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HomeMy WebLinkAboutWQ0005555_Monitoring - 11-2023_20231227Monitoring Report Submittal Permit Number#* Name of Facility:* Month: * November Report Information wg0005555 Weyerhaeuser Company Type * NDMR, NDAR-1, NDAR-2, NDMLR G W-59 Confirmation Email Address: * Name of Submitter: * Signature: Date of submittal: Initial Review Year:* 2023 Upload Document* 11 2023 NDAR & NDMR.pdf 5.95MB PDF Only Nov GW-59 report.pdf 13.99MB PDF Only Please upload one PDF containing all applicable monitoring reports (i.e., NDMR, NDAR-1, NDAR-2, NDMLR, GW-59). dennis.atkinson@weyerhaeuser.com Dennis R Atkinson �'.rLQ�:rOAa' 12/27/2023 This will be filled in automatically Reviewer: Wanda.Gerald Is the project number correct?* wg0005555 Is the monitoring report accepted?* Yes No Regional Office* Winston-Salem Reviewer: _anonymous Review Date: 1/11/2024 FORM: NDMR 05-16 NON -DISCHARGE MONITORING REPORT (NDMR) Page _1_of_3_ Permit No.: W00005555 Facility Name: Weyerhaeuser - Elkin OSB Mill WWTF County: Surry Month: November Year: 2023 PPI: 001 Flow Measuring Point: Influent Ertlurnt No flow generate t Parameter Monitoring Point: r' Influent ;rii,ent Groundwater Lowering Surface water Parameter Code 11. 50050 00310 00916 00680 00940 01034 31616 71880 00927 71900 00610 00625 00620 00600 00340 00400 > f6 m E U �0 0 o o ° O E E E R c2 L' Uo U u_ � ' O OnQ E c ~- Z c ~ zO O Uco _o 24-hr hrs GPD mg/L mg/L mg/L mg/L mg/L #/100 mL mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L su 1 08:00 8 0 2 08.00 8 0 3 08.00 6 0 4 0 5 0 6 0&00 8 0 809 7 0 8 0 9 0800 8 0 101 08:00 6 0 11 0 12 0 13 0 7 79 14 0 15 0 161 0 17 0 18 0 19 0 20 10 7 61 21 0 221 0 23 0 24 0 25 0 26 0 27 08.00 8 0 7 75 281 0800 8 13,632 29 08,00 6 0 30 0800 8 0 296 30.1 716 183 0,0359 33 <0 5 25.1 <0.00200 1.06 60.5 <10.0 67 1 3280 9.1 31 08:00 1 6 Average: 454 296.00 30.10 716.00 183.00 0.04 33.00 000 25.10 0.00 106 60,50 0.00 67 10 3,280.00 Daily Maximum: 13,632 296.00 30.10 716.00 183.00 0,04 33.00 0.50 25.10 0,00 1.06 60.50 10.00 67 10 3,280.00 9.10 Daily Minimum: 0 296.00 30.10 716.00 183.00 0.04 33.00 0.50 25.10 0-00 106 60.50 10.00 67 10 3,280.00 761 Sampling Type: Recorder Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Monthly Limit: Daily Limit: 28,800 Sample Frequency: Continuous 3 X Year 3 X Year 3 X Year 3 X Year 3 X Year 3 X Year 3 X Year 3 X Year 3 X Year 3 X Year 3 X Year 3 X Year 3 X Year I 3 X Year Per Lvent FORM NDMR 05-16 NON -DISCHARGE MONITORING REPORT (NDMR) Page 2_ of3_ Permit No.: WQ0005555 Facility Name: Weyerhaeuser - Elkin OSB Mill WWTF County: Surry Month: November Year: 2023 PPI: 001 Flow Measuring Point: l Influent = Dtiuent No flow generatni Parameter Monitoring Point: I Intlurnt Pffluent ❑ Groundwater Lowering ❑ Surface water Parameter Code -► 34694 00665 WQ09C 00931 00929 70300 00530 ❑@ Q E a> E E! n O C C ( o a 0 :CE° Ca 0 0 =O ' Q C: _ O_ Y Q E 7 )0 U O N O N O nU) v v m0 C •6 C O U)o Cn cn 24-hr hrs mg/L mg/L mg/L Ratio mg/L mg/L mg/L 1 08:00 8 2 08:00 8 3 0800 6 4 5 6 08:00 8 7 8 9 1 08:00 8 10 08:00 6 11 12 13 14 15 16 17 18 19 20 21 — 22 23 24 25 26 27 08:00 8 28 08:00 8 29 08:00 6 301 08:00 8 <0.005 3.54 24.9 1.3 1260 5460 1 110 311 08:00 6 Average: #DIV/0! 3.54 24.90 1.30 1,260.00 5,460.00 110.00 Daily Maximum: 0.00 3.54 24.90 1.30 1.260.00 5,460.00 110.00 Daily Minimum: 0.00 3.54 24.90 1.30 1,260.00 5,460.00 110.00 Sampling Type: Grab I Grab Calculated Calculated Grab Grab Grab Monthly Limit: Daily Limit: Sample Frequency: 3 X Year 3 X Year 3 X Year 3 X Year 3 X Year 3 X Year 3 X Year FORM: NDMR 05-16 NON -DISCHARGE MONITORING REPORT (NDMR) Page _3_of_3_ Sampling Person(s) Certified Laboratories Name: David Morris Name: WayPoint Anaylical - Cert. No. 402 Name: Brody Edwards Name: PACE - Cert No. 40 & 633 Does all monitoring data and sampling frequencies meet the requirements in Attachment A of your permit? O Compliant ❑ Non -Compliant If the facility is non -compliant, please explain in the space below the reason(s) the facility was not in compliance. Provide in your explanation the date(s) of the non-compliance and describe the corrective action(s) taken. Attach additional sheets if necessary. Operator in Responsible Charge (ORC) Certification Permittee Certification ORC: Dennis R. Atkinson Permittee: Weyerhaeuser Co. Certification No.: 15574 Signing official: Steve Kobelak Grade: SI Phone Number: 336-526-6437 Signing Official's Title: Mill Manger Has the ORC changed since the previous NDMR? ❑ yes E No Phone Number: 336-5 -6456 Permit Expiration: 8/31/2025 /oL/ � d2 ��. • 2-� Z 3 Signature Date Signature Date By this signature, I certify that this report is accurrate and complete to the best of my knowledge. I certify, under penally of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that all qualified personnel properly gathered and evaluated the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations. Mail Original and Two Copies to: Division of Water Resources Information Processing Unit 1617 Mail Service Center Raleigh, North Carolina 27699-1617 WayPAoint NALYTICAL 12/19/2023 Weyerhaeuser Corporation Dennis Atkinson 524 Pride Way Elkin, NC, 28621 Ref: Analytical Testing Lab Report Number: 23-334-0020 Client Project Description: Wastewater EFF Dear Dennis Atkinson: 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www.waypointanalytical.com Waypoint Analytical, LLC (Charlotte) received sample(s) on 11/30/2023 for the analyses presented in the following report. The above referenced project has been analyzed per your instructions. The analyses were performed in accordance with the applicable analytical method. The analytical data has been validated using standard quality control measures performed as required by the analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all parameters were performed in accordance with guidelines established by the USEPA (including 40 CFR 136 Method Update Rule May 2021) unless otherwise indicated. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time. Refer to sample analysis time for confirmation of holding time compliance. The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as - received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information. Sincerely, Terri W Cole Laboratory Project Manager Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis. Page 1 of 15 Waypoint. ANALYTICAL 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www.waypointanalytical.com Certification Summary Laboratory ID: WP CNC: Waypoint Analytical Carolina, Inc. (C), Charlotte, NC State Program Lab ID Expiration Date North Carolina State Program 37735 07/31/2024 North Carolina State Program 402 12/31/2023 South Carolina State Program 99012 07/31/2024 South Carolina State Program 99012 12/31/2023 Laboratory ID: WP MTN: Waypoint Analytical, LLC., Memphis, TN State Program Lab ID Expiration Date Alabama State Program 40750 02/29/2024 Arkansas State Program 88-0650 02/07/2024 California State Program 2904 06/30/2024 Florida State Program - NELAP E871157 06/30/2024 Georgia State Program C044 11/14/2025 Georgia State Program 04015 06/30/2024 Illinois State Program - NELAP 200078 10/31/2024 Kentucky State Program 80215 06/30/2024 Kentucky State Program KY90047 12/31/2023 Louisiana State Program - NELAP LA037 12/31/2023 Louisiana State Program - NELAP 04015 06/30/2024 Mississippi State Program MS 11/14/2025 North Carolina State Program 47701 07/31/2024 North Carolina State Program 415 12/31/2023 Pennsylvania State Program - NELAP 68-03195 05/31/2024 South Carolina State Program 84002 06/30/2024 Tennessee State Program 02027 11/14/2025 Texas State Program - NELAP T104704180 09/30/2024 Virginia State Program 00106 06/30/2024 Virginia State Program - NELAP 460181 09/14/2024 Page 1 of 1 00016/23-334-0020 Page 2 of 15 Waypoint.(2) ANALYTICAL Report Number: 23-334-0020 Client Project Description: Wastewater EFF 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www.waypointanalytical.com Sample Summary Table Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID 90539 EFF Aqueous 11/30/2023 11:00 11/30/2023 13:55 90539 EFF Aqueous 11/30/2023 11:00 11/30/2023 13:55 4500NH3D-2011 WP MTN 90539 EFF Aqueous 11/30/2023 11:00 11/30/2023 13:55 5310C-2011 WP MTN 90539 EFF Aqueous 11/30/2023 11:00 11/30/2023 13:55 8315A WP MTN 90539 EFF Aqueous 11/30/2023 11:00 11/30/2023 13:55 4500NORGD-2011 WP MTN 90540 Field Aqueous 11/30/2023 11/30/2023 13:55 WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN Page 3 of 15 WayPAoint NALYTICAL Client: Weyerhaeuser Corporation Project: Wastewater EFF Lab Report Number: 23-334-0020 Date: 12/15/2023 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www.waypointanalytical.com CASE NARRATIVE Total Metals Method EPA-200.7 Sample 90539 (EFF) Analyte: Sodium QC Batch No: V40962N40805 Matrix spike/matrix spike duplicate recoveries are outside of control limits. Acceptable LCS recovery indicates the system was in control, but the reported result could be affected by matrix interference. Mercury Method 245.1 (Prep) Sample 90539 (EFF) QC Batch No: V40972N40972 The sample was diluted due to the nature of the sample matrix. Reporting limits have been adjusted accordingly. Anions by Ion Chromatography Method 300.0 Sample 90484 Analyte: Chloride QC Batch No: V40883N40882 Matrix spike/matrix spike duplicate recoveries are outside of control limits. Acceptable LCS recovery indicates the system was in control, but the reported result could be affected by matrix interference. Sample 90484 Analyte: Nitrate-N QC Batch No: V40883N40882 The MS/MSD recoveries are outside QC limits due to the level of analyte present in the parent sample relative to the spike level. RPD is based on the MS/MSD results and should be evaluated as laboratory duplicates. 625.1 - Base/Neutrals and Acids by GC/MS Method 625.1 Sample 90539 (EFF) QC Batch No: V40789N40760 Surrogate(s) were flagged for recoveries in the associated project sample. During the extraction step, the extraction technician noted that a significant emulsion formed. Batch QC samples (Method Blank and Laboratory Control Samples) all showed surrogate recoveries within QC limits, indicating that the biased recoveries were due to the sample matrix. Fecal Coliform MPN Method 9221E-2011 QC Batch No: V40774 Duplicate result: <2.0 MPN / 100ml Volatile Organic Compounds - GC/MS Method 8260D Sample 90539 (EFF) QC Batch No: V41023N41022 The sample was diluted due to the nature of the sample matrix. Reporting limits have been adjusted accordingly. Sample was a very dark brown hue. Lower dilution not possible. Analyte: Ethanol QC Batch No: V41023/V41022 Page 4 of 15 0 Waypoint. ANALYTICAL 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www.waypointanalytical.com Relative Percent Difference (RPD) for the duplicate analysis was outside of the allowable QC limits. Analyte: tert-Amyl alcohol QC Batch No: V41023IV41022 Relative Percent Difference (RPD) for the duplicate analysis was outside of the allowable QC limits. Page 5 of 15 Waypointo ANALYTICAL 00052 Weyerhaeuser Corporation Project Dennis Atkinson 524 Pride Way Information Elkin , NC 28621 Report Number : 23-334-0020 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www.waypointanalytical.com Wastewater EFF REPORT OPANAL YSIS Report Date : 12/19/2023 Received : 11/30/2023 Lab No : 90539 Sample ID : EFF Matrix: Aqueous Sampled: 11/30/2023 11:00 Test Results Units MDL MQL DF Date / Time By Analytical Analyzed Method Fecal Coliform MPN/g 33.0 MPN/100ml- 2.0 1 11/30/23 14:32 JMD 9221E-2011 Sodium Absorption Ratio 1.30 Ratio 0.100 1 12/05/23 18:07 CALCULATION Plant Available Nitrogen 24.9 mg/L 0.100 1 11/30/23 17:55 CALCULATION Ammonia Nitrogen 1.06 mg/L 0.040 0.100 1 12/08/23 16:01 DJJC 4500NH3D-2011 Biochemical Oxygen Demand (5-day) 296 mg/L 2.0 1 11/30/23 13:09 SLO 5210E-2015 Chloride 183 mg/L 50.0 50 11/30/23 17:55 NDL 300.0 COD (Chemical Oxygen Demand) 3280 mg/L 90 1 12/04/23 13:46 SLO 5220D-2011 Nitrate (NO3-N) <10.0 mg/L 10.0 50 11/30/23 17:55 NDL 300.0 Nitrite (NO2-N) 6.58 mg/L 5.00 50 11/30/23 17:55 NDL 300.0 Nitrate+ Nitrite- N 6.58 mg/L 5.00 50 11/30/23 17:55 300.0 Total Dissolved Solids 5460 mg/L 50 1 12/06/23 13:30 RLW 2540C-2015 Total Suspended Solids 110 mg/L 26.5 1 12/04/23 09:20 JMD 2540D-2015 Total Kjeldahl Nitrogen 60.5 mg/L 17.1 25.0 1 12/14/23 12:53 ANH 4500NORGD-2011 Total Nitrogen 67.1 mg/L 25.0 1 11/30/23 17:55 CALCULATION Phosphorus 3.54 mg/L 0.100 1 12/12/23 14:40 JKC EPA-200.7 TOC 716 mg/L 100 100 12/10/23 14:25 ASH 531OC-2011 Calcium 30.1 mg/L 0.400 1 12/06/2314:17 JKC EPA-200.7 Chromium 0.0359 mg/L 0.0060 1 12/06/2314:17 JKC EPA-200.7 Magnesium 25.1 mg/L 0.200 1 12105/2318:07 JKC EPA-200.7 Mercury (Total) <0.00200 mg/L 0.00200 1 12/07/23 16:44 JKC 245.1 Sodium 1260 mg/L 16.0 20 12/06/2314:03 JKC EPA-200.7 Qualifiers/ Outside QC Limit DF Dilution Factor Definitions J Estimated value MQL Method Quantitation Limit Page 6 of 15 0 Waypoint. 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 ANALYTICAL www.waypointanalytical.com 00052 Weyerhaeuser Corporation Project Wastewater EFF Dennis Atkinson Report Date : 12/19/2023 524 Pride Way Information : Received : 11/30/2023 Elkin , NC 28621 Report Number : 23-334-0020 REPORT OPANALYSIS Lab No : 90539 Matrix: Aqueous Sample ID: EFF Sampled: 11/30/2023 11:00 Analytical Method: 625.1 Prep Batch(es): V40760 12/01/23 10:04 Prep Method: 625.1 (Prep) Test Results Units MDL MQL DF Date / Time By Analytical Analyzed Batch Phenol <0.005 mg/L 0.005 1 12/01/2314:53 AMP V40789 Surrogate: Phenol-d5 3.98 * Limits: 10-63% 1 12/01/23 14:53 AMP 625.1 Surrogate: 2-Fluorophenol 4.90 * Limits: 22-84% 1 12/01/2314:53 AMP V40789 Surrogate: 2,4,6-Tribromophenol 4.74 * Limits: 31-144% 1 12/01/2314:53 AMP V40789 Analytical Method: 8260D Prep Batch(es): V41497 12/07/23 09:00 Prep Method: 5030E Test Results Units MDL MOL DF Date / Time By Analytical Analyzed Batch Acetone 120 Ng/L 18.0 50.0 10 12/07/23 20:20 MSA V41498 Acrolein <20.0 Vg/L 20.0 50.0 10 12/07/23 20:20 MSA V41498 Acrylonitrile <2.30 Ng/L 2.30 50.0 10 12/07/23 20:20 MSA V41498 Benzene <1.80 Ng/L 1.80 5.00 10 12/07/23 20:20 MSA V41498 Bromobenzene <2.10 ug/L 2.10 5.00 10 12/07/23 20:20 MSA V41498 Bromochloromethane <4.20 Ng/L 4.20 10.0 10 12/07/23 20:20 MSA V41498 Bromodichloromethane <1.60 Ng/L 1.60 5.00 10 12/07/23 20:20 MSA V41498 Bromoform <15.0 Ng/L 15.0 50.0 10 12/07/23 20:20 MSA V41498 Bromomethane <2.80 ug/L 2.80 10.0 10 12/07/23 20:20 MSA V41498 n-Butylbenzene <1.85 Ng/L 1.85 10.0 10 12/07/23 20:20 MSA V41498 sec -Butyl benzene <2.00 Ng/L 2.00 5.00 10 12/07/23 20:20 MSA V41498 tert-Butyl benzene <9.20 Ng/L 9.20 20.0 10 12/07/23 20:20 MSA V41498 Carbon Disulfide <1.50 Ng/L 1.50 50.0 10 12/07/23 20:20 MSA V41498 Carbon Tetrachloride <1.80 Ng/L 1.80 5.00 10 12/07/23 20:20 MSA V41498 Qualifiers/ * Outside QC Limit DF Dilution Factor Definitions I Estimated value MQL Method Quantitation Limit Page 7 of 15 Waypointo ANALYTICAL 00052 Weyerhaeuser Corporation Project Dennis Atkinson 524 Pride Way Information Elkin , NC 28621 Report Number : 23-334-0020 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www.waypointanalytical.com Wastewater EFF REPORT OF ANAL YSiS Report Date : 12/19/2023 Received : 11/30/2023 Lab No : 90539 Sample ID : EFF Matrix: Aqueous Sampled: 11/30/2023 11:00 Analytical Method: 8260D Prep Batch(es): V41497 12/07/23 09:00 Prep Method: 5030E Test Results Units MDL MQL DF Date / Time By Analytical Analyzed Batch Chlorobenzene <1.90 N9/L 1.90 5.00 10 12/07/23 20:20 MSA V41498 Chlorodibromomethane <1.90 U9/L 1.90 5.00 10 12/07/23 20:20 MSA V41498 Chloroethane <4.30 u9/L 4.30 10.0 10 12/07/23 20:20 MSA V41498 Chloroform <2.20 N9/L 2.20 5.00 10 12/07/23 20:20 MSA V41498 Chloromethane <2.20 u9/L 2.20 5.00 10 12/07/23 20:20 MSA V41498 2-Chlorotoluene <2.00 u9/L 2.00 5.00 10 12/07/23 20:20 MSA V41498 4-Chlorotoluene <2.00 N9/L 2.00 5.00 10 12/07/23 20:20 MSA V41498 Di -Isopropyl Ether (DIPE) <9.60 N9/L 9.60 50.0 10 12/07/23 20:20 MSA V41498 1,2-Dibromo-3-Chloropropane <11.0 N9/L 11.0 20.0 10 12/07/23 20:20 MSA V41498 1,2-Dibromoethane <2.00 N9/L 2.00 5.00 10 12/07/23 20:20 MSA V41498 Dibromomethane <2.30 N9/L 2.30 5.00 10 12/07/23 20:20 MSA V41498 1,2-Dichlorobenzene <2.20 pg/L 2.20 5.00 10 12/07/23 20:20 MSA V41498 1,3-Dichlorobenzene <1.90 N9/L 1.90 5.00 10 12/07/23 20:20 MSA V41498 1,4-Dichlorobenzene <2.10 N9/L 2.10 5.00 10 12/07/23 20:20 MSA V41498 Dichlorodifluoromethane <12.0 N9/L 12.0 50.0 10 12/07/23 20:20 MSA V41498 1,1-Dichloroethane <2.40 N9/L 2.40 5.00 10 12/07/23 20:20 MSA V41498 1,2-Dichloroethane <1.50 u9/L 1.50 5.00 10 12/07/23 20:20 MSA V41498 1,1-Dichloroethene <1.50 u9/L 1.50 5.00 10 12/07/23 20:20 MSA V41498 cis- 1,2-Dichloroethene <2.00 u9/L 2.00 5.00 10 12/07/23 20:20 MSA V41498 trans-1,2-Dichloroethene <1.80 N9/L 1.80 5.00 10 12/07/23 20:20 MSA V41498 1,2-Dichloropropane <1.90 N9/L 1.90 5.00 10 12/07/23 20:20 MSA V41498 1,3-Dichloropropane <1.30 N9/L 1.30 5.00 10 12/07/23 20:20 MSA V41498 Qualifiers/ * Outside QC Limit DF Dilution Factor Definitions I Estimated value MQL Method Quantitation Limit Page 8 of 15 0 Waypoint. 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 ANALYTICAL www.waypointanalytical.com 00052 Weyerhaeuser Corporation Project Wastewater EFF Dennis Atkinson Report Date : 12/19/2023 524 Pride Way Information : Received : 11/30/2023 Elkin , NC 28621 Report Number : 23-334-0020 REPORT OFANAL YSIS Lab No : 90539 Matrix: Aqueous Sample ID : EFF Sampled: 11/30/2023 11:00 Analytical Method: 8260D Prep Batch(es): V41497 12/07/23 09:00 Prep Method: 5030E Test Results Units MDL MQL DF Date / Time By Analytical Analyzed Batch 2,2-Dichloropropane <2.10 pg/L 2.10 20.0 10 12/07/23 20:20 MSA V41498 1,1-Dichloropropene <2.00 pg/L 2.00 5.00 10 12/07/23 20:20 MSA V41498 cis- 1,3-Dichloropropene <2.10 pg/L 2.10 5.00 10 12/07/23 20:20 MSA V41498 trans-1,3-Dichloropropene <1.50 pg/L 1.50 5.00 10 12/07/23 20:20 MSA V41498 Ethylbenzene <1.70 pg/L 1.70 5.00 10 12/07/23 20:20 MSA V41498 Ethyl Tertiary Butyl Ether (ETBE) <18.0 pg/L 18.0 100 10 12/07/23 20:20 MSA V41498 Hexachlorobutadiene <3.50 pg/L 3.50 20.0 10 12/07/23 20:20 MSA V41498 n-Hexane <13.0 pg/L 13.0 100 10 12/07/23 20:20 MSA V41498 2-Hexanone <3.80 pg/L 3.80 50.0 10 12/07/23 20:20 MSA V41498 Isopropylbenzene <1.80 pg/L 1.80 50.0 10 12/07/23 20:20 MSA V41498 4-Isopropyl toluene <0.890 pg/L 0.890 5.00 10 12/07/23 20:20 MSA V41498 Methyl Ethyl Ketone (MEK) <7.10 pg/L 7.10 50.0 10 12/07/23 20:20 MSA V41498 Methyl tert-butyl ether (MTBE) <1.40 pg/L 1.40 5.00 10 12/07/23 20:20 MSA V41498 4-Methyl-2-Pentanone <10.0 pg/L 10.0 50.0 10 12/07/23 20:20 MSA V41498 Methylene Chloride <3.30 pg/L 3.30 10.0 10 12/07/23 20:20 MSA V41498 Naphthalene <4.70 p9/L 4.70 10.0 10 12/07/23 20:20 MSA V41498 n-Propylbenzene <1.90 pg/L 1.90 5.00 10 12/07/23 20:20 MSA V41498 Styrene <2.20 pg/L 2.20 5.00 10 12/07/23 20:20 MSA V41498 1, 1, 1,2-Tetrachloroethane <1.60 pg/L 1.60 5.00 10 12/07/23 20:20 MSA V41498 1,1,2,2-Tetrachioroethane <1.60 pg/L 1.60 5.00 10 12/07/23 20:20 MSA V41498 Tetrachloroethene <2.20 pg/L 2.20 5.00 10 12/07/23 20:20 MSA V41498 Toluene <2.20 pg/L 2.20 5.00 10 12/07/23 20:20 MSA V41498 Qualifiers/ * Outside QC Limit DF Dilution Factor Definitions J Estimated value MQL Method Quantitation Limit Page 9 of 15 Waypointo ANALYTICAL 00052 Weyerhaeuser Corporation Project Dennis Atkinson 524 Pride Way Information Elkin , NC 28621 Report Number : 23-334-0020 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www.waypointanalytical.com Wastewater EFF REPORT OFANALYSIS Report Date : 12/19/2023 Received : 11/30/2023 Lab No : 90539 Sample ID : EFF Matrix: Aqueous Sampled: 11/30/2023 11:00 Analytical Method: 8260D Prep Batch(es): V41497 12/07/23 09:00 Prep Method: 5030E Test Results Units MDL MQL DF Date /Time By Analytical Analyzed Batch 1,2,3-Trichlorobenzene <3.80 pg/L 3.80 20.0 10 12/07/23 20:20 MSA V41498 1,2,4-Trichlorobenzene <3.10 pg/L 3.10 10.0 10 12/07/23 20:20 MSA V41498 1,1,1-Trichloroethane <1.60 pg/L 1.60 5.00 10 12/07/23 20:20 MSA V41498 1,1,2-Trichloroethane <0.960 pg/L 0.960 5.00 10 12/07/23 20:20 MSA V41498 Trchloroethene <1.80 p9/L 1.80 5.00 10 12/07/23 20:20 MSA V41498 Trichlorofluoromethane <1.80 pg/L 1.80 5.00 10 12/07/23 20:20 MSA V41498 1,2,3-Trichloropropane <2.70 pg/L 2.70 10.0 10 12/07/23 20:20 MSA V41498 1,3,5-Trimethyl benzene <1.80 pg/L 1.80 5.00 10 12/07/23 20:20 MSA V41498 Vinyl Acetate <10.0 pg/L 10.0 20.0 10 12/07/23 20:20 MSA V41498 Vinyl Chloride <1.70 pg/L 1.70 5.00 10 12/07/23 20:20 MSA V41498 o-Xylene <2.10 pg/L 2.10 5.00 10 12/07/23 20:20 MSA V41498 m,p-Xylene <4.20 pg/L 4.20 10.0 10 12/07/23 20:20 MSA V41498 Xylene (Total) <2.1 pg/L 2.10 5.00 10 12/07/23 20:20 V41498 Surrogate: 4-Bromofluorobenzene 103 Limits: 80-124% 10 12/07/23 20:20 MSA V41498 Surrogate: Dibromofluoromethane 97.8 Limits: 75-129% 10 12/07/23 20:20 MSA V41498 Surrogate: 1,2-Dichloroethane - d4 93.0 Limits: 63-136% 10 12/07/23 20:20 MSA V41498 Surrogate: Toluene-d8 101 Limits: 77-123% 10 12/07/23 20:20 MSA V41498 Qualifiers/ * Outside QC Limit DF Dilution Factor Definitions I Estimated value MQL Method Quantitation Limit Page 10 of 15 Waypointo ANALYTICAL 00052 Weyerhaeuser Corporation Project Dennis Atkinson 524 Pride Way Information Elkin , NC 28621 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www.waypointanalytical.com Wastewater EFF Report Date : 12/19/2023 Received : 11/30/2023 Report Number : 23-334-0020 REPORT OFANAL YSIS Lab No : 90539 Matrix: Aqueous Sample ID: EFF Sampled: 11/30/2023 11:00 Analytical Method: 8315A Prep Batch(es): L720177 12/03/23 16:00 Prep Method: 8315A Test Results Units MDL MQL DF Date / Time By Analytical Analyzed Batch Formaldehyde Qualifiers/ Outside QC Limit Definitions J Estimated value <500 Ng/L 500 1 12/04/23 15:26 KDL L720486 DF Dilution Factor MQL Method Quantitation Limit Page 11 of 15 0 Waypoint, 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 ANALYTICAL www.waypointanalytical.com 00052 Weyerhaeuser Corporation Project Wastewater EFF Dennis Atkinson Report Date : 12/19/2023 524 Pride Way Information : Received : 11/30/2023 Elkin , NC 28621 Report Number : 23-334-0020 REPORT OFANAL YSIS Lab No : 90540 Matrix: Aqueous Sample ID : Field Sampled: 11/30/2023 0:00 Test Results Units MQL DF Date / Time By Analytical Analyzed Method pH 9.1 s.u. 1 11/30/2311:00 FLD FIELD Temperature 6.0 C 0.1 1 11/30/23 11:00 FLD FIELD Qualifiers/ * Outside QC Limit Definitions 3 Estimated value DF Dilution Factor MQL Method Quantitation Limit Page 12 of 15 (D Waypoint . ANALYTICAL 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www.waypointanalytical.com Shipment Receipt Form Customer Number: 00052 Customer Name: Weyerhaeuser Corporation Report Number: 23-334-0020 Shipping Method 0 Fed Ex 0 US Postal (# Lab 0 UPS 0 Client 0 Courier 0 Other: Thermometer ID: IIRT152.2C Shipping container/cooler uncompromised? # Yes 0 No Number of coolers/boxes received Custody seals intact on shipping container/cooler? 0 Yes 0 No # Not Present Custody seals intact on sample bottles? 0 Yes 0 No 0 Not Present Chain of Custody (COC) present? * Yes 0 No COC agrees with sample label(s)? # Yes 0 No COC properly completed * Yes 0 No Samples in proper containers? 0 Yes 0 No Sample containers intact? 0 Yes 0 No Sufficient sample volume for indicated test(s)? 0 Yes 0 No All samples received within holding time? 0 Yes 0 No Cooler temperature in compliance? Yes 0 No Cooler/Samples arrived at the laboratory on ice. Samples were considered acceptable as cooling process had begun. 0 Yes 0 No Water - Sample containers properly preserved Yes 0 No 0 N/A Water - VOA vials free of headspace # Yes 0 No 0 N/A Trip Blanks received with VOAs 0 Yes * No 0 N/A Soil VOA method 5035 — compliance criteria met 0 Yes 0 No (# N/A High concentration container (48 hr) F_ High concentration pre -weighed (methanol -14 d) Low concentration EnCore samplers (48 hr) F_ Low conc pre -weighed vials (Sod Bis -14 d) Special precautions or instructions included? 0 Yes # No Comments: Signature: 'Angelo Norvell Date & Time: 11/30/2023 15.01.07_' Page 13 of 15 Waypoint. ANALYTICAL 449 Springbrook Road • Charlotte. NC 28217 Phone 704/529-6364 • Fax: 704/525.0409 Client Company Name:_�4uS�.�r Report To/Contact Name: Reporting Address: CHAIN OF CUSTODY RECORD LA13 USE ONLY PAGE OF 2 QUOTE a TO ENSURE PROPER BILLING:_. _ Samples INTACT upon arrival? YES NO NIA Project Name: Received IN ICE? Short Hold Analysis (Yes) (No) UST Project: (Yes) (No) PROPER PRESERVATIVES Indicated? _ 'Please ATTACH any project specific reporting (QC LEVEL 1 II III IV) Received WITHIN HOLDING TIMESI provisions and/or QC Requirements CUSTODY SEALS INTACTI Invoice To: VOLATILES reed W/OUT HEADSPACE? PROPER CONTAIN RS used? TEMP Therm ID: Observed ��� _ G /Corr'C Phone:___ Fax (Yes)(No): _ ��� ��lN�! !!�!, ! !! '3-334-0020 111111I11111I111IIU1111IU11III111II1NII��I���l�lllll��l� TO BE FILLEDIN BY CLIENT/SAMPLING PERSONNEL Email Address: 005-1 —_ 'o' EDD Type: PDF_ Excel_Other _ Wewrhaeusen Coroomoon t�5906' Certification: NC _ SC waslav�der Site Location Name: Site Location Physical Address: Other— N/A - --- Water Chlorinated: YES_ NO ✓ / Samples RENDERED BYWAYPUINI ANALTIILAL.LLL SU�U=r.,, Iced Upon Collection: YES Y NO_ TIME MATRIX CLIENT DATE COLLECTED (SOIL, SAMPLE DESCRIPTION COLLECTED MILITARY WATER, OR SAMPLE CONTAINER .g LYg ,i S ED \ PRESERVA- 0 - TIVES�! /� REMARKS ID NO. 'TYPE I HOURS SLUDGE) SEE BELOW NO. SIZE ��� ��/x� ��; `G ,rt 'J E N 1-3rCcz, Flo C§ph x - _LX P bolo N &S FJ4 1 X f — P I I Samplers Signature _ Sampled By (Print Name)IMIA Qrt_LS I Affiliabon q� t o USE e NLY Upon relinquishing, this Chain of Cu tody Is your authorization for Waypoint Analytical to proceed with the analyses as requested above. An changes must be submitted in writing to the Waypoint Analytical Project Manager. There will be charges for any changes after analyses have been initialized. She Arrival Time: Ro!,vl iS:g, Recetmd By 'Sgnatwel Date Wilar ,Houn s Additional Comments. Site Departure Time: Race,,W13y ISgnah, - Date Field Tech Fee: Rrrna,n.nc-0 dy ,S,p^at a... Recerreo For Iftyr.'"rd Aniyt Gat Mileage: Meatoa M Srvtnten: NOTE: ALL SAMPLE COOLERS SHOULD BE TAPED SHUT WITH CUSTODY SEALS FOR TRANSPORTATION TO THE LABORATORY. I COC Gfouo No SAMPLES ARE NOT ACCEPTED AND VERIFIED AGAINST CDC UNTIL RECEIVED AT THE LABORATORY A J Fed E. J UPS J wamgmu M. nruea: ull: UrWUNLJVVAI CKr UKmrr,rnv YYA1LK: SULIU WASiE: KGKA: 13KWNFLU i LANDFILL OTHER: JNCJSC JNC JSC JNC JSC JNC JSC JNC JSC JNC JSC JNC JSC'JNC JSC JNC JSC J J J J — J J J J .. J ORIGINAL 'CONTAINER TYPE CODES' A n Amber C = Clear G= Glass P = Plastic: TL = Teflon -Lined Cat) VOA = Volatile Orqanics Analvsis (Zero Head SDacel 1 Waypoint_ ANALYTICAL 449 Springbrook Road • Charlotte, NC 28217 Phone 704/529-663644-FFax: 7�04115�25-0040,9r- Client Company Name:W J�u.]C�t---- Report To/Contact Name:-_ Reporting Address: Phone: �� Fax (Ye�s)� N j: Email Address: _ EDD Type: PDF— Excel —Other — Site Location Name: Site Location Physical Address: CHAIN OF CUSTODY RECORD PAGE L_ OF Z QUOTE R TO ENSURE PROPER BILLING:_ - Project Name: Short Hold Analysis (Yes) (No) UST Project: (Yes) (No) 'Please ATTACH any project specific reporting (QC LEVEL 1 II III IV) - provisions and/or QC Requirements Invoice To: Address: Ilu Illn IIIII II1I1I III11 IIII IIII 1INI IIII IIII IIIII INI II11 °°,a Weyerhaeuser ::01mla11on :4 59 06 Waslev.Wer ILR t1SE C YES NO NIA Samples INTACT upon arrival? _- Received IN ICE? PROPER PRESERVATIVES indicated? Received WITHIN HOLDING TIMES? CUSTODY SEALS INTACT? VOLATILES rec'd WIOUT HEADSPACEI PROPER CONTAt S usedl TEMP: Therm ID:Observed ?.:'�C /Corr 9.2'C TO BE FILLEDIN BY CLIENT/SAMPLING PERSONNEL Certification: NC­�/ SC_____ Other_ N/A - Water Chlorinated: YES__ NOI/ samples Iced upon Conecuon: 7 ca nv_ CLIENT DATE TIME COLLECTED MATRIX SAMPLE CONTAINER (SOIL. PRESERVA- ANALYSIS REQU TED %-'� 0� �/ REMARKS ID NO. SAMPLE DESCRIPTION COLLECTED MILITARY WATER. OR { 'TYPE NO I SIZE TNES ✓ ! �"(L '`9 d HOURS SLUDGE) SEE BELOW C FIP %3yz3 �/o I 25o Noive (OCO No P l 2 0 o3 _.. .— ._._ (A 2 1c co, 42-SNX Sampler's Signature _ _ Sampled By (Print Name) Affiliation%�: Upon relinquishing. this Chain o Custody is your authorization for Waypoint Analytical to proceed with the analyses as requested above. An changes must be Site Arrival Time: submitted In writing to the Waypoint Analytical Project Manager. There will be charges for any changes after analyses have been initialized. K my By c ky Rece"a ey Ismyaneer 1k1,Z3 13�5 Dale i nna IaryrHo„n Additional Comments: Site Departure Time: Refrm, lyna;wei Rece«ea By I SAnatu— I Dar. r Field Tech Fee: Re4nObfheO By fSx}rlawn � -- --- -- --- Rrrahvad For Wayro,..' ,�• B� a -- — /�i1 , l Mileage: 2 j� I V 3e /3S II kwhoa o! Srmp"M NOTE. ALL SAMPLE COOLERS SHOULD BE TAPED SHUT WITH CUSTODY SEAL R TRANSPORT ORATORY. .00 �ou0 No SAMPLES ARE NOT ACCEPTED AND VERIFIED AGAINST CDC UNTIL RECEIVED AT THE LABORATORY JFea E. J UPS J Hi1hA iP1Mre11 yplfnl Ate, IV1:'.1� FrWq SeJ1: Krf J ()thbr _ _ NPD S: I UST: GR NOWATER: DRINKING WATER: SOLID WASTE: I RCRA: BRWNFLD LANDFILL OTHER: JNCJSC -INC JSC J C JSC JNC JSC JNC JSC -INC JSC I JNC JSC ' JNC JSC JNC JSC -f-- IJ---- IJ-- -- I J IJ J_ J J__ J •rnr,nrn r►Ico Tvoc rnnl=c• a = Amhpr r = innapr A- Gla%R P a Plastic: TL = Teflon -Lined Can VOA =Volatile Organics Analysts (Zero Head Space) ORIGINAL H W O Ln w FORM NDAR-1 08-11 NON -DISCHARGE APPLICATION REPORT (NDAR-11 Page 1 of Permit No.: W00005555 Facility Name: Weyerhaeuser - Elkin, NC County: Surry Month: November Year: 2023 Did irrigation Field Name: 01 Field Name: 02 Field Name: 03 Field Name: 04 occur Area (acres): 2.17 Area (acres): 2.17 Area (acres): 2.17 Area (acres): 2.17 at this facility? Cover Crop:Ha Y Cover Crop: P� Ha Y Cover Crop: p� Ha Y Cover Crop: P� Ha Y YES NO Hourly Rate (in): 0.25 Hourly Rate (in): 0.25 Hourly Rate (in): 0.25 Hourly Rate (in): 0.25 Annual Rate (in): 20 Annual Rate (in): 20 Annual Rate (in): 20 Annual Rate (in): 20 Weather Freeboard Field Irrigated? ❑ YES 0 NO Field Irrigated? C7 YES NO Field Irrigated? i 1 YES - NO Field Irrigated? = YES _ NO T a� O E 3 f` o !9 m m O iv v V) .0 �' U_ >+ O_ ,� n. a, v E .2 7 a o a 9 d y E 01 i- rn T E la o o E M 7` C X p f�0 ca 2 0 E d a o a Ql E F L rn C O p E rn 7 C: C 'X O a 2 a m E d 7 a o a v d .U.. E n !- - rn 1 C A O o E rn 7 >' C 'X =p M m 2 0 m o E N 7 Q o a N .�, E m F- rn >. C M o o E m > >' C E LE 'K p M w 0 o °F in ft ft gal min in in gal min in in gal min in in gal min in in 1 0 2.74 2 0 2.76 3 0 2.77 4 0 2.41 5 0 2.42 6 0 2.42 7 0 2.55 8 0 2.56 9 0 2.57 10 0 2.57 11 0.13 2.69 12 C 59 0 2.69 3,832 15 0.07 0.07 7,517 30 0.13 0.13 131 0 2.54 14 0 2.54 15 0 2.55 16 C 70 0 2.56 8,503 30 0.14 0.14 T574 30 013 0.13 17 0 2.79 18 0 2.8 191 0 2.22 20 0 2.21 21 0.52 2.16 22 1.1 2.04 23 0 2.14 24 C 59 0 2.14 7,537 30 0.13 0.13 8.763 30 0.15 015 251 0 2.35 26 C 47 0 2.36 8,433 30 0.14 0.14 27 0 2.55 28 0 2.55 29 0 2.55 30 C 61 0 2.55 8,426 30 0.14 0.14 31 Monthly Loading: 0 0.00 0 0.00 36,731 0.621 23.854 0 40 12 Month Floating Total (in): 12.33 12.01 59 17,55 FORM: NDAR-1 08-11 NnN-nISCHARGF APPI ICATInN RFPnRT INnAR-11 Page 2 of 4 Permit No.: W00005555 Facility Name: Weyerhaeuser - Elkin, NC County: Surry Month: November Year: 2023 Did irrigation occur Field Name: 05 Field Name: 06 Field Name: 07 Field Name: 08 Area (acres): 2.29 Area (acres): 1.3 Area (acres): 2.01 Area (acres): 2.08 at this facility? Cover Crop:Ha Y Cover Crop: p� Ha Y Cover Crop: P� Ha Y Cover Crop: P� Ha Y YFS NO Hourly Rate (in): 0.25 Hourly Rate (in): 0.25 Hourly Rate (in): 0.25 Hourly Rate (in): 0.25 Annual Rate (in): 20 Annual Rate (in): 20 Annual Rate (in): 20 Annual Rate (in): 20 Weather Freeboard Field Irrigated? YES No Field Irrigated? ❑ YES 171 NO Field Irrigated? i YES - NO Field Irrigated? ! YES :_ NO n U d j o a� N 0 9 >' CL M E 2 d° a > E @ o E E o E .° > Q E mo E 2 > E _ o_o E rn ° E .� .2 CL 0 CL > a C) d E = > vC a J E rnc E °oo x J °F in ft ft gal min in in gal min in in gal min in in gal min in in 1 0 2.74 2 0 2.76 3 0 2.77 4 0 2.41 5 0 2.42 6 PC 72 0 2.42 8,832 30 0.14 0.14 7 0 2.55 8 0 2.56 9 0 2.57 10 CL 62 0 2.57 8,592 30 1 0.14 0.14 11 0.13 2.69 121 C 48 0 2.69 6,325 30 0.12 0.12 13 0 2.54 14 0 2.54 15 0 2.55 16 0 2.56 17 0 2.79 181 0 2.8 19 0 2.22 20 0 2.21 21 0.52 2.16 22 C 60 1.1 2.04 7,872 30 0.14 0.14 23 0 2.14 241 0 2.14 25 0 2.35 26 CL 49 0 2.36 6,334 30 0.12 0.12 27 0 2.55 28 0 2.55 29 0 2.55 30 0 2.55 31 Monthly Loading: 17,424 0.28 0 0.00 20,531 0.38 0 0.00 12 Month Floating Total (in): 13.43 12.951 9.11 10.45 FORM NDAR-1 08-11 Nr7N_IIIS('HARrF APPI ICATInN RFPORT INnAR-11 Page 3 of 4 Permit No.: W00005555 Facility Name: Weyerhaeuser - Elkin, NC County: Surry Month: November Year: 2023 Did irrigation Field Name: A Field Name: B Field Name: CN Field Name: CS occur Area (acres): 2.8 Area (acres): 2.56 Area (acres): 1.96 Area (acres): 1.24 at this facility? Cover Crop:Ha Y Cover Crop: P� Ha Y Cover Crop: P� Ha Y Cover Crop: P� Ha Y Y[ S NO Hourly Rate (in): 0.25 Hourly Rate (in): 0.25 Hourly Rate (in): 0.25 Hourly Rate (in): 0.25 Annual Rate (in): 31.8 Annual Rate (in): 31.8 Annual Rate (in): 31.8 Annual Rate (in): 31.8 Weather Freeboard Field Irrigated? YES ] No Field Irrigated? YES [-1 NO Field Irrigated? ' _' YES 7 NO Field Irrigated? ! YES NO > ❑ ° E � ° E F ` a fn i >a ❑ to L w - E ° i Q E - J E �rn E J °� . > Q : - m J E am E_ . J my = > Q - rn J E aar - E= J c v . = i Q o - rn ° J E Trn = c _° J °F in ft ft gal min in in gal min in in gal min in in gal min in in 1 0 2.74 2 0 2.76 3 0 2.77 4 0 2.41 5 0 2.42 6 0 2.42 7 0 2.55 8 0 2.56 9 0 2.57 10 0 2.57 11 0.13 2.69 12 0 2.69 13 0 2.54 14 1 0 2.54 151 0 2.55 16 0 2.56 17 0 2.79 18 0 2.8 19 0 2.22 20 0 2.21 21 0.52 2.16 22 1.1 2.04 23 0 2.14 241 0 2.14 25 0 2.35 26 0 2.36 27 0 2.55 28 0 2.55 29 0 2.55 30 0 2.55 31 Monthly Loading: 0 0.00 0 0.00 0 a00 0 0.00 12 Month Floating Total (in): 2 01 - 0.27 1 71 1. 11 FORM NDAR-1 08-1 1 NON -DISCHARGE APPLICATION REPORT (NDAR-1) Page 4 of 4 Did the application rates exceed the limits in Attachment B of your permit? l] Compliant ❑ Non -Compliant Were adequate measures taken to prevent effluent ponding in or runoff from the sites? (]Compliant El Non -Compliant Was a suitable vegetative cover maintained on all sites as specified in your permit? El Compliant [I Non -Compliant Were all setbacks listed in your permit maintained for every application to each permitted site? 2Compliant El Non -Compliant Were all freeboards maintained in accordance with the specified freeboard heights in your permit? El Compliant El Non -Compliant If the facility is non -compliant, please explain in the space below the reason(s) the facility was not in compliance. Provide in your explanation the date(s) of the non-compliance and describe the corrective action(s) taken Attach additional sheets if necessary. Operator in Responsible Charge (ORC) Certification Permittee Certification ORC: Dennis R. Atkinson Permittee: Weyerhaeuser Company Certification No.: 15574 Signing Official: Steve Kobelak Grade: SI Phone Number: 336-526-6437 Signing Officials Title: Mill Manager Has the ORC changed since the previous NDAR-1? ❑ Yes LJ No Phone Number: 336-526-6456 Permit Exp.: 8/31/25 t W ` .1- 2� L3 gnature Date Signature Date By this signature, I certify that this report is accurrate and complete to the best of my knowledge. I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that all qualified personnel properly gathered and evaluated the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete- I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing viotations Mail Original and Two Copies to: Division of Water Quality Information Processing Unit 1617 Mail Service Center Raleigh, North Carolina 27699-1617