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HomeMy WebLinkAboutWQ0004972_Monitoring - 11-2023_20231223Monitoring Report Submittal Permit Number#* Name of Facility:* Month: * November Report Information WQ0004972 Forest Lake RV WWTP Type * NDMR, NDAR-1, NDAR-2, NDMLR Confirmation Email Address: * Name of Submitter: * Signature: Date of submittal: Initial Review Year:* 2023 Upload Document* 2023_November_Monthly_WQ0004972 1.53M B complete.pdf PDF Only Please upload one PDF containing all applicable monitoring reports (i.e., NDMR, NDAR-1, NDAR-2, NDMLR, GW-59). agrenier@greenerehssolutions.com Amanda Grenier Gf•,�"a e*~Ot 12/23/2023 This will be filled in automatically Reviewer: Wanda.Gerald Is the project number correct?* WQ0004972 Is the monitoring report accepted?* Yes No Regional Office* Winston-Salem Reviewer: _anonymous Review Date: 1/10/2024 DocuSign Envelope ID: 4D01AB77-3CCC-4F66-A065-C201147C2550 Permit No.: WQ0004972 Facility Name: Forest Lake Preserve ELS County: Davie Month: November Year: 2023 PPI: 001 Flow Measuring Point: ❑ Influent 0 Effluent ❑ No flow generated Parameter Monitoring Point: ❑ Influent ❑ Effluent ElGroundwater Lowering El Surface Water Parameter Code 0 50050 00400 50060 1 70300 00530 00310 31616 00600 00610 00625 00630 00620 00615 00665 00940 oR QVdE o C H£ O O c O � > O O N La co 'o a CL F- N !n rnn O m c LL W ) a z R O E a t y Q w az 0 zz z Z WO 3L U)� 0 s a :2 OQ � 24-hr hrs GPD su mg/L mg/L mg/L mg/L #/100 mL mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L 1 08:00 5 38,079 7.2 2.6 2 08:00 5 34,220 7.1 2.7 3 08:00 5 37,694 6.9 0.9 4 31,952 5 22,156 6 08:00 5 28,973 6.9 0.3 7 08:00 5 22,382 7 2.4 8 08:00 5 21,784 6.8 2.6 9 08:00 5 26,498 6.8 4.1 10 HOLIDAY 17,651 H H 11 3,064 12 28,523 13 08:00 5 26,591 6.9 2 14 08:00 5 20,969 6.2 1.4 15 08:00 5 17,499 6 0.7 402 50.5 8.5 3200 33.8 0.64 6.7 27.1 27.1 <0.4 11.6 58.5 16 08:00 5 20,849 6.2 2.6 17 08:00 5 21,856 6.2 0.7 18 24,780 19 21,486 20 08:00 5 24,697 6.4 0.4 21 08:00 5 27,994 6.3 1.7 22 08:00 5 40,440 6.1 1.3 23 HOLIDAY 31,196 H H 24 Holiday 24,722 H H 25 29,598 26 29,638 27 08:00 5 31,049 6.4 1.2 28 08:00 5 30,446 6.2 1.7 29 08:00 5 33,429 5.9 1.4 30 08:00 5 32,277 6.4 1.6 31 Average: 26,750 1.47 402.00 50.50 8.50 3,200.00 33.80 0.64 6.70 27.10 27.10 0.00 11.60 58.50 Daily Maximum: 40,440 7.20 4.10 402.00 50.50 8.50 3,200.00 33.80 0.64 6.70 27.10 27.10 0.40 11.60 58.50 Daily Minimum: 3,064 5.90 0.30 402.00 50.50 8.50 3,200.00 33.80 0.64 6.70 27.10 27.10 0.40 11.60 58.50 Sampling Type: Monthly Avg. Limit: Daily Limit: LSample Frequency: Continuous 5x/Week 5X/Week Monthly Monthly Monthly Monthly Monthly Monthly Monthly Monthly Monthly Monthly Monthly 3X/year DocuSign Envelope ID: 4D01AB77-3CCC-4F66-A065-C201147C2550 Sampling Person(s) Certified Laboratories Name: Sam Perry Name: Name: Greener EHS Solutions, LLC Name: Pace Analytical Does all monitoring data and sampling frequencies meet the requirements in Attachment A of your permit? ❑ Compliant 0 Non -Compliant If the facility is non -compliant, please explain in the space below the reason(s) the facility was not in compliance. Provide in your explanation the date(s) of the non-compliance and describe the corrective action(s) taken. Attach additional sheets if necessary. The Monthly average flow exceeded the permitted flow of 24,400 gpd. The permitted application rate was not exceeded. The flow meter was calibrated on June 27, 2023 and the meter was reading significantly low before the calibration. This was noted on the June 2023 NDMR. The plant is in the process of an upgrade to increase the capacity as well as investigating extraneous flow for 1/1 and leaking fixtures. Lab Qualifiers, 11/15/23 on Phosphorus, TKN, and Chloride, M1 - Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery. Also on Phosphorus, R1 - RPD value was outside control limits. Operator in Responsible Charge (ORC) Certification Permittee Certification ORC: Sam Perry Permittee: MHC TT, LP Certification No.: 1014038 Signing Official: George Gudgeon Grade: SI Phone Number: 919-548-2381 Signing Officials Title: Sr. Vice President Has the ORC changed since the previous NDMR? ❑ Yes El No Phone Number: 312-279-1400 Permit Expiration: 10/31/2027 ' 12/22/23 �=-- 12/21/2023 I 2 Signature Date Signature Date By this signature, I certify that this report is accurrate and complete to the best of my knowledge. I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that all qualified personnel properly gathered and evaluated the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations. Mail Original and Two Copies to: Division of Water Resources Information Processing Unit 1617 Mail Service Center Raleigh, North Carolina 27699-1617 19 DocuSign Envelope ID: 4D01AB77-3CCC-4F66-A065-C201147C2550 I-- IVON-DISCHARGE APPLICATION REPORT (NDAR-1) Page of Permit No.: Q11149 • D.vie Month: November1 irrigation • occur at this facility'? . .. . .. . .. . .. ■ NO Hourly Rate (in): Hourly Rate (in): Hourly Rate (in): Annual Rate (in): Annual Rate (in): Field Irrigated? Field Irrigated? loll mmmm'mmm mmm mmmm I in in Monthly •.• . ���j�����j���j����j��j 111�j���j�/�j���j�% 1 11j���j���j����j 111����j� 12 Month Floating Total (irs DocuSign Envelope ID: 4D01AB77-3CCC-4F66-A065-C201147C2550 Did the application rates exceed the limits in Attachment B of your permit? 0 Compliant ❑ Non -Compliant Were adequate measures taken to prevent effluent ponding in or runoff from the sites? E Compliant ❑ Non -Compliant Was a suitable vegetative cover maintained on all sites as specified in your permit? E Compliant ❑ Non -Compliant Were all setbacks listed in your permit maintained for every application to each permitted site? E Compliant ❑ Non -Compliant Were all freeboards maintained in accordance with the specified freeboard heights in your permit? E Compliant ❑ Non -Compliant If the facility is non -compliant, please explain in the space below the reason(s) the facility was not in compliance. Provide in your explanation the date(s) of the non-compliance and describe the corrective action(s) taken. Attach additional sheets if necessary. Operator in Responsible Charge (ORC) Certification Permittee Certification ORC: Sam Perry Permittee: MHC TT, LP Certification No.: 1014038 Signing Official: George Gudgeon Grade: SI Phone Number: 919-548-2381 Signing Officials Title: Sr. Vice President Has the ORC changed since the previous NDAR-1? ❑ Yes O No Phone Number: 312-279-1400 Permit Exp.: 10/31/27 ' 12/22/23 12/21/2023 Sa erry (D 22, 2023 11:12 EST) Signature Date Signature Date By this signature, I certify that this report is accurrate and complete to the best of my knowledge. I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that all qualified personnel properly gathered and evaluated the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations. Mail Original and Two Copies to: Division of Water Resources Information Processing Unit 1617 Mail Service Center Raleigh, North Carolina 27699-1617 2: DocuSign Envelope ID: 4D01AB77-3CCC-4F66-A065-C201147C2550 aceo Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 December 01, 2023 Amanda D. Grenier Greener EHS Solutions 21 Selby Ct. Holly Springs, NC 27540 RE: Project: FOREST LAKE-NOVEMBER Pace Project No.: 92698903 Dear Amanda Grenier: Enclosed are the analytical results for sample(s) received by the laboratory on November 15, 2023. The results relate only to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report. The test results provided in this final report were generated by each of the following laboratories within the Pace Network: • Pace Analytical Services - Asheville • Pace Analytical Services - Charlotte If you have any questions concerning this report, please feel free to contact me. Sincerely, Matthew Brainard matthew.brainard@pacelabs.com 704-977-0942 Project Manager Enclosures REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 of 18 DocuSign Envelope ID: 4D01AB77-3CCC-4F66-A065-C201147C2550 aceo Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: FOREST LAKE-NOVEMBER Pace Project No.: 92698903 Pace Analytical Services Charlotte South Carolina Laboratory ID: 99006 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 North Carolina Drinking Water Certification #: 37706 North Carolina Field Services Certification #: 5342 North Carolina Wastewater Certification #: 12 South Carolina Laboratory ID: 99006 Pace Analytical Services Asheville 2225 Riverside Drive, Asheville, NC 28804 Florida/NELAP Certification #: E87648 North Carolina Drinking Water Certification #: 37712 North Carolina Wastewater Certification #: 40 CERTIFICATIONS South Carolina Certification #: 99006001 South Carolina Drinking Water Cert. #: 99006003 Florida/NELAP Certification #: E87627 Kentucky UST Certification #: 84 Louisiana DoH Drinking Water #: LA029 Virginia/VELAP Certification #: 460221 South Carolina Laboratory ID: 99030 South Carolina Certification #: 99030001 Virginia/VELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 2 of 18 DocuSign Envelope ID: 4D01AB77-3CCC-4F66-A065-C201147C2550 Pace Analytical Services, LLC �aceo 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 SAMPLE ANALYTE COUNT Project: FOREST LAKE-NOVEMBER Pace Project No.: 92698903 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92698903001 EFFLUENT GRAB SM 9222D-2015 KDF 1 PASI-C SM 2540C-2015 JAY 1 PASI-A SM 2540D-2015 JAY 1 PASI-A SM 521OB-2016 ABB 1 PASI-A TKN+NO3+NO2 Calculation KDF1 1 PASI-A EPA 350.1 Rev 2.0 1993 NCF 1 PASI-A EPA 351.2 Rev 2.0 1993 MFO 1 PASI-A EPA 353.2 Rev 2.0 1993 MFO 1 PASI-A EPA 365.1 Rev 2.0 1993 MFO 1 PASI-A SM 4500-CI-E-2011 KDF1 1 PASI-A PASI-A = Pace Analytical Services - Asheville PASI-C = Pace Analytical Services - Charlotte REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 3 of 18 DocuSign Envelope ID: 4D01AB77-3CCC-4F66-A065-C201147C2550 Pace Analytical Services, LLC �aceo 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: FOREST LAKE-NOVEMBER Pace Project No.: 92698903 Sample: EFFLUENT GRAB Lab ID: 92698903001 Collected: 11/15/23 12:00 Received: 11/15/23 12:15 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual MBIO 9222D Fecal Coliform CHT Analytical Method: SM 9222D-2015 Preparation Method: SM 9222D-2015 Pace Analytical Services - Charlotte Fecal Coliforms 3200 CFU/100 mL 1.0 1 11/15/23 16:34 11/16/23 14:55 2540C Total Dissolved Solids Analytical Method: SM 254OC-2015 Pace Analytical Services -Asheville Total Dissolved Solids 402 mg/L 25.0 1 11/17/23 10:33 2540D Total Suspended Solids Analytical Method: SM 2540D-2015 Pace Analytical Services -Asheville Total Suspended Solids 50.5 mg/L 12.5 1 11/20/23 12:51 5210B BOD, 5 day Analytical Method: SM 521OB-2016 Pace Analytical Services -Asheville BOD, 5 day 8.5 mg/L 2.0 1 11/16/23 16:54 11/21/23 12:09 Total Nitrogen Calculation Analytical Method: TKN+NO3+NO2 Calculation Pace Analytical Services -Asheville Total Nitrogen 33.8 mg/L 0.040 1 11/30/23 14:15 350.1 Ammonia Analytical Method: EPA 350.1 Rev 2.0 1993 Pace Analytical Services -Asheville Nitrogen, Ammonia 0.64 mg/L 0.10 1 11/30/23 05:39 7664-41-7 351.2 Total Kjeldahl Nitrogen Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993 Pace Analytical Services -Asheville Nitrogen, Kjeldahl, Total 6.7 mg/L 0.50 1 11/29/23 16:58 11/30/23 05:52 7727-37-9 353.2 Nitrogen, NO2/NO3 unpres Analytical Method: EPA 353.2 Rev 2.0 1993 Pace Analytical Services -Asheville Nitrogen, Nitrate 27.1 mg/L 0.40 10 11/16/23 00:04 14797-55-8 365.1 Phosphorus, Total Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation Method: EPA 365.1 Rev 2.0 1993 Pace Analytical Services -Asheville Phosphorus 11.6 mg/L 0.25 5 11/30/23 19:23 12/01/23 01:25 7723-14-0 4500 Chloride Analytical Method: SM 4500-CI-E-2011 Pace Analytical Services -Asheville Chloride 58.5 mg/L 3.0 3 11/29/2313:59 16887-00-6 M1 Date: 12/01 /2023 08:27 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 4 of 18 DocuSign Envelope ID: 4D01AB77-3CCC-4F66-A065-C201147C2550 Pace Analytical Services, LLC �aceo 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: FOREST LAKE-NOVEMBER Pace Project No.: 92698903 QC Batch: 813569 Analysis Method: SM 9222D-2015 QC Batch Method: SM 9222D-2015 Analysis Description: 9222D Fecal Coliform(MF) - CHT Laboratory: Pace Analytical Services - Charlotte Associated Lab Samples: 92698903001 METHOD BLANK: 4212334 Matrix: Water Associated Lab Samples: 92698903001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Fecal Coliforms CFU/100 mL ND 1.0 11/16/23 14:55 SAMPLE DUPLICATE: 4212335 Parameter Fecal Coliforms 92698901004 Dup Units Result Result RPD Qualifiers CFU/100 mL ND ND Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/01 /2023 08:27 AM without the written consent of Pace Analytical Services, LLC. Page 5 of 18 DocuSign Envelope ID: 4D01AB77-3CCC-4F66-A065-C201147C2550 Pace Analytical Services, LLC �aceo 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: FOREST LAKE-NOVEMBER Pace Project No.: 92698903 QC Batch: 814024 Analysis Method: SM 2540C-2015 QC Batch Method: SM 2540C-2015 Analysis Description: 2540C Total Dissolved Solids Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92698903001 METHOD BLANK: 4214348 Associated Lab Samples: 92698903001 Parameter Units Total Dissolved Solids mg/L LABORATORY CONTROL SAMPLE: 4214349 Parameter Units Total Dissolved Solids mg/L SAMPLE DUPLICATE: 4214350 Parameter Units Total Dissolved Solids mg/L Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 25.0 11 /17/23 10:30 Spike LCS LCS % Rec Conc. Result % Rec Limits Qualifiers 250 252 101 90-110 92698683014 Dup Result Result RPD Qualifiers 708 707 0 SAMPLE DUPLICATE: 4214351 92699055002 Dup Parameter Units Result Result Total Dissolved Solids mg/L 808 808 RPD Qualifiers 0 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/01 /2023 08:27 AM without the written consent of Pace Analytical Services, LLC. Page 6 of 18 DocuSign Envelope ID: 4D01AB77-3CCC-4F66-A065-C201147C2550 Pace Analytical Services, LLC �aceo 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: FOREST LAKE-NOVEMBER Pace Project No.: 92698903 QC Batch: 814296 Analysis Method: SM 2540D-2015 QC Batch Method: SM 2540D-2015 Analysis Description: 2540D Total Suspended Solids Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92698903001 METHOD BLANK: 4216181 Associated Lab Samples: 92698903001 Parameter Units Total Suspended Solids mg/L LABORATORY CONTROL SAMPLE: 4216182 Parameter Units Total Suspended Solids mg/L SAMPLE DUPLICATE: 4216792 Parameter Units Total Suspended Solids mg/L Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 2.5 11 /20/23 12:48 Spike LCS LCS % Rec Conc. Result % Rec Limits Qualifiers 250 238 95 90-110 92698825003 Dup Result Result RPD Qualifiers 2740 2640 4 SAMPLE DUPLICATE: 4216793 92698931001 Dup Parameter Units Result Result Total Suspended Solids mg/L 4170 4130 RPD Qualifiers 1 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/01 /2023 08:27 AM without the written consent of Pace Analytical Services, LLC. Page 7 of 18 DocuSign Envelope ID: 4D01AB77-3CCC-4F66-A065-C201147C2550 Pace Analytical Services, LLC �aceo 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: FOREST LAKE-NOVEMBER Pace Project No.: 92698903 QC Batch: 813829 Analysis Method: SM 521 OB-2016 QC Batch Method: SM 521OB-2016 Analysis Description: 5210E BOD, 5 day Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92698903001 METHOD BLANK: 4213532 Associated Lab Samples: 92698903001 Parameter Units BOD, 5 day mg/L LABORATORY CONTROL SAMPLE: 4213534 Parameter Units BOD, 5 day mg/L Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 2.0 11/21/2311:01 Spike LCS LCS % Rec Conc. Result % Rec Limits Qualifiers 198 188 95 84.6-115 SAMPLE DUPLICATE: 4213535 92698823002 Dup Parameter Units Result Result BOD, 5 day mg/L ND ND RPD Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/01 /2023 08:27 AM without the written consent of Pace Analytical Services, LLC. Page 8 of 18 DocuSign Envelope ID: 4D01AB77-3CCC-4F66-A065-C201147C2550 Pace Analytical Services, LLC �aceo 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: FOREST LAKE-NOVEMBER Pace Project No.: 92698903 QC Batch: 816226 Analysis Method: EPA 350.1 Rev 2.0 1993 QC Batch Method: EPA 350.1 Rev 2.0 1993 Analysis Description: 350.1 Ammonia Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92698903001 METHOD BLANK: 4224999 Associated Lab Samples: 92698903001 Parameter Units Nitrogen, Ammonia mg/L LABORATORY CONTROL SAMPLE: 4225000 Parameter Units Nitrogen, Ammonia mg/L Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 0.10 11 /30/23 04:37 Spike LCS LCS % Rec Conc. Result % Rec Limits Qualifiers 5 4.9 98 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4225001 4225002 MS MSD 92698901003 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, Ammonia mg/L ND 5 5 4.6 4.6 92 92 90-110 0 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4225003 4225004 MS MSD 92698901004 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, Ammonia mg/L ND 5 5 4.7 4.7 94 94 90-110 1 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/01 /2023 08:27 AM without the written consent of Pace Analytical Services, LLC. Page 9 of 18 DocuSign Envelope ID: 4D01AB77-3CCC-4F66-A065-C201147C2550 Pace Analytical Services, LLC �aceo 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: FOREST LAKE-NOVEMBER Pace Project No.: 92698903 QC Batch: 816054 Analysis Method: EPA 351.2 Rev 2.0 1993 QC Batch Method: EPA 351.2 Rev 2.0 1993 Analysis Description: 351.2 TKN Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92698903001 METHOD BLANK: 4223818 Associated Lab Samples: 92698903001 Parameter Units Nitrogen, Kjeldahl, Total mg/L LABORATORY CONTROL SAMPLE: 4223819 Parameter Units Nitrogen, Kjeldahl, Total mg/L Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 0.50 11 /30/23 05:48 Spike LCS LCS % Rec Conc. Result % Rec Limits Qualifiers 10 10.4 104 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4223820 4223821 MS MSD 92699840003 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, Kjeldahl, Total mg/L 0.68 10 10 12.3 11.7 117 111 90-110 5 M1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4223822 4223823 MS MSD 92699840004 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, Kjeldahl, Total mg/L 0.82 10 10 11.6 11.5 107 107 90-110 0 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/01 /2023 08:27 AM without the written consent of Pace Analytical Services, LLC. Page 10 of 18 DocuSign Envelope ID: 4D01AB77-3CCC-4F66-A065-C201147C2550 Pace Analytical Services, LLC �aceo 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: FOREST LAKE-NOVEMBER Pace Project No.: 92698903 QC Batch: 813618 Analysis Method: EPA 353.2 Rev 2.0 1993 QC Batch Method: EPA 353.2 Rev 2.0 1993 Analysis Description: 353.2 Nitrate + Nitrite, Unpres. Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92698903001 METHOD BLANK: 4212596 Associated Lab Samples: 92698903001 Parameter Units Nitrogen, Nitrate mg/L LABORATORY CONTROL SAMPLE: 4212597 Parameter Units Nitrogen, Nitrate mg/L Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 0.040 11 /15/23 23:43 Spike LCS LCS % Rec Conc. Result % Rec Limits Qualifiers 1.5 1.5 100 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4212598 4212599 MS MSD 92698744001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, Nitrate mg/L 0.074 1.5 1.5 1.5 1.5 98 98 90-110 0 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/01 /2023 08:27 AM without the written consent of Pace Analytical Services, LLC. Page 11 of 18 DocuSign Envelope ID: 4D01AB77-3CCC-4F66-A065-C201147C2550 Pace Analytical Services, LLC �aceo 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: FOREST LAKE-NOVEMBER Pace Project No.: 92698903 QC Batch: 816370 Analysis Method: EPA 365.1 Rev 2.0 1993 QC Batch Method: EPA 365.1 Rev 2.0 1993 Analysis Description: 365.1 Phosphorus, Total Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92698903001 METHOD BLANK: 4225495 Associated Lab Samples: 92698903001 Parameter Units Phosphorus mg/L LABORATORY CONTROL SAMPLE: 4225496 Parameter Units Phosphorus mg/L Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 0.050 11 /30/23 23:50 Spike LCS LCS % Rec Conc. Result % Rec Limits Qualifiers 2.5 2.6 104 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4225497 4225498 MS MSD 92698901001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Phosphorus mg/L 0.11 2.5 2.5 2.6 2.6 99 98 90-110 1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4225499 4225500 MS MSD 92698901002 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Phosphorus mg/L 0.071 2.5 2.5 2.6 2.3 99 89 90-110 11 M1,R1 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/01 /2023 08:27 AM without the written consent of Pace Analytical Services, LLC. Page 12 of 18 DocuSign Envelope ID: 4D01AB77-3CCC-4F66-A065-C201147C2550 Pace Analytical Services, LLC �aceo 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: FOREST LAKE-NOVEMBER Pace Project No.: 92698903 QC Batch: 815974 Analysis Method: SM 4500-CI-E-2011 QC Batch Method: SM 4500-CI-E-2011 Analysis Description: 4500 Chloride Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92698903001 METHOD BLANK: 4223384 Associated Lab Samples: 92698903001 Parameter Units Chloride mg/L LABORATORY CONTROL SAMPLE: 4223385 Parameter Units Chloride mg/L Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 1.0 11 /29/23 13:56 Spike LCS LCS % Rec Conc. Result % Rec Limits Qualifiers 20 20.1 101 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4223386 4223387 MS MSD 92698903001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Chloride mg/L 58.5 10 10 64.9 65.2 63 66 90-110 0 M1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4223388 4223389 MS MSD 92699488001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Chloride mg/L 25.8 10 10 35.0 35.1 92 93 90-110 0 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/01 /2023 08:27 AM without the written consent of Pace Analytical Services, LLC. Page 13 of 18 DocuSign Envelope ID: 4D01AB77-3CCC-4F66-A065-C201147C2550 aceo Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALIFIERS Project: FOREST LAKE-NOVEMBER Pace Project No.: 92698903 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as "Total" may vary slightly from the sum of the reported component parameters. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TN -The NELAC Institute. ANALYTE QUALIFIERS M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery. R1 RPD value was outside control limits. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/01 /2023 08:27 AM without the written consent of Pace Analytical Services, LLC. Page 14 of 18 DocuSign Envelope ID: 4D01AB77-3CCC-4F66-A065-C201147C2550 aceo Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: Pace Project No.: FOREST LAKE-NOVEMBER 92698903 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92698903001 EFFLUENT GRAB SM 9222D-2015 813569 SM 9222D-2015 813570 92698903001 EFFLUENT GRAB SM 254OC-2015 814024 92698903001 EFFLUENT GRAB SM 2540D-2015 814296 92698903001 EFFLUENT GRAB SM 521 OB-2016 813829 SM 521 OB-2016 813899 92698903001 EFFLUENT GRAB TKN+NO3+NO2 816444 Calculation 92698903001 EFFLUENT GRAB EPA 350.1 Rev 2.0 1993 816226 92698903001 EFFLUENT GRAB EPA 351.2 Rev 2.0 1993 816054 EPA 351.2 Rev 2.0 1993 816244 92698903001 EFFLUENT GRAB EPA 353.2 Rev 2.0 1993 813618 92698903001 EFFLUENT GRAB EPA 365.1 Rev 2.0 1993 816370 EPA 365.1 Rev 2.0 1993 816576 92698903001 EFFLUENT GRAB SM 4500-CI-E-2011 815974 Date: 12/01 /2023 08:27 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 15 of 18 DocuSign Envelope ID: 4D01AB77-3CCC-4F66-A065-C201147C2550 , )2 -$ample Condition Upon Receipt 'pace - - - - --- Effective Date: 11/14/2022 Laboratory receiving samples: Asheville ❑ Eden❑ Greenwood ❑ Huntersville0 Raleigh❑ Mechanicsville❑ Atlanta❑ Kernersvillel—I SampleClient Name: /' ; i Upon • l e �( r_ 145 )CI I Project tt: W0# : 92698903 Courier: [—]Fed Ex ❑UPS [:]LISPS ❑Client IIIIII III II'lll II'I III ❑ Commercial []Pace ❑Other: 92696903 , Custody Seal Present? ❑Yes pNo Seals Intact? []Yes ❑No Packing Material: ❑Bubble Wrap ❑Bubble Bags ❑None ❑ Other Thermometer: (� ❑ IR Gun 10: �V 7U Type of Ice: cowet (� Correction Factor: Cooler Temp: 1 Add/Subtract ('C) Cooler Temp Corrected (°C): USDA Regulated Soil ( Q N/A, water sample) Did samples originate in a quarantine zone within the United States: CA. NY, or SC Date/initials Person Examining Contents:'/ r//z Biological Tissue Frozen? r [-]Yes ❑No ❑N/A ❑[clue ❑None Temp should be above freezing to 6°C ❑Samples out of temp criteria. Samples on ice, cooling process has begun Did samnles oticinatp from a Fnrpivn cnurrp tintprnatinnally (check maps)? ❑Yes ❑No including Hawaii and Puerto Rico)? []Yes []No Comments/Discrepancy: Chain of Custody Present? ZYes ❑No ❑N/A 1. Samples Arrived within Hold Time? E)Yes ❑No ❑N/A 2. Short Hold Time Analysis (<72 hr.)? QLYes (:]No ❑N/A 3. Rush Turn Around Time Requested? ❑Yes PNo []N/A 4. Sufficient Volume? bYes ❑No ❑N/A 5. Correct Containers Used? -Pace Containers Used? byes PYes []NO [:]No ❑N/A ❑N/A 6. Containers Intact? Yes ❑No ❑N/A 7. Dissolved analysis: Samples Field Filtered? ❑Yes ❑No ❑$ /A R. Sample Labels Match COC? -Includes Oate/Time/ID/Analysis Matrix: Pyes ,ill.' ❑No ❑N/A 9. Headspace in VOA Vials (>5.6mm)? ❑Yes []No jjN/A 10. Trip Blank Present? Trip Blank Custody Seals Present? ❑Yes Des []NO []No ❑N/A A N/A 11. COMMENTS/SAMPLE DISCREPANCY Lot ID of split containers: CLIENT NOT Person contacted: Date/Time: Project Manager SCURF Review: Date: Project Manager SRF Review: Date: Field Data Required? ❑Yes "No Qualtrax ID: 69614 Page 1 of 2 Page 16 of 18 DocuSign Envelope ID: 4D01AB77-3CCC-4F66-A065-C201147C2550_ .J2 Sample Condition Upon Receipt ace - Effective Date: 11/14/2022 *Check mark top half of box if pH and/or dechlorination is verified and Project I within the acceptance range for preservation samples. Exceptions: VOA, Coliform, TOC, Oil and Grease, DRO/8015 (water( DOC, LLHg "Bottom half of box is to list number of bottles ***Check all unpreserved Nitrates for chlorine WO#:92698903 PM: MWB Due Date: 12/01/23 CLIENT: 92-Greener U A a, Z U V U \ E a — Z 13 2 N a D V a J E ,n N 7 V a M \ Z "a 2 vdi a 7 V N a J E o u1 > M o Cl Z N a u ✓ a J E o to > N a Co Q Z CJ c d °JEE%n _ .••1 > .-1 d m _ U N V G 4 O = �, '.' u y ,..1 H O d m N d M O x u N A a J o i N Z M a Co O 2 u ¢ N V "' „ rs J ti N sf a m U N = ? = O 2 V N q a ECJ v - A q d to CJ C N a Cl '.' o E v LL'. Ur yy 7 \ Z Z N N .n E Q — r.1 ►1 (7 Q N y a v = CJ n E Q ri _ ••1 t7 Q 2 'O N o O W M E ¢ - E o N rn t7 Q N = O. O = y E ¢ .-J N .-i l� Q N v CL c _ .0 E q - f o N V1 M l7 Q \ Z _ = Z C! a E Q E O 'T O Q1 t) O 2 U = ¢ O > E O a 2 M l7 O \ Z O Z q O > .� M t9 > \ 'a 01 a c J ¢ 0 > O 01 V > Z O d n = q O > v M l9 O Z CJ � c U M G. Vl ' n a Y Z A > , :, Y C a V, >ut V ]L t7 \ > A Z it N y1 E N i1 1~/1 a N i0 Z '° iL CJ V1 J E O N N N a H Q1 O rNi z 1 E ON N r&i� a CJ H 40 > q oJf O "J = O L7 ¢ Q H O � JE O N N > } c E JE O v 01 O O VCN� \ 2 \ 3 4 -- 5 6 1 N\ 7 8 g 10 11 12 pH Adjustment Log for Preserved Samples Sample ID Type of Preservative pH upon receipt Date preservation adjusted Time preservation adjusted Amount of Preservative added lot f1 NOW. vvnerlevel u1e1e is a discrepancy anecung North Carouna compuance samples, a copy of this form will be sent to the North Carolina DENR Certification Office (i.e. Out of hold, incorrect preservative, out of temp, incorrect containers. Page 17 of 18 Qualtrax ID: 69614 Page 2 of 2 DocuSign Envelope ID: 4D01AB77-3CCC-4F66-A065-C201147C2550 _ _ M3 h 3 / 3 3 Cb _ _ — 0 n 3 -4- X o n. o 3 3 F ° ° z 0 Ci o o Q; o -s ( =p �= �o t F z m o = Z F _ — a m 0 a � c � N a — � 3 3 3 3 m 3 = `c 0 o Oo ' 3 0 _ — o 0 o n — # o T n a o �, a n � a s 1 3- o - -o " �O _ _ D O - - A o_ ; Z 3 F s - s - 3 3 3 CJ o - o r1 N y3 o o � — N o m (p<o F5-:--- -i Ammonia/ T. Phos BOD 5-day n a n Chloride a + o Fecal Coliform MF. M-FC Nitrate Y — - o o _ o (�i 3 3 3 - r rn m d TDS - � m TSSD o i o Total Nitrogen & TKN m > _ a — a n — _ � w oa N 2 Lab Use Only 0 p v^ 3 r S A D 3 v o Q\ - - u o_ - - S x rQ rQ 3 3 0"_ o 3 3 00 E o$ a 3 , - a u �• z v — o N ? - 0 o a — Z ar 3 l g a -g -= 3 a - - o Dn� =8 a o a -_ _ v P -= - Preservation nonconformance identified for — — Page 18 of 1 sample. — 2023_November Monthly Report for signature Final Audit Report 2023-12-22 Created: 2023-12-22 By: Amanda Grenier (agrenier@greenerehssolutions.com) Status: Signed Transaction ID: CBJCHBCAABAAT523KPWcGOBQPpk2LVVYZVlo2tvzS31e "2023_November_Monthly Report for signature" History Document created by Amanda Grenier (agrenier@greenerehssolutions.com) 2023-12-22 - 3:42:54 PM GMT Document emailed to Sam Perry (sperry@greenerehssolutions.com) for signature 2023-12-22 - 3:42:59 PM GMT Email viewed by Sam Perry (sperry@greenerehssolutions.com) 2023-12-22 - 4:10:57 PM GMT Document e-signed by Sam Perry (sperry@greenerehssolutions.com) Signature Date: 2023-12-22 - 4:12:42 PM GMT - Time Source: server Agreement completed. 2023-12-22 - 4:12:42 PM GMT a Adobe Acrobat Sign