND
ND
Methyl parathion
ug/kg
ND
ND
n-Decane
ug/kg
ND
ND
N-Nitroso-di-n-butylamine
ug/kg
ND
ND
N-Nitroso-di-n-propylamine
ug/kg
ND
ND
N-Nitrosodiethylamine
ug/kg
ND
ND
N-Nitrosodimethylamine
ug/kg
ND V
ND
N-Nitrosodiphenylamine
ug/kg
ND
ND
N-Nitrosomethylethylamine
ug/kg
ND
ND
N-Nitrosomorpholine
ug/kg
ND
ND
N-Nitrosopiperidine
ug/kg
ND
ND
N-Nitrosopyrrolidine
ug/kg
ND
ND
n-Octadecane
ug/kg
ND
ND
Naphthalene
ug/kg
ND
ND
Nitrobenzene
ug/kg
ND
ND
O,O,O-Triethylphosphorothioate
ug/kg
ND
ND
O-Toluidine
ug/kg
ND
ND
P-Dimethylaminoazobenzene
ug/kg
ND
ND
p-Phenylenediamine
ug/kg
ND
ND
Parathion (Ethyl parathion)
ug/kg
ND
ND
Pentachlorobenzene
ug/kg
ND
ND
Pentachloroethane
ug/kg
ND
ND
Pentachloronitrobenzene
ug/kg
ND
ND
Pentachlorophenol
ug/kg
ND
ND
Phenacetin
ug/kg
ND
ND
Phenanthrene
ug/kg
ND
ND
Phenol
ug/kg
ND
ND
Phorate
ug/kg
ND
ND
Phthalic anhydride
ug/kg
ND
ND
Pronamide
ug/kg
ND
ND
Pyrene
ug/kg
ND
ND
Pyridine
ug/kg
ND
ND
Safrole
ug/kg
ND
ND
Sulfotepp (ThiodiphosphoricAc
ug/kg
ND
ND
Terpineol
ug/kg
ND
ND
Thionazin
ug/kg
ND
ND
2,4,6-Tribromophenol (S)
%
0
0
RPD Qualifiers
IH
IL
IL
S4
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/25/2022 02:36 PM without the written consent of Pace Analytical Services, LLC. Page 126 of 165

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: WASTE CHARACTERIZATION
Pace Project No.: 92621331
SAMPLE DUPLICATE: 3752589
Parameter
2-Fluorobiphenyl (S)
2-Fluorophenol(S)
Nitrobenzene-d5 (S)
Phenol-d6 (S)
Terphenyl-d14 (S)
Units
QUALITY CONTROL DATA
92621331007 Dup
Result Result RPD Qualifiers
0 0 D3,S4
0 0 S4
0 0 S4
0 0 S4
0 0 S4
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/25/2022 02:36 PM without the written consent of Pace Analytical Services, LLC.
Page 127 of 165

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: WASTE CHARACTERIZATION
Pace Project No.: 92621331
QC Batch: 718782 Analysis Method: SW-846
QC Batch Method: SW-846 Analysis Description: Dry Weight/Percent Moisture
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92621331001, 92621331002, 92621331003, 92621331004, 92621331005, 92621331006, 92621331007,
92621331008,92621331009,92621331010,92621331011,92621331012,92621331013,92621331014
SAMPLE DUPLICATE: 3746810
92621086006 Dup
Parameter Units Result Result RPD Qualifiers
Percent Moisture % 14.5 14.8 2 N2
SAMPLE DUPLICATE: 3746811
Parameter
Percent Moisture
92621510002
Units Result
99
Dup
Result
102
RPD Qualifiers
3 N2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/25/2022 02:36 PM without the written consent of Pace Analytical Services, LLC.
Page 128 of 165

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: WASTE CHARACTERIZATION
Pace Project No.: 92621331
QC Batch: 718757 Analysis Method: EPA 1010B
QC Batch Method: EPA 1010E Analysis Description: 1010 Flash Point, Closed Cup
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92621331001, 92621331002, 92621331003, 92621331004, 92621331005, 92621331006, 92621331007,
92621331008
SAMPLE DUPLICATE: 3746590
92620212001 Dup
Parameter Units Result Result RPD Qualifiers
Flashpoint deg F >200 >200
in
r
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/25/2022 02:36 PM without the written consent of Pace Analytical Services, LLC.
Page 129 of 165

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: WASTE CHARACTERIZATION
Pace Project No.: 92621331
QC Batch: 718989 Analysis Method: EPA 1010B
QC Batch Method: EPA 1010E Analysis Description: 1010 Flash Point, Closed Cup
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92621331009, 92621331010
SAMPLE DUPLICATE: 3747609
92621331009 Dup
Parameter Units Result Result RPD Qualifiers
Flashpoint deg F >200 >200
VkW
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/25/2022 02:36 PM without the written consent of Pace Analytical Services, LLC. Page 130 of 165

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: WASTE CHARACTERIZATION
Pace Project No.: 92621331
QC Batch: 1914084 Analysis Method: SM 2540G
QC Batch Method: SM 2540 G Analysis Description: Total Solids 2540 G-2011
Laboratory: Pace National - Mt. Juliet
Associated Lab Samples: 92621331001
METHOD BLANK: R3829703-1
Associated Lab Samples: 92621331001
Parameter Units
Total Solids %
LABORATORY CONTROL SAMPLE: R3829703-2
Parameter Units
Total Solids %
Matrix: Solid
Blank Reporting
Result Limit
ND
Spike LCS
Conc. Result
50.0 50.0
Analyzed Qualifiers
08/23/22 10:58
LCS % Rec
% Rec Limits Qualifiers
100 85.0-115
SAMPLE DUPLICATE: R3829703-3
L1527622-06 Dup
Parameter Units Result Result RPD Qualifiers
Total Solids % 89.3 91.4 2.36
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/25/2022 02:36 PM without the written consent of Pace Analytical Services, LLC. Page 131 of 165

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: WASTE CHARACTERIZATION
Pace Project No.: 92621331
QC Batch: 1914085 Analysis Method: SM 2540G
QC Batch Method: SM 2540 G Analysis Description: Total Solids 2540 G-2011
Laboratory: Pace National - Mt. Juliet
Associated Lab Samples: 92621331002, 92621331003, 92621331004, 92621331005, 92621331006, 92621331007, 92621331008,
92621331009,92621331010
METHOD BLANK: R3829697-1 Matrix: Solid
Associated Lab Samples: 92621331002, 92621331003, 92621331004, 92621331005, 92621331006, 92621331007, 92621331008,
92621331009,92621331010
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Total Solids % 0.00200 08/23/22 10:31
LABORATORY CONTROL SAMPLE:
R3829697-2
Spike LCS LCS
% Rec
Parameter
Units
Conc. Result % Rec
Limits Qualifiers
Total Solids
%
50.0 50.0 100
85.0-115
SAMPLE DUPLICATE: R3829697-3
92621331009 Dup
Parameter
Units
Result Result RPD
Qualifiers
Total Solids
%
50.6 50.2 0.771
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/25/2022 02:36 PM without the written consent of Pace Analytical Services, LLC.
Page 132 of 165

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: WASTE CHARACTERIZATION
Pace Project No.: 92621331
QC Batch: 718542 Analysis Method: SM 4500-S2D-2011 Modified
QC Batch Method: SM 4500-S2D-2011 Modified Analysis Description: 4500S2D Sulfide Soil
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92621331001, 92621331002, 92621331003, 92621331004, 92621331005, 92621331006, 92621331007,
92621331008,92621331009,92621331010
METHOD BLANK: 3745656 Matrix: Solid
Associated Lab Samples: 92621331001, 92621331002, 92621331003, 92621331004, 92621331005, 92621331006, 92621331007,
92621331008,92621331009,92621331010
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Sulfide mg/kg ND 5.0 08/20/22 06:36
LABORATORY CONTROL SAMPLE: 3745657
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Sulfide mg/kg 25 26.4 106 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3745683 3745684
MS MSD
92621331010 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Sulfide mg/kg ND 50.5 48.9 40.5 43.2 78 86 80-120 6 M1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 10/25/2022 02:36 PM without the written consent of Pace Analytical Services, LLC.
Page 133 of 165

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: WASTE CHARACTERIZATION
Pace Project No.: 92621331
QC Batch: 718962 Analysis Method: EPA 9045D
QC Batch Method: EPA 9045D Analysis Description: 9045 pH
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92621331001, 92621331002, 92621331003, 92621331004, 92621331005, 92621331006, 92621331007,
92621331008,92621331009,92621331010
SAMPLE DUPLICATE: 3747380
92621584001 Dup
Parameter Units Result Result RPD Qualifiers
pH at 25 Degrees C Std. Units 7.1 7.2 1 H3
SAMPLE DUPLICATE: 3747381
92621331005 Dup
Parameter Units Result Result RPD Qualifiers
pH at 25 Degrees C Std. Units 4.3 4.2 1 H3
IV
r�9
F]
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/25/2022 02:36 PM without the written consent of Pace Analytical Services, LLC.
Page 134 of 165

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: WASTE CHARACTERIZATION
Pace Project No.: 92621331
QC Batch: 724325 Analysis Method: EPA 7196A
QC Batch Method: EPA 7196A Modified Analysis Description: 7196 Chromium, Hexavalent
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92621331015, 92621331016, 92621331017, 92621331018
METHOD BLANK: 3774026
Matrix:
Solid
Associated Lab Samples: 92621331015, 92621331016,
92621331017, 92621331018
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Chromium, Hexavalent
mg/kg
ND
4.9
09/22/22 11:55
LABORATORY CONTROL SAMPLE:
3774027
Spike
LCS
LCS % Rec
Parameter
Units
Conc.
Result
% Rec Limits Qualifiers
Chromium, Hexavalent
mg/kg
24.5
24.5
100 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3774028 3774029
MS MSD
92626270001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Chromium, Hexavalent mg/kg ND 27.7 26.3 ND ND 12 9 75-125 M1
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3774030 3774031
MS MSD
92626270002 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Chromium, Hexavalent mg/kg ND 16.6 21.5 ND ND 5 8 75-125 M1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/25/2022 02:36 PM without the written consent of Pace Analytical Services, LLC.
Page 135 of 165

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: WASTE CHARACTERIZATION
Pace Project No.: 92621331
QC Batch: 851927 Analysis Method: EPA 9012
QC Batch Method: EPA 9012 Analysis Description: 9012 Cyanide
Laboratory: Pace Analytical Services - Ormond Beach
Associated Lab Samples: 92621331001, 92621331002, 92621331003, 92621331004, 92621331005, 92621331006, 92621331007,
92621331008,92621331009,92621331010
METHOD BLANK: 4687814 Matrix: Solid
Associated Lab Samples: 92621331001, 92621331002, 92621331003, 92621331004, 92621331005, 92621331006, 92621331007,
92621331008,92621331009,92621331010
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Cyanide mg/kg ND 0.26 08/29/2213:39
LABORATORY CONTROL SAMPLE: 4687815
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Cyanide mg/kg 1.3 1.3 99 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4688065 4688066
MS MSD
92621331001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Cyanide mg/kg 5.1 1.17 1.13 4.0 9.5 -86 388 80-120 80 M1,R1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 10/25/2022 02:36 PM without the written consent of Pace Analytical Services, LLC.
Page 136 of 165

lceAnalyircal
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALIFIERS
Project: WASTE CHARACTERIZATION
Pace Project No.: 92621331
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TN -The NELAC Institute.
SAMPLE QUALIFIERS
Sample: 92621331004
Ill OP Pesticides by Method 8141 B - Cannot run at lower dilution due to viscosity of extract
BATCH QUALIFIERS
Batch: 851684
Ill Sample was diluted due to the presence of high levels of non -target analytes or other matrix interference.
ANALYTE QUALIFIERS
1g Sample was diluted due to the presence of high levels of non -target analytes or other matrix interference.
D3 Sample was diluted due to the presence of high levels of non -target analytes or other matrix interference.
H2 Extraction or preparation conducted outside EPA method holding time.
H3 Sample was received or analysis requested beyond the recognized method holding time.
IH This analyte exceeded secondary source verification criteria high for the initial calibration. The reported results should be
considered an estimated value.
IL This analyte exceeded secondary source verification criteria low for the initial calibration. The reported results should be
considered an estimated value.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/25/2022 02:36 PM without the written consent of Pace Analytical Services, LLC. Page 137 of 165

Pace Analytical Services, LLC
ceAnalytrcal ® 9800 Kiney Ave. Suite 100
Huntersville, NC 28078078
www.pacelabs.com [phone]
QUALIFIERS
Project: WASTE CHARACTERIZATION
Pace Project No.: 92621331
ANALYTE QUALIFIERS
LO Analyte recovery in the laboratory control sample (LCS) was outside QC limits.
L2 Analyte recovery in the laboratory control sample (LCS) was below QC limits. Results for this analyte in associated
samples may be biased low.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
N2 The lab does not hold NELAC/TNI accreditation for this parameter but other accreditations/certifications may apply. A
complete list of accreditations/certifications is available upon request.
R1 RPD value was outside control limits.
S4 Surrogate recovery not evaluated against control limits due to sample dilution.
S5 Surrogate recovery outside control limits due to matrix interferences (not confirmed by re -analysis).
v1 The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in the
associated samples may have a high bias.
v2 The continuing calibration verification was below the method acceptance limit. The analyte was not detected in the
associated samples and the sensitivity of the instrument was verified with a reporting limit check standard.
v3 The continuing calibration verification was below the method acceptance limit. Any detection for the analyte in the
associated samples may have low bias.
r�9
?AA"
REPORT OF LABORATORY ANALYSIS
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Date: 10/25/2022 02:36 PM without the written consent of Pace Analytical Services, LLC. Page 138 of 165

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project:
Pace Project No.:
WASTE CHARACTERIZATION
92621331
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Batch
92621331001
GP-1 2-3'
3546
1914170
EPA 8141 B
1914170
92621331002
GP-2 2-3'
3546
1914170
EPA 8141 B
1914170
92621331003
GP-3 2-3'
3546
1914170
EPA 8141 B
1914170
92621331004
GP-4 2-3'
3546
1914170
EPA 8141 B
1914170
92621331005
GP-5 2-3'
3546
1914170
EPA 8141 B
1914170
92621331006
GP-6 2-3'
3546
1914170
EPA 8141 B
1914170
92621331007
GP-7 2-3'
3546
1914170
EPA 8141 B
1914170
92621331008
HA-1 2-3'
3546
1914170
EPA 8141B
1914170
92621331009
HA-2 2-3'
3546
1914170
EPA 8141 B
1914170
92621331010
SURFACE
BASIN 3
3546
1914170
EPA 8141 B
1914170
92621331001
GP-1 2-3'
EPA 3546
719156
EPA 8081 B
719505
92621331002
GP-2 2-3'
EPA 3546
719156
EPA 8081 B
719505
92621331003
GP-3 2-3'
EPA 3546
719156
EPA 8081 B
719505
92621331004
GP-4 2-3'
EPA 3546
720087
EPA 8081 B
720186
92621331005
GP-5 2-3'
EPA 3546
720087
EPA 8081 B
720186
92621331006
GP-6 2-3'
EPA 3546
719156
EPA 8081 B
719505
92621331007
GP-7 2-3'
EPA 3546
719156
EPA 8081 B
719505
92621331008
HA-1 2-3'
EPA 3546
719156
EPA 8081 B
719505
92621331009
HA-2 2-3'
EPA 3546
719156
EPA 8081 B
719505
92621331010
SURFACE
BASIN 3
EPA 3546
719156
EPA 8081 B
719505
92621331001
GP-1 2-3'
EPA 3546
718460
EPA 8082A
718901
92621331002
GP-2 2-3'
EPA 3546
718460
EPA 8082A
718901
92621331003
GP-3 2-3'
EPA 3546
718460
EPA 8082A
718901
92621331004
GP-4 2-3'
EPA 3546
718460
EPA 8082A
718901
92621331005
GP-5 2-3'
EPA 3546
718460
EPA 8082A
718901
92621331006
GP-6 2-3'
EPA 3546
718460
EPA 8082A
718901
92621331007
GP-7 2-3'
EPA 3546
718460
EPA 8082A
718901
92621331008
HA-1 2-3'
EPA 3546
718460
EPA 8082A
718901
92621331009
HA-2 2-3'
EPA 3546
718460
EPA 8082A
718901
92621331010
SURFACE
BASIN 3
EPA 3546
718460
EPA 8082A
718901
92621331001
GP-1 2-3'
EPA 3050
852504
EPA 6010
852521
92621331002
GP-2 2-3'
EPA 3050
852452
EPA 6010
852481
92621331003
GP-3 2-3'
EPA 3050
852452
EPA 6010
852481
92621331004
GP-4 2-3'
EPA 3050
852452
EPA 6010
852481
92621331005
GP-5 2-3'
EPA 3050
852452
EPA 6010
852481
92621331006
GP-6 2-3'
EPA 3050
852452
EPA 6010
852481
92621331007
GP-7 2-3'
EPA 3050
852452
EPA 6010
852481
92621331008
HA-1 2-3'
EPA 3050
852452
EPA 6010
852481
92621331009
HA-2 2-3'
EPA 3050
852452
EPA 6010
852481
92621331010
SURFACE
BASIN 3
EPA 3050
852452
EPA6010
852481
92621331015
Basin 1
EPA 3010A
846729
EPA 6010D
846834
92621331016
Basin 2
EPA 3010A
846729
EPA 6010D
846834
92621331017
Basin 3
EPA 3010A
848727
EPA 6010D
848878
92621331018
Basin 4
EPA 3010A
848727
EPA 6010D
848878
Date: 10/25/2022 02:36 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 139 of 165

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project:
Pace Project No.:
WASTE CHARACTERIZATION
92621331
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Batch
92621331001
GP-1 2-3'
EPA 3050
851671
EPA 6020
851684
92621331002
GP-2 2-3'
EPA 3050
851671
EPA 6020
851684
92621331003
GP-3 2-3'
EPA 3050
851671
EPA 6020
851684
92621331004
GP-4 2-3'
EPA 3050
851671
EPA 6020
851684
92621331005
GP-5 2-3'
EPA 3050
851671
EPA 6020
851684
92621331006
GP-6 2-3'
EPA 3050
851671
EPA 6020
851684
92621331007
GP-7 2-3'
EPA 3050
851671
EPA 6020
851684
92621331008
HA-1 2-3'
EPA 3050
851671
EPA 6020
851684
92621331009
HA-2 2-3'
EPA 3050
851671
EPA 6020
851684
92621331010
SURFACE BASIN 3
EPA 3050
851671
EPA 6020
851684
92621331015
Basin 1
EPA 7470A
845066
EPA 7470A
845240
92621331016
Basin 2
EPA 7470A
845066
EPA 7470A
845240
92621331017
Basin 3
EPA 7470A
845983
EPA 7470A
846075
92621331018
Basin 4
EPA 7470A
845983
EPA 7470A
846075
92621331001
GP-1 2-3'
EPA 7471
850454
EPA 7471
850656
92621331002
GP-2 2-3'
EPA 7471
850454
EPA 7471
850656
92621331003
GP-3 2-3'
EPA 7471
850454
EPA 7471
850656
92621331004
GP-4 2-3'
EPA 7471
850454
EPA 7471
850656
92621331005
GP-5 2-3'
EPA 7471
850454
EPA 7471
850656
92621331006
GP-6 2-3'
EPA 7471
850454
EPA 7471
850656
92621331007
GP-7 2-3'
EPA 7471
850454
EPA 7471
850656
92621331008
HA-1 2-3'
EPA 7471
850454
EPA 7471
850656
92621331009
HA-2 2-3'
EPA 7471
850454
EPA 7471
850656
92621331010
SURFACE BASIN 3
EPA 7471
850454
EPA 7471
850656
92621331001
GP-1 2-3'
EPA 3546
720089
EPA 8270E
720305
92621331002
GP-2 2-3'
EPA 3546
720089
EPA 8270E
720305
92621331003
GP-3 2-3'
EPA 3546
720089
EPA 8270E
720305
92621331004
GP-4 2-3'
EPA 3546
720089
EPA 8270E
720305
92621331005
GP-5 2-3'
EPA 3546
720089
EPA 8270E
720305
92621331006
GP-6 2-3'
EPA 3546
720089
EPA 8270E
720305
92621331007
GP-7 2-3'
EPA 3546
720089
EPA 8270E
720305
92621331008
HA-1 2-3'
EPA 3546
719449
EPA 8270E
719810
92621331009
HA-2 2-3'
EPA 3546
719449
EPA 8270E
719810
92621331010
SURFACE BASIN 3
EPA 3546
720089
EPA 8270E
720305
92621331011
GP-1 2-3'
EPA 5035A/5030B
718270
EPA 8260D
718400
92621331012
GP-6 2-3'
EPA 5035A/5030B
718270
EPA 8260D
718400
92621331013
HA-1 2-3'
EPA 5035A/5030B
718270
EPA 8260D
718400
92621331014
HA-2 2-3'
EPA 5035A/5030B
718270
EPA 8260D
718400
92621331001
GP-1 2-3'
SW-846
718782
92621331002
GP-2 2-3'
SW-846
718782
92621331003
GP-3 2-3'
SW-846
718782
92621331004
GP-4 2-3'
SW-846
718782
92621331005
GP-5 2-3'
SW-846
718782
92621331006
GP-6 2-3'
SW-846
718782
92621331007
GP-7 2-3'
SW-846
718782
REPORT OF LABORATORY
ANALYSIS
This report shall not be reproduced, except
in full,
Date: 10/25/2022 02:36
PM
without the written consent of Pace Analytical Services, LLC.
Page 140 of 165

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project:
WASTE CHARACTERIZATION
Pace Project No.:
92621331
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Batch
92621331008
HA-1 2-3'
SW-846
718782
92621331009
HA-2 2-3'
SW-846
718782
92621331010
SURFACE BASIN 3
SW-846
718782
92621331011
GP-1 2-3'
SW-846
718782
92621331012
GP-6 2-3'
SW-846
718782
92621331013
HA-1 2-3'
SW-846
718782
92621331014
HA-2 2-3'
SW-846
718782
92621331001
GP-1 2-3'
EPA 1010B
718757
92621331002
GP-2 2-3'
EPA 1010B
718757
92621331003
GP-3 2-3'
EPA 1010B
718757
92621331004
GP-4 2-3'
EPA 1010B
718757
92621331005
GP-5 2-3'
EPA 1010B
718757
92621331006
GP-6 2-3'
EPA 1010B
718757
92621331007
GP-7 2-3'
EPA 1010B
718757
92621331008
HA-1 2-3'
EPA 1010B
718757
92621331009
HA-2 2-3'
EPA 1010B
718989
92621331010
SURFACE BASIN 3
EPA 1010B
718989
92621331001
GP-1 2-3'
SM 2540 G
1914084
SM 2540G
1914084
92621331002
GP-2 2-3'
SM 2540 G
1914085
SM 2540G
1914085
92621331003
GP-3 2-3'
SM 2540 G
1914085
SM 2540G
1914085
92621331004
GP-4 2-3'
SM 2540 G
1914085
SM 2540G
1914085
92621331005
GP-5 2-3'
SM 2540 G
1914085
SM 2540G
1914085
92621331006
GP-6 2-3'
SM 2540 G
1914085
SM 2540G
1914085
92621331007
GP-7 2-3'
SM 2540 G
1914085
SM 2540G
1914085
92621331008
HA-1 2-3'
SM 2540 G
1914085
SM 2540G
1914085
92621331009
HA-2 2-3'
SM 2540 G
1914085
SM 2540G
1914085
92621331010
SURFACE BASIN 3
SM 2540 G
1914085
SM 2540G
1914085
92621331001
GP-1 2-3'
SM 4500-S2D-2011
718542
SM 4500-S2D-2011
718553
Modified
Modified
92621331002
GP-2 2-3'
SM 4500-S2D-2011
718542
SM 4500-S2D-2011
718553
Modified
Modified
92621331003
GP-3 2-3'
SM 4500-S2D-2011
718542
SM 4500-S2D-2011
718553
Modified
Modified
92621331004
GP-4 2-3'
SM 4500-S2D-2011
718542
SM 4500-S2D-2011
718553
Modified
Modified
92621331005
GP-5 2-3'
SM 4500-S2D-2011
718542
SM 4500-S2D-2011
718553
Modified
Modified
92621331006
GP-6 2-3'
SM 4500-S2D-2011
718542
SM 4500-S2D-2011
718553
Modified
Modified
92621331007
GP-7 2-3'
SM 4500-S2D-2011
718542
SM 4500-S2D-2011
718553
Modified
Modified
92621331008
HA-1 2-3'
SM 4500-S2D-2011
718542
SM 4500-S2D-2011
718553
Modified
Modified
92621331009
HA-2 2-3'
SM 4500-S2D-2011
718542
SM 4500-S2D-2011
718553
Modified
Modified
92621331010
SURFACE BASIN 3
SM 4500-S2D-2011
718542
SM 4500-S2D-2011
718553
Modified
Modified
92621331001
GP-1 2-3'
EPA 9045D
718962
92621331002
GP-2 2-3'
EPA 9045D
718962
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/25/2022 02:36 PM without the written consent of Pace Analytical Services, LLC. Page 141 of 165

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: WASTE CHARACTERIZATION
Pace Project No.: 92621331
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Analytical
Batch
92621331003
GP-3 2-3'
EPA 9045D
718962
92621331004
GP-4 2-3'
EPA 9045D
718962
92621331005
GP-5 2-3'
EPA 9045D
718962
92621331006
GP-6 2-3'
EPA 9045D
718962
92621331007
GP-7 2-3'
EPA 9045D
718962
92621331008
HA-1 2-3'
EPA 9045D
718962
92621331009
HA-2 2-3'
EPA 9045D
718962
92621331010
SURFACE BASIN 3
EPA 9045D
718962
92621331015
Basin 1
EPA 7196A Modified
724325
EPA 7196A
725058
92621331016
Basin 2
EPA 7196A Modified
724325
EPA 7196A
725058
92621331017
Basin 3
EPA 7196A Modified
724325
EPA 7196A
725058
92621331018
Basin 4
EPA 7196A Modified
724325
EPA 7196A
725058
92621331001
GP-1 2-3'
EPA 9012
851927
EPA 9012
852013
92621331002
GP-2 2-3'
EPA 9012
851927
EPA 9012
852013
92621331003
GP-3 2-3'
EPA 9012
851927
EPA 9012
852013
92621331004
GP-4 2-3'
EPA 9012
851927
EPA 9012
852013
92621331005
GP-5 2-3'
EPA 9012 r
851927
EPA 9012
852013
92621331006
GP-6 2-3'
EPA 9012
851927
EPA 9012
852013
92621331007
GP-7 2-3'
EPA 9012
851927
EPA 9012
852013
92621331008
HA-1 2-3'
EPA 9012
851927
EPA 9012
852013
92621331009
HA-2 2-3'
EPA 9012
851927
EPA 9012
852013
92621331010
SURFACE BASIN 3
EPA 9012
851927
EPA 9012
852013
Date: 10/25/2022 02:36 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 142 of 165

us.+tr_I ILIU—. I=tvv-r mIvl-r1UIV'I-UUti3 vU7 5arnple Condition Upon Receipt
Effective Date: 05/12/202205/12/2022
Laboratory receiving samples:
Asheville D Eden❑ Greenwood 0. Huntersville [✓j Raleigh❑ MechanicsvilleF] Atlanta❑ Kernersville❑
SampleUpon . d. Client Name:
't,t WO# : 92'621331
Receipt Project,
Courier: ❑Fed Ex ❑UPS ❑U5 5
❑ Commercial ❑pace ❑Other: II II II I ! I
92621331
Packing Material: ❑Bubble Wrap
Thermo me er:
No Seals Intact? ❑Yes
Bubble Bags ❑None ❑ other
�IR Gun ID: R �JJL Type of Ice: dwLt [-]Blue
Correction Factor:
Cooler Temp: �'� l� ,ti Add/Subtract i(r'C)
\
Cooler Temp Corrected (°C): VLA v, ,\'7
USDA Regulated Soil (❑ N/A, water sample)
Did samples originate in a �ivarantine zone within the United States: CA, NY, or SC
(check maps)? 11Yes 1�INn
Chain of Custody Present?
Samples Arrived within Hold Time?
Short Hold Time Analysis (02 hr,)?
Rush Turn Around Time Requested?
5ufficient Volume?
Correct Containers Used?
-Pace Containers Used?
Containers Intact?
Dissolved analysis: Samples Field Filtered?
Sample Labels Match CpC? LA
Lyyes
LJNo
❑N/A
1
ElYes
❑No
❑N/A
2
❑Yes
Q6
❑N/A
3.
❑Yes
dNo
❑N/A
4.
[Ayes
[:]No
El N/A
S.
dyes
❑Nn
❑N/A
6.
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[:]No
❑N/A
Yes
❑Na
❑N/A
7.
Yes
ON.
N/A
8.
ON.,
7'L
91Nn
❑N/A
9.
Date/Initials Person Examining Contents: W {?'iZ
Biological TissFrozen?
❑Yes [:]No2N/A
❑None
Temp should be above freezing to 6'C
[]Samples out of temp Criteria. Samples on ice, cooling process
has 4egun
Did samples originate from a foreign source (in( tttionaily,
including Hawaii and Puerto Rico)? []YesdNg
Cam ments/Disrre n a n ry r
-includes Date/Time/ID/Analysis Matrix: Lam•
Headspace in VOA Viais (>5-6mm)? [I Yes ❑Na 6N/A 10.
Trip Blank Present? []Yes ❑No N/A 11.
Trip Blank Custody Seals present? ❑Yes ❑No LIEN/A
COMMENTS/SAMPLE DISCREPANCY U1'\ Fleld Data Required? [-]Yes ❑No
(71 P'����
)L Lot ID of split containers:
CLIENT NOTIFICATION/RESOLUTION
ersorrzonta ate irne:
Project Manager SCURF Review: Date:
Pr€3ipct Manappr +RF Pwui.'u.
Qualtrax ID: 69614
Page 1 of 2
Page 143 of 165 1

vti.m i ILIV. s--lvv-r F-%m-nuts ll-uuo} 5 vu-t sample uonamon Upon Kecelpt
ace -
Effective Date: 05/121202205/12/2022
*Check mark top half of box if pH and/or dechlorination is verified and
within the acceptance range for preservation samples.
Exceptions: VOA, Coliform, TOC, Oil and Grease, DRO/8015 (water) DOC, LLHg
**Bottom half of box is to list number of bottles
***Check all unpreserved Nitrates for chlorine
Proect Wolf: 92:631 21 __
PM: B�
s Due Date: 08/26/22
CLIENT': 92—Nava NC
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�ruL— vu ueuevei utere rs a aiscrepancyattecting North Larohna compliance samples, a copy of this form will be sent to the North Carolina DENR Certification Office (i.e.
Out of hold, incorrect preservative, out of temp, incorrect containers.
Qualtrax ID: 69614
Page 2 of 2 Page 144 of 165

' Gi�iPi rQ L--v r rkrvi nury i-uuoi vu ilvaampie Lon aition upon Keceipt
Effective Date: 05112/202205/12/202Z
*Check mark top half of box if pH and/or dechlorination is verified and
within the acceptance range for preservation samples.
Exceptions: VOA, Conform, TOC, Oil and Grease, DRO/8015 (water} DOC, LLHg
*'"Bottom half of box is to list number of bottles
***Check all unpreserved Nitrates for chlorine
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adjusted added
yr il'i�CYCI riie�c ID d wscrepaacy anectsng Nortn tarouna compliance samples, a copy of this form will tre sent to the North Carolina DENR Certification Office (i.e.
Out of hold, incorrect preservative, out of temp, incorrect containers,
Qualtrax ID: 69614 Page 2 of 2 Page 145 of 165

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Page 146 of 165

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Page 147 of 165

ANALYTICAL ENVIRONMENTAL SERVICES, INC.
AES
August 29, 2022
Bonnie Vang
Pace Analytical Services, Inc.
9800 Kincey Ave Suite 100
Huntersville NC 28078-8400
RE: 92621331
Dear Bonnie Vang: Order No: 2208Q56
Analytical Environmental Services, Inc. received 10 samples on 8/24/2022 9:48:00 AM
for the analyses presented in following report.
"No problems were encountered during the analyses except as noted in the Case Narrative or by qualifiers in
the report or QC Summary. Additionally, all results for the associated Quality Control samples were within
EPA and/or AES established limits.
AES' certifications are as follows:
-NELAP/Florida State Laboratory ID E87582 for analysis of Non -Potable Water, Solid & Chemical Materials,
Air & Emissions for Organics, and Drinking Water Microbiology & Metals, effective 07/01/22-06/30/23.
-North Carolina Certification number 562 for analysis of Surface Water, Groundwater, Effluent, effective until
12/31 /22. 0 "
-South Carolina Environmental Laboratory Certification number 98016003 effective until 6/30/23.
These results relate only to the items tested as received. This report may only be reproduced in full and with
written permission from the laboratory.
If you have any questions regarding these test results, please feel free to call.
Sincerely,
��risr
Haris Bejdic
Project Manager
3080 Presi4ential Drive • Atlanta, Georgia 30340 -Tel: 770.457,8177 • Fax: 770.457-S188 • Toll F.,e:800.972.4889
www.aesatlanta.com
Page 148 of 165
Page 1 of 18

Chain of Custody
PASI Charlotte Laboratory
acle nalytf )
,+
wwN,�FCNahb-cow
11II1IHIfl1IIIIIII�III��llll��lllll�ll��
'Z'0�,� �
Workorder: 92821331
1Norkorder Name: WASTE CHARACTERIZATION
Results Requested By, 8l2W2022
Fie rt 11nV*h;o Ta
Subcnntraat to
R u6s[ed Anal sls
Bonnie Vang
AES
Pace Analytical Chad atte
p.0.
BV 92 21331
9800 KinceyAve. Suite 100
3080 Presidential Dr,
Huntemville- NC 29078
Atlanta, GAS 30340
Phone {7D4)875-9092
Email- bonnie.vang pacelabs.corn
,State of sample Origin_ NO
PreserVedConte Iners
=
zolfact
Item sampla Id
DatelTima "10 Eo
matrix
LA13 USE ONLY
1 OP. 12-21
$11B1202210:45 92621331001
Solid
]
X
2 Gig-22-2'
811&202210;55 92521331M
Sakld
1
X
3 GP-3 2.T
M612022 11165 9262133tow
$tdl4
X
d GPA 2-3
EW1612022 11:30 92921331004
901ld
j
X
5 GP-5 Z-31
811WIDL12 12'01) 926213310066
Solid
X
e GP52-3'
M6120221210 92621331W
witt
k
7 GP-72-3'
&1$120221140 92fi21331007
solid
1
XC
8 NAB l 2-3'
Q11e12022 13-U0 92621331008
Solid
_
9 11A-22•3'
6f9$1 =13:15 92521331009
Sold
1
X
10 SURF 9ASIN 3
811WZD22 13:30 92621331010
Solid
X.'{
11
12
13
1
Thursday. Augmt 19. 2022 5-45:D1 PM
FMT•A4LL-C-002reu04 24Mafrh20a9 Page i c,f ='
Page 2 of 18

Transfers Waned By
I
2
3
Cooler Tam nerature a
P hursday. AUgwst 18 2p22 5.45.03 Ph1
datENTimo- Racelvo-d By D�tarrlrna
I i �c-Butyl-4,G-dinitraphenol
An suv (Z,4,5-Tp)
2,4,5-T
°C—T Custodv Seal Y or N Received on -ice Y or N Samples Intact Y or N
FMT-ALL-C-002rev.W 24Mamh2009
Pane 2 of 2
Page 3 of 18

Analytical Environmental Services, Inc
Date: 29-Aug-22
Client: Pace Analytical Services, Inc.
Project: 92621331 Case Narrative
Lab ID: 2208Q56
Herbicide Analysis by Method 8151:
Due to sample matrix, samples 2208Q56-006A,--007A, -008A, and -010A required dilution during preparation and/or analysis,
resulting in elevated reporting limits.
Page 151 of 165
Page 4 of 18

Analytical Environmental Services, Inc
Date: 29-Aug-22
Client:
Pace Analytical Services, Inc.
Client Sample ID:
GP-1 2-3'
Project Name:
92621331
Collection Date:
8/16/2022 10:45:00 AM
Lab ID:
2208Q56-001
Matrix:
Solid
Reporting
Dilution
Analyses
Result
Qual
Unihate ARatghID
Analyst
Limit
Factor
CHLORINATED HERBICIDES SW8151A
(SW3550C)
2,4,5-T
BRL
38
ug/Kg-dry 341875
1
08/25/2022 16:27
UH
2,4,5-TP (Silvex)
BRL
38
ug/Kg-dry 341875
1
08/25/2022 16:27
UH
2,4-D
BRL
38
ug/Kg-dry 341875
1
08/25/2022 16:27
UH
Dinoseb
BRL
99
ug/Kg-dry 341875
1
08/26/202216:10
UH
Surr: DCAA
80.3
42-120
%REC 341875
1
08/25/2022 16:27
UH
PERCENT MOISTURE D2216
Percent Moisture
13.8
0
wt% R494545
1
08/24/2022 00:00
JW
Qualifiers: • value exceeds maximum contaminant level
BRL Below reporting limit
H Holding times for preparation or analysis exceeded
N Analyte not NELAC certified
B Analyte detected in the associated method blank
> Greater than Result value
E Estimated (value above quantiitatiion range)
S Spike Recovery outside limits due to matrix
Nan See case narrative
F Analyzed in the lab which is a deviation from the method
< Less than Result value
J Estimated value detected below Reporting Limit
Page 152 of 165
Page 5 of 18

Analytical Environmental Services, Inc
Date: 29-Aug-22
Client:
Pace Analytical Services, Inc.
Client Sample ID:
GP-2 2-3'
Project Name:
92621331
Collection Date:
8/16/2022 10:55:00 AM
Lab ID:
2208Q56-002
Matrix:
Solid
Reporting
Dilution
Analyses
Result
Qual
Un�ate A>aat¢la�tD
Analyst
Limit
Factor
CHLORINATED HERBICIDES SW8151A
(SW35500
2,4,5-T
BRL
54
ug/Kg-dry 341875
1
08/25/2022 16:47
UH
2,4,5-TP (Silvex)
BRL
54
ug/Kg-dry 341875
1
08/25/2022 16:47
UH
2,4-D
BRL
54
ug/Kg-dry 341875
1
08/25/2022 16:47
UH
Dinoseb
BRL
140
ug/Kg-dry 341875
1
08/26/202216:31
UH
Surr: DCAA
65.7
42-120
%REC 341875
1
08/25/2022 16:47
UH
PERCENT MOISTURE D2216
Percent Moisture
39.0
0
wt% R494545
1
08/24/2022 00:00
JW
Qualifiers: • value exceeds maximum contaminant level
BRL Below reporting limit
H Holding times for preparation or analysis exceeded
N Analyte not NELAC certified
B Analyte detected in the associated method blank
> Greater than Result value
E Estimated (value above quantiitation range)
S Spike Recovery outside limits due to matrix
Nan See case narrative
F Analyzed in the lab which is a deviation from the method
< Less than Result value
J Estimated value detected below Reporting Limit Page 153 of 165
Page 6 of 18

Analytical Environmental Services, Inc
Date: 29-Aug-22
Client:
Pace Analytical Services, Inc.
Client Sample ID:
GP-3 2-3'
Project Name:
92621331
Collection Date:
8/16/2022 11:05:00 AM
Lab ID:
2208Q56-003
Matrix:
Solid
Reporting
Dilution
Analyses
Result
Qual
Un�ate A>aat¢la�tD
Analyst
Limit
Factor
CHLORINATED HERBICIDES SW8151A
(SW35500
2,4,5-T
BRL
250
ug/Kg-dry 341875
1
08/25/2022 18:55
UH
2,4,5-TP (Silvex)
BRL
250
ug/Kg-dry 341875
1
08/25/2022 18:55
UH
2,4-D
BRL
250
ug/Kg-dry 341875
1
08/25/2022 18:55
UH
Dinoseb
BRL
640
ug/Kg-dry 341875
1
08/26/202216:52
UH
Surr: DCAA
96.9
42-120
%REC 341875
1
08/25/2022 18:55
UH
PERCENT MOISTURE D2216
Percent Moisture
43.0
0
wt% R494545
1
08/24/2022 00:00
JW
Qualifiers: • value exceeds maximum contaminant level
BRL Below reporting limit
H Holding times for preparation or analysis exceeded
N Analyte not NELAC certified
B Analyte detected in the associated method blank
> Greater than Result value
E Estimated (value above quantiitation range)
S Spike Recovery outside limits due to matrix
Nan See case narrative
F Analyzed in the lab which is a deviation from the method
< Less than Result value
J Estimated value detected below Reporting Limit
Page 154 of 165
Page 7 of 18

Analytical Environmental Services, Inc
Date: 29-Aug-22
Client:
Pace Analytical Services, Inc.
Client Sample ID:
GP-4 2-3'
Project Name:
92621331
Collection Date:
8/16/2022 11:30:00 AM
Lab ID:
2208Q56-004
Matrix:
Solid
Reporting
Dilution
Analyses
Result
Qual
Un�ate A>aat¢la�tD
Analyst
Limit
Factor
CHLORINATED HERBICIDES SW8151A
(SW35500
2,4,5-T
BRL
55
ug/Kg-dry 341875
1
08/25/2022 19:16
UH
2,4,5-TP (Silvex)
BRL
55
ug/Kg-dry 341875
1
08/25/2022 19:16
UH
2,4-D
BRL
55
ug/Kg-dry 341875
1
08/25/2022 19:16
UH
Dinoseb
BRL
140
ug/Kg-dry 341875
1
08/26/202218:09
UH
Surr: DCAA
84.2
42-120
%REC 341875
1
08/25/2022 19:16
UH
PERCENT MOISTURE D2216
Percent Moisture
39.7
0
wt% R494545
1
08/24/2022 00:00
JW
Qualifiers: • value exceeds maximum contaminant level
BRL Below reporting limit
H Holding times for preparation or analysis exceeded
N Analyte not NELAC certified
B Analyte detected in the associated method blank
> Greater than Result value
E Estimated (value above quantiitation range)
S Spike Recovery outside limits due to matrix
Nan See case narrative
F Analyzed in the lab which is a deviation from the method
< Less than Result value
J Estimated value detected below Reporting Limit Page 155 of 165
Page 8 of 18

Analytical Environmental Services, Inc
Date: 29-Aug-22
Client:
Pace Analytical Services, Inc.
Client Sample ID:
GP-5 2-3'
Project Name:
92621331
Collection Date:
8/16/2022 12:00:00 PM
Lab ID:
2208Q56-005
Matrix:
Solid
Reporting
Dilution
Analyses
Result
Qual
Un�ate A>aat¢la�tD
Analyst
Limit
Factor
CHLORINATED HERBICIDES SW8151A
(SW35500
2,4,5-T
BRL
52
ug/Kg-dry 341875
1
08/25/2022 19:37
UH
2,4,5-TP (Silvex)
BRL
52
ug/Kg-dry 341875
1
08/25/2022 19:37
UH
2,4-D
BRL
52
ug/Kg-dry 341875
1
08/25/2022 19:37
UH
Dinoseb
BRL
130
ug/Kg-dry 341875
1
08/26/202218:29
UH
Surr: DCAA
83.9
42-120
%REC 341875
1
08/25/2022 19:37
UH
PERCENT MOISTURE D2216
Percent Moisture
36.1
0
wt% R494545
1
08/24/2022 00:00
JW
Qualifiers: • value exceeds maximum contaminant level
BRL Below reporting limit
H Holding times for preparation or analysis exceeded
N Analyte not NELAC certified
B Analyte detected in the associated method blank
> Greater than Result value
E Estimated (value above quantiitation range)
S Spike Recovery outside limits due to matrix
Nan See case narrative
F Analyzed in the lab which is a deviation from the method
< Less than Result value
J Estimated value detected below Reporting Limit Page 156 of 165
Page 9 of 18

Analytical Environmental Services, Inc
Date: 29-Aug-22
Client:
Pace Analytical Services, Inc.
Client Sample ID:
GP-6 2-3'
Project Name:
92621331
Collection Date:
8/16/2022 12:30:00 PM
Lab ID:
2208Q56-006
Matrix:
Solid
Reporting
Dilution
Analyses
Result
Qual
Un�ate A>aat¢la�tD
Analyst
Limit
Factor
CHLORINATED HERBICIDES SW8151A
(SW35500
2,4,5-T
BRL
60
ug/Kg-dry 341875
1
08/25/202219:58
UH
2,4,5-TP (Silvex)
BRL
300
ug/Kg-dry 341875
5
08/26/2022 14:25
UH
2,4-D
BRL
300
ug/Kg-dry 341875
5
08/26/202214:25
UH
Dinoseb
BRL
150
ug/Kg-dry 341875
1
08/26/202218:50
UH
Surr: DCAA
79.8
42-120
%REC 341875
1
08/25/2022 19:58
UH
PERCENT MOISTURE D2216
Percent Moisture
44.8
0
wt% R494545
1
08/24/2022 00:00
JW
Qualifiers: • value exceeds maximum contaminant level
BRL Below reporting limit
H Holding times for preparation or analysis exceeded
N Analyte not NELAC certified
B Analyte detected in the associated method blank
> Greater than Result value
E Estimated (value above quantiitation range)
S Spike Recovery outside limits due to matrix
Nan See case narrative
F Analyzed in the lab which is a deviation from the method
< Less than Result value
J Estimated value detected below Reporting Limit
Page 157 of 165
Page 10 of 18

Analytical Environmental Services, Inc
Date: 29-Aug-22
Client:
Pace Analytical Services, Inc.
Client Sample ID:
GP-7 2-3'
Project Name:
92621331
Collection Date:
8/16/2022 12:40:00 PM
Lab ID:
2208Q56-007
Matrix:
Solid
Reporting
Dilution
Analyses
Result
Qual
Un�ate A>aat¢la�tD
Analyst
Limit
Factor
CHLORINATED HERBICIDES SW8151A
(SW35500
2,4,5-T
BRL
51
ug/Kg-dry 341875
1
08/25/2022 20:19
UH
2,4,5-TP (Silvex)
BRL
250
ug/Kg-dry 341875
5
08/26/2022 14:46
UH
2,4-D
BRL
250
ug/Kg-dry 341875
5
08/26/202214:46
UH
Dinoseb
BRL
130
ug/Kg-dry 341875
1
08/26/202219:11
UH
Surr: DCAA
80.1
42-120
%REC 341875
1
08/25/2022 20:19
UH
PERCENT MOISTURE D2216
Percent Moisture
35.4
0
wt% R494545
1
08/24/2022 00:00
JW
Qualifiers: • value exceeds maximum contaminant level
BRL Below reporting limit
H Holding times for preparation or analysis exceeded
N Analyte not NELAC certified
B Analyte detected in the associated method blank
> Greater than Result value
E Estimated (value above quantiitation range)
S Spike Recovery outside limits due to matrix
Nan See case narrative
F Analyzed in the lab which is a deviation from the method
< Less than Result value
J Estimated value detected below Reporting Limit Page 158 of 165
Page 11 of 18

Analytical Environmental Services, Inc
Date: 29-Aug-22
Client:
Pace Analytical Services, Inc.
Client Sample ID:
HA-1 2-3'
Project Name:
92621331
Collection Date:
8/16/2022 1:00:00 PM
Lab ID:
2208Q56-008
Matrix:
Solid
Reporting
Dilution
Analyses
Result
Qual
Un�ate A>aat¢la�tD
Analyst
Limit
Factor
CHLORINATED HERBICIDES SW8151A
(SW35500
2,4,5-T
BRL
53
ug/Kg-dry 341875
1
08/25/2022 21:43
UH
2,4,5-TP (Silvex)
BRL
53
ug/Kg-dry 341875
1
08/25/2022 21:43
UH
2,4-D
BRL
270
ug/Kg-dry 341875
5
08/26/202215:07
UH
Dinoseb
BRL
140
ug/Kg-dry 341875
1
08/26/202219:32
UH
Surr: DCAA
85.2
42-120
%REC 341875
1
08/25/2022 21:43
UH
PERCENT MOISTURE D2216
Percent Moisture
38.2
0
wt% R494545
1
08/24/2022 00:00
JW
Qualifiers: • value exceeds maximum contaminant level
BRL Below reporting limit
H Holding times for preparation or analysis exceeded
N Analyte not NELAC certified
B Analyte detected in the associated method blank
> Greater than Result value
E Estimated (value above quantiitation range)
S Spike Recovery outside limits due to matrix
Nan See case narrative
F Analyzed in the lab which is a deviation from the method
< Less than Result value
J Estimated value detected below Reporting Limit Page 159 of 165
Page 12 of 18

Analytical Environmental Services, Inc
Date: 29-Aug-22
Client:
Pace Analytical Services, Inc.
Client Sample ID:
HA-2 2-3'
Project Name:
92621331
Collection Date:
8/16/2022 1:15:00 PM
Lab ID:
2208Q56-009
Matrix:
Solid
Reporting
Dilution
Analyses
Result
Qual
Un�ate A>aat¢la�tD
Analyst
Limit
Factor
CHLORINATED HERBICIDES SW8151A
(SW35500
2,4,5-T
BRL
92
ug/Kg-dry 341875
1
08/25/2022 20:39
UH
2,4,5-TP (Silvex)
BRL
92
ug/Kg-dry 341875
1
08/25/2022 20:39
UH
2,4-D
BRL
92
ug/Kg-dry 341875
1
08/25/2022 20:39
UH
Dinoseb
BRL
240
ug/Kg-dry 341875
1
08/26/202219:53
UH
Surr: DCAA
69.7
42-120
%REC 341875
1
08/25/2022 20:39
UH
PERCENT MOISTURE D2216
Percent Moisture
46.5
0
wt% R494545
1
08/24/2022 00:00
JW
Qualifiers: • value exceeds maximum contaminant level
BRL Below reporting limit
H Holding times for preparation or analysis exceeded
N Analyte not NELAC certified
B Analyte detected in the associated method blank
> Greater than Result value
E Estimated (value above quantiitation range)
S Spike Recovery outside limits due to matrix
Nan See case narrative
F Analyzed in the lab which is a deviation from the method
< Less than Result value
J Estimated value detected below Reporting Limit Page 160 of 165
Page 13 of 18

Analytical Environmental Services, Inc
Date: 29-Aug-22
Client:
Pace Analytical Services, Inc.
Client Sample ID:
SURFACE BASIN 3
Project Name:
92621331
Collection Date:
8/16/2022 1:30:00 PM
Lab ID:
2208Q56-010
Matrix:
Solid
Reporting
Dilution
Analyses
Result
Qual
Un�ate A>aat¢la�tD
Analyst
Limit
Factor
CHLORINATED HERBICIDES SW8151A
(SW35500
2,4,5-T
BRL
67
ug/Kg-dry 341875
1
08/25/2022 21:00
UH
2,4,5-TP (Silvex)
BRL
340
ug/Kg-dry 341875
5
08/26/2022 15:49
UH
2,4-D
BRL
67
ug/Kg-dry 341875
1
08/25/2022 21:00
UH
Dinoseb
BRL
170
ug/Kg-dry 341875
1
08/26/2022 21:44
UH
Surr: DCAA
69
42-120
%REC 341875
1
08/25/2022 21:00
UH
PERCENT MOISTURE D2216
Percent Moisture
51.0
0
wt% R494545
1
08/24/2022 00:00
JW
Qualifiers: • value exceeds maximum contaminant level
BRL Below reporting limit
H Holding times for preparation or analysis exceeded
N Analyte not NELAC certified
B Analyte detected in the associated method blank
> Greater than Result value
E Estimated (value above quantiitation range)
S Spike Recovery outside limits due to matrix
Nan See case narrative
F Analyzed in the lab which is a deviation from the method
< Less than Result value
J Estimated value detected below Reporting Limit
Page 161 of 165
Page 14 of 18

ANALyricAL
ENVIRONMENTAL.
AES SERVICES, INC.
1. Client Name: Pace Analytical Services, Inc.
SAMPLE/COOLER RECEIPT CHECKLIST
2. Carrier: FedEx ❑� UPS ❑ USPS ❑ Client ❑ Courier❑ Othei
Yes No N/A
3.
4.
5.
6.
7.
8.
9.
10.
11.
12.
AES Work Order Number: 2208Q56
Details
Clear Save as
Comments
Shipping container/cooler received in good condition?
U
damaged ❑ leaking ❑ other❑
Custody seals present on shipping container?
•
Custody seals intact on shipping container?
•
Temperature blanks present?
•
Cooler temperature(s) within limits of 0-6°C? [See item 13 and 14 for
temperature recordings.]
O
O
®
Cooling initiated for recently collected samples / ice
present ❑
Chain of Custody (COC) present?
•
Chain of Custody signed, dated, and timed when relinquished and received?
•
Sampler name and/or signature on COC?
•
Were all samples received within holding time?
•
TAT marked on the COC?
•
If no TAT indicated, proceeded with standard TAT per Terms & Conditions. ❑
13. Cooler 1 Temperature 1•6 °C Cooler 2 Temperature
14. Cooler 5 Temperature °C Cooler 6 Temperature
15. Comments:
16.
17.
18.
19.
20.
21.
22.
23.
24.
25.
26.
°C Cooler 3 Temperature °C Cooler 4 Temperature °C
°C Cooler 7 Temperature °C Cooler 8 Temperature °C
I certify that I have completed sections 1-15 (dated initials). HIM 8/24/22
Yes No N/A Details Comments
Were sample containers intact upon receipt?
•
Custody seals present on sample containers?
O
Custody seals intact on sample containers?
0Q
•
Do sample container labels match the COC?
O
O
O
incomplete info --1 illegible ❑
no label ❑ other ❑
Are analyses requested indicated on the COC?
•
Were all of the samples listed on the COC received?
O
®
samples received but not listed on COC
samples listed on COC not received
Was the sample collection date/time noted?
•
Did we receive sufficient sample volume for indicated analyses?
•
Were samples received in appropriate containers?
•
O
Were VOA samples received without headspace (< 1/4" bubble)?
•
Were trip blanks submitted?
•
listed on COC ❑ not listed on COC
27. Comments:
This section only applies to samples where pH can be I certify that I have completed sections 16-27 (dated initials). HM 8/24/22
checked at Sample Receipt. Yes No N/A Details Comments
28. Have containers needing chemical preservation been checked? * •
29. Containers meet preservation guidelines? I •
30. Was pH adjusted at Sample Receipt? •
' Note: Certain analyses require chemical preservation but must be checked in the laboratory and not upon Sample Receipt such as Coliforms, VOCs and Oil & Grease/TPH.
This also excludes metals by EPA 200.7, 200.8 and 245.1 which will be verified between 16 and 24 hours after preservation.
I certify that I have completed sections 28-30 (dated initials). HM 8/24/22
Page 162 of 165
Checklist 7.9.20 Rev 3
Page 15 of 18

Analytical Environmental Services, Inc Date: 29-Aug-22
Client: Pace Analytical Services, Inc. ANALYTICAL QC SUMMARY REPORT
Project Name: 92621331
Workorder: 2208Q56 BatchID• 341875
Sample ID: MB-341875
Client ID:
Units:
ug/Kg Run No: Prep Date: 08/24/2022
494780
SampleType: MBLK
TestCode:
CHLORINATED HERBICIDES SW8151A BatchID08/24/2022
34W51ysis Date: Seq No:
11553555
Analyte
Result
RPT Limit SPK value SPK Ref Val %REC
Low Limit High Limit RPIZ"f Val %RPD
RPD Limit
2,4,5-T BRL 33
2,4,5-TP (Silvex) BRL 33 f
2,4-D BRL 33
Dinoseb BRL 85
Surr: DCAA 103.8 0 166.7 62.3 42 120
Sample ID: LCS-341875
Client ID:
Units: ug/Kg
Prep Date: 08/24/2022
Run No: 494780
SampleType: LCS
TestCode: CHLORINATED HERBICIDES SW8151A
BatchID: 341875
Analysis Date: 08/24/2022
Seq No: 11553554
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit
High Limit RPD Ref Val %RPD
RPD Limit Qual
2,4,5-T
111.5
33
166.7
66.9
50.5
120
2,4,5-TP (Silvex)
104.1
33
166.7
62.5
52.8
120
2,4-D
111.2
33
166.7
66.7
50.6
120
Surr: DCAA
109.3
0
166.7
65.6
42
120
Sample ID: 2208090-001BMS
Client ID:
Units: ug/Kg-dry Prep Date: 08/24/2022
Run No: 494780
SampleType: MS
TestCode: CHLORINATED HERBICIDES SW8151A
BatchID: 341875 Analysis Date: 08/24/2022
Sell No: 11553552
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit Hi�i imit RPD Ref Val %RPD
RPD Limit Qual
2,4,5-T
140.8
37
185.5
75.9
40.6
120
2,4,5-TP (Silvex)
130.4
37
185.5
70.3
42
120
2,4-D
145.2
37
185.5
78.3
40.3
118
Surr: DCAA
136.9
0
185.5
73.8
42
120
Sample ID: 2208090-001BMSD
Client ID:
Units: ug/Kg-dry Prep Date: 08/24/2022
Run No: 494780
SampleType: MSD
TestCode: CHLORINATED HERBICIDES SW8151A
BatchID: 341875 Analysis Date: 08/24/2022
Seq No: 11553553
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit High Limit RPD Ref Val %RPD
RPD Limit Qual
Qualifiers: > Greater than Result value < Less than Result value B Analyte detected in the associated method blank
BRL Below reporting limit E Estimated (value above quantitation range) H Holding times for preparation or analysis exceeded
J Estimated value detected below Reporting Limit N Analyte not NELAC certified R RPD outside limits due to matrix
Rpt Lim Reporting Limit S Spike Recovery outside limits due to matrix Page 163 of 165
Page 16 of 18

Analytical Environmental Services, Inc Date: 29-Aug-22
Client: Pace Analytical Services, Inc. ANALYTICAL QC SUMMARY REPORT
Project Name: 92621331
Workorder: 2208Q56 BatchID• 341875
Sample ID: 2208090-001BMSD
Client ID:
Units:
ug/Kg-cRyln No: Prep Date: 08/24/2022
494780
SampleType: MSD
TestCode:
CHLORINATED HERBICIDES SW8151A Batchl18/24/2022
34MSlysis Date: Seq No:
11553553
Analyte
Result
RPT Limit SPK value SPK Ref Val %REC
Low Limit High Limit RPQdWf Val %RPD
RPD Limit
2,4,5-T
135.7
37
185.5
73.2
40.6
120
140.8
3.64
23.8
2,4,5-TP (Silvex)
117.0
37
185.5
63.1
42
120
130.4
10.9
23.1
2,4-D
131.2
37
185.5
70.7
40.3
118
145.2
10.2
24.9
Surr: DCAA
132.1
0
185.5
71.2
42
120
136.9
0
0
Qualifiers: > Greater than Result value
BRL Below reporting limit
J Estimated value detected below Reporting Limit
Rpt Lim Reporting Limit
< Less than Result value
E Estimated (value above quantitation range)
N Analyte not NELAC certified
S Spike Recovery outside limits due to matrix
B Analyte detected in the associated method blank
H Holding times for preparation or analysis exceeded
R RPD outside limits due to matrix
Page 164 of 165
Page 17 of 18

Page 165 of 165
Page 18 of 18