NC0021253_Renewal (Application)_20240109

�ROY COOPER •
I /
Governor v, d • N
ELIZABETH S.BISER ' . '^°r,,;r• •
Secretary 4.Q..,v . ,
RICHARD E.ROGERS,JR. NORTH CAROLINA
Director Environmental Quality
January 10, 2024
City of Havelock
Attn: Rick Day, Public Services Dir.
PO Box 368
Havelock, NC 28532-0368
Subject: Permit Renewal
Application No. NC0021253
Havelock WWTP
Craven County
Dear Applicant:
The Water Quality Permitting Section acknowledges the January 09, 2024, receipt of your permit renewal application and
supporting documentation. Your application will be assigned to a permit writer within the Section's NPDES WW permitting
branch. Per G.S. 150E-3 your current permit does not expire until permit decision on the application is made.
Continuation of the current permit is contingent on timely and sufficient application for renewal of the current permit. The
permit writer will contact you if additional information is required to complete your permit renewal. Please respond in a
timely manner to requests for additional information necessary to allow a complete review of the application and renewal
of the permit.
Information regarding the status of your renewal application can be found online using the Department of Environmental
Quality's Environmental Application Tracker at:
https://deci.nc.gov/permits-regulations/permit-guidance/environmental-application-tracker
If you have any additional questions about the permit, please contact the primary reviewer of the application using the
links available within the Application Tracker.
Sincerely
Xfien't,
Wren T dfor
Administrative Assistant
Water Quality Permitting Section
cc: Rodney George, ORC
ec: Todd Davis-Hazen & Sawyer
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City of Havelock Wastewater Treatment Plant
NPDES Permit Renewal Application
Application No. NC0021253
City of Havelock, North Carolina
December 2023

Hazen
4011 Westchase Blvd. Tel [phone]
RECEIVED
Suite 500 Fax [phone]
Raleigh,North Carolina 27607 JAN 0 9 2024
Transmittal Letter NpDES
To: Copies: NCDEQIDWR 1
Mike Montebello
Water Quality Permitting Section —NPDES Unit
512 N. Salisbury Street(9th Floor)
Raleigh, NC 27604
From: Date:
Mary Sadler January 4, 2024
Subject:
Havelock WWTP NPDES Permit Renewal Application
We are sending you:
® Attached ❑ Under Separate Cover Via the Following Items:
❑ Shop Drawings ❑ Plans ❑ Specifications ❑ Change Order
❑ Prints ❑ Samples ❑ Copy of Letter ❑ Reports
® Other: Havelock WWTP NPDES Permit Renewal Application
Copies Date Drawing No. Rev. Description Action*
3 12/23 ---- Havelock WWTP NPDES Permit Renewal Application
1 12/23 Digital Copy of Havelock WWTP NPDES Permit Renewal
Application
Action*
❑ A Approved ❑ CR Correct and Resubmit ❑ Resubmit Copies
❑ AN Approved As Noted ❑ F File ❑ Return Copies
❑ AS As Requested ® FA For Approval ❑ Review and Comment
❑ Other:
Mailing Method
❑ U.S.Postal Service 1st Class ❑ Courier/Hand Delivery ❑ FedEx Priority Overnight ❑ FedEx 2-Day Delivery
❑ Certified/Registered Mail ❑ United Postal Service(UPS) ❑ FedEx Standard Overnight ❑ FedEx Economy
❑ Other:
Comments:

OATt!
Cioo....„A' GRO� CITY OF HAVELOCK
11) Post Office Box 368
1 Governmental Ave.
RECEIVED
Havelock,NC 28532-co.,+ORA?6p..
JAN 0 9 2n74
NCDEQIDWRINPDES
December 27, 2023
Mr. Mike Montebello
Water Quality Permitting Section—NPDES
Division of Water Resources
North Carolina Department of Environmental Quality
1617 Mail Service Center Raleigh,NC,27699-1617
Re: NPDES Permit Renewal Application(NC0021253)
City of Havelock Wastewater Treatment Plant
City of Havelock,North Carolina
Dear Mr.Montebello:
The City of Havelock Public Services Department is permitted to discharge 2.25 million gallons per day
(mgd)of treated effluent from the City of Havelock Wastewater Treatment Plant(WWTP)to the Neuse
River per North Carolina NPDES Permit NC0021253.This NPDES permit is scheduled to expire on June 30,
2024.The enclosed application is for the renewal of this permit.In accordance with the requirements of
federal(40 CFR 122)and state(15A NCAC 2H.0105(3))regulations,we are submitting three signed copies
and one electronic file of the completed application package and associated attachments and figures.The
application package includes the following information:
• Tab A: NPDES Permit Application—EPA Form 2A
• Tab B: EPA Form 2A Additional Information(Process Narrative,Topographic Map,and Process
Flow Diagrams)
• Tab C: City of Havelock WWTP Sludge Management Plan
• Tab D: First Species Effluent Toxicity Testing,2020-2023
• Tab E: Annual Priority Pollutant Analysis Results,2021-2023
• Tab F: Mercury Analytical Data,2022-2023
• Tab G: Second Species Effluent Toxicity Testing(pending)
Phone[phone] www.havelocknc.us Fax[phone]

At the time of this application submittal,the required second species toxicity testing events have not yet been
completed. The four second species effluent toxicity tests are currently scheduled to be completed in
December 2023,January 2024,March 2024,and April 2024.The second species toxicity tests will be
forwarded to the Division of Water Resources(DWR)along with revisions to Part E of EPA Form 2A to
include these results.All second species toxicity tests will be submitted prior to the current permit expiration
date of June 30,2024.
During the preparation of our application,we discovered a reporting error in our Discharge Monitoring Report
(DMR)for mercury. Mercury samples were collected in May 2022,May 2023, and August 2023.The mercury
data was reported incorrectly on our DMRs with the units of ug/L;however,a review of the laboratory
analytical reports confirmed that the data should have been reported in our DMRs as ng/L. The laboratory
analytical reports supporting the correct mercury concentrations in ng/L are provided in Tab F of this renewal
application package. The corrected mercury data was used to complete Table C of EPA Form 2A. The
following table provides a summary of the reported DMR mercury values and the corrected mercury values:
Sample Date Reported Actual(Corrected)
Mercury Result Mercury Result
May 11,2022 1.4 µg/L 1.4 ng/L
May 3,2023 <1 µg/L <1 ng/L
August 3,2023 <1 µg/L <1 ng/L
If you have any questions regarding any of the NPDES permit renewal application materials,please contact me
at(252)444-6409 or [e-mail].
Sincerely,
Rick Day
Public Services Director
Attachments
cc:
Rodney George,City of Havelock
Mary Sadler,PE,Hazen and Sawyer
Jocelyn Russell,PE,Hazen and Sawyer
Todd Davis,PE,Hazen and Sawyer
Phone[phone] www.havelocknc.us Fax[phone]

City of Havelock Wastewater Treatment Plant
NPDES Permit No.NC0021253
Outfall 002
Table of Contents
Tab A. EPA Form 2A
Tab B. EPA Form 2A Additional Information
a. Figure 1 -Topographic Map
b. Figure 2—Site Map
c. Figure 3—Phase 1 Process Flow Diagram(2.25 mgd)
d. Figure 4-Phase 2 Process Flow Diagram(2.8 mgd)
e. Figure 5 -Phase 3 Process Flow Diagram(3.5 mgd)
f. Process Narrative
Tab C. Sludge Management Plan
Tab D. Summary of First Species Effluent Toxicity Testing,2020 to 2023
Tab E. Annual Priority Pollutant Analysis Results, 2021 to 2023
Tab F. Mercury Testing Laboratory Reports
Tab G. Second Species Toxicity Testing Results, Pending

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NPDES Permit Application -
EPA Form 2A

EPA Identification Number NPDES Permit Number I Facility Name Form Approved 03/05/19
110012588280 NC0021253 I City of Havelock WWTP OMB No.2040-0004
Form U.S.Environmental Protection Agency
2A a EPA Application for NPDES Permit to Discharge Wastewater
NPDES NEW AND EXISTING PUBLICLY OWNED TREATMENT WORKS
SECTION 1.BASIC APPLICATION INFORMATION FOR ALL APPLICANTS(40 CFR 122.21(j)(1)and(9))
1.1 Facility name
City of Havelock Wastewater Treatment Plant
Mailing address(street or P.O.box)
P.O.Box 368
City or town State ZIP code
o Havelock NC 28532
EContact name(first and last) Title Phone number Email address
Rodney George WWTP ORC [phone] [e-mail]
Location address(street,route number,or other specific identifier) D Same as mailing address
co 304 North Jackson Dr.
City or town State ZIP code
Havelock NC 28532
1.2 Is this application for a facility that has yet to commence discharge?
❑ Yes 4 See instructions on data submission 0 No
requirements for new dischargers.
1.3 Is applicant different from entity listed under Item 1.1 above?
0 Yes ❑ No 4 SKIP to Item 1.4.
Applicant name
City of Havelock
= Applicant address(street or P.O.box)
g P.O.Box 368
oCity or town State ZIP code
= Havelock NC 28532
co Contact name(first and last) Title Phone number Email address
a Rick Day Public Services Director [phone] [e-mail]
a 1.4 Is the applicant the facility's owner,operator,or both?(Check only one response.)
❑ Owner 0 Operator ❑✓ Both
1.5 To which entity should the NPDES permitting authority send correspondence?(Check only one response.)
❑ Facility 0 Applicant ❑ Facility and applicant
(they are one and the same)
1.6 Indicate below any existing environmental permits.(Check all that apply and print or type the corresponding permit
r number for each.)
�, Existing Environmental Permits
a7.6 r❑ NPDES(discharges to surface ❑ RCRA(hazardous waste) ❑ UIC(underground injection
0 water) control)
E NC0021253
c
o ✓❑ PSD(air emissions) ❑ Nonattainment program(CAA) ❑ NESHAPs(CM)
c
w 09110G01(General Air Permit)
DI
N ❑ Ocean dumping(MPRSA) ❑ Dredge or fill(CWA Section ❑✓ Other(specify)
w 404) WQ0000702(Land Application Permit)
WQCS00104(Collection System Permit)
EPA Form 3510-2A(Revised 3-19) Page 1

EPA Identification Number NPDES Permit Number Facility Name Form Approved 03/05/19
110012588280 NC0021253 City of Havelock WWTP OMB No.2040-0004
1.7 Provide the collection system information requested below for the treatment works.
Municipality Population Collection System Type
Served Served (indicate percentage) Ownership Status
Havelock,NC 12,900 100 %separate sanitary sewer 0 Own Ill Maintain
CD %combined storm and sanitary sewer ❑ Own 0 Maintain
d 0 Unknown ❑ Own 0 Maintain
co %separate sanitary sewer ❑ Own ❑ Maintain
%combined storm and sanitary sewer ❑ Own ❑ Maintain
-5 ❑ Unknown ❑ Own ❑ Maintain
c.
a %separate sanitary sewer 0 Own ❑ Maintain
c %combined storm and sanitary sewer El Own ❑ Maintain
E ❑ Unknown ElOwn ElMaintain
w %separate sanitary sewer 0 Own 0 Maintain
%combined storm and sanitary sewer ❑ Own ❑ Maintain
c ❑ Unknown 0 Own ❑ Maintain
dTotal 12,900
Population
ci Served
Separate Sanitary Sewer System Combined Storm and
Sanitary Sewer
Total percentage of each type of
sewer line(in miles) 100
Z' 1.8 Is the treatment works located in Indian Country?
•
o ❑ Yes 0 No
0
(.)
R 1.9 Does the facility discharge to a receiving water that flows through Indian Country?
c 0 Yes No
1.10 Provide design and actual flow rates in the designated spaces. Design Flow Rate
2.25 mgd
To
Annual Average Flow Rates(Actual)
v Two Years Ago Last Year This Year
c o ce
03 2021 1.37 mgd 2022 1.18 mgd Jan-Oct 1.26 mgd
En 2023
Maximum Daily Flow Rates(Actual)
o Two Years Ago Last Year This Year
2021 3.22 mgd 2022 3.00 mgd Jan-Oct 3.01 mgd
2023
(n 1.11 Provide the total number of effluent discharge points to waters of the United States by type.
w
o Total Number of Effluent Dischar a Points by T e
°- a Constructed
a'~ Treated Effluent Untreated Effluent Combined Sewer Bypasses Emergency
s Overflows Overflows
U —
N
6 1 0 0 0 0
EPA Form 3510-2A(Revised 3-19) Page 2

EPA Identification Number NPDES Permit Number Facility Name Form Approved 03/05/19
110012588280 NC0021253 City of Havelock WWTP OMB No.2040-0004
1
Outfalls Other Than to Waters of the United States
1.12 Does the POTW discharge wastewater to basins,ponds,or other surface impoundments that do not have outlets for
discharge to waters of the United States?
❑ Yes ❑✓ No 4 SKIP to Item 1.14.
1.13 Provide the location of each surface impoundment and associated discharge information in the table below.
Surface Impoundment Location and Discharge Data
Average Daily Volume Continuous or Intermittent
Location Discharged to Surface
Impoundment _ (check one)
Continuous
gpd 0 Intermittent
O Continuous
gpd 0 Intermittent
❑ Continuous
tr) gpd ❑ Intermittent
2 1.14 Is wastewater applied to land?
❑ Yes 0 No 4 SKIP to Item 1.16.
0 1.15 Provide the land a lication site and discharge data requested below.
Land Application Site and Discharge Data
oAverage Daily Volume Continuous or
Location Size A lied Intermittent
pp (check one)
ro acres d ❑ Continuous
o gip' 0 Intermittent
❑ Continuous
acres gpd 0 Intermittent
0
acres d El Continuous
gp 0 Intermittent
7, 1.16 Is effluent transported to another facility for treatment prior to discharge?
❑ Yes ❑✓ No 4 SKIP to Item 1.21.
1.17 Describe the means by which the effluent is transported(e.g.,tank truck,pipe).
1.18 Is the effluent transported by a party other than the applicant?
❑ Yes ❑ No 4 SKIP to Item 1.20.
1.19 Provide information on the transporter below.
Transporter Data
Entity name Mailing address(street or P.O.box)
City or town State ZIP code
Contact name(first and last) Title
Phone number Email address
EPA Form 3510-2A(Revised 3-19) Page 3

EPA Identification Number NPDES Permit Number Facility Name Form Approved 03/05/19
110012588280 NC0021253 City of Havelock WWTP OMB No.2040-0004
1.20 In the table below,indicate the name,address,contact information, NPDES number,and average daily flow rate of the
receiving facility. 1
Receiving Facility Data
13 d Facility name Mailing address(street or P.O.box)
City or town State ZIP code
0
U
u, Contact name(first and last) Title
0
-c
d Phone number Email address
m
o-
0 NPDES number of receiving facility(if any) 0 None
Average daily flow rate mgd
0 1.21 Is the wastewater disposed of in a manner other than those already mentioned in Items 1.14 through 1.21 that do not
8 have outlets to waters of the United States(e.g.,underground percolation,underground injection)?
CD
E"
03 ❑ Yes El No 4 SKIP to(tern 1.23.
a
0 1.22 Provide information in the table below on these other disposal methods.
d Information on Other Disposal Methods
o Disposal Location of Size of Annual Average Continuous or Intermittent
-a Method Disposal Site Disposal Site Daily Discharge (check one)
Description Volume
TO ❑ Continuous
3 acres gpd ❑ Intermittent
o 0 Continuous
acres gpd 0 Intermittent
acresgpd 0 Continuous
❑ Intermittent
1.23 Do you intend to request or renew one or more of the variances authorized at 40 CFR 122.21(n)?(Check all that apply.
(...1 0 Consult with your NPDES permitting authority to determine what information needs to be submitted and when.)
0 ❑ Discharges into marine waters(CWA ❑ Water quality related effluent limitation(CWA Section
Section 301(h)) 302(b)(2))
0 Not applicable
1.24 Are any operational or maintenance aspects(related to wastewater treatment and effluent quality)of the treatment works
the responsibility of a contractor?
0 Yes ❑ No-SKIP to Section 2.
1.25 Provide location and contact information for each contractor in addition to a description of the contractor's operational
and maintenance responsibilities.
Contractor Information
Contractor 1 Contractor 2 Contractor 3
o Contractor name
Lewis Farms Wilcox&Mabe Soil Solutions,I
E (company name)
Mailing address
(street or P.O.box) 8155 Malpass Corner Road 7231E Summerfield Road
`o City,state,and ZIP Currie,NC 28435 Summerfield,NC 27358
03 code
ci last) Candice name(first and Candice Wells Martin Mabe
Phone number [phone] [phone]
Email address [e-mail] [e-mail]
Operational and Remove and land apply Complete land application
maintenance biosolids to permitted sites. sludge reporting.
responsibilities of
contractor
EPA Form 3510-2A(Revised 3-19) Page 4

EPA Identification Number NPDES Permit Number Facility Name Form Approved 03/05/19
110012588280 NC0021253 City of Havelock WWTP OMB No.2040-0004
SECTION 2.ADDITIONAL INFORMATION(40 CFR 122.21(j)(1)and(2))
0 Outfalls to Waters of the United States
rn
2.1 Does the treatment works have a design flow greater than or equal to 0.1 mgd?
o ❑✓ Yes ❑ No 4 SKIP to Section 3.
c 2.2 Provide the treatment works'current average daily volume of inflow Average Daily Volume of Inflow and Infiltration
and infiltration. 208,000 gpd
Indicate the steps the facility is taking to minimize inflow and infiltration.
c The City of Havelock is maintaining ongoing efforts to identify and rehabilitate sources of I/I in their collection system.
Co
0
w
2.3 Have you attached a topographic map to this application that contains all the required information?(See instructions for
specific requirements.)
o Please reference Figure 1 for topographic
'o ❑.l Yes ❑ No map and Figure 2 for plant site map.
E 2.4 Have you attached a process flow diagram or schematic to this application that contains all the required information?
`° (See instructions for specific requirements.) Please reference Figure 3 through Figure 5 for
it c process flow diagram and the "Additional
❑ Yes ❑ No Information"sheets for process description.
2.5 Are improvements to the facility scheduled?
❑ Yes 0 No 4 SKIP to Section 3.
Briefly list and describe the scheduled improvements.
0
is 1.
U)
E
d
a 2.
CO 3.
d
4.
co
0
Co 2.6 Provide scheduled or actual dates of completion for improvements.
Scheduled or Actual Dates of Completion for Improvements
Affected Attainment of
d Scheduled Begin End Begin
> Outfalls Operational
a Improvement (list outfali Construction Construction Discharge Level
(from above) number) (MM/DDIYYYY) (MM/DD/YYYY) (MM/DD/YYYY) (MM/DD/YYYY)
1.
U 2.
U)
3.
4.
2.7 Have appropriate permits/clearances concerning other federal/state requirements been obtained?Briefly explain your
response.
D Yes ❑ No ❑ None required or applicable
Explanation:
EPA Form 3510-2A(Revised 3-19) Page 5

EPA Identification Number NPDES Permit Number Facility Name Form Approved 03/05/19
110012588280 NC0021253 City of Havelock WWTP OMB No.2040-0004
SECTION 3.INFORMATION ON EFFLUENT DISCHARGES(40 CFR 122.21(j)3)to(5))
3.1 Provide the following information for each outfall. (Attach additional sheets if you have more than three outfalls.)
Outfall Number 002 Outfall Number Outfall Number
State North Carolina
to76 County Craven
szi City or town City of Havelock
w
0
s Distance from shore 2,040 ft• ft. ft.
Q
Depth below surface 10 ft. ft. ft.
0
Average daily flow rate 1.33 mgd mgd mgd
Latitude 34° 57' 11" N
Longitude 76° 52' 37" W
CO
3.2 Do any of the outfalls described under Item 3.1 have seasonal or periodic discharges?
o ❑ Yes 0 No 4 SKIP to Item 3.4.
3.3 If so,provide the following information for each applicable outfall.
Outfall Number Outfall Number Outfall Number
Number of times per year
o discharge occurs
a Average duration of each
`o discharge(specify units)
Average flow of each
discharge mgd mgd mgd
Months in which discharge
occurs l_
3.4 Are any of the outfalls listed under(tern 3.1 equipped with a diffuser?
❑✓ Yes ❑ No 4 SKIP to Item 3.6.
3.5 Briefly describe the diffuser type at each applicable outfall.
0.
Outfall Number 002 Outfall Number Outfall Number
The effluent discharges into
the Neuse River through a
multi port diffuser located
approximately 2,040 feet
from the shoreline.
4-6
co' 3 6 Does the treatment works discharge or plan to discharge wastewater to waters of the United States from one or more
u) • discharge points?
15
ElYes ❑ No 4SKIP to Section 6.
EPA Form 3510-2A(Revised 3-19) Page 6

EPA Identification Number NPDES Permit Number Facility Name Form Approved 03/05/19
110012588280 NC0021253 City of Havelock WWTP OMB No.2040-0004
3.7 Provide the receiving water and related information(f known)for each outfall.
Outfall Number 002 Outfall Number Outfall Number
Receiving water name Neuse River
Name of watershed, river,
0 or stream system Neuse River
U.S.Soil Conservation
-L
y Service 14-digit watershed 03020204050020
o code
2. Name of state Neuse River
management/river basin
rn
c U.S. Geological Survey
a) 8-digit hydrologic 03020204
cc cataloging unit code
Critical low flow(acute) Unkown cfs cfs cfs
Critical low flow(chronic) Unkown cfs cfs cfs
Total hardness at critical mg/L of mg/L of mg/L of
low flow Unkown CaCO3 CaCO3 CaCO3
3.8 Provide the following information describin tc�he treatment provided for discharges from each outfall.
Outfall Number °02 Outfall Number Outfall Number
Highest Level of ❑ Primary 0 Primary 0 Primary
Treatment(check all that 0 Equivalent to 0 Equivalent to 0 Equivalent to
apply per outfall) secondary secondary secondary
0 Secondary 0 Secondary 0 Secondary
El Advanced 0 Advanced 0 Advanced
El Other(specify) ❑ Other(specify) 0 Other(specify)
c Denitrification filters
o
—
'Q Design Removal Rates by
.5 Outfall 002
u) -
d
in BOD5 or CBOD5 96 % % %
c
E
m TSS 84 % % 0/0
E-
❑ Not applicable 0 Not applicable 0 Not applicable
Phosphorus % °
78 °/o /o
❑ Not applicable 0 Not applicable 0 Not applicable
Nitrogen 91 % °/° %
Other(specify) ❑ Not applicable ❑ Not applicable 0 Not applicable
EPA Form 3510-2A(Revised 3-19) Page 7

EPA Identification Number NPDES Permit Number Facility Name Form Approved 03/05/19
110012588280 NC0021253 City of Havelock WWTP OMB No.2040-0004
3.9 Describe the type of disinfection used for the effluent from each outfall in the table below. If disinfection varies by
season,describe below.
-0
0
U
= Outfall Number 002 Outfall Number Outfall Number
0
a Disinfection type Ultraviolet Disinfection
U
to
i c Seasons used All seasons
d
E
Dechlorination used? ❑✓ Not applicable ❑ Not applicable ❑ Not applicable
❑ Yes ❑ Yes ❑ Yes
❑ No ❑ No ❑ No
3.10 Have you completed monitoring for all Table A parameters and attached the results to the application package?
0 Yes ❑ No
3.11 Have you conducted any WET tests during the 4.5 years prior to the date of the application on any of the facility's
discharges or on any receiving water near the discharge points?
❑✓ Yes El No 4 SKIP to Item 3.13.
3.12 Indicate the number of acute and chronic WET tests conducted since the last permit reissuance of the facility's
discharges by outfall number or of the receiving water near the discharge points.
Outfall Number 002 r Outfall Number Outfall Number
Acute 1 Chronic Acute Chronic Acute Chronic
Number of tests of discharge 0 14
water
Number of tests of receiving
water o 0
3.13 Does the treatment works have a design flow greater than or equal to 0.1 mgd?
❑✓ Yes ❑ No 4 SKIP to Item 3.16.
0 3.14 Does the POTW use chlorine for disinfection,use chlorine elsewhere in the treatment process,or otherwise have
= reasonable potential to discharge chlorine in its effluent?
El Yes Complete Table B,including chlorine. ElNo 4 Complete Table B,omitting chlorine.
CD
3.15 Have you completed monitoring for all applicable Table B pollutants and attached the results to this application
package?
0 Yes ❑ No
3.16 Does one or more of the following conditions apply?
• The facility has a design flow greater than or equal to 1 mgd.
• The POTW has an approved pretreatment program or is required to develop such a program.
• The NPDES permitting authority has informed the POTW that it must sample for the parameters in Table C,must
sample other additional parameters(Table D),or submit the results of WET tests for acute or chronic toxicity for
each of its discharge outfalls(Table E).
Yes 4 Complete Tables C, D,and E as
CI applicable. CINo 4 SKIP to Section 4.
3.17 Have you completed monitoring for all applicable Table C pollutants and attached the results to this application
package?
❑✓ Yes ❑ No
3.18 Have you completed monitoring for all applicable Table D pollutants required by your NPDES permitting authority and
attached the results to this application package?
❑ Yes ❑ No additional sampling required by NPDES
permitting authority.
EPA Form 3510-2A(Revised 3-19) Page 8

EPA Identification Number NPDES Permit Number Facility Name Form Approved 03/05/19
110012588280 NC0021253 City of Havelock WWTP OMB No.2040-0004
3.19 Has the POTW conducted either(1)minimum of four quarterly WET tests for one year preceding this permit application
or(2)at least four annual WET tests in the past 4.5 years?
❑ Yes 0 No+ Complete tests and Table E and SKIP to
Item 3.26.
3.20 Have you previously submitted the results of the above tests to your NPDES permitting authority?
El Yes ❑ No 4 Provide results in Table E and SKIP to
Item 3.26.
3.21 Indicate the dates the data were submitted to your NPDES permitting authority and provide a summary of the results.
Date(s)Submitted Summary of Results
(MM/DD/YYYY)
Second species toxicity tests pending.Part E will be revised and
submitted once second species toxicity results are received.All second
-oi species toxicity results will be submitted prior to the expiration of this
permit on June 30,2024.
.c
co 3.22 Regardless of how you provided your WET testing data to the NPDES permitting authority,did any of the tests result in
toxicity?
❑ Yes ❑✓ No 4 SKIP to Item 3.26.
w 3.23 Describe the cause(s)of the toxicity:
No chronic WET violations occurred with C.daphnia testing.Second species testing is pending.
3.24 Has the treatment works conducted a toxicity reduction evaluation?
❑ Yes ❑✓ No 4 SKIP to Item 3.26.
3.25 Provide details of any toxicity reduction evaluations conducted.
3.26 Have you completed Table E for all applicable outfalls and attached the results to the application package?
El Yes ❑✓ No-Second species toxicity tests pending.
SECTION 4.INDUSTRIAL DISCHARGES AND HAZARDOUS WASTES(40 CFR 122.21(j)(6)and(7))
4.1 Does the POTW receive discharges from SIUs or NSCIUs?
❑ Yes ❑✓ No 4 SKIP to Item 4.7.
4.2 Indicate the number of SIUs and NSCIUs that discharge to the POTW.
Number of SIUs Number of NSCIUs
0
7- 4.3 Does the POTW have an approved pretreatment program?
_ ❑ Yes El No
4.4 Have you submitted either of the following to the NPDES permitting authority that contains information substantially
identical to that required in Table F:(1)a pretreatment program annual report submitted within one year of the
application or(2)a pretreatment program?
❑ Yes ❑ No 4 SKIP to Item 4.6.
0
76 4.5 Identify the title and date of the annual report or pretreatment program referenced in Item 4.4.SKIP to Item 4.7.
-4
—
4.6 Have you completed and attached Table F to this application package?
❑ Yes ❑ No
EPA Form 3510-2A(Revised 3-19) Page 9

EPA Identification Number NPDES Permit Number Facility Name Form Approved 03/05/19
110012588280 NC0021253 City of Havelock WWTP OMB No.2040-0004
4.7 Does the POTW receive, or has it been notified that it will receive, by truck, rail, or dedicated pipe,any wastes that are
regulated as RCRA hazardous wastes pursuant to 40 CFR 261?
El Yes ❑ No 4 SKIP to Item 4.9.
4.8 If yes, provide the following information:
Annual
Hazardous Waste Waste Transport Method Amount of Units
Number (check all that apply) Waste
Received
❑ Truck ❑ Rail
❑ Dedicated pipe ❑ Other(specify)
0
C,)
❑ Truck El Rail
❑ Dedicated pipe ❑ Other(specify)
0
N ❑ Truck ❑ Rail
_ ❑ Dedicated pipe ❑ Other(specify)
4.9 Does the POTW receive,or has it been notified that it will receive,wastewaters that originate from remedial activities,
including those undertaken pursuant to CERCLA and Sections 3004(7)or 3008(h)of RCRA?
D Yes 0 No 4 SKIP to Section 5.
3 4.10 Does the POTW receive(or expect to receive)less than 15 kilograms per month of non-acute hazardous wastes as
specified in 40 CFR 261.30(d)and 261.33(e)?
❑ Yes 4 SKIP to Section 5. ❑ No
4.11 Have you reported the following information in an attachment to this application: identification and description of the
site(s)or facility(ies)at which the wastewater originates;the identities of the wastewater's hazardous constituents;and
the extent of treatment, if any,the wastewater receives or will receive before entering the POTW?
❑ Yes ❑ No
SECTION 5.COMBINED SEWER OVERFLOWS(40 CFR 122.21(j)(8))
5.1 Does the treatment works have a combined sewer system?
am ❑ Yes Cl No 4SKIP to Section 6.
-0 5.2 Have you attached a CSO system map to this application?(See instructions for map requirements.)
❑ Yes ❑ No
5.3 Have you attached a CSO system diagram to this application?(See instructions for diagram requirements.)
0 ❑ Yes ❑ No
EPA Form 3510-2A(Revised 3-19) Page 10

EPA Identification Number NPDES Permit Number Facility Name Form Approved 03/05/19
110012588280 NC0021253 City of Havelock WWTP OMB No.2040-0004
5.4 For each CSO outfall,provide the following information. (Attach additional sheets as necessary.)
CSO Outfall Number CSO Outfall Number CSO Outfall Number
City or town
0 —
• State and ZIP code
t.>
N
o County
�a —
11 ° , II , 1/= Latitude °
0
o ° , ° „
cn Longitude °
Distance from shore ft. ft. ft.
Depth below surface ft. ft. ft.
5.5 Did the POTW monitor any of the following items in the past year for its CSO outfalls?
CSO Outfall Number CSO Outfall Number CSO Outfall Number
Rainfall ❑ Yes ❑ No 0 Yes 0 No 0 Yes ❑ No
rn
c
.o CSO flow volume ❑ Yes ❑ No ❑ Yes ❑ No ❑ Yes ❑ No
CSO pollutant ❑ Yes 0 No ❑ Yes ❑ No ❑ Yes ❑ No
o concentrations
cn
cs Receiving water quality ❑ Yes 0 No ❑ Yes ❑ No ❑ Yes ❑ No
CSO frequency ❑ Yes ❑ No ❑ Yes ❑ No ❑ Yes ❑ No
Number of storm events ❑ Yes ❑ No ❑ Yes ❑ No ❑ Yes ❑ No
5.6 Provide the following information for each of your CSO outfalls.
CSO Outfall Number CSO Outfall Number CSO Outfall Number
CO
>- Number of CSO events in events events events
;, the past year
ea
= Average duration per hours hours hours
c event ❑Actual or❑ Estimated ❑Actual or El Estimated 0 Actual or❑ Estimated
d
>
u' million gallons million gallons million gallons
o Average volume per event
U 0 Actual or 0 Estimated ❑Actual or 0 Estimated ❑Actual or❑ Estimated
Minimum rainfall causing inches of rainfall inches of rainfall inches of rainfall
a CSO event in last year ❑Actual or❑ Estimated ❑Actual or❑ Estimated ❑Actual or❑ Estimated
EPA Form 3510-2A(Revised 3-19) Page 11

EPA Identification Number NPDES Permit Number Facility Name
Form Approved 03l05/19
110012588280
NC0021253 City of Havelock WWTP OMB No.2040-0004
5.7 Provide the information in the table below for each of your CSO outfalls.
CSO Outfall Number CSO Outfall Number CSO Outfall Number
Receiving water name
Name of watershed/
stream system
U.S. Soil Conservation 0 Unknown ❑ Unknown ❑Unknown
Service 14-digit
m watershed code
(if known)
Name of state
0
management/river basin
U.S.Geological Survey ❑Unknown ❑Unknown 0 Unknown
8-Digit Hydrologic Unit
Code(if known)
Description of known
water quality impacts on
receiving stream by CSO
(see instructions for
examples
SECTION 6.CHECKLIST AND CERTIFICATION STATEMENT(40 CFR 122.22(a)and(d))
6.1 In Column 1 below,mark the sections of Form 2A that you have completed and are submitting with your application.For
each section,specify in Column 2 any Y attachments that you are enclosing to alert the permitting authority.Note that not
all applicants are required to rovide attachments.
Column 1 Column 2
0 Section 1: Basic Application
Information for All Applicants ❑ wi variance request(s) X❑ w/additional attachments
❑ Section 2:Additional 0 w!topographic map ❑ w/process flow diagram
Information © w/additional attachments
0 w/Table A ❑ w/Table D
Ei Section 3: Information on
Effluent Discharges w!Table B ❑X w/Table E
❑X w/Table C ❑X w/additional attachments
Tu. Section 4: Industrial ❑ w/SiU and NSCIU attachments ❑ w/Table F
❑ Discharges and Hazardous
Wastes
R ❑ w/additional attachments
0 Section 5:Combined Sewer ❑ w!CSO map ❑ w/additional attachments
Overflows ❑ w/CSO system diagram
❑ Section 6: Checklist and
Certification Statement ❑ w/attachments
1-32 6.2 Certification Statement
d
I certify under penalty of law that this document and all attachments were prepared under my direction or supervision in
accordance with a system designed to assure that qualified personnel properly gather and evaluate the information
submitted. Based on my inquiry of the person or persons who manage the system,or those persons directly responsible
for gathering the information,the information submitted is,to the best of my knowledge and belief,true, accurate,and
complete. I am aware that there are significant penalties for submitting false information,including the possibility of fine
and imprisonment for.knowing violations.
Name(print or type first and last name) Official title
Rodney George ORC I Supervisor
Si Date signed
12/21/2023
EPA Form 3510-2A(Revised 3-19) Page 12

EPA Identification Number NPDES Permit Number Facility Name Outfall Number Form Approved 03/05/19
110012588280 NC0021253 City of Havelock WWTP 002 OMB No.2040-0004
TABLE A.EFFLUENT PARAMETERS FOR ALL POTWS
Maximum Daily Discharge Average Daily Discharge Analytical ML or MDL
Pollutant Number of Methods Include units)
Value Units Value Units Samples0 ML
(
Biochemical oxygen demand
❑BODE or 0 CBOD5 62 mg/L 4.32 mg/L 875 SM 5210E 2 mg/L E MDL
(report one)
ML
Enterococci 1300 MPN/100 mL 7.22 MPN/100 ml. 359 SM 9222D 1 MPN/100mLD MDL
Design flow rate 3.60 mgd 1.33 mgd 1,279 � ��
pH (minimum) 6.45 SU v •
• ',
pH(maximum) 8.60 SU
'
Temperature(winter) 23.8 "C 18.0 °C 302
Temperature(summer) 29.9 "C 24.3 "C 573
Total suspended solids(TSS) 5.50 mg/L O
2.52 mg/L 361 SM 2540D 2.5 mg/L ❑ML
MDL
1 Sampling shall be conducted according to sufficiently sensitive test procedures(i.e.,methods)approved under 40 CFR 136 for the analysis of pollutants or pollutant parameters or
required under 40 CFR chapter I,subchapter N or 0.See instructions and 40 CFR 122.21(e)(3).
Data from May 2020 through October 2023 included in analysis. Current permit became effective May 1, 2020.
EPA Form 3510-2A(Revised 3-19) Page 13

This page intentionally left blank.

EPA iuenuucation Number NPDES Permit Number Facility Name Outfall Number Form Approved 03/05/19
110012588280 NC0021253 City of Havelock WWTP 002 OMB No.2040-0004
TABLE B.EFFLUENT PARAMETERS FOR ALL POTWS WITH A FLOW EQUAL TO OR GREATER THAN 0.1 MGD
Maximum Daily Discharge Average Daily Discharge Analytical ML or MDL
Pollutant Number of Methods Include units
Value Units Value Units Samples Methods (
)
0 ML
Ammonia(as N) 0.93 mg/L 0.16 mg/L 360 EPA 350.1 0.04 mg/L t7 MDL
Chlorine ❑ML
(total residual,TRC)2 N/A N/A N/A N/A N/A N/A N/A ❑MDL
0 ML
Dissolved oxygen 19.6 mg/L 7.43 mg/L 873 SM 4500-H+B >5.0 mg/L l7 MDL
0 ML
Nitrate/nitrite 10.7 mg/L 2.24 mg/L 177 EPA 353.2 0.04 mg/L E MDL
ML
Kjeldahl nitrogen 2.10 mg/L 1.20 mg/L 178 EPA 351.2 0.3 mg/L ❑❑MDL
0 ML
Oil and grease <5 mg/L <5 mg/L 3 EPA 1664B 5.0 mg/L 2 MDL
0 ML
Phosphorus 5.38 mg/L 0.97 mg/L 178 EPA 365.4 1.0 mg/L ED MDL
0 ML
Total dissolved solids 1,100 mg/L 590 mg/L 3 SM 2340-C 1.0 mg/L O MDL
1 Sampling shall be conducted according to sufficiently sensitive test procedures(i.e., methods)approved under 40 CFR 136 for the analysis of pollutants or pollutant parameters or
required under 40 CFR chapter I,subchapter N or 0.See instructions and 40 CFR 122.21(e)(3).
2 Facilities that do not use chlorine for disinfection,do not use chlorine elsewhere in the treatment process, and have no reasonable potential to discharge chlorine in their effluent are not
required to report data for chlorine.
Notes:
1 . NC DENR DWR PQL reported for Total Kjeldahl Nitrogen as an alternative to laboratory specific MDL
2. Permit requires effluent DO concentration mg/L.
EPA Form 3510-2A(Revised 3-19) Page 15

This page intentionally left blank.

EPA Identification Number NPDES Permit Number Facility Name Outfall Number Form Approved 03/05/19
110012588280 NC0021253 City of Havelock WWTP 002 OMB No.2040-0004
TABLE C.EFFLUENT PARAMETERS FOR SELECTED POTWS
Maximum Daily Discharge Average Daily Discharge Analytical ML or MDL
Pollutant - -
Value Units Value Units Number of Method1 (include units)
Samples
Metals,Cyanide,and Total Phenols
0 ML
Hardness(as CaCO3) 108 mg/L 105 mg/L 3 SM 2340-C 1 mg/L 2 MDL
' • • • • µg/L 3 EPA 200.8 3/1 /L ❑ML
µg E l MDL
Arsenic, • • •• " i µg/L 3 SM 3113B-10 2 µg/L ❑ML
l7 MDL
total0 ML
• •• " µg/L 3 EPA 200.7 1 µg/L 2 MDL
Cadmium,total recoverable <0.5 µg/L <0.5 µg/L 3 SM 3113E-4 0.5 µ 2g/L ❑ML
MDL
Chromium,total recoverable <5.0 µg/L <5.0 µg/1. 3 EPA 200.7 5 /L ❑ML
µg 0 MDL
Copper,total recoverable 57 µg/L 9.6 µ µgg/L 17 EPA 200.7 2 /L ❑ML
O MDL
Lead,total recoverable <2.0 µg/L <2.0 µg/L 3 SM 3113B-10 2 µg/L ❑ML
l7 MDL
0 ML
Mercury,total recoverable 1.4 ng/L 0.80 ng/L 3 EPA 1631E 1.0 ng/L El MDL
Nickel,total recoverable 7.0 µg/L 3.3 µg/L 3 EPA 200.7 2 µg/L O❑ML
MDL
Selenium,total recoverable <1.0 µg/L <1.0 µg/L 3 EPA 200.8 1 kg• /L ❑ML
O MDL
Silver,total recoverable <1.0 i.tg/L <1.0 µg/L 3 EPA 200.7 1 µg/L ❑ML
2 MDL
Thallium,total recoverable <to µg/L <1.0 µg/L 3 EPA 200.8 1 µg/L ❑ML
0 MDL
Zinc,total recoverable 47.0 µg/L 40.7 µg/L 3 EPA 200.7 20 µg/L 0 ML
0 MDL
ML
Cyanide <0.005 mg/L <0.005 mg/L 3 SM 4500CNE-11 0.005 mg/L 0 MDL
ML
Total phenolic compounds 0.119 mg/L 0.046 mg/L 3 EPA 420.4 0.02 mg/L (3 MDL
Volatile Organic Compounds
Acrolein <100/<50 µg/L <100/<50 µg/L 3 EPA 624.1 100/50 /L❑ML
Ng l7 MDL
Acrylonitri!e <50 µg/L <50 µg/L 3 EPA 624.1 50 µg/L ❑ML
2 MDL
0 ML
Benzene I <5 µg/L <5 µg/L 3 EPA 624.1 5 µg/L E MDL
Bromoform I <5 µg/L <5 µg/L 3 EPA 624.1 0 ML
5 µg/L El MDL
Note:
1. Mercury data was reported incorrectly on DMRs with the units of ug/L. A review of the laboratory analytical reports confirmed

EPA ioentmcation Number NPDES Permit Number Facility Name Outfall Number Form Approved 03/05/19
110012588280 NC0021253 City of Havelock WWTP 002 OMB No.2040-0004
TABLE C.EFFLUENT PARAMETERS FOR SELECTED POTWS
Maximum Daily Discharge Average Daily Discharge Analytical ML or MDL
Pollutant Number of Method1 (include units)
Value Units Value Units Samples
Carbon tetrachloride <5 µg/L <5 µg/L 3 EPA 624.1 5
µg/L 0 ML
MDL
Chlorobenzene <5 µg/L <5 µg/L 3 EPA 624.1 5 /L ❑ML
µg O MDL_
Chlorodibromomethane <5 µg/L <5 µg/L 3 EPA 624.1 5 µg/L ❑ML
O MDL
Chloroethane <10 µg/L <10 RA3 EPA 624.1 10 µg/L ❑ML
0 MDL
2-chloroethylvinyl ether <5 µg/L <5 µg/L 3 EPA 624.1 5 /L ❑ML
µg 0 MDL
0 ML
Chloroform <5 µg/L <5 µg/L 3 EPA 624.1 5 µg/L 2 MDL
Dichlorobromomethane <5 µg/L <5 µg/L 3 EPA 624.1 5 µg/L ❑ML
0 MDL
1,1-dichloroethane <5 µg/L <5 µg/L 3 EPA 624.1 5 µg/L ❑ML
0 MDL
1,2-dichloroethane <5 µg/L <5 RA3 EPA 624.1 5 /L ❑ML
µg 0 MDL
trans-1,2-dichloroethylene <5 µg/L <5 p.g/L 3 EPA 624.1 5 /L ❑ML
µg MDL
1,1-dichloroethylene <5 µg/L <5 µg/L 3 EPA 624.1 5 µg/L ❑ML
1:1 MDL
1,2-dichloropropane <5 µg/L <5 µg/L 3 EPA 624.1 5 /L ❑ML
µg 0 MDL
1,3-dichloropropylene <5 pg/L <5 µg/L 3 EPA 624.1 5 µ g/L ❑ML
2 MDL
Ethylbenzene <5 RA <5 µg/L 3 EPA 624.1 5 µg/L 021 M MDD
L
Methyl bromide <10 µg/L <10 µg/L 3 EPA 624.1 10 µg/L ❑ML
O MDL
Methyl chloride <10 µg/L <10 µg/L 3 EPA 624.1 10 µg/L O ML
MDL
Methylene chloride <10 µg/L <10 µg/L 3 EPA 624.1 10 µg/L ❑ML
O MDL
0 ML
1,1,2,2-tetrachloroethane <5 µg/L <5 µg/L 3 EPA 624.1 5 µg/L 0 MDL
Tetrachloroethylene <5 µg/L <5 µg/L 3 EPA 624.1 5 µg/L ❑ML
.0 MDL
Toluene <5 RA <5 µg/L 3 EPA 624.1 5 µg/L 0 ML
I MDL
1,1,1-trichloroethane <5 µg/L <5 µg/L 3 EPA 624.1 5 µg/L ML
O MDL
1,1,2-trichloroethane <5 µg/L <5 µg/L 3 EPA 624.1 5 µg/L ML
l7 MDL
EPA Form 3510-2A(Revised 3-19) Page 18

EPA Identification Number NPDES Permit Number Facility Name Outfall Number Form Approved 03/05/19
110012588280 NC0021253 City of Havelock WWTP 002 OMB No.2040-0004
TABLE C.EFFLUENT PARAMETERS FOR SELECTED POTWS
Maximum Daily Discharge Average Daily Discharge 1
Analytical ML or MDL
Pollutant -- Number of Method1 (include units)
Value Units Value Units Samples
Trichloroethylene <5 µg/L <5 µ MA 3 EPA 624.1 5 /L ❑ML
El MDL
Vinyl chloride <10 µ µgg/L <10 µg/L 3 EPA 624.1 10 /L ❑ML
EMDL
Acid-Extractable Compounds
p-chloro-m-cresol <20 µg/L <20 µg/L 3 EPA 625.1 20 µg/L 0 ML
EMDL
2-chlorophenol <10 µg/L <10 µg/L 3 EPA 625.1 10 µg/L ❑ML
O MDL
0 ML
2,4-dichlorophenol <10 µg/L <10 µg/L 3 EPA 625.1 10 µg/L E MDL
2,4-dimethylphenol <10 µg/L <10 µg/L 3 EPA 625.1 10 µg/L ❑ML
E MDL
4,6-dinitro-o-cresol <50 µg/L <50 µg/L 3 EPA 625.1 50 µ g/L ❑ML
E MDL
2,4-dinitrophenol <50 µg/L <50 µg/L 3 EPA 625.1 50 µg/L 0 ML
E MDL
2-nitrophenol <10 µg/L <10 µg/L 3 EPA 625.1 10 µg/L ML
E MDL
0 ML
4-nitropheno! <50 µg/L <50 µg/L 3 EPA 625.1 50 µg/L E MDL
Pentachlorophenol <50 µg/L <50 µg/L 3 EPA 625.1 50 µg/L ❑ML
E MDL
—
0 ML
Phenol <10 µg/L <10 µg/L 3 EPA 625.1 10 µg/L E MDL
0 ML
2,4,6-trichlorophenol <10 µg/L <10 ug/L 3 EPA 625.1 10 µg/L E MDL
Base-Neutral Compounds
Acenaphthene <10 µg/L <10 µg µg
/L 3 ) EPA 625.1 10 /L ❑ML
E MDL
Acenaphthylene <10 µg/L <10 µg/L 3 EPA 625.1 10 µg/L ❑ML
E MDL
Anthracene <10 µg/L <10 µg/L 3 EPA 625.1 10 µg/L ❑ML
EMDL
Benzidine <100 HA <100 µg/L 3 EPA 625.1 100 µg/L ❑ML
E MDL
Benzo(a)anthracene <10 µg/L <10 µg/L 3 EPA 625.1 10 µg/L E ML
MDL
El ML
Benzo(a)pyrene <10 µg/L <10 µg/L 3 EPA 625.1 10 µg/L E MDL
0 ML
3,4-benzofluoranthene <10 µg/L <10 µg/L 3 EPA 625.1 10 µg/L E MDL
EPA Form 3510-2A(Revised 3-19) Page 19

EPA iaenuncation Number NPDES Permit Number Facility Name Outfall Number Form Approved 03/05/19
110012588280 NC0021253 City of Havelock WWTP 002 0MB No.2040-0004
TABLE C.EFFLUENT PARAMETERS FOR SELECTED POTWS
Maximum Daily Discharge Average Daily Discharge Analytical ML or MDL
Pollutant
Value Units Value Units Number of Method1 (include units)
Samples
Benzo(ghi)perylene <10 µg/L <10 µg/L 3 EPA 625.1 10 µg/L ❑ML
l7MDL _
Benzo(k)fluoranthene <10 µg/L <10 µpag/L 3 EPA 625.1 10 µ ❑ML
0 MDL
Bis(2-chloroethoxy)methane <10 µg/L <10 µg/L 3 EPA 625.1 10 µg/L ID ML
l7 MDL
Bis(2-chloroethyl)ether <10 µg/L <10 µg/L 3 EPA 625.1 10 /L El ML
µg l7 MDL
Bis(2-chloroisopropyl)ether <10 µg/L <10 RA3 EPA 625.1 10 µg/L ❑ML
❑MDL
Bis(2-ethylhexyl)phthalate <20 µg/L <20 µg/L 3 EPA 625.1 20 µg/L ❑ML
O MDL
4-bromophenyl phenyl ether <10 µg/L <10 µg/L 3 EPA 625.1 10 µg/L ❑ML
_ O MDL
0 ML
Butyl benzyl phthalate <10 µg/L <10 µg/L 3 EPA 625.1 10 µg/L 0 MDL
2-chloronaphthalene <10 µg/L <10 µg/L 3 EPA 625.1 10 µg/L ❑ML
l7 MDL
4-chlorophenyl phenyl ether <10 µg/L <10 µg/L 3 EPA 625.1 10 µg/L ❑ML
0 MDL
0 ML
Chrysene <10 µg/L <10 µg/L 3 EPA 625.1 10 µg/L O MDL
di-n-butyl phthalate <10 µg/L <10 µg/L 3 EPA 625.1 10 µg/L ❑ML
12 MDL
di-n-octyl phthalate <10 µg/L <10 µg/L 3 EPA 625.1 10 µg/L ❑ML
l7 MDL
Dibenzo(a,h)anthracene <10 µg/L <10 µg/L 3 EPA 625.1 10 µg/L ❑ML
o MDL
1,2-dichlorobenzene <10 µg/L <10 µg/L 3 EPA 625.1 10 µg/L ❑ML
l7 MDL
1,3-dichlorobenzene <10 µg/L <10 µg/L 3 EPA 625.1 10 µg/L ❑ML
tEl MDL
1,4-dichlorobenzene <10 µg/L <10 µg/L 3 EPA 625.1 10 µg/L ❑ML
Q MDL
3,3-dichlorobenzidine <10 µg/L <10 p.g/L 3 EPA 625.1 10 µg/L El ML
O MDL
Diethyl phthalate <10 µg/L <10 µg/L 3 EPA 625.1 10 µg/L ❑ML
O MDL
Dimethyl phthalate <10 µg/L <10 µg/L 3 EPA 625.1 10 µg/L ❑ML
o MDL
0 ML
2,4-dinitrotoluene <10 µg/L <10 µg/L 3 EPA 625.1 10 µg/L tEl MDL
o ML
2,6-dinitrotoluene <10 µg/L <10 µg/L 3 EPA 625.1 10 µg/L 0 MDL
EPA Form 3510-2A(Revised 3-19) Page 20

EPA Identification Number NPDES Permit Number Facility Name Outfall Number Form Approved 03/05/19
110012588280 NC0021253 City of Havelock WWTP 002 OMB No.2040-0004
TABLE C.EFFLUENT PARAMETERS FOR SELECTED POTWS
Maximum Daily Discharge Average Daily Discharge Analytical ML or MDL
Pollutant Number of Method1 (include units)
Value Units Value Units Samples
o ML
1,2-diphenylhydrazine <10 µg/L <10 µg/L 3 EPA 625.1 10 µg/L t l MDL
Fluoranthene <10 µg/L <10 µg/L 3 EPA 625.1 10 µg/L ML
O MDL
Fluorene <10 µg/L <10 RA3 EPA 625.1 10 µg/L 0 ML
2 MDL
Hexachlorobenzene <10 µg/L <10 RA3 EPA 625.1 10 µg/L 0 ML
O MDL
Hexachlorobutadiene <10 µg/L <10 p.g/L 3 EPA 625.1 10
µg/L 0 MDL
Hexachlorocyclo-pentadiene <10 µg/L <10 µg/L 3 EPA 625.1 10 µg/L ❑ML
O MDL
Hexachloroethane <10 µg/L <10 µg/L 3 EPA 625.1 10 µg/L DO M
O MDL
Indeno(1,2,3-cd)pyrene <10 µg/L <10 µg/L 3 EPA 625.1 10 µg/L 0 ML
_ l MDL
Isophorone <10 µg/L <10 µg/L 3 EPA 625.1 10 µg/L 0 ML
OMDL0 ML
_
Naphthalene <10 µg/L <10 µg/L 3 EPA 625.1 10 µg/L El MDL
Nitrobenzene <10 ❑ML
µg/l. <10 µg/L 3 EPA 625.1 10
µB/L O MDL
N-nitrosodi-n-propylamine <10 µg/L <10 µg/L 3 EPA 625.1 10 µg/L 2 ML O MDL
N-nitrosodimethylamine <10 µg/L <10 µg/L 3 EPA 625.1 10 /L 0 ML
µg O MDL
0 ML
N-nitrosodiphenylamine <10 µg/L <10 µg/L 3 EPA 625.1 10 µg/L t]MDL
Phenanthrene <10 µg/L <10 µg/L 3 EPA 625.1 10 /L l ML
µg E MDL
Pyrene <10 µg/L <10 µg/L 3 EPA 625.1 10 µg/L 0 ML 0 MDL
1,2,4-trichlorobenzene <10 µg/L <10 µg/L 3 EPA 625.1 10 µg/L 0 ML
O MDL
1 Sampling shall be conducted according to sufficiently sensitive test procedures(i.e.,methods)approved under 40 CFR 136 for the analysis of pollutants or pollutant parameters or
required under 40 CFR Chapter I,Subchapter N or 0.See instructions and 40 CFR 122.21(e)(3).
EPA Form 3510-2A(Revised 3-19) Page 21

This page intentionally left blank.

EPA Identification Number NPDES Permit Number Facility Name Outfall Number Form Approved 03/05/19
110012588280 NC0021253 City of Havelock WWTP 002 OMB No.2040-0004
TABLE D.ADDITIONAL POLLUTANTS AS REQUIRED BY NPDES PERMITTING AUTHORITY
Maximum Daily Discharge Average Daily Dischar e
Pollutant — Analytical ML or MDL
Number of
(list) Value Units Value Units Methods (include units)
Samples
❑ No additional sampling is required by NPDES permitting authority.
❑ML
❑MDL
❑ML
❑MDL
❑ML
❑MDL
❑ML
❑MDL
❑ML
❑MDL
❑ML
❑MDL
❑ML
❑MDL
❑ML
_ ❑MDL
❑ML
❑MDL
❑ML
CI MDL
❑ML
❑MDL
❑ML
❑MDL
ML
❑MDL
❑ML
❑MDL
❑ML
_ _ ❑MDL
❑ML
❑MDL
❑ML
❑MDL
1 Sampling shall be conducted according to sufficiently sensitive test procedures(i.e.,methods)approved under 40 CFR 136 for the analysis of pollutants or pollutant parameters or required
under 40 CFR chapter I,subchapter N or 0.See instructions and 40 CFR 122.21(e)(3).
EPA Form 3510-2A(Revised 3-19) Page 23

This page intentionally left blank.

EPA Identification Number NPDES Permit Number Facility Name Outfall Number Form Approved 03/05/19
110012588280 NC0021253 City of Havelock WWTP 002 OMB No.2040-0004
TABLE E.EFFLUENT MONITORING FOR WHOLE EFFLUENT TOXICITY
The table provides response space for one whole effluent toxicity sample.Copy the table to report additional test results.
Test Information
Test Number Test Number Test Number
Test species
Age at initiation of test
Outfall number Second species toxicity tests pending. Part E will be revised and
Date sample collected submitted once second species toxicity results are received. All
Date test started second species toxicity results will be submitted prior to the
Duration expiration of this permit on June 30, 2024.
i
Toxicity Test Methods
Test method number
Manual title
Edition number and year of publication
Page number(s)
Sample Type
Check one: ❑ Grab ❑ Grab ❑ Grab
❑ 24-hour composite ❑ 24-hour composite ❑ 24-hour composite
Sample Location
Check one: ❑ Before Disinfection ❑ Before Disinfection ❑ Before disinfection
❑ After Disinfection ❑ After Disinfection ❑ After disinfection
❑ After Dechlorination ❑ After Dechlorination ❑ After dechlorination
Point in Treatment Process
Describe the point in the treatment process
at which the sample was collected for each
test.
Toxicity Type
Indicate for each test whether the test was ❑ Acute I ❑ Acute ❑ Acute
performed to asses acute or chronic toxicity,
or both.(Check one response.) ❑ Chronic El Chronic El Chronic
❑ Both ❑ Both ❑ Both
EPA Form 3510-2A(Revised 3-19) Page 25

EPA Identification Number NPDES Permit Number Facility Name Outfall Number Form Approved 03/05/19
110012588280 NC00212.53 City of Havelock WWTP 002 OMB No.2040-0004
TABLE E.EFFLUENT MONITORING FOR WHOLE EFFLUENT TOXICITY
The table provides response space for one whole effluent toxicity sample. Copy the table to report additional test results.
Test Number Test Number Test Number
Test Type
Indicate the type of test performed.(Check one ❑ Static ❑ Static ❑ Static
response.)
❑ Static-renewal ❑ Static-renewal ❑ Static-renewal
❑ Flow-through ❑ Flow-through ❑ Flow-through
Source of Dilution Water
Indicate the source of dilution water.(Check ❑ Laboratory water ❑ Laboratory water 0 Laboratory water
one response.)
❑ Receiving water ❑ Receiving water ❑ Receiving water
If laboratory water, specify type.
If receiving water, specify source.
Type of Dilution Water _
Indicate the type of dilution water. If salt ❑ Fresh water ❑ Fresh water � ❑ Fresh water
water, specify"natural"or type of artificial ,—,
sea salts or brine used. t J Salt water(specify) CISalt water(specify) CISalt water(specify)
Percentage Effluent Used
Specify the percentage effluent used for all
concentrations in the test series.
Parameters Tested
Check the parameters tested. ❑ pH ❑ Ammonia ❑ pH ❑ Ammonia ❑ pH ❑ Ammonia
❑ Salinity ❑ Dissolved oxygen El Salinity ❑ Dissolved oxygen ❑ Salinity ❑ Dissolved oxygen
❑ Temperature ❑ Temperature I ❑ Temperature
Acute Test Results
Percent survival in 100%effluent % % %
LCso
95%confidence interval % % %
Control percent survival
EPA Form 3510-2A(Revised 3-19) Page 26

EPA Identification Number NPDES Permit Number Facility Name Outfall Number Form Approved 03/05/19
110012588280 NC0021253 City of Havelock WWTP 002 OMB No.2040-0004
TABLE E.EFFLUENT MONITORING FOR WHOLE EFFLUENT TOXICITY
The table provides response space for one whole effluent toxicity sample.Copy the table to report additional test results.
Test Number Test Number Test Number
Acute Test Results Continued _
Other(describe)
Chronic Test Results
NOEL
I C 2 5
Control percent survival
Other(describe)
Quality ControllQuality Assurance
Is reference toxicant data available? ❑ Yes ❑ No ❑ Yes ❑ No ❑ Yes ❑ No
Was reference toxicant test within
acceptable bounds? ElYes 0 No ElYes ❑ No 0 Yes 0 No
What date was reference toxicant test run
(MM/DD/YYYY)?
Other(describe)
EPA Form 3510-2A(Revised 3-19) Page 27

This page intentionally left blank.

EPA Identification Number NPDES Permit Number Facility Name Form Approved 03/05/19
110012588280 NC0021253 City of Havelock WWTP OMB No.2040-0004
TABLE F.INDUSTRIAL DISCHARGE INFORMATION
Response space is provided for three SIUs.Copy the table to report information for additional Sills.
SIU__ SIU SIU
Name of SIU
Mailing address(street or P.O.box)
City,state,and ZIP code
Description of all industrial processes that affect
or contribute to the discharge.
List the principal products and raw materials that
affect or contribute to the SIU's discharge.
Indicate the average daily volume of wastewater
discharged by the SIU. gpd gpd gpd
How much of the average daily volume is
attributable to process flow? gpd gpd gpd
How much of the average daily volume is
attributable to non-process flow? gpd gpd gpd
Is the SIU subject to local limits?
❑ Yes ❑ No ❑ Yes ❑ No ❑ Yes ❑ No
Is the SIU subject to categorical standards?
I ❑ Yes ❑ No ❑ Yes ❑ No ❑ Yes ❑ No
EPA Form 3510-2A(Revised 3-19) Page 29

trH identification Number NPDES Permit Number Facility Name Form Approved 03/05/19
110012588280 NC0021253 City of Havelock WWTP OMB No.2040-0004
TABLE F.INDUSTRIAL DISCHARGE INFORMATION
Response space is provided for three SIUs.Copy the table to report information for additional SIUs.
SIU SIU SIU
Under what categories and subcategories is the
SIU subject?
Has the POTW experienced problems(e.g.,
upsets,pass-through interferences)in the past 4.5 ❑ Yes 0 No ❑ Yes ❑ No ❑ Yes ❑ No
years that are attributable to the SIU? _
If yes,describe.
EPA Form 3510-2A(Revised 3-19) Page 30

Tab B
EPA Form 2A Additional Information
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t-';
, ' Constructed as Part of Phase 1 of WWTP Expansion
Lat 34° 57' 11" t,
Long 76° 52'37"
` -- T om.. .4
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Influent Force Mains N �,r+oRn ,,klr
Figure 1
Gravity Interceptors '`
W E _ - `
WWTP Location Map
24-inch Effluent Pipe
f azen City of Havelock, NC
USA To po Maps s NC0021253
0 02 0.4 0.8 2.3 of Form 2A
Miles ��''HIUN sr,0/

BOWER —
BUILDING
N0.2
CHEMICAL STORAGE
AND FEED FACILITY FINAL CLARIFIER
MAINTENANCE PUMPING STATION
BUILDING — COARSE BUBBLE STABILIZED SOLIDS
�______.,_._____. COARSE BUBBLE AERATION BASINS HOLDING BASIN
AERATION BASIN NO.182
NO.3
v
ii /*
❑ I O
J FILTER BACKWASH
WASTE DETENTION BASIN
DENITRIFICATION SOLIDS
FILTERS HANDLING
FINAL CLARIFIER WASTE SOLIDS HOLDING TANK BUILDING
NO.2
L
FINAL CLARIFIER J WAS CONTROL STATION O
FLOW DISTRIBUTION
VISTRUCTURE RAS CONTROL i k FINE BUBBLE
�111t'lllll'�III'r///////// STATION ■ AERATION BASIN NO.2
III SLUDGE
■ UV PUMPING
DISINFECTION STATION
AERATION BASIN BASIN
DISTRIBUTION BOX
.11
FINAL CLARIFIERNO.1 ■ -�
.
CONTROL BUILDING I F
REAERATION
BASIN
FINE BUBBLE
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�\ —El 111 El
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ENGINE- \ �J 0 EFFLUENT
TRANSFORMER GENERATOR I0 INFLUENT PUMPING STATION
BUILDING PUMPING STATIONS
BAR SCREEN ~J 1 GRIT REM
AND GRIT
REMOVAL
(BYPASS UNIT) BAR
SCREEN Figure 2
WWTP Site Map
City of Havelock, NC
NC0021253
3DBU8-012 Figure 2.odr 2.3 of Form 2A

Legend
FBW =Filter Backwash
FBWR =Filter Backwash Return
RAS =Return Activated Sludge
WAS =Waste Activated Sludge
TWAS =Thickened Waste Activated
Sludge
El =Flow Meter
Q=2.25 mgd Q=3.55 mgd
Grit
// /// �
Aeration Basin
Removal
Plant Influent ♦ / —
Bar Screens — ► - I Distribution O. IN- — ►
/ / / / / Box cyj l�fr
Fine Bubble Coarse Bubble
Influent Pump Aeration Basins Aeration Basins Final Clarifier
Stations Pump Station
RAS (?=1.13 mgd
Grit FBWR
Polyaluminum
Q=0.15 mgd Methanol Chloride
FBW Waste Q=2.4 mgd - r— Q=3.55 mgd
Reaeration Detention Basin
Tank _
r
o`er. —t-- MAK" _ — Final Distribution4
ClarifiersNrez Box
Cascade Effluent Pump UV Disinfection Denitrification�r
Aerator Station FBW Q=0.15 mgci Filters
-- Q=1.15 mgd
Ily Q=0.02 mgd Polymer
Diffuser in il 1 If 4-104— "
Neuse River
Stabilized TWAS Pumps Gravity Belt GBT Feed Pump Waste Solids WAS Control RAS Control
Solids Holding Thickener Holding Tank Station Station
Basin Q=0.01 mgd Q=0.03 mgd
V
Truck Hauling Figure 3
41 to Land Application WWTP Process Flow Diagram:
Permitted Capacity of 2.25 mgd
City of Havelock, NC
NC0021253
2.4 of Form 2A
30906-012 Figure 3.cdr

Legend
FBW =Filter Backwash
FBWR =Filter Backwash Return
RAS =Return Activated Sludge
WAS =Waste Activated Sludge
TWAS =Thickened Waste Activated
Sludge
M =Flow Meter
Q=2.8 mgd Q=4.4 mgd
rrocr
Grit
Removal J////
Plant Influent / ° ° Q ° °
g ♦ Bar Screens ► —* _ °b� c° ° c ti °tt o Q Q
\\\ v 2rA Influent Pump* `• r' ' Final Clarifier
Stations 3 Stage BNR Basin Pump Station
RAS Q=1.4 mgd
ill.
Grit FBWR 1ml Polyaluminum
Q=0.2 mgd Methanol Chloride
Q=2.8 mgd Q=2.8 mgd FBW Waste
Reaeration Detention Basin Q=3.0 mgd Q=4.4 mgd
Tank
. 4 M — 4--- 4 — Final 4 - Distribution
11111."" 1 Clarifiers Box
Cascade Effluent Pump UV Disinfection Denitrification \\ V
Aerator Station FBW 0=0 2 mgd Filters
- Q=1.4 mgd
• Q=0.024 mgd Polymer
0 fsl
Diffuser in
EQ EU 1 ,:? ED
4—killl-- lio.41 M 4 11,
Neuse River - , —
Stabilized TWAS Pumps Gravity Belt GBT Feed Pump Waste Solids WAS Control RAS Control
Solids Holding Thickener Holding Tank Station Station
Basin Q=0.014 mgd Q=0.038 mgd
Q=0.038 mgd Q=1.4 mgd
V
I.11_ Truck Hauling Figure 4
to Land Application WWTP Process Flow Diagram:
Permitted Capacity of 2.8 mgd
City of Havelock, NC
NC0021253
2.4 of Form 2A
30906-01 2 Figure 3 cdr

Legend
FBW =Filter Backwash
FBWR =Filter Backwash Return
RAS =Return Activated Sludge
WAS =Waste Activated Sludge
TWAS =Thickened Waste Activated
Sludge
El =Flow Meter
Q=3.5 mgd Q=5.5 mgd
NRCy
Grit
J// J// Removal ° c. ° o
Plant Influent V/B
ar Screens i 0 6° ° °°° eoa •R o--- -_►
C1=3.S mgd ar / /n ,\^Jr nsrowc ' ••Rt.
NZ /A Influent Pump* 'P t •t a L~ •~ Final Clarifier
Stations 5 Stage BNR Basin Pump Station
RAS Q=1.75 mgd
Illi
Grit FBWR iml Polyaluminum
Q=0.25 mgd Chloride
Methanol
Q=3.5 mgd - Q=3.5 mgd FBW Waste Q=3.75 mgd - r Q=5.5 mgd
Reaeration Detention Basin
Tank
,r FM-- — ♦- t Final 1--- Distribution i
,",..i,_`: NClarifiers Box
Cascade Effluent Pump UV Disinfection ADenitrification
Aerator Station FBW Q=0.25 mad Filters
Q=1.8 mgd
♦ Q=0.03 mgd Polymer
'
SjV vVI
v
v - � f t — � M a A M
Diffuser in
Neuse River - -
Stabilized TWAS Pumps i Gravity Belt GBT Feed Pump Waste Solids WAS Control RAS Control
Solids Holding i Thickener Holding Tank Station Station
Basin Q=0.02 mgd Q=0.05 mgd
Q=0.05 mgd — — Q=1.75 mgd
V
1[111- �I Truck Hauling Figure 5
n
`J I to Land Application WWTP Process Flow Diagram:
Permitted Capacity of 3.5 mgd
City of Havelock, NC
NC0021253
2.4 of Form 2A
30906-012 Figure 3.cdr -

City of Havelock WWTP
Permit No. NC0021253
Outfall 002
Additional Information
B.2 Topographic Map
See Figure 1 for topographic map and Figure 2 for a plant site map.
B.3.1 Process Flow Description — Permitted Capacity of 2.25 mgd
The Havelock WWTP provides advanced wastewater treatment, including
nitrogen removal, to meet effluent limits for discharge to the Neuse River. The
major processes at the WWTP include screening, grit removal, a single-stage
nitrification activated sludge process, denitrification filters, ultraviolet
disinfection, re-aeration, gravity belt thickening, and stabilized solids storage.
As part of the Phase 1 WWTP expansion, completed in May 2015, an effluent
pump station, an outfall pipeline, a cascade aerator, and a diffuser in the Neuse
River were constructed.
Screening
Influent wastewater is conveyed to the Havelock WWTP by a combination of
gravity interceptors and force mains. The influent flow is combined into a 24-
inch pipeline at the screening facility that passes through a bar screen designed
to remove large solids and debris from the influent wastewater to prevent
clogging and interference with operation of downstream pumps and other
process equipment.
Grit Removal
After passing through the bar screen, the influent wastewater flows to a vortex
(Pista) grit collector through a 24-inch pipe. After the grit is removed, the grit
collector effluent flows to the influent pump stations.
Influent Pump Stations
The Havelock WWTP is equipped with two influent pump stations. Effluent from
the grit removal facility flows through an 18-inch pipe to a tee with a 20-inch
pipe. The 20-inch pipe interconnects two wet wells, which are used in
combination with pumps to convey the influent wastewater to the aeration
basins. Each influent pump station is comprised of a wet well and three influent
pumps. One influent pump station contains three submersible pumps. The
second influent pump station is a dry pit/wet pit configuration with three pumps.
All pumps are controlled via float switches in the wet well to keep pace with the
1

City of Havelock WWTP
Permit No. NC0021253
Outfall 002
plant influent flow rate. In addition to raw wastewater, return activated sludge
(RAS) from the secondary treatment stage is returned to the influent pump
station for conveyance to the aeration basin distribution box. Flow from the
influent pump stations are conveyed through 10-inch and 12-inch pipes to the
aeration basin distribution box.
Activated Sludge System
The Y
purpose ur of the activated sludge system is to achieve the BOD removal,
P P g
phosphorus removal, and nitrification necessary to comply with the stringent
effluent requirements in the permit. The activated sludge system includes fine
and coarse bubble aeration basins, intermediate pumping, final clarifier
distribution box, final clarifiers, and RAS and waste activated sludge (WAS)
conveyance.
Fine Bubble Aeration
Wastewater enters the fine bubble aeration basins mixed with RAS through a
distribution box. Two sharp-crested weirs split the flow equally between two
aeration basins. The two circular tanks are equipped with a fine bubble aeration
system with ceramic disc diffusers. The diffusers provide the dissolved oxygen
and mixing necessary for operation of the activated sludge process.
Coarse Bubble Aeration
The mixed liquor from each of the fine bubble aeration basins flows through 16-
inch pipes to the coarse bubble aeration basins for additional BOD removal
and/or nitrification. The three coarse bubble aeration basins are operated in
series in normal operation and are equipped with a coarse bubble aeration
system.
Final Clarifier Pump Station
Effluent from the second-stage aeration basin flows by gravity to the final
clarifier pump station wet well via 16-inch piping. The Final Clarifier Pump
Station lifts the mixed liquor to a high enough elevation that the wastewater can
flow by gravity through the rest of the treatment plant. A 20-inch pipe conveys
the pumped flow from the final clarifier pump station to the final clarifier
distribution box. A polyaluminum chloride (PACT) storage and feed system is
provided to feed PACI to the Final Clarifier Pump Station discharge to enhance
suspended solids removal and provide phosphorus removal in the final
clarifiers via precipitation.
2

City of Havelock WWTP
Permit No. NC0021253
Outfal! 002
Final Clarifiers
Two 65-foot diameter clarifiers are provided to settle out solids from the mixed
liquor. The final clarifiers provide quiescent flow conditions to allow the mixed
liquor solids to settle to the bottom of the clarifiers. The settled solids are either
returned to the first-stage aeration basins as RAS or wasted to the Waste
Solids Holding Tank as WAS. The clarified effluent flows over the final clarifier
effluent V-notch weirs to the denitrification filters, where the wastewater
undergoes further treatment.
RAS and WAS Conveyance
The RAS and WAS Control Stations control the flow rate of settled activated
sludge from the final clarifiers to the influent pump stations and the Waste
Solids Holding Tank, respectively. WAS flows to the Waste Solids Holding
Tank, and from there is periodically pumped to the gravity belt thickeners for
thickening prior to stabilization and ultimate disposal. The RAS and WAS flows
are measured by four strap-on ultrasonic flow meters, with one RAS flow meter
and one WAS flow meter for each clarifier. RAS and WAS are conveyed by gravity
and manually-operated pinch valves downstream of the flow meters are used to
control the flow rates.
Denitrification Filters
The denitrification filters remove additional suspended solids from the final clarifier
effluent and remove nitrogen through denitrification to comply with the total
nitrogen limit. Final clarifier effluent flows by gravity to three denitrification filters.
An underdrain system collects the filtered wastewater and directs it to a 20-inch
pipe that flows by gravity to the disinfection facilities. The Havelock WWTP uses
methanol as its carbon source, and typically adds between 40 and 80 gallons
per day to the filters. Backwash water is drained to the Filter Backwash Waste
Detention Basin, and from there is returned to the influent pump stations.
Ultraviolet Disinfection
Disinfection is accomplished using ultraviolet (UV) disinfection technology.
Filtered wastewater effluent enters the UV disinfection facilities through a 16-
inch and 20-inch parallel pipeline. The old chlorine contact tank was retrofitted
to accommodate the UV modules and now serves as the disinfection channel.
3

City of Havelock WWTP
Permit No. NC0021253
Outfall 002
Re-aeration
The re-aeration facilities are located at the Re-aeration Basin and can be used
to provide additional dissolved oxygen in the UV disinfection effluent. Two
platform-mounted mechanical surface aerators are provided in the Re-aeration
Basin. The backwash supply pumps for the denitrification filters are also located
in the Re-aeration Basin.
Effluent Pump Station
The effluent pump station conveys flow through approximately 30,000 linear
feet of 24-inch piping to the Neuse River.
Cascade Aerator
Prior to discharging into the Neuse River, the effluent passes through a
cascade aerator. The cascade aerator is boated near the bank of the Neuse
River and increases the effluent's dissolved oxygen levels to meet permit
requirements.
Diffuser in the Neuse River
After passing through the cascade aerator, the effluent discharges into the
Neuse River through a multi port diffuser located approximately 2,040 feet from
the shoreline.
Please reference Figure 3 for the process flow diagram at a permitted
capacity of 2.25 mgd.
B.3.2 Process Flow Description — Future Permitted Flow Capacity of 2.8 mgd
The process flow at a permitted capacity of 2.8 mgd will be the same as at
2.25 mgd, with the exception that the Activated Sludge system will be
upgraded to a 3-Stage BNR basin to meet nutrient limits.
Please reference Figure 4 for the process flow diagram at a permitted
capacity of 2.8 mgd.
4

City of Havelock WWTP
Permit No. NC0021253
Outfall 002
B.3.3 Process Flow Description — Future Permitted Flow Capacity of 3.5 mgd
The process flow at a permitted capacity of 3.5 mgd will be the same as at
2.25 mgd, with the exception that the Activated Sludge system will be
upgraded to a 5-Stage BNR basin to meet nutrient limits.
Please reference Figure 5 for theprocess flow diagram at a permitted
9 9
capacity of 3.5 mgd.
5

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City of Havelock WWTP Sludge `°
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Solids Treatment
Solids in the form of WAS from the Havelock WWTP currently undergo further treatment
for eventual disposal as a land application product. The existing solids processing
facilities include thickening, WAS holding tank, one 1-meter gravity belt thickener (GBT),
polymer feed system, GBT feed pumps, thickened WAS (TWAS) feed pumps, and a
stabilized solids holding basin.
The solids thickening process is designed to reduce the volume of WAS from the activated
sludge process. WAS is removed from the final clarifiers and drained by gravity to the
Waste Solids Holding Tank for short-term storage prior to thickening. Each clarifier has
a separate wasting line and pinch valve in the WAS Control Station for controlling WAS
flow to the Waste Solids Holding Tank. Flow meters in the WAS Control Station indicate
WAS flow rate for each final clarifier. Submersible pumps are provided in the Waste
Solids Holding Tank for pumping WAS to the gravity belt thickeners in the Solids Handling
Building. Chemical conditioning of the solids with polymer is provided to separate the
flocculated solids from the free water. The thickened waste activated sludge (TWAS)
from the GBT is collected in a thickened solids hopper, from which it is pumped to the
Solids Stabilization Tank by two TWAS pumps. Free water is drained back to the Influent
Pump Station.
The stabilized solids holding basin is used to store thickened stabilized solids prior to
liquid land application on permitted privately-owned farmland. Piping is provided for
withdrawal of solids from the holding basin and to load the solids into a truck. Decanting
of supernatant to the influent pump stations is also possible using a portable pump.

NORTH CAROLINA
ENVIRONMENTAL MANAGEMENT COMMISSION
DEPARTMENT OF ENVIRONMENT AND NATURAL RESOURCES
RALEIGH
LAND APPLICATION OF CLASS B WASTEWATER TREATMENT PLANT RESIDUALS
PERMIT(NON-DEDICATED)
In accordance with the provisions of Article 21 of Chapter 143, General Statutes of North Carolina as
amended,and other applicable Laws, Rules,and Regulations
PERMISSION IS HEREBY GRANTED TO
City of Havelock
Craven County
FOR THE
continued operation of a residuals management program for the City of Havelock and consisting of the
land application of Class B Wastewater Treatment Plant residuals generated by the approved facilities
listed in Attachment A to the approved sites listed in Attachment B with no discharge of wastes to surface
waters, pursuant to the application received January 20, 2015, and in conformity with other supporting
data subsequently filed and approved by the Department of Environment and Natural Resources and
considered a part of this permit. The use and disposal of residuals arc regulated under Title 40 Code of
Federal Regulations Part 503. This permit does not exempt the Permittee from complying with the federal
regulations.
This permit shall be effective from the date of issuance until March 31, 2017, shall void Permit No.
WQ0000702 issued April 7, 2008, and shall be subject to the following specified conditions and
1 imitations:
SCHEDULES
1. No later than six months prior to the expiration of this permit, the Permittee shall request renewal of
this permit on official Division forms. Upon receipt of the request, the Division will review the
adequacy of the facilities described therein, and if warranted, will renew the permit for such period of
time and under such conditions and limitations as it may deem appropriate. Please note Rule 15A
NCAC 02T .0105(d) requires an updated site map to be submitted with the permit renewal
application. [15A NCAC 02T .0108(b)(2),02T.105(d),02T.01091
2. The Permittee shall be in full compliance with the regional office notification requirements
established in Condition 11I.3. within 90 days of the effective date of this permit. [15A NCAC 02T
.01 08(b)(2)]
3. The Permittee shall submit the Operation and Maintenance (O&M) plan as required in Condition
II1.4. to the Division within 90 days of the effective date of this permit. [15A NCAC 02T
.0108(b)(2)]
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4. The Permittee shall be in full compliance with the signage requirements established in Condition
111.13. within 180 days of the effective date of this permit. [15A NCAC 02T.0108(b)(2)]
11. PERFORMANCE STANDARDS
1. The subject residuals management program shall be effectively maintained and operated at all times
so there is no discharge to surface waters, nor any contravention of groundwater or surface water
standards. In the event the facilities fail to perform satisfactorily, including the creation of nuisance
conditions due to improper operation and maintenance, the Permittee shall immediately cease land
applying residuals to the site, contact the Washington regional office supervisor, and take any
immediate corrective actions. [G.S. 143-215.1]
2. This permit shall not relieve the Permittee of responsibility for damages to groundwater or surface
water resulting from the operation of this residuals management program. [15A NCAC 02B .0200,
02L .0100]
3. Only residuals generated by the facilities listed in Attachment A are approved for land application in
accordance with this permit. [G.S. 143-215.1]
4. Only the sites listed in Attachment B are approved for residuals land application. [G.S. 143-215.1]
5. Pollutant concentrations in residuals applied to land application sites listed in Attachment B shall not
exceed the following Ceiling Concentrations (i.e., dry weight basis) or Cumulative Pollutant
Loading Rates(CPLRs): •
Parameter Ceiling Concentration CPLR •
(milligrams per kilogram) (pounds per acre)
Arsenic 75 36
Cadmium 85 34
Copper 4,300 1,338
Lead 840 267
Mercury 57 15
Molybdenum 75 n/a
Nickel 420 374
Selenium 100 89
Zinc 7,500 2,498
The Permittee shall determine compliance with the CPLRs using one of the following methods:
a. By calculating the existing cumulative level of pollutants using actual analytical data from all
historical land application events of residuals,or
b. For land where residuals application have not occurred or for which the required data is
incomplete,by determining background concentrations through representative soil sampling.
[15A NCAC 02T .1105]
6. Residuals that are land applied shall meet Class B pathogen reduction requirements in 15A NCAC
02T .1106 (a) and (c). Exceptions to this requirement shall be specified in Attachment A. [15A
NCAC 02T .1106]
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7. Biological residuals (i.e. residuals generated during the treatment of domestic or animal processing
wastewa
ter,
ter, or the biological treatment of industrial wastewater, and as identified in Attachment A)
that are land applied shall meet one of the vector attraction reduction alternatives in I 5A NCAC 02T
.1107(a). Exceptions to this requirement shall be specified in Attachment A. [15A NCAC 02T
.1107]
8. Setbacks for Class B land application sites shall be as follows:
Setback by application type
(feet)
Setback Description Vehicular Irrigation
Surface Surface Injection/
Application Application Incorporation
Habitable residence or place of public assembly
under separate ownership or not to he maintained as 400 400 200
part of the project site
Habitable residence or places of public assembly
owned by the Permittee,the owner of the land,or the 0 200 0
lessee/operator of the land to be maintained as part
of the project site
Property lines 50 150 50
Public right of way 50 50 50
Private or public water supply 100 100 100
Surface waters(streams—intermittent and perennial, 100 100 50
perennial waterbodies,and wetlands)
Surface water diversions(ephemeral streams, 25 100 25
waterways,ditches)
Groundwater lowering ditches(where the bottom of 25 100 25
the ditch intersects the SHWT)
Subsurface groundwater lowering system 0 100 0
Wells with exception to monitoring wells 100 100 100
Bedrock outcrops 25 25 25
Top of slope of embankments or cuts of two feet or 15 15 15
more in vertical height
Building foundations or basements 0 15 0
Water lines 0 10 0
Swim ing pools 100 100 100
Nitrification fields 0 20 0
[15A NCAC 02T.1108]
9. Land application areas shall be clearly marked on each site prior to and during any residuals
application event. [15A NCAC 02T.0108(b)(I)]
10. Bulk residuals and other sources of Plant Available Nitrogen (PAN) shall not be applied in
exceedance of agronomic rates. Appropriate agronomic rates shall be calculated using expected
nitrogen requirements based on the determined Realistic Yield Expectations (RYE) using any of the
following methods:
a. Division's pre-approved site specific historical data for specific crop or soil types by calculating
the mean of the best three yields of the last five consecutive crop harvests for each field.

b. North Carolina Historical Data for specific crop and soil types as provided by North Carolina
State University Department of Soil Science (http://nutrients.soil.ncsu.edu/yields/index.php).
A copy shall be kept on file and reprinted every five years in accordance with Condition IV.5.
c. If the RYE cannot be determined using methods (a) or(b) above, the Permittee may use the RYE
and appropriate nutrient application rates reported in any of the following documents:
i. Crop management plan as outlined by the local Cooperative Extension Office, the North
Carolina Department of Agriculture and Consumer Services, the Natural Resource
Conservation Service,or other agronomist.
ii. Waste Utilization Plan as outlined by the Senate Bill 1217 interagency Group - Guidance
Document: Chapter 1
(http://www.ncagr.gov/SWC/tech/documents/9th Guidance Doc 100109.pdf).
iii. Certified Nutrient Management Plan as outlined by the Natural Resources Conservation
Services (NRCS). These plans must meet the USDA-NRCS 590 Nutrient Management
Standards(ftp://ftp-fc.sc.egov.usda.gov/NHQ/practice-standards/standards/590.pdf).
d. If the RYE and appropriate nutrient application rates cannot be determined, the Permittee shall
contact the Division to determine necessary action.
[15A NCAC 02T.1109(b)(1)(k)]
11. When residuals are land applied to grazed pasture, hay crop realistic nitrogen rate shall be reduced by
25% in accordance with the USDA-NRCS 590 Nutrient Management Standards. [15A NCAC 02T
.0108(b)(1)]
12. If land application sites are to be over-seeded or double-cropped (e.g., bermuda grass in the summer
and rye grass in the winter with both crops to receive residuals), then the second crop can receive an
application of PAN at a rate not to exceed 50 pounds per acre per year(lbs/ac/yr). This practice may
be allowed as long as the second crop is to be harvested or grazed. If the second crop is to be planted
for erosion control only and is to be tilled into the soil, then no additional PAN shall be applied. [15A
NCAC 02T .0108(b)(1)]
13. Prior to land application of residuals containing a sodium adsorption ratio (SAR) of 10 or higher, the
Permittee shall obtain and implement recommendations from at least one of the following: the local
Cooperative Extension Office; the Department of Agriculture and Consumer Services; the Natural
Resource Conservation Service; a North Carolina Licensed Soil Scientist; or an agronomist. The
recommendations shall address the sodium application rate,soil amendments (e.g., gypsum, etc.),or a
mechanism for maintaining site integrity and conditions conducive to crop growth. The Permittee
shall maintain written records of these recommendations and details of their implementation. [15A
NCAC 02T .0108(b)(1)]
14. These residuals land application sites were individually permitted on or after December 30, 1983;
therefore, the compliance boundary is established at either 250 feet from the residual land application
area, or 50 feet within the property boundary, whichever is closest to the residual land application
area. An exceedance of groundwater standards at or beyond the compliance boundary is subject to
remediation action according to 15A NCAC 02L .0106(d) (2) as well as enforcement actions in
accordance with North Carolina General Statute 143-215.6A through 143-215.6C, Any approved
relocation of the COMPLIANCE BOUNDARY will be noted in Attachment B. [15A NCAC 02L
.0107(a)]
15. The review boundary shall be established midway between the compliance boundary and the residual
land application area. Any exceedance of groundwater standards at the review boundary shall require
action in accordance with 15A NCAC 02L .0106. [15A NCAC 02L.0108]
weinnnn1m ch..11 Vc.rcinn I cn I n 1 PROP 4 of 17

IIi. OPERATION AND MAINTENANCE REQUIREMENTS
1. The residuals management program shall be properly maintained and operated at all times. The
program shall be effectively maintained and operated as a non-discharge system to prevent any
contravention of surface water or groundwater standards. [15A NCAC 02T.1110]
2. The Washington Regional Office, telephone number [phone], and the appropriate local
government official (i.e., county manager, city manager, or health director) shall be notified at least
48 hours prior to the initial residuals land application to any new land application site. Notification to
the regional supervisor shall be made from 8:00 a.m. until 5:00 p.m. on Monday through Friday,
excluding State Holidays. [15A NCAC 02T .0108(b)(1)]
3. The Washington Regional Office shall be notified via email or telephone, [phone], at least 24
hours prior to conducting any land application activity, Such notification shall indicate, at a
minimum, the anticipated application times, field IDs, and location of land application activities. If it
becomes necessary to apply to additional fields due to unforeseen events, the Regional Office shall be
notified prior to commencing the application to those fields. [15A NCAC 02'T.0108(b)(1)]
4. The Permittee shall maintain an approved Operation and Maintenance Plan (O&M Plan)
Modifications to the O&M Plan shall be approved by the Division prior to utilization of the new plan.
The O&M Plan,at the minimum, shall include:
a. Operational functions;
b. Maintenance schedules;
c. Safety measures;
d. Spill response plan;
e. Inspection plan including the following information:
i. Names and/or titles of personnel responsible for conducting the inspections;
ii. Frequency and location of inspections, including those to be conducted by the ORC, and
procedures to assure that the selected location(s) and inspection frequency are representative
of the residuals management program;
iii. Detailed description of inspection procedures including record keeping and actions to be
taken by the inspector in the event that noncompliance is observed pursuant to the
noncompliance notification requirements under the monitoring and reporting section of the
permit;
f. Sampling and monitoring plan including the following information:
i. Names and/or titles of personnel responsible for conducting the sampling and monitoring;
ii. Detailed description of monitoring procedures including parameters to be monitored;
iii. Sampling frequency and procedures to assure that representative samples are being collected.
Fluctuation in temperature, flow, and other operating conditions can affect the quality of the
residuals gathered during a particular sampling event. The sampling plan shall account for
any foreseen fluctuations in residuals quality and indicate the most limiting times for
residuals to meet pathogen and vector attraction reduction requirements (e.g. facilities that
land apply multiple times per year but have an annual sampling frequency, may need to
. sample during winter months when pathogen reduction is most likely to be negatively
affected by cold temperatures).
[15A NCAC 02T .1100]
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5. Upon the Water Pollution Control System Operators Certification Commission's (WPCSOCC)
classification of the facility, the Permittee shall designate and employ a certified operator in
responsible charge (ORC) and one or more certified operators as back-up ORCs in accordance with
15A NCAC 08G .0201. The ORC or his back-up shall visit the facilities in accordance with 15A
NCAC 08G. 0204, or as specified in the most recently approved O&M plan (i.e., see Condition
III.4.), and shall comply with all other conditions of I5A NCAC 08G. 0204. For more information
regarding classification and designation requirements, please contact the Division of Water
Resources'Protection and Enforcement Branch at(919) 707-9105. [15A NCAC 02T.0117]
6. When the Permittee land applies bulk residuals, a copy of this permit and a copy of O&M Plan shall
be maintained at the land application sites during land application activities. [15A NCAC 02T
.0108(b)(1)]
7. When the Permittee transports or land applies bulk residuals, the spill control provisions shall be
maintained in all residuals transport and application vehicles. [15A NCAC 02T.1110]
8. Residuals shall not be stored at any land application site, unless written approval has been requested
and received from the Division. [G.S. 143-215.1]
9. When the Permittee land applies bulk residuals, adequate measures shall be taken to prevent wind
erosion and surface runoff from conveying residuals from the land application sites onto adjacent
properties or into surface waters. [G.S. 143-215.1]
10. When the Permittee land applies bulk residuals, a suitable vegetative cover shall be maintained on
land application sites onto which residuals are applied, or application shall be in accordance with the
crop management plan outlined by the local Cooperative Extension Office, the Department of
Agriculture and Consumer Services, the Natural Resource Conservation Service, or an agronomist
and as approved by the Division. [15A NCAC 02T.1109(b)(1)]
1 1. Bulk re
siduals shall not be land applied under the following conditions;
a. If the residuals are likely to adversely affect a threatened or endangered species listed under
section 4 of the Endangered Species Act or its designated critical habitat;
b. If the application causes prolonged nuisance conditions;
c. If the land fails to assimilate the bulk residuals or the application causes the contravention of
surface water or groundwater standards;
d. If the land is flooded, frozen or snow-covered, or is otherwise in a condition such that runoff of
the residuals would occur;
e. Within the 100-year flood elevation, unless the bulk residuals are injected or incorporated within
a 24-hour period following a residuals land application event;
f. During a measurable precipitation event (i.e., greater than 0.01 inch per hour), or within 24 hours
following a rainfall event of 0.5 inches or greater in a 24-hour period;
g. If the slope is greater than 10% for surface applied liquid residuals, or if the slope is greater than
18% for injected or incorporated bulk liquid residuals;
h. If the soil pH is not maintained at 6.0 or greater, unless sufficient amounts of lime are applied to
achieve a final soil pH of at least 6.0, or if an agronomist provides information indicating that the
pH of the soil, residuals and lime mixture is suitable for the specified crop. Any approved
variations to the acceptable soil pH (6.0)will be noted in this permit;
i. If the land does not have an established vegetative cover unless the residuals are incorporated or
injected within a 24-hour period following a residuals land application event. Any field that is in
a USDA no-till program shall be exempted from meeting this vegetative cover requirement;
WQ0000702 Version 3.2 shpt i ;n I n 1 r

j. If the vertical separation between the seasonal high water table and the depth of residuals
application is less than one foot;
k. If the vertical separation of bedrock and the depth of residuals application is less than one foot;
I. Application exceeds agronomic rates.
[l5A NCAC 02T.1109]
12. The following public access restrictions apply to residual land application sites:
a. Public access to public contact sites(e.g., golf courses,parks,ball fields, etc.)shall be restricted
for 365 days after a residuals land application event;
b. Public access to non-public contact sites shall be restricted for 30 days after a residuals land
application event.
[15A NCAC 02T.l 109(b)(2)]
13. Public access controls shall include the posting of signs with a minimum area of 3 square feet (e.g.,
1.5' x 2'). Each sign shall indicate the activities conducted at each site,permit number, and name and
contact information, including the Permittee or applicator's telephone number. Signs shall be posted
in a clearly visible and conspicuous manner at the entrance to each land application site during a land
application event, and for as long as the public access restrictions required under Condition 1II.12.
apply. [15A NCAC 02T .0108(b)(l)]
14. The following harvesting and grazing restrictions apply to residual land application sites after each
land application event:
I
Harvesting and Grazing Description Kestrieted
Duration
Animals shall not be allowed to graze during land application activities and
restricted period. Sites that are to be used for grazing shall have fencing to 30 days
prevent access after each land application event.
Food crops, feed crops and fiber crops shall not be harvested for: 30 days
Turf grown on land where residuals have been applied shall not be harvested for: 12 months
Food crops with harvested parts that touch the residual/soil mixture and are
totally above the land surface(e.g.,tobacco, melons, cucumbers, squash, etc.) l4 months
shall not be harvested for:
When the residuals remain on the land surface for four months or longer prior to
incorporation into the soil, food crops with harvested parts below the land
surface(e.g., root crops such as potatoes,carrots; radishes, etc.)shall not be 20 months
harvested for:
When the residuals remain on the land surface for less than four months prior to
incorporation into the soil,food crops with harvested parts below the land 38 months
surface shall not be harvested for:
[15A NCAC 02T .1109(b)(3)]
15. The Permittee shall acquire from each landowner or lessee/operator a statement detailing the volume
of other nutrient sources (i.e., manufactured fertilizers, manures, or other animal waste products) that
have been applied to the site, and a copy of the most recent Nutrient Management Plan (NMP) for
those operations where a NMP is required by the US Department of Agriculture—National Resources
Conservation Service (NRCS) or other State Agencies. The Permittee shall calculate allowable
nutrient loading rates based on the provided information and use appropriate reductions.
WQ0000702 Version 3.2 Shell VPrsin„ 1 in 1 n 1 n_... _yin

For the purpose of this permit condition, a Crop Management Plan (CMP), Waste Utilization Plan
(WUP) or Certified Nutrient Management Plan (CNMP) shall also be considered a Nutrient
Management Plan. [15A NCAC 02T .0108(b) (1), 02T.1104(c)(4)]
16. No residuals shall be land applied unless the submitted Land Owner Agreement Attachment (LOAA)
between the Permittee and landowners or lessees/operators of the land application site is in full force
and effect. These agreements shall be considered expired concurrent with the permit expiration date,
and shall be renewed during the permit renewal process. [15A NCAC 02T .1 104(c)(4)]
IV. MONITORING ANI)REPORTING REQUIREMENTS
1. Any Division required monitoring (including groundwater, plant tissue, soil and surface water
analyses) necessary to ensure groundwater and surface water protection shall be established, and an
acceptable sample reporting schedule shall be followed. [15A NCAC 02T.0108(c)]
2. Residuals shall be analyzed to demonstrate they are non-hazardous under the Resource Conservation
and Recovery Act (RCRA). Residuals that tests or is classified as a hazardous or toxic waste
under 40 CFR Part 261 shall not be used or disposed under this permit. The analyses
[corrosivity,ignitability, reactivity, and toxicity characteristic leaching procedure (TCLP)] shall
be performed at the frequency specified in Attachment A, and the Permittee shall maintain these
results for a minimum of five years. Any exceptions from the requirements in this condition shall be
specified in Attachment A.
The TCLP analysis shall include the following parameters (the regulatory level in milligrams per liter
is in parentheses):
Arsenic(5.0) 1,4-Dichlorobenzene(7.5) Nitrobenzene(2.0)
Barium(100.0) _ 1,2-Dichloroethane(0.5) Pentachlorophenol (100.0)
Benzene(0.5) 1,1-•Dichloroethylene(0.7) Pyridine(5.0)
Cadmium(1.0) 2,4-Dinitrotoluene(0.13) Selenium(1.0)
Carbon tetrachloride(0.5) Endrin(0.02) Silver(5.0)
Chlordane(0.03) Hexachlorobenzene(0.13) Tetrachloroethylene(0.7)
Chlorobenzene I OOA Heptachlor(and its hydroxide)
( ) (0.008) Toxaphene(0.5)
Chloroform(6.0) Hexachloro-1,3-butadiene(0.5) Trichloroethylene(0.5)
Chromium(5,0) 1-lexachloroethane(3.0) 2,4,5-Trichlorophenol(400.0)
m-Cresol (200.0) Lead(5.0) 2,4,6-Trichlorophenol (2.0)
o-Cresol(200.0) Lindane(0.4) 2,4,5-TP(Silvex) (1.0)
p-Cresol(200.0) Mercury(0.2) Vinyl chloride(0.2)
Cresol (200.0) Methoxychlor(10.0)
2,4-D(10.0) Methyl ethyl ketone(200.0)
Once the residuals have been monitored for two years at the frequency specified in Attachment A, the
Permittee may submit a permit modification request to reduce the frequency of this monitoring
requirement. In no case shall the monitoring frequency be less than once per permit cycle.
[15A NCAC 1 3A .0102(b),02T.1101,02T .1105]
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3. An analysis shall be conducted on residuals from each source generating facility at the frequency
• specified in Attachment A, and the Permittee shall maintain the results for a minimum of five years.
The analysis shall include the following parameters:
Aluminum Mercury Potassium
Ammonia-Nitrogen Molybdenum Selenium
Arsenic Nickel Sodium
Cadmium Nitrate-Nitrite Nitrogen Sodium Adsorption Ratio
(SAR)
Calcium Percent Total Solids TKN
Copper pH Zinc
Lead Phosphorus
Magnesium Plant Available Nitrogen
(by calculation)
[15A NCAC 02T.1101]
4. Residuals shall be monitored for compliance with pathogen and vector attraction reduction
requirements at the frequency specified in Attachment A, and at the time indicated in the sampling
and monitoring sections of the approved O&M plan. The required data shall be specific to the
stabilization process utilized, and sufficient to demonstrate compliance with the Class B pathogen
reduction requirements in 15A NCAC 02T .1106 (a) and (c), and one vector attraction reduction
requirement in 15A NCAC 02T .1107 (a) shall be met. Any exceptions from the requirements in this
condition shall be specified in Attachment A. [15A NCAC 02T.1106,02T.1107,02T.1111(c)]
5. An annual representative soils analysis (i.e., Standard Soil Fertility Analysis) shall be conducted on
each land application site listed in Attachment B on which a residuals land application event will
occur in the respective calendar year. This analysis shall be in accordance with the"Guidance on Soil
Sampling" located in the Sampling Instructions section of the NC Department of Agriculture &
Consumer Services' website (http://www.ncagr gov/agronomi/pubs.htm). The Permittee shall
maintain these results and a description of the sampling methodologies used to determine soil fertility
for a period of no less than five years, and shall be made available to the Division upon request. At a
minimum,the Stan
dard nd Soil Fertility Analysis si shall include the followingparameters:
Acidity Exchangeable Sodium Percentage Pho_photus
Base Saturation(by calculation) Magnesium Potassium
Calcium Manganese Sodium
r
Cation Exchange Capacity Percent Hunuc Matter Zinc
Copper pH
[15A NCAC 02T.1111(d)]
6. Laboratory parameter analyses shall be performed on the residuals as they are land applied, and shall
be in accordance with the monitoring requirements in 15A NCAC 02B .0505. [15A NCAC 02B
.0505]
\xrnnnnrrmr»\Ar,•;,.,, 1 1 CM ni o n..r i,1

7. The Permittee shall maintain records tracking all residual land application events. At a minimum,
these records shall include the following:
• a. Source of residuals;
b. Date of land application;
c. Location of land application(i.e., site, field,or zone number as listed in Attachment B);
d. Approximate areas applied to(acres);
e. Method of land application;
f. Weather conditions (e.g.,sunny,cloudy,raining, etc.);
g. Predominant Soil Mapping Unit(e.g.,CbB2);
h. Soil conditions(e.g.,dry, wet,frozen, etc.);
i. Type of crop or crops to be grown on field;
j. Nitrogen Application Rate based on RYEs (if using data obtained from the North Carolina State
University Department of Soil Science Website, the printout page shall be kept on file and
reprinted every five years);
k. Volume of residuals land applied in gallons per acre, cubic yard per acre,thy tons per acre,or wet
ton per acre;
1. Volume of animal waste or other nutrient source applied in gallons per acre, dry ton per acre, or
wet tons per acre;
in. Volume of soil amendments (e.g., lime, gypsum, etc.) applied in gallons per acre, dry ton per
acre, or wet tons per acre;and
n. Annual and cumulative totals in dry tons per acre of residuals as well as animal waste and other
sources of nutrients (e.g., if applicable), annual and cumulative pounds per acre of each heavy
metal (e.g., shall include, but shall not be limited to, arsenic, cadmium, copper, lead, mercury,
molybdenum, nickel, selenium,and zinc), annual pounds per acre of PAN,and annual pounds per
acre of h p o.phorus applied to each field.
[15A NCAC 02T .0109(a)]
8. Three copies of an annual report shall be submitted on or before March 1". The annual report shall
meet the requirements described in the Instructions for Residuals Application Annual Reporting
Forms. Instructions for reporting and annual report forms are available at
http://portal.nedenr.org/web/wq/aps/lau/reporting, or can be obtained by contacting the Land
Application Unit directly. The annual report shall be submitted to the following address:
Division of Water Resources
Information Processing Unit
1617 Mail Service Center
Raleigh,North Carolina 27699-1617
[15A NCAC 02T.111.1(a)]
9. Noncompliance Notification
The Permittee shall report by telephone to the Washington Regional Office, telephone number (252)
946-6481, as soon as possible, but in no case more than 24 hours or on the next working day
following the occurrence or first knowledge of the occurrence of any of the following:
a. Land application of residuals abnormal in quantity or characteristic.
b. Any failure of the land application program resulting in a release of material to surface waters.
WQ0000702 Version 3.2 Shell Veccinn 1 6(11 n 1 n.,,,e 11

c. Any time self-monitoring indicates the facility has gone out of compliance with its permit
limitations.
d. Any process unit failure, due to known or unknown reasons, rendering the facility incapable of
adequate residual treatment.
e. Any spill or discharge from a vehicle or piping system during residuals transportation.
Any emergency requiring immediate reporting(e.g., discharges to surface waters, imminent failure of
a storage structure, etc.) outside normal business hours shall be reported to the Division's Emergency
Response personnel at telephone number(800)662-7956, [phone], or(919) 733-3300.Persons
reporting such occurrences by telephone shall also file a written report in letter form within five days
following first knowledge of the occurrence. This report shall outline the actions taken or proposed to
be taken to ensure that the problem does not recur. [15A NCAC 02T .0105(1),02T.0108(b)(1)]
V. INSPECTIONS
1. The Permittee shall provide adequate inspection and maintenance to ensure proper operation of the
subject facilities and shall be in accordance with the approved O&M Plan. [15A NCAC 02T
.0108(b)]
2. Prior to each bulk residuals land application event, the Permittee or his designee shall inspect the
residuals transport and application facilities to prevent malfunctions, facility deterioration and
operator errors resulting in discharges, which may cause the release of wastes to the environment, a
threat to human health or a public nuisance. The Permittee shall maintain an inspection log that
includes, at a minimum, the date and time of inspection, observations made, and any maintenance,
repairs, or corrective actions taken. The Permittee shall maintain this inspection log for a period of
five years from the date of inspection, and this log shall be made available to the Division upon
request. [15A NCAC 02T .0108(b)]
3. Any duly authorized Division representative may, upon presentation of credentials, enter and inspect
any property,premises or place on or related to the land application sites or facilities permitted herein
at any reasonable time for the purpose of determining compliance with this permit; may inspect or
copy any records required to be maintained under the terms and conditions of this permit; and may
collect groundwater,surface water or leachate samples. [G.S. 143-215.3(a)(2)]
VI. GENERAL CONDITIONS
1. Failure to comply with the conditions and limitations contained herein may subject the Permittee to
an enforcement action by the Division in accordance with North Carolina General Statutes 143-
215.6A to 143-215.6C. [G.S. 143-215.6A to 143-215.6C]
2. This permit shall become voidable if the residuals land application events are not carried out in
accordance with the conditions of this permit. [15A NCAC 02T .0110]
3. This permit is effective only with respect to the nature and volume of residuals described in the
permit application and other supporting documentation. [G.S. 143-215.1]
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4. The issuance of this permit does not exempt the Permittee from complying with any and all statutes,
rules, regulations, or ordinances, which may be imposed by other jurisdictional government agencies
(e.g., local, state, and federal). Of particular concern to the Division are applicable river buffer rules
in 15A NCAC 02B .0200; erosion and sedimentation control requirements in 15A NCAC Chapter 4
and under the Division's General Permit NCG010000; any requirements pertaining to wetlands under
15A NCAC 02B .0200 and 02H .0500; and documentation of compliance with Article 21 Part 6 of
Chapter 143 of the General Statutes. [15A NCAC 02T .0105(c)(6)]
5. In the event the residuals program changes ownership or the Permittee changes his name, a formal
permit modification request shall be submitted to the Division. This request shall be made on official
Division forms, and shall include appropriate documentation from the parties involved and other
supporting documentation as necessary. The Permittee of record shall remain fully responsible for
maintaining and operating the residuals program permitted herein until a permit is issued to the new
owner. [15A NCAC 02T .0104]
6. This permit is subject to revocation or unilateral modification upon 60 days notice from the Division
Director, in whole or part for the requirements listed in 15A NCAC 02T .0110. [15A NCAC 02T
.0110]
7. Unless the Division Director grants a variance, expansion of the permitted residuals program
contained herein shall not be granted if the Permittee exemplifies any of the criteria in 15A NCAC
02T.0120(b). [15A NCAC 02T.0120]
8. The Permittee shall pay the annual fee within 30 days after being billed by the Division. Failure to
pay the annual fee accordingly shall be cause for the Division to revoke this permit. [15A NCAC 02T
.0105(e)(3)]
Permit issued this the 24th day of March 2015
NORTH CAROLINA ENVIRONMENTAL MANAGEMENT COMMISSION
o .Jay uimerman,Director
ivision of Water Resources
By Authority of the Environmental Management Commission
Permit Number WQ0000702
WQ0000702 Version 3.2 Shell Version 150101 Pan 12 of 12

ATTACHMENT A-Approved Residual Sources Certification Date: March 24,2015
CITY OF HAVELOCK Permit Number: WQ0000702 Version: 3.2
Approved
Monitoring Monitoring
Monitoring Mineralization
Maximum Frequency for Rate
Owner Facility Name County Permit Biological DryTons Frequency for Frequency for
Number Residuals Non-hazardous Metals and Pathogen& [Raw=0.4;
Per Year 3,; Vector Attraction Aerobic=0.3;
Characteristics- Nutrients
Reductions a'' Anaerobic=0 2;
Compost=0.I)
City of Havelock Havelock WWTP Craven NC0021253 Yes 415 Annually See Table Below See Table Below** 0.3
Total 415
I. Maximum Dry Tons per Year is the amount of residuals approved for land application from each permitted facility.
2. Analyses to demonstrate that residuals are non-hazardous(i.e.,TCLP,ignitability,reactivity,and corrosivity)as stipulated under permit Condition IV.2.
3. Testing of metals and nutrients as stipulated under permit Condition 1 V.3.
4. Analyses of pathogen and vector attraction reductions as stipulated under permit Condition IV.4.
5. Monitoring frequencies are based on the actual dry tons applied per year using the table below,unless specified above.
Dry Tons Generated Monitoring Frequency
(short tons per year) (Established in 40 CFR 503 and I5A NCAC 02T.1111)
<319 I./Year
=>319-<I,650 I/Quarter(4 times per year)
=>1,650-<16,500 1/60 Days(6 times per year)
=>16.500 I/month(12 times per year)
If no land application events occur during a required sampling period(e.g.no land application occur during an entire year when annual monitoring is required),then no
sampling data is required during the period of inactivity.The annual report shall include an explanation for missing sampling data.Those required to submit the annual
report to EPA may be required to make up the missed sampling,contact the EPA for additional information and clarification.
WQ0000702 Version 3.2 Attachment A Page I of 1

THIS PAGE BLANK

ATTACHMENT B-Approved Land Application Sites Certification Date: March 24,2015
CITY OF HAVELOCK Permit Number: WQ0000702 Version: 3.2
Net
Field/Site Owner Lessee _ County Latitude Longitude Acreage Dominant Soil Series Footnotes
NC-CV-1-1 Al Campbell. Robert G. McCoy,Charles Myron Craven 35'12'39- 77'25'06- 8.90 Pa-Pantego fine sandy loam
NC-CV-I-1 B Campbell,Robert C. McCoy.Charles Myron Craven 35'12'38' 77"25'06' 7.00 Pa--Pantego tine sandy loam
NC-CV-I-ICI Campbell, Robert C. McCoy,Charles Myron Craven 35'12'31- 7725'09- 12.90 Pa-Pantego tine sandy loam
NC-CV-I-1 D Campbell. Robert G. McCoy.Charles Myron Craven 35'12'32- 77'25'15' 31.20 Pa-Pantego tine sandy loam
NC-CV-1-I E Campbell, Robert G. McCoy,Charles Myron Craven 35'12'32- 77'25'I8' 16.40 ; Pa Pantego tine sandy loam
r '
NC-CV-I-IG Campbell, Robert G. McCoy,Charles Myron Craven 35°12'20- 77°25'02- 9.40 Pa- Pantego One sandy loam
NC-CV-1-I H Campbell. Robert G. McCoy,Charles Myron Craven 35°12'12" 77'25'07- 26.00 Pa-Pantego tine sandy loam
NC-CV-I-2A Campbell, Robert G. j McCoy,Charles Myron Craven 35°12'20" 77'25'39- 13.50 Pa- Pantego fine sandy loam
NC-CV-1-2A Campbell. Robert G. McCoy,Charles Myron Craven 35°l2'10- 77°25'23- 5.50 Pa-Pantego tine sandy loam
Total Pr C.'ouny 130.8
NC-PA-2-IA Spencer Farms. Inc. Pamlico 35'09'56' 76'49';r" 10.18 Yo-Yon_esloamyfinesand
NC-PA-2-1 B Spencer Farms, Inc. Pamlico 35°09'55- 76°49'28- 9.71 Yo-Yonges loamy fine sand
NC-PA-2-IC Spencer Farms, Inc. Pamlico 3.5°09.55' 76°49'26- 10.24 Ye-Yonges loamy fine send
NC-PA-2-1 D Spencer Farms, Inc. Pamlico 35''09'55' 76'49'23- 10.25 Yo-Yonges loamy One sand
NC-PA-2-I E Spencer Farms, Inc. Pamlico 35°09'55" 76°49'20- 10.12 Ye-Yonges loamy fine sand
NC-PA-2-IF Spencer Farms,Inc. Pamlico 35'09'55' 76°49'17' 10.05 Ye-Yonges loamy One sand
NC-PA-2-1 G Spencer Farms, Inc. Pamlico 35'09'55- 76°49'I5" 9.52 i Yo-Yonges loamy fine sand
NC-PA-2-2A Spencer Farms, Inc. Pamlico 35'09'I7" 76'40'20- 2.94 Ar-Argent loam
NC-PA-2-2B Spencer Farms. Inc. Pamlico 35°09'16- 76°49'15' 6.26 Ar--Argent loam
NC-PA-2-2C Spencer Farms, Inc. Pamlico 35'09'16'. 76°49'I I" 6.48 Yo-Yonges loamy fine sand
NC-PA-2-2D Spencer Farms, Inc. Pamlico 35°09'I6- 76'49.07- 7.04 Yo-Yonges loamy fine sand
NC-PA-2-2E Spencer Farms. Inc. Pamlico 35°09'I7- 76°49'03- 6.28 Yo-Yonges loamy fine sand
NC-PA-2-3A Spencer Farms. Inc. [Pamlico 35°09'19" 76°49'00- 5.42 Yo-Yonges loamy fine sand
WQ0000702 Version 3.2 Attachment B Page l of 3

ATTACHMENT B- Approved Land Application Sites Certification Date: March 24,2015
CITY OF HAVELOCK Permit Number: WQ0000702 Version: 3.2
NC-PA-2-3B Spencer Farms,Inc. I Pamlico 35°09'I9" 76°48'57" 4.04 Yo—Yonges loamy tine sand
NC-PA-2-3C Spencer Farms,Inc. t Pamlico 35°09'19" 76'48'55" 5.64 Yo—Yonges loamy tine sand 1
NC-PA-2-3D Spencer Farms.Inc. Pamlico 35°09'19" 76'48'51" 8.04 Sk-Stockade loamy tine sand
tt
NC-PA-2-3E Spencer Farms,Inc. Pamlico 35"09'20" 76°48'48" 7.42 1 Sk-Stockade loamy tine sand
NC-PA-2-3F Spencer Farms.Inc. Pamlico 35°09'20" 76'48'45" 7.42 I Sk-Stockade loamy tine sand
NC-PA-2-3G Spencer Farms,Inc. Pamlico 35°09'20" 76°48'42" 6.65 Sk-Stockade loamy fine sand
NC-PA-2-4A Spencer Farms,Inc. Pamlico 35°09'27" 76'49'02" 2.43 Yo—Yonges loamy tine sand
NC-PA-2-4B Spencer Farms, Inc. Pamlico 35°09'34" 76°48'54" 4.34 Sk-Stockade loamy fine sand
NC-PA-2-4C Spencer Farms.Inc. Pamlico 35°09'32'. 76'48'54" 4.51 Sk-Stockade loamy tine sand
NC-PA-2-4D Spencer Farms,Inc. Pamlico 35°09.31" 76°48.53" 3.62 Sk-Stockade loamy tine sand
NC-PA-2-4E Spencer Farms,Inc. Pamlico 35'09'29" 76°48'52" 3.55 Sk-Stockade loamy tine sand
NC-PA-2-4F Spencer Farms, Inc. Pamlico 35°09'28" 76'48'52" 3.60 Sk-Stockade loamy fine sand
NC-PA-2-4G Spencer Farms,Inc. Pamlico 35"09'26" 76°48'51" 3.55 Sk-Stockade loamy fine sand
NC-PA-2-5A Spencer Farms.Inc. Pamlico 35'09'39" 76°49'04" 5.21 Sk-Stockade loamy fine sand
NC-PA-2-5B Spencer Farms,Inc. Pamlico 35"09'40" 76°49'02" 6.48 Sk-Stockade loamy fine sand
NC-PA-2-5C Spencer Farms,Inc. Pamlico 35'09'40" 76°48'58" 6.16 Sk-Stockade loamy fine sand
NC-PA-2-5D Spencer Farms,Inc. Pamlico 35'09'41" 76°48'55" 6.26 Sk-Stockade loamy tine sand
NC-PA-2-5E Spencer Farms, Inc. Pamlico 35'09'41" 76°48'52" 3.90 Sk-Stockade loamy fine sand
NC-PA-2-5F Spencer Farms.Inc. Pamlico 35'09'42" 76'48.49" 3.59 Sk-Stockade loamy fine sand
NC-PA-2-6A , Spencer Farms.Inc. Pamlico 35'09'51" 76°50'21" 5.21 Sk-Stockade loamy fine sand
NC-PA-2-6B Spencer Farms,Inc. Pamlico 35°09'52" 76°50'I T 6.48 Sk-Stockade loamy tine sand
NC-PA-2-6C Spencer Farms, Inc. Pamlico 35°09'53" 76°50.13" 6.16 Sk-Stockade loamy tine sand
NC-PA-2-6D Spencer Farms.Inc. Pamlico 35°09'54" t 76°50'l0" 6.26 Yo—Yonges loamy tine sand
NC-PA-2-6E Spencer Farms.Inc. Pamlico 35'09'55" 76°50'06" 3.90 Yo—Yonges loamy tine sand
•
NC-PA-2-6F Spencer Farms,Inc. Pamlico 35°09'55" 76'50'04" 3.59 Yo—Yonges loamy fine sand
r
NC-PA-2-6G Spencer Farms, Inc. Pamlico 35°09'56" 76°50'0I" 3.84 Ar—Argent loam
WQ0000702 Version 3.2 Attachment B
Page 2 of 3

I
ATTACHMENT B- Approved Land Application Sites Certification Date: March 24,2015
CITY OF HAVELOCK Permit Number: WQ0000702 Version:3.2
NC-PA-2-7A Spencer Farms,Inc. Pamlico 35'09'56' 76°49'59" 2.18 Ar—Argent loamI.
NC-PA-2-7B Spencer Farms.Inc. Pamlico 35°09.57" 76"49'57" 2.57 Ar—Argent loam
NC-PA-2-7C Spencer Farms.Inc. Pamlico 35°09'57" 76°49'55" 3.32 Ar—Argent loam
NC-PA-2-7D Spencer Farms,Inc. Pamlico 35°09'58" 76°49'53" 3.32 Ar—Argent loam
NC-PA-2-7E Spencer Farms,Inc. Pamlico 35°09'59" 76°49'S0" 3.26 Ar—Argent loam
NC-PA-2-7F Spencer Farms, Inc. Pamlico 35°09'59" 76°49'48" 3.03 Ar—Argent loam
NC-PA-2-7G Spencer Farms.Inc. Pamlico 35'10'00" 76°49'46" 3.53 Ar—Argent loam
NC-PA-2-7H Spencer Farms, Inc. Pamlico 35°10'00" 76°49'43" 3.28 Yo—Yonges loamy tine sand
•
NC-P A-2-71 Spencer Farms,Inc. Pamlico 35°10'01" 76"49'41" 3.25 Yo—Yonges loamy fine sand
NC-PA-2-7J Spencer Farms,Inc. Pamlico 35°I0'01" 76'49'39" 3.25 Yo—Yonges loamy fine sand
NC-PA-2-7K Spencer Farms,Inc. Pamlico 35"I0'02" 76°49'37" 2.47 Yo—Yonges loamy fine sand
Total for County 269.80
Total 400.60
1. A re-defined compliance boundary has been approved for this land application site. This re-defined compliance boundary is between fields NC-CV-1-IA and NC-CV-1-1 C and shall be
located at 50 feet from the water supply well on Robert G.Campbell's property. Note that the 100-foot setback between wells and the land application area shall still be met.
WQ0000702 Version 3.2 Attachment B Page 3 of 3

THIS PAGE BLANK

}
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REFERENCE:
ti
GIS DATA LAYERS WERE OBTAINED FROM ESRI,INC. PLEASE NOTE THIS MAP IS FOR INFORMATIONAL 4
PURPOSES ONLY, IT IS NOT MEANT FOR DESIGN,LEGAL,OR ANY OTHER USES. THERE ARE NO v
GUARANTEES ABOUT ITS ACCURACY, S&ME,INC.ASSUMES NO RESPONSIBILITY FOR ANY DECISION
MADE OR ANYACTIONS TAKEN BY THE USER BASED UPON THIS INFORMATION. Field BoundaryI ,
SCALE. 1 =, 1 miles ������ FIGURE 1
SPENCER FAR
DATE 11-06-14 "' 40; SIT( NC-P CITY OF HAVELOCK
DRAWNBY: MEM VICINITY l 503 LAND APPLICATION PROGRAM
WWW.SMEINC.COIVI
PROJECTNO.-----1CITY OF HAVELOCK LAND AI CRAVEN COUNTY
1588-09-059 i ENGINEERING LICENSE NO F 0176 PAMLICO COUNTY, NO
_._ WQ0000702
SITE LOCATION MAP

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BIOSOLIDS MANAGEMENT SERVICE AGREEMENT
This SERVICE AGREEMENT(hereinafter called the AGREEMENT)made and entered into
this 1st day of November 2006 (the EFFECTIVE DATE)by and between City of Havelock,NC
(hereinafter called CUSTOMER),and Synagro Central,LLC,(hereinafter called CONTRACTOR
which term shall include its successors and assigns).
WITNESSETH:
In consideration of the following covenants and AGREEMENTS, the CUSTOMER and the
CONTRACTOR hereby mutually agree as follows:
1. SCOPE
1.1. The CONTRACTOR shall provide biosolids management services that include
removal,transportation,and land application or other beneficial reuse in accordance with the
terms of this AGREEMENT(hereinafter called SERVICES)of the CUSTOMER'S biosolids
which constitute primarily (liquid semi-solids) residue generated during the treatment of
wastewater(hereinafter called BIOSOLIDS)at the city's wastewater treatment plant located
in Havelock,North Carolina(the PLANT).
2. CONTRACTOR OBLIGATIONS
The CONTRACTOR shall:
2.1. Within four(4) weeks after receipt of notice from CUSTOMER, cause the removal,
transportation,and land application of CUSTOMER'S BIOSOLIDS and,in connection
with such activities,maintain AUTHORIZATIONS and landowner AGREEMENTS
required of CONTRACTOR for agricultural land application and/or disturbed land
reclamation in accordance with all applicable LEGAL REQUIREMENTS which are
currently in effect, or which take effect during the term of this AGREEMENT.
2.2. At the written request of CUSTOMER, and as applicable, provide any
AUTHORIZATIONS which are issued by applicable GOVERNMENTAL
AUTHORITIES for all land approved for BIOSOLIDS land application.
2.3. Notify the CUSTOMER of any notice of violation, action, suit, claim, or legal
proceeding against CONTRACTOR relating to any aspect of the CUSTOMER'S
BIOSOLIDS managed pursuant to this AGREEMENT.
2.4. For BIOSOLIDS which are land applied,employ land application methods approved
or allowed by applicable GOVERNMENTAL AUTHORITIES.
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Havelock Agreement-Final 11 07 06.dcc

2.5. Develop and implement monitoring, record keeping, and reporting programs as
required by applicable LEGAL REQUIREMENTS, and as set forth in Section 6 of
this AGREEMENT.
2.6. Provide proof of liability and workers' compensation insurance, as set forth in
Section 4 of this AGREEMENT.
2.7. Indemnify CUSTOMER,and hold harmless CUSTOMER,its subsidiaries,affiliates,
successors and assigns and their respective directors, officers, employees,
shareholders, representatives and agents (hereinafter referred to collectively in this
section as CUSTOMER INDEMNITEES) from and against any and all claims,
liabilities,lawsuits,and causes of action,together with reasonable costs,expenses,and
attorneys' fees associated therewith and all amounts paid in defense or settlement of
the foregoing, which may be imposed upon or incurred by CUSTOMER
INDEMNITEES or asserted against CUSTOMER INDEMNITEES by any other
person or persons (including GOVERNMENTAL AUTHORITIES), to the extent
caused by CONTRACTOR'S breach of its obligations under this AGREEMENT or
violation of applicable LEGAL REQUIREMENTS.
2.8. Comply in all material respects with all LEGAL REQUIREMENTS applicable to
CONTRACTOR'S provision of the SERVICES.
2.9. CONTRACTOR'S obligations to take,receive or beneficially reuse BIOSOLIDS shall
be suspended during a Force Majeure.
3. CUSTOMER
The CUSTOMER shall:
3.1. Provide to CONTRACTOR for off-site beneficial reuse 100% of all liquid
BIOSOLIDS generated at the PLANT.
3.2. Provide CONTRACTOR with reasonable access to the CUSTOMER'S BIOSOLID'S
delivery system,except as reasonably required for safety or emergency considerations,
or planned shutdown of the PLANT. It is agreed that when safety, emergency or
shutdown conditions prevent access, that both parties will attempt to resolve such
conditions as expeditiously as possible.
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Havelock Agreement-Final 11 07 06.dor

3.3. Provide CONTRACTOR written notice of the concentration of total nitrogen(as N on
a dry weight basis) in the BIOSOLIDS which CUSTOMER provides,plus all other
information which CONTRACTOR may request to facilitate its compliance with
applicable LEGAL REQUIREMENTS,including without limitation the requirements
of 40 C.F.R.Part 503. Information which CONTRACTOR may obtain shall include,
without limitation,the monthly average concentrations(in milligrams per kilogram)of
arsenic, cadmium, copper, lead, mercury, nickel, selenium, and zinc or other
potentially Hazardous Materials present in the BIOSOLIDS, the level of pathogen
reduction which CUSTOMER has achieved. The methods and procedures by which
CUSTOMER samples and analyzes concentrations of potentially HAZARDOUS
MATERIALS, pathogen reduction, shall comply with methods and procedures
prescribed by applicable LEGAL REQUIREMENTS, including without limitation
40 C.F.R.Part 503. CUSTOMER shall provide CONTRACTOR with a certification
regarding concentrations of HAZARDOUS MATERIALS, pathogen reduction, as
well as certification that all methods and procedures used by customer for the
sampling and analysis of BIOSOLIDS comply with requirements of 40 C.F.R. Part
503,and any other applicable LEGAL REQUIREMENTS. The faun of certification,
and the type of information which the CONTRACTOR may request from
CUSTOMER may include the form of certification or the type of information which
CUSTOMER must maintain under 40 C.F.R. § 503.17. CONTRACTOR shall have
the undisputed right to rely upon any information or certification provided by
CUSTOMER, and shall not have any independent duty to investigate or inquire
regarding the subject matter of the CUSTOMER'S certification or of the information
which CUSTOMER provides to CONTRACTOR.
3.4. Not provide to CONTRACTOR any BIOSOLIDS which contain HAZARDOUS
MATERIAL or are hazardous in accordance with 40 C.F.R. Part 261, other federal
law,state law,or which contains a concentration of polychlorinated biphenyls equal to
or greater than 50 milligrams per kilogram of total solids (on a dry weight basis).
3.5. Provide CONTRACTOR with at least [four (4) weeks] advance notice of when
CUSTOMER desires for CONTRACTOR to remove BIOSOLIDS from the PLANT.
3.6. Indemnify,defend,and protect CONTRACTOR from and against all claims,damages,
losses,costs,suits,settlements,causes of action,liabilities,fines,penalties,costs,and
expenses(including but not limited to,investigation and legal expenses,and costs and
expenses associated with Remedial Work)(collectively,CLAIMS)arising out of or in
connection with any acts or omissions of CUSTOMER, or its employees, officers,
directors, representatives, contractors, subcontractors, agents, or affiliates, or any
licensee or invitee of the PLANT (other than CONTRACTOR), or CUSTOMER'S
breach of any of its obligations under this AGREEMENT, or any violation of any
applicable LEGAL REQUIREMENT by CUSTOMER or any of its employees,
officers,directors,representatives,agents,contractors,subcontractors,or affiliates,or
-3-
Havelock Agreement-Final 11 07 06.dcc

its licensees or invitees (other than CONTRACTOR) or any discrepancy in the
character or composition of the BIOSOLIUS from the PLANT compared to analytical
results, certifications or other information provided by CUSTOMER to
CONTRACTOR.
3.7. From time to time, as requested by CONTRACTOR, review a list of proposed land
application sites at which BIOSOLIDS from the PLANT may be applied, and select
from such sites those sites to which CUSTOMER desires for its BIOSOLIDS to be
applied, and such sites to which it does not desire its BIOSOLIDS to be applied. In
the absence of specific designations by CUSTOMER,CUSTOMER agrees that it shall
have been deemed to select any and/or all of such application as satisfactory locations
for its BIOSOLIDS.
3.8. Notify the CONTRACTOR of operating changes or any other conditions that would
reasonably be expected to affect the BIOSOLIDS handled by CONTRACTOR under
this AGREEMENT.
4. INSURANCE
The CONTRACTOR shall maintain and provide the CUSTOMER evidence of insurance as
follows:
4.1. Worker's Compensation meeting at least the minimum requirements of the laws of the
State of North Carolina, and Employer's Liability with a minimum single limit of
$1,000,000.
4.2. Commercial General Liability and Automobile Liability Insurance to include premises
operations and subcontractors. Completed Operations and Contractual Liability are to
be included under the Commercial General Liability coverage. The insurance policies
will have limits of no less than $1,000,000.00 per occurrence and $ 2,000,000.00
aggregate. CUSTOMER shall be named as an additional insured.
5. PAYMENT
The CONTRACTOR shall provide the CUSTOMER with an accounting of the gallons of
BIOSOLIDS removed from the CUSTOMER'S PLANT,and such other information as shall
be reasonably requested. CONTRACTOR will utilize a measurement method based on the
number of tanker loads of BIOSOLIDS removed from the CUSTOMERS'S PLANT and the
capacity,in gallons,of the tankers.The CUSTOMER will be provided with manifests for all
loads removed by the CONTRACTOR.
5.1. The CONTRACTOR shall submit invoices once each month for SERVICES provided
by CONTRACTOR, using the rates and the amounts agreed in Section 10 of this
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Havelock Agreement-Final 11 07 06.doc

AGREEMENT. The CUSTOMER shall pay all invoices within 30 days after receipt
of the invoice.
5.2. It is agreed that in the event of any dispute concerning invoice amount,CUSTOMER
will pay undisputed invoice amounts within 30 days after receipt of the invoice.
6. RECORD KEEPING
The CONTRACTOR shall maintain records and submit summary reports to the
CUSTOMER after each hauling event (as requested by CUSTOMER) and on an annual,
cumulative basis. Reports shall include information regarding, but not be limited to:
6.1. Number of loads transported and applied with identification of utilization site(s).
6.2. Such other information as will reasonably allow CUSTOMER to fulfill its
recordkeeping, and reporting requirements under applicable LEGAL
REQUIREMENTS and such other information reasonably deemed by the
CUSTOMER as necessary for this AGREEMENT and which is kept by
CONTRACTOR in the normal course of its business.
7. NOTICES
Except as otherwise provided herein,any notice,demand or other contract disputes or shall
be in writing and shall be personally served, sent by commercial courier service or prepaid
registered or certified mail, or sent by telephonic facsimile delivery with confirmation
thereof. Any such notice shall be deemed communicated upon receipt.
7.1. The following address is hereby designated as the legal address of the
CONTRACTOR. Such address may be changed at any time by notice in writing
delivered to CUSTOMER.
Synagro Central, LLC
7014 E. Baltimore Street
Baltimore,MD 21224
[phone]
Fax: [phone]
Attention: [Stephen Toft]
With a copy to:
Alvin L. Thomas II
General Counsel
Synagro Technologies, Inc.
-5-
Havelock Agreement-Final 11 07 06.doc

1800 Bering Drive, Suite 1000
Houston, Texas 77057
[phone]
[phone] (Fax)
7.2. The following address is hereby designated as the legal address of the CUSTOMER.
Such address may be changed at any time by notice in writing delivered to
CONTRACTOR.
Name: City of Havelock
Street Address: PO Drawer 368
Mailing Address: Havelock,NC [28532]
Phone Number: [phone]
Contact Person: Dave Harvell
Fax: [phone]
8. FORCE MAJEURE
Wherever the word"Force Majeure"is used, it should be understood to mean:
8.1. acts of God, landslides, lightning, earthquakes, hurricanes, tornadoes,blizzards and
other adverse and inclement weather,fires,explosions,floods,acts of a public enemy,
wars,blockades, insurrections,riots or civil disturbances;
8.2. labor disputes, strikes,Work slowdowns, or Work stoppages;
8.3. orders or judgements of any Federal, State or local court, administrative agency or
governmental body,if not the result of willful or negligent action of the party relying
thereon;
8.4. power failure and outages affecting the Premises; and
8.5. any other similar cause or event,including a change in law,regulation, ordinance or
permit, provided that the foregoing is beyond the reasonable control of the party
claiming Force Majeure.
If, because of Force Majeure any party's cost is increased by more than 15% or any party
hereto is rendered unable, wholly or in part,to carry out its obligations under this Contract,
then such party shall give to the other party prompt written notice of the Force Majeure with
reasonable full details concerning it;thereupon the obligation of the party giving the notice,so
far as they are affected by the Force Majeure, shall be suspended during,but no longer than,
the continuance of the Force Majeure. The affected party shall use all possible diligence to
remove the Force Majeure as quickly as possible,but his obligation shall not be deemed to
-6-
Havelock Agreement-Final 11 07 06.dcc

require the settlement of any strike,lockout,or other labor difficulty contrary to the wishes of
the party involved.
9. TERM
9.1. This AGREEMENT shall be effective from the EFFECTIVE DATE until the 30th day
of September 2011 (the INITIAL TERM). At the end of this term, this
AGREEMENT may be extended on a yearly basis for five (5) additional one year
teiius at the option of CUSTOMER and at the mutual agreement in writing of both
parties. The non-defaulting party may terminate this AGREEMENT and shall have no
further obligations to the other party under this AGREEMENT if(i)the other party
fails to observe or perform any material covenant or agreement contained in this
agreement for ten (10) business days after written notice thereof has been given to
such other party by the non-defaulting party or(ii) at any time upon the insolvency of
the other party, or the institution by or against the other party of any proceeding in
bankruptcy or insolvency or for the appointment of a receiver or trustee or for an
assignment for the benefit of creditors.
9.2. CONTRACTOR may terminate this AGREEMENT at any time upon written notice to
CUSTOMER and have no further obligation to CUSTOMER if:
9.2.1. The CONTRACTOR is unable to utilize the BIOSOLIDS due to a change in
any LEGAL REQUIREMENTS that renders the SERVICES illegal,or place
such restrictions or requirements thereon so as to make the provision of the
SERVICES cost prohibitive or to otherwise frustrate the commercial intent of
this AGREEMENT.
9.2.2. The BIOSOLIDS become unsuitable for land application by the
CONTRACTOR by reason of(i) the act or omission of any third party or
CUSTOMER, and through no fault of CONTRACTOR,or(ii) the condition
of the BIOSOLIDS is materially inconsistent with the description and
analysis,certifications or other infoiivatian the CUSTOMER has provided to
the CONTRACTOR regarding the BIOSOLIDS, or (iii) CUSTOMER
breaches its obligations hereunder regarding the quality of the BIOSOLIDS.
9.3. In the event of any change in federal,state or local law or regulation,or any change in
any one of CONTRACTOR'S permits,which is implemented during the Term of this
AGREEMENT and which results in a significant increase or decrease in the cost of
performing the SERVICES,the CUSTOMER and CONTRACTOR agree to attempt
to negotiate a mutually agreeable adjustment to that payment teinns specified in this
AGREEMENT. Should agreement not be reached, either party may terminate this
AGREEMENT as specified in Article 9.
-7-
Havelock Agreement-Final 11 07 06.dec

10. PRICE
10.1. Except as otherwise provided in this AGREEMENT, CUSTOMER will pay the
following fixed prices for CONTRACTOR'S SERVICES hereunder for the duration
of the INITIAL TERM of this Agreement
Liquid Land Application =$0.057 per gallon
Mobilization =Included at no charge
503 Compliance Sampling (if needed)= Cost plus 15%
Ag-lime (if needed) =Included at no charge
Land Permitting(min 100 acres)= $25.00 per acre
10.2. Upon increases in CONTRACTOR'S costs due to changes in LEGAL
REQUIREMENTS,CONTRACTOR may no more than once each anniversary year,
request an increase in the fixed prices set forth hereunder. The parties shall in good
faith attempt to negotiate such increase and if successful such shall be effective as of
the beginning of the then most current anniversary of the EFFECTIVE DATE. In
addition,there will be an annual adjustment for price paid for SERVICES provided
by the CONTRACTOR on the anniversary date of the EFFECIVE DATE. The first
adjustment shall be on October 1, 2007, and shall be repeated at the end of each
twelve months thereafter. The adjustment will be the percent increase or decrease in
the Consumer price Index for All Urban Consumers(CPI-U)as published by the U.S.
Department of Labor. The adjustment will be made by multiplying the percent
increase or decrease in the CPI-U over the most recent twelve months reported times
the current unit price and adding or subtracting the adjustment to the price used
during the previous twelve months.
11. MISCELLANEOUS PROVISIONS.
11.1. Assignment. The CUSTOMER and/or CONTRACTOR shall have the right to assign
this AGREEMENT in writing to any successor in interest, subject to the written
approval of the other party,which approval shall not be unreasonably withheld.
11.2. Governing Law. THIS AGREEMENT AND ALL THE RIGHTS AND DUTIES
OF THE PARTIES ARISING FROM OR RELATING IN ANY WAY TO THE
SUBJECT MATTER OF THIS AGREEMENT OR THE TRANSACTIONS
CONTEMPLATED BY IT,SHALL BE GOVERNED BY,CONSTRUED,AND
ENFORCED IN ACCORDANCE WITH THE LAWS OF THE STATE OF
NORTH CAROLINA.
11.3. Costs and Fees. The prevailing party in any legal proceeding brought by or against
the other party to enforce any provision or term of this AGREEMENT shall be entitled
-s-
Havelock Agreement-Final 11 07 06.dcc

to recover against the non-prevailing party the reasonable attorneys'fees,court costs
and other expenses incurred by the prevailing party.
11.4. Consent to Breach Not Waiver. No term or provision hereof shall be deemed
waived and no breach excused,unless such waiver or consent be in writing and signed
by the party claimed to have waived or consented. No consent by any party to, or
waiver of, a breach by the other party shall constitute a consent to, waiver of, or
excuse of any other different or subsequent breach.
11.5. Severability. If any term or provision of this AGREEMENT should be declared
invalid by a court of competent jurisdiction,(i)the remaining terms and provisions of
this AGREEMENT shall be unimpaired,and(ii)the invalid term or provision shall be
replaced by such valid term or provision as comes closest to the intention underlying
the invalid term or provision.
11.6. ENTIRE AGREEMENT. THIS AGREEMENT INCLUDES AND
INCORPORATES BY REFERENCE AS IF FULLY SET FORTH HEREIN,
ALL OF THE TERMS,CONDITIONS AND OBLIGATIONS CONTAINED IN
THIS AGREEMENT, THE INFORMATION FOR PROPOSERS, SPECIFIC
PROVISIONS, AND DRAFT SERVICE AGREEMENT (AS AMENDED).
THIS AGREEMENT, TAKEN WITH THE INFORMATION FOR
PROPOSERS, SPECIFIC PROVISIONS, AND DRAFT SERVICE
AGREEMENT(AS AMENDED)HERETO CONSTITUTES THE COMPLETE
AND EXCLUSIVE STATEMENT OF THE AGREEMENT BETWEEN THE
PARTIES WITH REGARD TO THE MATTERS SET FORTH HEREIN,AND
ALL OTHER AGREEMENTS, PROPOSALS, AND REPRESENTATIONS,
ORAL OR WRITTEN,EXPRESS OR IMPLIED,WITH REGARD THERETO
ARE SUPERSEDED..
11.7. Amendments. This AGREEMENT may be amended from time to time only by an
instrument in writing signed by the parties to this AGREEMENT.
11.8. Counterparts. This AGREEMENT maybe executed in counterparts,which together
shall constitute one and the same contract. The parties may execute more than one
copy of this AGREEMENT, each of which shall constitute an original.
11.9 Preaudit Certification. This instrument has been preaudited in the manner required
by the Local Government Budget and Fiscal Control Act.
Lee *. Tillman,Director of Finance
-9-
Havelock Agreement-Final 11 07 06.dcc

12. DEFINITIONS
12.1. "AUTHORIZATIONS" means all authorizations, permits, applications, notices of
intent, registrations, variances, and exemptions, required for the removal,
transportation and land application of BIOSOLIDS in compliance with all applicable
LEGAL REQUIREMENTS.
12.2. `BIOSOLIDS" means sludge meeting Class B pathogen requirements, vector
attraction reduction requirements and pollutant concentrations(as defined by 40 CFR
Part 503 and State of North Carolina requirements for land application). Biosolids
do not include any hazardous materials or substance and must be suitable for land
application under the applicable law.
12.3. "ENVIRONMENTAL LAWS" means any AUTHORIZATION and any applicable
federal, state, or local law, rule, regulation, ordinance, order, decision, principle of
common law, consent decree or order, of any GOVERNMENTAL AUTHORITY,
now or hereafter in effect relating to HAZARDOUS MATERIALS,BIOSOLIDS,or
the protection of the environment,health and safety,or a community's right to know,
including without limitation, the Comprehensive Environmental Response,
Compensation, and Liability Act,the Resource Conservation and Recovery Act, the
Safe Drinking Water Act, the Clean Water Act, the Clean Air Act, the Emergency
Planning and Community Right to Know Act,the Hazardous Materials Transportation
Act, the Occupational Safety and Health Act, and any analogous state or local law.
12.4. "GOVERNMENTAL AUTHORITY"means any foreign governmental authority,the
United States of America, any State of the United States of America, any local
authority, and any political subdivision of any of the foregoing, and any agency,
department, commission, board, bureau, court, tribunal or any other governmental
authority having jurisdiction over this AGREEMENT,BIOS OLIDS,or COMPANY,
HAULER, or any of their respective assets,properties, sites, facilities or operations.
12.5. "HAZARDOUS MATERIALS"means any"petroleum," "oil," "hazardous waste,"
"hazardous substance," "toxic substance," and"extremely hazardous substance" as
such terms are defined,listed,or regulated under ENVIRONMENTAL LAWS,or as
they become defined, listed, or regulated under ENVIRONMENTAL LAWS.
12.6. "LEGAL REQUIREMENT means any AU'CHORIZATION and any applicable
federal, state, or local law, rule, regulation, ordinance, order, decision, principle of
common law, consent decree or order, of any GOVERNMENTAL AUTHORITY,
now or hereafter in effect,including without limitation,ENVIRONMENTAL LAWS.
-10-
Havelock Agreement-Final I 1 07 06.doc

12.7. "REMEDIAL WORK" means investigation, monitoring, clean-up, containment,
removal, storage, remedial or restoration work associated with HAZARDOUS
MATERIALS or BIOSOLIDS.
IN WITNESS WHEREOF,the parties of this AGREEMENT have hereunto set their hands and seals,
dated as o the day and year first herein written.
Have ck, C . ("CUSTO R") •
y: k/ a. ATTEST:
ame&Title: euv 2S W. crepm,a-r) Name &Title: Q.;iki..1 , Insi cyk,-
IN\Of\O r Th a Gib C11iKL
Synagro Central, LLC. ("CONTRACTOR")
if,. G ,; /fe--- __._ATTEST: l ) �--�
Name & Title: Alvin L. Thomas, Vice President Name&Title:Dovsha G.Roscoe,Asst.Secretary
_11 _
Havelock Agreement-Final 11 07 06.doc

Amended
Appendix A-Draft Service Agreement
1. General
I. No residuals management operations shall occur on Sundays or legal holidays without
the approval of the Wastewater Treatment Supervisor.
It. All operators shall be well versed with regulations and requirements stipulated in the
EPA 40 C.F.R. Part 503 regulations and the Generator's land application permit
WQ0000702 with the State of North Carolina Department of Environment and Natural
Resources(NCDENR).
III. The total percent solids of the residuals produced by the Generator's facilities shall vary
from 3%to 6%.n1neScontractoremusttprovrne eguipmentrtiiat canf ctior.properly in
this range.
IV. The Contractor shall remove all unused materials, tools, equipment and machinery,
waste materials,refuse and other debris from loading area and land application sites.
The Contractor shall see that these sites are at all times left in a neat and orderly
condition.
V. Liquid residuals shall be transported in sealed tank bodies. The capacity of all tankers
and/or any other containers used to calculate the volume of residuals hauled for
payment should be certified by an independent agency capable of perfoiwing such
certification. This certification information shall be supplied in writing to the
Wastewater Treatment Supervisor before residuals are hauled for payment.
VI. All application and transportation vehicles shall be cleaned no less than once per
month. If residuals are spilled onto vehicles, contractor shall see that the vehicles are
cleaned by the next working day.
VII. The Contractor shall be responsible for repair/replacement of all pavement, driveways,
fences, shrubs, lawns,trees and other public or private property damaged as result of
work performed under agreement with the Generator.
30

VIII. The Contractor shall at all times have a competent project manager or other
representative on the work site who shall have full authority to act for the Contractor
and who shall see that the work under the Contract is executed in accordance with the
agreement documents. All communications with the project manager shall be binding
as if given to the Contractor but must be confirmed in writing within 24 hours.
2. Permitting
I. The Contractor shall be responsible for the procurement of additional sites suitable for
land application and shall be responsible for obtaining and compiling the infoitnation
^ in accor.dance with f schedule
necessary for generation of permit applications/renewals. At a minimum, sufficient
acreage must be permitted to annually compensate for the number of acres lost during
the prior year and any increase in biosolids productions. which approval shall not be unreasonably
withheld A
II. All sites shall meet the approval of the Generator prior to permitting by the State. The
Generator also reserves the right to prohibit the permitting of any site,but such Prohibition is subject to the
reasonableness standard.
ill. A copy of the Land Application Permit WQ0000702 and all site maps shall be
maintained on each application vehicle at all times when residuals are being applied.
give Generator reasonable notice
IV. The Contractor shall roceimx)caks5iwi prior to any correspondence with regulatory
agencies regarding regulatory issues concerning the Generator. All correspondences
shall be copied to the Generator.
V. On a yearly basis, every permitting event, or in the event that development or other
issues require changes in buffers/maps, the Contractor shall be responsible for
providing updated maps for the Land Application Site Books. The project manager
shall evaluate each site during application event for possible adjustments to
buffers/maps.
3. Emergency Response/Spills
I. The Contractor shall submit to the Generator for approval a Spill Control Plan.
II. A copy of the Spill Control Plan shall be maintained in each transport and application
vehicle used by the Contractor.
31

lll. Any spills involved with the loading, transportation and/or application of the said
residuals shall be deemed the responsibility of the Contractor and shall be cleaned up
A reasonable
immediately to the satisfaction of the Generator,NCDENR,Division of Water Quality
andlor any landowner that may be involved. Any occurrences shall be immediately
reported to the Wastewater Treatment Supervisor.
4. Beneficial Reuse
I. The Contractor shall utilize equipment capable of both surface application and
iebnse arce injection/incorporation End shall provide such capability at the request of the
nerato
Ydliatkifigtx&as is required to meet vector attraction reduction requirements.at a negotiated price)
II. No residuals generated by the Generator shall be stored at facilities or land-applied on
land not permitted/approved in the Generator's land application permit for NC DENR.
M. All buffer zones shall be marked cx4:toctx prior to land application.
IV. Any interruption(other than inclement weather) of the beneficial reuse activities for any
period of time longer than(2)days shall be reported to the Generator immediately,
when such interruption is determined.
ensure
V. The Contractor shall provide adequate supervision of its employees to r g2�X�proper
application techniques are being utilized at all times.
VI. The Contractor shall provide individuals who are capable of and can maintain good
relations with the program participants. Failure to do so shall be grounds for the
immediate suspension of work and the possibility of the revocation of agreement.
VII. The Contractor shall make every effort to provide residuals application to all program
participants.
VTTT. The Contractor shall provide the landowner with a copy of the analysis of residuals Iand
applied to his/her field.(farm report)
IX. Transporters of the Contractor should be aware that they present an image of the
Generator, therefore they should properly and professionally respond to any complaints
by citizens andlor the Generator. This includes but is not limited to obeying all traffic
laws.
32

5. Monitorutg/Recordkeeping
I. The Contractor shall be responsible for all monitoring at the land application sites as
required by the Generator's Land Application permit#WQ0000702 and the EPA 40
C.F.R. Part. All residuals sampling shall be the responsibility of the Generator's
WWTP Personnel.
II. All infonnation shall be kept on file with the Contractor and the Generator. The
Generator requires that the Contractor have a database management system for the
storage of data for residuals management activities performed for the Generator. mac
at?ttootioacquicttalboboacmco6timoprogpanoggimxxi&NlxfooMgictgxcig4RXRRIMMIZIkxx
M. The Contractor shall keep daily logs indicating tanker loading, transportation, and
application volumes. These logs shall be totaled daily and a copy submitted to the
Generator's Residuals Supervisor no later than 4:00 p.m. on the first working day of the
following week.
IV. A report, after each land application event, shall be provided to the Generator indicating
volume of residuals, application rate per acre, land applied, and land application site
information. This information shall include all information as required by the land
application permit and 40 C.F.R. Part 503 regulations. These records shall be
submitted to the Generator by the 15th day of the following month after the application
event
6. Public Education/Acceptance
cooperate with Generator
I. The Contractor shall liodrxxrbarct in a Public Education Campaign for the Generator.
II. The Contractor shall assist the Generator with the handling of complaints and/or
questions regarding all residual management activities.
M. The Contractor shall maintain good relations with program participants and shall
provide documented notification of biosolids issues that could impact
program/participants.
IV. The Contractor shall assist the Generator with any other public notification that may be
required by the regulatory agencies.
33

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First Species Effluent Toxicity Testing ,
2020-2023

Summary of City of Havelock WWTP
First Species Effluent Toxicity Testing Summary Table
Sample Date Contract Lab Organism Location Pass/Fail %Survival
Tuesday,July 14,2020 ETT Environmental,Inc Americamysis bahia EFF Pass 97.5%
Tuesday,October 13,2020 ETT Environmental,Inc Americamysis bahia EFF Pass 100%
Tuesday,January 26,2021 ETT Environmental,Inc Americamysis bahia EFF Pass 100%
Tuesday,April 13,2021 ETT Environmental,Inc Americamysis bahia EFF Pass 100%
Tuesday,July 13,2021 ETT Environmental,Inc Americamysis bahia EFF Pass 97.4%
Tuesday,October 12,2021 ETT Environmental,Inc Americamysis bahia EFF Pass 100%
Tuesday,January 25,2022 ETT Environmental,Inc I Americamysis bahia EFF Pass 100%
Tuesday,April 5,2022 ETT Environmental,Inc Americamysis bahia EFF Pass 100%
Tuesday,July 12,2022 ETT Environmental,Inc Americamysis bahia EFF Pass 97.3%
Tuesday,October 4,2022 ETT Environmental,Inc Americamysis bahia EFF Pass 100%
Tuesday,January 10,2023 ETT Environmental,Inc Americamysis bahia EFF Pass 100%
Tuesday,April 4,2023 ETT Environmental,Inc Americamysis bahia EFF Pass 100%
Tuesday,July 11,2023 ETT Environmental,Inc Americamysis bahia EFF Pass 100%
Tuesday,October 10,2023 I ETT Environmental,Inc Americamysis bahia EFF
III Pass 100%

env rontner►ta,Inc. [phone].FAX [phone]
P Q.Box 1 E414, Greenv He, SC 29606 4 Craftsman Court,Graer,SC 29650
1
Americamysis bahia Survival and Growth Test kA�
EPA-821-R-02-014 Method 1007 Jf �,le I 11°
Ive)
Client: CITY OF HAVELOCK
Facility:WWTP
NPDES#:NC0021253
Test Date: 14Jul-20
•
Laboratory Sample ID#:T56948
Test Reviewed and Approved By:
Robert W.Kelley,Ph.D. Farhad Rostampour
QA/QC Officer Laboratory Director
Certification#E87819
SCDHEC Certification#23104
Test results presented in this report conform to all requirements of
NELAC,conducted under NELAC Certification Number E87819
Florida Dept.of Health.Included results pertain only to provided samples. NCDENR Certification# 022
Page 1 of 6
L

Effluent Toxicity Report Form •Chronic Mysidopsis Pass/Fail Date: 14-Jul-20
Facilit : Havelock NPDES# NC0021253 Pipe#: 001 County: Craven
Laboratory Performing Test: ETT Environmental Inc. Comments:
x -
Signature of Operator in Responsible Charge
Signature of Laboratory Supervisor
-
MAIL ORIGINAL TO: Environmental Sciences Branch
Division of Water Quality
NC DENR
1621 Mail Service Center
Raleigh,NC 27699-1621
Control Replicates 2 3 4 5 6 7 8
Surviving# 5 5 5 4 5 4 5 5 %Survival 100.0%
Original# 5 5 5 4 5 4 5 5
Weight(per Original) 0.358 0.346 0.426 0.4025 0.386 0.395 0.392 0.342 Avg Weight(mg) 0.381
Treatment 2 Replicates 1 2 3 4 5 6 7 8
I
Surviving# 5 5 4 5 5 5 5 5 %Survival 97.5%
Original# 5 5 5 5 5 5 5 5
Weight(per Original) 0.396 0.378 0.356 0.408 0.458 0.42 0.418 0.362 Avg Weight(mg) 0.400
Water Quality Data
Day
Control 0 2 3 4 5 6 7 Test Results
pH Initial I 7.9 7.9 8.3 8.3 8.2 8.2 8.2
pH Final 7.8 7.9 7.8 7.8 7.8 7.9 7.2 Significant Mortality?
DO Initial 7.3 7.1 6.8 6.8 6.5 7.0 7.4 Yes No
DO Final 5.5 5.1 5.1 4.3 4.3 5.0 3.9 ( X 1
Temp Initial 24.7 25.6 . 25.5 25.4 25.5 25.6 25.1 Check One
Temp Final 26.1 26.1 26.1 26.1 26.2 26.1 26.1
Salinity Initial 25.9 26.2 27.2 27.2 25.6 25.8 24.9 Growth
caic. t -0.54
Treatment 0 1 2 3 4 5 6 7 Tabular t I - 1.76
pH Initial 7.9 8.0 8.3 8.2 8.2 8.2 8.2 Fecundity
pH Final 7.9 8.0 8.0 7.9 7.8 7.8 7.6 Rank Sum
DO Initial 7.2 7.2 6.8 6.8 6.9 7.0 7.2 Cnt.Value
DO Final 5.7 4.7 5.5 4.5 4.6 4.4 5.0
Temp Initial 25.0 25.6 25.6 25.7 25.6 25.8 25.4 PASS FAIL
Temp Final 26.1 26.1 26.1 26.1 26.2 26.1 26.1 X
Salinity Initial 26.0 26.2 25.2 25.2 25.9 25.8 _ 25.5 Chock One
Sample Test Date: 14-Jul-20
Collection Start Date 12-Jui-20 14-Jul-20 16-Jul-20 Effluent Test Concentration: 15%
Grab 5 replicates were set for each control test replicate;where<5 are shown the organisms were lost during renews
Composite(Duration) 24 hr 24 hr 24 hr 5 replicates ware set for each treatment test replicate;where<5 are shown the organisms were lost during renewal
Conductivity(pmhos/cm) 627 531 580
Chlonr.e(mg/L) <0.05 0.06 <0.05
Sample Temp.at Receipt 0.4 0.3 0.3
DWQ Form AT-4(6/99)
Page 2 of 6

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E11 . (E6d)877.6942 ,FAX[phone]
P.O.Box 1E4114,Greenvlie, SC 29606 4 Craftsman Court,Greer,SC 29650
Americamysis bahia Survival and Growth Test
EPA-821-R-02-014 Method 1007
Client: CITY OF HAVELOCK
Facility: WWTP
NPDES#:NC0021253
Test Date: 13-Oct-20
Laboratory Sample ID#: T57604
Test Reviewed and Approved By:
Robert W.Kelley,Ph.D. Farhad Rostantpour
QA/QC Officer Laboratory Director
—` Certification#E87819
SCDHEC Certification#23104
Test results presented in this report conform to all requirements of
NELAC,conducted under NELAC Certification Number E87819
Florida Dept.of Health.Included results pertain only to provided samples. NCDENR Certification# 022
Page 1 of 6

Effluent Toxicity Report Form -Chronic Mysidopsis Pass/Fail
Date: 13-Oct-20
Facili : Havelock NPDES# NC0021253 Pipe#: 001 Coun : Craven
Laboratory Performing Test: ETT Environmental Inc. Comments:
x
Signature of Operator in Responsible Charge
x . ... /: _-
Signature of Laboratory Supervisor
MAIL ORIGINAL TO: Environmental Sciences Branch
Division of Water Quality
NC DENR
1621 Mail Service Center
Raleigh,NC 27699-1621
Control Replicates 1 2 3 4 5 6 7 d
Surviving# 5 4 5 4 5 5 5 5 %Survival 97.4%
Original# 5 5 5 4 5 5 5 5
Weight(per Original) 0.442 0.312 0.48 0.4675 0.376 0.558 0.524 0.536 Avg Weight(mg) 0.462
Treatment 2 Replicates 1 2 3 4 5 6 7 8
Surviving# 4 5 5 5 5 5 5 4 %Survival 100.0%
Original# 4 5 5 5 5 5 5 4
Weight(per Original) 0.5125 0.44 0.476 0.478 C.426 1 0.506 0.45 0.455 Avg Weight(mg) 0.468
1 Water Quality Data
Day
Control 0 1 2 3 4 5 6 7 Test Results
pH Initial 7.8 7.9 8.3 8.1 8.0 7.8 8.1
pH Final 7.8 7.8 7.6 7.5 7.6 7.5 8.2 Significant Mortality?
DO Initial 7.0 6.9 6.3 6.4 6.7 7.0 6.4 Yes No
DO Final 6.5 6.3 4.8 5.1 6.0 4.8 5.7 X
Temp Initial 24.7 25.0 25.2 25.2 25.1 25.3 25.1 Check One
Temp Final 26.1 26.0 26.0 26.0 25.9 25.9 26.0
Salinity Initial 24.6 25.4 25.3 25.5 25.1 24.9 25.1 Growth
- Cale. t -0.19
Treatment 0 2 3 4 5 6 7 Tabular t 1.76
pH Initial 6.8 7.0 8.3 8.1 8.0 7.8 8.1 Fecundity
pH Final 7.5 8.0 7.7 7.7 7 6 7.7 8.3 Rank Surn
DO Initial 6.9 6.9 6.4 6.1 6.7 6.6 6.6 Cdt.Value _
DO Final 6.4 4.5 4.5 5.6 5.3 4.4 5.6
Temp Initial 25.0 25.1 25.7 25.6 25.2 25.5 25.2 PASS FAIL
Temp Final 26.1 26.0 26.0 26.0 25.9 25.9 26.0 X
Salinity Initial 24.2 24.2 24.5 24.0 24.3 24.4 24.4 Check One
Sample Test Date: 13-Oct-20
Collection Start Date 11-Oct-20 13-Oct-20 15-Oct-20 Effluent Test Concentration: 15%
•
Grab _ 5 replicates were set for eacn control test replicate;where<5 are shown the organisms were lost during renews
Composite(Duration) 24 hr 24 hr 24 hr 5 replicates were set for each treatment test replicate;where<5 are shown the organisms were lost during rene
Conductivity(pmhos/cm) 630 599 605
Chiorine(mg/L) <0.05 <0.05 <0.05
Sample Temp.at Receipt 0.8 0.3 1.0
DWQ Form AT-4(6/99)
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PO Box 1 6414 Greenville,SC 29606-7414
[phone], [phone] Fax:[phone]
Shipping Address:4 Craftsman Ct,Greer,SC 29650
\VWW.ETTENVlnoee NTAI—COM
flicnt: I-�--
4" 1 �G I �.1— �7 Program Containers Preservative Parameters
` -S ,-� C,..,----
Whole Effluent Toxicity-
state: A/e= l�PDESr7: /!VG e�f" ;2 l .,
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Acute Chronic• Test Organisms
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the doted(ire b co .� >=ht,, - O. 2 -° ? r -_ - ,N E.
SAMPLE ID o — _ v =znc - _ _ - , a
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Special Instructions:
Sample Custody Transfer Record Secure Receipt Sample
Date Time relinquished By/Organization Received By/Organization Area I Temp`C Preserved?
G
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COMPOSITE SAMPLING PROCEDURES TEMPERATURE MONITORING PROCEDURES HOLD TIME PROCEDURES
Composite samples must be collected over a 24 hour period. Sample temperature during collection and transport must be between For toxicity testing the sample must first be used within 36 hours
Time Proportional: I sample each hour for 24 hours.Equal voter 0.0 and 6.0°C.Samples must not be frozen.Use water ice in sealed bags. of sample collection(completion of composite sample).
or at minimum I sample every 4 hours over 24 hours. Sample may not be used after 72 hours from sample collection.
Flow Prc nal:As per instructions in NPDES permit.

6f�.... CHAIN OF CUSTODY RECORD
r .' 3r�i g !Page J of /
PO Box 16414 Greenville SC 29605-7414
[phone], (800)891 -2325 Fax[phone]
Shipping Address:4 Crafts man Ct,Greer,SC 29650
W W W.ETTENVIRONMENTF..—L.CON
Client: `
I
i --/ o— f r1C ifC lCje�h. Program Containers Preservative Parameters
Facility: 7 iC/� T r� `�� I ,
lY Whole Effluent Toxicity tnc
State: GG 5 ) r•
/�� 1PD)S f 3 Acute Chronic Test Organisms
J - 0
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the dotted line '_ c E = U H 3mlano, _ _ " z
U G U O C r O U '4..142011 - _
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Sample Custody Ti—ansfer Record Secure Receipt Sample
Date 'V Time lin wished By/Organization Received By/Organization (Area Temp CC Preserved?
r
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COAlPOSJTE S41/PLIAr PROCEDURES TEMPERATURE A'ONITORJNG PROCEDURES HOLD TIME PROCEDURES
Composite samples must be collected over a 24 hour period. Sample temperature during collection and transport must be between For toxicity testing the sample must first be used within 36 hours
Time Proportional: I san-itple each hour for 24 hours.Equal volui 0.0 and 6.0°C.Samples must not be frozen Use water ice in sealed bags. of sample collection(completion of composite sample).
or at minimum 1 sample every 4 hours over 24 hours. Sample may not be used after 72 hours from sample collection.
Plow Pro il:As peas instructions in NPDES permit.

ET ,:.:::: . ,
CHAIN OF CUSTODY RECORD
rearm manti.�t1 Glk-. Page _ of
PO Box 16414,Greenville, SC 29606-7414
[phone], [phone] Fax:[phone]
Shipping Address:4 Craftsman Ct,Greer,SC 29650
WWW.ETT ENV IR0NMENTAL.0 ON
Client: ,
+'3 . y (J" riCI jG/�,,4,t kr� '-r l� Program Containers jPreseoative 2arameters
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State: �,/� NPDES 4: !! ���r?(! Whole G[nucnt Tn idn' n
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Sign,and Print below 3 o _ 0 =HCL 0 t) _ = - ' _ rs _N
thCS' e dotted line u .� r =ttno5 --
SAMPLE ID U Composite start Detel Time Snmptc Collection Dnrc Time Collected by (, tn- op 7 en c 0 J G=p cr U o — — Chemical Analysis a Other
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Sample Custody Transfer Record Secure Receipt Sample
Date gTime Reliiinn)quishedByIOrganization / 1 (�( } / t Received ByIOrganir_ation Area Temp°C Preser;cd'?
ra-t"l-�o D'3t{0 ✓✓ ' - /_ A-. M c P c.E,a�.J 1-/ /0
COMPOSITE S,IMPLIArG PROCEDURES TEMPERATURE AIONITORING PROCEDURES HOLD TIME PROCEDURES
Composite samples trust be collected over a 24 hour period. Sample temperature during collection and transport must be between For toxicity testing the sample must first be used within 36 hour
Time Proportional: 1 sample each hour for 24 hours.Equal volut 0.0 and 6.0°C.Samples must not be frozen.Use water ice in sealed bags. of sample collection(completion of composite sample).
or at minimum I sample every 4 hours over 24 hours. Sample may not be used after 72 hours from sample collection.
Plow Prc---= nai:As per instructions in NPDES permit.

irsiiiqi:t' 115,4-Vtii
EJ
ernftrantnonta Ilic.
(ltG4)877-6942 .FAX[phone]
P.O.Box 1MK Green lie, SC Z9606
4 Craftsman Court,Greer,SC 29650
Americamysis bahia Survival and Growth Test
EPA-821-R-02-014 Method 1007
Client: CITY OF HAVELOCK
Facility:WWTP
NPDES#:NC0021253
Test Date: 26-Jan-21
Laboratory Sample ID#:T58365
Test Reviewed and Approved By:
44.E /V4
Robert W.Kelley,Ph.D.
QA/QC Officer
t i i "Certification 11E87819
9R,8 SCDHEC Certification#23104
Test results presented in this report conform to all requirements of
NELAC,conducted under NELAC Certification Number E87819
Florida Dept.of Health.Included results pertain only to provided samples. NCDENR Certification if/ 022
Page 1 of 6

Effluent Toxicity Report Form -Chronic Mysidopsis Pass/Fail
Facili : Havelock Date: 26-Jan-21
Laboratory Performing Test: ETT Environmental Inc Comments:ES# NC0021253 C .e#: 001 Coun Craven
X
Signature of Operator in Responsible Charge
Signature of Laboratory Supervisor
MAIL ORIGINAL TO: Environmental Sciences Branch
Division of Water Quality
NC DENR
1621 Mail Service Center
Raleigh,NC 27699-1621
Control Replicates 1 2 3 4 5 6 7
8
Surviving# 5 4 6 6 5 5 5 I 5 %Survival I 100.0%
• Original# 5 4 5 5 5 5 5 5
Weight(per Original) 0.334 0.333 0.330 0,372 0.308 0.434 0.418 0.424 Avg Weight(mg)I-0.36g
Treatment 2 Replicates 1 2 3 4 5 6 7 8
Surviving# 5 5 5 5 6
5 5 5 %Survival? 100.E%i
Originei# 5 5 5 6 5 5 5 6
Weight(per Original) 0.366 0,336 0.368 0.426 0.358 0.374 0.414 0.31E Avg Weight(mg)I 0.370 I
Water Quality Date
Day
Control 0 1 2 3 4 5 6 7 Test Results
pH Initial 8.7 8.1 7.6 8.1 8.1 8.0 8.0
pH Final 7.8 7.2 7.7 7.9 7.8 7.4 7.8 Significant Mortality?
DO Initial 8.5 7.0 6.4 6.9 7.1 7.0 6.7 I Yes No
DO Final 6.9 4.7 5.1 6.5 5.4 4.0 6.8 I 1 X I
Temp Initial 24.7 25.8 25.4 25,3 25.3 25.6 25.0 Chezlt One
Temp Final 28.0 26.2 _ 26.1 28.2 26.1 26.2 26,1
Salinity Iniliai 25.3 26.5 25.4 25.2 26.2 26.2 26.0 Growth
Cale- t 0.04
Treatment 0 I 2 3 4 5 6 7 Tabular 1.76
pH initial 8.6 8.6 7.8 8.1 8.2 8.1 8.0 Fecundity
pH Final 7.7 7.3 7.8 7.9 7.9 7.5 7.9 Rank Sum
DO Initial 8.5 6.5 6.4 6.7 7.0 6.4 6.7 Cdl Value
-1
DO Final 4.8 4.4 5.0 5,9 5.4 3,9 6.9
Temp Initial 25.0 25.6 25.1 25.6 25.5 25.7 25.8 PASS FAIL
Temp Final 26.0 26.2 26.1 26.2 26.1 26.2 26,1 L X
Salinity Initial 24.5 24.5 24.4 24.9 25.0 25.1 25.3 Check One
Sample Test Dale: 26-Jan-21
Collection Start Date 24-Jan-21 26-Jan-21 28-Jan-21 Effluent Test Concentration: 15%
Grab 5 replicates ware set for each control test replicate;where<5 era shown the organisms were lost during renew
•
Composite(Duration) 24 hr 24 hr 24 hr 5 replicates were sal for each treatment test replicate;where<5 are shown the organisms were lost during rene
Conductivity(prnhos/cm) 600 537 484
Chlorine(mg/L) <0.05 <0,05 <0.05
Sample Temp.at Receipt 0.3 0.5 0.1
DWQ Form AT-4(6/99)
Page 2 of 6

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. ____.__ ___________ .
ETT • CHAIN OF CUSTODY RECORD
iirg::f..r ik,:3if,,I So-. l�tieam'mu.4ly Inge Dr
PO Box 16414,Greenville,SC 2 96 0 6-741 4
[phone], [phone] Fax[phone]
Shipping Address:4 Craftsman Ct,Greer,SC 29650
WWWCTrEP VIRO NMCNTAL.COM
Client: -? / ��C
C r Program Containers Preservative Parameters
Facility: \ f�I
P\�✓M j I — .
Y" 7— �?('�j «'hole Effluent Toxicity state: /\ ( - NPDES 4: C e b_ Ic i' `^
Acute Chronic Test Organisms
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3 pm
U (Composite only) (Grob or Composite) < p r`.. S U wE. U 'o — Z
U Sign,and Print below > U = I z.H a S _ ° 2 _ St 2 _ U = a s
J i J V O U L U U - 7., = E ...1 _
G the dotted line —a. = __ = U •21 H c s"t�os n o • i — = o
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SEfitteni-
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p'1' 1Goo (a o ,_bc _ ^110f a.ir ✓ IV @CO((tc -ltr\ 55565 t
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Special Instruct ons: .7 1.V_-t__S re-CO`aed e.. —by
Sample Custody Transfer Record Secure Receipt Sample
Date Time Relinquished By/Organization Received By/Organization Area Temp°C Preserved?
A;rpa(FPO irk tear(/ C; lU Of 4 \r Qr
1 j�fo'�r �' .G� r tEx ( 76-1/ii6,-,/- 7--- (i D.3
G-
COMPOSITE SAMPLING PROCEDURES TEMPERATURE MONITORING PROCEDURES HOLD TIME PROCED(- S
Composite samples must be collected over a 24 hour period. Sample temperature during collection and transport must be between For toxicity testing the sample must first be used within 36 hours
Time Proportional:1 sample each hour for 24 hours.Equal volm 0.0 and 6.0°C.Samples must not be frozen.Use water ice in sealed bags. of sample collection(completion of composite sample).
or at minimum I sample every 4 hours over 24 hours. Sample may not be used after 72 hours from sample collection.
Flow Proportional:As per instructions in NPDES permit.

ETTCHAIN OF CUSTODY RECORD
PO Box 16414,Greenville,SC 25 6 0 6-741 4
[phone], [phone] Fax[phone]
Shipping Address:4 Craftsman Ct,Greer,SC 29650
W W W.LTYENVI RON MENTAL-CCM
Client: (` E
C 1 cyerkS`"ioapAoc K\_ Program Cantnincrs Preservative Parameters
Facility47; r
Whole ElIIucnt Toxicity
State: a C NPDES#: IN C C)(-)-, s--.), Acute Chronic Test Organisms
S _ n
c U y [
U (Composite only) (Grab or Composite) I • r_ C _ - 0 _ z
e J
Sign,and Print below > = x ^ z-HCL = - = •z - G = w = cn
6 c the dotted Line _ " C U E.? ) H'IO `-_' _' _ _ �' ' C .E
o 4-7 4 .N , U 4' MOH - = al a = - - >. > _ PIE - o
SAMPLE ID U Cumpatitc Stan Date Time Sample Collection Dote Time Collected by U tq to Z O E: U j u 6.0d, a o  _ j: _
6-Odsr U :J v !] I.� ;.� _. U -l ,z Chemical Analysis E.Other e
rt`�� ,- 6 al (�� =�� � 1��"ma's`'', �/ �S( � .7 gc Ol reCI,i OA 5 Z 5960.
._
Special Instructions:
Sample Custody Transfer Record Secure Receipt Sample
Date Time Relirouished By/Oreaniz4tion ` B Received By/Organization Area Temp'C Preserved?
ll��
l°7`�+ fag() OC\\+A Atc\e�C/ C, , Ty of F1�d..�OCit;
1
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COMPOSITE SAMPLING PROCEDURES 'TEMPERATURE MONITORING PROCEDURES HOLD TIME PROCEDURES
Composite samples must be collected over a 24 hour period. Sample temperature during collection and transport must be between For toxicity testing the sample must first be used within.36 hours
Time Proportional:1 sample each hour for 24 hours.Equalyolur 0.0 and 6.0°C.Samples must not be frozen.Use water ice in sealed bags. of sample collection(completion of composite sample).
or at minimum I sample every 4 hours over 24 hours. Sample may not be used after 72 hours from sample collection.
Flow Proportional:As per instructions in NPDES permit.

_ _ _
_ _
ETT
CHAIN OF CUSTODY RECORD
[Page. of PO Box 16414,Greenville,SC 29606-7414
[phone], [phone] Fax[phone] /
Shipping Address:4 Craftsman Ct,Greer,SC 29650
WWW.CPYENVIRC NM ENl'ALCCM
Client: �`
C 1 O HQ.\./EIC C)j Program Container Prescn•at ve Parameters
Facility:\ n ^ I _
h /V , s-te��` � I Whole Effluent Toxicity '
State: Iv C NPDES (\fCC) ,I'' ,,, ;,
` Acute Chronic Test Organisms
1 7-
a
U (Composite only) (Crab or Composite) < o p_ = o L U _o = Z
U - U - _ = 8
'a - ,, r 1-1�Soe n y - o
Sign,and Print below > : _ o I z-rut = z —n
U o; - i
= othe dotted line = = c .: -
SAMPLE 1D z- C°mpoate Stott Dote rime Stun*Collection ante Time Collected by U j Z !a C7 j s=ZmAc v - _ - _ `.=1 c
5-otl,r. < V U Ci Li: nI F. .� Chemical Analysis a Other
Elf, � fi 1 at 1-� t boa �r f f 5S3(06C
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'
1
Sample Custody Transfer Record Secure Receipt Sample
Date Time Relinquished By/Oraanizz-on Received By/Organization
Area Tema°C Preserved?
�a► i�1c� Oev 1, c,i7
a of 1-6/elea( _ _
}'f f 5 ( � ' '' .,, /err o+ 1
7
COMPOSITE SAMPUNG PROCEDURES TEdIPER,ITURE MONITORING PROCEDURES HOLD TI.(IE PROCEDURES
Composite samples must be collected over a 24 hour period. Sample temperature during collection and transport must be between For toxicity testing the sample must fits:be used within 36 hours
Time Proportional:1 sample each hour for 24 hours.Equal vole;0.0 and 6.0°C.Samples must not be frozen.Use water ice in sealed bags. of sample collection(completion of composite sample).
or at minimum I sample every 4 hours over 24 hours. Sample may not be used after 72 holm from sample:collection.
Flow Proportional:As per instructions in NPDES permit.

I i
4 4nu ,Int. (E84)877.8942.FAX(884)B77.6938
P.O,Box 184 4.Weeny Ile.SC 29606 4 Craftsman Cain,&em,SC 25550
Amnerieamysis bahia Survival and Growth Test
EPA-821-JET-02-014 Method 1007
Client: CITY OF HAVELOCK
Facility:WWTP
NPDES#:NC0021253
Test Date: 13-Apr-21
Laboratory Sample ID#:T58979
Test Reviewed and Approved By:
Alit` 4/4
1 .
Robert W.Kelley,Ph.D. /
QAJQC Officer 9,6 7 2;
,
' Certification#F.87819
•e ') ficaon SCDHEC. Certifies on#23104
Teat results presented in this report conform to all requirements of
NBLAC,conducted under-NBLAC Certification Number B87819
Florida Dept.of Health.!Deluded results pertain only to provided samples. NCDENR Certilict on# 022
Page 1 of 6

Effluent Toxicity Report Form -Chronic Mysidopsis Pass/Fall
Facilit r�Havelock Date: 13-Apr-29
NPDES# NC0021253 Pipe#: 001 County: Craven
Laboratory Performlig Test: ETTEnvmental Inc.
X iron Comments:
i
Slgnatu.!of Ope :torn R8.8121.1115 rge4
Sign: . :o .t. to , Su•ervlsor
IllV MAIL.ORIGINAL,TO:Environmental clences Branch
Division of Water Quality
NC DENR
1621 Mail Service Center
Raleigh,NC 27699-1621
Control Replicates 1 2 3 4 6 6• 7 B
Sur4v1nt# 4 5 5 4 4 5
3 4 X3urvlvsll 100.0%I
Origin# 4 5 6 4 4 5 3 4
Weight(per Original) 0,3825 0.3360 0.3520 0,4900 0.4260 0.4180 0.3887 0.3126 Avg Weight(mg)I 0.3853
Treatment 2 Replicates 1 2 3 4 5 g
7 8
Surviving IS 6 5 5 4 4 4 6 I 3 %Survival I 100.0%I
Ortglna# 5 5 6 4 4 4 5 3
Weight(per Original) 0.3280 0.3840 0.4040 0.3926 0.3550 0.4125 0.3180 0.3025 Avg Weight(mg)[ 0.3821 I
Water Quality Dele
DAY
Control 0 1
2
3 4 ...5 6 7 i
Test Results
pH inllal 8.1 7.9 7.8 7.8 8.2 8.1 7.0
pH Fl mal 7.4 7.5 7.4 7.7 7,6 7.7 7.6
SlgdAcanl Mc ally?
DO Iniial 8.9 8.1 8.8 8.4 8.1 5.9 I 8.0
r Yes No
DO Fi+al 6,4 8.2 6,3 4,1 4,9 4.5 4.9
I I
X
Temp In!gal 24.7 24.6 24.7 24.7 26.4 26.3 26.2
cnect one
Temp Fl ial 28,0 28.0 28.0 25,9 26.1 28.1 28.2
Salinity lnlial 24.7 26.0 24,6 24.7 26.8
26.4 25.2 G•4,th
,M cats t 0.93 I
Treatment 0 1 2 3 4 6 8 7 1
Tatxiar t 1.78
pH Inlial 8.2 7.9 7.8 7,7 8.3 8,1 8.1
Few idly
pH Floral 7.5 7.6 7.5 8.0 7.8 7.7 7,8
Rank Gum
DO Ira el 8.5 6.6 8.6 8.4 B.B 8.7 8.4
Cr t.Value
DO Fl a! 4.1 5.2 4,9 5.0 4.9 5.0
5.7
Tamp leliel 25.0 26.7 26.6 25,7 25.8 26,2 25,6
, PASS FAIL
Temp Fl tal 28,0 28,0 26.0 25.9 28.1 28.1 28.2 I X I
Sanity Int Jal 24.7 24.8 24.8 24.0 25.6 26.6 25.5
Chen/One
Sample Teat Data:
Collection Start D rle 11-Apr-21 13-Apr-21 15•Apr-21 Effluent Teat Concentration: 15%
Grab 5 replicates were eel for each control toot replicate;whom<5 ore ehovn the organleme were teat during renews
Composite(Dungan) 24 hr 24 hr 24 hr 5 replicates were sot for each treatment lest replicate;whore<6 are shown tho organisms wore goat during lane
Conductivity(pmhoslan) 623 845 846
Chlorine(mgt.) <0,05 <0.05 <0.05
Sample Temp.at Rectipt 1,6 0.8 0.2
DWQ Form AT-4(6/99)
Page 2 of 6

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ETT . cHALv OF CUSTODY RECORD
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PO Box 16414,Greenville.SC 2J6t i-t414 !
(364)sn-6942, [phone] Fac(064)877 6938
Shipping Address:4 Cratterrzn Ct.Greer,SC 2.9titU
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Progrrro Containers P2srn�tirc Yarsmctc •
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Special Instructions:
Sample Custody Transfer Record Secure Receipt Sample
Date Time j Relinquished Byy//Orniz_ation f r_ Received By 1 Orrttization Area Temp°C Preserved?
6-11
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COMPOSITE SAMPLING PROCEDURES TEMPERATURE MONTTOIUNC PROCEDURES FOLD TIME PROCEDURES
Composite samples must be collected aver a 24 hour period. Sample temperature during collection and transport must be between For toalcity testing the sample must first be used within 36 hours
Time Proportional:I sample each hour for 24 hours.Equal vol 0.0 and 6.0°C.Samples must not be frozen.Use water ice in sealed bags. of sample collection(completion of composite sample).
or at minimum I sample every 4 hours over 24 hours. Sample may not be used after 72 hours from sample collection.
Flow Proportional:As per instructions in NPDES 1

ETT
CHAIN OF CUSTODY RECORD
•
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PO Bac 16414,Greenville,SC 2950Cr7414 •
[phone], [phone] Fax[phone]
Snipping Address 4 Craftsman t .Greer,SC 29550
WWW.tt,,NVS=NM WTAL.CCM
Client - SI S
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Facility: 1 I t
V� 1 Whale Effluent Tasioty -,-
State: t'v3( PIPDES m K3C, (DJ!l 2- Acute Chroak Test Or`uaI
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SAiv>PLE ID U a ^ c.. ,, a •1-uax - - 6 o` = c - o N
Campw!u Sort Dine Time Samptccoaiat Data Time Galleried by (3 ri7 ,Z o O > u tenth " `� ' -I - G_�- ? = +,_,
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Date Time Relinquished By/Oritanisarion Received By I Organization Area Temo'C Preserved?
!I h`b1_QB�o . .,,a L 10 6 .
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COMPOSITE SAMPLING PROCEDURES TEMPERATURE AMONITORING PROCEDURES 'HOW TIME PROCEDURES
Composite samples must be collected over a 24 hour period. Sample temperature during collection and transport must be between For toxicity testing the sample mast first be used within 36 hours
Time Proportional:1 sample each hour for 24 hours.Equal valor 0.0 and 6.0°C.Samples must not be frozen.Use water ice in sealed bags. of sample collection(completion of composite sample).
or at minimum 1 sample every 4 hours over 24 hours. j Sample may not be used after 72 hours from sample collection.
Flow Proportional:As per instructions in h1PDES permit

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PO Box 16414,GmenvWe,SC 29806-7414
1 18/7-044Z (&SJ 89 i-t927 r ..(804)877 882
Shipping Address:4 Craftsman Ct.Greer,SC 29650
WWW.Cr1 CW,PONMSNTAL.COn
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Special Instructions:
•
Sample Custody Transfer Record Secure Receipt ( Sample
Date Time Relinquished By!Or anization Received By/Organization Area Temp°C Preserved?
q--t�-al (430 Dom`+i, /0 .y of rKfe,106fr ,ta tto I 041(3 i 2., OctDD ! t-(.2
COMPOSITE SAMPLING PROCEDURES TEM'ERATURE MONITORING PROCEDURES HOLD TIME PROCEDURES
Composite samples must be collected over a 24 hour period. Sample temperature during collection and transport must be between For toxicity testing the sample must fast be used within 36 hours
Time Proportional:1 sample each hour for 24 hours.Equal volur 0.0 and 6.0°C.Samples must not be frozen.Use water ice in sealed bags. of sample collection(completion of composite sample).
or at minimum I sample every4 hours over 24 hours. Sample may not be used after 72 hours from sample collection.
Flow Proportional:As per instructions in NPDES permit

•
,:'„' .-'envtronmen a,Inc.
(E64)677-6442 .FAX(864)8?7.6938
P.O. Box I E414.Greene Ile, SC 29606
4 Craftsman Coal,Grunt,SC 29650
Americamysis bahia Survival and Growth Test
EPA-821-R-02-014 Method 1007
Client: CITY OF HAVELOCK
Facility:WWTP
NPDES#:NC0021253
Test Date: 13.1u1-21
Laboratory Sample ID#: T59615 ,
Test Reviewed and Approved By:
4/4 rat, 7. .
Robert W.Kelley,Ph.D. Patrick D.Timms
President QA/QC Officer
1
•• Certification#E87819 SCDHEC Certification#23104,
Test results presented in this report conform to all requirements of
NELAC,conducted under NELAC Certification Number h$7819
Florida Dept.of Health.Included results pertain only to provided samples. NCDENIZ certification# 022
r
Page 1 of 6

Effluent Toxicity Report Form -Chronic Mysidopsis Pass/Fail
Facilit : Havelock Date: 13-Jul=21
NPDES# NC0021253 Pi.e#: 001 County; Craven
Laboratory Perform in T st: ETT Environmental Inc
x Comments:
signature of Operator I nsl Charge
`x f /
Signature of Laboratory Supervisor
MAIL ORIGINAL TO: Environmental Sciences Branch
Division of Water Quality
NC DENR
1621 Mail Service Center
Raleigh,NC 27699-1621
Control Replicates 1 2 3 4
5 6 7 8
Surviving# 4 5 4 5 5
4 I 5 5 I %Survival( 97.4%
Original# 4 5 6 5 5 4
6 5
Weight(par Original) 0.285 0.298 0.266 0.318 0.350 0.313 0.416 0,338 Avg Weight(mg)I 0.323 I
Treatment 2 Replicates .- 1 2 3 4 5
6 7 6
Surviving# 5 5 4 5 4
5 5 5 ^l.SuovalI 97.4%I Original# 5 5 4 5 5 5
5 8
Weight(per Original) 0.362 0.272 0.348 0,340 0.408 I 0.380 0.428 0.388 Avg Weight(mg)I 0.363
Water Quality Data
Day
Control 0 1 2 3 4 5 6.
7 _ Test Results
pH Initial 7.6 7.7 8.0 7.9 6.1 8.0 7.9
pH Final 7.7 7,4 7.4 7.4 7.4 7.4 7.9
Significant Mortality?
DO Initial 7.1 7.1 7.0 8.3 6.3 6.3 6.5
Yes No
DO Final 6.8 4,1 4.8 5.2 5.1 5.2 5.4 I_ f X J
Temp Initial 25.2 25,5 25.8 25.5 25.4 26.5 26.6
1 Check One
Temp Final 26.0 28.1 28.1 28.0 28,1 28.1 25.7
Salinity Initial 27.2 27.0 26.3 22.7 23.6 23.6 23.4
i Growth
Cale. I -1.71 i
Treatment 0 1 2 3 4 5 6 7
Tabulart , 1.76
pH initial 7.8 7.8 8.0 8.0 8.1 8.0 8.0
Fecundity
pH Final 7.7 7.6 7.6 7.8 7.7 i 8.0 Rank Sum
DO Iniryai 7.0 7.0 6.9 6.6 8.6 6.8
_ cfit.Value
DO Final 4,9 4.5 5.2 5.1 5.2 5.1 5.0
Temp Initial 25.0 25,4 26.0 25.3 25.6 26.6 26.6
PASS FAIL
Temp Final 26.0 26.1 26.1 1 26.0 26.1 28,1 26.7 X I
Salinity Initial 27.1 27.0 25.3 21.5 ' 20.6 20.9 20.0
Check Ono
Sample Test Date:
Collection Start Date 11,11.1.21 13-Jul•21 15-Jul-21 Effluent Test Concentration: 15% '
Grab _ 5 replicate,were set for each control test replicate:where<5 are shown the organisms were lost during renew:.
Composite(Duration) 24 hr 24 hr 24 hr 6 replicates Were set for each treatment test replicate;where<
Conductivity(mhos/cm) 654 637 a 5 are shown the organisms were tout during rene
856
Chlorine(mglt.) <0.05 <0.05 <0.05
Sample Temp.al Receipt 1,5 1.5 1.0
DWQ Form AT-4(6/99) Ili
Page2of6
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CHAIN OF CUSTODY RECORD
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State: 9Vf-� 1\'PDES r: Al,1 C.00Th r
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COMPOSITE SAMPLING PROCEDURES TE/IPER:1TURE MOV7TORING PROCEDURESr a,.
HOLD
TIME PROCFDJ_,�o
Composite samples must be collected over a 24 hour period. Sample temperature during collection and transport must be between For toxicity testing the sample must first be used within 36 hours
Time Proportional:1 sample each hour for 24 hours.Equal volm 0.0 and 6.0°C.Samples must not be frozen.Use water ice in sealed bags. ofsample collection(completion of composite sample).
or at minimum I sample every 4 hours over 24 hours. Sample may not be used after 72 hours front sample collection.
Flow Proportional:As per instructions in NPDES permit.

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(864)877—S942, [phone] Fax[phone]
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www.er-m,,,RON.c,, .COM
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State: NC_ NPDLS r: sv.)L66 21 Z-".3 Whole Effluent Toxicity
Acute Test Organisms
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COA POSITE SAMPLING PROCEDURES MONITORINGI
T rL1PERr1TURE PROCEDURES HOLD TLIIEPROCFJU.R.S
Composite samples must be collected over a 24 hour period. Sample temperature during collection and transport must be between For toxicity testing the sample must first be used within 36 hours
Time Proportional:1 sample each hour for 24 hours.Equal volui 0.0 and 6.0°C.Samples must not be frozen.Use water ice in sealed bags. of sample collection(completion of composite sample).
or at minimum I sample even 4 hours over 24 hours. Sample may not be used after 72 hours from sample collection.
FIow Proportional:As per instructions in I\'PDES permit

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PO Box 16414,Greenville,SC 29506-7414
[phone], [phone] Fa [phone]
Shipping Address:4 Craftsman Ot,Greer,SC 29650
www-GITENVIRONP-ICNTAL-CONI
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COMPOSITE SAMPLING PROCEDURES TEMPERATURE MONITORING PROCEDURES HOLD TIME PROCEDURES
Composite samples must be collected over a 24 hour period. Sample temperature during collection and transport must be between For toxicity testing the sample must first be used within 36 hours
Time Proportional:1 sample each hour for 24 hours.Equal volut 0.0 and 6.0°C.Samples must not be frozen.Use water ice in sealed bags, of sample collection(completion of composite sample).
or at minimum I sample every 4 hours over 24 hours.
!Sample may not be used after 72 hours from sample collection.
Flow Proportional:As per instructions in NPDES permit

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envtrnnmanta.Inc.
[phone] .FAX(864)877_G938
P.O. Box 16414,Greeevlle,5C 28605
4 Craftsman Calri,Grier,SC 29650
Americamysis bahia Survival and Growth Test
EPA-821-R-02-014 Method 1007
Client: CITY OF HAVELOCK
Facility: WWTP
NPDES#:NC0021253
Test Date: 12-Oct-21
Laboratory Sample ID#:T60355
Test Reviewed and Approved By:
Robert W.Kelley,Ph.D. Patrick D.Timms
President OA/QC Officer
edR/ ,,Certification#E87819 SCDHEC Certification#23104
Test results presented in this report conform to all requirements of
NELAC,conducted under NELAC Cenifcation Number E87819
Florida Dept.of Health.Included results pertain only to provided samples. NCDENR Certification# 022
Page i of 6

Effluent Toxicity Report Form -Chronic Mysidopsis Pass/Fail
Facili : Havelock Date: 12-Oct-21
NPDES# NC0021253 Piae#: 001 Coun Craven ,
Laboratory Performing Test: ETT'Environmental Inc:
Comments:
X
SJgnatu ,„p ra c-1F43 pens ble Charge
X -
Signature of Laboratory Supervisor' m
MAIL ORIGINAL TO: Environmental Sciences Branch
Division of Water Quality
NC DENR
1621 Mail Service Center
Raleigh,NC 27699-1621
Control Replicates 1 2 3 4 5 6 7 8
Surviving# 3 5 5 5 5 6 4 3 %Survival 100.0%
Origins/# 3 5 5 5 6 6 4 3
Weight(per Original) 0.203 0.196 0.306 0.192 0.320 0.240 0.245 0.300 Avg Weight(mg)I 0.250 ,
Treatment 2 Replicates 1 2 3 4 5 6 7 8
Surviving# 5 5 5 4 4 6 5 3 %Survival I 100.0%I
Original# 5 5 5 4 4 5 5 3
Weight(per Original) 0.228 0.252 0.240 0.250 0.240 0.246 0.228 0.257 Avg Weight(mg)r 0.243-1
Water Quality Data
Day
Control 0 1 2 _ 3 4 5 6 7 Test Results
pH initial 8.1 8.3 8.0 8.0 7.9 8.4 6.2
pH Final 7.9 7.7 7.8 7.3 7.8 8.1 8.0 Significant Mortality?
00 initial 7.6 6.1 7.1 7.2 7.0 6.5 6.6 _ Yea No
DO Final 4.6 5.4 6.9 5.1 4.3 5.0 6.3 X
,
Temp initial 24.7 25.5 25.5 25.8 25.5 25.3 25.1 Check One
Temp Final 26.9 26.1 26.1 28.1 28.0 25.7 25.9
Salinity Initlai 25.8 26.0 25.6 25.4 24.9 24.9 25.0 Growth
.�_ Cale t 0.41
alMNINUMIIIINNI
Treatment 0 1 2 3 4 5 6 7 Tabular i 1.76
pH Initial 8.3 8.4 8.1 8.1 8.0 8.1 8.2 Fecundit
pH Final 8.0 7.8 7.9 8.0 8.0 7.9 8.1 Rank Sum
DO Initial 8.0 8.0 7.0 7.3 7.0 6.6 8.7 Cr1L Value
DO Final 4.1 5.7 5.4 6.8 5.2 5.3 6.3 _
Temp Initial 25,0 25.7 25,8 25.7 25.5 25.2 25.4 PASS FAIL
Temp Final 25.9 26.1 26.1 26.1 26.0 25.7 25.9 LX____L__.
Salinity initial 23.8 23.7 24.5 24.3 24.8 24.9 24.4 Check One
Sample Test Date: 12-Oct-21
Collection Start Dale 10.Oct-21 12-Oct-21 14-Oct-21 Effluent Test Commntration: 15%
Grab 6 replicates were set for each control test replicate;where<5 are shown the organisms were lost during renew.
Composite(Duration) 24 hr 24 hr 24 hr 5 replicates were set for each treatment test replicate;where<5 are shown the organisms were lost during rene
Conductivity(prrdlos/cm) 704 713 713
Chlorine(rngiL) <0.05 <0.05 <0.05
Semple Temp.at Receipt 1.5 0.8 0.2
DWQ Form AT-4(6799)
Page 2 of 6

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a to to to
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.' . r, ClIALN OF GUSTO;DIY RECORD
r•x„'�' •,- tom '�-ui ''°aF-' _
`,kip..°_.r'"a?", ^_rSiC:9 fl Past o_
^PO Box 16414,Greenville,SC 29 6 0 6-741 4
[phone], [phone] Fa c(864)877 6938
Shipping Address:4 Craftsman Ct,Greer,SC 29650
•
W W W.crrCNV I RO N HLNTALCOwt
Client' t �
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i1' I a4 t4Av LbCk Program a Containers Preservative Parameters
Facility:(,/ E V f
W -it Whol
e Lml'CC!Toxicity Cth' C
State: Wt. NPDES 4: /C„0D4..t „�}°� Acute cChronic• TestOreanisms •
'_o C
(Composite only) (Grab or Composite) < $ = J J
U - •c I-H2504 _ E _ = 5 s
c Sion,and print below 3 U HCt <
O = :,HNO3s v cr ^ -� 7 6
the dotted lime = E c _ y 4-NaOH P- a a = � _ -- N _
c B.
SAMPLE ID O CompwitcStart Date Time Sample Ccltcctioc Date Time Collected by U ci5 co Z F U > 5.6thec`. ' CJ U ui Q 2 :A ._. U 1- 3 2 Chernicat Analysis&Other
ftnivAotAS - 5 acute-tLtls�
A
0 A !
ISpecial Instructions:
! Secure Receipt Sample
!Sample Custody Transfer Record
I
l Date Time Relinquished By/Orsanimtion Received By/Orsanintion Area Temp'C Preserved?
I\1.A....\ Ilta.f+ I Obit,'Ar11: s / LSI'l O HgdPA)a
—f 4 i4. 1 CIT /bf h/ f 010 ISl
1
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COMPOSITE SAMPLING PROCEDURES TEMPERATURE MONITORING PROCEDURES HOLD TIME PROCEDURES
Composite samples must be collected over a 24 hour period. Sample temperature during collection and transport must be between For toxicity testing the sample must first be used within 36 hours
Time Proportional:1 sample each hour for 24 hours.Equal volut 0.0 and 6.0°C.Samples must not be frozen.Use water ice in sealed bags. of sample collection(completion of composite sample).
or at minimum I sample every 4 hours over 24 hours. Sample may not be used after 72 hours from sample collection.
I

#;.. „^ CHAIN OF CUSTODY RECORD
[.�N�iw�'rviararnr+:'i%..,,f,e-- P 1�"2?Y - f
Paso
o_
PO Box 16414,Greenville,SC 29 6 0 6-741 4^
[phone], [phone] Fast(864)877 6935
Shipping Address:4 Craftsman Ct.Greer,SC 29650
WWW-C T TCNVI R O NM CNTAL.0 OM
Client:ClT? �� }HAvEL PLC
Program Containers Prescn•ativc Paramcicrs
Facility:I t AsTS Oti I f f
�L Whole Effluent To=ieitti�
State: NC, ItP DES 4:fig,ab a1;...53 n
AculcChroric Test Organisms '
•
— d n
U (Composite only) (Gabor Composite) < o - U rJ , o _ z
Sipe,and Print below 3 o 2.HCL = .1-__.-
o _ a' _
v the dotted line __ "' U `—' h = a-UoOti = c o - 'g. -
SAMPLE ID Cc cpc a Start Date Time 5nnpk Col/cc-Lion Dxte urns Ccllcctcd by U l r% c Z E V > 6.0i cr < < .Z.: U U ^ n T U = > 2 Chemical Analysis L Other
AlliP� I
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rGTt a1�—
.ffLtjcA [0.1). I to.I,.X‘ \��. _--- V GI! '�� 11" BUD B
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Special Instructions:
Sample Custody Transfer Record Secure Receipt Sample
Date Time Relinquished By I Organization Received By I Organization Area Temp'C Preserved?
IC.''$.at lea pMU1�/A 'f C Tytsfk4va ot.k 6 f • c )o 4 o (c
COMPOSITE SAMPLING PROCEDURES TEMPERATURE MONITORING PROCEDURES I HOLD TIME PROCEDURES
Composite samples must be collected over a 24 hour period. Sample temperaetre during collection and transport must be between For toxicity resting the sample mus firs be used within 35 hours
Time Proportional:1 sample each hour for 24 hours.Equal v0I1.11 0.0 and 6.0'C.Samples must not be frozen.Use water ice in sealed bags. of sample collection(completion of composite sample).
or at minimum 1 sample every 4 hours over 24 hours. Sample may not be used after 72 hours from sample collection.
Flow Proportional:As per instructions in NPDES permit-

.. . ..________. ..________________ ____ — ------ _______ ________.____ __ ______________.
ETTCHAIN OF CUSTODY RECORD
f,i'*� tW dy e�?1..7,,� 11: tiy,y.
PO Box 16414,Greenvale,SC 29606-7414
[phone], (BOO)891-2325 Fax[phone]
Shipping Address:4 Craftsman Ct,Greer,SC 29650
WWW.CTTCN VIRONMCNTAL.COM
Client: -tri bC H VELoc.k
Program Containers Preservative Parameters
Facility:``'',,jj��.p� yy
WPO e*WA TF a Whole Effluent Toxicity n
State: WC, NPDES P.: WU an_' -3 Acute Chronic Test organisms i
(Composite only) (Grab or Composite) 8 o - U , - J o _ Z t
U d o = 1.YS0. E = o ._c o. s
,= Sign,and Print below = r o Z.HCL n _ an .m _ E N
E the dotted line = E N U o - a�V H o c a s _ —
N � •� ` N
U D ., O O O O V $s zmlc G V .- .. .' G _• T= r� _
SAMPLE M � Compositc Start nate Time SAmptcContaion Dote Time Collected by CJ to c Z : i= U > 6.0d,,,. <�< CJ U C.) d ,_ 7 of = U 1- Chemical Analysis&Other
if wE C to.14.�1 t000 th.1 -° 4 lam 1,, % a V 51/ v
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Special Instructions: co i 1 e GTl•
e'A ii f OS, , 61) 01119.zf
Sample Custody Transfer Record Secure Receipt Sample
Date Time Relinquished By I Oreanization Received By/Organization Area Tema°C ?reserved?
tO•i5.D1 i LA q 0W1/90141201$ «Ty bF U4vakk
to-ve_24 (ifrd Feces r ( ! Q,2-
COMPOSITE SAMPLING PROCEDURES TEMPERATURE MONITORING PROCEDURES HOLD TIME PROCEDURES
Composite samples must be collected over a 24 hour period. Sample temperature during collection and transport must be between For toxicity testing the sample mast first be used within 36 hours
Time Proportional:1 sample each hour for 24 hours.Equal yolul 0.0 and 6.0°C.Samples must not be frozen.Use water ice in sealed bags. of sample collection(completion of composite sample).
or at minimum I sample every 4 hours over 24 hours. Sample may not be used after 72 hours from sample collection.
Flow Proportional:As per instructions in NPDES permit _

a.imtrocsn enta9.litr.. (L 4)1177 GQ42.FAX{$t 4) 7'7.603t
P.O.Box 16414,Green Me,SC 29605 4 Craftsman Couri,Gram,SC 29650
Amerieamysis bahia Survival and Growth Test
EPA-821-R-02-014 Method 1007
Client: CITY OF HAVELOCK
Facility:WWTP
NPDES#:NC0021253
Test Date: 25-Jan-22
Laboratory Sample ID#:T61096
Test Reviewed and Approved By:
Robert W.Kelley,Ph.D. Patrick D.Timms
President QAIQC Officer
r 1
'� . '��..j' !Certification#E87819 8COHEC Certification 423104
Test results presented in this report conform to all requirements of
NLLAC,conducted under NELAC Cenifreatlon Number E87819
Florida Dept.of Health.Included results pertain only to provided samples. NCDENR Certification# 022
Page 1 of 6

Effluent Toxicity Report Form-Chronic Mysidopsis Pass/Fail Date: 25-Jan-22
Facili : Havelock NPDES it NC0021253 Pi e#: 001 Coun : Craven
La rmi g je t: ETT Environmental Inc. Comments:
'n�
X _ _
Signature of Operator in Responsible Charge
X ), fit 4 -
Signature of Laboratory Supervisor
MAIL ORIGINAL TO: Environmental Sciences Branch
Division of Water Quality
NC DENR
1621 Mail Service Center
Raleigh,NC 27699-1621
Control Replicates 1 2 3 4 5 6 7 8
I
Surviving# 5 5 5 4 4 4 6 6-H %Survival 1 u0.0%
Original# 5 5 6 4 4 4 5 5
Weight(per Original) 0.306 0.268 0,362 0.335 0.268 0.353 0.334 0.3031 Avg Weight(mg) 0.315
Treatment 2 Replicates 1 2 3 4 5 6 7 8
Surviving# 5 5 5 5 I 5 5 4 5 %Survival 100.0%
Original# 5 6 6 6 5 5 4 5
Weight(per Original) 0.29 0.362 0.35 0.288 0.37 0.386 0,415 0.366 Avg Weight(mg) 0.351
Water Quality Data
Day
Control 0 1 2 3 4 5 6 7 Test Results
pH Inittai 8.2 8.3 0.2 8.3 8.3 8.3 8.3
pH Final 7.8 7.7 7.7 7.9 8.0 7.9 7.6 Significant Mortality?
DO Initial 7.0 7.2 7,1 6.7 6.8 6.3 6.5 Yes No
DO Final 8.5 8.3 4.1 5.3 4.8 5.2 4.7 r-T X 1
Temp Initial 24.7 25.4 25.5 25.1 25.3 25.1 25.3 Check Ono
Temp Final 25.9 28.0 25,7 25.9 25.9 _ 25.9 25.9
Salinity Initial 25.0 24.8 24.6 24.3 24.4 24.4 24.5 Growth
Cato. I -2.56
Treatment 0 1 2 3 4 5 6 7 Tabular t 1.76 j
pH Initial 8.2 8.1 8.1 8.4 8.3 8.3 8.3 Fecundity
pH Final 8.0 7.8 7.8 7.9 8.0 8.0 8.0 Rank Sum
DO Initial 6.8 6.8 6.8 6.7 6.8 6.5 6.7 Cdl.Value
DO Final 5.1 5.2 4.1 4.7 4.5 4.8 6,2
Temp initial 25.0 25.2 25.4 25.3 25.6 _ 26.2 25.4 PASS FAIL
Temp Final 25.9 26.0 26.7 25.9 26.9 25.9 25.9 I X I
Salinity initial 24.8 24.9 24.6 24.6 -24.9 25.1 26.1 Check One
Sample Test Date: 25-Jan-22 1505- 1-Feb-22 1343
Coliaction Start Date 23-Jan-22 25Jan-22 27-Jan-22 Effluent Test Concentration: 15%
Grab 5 replicates were set for each ccnlrol test replicate;where<5 are shown Lhe organisms were lost during renews
Composite(Duration) 24 hr 24 hr 24 hr 5 replicates were set for each treatment test replicate;Mere=5 are shown the organism were lost during cane
1 Conductivity(pmhoslcm) 575 670 588
Chlorine(mg/1.) <0.05 <0.05 <0.05
Sample Temp.at Receipt 1.2 0.5 0.1
0WQ Form AT-4(6199)
Page 2 of 6

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CHAIN OF CUSTODY RECORD
v. 0_2_ f Pz e of
PO Box 16414,Greenville,SC 28606 74t4 It
[phone], [phone] Fax[phone]
Shipping Addtrss.4 Crafts,r�„Ct.Greer,SC 29850
WWW.ETTCNViRO NH CIl&VCOM
CIient:r^-! Or ��l t 6 � I
l.°.', (t -p/ 91 /It itiOC.I` Program Containers Preservative; Parameters
Fa /C C J 'Whole EmocntTozic p• II1
(State: r�I'DIS�. V l.na f`e ` I n
Acute Chronic Test Or:maisms I
_ d I —
o V _
U (Composite only) (Grab or Composite) . o c — o .� U G n
$ v _ o Z
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ci the dotted Iine — U n s-rA os c p. _ '— j{v o = ; •=n An\SOH m = p .p _ = , o 2 ` ti p t
Xi
SAMPLE ID . COMM./It M./It stun Date Time sample C°llc¢i°n Date Time Colic try 0 Ci h z = U > 8 $ znAc v 'Z - V . = - >.= _ —
o-0d= F <lU U U t] >= 2 ;q _ U 3 Z Chemical Anzlysis&Other
c f a- -ak I o lecol_D ✓ 5 I ® Comet;+�Q n..E_Fik_kf A �a ��vinA,5 _ E ► E I IV IL :�� (D1o��A
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Sample Custody Transfer Record
Secure Receipt Sample
Date Time Relinquished By/Organization jJ Received By I Or_aanization Area Temp°C , Preserved?
° ° II D{i'UI •
QCIZ lCi ( I
Dti '/.S) 0°lced 0,161Clitl'id 6031/10-1T I l 1. 2
l I f
COMPOSITE SrIMPLING PROCEDURES TEMPERATUREMONITORING PROCEDURES HOLD TIME PROCEDURE'S'
Composite samples must be collected over a 24 hour period. Sample temperature during collection and transport must be between For toxicity testing the sample must first be used within 36 hours
Time Proportional:1 sample each hour for 24 hours.Equal volur 0.0 and 6.0°C.Samples must not be frozen.Use water ice in sealed bags. of sample collection(completion(pi-composite sample).
or at minimum I sample every 4 hours over 24 hours. Sample may not be used a.ter 72 hours from sample collection.
Flow Proportional:As per instructions in NPDES pennit

. _. -...._
._._ _ _ ______ ______ .._
E• ,. ...,T
s""5,,. c - OF CUSTODY RECORD
PO Elm 16414 Gretanvme SC;29506-7414 jPa?e of
[phone], [phone] Fax[phone] L
Shipping Address 4 Craftsman Ct,Geer,SC 29650
w W W-CTT6N V I R O NM LNTAL.LO M
!Client:/s�� ('
t-,-- Of lock Program Containers Preservative: I
Parameters
Facility:` / leWkfer
State: Al ( NPDES#: Wr�" i+�d ri'hoteGf7lacacTozic q
1 Acute Chronic Test Or
ganisms
Q 1 ^ ,
ti
U (Composite only) (Grab or Composite) o o U 'o S
o U
Sign,and Print below zl- o. _ m L m
the dotted line `_' -too n ' `_' in _ ? _
l q ast�ott ° o _ = o .= i L N Q
SAMPLE ID C°mpa mSm z mu Time Sample CnIlcn oa Date Time Coale b e — S 5'Z°Ac t o = ^ " ' B T I T J E
Y Y...� ;16:8
°' G-0:h, v U U t 2 :q = U = > 2 Chemical Analysts LO:her
LL—
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Special Instructions:
1Sample Custody Transfer Record
Secure Receipt Sample
Date Time Relinquished By/Organization Received By/Organization Area Temp Preserved?
+t �' 1 b • '�l OEM A . , t 1-- Q-P LifkA t,k-* I I
,i5,-, ,,p-i- i� I Q....,...___
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COMPOSITE SAMPLING PROCEDURES TEJL1PERITURE MONITORING PROCEDURES HOLD TJ E PROCEDURES
Composite samples must be collected over a 24 hour period. Sample temperature during collection and transport must be between For toxicity testing the sample mug.5r st be used within 36 hours
Time Proportional:I sample each hour for 24 hours.Equal volur 0.0 and 6.0°C.Samples must not be frozen.Use water ice in sealed bans. ofsarnple collection(completion of composite sample).
or at minimum I sample every 4 hours over 24 hours. Sample may not be used after 72 hours from sample collection.
Flow Proportional:As per instructions in NPDES permit-

._____
_ ______ _______
ETT
cHA.i OF CUSTODY RECORD
Page I ofPOBox 16414,CSrsenWtl ,SC 2 9 6 0 8-741 4
[phone], [phone] Fax[phone]
Shipping Address:4 Craftsman Ct,Greer,SC 29850
WWW.CTTC'N V IRG NM GC:W..=M
Client \
Pacilify: ��(� � Program Containers Preservative
Parameters
"ii I
Whole st Orgo
State: NPDES I
touts Chronic 2crt Organisms
•
d
Z
(Composite only) (OraborCnmposite) a' — o CI =�
v < o o - U Ft; -
Sion,and Print below 3 = -to — Z.N� _ — c U o
El
c3 the dotted line E U o `' 3•xi o>" ° ° _ `^ ` = ' <
= F `•2 4.lS0ri = U o o E o - N 2
SAMPLE ID o Composite to Start Date Time Sample Collection Dote Time Coi!ected by U is c' Z o a`. 0 j = 3=7n,tc F o = = = T. --,,? i F�
6•Dbiz < U U U E. :r�,_. U =1 Chemical Analysis Lgthcr
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6- 11:er\ 1. :?-d Ir �> l �� v ai/ (, v' i J G
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Special Instructions:
i
• Sample Custody Transfer Record Secure Receipt Sample
Date Time RelinTi ished By!Organ 'on Received By!Organization Area Temp°C Pr served?
"ram? i 7 ,/ OiNiPalc,lr
/17--97--- I 1 0. f
1
COMPOSITE SAMPLING PROCEDURES TEMPERATURE MONITORING PROCEDURES HOLD TIA E'PROCEDURES
Composite samples must be collected over a 24 hour period. Sample temperature during collection and transport must be bet ecn For toxicity testing the sample must 11.sL be used within 36 hours
Time Proportional:1 sample each hour for 24 hours.Equal volur 0.0 and 6.0°C.Samples must not be frozen.Use water ice in sealed bags. of sample collection(completion of composite sample).
or at minimum I sample every 4 hours over 24 hours. Sample may not be used after 72 horns from sample collection.
Flow Proportional:As Der instructions in NPDES permit I

ET,. en i.lm:. (c6d}a77- 42 .FAX[phone]
P.O.Dox I6414, GieenvHe. SC 25606 4 Craftsman Cant.Greet.SC 29650
Al:r errllealnayslls b&Fria Smrviva1< and Growth Test
E]PA--82I-R-02-014 Method 1007
Client: CITY OF HAVELOCK
Facility:WWTP
NPDES#: NC0021253
Test Date: 05-Apr-22
Laboratory Sample ID#:T61631
Test Reviewed and Approved By:
Robert W.Kelley,Ph.D. Patrick D.Timms
President QAJQC Officer
x .t
Certification#E87819 SCDHEC Certification#23104
Test results preac..:ed in this report conform to all requirements of
NELAC,conductri ender NELAC Certification Number E87819
Florida Dept.of H,alth.Included results pertain only to provided samples. NCD E N R Certification# 022
Page 1 of 6

Effluent Toxicity ire, t-t Form -Chronic (Viysidopsis Pass/Fail Date: 05-Apr-22
Facility: Havelock NPDES II NC0021253 Pipe_#: _001 Coun _ Craven
Laboratory Performing Test: 1.! I(ii(milt rti=ni 1'l pn iA, I Comments:
x _ I --
Sign ttlre of Opera rin f espo ibh Charge
Signature of Lab& toorry SupetvisZ7i'" . -
r .J Z}la� .1,r,C. !.6 ;✓nvironmental geieylces Iira11e11 -----
Division of Water Quality
NC DENR
1621 Mail Servic.c Center
Raleigh,NC 27699-1621
Control Replicates 1 2 3 4 5 6 7 8
I
Surviving# 5 j 5 5 4 ' 5 ' 5 5 5 %SumvalI 100.0%]
Original# 5 , 5 tl 5 I 4 5 5 5 5
Weight(per Original) C 2;n 1. 12 ! 3.342 . C.303 i 0.256 0.338 0.290 0.25'0 Avg Weight
Treatment 2 Replicates , 2 3 4 5 6 7 8
S:rrvving17 -4 5 4 , c 1_ 5 I 5 I 5-1 %Survival 100.0°fo
Onglnal# , ' o 4-- •-_�5 I 5 I+5 5
Weight(per Original) L0.348 -_ 6.336 I 0.284 f 0.335 i 0.296 I 0.324 I 0.306 I 0.264 t Avg Weight(me) 0.312
f Water Quality Data
Day
Control 0 2 3 4 5 6 7 Test Results
pH Initial 8.3 8.2 I 8.5 8.2 8.2 8.3 8.3
pH Final 8.0 I 8.2 [ 8.0 8.1 1 7.9 7.9 7.8 Significant Mortality?
1
DO Initial 4.0 6.8 6.2 , 6.5 6.5 6.3 65 Yes No
l.
DOFinalI 6a 46 55 5.4 I 5. I 4.7 5.3 �-1 X
Tern?Initial 2 ? ? 4 26.2 25 3__-', 2F.4 2E 6 25.3 I Check One
Temp Final 25.6 • 25.3 i 25.6 , 25 6 25.8 i 25.7 I 25.9
Salinity In:bat! 25.4_____ 25_.1 26.2 26.2 26.1 26.5 1 26.4 I Growth
Cabo. t -0.63
Treatment 0 1 _ 2 3
- _ __ _.__. 4 5 6 7 Tabular 1.76 _J
pHInita 33 2 --a5_ 5_2 8.2 8.2 I 6.4 I Fecundity
pH Final I =.4 _ 8 4 C.1 5.2 I 3.0 8.0 8.0 Rank Sum
DO initial I 6.4 „64 2 6.5 _4 5.3 ( 5.5 CriL Value _,
DO Final -'µ a
i 5.2 4.8 I 6.3 5.4 I 4.6 ( 4.7 5.5 Torn?Initial 25.0 25.4
25.5 25.3 25.2 I 25.4 _ 5.5 2 `
1 1 PASS FAIT.
11
Tam.?Final _ 25 25.3 25.5 25.5 i 25.3 i 25.7 1 25.9 X
Salinity Initial 24.5 _ 24.3 24.3 24.6 25.2 I 25.3 25.4 I _J Check One
{ Sample, - - Test Dale: 05-Apr-22 L_____
Collection Start Date 03-A?r-22 C6-.',3:•22 07•A?r-22 I Effluent Test Concentration: 15%
Grab I -__.-. _ 8 replicates par traatnent 15 myslds per replicate
Conposae(Cwation) 24 I.: :; .r 2;hr Where<5 rmsids for original#are shown,the organisms were lust during renewal or cannibalized.
Conductivity(pmhoskm) 643 671 i 621 I
Chlorine(mg/L) <0,05 <C.C,S f <0.C5
Sample Temp.at Receipt ::. .2 1
DWO Form AT-4(6/99)
Page 2 of 6

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CH.A.r..I1 OTT CUSTODY PPCORD
?'Lro T. e�+° 1P5.c of k
7 Far 15414,C eenvl4c.SC 29606 7414 1.._.__ 1
64)877-6942, [phone]
Chipoino Addruss:4 Cra0 srnan Ct,Greer,SC 29650 ,
www.ettlab.srg
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Satrple Custody Transfer Record ____. •4^— ��— Secure Receipt Sample
Date Time Relinquished By/Organization Received Bv/Organization Area Temo'C Preserved?
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COMPOSITE SAMPLING PROCEDURES TEMPERATURE MONITORING PROCEDURES HOLD TIME PROCEDURES
Composite samples must be collected over a 24 hour period. Sample temperature during collection and transport must be between For toxicity testing the sample must first be used within 36 hours
Time Proportional: I sample each hour for 24 hours.Equal volui 0.0 and 6.0`C.Samples must not be&ozen_Use water ice in sealed bags. of sample collection(completion of composite sample).
or at minimum 1 sample even 4 hours over 24 hours. Sample may not be used after 72 hours from sample collection.
Flow Proportional:As per instructions in NPDES permit.

C/TA.IPT OF CUSTODY CO
i'� r ,i ;:` INtge ..... _of #
OEra , , r em.11e,SC29606i4,4
[phone], [phone]
S::ippinn Aocircns:4 Cr5crnan Ct,Greer,SC 2S650
www.ettlab.org
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Composite samples must be collected over a 24 hour period. Sample temperature during collection and transport must be between For toxicim testing the sample must first'be used within 36 hours
Time Proportional: 1 sample each hour for 24 hours_Equal volut 0.0 and 6.0°C.Samples must not be frozen.Use water ice in sealed bags. of sample collection(completion of composite sample).
or at minimum 1 sample every 4 hours over 24 hours. Sample may not be used after 72 hours from sample collection.
Flow Proportional:As per instructions in NPDES permit. I 1

[phone], [phone]
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Shtpp!ng ACr s:4 Cr2:•:eman Ct,Greer,SC 29550
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COMPOSITE SAMPLING PROCEDURES TEMPERATURE MONITORING PROCEDURES HOLD TLDIE?ROCEDUP,ES
Composite samples must be collected over a 24 hour period. Sample temperature during collection and transport must be between For toxicity testing the sample must first be used within 36 hours
Time Proportional:1 sample each hour for 24 hours.Equal voles 0.0 and 6.0°C.Samples must not be frozen.Use water ice in sealed bags. of sample collection(completion of composite sample).
or at minimum I sample every 4 hours over 24 hours. Sample may nor be used after 72 hours front sample collection.
Flow Proportional:As per instructions in NPDES oernlit. 1

env remnants.Inc. (E64)677.6942 .FAX(864)877•6938
P.O.Aox IE414,Greenvale, SC 29606 4 Craftsman Ctxmi,Graer,SC 29660
Americamysis bahia Survival and Growth Test
EPA-821-R-02-014 Method 1007
Client: CITY OF HAVELOCK
Facility:WWTP
NPDES#:NC0021253
Test Date: 12-Jul-22
Laboratory Sample ID#:T62407
Test Reviewed and Approved By:
4old V' i, e t,.'
Robert W.Kelley,Ph.D. Patrick D.Timms
President QAJOC Officer
/eCCIS
YitQ_
Certification 4E87819 SCDHEC Certification#23104
Test results presented in this report conform to all requirements of
NELAC,conducted under NELAC Certification Number E87819
Florida Dept.of Health.Included results pertain only to provided samples. NCDEN R Certification# 022
Page 1 of 6

Effluent Toxicity Report Form -Chronic Mysidopsis Pass/Fail
Facllit : Havelock Date: 12-Jul-22
NPDES# NC0021253 Pipet!: 001 County: Craven
Laboratory Performing Test: ETT Environmental Inc.
Comments:
X
Slgnat rejo ,peratrrin Re ponsible Charge 4Signature of Laborat ry Supervisor
MAIL ORIGINAL TO: Environmental Sciences Branch
Division of Water Quality
NC DENR
1621 Mail Service Center
Raleigh,NC 27699-1621
Control Replicates 1 2 3 4 5 6 7 8
Surviving# 5 5 4 5 5 4 5 4 1 %SurvivalI 94.9%1
Original# 5 5 5 5 5 - 5 6 4
Weight(per Original) 0.226 0.346 0.284 0.368 0.392 0.256 0.280 0393 Avg Weight(ng)I�,37$
Treatment 2 Replicates 1 2 3 4 6 6 7 8
Surviving# 4 5 5 5 3 5 5 4 %Survival 97.3%
Original# 4 5 5 5 3 5 5 5
Weight(per Original) 0.408 0,348 0.350 0.362 0.417 0.350 0.370 0.253 Avg Weight(mg)[ 0..357
Water Quality Data
Day
Control 0 1 2 3 4 5 6 7 Test Results
pH Initial 6,2 8.3 7.7 7.7 7.8 6.2 8.2
pH Final 8.1 7.6 8.1 8.0 7,7 7.6 7,8 Significant Mortality?
DO Initial 6.2 8.8 7.1 7.1 7.0 6.9 6.6 Yes Ho
DO Final 7.4 5.5 6,2 6.2 4.5 4.2 6.3 L_____ X _.1Temp[nibs' 24.7 25.2 25.2 25.3 25.4 25.5 25.4 Check One
Temp Final 25.9 26.4 26.1 26.2 26.0 26,2 28.2
Salinity Initial 25.8 25.8 25.8 25.6 25.9 26.0 26.3 Growth
Caic. t -1.37
Treatment 0 1 2 3 4 5 6 7 Tabular t 1.76
pH Initial 8.2 8.4 7.8 8.0 8.1 8.2 8.1 Fecundity
pH Final 8.1 7.5 8.1 8.1 8.0 7.9 7,8 Rank Sum
DO Initial 6.5 6,5 7.2 7.1 7,7 6.7 6.8 Crit.Value
DO Final 6.5 4.9 5.9 6.1 5.2 4.7 6.9
Temp Initial 25.0 25,6 25.3 25.4 25.5 25.6 25.7 PASS FAIL
Temp Final 25.9 26.4 26.1 26.2 26.0 26.2 28.3 X
Salinity Initial 25.6 25.6 26.8 26.7 26.7 25.6_ 25.7 Chock Ono
Sample Test Date; 12Jul-22
Collection Start Date 10Ju1.22 12-Jul-22 14-Jul-22 Effluent Test Concentration: 15%
Grab :8 replicates per treatment/5 rn clds per reepitcale
Composite(Duration)^ 24 hr 24 hr 24 hr Where<5 myslds for original#are Chown,the organisms were lost during renewal or cannibalized.
Conductivity(pndros/cm) 650 711 692
Chlcrine(mg/L) <0.05 <0.05 <0.05
Semple Temp.at Receipt 1.9 0.1 0.7
DWQ Form AT-4(6/99)
Page 2 of 6

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514347 '(w',11-Lyyv tro¢ am^m�.�;v�5�'� o'r'.„7--
PO Hex 16414,Greenville,SC 29608-7414
[phone], [phone] Fax[phone]
Shipping Address:4 Craftsman Ct,Greer,SC 29650
WWW.CTTGNVI RONMGNTAL.G0M CIicnt:CZty of R d &cj P rogram ConGlincrs ,Preservative Para E
Facility:id4S.T-� W4TE
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Stater 1PD)S K Hr.( ° �� � I ^Acute Chronic• Test 0r_anisau
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SAMPLE ID co, p " tr., 6 o = = 23 s=znAc o 6 =. _.,I -= s�. .
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Sample Custody Transfer Record Secure Receipt Sample
Date Time Relinouished By/Oreaaization Received By/Orzanizaticn Area Temp=C Preserved?
. tl. .a 1`if1 OfVilvADAilsf C-1 y ct .1AV.Loc...k
COMPOSITE S4MPLIWG PROCEDURES TEMPERATURE MONITORJI'G PROCEDURES HOLD TIME PROCEDURES
Composite samples must be collected over a 24 hour period. Sample temperature during collection and transport must be between For toxicity testing the sample must first be used within 36 hours
Time Proportional:1 sample each hour for 24 hours.Equal volur 0.0 and 6.0°C.Samples must not be frozen.Use water ice in sealed bag:;. of sample collection(completion of composite sample).
or at minimum 1 sample every 4 hours over 24 hours. Sample may not be used after 72 hours front sample collection.
Flow Proportional:As per instructions in NPDES permit

ETTCHAIN OF CUSTODY RECORD
a i r 3. . .o ,I - r,? Pale of
PO Box 16414,Greenville,SC 29606-7414
[phone], [phone]
Shipping Address:4 Craftsman Ct,Greer,SC 29550
www.etilah.org
Client: (.'' \f CA V _E—L-0-0‹
��f�/4 p Program Containers Preservative Parameters
wW�[//T 5/' -+V1-E�l
n`h°lo Effluent Toxicity
�•Arc-?a,1i75
State: NPDESAwtc Chronic Test Organ sms
1 , ' 1
ti _ o y t, n
U (Composite only) (Grab or Composite) < J o - U = v — ' z
CC o = _ I�H?s0. ��, = `—�' - — = _'
Sion,and Print below > — = „co a 2"HCI. = = = -- _ co = ' S _ y' s
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Sample Custody Transfer Record Secure Receipt Sample
Date Time Relinquished By!Drganimtion Received By/Organization fare` Temo no Preserved?
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COMPOSITE S4MPLING PROCEDURES TEMPERATURE MONITORING PROCEDURES HOLD TIME PROCEDURES
Composite samples must be collected over a 24 hour period. Sample temperature during collection and transport must be between For toxicity testing the sample must firs be used within 36 hours
Time Proportional:I sample each hour for 24 hours.Equal vole:0.0 and 6.0°C.Samples must not be frozen.Use water ice in sealed bags. of sample collection(completion of composite sample).
or at minimum I sample every 4 hours over 24 hours. Sample may not be used after 72 hours from sample collection.
Flow Proportional:As per instructions in NPDES permit

ETTCH ? OF CUSTODY RECORD
:5,17C„��h _ �____J1____ .:N Page of
PO Box 16414,Greenville,SC 29806-7414 t
[phone], [phone] Fax[phone]
Shipping Address:4 Craftsman Ct,Greer,SC 29650
W W W.CTTCN VI RONM MMAL.0 OM
Client:/ITJ of 1 4JEL �
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Facility: )_r�e, ev.1��
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State:A/4.- NPDES#•:A(c_,Obs4As 3 Acute Chronic Test Organisms
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U (Composite only) (Grab or Composite) . o` - a i J _p = Z
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Sample.Custody Transfer Record Secure Receipt Sample
Date Time Relinquished By/Oreaniza_tion Received By/Organization Area Temp°C Preserved?
7.15.22 11-131) 10EViii'4a1ln15/ ., bf1-( v 04.4
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COMPOSITE SAMPLING PROCEDURES TEMPERATURE M11ON TORING PROCEDURES HOLD TIME PROCEDURES
Composite samples must be collected over a 24 hour period. Sample temperature during collection and transport must be between For toxicity testing the sample must first be used within 36 hours
Time Proportional:1 sample each hour for 24 hours.Equal volut 0.0 and 6.0°C.Samples must not be frozen.Use water ice in sealed bags. of sample collection(completion of composite sample).
or at minimum I sample every 4 hours over 24 hours. Sample may not be used after 72 hours from sample collection.
Flow Proportional:As per instructions in NPDES permit.

(E64)87741a.v42 .FAX(8664)erf 6938
P.O.Box I C'414.Greenv Ile. 5C 29N6 4 Craftsman Cc4il 1,Greer,SC 29650
Americamysis bahia Survival and Growth Test
EPA-821-R-02-014 Method 1007
Client: CITY OF HAVELOCK
Facility:WWTP
NPDES#:NC0021253
Test Date: 04-Oct-22
Laboratory Sample ID#:T63089
Test Reviewed and Appruved By:
Robert W.Kelley,Ph.D. Patrick D.Timms
President QA/QC Officer
„'p I�CUTp�1,
psi ,fit JCertificationf1E87819
;r•`ydoDbcte SCDHEC Certification 423104
Test results presented in this report conform to all requirements of
NELAC,conducted under NEIAC Certification Number E87819
Florida Dept.of Health.Included results pertain only to provided samples. NCDENlt Certification II 022
Page 1 of 6

Effluent Toxicity Report Form -Chronic Mysidopsis Fass/Fail
Facili : Havelock - Date: 04 oct 22
NPDES# NC0021253 Pi.e#: 001 Coun : Craven
Laboratory Performing Test: ETT Environmental Inc.
Comments: •
X
Signature-pf0erator in R ponsl le- Charge
Signature of Laborato -Supervisor
MAIL ORIGINAL TO: Environmental Sciences Branch
Division of Water Quality
NC DENR
1621 Mail Service Center
Raleigh,NC 27699-1621
Control Replicates 1 2 3 4 5 6 7
8
SuMving# 5 5 5 5 5 I 5 ,r 4 %Survival 11 00.0%I
Original# 5 5 5 5 5 6 5 4
,
Weight(per Original) 0.230 0.182 0.300 0.234 0.298 0.260 0.292 0.2875 Avg Weight(mg) 0.26
Treatment 2 Replicates 1 2 3 4 5 6 7 8
Surviving# 5 5 5 I 6 4 , 5 5 4 I
%Survival 1 100.0%
Original# 5 - 5 5 5 4 5 5 4
Weight(per Original) 0.208 0.268 0.308 0.168 0.245 0.250 0.258 0.290 Avg Weight(mg) 0.25
Water Quality Data
Day
,
Control 0 1 2 3 4 5 6 7 Test Results
pH Initial 8.2 8.3 8.2 8.2 8.2 8.2 I 8.2
pH Final 8.2 8.2 7.9 7.9 7.8 7.9 7.7 Significant Mortality?
DO Initial 7.7 7.1 7.4 7.4 7.3 6.6 7.1 Yes No
DO Final 8.4 6.5 6.7 6.6 6.1 6.4 5.9
Temp Initial 25.2 25.4 25.6 25.5 25.6 25.5 25.4 Check One x
Temp Final 28.0 26,1 28.0 26.1 26.0 25.8 25.7
Salinity Initial 24.6 25.2 25.3 25.2 25.3 24.9 24.6 Growth
Calc. t 0.43
Treatment 0 1 2 3 4 5 6 7 TabularI 1.78
pH initial 8.5 8.3 8.3 8.3 8.1 8.3 8.2 Ferxmdity
pH Final 8.2 8.2 8.0 7.9 8.1 8.0 7,9 Rank Sum
DO Initial 7.7 7.7 7.6 7.6 7.5 6.9 7.0 Ca Value
DO Fins: 6.3 6.1 6.3 6.2 6.5 5.4 5.5
Temp Initial 25.0 25.8 25.7 25.8 25.7 25.8 25.7 PASS FAIL
Temp Final 26.0 28.1 28.0 26.1 26.0 25.8 25.7 X
Salinity Initial 23.5 24.6 25.4 25,3 24.6 24.8 24.7 Check Ono
Sample Test Data: 04-Oct•22
Collection Start Dale 02-Oct-22 04.Oct-22 06-Oct-22 Effluent Test Concentration: 15%
Grab 5 repiicaies were sat for earn control test replicate;whom<5 aro shown the organisms were lost during renews
Composite(Duration) 24 hr 24 hr 24 hr 5 epiicvtes were set for each treatment test replicate;where<5 aro shown the organisms were lost during rene
Conductivity(prnhos/cm) 674 662 636
Chlorine(rng/L) <0.05 <0.05 <0.05
Sample Temp.al Receipt 1.5 0.8 0.5
DWO Form AT-4(6799)
Page 2 of 6

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ETT :
CHAINOF CUSTODY RECORD
u a ih lip ltiM E13. -e *1I Page [ of 1
PO Box 16414,Greenville,SC 29606-7414 '
[phone], [phone]
Shipping Address:4 Craftsman Ct,Greer,SC 29650
wwwettlab.srg •
Client: P
—
C tt-.I c)t- NZId
DI,1Z Program Containers Preservative Parameters
Facility: �r a.$2 l
�"� � I Whole EfllucatToxicity
State: 'VC. NPDES rt!: ,A/CCO2125 3 Acute Chronics Test Organisms —
I
i — p C. 5- IC'
(Composite only) (Grob or Composite) u ?-, F. j _ _ _ 3 Z_
U u o u 1.HSOt y - _ n = _ cr
Sign,and Print below _ ^ -0 _ldCt — — z i_ _ _ _
C3 t1. he dotted line _ U " h ;>Naor = = c 5 '' :v - N -
SAMPLE ID C% CompositeSten Da.c T,me Sample Collcaio1 Dote Time Coll ed y aU r] en Z ea C. Ci > —tI G.chi„, G f U U U Q 2 n =il i Z Chemical Analysis 2.Other
E �lueh� G d0.�.22 10 �,22 i►ob S ,( CI C-61lec4C, (01.)b90
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Special Instructions:
Sample Custody Transfer Record Secure Receipt Sample
•
Date Time Relingt- ed By/Organization Received By/Organization Area Tento CC Preserved?
[0 t(,�A?l � �(�--•.P :� A. V C;f{ of iio ve dt I _
COMPOSITE SAMPLING PROCEDURES TEMPERATURE MONITORING PROCEDURES I HOLD TIME PROCEDURES
Composite samples must be collected over a 24 hour period. Sample temperature during collection and transport must be between For toxicity testing the sample must first be used within 36 hours
Time Proportional:l sample each hour for 24 hours.Equal volur 0.0 and 6.0°C.Samples must not be frozen.Use water ice in sealed bags. of sample collection(completion of composite sample).
or at minimum I sample every 4 hours over 24 hours. Sample may not be used after)2 hours front sample collection.
Flow Proportional:As per instructions in NPDES permit.

CHALN OF CUSTODY RECORD
' Us E-.. 7, gE,,-,-e�. '__s" gragg iPase J of ) i
PO Box 16414,Greenville,SC 296 0 6-741 4
[phone], [phone] Fax[phone]E
Shipping Address•.4 Craftsman Ct,Greer,SC 29850
WWW.C;TCN V1RO NMCNTAL.CaM
Client: ff
C r47 Og 14,vel{o2, Program Containers Preservative Parameters
Facility: Was-e,,,v, 6, .
State: whole Effluent Toxicity
�I
Air NPDES NC. 02a253 AcuteChronic! TtstOrgenisrts
i r,
(Composite only) (Grab or Composite) { �—o = o u. CJ o — Z
U _ r: U �i = a — v G
a. b = !=H'S0: `5, )E 2 — = —
Sign,and Print below Z. 3 — = 8o a-HCL = — _ cn ° ^ ;L s
U r3 the dotted line = c .c c B ;- 0;i ' ' o o = E U 5 —• E t .� —
o " o F, o 0 o u s-znA. B o _ f , s,
SAINIPLE ID Compcz;tc5t rt Dctc Tme ISs.•npit Cofl=tt n Dine Time Collected by J rn as Z ` C7 > s od,= G J I C U n G u. U = 3 c Chemical Analysis&Other
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��S q 5r� la G ID. i2 �D.j•LZ103© C -- \l V_ ALY Y 4i 0.41 aG_
v I,
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Special Instructions:
i
Sample Custody Transfer Record Secure Receipt Sample
Date Time Relinquished By/Organ' or. Received By/Oreanization . Area Temo`C Preserved?
10.5,2211130 0gViA - e—; avr. g
to ;� Og15
l � e..-4Fx I
I
COMPOSITE SAMPLING PROCEDURES I TEMPERATURE MONITORING PROCEDURES HOLD TIME PROCEDURES
Composite samples must be collected over a 24 hour period. Sample temperature during collection and transport must be between For toxicity resting the sample most first be used within 36 hours
Time Proportional:1 sample each hour for24 hours.Equal voles 0.0 and 6.0°C.Samples must not be frozen.Use water ice in sealed bags. of sample collection(completion of composite sample).
or at minimum I sample every 4 hours over 24 hours. Sample may not be used afrer 72 hours from sample collection.
Flow Proportional:As per instructions in NPDES permit

ETT
C-y-y��y-^^-1��yrr//``'' �F UC (O Y RECORD
tt'I JtgldU: Page—_of_j___-
PO Box 16414,Greenville,SC 2960E-7414
[phone], [phone]
Shipping Address:4 Craftsman Ct.Greer,SC 25650
www.ettlab.org
Client: C i-
Ili 0-P I ,
� v t Program Containers Preservative Parameters
Facility:1, /(c rt I P = I
^'l f� \VholcEmuccr Tozicin•
State: f'\ NPDES _ C 00 ,.1 Acute Chronic Test Organisms It
52 i _ E -
(Composite only) (Grab or Composite) < o = ° .= U = = Z
CC Y = E. t-H250 _ = _ _ - -= - -
Sign,and Print below 3 0 = o 2-HCt = - — _ . _ _ _ r
the dotted line = — c� "' _ "t{t o' o _ _ ✓ _
SAMPLE ID Co Ptr-
3 = = ° — — _ _ = —
�? mpofltcSanDnte Time Sam leCalleeuonD°;e Time Collected by J rq ;n Z. e< J > = �mZ.•d,,, I
< < C) C.) ,J 0 -1T_ s = U = 3 7 Chemical Analysis ZOther
G-Od;_.
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ECCltu✓�k C Io.2.22 Io•3.2Z 1D� (%� ` . i1I I G . �`c U. 15 &i �`
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Special Instructions:
Sample Custody Transfer Record Secure Receipt Sample
Date Time Relinquished By/Organizationf Received By/Organization .Area Tema cC Preserved'?
(o-i); 11- 06%,: (.4, f / 6;hi o f H h-,: ' Q.
oi ,7:7, a9 / n 1.•
•
COMPOSITE SAMPLING PROCEDURES TEMPERATURE MONITORING PROCEDURES HOLD TIME PROCEDURES
Composite samples must be collected over a 24 hour period. Sample temperature during collection and transport must be between For toxicity testing the sample must first be used within 36 hours
Time Proportional:1 sample each hour for 24 hours.Equal volur 0.0 and 6.0°C.Samples must not be frozen.Use water ice in-sealed bags. of sample collection(completion of composite sample).
or at minimum I sample every 4 hours over 24 hours. Sample may not be used after 72 hours from sample collection.
Flow Proportional:As per instructions in NPDES permit t .

Eenv raiment*,inc. (E64)877-66942 .FAX[phone]E
P.O.Box 1E414,Greenv.Ile, SC 29606 4 Craftsman Court, Greer,SC 29650
Americamysis bahia Survival and Growth Test
EPA-821-R-02-014 Method 1007
Client: CITY OF HAVELOCK
Facility:WWTP
NPDES#:NC0021253
Test Date: 10-Jan-23
..3
Laboratory Sample ID#:T63853
Test Reviewed and Approved By:
Robert W.Kelley,Ph.D. Patrick D.Timms
President QA/QC Officer
ertification NE87819
SCDHEC Certification N23104
Test results presented in this report confonn to all requirements of
NELAC,conducted under NELAC Certification Number E87819
Florida Dept.of Health.Included results pertain only to provided samples. NCDENR Certification N 022
Page 1 of 6

Effluent Toxicity Report Form - Chronic Mysidopsis Pass/Fail Date: 10-Jan-23
Facilit : Havelock NPDES# NC0021253 Pi•e#: 001 Count : Craven I
aboratory Perform) g Tes: ETT Environmental Inc. Comments:
�ff_- --
Signature of Opera1r4 in rtesponsibIk6harge
Signature of Laboratory Supervisor
MAIL ORIGINAL TO: Environmental Sciences Branch
Division of Water Quality
NC DENR
1621 Mail Service Center
Raleigh,NC 27699-1621
Control Replicates 1 2 3 4 5 6 7 8
1
Surviving# 5 5 4 4 5 5 4 5 %Survival 94.9%
Original# 5 5 5 5 5 5 4 5
Weight(per Original) 0.310 0.256 0.494 0.208 0.25 0.294 0.290 0.196 1 Avg Weight(mg)r 0.287
Treatment 2 Replicates 1 2 3 4 5 6 7 8
Surviving# 5 5 5 5 5 5 5 5 %Survival 100.0%u
Original# 5 5 5 5 5 5 5 5
Weight(per Original) 0.302 0.298 0.294 0.294 0.218 0.418 0.31 0.234 Avg Weight(mg) 0.296
later Quality Data
Day
Control 0 1 2 3 4 5 6 7 Test Results
pH Initial 8.4 8.3 8.2 8.3 8.3 8.3 8.2
pH Final _ 7.8 8.2 7.7 7.7 8.1 7.9 8.3 I Significant Mortality?
DO Initial 7.3 6.9 7.1 6.3 6.6 6.9 7.2 Yes No-
DO Final 5.1 6.6 5.2 4.7 5,5 5.9 6.5 1--------1 X
Temp Initial 25.2 25.3 25.3 25.4 25.2 25.2 24.3 Check One
Temp Final 25.6 25.7 26.0 25.6 25.5 25.6 25.9
Salinity Initial 23.7 24.7 24.2 25.3 25.5 25.6 25.8 Growth
Calc. 1 -0.22
Treatment 0 1 2 3 4 5 6 7 Tabular t 1.76
pH Initial 8.4 8.2 8.4 8.4 8.3 8.4 8.3 Fecundity
pH Final 8.0 8.3 7.9 7.9 8.2 7.9 8.4 Rank Suns
DO Initial 7.4 7.4 8.0 6.6 6.8 6.7 7.2 Crit.Value
DO Final 5.2 6.3 4,9 4.6 4.8 5.1 6.3
Temp Initial 25.0 25.2 25.4 25.6 25.0 25.2 25.4 PASS FAIL
-1
Temp Final 25.6 25.7 26.0 25.6 25.5 25.6 25.9 X _I
Salinity Initial 24.9 25.4 25.1 25.0 25.7 26.0 26.0 Check One
Sample Test Date: 10-Jan-23
Collection Start Date 08-Jan-23 10-Jan-23 12-Jan-23 Effluent Test Concentration: 15%
Grab 5 replicates were set for each control test replicate;where<5 are shown the organisms awe lost during renew.
Composite(Duration) 24 hr 24 hr 24 hr 5 replicates were set for each treatment test replicate;where<5 are shown the organisms were lost during rene
Conductivity(prnhoslcm) 638 652 700
Chlorine(mg/L) <0.05 <0.05 <0.05
Sample Temp.at Receipt 0.3 0.4 0.8
DWQ Form AT-4(6/99)
Page 2 of 6
I

Day 1 Day 2 Day 3 Day 4 Day 5 Day 6 Day 7 Weight Fecundity oriq
source rep Dead Lost/Dead Lost Dead Lost Dead Lost Dead Lost Dead Lost Dead Lost mg N-Grav Gravid Survival II Lab/ T63653
A 0 0 0 0 0 0 0 0 0 0 0 0 0 0 1.55 5 5 Client havelock
B 0 0 0 0 0 0 0 0 0 0 0 0 0 0 1.28 5 5 Sample ID \YWTP
C 0 0 0 0 0 0 1 0 0 0 0 0 0 0 2.47 4 5 NPOEss NC0021253
D 0 0 0 0 0 0 1 0 0 0 0 0 0 0 1.04 4 5 County Craven
control E 0 U 0 0 0 0 0 0 0 0 0 0 0 0 1.25 5 5 Month 1
F 0 0 0 0 0 0 0 0 0 0 0 0 0 0 1.47 5 5 start a red Date 10-Jan-23
G 0 0 0 0 0 0 0 0 0 0 0 0 0 1 1.16 4 4 Start a tad Time 02;45 PM _
H 0 0 0 0_0 0 0 0 0 0 0 0 0 0 0.98 5 5 Started a fed By JG
A f 0.00 5 5 Test Organism A.BAHIA
B 0.00 5 5 Coo,born data 03-Jan-23
C 0.00 5 5 Noo.born time_1400.1630
D _ 0.00 5 5 Test Type NCPF _
0 E 1 0.00 5 5 Dilution Water Instant Ocean
F 0.00 5 5 Units for Cone. %
G 0.00 5 5 33rd BROOD
H 0.00 _ 5 5 Test vessels 400 nil
A 0.00 5 5 Test volume 150 MI
B 0.00 5 5 Incubator I 1
C _ 0.00 5 5 Light 168/8dk
D 0.00 5 5 Elf.Init.Tomp•C 25.0 _
0 E 0.00 5 5 Feeding WI Artemis rso
F 1
1 0.00 5 5 Test method EPA a21.R-02-0N:IDe/
G 0.00 5 5
H 0.00 5 5
A 0.00 5 5
B 0.00 5. 5
C 0.00 5 5
D 0.00 _ 5 5
0 E - 0.00 5 5
F _ 0.00 5 5 Comments
G 0.00 5 5 All tops har•: 5
H ___ 0.00 5 5 organisms unless noted otherwise.
A 0.00 5 5
B s 0.00 -_ 5 5 Control ini temp 11 a^�'�,, 4164
64
C 0.00 - 5 5
D _ 0.00 - 5 5
B E 0.00 5 5
t
F 0.00 5 5
G �- 0.00 - 5 5
_ H _ . 0.00 __ I_ 5 5
A 0 0 0 0 0 0 0 0 0 0 0 -7 -0 0 1.51 5 5
B 0 0 0 0 0 0 0 0 0 0 0 0 0 0 1.49 5 5
C 0 0 0 0 0 0 0 0 0 0 0 0 0 0 1.47 5 5
D 0 0 0 0 0 0 0 0 0 0 0 0 0 0 1.4; 5 5
1 0 E 0 0 0 0 0 0 0 0 0 0 0 0 0 0 1.09 5 5
F 0 0 0 0 0 0 0 U 0 0 0 0 0 0 2.09 5- 5
G 0 0 0 0 0 0 0 0 0 0 01 0 0 0 _i.55 5 5
H 0 0 0 0 0 0- 0 0 0 0 01 0 0 0 1.17 5 5
Ref,e1 AM JC JG AM JC JC _ End Date
Fed AM JC JG AM JC JC
Di55 PM e2.35 PN 12.55 Pu 1120 ArI 09.er AFI 01'.3epe 17-Jan-23 I JC
Eewenrnew 1e1P.•e 25.2 25.4 25.6 25.0 25.2 25.4 01 02 PM
oa temp.0 25.6 25.7 26 25.6 25.5 25.6 25.91 D=Dead N/A-Lost or not used
Coot.Dtuee temp.•e 25.3 25.3 25.4 25.2 25.2 24.3
Page 3 of 6

ETri CHAIN OF CUSTODY RECORD
y" ", - e 3 Seri Page of
PO Box 16414,Greenville,SC 29806-7414
[phone], [phone]
Shipping Address:4 Craftsman Ct,Greer,SC 29650
www.ettlab.org
Client:G z rY Of ilAvet
OC./S Program Containers Preservative Parameters
Facility: J45fr;JAfe.�
F" Whole GfTtocnt Toxicity •Q
State: A/L NPDES#: / 4 Q OZ/2 s''3 Actne Chronic Test Orgonisms �.,
ci Q
E (Composite on V t° — O : U
U only) (Grab or Composite) < p �_ 'ir . c = O
Sign,and Print below 3 o 2-HCI i a co' o ti >_ rn
<
U the dotted line e E .� o V " C d OH 0 o •- = - - 2 ,y E o •• ", .o �''
o 6 o 5 n o u S-'°Ft v v Ce c T> ii c iE_t =••1 ? F
SAMPLE ID �? Composite Sion Dnte Time Sarsgk Carction Date Time Collected by U vt r� 2 a C7 > 5.o < < U U C..i d z Z iir _ U _ 3 2 Chemical Analysis&Other
1
Special Instructions: - �'-
Sample Custody Transfer Record Secure Receipt Sample
Date Time Relinquished By/Omani tion Received By/Orzartization Area Temp°C Preserved?
\_C\t-S \y3° 1.iA AA.id oct t.e .y fill on )}A.'a 01-(
COMPOSITE SAMPLING PROCEDURES TEMPERATURE MONITORING PROCEDURES HOLD TIME PROCEDURES
Composite samples must be collected over a 24 hour period. Sample temperature during collection and transport must be between For toxicity testing the sample must first be used within 36 hours
Time Proportional: I sample each hour for 24 hours.Equal volur 0.0 and 6.0°C.Samples must not be frozen.Use water ice in sealed bags. of sample collection(completion of composite sample).
or at minimum I sample every 4 hours over 24 hours. Sample may not be used after 72 hours from sample collection.
Flow Proportional:As per instructions in NPDES permit.
Page 4 of 6

•
CHAINETt OF CUSTODY RECORD III
,„.a, . ,,,elI EI ertl Page 4_of 4
PO Box 16414,Greenville,SC 29606-7414
[phone]. [phone]
Shipping Address:4 Craftsman Ct.Greer,SC 29850
www.ettleb.org
Client: - -
C'±A`t' SR- p,Q►V EWt..Nr..- Program Containers Preservative Parameters
Facility:
LJ t V Yr;*,J PVC ti w tyholc Emvcat ToxicityQ
State: /t/G NPDES#: fiC 0 0Z.12S3 Acute :ro;
Test Organisms O
I O
`o (Composite only) (Grab or Composite) < o �, .- tz. . o „ _ Z
o .� 1-rases = = = = :n
Sign,and Print below 3 U — 2-lt� G - 2 so 2 y o Elm >
the dotted line e - E u •� H c '-HI o: y -c p — c
U c E • .. 'o 4.tvoti _ _ o o E N t _ o t
O u p ai e o o _ 5.2uAc u U  is c c :�. > >,= V '_7
SAMPLE ID Cc:�positc 5tc t Dote Time Scrpk Collcoion Dotc Time Collected by U to :o Z nu O. C7 > 6.o,l, . < < U U U Q t= to _ U = 3 Chemical Analysis 8.Other
RA MO Dl i / ,� o r► / S f / / e ,. LK,S'a
a
E(-Ft.Jr�r 4 /-1Q- Z7 ieja J-l/_ t3 10:3c 1�'_,G -- F' 604- i/ V S--f d C �3353i1
..
, 1 . .. . :
__
Special Instructions: --
Sample Custody Transfer Record Secure Receipt Sample
Date Time Relinquished By/Organization Received By/Organi ion Area Temp°C Preserved?
(- ,t-t3 do wRµG) 05u,o..4/ire" DC- 1)14Jec.o tliglz09 E-77-- 9.17
COMPOSITE SAMPLING PROCEDURES f TEMPERATURE MONITORING PROCEDURES HOLD TIME PROCEDURES
Composite samples must be collected over a 24 hour period. Sample temperature during collection and transport must be between For toxicity testing the sample must first be used within 36 hours
Time Proportional: I sample each hour for 24 hours.Equal volur OM and 6.0°C.Samples must not be frozen.Use water ice in scaled bags. of sample collection(completion of composite sample).
or at minimum 1 sample every 4 hours over 24 hours. Sample may not be used after 72 hours from sample collection.
Flow Proportional:As per instructions in NPDES permit.
Page 5 of 6

T'i CHMN OF CUSTODY RECORD
ti�ttttom a .ei1K?I.0 1611 .:� Page of
PO Box 16414.Greenvl"e,SC 29606.7414
[phone], [phone]
Shipping Address:4 Craftsman Ct,Greer,SC 28650
www.ettleb.arg
Client .,�_/
Client:,
7 / 0 F. .OvF(c ck Program Containers Preservative Parameters
Facility: y�t fe-uA�,.eM t
/"f 'Mole Emacat Toxicity '
State: re. NPDES#: fVG 0 b Z/2,1'3 Acute Chronic Tat Organisms Q
G
2 r? — O 2 Cr..l
U (Composite only) (Grab or Composite) < o c�-i —E C) t U o ' t7
U � o` er 1-H2SO4 h .- "S"c - c - •� J P. u
Sign,and Print below > c c o 2-Hm 2 oo 2 _ ^ is >
the dotted line c ^ C V •2 - '•H!•Oo s> c 7 u g ` 'a <
U a = • c " = l•K.1OH : = o o c y o P. _
SAMPLE ID �? acmpm;teslarr Dase Time s " o 5 o ° --* c = s°2aAe v o - - " e = a,. 's m v
amp:e Conruioo Darr 'Time Col Urn rn z .e a C > 6.0� < < U U U CS t rn _ U = 3 2 Chemical Analysis&Other
GvU Erfr�^'
rit LVtpir G /-12-Z3 J- 13-Zd JJ.�05, - n - Z f G ✓ ✓ V �' �4S53G
e l
Special Instructions:
Sample Custody Transfer Record Secure Receipt Sample
Date Time Relinquished By/002anization Received By/0reanization Area T p°C Preserved?
1-71-zjtyy-, 0ev pf r//Jae.1 X.,1--r 6c- `/l iuftoc.Y alt_ 6
t-V•-t.?-3 No FkD 1 X A .PA(AV /&T I D,f?
COMPOSITE SAMPLING PROCEDURES TEMPERATURE MONITORING PROCEDURES HOLD TIME PROCEDURES
Composite samples must be collected over a 24 hour period. Sample temperature during collection and transport must be between For toxicity testing the sample must first be used within 36 hours
Time Proportional: I sample each hour for 24 hours.Equal volur 0.0 and 6.0°C.Samples must not be frozen.Use water ice in seated bags. of sample collection(completion of composite sample).
or at minimum I sample every 4 hours over 24 hours. Sample may not be used after 72 hours from sample collection.
Flow Proportional:As per instructions in NPDES permit.
Page 6 of 6

ET.R.T„,,,. (E64)677-6c42 .FAX[phone]
P.U. Box 16414, Greenville. SC 29605 4 Craftsman Court.Graer,SC 29650
Americamysis bahia Survival and Growth Test
EPA-821-R-02-014 Method 1007
Client: CITY OF HAVELOCK
Facility:WWTP
NPDES#:NC0021253
Test Date: 04-Apr-23
Laboratory Sample ID#:T64516
Test Reviewed and Approved By:
Robert W.Kelley,Ph.D. Patrick D.Timms
President QA/QC Officer
ieCC71F'.
Certification 4E87819
4-8 ' SCI3H EC Certification#23104
Test results presented in this report conform to all requirements of
NELAC,conducted under NELAC Certification Number E87819
Florida Dept.of Health.Included results pertain only to provided samples. NCDE N R Certification# 022
Page 1 of 6

Effluent Toxicity Report Form -Chronic Mysidopsis Pass/Fail Date: 04-Apr-23
Facilit : Havelock NPDES II NC0021253 Pipe#: 001 Count : Craven
_aboratory Performing Test: ETT Environmental Inc. Comments: _
Signature of Operator in Responsible Charge
x 4Aft e✓V4.
Signature of Laboratory Supervisor
MAIL ORIGINAL TO: Environmental Sciences Branch
Division of Water Quality
NC DENR
1621 Mail Service Center
Raleigh,NC 27699-1621
Control Replicates 1 2 3 4 5 6 7 8
Surviving# 5 5 4 5 5 5 5 5 %Survival r 97.5%
Original# 5 5 5 5 5 5 5 5
Weight(per Original) 0.260 0 284 0.242 0.258 0.252 0.330 0.308 _ 0.316 Avg Weight(mg) 0.281
Treatment 2 Replicates 1 2 3 4 5 6 7 8
Surviving# 5 4 5 5 5 5 5 5 %Survival 100.0%
Original# 5 4 5 5 - 5 5 5 5
1
Weight(per Original) 0.304 0.288 0.312 0.260 0.324 0.300 0.270 0.240 Avg Weight(mg)I 0.286
Water Quality Data
Day
Control 0 1 2 3 4 5 6 7 Test Results
pH Initial 8 1 8.2 8.1 8.2 8.2 8.1 8.2
off Final 7.7 7.7 7.9 7.9 7 6 7.6 8.1 Significant Mortality+
DO Initial l 6.5 6.2 6.5 7.0 7.3 6.3 6.5 Yes No
I .
DO Final 4.7 4.3 5.8 5.9 5.3 4.7 6.1 I X
Temp Initial 25.2 25.6 25.1 25.3 25.3 25.2 25.4 Check One
Temp Final 25.9 26.1 26.2 26.2 26.1 25.9 26.0
•
Salinity Initial 24.1 24.7 25.1 24.1 24.5 24.6 25.0 Growth
Calc. t -0.30
Treatment 0 1 2 3 4 5 6 7 Tabular t 1.76
1
pH initial 8.1 8.3 82 8.3 8.3 8.2 8.3 Fecundity
pH Final 8.0 7.8 7.9 8.1 7.8 7.9 8.1 Rank Sum
DO Inihel 6.7 6.7 6.7 7.0 7.0 6.7 6.0 CM.Value
DO Final 4.7 4.3 5.3 5.9 5.2 4.9 5.6
Temp Initial 25.0 25.4 25.2 25.5 25.6 25.4 25.5 PASS FAIL
Temp Fine! 25.9 26.1 25.2 26.2 26.1 25.9 26.0 X
Salinity Initial 26.3 26.2 25.1 25.1 25.8 26.1 26.1 I ( Check One
Sample Test Date: o4-Apr-23
Collection Start Date 02-Apr-23 04-Apr-23 06-Apr-23 Effluent Test Concentration: 15%
Grab 5 replicates were set for each contra;test replicate;where<5 are shown the organisms were lost during renew:
Composite(Duration) 24 hr 24 hr 24 hr 5 replicates were set for each Lealment lest replicate;where<5 are shown the organisms were lost during rune
Conductivity(pmhos/cm) 647 670 669
Chlorine(mg7L) <0.05 <0.05 <0.05
Sample Temp.at Receipt 0.6 0.9 0.5
DWQ Form AT-4(6/99)
Page 2 of 6

Day 1 Day 2 Day 3 Day 4 Day 5 Day 6 Day 7 Weight Fecundity Orl
source rep Deed Lost Dead Lost Deed lost tlead Lost Dead lost Deed Loot Oeed teal erg N-lG raw Grev'.d •Survival it Labs •T64516
A 0 0 0 0 0 0r 0 0 0 0 0 0 0 0 1.30 5 5 client Hevo:ock
B 0 0 0 0 0 0 0 0 0 0 0 0 0 0 1.42 5 5 Sample ID WWTP
C 0 0 0 0 0 0 0 0 0 0 1 0 0 0 1.21 4 5 NPDEstl NC0021253
D 0 0 0 0 0 0 0 0 0 0 0 0 0 0 1.29 5 5 County Craven
control E 0 0 0 0 0 0 0 0 0 0 0 0 0 0 1.26 5 5 Month 4
F 0 0 0 0 0 0 0 0 0 0 0 0 0 0 1.65 5 5 Start 6 ted Date _04-Apr-23
G 0 0 0 0 0 0 0 0 0 0 0 0 0 0 1.54 5 5 Start&tod Time 03:15 PM
H 0 0 0 0 0 0 0 0 0 0 0 0 0 0 1.58 5 5 Started a tod By AM
A II IIIIIIII 0.00 5 5 Teal Organism ABAHIA
B 0.00 5 5 Neo.born date 28-Mar-23
C 0.00 5 5 Non.born time 1400-1630
D 0.00 5 5 Teat Type NCCPF
0 E 0.00 5 5 Dilution Water Instant Ocean
F 0.00 5 5 Unita for Cone %p
G 0.00 5 5 %3rd BROOD
H 0.00 5 5 Test vessels _ 400 mi
_
A 0.00 5 5 Test volume _ 150 mt
B1111
0.00 5 5 incubators 1
0.00 5 5 Light 161U8dk
D 0.00 5 5 Eft.Inn.Temp•C 25.0 ,
0 E 0.00 5 5 Feeding w/Artomla 750 1
F 0.00 5 5 Teat method EPA o:r•a-aa.ot.:toor
G 0.00 5 5
H 0.00 5 5
A 0.00 5 5
B 0.00 5 5
C 0.00 5 5
D 0.00 5 5
0 E 0.00 5 5
F 0.00 5 5 Comments
G 0.00 5 5 All reps have 5
H 0.00 5 5 .rganisms unless noted otherwise.
A 0.00 5 5
8 0.00 5 5 'cntrol 4li temp `;2
C 0.00 5 5
D 0.00 5 5
0 E 0.00 5 5
F 0.00 5 5
G 0.00 5 5
I H 0 00 5 5
A 0 0 0 0 0 0 0 0 0 0 0 0 1.52 5 5
8 0 0 0 1 0 0 0 0 0 0 0 0 1.15 4 4
C 0 0 0 0 0 0 0 0 0 0 0 0 1.56 5 5
D 0 0 0 0 0 0 0 0 0 0 0 0 1.25 S 5
15 E 0 0 0 0 0 0 0 0 0 0- 0 0 1.62 5 5
F 0 0 0 0 0 0 0 0 0 0 0 0 1.50 5 5
G 0 0 0 0 0 0 0 0 0 0 0 0 1.35 5 5
H 0 0 0 0 0 0 0 0 0 0 0 0 1.20 5 5
Renew JG AM JC JC AM JG End Date
�.
Pee JG AM JC JC AM JG
Ten, A
Tu lee A le11.1. 0205 PIA 01:A9 PIA 1100Att 122r Pa 01.30 PIJ 11:24 All I 11-Apr-23 AM
Plr,.nl h..e temp.•C 25.4 25.2 25.5 25.6 25.4 25.5 er en Pa 1
OP temp.-c 25.9 26.1 26.2 26.2 26.1 25.9 261 D=Dead NIA-Lost or not used
Cowah..temp.•c 25.6 25.1 25.3 25.3 25.2 25.4
Page 3 of 6

•
ETT CHAIN OF CUSTODY RECORD S
3 "m',5,,;�','r "'e :iu� 'EuT Page of r
PO Box 16414,Greenvite,SC 29808.7414
[phone], [phone]
Shipping Address:4 Craftsman Ct,Greer,SC 29650
www.ettlsb.arg
Client: e tt,..t y do giveiocx/ ( _ tProgram Containers Preservative Parameters
Facility: (� A5'1 like,'Y�
WA \\'hole Effluent To:idry�
State: A/C---A/C--- N NPDES#: oa r4S.
�}5` 3 °
Acute Chronic Test Organisms
t
o c= o _
(Composite orty) (Grab or Composite) < T — U _ Z
u Post o o ` U _•
Os — -. - ^ I.H2S0a H = = - ✓;
V V rn
Sign,and Print below 3 = i:a ^ z-HCL , 0 0 = =a, inn _ o m 2
n the dotted line — E c a a-a0H c o a C y .� `_2 -
0 0 — o
SAMPLE ID i2 Compasttc5urt Dbtc Tlme SanpleCaaeatieo Dotc Tlmo Cotteued by U c c i Z no ii F. > u p r < < U U Ci O ` iq 7,U E i ± Chemical Analysis&Other
'(I 11 .s 7 r
lie&I-AO L„, t o
•
Special Instructions:
Sample Custody Transfer Record Secure Receipt Sample
Date Time 'elinquished By/Organization Received By/Organization Area Temp°C Preserved?
3.g3 i0: ea r. C :ly e4 J-k J0 ,k Hai-.
)`014S o .04 - -(&P;Al- I 0
COMPOSITE SAMPLING PROCEDURES TEMPERATURE MON/TORING PROCEDURES HOLD TIME PROCEDURES
Composite samples must be collected over a 24 hour period. Sample temperature during collection and transport must be between For toxicity testing the sample must first be used within 36 hours
Time Proportional: l sample each hour for 24 hours.Equal volur 0.0 and 6.0°C.Samples must not be frozen.Use water ice in sealed bags, of sample collection(completion of composite sample).
or at minimum I sample every 4 hours over 24 hours. Sample may not be used after 72 hours from sample collection.
Flow Proportional:As per instructions in NPDES permit.
Page 4 of 6

ETTCHAIN OF CUSTODY RECORD
`' :•i=9-' Ell:' irO11'ii ettitegt: Page of
PO Box 16414,Greenville,SC 2960E-7414
[phone], [phone]
Shipping Address:4 Craftsman Ct,Greer,SC 28650
www.ettieb.org
Client:
L-i_ pc- taflv k... cv. Program Containers Preservative Parameters
Facility: 1..J(hSt E u
per C.\Z- Whole Effluent Toxicity e-
State: /VG NPDES#: /1/4 oOZ 12 S 3 Acute Chronic Test Organisms
ci 0
ci - o .3 0
e ("eiComposite only) (Grab or Composite) < o c a U v .
U 1 " = = c H
( c = o t-112SO4 c c = Tin
Sign,and Print below 3 -- ', 2, o 2-i)Ct ' o _ •:� n = m ?_
o i-14:Oi 5 -. _ '� o —
U the dotted line c k H = a-tda0Fi o o o = c o •--, o _ _e. -
SAMPLE ID Campasita Start Data Time sentpie Cauceion Dote Time Collected by C5 .J Tin Z C7 > b o r '< < U U Ci 2 :i1 T V L- 8 2 Chemical Anatysis 8 Other -
1 Az11 US;td , ! Zy S ` ` / Y 9 Lot,tjjCP-a d` (_(f 71�J
FFFIt.t:.,.r c (if-it 23 /oJ cI t-(-S- 23 /03„ �- C v �/ (�
—
i �. I _ i i _
Special Instructions:
Sample Custody Transfer Record Secure Receipt Sample
Date Time Relinquished By I Oreanization Received By/Oreanization Area Temp°C Preserved?
9-S'V3 fy3' WAa_a G.) LX1'12-v1 City aC' NA4 L QC -red X
g(�1a3 1�_ _ a- 9
COMPOSITE SAMPLING PROCEDURES TEMPERATURE MONITORING PROCEDURES HOLD TIME PROCEDURES
Composite samples must be collected over a 24 hour period. Sample temperature during collection and transport must be between For toxicity testing the sample must first be used«ithin 36 hours
Time Proportional: I sample each hour for 24 hours.Equal volut{0.0 and 6.0°C.Samples must not be frozen.Use water ice in sealed bags. of sample collection(completion of composite sample).
or at minimum I sample every 4 hours over 24 hours. Sample may not be used after 72 hours from sample collection.
Flow Proportional:As per instructions in NPDES permit.
Page 5 of 6

ET'i'
CHAIN OF CUSTODY RECORD
:�^" ,�f: ,, „ .t-fir :c
..- ,. t __y.:., :- Page _L___of_4__
PO Box 16414.Greenville,SC 29606-7414
[phone], [phone]
Shipping Address:4 Craftsman Ct,Greer,SC 29650
www.ettlab.erg y
Client: C)/L \) in 9 G 401 Vla ILoe f� Program
Containers Preservative Parameters
Facility: W, f• n+fi twit o-r `
tl�I V+ /r , whole Effluent Toxicity Q
State: �l' NPDES#: y Q d v I t q. £j /i 1 Acute Chronic Test Organisms
ti Q
g _ a c c
U (Composite only) (Grab or Composite) < o ` r . o e
— _ ^ _ ? :n
Sign,and Print below i T c v o u 2.HCL a _ :n ,—f g <
the dotted line g E E 4 h � a. o+ = c o E U = 1. 2 0 C 2 -
SAMPLE 1D c eaa i o o 0 0 o e C o u 3=7sAe v o — — = — > c J = — —
�ruCthStart Datc -limo Svup(tt Co5uetioc Dcte Time Collected by vi v7 Z i= U > 6.o� < < V V V LI C 2 :n = U 1- L ��Chhemleal Analysts 8,Other
E F�l�I P�-t C I�D dfl��Z� t 19t9 J 4-p�h Pr f,,,, ' _/ S. / $�,l t� V V' W C 4(,} p e 4 0 n &46I .
Special Instructions:
Sample Custody Transfer Record Secure Receipt Sample
Date Time Relinquished By/Organization Received By/Organization Area Temp°C Preserved?
a/o1/t0:41° s}--epNHA fIA„tl (/ c-tt- 0IC 1-1-61vt' la edEx„
k Z3 o o Fed(( ,t.:rt� 1 r— Ot 5
COMPOSITE SAMPLING PROCEDURES TEMPERATURE MONITORING PROCEDURES HOLD TIME PROCEDURES
Composite samples must be collected over a 24 hour period. Sample temperature during collection and transport must be between For toxicity testing the sample must first be used within 36 hours
Time Proportional: I sample each hour for 24 hours.Equal volur 0.0 and 6.0°C.Samples must not be frozen.Use water ice in sealed bags. of sample collection(completion of composite sample).
or at minimum I sample every 4 hours over 24 hours. Sample may not be used afrer 72 hours from sample collection.
Flow Proportional:As per instructions in NPDES permit.
Page 6 of 6

ETmjne. (E64)877-6942 .FAX[phone]
P.O.Box IC414,GreenvIle,SC 29606 4 Craftsman Court,Greer,SC 29650
Americamysis bahia Survival and Growth Test
EPA-821-R-02-014 Method 1007
Client: CITY OF HAVELOCK
Facility:WWTP
NPDES#:NC0021253
Test Date: il-Jul-23
Laboratory Sample ID#:T65180
Test Reviewed and Approved By:
Robert W.Kelley,Ph.D. Amy McMahan
President QA/C Review
?4 t rj
Certification#E87819
SCDHEC Certification#23104
Test results presented in this report conform to all requirements of
NELAC,conducted under NELAC Certification Number E87819
Florida Dept.of Health.Included results pertain only to provided samples. NCDENR Certification# 022
Page 1 of 6

Effluent Toxicity Report Form -Chronic Mysidopsis Pass/Fail Date: 02-Aug-23
Facilit : Havelock NPDES It NC0021253 Pi.etI: 001 Count : Craven
•
'_aboratory Performing Test: ETT Environmental Inc. Comments:
Signature of Operator in Responsible Charge
•
Signature of Laboratory Supervisor
•
MAIL ORIGINAL TO: Environmental Sciences Branch
Division of Water Quality
NC DENR
1621 Mail Service Center
Raleigh,NC 27699-1621
Control Replicates 1 2 3 4 5 6 7 8
Surviving# 5 5 6 5 5 5 5 5 I %Survival I 100.0%J
Original# 5 5 5 5 5 5 5 5
Weight(per Original) 0.283 0.222 0.224 0.249 0.252 0.209 0.203 0.248 Avg Weight(mg) 0.236
Treatment 2 Replicates 1 2 3 4 5 6 7 8
Surviving# 5 5 5 5 5 5 4 5 %Survival 100.0%
Original# 5 5 5 5 5 5 4 5
Weight(per Original) 0.308 0.200 0.268 0.286 0.366 0.280 0.345 0.218 -Avg Weight(mg) 0.284 I I
Vater Quality Data
Day
Control 0 1 2 3 4 5 6 7 Test Results
pH Initial 8.0 8.1 8.0 8.2 8.2 8.1 8.1
pH Final 7.8 8.0 7.7 7.8 8.0 7.7 7,8 Significant Mortality?
DO Initial 6 7 7.1 7.2 6.8 6.9 7.0 6.9 Yes No
DO Final 6.4 6.5 5.0 6.7 6.9 4.9 5.5 I X
Temp Initial 25.1 25.5 25.4 25.2 25.6 25.5 25.4 Check One
Temp Final 25.9 26.0 26 2 26.1 26.1 25.9 25,7
Salinity Initial f 24.8 25.4 25.8 26.4 26.3 25.8 24.9 Growth
Celc. t -0.25
Treatment 0 1 2 3 4 5 6 7 Tabulart 1.76
pH Initial 8.1 8.1 8.2 8.1 8.1 8.1 7.7 Fecundity
pH Final 8.1 8.0 7.8 7.8 8.0 7.6 7,7 Rank Sum
DO Initial 6.7 6.7 7.0 6.6 7.1 7.0 3.9 Cat.Value
DO Final 6.5 6.4 4.7 5.6 5.3 3.2 4.3
Temp Initial 25.0 25.7 25.6 25.4 25.5 25.7 25.6 PASS FAIL
Temp Final 25.9 26.0 26.2 26.1 26.1 25.9 25.7 X
Salinity Initial 24.9 25.2 25.9 26.2 26.1 26.2 25.8 Check One
Sample Test Date: 11-Jub23
Collection Start Date 09-Jul-23 11-Jul-23 13-Jul-23 Effluent Test Concentration: 15%
Grab 5 replicates were set for each control lest replicate;where<5 are shown the organisms were lost during renew.
Composite(Duration) 24 hr 24 hr 24 hr 5 replicates were set for each treatment test replicate;where<5 are shown the organisms were lost during rene
Conductivity(pmhoslcm) 620 643 661
Chlorine(mg/L) <0.05 <0.05 <0.05
Sample Temp.at Receipt 0.5 0.5 1.2
DWQ Form AT-4(6199)
Page 2 of 6

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0 . .. , r
0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 z I cD rn V
m o (�4 N N
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Q m 0 0 0 0 - 0 0 0 0 0 0 0 0 0 0 0 _
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m J N IN ,, N N N
o o 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0
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Om m o 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 < E ^ N N N
y o 0 0 0 0 0 0 0 0 0 0 0 0 0'0 0 (0 cO V
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o m o 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 i
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ET'
a
1 CHAIN OF CUSTODY RECORD
PO box 16414,Greenville.SC 29606-7414
[phone], [phone]
Shipping Address:4 Craftsman CI.Greer,SC 29650
wwwsttlaberg
Client: 1
c 11'y 0 iiml)c j. Program Containers Preservative Parameters
Facility: vu (
State �ll�'L�'L�3 \\Chronic
Effluent Test Organisms
N l� NPDES#: n
Acute Chronic Organisms _
a-
U (Composite only) (Grab or Composite) < o CJ V o . z
a c lv .L _ e s: c
.n Sign,and Print below 3 g %a o 2d HC1. a as 2 •= - ^ a.r > �'
v the dotted tine a E v a - _ 3•1 01 g1. •E 5 g = ? Ft-
V o c c sn 2Mc t� v Z.
o `_-' ` 'A ' o [~St W 5
SAMPLE ID Composite Start note Time Sample Collection Dote Thne Collected by U to to Z x a J Ti> 6.other < G U U CJ d tom. rn T U�;= 3 2 Chemical Analysis&Other
,I- L ll ;t3 so.0, (cotes v:ut- a a-ct-- J 2 0,1 N (NI J �,(v,.c. �5t8b�
1
,
Special Instructions: I I
Sample Custody Transfer Record Secure Receipt Sample
Date Tim Relin uished By/Organization Received By/Organization Area Temp°C Preserved?
P-I1t1Tb tki30 Yf6 eit -- ei r Qo ) -7-- D.5
COMPOSITE SAMPLING PROCEDURES TEAIPER4TURE MONITORING PROCEDURES HOLD TIME PROCEDURES
Composite samples must be collected over a 24 hour period. Sample temperature during collection and transport must be between For toxicity testing the sample must first be used within 36 hours
Time Proportional:I sample each hour for 24 hours.Equal volur 0.0 and 6.0°C.Samples must not be frozen.Use water ice in sealed bags. of sample collection(completion of composite sample).
or at minimum I sample every 4 hours over 24 hours. Sample may not be used after 72 hours from sample collection.
Flow Proportional:As per instructions in NPDES permit. I
Page 4 of 6

ETTCHAIN OF CUSTODY RECORD
r ? r':rL.11� *` u `" '*_ram`:--1-*
,_..„-, ,- . . eroar 0 ,c ;e Page of
PO Box 16414,Greene d]e.SC 29806-7414
[phone]. [phone]
Shipping Address:4 Craftsman Ct,Greer,SC 29650
www.ettlab.erg
CIient:
C �I
' 7 o- V1uVe-I0GI�. Program 1 Containers Preservative Parameters
Facility: \-I oks)_€
�I_ "A""� `� t \Thole Effluent Toxicity
State: 11 {r NPDES 4: lY v( L 1 —3 Acute prank Test Organisms L
ci 0
C U 0 JFlu
i
U (Composite only) (Crb or Composite) •C c ' U t U 2 _ J
C � — E 1.H2S01 = c '- •E a,, ,U G U �
Sign,and Print below > e' : c 2-HCt c m = 2. u rn
the dotted line 3 U •� _ s-teao; ,, _ - .n - 4 o c 'o H
SAMPLE ID i Compositeu O C v s.2:nnc u c>  T_tt j a L7
Suns Hare Time Semple Co:tttti°u Dale Time Collected by U rn � Z � c t7 > 6„C�hcr � G rJ U U � L � to _• U i— 2 Chemlcat Analysts 8 other
ef£1 }� 1 tkt\t1 ion 11Ii h:: /00-- - I1414,- I I g i f I �, ��c,� ( 6t O
�, � )
Special Instructions:
Sample Custody Transfer Record Secure Receipt Sample
Date Time Relinquished By!Oreanization Received By/Oreanization Area Temp°C Preserved?
1 Wi.\fC kkkr&D Jacob OAIN,/[e,Ay p-P \-{r ( k FctE 1
�Il3 a3 30 x . etc 0.6
COMPOSITE SAMPLING PROCEDURES TEMPERATURE MONITORING PROCEDURES HOLD TIME PROCEDURES
Composite samples must be collected over a 24 hour period. Sample temperature during collection and transport must be between For toxicity testing the sample must first be used within 36 hours
Time Proportional:I sample each hour for 24 hours.Equal volur 0.0 and 6.0°C.Samples must not be frozen.Use water ice in sealed bags. of sample collection(completion of composite sample).
or at minimum I sample every 4 hours over 24 hours. Sample may not be used after 72 hours from sample collection.
Flow Proportional:As per instructions in NPDES permit.
Page 5 of 6

ETTCHAIN OF CUSTODY RECORD
,1. livir,on ae '. Page of
PO Box 16414.Greenville,SC 29606-7414
[phone]. [phone]
Shipping Address:4 Craftsman Ct.Greer,SC 29650
www.ettlab.org
Client: �`�" t^GL Program Containers Preservative Parameters
Facility: kVT C S L Ve �" {`yry� /� ut Whole Emaent Toxicity
State: %V.L NPDES#: rl Ace Chronic Test Orgaolsms O
- C1
ci G'
o Q
h (Composite only) (Cob or Compc,nc) •- _ Z
4 0 0 'c U U o
ci I•H:Soi = c � ca
Sign,and Print below HNO33 c o 2-Het a �, Ya = o t_
the dotted line c E �' •`-' ti E 4 No0H 0 � E f_' _
4.NaoH � `o o � � � o �. r" •�
SAMPLE ID o cam S o d o o J o 5n70Ae G o = = 7 G G 7,- y- rn P —
poziteSran Da[c Time Sampk Collection Mtn Time Collected by U cn ca Z F. C7 > 6.,other G G U U U tZ r_. .4 rn U _ 3 L Chemleal Analyst 8 Other
teias
Mi" c ?Iv'sI'�-3 tt ')f't3 1t=et.__ i t- if DAk Cj,S"° C (QS c-
—
___.] _ t
JSpec:. 1 Instructions:
Sample Cuctody Transfer Record Secure Receipt Sample
Date Time Rein uished By!Organization Received By/Organization Area Temp`C Preserved?
Ii (t3o Ott,, C't edikeloGk. tOlielellS4Lad gint6621r,-
I
COMPOSITE SAMPLING PROCEDURES TEMPERATURE MONITORING PROCEDURES HOLD TIME PROCEDURES
Composite Samples must be collected over a 24 hour period. Sample temperature during collection and transport must be between For toxicity testing the sample must first be used within 36 hours
Time Proportional: I sample each hour for 24 hours.Equal volu 0.0 and 6.0°C.Samples must not be frozen.Use water ice in staled bags. of sample collection(completion of composite sample).
or at minimum I sample every 4 hours over 24 hours. Sample may not be used after 72 hours from sample collection.
Flow Pro rtional:As r instructions in NPDES it. ____
t\ Page 6 of 6

ET....t�,Inc. (£64)877.6942 .FAX[phone]
P.O.Box 16414,Greenville,SC 29606 4 Craftsman Court,Greer,SC 29650
Americamysis bahia Survival and Growth Test
EPA-821-R-02-014 Method 1007
Client: CITY OF HAVELOCK
Facility:WWTP
NPDES#:NC0021253
Test Date: 10-Oct-23
Laboratory Sample ID#:T65883
Test Reviewed and Approved By:
eohert g&llect £ + .
Robert W.Kelley,Ph.D. Amy McMahan
President QA/QC Review
ti ®"�1
P" r
Certification#E87819
4 SCDHEC Certification#23104
Test results presented in this report conform to all requirements of
NELAC,conducted under NELAC Certification Number E87819
Florida Dept.of Health.Included results pertain only to provided samples. NCDENR Certification 4 022
Page 1 of 6

Effluent Toxicity Report Form - Chronic Mysidopsis Pass/Fail Date: 10-Oct-23
Facility: Havelock NPDES II NC0021253 Pipe#: 001 County: Craven
Laboratory Performing Test: ETT Environmental Inc. Comments:
x
Signature of Operator in Responsible Charge
X deohert g&llew
Signature of Laboratory Supervisor
MAIL ORIGINAL TO: Environmental Sciences Branch
Division of Water Quality
NC DENR
1621 Mail Service Center
Raleigh,NC 27699-1621
Control Replicates 1 2 3 4 5 6 7 a
Surviving 0 5 5 5 5 5 5 4 4 %Survival 100.0%
Original 5 5 5 5 5 5 4 4
Weight(per Original) 0.396 0.376 0.442 0.394 0.334 0.450 0.345 0.375 Avg Weight(mg) 0.389
Treatment 2 Replicates 1 2 3 4 5 6 7 8
Surviving 0 5 4 5 5 4 4 5 4 { %Survival I 100.0%
Original# 5 4 5 5 4 4 5 4
• Weight(per Original) 0.766 0.4075 0.410 0.432 0.4425 0.4775 0.436 0.4325 Avg Weight(mg) 0.476
Water Quality Data
Day
Control 0 1 2 3 4 5 6 7 Test Results
pH Initial 8.2 8.2 8.3 8.2 8.1 8.3 8.2
pH Final^ 7.9 8.0 7.9 7./ 8.0 8.0 7.7 Significant Mortality?
DO Inibal 6.9 7.1 6.9 7.1 7.0 7.6 7.5 Yes No
DO Final 6.7 6.8 6.9 6.0 7.4 7.3 6.3 X
Temp Initial 25.2 25.5 25.4 25.5 25.4 25.5 25.8 Check Ono
Temp Final 26.0 25.9 26.0 25.9 25.9 26.0 26.1
Salinity Initial 25.3 25.5 25.5 25.4 25.5 25.1 25.5 Growth _
Cain. I Ir -1.94
Treatment 0 1 2 3 4 5 6 7 Tabular t L_- 1.76
pH Initial 8.3 8.3 8,3 8.2 8.2 8.3 8.2 Fecundity
pH Final 8.0 8.2 8.1 7.9 8.1 8.0 7.8 Rank Sum
DO Initial 7.1 7.1 7.6 7.5 7.1 7.3 7.2 Crit.Value It
DO Final 6.7 6.9 6.8 5.9 7.3 5,9 5.1
Temp Initial 25.0 25.6 25.8 25.7 25.7 25.8 25.7 PASS FAIL
Temp Final 26.0 25.9 26.0 25.9 25.9 26.0 26.1 X
Salinity Initial 24,6 24.5 24.4 24.6 24.7 24,5 24.7 Check One
Sample Test Date: 10.Oct-23
Collection Start Date 08-Oct-23 10.0ct-23 12-Oct-23 Effluent Test Concentration: 15%
Grab 5 replicates were set for each control test replicate;where<5 are shown the organisms were lost during renews
Composite(Duration) 24 hr 24 hr 24 hr 5 replicates were sot for each treatrnent test replicate;where<5 are shown the organisms were lost during reno
Conductivity(pmhosicm) 720 681 800
Chlorine(rng/L) <0.05 <0.05 <0.05
Sample Temp.al Receipt 0.1 1.0 0.5
OWO Form AT-4(6/99)
Page 2 of 6

Day 1 Day 2 Day 3 Day 4 Day 5 Day 6 Day 7 eight Fecundity orig
150urc0 rep seed lost coed Lost Dead Lost Dead Lost Dead Lost Dead Lost aead Lost mg H-Grev Gravid Survival # Lebo T65883
A 0 0 0 0 0 0 0 0 0 0 0 0 0 0 1.98 5 5 Client Havelock
8 0 0 0 0 0 0 0 0 0 0 0 0 0 0 1.88 5 5 Sample ID WWTP
C 0 0 0 0 0 0 0 0 0 0 0 0 0 0 2.21 5 5 NPDESII NC0021253
D 0 0 0113 0 0 0 0 0 0 0 0 0 0 1.97 5 5 County Craven i
COf1TrO1 ©© 0 0 0 0 0 0 0 0 0 0 0 0 0 0 1.67 5 5 Month 10
0 0 0 0 0 0 0 0 0 0 0 0 0 0 2.25- 5 5 Start&fed Date 10.Oct-23 _
1111 0 0 0 0 0 0 0 0 0 0 113 0 0 _1.38 4 stem a fed Time 02:00 PM
H 0 0 0 0 0 0 0 0 0 0 0 1 0 0 1.50 11111 4 Storied&tart By JC
A
5 Teat Organism A.BAHIA
8 5 Nee born date 03.0ct-23
C 5 Hen.born time 1400.1630
D
6 Teel Typo NCCPF
0 --------------- ial 5 Dilution Water Instant Ocean _
--- -- -------- 5 Units for Canc. %
--- -- -M------ 5 X3rd BROOD
©------- --- 5 5 Test veseela 400 ant -
A I _5 5 Test volume 150 mi
IIIIIIIIIIIIIIIII 5 5 Incubator/ i
$ 5 5 Light 8dk
-
51 5 EN I Temp 250 ~
O ®..III■..... III■.._ 5 5 Test me w/Ahoddemla rso
EPA 811-F-01.01e:ra01
INiiiiiiuiiiL
55 5
5
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5 5
5 5
6 111111111111111111111Mill5 5 All reps have Comment;
ants
-------- ---- 5 .rganisms unless noted otherwise.
A I
B 5 Control Ini temp . '- " ^+;•
C _---- ------ -- 5 5 ..
D -----:---------I
D ------ ----- 5 5 •BS 10/10/23
©----------- _ 5 5 7 DAYS OLD
-- --------- -= 5
•
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0
3
B 0 0 s t „ 0 s t s 6 t 1.63E 4
1 1.63 4
11111 0 0 0 0 0 0 0 0 0 0 E3 0 0 2.05 5 5
D 0 0 0 0 0 0 0 0 0 0 0 0 0 2.16 IIIII5 5
15 0 0 0 0 0 0 0 0 0 0 0 0 0 1 1.77MIN 4 4
0 1 0 0 0 0 0 0 0 0 0 0 0 0 1.51 41 4
0 0 0 6 0 0 0 0 0 0 0 0 ©2.18 _ 5
0 0 0 a 0 0 0 0 0 0 0 0 0M 1.73MIN 4 4
Raney JG JG JZ JG JC JZ End Date
Fed JG JG JZ JG JC JZ Time lea a tor.", 02.18 PM 0220 PN 03.361,1 II to A4 09,11AM la P 3 I 17-Oct-23 JC
Eeueni New letup.•C 25.6 25.8 25.7 25.7 25.8 25.7 o121 PM
Old lamp•c 26 25.9 26 25.9 25.9 26 26.1 D=Dead NIA•Lost or not used
canvas N..amp.•c 25.5 25.4 25.5 25.4 25.5 25.8
Page 3 of 6

ETTCAN OF CUSTODY RECORD
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PO Sox 16414,Greenville,SC 2950E-7414
[phone], [phone]
ShippEng Address:4 Craftsman Ct,Greer,SC 29650
www.ettlab.arg
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Sample Custody Transfer Record Secure Receipt Sample
Date Time •!/ ,Relinquished By I Organization Received By/Organization Area Temp°C Preserved?
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COMPOSITE SAMPLING PROCEDURES TEMPERATURE MONITORING PROCEDURES HOLD TIME PROCEDURES
Composite samples must he collected over a 24 hour period. Sample temperature during collection and transport must be between For toxicity testing the sample must first be used within 36 hours
Time Proportional:I sample each hour for 24 hours.Equal volur 0.0 and 6.0°C.Samples must not be frozen.Use water ice in sealed bags. of sample collection(completion of composite sample).
or at minimum I sample every 4 hours over 24 hours. Sample may not be used after 72 hours from sample collection.
Flow Proportional:As per instructions in NPDES permit.
-- - Page4 of 6

ET_. 1.,
CHAIN OF CUSTODY RECORD
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[phone], (SOO)891-2325
Shipping Address:4 Craftsman Ct,Greer,SC 29650
www.attlab.org
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Composite samples must be collected over a 24 hour period. Sample temperature during collection and transport must be between For toxicity testing the sample must first be used within 36 hours
Time Proportional: I sample each hour for 24 hours.Equal volu 0.0 and 6.0°C.Samples must not be frozen.Use water ice in sealed bags. of sample collection(completion of composite sample).
or at minimum I sample every 4 hours over 24 hours. Sample may not be used after 72 hours from sample collection.
Flow Pro ortional:As r instructions in NPDES ermit.
—Page 5 of 6 - — •
—

ET. ji.,
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F Y,ter � $ �:
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[phone], [phone]
Shipping Address:4 Craftsman Ct.Greer,SC 29650
www.ettlab.arg
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Sample Custody Transfer Record Secure Receipt Sample
Date Time Relinquished By/Organization Received By/Organization Area Temp°C Preserved?
(4.1111 1M1 0 i Jacob 6v++(ekv I C. TP owe(ack.
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COMPOSITE SAMPLING PROCEDURES iTEMPERATURE MONITORING PROCEDURES HOLD TIME PROCEDURES
Composite samples must be collected over a 24 hour period. Sample temperature during collection and transport must be between For toxicity testing the sample must first be used within 36 hours
Time Proportional: I sample each hour for 24 hours.Equal vole 0.0 and 6.0°C.Samples must not be frozen.Use water ice in sealed bags. of sample collection(completion of composite sample).
or at minimum 1 sample every 4 hours over 24 hours. j Sample may not be used after 72 hours from sample collection.
Flow Proportional:As per instructions in NPDES permit.
— - Page 6 of 6 —

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Tab E
Annual Priority Pollutant Analysis
Results, 2021 -2023
L

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Drinking Water ID: 37715
{�
Wastewater ID: 10
CC I"OAK 'I>DRIVE
ID#: 204 H
CITY OF HAVELOCK
MR. JAMES CARTER
WASTEWATER TREATMENT PLANT DATE COLLECTED: 02/02/21
304 N. JACKSON DRIVE DATE REPORTED : 02/19/21
HAVELOCK ,NC 28532
REVIEWED BY: {.
Effluent Analysis Method
PARAMETERS Date Analyst Code
Ammonia Nitrogen as N, mg/l 0.13 02/03/21 KES 350.1 R2-93
Total Kjeldahl Nitrogen as N,mg/1 1.05 02/05/21 TLH 351.2 R2-93
Nitrate-I-Nitrite as N, mg/1 2.75 02/03/21 DTL 353.2 R2-93
Total Phosphorus as P, mg/I 0.42 02/05/21 KES 365.4-74
)il & Grease (HEM), mg/I <5.0 02/04/21 KDS I664B
'henol, ag/I TESTED
Total Cyanide, mg/1 <0.005 02/08/21 KDS 4500CNE-11
Total Hardness, mg/I 100 02/08/21 MBS 2340C-11
Total Dissolved Residue, mg/1 260 02/05/21 KDS D5907-13
Antimony, ug/1 <3.0 02/10/21 NAB EPA200.8
Arsenic, ug/I <2.0 02/08/21 MTM 3113B-10
Beryllium, ug/1 <1.0 02/05/21 LFJ EPA200.7
Cadmium, ug/I <0.5 02/05/21 MTM 3113B-04
Total Chromium, ug/1 <5.0 02/05/21 LFJ EPA200.7
Copper, ug/I 4 02/05/21 LFJ EPA200.7
Lead, ug/I <2.0 02/05/21 MTM 3113B-10
Nickel, ug/1 <2.0 02/05/21 LFJ EPA200.7
Selenium, ug/I <1.0 02/11/21 NAB EPA200.8
Silver, ug/l <1.0 02/05/21 LFJ EPA200.7
Thallium, ug/I <1.0 02/10/21 NAB EPA200.8
Zinc, ug/I 47 02/05/21 LFJ EPA200.7
•
NOTE: Any result listed above as"TF,S'I'ED"was sub-contracted to another laboratory. The corresponding results are attached.

Ci 11
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11
Drinking Water ID, 37715
Waetewater ID: 10
CLIENT: CITY OF HAVELOCK CLIENT ID: 204 H
MR. JAMES CARTER
WASTEWATER TREATMENT PLANT ANALYST: JAP
304 N. JACKSON DRIVE DATE COLLECTED: 02/02/21
HAVELOCK, NC 28532 DATE ANALYZED: 02/03/21
DATE REPORTED: 02/19/21
REVIEWED BY: /~-
VOLATILE ORGANICS
EPA METHOD 624.1
Effluent
PARAMETERS, ugh
1. Chloromethane <10.00
2. Vinyl Chloride <10.00
3. Bromomethane <10.00
4. Chloroethane <10.00
5. Trichlorofluoromethane <5.00
6. 1,1-Dichloroethane <5.00
7. Methylene Chloride <10.00
8. trans-1,2-Dichloroethene <5.00
9. 1,1-Dichloroethene <5.00
10. Chloroform <5.00
11. 1,1,1-Trichloroethane <5.00
12. Carbon Tetrachloride <5.00
13, Benzene <5.00
14. 1,2-Dichloroethane <5.00
15. Trichloroethene <5.00
16. 1,2-Dichloropropane <5.00
17. Bromodichloromethane <5.00
18. 2-Chloroethylvinyl Ether <5.00
19. cis-1,3-Dichloropropene <5.00
20. Toluene <5.00
21. trans-1,3-Dichloropropene <5.00
22. 1,1,2-Trichloroethane <5.00
23. Tetrachloroethene <5.00
24. Dibromochloromethane <5,00
25. Chlorobenzene <5.00
26. Ethylbenzene <5.00
27. Bromoform <5.00
28. 1,1,2,2-Tetrachloroethane <5.00
29. 1,3-Dichlorobenzene <5.00
30. 1,4-Dichlorobenzene <5.00
31. 1,2-Dichlorobenzene <5.00
32. Acrolein <100.00
33. Acrylanitrile <50.00

_ o � c rititt all I © ric1i
" Drinking Water ZDs 37715rt
Wastewater ID! 10
+ "{`GR 14. r;° a ,;,,e.. s ' 4 s ".+;.t t t s 7 v v r
��' ,.2.. a� ,� "`' 3.F r ¢ar o- i "= &.w h "i. n^�- .a
CLIENT: CITY OF HAVELOCK CLIENT ID: 204 H
MR. JAMES CARTER
WASTEWATER TREATMENT PLANT ANALYST: JAP
304 N. JACKSON DRIVE DATE COLLECTED: 02/02/21 Page: 1
HAVELOCK, NC 28532 DATE EXTRACTED: 02/04/21
DATE ANALYZED: 02/05/21
REVIEWED BY: _ '--�_ DATE REPORTED: 02/19/21
SEMIVOLATILE ORGANICS
EPA METHOD 625.1
Effluent
PARAMETERS, ugh'
1. N-Nitrosodimethylamine <10.00
2. Phenol <10,00
3. Bis(2-Chloroethyl) Ether <10.00
4. 2-Chlorophenol <10.00
5. 1,3-Dichlorobenzene <10.00
6. 1,4-Diehlorobenzene <10.00
7. 1,2-Dichlorobenzene <10.00
8. Bis(2-Chloro-l-methylethyl) Ether <10.00
9. Hexachloroethane <10.00
10. N-Nitroso-Di-N-Propylamine <10.00
11. Nitrobenzene <10.00
12, Isophorone <10.00
13. 2-Nitrophenol <10.00
14. 2,4-Dimethylphenol <10.00
15. Bis(2-Chloroethoxy) Methane <10.00
16. 2,4-Dichlorophenol <10.00
17. 1,2,4-Trichlorobenzene <10.00
18. Naphthalene <10.00
19. Hexachlorobutadiene <10.00
20. 4-Chloro-3-Methylphenol <20.00
21. Hexachlorocyclopentadiene <10.00
22. 2,4,6-Trichlorophenol <10.00
23. 2-Chloronaphthalene <10.00
24. Acenaphthylcnc <10.00
25. Dimethylphthalate <10.00
26. 2,6-Dinitrotoluene <10.00
27. Acenaphthene <10.00
28. 2,4-Dinitrophenol <50.00
29. 4-Nitrophenol <50.00
30. 2,4-Duiitrotoluene <10.00
31. Fluorene <10,00
32. Diethylphthalate <10.00
33. 4-Chlorophenyl Phenyl Ether <10.00
34. 4,6-Dinitro-2-Methylphenol <50.00
35. N-Nitrosodiphenylamine <10.00
36. 4-Bromophenyl Phenyl Ether <10.00
37. Hexachlorobenzene <10.00
38. Pentachlorophenol <50.00
39. Phenanthrene <10.00
40. Anthracene <10.00
41. Di-N-Butylphthalate <10.00
42. Fluoranthene <10.00
43. Benzidine <100.00
44. Pyrene <10.00
45. Butylbenzylphthlate <10.00
46. Benzo[a]anthracene <10.00
47. 3,3'-Dichlorobcnzidine <10.00
48. Chrysene <10.00

1_ ,iliCliVERgEt( _ENTPOR Dad
Drinking Water IDa37715
Wastewater ID: 10
yry REr
CLIENT: CITY OF HAVELOCK CLIENT ID: 204 H
MR. JAMES CARTER
WASTEWATER TREATMENT PLANT ANALYST: JAP
304 N. JACKSON DRIVE DATE COLLECTED: 02/02/21 Page: 2
HAVELOCK, NC 28532 DATE EXTRACTED: 02/04/21
DATE ANALYZED: 02/05/21
REVIEWED BY: , ��, DATE REPORTED: 02/19/21
SEMIVOLATILE ORGANICS
EPA METHOD 625.1
Effluent
PARAMETERS, ugh
49. Bis(2-Ethylhexyl)phthalate <20.00
50. Di-N-Octylphthalate <10.00
51. Benzo[b]fluoranthene <10.00
52. Benzo[k]fluoranthene <10.00
53. Benzo[a]pyrene <10.00
54. Indeno(1,2,3-C,d)pyrene <10.00
55. Dibenzo[a,h]anthracene <10.00
56. Benzo[g,h,i]perylene <10.00
57. 1,2-Diphenylhydrazine <10.00

Pace Analytical Services,LLC
9800 Kincey Ave. Suite 100
aceAnalytical Huntersville,NC 28078
www.pacelabs.com [phone]
Page 1 of 1
Laboratory Report
Mark Oliveira Report Date: 02/11/2021
Environment 1 Date Received: 02/04/2021
114 Oakmont Dr
Greenville, NC 27858
Project: City of Havelock
Pace Project No.:92520305
Sample: City of Havelock-Effluent Lab ID: 92520305001 Collected: 02/02/21 10:15 Matrix: Water
Method Parameters Results Units Report Limit Analyzed Qualifiers
EPA420.4 Rev 1.0 1993 Phenol ND mg/L 0.020 02/11/21 09:14
Reviewed by: CC � c�f4/c
Stephanie Knott
336-996-2841
[e-mail]
Pace Analytical Services Asheville
2225 Riverside Drive,Asheville,NC 28804 North Carolina Wastewater Certification#:40
Florida/NELAP Certification#: E87648 South Carolina Certification#:99030001
North Carolina Drinking Water Certification#:37712 VirginiaNELAP Certification#:460222
Page 1 of

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Environment 1,Inc. C1-121 IN U14 Cf..iblUlt,I ItrA_Aiittli
P.O.Box 7085, 114 Oakmont Dr. ei)\* Fag,: 1 o i- 2
Greenville,NC 27858
en v i ronment 1,i nc.corn, DISINFECTION I I J jip CHLORINE NEUTRALIZED AT COLLECTION
Phone[phone] •Fax[phone] el
CHLORINE CLIENT: 204 H Week: 11
UV Ll 4c1 ha 42 4) .a 71 Q. .. -2..,72,L, 72 pH CHECK(LAB)
CITY OF HAVELOCK ij NONE PP P P G G P P P P P P G G G G CCKTAINER TYPE,P'G
MR.JAMES CARTER
WASTEWATER TREATMENT PLANT
304 N.JACKSON DRIVE LI CCCCCCDCA A AAA A A CHEMICAL PRESERVATION
HAVELOCK NC 28532
6 .. A-NONE D-NAOH
E 1= 7 _.., ti)
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SAMPLE LOCATION DATE TIME .P. .- W tax ?.,-. 'et E4 Z E4 0 IZ,1 0
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Effluent iw-')ZD-1. i)15- j 1 16 LIA: '6.1' ›.'," ..t. eicianuffi CLASSIFICATION:
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II 1111111111111111111111111 FLI
111 DWR/GW
1111 III
J Ma rj SOLID WASTE SECTION 1111 111.11111 CHAIN OF CUSTODY(SEAL)MAINTAINED
DURING HIPMENT/DELIVERY
Y N
SAMPLES COI 1 PCTED BY:
I I (Please Pan)
1
Petkl QtNIN,C
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SAMPLES RECEIVED IN LAB AT
RELINQUISHED BiF.1 .1(SANIPLER) DAIE/yME REpEIVEDB SIG.) DATE/TIME COMMBITS.
r--...iih-........ .. --- ';•1 110 !ifq t `.5
RELINQUISHED BY(SIG.) DATE/TIME RECENED BY(SG.) DATET1ME
I -1
RELINQUISHED BY(51G.) DATEIT1ME RECEIVE/BY(SIG) DAMTIME 1
I l 1
.EASE READ Instructions for completing this form on the reverse side. Sampler must place a"C"for composite sample or a"G"for
FOAM 45 Grab sample in the blocks above for each parameter requested, . _
387072
.

Environment 1,Inc. ‘...,ratt..ILLNI kie.t. t,..,+LILY 1.'0,..rilL.0 A.P.O.Box Box 7085, 114 Oakmont Dr. page 2 ,.,f. 2
Greenville,NC 27858
environmentlinc.com i DISINFECTION 1I1 1111111111 CHLORINE NEUTRALIZED AT COI I FCTION
D
Phone[phone]*.Fax[phone]
CHLORINE
CLIENT: 204 H Week: 11
lil. UV 72-72 -7 ph CHECK ILAB)
—
DITY OF HAVELOCK [:1 NONE G G G I CONTAINEFI TYPE.PIG
VER.JAMES CARTER
WASTEWATER TREATMENT PLANT ---
1
304 N.JACKSON DRIVE
IIAVELOCK NC 28532 .L1 cHailCAL PRESERVATION
=-2.-----1.--)--1---.
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A-NONE D-NAOH
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G-NATHIOSULFATE
SAMPLE LOCATION DATE TIME
ikir I . .
Effluent 1i), I p:I Ak 16 it. Px.. , ..(81-111111111111m. L 1 CLASSIFICATION
111111= I 11111 a WASTEWATER(NPOES)
III IIII I
I I 111 1:1 DRINKINGWAIER
I DWRit:-.. 1
11111111111111
1111111111111111 111 NM E:1 SOUD WASTE SECTION
MI= III _, _
id
11.11 CHAIN OF CUSTODY(SEAL) MAINTAINEC
DURING SHIPMENT/DELIVERY
Y ) t•I
IMII II 1 ll 111111
III 111111.1M1 SAMPLES COLLECTED BY:
(Pion?Print)
1
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[ SAMPLES RECEIVED IN LAB AT Z•1 'i
R QUISHED BY r)(SAMPLER) DATE/T1ME RECEIVED BY 1.) DATETIME ,,,., CO-' MMENTS:
ag' 1 I VLIS Waft I I 1-.54/
RELINQUISHED BY(SIG.) DATE/TIME RECEIVED BY;SIG.) DATEMME
1 I
RELINQUISHED BY(SIG) I DATFJTIME RECEIVED BY( G.) DATE/TIME
1 I I
omposite sample or a"G for
" " c "
LEASE READ Instructions for completing this form on the,reverse side Sampler must place a C for.
FORM 45 Grab sample in the blacks above for each parameter requested. 387071

L uD iN it lip 1 ©ii
t
,
Drinking Water ID: 377
�t7 x ' Wastewater ID; 10
14 OAKMONT E
GtREENViLLE N u. 2r-6;a
ID#: 204 H
CITY OF HAVELOCK
DEVIN ADAMS
WASTEWATER TREATMENT PLANT DATE COLLECTED: 05/25/22
304 N. JACKSON DRIVE DATE REPORTED : 07/05/22
HAVELOCK, NC 28532
REVIEWED BY:
Effluent Analysis Method
PARAMETERS Date Analyst Code
Ammonia Nitrogen as N, mg/t 0.17 05/31/22 TRJ 350.1 R2-93
Total I4;jeldahl Nitrogen as N,mg/l 1.26 06/02/22 TRJ 351.2 R2-93
Nitrate+Nitrite as N, mg/1 2.76 06/01/22 TRJ 353.2 R2-93
Total Phosphorus as P, mg/1 1.43 06/02/22 BMD 365.4-74
Oil & Grease (HEM), mg/1 <5.0 05/31/22 BMD 1664B
Phenol, ug/I TESTED
Total Cyanide, mg/1 <0.005 06/06/22 HMM 4500CNE-16
Total Hardness, mg/1 108 05/31/22 DNS 2340C-11
Total Dissolved Residue, mg/1 410 05/26/22 HMV D5907-13
Antimony, ug/I <3.0 06/30/22 NAB EPA200.8
Arsenic, ug/I <2.0 06/01/22 MTM 3113B-10
Beryllium, ug/I <1.0 06/01/22 LFJ EPA200.7
Cadmium, ug/1 <0.5 05/31/22 MTM 3113B-10
Total Chromium, ug/I <5.0 06/01/22 LFJ EPA200.7
Copper, ug/1 5 06/01/22 LFJ EPA200.7
Lead, ug/I <2.0 06/03/22 MTM 3113I1-10
Nickel, ug/1 2 06/01/22 LFJ EPA200.7
Selenium, ug/I <1.0 06/20/22 NAB EPA200.8
Silver, ug/I <1.0 06/01/22 LFJ EPA200.7
Thallium, ug/I <1.0 06/20/22 NAB EPA200.8
Zinc, ug/1 41 06/01/22 LFJ EPA200.7
NOTE: Any result listed above as"TESTED"was sub-contracted to another laboratory. The corresponding results are attached.

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it
Drinking Water ID: 377
Wautewator ID: iQ
14 OAKMONT MA
GREE€, ILLE ,t�, I� a ,.,,el.1._ t:�
FAX[phone]'t..
CLIENT: CITY OF HAVELOCK CLIENT ID: 204 H
DEVIN ADAMS
WASTEWATER TREATMENT PLANT ANALYST: JAP
304 N. JACKSON DRIVE DATE COLLECTED: 05/25/22
HAVELOCK, NC 28532 DATE ANALYZED: 05/26/22
REVIEWED BY: /./ / `-^ \ DATE REPORTED: 07/05/22
VOLATILE ORGANICS
EPA METHOD 624.1
Effluent
PARAMETERS, ugh
1. Chloromethane <10.00
2. Vinyl Chloride <10.00
3. Bromomethane <10.00
4. Chloroethane <10.00
5. Trichlorofluoromethane <5.00
6. 1,1-Dichloroethane <5.00
7. Methylene Chloride <10.00
8. trans-1,2-Dichloroethene <5.00
9. 1,1-Dichloroethene <5.00
10. Chloroform <5.00
11. 1,1,1-Trichloroethane <5.00
12. Carbon Tetrachloride <5.00
13. Benzene <5.00
14. 1,2-Dichloroethane <5.00
15. Trichtoroethehe <5.00
16. 1,2-Dichloropropane <5,00
17. Bromodichloromethane <5.00
18. 2-Chloroethylvinyl Ether <5.00
19. cis-1,3-Dichloropropene <5.00
20. Toluene <5.00
21. trans-1,3-Dichloropropene <5.00
22. 1,1,2-Trichloroethane <5.00
23. Tetrachloroethene <5.00
24. Dibromochloromethane <5.00
25. Chlorobenzene <5.00
26. Ethylbenzene <5.00
27. Bromoforrn <5.00
28. 1,1,2,2-Tetrachloroethane <5.00
29. 1,3-Dichlorobenzene <5.00
30. 1,4-Dichlorobenzene <5.00
31. 1,2-Dichlorobenzene <5.00
32. Acrolein <50.00
33. Acrylonitrile <50.00

• E11:0Wif(DIMUtigitii haSTP©riVrkol,
y' ld tj aT rk Yr -- u.a._ „W
4A: ' ' � } s Drinking Water ID: 377
�`"` "� Wastewater ID: 10
14 OAK COVE ,• == e a4a s
Gl E ILLE N.G. 27658t .1 #1 { } f
FAX( ) 58µo3
CLIENT: CITY OF HAVELOCK CLIENT ID: 204 H
DEVIN ADAMS
WASTEWATER TREATMENT PLANT ANALYST: HIC
304 N. JACKSON DRIVE DATE COLLECTED: 05/25/22 Page: 1
HAVELOCK, NC 28532 DATE EXTRACTED: 06/01/22
.� J` DATE ANALYZED: 06/03/22
REVIEWED BY: �._ DATE REPORTED: 07/05/22
SEMIVOLATILE ORGANICS
EPA METHOD 625.1
Effluent
PARAMETERS, ugh!
1. N-Nitrosodimethyiamine <10.00
2. Phenol <10.00
3. Bis(2-Chloroethyl) Ether <10.00
4. 2-Chlorophenol <10.00
5. 1,3-Dichlorobenzene <10.00
6. 1,4-Dichlorobenzene <10.00
7. 1,2-Dichlorobenzene <10.00
8. Bis(2-Chloro-l-methylethyl) Ether <10.00
9. Hexachloroethane <10.00
10. N-Nitroso-Di-N-Propylamnie <10.00
11. Nitrobenzene <10.00
12. Isophorone <10.00
13. 2-Nitrophenol <10.00
14. 2,4-Dimethylphenol <10,00
15. Bis(2-Chloroethoxy) Methane <10.00
16. 2,4-Dichlorophenol <10.00
17. 1,2,4-Trichlorohenzene <10.00
18. Naphthalene <10.00
19. Hexachlorobutadiene <10.00
20. 4-Chloro-3-Methylphenol <20.00
21. Hexachlorocyclopentadiene <10.00
22. 2,4,6-Trichlorophenol <10.00
23. 2-Chloronaphthalene <10,00
24. Acenaphthylene <10.00
25. Dimethylphthalate <10.00
26. 2.6-Dinitrotoluene <10.00
27. Acenaphthene <10.00
28. 2,4-Diuitrophenol <50.00
29. 4-Nitrophenol <50.00
30. 2,4-Dinitrotoluene <10.00
31. Fluorene <10.00
32. Diethylphthalate <10.00
33. 4-Chlorophenyl Phenyl Ether <10.00
34. 4,6-Dinitro-2-Methylphenol <50.00
35. N-Nitrosodiphenylamine <10.00
36. 4-Bromophenyl Phenyl Ether <10.00
37. Hexachlorobenzene <10.00
38. Pentachlorophenol <50.00
39. Phenanthrene <10.00
40. Anthracene <10.00
41. Di-N-Butylphthalate <10.00
42. Fluoranthene <10.00
43. Benziduie <100.00
44. Pyrene <10.00
45. Butylbenzylphthlate <10.00
46. Benzo[a]antluracene <10.00
47. 3,3'-Dichlorobenzidine <10.00
48. Chrysene <10.00

itaw![r©mom Impavifmamp.
s .
Drinking Water ID: 377
i< VR'S3\1Yt ., . „ tawater ID. 20
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LJ37i �Z'liY� `x �`���
GREE VILLE, N: . 27858 $fit t 1+ t { ¢ �+
FAX f 52)758-0832
CLIENT: CITY OF HAVELOCK CLIENT ID: 204 H
DEVIN
ADAMS
WASTEWATER TREATMENT PLANT ANALYST: HIC
304 N. JACKSON DRIVE DATE COLLECTED: 05/25/22 Page: 2
HAVELOCK, NC 28532 DATE EXTRACTED: 06/01/22
DATE ANALYZED: 06/03/22
REVIEWED BY: /f _ DATE REPORTED: 07/05/22
SEMIVOLATILE ORGANICS
EPA METHOD 625.1
Effluent
PARAMETERS, ugh
49. Bis(2-Ethylhexyl)phthalate <20.00
50. Di-N-Octylphthalate <10.00
51. Benzo[b]fluoranthene <10.00
52. Benzo[k]fluoranthene <10.00
53. Benzo[a]pyrene <10.00
54. Indeno(1,2,3-C,d)pyrene <10.00
55. Diben;:o[a,h]anthracene <10.00
56. Benzo[g,h,i]perylene <10.00
57. 1,2-Diphenylhydrazine <10.00