Loading...
HomeMy WebLinkAboutWQ0001817_Monitoring - 11-2023_20231226 (2)Monitoring Report Submittal ................................................... Permit Number#* WQ0001817 Name of Facility:* Month: * November Report Information Albemarle Utility Company Year:* 2023 Type* Upload Document* NDMR, NDAR-1, NDAR-2, NDMLR November 2023 MR's.pdf 8.39MB PDF Only GW-59 November 2023 MW.s.pdf 26.49MB PDF Only Please upload one PDF containing all applicable monitoring reports (i.e., NDMR, NDAR-1, NDAR-2, NDMLR, GW-59). Confirmation Email Address: * danny.perry@albemarleplantation.com Name of Submitter: * Danny S Perry Signature: a�a�rirJ S� t tf Date of submittal: 12/26/2023 This will be filled in automatically Initial Review Reviewer: Wanda.Gerald Is the project number correct?* WQ0001817 Is the monitoring report accepted?* Yes No Regional Office* Washington Reviewer: _anonymous Review Date: 1/16/2024 SUBMIT FORM ON YELLOW PAPER ONLY • • DEPARTMENT OF ENVIRONMENTAL QUALITY - DIV. OF WATER RESOURCES GROUNDWATER QUALITY MONITORING: INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM • • 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: Expiration Date: 05-31-2025 Facility Name: Albemarle Utility Comapany Non -Discharge WQ0001817 UIC Permit Name (if different): NPDES Other Facility Address: 862 Holiday Island RD TYPE OF PERMITTED OPERATION BEING MONITORED ❑■ Lagoon ❑ Remediation: Infiltration Gallery Hertford N.0 27944 County Perqimans ❑■ Spray Field ❑ Remediation: Contact Person: Danny Shelton Perry ORC Telephone#: 252-426-1007 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name: North of Holding Lagoon No. of wells to be sampled: 10 ❑ Water Source Heat Pump ❑ Other: from Permit SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW -1 Date sample collected: 11/16/2023 FIELD ANALYSES: WAS Well Depth: 20 ft. Well Diameter: 2 in. pH 00400: 5.2 units Temp. 000lo: 19.5 °C DRY at Depth to Water Level 82546:18.0 ft. below measuring point Screened Interval: -5 ft. to -20 ft. Spec. Cond. 00094: µM of timehos sampling, Measuring Point is 3 ft. above land surface Relative M.P. Elevation: ft. Odor 00085: None check Volume of water pumped/bailed before sampling: 5.0 gallons Appearance Tan here:❑ Samples for metals were collected unfiltered: ❑ YES ❑■ NO and field acidified: ❑ YES ■❑ NO LABORATORY INFORMATION Date sample analyzed:11/16/2023 Laboratory Name: Environmental Chemists, Inc Certification No. 94 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 0.26 mg/L Pb - Lead 01051 ug/L Coliform: MF Fecal 31616 <1 /100mL Nitrate (NO3) as N 00620 <0.02 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 70300 179 mg/L Al - Aluminum 01105 mg/L pH (Lab) 00403 5.2 units Ba - Barium 01007 ug/L TOC 00680 4.2 mg/L Ca - Calcium 00916 mg/L Chloride 00940 61 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total olo34 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? ❑ Yes (1) ❑ No (0) pecific Conductance 00095 µMhos K - Potassium 00937 mg/L VOC 7873 method # Total Ammonia 00610 <0.2 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen; NH, as N; Ammonia Nitrogen, Total) Mn - Manganese 01055 ug/L , method # TKN as N 00625 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% Shayne Lamb Corporate Secretary Permittee (or Authorized Aqent) Name and Title - Please print or type GW-59 Rev.06-07-2018 M ANALYTICAL 8 CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab - 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 - 910.347.5843 Lab; `Fax i nfoi.4-environmentalchem ists.com Albemarle Utility Date of Report: Dec 21, 2023 862 Holiday Island Road Customer PO M Hertford NC 27944 Customer ID: 09110024 Attention Report #: 2023-26955 Project ID: Monitoring Wells Lab ID Sample ID: Collect Date/Time Matrix Sampled by 23-65312 Site: MWA 11/16/2023 11:50 AM Water jcb/envirochem Test Method Results Date Analyzed Color Color Tan 11/16/2023 Depth to water, ft. Depth to Water. Ft. 18.0 feet 11 /16/2023 Ammonia Nitrogen EPA 350.1. Rev. 2.0, 1993 < 0.2 mg/L 11/29/2023 Gallons bailed before sampling Gallons Bailed before sampling 5.0 gallons 11/16/2023 Odor Qualitative None 11/16/2023 Total Dissolved Solids (TDS) SM 2540 C-2015 179 mg/L 11/17/2023 Temperature SM 2550 B-2010 19.5 C 11/16/2023 pH SM 4500 H B-2011 5.2 units 11/16/2023 Total Organic Carbon (TOC) SM 5310 B-2014 4.2 mg/L 11/20/2023 1. 1, 1,2-Tetrachloroethane SM6200B-2011 <0.5pg/L 11/20/2023 1, 1, 1 -Trichloroethane SM 6200 B-2011 <0.5 pg/L 11/20/2023 1,1,2,2-Tetrachloroethane SM 6200 8.2011 <0.5 pg/L 11/20/2023 1,1,2-Trichloroethane SM 6200 B-2011 <0.5 pg/L 11/20/2023 1,1-D ich loroeth an a SM 8200 B-2011 <0.5 pg/L 11/20/2023 1,1-D ichloroethene SM 6200 B-2011 <0.5 pg/L 11 /2012023 1,1-Dichloropropene SM 8200 B-2011 <0.5 pg/L 11/20/2023 1,2,3-Trichlorobenzene SM 6200 B-2011 <0.5 pg/L 11/20/2023 1,2,3-Trichloropropane SM 6200 B-2011 <0.5 pg/L 11/20/2023 1,2,4-Trichlorobenzene SM 6200 6-2011 <0.5 pg/L 11/2012023 1,2,4-Trimethylbenzene SM 6200 B-2011 <0.5 pg/L 11/20/2023 1,2-Dibromo-3-Chloropropane SM 6200 B-2011 <0.5 pg/L 11/20/2023 1,2-Dibromoethane SM 6200 8-2011 <0.5 pg/L 11/20/2023 1,2-Dichlorobenzene SM 6200 B-2011 <0.5 pg/L 11/20/2023 1,2-Dichloroethane SM 6200 B-2011 <0.5 pg/L 11/20/2023 1,2-Dichloropropane SM 6200 B-2011 <0.5 pg/L 11/20/2023 1, 3, 5-Trimethylbenzene SM 6200 B-2011 <0.5 pg/L 11/20/2023 Report #: 2023-26955 Page 1 of 30 Environmental Chemists, Inc. " 6602 Windmi:l Way, Wilmington, NC 28405 " 910.392.0223 Lab . 910.392.4424 Fax " 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 - 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS info@environmentalchemists.com Albemarle Utility Date of Report: Dec 21, 2023 862 Holiday Island Road Customer PO #: Hertford NC 27944 Customer ID: 09110024 Attention: Report #: 2023-26955 Project ID: Monitoring Wells 1,3-Dichlorobenzene SM 0200 B-2011 <0.5 Ng/L 11/20/2023 1,3-Dichloropropane SM 8200 B-2011 <0.5 Ng/L 11/20/2023 1,4-Dichlorobenzene SM 6200 B-2011 <0.5 pg/L 11/20/2023 2,2-Dichloropropane SM 6200 B-2011 <0.5 lag/L 11/20/2023 2-Chlorotoluene SM 6200 B-2011 <0.5 lag/L 11/20/2023 4-Chlorotoluene SM 6200 8-2011 <0.5 pg/L 11/20/2023 Benzene SM 6200 B-2011 <0.5 pg/L 11/20/2023 Bromobenzene SM 6200 B-2011 <0.5 pg/L 11/20/2023 Bromochloromethane SM 6200 B-2011 <0.5 Ng/L 11/2012023 Bromodichloromethane SM 6200 B-2011 <0.5 Ng/L 11/20/2023 Bromoform SM 6200 B-2011 <0.5 pg/L 11/20/2023 Bromomethane SM 6200 B-2011 <0.5 pg/L 11/20/2023 Carbon tetrachloride SM 6200 B-2011 <0.5 pg/L 11/20/2023 Chlorobenzene SM 6200 8-2011 <0.5 pg/L 11/20/2023 Chloroethane SM 6200 B-2011 <0.5 pg/L 11/20/2023 Chloroform SM 0200 B-2011 <0.5 pg/L 11/20/2023 Chloromethane SM 6200 B-2011 <0.5 Ng/L 11/20/2023 cis-1,2-Dich loroethene SM 6200 B-2011 <0.5 Ng/L 11/20/2023 cis-1, 3-Dich loro propene SM 6200 B-2011 <0.5 pg/L 11/20/2023 Dibromochloromethane SM 6200 B-2011 <0.5pg/L 11/20/2023 D iromomethane SM 6200 8-20.11 <0. 5 pg/L 11/20/2023 Dichlorodifluoromethane SM 6200 8-2011 <0.5 pg/L 11/20/2023 Ethylbenzene SM 6200 B-2011 <0.5 pg/L 11/20/2023 Hexachlorobutadiene SM 6200 B-2011 <0.5 pg/L 11/20/2023 Isopropylbenzene SM 6200 B-2011 <0.5 pg/L 11/20/2023 M+P Xylene SM 6200 B-2011 <1.0 pg/L 11/20/2023 Methylene chloride SM 6200 B-2011 <0.51ag/L 11/20/2023 Naphthalene SM 6200 B-2011 <0.5 lag/L 11/20/2023 n-Butylbenzene SM 6200 a-2011 <0.5 pg/L 11/20/2023 Report at: 2023-26955 Page 2 of 30 ANALYTICAL & CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 r 910.392.0223 Lab W 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 . 252.473.5702 Lab r Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab;' Fax infor« environmentalchemists.com Albemarle Utility Date of Report: Dec 21, 2023 862 Holiday Island Road Customer PO #: Hertford NC 27944 Customer ID: 09110024 Attention: Report #: 2023-26955 Project ID: Monitoring Wells n-Propylbenzene SM 6200 B-2011 <0.5 pg/L 11/20/2023 ortho-Xylene SM 6200 B-2011 <0.5 pg/L 11/20/2023 p-Isopropyltoluene SM 6200 B-2011 <0.5 pg/L 11/20/2023 sec-Butylbenzene SM 6200 B-2011 <0.5 pg/L 11/20/2023 Styrene SM 8200 B-2011 <0.5 pg/L 11/20/2023 tert-Butylbenzene SM 6200 B-2011 <0.5 pg/L 11/20/2023 Tetrachloroethene SM 6200 8-2011 <0.5 pg/L 11/20/2023 Toluene SM 0200 B-2011 <0.5 pg/L 11/20/2023 Trans-1,2-Dichloroethene SM 6200 B-2011 <0.5 pg/L 11/20/2023 Trans-1,3-dichloropropene SM6200B-2011 <0.5pg/L 11/20/2023 Trichloroethene SM 6200 B-2011 <0.5 pg/L 11/20/2023 Trichlorofluoromethane SM 6200 B-2011 <0.5 pg/L 11/20/2023 Vinyl chloride SM 6200 B-2011 <0.5 pg/L 11/20/2023 Fecal Coliform SM 9222 0-2016 MF <1 Colonies/100ml- 11/16/2023 Chloride SM4500 CI E-2011 61 mg/L 11/24/2023 Nitrate Nitrogen (Calc) Nitrite Nitrogen EPA 353 2, Rev. 2 0,1993 0.26 mg/L 11 /16/2023 Nitrate+Nitrite-Nitrogen EPA 353.2, Rev 2.0. 1993 0.06mg/L 11/20/2023 Nitrate Nitrogen Subtraction Method <0.02 mg/L 12/15/2023 9 Report t 2023-26955 Page 3 of 30 SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: • • DEPARTMENT OF ENVIRONMENTAL QUALITY - DIV. OF WATER RESOURCES INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: Expiration Date: 05-31-2025 Facility Name: Albemarle Utility Company Non -Discharge WQ0001817 UIC Permit Name (if different): NPDES Other Facility Address: 862 Holiday Island Rd TYPE OF PERMITTED OPERATION BEING MONITORED Hertford NC 27944 County Perquimans ❑■ Lagoon ❑ Remediation: Infiltration Gallery ❑■ Spray Field ❑ Remediation: Contact Person: Danny Shelton Perry ORC Telephone#: 252-426-1007 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name: East of Baffle Lagoon No. of wells to be sampled: 10 ❑ Water Source Heat Pump ❑ Other: from Permit SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW-2 Date sample collected: 11/16/2023 FIELD ANALYSES: WAS Well Depth: 12 ft. Well Diameter: 2 in. pH 00400: 5.0 units Temp. 000lo: 19.8 °C DRY at Depth to Water Level 82546: 8.4 ft. below measuring point Screened Interval: -2 ft. to -12 ft. Spec. Cond. 00094: µMhos time of 3 sampling,check Measuring Point is ft. above land surface Relative M.P. Elevation: ft. Odor 000m: Sulfur Volume of water pumped/bailed before sampling: 1.0 gallons Appearance Grey/Turbid here: El Samples for metals were collected unfiltered: ❑ YES ❑■ NO and field acidified: ❑ YES ❑■ NO LABORATORY INFORMATION Date sample analyzed:11/16/2023 Laboratory Name: Environment Chemists, Inc Certification No. 94 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 0.17 mg/L Pb - Lead 01051 ug/L Coliform: MF Fecal 31616 <1 colonies /100mL Nitrate (NO3) as N 00620 <0.02 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 70300 993 mg/L Al - Aluminum of lo5 mg/L pH (Lab) 00403 5.0 units Ba - Barium 01007 ug/L TOC 00680 20.7 mg/L Ca - Calcium 00916 mg/L Chloride 00940 25 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total 01034 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? ❑ Yes (1) ❑ No (0) Specific Conductance 00095 µMhos K - Potassium 00937 mg/L VOC 7873 method # Total Ammonia 00610 0.8 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen; NH3as N; Ammonia Nitrogen, Total) Mn - Manganese o1055 ug/L method # TKN as N 00625 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% GW-59 Rev.06-07-2018 '3M ANALYTICAL & CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 - 910.392.0223 Lab - 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 - 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 - 910.347.5843 Lab,' Fax info,ci environmentalchemists com Albemarle Utility Date of Report: Dec 21, 2023 862 Holiday Island Road Customer PO M Hertford NC 27944 Customer ID: 09110024 Attention: Report M 2023-26955 Project ID: Monitoring Wells Lab ID Sample ID: Collect Date/Time Matrix Sampled by 23-65316 Site: MW-2 11/16/2023 11:35 AM Water jcb/envirochem Test Method Results Date Analyzed Color color Grey/Turbid 11 /16/2023 Depth to water, ft. Depth to water, Ft. 8.4 feet 11/16/2023 Ammonia Nitrogen EPA 350.1. Rev. 2.0. 1993 0.8 mg/L 11/29/2023 Gallons bailed before sampling Gallons Bailed before sampling 1 (dry) gallons 11/16/2023 Odor Qualitative Sulfur 11/16/2023 Total Dissolved Solids (TDS) SM 2540 C-2015 993 mg/L 11/17/2023 Temperature SM 2550 B-2010 19.8 C 11/16/2023 pH SM 4500 H B-2011 5.0 units 11/16/2023 Total Organic Carbon (TOC) SM S310 B-2014 20.7 mg/L 11/20/2023 1,1.1.2-Tetrachloroethane SM 6200 B-2011 <0.5 pg/L 11/20/2023 1,1,1-Trichloroethane SM 6200 0-2011 <0.5 pg/L 11/20/2023 1,1,2,2-Tetrachloroethane SM6200B-2011 <0.5pg/L 11/20/2023 1,1,2-Trichloroethane SM 6200 B-2011 <0.5 pg/L 11/20/2023 1,1-Dichloroethane SM 6200 B-2011 <0.5 pg/L 11/20/2023 1,1-Dichloroethene SM 8200 B-2011 <0.5 pg/L 11/20/2023 1,1-Dichloropropene SM 8200 B-2011 <0, 5 pg/L 11/20/2023 1,2,3-Trichlorobenzene SM 6200 B-2011 <0.5 pg/L 11/20/2023 1,2,3-Trichloropropane SM 6200 B-20i 1 <0.5 pg/L 11/20/2023 1,2,4-Trichlorobenzene SM 6200 8.2011 <0.5 pg/L 11/20/2023 1,2,4-Trimethylbenzene SM 6200 B-2011 <0.5 pg/L 11/20/2023 1.2-Dibromo-3-Chloropropane SM 6200 B-2011 <0.5 pg/L 11/20/2023 1,2-Dibromoethane SM 6200 B-2011 <0.5 pg/L 11/20/2023 1,2-Dichlorobenzene SM 8200 B-2011 <0.5 pg/L 11/20/2023 1,2-Dichloroethane SM 6200 8.2011 <0.5 pg/L 11/20/2023 1,2-Dichloropropane SM 6200 8-2011 <0.5 pg/L 11/20/2023 1,3,5-Trimethylbenzene SM 6200 8-2011 <0.5 pg/L 11/20/2023 Report# 2023-26955 Page 4 of 30 envirochem ANALYTICAL & CONSULTING CHEMISTS Albemarle Utility 862 Holiday Island Road Hertford NC 27944 Attention: Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 - 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab ,'Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax info verivironmentalchemists.com Date of Report: Dec 21, 2023 Customer PO #: Customer ID: 09110024 Report #: 2023-26955 Project ID: Monitoring Wells 1,3-DichlorobenzeneSM 8200 8-2011 <0.5pg/L-11/2._n0..l.20w...2_3.. „ 1,3-Dichloropropane SM 6200 B-2011 <0.5 pg/L 11/20/2023 1,4-Dichlorobenzene SM 6200 8-2011 <0.5 pg/L 11/20/2023 2,2-Dichloropropane SM 6200 B-2011 <0.5 pg/L 11/20/2023 2-Chlorotoluene SM 6200 B-2011 <0.5 pg/L 11/20/2023 4-Chlorotoluene SM 6200 B-2011 <0.5 pg/L 11/20/2023 Benzene SM 0200 B-2011 <0.5 pg/L 11/20/2023 Bromobenzene SM 6200 B-2011 <0 5 pg/L 11/20/2023 Bromochloromethane SM5200 B-2011 <0.5 pg/L 11/20/2023 Bromodichloromethane SM 6200 B-2011 <0.5 pg/L 11 /20/2023 Bromoform SM 6200 B-2011 <0.5 pg/L 11/20/2023 Bromomethane SM 6200 B-2011 <0.5 p g/L 11/20/2023 Carbon tetrachloride SM 8200 B-2011 <0.5 pg/L 11/20/2023 Chlorobenzene SM 6200 B-2011 <0.5 pg/L 11/20/2023 Chloroethane SM 6200 B-2011 <0.5 pg/L 11/20/2023 Chloroform SM 6200 8-2011 <0.5 pg/L 11/20/2023 Chloromethane SM 6200 B-2011 <0.5 pg/L 11/20/2023 cls-1, 2-Dich loroethene SM 6200 8-2011 <0.5 pg/L 11/20/2023 cis- 1. 3-Dichloropropene SM 6200 B-2011 <0. 5 pg/L 11/20/2023 Dibromochloromethane SM 6200 B-2011 <0. 5 pg/L 11/20/2023 Dibromomethane SM 6200 B-2011 <0 5 pg/L 11/20/2023 Dichlorodifluoromethane SM 6200 B-2011 <0 5 pg/L 11/20/2023 Ethylbenzene SM 6200 B-2011 <0.5 pg/L 11/20/2023 Hexachlorobutadiene SM 6200 B-2011 <0.5 pg/L 11 /20/2023 Isopropylbenzene SM 6200 B-2011 <0.5 pg/L 11/20/2023 M+P Xylene SM 6200 B-2011 <1.0 pg/L 11/20/2023 Methylene chloride SM 6200 B-2011 <0.5 pg/L 11 /20/2023 Naphthalene SM 6200 B-2011 <0.5 pg/L 11 /20/2023 n-Butylbenzene SM 6200 B-2011 <0.5 pg/L 11 /20/2023 Report #: 2023-26955 Page 5 of 30 ANALYTICAL & CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab o 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 . 252.473.5702 Lab Fax 255-A Wilmington Highway, Jacksonville, NC 28540 - 910.347.5843 Lab: Fax info@environmentalchemists.com Albemarle Utility Date of Report: Dec 21, 2023 862 Holiday Island Road Customer PO #: Hertford NC 27944 Customer ID: 09110024 Attention: Report #: 2023-26955 Project ID: Monitoring Wells n-Propylbenzene SM 6200 B-2011 <0.5 µg/L 11/20/2023 ortho-Xylene SM 6200 B-2011 <0.5 µg/L 11/20/2023 p-Isopropyltoluene SM 6200 B-2011 <0.5 µg/L 11/20/2023 sec-Butylbenzene SM 6200 B-2011 <0.5 µg/L 11/20/2023 Styrene SM 6200 B-2011 <0.5 µg/L 11/20/2023 tert-Butylbenzene SM 6200 B-2011 <0.5 µg/L 11/20/2023 Tetrachloroethene SM 6200 B-2011 <0.5 µg/L 11/20/2023 Toluene SM 6200 B-2011 <0.5 µg/L 11/20/2023 Trans-1,2-Dichloroethene SM6200B-2011 <0.5µg/L 11/20/2023 Trans-1,3-dichloropropene SM6200B-2011 <0.5µg/L 11/20/2023 Trichloroethene SM 6200 B-2011 <0.5 µg/L 11/20/2023 Trichlorofluoromethane SM 6200 B-2011 <0.5 µg/L 11/20/2023 Vinyl chloride SM 6200 B-2011 <0.5 µg/L 11/20/2023 Fecal Coliform SM9222 D-2015MF <1 Colonies/100ml- 11/16/2023 Chloride SM4500 CI E-2011 25 mg/L 11 /24/2023 Nitrate Nitrogen (Cale) Nitrite Nitrogen EPA 353 2 Rev 2 0, 1993 0.17 mg/L 11 /16/2023 Nitrate+Nitrite-Nitrogen EPA 353 2 Rev 2 Or 1993 0.04 mg/L 11/20/2023 Nitrate Nitrogen Subtraction Method <0.02 mg/L 12/15/2023 Report N: 2023-26955 Page 6 of 30 SUBMIT FORM ON YELLOW PAPER ONLY • • DEPARTMENT OF ENVIRONMENTAL QUALITY - DIV. OF WATER RESOURCES GROUNDWATER QUALITY MONITORING: INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 FACILITY INFORMATION Please Pnnt Clearly or Type PERMIT Number: Expiration Date: 05-31-2025 Facility Name: Albemarle Utility Company Non -Discharge WQ0001817 UIC NPDES Other Permit Name (if different): Facility Address: 862 Holiday Island Rd TYPE OF PERMITTED OPERATION BEING MONITORED M Lagoon ❑ Remediation: Infiltration Gallery Hertford NC 27944 County Perquimans ❑■ Spray Field ❑ Remediation: Contact Person: Danny Shelton Perry ORC Telephone#: 252-426-1007 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name: South East of Spray field No. of wells to be sampled: 10 ❑ Water Source Heat Pump ❑ Other: from Permit SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW - 3 Date sample collected: 11/16/2023 FIELD ANALYSES: WAS Well Depth: 12 ft. Well Diameter: 2 in. pH oo400: 6.0 units Temp. 000lo: 1 9.4 °C DRY at Depth to Water Level 82546: 8.9 ft. below measuring point Screened Interval: -2 ft. to -12 ft. Spec. Cond. 00094: µMhos time of sampling, Measuring Point is 3 ft. above land surface Relative M.P. Elevation: ft. Odor 00085: none check Volume of water pumped/bailed before sampling: 2 gallons Appearance Grey/Turbid here:❑ Samples for metals were collected unfiltered: ❑ YES K NO and field acidified: ❑ YES ■❑ NO LABORATORY INFORMATION Date sample analyzed:11/16/2023 Laboratory Name: Environmental Chemists, Inc Certification No. 94 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 0.22 mg/L Pb - Lead 01051 ug/L Coliform: MF Fecal 31616 <1 colonies /100mL Nitrate (NO3) as N 00620 0.22 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 70300 390 mg/L Al - Aluminum 01105 mg/L pH (Lab) 00403 6.0 units Ba - Barium 01007 ug/L TOC 00680 31.1 mg/L Ca - Calcium 00916 mg/L Chloride 00940 15 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total olo34 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? ❑ Yes (1) ❑ No (0) pecific Conductance 00095 µMhos K - Potassium 00937 mg/L VOC 7873 method # Total Ammonia 00610 0.5 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen; NH3asN; Ammonia Nitrogen, Total) Mn - Manganese o1055 ug/L , method # TKN as N 00625 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% Shayne Byrum - Corporate Secretary Permittee (or Authorized Aqent) Name and Title - Please print or type GW-59 Rev.06-07-2018 i.0 ANALYTICAL & CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 - 910.392.0223 Lab - 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 - 910.347.5843 Lab Fax in foirtsnvi ronmen talchemists.com Albemarle Utility Date of Report: Dec 21, 2023 862 Holiday Island Road Customer PO #: Hertford NC 27944 Customer ID: 09110024 Attention: Report #: 2023-26955 Project ID: Monitoring Wells Lab ID Sample ID: Collect Date/Time Matrix Sampled by 23-65317 Site: MW-3 11/16/2023 11.25 AM Water jcb/envirochem Test Method Results Date Analyzed Color color Grey/Turbid 11/16/2023 Depth to water, ft. Depth to water, Ft 8.9 feet 11/16/2023 Ammonia Nitrogen EPA 360.1. Rev. 2.0, 1993 0.5 mg/L 11 /29/2023 Gallons bailed before sampling Gallons Bailed before sampling 2 (dry) gallons 11/16/2023 Odor Qualitative None 11/16/2023 Total Dissolved Solids (TDS) SM 2540 c-2015 390 mg/L 11 /17/2023 Temperature SM 2550 B-2010 19.4 C 11/16/2023 pH SM4500 H 8.2011 6.0 units 11/16/2023 Total Organic Carbon (TOC) SM 5310 B-2014 31.1 mg/L 11/20/2023 1, 1, 1,2-Tetrachloroethane SM 6200 B-2011 <0.5 pg/L 11/20/2023 1, 1, 1 -Trichloroethane SM 6200 B-2011 <0.5 pg/L 11/20/2023 1,1,2,2-Tetrachloroethane SM 6200 B-2011 <0.5 pg/L 11/20/2023 1,1, 2-Trichloroethane SM 6200 B-2011 <0, 5 pg/L 11/20/2023 1,1-Dichloroetha ne SM 6200 B-2011 <0, 5 pg/L 11/20/2023 1,1-Dichloroethene SM 6200 B-2011 <0.5 pg/L 11/20/2023 1,1-Dichloropropene SM 6200 B-2011 <0.5 pg/L 11/20/2023 1,2,3-Trichlorobenzene SM 6200 B-2011 <0.5 pg/L 11/20/2023 1,2,3-Trichloropropane SM 6200 B-2611 <0.5 pg/L 11/20/2023 1,2,4-Trichlorobenzene SM 8200 B-2011 <0.5 Ng/L 11/20/2023 1,2,4-Trimethylbenzene SM 6200 B-2011 <0.5 pg/L 11/20/2023 1,2-Dibromo-3-Chloropropane SM6200B-2011 <0,5pg/L 11/20/2023 1,2-Dibromoethane SM 6200 B-2011 <0.5 pg/L 11/20/2023 1, 2-Dich lorobenzene SM 6200 B-2011 <0.5 pg/L 11 /20/2023 1,2-Dichloroethane SM 6200 B-2011 <0.5 pg/L 11/20/2023 1,2-Dichloropropane SM 6200 B-2011 <0.5 pg/L 11/20/2023 1,3,5-Trimethylbenzene SM 0200 8-2011 <0.5 Ng/L 11/20/2023 Report # 2023-26955 Page 7 of 30 Environmental Chemists, Inc. 1 6602 Windmill Way, Wilmington, NC 28405 - 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 5� 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS info@environmentalchemisls.com Albemarle Utility Date of Report: Dec 21, 2023 862 Holiday Island Road Customer PO #: Hertford NC 27944 Customer ID: 09110024 Attention: Report #: 2023-26955 Project ID: Monitoring Wells 1,3-Dichlorobenzene sM520oa-2011 <05pg/L 11/20/2023nx 1 1, 3-Dich loropropane SM 8200 B-2011 <0.5 pg/L 11/20/2023 1,4-Dichlorobenzene SM 6200 B-2011 <0.5 pg/L 11/20/2023 2,2-Dichloropropane SM 6200 B-2011 <0.5 pg/L 11/20/2023 2-Chlorotoluene SM 6200 B-2011 <0.5 pg/L 11/20/2023 4-Chlorotoluene SM 6200 B-2011 <0.5 pg/L 11/20/2023 Benzene SM 6200 B-2011 <0.5 pg/L 11/20/2023 Bromobenzene SM 6200 B-2011 <0.5 pg/L 11/20/2023 Bromochloromethane SM 6200 8-2011 <0.5 pg/L 11 /20/2023 Bromodichloromethane SM 6200 8-2011 <0.5 pg/L 11/20/2023 Bromoform SM 6200 B-2011 <0.5 pg/L 11/20/2023 Bromomethane SM 6200 B-2011 <0.5 pg/L 11/20/2023 Carbon tetrachloride SM 6200 B-2011 <0.5 pg/L 11/20/2023 Chlorobenzene SM 6200 B-2011 <0.5 pg/L 11/20/2023 Chloroethane SM 6200 B-2011 <0.5 pg/L 11/20/2023 Chloroform SM 6200 B-2011 <0.5 pg/L 11/20/2023 Chloromethane SM 6200 B-2011 <0.5 pg/L 11/20/2023 cis-1,2-Dichloroethene SM 6200 B-2011 <0.5 pg/L 11/20/2023 cis-1,3-Dlchloropropene SM 6200 B-2011 <0.5 pg/L 11/20/2023 Dibromochlorom ethane SM 6200 B-2011 <0.5 pg/L 11/20/2023 Dibromomethane SM 6200 B-2011 <0.5 pg/L 11/20/2023 Dichlorodifluoromethane SM 6200 B-2011 <0.5 pg/L 11/20/2023 Ethylbenzene SM 6200 B-2011 <0.5 pg/L 11/20/2023 Hexachlorobutadiene SM 6200 B-2011 <0,5 pg/L 11/20/2023 Isopropylbenzene SM 8200 B-2011 <0.5 pg/L 11/20/2023 M+P Xylene SM 6200 B-2011 <1.0 pg/L 11/20/2023 Methylene chloride SM 6200 B-2011 <0.5pg/L 11/20/2023 Naphthalene SM 8200 B-2011 <0.5 pg/L 11 /20/2023 n-Butylbenzene SM 6200 B-2011 <0.5 pg/L 11/20/2023 Report # 2023-26955 Page 8 of 30 Environmental Chemists, Inc. enviroc 6602 Windmill Way, Wilmington, NC 284115 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab.rFax 255-A Wilmington Highway, Jack onvale, NC 28540 . 910.347.5843 Lab'Fax ANALYTICAL & CONSULTING CHEMISTS info'zienvironmentalchemists.com Albemarle Utility Date of Report: Dec 21, 2023 862 Holiday Island Road Customer PO #: Hertford NC 27944 Customer ID: 09110024 Attention: Report #: 2023-26955 Project ID: Monitoring Wells n-Propylbenzene SM 6200 B-2011 <0.5 pg/L 11/20/2023 ortho-Xylene SM 8200 6-2011 <0.5 pg/L 11/20/2023 p-Isopropyltoluene SM 8200 B-2011 <0.5 pg/L 11/20/2023 sec-Butylbenzene SM 8200 B-2011 <0.5 pg/L 11/20/2023 Styrene SM 6200 B-2011 <0.5 Ng/L 11/20/2023 tert-Butylbenzene SM 6200 B-2011 <0, 5 pg/L 11/20/2023 Tetrachloroethene SM 6200 B-2011 <0, 5 pg/L 11/20/2023 Toluene SM 6200 B-2011 <0, 5 pg/L 11/20/2023 Trans-1,2-Dichloroethene SM6200B-2011 <05pg/L 11/20/2023 Trans-1,3-dichloropropene SM6200B-2011 <05pg/L 11/20/2023 Trcchloroethene SM 6200 B-2011 <0.5 pg/L 11/20/2023 Trichlorofluoromethane SM 6200 B-2011 <0.5 pg/L 11/20/2023 Vinyl chloride SM 6"0 B-2011 <0.5 pg/L 11/20/2023 Fecal Coliform SM 9222 D-201 5 MF <1 Colonies/100ml- 11/16/2023 Chloride SM4500 CI E-2011 15 mg/L 11/24/2023 Nitrate Nitrogen (Cale) Nitrite Nitrogen EPA 353 2, Rev. 2.0, 1993 0.22 mg/L 11/16/2023 Nitrate+Nitrite-Nitrogen EPA 3632. Rev 20 1993 0.44 mg/L 11/20/2023 Nitrate Nitrogen Subtraction Method 0.22 mg/L 12/15/2023 Report #t 2023-26955 Page 9 of 30 SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: • • DEPARTMENT OF ENVIRONMENTAL QUALITY - DIV. OF WATER RESOURCES INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: Expiration Date: 05-31-2025 Facility Name: Albemarle Utility Company Non -Discharge W00001817 UIC Permit Name (if different): NPDES Other Facility Address: 862 Holiday Island Rd TYPE OF PERMITTED OPERATION BEING MONITORED ❑■ Lagoon ❑ Remediation: Infiltration Gallery Hertford NC 27944 County Perquimans ❑■ Spray Field ❑ Remediation: Contact Person: Danny Shelton Perry ORC Telephone#: 252-426-1007 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name: South West of Spray Feld No. of wells to be sampled: 10 ❑ Water Source Heat Pump ❑ Other: from Permit SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW - 4 Date sample collected: 11/16/2023 FIELD ANALYSES: WAS Well Depth: 12 ft. Well Diameter: 2 in. pH 00400: 6.1 units Temp. 000lo: 19.3 °C DRY at Depth to Water Level 82546: 9.1 ft. below measuring point Screened Interval: -2 ft. to -12 ft. Spec. Cond. 00094: µMhos time of 3 sampling,check Measuring Point is ft. above land surface Relative M.P. Elevation: ft. Odor 00085: none Volume of water pumped/bailed before sampling: 3 gallons Appearance Tan here:❑ Samples for metals were collected unfiltered: ❑ YES ❑■ NO and field acidified: ❑ YES ❑■ NO LABORATORY INFORMATION Date sample analyzed: 11 /16/2023 Laboratory Name: Environmental Chemists, Inc Certification No. 94 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 0.04 mg/L Pb - Lead 01051 ug/L Coliform: MF Fecal 31616 <1 colonies /100ml- Nitrate (NO3) as N 00620 0.76 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 70300 274 mg/L All - Aluminum 01105 mg/L pH (Lab) 00403 6.1 units Ba - Barium 01007 ug/L TOC 00680 41.4 mg/L Ca - Calcium 00916 mg/L Chloride oo94o 14 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total 01034 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? ❑ Yes (1) ❑ No (0) pecific Conductance 00095 µMhos K - Potassium 00937 mg/L VOC 7873 method # Total Ammonia 00610 <0.2 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen; NH, as N; Ammonia Nitrogen, Total) Mn - Manganese o1o55 ug/L , method # TKN as N 00625 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% Shayne Lamb - Corporate Secretary Permittee (or Authorized Aqent) Name and Title - Please print or type Siqnature of PermiVee (or Authorized Agent) (Date 23 GW-59 Rev.06-07-2018 ANALYTICAL & CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab r 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 ■ 910.347.5843 Lab, Fax info@environmentalchemists.com environmentalchemists.com Albemarle Utility Date of Report: Dec 21, 2023 862 Holiday Island Road Customer PO #: Hertford NC 27944 Customer ID: 09110024 Attention: Report #: 2023-26955 Project ID: Monitoring Wells Lab ID Sample ID: Collect Date/Time Matrix Sampled by 23-65318 Site: MW-4 11/16/2023 11:15 AM Water jcb/envirochem Test Method Results Date Analyzed Color Color Tan 11 /16/2023 Depth to water, ft. Depth to water. Ft 9.1 feet 11/16/2023 Ammonia Nitrogen EPA 3501. Rev. 2 0, 1993 < 0.2 mg/L 11/29/2023 Gallons bailed before sampling Garons Bailed before sampling 3 (dry) gallons 11/16/2023 Odor Qua*datve None 11/16/2023 Total Dissolved Solids (TDS) SM 2540 C-2016 274 mg/L 11/17/2023 Temperature SM 2550 B-2010 19.3 C 11/16/2023 pH SM4500 H 8-2011 6.1 units 11/16/2023 Total Organic Carbon (TOC) SM 5310 B-2014 41.4 mg/L 11/20/2023 1. 1, 1,2-Tetrachloroethane SM 6200 8•2011 <0.5 Wg/L 11/20/2023 1, 1, 1 -Trichloroethane SM 6200 B-2011 <0.5 µg/L 11/20/2023 1,1,2,2-Tetrachloroethane SM6200B-2011 <0.5µg/L 11120/2023 1,1,2-Trichloroethane SM 6200 B-2011 <0.5 µg/L 11120/2023 1, 1 -Dichloroethane SM 6200 B-2011 <0.5 µg/L 11/20/2023 1,1-Dichloroethene SM 6200 8-2011 <0.5 µg/L 11 /20/2023 1,1-Dich loropropene SM 6200 8.2011 <0.5 µg/L 11/20/2023 1,2,3-Trichlorobenzene SM 6200 8.2011 <0.5 µg/L 11/20/2023 1,2,3-Trichloropropane SM 6200 B-2011 <0:5 µg/L 11/20/2023 1,2,4-Trichlorobenzene SM 6200 8-2011 <0 5 µg/L 11/20/2023 1,2,4-Trimethylbenzene SM 6200 B-2011 <0.5 µg/L 11/20/2023 1,2-Dibromo-3-Chloropropane SM62008-2011 <0.5µg/L 11/20/2023 1,2-Dibromoethane SM 6200 B-2011 <0.5 µg/L 11/20/2023 1, 2-Dich lorobenzen a SM 6200 8-2011 <0. 5 pg/L 11 /20/2023 1, 2-Dichloroethane SM 6200 B-2011 <0. 5 µ g/L 11/20/2023 1,2-Dichloropropane SM 6200 8-2011 <0.5 µg/L 11/20/2023 1, 3,5-Trimethyl benzene SM 6200 B-2011 <0.5 µg/L 11/20/2023 Report # 2023-26955 Page 10 of 30 :enviroehem ANALYTICAL & CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 * 910.392.0223 Lab 4 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 252.473.5702 Lab/Fax 255 A Wilmington Highway, Jacksonville, NC 28540 , 910.347.5843 Lab; Fax info@environmentalchemists.com Albemarle Utility Date of Report: Dec 21, 2023 862 Holiday Island Road Customer PO #: Hertford NC 27944 Customer ID: 09110024 Attention: Report #: 2023-26955 Project ID: Monitoring Wells 1, 3-Dichlorobenzene SM 6200 B-2011 <0.5 p g/L 11/20/2023 1, 3-Dich loropropane SM 6200 B-2011 <0.5 pg/L 11/20/2023 1,4-Dichlorobenzene SM 6200 B-2011 <0.5 pg/L 11/20/2023 2,2-Dichloropropane SM 6200 B-2011 <0.5 pg/L 11/20/2023 2-Chlorotoluene SM 6200 B-2011 <0.5 pg/L 11/20/2023 4-Chlorotoluene SM 6200 B-2011 <0.5 pg/L 11/20/2023 Benzene SM 6200 B-2011 <0.5 pg/L 11/20/2023 Bromobenzene SM 6200 B-2011 <0.5 pg/L 11/20/2023 Bromochloromethane SM 6200 B-2011 <0.5 pg/L 11/20/2023 Bromodichloromethane SM 6200 B-2011 <0 5 pg/L 11/20/2023 Bromoform SM 6200 B-2011 <0.5 pg/L 11/20/2023 Bromomethane SM 6200 B-2011 <0.5 pg/L 11/20/2023 Carbon tetrachloride SM 6200 B-2011 <0.5 pg/L 11/20/2023 Chlorobenzene SM 5200 B-2011 <0.5 pg/L 11 /20/2023 Chloroethane SM 5200 B-2011 <0.5 pg/L 11/20/2023 Chloroform SM 6200 B-2011 <0.5 pg/L 11/20/2023 Chloromethane SM 6200 B-2011 <0.5 pg/L 11/20/2023 cis- 1,2-Dichloroethene SM 6200 B-2011 <0.5 pg/L 11/20/2023 cis- 1, 3-Dichloropropene SM 6200 B-2011 <0.5 pg/L 11/20/2023 Dlbromochloromethane SM 6200 B-2011 <0.5 pg/L 11/20/2023 Dibromomethane SM 6200 B-2011 <0.5 pg/L 11/20/2023 Dichlorodifluoromethane SM 6200 B-2011 <0.5 pg/L 11/20/2023 Ethylbenzene SM $200 B-2011 <0.5 pg/L 11/20/2023 Hexachlorobutadiene SM $200 B-2011 <0.5 pg/L 11/20/2023 Isopropyl benzene SM 6200 B-2011 <0.5 pg/L 11/20/2023 M+P Xylene SM 6200 B-2011 <1.0 pg/L 11/20/2023 Methylene chloride SM 8200 B-2011 <0.5 pg/L 11/20/2023 Naphthalene SM 6200 B-2011 <0.5 pg/L 11/20/2023 n-Butylbenzene SM 6200 8-2011 <0.5 pg/L 11/20/2023 Report M 2023.26955 Page 11 c9 30 Environmental Chemists, Inc. envirochem w 6602 Windmill Way, Wilmington, NC 28405 ' 910.392.0223 Lab • 910-392.4424 Fax 710 8owsertown Road, Manteo, NC 27954 * 252.473.5702 Lab/Fax sM 255-A Wilmington Highway, Jacksonville, NC 28540 ' 910.347.5843 Lab /Fax ANALYTICAL & CONSULTING CHEMISTS info;a environmentalchemists.com Albemarle Utility Date of Report: Dec 21, 2023 862 Holiday Island Road Customer PO #: Hertford NC 27944 Customer ID: 09110024 Attention: Report #: 2023.26955 Project ID: Monitoring Wells n-Propylbenzene SM 6200 B-2011 <0.5 pg/L 11/20/2023 µl x5 ortho-Xylene SM 8200 8.2011 <0.5 pg/L 11/20/2023 p-Isopropyltoluene SM 6200 B-2011 <0.5 pg/L 11/20/2023 sec-Butylbenzene SM 8200 B-2011 <0.5 pg/L 11 /20/2023 Styrene SM 6200 B-2011 <0.5 pg/L 11/20/2023 tert-Butylbenzene SM 6200 B-2011 <0.5 pg/L 11/20/2023 Tetrachloroethene SM 6200 B-2011 <0.5 pg/L 11/20/2023 Toluene SM 8200 B-2011 <0.5 N g/L 11/20/2023 Trans-1,2-Dichloroethene SM6200B-2011 <0.5pg/L 11/20/2023 Trans-1,3-dichloropropene SM6200B-2011 <0.5pg/L 11/20/2023 Trichloroethene SM 6200 B-2011 <0.5 pg/L 11/20/2023 Trichlorofluoromethane SM 6200 B-2011 <0.5 pg/L 11/20/2023 Vinyl chloride SM62008.2011 <0.5pg/L 11/20/2023 Fecal Coliform SM 9222 Q-2015 W <1 Colonies/100ml- 11/16/2023 Chloride SM4500 CI E-2011 14 mg/L 11/24/2023 Nitrate Nitrogen (Cale) Nitrite Nitrogen EPA 353 2. Rev 2 0, 1993 0.04 mg/L 11/16/2023 Nitrate+Nitrite-Nitrogen EPA 353.2. Rev 20 1993 0.80mg/L 11/20/2023 Nitrate Nitrogen Subtraction Method 0.76 mg/L 12/15/2023 9 Report 0 . 2023-26955 Page 12 of 30 SUBMIT FORM ON YELLOW PAPER ONLY • DEPARTMENT OF ENVIRONMENTAL QUALITY - DIV. OF WATER RESOURCES GROUNDWATER QUALITY MONITORING: INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM 1 '17 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: Expiration Date: 05-31-2025 Facility Name: Albemarle Utility Company Non -Discharge WQ0001817 UIC NPDES Other Permit Name (if different): Facility Address: 862 Holiday Island Rd TYPE OF PERMITTED OPERATION BEING MONITORED ❑■ Lagoon ❑ Remediation: Infiltration Gallery Hertford NC 27944 County Perquimans ❑■ Spray Field ❑ Remediation: Contact Person: Danny Shelton Perry ORC Telephone#: 252-426-1007 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name: South West of Sprayfield No. of wells to be sampled: 10 ❑ Water Source Heat Pump ❑ Other: from Permit SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW - 5 Date sample collected: 11/16/2023 FIELD ANALYSES: WAS Well Depth: 15 ft. Well Diameter: 2 in. pH 00400: 6.0 units Temp. oo010: 1 8.9 °C DRY at Depth to Water Level 82546: 11.3 ft. below measuring point Screened Interval: 12 ft. to 2 ft. Spec. Cond. 00094: µMhos time ofsampling, Measuring Point is 3 ft. above land surface Relative M.P. Elevation: ft. Odor 00085: None check Volume of water pumped/bailed before sampling: 5.0 gallons Appearance Tan/Clear here:❑ Samples for metals were collected unfiltered: ❑ YES ® NO and field acidified: ❑ YES ❑■ NO LABORATORY INFORMATION Date sample analyzed:11/16/2023 Laboratory Name: Environmental Chemists, Inc Certification No. 94 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 0.03 mg/L Pb - Lead 01051 ug/L Coliform: MF Fecal 31616 <1 colonies /100mL Nitrate (NO3) as N 00620 0.08 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 70300 434 mg/L Al - Aluminum w im mg/L pH (Lab) 00403 6.0 units Ba - Barium 01007 ug/L TOC 00680 3.4 mg/L Ca - Calcium 00916 mg/L Chloride 00940 112 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total 01034 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? ❑ Yes (1) ❑ No (0) pecific Conductance 00095 µMhos K - Potassium 00937 mg/L VOC 7873 method # Total Ammonia 00610 <0•2 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen, NH3as N; Ammonia Nitrogen, Total) Mn - Manganese 01055 ug/L , method # TKN as N 00625 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%. Shayne Lamb - Corporate Secretary Permittee (or Authorized Aqent) Name and Title - Please print or type GW-59 Rev.06-07-2018 r"novirochem 6 ANALYTICAL & CONSULTING CHEMISTS Albemarle Utility 862 Holiday Island Road Hertford NC Attention: Lab 1D Sample ID: 23-65319 Site: MW-5 Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 ` 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax mfotu?rm ironmentalchemists.com Date of Report: Dec 21, 2023 Customer PO #: 27944 Customer ID: 09110024 Report #: 2023-26955 Project ID: Monitoring Wells Collect Date/Time Matrix Sampled by 11/16/2023 11:05 AM Water jcb/envirochem Test Method Results Date Analyzed Color Color Depth to water, ft. Depth to water, Ft. Ammonia Nitrogen EPA 350.1. Rev. 2.0 1993 Gallons bailed before sampling Gallons Balled before sampling Odor Qualitative Total Dissolved Solids (TDS) SM2540C-2015 Temperature SM 2550 B-2010 pH SM 4500 H B-2011 Total Organic Carbon (TOC) SM 5310 B-2014 1. 1, 1,2-Tetrachloroethane SM 6200 B-2011 1, 1, 1 -Trichloroethane SM 6200 B-2011 1,1,2,2-Tetrachloroethane SM6200B-2011 1,1, 2-Trich loroethane SM 6200 B-2011 1,1-Dich loroetha ne SM 6200 8-2011 1,1-Dichloroethene SM 6200 B-2011 1,1-Dichloropropene SM 6200 B-2011 1,2, 3-Trichlorobenzene SM 8200 8-2011 1,2,3-Trichloropropane SM 6200 8-2011 1,2,4-Trichlorobenzene SM 6200 B-2011 1,2,4-Trimethylbenzene SM 6200 8-2011 1,2-Dibromo-3-Chloropropane SM6200B-2011 1,2-Dibromoethane SM 6200 13-2011 1,2-Dichlorobenzene SM 6200 B-2011 1,2-Dich loroethane SM 6200 B-2011 1,2-Dichloropropane SM 6200 B-2011 1,3,5-Trimethylbenzene SM 6200 B-2011 Tan/Clear 11/16/2023 11.3 feet 11/16/2023 < 0.2 mg/L 11/29/2023 5.Ogallons 11/16/2023 None 11/16/2023 434 mg/L 11/17/2023 18.9 C 11/16/2023 6.Ounits 11/16/2023 3.4 mg/L 11/20/2023 <0.5 pg/L 11/20/2023 <0.5 pg/L 11/20/2023 <0.5 pg/L 11/20/2023 <0.5 pg/L 11/20/2023 <0.5 pg/L 11/20/2023 <0.5 pg/L 11/20/2023 <0.5pg/L 11/20/2023 <0.5 pg/L 11/20/2023 <0.5 pg/L 11/20/2023 <0.5 pg/L 11/20/2023 <0.5 pg/L 11/20/2023 <0.5 pg/L 11/20/2023 <0.5 pg/L 11/20/2023 <0.5 pg/L 11/20/2023 <0.5 pg/L 11/20/2023 <0.5 pg/L 11/20/2023 <0.5 pg/L 11/20/2023 Report 0: 2023-26955 Page 13 of 30 F"007 -44"N Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 r 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 * 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 ' 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS info@cnvironmcntalchemists.com environmentalchemists.com Albemarle Utility Date of Report: Dec 21. 2023 862 Holiday Island Road Customer PO M Hertford NC 27944 Customer ID: 09110024 Attention: Report M 2023-26955 Project ID: Monitoring Wells 1,3-Dichlorobenzene sM6200B-2011 <0.5pg/L 11/20/2023 1,3-Dichloropropane SM 6200 B-2011 <0.5 pg/L 11/20/2023 1,4-Dichlorobenzene SM 6200 8-2011 <0.5 pg/L 11/20/2023 2,2-Dichloropropane SM 6200 B-2011 <0.5 pg/L 11/20/2023 2-Chlorotoluene SM6200B-2011 <0 5pg/L 11/2012023 4-Chlorotoluene SM8200 B-2011 <0 5 pg/L 11/20/2023 Benzene SM 0200 B-2011 <0 5 pg/L 11/20/2023 Bromobenzene SM 6200 B-2011 <0 5 pg/L 11/20/2023 Bromochloromethane SM 6200 B-2011 <0.5 pg/L 11/20/2023 Bromod ichloromethane SM 6200 B-2011 <0.5 pg/L 11/20/2023 Bromoform SM 6200 8•2011 <0.5 pg/L 11/20/2023 Bromomethane SM 6200 B-2011 <0.5 pg/L 11/20/2023 Carbon tetrachloride SM 6200 B-2011 <0.5 pg/L 11/2-0/2023 Chlorobenzene SM 0200 B-2011 <0.5 pg/L 11/20/2023 Chloroethane SM 6200 B-2011 <0.5 pg/L 11/20/2023 Chloroform SM 6200 B-2011 <0.5 pg/L 11/20/2023 Chlorometha ne SM 6200 B-2011 <0.5 pg/L 11/20/2023 cis-1,2-Dichloroethene SM 6200 B-2011 <0.5 pg/L 11/20/2023 cis-1,3-Dichloropropene SM 6200 B-2011 <0 5 pg/L 11/20/2023 Dibromochloromethane SM 6200 B-2011 <0.5 pg/L 11/20/2023 Dibromomethane SM 6200 B-2011 <0.5 pg/L 11/20/2023 Dichlorodifluoromethane SM 6200 B-2011 <0.5 pg/L 11/20/2023 Ethylbenzene SM 6200 B-2011 <0.5 pg/L 11/20/2023 Hexachlorobutadiene SM 6200 B-2011 <0.5 pg/L 11/20/2023 Isopropylbenzene SM 6200 B-2011 <0.5 pg/L 11/20/2023 M+P Xylene SM 6200 B-2011 <1.0 pg/L 11/20/2023 Methylene chloride SM6200B-2011 <0.5pg/L 11/20/2023 Naphthalene SM 6200 B-2011 <0.5 pg/L 11/20/2023 n-BUtylbenzene SM 6200 B-2011 <0.5 pg/L 11/20/2023 Report* 2023.26955 Page 14 of 30 F"0P--. -:"qq7 Environmental Chemists, Inc. envirochem 6602 Windmill Way, Wilmington, NC 28405 ' 910-392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 ' 252.473.5702 Lab.'Fax 255-A Wilmington Highway, Jacksonville, NC 28540 ' 910.347.5843 Lab: Fax ANALYTICAL 8 CONSULTING CHEMISTS info@environmentalchemists.com Albemarle Utility Date of Report: Dec 21, 2023 862 Holiday Island Road Customer PO #: Hertford NC 27944 Customer ID: 09110024 Attention: Report #: 2023-26955 Project ID: Monitoring Wells n-Propylbenzene SM 6200 B-2011 <0.5 pg/L 11/20/2023 ortho-Xylene SM 6200 B-2011 <0.5 pg/L 11/20/2023 p-Isopropyltoluene SM 6200 B-2011 <0.5 pg/L 11/20/2023 sec-Butylbenzene SM 8200 B-2011 <0.5 pg/L 11/20/2023 Styrene SM 6200 B-2011 <0.5 NgIL 11/20/2023 tert-Butylbenzene SM 6200 B-2011 <0.5 pg/L 11/20/2023 Tetrachloroethene SM 6200 B-2011 <0.5 NgIL 11/20/2023 Toluene SM 6200 B-2011 <0.5 pg/L 11/20/2023 Trans-1,2-Dichloroethene SM 6200 B-2011 <0.5 pg/L 11/20/2023 Trans-1,3-dichloropropene SM6200B-2011 <0.5pg/L 11/20/2023 Trichloroethene SM 6200 B-2011 <0.5 pg/L 11/20/2023 Trichlorofluoromethane SM 6200 B-2011 <0.5 pg/L 11/20/2023 Vinyl chloride SM 6200 8-2011 <0.5 pg/L 11/20/2023 Fecal Coliform SM9222D-2015MF <1 Colonies/100mi- 11/16/2023 Chloride SM4500 ci E-2011 112 mg/L 11/24/2023 Nitrate Nitrogen (Calc) Nitrite Nitrogen EPA 363.2. Rev 2.0, 1993 0.03 mg/L 11 /16/2023 Nitrate+ N itrite-N itrogen EPA 353.2. Rev 2.0, 1993 0.11 mg/L 11/20/2023 Nitrate Nitrogen Subtraction Method 0.08 mg/L 12/15/2023 9 Report 0, 2023-26955 Page 16 of 30 SUBMIT FORM ON YELLOW PAPER ONLY • • DEPARTMENT OF ENVIRONMENTAL QUALITY - DIV. OF WATER RESOURCES GROUNDWATER QUALITY MONITORING: INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM • • 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: Expiration Date: 05-25-2025 Facility Name: Albemarle Utility Company Non -Discharge WQ0001817 UIC NPDES Other Permit Name (if different): Facility Address: 862 Holiday Island Rd TYPE OF PERMITTED OPERATION BEING MONITORED ❑■ Lagoon ❑ Remediation: Infiltration Gallery Hertford NC 27944 County Perquimans ❑� Spray Field ❑ Remediation: Contact Person: Danny Shelton Perry ORC Telephone#: 252-426-1007 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name: West Of Spray Field No. of wells to be sampled: 10 ❑ Water Source Heat Pump ❑ Other: from Permit SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW - 6 Date sample collected: 11/16/2023 FIELD ANALYSES: WAS Well Depth: 12 ft. Well Diameter: 2 in. pH 00400: 6.2 units Temp. 000lo: 1 8.6 °C DRY at Depth to Water Level 82546: 11.8 ft. below measuring point Screened Interval: -2 ft. to -12 ft. Spec. Cond. 00094: µMhos time ofsampling, Measuring Point is 3 ft. above land surface Relative M.P. Elevation: ft. Odor 00085: none check Volume of water pumped/bailed before Sampling: 5.0 gallons Appearance Tan here: El Samples for metals were collected unfiltered: El NNO and field acidified: ❑YES ❑■ NO LABORATORY INFORMATION Date sample analyzed:11/16/2023 Laboratory Name: Environmental Chemists, Inc Certification No. 94 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 0.17 mg/L Pb - Lead o1o51 ug/L Coliform: MF Fecal 31616 <1 colonies /100mL Nitrate (NO3) as N 00620 <0.02 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 70300 605 mg/L Al - Aluminum 01105 mg/L pH (Lab) 00403 6.2 units Ba - Barium 01007 ug/L TOC 00680 3.8 mg/L Ca - Calcium 00916 mg/L Chloride 00940 154 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total 01034 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? ❑ Yes (1) ❑ No (0) pecific Conductance 00095 µMhos K - Potassium 00937 mg/L VOC 7873 method # Total Ammonia 00610 <0.2 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen; NH, as N; Ammonia Nitrogen, Total) Mn - Manganese 01055 ug/L , method # TKN as N 00625 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% Shayne Lamb - Corporate Secretary Permittee (or Authorized Aqent) Name and Title - Please print or type GW-59 Rev.06-07-2018 [envirochem ANALYTICAL & CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 ` 910.392.0223 Lab E 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 ` 252.473.5702 Lab, Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab., Fax info-P environmentalchemists.com Albemarle Utility Date of Report: Dec 21, 2023 862 Holiday Island Road Customer PO #: Hertford NC 27944 Customer ID: 09110024 Attention: Report #: 2023-26955 Project ID: Monitoring Wells Lab ID Sample ID: Collect Date/Time Matrix Sampled byw- 23-65320 Site: MW-6 11/16/2023 10:55 AM Water jcb/envirochem Test Method Results Date Analyzed Color Color Depth to water, ft. Depth to water. Ft. Ammonia Nitrogen EPA 3501. Rev. 2.0,1993 Gallons bailed before sampling Gallons Baited before se-rpling Odor dual tatrve Total Dissolved Solids (TDS) SM 2540 C-2015 Temperature SM 2550 B-2010 pH SM 4500 H B-2011 Total Organic Carbon (TOC) SM $310 B-2014 1, 1, 1,2-Tetrachloroethane SM 6200 B-2011 1.1,1-Trichloroethane SM 6200 B-2011 1.1,2.2-Tetrachloroethane SM 6200 B-2011 1,1,2-Trichloroethane sM 62oo B-2011 1,1-Dich loroethane SM 6200 B-2011 1,1-Dichloroethene SM 6200 0-2011 1,1-Dichloropropene SM 0200 B-2011 1,2.3-Trichlorobenzene SM 6200 B-2011 1,2.,3-Trichloropropane SM 6200 B-2611 1,2,4-Trichlorobenzene SM 6200 B-2011 1, 2,4-Trimethylbenzene SM 6200 B-2011 1,2-Dibromo-3-Chloropropane SM6200B-2011 1, 2-Dibromoethane SM 6200 B-2011 1,2-Dich lorobenzene SM 6200 B-2011 1,2-Dichloroethane SM 6200 B-2011 1,2-Dichloropropane SM 6200 B-2011 1,3,5-Trimethylbenzene SM 6200 a-2011 Tan 11/16/2023 11.8 feet 11/16/2023 < 0.2 mg/L 11/29/2023 5.Ogallons 11/16/2023 None 11/16/2023 605 mg/L 11 /17/2023 18.6 C 11/16/2023 6.2units 11/16/2023 3.8 mg/L 11/20/2023 <0.5 pg/L 11/20/2023 <0.5 Ng/L 11/20/2023 <0.5 pg/L 11/20/2023 <0.5 pg/L 11/20/2023 <0.5 pg/L 11/20/2023 <0.5 ug/L 11/20/2023 <0.5 pg/L 11/20/2023 <0-5 ug/L 11/20/2023 <0.5 pg/L 11/20/2023 <0.5 pg/L 11/20/2023 <0.5 Ng/L 11/20/2023 <0.5 pg/L 11/20/2023 <0.5lig/L 1112012023 <0.5 pg/L 11/20/2023 <0.5 pg/L 11/20/2023 <0.5 pg/L 11/20/2023 <0.5 pg/L 11/20/2023 Report # 2023-26955 Page 16 of 30 77 Environmental Chemists, Inc. envirochem , 6602 Windmill Way, Wilmington, NC 28405 * 910.392.0223 Lab .. 910.392.4424 Fax 710 $owsertown Road, Manteo, NC 27954 * 252.473,5702 Lab Fax 255-A Wilmington Highway, Jacksonville, NC 28540 - 910.347.5843 Lab: Fax ANALYTICAL 8 CONSULTING CHEMISTS info@environmentalchemists.com Albemarle Utility Date of Report: Dec 21, 2023 862 Holiday Island Road Customer PO #: Hertford NC 27944 Customer ID: 09110024 Attention: Report #: 2023-26955 Project ID: Monitoring Wells 1,3-Dich lorobenzene SM 6200 B-2011 <0.5 pg/L 11/20/2023 1,3-Dichloropropane SM 6200 B-2011 <0.5 pg/L 11/20/2023 1,4-Dichlorobenzene SM 6200 B-2011 <0.5 pg/L 11/20/2023 2,2-Dichloropropane SM 6200 B-2011 <0.5 pg/L 11/20/2023 2-Chlorotoluene SM 5200 B-2011 <0.5 pg/L 11/20/2023 4-Chlorotoluene SM 6200 B-2011 <0.5 pg/L 11/20/2023 Benzene SM 6200 B-2011 <0.5 pg/L 11/20/2023 Bromobenzene SM 6200 B-2011 <0.5 pg/L 11/20/2023 Bromochioromethane SM 6200 8-2011 <0.5 pg/L 11/20/2023 Bromodichloromethane SM 6200 B-2011 <0.5 pg/L 11/20/2023 Brornoform SM $200 B-2011 <0.5 pg/L 11 /20/2023 Bromomethane SM 6200 8.2011 <0.5 pg/L 11/20/2023 Carbon tetrachloride SM 6200 B-2011 <0.5 pg/L 11/20/2023 Chlorobenzene SM 6200 B-2011 <0.5 pg/L 11/20/2023 Chloroethane SM 6200 B 2011 <0.5 pg/L 11/20/2023 Chloroform SM 6200 B 2011 <0.5 pg/L 11 /20/2023 Chloromethane SM 6200 8-2011 <0.5 pg/L 11/20/2023 cis-1, 2-Dichloroethene SM 6200 B-2011 <0.5 pg/L 11/20/2023 cis-1,3-Dich loropropene SM e200 B-2011 <0.5 pg/L 11/20/2023 Dibromochloromethane SM 6200 B-2011 <0.5 pg/L 11 /20/2023 Dibromomethane SM 6200 B-2011 <0.5 pg/L 11/20/2023 Dichlorodifluoromethane SM 6200 B-2011 <0.5 pg/L 11/20/2023 Ethylbenzene SM 6200 B-2011 <0.5 pg/L 11/20/2023 Hexachlorobutadiene SM e200 B-2011 <0.5 pg/L 11/20/2023 Isopropylbenzene SM 6200 B-2011 <0.5 pg1L 11/20/2023 M+P Xylene SM 6200 8.2011 <1.0 pg/L 11/20/2023 Methylene chloride SM 6200 B-2011 <0.5 pg/L 11/20/2023 Naphthalene SM 6200 B-2011 <0.5 pg/L 11 /20/2023 n-Butylbenzene SM 6200 B-2011 <0.5 pg/L 11/20/2023 Report # 2023-26955 Page 17 a130 Environmental Chemists, Inc. ' 1 6602 Windmill Way, Wilmington, NC 28405 910.392.0223 Lab ' 910.392:,4424 Fax M 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab.'Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab Fax ANALYTICAL & CONSULTING CHEMISTS info,a.environmentalchemists.com Albemarle Utility Date of Report: Dec 21, 2023 862 Holiday Island Road Customer PO #: Hertford NC 27944 Customer ID: 09110024 Attention: Report #: 2023-26955 Project ID: Monitoring Wells n-Propylbenzene SM 5200 B-2011 <0.5 Ng/L 11/20/2023 ortho-Xylene SM 6200 B-2011 <0.5 pg/L 11/20/2023 p-Isopropyltoluene SM 6200 B-2011 <0.5 pg/L 11/20/2023 sec-Butylbenzene SM 6200 B-2011 <0.5 pg/L 11/20/2023 Styrene SM 6200 B-2011 <0.5 pg/L 11/20/2023 ter(-Butylbenzene SM 8200 B-2011 <0.5 pg/L 11/20/2023 Tetrachloroethene SM 6200 B-2011 <0.5 pg/L 11/20/2023 Toluene SM 6200 B-2011 <0.5 pg/L 11/20/2023 Trans-1,2-Dichloroethene SM 6200 B-2011 <0.5 pg/L 11/20/2023 Trans-1,3-dichloropropene SM62008.2011 <0.5Ug/L 11/20/2023 Trichloroethene SM 6200 B-2011 <0.5 pg/L 11/20/2023 Trichlorofluoromethane SM 6200 B-2011 <0.5 wg/L 11/20/2023 Vinyl chloride SM 6200 B-2011 <0.5 pg/L 11/20/2023 Fecal Coliform SM 9222 D-2015 MF <1 Colonies/100ml- 11/16/2023 Chloride SM4500 CI E-2011 154 mg/L 11/24/2023 Nitrate Nitrogen (Cale) Nitrite Nitrogen EPA 353.2,Rev 2.0,1993 0.17mg/L 11/16/2023 Nitrate+ N itrite- Nitrogen EPA 363.2. Rev 2.0. 1993 0.04 mg/L 11/20/2023 Nitrate Nitrogen Subtraction Method <0.02 mg/L 12/15/2023 9 Report* 2023-26955 Page 18 of 30 SUBMIT FORM ON YELLOW PAPER ONLY DEPARTMENT OF ENVIRONMENTAL QUALITY - DIV. OF WATER RESOURCES GROUNDWATER QUALITY MONITORING: All, INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM • • 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: Expiration Date: 05-31-2025 Facility Name: Albemarle Utility Company Non -Discharge WQ0001817 UIC NPDES Other Permit Name (if different): Facility Address: 862 Holiday Island Rd TYPE OF PERMITTED OPERATION BEING MONITORED ❑■ Lagoon ❑ Remediation: Infiltration Gallery Hertford NC 27944 County Perquimans ❑■ Spray Field ❑ Remediation: Contact Person: Danny Shelton Perry ORC Telephone#: 252-426-1007 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name: West of Baffle lagoon No. of wells to be sampled: 10 ❑ Water Source Heat Pump ❑ Other: from Permit SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW - 7 Date sample collected: 11/16/2023 FIELD ANALYSES: WAS Well Depth: 16.9 ft. Well Diameter: 2 in. pH 00400: 5.7 units Temp. 000lo: 1 8.5 °C DRY at Depth to Water Level 825a6: 6.0 ft. below measuring point Screened Interval: 11.9 ft. p g p to 16.9 ft. Spec. Cond. 000sa: µ Mhos time of sampling, Measuring Point is 2•5 ft. above land surface Relative M.P. Elevation: ft. Odor 000m: none check Volume of water pumped/bailed before sampling: 5.0 gallons Appearance Red/Tan here: El Samples for metals were collected unfiltered: ❑ YES K NO and field acidified: ❑ YES ❑■ NO LABORATORY INFORMATION Date sample analyzed:11/16/2023 Laboratory Name: Environmental Chemists, Inc Certification No. 94 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 < 0.02 mg/L Pb - Lead 01051 ug/L Coliform: MF Fecal 31616 <1 colonies /100mL Nitrate (NO3) as N 00620 <0.02 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 70300 268 mg/L Al - Aluminum 01105 mg/L pH (Lab) 00403 5.7 units Ba - Barium 01007 ug/L TOC 00680 21.7 mg/L Ca - Calcium 00916 mg/L Chloride 00940 40 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total 01034 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? ❑ Yes (1) ❑ No (0) pecific Conductance 00095 µMhos K - Potassium 00937 mg/L VOC 7873 method # Total Ammonia 00610 <0.2 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen, NH3as N; Ammonia Nitrogen, Total) Mn - Manganese 01055 ug/L , method # TKN as N 00625 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% Lamb - Corporate Secretary 12�2�123 Permittee (or Authorized Aqent) Name and Title - Please print or type GW-59 Rev.06-07-2018 envirochem ANALYTICAL & CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 " 910.392.0223 Lab " 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 * 252.473.5702 Lab:' Fax 255-A Wilmington Highway, Jacksonville, NC 28540 " 910.347.5843 Lab:! Fax info:,,:environ mentalchemists.com Albemarle Utility Date of Report: Dec 21, 2023 862 Holiday Island Road Customer PO #: Hertford NC 27944 Customer ID: 09110024 Attention: Report #: 2023-26955 Project ID: Monitoring Wells Lab ID Sample ID: Collect Date/Time Matrix Sampled by 23-65321 Site: MW-7 11/16/2023 10:45 AM Water jcb/envirochem Test Method Color Cdor Depth to water, ft. Depth to Water Ft. Ammonia Nitrogen EPA 3501 Rev.2.0.1953 Gallons bailed before sampling Gallons Ba'ed before sampling Odor Qua ltative Total Dissolved Solids (TDS) SM 2540 C•2015 Temperature SM 2550 8.2010 pH SM 4500 H B-2011 Total Organic Carbon (TOC) SM 6310 B-2014 1. 1. 1, 2-Tetrachloroethane SM 6200 B-2011 1,1.1-Trichloroethane SM 6200 B-2011 1,1,2,2-Tetrachloroethane SM 6200 B-2011 1,1, 2-Trichloroethane SM 6200 8-2011 1,1-Dichloroethane SM 6200 8-2011 1,1-Dichloroethene SM 6200 B-2011 1,1-Dichloropropene SM 6200 B-2011 1,2, 3-Trichlorobenzene SM 6200 B-2011 1,2.3-Trichloropropane SM 6200 B-2011 1,2,4-Trichlorobenzene SM 6200 B-2011 1,2,4-Trimethylbenzene SM 6200 B-2011 1,2-Dibromo-3-Chloropropane SM0200B-2011 1,2-Dibromoethane SM 6200 B-2011 1,2-Dichlorobenzene SM 6200 B-2011 1,2-Dichloroethane SM 6200 B-2011 1,2-Dichloropropane SM 6200 B-2011 1,3,5-Trimethylbenzene sM6200 B-2011 Results Date Analyzed Red/Tan 11/16/2023 6.0 feet 11 /16/2023 < 0.2 mg/L 11/29/2023 S.Ogallons 11/16/2023 None 11 /16/2023 268mg/L 11/17/2023 18.5 C 11/16/2023 5.7 units 11/16/2023 12.7 mg/L 11/27/2023 <0.5 pg/L 11120/2023 <0.5 pg/L 11/20/2023 <0.5 pg/L 11/20/2023 <0.5 pg/L 11/20/2023 <0.5 pg/L 11/20/2023 <0.5 pg/L 11/20/2023 <0.5 pg/L 11/20/2023 <0.5 pg/L 11/20/2023 <0.5 pg/L 11/20/2023 <0.5 pg/L 11/20/2023 <0.5 pg/L 11/20/2023 <0.5 pg/L 11/20/2023 <0.5 pg/L 11/20/2023 <0.5 pg/L 11/20/2023 <0.5 pg/L 11/20/2023 <0.5 pg/L 11 /20/2023 <0.5 pg/L 11/20/2023 Report $ . 2023-26955 Page 19 of 30 Environmental Chemists, Inc. 1 6602 Windmill Way, Wilmington, NC 28405 . 910.392.0223 Lab f 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax '" 255 A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 LabiFax ANALYTICAL & CONSULTING CHEMISTS info;aenvironmentalchemists.com Albemarle Utility Date of Report: Dec 21, 2023 862 Holiday Island Road Customer PO #: Hertford NC 27944 Customer ID: 09110024 Attention Report #: 2023-26955 Project ID: Monitoring Wells 1,3-Dichlorobenzene SM 6200 8-2011 <0.5 pg/L 11/20/2023 .M 1,3-Dichloropropane SM 6200 B-2011 <0.5 pg/L 11/20/2023 1,4-Dichlorobenzene SM 8200 B-2011 <0.5 pg/L 11/20/2023 2,2-Dichloropropane SM e200 B-2011 <0.5 pg/L 11/20/2023 2-Chlorotoluene SM 6200 B-2011 <0.5 pg/L 11/20/2023 4-Chlorotoluene SM 6200 B-2011 <0.5 pg/L 11/20/2023 Benzene SM 6200 B-2011 <0.5 pg/L 11/20/2023 Bromobenzene SM 6200 B-2011 <0.5 pg/L 11/20/2023 Bromochloromethane SM 6200 B-2011 <0.5 pg/L 11/20/2023 Bromod ichloro methane SM 6200 8-2011 <0.5 pg/L 11/20/2023 Bromoform SM 6200 B-2011 <0.5 pg/L 11 /20/2023 Bromomethane SM 6200 B-2011 <0.5 pg/L 11/20/2023 Carbon tetrachloride SM 0200 B-2011 <0.5 pg/L 11/20/2023 Chlorobenzene SM 6200 B-2011 <0.5 pg/L 11/20/2023 Chloroethane SM 6200 B-2011 <0.5 pg/L 11/20/2023 Chloroform SM 6200 B-2011 <0.5 pg/L 11/20/2023 Chloromethane SM 6200 B-2011 <0.5 pg/L 11/20/2023 cis-1,2-Dichloroethene SM 6200 B-2011 <0.5 pg/L 11/20/2023 cis-1, 3-Dichloropropene SM 6200 B-2011 <0.5 pg/L 11/20/2023 Dibromochloromethane SM 6200 B-2011 <0.5 pg/L 11/20/2023 Dibromomethane SM 6200 B-2011 <0.5 pg/L 11/20/2023 Dichlorodifluoromethane SM 6200 B-2011 <0.5 pg/L 11/20/2023 Ethylbenzene SM 8200 B-2011 <0.5 pg/L 11/20/2023 Hexachlorobutadiene SM 6200 B-2011 <0.5 pg/L 11/20/2023 Isopropylbenzene SM 6200 B-2011 <0.5 pg/L 11/20/2023 M+P Xylene SM 6200 B-2011 <1.0 pg/L 11/20/2023 Methylene chloride SM 6200 B-2011 <0.5 pg/L 11/20/2023 Naphthalene SM 6200 B-2011 <0.5 pg/L 11 /2012023 n-Butylbenzene SM 6200 B-2011 <0.5 pg/L 11/20/2023 Report #: 2023-26955 Page 20 of 30 Environmental Chemists, Inc. envirochemw 6602 Windmill Way, Wilmington, NC 28405 ' 910.392.0223 Lab " 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax M 255-A Wilmington Highway, Jacksonville, NC 28540 ' 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS info- a environmentalchemists.com Albemarle Utility Date of Report: Dec 21, 2023 862 Holiday Island Road Customer PO #: Hertford NC 27944 Customer ID: 09110024 Attention: Report #: 2023-26955 Project ID: Monitoring Wells n-Propylbenzene SM 6200 B-2011 <0.5 pg/L 11/20/2023 ortho-Xylene SM 6200 a-2011 <0.5 pg/L 11/20/2023 p-Isopropyltoluens SM 6200 B-2011 <0.5 pg/L 11/20/2023 sec-Butylbenzene SM 6200 B-2011 <0.5 pg/L 11/20/2023 Styrene SM 6200 B-2011 <0.5 pg/L 11/20/2023 tert-Butyl benzene SM 6200 B-2011 <0.5 pg/L 11/20/2023 Tetrachloroethene SM 6200 B-2011 <0.5 pg/L 11/20/2023 Toluene SM 6200 B-2011 <0.5 pg/L 11/20/2023 Trans-1,2-Dichloroethene SM 6200 B-2011 <0.5 pg/L 11/20/2023 Trans-1,3-dichloropropene SM 6200 B-2011 <0.5 pg/L 11/20/2023 Trichloroethene SM 6200 B-2011 <0.5 pg/L 11/20/2023 Trichlorofluoromethane SM 6200 B-2011 <0.5 pg/L 11/20/2023 Vinyl chloride SM 6200 B-2011 <0.5 pg/L 11/20/2023 Fecal Coliform SM 9222 D-2015 MF <1 Colonies/100ml- 11/16/2023 Chloride SM4600 CI E-2011 40 mg/L 11/24/2023 Nitrate Nitrogen (Calc) Nitrite Nitrogen EPA 353.2. Rev 2.0, 1993 < 0.02 mg/L 11/16/2023 Nitrate+Nitrite-Nitrogen EPA 353 2, Rev 2.0,1993 < 0.02 mg/L 11/20/2023 Nitrate Nitrogen Subtraction Method <0.02 mg/L 12/15/2023 6 Report * 2023-26955 Page 21 of 30 SUBMIT FORM ON YELLOW PAPER ONLY • • DEPARTMENT OF ENVIRONMENTAL QUALITY - DIV. OF WATER RESOURCES GROUNDWATER QUALITY MONITORING: INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM • • • • 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: Expiration Date: 05-31-2025 Facility Name: Albemarle Utility Company Non -Discharge WQ0001817 UIC Permit Name (if different): NPDES Other Facility Address: 862 Holiday Island Rd TYPE OF PERMITTED OPERATION BEING MONITORED ❑■ Lagoon ❑ Remediation: Infiltration Gallery Hertford NC 27944 County Perquimans ❑■ Spray Field ❑ Remediation: Contact Person: Danny Shelton Perry ORC Telephone#: 252-426-1007 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name: East of Spray Field No. of wells to be sampled: 10 ❑ Water Source Heat Pump ❑ Other: from Permit SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW - 8 Date sample collected: 11/16/2023 FIELD ANALYSES: WAS Well Depth: 15 ft. Well Diameter: 2 in. pH 00400: 5.4 units Temp. 000lo: 19.3 °C DRY at Depth to Water Level 82546: 9.0 ft. below measuring point Screened Interval: 5 ft. to 15 ft. Spec. Cond. o0094: µMhos time of sampling,check Measuring Point is 3 ft. above land surface Relative M.P. Elevation: ft. Odor 00085: Sulfur Volume of water pumped/bailed before sampling: 5.0 gallons Appearance Tan here: El Samples for metals were collected unfiltered: ❑ YES ❑■ NO and field acidified: ❑ YES ❑■ NO LABORATORY INFORMATION Date sample analyzed:11/16/2023 Laboratory Name: Environmental Chemists, Inc Certification No. 94 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 0.06 mg/L Pb - Lead o1o51 ug/L Coliform: MF Fecal 31616 <1 colonies /100mL Nitrate (NO3) as N 00620 < 0.02 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 70300 490 mg/L Al - Aluminum 01105 mg/L pH (Lab) 00403 5.4 units Ba - Barium 01007 ug/L TOC 00680 1.4 mg/L Ca - Calcium 00916 mg/L Chloride 00940 200 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total olo34 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? ❑ Yes (1) ❑ No (0) pecific Conductance 00095 µMhos K - Potassium 00937 mg/L VOC 7873 method # Total Ammonia 00610 < 0.2 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen; NH3as N; Ammonia Nitrogen, Total) Mn - Manganese o1055 ug/L , method # TKN as N 00625 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only • I certify that. to the best of my knowledge and belief, the information submitted in this report is true, acct DWR-certified laboratory. I am aware that there are significant penalties for submitting false information Corporate Permittee (or Authorized Aqent) Name and Title - Please print or type GW-59 Rev.06-07-2018 mg/L Effluent Total VOCs: Signature of mg/L VOC Removal% 12 2t� 23 (Date) lrw-- ---"N k ANALYTICAL & CONSULTING CHEMISTS Albemarle Utility 862 Holiday Island Road Hertford NC Attention: Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 4 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax i nfo; a.envi ronmentalchemists.com Date of Report: Dec 21, 2023 Customer PO M 27944 Customer ID: 09110024 Report M 2023-26955 Project ID: Monitoring Wells Lab ID� Sample ID: Collect Date/Time Matrix Sampled by n..mm,... . 23-65322 Site: MW-8 11/16/2023 10:00 AM Water jcb/envirochem Test Method Results Date Analyzed Color Color Tan 11/16/2023 Depth to water, ft. Depth to Water. Ft 9.0 feet 11/16/2023 Ammonia Nitrogen EPA 350 1 Rev 2 0. 1993 < 0.2 mg/L 11/29t2023 Gallons bailed before sampling Gallons Bailed before sampling 5.0 gallons 11/16/2023 Odor Qual tat ve Sulfur 11/16/2023 Total Dissolved Solids (TDS) SM 2540 C-2015 490 mg/L 11/17/2023 Temperature SM 2550 B-2010 19.3 C 11/16/2023 pH SM 4500 H B-2011 5.4 units 11/16/2023 Total Organic Carbon (TOC) SM 5310 B-2014 1.4 mg/L 11/20/2023 1. 1, 1,2-Tetrachloroethane SM 6200 B-2011 <0.5 pg/L 11/20/2023 1, 1. 1 -Trichloroethane SM 6200 8.2011 <0.5 pg/L 11/20/2023 1,1,2,2-Tetrachloroethane SM6200B-2011 <0.5pg/L 11/20/2023 1,1, 2-Trichloroethane SM 6200 B-2011 <0.5 pg/L 11 /20/2023 1,1-Dichloroethane SM 6200 B-2011 <0.5 pg/L 11/20/2023 1,1-Dichloroethene SM 6200 B-2011 <0.5 pg/L 11/20/2023 1,1-Dichloropropene SM 6200 B-2011 <0.5 pg/L 11/20/2023 1,2,3-Trichlorobenzene SM 0200 B-2011 <0.5 Ng/L 11/20/2023 1,2,3-Trichloropropane SM 6200 B-2011 <0.5 pg/L 11/20/2023 1,2,4-Tdchlorobenzene SM 8200 8-2011 <0.5 pg/L 11/20/2023 1,2,4-Trimethylbenzene SM 8200 B-2011 <0.5 pg/L 11/20/2023 1,2-Dibromo-3-Chloropropane SM 6200 B-2011 <0.5 pg/L 11/20/2023 1,2-Dibromoethane SM 6200 B-2011 <0.5 pg/L 11/20/2023 1,2-Dichlorobenzene SM 6200 B-2011 <0.5 pg/L 11/20/2023 1,2-Dichloroethane SM 6200 8-2011 <0.5 pg/L 11 /2012023 1,2-Dichloropropane SM 6200 B-2011 <0.5 pg/L 11/20/2023 1, 3,5-Trimethylbenzene SM 6200 B-2011 <0.5 Ng/L 11/20/2023 Report N: 2023-26955 Page 22 of 30 rEnvip-- --7 ronmental Chemists, Inc. nvirochem6602 Windmill Way, Wilmmgton, NC 28405 1 910.392.0223 Lab 1 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 � 252.473.5702 Lab Fax 255 A Wilmington Highway, Jacksonville, NC 28540 ' 910.347.5843 Lab Fax ANALYTICAL 8, CONSULTING CHEMISTS mfo�a environmentalchemists.com Albemarle Utility 862 Holiday Island Road Hertford NC Attention- 27944 Date of Report: Dec 21, 2023 Customer PO #: Customer ID: 09110024 Report #: 2023-26955 Project ID: Monitoring Wells 1,3-Dichlorobenzene SM 6200 B-2011 <0.5 pg/L 11/20/2023 1.3-Dichloropropane SM 6200 B-2011 <0.5 pg/L 11/20/2023 1.4-Dichlorobenzene SM 6200 B-2011 <0 5 pg/L 11/20/2023 2,2-Dichloropropane SM6200B-2011 <05pg/L 11/20/2023 2-Chlorotoluene SM 6200 B-2011 <0 5 pg/L 11/20/2023 4-Chlorotoluene SM 6200 B-2011 <0 5 pg/L 11/20/2023 Benzene SM 6200 B-2011 <0 5 pg/L 11/20/2023 Bromobenzene SM 6200 8-2011 <0.5 pg/L 11/20/2023 Bromochloromethane SM 6200 B-2011 <0.5 pg/L 11/20/2023 Bromodichloromethane SM 6200 B-2011 <0.5 pg/L 11/20/2023 Bromoform SM 6200 B-2011 <0.5 pg/L 11/20/2023 Bromomethane SM 6200 8-2011 <0.5 pg/L 11/20/2023 Carbon tetrachloride SM6200 B-2011 <0.5 pg/L 11/20/2023 Chlorobenzene SM 6200 B-2011 <0.5 pg/L 11/20/2023 Chloroethane SM 6200 B-2011 <0.5 pg/L 11/20/2023 Chloroform SM 6200 B-2011 <0.5 pg/L 11/20/2023 Chloromethane SM 6200 B-2011 <0.5 pg/L 11/20/2023 cis- 1.2-Dichloroethene SM 6200 B-2011 <0.5 pg/L 11/20/2023 cis- 1.3-Dichloropropene SM 6200 B-2011 <0.5 pg/L 11/20/2023 Dibromochloromethane SM 6200 B-2011 <0.5 pg/L 11/20/2023 Dlbromomethane SM 6200 B-2011 <0.5 pg/L 11/20/2023 Dlchlorodifluoromethane SM 6200 B-2011 <0.5 pg/L 11/20/2023 Ethylbenzene SM 6200 B-2011 <0.5 pg/L 11/20/2023 Hexachlorobutadiene SM 6200 B-2011 <0.5 pg/L 11/20/2023 Isopropylbenzene SM 6200 B-2011 <0.5 pg/L 11/20/2023 M+P Xylene SM 6200 6-2011 <1.0 pg/L 11/20/2023 Methylene chloride SM 6200 B-2011 <0.5 pg/L 11/20/2023 Naphthalene SM 6200 B-2011 <0.5 pg/L 11/20/2023 n-Butylbenzene SM 6200 B-2011 <0.5 pg/L 11/20/2023 repo+^ it: 2023-26955 Page 23 o130 Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab ' 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 ' 252.473.5702 Lab/Fax SM 255-A Wilmington Highway, Jacksonville, NC 28540 ' 910.347.5843 Lab 'Fax ANALYTICAL $ CONSULTING CHEMISTS info,,( environmentalchemists.com Albemarle Utility Date of Report: Dec 21, 2023 862 Holiday Island Road Customer PO #: Hertford NC 27944 Customer ID: 09110024 Attention: Report #: 2023-26955 Project ID: Monitoring Wells n-Propylbenzene SM 6200 B-2011 <0.5 Ng/L 11/20/2023 ortho-Xylene SM6200 8-2011 <0.5 pg/L 11/20/2023 p-Isopropyltoluene SM 6200 B-2011 <0.5 Ng/L 11/20/2023 sec-Butylbenzene SM 6200 B-2011 <0.5 pg/L 11/20/2023 Styrene SM 6200 B-2011 <0 5 pg/L 11/20/2023 tert-Butylbenzene SM e200 B-2011 <0.5 pg/L 11/20/2023 Tetrachloroethene SM 6200 B-2011 <0.5 pg/L 11/20/2023 Toluene SM 6200 B-2011 <0.5 pg/L 11/20/2023 Trans-1,2-Dichloroethene SM 6200 B-2011 <0.5 pg/L 11/20/2023 Trans-1,3-dichloropropene SM62008-2011 <0.5pg/L 11/20/2023 Trichloroethene SM 6200 B-2011 <0.5 pg/L 11/20/2023 Trichlorofluoromethane SM $200 8-2011 <0.5 pg/L 11/20/2023 Vinyl chloride SM 8200 B-2011 <0.5 pg/L 11/20/2023 Fecal Coliform SM 9222 0-2015 MF <1 Colonies/100ml- 11 /16/2023 Chloride SM4500 c1 E-2011 200 mg/L 11/24/2023 Nitrate Nitrogen (Cale) Nitrite Nitrogen EPA 353 2, Rev 2 0, 1993 0.06 mg/L 11/16/2023 Nitrate+Nitrite-Nitrogen EPA 353 2, Rev 2 0, 1993 0.05 mg/L 11/20/2023 Nitrate Nitrogen Subtraction Method <0.02 mg/L 12115/2023 Report # 2023.26966 Page 24 of 30 SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: • • DEPARTMENT OF ENVIRONMENTAL QUALITY - DIV. OF WATER RESOURCES INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM • • • • 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: Expiration Date: 05-31-2025 Facility Name: Albemarle Utility Company Non -Discharge WQ0001817 UIC Permit Name (if different): NPDES Other Facility Address: 862 Holiday Island Rd TYPE OF PERMITTED OPERATION BEING MONITORED Hertford NC 27944 County Perquimans ❑■ Lagoon ❑ Remediation: Infiltration Gallery ❑■ Spray Field ❑ Remediation: Contact Person: Danny Shelton Perry ORC Telephone#: 252-426-1007 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name: West of Spray Field No. of wells to be sampled: 10 ❑ Water Source Heat Pump ❑ Other: from Permit SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW - 9 Date sample collected: 11/16/2023 FIELD ANALYSES: WAS Well Depth: 15 ft. Well Diameter: 2 in. pH 00400: 5.2 units Temp. 000lo: 18.8 °C DRY at Depth to Water Level 82546: 12.1 ft. below measuring point Screened Interval: 4 ft. to 14 ft. Spec. Cond. 000sa: µ of timeMhos sampling, Measuring Point is 3 ft. above land surface Relative M.P. Elevation: ft. Odor 00085: Sulfur check Volume of water pumped/bailed before sampling: 5.0 gallons Appearance Tan/Clear here: El Samples for metals were collected unfiltered: ❑ YES ❑■ NO and field acidified: ❑ YES ❑■ NO LABORATORY INFORMATION Date sample analyzed: 11 /16/2023 Laboratory Name: Environmental Chemists, Inc Certification No. 94 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 0.03 mg/L Pb - Lead 01051 ug/L Coliform: MF Fecal 31616 2 colonies /100mL Nitrate (NO3) as N 00620 0.12 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 70300 74.0 mg/L Al - Aluminum 01105 mg/L pH (Lab) 00403 5.2 units Ba - Barium 01007 ug/L TOC 00680 1.0 mg/L Ca - Calcium 00916 mg/L Chloride 00940 5 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total olo34 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? ❑ Yes (1) ❑ No (0) pecific Conductance 00095 µMhos K - Potassium 00937 mg/L VOC 7873 method # Total Ammonia 00610 <0.2 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen, NH3as N; Ammonia Nitrogen, Total) Mn - Manganese 01055 ug/L , method # TKN as N 00625 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% Shayne Lamb - Corporate Secretary Permittee (or Authorized Aqent) Name and Title - Please print or type GW-59 Rev.06-07-2018 :envirochem ANALYTICAL & CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 * 910,392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 * 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax info@environmentalchemists.com Albemarle Utility Date of Report: Dec 21, 2023 862 Holiday Island Road Customer PO #: Hertford NC 27944 Customer ID: 09110024 Attention: Report #: 2023-26955 Project ID: Monitoring Wells Lab ID Sample ID: Collect Datef!'ime Matrix Sampled by,_.2W ...,. 23-65323 Site: MW-9 11/16/2023 10:30 AM Water jcb/envirochem Test Method Results Date Analyzed Color caor Tan/Clear 11/16/2023 Depth to water, f , Depth to Water, Ft 12.1 feet 11/16/2023 Ammonia Nitrogen EPA 350.1, Rev 2.0, 1993 < 0.2 mg/L 11/29/2023 Gallons bailed before sampling Gallons Bailed before samp ng 5.0 gallons 11/16/2023 Odor Qualitative Sulfur 11/16/2023 Total Dissolved Solids (TDS) SM 2540 c-2015 74.0 mg/L 11/17/2023 Temperature SM 2550 B-2010 18.8 C 11/16/2023 pH SM 4500 H B-2011 5.2 units 11/16/2023 Total Organic Carbon (TOC) SM 5310 8-2014 1.0 mg/L 11/20/2023 1. 1, 1,2-Tetrachloroethane SM 6200 8-2011 <0.5 µg/L 11/20/2023 1, 1, 1 -Trichloroethane SM 8200 B-2011 <0.5 µg/L 11/20/2023 1,1,2,2-Tetrachloroethane SM 6200 B-2011 <0.5 µg/L 11/20/2023 1, 1, 2-Trichloroethane SM 6200 B-2011 <0.5 µg/L 11/20/2023 1,1-Dichloroethane SM 6200 B-2011 <0.5 µg/L 11/20/2023 1,1-Dichloroethene SM 6200 B-2011 <0.5 µg/L 11/20/2023 1,1-Dichloropropene SM 6200 B-2011 <0.5 µg/L 11/20/2023 1,2, 3-Trichlorobenzene SM 6200 B-2011 <0.5 µg/L 11 /20/2023 1,2,3-Trichloropropane SM 6200 B-2011 <0.5 µg/L 11/20/2023 1,2,4-Trichlorobenzene SM 6200 B-2011 <0.5 µg/L 11/20/2023 1,2,4-Trimethylbenzene SM 6200 B-2011 <0.5 µg/L 11/20/2023 1,2-Dibromo-3-Chloropropane SM 6200 B-2011 <0.5 µg/L 11/20/2023 1,2-Dibromoethane SM 8200 B-2011 <0.5 µg/L 11/20/2023 1,2-Dichlorobenzene SM 6200 8-2011 <0.5 µg/L 11/20/2023 1,2-Dichloroethane SM 6200 B-2011 <0.5 µg/L 11/20/2023 1,2-Dichloropropane SM 6200 a-2011 <0.5 µg/L 11/20/2023 1, 3, 5-Trimethylbenzene SM 5200 B-2011 <0.5 µg/L 11/20/2023 Report p 2023.26955 Page 25 of 30 Environmental Chemists, Inc. 1 6ti02 Windmill Way, Wilmington, NC 28405 910.392.0223 Lab 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab ' Fax _M 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS infou environmentalchemists.com Albemarle Utility 862 Holiday Island Road Hertford NC Attention: 27944 Date of Report: Dec 21, 2023 Customer PO #: Customer ID: 09110024 Report #: 2023-26955 Project ID: Monitoring Wells 1,3-Dichlorobenzene SM6200B-2011 <0.5pg/L 11/20/2023x 1,3-Dichloropropane SM 6200 B-2011 <0.5 pg/L 11/20/2023 1,4-Dichlorobenzene SM 6200 B-2011 <0.5 pg/L 11/20/2023 2,2-Dichloropropane SM 6200 B-2011 <0.5 pg/L 11/20/2023 2-Chlorotoluene SM 8200 9-2011 <0.5 pg/L 11/20/2023 4-Chlorotoluene SM 5200 &2011 <0.5 pg/L 11/20/2023 Benzene SM 6200 &2011 <0.5 pg/L 11/20/2023 Bromobenzene SM 6200 &2011 <0,5 pg/L 11/20/2023 Bromochloromethane SM 6200 B-2011 <0.5 pg/L 11/20/2023 Bromodichloromethane SM 6200 B-2011 <0.5 pg/L 11/20/2023 Bromoform SM 6200 B-2011 <0.5 pg/L 11/20/2023 Bromomethane SM 6200 B-2011 <0.5 pg/L 11/20/2023 Carbon tetrachloride SM 6200 8-2011 <0.5 pg/L 11/20/2023 Chlorobenzene SM 6200 B-2011 <0.5 pg/L 11/20/2023 Chloroethane SM 6200 B-2011 <0.5 pg/L 11/20/2023 Chloroform SM 8200 B-2011 <0.5 pg/L 11/20/2023 Chloromethane SM 6200 B-2011 <0.5 pg/L 11/20/2023 cis- 1,2-Dich loroethene SM 6200 B-2011 <0.5 pg/L 11/20/2023 cis-1,3-Dichloropropene SM 6200 B-2011 <0.5 pg/L 11/20/2023 Dibromochloromethane SM 6200 B-2011 <0.5 pg/L 11/20/2023 Dibromomethane SM 6200 B-2011 <0.5 pg/L 11/20/2023 Dichlorodifluoromethane SM 5200 B-2011 <0.5 pg/L 11/20/2023 Ethylbenzene SM6200 B-2011 <0.5 pg/L 11/20/2023 Hexachlorobutadiene SM 6200 B-2011 <0.5 pg/L 11/20/2023 Isopropylbenzene SM 82M B-2011 <0.5 pg/L 11/20/2023 M+P Xylene SM 6200 B-2011 <1.0 pg/L 11/20/2023 Methylene chloride SM 6200 B-2011 <0.5 pg/L 11/20/2023 Naphthalene SM 8200 B-2011 <0.5 pg/L 11/20/2023 n-Butylbenzene SM 6200 B-2011 <0.5 pg/L 11/20/2023 Report # 2023-26955 Page 26 of 30 [envirochem ANALYTICAL & CONSULTING CHEMISTS Albemarle Utility 862 Holiday Island Road Hertford NC Attention: Environmental Chemists, Inc. 6602 Windmi:l Way, Wilmington, NC 28405 - 910.392.0223 Lab - 910,392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab,, Fax 255-A Wilmington Highway, Jacksonville, NC 28540 - 910.347.5843 Lab/Fax info@cnvironmentalchemists.com Date of Report: Dec 21, 2023 Customer PO #: 27944 Customer 10: 09110024 Report #: 2023-26955 Project ID: Monitoring Wells n-Propylbenzene SM 0200 B-2011 ortho-Xylene SM 6200 8-2011 p-Isopropyltoluene SM 6200 B-2011 sec-Butylbenzene SM 6200 B-2011 Styrene SM620D B-2011 tert-Butyl benzene SM 6200 B-2011 Tetrachloroethene SM 6200 B-2011 Toluene SM 6200 8-2011 Trans-1,2-Dichloroethene SM 6200 B-2011 Trans-1,3-dichloropropene SM6200B-2011 Trichloroethene SM 0200 0-2011 Trichlorofluoromethane SM 6200 B-2011 Vinyl chloride SM 6200 B-2011 Fecal Coliform SM 9222 D-2015 MF Chloride SM4500 CI E-2011 Nitrate Nitrogen (Calc) <0.5 pg/L 11/20/2023 <0.5 pg/L 11/20/2023 <0.5 pg/L 11/20/2023 <0.5 pg/L 11/20/2023 <0.5 pg/L 11 /20/2023 <0.5 pg/L 11/20/2023 <0.5 pg/L 11/20/2023 <0.5 pg/L 11/20/2023 <0.5 pg/L 11 /20/2023 <0.5 pg/L 11/20/2023 <0.5 pg/L 11/20/2023 <0.5 pg/L 11/20/2023 <0.5 pg/L 11/20/2023 2 Colonies/100mL 11/16/2023 5 mg/L 11 /24/2023 Nitrite Nitrogen EPA 353.2, Rev 2 0.1993 0.03 mg/L 11 /16/2023 Nitrate+Nitrite-Nitrogen EPA 3632 Rev 20 1993 0.15 mg/L 11/20/2023 Nitrate Nitrogen Subtraction Method 0.12 mg/L 12/15/2023 Report * 2023.26955 Page 27 of 30 SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: • • DEPARTMENT OF ENVIRONMENTAL QUALITY - DIV. OF WATER RESOURCES INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: Expiration Date: 05-31-2025 Facility Name: Albemarle Utility Company Non -Discharge WQ0001817 UIC Permit Name (if different): NPDES Other Facility Address: 862 Holiday Island Rd TYPE OF PERMITTED OPERATION BEING MONITORED ❑■ Lagoon ❑ Remediation: Infiltration Gallery Hertford N.C. 27944 County Perquimans ❑■ Spray Field ❑ Remediation: Contact Person: Danny Shelton Perry ORC Telephone#: 252426-1007 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name: South of Spray Field No. of wells to be sampled: 10 ❑ Water Source Heat Pump ❑ Other: from Permit SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW-10 Date sample collected: 11/16/2023 FIELD ANALYSES: WAS Well Depth: 15 ft. Well Diameter: 2 in. pH o0400: 5.9 units Temp. 000lo: 19.6 °C DRY at Depth to Water Level 82546: 12.8 ft. below measuring point Screened Interval: 5 ft. to 14 ft. Spec. Cond. 00094: µMhos time of sampling, Measuring Point is 3 ft. above land surface Relative M.P. Elevation: ft. Odor 00085: None check Volume of water pumped/bailed before sampling: 5.0 gallons Appearance Tan/Clear here:❑ Samples for metals were collected unfiltered: ❑ YES ❑■ NO and field acidified: ❑ YES ❑■ NO LABORATORY INFORMATION Date sample analyzed:11/16/2023 Laboratory Name: Environmental Chemists„ Inc Certification No. 94 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 <0.02 mg/L Pb - Lead 01051 ug/L Coliform: MF Fecal 31616 <1 colonies /100mL Nitrate (NO3) as N 00620 0.99 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 70300 417 mg/L All - Aluminum of lo5 mg/L pH (Lab) 00403 5.9 units Ba - Barium 01007 ug/L TOC 00680 1.6 mg/L Ca - Calcium 00916 mg/L Chloride 00940 185 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total oio34 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? ❑ Yes (1) ❑ No (0) pecific Conductance 00095 µMhos K - Potassium 00937 mg/L VOC 7873 method # Total Ammonia 00610 <0.2 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen: NH3as N. Ammonia Nitrogen, Total) Mn - Manganese 01055 ug/L , method # TKN as N 00625 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% Shayne Lamb Corporate Secretary Permittee (or Authorized Aqent) Name and Title - Please print or type GW-59 Rev.06-07-2018 Environmental Chemists, Inc. envirochem 6602 Windmill Way, Wilmington, NC 28405 . 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab :'Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab 'Fax ANALYTICAL & CONSULTING CHEMISTS mfotu°environmentalchemists.com Albemarle Utility Date of Report: Dec 21, 2023 862 Holiday Island Road Customer PO M Hertford NC 27944 Customer ID: 09110024 Attention. Report M 2023-26955 Project ID: Monitoring Wells Lab ID Sample ID: Collect Date/Time Matrix Sampled b 23-65324 Site: MW-10 11/16/2023 10:15 AM Water jcb/envirochem Test _ Method Results Date Analyzed Color Color Tan/Clear 11/16/2023 Depth to water, ft. Depth to water, Ft. 12.8 feet 11/16/2023 Ammonia Nitrogen EPA 350 1, Rev 2,0, 1993 < 0.2 mg/L 11/29/2023 Gallons bailed before sampling Gallons Bailed before sampmg 5.Ogallons 11/16/2023 Odor Qualitative None 11/16/2023 Total Dissolved Solids (TDS) SM2540 C-2015 417 mg/L 11/17/2023 Temperature SM 2550 B-2010 19.6 C 11/16/2023 pH SM4500 H B-2011 5.9 units 11/16/2023 Total Organic Carbon (TOC) SM 5310 B-2014 1.6 mg/L 11/20/2023 1.1,1,2-Tetrachloroethane sM6200B-2011 <0.5pg/L 11/20/2023 1.1, 1 -Trichloroethane SM 6200 B-2011 <0 5 }1g/L 11/20/2023 1,1,2:2-Tetrachloroethane SM6200B-2011 <0.5pg/L 11/20/2023 1,1, 2-Trichloroethane SM 8200 B-2011 <0.5 pg/L 11/20/2023 1,1-Dich loroethane SM 8200 B-2011 <0. 5 pg/L 11/20/2023 1,1-Dichloroethene SM 6200 B-2011 <0.5 pg/L 11/20/2023 1,1-Dich loropropene SM 6200 B-2011 <0.5 }ag/L 11/20/2023 1,2,3-Trichlorobenzene SM 6200 B-2011 <0.5 pg/L 11/20/2023 1,2,3-Trichloropropane SM 6200 B-2011 <0.5 pg/L 11/20/2023 1,2,4-Trichlorobenzene SM 6200 B-2011 <0 5 pg/L 11/20/2023 1,2,4-Trimethylbenzene SM6200B-2011 <0 5pg/L 11/20/2023 1,2-Dibromo-3-Chloropropane SM6200B-2011 <0.5pg/L 11/20/2023 1,2-Dibromoethane SM 6200 8-2011 <0.5 pg/L 11/20/2023 1,2-Dichlorobenzene SM 6200 B-2011 <0.5 pg/L 11/20/2023 1,2-Dich loroethane SM 6200 B-2011 <0.5 pg/L 11/20/2023 1,2-Dichloropropane SM 8200 B-2011 <0.5 pg/L 11/20/2023 1, 3, 5-Trimethyl benzene SM 6200 B-2011 <0.5 pg/L 11/20/2023 Report0:: 2023.26955 Page 28 of 30 :envirochem ANALYTICAL 8 CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab ` 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab, Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax info; a:environmentalchemists.com Albemarle Utility Date of Report: Dec 21, 2023 862 Holiday Island Road Customer PO #: Hertford NC 27944 Customer ID: 09110024 Attentions Report #: 2023-26955 Project ID: Monitoring Wells 1, 3-Dichlorobenzene SM 6200 B-2011 <0.5 pg/L 11/20/2023 1,3-Dichloropropane SM 6200 B-2011 <0.5 pg/L 11/20/2023 1,4-Dichlorobenzene SM 6200 B-2011 <0.5 pg/L 11/20/2023 2,2-Dichloropropane SM 6200 8-2011 <0.5 pg/L 11/20/2023 2-Chlorotoluene SM e200 B-2011 <0.5 pg/L 11/20/2023 4-Chlorotoluene SM 6200 B-2011 <0.5 pg/L 11/20/2023 Benzene SM 6200 B-2011 <0.5 pg/L 11/20/2023 Bromobenzene SM6200 B-2011 <0.5 pg/L 11/20/2023 Bromoch lorom ethane SM 6200 B-2011 <0.5 pg/L 11/20/2023 Bromodichloromethane SM 6200 B-2011 <0.5 pg/L 11/20/2023 Bromoform SM 6200 B-2011 <0.5 pg/L 11/20/2023 Bromomethane SM 6200 B-2011 <0.5pg/L 11/20/2023 Carbon tetrachloride SM 8200 B-2011 <0.5 pg/L 11/20/2023 Chlorobenzene SM 6200 B-2011 <0.5 pg/L 11/20/2023 Chloroethane SM 6200 B-2011 <0.5 pg/L 11/20/2023 Chloroform SM 6200 8-2011 <0.5 pg/L 11/20/2023 Chioromethane SM 6200 B-2011 <0.5 pg/L 11/20/2023 cis-1,2-Dichloroethene SM 6200 B-2011 <0.5 pg/L 11/20/2023 cis- 1, 3-Dichloropropene SM620OB-2011 <0.5pg/L 11/20/2023 Dibromochloromethane SM 6200 B-2011 <0.5 pg/L 11/20/2023 Dibromomethane SM 6200 B-2011 <0.5 pg/L 11/20/2023 Dichlorodifluoromethane SM 6200 B-2011 <0.5 pg/L 11/20/2023 Ethylbenzene SM 6200 8-2011 <0.5 pg/L 11/20/2023 Hexachlorobutadiene SM 6200 B-2011 <0.5 pg/L 11/20/2023 Isopropylbenzene SM 6200 B-2011 <0.5 pg/L 11/20/2023 M+P Xylene SM 8200 8-2011 <1.0 NgIL 11/20/2023 Methylene chloride SM 6200 8-2011 <0.5 pg/L 11/20/2023 Naphthalene SM 6200 B-2011 <0.5 pg/L 11/20/2023 n-Butylbenzene SM 6200 B-2011 <0.5 pg/L 11/20/2023 Report # . 2023.26955 Page 29 of 30 Environmental Chemists, Inc. envirochem 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Labi. Fax '" 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab, Fax ANALYTICAL & CONSULTING CHEMISTS infoiaenvironmentalchemists.com Albemarle Utility 862 Holiday Island Road Hertford NC Attention: 27944 Date of Report: Dec 21, 2023 Customer PO #: Customer ID: 09110024 Report #: 2023-26955 Project ID: Monitoring Wells n-Propylbenzene SM6200B-2011 <0.5pg/L 11/20/2023 ortho-Xylene SM 820o B-2011 <0.5 pg/L 11/20/2023 p-Isopropyltoluene SM 6200 8-2011 <0.5 pg/L 11/20/2023 sec-Butylbenzene SM 6200 B-2011 <0.5 pg/L 11/20/2023 Styrene SM 6200 B-2011 <0.5 pg/L 11/20/2023 tert-Butylbenzene SM 6200 B-2011 <0.5 pg/L 11/20/2023 Tetrachloroethene SM 6200 B-2011 <0.5 pg/L 11/20/2023 Toluene SM 8200 8-2011 <0,5 pg/L 11/20/2023 Trans-1,2-Dichloroethene SM 6200 B-2011 <0.5 pg/L 11/20/2023 Trans-1,3-dichloropropene SM6200B-2011 <0.5pg/L 11/20/2023 Trichloroethene SM 6200 B-2011 <0.5 pg/L 11/20/2023 Trichlorofluoromethane SM 6200 B-2011 <0.5 pg/L 11/20/2023 Vinyl chloride SM 6200 B-2011 <0.5 pg/L 11 /20/2023 Fecal Coliform SM9222 D-2016MF <1 Colonies/100ml- 11/16/2023 Chloride SM4500 a E-2011 185 mg/L 11/24/2023 Nitrate Nitrogen (Calc) Nitrite Nitrogen EPA 353.2, Rev. 2.0, 1993 < 0.02 mg/L 11 /16/2023 Nitrate+Nitrite-Nitrogen EPA 363.2, Rev 2.0,1993 0.99 mg/L 11120/2023 Nitrate Nitrogen Subtraction Method 0.99mg/L 12/15/2023 Comment: Reviewed by: Report 0: 2023.26956 Page 30 of 30 GW-59A COMPLIANCE REPORT FORM Permit # 6117 (Submit one each monitoring period with GW-59 forms.) I Enter date monitoring results were due. CII13 Will this monitoring report (GW-59 and GW-59A) YES NO be submitted after the established due date? 2 Was any required information missing on the GW-59 report forms? YE NO IF the answer to question 1 or 2 is "YES", list in the space provided below the well identification number(s) and explain the problems encountered in obtaining the required information. 3 Are any of the monitor wells in need of repair or maintenance (damaged casing, unlocked or missing cap, missing YES O identification plate, area overgrown, etc.)? ff the answer is "Yes", contact the Regional Office. for guidance. 4 Are any monitored constituents equal to or above the established standards? YES NO If the answer to question 4 is "NO", skip to section 8. If the answer to question 4 is "YES" list the affected wells individually with constituent(s) and concentration(s) exceeding standards in the space provided below: II 5 For the constituents identified in question 4 above, have standards been exceeded previously for the YES NO same constituent(s) in the same well(s) in the last two years? If the answer to question 5 is "NO", skip to section 8. If the answer to question 5 is "YES", list in the space provided below, each well with constituent(s) exceeding standards, concentration(s) reported, and sample collection date for each/occurrence (for the last two years). Are the monitoring wells listed in section 5 located at or beyond the review boundary? YES NO If the answer is "YES", a groundwater quality problem maybe occurring. CONTACT THE REGIONAL OFFICE IMMEDIATELY FOR GUIDANCE. If the answer is "NO", monitoring wells maybe improperly located, contact the Regional Office. 7 Is the permittee implementing previously approved actions required by the Division involving this YES N groundwater quality problem? If the answer to question 7 is "YES", describe those actions in the space provided below. If the answer to question 7 is "NO", contact the Regional Office within 90 days: an evaluation may be required to determine the impact the waste disposal system is having at the review and compliance boundaries surrounding this facility. Failure to do so may subject the permittee to a Notice of Violation, fines, and/or penalties. 8 The person completing this portion (GW-59A) of the monitoring report should sign below and submit this form with GW-59 forms for required wells to the address provided at the top of the current GW-59 form. I hereby acknowledge that the above information was evaluated and the information submitted in this report (Compliance Report GW-59A is true and complete to the best of my knowledge. 12 2� 23 Signature of PcWittee (or Authorized Agent) Dat GW-59A 12/8/2003 Z' o 'o p� et mw 3 7 7/5— AA 6 O's - 3� _3 y d) r��ti ins M I0RO Ly 5' r N �A •q � J 7-t-71S