NC0047562_Pollutant Scan_20240117

r: -71 Environmental Chemists, Inc.
nvirochem 6602 Windmill Way,Wilmington,NC 28405 - 910.392.0223 Lab • 910.392.4424 Fax
sM 710 Bowsertown Road,Manteo,NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway,Jacksonville,NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL&CONSULTING CHEMISTS info,a environmentalchemists.com
Cameron Testing Services, Inc. Date of Report: Jan 09, 2024
219 South Steele St. Customer PO#: 2311-0045
Sanford NC 27330 Customer ID: 12090010
Attention: Report#: 2023-25860
Project ID: Hamlet
Lab ID Sample ID: 2311-0045 Collect Date/Time Matrix Sampled by
23-62706 Site: 2311-0045-01 11/7/2023 8:00 AM Water Client
Test Method Results Date Analyzed
Antimony EPA 200.7,Rev 4.4,1994 <0.01 mg/L 11/16/2023
Copper EPA 200.7,Rev 4.4,1994 0.011 mg/L 11/16/2023
Lead EPA 200.7,Rev 4.4.1994 <0.01 mg/L 11/16/2023
Nickel EPA 200.7,Rev 4.4. 1994 <0.01 mg/L 11/16/2023
Selenium EPA 200.7,Rev 4.4,1994 <0.01 mg/L 11/16/2023
Silver EPA 200.7,Rev 4.4,1994 <0.01 mg/L 11/16/2023
Thallium EPA 200.7,Rev 4.4,1994 <0.01 mg/L 11/16/2023
Zinc EPA 200.7.Rev 4.4,1994 0.026 mg/L 11/16/2023
Arsenic EPA 2007,. Rev.4 4,1994 <0.01 mg/L 11/16/2023
Beryllium EPA 200.7,Rev.4.4,1994 <0.01 mg/L 11/16/2023
Cadmium EPA 200.7,Rev.4.4,1994 <0.01 mg/L 11/16/2023
Chromium EPA 200.7,Rev.4.4,1994 <0.01 mg/L 11/16/2023
Ammonia Nitrogen EPA 350.1,Rev.2.0,1993 < 0.2 mg/L 11/15/2023
Total Kjeldahl Nitrogen (TKN) EPA 351.2,Rev.2.0,1993 <0.5 mg/L 11/10/2023
Total Hardness SM 2340 c-2011 17 mg/L 01/09/2024
Total Dissolved Solids (TDS) SM 2540 c-2015 389 mg/L 11/08/2023
Total Phosphorus SM 4500 P(F-H)-2011 0.69 mg/L 11/13/2023
Nitrate Nitrogen (Calc)
Nitrite Nitrogen EPA 353.2,Rev.2.0,1993 < 0.02 mg/L 11/07/2023
Nitrate+Nitrite-Nitrogen EPA 353.2.Rev.2.0,1993 20.0 mg/L 11/13/2023
Nitrate Nitrogen Subtraction Method 20.0 mg/L 11/20/2023
Report#:: 2023-25860 Page 1 of 5

-,qql
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington,NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
sM 7I0 Bowsertown Road,Manteo,NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway,Jacksonville,NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL&CONSULTING CHEMISTS info(«environmentalchemists.com
Cameron Testing Services, Inc. Date of Report: Jan 09, 2024
219 South Steele St. Customer PO#: 2311-0045
Sanford NC 27330 Customer ID: 12090010
Attention: Report#: 2023-25860
Project ID: Hamlet
Lab ID Sample ID: 2311-0045 Collect Date/Time Matrix Sampled by
23-62707 Site: 2311-0045-02 11/7/2023 8:00 AM Water Client
Test Method Results Date Analyzed
Oil & Grease(O&G) EPA 1664 Rev.B <6.25 mg/L 11/21/2023
Reporting limit elevated due to insufficient sample volume.
Cyanide EPA 335.4,Rev.1.0,1993 < 0.005 mg/L 11/14/2023
Inorganic Phenols EPA420.4,Rev 1.0,1993 <0.005 mg/L 11/20/2023
1,1,1-Trichloroethane EPA 624.1 <0.5 µg/L 11/15/2023
1,1,2,2-Tetrachloroethane EPA 624.1 <0.5 µg/L 11/15/2023
1,1,2-Trichloroethane EPA 624.1 <0.5 µg/L 11/15/2023
1,1-Dichloroethane EPA 624.1 <0.5 µg/L 11/15/2023
1,1-Dichloroethene EPA 624.1 <0.5 µg/L 11/15/2023
1,2-Dichlorobenzene EPA 624.1 <0.5 µg/L 11/15/2023
1,2-Dichloroethane EPA 624.1 <0.5 µg/L 11/15/2023
1,2-Dichloropropane EPA 824.1 <0.5 µg/L 11/15/2023
1,3-Dichlorobenzene EPA 624.1 <0.5 µg/L 11/15/2023
1,4-Dichlorobenzene EPA 624.1 <0.5 µg/L 11/15/2023
Acrolein EPA 624.1 <20 µg/L 11/15/2023
Acrylonitrile EPA 624.1 <5 µg/L 11/15/2023
Benzene EPA 624.1 <0.5 µg/L 11/15/2023
Bromodichloromethane EPA 624.1 2.53 µg/L 11/15/2023
Bromoform EPA 624.1 <0.5 µg/L 11/15/2023
Bromomethane EPA 624.1 <0.5 µg/L 11/15/2023
Carbon Tetrachloride EPA 624.1 <0.5 µg/L 11/15/2023
Chlorobenzene EPA 624.1 <0.5 µg/L 11/15/2023
Chloroethane EPA 624.1 <0.5 µg/L 11/15/2023
Chloroform EPA 624.1 17.7 µg/L 11/15/2023
Chloromethane EPA 624.1 <0.5 µg/L 11/15/2023
cis-1,3-Dichloropropene EPA 624.1 <0.5 µg/L 11/15/2023
Report#:: 2023-25660
Page 2 of 5

Fool" Environmental Chemists, Inc.
envirochem 6602 Windmill Way,Wilmington,NC 28405 & 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road,Manteo,NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway,Jacksonville,NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL&CONSULTING CHEMISTS info(a environmentalchemists.com
Cameron Testing Services, Inc. Date of Report: Jan 09, 2024
219 South Steele St. Customer PO#: 2311-0045
Sanford NC 27330 Customer ID: 12090010
Attention: Report#: 2023-25860
Project ID: Hamlet
Dibromochloromethane EPA 624.1 <0.5 pg/L 11/15/2023
Ethylbenzene EPA 624.1 <0.5 pg/L 11/15/2023
M+P Xylene EPA 624.1 <1.0 pg/L 11/15/2023
Methylene chloride EPA 624.1 <0.5 pg/L 11/15/2023
ortho-Xylene EPA 624.1 <0.5 pg/L 11/15/2023
Tetrachloroethene EPA 624.1 <0.5 pg/L 11/15/2023
Toluene EPA 624.1 <0.5 pg/L 11/15/2023
Trans-1,2-Dichloroethene EPA 624.1 <0.5 pg/L 11/15/2023
trans-1,3-Dichloropropene EPA 624.1 <0.5 pg/L 11/15/2023
Trichloroethene EPA 624.1 <0.5 pg/L 11/15/2023
Trichlorofluoromethane EPA 624.1 <0.5 pg/L 11/15/2023
Vinyl chloride EPA 624.1 <0.5 pg/L 11/15/2023
2,4,6-Trichlorophenol EPA 625.1 <4.76 pg/L 11/08/2023
2,4-Dichlorophenol EPA 625.1 <4.76 pg/L 11/08/2023
2,4-Dimethylphenol EPA 625.1 <4.76 pg/L 11/08/2023
2,4-Dinitrophenol EPA 625.1 <23.8 pg/L 11/08/2023
2-Chlorophenol EPA 625.1 <4.76 pg/L 11/08/2023
2-Methyl-4,6-dinitrophenol EPA 625.1 <23.8 pg/L 11/08/2023
2-Nitrophenol EPA 625.1 <23.8 pg/L 11/08/2023
4-Chloro-3-methylphenol EPA 625.1 <4.76 pg/L 11/08/2023
4-Nitrophenol EPA 625.1 <23.8 pg/L 11/08/2023
Pentachlorophenol EPA 625.1 <23.8 pg/L 11/08/2023
Phenol EPA 625.1 <4.76 pg/L 11/08/2023
1,2 Diphenylhydrazine EPA 625.1 <4.76 pg/L 11/08/2023
1,2,4-Trichlorobenzene EPA 625.1 <4.76 pg/L 11/08/2023
1,2-Dichlorobenzene EPA 625.1 <4.76 pg/L 11/08/2023
1,3-Dichlorobenzene EPA 625.1 <4.76 pg/L 11/08/2023
1,4-Dichlorobenzene EPA 625.1 <4.76 pg/L 11/08/2023
1-Methylnaphthalene EPA 625.1 <4.76 pg/L 11/08/2023
2,4-Dinitrotoluene EPA 626.1 <4.76 pg/L 11/08/2023
Report#:', 2023-25860
Page 3 of 5

-71
ro"" 0
Environmental Chemists, Inc.
6602 Windmill Way,Wilmington,NC 28405 • 910,392.0223 Lab • 910,392.4424 Fax
-� 710 Bowsertown Road,Manteo,NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway,Jacksonville,NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL&CONSULTING CHEMISTS info(a environmentalchemists.com
Cameron Testing Services, Inc. Date of Report: Jan 09, 2024
219 South Steele St. Customer PO #: 2311-0045
Sanford NC 27330 Customer ID: 12090010
Attention: Report#: 2023-25860
Project ID: Hamlet
2,6-Dinitrotoluene EPA 625 1 <4.76 pg/L 11/08/2023
2-Chloronaphthalene EPA 625.1 <4.76 pg/L 11/08/2023
2-Methyl naphthalene EPA 625 1 <4.76 pg/L 11/08/2023
3,3'-Dichlorobenzidine EPA 625.1 <9.52 pg/L 11/08/2023
4-Bromophenyl phenyl ether EPA 625.1 <4.76 pg/L 11/08/2023
4-Chlorophenyl phenyl ether EPA 625.1 <4.76 pg/L 11/08/2023
Acenaphthene EPA 625.1 <4.76 pg/L 11/08/2023
Acenaphthylene EPA 625.1 <4.76 pg/L 11/08/2023
Anthracene EPA 625.1 <4.76 pg/L 11/08/2023
Benzidine EPA 625.1 <9.52 pg/L 11/08/2023
Benzo [alpyrene EPA 625.1
<4.76 pg/L 11/08/2023
Benzo(a)anth race ne EPA 625.1 <4.76 pg/L 11/08/2023
Benzo(b)fluoranthene EPA 625.1 <4.76 pg/L 11/08/2023
Benzo(g,h,i)perylene EPA 625.1 <4.76 pg/L 11/08/2023
Benzo(k)fluoranthene EPA 625.1 <4.76 pg/L 11/08/2023
Bis ( chloromethyl ) ether EPA 625.1 <4.78 p9/L 11/08/2023
Bis(2-Chloroethoxy)methane EPA 625.1 <4.76 pg/L 11/08/2023
Bis(2-Chloroethyl)ether EPA 625.1 <4.76 pg/L 11/08/2023
Bis(2-Chloroisopropyl)ether EPA 625.1 <4.76pg/L 11/08/2023
Bis(2-ethyihexyi)phthalate EPA 625.1 <4.76 pg/L 11/08/2023
Butylbenzylphthalate EPA 625.1 <4,7$pg/L 11/08/2023
Chrysene EPA 625.1 <4.76 pg/L 11/08/2023
Dibenzo(a,h)anthracene EPA 625.1 <4.76 pg/L 11/08/2023
Diethylphthalate EPA 625.1 <4.76 pg/L 11/08/2023
Dimethylphthalate EPA 625.1 <4.76 pg/L 11/08/2023
Di-n-Butylphthalate EPA 625.1 <4.76 pg/L 11/08/2023
D i-n-Octylphtha late EPA 625.1 <4.76 pg/L 11/08/2023
Fluoranthene EPA 625.1 <4.76 pg/L 11/08/2023
Fluorene EPA 625.1 <4.76 pg/L 11/08/2023
Hexachlorobenzene EPA 625.1 <4.76 pg/L 11/08/2023
Report#-: 2023-25860
Page 4 of 5

Environmental Chemists, Inc.
envirochem 6602 Windmill Way, Wilmington,NC 28405 • 910,392.0223 Lab • 910.392.4424 Fax
sM 710 Bowsertown Road,Manteo,NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway,Jacksonville,NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL&CONSULTING CHEMISTS info a environmentalchemists.com
Cameron Testing Services, Inc. Date of Report: Jan 09, 2024
219 South Steele St. Customer PO#: 2311-0045
Sanford NC 27330 Customer ID: 12090010
Attention: Report#: 2023-25860
Project ID: Hamlet
Hexachlorobutadiene EPA 6251 <4.76 pg/L 11/08/2023
Hexachlorocyclopentadiene EPA 625.1 <23.8 pg/L 11/08/2023
Hexachloroethane EPA 625.1 <4.76 pg/L 11/08/2023
I ndeno(1,2,3-cd)pyrene EPA 625.1 <4.76 pg/L 11/08/2023
lsophorone EPA 625.1 <4.76 pg/L 11/08/2023
Naphthalene EPA 625.1 <4.76 pg/L 11/08/2023
Nitrobenzene EPA 625.1 <4.76 pg/L 11/08/2023
N-nitroso-dimethylamine(NDMA) EPA 625.1 <4.76pg/L 11/08/2023
N-Nitroso-di-n-propylamine EPA 625.1 <4.76 pg/L 11/08/2023
N-Nitroso-diphenylamine EPA 625.1 <4.76 pg/L 11/08/2023
Phenanthrene EPA 625.1 <4.76 pg/L 11/08/2023
Pyrene EPA 625.1 <4.76 pg/L 11/08/2023
Comment:
Reviewed by: r �
Report#:: 2023-25860
Page 5 of 5

Environmental Chemist, Inc., Wilmington, NC Lab#94
6602 Windmill Way
Wilmington, NC 28405
Sample Receipt Checklist 910.392.0223
Client_ T'<�� �- Date: ,l
1 Z Report Number:_2023- o�Sg�
Receipt of sample: ECHEM Pickup Client Delivery ,❑ UPS O Fed Ex ❑ Other ❑
❑ YES ❑ NO ❑ N/A 1. Were custody seals present on the cooler?
❑ YES ❑ NO ❑ N/A 2. If custody seals were present, were they intact/unbroken?
Original temperature upon receipt °C Corrected temperature upon receipt How temperature taken: ❑ Temperature Blanknst aC
IR Gun ID: Thomas Traceable S/N 210886869 IR Gun Corr❑ectionFactor'C ottBott1050
YES ❑ NO 3. If temperature of cooler exceeded 6°C, was Project Mgr./QA notified?
YES ❑ NO 4. Were proper custody procedures (relinquished/received)followed?
YES ❑ NO 5. Were sample ID's listed on the COC?
YES ❑ NO 6. Were samples ID's listed on sample containers?
YES ❑ NO 7. Were collection date and time listed on the COC?
YES ❑ NO 8. Were tests to be performed listed on the COC?
YES ❑ NO 9. Did samples arrive in proper containers for each test?
YES ❑ NO 10. Did samples arrive in good condition for each test?
YES ❑ NO 11. Was adequate sample volume available?'
YES ❑ NO 12. Were samples received within proper holding time for requested tests?
YES ❑ NO 13. Were acid preserved samples received at a pH of<2?
YES ❑ NO 14. Were cyanide samples received at a pH >12?
❑ YES ❑ NO 15. Were sulfide samples received at a pH >9?
YES ❑ NO 16. Were NH3/TKN/Phenol received at a chlorine residual of<0.5 m/L? **
Z YES ❑ NO 17. Were Sulfide/Cyanide received at a chlorine residual of<0.5 m/L?
❑ YES ❑ NO 18. Were orthophosphate samples filtered in the field within 15 minutes?
* TOC/Volatiles are pH checked at time of analysis and recorded on the benchsheet.
** Bacteria samples are checked for Chlorine at time of analysis and recorded on the benchsheet.
Sample Preservation: (Must be completed for any sample(s) incorrectly preserved or with headspace)
Sample(s) were received incorrectly preserved and were adjusted accordingly
by adding (circle one): H2SO4 HNO3 HCI NaOH
Time of preservation: If more than one preservative is needed, notate in comments below
Note:Notify customer service immediately for incorrectly preserved samples.Obtain a new sample or
notify the state lab if directed to analyzed by the customer.Who was notified,date and time:
Volatiles Sample(s) were received with headspace
COMMENTS:
DOC. QA.002 Rev 1

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�a� eve � Nle%'c°u2y
® LaboratoriesLLC 1
2040 Savage Road I Charleston SC 291407
meulbt; r of The GEL Group INC; 843 556 8171
gei com
November 30, 2023
Chris Cameron
Cameron Testing Services,Inc.
219 S.Steele St.
Sanford,North Carolina 27330
Re:Routine Analytical
Work Order:645884
Dear Chris Cameron:
GEL Laboratories,LLC(GEL)appreciates the opportunity to provide the enclosed analytical results for the
sample(s)we received on November 17,2023.This original data report has been prepared and reviewed in
accordance with GEL's standard operating procedures.
The samples were delivered with proper chain of custody documentation and signatures.All sample containers
arrived without any visible signs of tampering or breakage.Containers indicated on chain of custody did not
match what was received.Five vials with liquid were included with one 250mL glass amber bottle..
Test results for NELAP or ISO 17025 accredited tests are verified to meet the requirements of those standards,
with any exceptions noted.The results reported relate only to the items tested and to the sample as received by
the laboratory.These results may not be reproduced except as full reports without approval by the laboratory.
Copies of GEL's accreditation and certifications can be found on our website at www.gel.com.
Our policy is to provide high quality,personalized analytical services to enable you to meet your analytical needs
on time every time.We trust that you will find everything in order and to your satisfaction.If you have any
questions,please do not hesitate to call me at(843)556-8171,ext.4422.
Sincerely,
4M jj,,�Z�
Adrian Melendrez for
Jacob Crook
Project Manager
Enclosures

GEL LABORATORIES LLC
2040 Savage Road Charleston SC 29407-[phone] -www.gel.com
Certificate of Analysis Report
for
CAMT001 Cameron Testing Services
Client SDG: 645884 GEL Work Order: 645884
The Qualifiers in this report are defined as follows:
* A quality control analyte recovery is outside of specified acceptance criteria
** Analyte is a Tracer compound
Analyte is a surrogate compound
U Analyte was analyzed for,but not detected above the MDL,MDA,MDC or LOD.
Where the analytical method has been performed under NELAP certification,the analysis has met all of the
requirements of the NELAC standard unless qualified on the Certificate of Analysis.
The designation ND, if present,appears in the result column when the analyte concentration is not detected above
the limit as defined in the'U'qualifier above.
This data report has been prepared and reviewed in accordance with GEL Laboratories LLC
standard operating procedures.Please direct any questions to your Project Manager,Jacob Crook.
Reviewed by
Page 2 of 10 SDG: 645884

GEL LABORATORIES LLC
2040 Savage Road Charleston SC 29407- [phone] -www.gel.com
Certificate of Analysis
Report Date: November 30,2023
Company : Cameron Testing Services,Inc.
Address : 219 S. Steele St.
Sanford,North Carolina 27330
Contact: Chris Cameron
Project: Routine Analytical
Client Sample ID: Hamlet Effluent Project: CAMT00122
Sample ID: 645884001 Client ID: CAMT001
Matrix: Waste Water
Collect Date: 02-NOV-23 08:00
Receive Date: 17-NOV-23
Collector: Client
Parameter Qualifier Result DL RL Units PF DF Analyst Date Time Batch Method
Mercury Analysis-CVAA -- - -
EPA 1631 Low Level Mercury Analysis "As Received"
Mercury U <0.500 0.200 0.500 ng/L I LYG1 11/28/23 1432 2531474 1
The following Analytical Methods were performed:
Method Description _ _ Analyst Comments
1 - EPA 1631E -
Notes:
Column headers are defined as follows:
DF:Dilution Factor Lc/LC:Critical Level
DL:Detection Limit PF:Prep Factor
MDA: Minimum Detectable Activity RL:Reporting Limit
MDC:Minimum Detectable Concentration SQL:Sample Quantitation Limit
Page 3 of 10 SDG: 645884

GEL LABORATORIES LLC
2040 Savage Road Charleston SC 29407- [phone] -www.gel.com
Certificate of Analysis
Report Date: November 30,2023
Company : Cameron Testing Services,Inc.
Address : 219 S. Steele St.
Sanford,North Carolina 27330
Contact: Chris Cameron
Project: Routine Analytical
Client Sample ID: Trip Blank Project: CAMT00122
Sample ID: 645884002 Client ID: CAMT001
Matrix: BLANK
Collect Date: 02-NOV-23 08:00
Receive Date: 17-NOV-23
Collector: Client
Parameter Qualifier Result DL RL Units PF DF Analyst Date Time Batch Method
Mercury Analysis-CVAA -
EPA 1631 Low Level Mercury Analysis "As Received"
Mercury U <0.2 0.200 0.500 ng/L I LYGI 11/28/23 1322 2531474 1
The following Analytical Methods were performed:
Method Description_ _ _ Analyst Comments
1 EPA 1631E -
Notes:
Colwnn headers are defined as follows:
DF:Dilution Factor Lc/LC:Critical Level
DL:Detection Limit PF:Prep Factor
MDA:Minimum Detectable Activity RL: Reporting Limit
MDC: Minimum Detectable Concentration SQL: Sample Quantitation Limit
Page 4 of 10 SDG: 645884

GEL LABORATORIES LLC
2040 Savage Road Charleston, SC 29407 -[phone] -www.gel.com
QC Summary
Cameron Testing Services,Inc. Report Date:November 30,2023
219 S.Steele St. Page I of
Sanford,North Carolina
Contact: Chris Cameron
Workorder: 645884
Parmname NOM _ Sample Qual QC Units RPD/D% REC% Range Anlst Date Time
Metals Analysis-Mercury - -
3atch 2531474
QC1205585903 LCS
Mercury 5.00 5.15 ng/L 103 (77%-123%) LYG1 11/28/2313:1
QC1205585902 MB
Mercury U ND ng/L 11/28/2313:0
QC1205585907 646101003 MS
Mercury 2.50 U <0.500 2.59 ng/L 87.7 (71%-125%) 11/28/2314:0
QC1205586275 646101003 MSD
Mercury 2.50 U <0.500 2.56 ng/L 1.2 86.5 (0%-24%) 11/28/2314:0
Notes:
The Qualifiers in this report are defined as follows:
U Analyte was analyzed for,but not detected above the MDL,MDA,MDC or LOD.
J Value is estimated
X Consult Case Narrative,Data Summary package,or Project Manager concerning this qualifier
N Metals--The Matrix spike sample recovery is not within specified control limits
H Analytical holding time was exceeded
< Result is less than value reported
> Result is greater than value reported
h Preparation or preservation holding time was exceeded
R Sample results are rejected
^ RPD of sample and duplicate evaluated using+/-RL. Concentrations are<5X the RL. Qualifier Not Applicable for Radiochemistry.
N/A RPD or%Recovery limits do not apply.
ND Analyte concentration is not detected above the detection limit
E %difference of sample and SD is>10%. Sample concentration must meet flagging criteria
NJ Consult Case Narrative,Data Summary package,or Project Manager concerning this qualifier
Q One or more quality control criteria have not been met.Refer to the applicable narrative or DER.
FB Mercury was found present at quantifiable concentrations in field blanks received with these samples. Data associated with the blank are deemed
invalid for reporting to regulatory agencies
Page 5 of 10 SDG: 645884

GEL LABORATORIES LLC
2040 Savage Road Charleston, SC 29407 -[phone] www.get.com
Workorder: 645884 QC Summary
Page 2 of
Parmname _ NOM _Sample-Qual QC Units RPD/D% REC% Range Anist Date Time
NI See case narrative
Y Other specific qualifiers were required to properly define the results.Consult case narrative.
J See case narrative for an explanation
N/A indicates that spike recovery limits do not apply when sample concentration exceeds spike cone.by a factor of 4 or more or%RPD not applicable.
^The Relative Percent Difference(RPD)obtained from the sample duplicate (DUP)is evaluated against the acceptance criteria when the sample is greater than
five times(5X)the contract required detection limit(RL).In cases where either the sample or duplicate value is less than 5X the RL,a control limit of+/-the
RL is used to evaluate the DUP result.
*Indicates that a Quality Control parameter was not within specifications.
For PS,PSD,and SDILT results,the values listed are the measured amounts,not final concentrations.
Where the analytical method has been performed under NELAP certification,the analysis has met all of the
requirements of the NELAC standard unless qualified on the QC Summary.
Page 6 of 10 SDG: 645884

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Client:M I LaboratffieS LLC SAMPLE RECEIPT&REVIEW FORM
talent:
-,Cq- SI)G/AWCOCfwGrk0Wer. J4Y 14-
Received qBy.- A
Date Received:
Cir.le Applicable;
FedEx Express FedEx Ground UPS Field Services Courier
Carrier and Trucking Number
L
L
Suspected HagAM Information
T" *If Net ennats>1 D4m on samples not marked"radioactive",contact the Radiation Safety Group for further investigation.
to 11a"zard Class Shipped: UN#:
A)Shipped as a DOT hazardous? IfUN2910.Is the Radioactive Shipment Survey Compliant?yes No—
I -
.-
B)Did the client designate the samples are to be
%.006
received w radioactive? !��Is on-11"w
Did the RSO classify the samples as imum Net Counts Observed*(Observed Counts-Area Background Counts): C-PM I mRfflr
radioactivC7 Classified an; R-d I Rod 2 Rad 3
7.3.
D)Did the client designate samples sac hazardous?
D ar H is yes,sated Hazards below.
Did the RSO Identify possible hazards?-- PCWs Flammable Foreign Soil RCRA Asbestos Beryllium Other..
- Sample Receipt Criteria C mmentsw'Qualifiery(Required for Nan-Cunforming Items)
Shipping containers received intact and Cirrk Applicable; Scab broken Damaged coutahtor Leaking container offier(dewrilm)
scaled?
2 Chain of custody domurwrits included Circle Applicable; Client contacted and provided MC COC created upon recolpt
with shipment?
Preservation Method: Wet ice Ice Packs Dryice None Other:
3 Samples requiring cold preservation *all temperatures am recorded in Isius
6 deg.C)7* fo 1, 1, J. �- - TEMP:
4 Daily check performed arm]passed on IR Temperature Device Seral#-.
temperature gun? Secondary'remperature Devi"Seri #(If Appli ble):
Circb
5 Sample containers intact and sealed? pplizable: Seals broken Damaged container Leakiugeordwinor QhW(dF,;.�rlb.)
6 Samples requiring chemical preservation SampleVs and Containers Affected:
at proper p117 If Preservation added,LoW
If yes,are Encores or Soil Kits present for solids?Yes—No NA _(If yes,take to VOA Freezer)
7 Do any samples require Volatile qP liquid VOA vials contain acid preservation?Yes-_Nn---NA—(If unknown,s Awt—N.)
Analysis?
Are liquid VOA vials free of headspaccf-Y-es
V Sample 113's arn!containers affected:
Nq-- NA--
8 Samplmq received within holding time? ID's NW tests affected:
9 Sample ID's on COC match ID's on ID's and containers affected:
bottles?
10 Date&time on COC match date&time Circle Applicable: No dates on containers No times on containers COC missing info Other(describe)
on bottles?
11 Number of containers received match CircleApplicable: No container count on coc scribe)
number indicated on COC?
12 Arc sample containers identifiableas
GEL provided by use of GEL labels?
13 COC form is properly signed in CircleApplicnble: Not relinquished Other(describe)
relinquished/received sections?
Comments(Use Continuation Form if needed):
V aryi r Cxrlb w V W
1'1�Uld ') r)C1UdV-Ck
PM(or PMA)rcvicvr.Initials
Date age 8 of 10 SDG: 645884 1-3 Page—t-of
P t
GL-CHL-SR-DOI Rov7

List of current GEL Certifications as of 30 November 2023
State _ Certification
Alabama 42200
Alaska - - - — 17-018
Alaska Drinking Water SC00012
Arkansas _ - 88-00651 -
CLIA t _ 42DO904046
California 2940
Colorado SC00012
Connecticut PH-0169
DoD FLAP/ISO I7025 A2LA 2567.01
_Florida NELAP_ _ E87156
Foreign Soils Permit 0330-15-00283,P330-15-00253
Georgia - I -SC00012 -I
Georgia SDW_A 967
Hawaii SC00012
- Idaho L SC00012
Illinois NELAP 20002q
_ Indiana — _C-SC-61 - #
Kansas NELAP
E-10332
Kentucky SDWA KY90129
Kentucky Wastewater KY90129
Louisiana Drinking Water LA024
Louisiana NELAP 03046(AI3-3904)
Maine 2023019
C _Maryland . - I _ - 270
Massachusetts_ t M-SCO 12
Massachusetts PFAS Approv }
Letter
Michigan _ --i 9976
Mississippi SCO0012
Nebraska f NE-OS-26-13 j
Nevada _ SC000122024-05
New Hampshire NELAP 2054
_ New Jersey NELAP _ SCO02
New Mexico SC00012
New York NELAP _ 11501
North Carolina 233
North Carolina SDWA 45709
North Dakota_ R-158
Oklahoma 2023-152
Pennsylvania NELAP 68-00485
Puerto Rico SC00012
- S.Carolina Radiochem 10120002
Sanitation Districts of L 9255651 j
_South_Carolina Chemistry_ 10120001
r Tennessee TN 02934
- _ Texas NELAP T T104704235-23-21
Utah NELAP SC000122023-38
Vermont 1 VT87156 -- {
Virginia NELAP j 460202
Washington - _C780
Page 9 of 10 SDG: 645884

Metals
Technical Case Narrative
Cameron Testing Services
SDG#: 645884
Product: Mercury Analysis Using the PS Analytical Millennium Automated Mercury Analyzer
Analytical Method:EPA 1631E
Analytical Procedure: GL-MA-E-018 REV# 19
Analytical Batch: 2531474
The following samples were analyzed using the above methods and analytical procedure(s).
GEL Sample ID# Client Sample Identification
645884001 Hamlet Effluent
645884002 Trip Blank
1205585902 Method Blank(MB)CVAF
1205585903 Laboratory Control Sample(LCS)
1205585907 646101003(NonSDGS)Matrix Spike(MS)
1205586275 646101003(NonSDGSD)Matrix Spike Duplicate(MSD)
The samples in this SDG were analyzed on an"as received"basis.
Data Summary
There are no exceptions,anomalies or deviations from the specified methods.All sample data provided in this
report met the acceptance criteria specified in the analytical methods and procedures for initial calibration,
continuing calibration,instrument controls and process controls where applicable.
Certification Statement
Where the analytical method has been performed under NELAP certification,the analysis has met all of the
requirements of the NELAC standard unless otherwise noted in the analytical case narrative.
Page 10 of 10 SDG: 645884