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Home My WebLink AboutNC0047562_Routine Analytical_20240119® Laboratories LLG ne nt;cr : ' The GEL Group INC November 30, 2023 Chris Cameron Cameron Testing Services, Inc. 219 S. Steele St. Sanford, North Carolina 27330 Re: Routine Analytical Work Order: 645884 Dear Chris Cameron: au3 �e�e � I'Ylel C612.J 20411 savage Road I Charleston SC 29407 8435568171 JAN 19 - -4 n�rDP rInwNIP'IPOES GEL Laboratories, LLC (GEL) appreciates the opportunity to provide the enclosed analytical results for the sample(s) we received on November 17, 2023.17his original data report has been prepared and reviewed in accordance with GEL's standard operating procedures. The samples were delivered with proper chain of custody documentation and signatures. All sample containers arrived without any visible signs of tampering or breakage. Containers indicated on chain of custody did not match what was received. Five vials with liquid were included with one 250mL glass amber bottle.. Test results for NL'LAP or ISO 17025 accredited tests are verified to meet the requirements of those standards, with any exceptions noted. The results reported relate only to the items tested and to the sample as received by the laboratory. These results may not be reproduced except as full reports without approval by the laboratory. Copies of GEL's acereditations and certifications can be found on our website at www.gel.com. Our policy is to provide high quality, personalized analytical services to enable you to meet your analytical needs on time every time. We trust that you will find everything in order and to your satisfaction. If you have any questions, please do not hesitate to call me at (843) 556-8171, ext. 4422. Sincerely, 4' M Adrian Melendrez for Jacob Crook Project Manager Enclosures gel com GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report for CAMT001 Cameron Testing Services Client SDG: 645884 GEL Work Order: 645884 The Qualifiers in this report are defined as follows: A quality control analyte recovery is outside of specified acceptance criteria * Analyte is a Tracer compound Analyte is a surrogate compound U Analyte was analyzed for, but not detected above the MDL, MDA, MDC or LOD. Where the analytical method has been performed under NELAP certification, the analysis has met all of the requirements of the NELAC standard unless qualified on the Certificate of Analysis. The designation ND, if present, appears in the result column when the analyte concentration is not detected above the limit as defined in the U qualifier above. This data report has been prepared and reviewed in accordance with GEL Laboratories LLC standard operating procedures. Please direct any questions to your Project Manager, Jacob Crook. Reviewed by Page 2 of 10 SDG: 645884 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.corn Certificate of Analysis Company : Cameron Testing Services, Inc. Address : 219 S. Steele St. Sanford, North Carolina 27330 Contact: Chris Cameron Project: Routine Analytical Client Sample ID: Hamlet Effluent Project: Sample ID: 645884001 Client Ill: Matrix: Waste Water Collect Date: 02-NOV-23 08:00 Receive Date: 17-NOV-23 Collector: Client Parameter Qualifier Result DI. Mercury Analysis-CVAA EPA 1631 Low Level Mercury Analysis "As Received" Mercury U c0.500 0.200 The following Analytical Methods were performed: Method Description I EPA 1631E Notes: Column headers are defined as follows: Report Date: November 30, 2023 CAMT00122 CAMT001 RL Units PF DF Analyst Date Time Batch Method 0.500 ng/L I LYGI 11/2823 1432 2531474 1 Analyst Comments DF: Dilution Factor Lc/LC: Critical Level DL: Detection Limit PF: Prep Factor MDA: Minimum Detectable Activity RL: Reporting Limit MDC: Minimum Detectable Concentration SQL: Sample Quantitation Limit Page 3 of 10 SDG: 645884 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company : Cameron Testing Services, Inc. Address : 219 S. Steele St. Sanford, North Carolina 27330 Contact: Chris Cameron Project: Routine Analytical Client Sample ID: Trip Blank Sample ID: 645884002 Matrix: BLANK Collect Date: 02-NOV-23 08:0,0 Receive Date: 17-NOV-23 Collector: Client Report Date: November 30, 2023 Project: CAMT00122 Client ID: CAMT001 Parameter Qualifier Result DL RL Units PF DF Analyst Date Time Batch Method Mercury Analysis-CVAA _ EPA 1631 Low Level Mercury Analysis "As Received" Mercury U t0.2 0.200 0.500 ng/1- I LYGI 11/28/23 1322 2531474 1 The following Analytical Methods were performed: Method Description Analyst Comments l EPA 1631 E Notes: Column headers are defined as follows: DF. Dilution Factor Lc/LC: Critical Level DL: Detection Limit PF: Prep Factor MDA: Minimum Detectable Activity RL: Reporting Limit MDC: Minimum Detectable Concentration SQL: Sample Quantitation Limit Page 4 of 10 SDG: 645884 GEL LABORATORIES LLC 2040 Savage Road Charleston, SC 29407 - (843) 556-8171 - www.gel.com QC Summary Cameron Testing Services, Inc. Report Date: November 30, 2023 219 S. Steele St. Page I of Sanford, North Carolina Contact: Chris Cameron Workorder: 645884 Parmname _ _..... NOM Sample Qual QC Units RPD/D% REC% Range Anlst Date Time Vletals Analysis -Mercury 3atch 25�1474 QC120558590.3 LCS Mercury 5.00 5.15 ng/L 103 (77%-123%) LYGI 11/28/2313:1 QC1205585902 MB Mercury QC1205585907 646101003 MS Mercury QC1205586275 646101003 MSD Mercury Notes: U ND ng/L 2.50 U <0.500 2.59 ng/L 87.7 (71 %-125%) 2.50 U <0.500 2.56 ng/L 1.2 86.5 (0%-24%) 1 1 /28/23 13:0 1 1 /28/23 14:0 1 1 /28/23 14:0 The Qualifiers in this report are defined as follows: U Analytc was analyzed for, but not detected above the MDL, MDA, MDC or LOD. J Value is estimated X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier N Mcta15--The Matrix spike sample recovery is not within specified control limits H Analytical holding time was exceeded < Result is less than value reported > Result is greater than value reported h Preparation or preservation holding time was exceeded R Sample results are rejected ^ RPD of sample and duplicate evaluated using +/-R1.. Concentrations are <5X the RL. Qualifier Not Applicable for Radiochemistry. N/A RPD or °Ic,Recovery limits do not apply. ND Analyte concentration is not detected above the detection limit E %difference of sample and SD is >10%. Sample concentration must meet flagging criteria NJ Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Q One or more quality control criteria have not been met. Refer to the applicable narrative or DER, FL3 Mercury was found present at quantifiable concentrations in field blanks received with these samples. Data associated with the blank are deemed invalid for reporting to regulatory agencies Page 5 of 10 SDG: 645884 GEL LABORATORIES LLC 2040 Savage Road Charleston, SC 29407 - (843) 556-8171 - www.gel.com Workorder: 645884 QC Summary Page 2 of N Parmname OM Sample Qual QC Units RPD/D%_ _ REC% Range Anlst Date Time NI Sec case narrative Y Other specific qualifiers were required to properly define the results. Consult case narrative. J See case narrative for an explanation N/A indicates that spike recovery limits do not apply when sample concentration exceeds spike cone. by a factor of 4 or more or %RPD not applicable. ^ The Relative Percent Difference (RPD) obtained from the sample duplicate (DUP) is evaluated against the acceptance criteria when the sample is greater than five times (5X) the contract required detection limit (RL). In cases where either the sample or duplicate value is less than 5X the RL, a control limit of +/- the RL is used to evaluate the DUP result. * Indicates that a Quality Control parameter was not within specifications. For PS, PSD, and .SDR-T results, the values listed are the measured amounts, not final concentrations. Where the analytical method has been performed under NELAP certification, the analysis has met all of the requirements of the NF,LAC standard unless qualified on the QC Summary. Page 6 of 10 SDG: 645884 2A \letals Arsenic IIg= Mercury , 13ariun, Sc- Selenium Cadmium AV Silver Chromium NIR= Misc. RCRA metals Lead (ill f )uutc �. l�n Name: J!i'ylERow —Z-) omcicd l)\- �41 J f,- n Chain of Custody and Analytica F_L Work Order Number: GEL Project Malrn;er Fa.c 14—'I�1r / a' cn Send Results 70: L11 Sample ID •DwaCanurd 00 - — - - - 00 " Far e•unrpredrr-c - indicale Mart and slop,lure rime ' (mmtild7T) Chain of Custody Signatures 2chnc;usttcd 111'(SiLnedI Date Virile 77 Kccct, •d h, (s1_ 3 Should this fj _ sample be coasidernl: •riser _ o � Collected Field sample — JAurtarp) QC F,hemd .lratru( "a "a (hlemm) Coate at ty t.h V 0 'L J p -w+, Muss(] S Charleston. SC''4J(17 1 Request I'hunc- (S4-3) 5564171 Sample Analysis Requested (s (Fill in the number of containers for each test) - Preservative Type (6) Comments Note: extra sample is required for sample F- specific QC — x TA"r Requested: Normal: Dale Ttmc fas Result: I I Yes I I No Select !klivcrablc:I ICofA I IOC. I ddu r orlal Remarks: F Rush: _ Specif}: _(Subject to Surcharge) level I [ ] Level ? I [ Lcccl 3 (]Level I 'or sample shipping and de/iverp details, see Sanrp/e Reeeipr Revienv form (SRRJ ar Loh Rceen rn•� Use On/r: ('usuxh .ka/ lnrucr' ] ] }'as I I .\'n Coe ter Temp. C Smrrp(r Collection Tinhe Zone. [ ]Eastern (] Pacific [ I Central f I Mountain I ]Other. o slue:, of ('us:,rlc N1❑ethc:- Cleat Defarmmcd .-t:,es ter sanepie. a as q u•ePR ES ERYEDJ' (7drs N \ottnal Sastplc.'r6 lnn Hlasd. FU Field Gqu:Want Blank. \IS \lal:ac Spike Sample. \ISU llam Spike (h+phralc S;plr• (G:zh(CnmpnsgrhrlJFdlrreJ Pn!11qutJmatnm.axrirme Date, ilna.„r- Y - livample„as mLiJIlterrJ _ • Time: h^.rn ('„arcs U\I' Urmktng 11 ate. G%v Cr,%md„fner. SW Surface w.-Ver. \YN ((-able (( wcr. W Wamr..ltl. >I:xa' I nrn:J. SO S,NI. SD S-dtmem. tit. Slude'. 3S S,J,J (1'251e.0 od. F• Filter r 11' �� !C[• :a®nle Reapesied ArmNi.czl me:knr ra•<utua•J pp /'� t 11 c S3GUa. 6UI nlrnJ7(Ia J and numhr ot'cont]users pro, OW ri.r each (t c a -'hale . 3, W11W -1-rt{ . 11 8 rC I 'ra•.cr,sn,c ra, a 11A If cdr—lih,nc AeW. NI \mic Acxr. Sll S,.J:um II,Jro„dr. SA Sul:i:rk Ac,d. A:\ %wn b :Ac,ar. IIX tic.m,e. St ti,nlnim Thinntd(ate. f!' VOIU t�"1e: \UN'\ OR POSSI1311•'IIa% a n+pnxnau,eisarJa•J Irareriddhlanl \RIl ('haracicristic Ilarards listed \\'asle In.r Please provi.le one• additiond derails be/m✓ regarc'ing handling and/or disposal concerns, (i.e.: Origin c!(sautp/e(sJ, type pj sire collectedfront, odd matrices. e1c.) I• L - r lantmable/lEtn ilable CO = Corrosive RE = Reactive 7:SCA Rctintated PCS = Polychlorinated hiphern'is L\\'= Listed Waste l F K. P and U-listed a wsles.l Waste code(s): 07'= Other / Unknown (t.e.: llieb /01r pH. asbestos. bert•llurm. irriaarrts. other mirc. twalib hazards. etc.) Description: [F14 I Laboratories irC Q A ANDr V to rvr, v— o Cllcnt: . uA/ —%,jW' la 1 UG me 9llr vv r UXIVI SDG/AWCOC(WwkOrder: d- Received II•y: Date Receiver: Mete AppIl"hlo: PedEx Express PedPx Oround UPS Field Services Courier thee Carrier and Tracking Number Ll 3 rapected lIer trd Information � z • rf Net Counts > 100epm on samples not marked -radioactive", contact the Radiation Ssfety Group for bather invastigation. azard Class Shipped; UN#; A)Shl d DOT 1 pa'rradous? If UN2910, Is the Radioactive Shipment Survey Compliant? Yu_ No` B) Did the client designate the samples are to be r Y trotalroryof �> I A `Y oil n received as radioactive? i� r ,1.. ,�1 zt�,,, •mum Not Counts Observed' (Observed Counts - Area Background Counts): CPM / mR/IIr C) Did the RS O classify the sarnples as radlonctivc7 — -- Classified ass Red I Red 2 Rad 3 D) Did ale client designate samples am hazardous? (0C tioladom lapels oii' • fjy ir d nt deslgW 1 :tp.(s f ,t 0071PIf-, ,?I• :` tTj Jr k a2 Lr11 f f D or H L yes, select Iiazsrda below. H Did the RSO idcnti osaible hazards? PCBs Flsrmablo Foreign Soil RCMA Asbestos Beryllium Other. ecc Sample Re Criteria .__ W � 'X. CeamrentslQualiGers (Required for Non-Cunfondng Iterna) Cjmk Applicable: . brokea Damaged coutaluar Leaking container (Nher (deacrilw) 1 Shipping containers received intact NW scaled? 2 Chain of cut:tody documents included Circle Applicabk: Clbnt concocted and provided 00C COC created upon receipt with shipmtcnt? 3 Sample. requiting cold preservation Preservation Method: Wet ice Ice Packs Dry Ice Nnne Other: *all within (0 5 G do g. C)7a s TEMP: ' temperatures are recordscd Daily check performed arul passed on IR Temperature Device Serial 8:A "Applic): temperature gun? Secon T dsrykr� Device 5 Sample containers intact and sealed? Circle Appfteable: Saab broken Damaged container Loakbog contatnor Other (describe) �nrPle Us sad Containers Affected: �Jf 6 Sany)Ic, acquiring chemical preservation ut proper pii? -_—_- _ Preservation added Laud: If Yes, are Encores or Suil Kits prosant for solids? Yes_ No_ NA —(If yes, take to VOA Pmczcr) 7 Du any samples require Volatile D liquid VOA vials contain add preaervation7 Yes_ Nn_ NA —(If unknown, select No) liquid VOA vials fax of headslace? yes' _A No_ NA_ �»alysis7 — Samplo ID'. and contehwrs arroclod: 8 Satnples n:ceivtxi within holding time? M s and tests affected: ID's and containers affected 9 Sample II )'s on COC match Ill's on baffles? i 10 Date, & time on COC match date & time Circle Applicable: No dates on dxmtamets No times on containers COC missing Info Other (descrifx ) on bottles? 11 Number of containers received match Circle Applicable: No cowabner count on COC Other ( 'be) number indicated on C'OC7 12 Are, suogdd containers identifiable as GEL rnvidcd by use of CBL labels? 13 COC form is properly signed in Circle Applicable: Not mtinquishod Other (describe) relinquished/received sections? Cornmcnfs (Ucc CuntJnwttion Form if needed): — �j V i i S W'cyt-\ 1,\ q u a an c� '-� 2 So r n l a sS xy) �,X—?r co ib w-,, wrill l+r�vi )nCIUCIVoI t) 'SV)'TMe0i PM (orPMA) review Initials _ /I i ` Date r � I1 7 \ •LS Page 8 of IO SDG: 645884 GL-CHL-SR-001 Rov7 List of current GEL Certfiications as of 30 November 2023 State _ — Certification Alabama 42200 Alaska � 17-018 � Alaska Drinking Water — ' SC00012 _ Arkansas 88-00651 CLIA 42DO904046 California 2940 Colorado SC00012 Connecticut PH-0169 i DoD FLAP/ ISO17025 A2LA 2567.01 Florida NELAP E87156 i Foreign Soils Permit P330-15-00283, P330-15-00253 Georgia SC00012 Georgia SDWA 967 _ Hawaii _..__ SC00012 Idaho _ — — SCM 12 _ Illinois NELAP 200029 Indiana C-SC-01 Kansas NELAP E-10332 Kentucky SDWA KY90129 Kentucky Wastewater KY90129 ; Louisiana Drinking Water LA024 Louisiana NELAP 03046 (AI33904) Maine 2023019 Maryland ! 270 Massachusetts M-SCO 12 Massachusetts PFAS Approv Letter i Michigan 9 9976 _ .._.. Mississippi SC00012 Nebraska I - NE-OS-2613 Nevada SC000122024-05 New Hampshire NELAP f 2054 New Jersey NELAP SC002 New Mexico - i SC00012 New York NF,LAP 11501 North Carolina 233 North Carolina SDWA 45709 North Dakota R-158 Oklahoma 2023-152 Pennsylvania NELAP 68-00485 Puerto Rico SC00012 i S. Carolina Radiochem l 10120002 Sanitation Districts of L _- 9255651 South Carolina Chemistry 1 10120001 Tennessee TN 02934 Texas NELAP T104704235-23-21 Utah NELAP SC000122023-38 Vermont I VT87156 Virginia NELAP 466202 Washington C780 Page 9 of 10 SDG: 645884 Metals Technical Case Narrative Cameron Testing Services SDG #: 645884 Product: Mercury Analysis Using the PS Analytical Millennium Automated Mercury Analyzer Analytical Method- EPA 1631E Analvtical Procedure: GL-MA-E-018 REV# 19 Analytical Batch: 2531474 The following samples were analyzed using the above methods and analytical procedurc(s). GEL Sample Ill# Client Sample Identification 645884001 Hamlet Effluent 645884002 Trip Blank 1205585902 Method Blank (MB)CVAF 1205585903 Laboratory Control Sample (LCS) 1205585907 646101003(NonSDGS) Matrix Spike (MS) 1205586275 646101003(NonSDGSD) Matrix Spike Duplicate (MSD) The samples in this SDG were analyzed on an "as received" basis. Data Summary: There are no exceptions, anomalies or deviations from the specified methods. All sample data provided in this report met the acceptance criteria specified in the analytical methods and procedures for initial calibration, continuing calibration, instrument controls and process controls where applicable. Certification Statement Where the analytical method has been performed under NELAP certification, the analysis has met all of the requirements of the NELAC standard unless otherwise noted in the analytical case narrative. Page 10 of 10 SDG: 645884 envirochem SM ANALYTICAL & CONSULTING CHEMISTS Cameron Testing Services, Inc. 219 South Steele St. Sanford NC 27330 Attention: Lab ID Sample ID: 2311-0045 23-62706 Site:2311-0045-01 Test Antimony Copper Lead Nickel Selenium Silver Thallium Zinc Arsenic Beryllium Cadmium Chromium Ammonia Nitrogen Total Kjeldahl Nitrogen (TKN) Total Hardness Total Dissolved Solids (TDS) Total Phosphorus Nitrate Nitrogen (Cale) Nitrite Nitrogen Nitrate+Nitrite-N itroge n Nitrate Nitrogen Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 lab/Fax infb'aenvironmentalchemists.com r1CO01-f15q Z Date of Report: Jan 09, 2024 Customer PO #: 2311-0045 Customer ID: 12090010 Report #: 2023-25860 Project ID: Hamlet Collect DatelTime Matrix 11/7/2023 8:00 AM Water Method EPA 200.7. Rev 4A, 1994 EPA 200.7. Rev 4.4, 1994 EPA 200.7, Rev 4.4, 1994 EPA 200.7, Rev 4.4, 1994 EPA 200.7, Rev 4.4, 1994 EPA 200.7, Rev 4A, 1994 EPA 200.7, Rev 4.4, 1994 EPA 200.7, Rev 4.4. 1994 EPA 2007,.Rev. 4 4, 1994 EPA 200.7, Rev. 4.4, 1994 EPA 200.7, Rev. 4.4, 1994 EPA 200.7, Rev, 4.4, 1994 EPA 350.1, Rev 2.0, 1993 EPA 351.2, Rev. 2.0, 1993 SM 2340 C-2011 SM 2540 C-2015 SM 4500 P (F-H)-2011 EPA 353.2, Rev. 2.0, 1993 EPA 353.2. Rev. 2,0, 1993 Subtraction Method Results Sampled by Client Date Analyzed <0.01 mg/L 11/16/2023 0.011 mg/L 11/16/2023 <0.01 mg/L 11/16/2023 <0.01 mg/L 11/16/2023 <0.01 mg/L 11/16/2023 <0.01 mg/L 11/16/2023 <0.01 mg/L 11/16/2023 0.026 mg/L 11/16/2023 <0.01 mg/L 11/16/2023 <0.01 mg/L 11/16/2023 <0.01 mg/L 11/16/2023 <0.01 mg/L 11/16/2023 < 0.2 mg/L 11/15/2023 < 0.5 mg/L 11/10/2023 17 mg/L 01/09/2024 389 mg/L 11/08/2023 0.69 mg/L 11/13/2023 < 0.02 mg/L 11 /07/2023 20.0mg/L 11/13/2023 20.0 mg/L 11/20/2023 Report #:: 2023-25860 Page 1 of 5 Environmental Chemists, Inc. envirochem 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax ' 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS info(a environmentit lchemists.com Cameron Testing Services, Inc. Date of Report: Jan 09, 2024 219 South Steele St. Customer PO #: 2311-0045 Sanford NC 27330 Customer ID: 12090010 Attention: Report #: 2023-25860 Project ID: Hamlet Lab ID Sample ID: 2311-0045 Collect Date/Time Matrix Sampled by 23-62707 Site: 2311-0045-02 11/7/2023 8:00 AM Water Client Test Method Results Date Analyzed Oil & Grease (O&G) EPA 1664 Rev. B <6.25 mg/L 11/21/2023 Reporting limit elevated due to insufficient sample volume. Cyanide EPA 335.4, Rev. 1.0, 1993 < 0.005 mg/L 11/14/2023 Inorganic Phenols EPA 420.4, Rev 1.0, 1993 <0.005 mg/L 11/20/2023 1, 1, 1 -Trichloroethane EPA 624.1 <0.5 pg/L 11/15/2023 1,1,2,2-Tetrachloroethane EPA 624.1 <0.5pg/L 11/15/2023 1,1,2-Trichloroethane EPA 624.1 <0.5 pg/L 11/15/2023 1,1-Dichloroethane EPA 624.1 <0.5 pg/L 11/15/2023 1, 1 -Dichloroethene EPA 624.1 <0.5 pg/L 11/15/2023 1,2-Dichlorobenzene EPA 624.1 <0.5 pg/L 11/15/2023 1, 2-Dichloroethane EPA 624.1 <0.5 pg/L 11/15/2023 1,2-Dichloropropane EPA 824.1 <0.5 pg/L 11/15/2023 1,3-Dichlorobenzene EPA 624.1 <0.5 pg/L 11/15/2023 1,4-Dichlorobenzene EPA 624.1 <0.5 pg/L 11/15/2023 Acrolein EPA 624.1 <20 pg/L 11/15/2023 Acrylonitrile EPA 624.1 <5 pg/L 11/15/2023 Benzene EPA 624.1 <0.5 pg/L 11/15/2023 Bromodichloromethane EPA 624.1 2.53 pg1L 11/15/2023 Bromoform EPA 624.1 <0.5 pg/L 11/15/2023 Bromomethane EPA 624.1 <0.5 pg/L 11/15/2023 Carbon Tetrachloride EPA 624.1 <0.5 pg/L 11/15/2023 Chlorobenzene EPA 624.1 <0.5 pg/L 11/15/2023 Chloroethane EPA 624.1 <0.5 pg/L 11/15/2023 Chloroform EPA 624.1 17.7 pg/L 11/15/2023 Chloromethane EPA 624.1 <0.5 pg/L 11/15/2023 cis-1,3-Dichloropropene EPA 624.1 <0.5 pg/L 11/15/2023 Report #:: 2023-25860 Page 2 of 5 --"47 F0100-. '. Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 - 910.392.0223 Lab - 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 - 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 - 910.347.5843 Lab/Fax ANALYTICAL 8 CONSULTING CHEMISTS info(raenvironmentalchemistscom Cameron Testing Services, Inc. 219 South Steele St. Sanford NC 27330 Attention: Date of Report: Jan 09, 2024 Customer PO #: 2311-0045 Customer ID: 12090010 Report #: 2023-25860 Project ID: Hamlet Dibromochloromethane EPA 624.1 <0.5 pg/L 11/15/2023 Ethylbenzene EPA 624.1 <0.5 pg/L 11/15/2023 M+P Xylene EPA 624.1 <1.0 pg/L 11/15/2023 Methylene chloride EPA 024.1 <0.5 Ng/L 11/15/2023 ortho-Xylene EPA 624.1 <0.5 pg/L 11/15/2023 Tetrachloroethene EPA 624.1 <0.5 pg/L 11/15/2023 Toluene EPA 624.1 <0.5 pg/L 11/15/2023 Trans- 1,2-Dichloroethene EPA 624.1 <0.5 pg/L 11/15/2023 trans- 1, 3-Dich loropropene EPA 624.1 <0.5pg/L 11/15/2023 Trichloroethene EPA 624.1 <0.5 pg/L 11/15/2023 Trichlorofluoromethane EPA 624.1 <0.5 pg/L 11/15/2023 Vinyl chloride EPA 624.1 <0.5 pg/L 11/15/2023 2,4,6-Trichlorophenol EPA 625.1 <4.76 pg/L 11/08/2023 2,4-Dichlorophenol EPA 625.1 <4.76 pg/L 11/08/2023 2,4-Dimethylphenol EPA625.1 <4.76 pg/L 11/08/2023 2,4-Dinitrophenol EPA 625.1 <23.8 pg/L 11/08/2023 2-Chlorophenol EPA 625.1 <4.76 Ng/L 11/08/2023 2-Methyl-4,6-dinitrophenol EPA 625.1 <23.8 pg/L 11/08/2023 2-Nitrophenol EPA 625.1 <23.8 Ng/L 11/08/2023 4-Chloro-3-methylphenol EPA 625.1 <4.76 pg/L 11 /0812023 4-Nitrophenol EPA 625.1 <23.8 pg/L 11/08/2023 Pentachlorophenol EPA 625.1 <23.8 pg/L 11108/2023 Phenol EPA 625.1 <4.76 pg/L 11/08/2023 1,2 Diphenylhydrazine EPA 625.1 <4.76pg/L 11/08/2023 1,2,4-Trichlorobenzene EPA625A <4.76 pg/L 11/08/2023 1,2-Dichlorobenzene EPA 625.1 <4.76 pg/L 11/08/2023 1,3-Dichlorobenzene EPA 625.1 <4.76 pg/L 11/08/2023 1,4-Dichlorobenzene EPA 625.1 <4.76 pg/L 11/08/2023 1-Methylnaphthalene EPA 625.1 <4.76 ug/L 11/08/2023 2,4-Dinitrotoluene EPA 825.1 <4.76 pg/L 11/08/2023 Report #': 2023.25860 Page 3 of 5 ro,ww--- --71 Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax SSA 710 Bow5ertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS info« environrnentalchemists.com Cameron Testing Services, Inc. Date of Report: Jan 09, 2024 219 South Steele St. Customer PO #: 2311-0045 Sanford NC 27330 Customer ID: 12090010 Attention: Report #: 2023-25860 Project ID: Hamlet 2,6-Dinitrotoluene EPA 625.1 <4.76 pg/L 11/0812023 2-Chloronaphthalene EPA 625.1 <4.76 ug/L 11/08/2023 2-Methyl naphthalene EPA 625.1 <4.76 pg/L 11 /08/2023 3, 3'-Dich lorobenzidine EPA 625.1 <9.52 pg/L 11/08/2023 4-Bromophenyl phenyl ether EPA 625.1 <4.76pg/L 11/08/2023 4-Chlorophenyl phenyl ether EPA 625.1 <4.76 pg/L 11/08/2023 Acenaphthene EPA 625.1 <4.76 ug/L 11/08/2023 Acenaphthylene EPA 625.1 <4.76 pg/L 11/08/2023 Anthracene EPA 625.1 <4.76 pg/L 11/08/2023 Benzidine EPA825.1 <9.52 pg/L 11/08/2023 Benzo (alpyrene EPA 625.1 <4.76 pg/L 11/08/2023 Benzo(a)anthracene EPA 625.1 <4.76 ug/L 11/08/2023 Benzo(b)fluoranthene EPA 625.1 <4.76 pg/L 11/08/2023 Benzo(g, h, i)perylene EPA 625.1 <4.76 pg/L 11/08/2023 Benzo(k)fluoranthene EPA 625.1 <4.76 pg/L 11/08/2023 Bis ( chloromethyl ) ether EPA625A <4,76µg/L 11/08/2023 Bis(2-Chloroethoxy)methane EPA 625.1 <4.76pg/L 11/08/2023 Bis(2-Chloroethyl)ether EPA 625.1 <4.76 pg/L 11/08/2023 Bis(2-Chloroisopropyl)ether EPA 625.1 <4.76pg/L 11/08/2023 Bis(2-ethylhexyl)phthalate EPA 625.1 <4.76 pg/L 11/08/2023 Butylbenzylphthalate EPA 625.1 <4.76 pg/L 11/08/2023 Chrysene EPA 625.1 <4.76 pg/L 11/08/2023 Dibenzo(a, h )anthracene EPA 625.1 <4.76 pg/L 11/08/2023 Diethylphthalate EPA 625.1 <4.76 pg/L 11/08/2023 Dimethylphthalate EPA 625.1 <4.76 u9/L 11/08/2023 Di-n-ButyIphthalate EPA 625.1 <4.76 pg/L 11/08/2023 Di-n-Octylphthalate EPA 625.1 <4.76 pg/L 11/08/2023 Fluoranthene EPA 625.1 <4.76 pg/L 11/08/2023 Fluorene EPA 625.1 <4.76 pg/L 11/08/2023 Hexachlorobenzene EPA 625.1 <4.76 pg/L 11/08/2023 Report #.: 2023-25860 Page 4 of 5 qq Environmental Chemists, Inc. envirochem 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910,392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax ANALYTICAL 8 CONSULTING CHEMISTS inro4environmentalchemists.com Cameron Testing Services, Inc. Date of Report: Jan 09, 2024 219 South Steele St. Customer PO #: 2311-0045 Sanford NC 27330 Customer ID: 12090010 Attention. Report #: 2023-25860 Project ID: Hamlet Hexachlorobutadiene EPA 6251 <4.76 pg/L 11/08/2023 Hexachlorocyclopentadiene EPA 625.1 <23.8pg/L 11/08/2023 Hexachloroethane EPA 625.1 <4.76 pg/L 11/08/2023 I ndeno(1, 2, 3-cd)pyrene EPA 625.1 <4.76 pg/L 11 /08/2023 Isophorone EPA 625.1 <4.76 pg/L 11/08/2023 Naphthalene EPA 625.1 <4.76 pg/L 11/08/2023 Nitrobenzene EPA 625.1 <4.76 pg/L 11/08/2023 N-nitroso-dimethylamine(NDMA) EPA 625A <4.76 pg/L 11/08/2023 N-Nitroso-di-n-propylamine EPA 625.1 <4.76 pg/L 11/08/2023 N-Nitroso-diphenylamine EPA 625.1 <4.76 Ng/L 11/08/2023 Phenanthrene EPA 625.1 <4.76 pg/L 11/08/2023 Pyrene EPA 625.1 <4.76 pg/L 11/08/2023 Comment: r Reviewed by: Report #:: 2023-25660 Page 5 of 5 Environmental Chemist, Inc., Wilmington, NC Lab #94 6602 Windmill Way Wilmington, NC 28405 Sample Receipt Checklist 910.392.0223 Client _ ] �p 11) "'z" Date:'( %, Report Number: _ 2023- Syg p CO of sample: ES ❑ NO ECHEM Pickup Client Delivery ❑ UPS ❑ FedEx ❑ Other ❑ ❑ N/A P'pt ❑ 1. Were custody seals present on the cooler?ES NO al temperature upon ❑ N/A receipt 2. If custody seals were present, were they intact/unbroken? °C Corrected temperature upon receipt---------------------------°C How temperature taken: ❑ Temperature Blank ❑ Against Bottles IR Gun ID: Thomas Traceable S/N 210886869 IR Gun Correction Factor °C: 0.0 YES YES ❑ NO ❑ 3. If temperature of cooler exceeded 6°C, was Project Mgr./QA notified? YES NO ❑ 4. Were per custody procedures (relinquished/received) followed? NO S. Were sample ID's listed on the COC? YES ❑ NO 6. Were samples ID's listed on sample containers? YES ❑ NO 7. Were collection date and time listed on the COC? YES ❑ NO 8. Were tests to be performed listed on the COC? YES ❑ NO 9. Did samples arrive in proper containers for each test? YES ❑ NO 10. Did samples arrive in good condition for each test? YES O NO 11. Was adequate sample volume available?' YES ❑ NO 12. Were samples received within proper holding time for requested tests? YES ❑ NO 13. Were acid preserved samples received at a pH of <2? YES ❑ NO ]A Were cyanide samples received at a pH >12? ❑ YES O NO 15. Were sulfide samples received at a pH >9? YES i YES ❑ NO ❑ 16. Were NH3/TKN/Phenol received at a chlorine residual of <0.5 m/L? ** ❑ NO 17. Were Sulfide/Cyanide received at a chlorine residual of <0.5 m/L? YES ❑ NO 16. Were orthophosphate samples filtered in the field within 15 minutes? * TOC/Volatiles are pH checked at time of analysis and recorded on the benchsheet. ** Bacteria samples are checked for Chlorine at time of analysis and recorded on the benchsheet. Sample Preservation: (Must be completed for any sample(s) incorrectly preserved or with headspace) Sample(s) were received incorrectly preserved and were adjusted accordingly by adding (circle one): H2SO4 HNO3 HCI NaOH Time of preservation: If more than one preservative is needed, notate in comments below Note: Notify customer service immediately for incorrectly preserved samples. Obtain a new sample or notify the state lab if directed to analyzed by the customer. Who was notified, date and time: Volatiles Sample(s) were received with headspace COMMENTS: DOC. QA.002 Rev 1 dM Analytical & Consulting Chemists ENVIRONMENTAL CHEMISTS, INC OFFICE: 9 0-3 2-0223IFAX910 92�245 NCDENR: DWQ CERTIFICATION # 94 NCDHHS: OLS CERTIFICATION # 37729 info@environmentalchemists.com COLLECTION AND CHAIN OF CUSTODY Client: Cameron Tesitng Services PROJECT NAME: Annual Monitoring and Pollutant Scan REPORT NO: 23 - z 5 Cps ADDRESS: 219 S. Steele St. CONTACT NAME: Maryanne Sims PO NO: Sanford, NC 27330 REPORT TO: msims@camerontesting.com PHONE/FAX: COPY TO: email: Sampled By: cAeeol C T-VOC. I - 1X1 Ir Sample Identification Collection C a f� w o _ 20 a_E � oJ u p a = W M Zz= - .I , - Licaul, PRESERVATION av - aon, OL- = Jtuage, utner: ANALYSIS REQUESTED Time Tempr W Z=Date oW _FV W _j w~ o 2311-0045-01 11/02/23 800 WW C P �PZ70 See Attached COC G G 2311-0045-02 WW C P (pZ707 (Reference your report 2022-21442) See Attached COC 11/02/23 800 G C G P G G C P (No Low Level Mercury) G G C P ------ G G C P G G C P G G C P I ]T� G G 1 NOTICE - DECHLORINATION: Samples for Ammonia, rKN, Cyanide, Phenol and Bacteria must be dechlorinated (0.5 ppm or less) i field at the time of collection. See reverse for Instructions Transfer Relinquished By: DatelTime Received y: Date/Time 2. Temperature when Ref oivr�ri ter• t . _ _ -_. _ — — _ _ _ _ . - - --_.,t-u.-Ni.cu: _Kelectea: Resam le Requested:_ _ Delivered By: Received B `� Comments: Y: Date: �� Time: TURNAROUND: 219 S. Steele Str. Sanford, NC 27= Cameron Testing Services, Inc. Phone: 919.20&4240 Chain of Custody NC WW/GW Cert_ #654 NC PHHS Cert # 37799 US o Cornpa"r Hamlet WWP-TP EPA 'Erna: NCO1918 Page of Contact +" dkwmry®hamietnc.us ------------�--- -- CTS lab, uselo� #N/A Phone — . _ Sarriple 7er)ip- Address (City, #N/A - - I Fax '(C) tab ID. #N/A Notes P/M -- -� — — Project: !Annual Monitoring & Pollutant Scan 'Copected: Rt:s A'tM Due: Narne. I Signature: Sample lnforination Number of bottles i :Requested Analysis Sample ID m E _ E ° °° U H c� 6 > m o Preservatives: (u)npreserved, H(CN. CTS Lab o (7 ao -' a m o 0 S H2(S)04. H(N)03, (Na)Thfouftje. Na(o)H, ID 0 Effluent _ .J '� - v 3 other Pq. Indicate -- Co WWI - - - - - - - - - --- - -- -- I -Nitrogen Co WWI _ - - - _Ammonia r-- - - - - - -- - _.._ 1 s 1 TKN' Nitrite/Nitrate P TPhos - - Co WVI/ -- 1u - - - _ — - -- - I - - -- TDS -Hardness --- -- - -- 1n-- Total Co WW --- - — Effluent -- 1n Sb,As,Be,Cd,Cr,Cu,Pb,Ni,Se,Ag,71,Zn Gr WW 1u _ 1� - _ �tssslue�i9�grg'' _Gr WW 1u - -- Gr WWI — :2Hcl:- HEM (Oil & Grease) - Gr WW _ - - - Cyanide-- - Gr WW i 3u ;--- - - - -- -- - - -- -- -- - -- - - j PPL Volatiles r WW �elin wished: _ 2u PPL Semivolatiles ' - Received: DatefriFne Rush work will require prior approval. Additional charges will apply