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HomeMy WebLinkAboutWQ0000889_Monitoring - 12-2023_20231228Monitoring Report Submittal Permit Number#* WQ0000889 Name of Facility:* PCS Phosphate Company, Inc. (Nutrien) Month: * December Year: * 2023 Report Information Type* Upload Document* GW-59 WQ0000889_Triennial Groundwater Monitoring 814.56KB Results Report _Nov 2023.pdf PDF Only Please upload one PDF containing all applicable monitoring reports (i.e., NDMR, NDAR-1, NDAR-2, NDMLR, GW-59). Confirmation Email Address: * James.Stroud@nutrien.com Name of Submitter: * James Chandler Stroud Signature: c%w, " C % rwal�t 1111?" le Date of submittal: 12/28/2023 This will be filled in automatically Initial Review Reviewer: Wanda.Gerald Is the project number correct?* W00000889 Is the monitoring report accepted?* Yes NO Regional Office* Washington Reviewer: _anonymous Review Date: 1/21/2024 Alutrien- Feeding the Future - CERTIFIED MAIL December 28, 2023 NCDEQ Division of Water Quality Groundwater Section — Permits and Compliance Unit 1617 Mail Service Center Raleigh, NC 27699-1617 Subject: Triennial Groundwater Monitoring Results Domestic Wastewater Treatment Plant — Permit No. WQ0000889 PCS Phosphate Company Inc.' — Aurora Division Dear Mr. Bullock, As required by Monitoring and Reporting Requirements specified in Section IV.10 of the above referenced permit, please find attached copy of the completed GW-59 forms for the WWMW #1, WWMW #2, WWMW #3, WWMW #4 monitoring wells, and a completed GW-59A form. Please note that this sampling event was conducted outside of the required sampling month (November) and is indicated accordingly on the GW-59 forms. Sampling was conducted as soon as possible during the following month to meet the reporting deadline. Please do not hesitate to call me at 252-402-6044 if I can answer any questions or provide any additional information regarding this report. Sincerely, James C dler Stroud Supervisor, Env. Affairs & Technical Services Nutrien — Aurora PC: 12-04-02 (w/attach) cc: K.A. Alnandy B.R. Curtis H.B. Mills 1530 NC Hwy 306 South, Aurora, NC USA 27806 j nubien.com 1 Effective January 1, 2018, PCS Phosphate Company, Inc. is an indirect subsidiary of Nutrien Ltd. PCS Phosphate Company, Inc. remains the legal operating entity and permittee. SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: • DEPARTMENT OF ENVIRONMENTAL QUALITY - DIV. OF WATER RESOURCES INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699.1617 Phone: 919-807.6306 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: W00000889 Expiration Date: 04/30/2028 Facility Name: PCS Phosphate Co. / Nutrien, Inc Non -Discharge X UIC Permit Name (if different): NPDES Other Facility Address: 1530 Hwy 306 South TYPE OF PERMITTED OPERATION BEING MONITORED Aurora (street) NC 28706 CountyBeaufort El Lagoon ❑Remediation: Infiltration Gallery (City) (State) (Zip) Eil Spray Field ❑Remediation: Contact Person: James Chandler Stroud Telephone#: (252)-3224111 ext. 8391 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name: WWTP No. of wells to be sampled. 4 El Water Source Heat Pump El Other: from Permit SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): WWMW-1 Date sample collected: 12-14-23 FIELD ANALYSES: WAS Well Depth: 21.5 ft. Well Diameter: 2 in. pH 00400: 7.44 units Temp. 000lo: 17.7 °C DRY at Depth to Water Level 82546:9.97 ft. below measuring point Screened Interval: 16.0 ft. to 21.0 ft. Spec. Cond. 00094: 627 µMhos time of MeasuringPoint is 2.50 ft. above land surface Relative M.P. Elevation: 20.78 ft. Odor o0085: None sampling, check Volume of water pumped/bailed before sampling: 2100 milliliters Appearance Clear here:❑ Samples for metals were collected unfiltered: ❑ YES ❑ NO ® N/A Field acidified: 0 YES El NO I] N/A LABORATORY INFORMATION Date sample analyzed: 12/14/23-12/24/23 Laboratory Name: PCS Phosphate Co. 1 Environment 1,Inc Certification No. # 330 / # 10 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 N/A mg/L Nitrite (NO2) as N 00615 N/A mg/L Pb -Lead 01051 N/A ug/L Coliform: MF Fecal 31616 < 1.0 /100mL Nitrate (NO3) as N 00620 0.04 mg/L Zn - Zinc 01092 N/A mg/L Coliform: MF Total 31504 N/A /100mL Phosphorus: Total as P 00665 0.050 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 N/A mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 7030o 360 mg/L Al -Aluminum o11o5 N/A mg/L pH (Lab) 00403 7.25 units Ba - Barium 01007 N/A ug/L TOC 00680 5.61 mg/L Ca - Calcium 00916 N/A mg/L Chloride oog4o <1.0 mg/L Cd - Cadmium 01027 N/A ug/L Arsenic 01002 N/A ug/L Chromium: Total 01034 N/A ug/L Grease and Oils 00552 NIA mg/L Cu -Copper 01042 N/A mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 N/A ug/L Fe - Iron 01045 N/A ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 N/A mg/L Hg -Mercury 71 goo N/A ug/L Lab Report Attached? 0 Yes (1) ❑ No (0) pecific Conductance 00095 N/A µMhos K - Potassium 00937 N/A mg/L VOC 7873 method # SM620OC-11 Total Ammonia 00610 1.04 mg/L Mg - Magnesium 00927 N/A mg/L method # (Ammonia Nitrogen; NH3 as N; Ammonia Nitrogen, Total) Mn - Manganese 01055 N/A ug/L method # TKN as N 00625 N/A mg/L Ni - Nickel 01067 N/A ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: N/A mg/L Effluent Total VOCs: N/A mg/L VOC Removal% N/A William M. Ponton, General Manager Permittee (or Authorized Agent) Name and Title - Please print or type (or Authorized Agent) art' Li �lm �a--� 12/28/23 (Date) GW-59 Rev.05-02-2017 SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: �16117 DEPARTMENT OF ENVIRONMENTAL QUALITY - DIV. OF WA ( FR RESOURCES INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM MAIL SERVICE CENTER, RALEIGH, NC 276994617 Phone: 919-807-6306 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: W00000889 Expiration Date: 04/30/2028 Facility Name: PCS Phosphate Co. / Nutrien,inc Non -Discharge X UIC Permit Name (if different): NPDES Other Facility Address: 1530 Hwy 306 South TYPE OF PERMITTED OPERATION BEING MONITORED Aurora (Street) NC 28706 County Beaufort El Lagoon ❑Remediation: Infiltration Gallery (city) (statai (zip) FE Spray Field ❑ Remediation: Contact Person: James Chandler Stroud Telephone#: (252)-322-4111 ext. 8391 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name: WWTP No. of wells to be sampled: 4 ❑ Water Source Heat Pump ❑ Other: from Permit SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): WWMW-2 Date sample collected: 12/14/23 FIELD ANALYSES: WAS Well Depth: 21.5 ft. Well Diameter: 2 in. pH 00400: 7.59 units Temp, 000lo: 18.9 °C DRY at Depth to Water Level 82546:10.78 ft. below measuring point Screened Interval: 16.0 ft. to 21.0 ft. Spec. Cond. 00094: 604 µMhos time of Measuring Point is 2•50 ft. above land surface Relative M.P. Elevation: 20.84 ft. Odor 000m: None sampling,check Volume of water pumped/bailed before sampling: 2100 milliliters Appearance Clear here:❑ Samples for metals were collected unfiltered: ❑ YES ❑ NO ®N/A Field acidified: 0 YES ❑ No E N/A LABORATORY INFORMATION Date sample analyzed: 12/14/23-12124/23 Laboratory Name: PCS Phosphate Co. 1 Environment 1,Inc Certification No. # 330 / # 10 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 N/A mg/L Nitrite (NO2) as N 00615 N/A mg/L Pb -Lead 01051 N/A ug/L Coliform: MF Fecal 31616 < 1.0 /100mL Nitrate (NO3) as N 00620 .29 mg/L Zn - Zinc 01092 N/A mg/L Coliform: MF Total 31504 N/A /100mL Phosphorus: Total as P 00665 0.020 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 N/A mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 703oo 320 mg/L Al -Aluminum 01105 N/A mg/L pH (Lab) 00403 7.47 units Ba - Barium 01007 N/A ug/L TOC 0068o 3.02 mg/L Ca - Calcium 00916 N/A mg/L Chloride 00940 10 mg/L Cd - Cadmium 01027 N/A ug/L Arsenic 01002 NIA ug/L Chromium: Total olo34 N/A ug/L Grease and Oils 00552 N/A mg/L Cu -Copper 01042 N/A mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 3273o N/A ug/L Fe - Iron 01045 N/A ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 N/A mg/L Hg - Mercury 71900 N/A ug/L Lab Report Attached? 0 Yes (1) ❑ No (0) Specific Conductance 00095 N/A µMhos K - Potassium 00937 N/A mg/L VOC 7873 method # SM6200 C-11 Total Ammonia 00610 0.12 mg/L Mg - Magnesium 00927 N/A mg/L method # (Ammonia Nitrogen; NH9as N; Ammonia Nitrogen, Total) Mn - Manganese 01055 N/A g ugJL ,method # TKN as N 00626 N/A mg/L Ni - Nickel 01067 N/A ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: N/A William M. Ponton, General Manager Permittee (or Authorized Agent) Name and Title - Please pint or type mg/L Effluent Total VOCs: N/A (or mg/L VOC Removal% N/A methodsved 12/28/23 (Date) GW-59 Rev.05-02-2017 SUBMIT FORM ON YELLOW PAPER ONLY Mail origin DEPARTMENT OF ENVIRONMENTAL QUALITY - DIV. OF WATER RESOURCES GROUNDWATER QUALITY MONITORING: INFORMATION PROCESSING UNIT I COMPLIANCE REPORT FORM 1617 MAIL SERVICE CENTER, RALEIGH, NC 276994617 Phone: 919-807-6306 Please Print Clearly or Type Facility Name: PCS Phosphate Co./Nutrien, Inc Permit Name (if different): Facility Address: 1530 Hwy 306 South Aurora, NC 27806 1530 Hwy 306 South tstrXdrora, NC 27806 County Beaufort (citv) i8tatO 00 act Person: James Chandler Stroud Location/Site Name: WWTP LL ID NUMBER (from Permit): WWMW-3 II Depth: 21.5 ft. Ith to Water Level 82546:10.68 ft. below measuring point Isuring Point is 2.50 ft. above land surface Telephone#: (252)-322-4111 ext: 8391 No. of wells to be sampled: 4 Date sample collected: 12/14/23 Well Diameter: 2 in. Screened Interval: 16.0 ft. Relative M.P. Elevation: 20.15 to 21.0 ft. ft. Number: WQ0000889Expiration Date: 12/28/23 :harge X UIC PDES Other VPE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑ Remediation: Infiltration Gallery ON Spray Field ❑ Remediation: ❑ Rotary Distributor ❑ Land Application of Sludge ❑ Water Source Heat Pump ❑ Other: FIELD ANALYSES: pH oo400: 7.26 units Temp. 000lo: 18.9 °C Spec. Cond. 00094: 1170 µMhos Odor 00085: None of water pumped/bailed before sampling: 2100 milliliters Appearance as for metals were collected unfiltered: ❑ YES ❑ NO ®N/A Field acidified: ❑ YES 0 NO PI N/A Clear Ite sample analyzed: 12/14/23-12/24123 Laboratory Name: PCS Phosphate Co. I Environment 1,lnc Certification No. # 330 / # 10 kRAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 N/A mg/L Nitrite (NO2) as N 00615 NIA mg/L Pb - Lead 01051 N/A ug/L Coliform: MF Fecal 31616 < 1.0 /100mL Nitrate (NO3) as N 00620 <0.04 mg/L Zn - Zinc 01092 N/A mg/L Coliform: MF Total 31504 N/A /100mL Phosphorus: Total as P 00665 0.025 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 N/A mg/L Other (Specify Compounds and Concentration Units): solved Solids:Total 7030o 660 mg/L Al - Aluminum o11o5 N/A mg/L pH (Lab) 00403 7.14 units Ba - Barium 01007 NIA ug/L TOC 0068o 3.53 mg/L Ca - Calcium 00916 N/A mg/L Chloride oog4o 150 mg/L Cd - Cadmium 01027 N/A ug/L Arsenic 01002 N/A ug/L Chromium: Total 010344 N/A ug/L Grease and Oils 00552 N/A mg/L Cu - Copper 01042 N/A mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 3273o N/A ug/L Fe - Iron 01045 N/A ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate oo945 N/A mg/L Hg - Mercury 719oo NIA ug/L Lab Report Attached? © Yes (1) ❑ No (0) ecific Conductance 00095 N/A µMhos K - Potassium 00937 N/A mg/L VOC 7873 method # SM620OC-11 Total Ammonia oo6lo 0.04 mg/L Mg - Magnesium 00927 N/A mg/L method # (Ammonia Nitrogen; NH3asN; Ammonia Nitrogen, Total) Mn - Manganese 01055 NIA g ug1L ,method # TKN as N 00625 N/A mg/L Ni - Nickel 01067 N/A ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: N/A William M. Ponton, General Manager Permittee (or Authorized Agent) Name and Title - Please print or type GW-59 Rev.05-02-2017 mg/L Effluent Total VOCs: N/A mg/L VOC Removal% N/A at Of —1 SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: • • DEPARTMENT OF ENVIRONMENTAL QUALITY - DIV. OF WATER RESOURCES INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM 1817 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: 919-807-5306 FACILITY INFORMATION ",�:asePnntClearly orType PERMIT Number: W00000889 Expiration Date: 04/30/2028 Facility Name: PCS Phosphate Co. I Nutrien, Inc Non -Discharge x UIC NPDES Other Permit Name (if different): Facility Address: 1530 Hwy 306 South TYPE OF PERMITTED OPERATION BEING MONITORED El Lagoon ❑Remediation: Infiltration Gallery Aurora (Street) NC 28706 County Beaufort (city) (Stite) (zip) F1 Spray Field ❑ Remediation: Contact Person: James Chandler Stroud Telephone#: (252)-322-4111 ext. 8391 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name: WWTP No. of wells to be sampled: 4 ❑ Water Source Heat Pump ❑ Other: from Permit) SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): WWMW-4 Date sample collected: 12/14/23 FIELD ANALYSES: WAS Well Depth: 21.5 ft. Well Diameter: 2 in. pH oo400: 7.54 units Temp. 000lo: 1 7.9 °C DRY at Depth to Water Level 82546:14.44 ft. below measuring point Screened Interval: 16.0 ft. to 21.0 ft. Spec. Cond. 00094: 1240 µMhos time of MeasuringPoint is 2.50 ft. above land surface Relative M.P. Elevation: 20.81 ft. Odor 000a5: None sampling, check Volume of water pumped/bailed before sampling: 2100 milliliters Appearance Clear here:❑ Samples for metals were collected unfiltered: ❑ YES ❑ NO ®N/A Field acidified: 0 YES ❑ NO El N/A LABORATORY INFORMATION Date sample analyzed: 12/14/23-12/18/23 Laboratory Name: PCS Phosphate Co. / Environment 1,Inc Certification No. # 330 / # 10 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 N/A mg/L Nitrite (NO2) as N 00615 N/A mg/L Pb - Lead 01051 N/A ug/L Coliform: MF Fecal 31616 < 1.0 /100mL Nitrate (NO3) as N 00620 0.12 mg/L Zn - Zinc 01092 N/A mg/L Coliform: MF Total 31504 N/A /100mL Phosphorus: Total as P 00665 0.073 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 N/A mg/L Other (Specify Compounds and Concentration Units): Dissolved Solids:Total 7o3oo 630 mg/L Al -Aluminum 01105 N/A mg/L pH (Lab) 00403 7.30 units Ba - Barium 01007 N/A ug/L TOC oo68o 3.59 mg/L Ca - Calcium 00916 N/A mg/L Chloride 00940 131 mg/L Cd -Cadmium 01027 N/A ug/L Arsenic 01002 N/A ug/L Chromium: Total olo34 N/A ug/L Grease and Oils 00552 N/A mg/L Cu - Copper 01042 NIA mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 N/A ug/L Fe - Iron 01045 N/A ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 N/A mg/L Hg - Mercury 71900 N/A ug/L Lab Report Attached? El Yes (1) ❑ No (0) pecific Conductance 00095 N/A µMhos K - Potassium 00937 N/A mg/L VOC 7873 method # N/A Total Ammonia 00610 0.25 mg/L Mg - Magnesium 00927 N/A mg/L method # (Ammonia Nitrogen; NH3 as N; Ammonia Nitrogen, Total) Mn - Manganese 01055 N/A ug/L method # TKN as N 00625 N/A mg/L Ni - Nickel 01067 N/A ug/L method # I -or Icemematlon systems only (Attach Lab Reports): Influent Total VOCs: N/A mg/L Effluent Total VOCs: N/A mg/L VOC Removal% NIA William M. Ponton, General Manager Permittee (or Authorized ggent) Name and Title - Please print or type GW-59 Rev.05-02-2017 GW-59A COMPLIANCE REPORT FORM Permit # WQ0000889 (Submit one each monitoring period with GW-59 forms.) Enter date monitoring results were due. (12/31/2023) Will this monitoring report (GW-59 and GW-59A) be YES NO submitted after the established due date? X 2 Was any required information missing on the GW-59 report forms? YES NO X IF the answer to question l or 2 is "YES", list in the space provided below the well identification number(s) and explain the problems encountered in obtaining the required information. 3 Are any of the monitor wells in need of repair or maintenance (damaged casing, unlocked or missiong cap, YES NO missing identification plate, area overgrown, etc.)? /f the answer is "Yes", contact the Regional Office for X guidance. 4 Are any monitored constituents equal to or above the established standards? YES NO X /f the answer to question 4 is 'NO', skip to section 8. /f the answer to question 4 is "YES", list the affected wells individually with constituent(s) and concentrations(s) exceeding standards in the space provided below.- -3 "it JMW-4 TDS -3 J We: W WKW No.1 is the established background monitoring well 5 For the constituents identified in question 4 above, have standards been exceeded previous for the same YES NO constituent(s) in the same well(s) X if the answer to question 5 is 'NO", skip to section 8. d the answer to question 5 is "YES", list in the space provided below, each well with constituent(s) exceeding standards, concentration(s) reported, and sample collection date for each occurrence (for the last two years). 711312023 3/1512023 11/812022 7/6/2022 3/812022 11/412021 7/2012021 WWMW-1 TDS 390 390 410 370 400 410 390 WWMW-2 TDS 460 420 420 320 340 410 390 WWMW-3 TDS 650 670 660 640 640 680 750 WWMW-4 TDS 570 670 630 640 690 680 660 6 Are the monitoring wells listed in section 5 located at or beyond the review boundary? YES NO X If the answer is "YES", a groundwater quality problem may be occurring. CONTACT THE REGIONAL OFFICE IMMEDIATELY FOR GUIDANCE. If the answer is "NO", monitoring wells may be improperly located; contact the Regional Office. * Only WWMW No. 1 is located bevond the review boundary. 7 Is the permittee implementing previously approved actions required by the Division involving this groundwater YES NO quality problem? X If the answer to question 7 is "YES", describe those actions in the space provided below. /f the answer to question 7 is 'NO'; contact the Regional Office within 90 days an evaluation may buir d to determine the impact the waste d/s on sal system is having at the review and compliance boundaries surrounding this facility. Failure to do so may subject the permittee to a Notice of Violation, fines—andlor penalties. Contacted WaRO 12/27/2023. 8 The person completing this portion (GW-59A) of the monitoring report should sign below and submit this form with GW-59 forms for required wells to be address provided at the top of the current GW-59 form. .................................................................................................................. :I:liereti :oc ntiwl..............shove.....ririta#ian:yias:eaialt�a#acl:acid:t ie: nfoti>hetioii:su it iitYeilF:irit�iis;report;" ................ :IOo7 a ' :Report G1�F=liJAI:{s xrae:arxd boii�plete #. tfie li.s#flf:iriv fCno�ivleilse :::........... . Signature of Permittee (or Authorized Agent) Date Waypointo ANALYTICAL 114 OAKMONT DRIVE GREENVILLE, NC 27858 CLIENT: NUTRIEN (WELLS 1-4) MR. BRYAN MILLS 1530 NC HWY. 306 SOUTH AURORA, NC 27806 REVIEWED BY: PARAMETERS, ug/l 49. 1,2,4-Trichlorobenzene 50. 1,1,1-Trichloroethane 51. 1,1,2-Trichloroethane 52. Trichloroethene 53. Trichlorofluoromethane 54. 1,2,3-Trichloropropane 55. 1,2,4-Trimethylbenzene 56. 1,3,5-Trimethylbenzene 57. Vinyl Chloride 58. Total Xylenes 59. Methyl Tert Butyl Ether VOLATILE ORGANICS STD. METHODS 8260D Domestic Mwell #1 < 0.50 < 0.50 < 0.50 < 0.50 <0.50 <0.50 < 0.50 <0.50 <0.50 < 1.00 < 1.00 Drinking Water ID: 37715 Waateaater ID: 10 PHONE (252) 756-6208 FAX (252) 756-0633 CLIENT ID: 1605 ANALYST: BLD DATE COLLECTED: 12/14/23 DATE ANALYZED: 12/15/23 DATE REPORTED: 12/27/23 Domestic Domestic Domestic Mwell #2 Mwell N3 � Mwell #4 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 < 1.00 < 1.00 < 1.00 < 1.00 < 1.00 < 1.00 Page: 2 Waypointo ANALYTICAL 114 OAKMONT DRIVE GREENVILLE, NC 27858 CLIENT: NUTRIEN (WELLS 1-4) MR. BRYAN MILLS 1530 NC HWY. 306 SOUTH AURORA, NC 27806 REVIEWED BY: VOLATILE ORGANICS STD. METHODS 8260D Drinking Water ID: 37715 Wastewater ID: 10 PHONE (252) 756-6208 FAX (252) 756-0633 CLIENT ID: 1605 ANALYST: BLD DATE COLLECTED: 12/14/23 DATE ANALYZED: 12/15/23 DATE REPORTED: 12/27/23 Domestic Domestic Domestic Domestic PARAMETERS, ug/l Mwell #1 Mwell #2 Mwell #3 Mwell #4 1. Benzene <0.50 <0.50 <0.50 <0.50 2. Bromobenzene <0.50 <0.50 <0.50 <0.50 3. Bromochloromethane <0.50 <0.50 <0.50 <0.50 4. Bromodichloromethane <0.50 <0.50 <0.50 <0.50 5. Bromoform <0.50 <0.50 <0.50 <0.50 6. Bromomethane <0.50 <0.50 <0.50 <0.50 7. N-Butylbenzene <0.50 <0.50 <0.50 <0.50 8. Sec-Butylbenzene <0.50 <0.50 <0.50 <0.50 9. Tert-Butylbenzene <0.50 <0.50 <0.50 <0.50 10. Carbon Tetrachloride <0.50 <0.50 <0.50 <0.50 11. Chlorobenzene <0.50 <0.50 <0.50 <0.50 12. Chloroethane <0.50 <0.50 <0.50 <0.50 13. Chloroform <0.50 <0.50 <0.50 <0.50 14. Chloromethane <0.50 <0.50 <0.50 <0.50 15. 2-Chlorotoluene <0.50 <0.50 <0.50 <0.50 16. 4-Chlorotoluene <0.50 <0.50 <0.50 <0.50 17. Dibromochloromethane <0.50 <0.50 <0.50 <0.50 18. 1,2-Dibromo-3-Chloropropane <0.50 <0.50 <0.50 <0.50 19. 1,2-Dibromoethane <0.50 <0.50 <0.50 <0.50 20. Dibromomethane 1 <0.50 <0.50 <0.50 <0.50 21. 1,2-Dichlorobenzene <0.50 <0.50 <0.50 <0.50 22. 1,3-Dichlorobenzene <0.50 <0.50 <0.50 <0.50 23. 1,4-Dichlorobenzene <0.50 <0.50 <0.50 <0.50 24. Dichlorodifluoromethane <0.50 <0.50 <0.50 <0.50 25. 1,1-Dichloroethane <0.50 <0.50 <0.50 <0.50 26. 1,2-Dichloroethane <0.50 <0.50 <0.50 <0.50 27. 1,1-Dichloroethene <0.50 <0.50 <0.50 <0.50 28. Cis-1,2-Dichloroethene <0.50 <0.50 <0.50 <0.50 29. trans-1,2-Dichloroethene <0.50 <0.50 <0.50 <0.50 30. 1,2-Dichloropropane <0.50 <0.50 <0.50 <0.50 31. 1,3-Dichloropropane <0.50 <0.50 <0.50 <0.50 32. 2,2-Dichloropropane <0.50 <0.50 <0.50 <0.50 33. 1,1-Dichloropropene <0.50 <0.50 <0.50 <0.50 34. Cis-1,3-Dichloropropene <0.50 <0.50 <0.50 <0.50 35. trans-1,3-Dichloropropene <0.50 <0.50 <0.50 <0.50 36. Ethylbenzene <0.50 <0.50 <0.50 <0.50 37. Hexachlorobutadiene <0.50 <0.50 <0.50 <0.50 38. Isopropylbenzene <0.50 <0.50 <0.50 <0.50 39. 4-Isopropyltoluene <0.50 <0.50 <0.50 <0.50 40. Methylene Chloride <0.50 <0.50 <0.50 <0.50 41. Naphthalene <0.50 <0.50 <0.50 <0.50 42. Propylbenzene <0.50 <0.50 <0.50 <0.50 43. Styrene <0.50 <0.50 <0.50 <0.50 44. 1,1,1,2-Tetrachloroethane <0.50 <0.50 <0.50 <0.50 45. 1,1,2,2-Tetrachloroethane <0.50 <0.50 <0.50 <0.50 46. Tetrachloroethene <0.50 <0.50 <0.50 <0.50 47. Toluene <0.50 <0.50 <0.50 <0.50 48. 1,2,3-Trichlorobenzene <0.50 <0.50 <0.50 <0.50 Page: 1