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NCG020330_2023 DMR_20240119 (5)
• %% eurofins Environment Testing ANALYTICAL REPORT PREPARED FOR Attn: Daniel Christman 3M Company 4191 Hwy 87 South Moncure, North Carolina 27559 Generated 12/19/2023 2:23:22 PM JOB DESCRIPTION 3M WMS - WW Inorganics Pittsboro, NC JOB NUMBER 410-152225-1 Eurofins Lancaster Laboratories Environment Testing, LLC 2425 New Holland Pike Lancaster PA 17601 Page 1 of 23 k�`� E0L See page two for job notes and contact information. g o 111 Eurofins Lancaster Laboratories Environment Testing, LLC Job Notes This report may not be reproduced except in full, and with written approval from the laboratory. The results relate only to the samples tested. For questions please contact the Project Manager at the e-mail address or telephone number listed on this page. Analytical test results meet all requirements of the associated regulatory program (i.e., NELAC (TNI), DoD, and ISO 17025) unless otherwise noted under the individual analysis. Authorization Generated 12/19/2023 2:23:22 PM Authorized for release by Nicole Brown,Project Manager Nicole.Brown@et.eurofinsus.com (717)471-3265 Eurofins Lancaster Laboratories is a laboratory within Eurofins Lancaster Laboratories Environment Testing, LLC,a company within Eurofins Environment Testing Group of Companies Page 2 of 23 12/19/2023 Eurofins Lancaster Laboratories Environment Testing, LLC Compliance Statement Analytical test results meet all requirements of the associated regulatory program (e.g., NELAC (TNI), DoD, and ISO 17025) unless otherwise noted under the individual analysis. Data qualifiers are applied to note exceptions. Noncompliant quality control (QC) is further explained in narrative comments. • QC results that exceed the upper limits and are associated with non-detect samples are qualified but further narration is not required since the bias is high and does not change a non-detect result. Further narration is also not required with QC blank detection when the associated sample concentration is non-detect or more than ten times the level in the blank. Matrix QC may not be reported if insufficient sample or site-specific QC samples were not submitted. In these situations, to demonstrate precision and accuracy at a batch level, a LCS/LCSD is performed, unless otherwise specified in the method. Surrogate and/or isotope dilution analyte recoveries (if applicable)which are outside of the QC window are confirmed unless attributed to a dilution or otherwise noted in the narrative. Regulated compliance samples (e.g. SDWA, NPDES) must comply with the associated agency requirements/permits. Measurement uncertainty values, as applicable, are available upon request. Test results relate only to the sample tested. Clients should be aware that a critical step in a chemical or microbiological analysis is the collection of the sample. Unless the sample analyzed is truly representative of the bulk of material involved, the test results will be meaningless. If you have questions regarding the proper techniques of collecting samples, please contact us. We cannot be held responsible for sample integrity, however, unless sampling has been performed by a member of our staff. Times are local to the area of activity. Parameters listed in the 40 CFR Part 136 Table II as "analyze immediately" and tested in the laboratory are not performed within 15 minutes of collection. This report shall not be reproduced except in full, without the written approval of the laboratory. WARRANTY AND LIMITS OF LIABILITY- In accepting analytical work, we warrant the accuracy of test results for the sample as submitted. The foregoing express warranty is exclusive and is given in lieu of all other warranties, expressed or implied, except as otherwise agreed. We disclaim any other warranties, expressed or implied, including a warranty of fitness for particular purpose and warranty of merchantability. In no event shall Eurofins Lancaster Laboratories Environmental, LLC be liable for indirect, special, consequential, or incidental damages including, but not limited to, damages for loss of profit or goodwill regardless of(A)the negligence (either sole or concurrent) of Eurofins Lancaster Laboratories Environmental and (B)whether Eurofins Lancaster Laboratories Environmental has been informed of the possibility of such damages. We accept no legal responsibility for the purposes for which the client uses the test results. Except as otherwise agreed, no purchase order or other order for work shall be accepted by Eurofins Lancaster Laboratories Environmental which includes any conditions that vary from the Standard Terms and Conditions, and Eurofins Lancaster Laboratories Environmental hereby objects to any conflicting terms contained in any acceptance or order submitted by client. 77( Page 3 of 23 12/19/2023 Client: 3M Company Laboratory Job ID:410-152225-1 Project/Site: 3M WMS-WW Inorganics Pittsboro, NC Table of Contents U Cover Page 1 Table of Contents 4 Definitions/Glossary 5 Case Narrative 6 Detection Summary 7 Client Sample Results 8 QC Sample Results 9 QC Association Summary 15 Lab Chronicle 18 Certification Summary 19 Method Summary 20 Sample Summary 21 Chain of Custody 22 Receipt Checklists 23 Eurofins Lancaster Laboratories Environment Testing LLC Page 4 of 23 12/19/2023 Definitions/Glossary Client:3M Company Job ID: 410-152225-1 Project/Site: 3M WMS-WW Inorganics Pittsboro, NC Qualifiers Metals Qualifier Qualifier Description J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value. General Chemistry Qualifier Qualifier Description cn Refer to Case Narrative for further detail Fl MS and/or MSD recovery exceeds control limits. H Sample was prepped or analyzed beyond the specified holding time.This does not meet regulatory requirements. HF Parameter with a holding time of 15 minutes.Test performed by laboratory at client's request.Sample was analyzed outside of hold time. J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value. s Seeded Control Blank(SCB)Recovery High Glossary Abbreviation These commonly used abbreviations may or may not be present in this report. u Listed under the"D"column to designate that the result is reported on a dry weight basis %R Percent Recovery CFL Contains Free Liquid CFU Colony Forming Unit CNF Contains No Free Liquid DER Duplicate Error Ratio(normalized absolute difference) Dil Fac Dilution Factor DL Detection Limit(DoD/DOE) DL,RA,RE,IN Indicates a Dilution,Re-analysis,Re-extraction,or additional Initial metals/anion analysis of the sample DLC Decision Level Concentration(Radiochemistry) EDL Estimated Detection Limit(Dioxin) LOD Limit of Detection(DoD/DOE) LOQ Limit of Quantitation(DoD/DOE) MCL EPA recommended"Maximum Contaminant Level" MDA Minimum Detectable Activity(Radiochemistry) MDC Minimum Detectable Concentration(Radiochemistry) MDL Method Detection Limit ML Minimum Level(Dioxin) MPN Most Probable Number MQL Method Quantitation Limit NC Not Calculated ND Not Detected at the reporting limit(or MDL or EDL if shown) NEG Negative/Absent POS Positive/Present PQL Practical Quantitation Limit PRES Presumptive QC Quality Control RER Relative Error Ratio(Radiochemistry) RL Reporting Limit or Requested Limit(Radiochemistry) RPD Relative Percent Difference,a measure of the relative difference between two points TEF Toxicity Equivalent Factor(Dioxin) TEQ Toxicity Equivalent Quotient(Dioxin) TNTC Too Numerous To Count Eurofins Lancaster Laboratories Environment Testing, LLC Page 5 of 23 12/19/2023 Case Narrative Client: 3M Company Job ID: 410-152225-1 Project: 3M WMS -WW Inorganics Pittsboro, NC Job ID: 410-152225-1 Eurofins Lancaster Laboratories Environment Job Narrative 410-152225-1 4 Analytical test results meet all requirements of the associated regulatory program listed on the Accreditation/Certification Summary Page unless otherwise noted under the individual analysis. Data qualifiers are applied to indicate exceptions. Noncompliant quality control (QC)is further explained in narrative comments. • Matrix QC may not be reported if insufficient sample or site-specific QC samples were not submitted. In these situations,to demonstrate precision and accuracy at a batch level, a LCS/LCSD may be performed, unless otherwise specified in the method. • Surrogate and/or isotope dilution analyte recoveries(if applicable)which are outside of the QC window are confirmed unless attributed to a dilution or otherwise noted in the narrative. Regulated compliance samples(e.g. SDWA, NPDES)must comply with the associated agency requirements/permits. Receipt The sample was received on 11/22/2023 10:12 AM. Unless otherwise noted below,the sample arrived in good condition, and, where required, properly preserved and on ice. The temperatures of the 3 coolers at receipt time were 0.3°C, 1.8°C and 3.3°C Receipt Exceptions The Field Sampler was not listed on the Chain of Custody.The client responded that the field sampler was Faelan Hoese. Volume was not submitted for TSS OF-002(410-152225-1) HPLC/IC No additional analytical or quality issues were noted,other than those described above or in the Definitions/Glossary page. Metals No additional analytical or quality issues were noted,other than those described above or in the Definitions/Glossary page. General Chemistry Method 2540D_SingleDry: The following sample was analyzed outside time I of analytical holding time because the volume for TSS was made available with only on a few minutes remaining in hold time : OF-002(410-152225-1). No additional analytical or quality issues were noted,other than those described above or in the Definitions/Glossary page. Eurofins Lancaster Laboratories Environment Testing, LLC Page 6 of 23 12/19/2023 Detection Summary Client: 3M Company Job ID:410-152225-1 Project/Site: 3M WMS-WW Inorganics Pittsboro, NC Client Sample ID: OF-002 Lab Sample ID: 410-152225-1 Analyte Result Qualifier RL MDL Unit Dil Fac D Method Prep Type Sulfate 16 7.5 2.5 mg/L 5 EPA 300.0 R2.1 Total/NA Copper 0.0012 0.0010 0.00036 mg/L 1 200.8 Rev 5.4 Total Recoverable El Iron 0.048 J 0.050 0.020 mg/L 1 200.8 Rev 5.4 Total Recoverable Turbidity 60 4.0 4.0 NTU 4 2130B-2011 Total/NA Total Suspended Solids 1.8 J H cn 4.8 1.6 mg/L 1 2540D-2011 Total/NA Cyanide,Total 0.0061 J 0.010 0.0050 mg/L 1 335.4 Total/NA Total Kjeldahl Nitrogen 0.64 J 1.0 0.50 mg/L 1 351.2 Total/NA pH 8.0 HF 0.01 0.01 S.U. 1 4500 H+B-2011 Total/NA Ammonia as N 0.052 J F1 0.10 0.050 mg/L 1 EPA 350.1 Total/NA This Detection Summary does not include radiochemical test results. Eurofins Lancaster Laboratories Environment Testing, LLC Page 7 of 23 12/19/2023 Client Sample Results Client: 3M Company Job ID:410-152225-1 Project/Site: 3M WMS-WW Inorganics Pittsboro, NC Client Sample ID: OF-002 Lab Sample ID: 410-152225-1 Date Collected: 11/21/23 12:30 Matrix:Wastewater Date Received: 11/22/23 10:12 Method: EPA 300.0 R2.1 -Anions, Ion Chromatography Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Fluoride ND 1.0 0.45 mg/L 12/14/23 08:20 5 Sulfate 16 7.5 2.5 mg/L 12/16/23 01:53 5 6 Method: EPA 200.8 Rev 5.4-Metals(ICP/MS)-Total Recoverable Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Antimony ND 0.0010 0.00020 mg/L 11/29/23 08:58 12/04/23 21:00 1 Chromium ND 0.0020 0.00055 mg/L 11/29/23 08:58 12/04/23 21:00 1 Copper 0.0012 0.0010 0.00036 mg/L 11/29/23 08:58 12/04/23 21:00 1 Iron 0.048 J 0.050 0.020 mg/L 11/29/23 08:58 12/04/23 21:00 1 Lead ND 0.00050 0.00012 mg/L 11/29/23 08:58 12/04/23 21:00 1 Nickel ND 0.0010 0.00040 mg/L 11/29/23 08:58 12/04/23 21:00 1 Selenium ND 0.0010 0.00028 mg/L 11/29/23 08:58 12/04/23 21:00 1 Zinc ND 0.010 0.0040 mg/L 11/29/23 08:58 12/04/23 21:00 1 Method: EPA 245.1 -Mercury(CVAA) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Mercury ND 0.00020 0.000079 mg/L 11/29/23 14:12 12/04/23 13:06 1 General Chemistry Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac HEM(Oil&Grease)(1664B) ND 5.9 1.6 mg/L 12/11/23 07:43 1 Turbidity(SM 2130B-2011) 60 4.0 4.0 NTU 11/22/23 19:30 4 Total Suspended Solids(SM 1.8 J H cn 4.8 1.6 mg/L 11/30/23 10:06 1 2540D-2011) Cyanide,Total(EPA 335.4) 0.0061 J 0.010 0.0050 mg/L 12/04/23 13:00 12/04/23 17:10 1 Total Kjeldahl Nitrogen(EPA 351.2) 0.64 J 1.0 0.50 mg/L 12/18/23 15:30 12/19/23 13:51 1 Nitrate Nitrite as N(EPA 353.2) ND 0.10 0.040 mg/L 12/01/23 11:11 1 Total Phosphorus as P(EPA 365.1) ND 0.10 0.050 mg/L 11/30/23 13:30 12/06/23 17:19 1 Chemical Oxygen Demand(EPA ND 75 25 mg/L 11/28/23 10:28 1 410.4) pH(SM 4500 H+B-2011) 8.0 HF 0.01 0.01 S.U. 11/30/23 23:04 1 Biochemical Oxygen Demand(SM ND s 2.0 2.0 mg/L 11/22/23 19:30 1 5210 B-2016) Ammonia as N(EPA 350.1) 0.052 J F1 0.10 0.050 mg/L 11/29/23 16:19 1 Eurofins Lancaster Laboratories Environment Testing, LLC Page 8 of 23 12/19/2023 QC Sample Results Client: 3M Company Job ID:410-152225-1 Project/Site: 3M WMS-WW Inorganics Pittsboro, NC Method: EPA 300.0 R2.1 -Anions, Ion Chromatography Lab Sample ID: MB 410-453769/5 Client Sample ID: Method Blank Matrix:Water Prep Type:Total/NA Analysis Batch:453769 MB MB Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Fluoride ND 0.20 0.090 mg/L 12/14/23 02:16 1 Lab Sample ID: LCS 410-453769/3 Client Sample ID: Lab Control Sample U Matrix:Water Prep Type:Total/NA Analysis Batch:453769 Spike LCS LCS %Rec Analyte Added Result Qualifier Unit D %Rec Limits Fluoride 0.750 0.787 mg/L 105 90_110 Lab Sample ID: LCSD 410-453769/4 Client Sample ID: Lab Control Sample Dup Matrix:Water Prep Type: Total/NA Analysis Batch:453769 Spike LCSD LCSD %Rec RPD Analyte Added Result Qualifier Unit D %Rec Limits RPD Limit Fluoride 0.750 0.789 mg/L 105 90-110 0 20 Lab Sample ID: MB 410-454836/5 Client Sample ID: Method Blank Matrix:Water Prep Type:Total/NA Analysis Batch:454836 MB MB Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Sulfate ND 1.5 0.50 mg/L 12/15/23 14:27 1 Lab Sample ID: LCS 410-454836/3 Client Sample ID: Lab Control Sample Matrix:Water Prep Type:Total/NA Analysis Batch:454836 Spike LCS LCS %Rec Analyte Added Result Qualifier Unit D %Rec Limits Sulfate 7.50 6.88 mg/L 92 90_110 Lab Sample ID: LCSD 410-454836/4 Client Sample ID: Lab Control Sample Dup Matrix:Water Prep Type:Total/NA Analysis Batch:454836 Spike LCSD LCSD %Rec RPD Analyte Added Result Qualifier Unit D %Rec Limits RPD Limit Sulfate 7.50 6.98 mg/L 93 90_110 1 20 Method: 200.8 Rev 5.4 - Metals (ICP/MS) Lab Sample ID: MB 410-447930/1-A Client Sample ID: Method Blank Matrix:Water Prep Type:Total Recoverable Analysis Batch:449990 Prep Batch:447930 MB MB Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Antimony ND 0.0010 0.00020 mg/L 11/29/23 08:58 12/04/23 20:24 1 Chromium ND 0.0020 0.00055 mg/L 11/29/23 08:58 12/04/23 20:24 1 Copper ND 0.0010 0.00036 mg/L 11/29/23 08:58 12/04/23 20:24 1 Iron ND 0.050 0.020 mg/L 11/29/23 08:58 12/04/23 20:24 1 Lead ND 0.00050 0.00012 mg/L 11/29/23 08:58 12/04/23 20:24 1 Nickel ND 0.0010 0.00040 mg/L 11/29/23 08:58 12/04/23 20:24 1 Eurofins Lancaster Laboratories Environment Testing, LLC Page 9 of 23 12/19/2023 QC Sample Results Client: 3M Company Job ID:410-152225-1 Project/Site: 3M WMS-WW Inorganics Pittsboro, NC Method: 200.8 Rev 5.4 - Metals (ICP/MS) (Continued) Lab Sample ID: MB 410-447930/1-A Client Sample ID: Method Blank Matrix:Water Prep Type:Total Recoverable Analysis Batch:449990 Prep Batch:447930 MB MB Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Selenium ND 0.0010 0.00028 mg/L 11/29/23 08:58 12/04/23 20:24 1 Zinc ND 0.010 0.0040 mg/L 11/29/23 08:58 12/04/23 20:24 1 Lab Sample ID: LCS 410-447930/2-A Client Sample ID: Lab Control Sample Matrix:Water Prep Type:Total Recoverable Analysis Batch:449990 Prep Batch:447930 Spike LCS LCS %Rec Analyte Added Result Qualifier Unit D %Rec Limits Antimony 0.100 0.0980 mg/L 98 85.115 Chromium 0.500 0.496 mg/L 99 85.115 Copper 0.500 0.489 mg/L 98 85.115 Iron 5.00 4.97 mg/L 99 85.115 Lead 0.0500 0.0487 mg/L 97 85.115 Nickel 0.500 0.491 mg/L 98 85.115 Selenium 0.100 0.0991 mg/L 99 85-115 Zinc 0.500 0.497 mg/L 99 85-115 Method: 245.1 - Mercury (CVAA) Lab Sample ID: MB 410-448123/1-A Client Sample ID: Method Blank Matrix:Water Prep Type:Total/NA Analysis Batch:449855 Prep Batch:448123 MB MB Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Mercury ND 0.000080 0.000032 mg/L 11/29/23 14:12 12/04/23 12:34 1 Lab Sample ID: LCS 410-448123/2-A Client Sample ID: Lab Control Sample Matrix:Water Prep Type:Total/NA Analysis Batch:449855 Prep Batch:448123 Spike LCS LCS %Rec Analyte Added Result Qualifier Unit D %Rec Limits Mercury 0.000400 0.000452 mg/L 113 85-115 Method: 1664B - HEM and SGT-HEM Lab Sample ID: MB 410-452280/1 Client Sample ID: Method Blank Matrix:Water Prep Type: Total/NA Analysis Batch:452280 MB MB Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac HEM(Oil&Grease) ND 5.0 1.4 mg/L 12/11/23 07:43 1 Lab Sample ID: LCS 410-452280/2 Client Sample ID: Lab Control Sample Matrix:Water Prep Type:Total/NA Analysis Batch:452280 Spike LCS LCS %Rec Analyte Added Result Qualifier Unit D %Rec Limits HEM(Oil&Grease) 40.0 37.5 mg/L 94 78-114 Eurofins Lancaster Laboratories Environment Testing, LLC Page 10 of 23 12/19/2023 QC Sample Results Client: 3M Company Job ID:410-152225-1 Project/Site: 3M WMS-WW Inorganics Pittsboro, NC Method: 1664B - HEM and SGT-HEM (Continued) Lab Sample ID: LCSD 410-452280/3 Client Sample ID: Lab Control Sample Dup Matrix:Water Prep Type:Total/NA Analysis Batch:452280 Spike LCSD LCSD %Rec RPD Analyte Added Result Qualifier Unit D %Rec Limits RPD Limit HEM(Oil&Grease) 40.0 37.4 mg/L 93 78.114 0 13 Method: 2130B-2011 -Turbidity U Lab Sample ID: MB 410-446603/3 Client Sample ID: Method Blank Matrix:Water Prep Type:Total/NA Analysis Batch:446603 MB MB Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Turbidity ND 1.0 1.0 NTU 11/22/23 19:30 1 Lab Sample ID: LCS 410-446603/4 Client Sample ID: Lab Control Sample Matrix:Water Prep Type:Total/NA Analysis Batch:446603 Spike LCS LCS %Rec Analyte Added Result Qualifier Unit D %Rec Limits Turbidity 10.0 10 NTU 102 86.110 Method: 2540D-2011 -Solids, Total Suspended (TSS) Lab Sample ID: MB 410-448515/1 Client Sample ID: Method Blank Matrix:Water Prep Type:Total/NA Analysis Batch:448515 MB MB Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Total Suspended Solids ND 3.0 1.0 mg/L 11/30/23 10:06 1 Lab Sample ID: LCS 410-448515/2 Client Sample ID: Lab Control Sample Matrix:Water Prep Type:Total/NA Analysis Batch:448515 Spike LCS LCS %Rec Analyte Added Result Qualifier Unit D %Rec Limits Total Suspended Solids 150 142 mg/L 94 89.105 Method: 335.4 -Cyanide, Total Lab Sample ID: MB 410-449840/2-A Client Sample ID: Method Blank Matrix:Water Prep Type:Total/NA Analysis Batch:449926 Prep Batch:449840 MB MB Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Cyanide,Total ND 0.010 0.0050 mg/L 12/04/23 13:00 12/04/23 16:24 1 Lab Sample ID: LCS 410-449840/1-A Client Sample ID: Lab Control Sample Matrix:Water Prep Type: Total/NA Analysis Batch:449926 Prep Batch:449840 Spike LCS LCS %Rec Analyte Added Result Qualifier Unit D %Rec Limits Cyanide,Total 0.200 0.200 mg/L 100 90-110 Eurofins Lancaster Laboratories Environment Testing, LLC Page 11 of 23 12/19/2023 QC Sample Results Client: 3M Company Job ID:410-152225-1 Project/Site: 3M WMS-WW Inorganics Pittsboro, NC Method: 351.2 - Nitrogen, Total Kjeldahl Lab Sample ID: MB 410-455400/2-A Client Sample ID: Method Blank Matrix:Water Prep Type:Total/NA Analysis Batch:455901 Prep Batch:455400 MB MB Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Total Kjeldahl Nitrogen ND 1.0 0.50 mg/L 12/18/23 15:30 12/19/23 13:36 1 Lab Sample ID: LCS 410-455400/1-A Client Sample ID: Lab Control Sample U Matrix:Water Prep Type:Total/NA Analysis Batch:455901 Prep Batch:455400 Spike LCS LCS %Rec Analyte Added Result Qualifier Unit D %Rec Limits Total Kjeldahl Nitrogen 4.86 4.75 mg/L 98 90-110 Method: 353.2 - Nitrogen, Nitrate-Nitrite Lab Sample ID: MB 410-449096/87 Client Sample ID: Method Blank Matrix:Water Prep Type:Total/NA Analysis Batch:449096 MB MB Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Nitrate Nitrite as N ND 0.10 0.040 mg/L 12/01/23 10:51 1 Lab Sample ID: LCS 410-449096/85 Client Sample ID: Lab Control Sample Matrix:Water Prep Type:Total/NA Analysis Batch:449096 Spike LCS LCS %Rec Analyte Added Result Qualifier Unit D %Rec Limits Nitrate Nitrite as N 2.50 2.24 mg/L 90 90-110 Lab Sample ID: LCSD 410-449096/86 Client Sample ID: Lab Control Sample Dup Matrix:Water Prep Type: Total/NA Analysis Batch:449096 Spike LCSD LCSD %Rec RPD Analyte Added Result Qualifier Unit D %Rec Limits RPD Limit Nitrate Nitrite as N 2.50 2.33 mg/L 93 90-110 4 20 Method: 365.1 - Phosphorus, Total Lab Sample ID: MB 410-447115/1-A Client Sample ID: Method Blank Matrix:Water Prep Type:Total/NA Analysis Batch:450977 Prep Batch:447115 MB MB Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Total Phosphorus as P ND 0.10 0.050 mg/L 11/30/23 13:30 12/06/23 17:13 1 Lab Sample ID: LCS 410-447115/2-A Client Sample ID: Lab Control Sample Matrix:Water Prep Type:Total/NA Analysis Batch:450977 Prep Batch:447115 Spike LCS LCS %Rec Analyte Added Result Qualifier Unit D %Rec Limits Total Phosphorus as P 1.43 1.37 mg/L 96 90-110 Eurofins Lancaster Laboratories Environment Testing, LLC Page 12 of 23 12/19/2023 QC Sample Results Client: 3M Company Job ID:410-152225-1 Project/Site: 3M WMS-WW Inorganics Pittsboro, NC Method: 410.4 -COD Lab Sample ID: MB 410-447633/35 Client Sample ID: Method Blank Matrix:Water Prep Type:Total/NA Analysis Batch:447633 MB MB Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Chemical Oxygen Demand ND 75 25 mg/L 11/28/23 11:32 1 Lab Sample ID: MB 410-447633/5 Client Sample ID: Method Blank 13 Matrix:Water Prep Type:Total/NA Analysis Batch:447633 MB MB Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Chemical Oxygen Demand ND 75 25 mg/L 11/28/23 09:48 1 Lab Sample ID: LCS 410-447633/36 Client Sample ID: Lab Control Sample Matrix:Water Prep Type: Total/NA Analysis Batch:447633 Spike LCS LCS %Rec Analyte Added Result Qualifier Unit D %Rec Limits Chemical Oxygen Demand 500 509 mg/L 102 90-110 Lab Sample ID: LCS 410-447633/6 Client Sample ID: Lab Control Sample Matrix:Water Prep Type:Total/NA Analysis Batch:447633 Spike LCS LCS %Rec Analyte Added Result Qualifier Unit D %Rec Limits Chemical Oxygen Demand 500 510 mg/L 102 90-110 Method: 4500 H+ B-2011 - pH Lab Sample ID: LCS 410-449072/3 Client Sample ID: Lab Control Sample Matrix:Water Prep Type:Total/NA Analysis Batch:449072 Spike LCS LCS %Rec Analyte Added Result Qualifier Unit D %Rec Limits pH 7.00 7.0 S.U. 99 95-105 Method: 5210 B-2016 - BOD, 5-Day Lab Sample ID: SCB 410-447210/4 Client Sample ID: Method Blank Matrix:Water Prep Type:Total/NA Analysis Batch:447210 SCB SCB Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Biochemical Oxygen Demand 1.09 s 0.0000010 0.0000010 mg/L 11/22/23 11:46 1 Lab Sample ID: USB 410-447210/2 Client Sample ID: Method Blank Matrix:Water Prep Type:Total/NA Analysis Batch:447210 USB USB Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Biochemical Oxygen Demand 0.177 0.0000010 0.0000010 mg/L 11/22/23 11:46 1 Eurofins Lancaster Laboratories Environment Testing, LLC Page 13 of 23 12/19/2023 QC Sample Results Client: 3M Company Job ID:410-152225-1 Project/Site: 3M WMS-WW Inorganics Pittsboro, NC Method: 5210 B-2016 - BOD, 5-Day (Continued) Lab Sample ID: LCS 410-447210/49 Client Sample ID: Lab Control Sample Matrix:Water Prep Type:Total/NA Analysis Batch:447210 Spike LCS LCS %Rec Analyte Added Result Qualifier Unit D %Rec Limits Biochemical Oxygen Demand 198 179 mg/L 90 85.115 Lab Sample ID: LCS 410-447210/71 Client Sample ID: Lab Control Sample U Matrix:Water Prep Type:Total/NA Analysis Batch:447210 Spike LCS LCS %Rec Analyte Added Result Qualifier Unit D %Rec Limits Biochemical Oxygen Demand 198 189 mg/L 95 85.115 Method: EPA 350.1 - Nitrogen, Ammonia Lab Sample ID: MB 410-448599/17 Client Sample ID: Method Blank Matrix:Water Prep Type:Total/NA Analysis Batch:448599 MB MB Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Ammonia as N ND 0.10 0.050 mg/L 11/29/23 15:40 1 Lab Sample ID: LCS 410-448599/15 Client Sample ID: Lab Control Sample Matrix:Water Prep Type:Total/NA Analysis Batch:448599 Spike LCS LCS %Rec Analyte Added Result Qualifier Unit D %Rec Limits Ammonia as N 1.99 2.02 mg/L 102 90-110 Lab Sample ID: LCSD 410-448599/16 Client Sample ID: Lab Control Sample Dup Matrix:Water Prep Type:Total/NA Analysis Batch:448599 Spike LCSD LCSD %Rec RPD Analyte Added Result Qualifier Unit D %Rec Limits RPD Limit Ammonia as N 1.99 2.04 mg/L 102 90-110 1 15 Lab Sample ID:410-152225-1 MS Client Sample ID:OF-002 Matrix:Wastewater Prep Type:Total/NA Analysis Batch:448599 Sample Sample Spike MS MS %Rec Analyte Result Qualifier Added Result Qualifier Unit D %Rec Limits Ammonia as N 0.052 J F1 2.49 2.17 F1 mg/L 85 90-110 Lab Sample ID:410-152225-1 DU Client Sample ID: OF-002 Matrix:Wastewater Prep Type:Total/NA Analysis Batch:448599 Sample Sample DU DU RPD Analyte Result Qualifier Result Qualifier Unit D RPD Limit Ammonia as N 0.052 J F1 0.0503 J mg/L 4 20 Eurofins Lancaster Laboratories Environment Testing, LLC Page 14 of 23 12/19/2023 QC Association Summary Client: 3M Company Job ID: 410-152225-1 Project/Site: 3M WMS-WW Inorganics Pittsboro, NC HPLC/IC Analysis Batch: 453769 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 410-152225-1 OF-002 Total/NA Wastewater EPA 300.0 R2.1 MB 410-453769/5 Method Blank Total/NA Water EPA 300.0 R2.1 LCS 410-453769/3 Lab Control Sample Total/NA Water EPA 300.0 R2.1 LCSD 41 0-4 53 7 6 9/4 Lab Control Sample Dup Total/NA Water EPA 300.0 R2.1 Analysis Batch:454836 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 410-152225-1 OF-002 Total/NA Wastewater EPA 300.0 R2.1 8 MB 410-454836/5 Method Blank Total/NA Water EPA 300.0 R2.1 LCS 410-454836/3 Lab Control Sample Total/NA Water EPA 300.0 R2.1 LCSD 410-454836/4 Lab Control Sample Dup Total/NA Water EPA 300.0 R2.1 Metals Prep Batch:447930 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 410-152225-1 OF-002 Total Recoverable Wastewater 200.8 Rev 5.4 MB 410-447930/1-A Method Blank Total Recoverable Water 200.8 Rev 5.4 LCS 410-447930/2-A Lab Control Sample Total Recoverable Water 200.8 Rev 5.4 Prep Batch:448123 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 410-152225-1 OF-002 Total/NA Wastewater 245.1 MB 410-448123/1-A Method Blank Total/NA Water 245.1 LCS 410-448123/2-A Lab Control Sample Total/NA Water 245.1 Analysis Batch:449855 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 410-152225-1 OF-002 Total/NA Wastewater 245.1 448123 MB 410-448123/1-A Method Blank Total/NA Water 245.1 448123 LCS 410-448123/2-A Lab Control Sample Total/NA Water 245.1 448123 Analysis Batch: 449990 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 410-152225-1 OF-002 Total Recoverable Wastewater 200.8 Rev 5.4 447930 MB 410-447930/1-A Method Blank Total Recoverable Water 200.8 Rev 5.4 447930 LCS 410-447930/2-A Lab Control Sample Total Recoverable Water 200.8 Rev 5.4 447930 General Chemistry Analysis Batch:446603 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 410-152225-1 OF-002 Total/NA Wastewater 2130B-2011 MB 410-446603/3 Method Blank Total/NA Water 2130B-2011 LCS 4 1 0-44 66 0 3/4 Lab Control Sample Total/NA Water 2130B-2011 Prep Batch:447115 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 410-152225-1 OF-002 Total/NA Wastewater 365.1 MB 410-447115/1-A Method Blank Total/NA Water 365.1 LCS 410-447115/2-A Lab Control Sample Total/NA Water 365.1 Eurofins Lancaster Laboratories Environment Testing, LLC Page 15 of 23 12/19/2023 QC Association Summary Client: 3M Company Job ID: 410-152225-1 Project/Site: 3M WMS-WW Inorganics Pittsboro, NC General Chemistry Analysis Batch: 447210 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 410-152225-1 OF-002 Total/NA Wastewater 5210 B-2016 SCB 410-447210/4 Method Blank Total/NA Water 5210 B-2016 USB 410-447210/2 Method Blank Total/NA Water 5210 B-2016 LCS 41 0-44 72 1 0/49 Lab Control Sample Total/NA Water 5210 B-2016 LCS 410-447210/71 Lab Control Sample Total/NA Water 5210 B-2016 Analysis Batch:447633 Iw Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 410-152225-1 OF-002 Total/NA Wastewater 410.4 MB 410-447633/35 Method Blank Total/NA Water 410.4 MB 410-447633/5 Method Blank Total/NA Water 410.4 LCS 410-447633/36 Lab Control Sample Total/NA Water 410.4 LCS 410-447633/6 Lab Control Sample Total/NA Water 410.4 Analysis Batch:448515 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 410-152225-1 OF-002 Total/NA Wastewater 2540D-2011 MB 410-448515/1 Method Blank Total/NA Water 2540D-2011 LCS 410-448515/2 Lab Control Sample Total/NA Water 2540D-2011 Analysis Batch: 448599 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 410-152225-1 OF-002 Total/NA Wastewater EPA 350.1 MB 410-448599/17 Method Blank Total/NA Water EPA 350.1 LCS 410-448599/15 Lab Control Sample Total/NA Water EPA 350.1 LCSD 410-448599/16 Lab Control Sample Dup Total/NA Water EPA 350.1 410-152225-1 MS OF-002 Total/NA Wastewater EPA 350.1 410-152225-1 DU OF-002 Total/NA Wastewater EPA 350.1 Analysis Batch: 449072 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 410-152225-1 OF-002 Total/NA Wastewater 4500 H+B-2011 LCS 410-449072/3 Lab Control Sample Total/NA Water 4500 H+B-2011 Analysis Batch: 449096 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 410-152225-1 OF-002 Total/NA Wastewater 353.2 MB 410-449096/87 Method Blank Total/NA Water 353.2 LCS 410-449096/85 Lab Control Sample Total/NA Water 353.2 LCSD 410-449096/86 Lab Control Sample Dup Total/NA Water 353.2 Prep Batch:449840 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 410-152225-1 OF-002 Total/NA Wastewater Distill/CN MB 410-449840/2-A Method Blank Total/NA Water Distill/CN LCS 410-449840/1-A Lab Control Sample Total/NA Water Distill/CN Analysis Batch: 449926 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 410-152225-1 OF-002 Total/NA Wastewater 335.4 449840 MB 410-449840/2-A Method Blank Total/NA Water 335.4 449840 Eurofins Lancaster Laboratories Environment Testing, LLC Page 16 of 23 12/19/2023 QC Association Summary Client: 3M Company Job ID: 410-152225-1 Project/Site: 3M WMS-WW Inorganics Pittsboro, NC General Chemistry(Continued) Analysis Batch: 449926(Continued) Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch LLCS 410-449840/1-A Lab Control Sample Total/NA Water 335.4 449840 Analysis Batch:450977 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 410-152225-1 OF-002 Total/NA Wastewater 365.1 447115 MB 410-447115/1-A Method Blank Total/NA Water 365.1 447115 LCS 410-447115/2-A Lab Control Sample Total/NA Water 365.1 447115 0 Analysis Batch: 452280 8 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 410-152225-1 OF-002 Total/NA Wastewater 1664B MB 410-452280/1 Method Blank Total/NA Water 1664B LCS 410-452280/2 Lab Control Sample Total/NA Water 1664B LCSD 410-452280/3 Lab Control Sample Dup Total/NA Water 1664B Prep Batch:455400 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 410-152225-1 OF-002 Total/NA Wastewater 351.2 MB 410-455400/2-A Method Blank Total/NA Water 351.2 LCS 410-455400/1-A Lab Control Sample Total/NA Water 351.2 Analysis Batch:455901 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 410-152225-1 OF-002 Total/NA Wastewater 351.2 455400 MB 410-455400/2-A Method Blank Total/NA Water 351.2 455400 LCS 410-455400/1-A Lab Control Sample Total/NA Water 351.2 455400 Eurofins Lancaster Laboratories Environment Testing, LLC Page 17 of 23 12/19/2023 Lab Chronicle Client: 3M Company Job ID:410-152225-1 Project/Site: 3M WMS-WW Inorganics Pittsboro, NC Client Sample ID: OF-002 Lab Sample ID: 410-152225-1 Date Collected: 11/21/23 12:30 Matrix:Wastewater Date Received: 11/22/23 10:12 Batch Batch Dilution Batch Prepared Prep Type Type Method Run Factor Number Analyst Lab or Analyzed Total/NA Analysis EPA 300.0 R2.1 5 454836 W7FX ELLE 12/16/23 01:53 Total/NA Analysis EPA 300.0 R2.1 5 453769 W7FX ELLE 12/14/23 08:20 Total Recoverable Prep 200.8 Rev 5.4 447930 NU9R ELLE 11/29/23 08:58 Total Recoverable Analysis 200.8 Rev 5.4 1 449990 UCIG ELLE 12/04/23 21:00 Total/NA Prep 245.1 448123 NU9R ELLE 11/29/23 14:12 Total/NA Analysis 245.1 1 449855 UEFS ELLE 12/04/23 13:06 Total/NA Analysis 1664B 1 452280 UYBO ELLE 12/11/23 07:43 9 Total/NA Analysis 2130B-2011 4 446603 UDS7 ELLE 11/22/23 19:30 Total/NA Analysis 2540D-2011 1 448515 M98K ELLE 11/30/23 10:06-12/01/23 06:20' Total/NA Prep Distill/CN 449840 NLE3 ELLE 12/04/23 13:00-12/04/23 14:45' Total/NA Analysis 335.4 1 449926 JCG7 ELLE 12/04/23 17:10 Total/NA Prep 351.2 455400 NLE3 ELLE 12/18/23 15:30-12/18/23 18:30' Total/NA Analysis 351.2 1 455901 JCG7 ELLE 12/19/23 13:51 Total/NA Analysis 353.2 1 449096 Q3HN ELLE 12/01/23 11:11 Total/NA Prep 365.1 447115 PQ9E ELLE 11/30/23 13:30-11/30/23 14:30' Total/NA Analysis 365.1 1 450977 JCG7 ELLE 12/06/23 17:19 Total/NA Analysis 410.4 1 447633 USAE ELLE 11/28/23 10:28 Total/NA Analysis 4500 H+B-2011 1 449072 D19Q ELLE 11/30/23 23:04 Total/NA Analysis 5210 B-2016 1 447210 B6LN ELLE 11/22/23 19:30 Total/NA Analysis EPA 350.1 1 448599 JCG7 ELLE 11/29/23 16:19 'This procedure uses a method stipulated length of time for the process. Both start and end times are displayed. Laboratory References: ELLE=Eurofins Lancaster Laboratories Environment Testing,LLC,2425 New Holland Pike,Lancaster,PA 17601,TEL(717)656-2300 Eurofins Lancaster Laboratories Environment Testing, LLC Page 18 of 23 12/19/2023 Accreditation/Certification Summary Client: 3M Company Job ID:410-152225-1 Project/Site: 3M WMS-WW Inorganics Pittsboro, NC Laboratory: Eurofins Lancaster Laboratories Environment Testing, LLC Unless otherwise noted,all analytes for this laboratory were covered under each accreditation/certification below. Authority Program Identification Number Expiration Date North Carolina(WW/SW) State 521 12-31-23 The following analytes are included in this report,but the laboratory is not certified by the governing authority. This list may include analytes for which the agency does not offer certification. Analysis Method Prep Method Matrix Analyte 2130B-2011 Wastewater Turbidity 2540D-2011 Wastewater Total Suspended Solids EPA 350.1 Wastewater Ammonia as N 10 Eurofins Lancaster Laboratories Environment Testing, LLC Page 19 of 23 12/19/2023 Method Summary Client: 3M Company Job ID: 410-152225-1 Project/Site: 3M WMS-WW Inorganics Pittsboro, NC Method Method Description Protocol Laboratory EPA 300.0 R2.1 Anions,Ion Chromatography EPA ELLE 200.8 Rev 5.4 Metals(ICP/MS) EPA ELLE 245.1 Mercury(CVAA) EPA ELLE 1664E HEM and SGT-HEM 1664B ELLE 2130E-2011 Turbidity SM ELLE 2540D-2011 Solids,Total Suspended(TSS) SM ELLE 335.4 Cyanide,Total EPA ELLE 351.2 Nitrogen,Total Kjeldahl EPA ELLE 353.2 Nitrogen,Nitrate-Nitrite EPA ELLE 365.1 Phosphorus,Total EPA ELLE 410.4 COD EPA ELLE 4500 H+B-2011 pH SM ELLE 5210 B-2016 BOD,5-Day SM ELLE EPA 350.1 Nitrogen,Ammonia EPA ELLE 200.8 Rev 5.4 Preparation,Total Recoverable Metals EPA ELLE 245.1 Preparation,Mercury EPA ELLE a 351.2 Nitrogen,Total Kjeldahl EPA ELLE 365.1 Sample Digestion for Total Phosphorus MCAWW ELLE Distill/CN Distillation,Cyanide None ELLE Protocol References: 1664B=EPA-821-98-002 EPA=US Environmental Protection Agency MCAWW="Methods For Chemical Analysis Of Water And Wastes",EPA-600/4-79-020,March 1983 And Subsequent Revisions. None=None SM="Standard Methods For The Examination Of Water And Wastewater" Laboratory References: ELLE=Eurofins Lancaster Laboratories Environment Testing,LLC,2425 New Holland Pike,Lancaster,PA 17601,TEL(717)656-2300 Eurofins Lancaster Laboratories Environment Testing, LLC Page 20 of 23 12/19/2023 Sample Summary Client: 3M Company Job ID:410-152225-1 Project/Site: 3M WMS-WW Inorganics Pittsboro, NC Lab Sample ID Client Sample ID Matrix Collected Received 410-152225-1 OF-002 Wastewater 11/21/23 12:30 11/22/23 10:12 El Eurofins Lancaster Laboratories Environment Testing, LLC Page 21 of 23 12/19/2023 es Environme Chain of Custody Record tiff eurofins Environment Testing 41 0-1 5 2225 Chain of Custody Sampler Lab PM Carrier Tracking No(s) COC No Brown,Nicole 410-101666-290251 Client Contact: Phone 'E-Mail State of Ongm Page' Daniel Christman Nicole Brown@et eurofinsus corn Page 1 of 1 Company PWSID Job 4 3M Company Analysis Requested Address: Due Date Requested: i i Preservation Codes: 4191 Hwy 87 South A-HCL M-Hexane Cdy. TAT Requested(days): B-NaOH N•None Moncure1 n C-Zn Acetate p-Na2045 w m D-Nitric Acid State.Zip- _ i; O 4- O-Na2S03 NC,27559 Compliance Project: :A Yes A No • .-r I- o E-NaHSO4 R-Na2S2O7 Phone POE - a ii o F-McOH S-H2SO4 919-642-4010(Tel) Purchase Order Requested a H•Amchlor ( q c ,°, H-Ascorbic Acitl T•TSP Dotletahytlrale Email. WOE Z rn w ° I-Ice ll-Acetone w V-MCAA dchristman©mmm.com m 2 . r c O /� K-EOtTA1ef W-pH 4.5 Protect Name Project p v o o 12 T J • Y-Triune 3M WMS-WW Inorganics Pittsboro,NC 41017322 4 ro ; a „v cL-EDT :? z-other (specify) Site SSOWS ~ LL n + cS Other:E m u r r- to y m o Z 10 Z% D o Is LI 2 r a e o i ? A u ' t '1 VI - Sample Matrix o fLLl a cu — 4t E Type (w.w.ar. T. C � c ill N zl orr 0 (j 5.$oua, C Z Sample (C=Comp, o•w..ran, v_ € OI o o o < !9 Sam.le Identification Sample Date Time G=grab) eT-rl.,..,.•.ir) L. 0.. P, rr H r. in P h Special Instructions/Note: Preservation Code, XX N S S N D A N N HB v— 'MI t\17-1(2;3__4 _ Water - ?i M C9o- l2;30 C> Water )[ y y X-?` ?` X_� >+- >+ it : ss _ '� - - - - - �7�--t � tee`--,-' _ EEO � - r 1 . 1 . 1 Possible Hazard identification Sample Disposal(A fee may be assessed if samples are retained longer than I month) Non-Hazard =Flammable 0 Skin Irritant = Poison B = Unknown Radiological =Return To Client =Disposal By Lab =Archive For Months Deliverable Requested I.II,III,IV.Other(specify) Special Instructions/OC Requirements. Empty Kit Relinquished by 'Date Time Method of Shipment Relinquished by (/` Date/Time Comµi Received by Date/Time Company r l 14.44 l2l(L3 - 2' '�C� Relinquished by Date/Time Company Received by Date/Time Company Relinquished by Date/Time Company Received by Date up 2_ Zi / 2' Com�ai)* Cu oily Seals Intact: Custody Seal No.- i c q G Cooler Temperature(s)°C and Other Remarks 0'1-�// 1/ /7j///•%/w('//'_ t .- t ��//t��V' Yes o No ��2 l� 0 Z Jn// ,73 0.3/0., Z.0/f, t( SA/1 Vim 0608202I Page 22 of 23 12/19/2023 Login Sample Receipt Checklist Client:3M Company Job Number:410-152225-1 Login Number: 152225 List Source:Eurofins Lancaster Laboratories Environment Testing,LLC List Number: 1 Creator:Reiff,Nicole L Question Answer Comment The cooler's custody seal is intact. True The cooler or samples do not appear to have been compromised or True tampered with. Samples were received on ice. True Cooler Temperature acceptable,where thermal pres is required(</=6C,not True frozen). Cooler Temperature is recorded. True WV:Container Temp acceptable,where thermal pres is required(</=6C,not N/A frozen). WV: Container Temperature is recorded. N/A COC is present. True COC is filled out in ink and legible. True COC is filled out with all pertinent information. True There are no discrepancies between the containers received and the COC. True Sample containers have legible labels. True 14 Containers are not broken or leaking. True Sample collection date/times are provided. True Appropriate sample containers are used. True Sample bottles are completely filled. True There is sufficient vol.for all requested analyses. True Is the Field Sampler's name present on COC? False Refer to Job Narrative for details. Sample custody seals are intact. N/A VOA sample vials do not have headspace>6mm in diameter(none,if from N/A WV)? Eurofins Lancaster Laboratories Environment Testing,LLC Page 23 of 23 12/19/2023