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HomeMy WebLinkAboutNC0060747-RESCINDEDd to SUBMIT FORM ON YELLOW PAPER ONLY Facility Name:_, Permit Name (If Facility Address Well Location/ Site Name: Please Print Print Clearly or Type z County IV.4P417 h�a,wN` tz(ZIP)c7 Telephone #:9/0... -21z, &Mi Z No. of Wells to be Sampled: e• Well Identification Number (from Permit): !n :u - Z For Groundwater Treatment Systems Well Depth: /R . it. Well Dlameter.? In. Check One: Screened Interval: ft. to ff. ❑ Influent (98) Depth to Water Level: `' ft. below measuring point. ❑ Effluent (99) Measuring Point Is 3 ft. above land surface. Gallons of water pumped/balled before sampling: Field analysis: pH - , Specific Conductance uMhos Temp."C, Odor Appearance PERMIT #: EXPIRATION DATE: Non -Discharge UIC NPDES NCyo607,Y7 TYPE OF PERMITTED OPERATION BEING MONITQPED:E Lagoon Rernediation:Inrillralloa—Dallefy_ Spray Field Rotary Dish Other: A. Land Application of NOTE: Values should reflect dissolved and s colloidal concentrations. r? Date sample collected: Dale sampleatlalyFpd: LaboratoryName: £tiv; a anr�n fa7 ! Certification No. iD PARAMETE$fZ (Samples for metals were collected unfiltered YES _NO and field aclditled COD �//8 mg/I Nitrite (NO2) as,N mg/I Coliform: MF Fecal /100ml Nitrate (NO3) as N Coliform: MF Total /100ml Phosphorus: Total as P _ mg/I (Note: Use MPN mathod for highly turbid samples) Orthophosphate mg/1 Dissolved Solids: Total : ca mg/I At - Aluminum- mg/I pH (when analyzed) units Be - Barium mg/I TOC v 9 5'6 mg/I "�Ca - Calcium mg/I Chloride i5 mg/I Co -Cadmium mg/I Arsenic mg/I Chromium: Total mg/I Grease and Oils mg/l. Cu - Copper mg/I Phenol mg/I Fe - Iron mg/I Sulfate mg/I Hg - Mercury mg/l Specific Conductance Z; v LiMhos K - Potassium mg/I Total Ammonia mg/1 Mg - Magnesium mg/I TKN as N ' mg/I Mn - Manganese mg/I S, _YES _ NO) NI - Nickel mg/I Pb - Leaf mg/I Zn - Zinc mg/l Ammonia Nitrogen mg/I Other (Specify Compounds and Concentration Units) ORGANICS: (GC,GC/MS,HPLC) (Specify test and method #.-Attach lab report.) Report Attached? Yes (1) No - (0) VOC method# - method # _ method # h GW-59 Rev. 4/98 EMWD,F@I@E@I,mq Flo offi @@TPOPaq@d NATIONAL MECHANICAL CARBON (WELLS) C/O MR. DEAN BYRD ` 5739 U.S. 401 SOUTH BUNNLEVEL ,NC 28323 . ,s COD, mg/1 Total Organic Carbon, mg/l Chloride, mg/l Total Dissolved Residue, mg/l Conductivity (at 25c), uMhos Monitoring Analysis Method Well #2 Date Analyst Code 418 04/10/01 TRB HACH8000 4956 04/17/01 SET EPA415.1' 15 04/04/01 CDH SM4500-CLB 209 04/02/01 TRB EPA160.1 214 04/04/01 HNB SM2510B Akins Water IDS 37715 Wastewater IDS 10. ID#: 434 DATE COLLECTED: 03/30/01 DATE REPORTED : 04/17/01 REVIEWED BY: - Laboratory Analyses —Environmental Consultants EnviwajgjjeuP 1, file. 0.0. Box 4 Oakmonl Dr. Greenville, NC 27858 Phone (252) 756-6208 " Fax (252) 756-0633 CLIENT:43a Week: 12 NATIONAL MfEC11ANICAL CARBON (W C/O MR. DEAN BYRD 5739 U.S. 401 SOUTII BUNNLEVEL NC 28323 (910) 893-4143 COLLECTION SAMPLE LOCATION DATE TIME CHAIN OF CUSTODY I2LCORD ❑ CHLORINE ❑ UV )� NONE P P P P P ❑ C C A A A z z boori a 7 InslrucBons for completing Ihis form are on the reverse side. FORM RS Di'Z i �S COMMENTS: CHLORINE NEUTRALIZED NEUTRALIZED AT COLLECTION PH CHECK (LAB) CONTAINER TYPE. P/G CHEMICAL PRESERVATION A -NONE D-NAOH B-HNO, E-HCL C-HSO F- � ZINCACETATE G- NATHIOSULFATE a CLASSIFICATION: ❑ WASTEWATER(NPDES) ❑ DRINKING WATER ❑ DWat-W ❑ SOLID WASTE SECTION ❑ OTHER SAMPLES COLLECTED BY: (Please Plin) K¢wnc�, w. ,�,I' r SAMPLES RECEIVED IN LAB AT _ •C Sampler must place a "C" for composite sample or a "G' for Grab sample in the blocks above for each parameter requested. N ° 50443 �wdoQMUMM2 T, 9M@@1Tp@1F(W@ 1 CLIENT: NATIONAL MECHANICAL CARBON (WELLS) CLIENT ID: 434 C/O MR. DEAN BYRD 5739 D.S. 401 SOUTH ANALYST: •CMS BDNNLEVEL, NC 28323 DATE COLLECTED: 03/30/01 DATE ANALYZED: 04/04/01 REVIEWED BY: DATE REPORTED: 04/11/01 f--- VOLATILE ORGANICS STANDARD METHODS 6230D PARMfETE11S; u&n Well tit Monitoring I. Benzene 2. Bramobenzeae 3. Bromochloromethane 4. Bremodichloromethane 5. 'Brotvoform 6. Bromomethane 7. N-Butylbenzene S. Sec-Butylbenzene 9. Tert-Butylbenzene 10. Carbon Tetrachloride 11. Chlorobenzene 12. Chloroethane 13. Chloroform 14. Chloromethane 15. 2-Chlorotoluene 16. 4Chlorotoluene 17. Dibromochloromethane IS. 1,2-Dibromo-3Chloropropane 19. 1,2-Dibromoethane 20. Dibromomethane 21. 1,2-Dichlorobenzene 22. 1,3-Dichlorobenzene 23. 1,4-Dichlorobenzene 24. Dichlorodilluoromethane 25. 14-Dichloroethane 26. 1,2-Dichloroethane 27. 1,1-Dichloroethene 28. Cis-1,2-Dichlormthene 29. trans-1,2-Dichloroethene 30. 1.2-Dichloropropane 31. 1,3-Dicbloropropane 32. 2,2-Dichloropropane 33. 1,1-Dichloropropene 34.. Cis-1,3-Dlchloropropene 35. trans-1,3-Dichloropropene 36. Ethylbenzene 37. Heiachlorobutadiene 39. lsupropylbenzene 39. 4-Isopropyltoluene 40. Methylene Chloride 41. Naphthalene 42. Propylhenzene 43. Styrene 44. 1,1,1,2-Tetr2chloroethane 45. 1,1,2,2-Tetr2chloroethane 46. Te rrchloroethene 47. Tciuene $8. 1, :,3-Trichlorobenzene <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.56 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 1.50 <0.50 LaboratoryAnalyses - Environmental Consultants Page: 1 CLIENT: N7TIONAL MECHANICAL CARBON (WELLS) CLIENT ID: 434 C/O MR. DEAN BYRD 5739 U.S. 401 SOUTH ANALYST: CMS BMINLEVEL, NC 28323 DATE COLLECTED: 03/30/01 Page: 2 DATE ANALYZED: 04/04/ol REVIEWED BY: ' DATE REPORTED: 04/11/01 ' VOLATILE ORGANICS ' STANDARD METHODS 6230D , ' PARAMETERS u 6/l Monitoring. Well Ii2 49. 1 2,4 Trlchlorobenzene <O.SD 50. 1,1,1-Trichloroethane <0.50 51. 1,1,2-Trichloraethane <0.50 52. Trichloroethene' <0.50 53. Trichlorofluoromethane <0.50 54.. 1,2,3-Trichloropropane <0.50 55. 1,2,4-Trhnethylbemene <0.50 ' 56. 1,3,5-Trimethylbenzene <0.50 57. Vinyl Chloride <0:50 58. Total Xylenes <1.00 .. LaboratoryAnalyses — Environmental Consultants O raw-� huts cL�sGn B d- b� a l«w-sLd &,TJ ws"" N E n tb +FE w e,t� e[ ser�9 as £- A- c �y w tK ct.ecl CUE P rt-, d /kccv�toinlca -ron tea --tin ��'Zi�(�. L°dli(o7oo� •-�Ly � -�� ` fur T ottP. �ogrzcQ r� c+J (ZT'S /von su sec SA-� . ko up-� u 1,Mow , ® {�s o Skip mia'� opo. c"vsLo�-C- i �oS oohl) prn o ¢sEfnlllJ ``^ r lJ 'POND CL.oSrtiQ� �9�15 6Gtn.) Co/�.,Pc,�+`�D L �r2�f SIr�P � ae+�,p 'Raheoa� 0 i m( t l [VLC .�p;..t, �- C J (e bd 1.9e.Q�.4evct""' t> . North Carolina -Department of Environment and Natural Resources -Division or Water Quality -Groundwater Section - 1636 Mail �� i l l O I Service Center -Raleigh, NC 27699-1639 -Phone No. (919) 733-3221 WELL ABANDONMENT RECORD .WELLCONTRACTOR �t r,\ne m s Curc(E We\1 ;ll;%c� WELL CONTRACTOR CERTIFICATION # e�3'13 WELL USE (Check Applicable Box): Residential ❑ Municipal ❑ Industrial ❑ Agricultural ❑ Monitoring v Recovery ❑ Heat Pump Water Injection Cl Other ❑ If Other, List Use: 232973 2. WELL LOCATION: (Show a sketch of the location on back of form.) /i Nearest Town: �t�f, County H a,z-ne_k C_oun�ll Name and Number, Community, Subdivision , Lot 3. OWNER: NR�A M� ks-A RT' AcA\ 4. ADDRESS:—op�A�h�yt��nn a nnLl 5. TOPOGRAPHY: draw, slope, hilltop, valley, flat rr p t (circle one) rt 6. TOTAL DEPTH: 1 l DIAMETER �? 7. CASING REMOVED: feet diameter N MIA ° DISINFECTION: t C up OF: N l 1i (Amount of 70% hypochlorite used:) 9. SEALING MATERIAL: Neat Cement Sand Cemen[ bags of cement bags of cement gallons ofwater �_ gallons of water_ ]L111G1 Type material Amount 10. EXPLAIN METHOD EMPLACEMENT OF MATERIAL. �n�e� %o lFar of We-k\ �- r"a1vF Surc Mt obs�ruc�' ras r]noQ obkn;l� io}ta1 1�e u. }u�.ne Al ^•E (_'v P..k �,�-o hell 11. DATE WELL ABANDONED Ca i —ZOO Quadrangle No. La WELL DIAGRAM: Draw a detailed sketch of the LU well showing total depth, depth and diameter of r screens remaining in the well, gravel interval, intervals of casing perforations, and depths and types of fill materials used. F Mmlmr Mbt N[MnaXe eNcavu (feel DGS) weue. Talal °e mat W<R tl I. Mav tor WeD Coa,ltu[tlao Oefa W: weo Neae tamblbm 2• Raf Mkku IUsea MaleMt ?V Wmeler. 2 'ID R Y 2.-�T_ Rm Screen Matenat PVC_ DUm er. Z -to to : / O R °acre oo4/, v0 Setl't O R m 5 Se M M Ae,+,,�If S Rm 7 c 0 0 Fee, umeMt /O — 3� Si lrie A 1 Dellm> % C R ld✓ %� � I do hereby certify that this well was abandoned in accordance with 15A NCAC 2C, well constructioe standards, and that a copy of the record has been rovided t 1 owner. ? a� m Signature of person abandoning t � 11 ate - 1 I Q I y b Ca 0 WELL LOCATION Draw location sketch on th verse of t ' s eet, showing the direction and distance` of the well to at lea ) nearby reference points such as roads, intersections and streams. Identify roads with State Highway road identification numbers. U( ZL Submit original to the Division of Water Quality, Groundwater Section, one copy to the owner within 30 days from completion of abandonment. GW-30 Revised 12/99 National Mechanical Carbon 504 North Ashe Avenue Dunn, NC 28334 (910)892-9677 June 22, 2001 Mr. Stephen A. Barnhardt Regional Groundwater Supervisor Fayetteville Regional Office NCDENR 225 Green Street Suite 714 Fayetteville, NC 28301 Dear Mr. Barnhardt: National Mechanical Carbon has properly abandoned the remaining monitoring well associated with the settling ponds that had been used under NPDES Permit # NC0060747, but have now been closed. A copy of the well drilling company's Well Abandonment Record is attached. Thank you for your assistance in closing out this project. Sincer Norb Dickmann Environmental Engineer ,. r_i ,.p l i L' .. Ali. ., �.•.I1 1_ �. .... ., .. 1 , i. ..u.,. .'lil,. .il .. ,,.1 .. �., t JUUlvll 11- V nlvl ury , �..w. v , /" u v v, •� GROGNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM Please Print Clearly or Type Facility Name: AIA-rIOAJAL M,1rWAt1ICAL/ C'APB6 Permit Name (if different): Fa ilityAddress: 50�/ N0P-r14 /-}cNe /avr tsr"0 I yNN NC 2$33Y_ County _W R?N [TT (l5latol lzo) Contact Person: ^/6 au 7rCKinnN Telephone #:9ia-8`12-8081 Well Location/ Site Name: M r-u • z No. of Wells to be Sampled: prom Perml' Well Identification Number (from Permit): m w- -J­ I For Groundwater Treatment Systems Well Depth: / 8 it. Well Diameter:? in. Check One: ❑ Influent (98) Screened Interval: It. to ft. I ❑ Effluent (99) Depth to Water Level: 6 ft. below measuring po'nt. Measuring Point (M.P.) is:3 ft. above land surface. Relative M.P. Elevation in ft.: Gallons of water pumped/balled before sampling: 3 _ Date sample collected: // 9 00 Field analysis: pH , Specific Conductance: uMhos Temp. L—°C, Odor Appearance DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES WATER QUALITY DIVISION, GROUNDWATER SECTION 1636 MAIL SERVICE CENTER PERMIT #: EXPIRATION DATE: _ Non -Discharge UIC NPDES NC OO b a 7 V 7 TYPE OF PERMITTE9 OPERATION BEING MONITORED Lagoon _Remediation:Infiltration able Spray Field _ Remediation: G Rotary Distributor _Land Applicalioy( SludF1 Other: %i•07AC£Nr To C/o to&1 rgAZ co NOTE: Values should reflect dissolved and �o colloidal concentrations. 3 tV Date sample analyzed: i///7/00 Laboratory Name: I P_ e r r t W Certification No. PARAMETERS (Samples for metals were collected unfiltered YES _NO and field acidified COD -79 mg/I Nitrite (NO2) as N mg/1 Coliform: MF Fecal /100ml Nitrate (NO3) as N mg/I Coliform: MF Total /100ml Phosphorus: Total as P mg/1 n Note: Use MPN method for highly turbid samples) Dissolved Solids: Total / f �f mg/I pH (when analyzed) units TOC Z 5. as mg/I Chloride 7-3 mg/I Arsenic mg/I Grease and Oils mg/I Phenol mg/I Sulfate mg/I Specific Conductance } 9 uMhos Total Ammonia mg/1 TKN as N mg/I u Rr1uIJI Iuby! IaLe AI - Aluminum •a• mg/I Ba - Barium mg/I Ca - Calcium mg/1 Cd - Cadmium mg/I Chromium: Total mg/I Cu - Copper mg/I Fe - Iron mg/I Hg - Mercury mg/I K - Potassium mg/I Mg - Magnesium mg/I Mn - Manganese mg/I _YES _ NO) Ni - Nickel mg/I Pb - Lead mg/I Zn - Zinc mg/I Arnmonia Nitrogen mg/I Other (Specify Compounds and Concentration Units) ORGANICS: (GC,GC/MS,HPLC) (Specify test and method If. Attach lab report.) Report Attached? Yes_(1) No_.(0) VOC : method it = method # _ method # _ Rev. 03/2000 SUBMIT FORM ON YEl LM PAPER ONLY FACILITY INFORMATION N� /Please Print Clearly or Type Facility Name: VA7'10 I- Permit Name (If different): Facry, ss: rltr1 323 county �RNETT rr) (state) (Zb) Contact Person: N a e a D/cr.n.a Telephone #: !�/a - $22 - 262r Well Location/ Site Name: /rrw - 2- No. of Wells to be Sampled: m. . tam acme Well ldentificationNumber (from Permit): Iniv-'Z For Groundwater Treatment Systems Well Depth: /6 ft. Well Diameter: _ In. Check One: Screened Interval: tL to It. ❑ Influent (98) Depth to Water Level: (aft. below measuring point. ❑ Effluent (99) Measuring Point Is ft. above land surface. Gallons of water pumpediballed before sampling: Field analysis: pH 6 • i , Specific Conductance uMhos Temp. 23 OC, Odor Appearance t042se PERMIT #: EXPIRATION DATE: Non -Discharge UIC - - NPDES AIC 06607Y7 TYPE OF PERMITTED OPERATION BEING MONITORED Lagoon Remedlallon: Infiltration Gallery---, Spray Field Remedlallon: 123 in Rotary Distributor _Land Appllcallon of Slutlge NOTE: Values should reflect dissolved and _ o colloidal concentrations. R Date sample collected: ?I—ZS100 Date samplehi@hal)I�F,ed:4�kz - Laboratory Name: cn Certllicatlon No. /aA- PARAMETE$$ (Samples for metals were collected unflltered YES _NO and field acidified COD i37 mg/I Nitrite (NO2) as N mg/I Coliform: MF Fecal /100ml Nitrate (NO3) as N mgA Coliform: MF Total /100ml Phosphorus: Total as P mg/I .(Nola: Use MPN method for highly turbid samples) Orthophosphate. mg/l mg/I Dissolved Solids: Total 2 /o S mg/I At - Aluminum pH (when analyzed) -unit Be - Barium mg/I yb. 6z mg/I Ca - Calcium mg/I CTOG hloride mg/I Cd - Cadmium mg/I Arsenic mg/I Chromium: Total mg/I Grease and Oils mg/I Cu - Copper mg/I Phenol mg/I Fe - Iron mg/I Sulfate mg/I Hg - Mercury mg/I Specific Conductance 2 87- uMhos K - Potassium mgA Total Ammonia mgA Mg - Magnesium mgA TKN as N mgA Mn - Manganese mg/I NI - Nickel— NTEP 13 70Qa _ mg/I Pb - Lea mg/I Zn - Zinc /�Y�Til-1al 0 CT mg/I Ammonia Nitrogeril ®FF9 mgA Other (Specify Compounds and Concentration Units) ORGANICS: (GC,GC/MS,HPLC) (Specify test and method#. Attach lab report.) Report Attached? Yes _(1) No _(0) V-OC method # _ method # method # SUBMIT FORM ON YELLOW PAPER ONL Vd,tt-0� orsT S ,N FACILITY INFORMATION Please Print Clearly or ryp PERMIT #: EXPIRATION DATE: Facility Name: i o,vAs / Non -Discharge UIC Permit Name (If different): NPDES NC oc A n 7 Y 7 Facility Address: Sn e4 ,v. Rsmc Ave. TYPE OF PERMITTED OPERATION BEING MONITORED °� 'n ,,,,,, u�mal Z S3-� 3 County % 2 - 80 8 I Lagoon Remedlalicn: Infiltration Gallery o =' Contact Person: ei ' e 7rc �"''^' Tele ne #: p Z Spray Field Remedlallon: a Well Location/Site Name: �w - < <ol Wells to be Sampled: p ,um e,m I Rotary Distributor land Application of q@Vge � s other. rZ srrc.v Scrrcrn+e, Pbe ib7+i.uy- umber from Permit): A"" - t Well Identification N( ) For Groundwater Treatment Systems �� Well Depth: 20 ft. Well Diameter: Z ft. to tt. In.' Check One: ❑ NOTE: Values should reflect dissolved and `' Screened Interval: - Influent (98) Depth to Water Level:'/7 ft. below measuring point. ❑Effluent (99) m colloidal concentrations. rio Measuring Point Is 3 ft. above land surface. r" 7 Date sample collected: iE100 Date samp�e°an led: 8 z o Gallons of water pumped/balled before sampling: 2. LaboratoryName: £yyi aay.,,e •r / Field analysis: pH 4.0 , Specific Conductance uMhos Ccca 2 o Certification No. /D Temp. 2- 00, Odor 1 Appearance PARAMETE$$ (Samples tar metals were collected unfiltered YES _NO and field acidified COD /S mg/l Nitrite (NO2) as N mg/1 Coliform: MF Fecal /100ml Nitrate (NO3) as N mg/1 mg/l Coliform: MF Total /100ml Phosphorus: Total as P . mg/l (Note: Use MPH method for highly turbid eampiee) Dissolved Solids: Total 68 mg/I Orthophosphate Al - Aluminum - g/l pH (when analyzed) units Be - Barium m mg/l TOC /• a z Chloride 8 ring/I mg/l Ca - Calcium Cd - Cadmium mg/l Arsenic mg/I Chromium: Total mg/1 Grease and Oils mg/I Cu - Copper mg/l Phenol mg/l Fe - Iron mg/l Sulfate mg/I Hg - Mercury mg/I Specific Conductance 7119 uMhos K - Potassium Total Ammonia mgA Mg - Magnesium mgn mg/I TKN as N mg/I Mn - Manganese GW-59 Rev. 4/98 ,YES _ NO) Ni - Nickel. mg/I Pb - Leaf] mg/l Zn - Zinc mgn Ammonia Nitrogen mgn Other (Specify Compounds and Concentration Units) ORGANICS: (GC,GC/MS,HPLC) (Specify test and method #. Attach lab report.) Report Attached? Yes _ (1) No_(0) VOC method # method # e method,# - SUBMIT FORM ON YELLOW PAPER ONLY Facility Name:_ Permit Name (If County 0 N rr Contact Person: Noue t7rc,c..t:°_; Telephone M21 -82Z-8dat Well Location/ Site Name: No. of Wells to be Sampled: Well Identification Number (fromPermit):_Mw-2 : For GroundwalerTreatment Systems Well Depth: ' Z ft ft. Well Diameter.- z In. Check Ono: Screened Interval: - ft. to ft. ❑ Influent (98) Depth to Water Level: ft. below measuring point. El Effluent (99) Measuring Point Is 3 ft. above land surface. Gallons of water pumped/balled before sampling: 3.3 Fleld analysls: pH , Specific Conductance uMhos Temp. _5_°C,Odor Appearance Murry PERMIT #: EXPIRATION DATE: TYPE OF PERMITTE12 OPERATION BEING MONITORED Lagoon Rerhedlalion: Infiltration Gallery Spray Field Remedlation: Rota r Distributor LandAIlicsawluoe iu✓ OtheAD_UAer.,r To ecD NOTE: Values shouldt reflect dissolved and colloidal concentrations. Date sample collected: 3 0 &p Date sample analyzed: `d r o0 LaboratoryName: 6w e i r:aN m," r I r Certification No. ie o 0 PARAMETEgg (Samples for metals were collected.unflitered YES _NO and field acidified COD 3S 3 mg/I Nitrite (NO2) as N mgA Coliform: MF Fecal /100mi Nitrate (NO3) as N mgA Coliform: MF Total k /100ml Phosohorus: Total as R maA (Note: Use MPN method for highly turbid samples) Dissolved Solids: Total pH (when analyzed) TOC 244 17ig/j units, S/ mgA, Chloride / 3 mg/i Arsenic mg/I Grease and Oils mg/( Phenol Ingo Sulfate mg/I; Specific Conductance 3 S Z uMhos Total Ammonia mgA TKN as N "" mgA Orthophosphate mgA At - Aluminum _ mg/l Be - Barium mg/l Ca - Calcium mgA Cd - Cadmium mg/I " Chromium: Total mgA Cu - Copper mgA Fe - Iron mg/l Hg - Mercury mgA K - Potasslum mgA Mg - Magnesium mgA Mn - Manganese mgA _YES _ NO) NI - Nickel Pb - Lead Zn -Zinc Ammonia Nitrogen Other (Specify Compounds and ORGANICS: (GC,GC/MS,HPLC) (Specify test and method #: Attach lob report.) Report Attached? Yes ----(I) No _ (0) VOID : method # o . : method # : method # SUBMIT FORM ON YELLOW PAPER ONLY Please Facility Name:_ Permit Name (if or .+.., c. z Count r-r Contact Person: NOA13 Drex.nA}jSiva) Telephone#: 91- a' 9z - aa84 Well Location/ Site Name:- M w - I No. of Wells to be Sampled: 7- Well Identification Number prom Permit): M w - I For GroundwalerTreabnenl systems Well Depth: • 20 8. Well Diameter:Z In. Check One: Screened Interval: ft. to it. ❑Influent (98) Depth to Water Level: / 6 ft. below measuring point. ❑ Effluent (99) Measuring Point Is 3 8. above land surface. Gallons of water pumped/bailed before sampling: 2. 6 Field analysis: pH 6• / , Specific Conductance uMhos Temp., _/_5 *C, Odor Appearance CLc,an PERMIT #: EXPIRATION.DATE: Non -Discharge UIC NPDES A r-'00A owes TYPE OF PERMITTE12 OPERATION BEING MONITORED Lagoon Remedlation: Infiltration Gallery Spray Field Remediation: Rotary Distributor Lend Appllcallon of Sludge Other:.. Berta{EN SfTTL/wb �O4SN/N4 �ONOS NOTE: Values should reflect dissolved and colloidal concentrations. o Date sample collected: _ AZIQIao Dale sample aQZed_ `/ LaboratoryName:-.vu,ao.vmawr I Certification No. YO PARAMETF,RS (Samples tar metals were collected unfiltered YES _NO and field acidified COD mg/I Nitrite (NO2) as N mgA Coliform: MF Fecal /loom[ Nitrate (NO3) as N mg/l Coliform: MF Total /100ml Phosohorus: Total as P mn/I (Note: Use MPN method for highly turbid samples) Dissolved Solids: Total pH (when analyzed) TOC 6 9 mgA units Z. a z mg/1 Chloride 9 mg/1 Arsenic mg/I Grease and Oils mg/I Phenol mg/I Sulfate mgA Specific Conductance tip.y uMhos Total Ammonia mg/I TKN as N mgA Orthophosphate mg/l At - Aluminum mgA Be - Barium mg/l Ca - Calcium mg/I Cd -Cadmium mg/I Chromium: Total mg/I Cu - Copper mg/1 Fe - Iron mg/1 Hg - Mercury mg/I K - Potassium mgA Mg'- Magnesium mgA Mn - Manganese mgA __YES _ NO) NI - Nickel Pb - Lead Zn - Zinc Ammonia Nitrogen Other (Specify Compounds and .P- m 0 mg/I mgA i Units)• ORGANICS: (GC,GC/MS,HP.LC) (Specify test and method #. Attach lab report.) Report Attached? Yes_(1) No_(0) VOC : method#. : method # - : method # e ,V, rypl1AV„(tl tlmrnama n :ma-measepnnror GW-59 Rev. 4/98 r l � SUBMIT FORM ON YELLOW PAPER ONLY I 3,011999 FACILITY INFORMATION Please Print Clearly or Type Facility Name:..9T<o �u .�-�iiQfq�ai�a CR%2ao a Permit Name (If different): Fa IityAddresa: SoH /VoRrrr AsM4t Ava n2" B0 N - 28323 County RN6TT (Cowl - 1 mtol. Contact Person: Aln R 13 DISm ^+ w,v Telephone #: (gi) 372- 80 E 1 Well Location/ Site Name: No. of Wells to be Sampled: o 7- Well Identification Number (from Permit): /Aw ! ' For Groundwater treatment Systems Well Depth: Z o N. Well Diameter. _7- In. Check One: Screened Interval: ft. to. ft. ❑ Influent (98) Depth to Water Level: / H ft. below measuring point. ❑ Effluent (99) Measuring Point Is 3 ft. above land surface. Gallons of water pumped/balled before sampling: Z Field analysis: pH 6• ! , Specific Conduclance uMhos Temp. /7 °C,Odor Appearance C&epR PARAMETE$$ (Samples for metals were collected i COD 20 mg/I. Coliform: MF Fecal /t00nil Coliform: MF Total /t 00ml (Note: ltse MPH method for hlghly.turbid samples) Dissolved Solids: Total 76 mgA pH (when analyzed) - - units TOG . Z. o7 mg/I Chloride 6• s mg/l Arsenic mg/I Grease and Oils mgll Phenol mgA Sulfate mgA' Specific Conductance 7Z. 7 uMho's. Total Ammonia mgtl TKN as N mg/l GW-59 Rev. 4199 PERMIT M } EXPIRATION DATE: Non -Discharge I UIC NPDES NC GOio7y7 TYPE OF PERMITTED OPERATION BEING MONITORED Lagoon I Ir MRemedlallon: Infiltration Gallery Spray Field I Remedlation: Rotary Distributor Land AppllcellQ�n of Sludge ✓OtheaB r: rcVea.v se -Tr �Jb . }17L,syA _, NOTE: Values should reflect dissolved and colloidal concentrations. Data sample collected: !! Z9 99 Date sample analyzed: !2 6 LaboyatoryName: £&v.yrA e,u in E PJ7* ! a Certification No. /O fared YES _NO and field acidified Nitrite (NO2) as N mg/I Nitrate (NO3) as N mg/I Phosphorus: Total as P mgA Orthophosphate mg/I At - Aluminum mg/I Be -.Barium mg/I Ca - Calcium mg/I Cd - Cadmium __ f n mg/I __ Chromium: Total mg/I Cu - Copper mg/I Fe - Iron - mg/I Hg - Mercury K - Potassiumrmyt ITEV)L mgA - mgA Mg - Magneslum FFICr rngll Mn - Manganese mgA YES _ NO) Zn - Zinc �x�A Ammonia Nitrogen Other (Specify Compounds and Conce lsf alioryutlnits) ORGANICS: (GC,GC/MS,HPLC) (Specify test and method #. Attach lob report.) Report Attached? Yes —(I) No _ (0) UOC : method # - : method # - : method # - e, . 1*1 SUBMIT FORM ON YELLOW PAPER ONLY Facility Name: /liR7ioivgc ///Gc UAViGAt G.4R3o../ Permit Name (If different): _ Well Location/ Site County R ^' Telephone N: No. of Wells to be Well Identification Number from Permit): 07w 7- For GraundwaterTreabnent Systems Well Depth: ft.- Well Diameter.?- in. Check one: Screened Interval: fL to ft. ❑ Influent (98) Depth to Water Level: Z ft. below measuring point. ❑ Effluent (99) Measuring Point Is 3 ft. above land surface. 1z Gallons of water pumpedfballed before sampling: Field analysis: pH 6. z- , Specific Conductance uMhos Temp. / 7 "C, Odor Appearance CCO44>�e PERMIT M. NPDES /vC 0e6407107 TYPE OF PERMITTED OPERATION BEING MONITORED Lagoon Remedlallon: Infiltration Gallery Spray Field i Remedlatlon: Rotary Distributor Lend Ayppllcalia t of Siud e Olhei: dh kaAr j-r rO re6ISH/N6 �OND NOTE: Values s colloidal Date sample colle Laboratory Name: Certification No. _ PARAMETF.RS (Samples for metals were,collecled unfiltered YES _NO and field acidified COD 13ti mg/I Nitrite (NO2) as N mgA Colilorm: MF Fecal /t00m1. Nitrate (NOO as N mg/I Coliform: MF Total /100ml Ph osphorus:'Total as P mgA (Note: Use MPN method for hlghlgturbld samples) Dissolved Solids: Total 3oz mgA Orthophosphate At - Aluminum mg/I mg/I pH (wfien analyzed) units Be - Barium mg/I TOC 34- y6 mg/l Ca - Calcium mg/l Chloride zS mg/I Cd - Cadmium mg/I Arsenic mg/I Chromium: Total mg/I Grease and Oils mgA Cu - Copper mg/I Phenol mgll Fe - Iron mg/l Sulfate mg'A Hg - Mercury mg/I Specific Conductance 5Iz I? uMhos K - Potassium mgA Total Ammonia 1`110 Mg - Magnesium mgA TKN as N mgA Mn - Manganese mgA reflect dissolved and - ca L9 99 Date sample _YES _ NO) o m= NI - Nickel C"mg/I Pb - Lead `a• 3mgn Ymg/I Zn - Zinc Ammonia Nitrogen mg/I Other (Specify Compounds and Concentration Units) ORGANICS: (GC,GC/MS,HPLC) (Specify test and method L Attach lab report.) Report Attached? Yes —(I) No _ (0) VOC : method 9 - : method 0 - i : method # GW-59 Rev. 4198 SUBMIT FORM ON YELLOW PAPER ONLY Clearly or Type FacililyName: /V,4Tin,uAc. /YlecrrrrA,ICAL Permit Name (if different): F clillyAddress: 50Y /VDR7H AsNe .9vc. 4NN veal rtC AB33y C6gjZNTT E I m (slate) Wi .ounty Contact Person: /Voxe 14=xm,4" Telephone #:(9ia)$gz-aogl Well Location/ Site Name: m w - Z- No. of Wells to be Sampled: o ? m Well Identification Number (from Permit): _ m w - z For Groundwater Treatment Systems Well Depth: / 8 ft. Well Diameter: Z In. Check One: Screened Interval: ft. to ft. ❑ Influent (90) Depth to Water Level: / r it. below measuring point. ❑ Effluent (99) PERMIT #: EXPIRATION DATE: r Non -Discharge— UIC 1 NPDES NC 006 o7y7 aEE OF PERMITTED OPERATION BEING MONITORED Lagoon Relhedlatlon: Infiltration Gallery Spray Field Remediatlon: Rotary Distributor Land Application of Sludge ✓ Other: ApSAceN7 T �3w s&1N4 P�Np NOTE: Values should reflect dissolved and colloidal concentrations. Measuring Point Is 3 ft. above land surface. Gallons of water pumped/balled before sampling: 7- Dale sample collected: 7 z8 99 Date sample analyzed: V-5/99 Field analysis: pH 6. O , Specific Conductance uMhos Laboratory Name: _EAWi Roeymr .er / Temp. /7 00, Odor Appearance Ccouoy Certification No. /O PARAMETE$$ (Samples for metals were collected unfiltered YES _NO and field acidified COD 351 mg/I Nitrite (NO2) as N mg/I Coliform: MF Fecal /100ml Nitrate (NO3) as N mg/I Conform: MF Total /100ml Phosphorus: Total as P mg/I (Note: Use MPN method for highly turbid samples) Dissolved Solids: Total / Z 6 mg/I pH (when analyzed) units TOC Z 9. 84 mg/I Chloride 9 mg/I Arsenic _ mg/I Grease and Oils mg/I Phenol mg/I Sulfate mg/I Specific Conductance Zoo uMhos Total Ammonia mg/I TKN as N mg/l I urtnopnospnate mg/I AI - Aluminum mg/I Ba - Barium mg/I Ca - Calcium --. — 91, Cd- Cadmium pG"'� �G� N t',i'g/I mm Chromium: Total mg/I Cu - Copper Vpg 1.000 mg/I Fe - Iron mg/I Hg - Mercury ter. ,> --;LL �$ mg/I K - Potassium �- r mg/l Mg - Magnesium mg/I Mn - Manganese mg/I -_YES _ NO) ,) NI - Nickel � mg/I Pb - Lead = mg/I Zn - Zinc rn `' mg/I Ammonia Nitrogen ��''- mg/I Other (Specify Compounds and CWenl{allon Units) N ni°l ORGANICS: (GC,GC/MS,HPLC) (Specify lest and method #. Attach lab report.) ReportAltached7 Yes (1) No_(0) VOC : method #= : method # : method # _ SUBMIT FORM ON YELLOW PAPER ONLY Please Print Clearlv or FacilityName:- /V,4-r/oAr!}L. /YIe .rtANrcAL(2erganrsl Permit Name (if different): Fa�IIIlyAddress:- 562 /Vo27u. 4sµe Ave. .11nn+n, /llC ZR33`/ County- fir�i enlerT rcM rsmiol (ZIP) . Contact Person: N-A n 'Dre Kn, p J Telephone N: (9/0 ) 89 z- 8 a a I Well Location/ Site Name: 1"W ') No. of Wells to be Samoled: 7- Well identification Number (from Permit): rh W — I For Groundwater Treatment Systems Well Depth: Zo It. Well Diameter: 7_ In. Check One: Screened Interval: ft. to ft. ❑ Influent (98) Depth to Water Level: / Z It. below measuring point. Measuring Point Is 3 ft. above land surface. ❑ Effluent (99) Gallons of water pumped/balled before sampling: Z Field analysis: pH 6.6 , Specific Conductance uMhos Temp. /7 °C, Odor Appearance CL r-gri PERMIT N: EXPIRATION DATE: Non -Discharge UIC NPDES NC 606074/7 TYPE OF PERMITTED OPERATION BEING MONITORED Lagoon Rerliediallon: Infiltration Gallery Spray Field Remedlalion: Rolary Distributor Land Applicalfon of Sludge JZ Other: /3CTwerC S£.TTL//V C- ; �OC.J.Sy _ per /', NOTE: Values should reflect dissolved and colloidal concentrations. Dale sample collected: z. d: 8 99 .S Dnte sample nnalyzed: 8 T G Laboratory Name: N V 1P a"m6 NT / Certification No. /o ,.o PARAMETE$$ (Samples for metals were collected unfiltered YES _NO and field acidified COD Z 3 mg/I Nitrite (NO2) as N mg/I Collform: MF Fecal /100ml Nitrate (NO3) as N Ing/I Coliform: MF Total /100ml Phosphorus: Total as P mg/I (Note: Use MPH method for highly turbid samples) Orthophosphate mg/I Dissolved Solids: Total 40 mgll AI - Aluminum �' l n I pH (when analyzed) units Ba - Barium ` I 2 3 4 mg/1 Ca - Calcium mg/I Chloride 7 mg11 Cd - Cadmium 'S€r? 8 mg/I Arsenic mg/I Chromium: Total mg/I Grease and Oils mg/I Cu - Copper Lpmg/I Phenol mg/I Fe - Iron P Ing/I Sulfate mg/I Hg - Mercury. ` mg/I Specific Conductance y uMhos K - Potassium mg/I Total Ammonia mg/I Mg - Magnesium mg/I TKN as N ' mg/I Mn - Manganese mg/I I ._YES _NO) rU ,-< NI - Nickel mg/I Pb - Lean Zn - Zinc I'' mg/I Ammonia Nitrogen ra -' mg/I Other (Specify Compounds and CYncen Units) n ; ORGANICS: (GC,GC/MS,HPLC) (Specify test and method N. Attach lab report.) ReportAttached? Yes (1) No_(0) VOC : method N = method N = method N = SUBMIT FORM ON YELLOW PAPER ONLY Please Print Facility Name:_ Permit Name (if A) C 2 K33 `1 County %/ARNerT l rYl t mto) (zip) Contact Person: illoae IJtCKMAN Telephone #: is 2- Well Location/ Site Name: w - 2 No. of Wells to be Sampled: Well Identification Number (from Permit): 61 w • Z For GroundwalerTrealmenlSystems Well Depth: ft. Well Dlameter: In. Check One: Screened Interval: ft. to ElInfluent (98) Depth to Water Level:_ 7 ft. below measurift. ng point. ❑ Effluent (99) Measuring Point is 3 ft. above land surface. Gallons of water pumped/balled before sampling: y Field analysis: pH 6. 3 , Specific Conductance uMhos Temp. ZI OC, Odor Appearance C'oaov �TuY:ero PERMIT it: EXPIRATION DATE: Non -Discharge UIC NPDES NC 00(6071/7 TYPE OF PERMITTED OPERATION BEING MONITORED Lagoon Remedlallon:Infiltration Gallery CD Spray Field Remedlatlon: w Rotary Distributor Land Application of Sludge co )v Other: 41):r-q ,r 7 POLISN1N4 reN rj I=;) NOTE: Values should reflect dissolved and ..� colloidal concentrations. Date sample collected: 1140198 Date sample analyzed:4 W/-9A Laboratory Name: fuvraor+me r:T— Certification No. 10 PARAMETERS (Samples for metals were collected unflltered YES _NO and field acidified _YES _ NO) = ? COD "7:84 mg/I Nitrite (NO2) as N mg/I NI - Nickel mg/1 Coliform: MF Fecal /100ml Nitrate (NO3) as N mg/I �. Pb - Learf V —., - mg/1 Coliform: MF Total. /100ml Phosphorus: Total as P mg/I Zn - Zinc "' r►tg/I (Note: Use MPN method for highly turbid samples) Orthophosphate mg/I Ammonia Nitrogen rt;,-�"' mg/I Dissolved Solids: Total i a 7 mg/I At - Aluminum mg/I Other(Specify Compounds and I;z cenlfa8on Units) pH .(when analyzed) units Ba - Barium mg/I TOC //. O / mg/I Ca - Calcium - mg/I Chloride ' 15 mg/I Cd - Cadmium mg/I Arsenic _ mg/I Chromium: Total mg/I Grease and Oils mg/I Cu - Copper mg/I Phenol mg/I Fe - Iron mg/I ORGANICS: (GC,GC/MS,HPLC) Sulfate mg/I Hg - Mercury mg/I (Specify test and method #. Attach lab report.) Specific Conductance 35y uMhos K - Potassium mg/I Report Attached? Yes (1) No _(0) Total Ammonia mg/I Mg - Magnesium mg/I VOC I : method #_ TKN as N mg/I Mn - Manganese mg/I : method # e : method # e or 10( GW-59 Rev. 4198 SUBMIT FORM ON YELLOW PAPER ONLY Print Clearly or Type Facility Name: NA7/ONAL. IMEC.NAN.CAL CARRON Permit Name (if different): Facility Address: SOH NeaTN /-isN,- Ave. `°°` County i• NC ZS33`i NA2e) TT t'c NoR6 DISKmA,i51°°I jzrol Telephone#:-(9ro)99z-8o81 Contact Person: Well Location/ Site Name: M W - I No. of Wells to be Sampled: o 2- m l Well Identification Number (from Permit): 'hw - I For Groundwater Treatment Systems Well Depth: ' 20 ft. Well Diameter:? in. Check One: Screened Interval: ft. to ft. ❑ Influent (98) Depth to Water Level: / Z ft. below measuring point. ❑ Effluent (99) Measuring Point Is 3 ft. above land surface. Gallons of water pumpedlbailed.before sampling: 2. Field. analysis: pH 6. / , Specific Conductance uMhos Temp. 20 °C, Odor Appearance LCAR PERMIT #: .EXPIRATION'DATE: TYPE OF PERMITTED OPERATION BEING MONITORED Lagoon Remedlallon: Infiltration GalleryCo co Spray Field Remedlation: Rotary Distributor Land Application of Sludge co Other., BLT el . SETTLWy C Paw5 /j& _PGYD f NOTE: Values should reflect dissolved and O� colloidal concentrations. Date sample collected: Date sample analyzed: Arz Laboratory Name: nI Certification No. 10 I Wu` PARAMETER (Samples for metals were collected. unfiltered YES _NO and field acidified COD 9=3`k mg/l Nitrite (NO2) as N mg/I Coliform: MF Fecal /100ml Nitrate (NO3) as N mg/I Coliform: MF Total /100ml Phosphorus: Total as P mg/I (Note: Use MPN method for highly turbid samples) Dissolved Solids: Total Y Z mg/I pH (when analyzed) units TOG < Z mg/I Chloride z z mgll Arsenic _ mgll Grease and Oils mgll Phenol mgll Sulfate mg/I Specific Conductance 76•,V uMhos Total Ammonia mg/I TKN as N mg/I unnopnospnate AI -Aluminum wyn mg/I Ba - Barium mg/I _ Ca - Calcium mg/I Cd - Cadmium mg/I Chromium: Total mg/I Cu - Copper mg/I Fe - Iron mg/I Hg - Mercury - mg/I K - Potassium mg/I Mg - Magnesium mg/I Mn - Manganese mg/1 S _YES _ NO) c NI - Nickel mg/I Pb - Lead mg/I Zn -Zino - mg/I Ammonia Nitrogen 1-o " mg/I Other (Specify Compounds and CCanceFit'ration Units) o ORGANICS: (GC,GC/MS,HPLC) (Specify test and method If. Attach lab report.) Report Attached? -Yes (1) No_(0) VOCmethod # _ method # method # _ -ii GW-59 Rev.4/98 Elm, 2 % UncupOPOW GREENVILLE, N.C. 27835-7085 - FAX (252) 756-0633 Drinking Water ID: 37715 Wastewater I➢: 10 NATIONAL MECHANICAL CARBON (WELLS) MR. DEAN 13YRD C/O TOWN OF .ERWIN P.O. BOX.459 ERWIN ,NC 28339 PARAMETERS COD, mill Total Organic Carbon, mg/l Chloride, mg/1 Total Dissolved Residue, mg/l Conductivity (at 25c), uMhos, ID#: 434 DATE COLLECTED: 11/10/98 DATE REPORTED : 11/17/98 REVIEWED BY: Monitoring Monitoring Analysis Method' Well #1 Well N2 1 Date Analyst Code 13 78 11/12/98 TRB HACH8000 <2.00 11.01 11/13/98 ACA EPA415.1 22 15 11/11/98 SWL SM4500-CLB 42 187 11/11/98 'JMH EPA160.1 76.4 354 11/10/98, JMH SM2510B s LaboratorvAnalvses — Environmental Consultants e suBm, I FORM ON YELLOW PAPER ONLY Facility Name: 'VPF 10MgL ccn.....,:� _-_-- --- Permit Name (if different): FaFilltyAddress: °y vot ORTH sHc' vc c 21?33ri County 1YAq vc-rT 1$mroi (zlvl Contact Person: /Voa a �(CK a Telephone #: tyio i z- b'o81 Well Location/ Site Name: /t� W 2 No. of Wells to be Sampled: rum ermi Well Identification Number (from Permit): m W - � For Groundwater ireaiment oys(ee Well Depth: ' / 8 it. Well Diameter: Z In. Check One: Screened Interval: ft. to • ft. ❑ Influent (98) Depth to Water Level: `/ ft. below measuring point. ❑ Effluent (99) Measuring Point Is 3 ft. above land `surface. Gallons of water pumped/bailed before sampling: 3 Field analysis: pH 6.1- , Specific Conductance uMhos r.., / 5 'C. Odor Appearance CIOVOY I e collected unfiltered YES _NO PARAMEjg.H (Samples for meta s war r //7 mgll Nitrite (NO2) as N COD Coliform: MF Fecal /100ml Nitrate (NO3) as N— Col(form: MF Total /100ml Phosphorus: Total as F (Note: Use MPN methodfor highly turbid samples) Solids: Total / 81 mg/I Orthophosphate Al - Aluminum Dissolved pH (when analyzed) units 3 9 , 88, g/I Ba - Barium Ca -Calcium - TOC Chloride Cd - Cadmium Arsenic _ mg/I Chromium: Total Grease and Oils mg/I mg/I Cu -Copper i Fe - Iron Phenol Sulfate mg/I Hg - Mercury. Specific Conductance 3o s Whos K - Potassium �� r ` Total Ammonia mg/l mg/I Mg - Magnesfuli Mn -Manganese TKN as N pti1 N (_j S Values should reflect dissolved colloidal concentrations. Date sample colle Laboratory Name: ana new ac(uu(eu mg/1 mgll mg/I mg/I mg/I mg/I mg/I n,mg/l 77r\ ' _ -„ Ni - Nickel mg/I Pb - Lead 14� It rlgll Zn - Zinc r. Ammonia Nitrogen !.Tng/I Other (Specify Compounds and ConcB_n7'iatlorrUnits ORGANICS: (GC,GC/MS,HPLC)•"( (Specify test and method #. Attach lab report.) ReportAttached? Yes (1) No __ (0) VOID method#= method # method # _ 17 GW-59 Rev. 4/98 ' SUBMIT FORM ON PAPER ONLY Print Clearly or Facility Name:' 7r0^'?l IYIPCMANrCR6 CnRAcN Permit Name (if different): - Facility Address: So A/o'kFN Asrre five 1)j A Nc 2833V County AaNcr^r Gontat"rlcLPerson: ' /Noes ArcAemnst � Telephonefe•C9ro 89z-8o8i Well Location/ Site Name: A9yV l No. of Wells to be Sampled, ,°m e,mn - Well Identification Number (from Permit): - .M W ` t For Groundwaler Treatment Systeros- WelfDepth: ' zo ft. Well Diameter:? In. Check One: Screened Interval: ft. to fl. Ej Influent (98) Depth to Water Level:—ft. below measuring point., Effluent (99) Measuring Point is 3 ft. above land surface. Gallons of water pumped/balled before sampling: Z' Field:analysis: pH Specific Conductance uMhos Temp. 5 CC, Odor Appearance -CLLAA PERMIT M EXPIRATION DA NPDES AIC 00607N7 0 ` TYPE OF PERMITTED OPERATION BEING MONITORED ` t Lagoon Rernedlalion:lnlil 03 Spray Field Remedlatton: Rotary Distributor _ Land Application of Sludge z j _Other: B£?w Lw/ SrTe n+G'-i POL�JHIN - NOTE: Values should reflect dlssolved'and . FAYE TTEVILLE colloidal concentrations. REG. OFFICE, Date sample collected: 31ZA9 Date sample analyzed:- LaboratoryName:'elyVrRow c.vT 7 Certificatlon,No. io PARAME105_.(Samples for metals were collected unfiltered' YES _NO and field acidified COD /y. mg/I Nitrite (NO2) as N mg/l Colifoim: MF Fecal /100ml Nitrate (NO3)`as.N mg/l Coliform: MF Total /100ml Phosphorus: Total as P mgll (Note: Use MPH method for highly turbid samples) 'Orthophosphate 'mg/I, mg/I. Dissolver Solids; Total Y Z mg/1 At = Aluminum - - '' mg/l ' -pH (when analyied) units . Be - Barium' mg/I TOC i". 3 / mg/I Ca - Calcium mg/I Chloride 7 Arsenic mg/I _ mg/I Cd —Cadmium Chromium: Total mg/I Grease and Oils - mg/I Cu - Copper mg/I Phenol mg/I Fe - Iron mg/F Sulfate mg/l. Hg -. Mercury. _ mg/I Specific Conductance 7 6,i 6 uMhos K -Potassium mg/l mg/I' Total Ammonia mg/I Mg - Magnesium ; Manganese mg/I TKN as N mg/I Mn - _YES _ NO) N1- Nickel Pb - Lead Zn - Zinc Ammonia Nitrogen - Other (Specify Compounds and Concentrator NCO] ORGANICS: (GC,GC/MS,HPLC) (Specify test add method #. Attach lab report.) - Report Attached? Yes_(I) No _ (0) VOC - method # _ method # :- method # = �RO DIVISION OF WATER QUALITY • GROUNDWATER SECTION GROUNDWATER QUALITY MONITORING: P.O. BOX 2 For forms 26- RALEIGH, NNC 27626.0678 > COMPLIANCE REPORT FORM please write or call: (919)733-3221 Type or Use a ball-point pen and press firmly. PERMIT NUMBER: (REQUIRED) Facility Name IVA-71012&L M C /4 A B ' Non -Discharge NPDES/C 00607L17 Address TYPE OF DISPOSAL OPERATION BEING MONITORED dAnJiC I' County (REQUIRED) Well Location 7b fnL I flfW& Roan Lagoon Septic Tank/DrainField Well Identification Number W 12 Well Depth / S Ft. Well DiameterZ"Sample (Screened) Interval k Ft. To _�Ft. spray Field Subsurface Low -Pressure Piping (LPP) Depth to Water Level _57 ft. below measuring point (before sampling) - Land Application of Sludge Measuring point is 3 ft. above land surface Rotary Distributor Other Gallons of water pumped/bailed before sampling Field Analysis: pH 5• b Specific Conductance uMhos Temp. / 5 oC Odor 7 q / 98 Lab Sample Analyzed 7 /O - `7 /1 S/9 § Appearance Date Sample Collecf{ed Date Laboratory Name LAly 1lipw11N F OJT 1 Certification No. SAMPLES FOR METALS WERE COLLECTED UNFILTERED AND FIELD ACIDIFIED _YES NO COD Z S mg/I Nitrite (NO2) as N 0 mg/I Ni - Nickel mg/I Coliform: MF Fecal /100m1 Nitrate (NO3) as N mg/I Pb - Lead mg/I Coliform: MF Total /100ml Phosphorus: Total as P mg/1 Zn - Zinc C= mg/I (Note: Use MPN method for highly turbid samples) Al - Aluminum mg/1 Pesticides/Herbicides — oEj Dissolved Solids: Total 4 30 mg/I Ba - Barium mg/I (Specify Compounds) pH (when analyzed) units Ca - Calcium mg/Iug/I TOC 7, is mg/I Cd - Cadmium mg/I _= �^ ug/I Chloride ! r mg/I Chromium: Total mg/I ^ ug/I Arsenic mg/1 Cu - Copper mg/I Other (Specify Compounds and-' o Grease and Oils mg/I Fe - Iron mg/I Concentration units) Hardness: Total mg/I Hg - Mercury mg/I Phenol mg/I K - Potassium mg/I Sulfate mg/I Mg - Magnesium _ _- — — mg/I 7 Specific Conductance, /9'7D uMhos Mn - Manganese mg/I d llL� Total Ammonia mg/I Na - Sodium mg/I TKN as N mg/I j Yr i 41 fen, I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE. Note: Values shoves�$oived and Colloidal ConCe t ti iis19(see #3 on back) CAC_ £ �'r See back for instructions. Signature of Permittee r Authorized Agent`) Date *• Submit blue and yellow copies only to address above. GW-59 REV. 8/96 Sa `"%A COLLECTION AND ANALYSIS OF GROUNDWATER SAMPLES I. Samples should be analyzed as soon as p6ssible after collection. SAMPLES WHICH ARE NOT ANALYSED WITHIN THE HOLDING TIME SPECI- FIED FOR THE METHOD USED (SEE #4., BELOW) MUST BE DISCARDED AND NEW SAMPLES COLLECTED. t 2. Metals Analyses: Use Standard Method 3030C for sample preparation (mercury excluded). DO NOT FILTER METALS SAMPLES IN THE FIELD ttt Unfiltered samples must be collected for metals, then field acidified with 5 ml concentrated nitric acid per liter of sample, and should be submitted to the lab within 24 hours. Sample preparation in the laboratory (extraction and filtration) must be completed within 72 hours of collection. 3. ANALYSES ARE TO BE MADE OF THE MOBILE CONSTITUENTS (DISSOLVED AS WELL AS COLLOIDAL) IN THE GROUNDWATER, NOT THOSE THAT ARE A PART OF SEDIMENT ASSOCIATED WITH WELL CONSTRUCTION OR SAMPLING PROCEDURES. CHECK WITH YOUR LABORATORY ON PROPER PROCEDURES FOR SAMPLE COLLECTION AND PRESERVATION. 4. As per Title 15, North Carolina Administrative Code, Subchapter 2L, analytical procedures shall be in accordance with the methods described in one of the following publications, or by other methods approved beforehand by the Director, Division of Environmental Management: (a) Standard Methods for the Examination of Water and Wastewater, 16th Edition, 1885 and 17th Edition, 1989, published jointly by American Public Health Association, American Water Works Association and Water Pollution Control Federation; (b) Methods for Chemical Analysis of Water and Waste, 1979, U.S. Environmental Protection Agency publication number EPA-600/4-79-020, as revised March 1983; (c) Test Methods for Evaluating Solid Wastes: Physical/Chemical Methods, 3rd Edition, 1986, U.S. Environmental Protection Agency publication number SW-846; (d) Test Procedures for the Analysis of Polluants Under the Clean Water Act, Federal Register Vol. 49, No. 209, 40 CFR Part 136, October 26, 1984; 5. Measure and record the depth of water in the well prior to pumping or bailing any water from the well. 6. At least 3 volumes of water in the well should be pumped or bailed prior to collecting a sample for analysis. If the well is pumped/bailed dry before 3 well volumes are removed, samples can be collected as soon as the well recovers to the point where enough water is available to collect your sample. 7. Determination for pH, Specific Conductance, temperature, odor and appearance must be made in the field on unfiltered samples when the sample is collected. 8. Field equipment must be calibrated in accordance with recommendations by the manufacturer. 9. Samples must be filtered through a 0.45 micron filter immediately after collection when a dissolved analysis is required. (See #4. above) 10.The sample container should be labeled at the time of collection with the facility name, well identification number and date and time collected. 11."Authorized agent' is any corporate officer or public official authorized by the company, corporation, or governmental body to sign official documents; DIVISION OF WATER QUALITY- GROUNDWATER SECTION 78 GROUNDWATER QUALITY MONITORING: PNC 2762 & For additional forms RALEIG H,'.NC.76&0578 COMPLIANCE REPORT FORM please wrlteor'call: (919)733.3221 Type or Use a ball-point pen and press firmly. Facili PERMIT NUMBER: (REQUIRED) Non -Discharge NPDEs A/C 6 O (, O 74 7 TYPE OF DISPOSAL OPERATION BEING MONITORED (REQUIRED) Well Location Ke'•ruteu Zurruma f /-o' JSH INa rQJJ Lagoon Well Identification Number \/ i Well Depth Z® Ft. Spray Field Well Diameter 2% Sample (Screened) Interval Z H Ft. To / S Ft. Septic Tank/Drain Field Subsurface Low -Pressure Piping (LPP) Depth to Water Level /0 ft. below measuring point (before sampling) land Application of Sludge Measuring point is -3 ft. above land surface Rotary Distributor X other 3 Gallons of water pumped/bailed before sampling Field Analysis: pH S. 5 Specific Conductance uMhos Temp. ( 6 oC Odor Appearance Date Sample Collected 7/A l R 8 Date Lab Sample Analyzed '7Tro -- 7 //s/9$ Laboratory Name F my 1 n' Onr xA c" 'r l Certification No. %Q SAMPLES FOR METALS WERE COLLECTED UNFILTERED AND FIELD ACIDIFIED _YES NO COD / Z mg/I Coliform: MF Fecal /100ml Coliform: MF Total /100ml (Note: Use MPN method for highly turbid samples) Dissolved Solids: Total 34o mg/I pH (when analyzed) units TOC i.31L mg/I Chloride io mg/I Arsenic mg/I Grease and Oils mg/I Hardness: Total mg/I Phenol mg/I Sulfate mg/I Specific Conductance 7 Z. 3 uMhos Total Ammonia mg/I TKN as N mg/I Nitrite (NO2) as N mg/I Ni - Nickel mg/I Nitrate (NO3) as N mg/I Pb - Lead mg/I Phosphorus: Total as P mg/I Zn - Zinc mg/I Al - Aluminum mg/I Pesticides/Herbicides _o Ba - Barium mg/I (Specify Compounds) CO o Ca - Calcium mg/I m , ug/I Cd - Cadmium mg/I �3 ug/I Chromium: Total mg/1 ' = ug/I Cu - Copper mg/I Other (Specify Compounds ando Fe - Iron mg/I Concentration units) m A� Hg - Mercury mg/I --—' K - Potassium mg/I Mg - Magnesium mg/I Mn - Manganese mg/I " V L", � Na - Sodium mg/I y V I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE. Note: Values shp L rgf#egtq!ssolved and II colloidal concentrations. (see #3 on back) d G-bA1T ��10/9 See back for instructions. 'Signature of Permittee ( Authorized Agent*) Date ** Submit blue and yellow copies only to address above. GW-59 REV. 8/96 COLLECTION AND ANALYSIS OF GROUNDWATER SAMPLES 1. Samples should be analyzed as soon as possible after collection. SAMPLES WHICH ARE NOT ANALYSED WITHIN THE HOLDING TIME SPECI- FIED FOR THE METHOD USED (SEE #4. BELOW) MUST BE DISCARDED AND NEW SAMPLES COLLECTED. 2. Metals Analyses: Use Standard Method 3030C for sample preparation (mercury excluded). DO NOT FILTER METALS SAMPLES IN THE FIELD 'If Unfiltered samples must be collected for metals, then field acidified with 5 ml concentrated nitric acid per liter of sample, and should be submitted to the lab within 24 hours. Sample preparation in the laboratory (extraction and filtration) must be completed within 72 hours of collection. 3. ANALYSES ARE TO BE MADE OF THE MOBILE CONSTITUENTS (DISSOLVED AS WELL AS COLLOIDAL) IN THE GROUNDWATER, NOT THOSE THAT ARE A PART OF SEDIMENT ASSOCIATED WITH WELL CONSTRUCTION OR SAMPLING PROCEDURES, CHECK WITH YOUR LABORATORY ON,PROPER PROCEDURES FOR SAMPLE COLLECTION AND PRESERVATION. 4. As per Title 15, North Carolina Administrative Code, Subchapter 2L, analytical procedures shall be in accordance with the methods described in one of the following publications, or by other methods approved beforehand by the Director, Division of Environmental Management: (a) Standard Methods for the Examination of Water and Wastewater, 16th Edition, 1985 and 17th Edition, 1989, published jointly by American Public Health Association, American Water Works Association and Water Pollution Control Federation; (b) Methods for Chemical Analysis of Water and Waste, 1979, U.S. Environmental Protection Agency publication number EPA-600/4-79-020, as revised March 1983; (c) Test Methods for Evaluating Solid Wastes: Physical/Chemical Methods, 3rd Edition, 1986, U.S. Environmental Protection Agency publication number SW-846; (d) Test Procedures for the Analysis of Polluants Under the Clean Water Act, Federal Register Vol. 49, No. 209, 40 CFR Part 136, October 26, 1984; 5. Measure and record the depth of water in the well prior to pumping or bailing any water from the well. 6. At least 3 volumes of water in the well should be pumped or bailed prior to collecting a sample for analysis. If the well is pumped/bailed dry before 3 well volumes are removed, samples can be collected as soon as the well recovers to the point where enough water is available to collect your sample. 7. Determination for pH, Specific Conductance, temperature, odor and appearance must be made in the field on unfiltered samples when the sample is collected. 8. Field equipment must be calibrated in accordance with recommendations by the manufacturer. 9. Samples must be filtered through a 0.45 micron filter immediately after collection when a dissolved analysis is required. (See #4. above) 10.The sample container should be labeled at the time of collection with the facility name, well identification number and date and time collected. 11."Authorized agent' is any corporate officer or public official authorized by the company, corporation, or governmental body to sign official documents. ♦rr �A � D DIVISION OF WATER QUALITY -GROUNDWATER SECTION GROUNDWATER QUALITY MONITORING: 1`P.O. sox29578 For additional forms RALEIGH, NC 27626- 7628-A578 COMPLIANCE REPORT FORM please write or call: (gig)733.3221 or Facility pen ano press Cou PERMIT NUMBER: (REQUIRED) Non -Discharge NPDES NC 00(0074'7 TYPE OF DISPOSAL OPERATION BEING MONITORED (REQUIRED) Well Location Elf'rw£ev SErre.t.Je f Yoatsr+irva M"D Well Identification Number VW 1 Well Depth 7-0 Ft. Well Diameter z Sample (Screened) Interval_ Ft. To /FFt. Depth to Water Level 41 ft. below measuring point (before sampling) Measuring point is 3 ft. above land surface Gallons of water pumped/bailed before sampling 3 - L Field Analysis: pH 5, 6 Specific Conductance uMhos Temp. / y oC Odor Date Sample Collected 31I R /93 Date Lab Sample Analyzed 3 18 — 3/ZY/98 Lagoon Spray Field Septic Tank/Drain Field Subsurface Low -Pressure Piping (LPP) Land. Application of Sludge N Other Rotary Distributor Rol,, ­ Appearance Laboratory Name £NytRoamew+r 1 Certification No. �b SAMPLES FOR METALS WERE COLLECTED UNFILTERED AND FIELD ACIDIFIED YES NO COD < I O mg/I Nitrite (NO2) as N mg/I Ni - Nickel �� �; mg/I Coliform: MF Fecal /100ml Nitrate (NO3) as N mg/I Pb - Lead ^' Ong/I Coliform: MF Total /100ml Phosphorus: Total as P mg/I Zn - Zinc ` ,mg/I (Note: Use MPN method for highly turbid samples) AI -Aluminum mg/I Pesticides/Herbicides =_ -- Dissolved Solids: Total 5! mg/I Ba - Barium mg/I (Specify Compounds) = v=T pH (when analyzed) units Ca - Calcium mg/I ug/I TOC r 33 mg/I Cd - Cadmium mg/I — ,'? ug/I Chloride 11 mg/I Chromium: Total mg/I ug/I Arsenic mg/I Cu - Copper mg/I Other (Specify Compounds and Grease and Oils mg/I Fe - Iron mg/I Concentration units) Hardness: Total mg/I Hg - Mercury mg/I CIO D Phenol mg/I K - Potassium mg/I Sulfate mg/I Mg - Magnesium mg/I Specific Conductance S/ uMhos Mn - Manganese mg/I Total Ammonia mg/I Na - Sodium mg/I TKN as N mg/I I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE. Note: Values should reflect dissolved and colloidal concentrations. (see #3 on back) �I_/Q.,�,,.� j�GgN r� y z 3 %$ ' See back for instructions. Ignature of Perm tee (or Authorized Agent') bate •• Submit blue and yellow copies only to address above. GW-59 REV. 8/96 COLLECTION AND ANALYSIS OF GROUNDWATER SAMPLES 1. Samples should be analyzed as soon as possible after collection. SAMPLES WHICH ARE NOT ANALYSED WITHIN THE HOLDING TIME SPECI- FIED FOR THE METHOD USED (SEE #4. BELOW) MUST BE DISCARDED AND NEW SAMPLES COLLECTED. 2. Metals Analyses: Use Standard Method 3030G;for sample preparation (mercury excluded). DO NOT FILTER METALS SAMPLES IN THE FIELD M Unfiltered samples must be collected for metaN, then field acidified with 5 ml concentrated nitric acid per liter of sample, and should be submitted to the lab within 24 hours. t Sample preparation in the laboratory (extraction and filtration) must be completed within 72 hours of collection. 3. ANALYSES ARE TO BE MADE OF THE MOBILE CONSTITUENTS (DISSOLVED AS WELL AS COLLOIDAL) IN THE GROUNDWATER, NOT THOSE THAT ARE A PART OF SEDIMENT ASSOCIATED WITH WELL CONSTRUCTION OR SAMPLING PROCEDURES. CHECK WITH YOUR LABORATORY ON PROPER PROCEDURES FOR SAMPLE COLLECTION AND PRESERVATION. 4. As per Title 15, North Carolina Administrative Code, Subchapter 2L, analytical procedures shall be in accordance with the methods described in one of the following publications, or by other methods approved beforehand by. the Director, Division of Environmental Management: (a) Standard Methods for the Examination of Water and Wastewater, 16th Edition, 1985and 17th Edition, 1989, published jointly by American Public Health Association, American Water Works Association and Water Pollution Control Federation; (b) Methods for Chemical Analysis of Water and Waste, 1979, U.S. Environmental Protection Agency publication number EPA-600/4-79-020, as revised March 1983; (c) Test Methods for Evaluating Solid Wastes: Physical/Chemical Methods, 3rd Edition,11986, U.S. Environmental Protection Agency publication number SW-846; (d) Test Procedures for the Analysis of Polluants Under the Clean Water Act, Federal Registef Vol, 49, No. 209, 40 CFR Part 136, October 26, 1984; 5. Measure and record the depth of water in the Well prior to pumping or bailing any water from the well. 6. At least 3 volumes of water in the well should ble pumped or bailed prior to collecting a sample for analysis.: If the well is pumped/bailed dry before 3 well volumes are removed, samples can be collected as soon as the well recovers to the point where enough water is available to collect your. sample. 7. Determination for pH, Specific Conductance, temperature, odor and appearance must be made in the field on unfiltered samples when the sample is collected. 8. Field equipment must be calibrated in accordance with recommendations by the manufacturer 9. Samples must be filtered through a 0.45 micron filter immediately after collection when a dissolved analysis is required. (See #4. above) 10.The sample container should be labeled at the time of collection with the facility name, well identification number and date and time collected. 11. "Authorized agent' is any corporate officer or public official authorized by the company, corporation, or governmental body to sign official documents. DIVISION OF WATER QUALITY - GROUNDWATERsSEOTIQN GROUNDWATER QUALITY MONITORING: eox 29578 For additional forms P.ORALEIGH, NO 27626.0578 COMPLIANCEREPORT FORM please write or calk (919)733.3221 Type or Use a ball-point pen and press firmly. PERMIT NUMBER: (REQUIRED) Facility Name A7/On/AG ECN /vrC L 0:'7 Non -Discharge Address Orl /U.Asur Avr. NPDES A/C 00607Y7 I w - Z County FIAAnt £TT TYPE OF DISPOSAL OPERATION BEING MONITORED (REQUIRED) Well Location To PP0Ll.Sa 'PoJD Lagoon Septic Tank/Drain Field Well Identification Number W If- Well Depth /S Ft. Well Diameter_7iSample (Screened) Interval 9 Ft. To / 7- Ft. Depth to Water Level Z ft. below measuring point (before sampling) Measuring point isft. above land surface 3 Gallons of water pumped/bailed before sampling Field Analysis: pH 5 7 Specific Conductance uMhos Temp.y Date Sample Collected ) 8J98 Date Lab Sample Analyzed 3 �1 Laboratory Name Cw v I Roni rvs w-r SAMPLES FOR METALS WERE COLLECTED UNFILTERED AND FIELD ACIDIFIED Spray Field Land Application of Rotary Distributor Appearance ication No. _ YES NO Subsurface Low -Pressure Piping (LPP) Other �� r i7�e.r 4Nra� COD mg/1 Nitrite (NO2) as N mg/I Ni - Nickel "; "-;mg/1 Coliform: MF Fecal /100ml Nitrate (NO3) as N mg/1 Pb - Lead a - r=mg/I Coliform: MF Total /100ml Phosphorus: Total as P mg/1 Zn - Zinc�g/I (Note: Use MPN method for highly turbid samples) Al - Aluminum mg/I Pesticides/Herbicides -� : ;`i Dissolved Solids: Total 5L mg/1 Ba - Barium mg/I (Specify Compounds) pH (when analyzed) C units Ca - Calcium mg/I - = yLg/I TOC mg/I Cd - Cadmium mg/I ; pug/I Chloride 31 mg/I Chromium: Total mg/I rs fir' ug/I Arsenic mg/I Cu - Copper mg/I Other (Specify Compounds and Grease and Oils mg/I Fe - Iron mg/1 Concentration units) Hardness: Total mg/I Hg - Mercury mg/I Phenol mg/I K - Potassium mg/I Sulfate mg/I Mg - Magnesium mg/I Specific Conductance 93 uMhos Mn - Manganese mg/I Total Ammonia mg/I Na - Sodium mg/I TKN as N mg/I I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE. Note: Values should reflect dissolved and colloidal concentrations. (see #3 on back) See back for instructions. ignature of Permittee r Authorized Agent*) Date •* Submit blue and yellow copies only to address above. GW-59 REV. 8/96 M 1. Samples should be analyzed as soon as possible after collection. SAMPLES WHICH ARE NOT ANALYSED WITHIN THE HOLDING TIME SPECI- FIED FOR THE METHOD USED (SEE #4. BELOW) MUST BE DISCARDED AND NEW SAMPLES COLLECTED. 2. Metals Analyses: Use Standard Method 3030C=for sample preparation (mercury excluded). DO NOT FILTER METALS SAMPLES IN THE FIELD H! Unfiltered samples must be collected for metals, then field acidified with 5 ml concentrated nitric acid per liter of sample, and should be submitted to the lab within 24 hours. 'r, Sample preparation in the laboratory (extraction and filtration) must be completed within 72 hours of collection. _ 3. ANALYSES ARE TO BE MADE OF THE MOBILE CONSTITUENTS (DISSOLVED AS WELL AS COLLOIDAL) IN THE GROUNDWATER, NOT THOSE THAT ARE A PART 9F SEDIMENT ASSOCIATED WITH WELL CONSTRUCTION OR SAMPLING PROCEDURES. CHECK WITH YOUR LABORATORY ON PROPER PROCEDURES FOR SAMPLE COLLECTION AND PRESERVATION. 4. As per Title 15, North Carolina Administrative Code, Subchapter 2L, analytical procedures shall be in accordance with the methods described in one of the following publications, or by other methods approved beforehand by the Director, Division of Environmental Management: (a) Standard Methods for the Examination of Water and Wastewater, 16th Edition, 1985 and 17th Edition, 1989, published jointly by American Public Health Association, American Water Works Association and Water Pollution Control Federation; (b) Methods for Chemical Analysis of Water and Waste, 1979, U.S. Environmental Protection Agency publication number EPA-600/4-79-020, as revised March 1983; (c) Test Methods for Evaluating Solid Wastes: Physical/Chemical Methods, 3rd Edition,1986, U.S. Environmental Protection Agency publication number SW-846; (d) Test Procedures for the Analysis of Palluants Under the Clean Water Act, Federal Register Vol. 49, No. 209, 40 CFR Part 136, October 26, 1984; 5. Measure and record the depth of water in the well prior to pumping or bailing any water from the well. 6. At least 3 volumes of water in the well should be pumped or bailed prior to collecting a sample for analysis. If the well is pumped/bailed dry before 3 well volumes are removed, samples can be collected as soon as the well recovers to the point where enough water is available to collect your sample. 7. Determination for pH, Specific Conductance, temperature, odor and appearance must be made in the field on unfiltered samples when the sample is collected. 8. Field equipment must be calibrated in accordance with recommendations by the manufacturer. 9. Samples must be filtered through a 0.45 micron filter immediately after collection when a dissolved analysis.is required. (See #4. above) 10.The sample container should be labeled at the time of collection with the facility name, well identification number and date and time collected. 11."Authorized agent' is any corporate officer or public official authorized by the company, corporation, or governmental body to sign official documents. - Type oruse a ball-point pen and press firmly. Facility Name bjAT16NAL. rAEGNANIC:At- CAR96wr - Address -SO4 NORTtV 1315ue Avt. Well Location County RAPw.T'T PERMIT NUMBER: (REQUIRED) Non -Discharge NPDES NC 0b60717 TYPE OF DISPOSAL OPERATION BEING MONITORED Septic Tank/Drain Field Well Identification Number W a Well Depth Well Diameter 0 2- Sample (Screened) Interval 10 Ft. To Z Spray Field Subsurface Low -Pressure Depth to Water Level 4 ft. below measuring point (before sampling) Land Application of Sludge Piping (LPP) Measuring point is 3 ft. above land surface other Gallons of water pumped/bailed before sampling Z Rotary Distributor SEi-TL1,& � I�ousw �.?0"11 Field Analysis: pH S. f Specific Conductance uMhos Temp. Ly °C Odor �N Appearance Date Sample Collected 12-I1-97 Date Lab Sample Analyzed 12-I'Z — 12-17-27 LaboratoryName GNyIP6NAENT I Certification No. /0 SAMPLES FOR METALS WERE COLLECTED UNFILTERED AND FIELD ACIDIFIED _YES NO COD 7 o mg/I Coliform: MF Fecal /100ml Coliform: MF Total /100m1 (Note: Use MPN method for highly turbid samples) Dissolved Solids: Total g/I pH (when analyzed) nits TOC 't mg/I Chloride 8 mg/I Arsenic mg/I Grease and Oils mg/I Hardness: Total mg/I Phenol mg/I Sulfate mg/I Specific Conductance 9 t uMhos Total Ammonia mg/I TKN as N mg/I Nitrite (NO2) as N _ Nitrate (NO3) as N _ Phosphorus: Total as Al - Aluminum Ba - Barium Ca - Calcium Cd - Cadmium Chromium: Total Cu - Copper Fe - Iron Hg - Mercury K - Potassium Mg - Magnesium Mn - Manganese Na - Sodium 7 Lagoon mg/I Ni - Nickel mg/I r}�g/I Pb - Lead —� = mg/I g/I Zn - Zinc mg/I mg/I Pesticides/Herbicides mg/I (Specify Compounds) iJo mg/I ug/I mg/I - ug/I mg/I ,= ug/I mg/I Other (Specify Compounds and Iv " mg/I Concentration units) :; mg/I mg/I mg/I mg/I n mg/I 1N�� I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE. Note: Values should reflect dissolved and colloidal concentrations. (see #3 on back) % Z`Z 3 /9 7 See back for instructions. signature of Permitta (or Authorized Agent') Date "" Submit blue, green, and yellow copies only to address above. GW-59 REV. 6/93 COLLECTION AND ANALYSIS OF GROUNDWATER SAMPLES 1. Samples should be analyzed as soon as possible after collection. SAMPLES WHICH ARE NOT ANALYSED WITHIN THE HOLDING TIME SPECI- FIED FOR THE METHOD USED (SEE #4. BELOW) MUST BE DISCARDED AND NEW SAMPLES COLLECTED. 2. Metals Analyses: Use Standard Method 3030C for sample preparation (mercury excluded). DO NOT FILTER METALS SAKI LES IN THE FIELD !!! Unfiltered samples must be collecie'd for'metals, then field acidified with 5 mi concentrated nitric acid per liter of sample, and should be submitted to the lab within 24 hours. Sample preparation in the laboratory (extraction and filtration) must be completed within 72 hours of collection. 3. ANALYSES ARE TO BE MADE OF THE MOBILE CONSTITUENTS (DISSOLVED AS WELL AS dOLLOIDAL) IN THE GROUNDWATER, NOT THOSE THAT ARE A PART OF SEDIMENT ASSOCIATED WITH WELL CONSTRUCTION OR SAMPLING PROCEDURES. CHECK WITH YOUR LABORATORY ON PROPER PROCEDURES FOR SAMPLE COLLECTION AND PRESERVATION. 4. Asper Title 15, North Carolina Administrative Code, Subchapter 2L, analytical procedures shall be in accordance with the methods described in one of the following publications, or by other methods approved beforehand by the Director, Division of Environmental Management: (a) Standard Methods for the Examination of Water and Wastewater, 16th Edition, 1985 and 17th Edition, 1989, published jointly by American Public Health Association, American Water Works Association and Water Pollution Control Federation; (b) Methods for Chemical Analysis of Water and Waste, 1979, U.S. Environmental Protection Agency publication number EPA-600/4-79-020, as revised March 1983; (c) Test Methods for Evaluating Solid Wastes: Physical/Chemical Methods, 3rd Edition, 1986, U.S. Environmental Protection Agency publication number SW-846; (d) Test Procedures for the Analysis of Polluants Under the Clean Water Act, Federal Register Vol. 49, No. 209, 40 CFR Part 136, October 26, 1984; , 5. Measure and record the depth of water in the well prior to pumping or bailing any water from the well. 6. At least 3 volumes of water in the well should be pumped or bailed prior to collecting a sample for analysis. If the well is pumped/bailed dry before 3 well volumes are removed, samples can be collected as soon as the well recovers to the point where enough water is available to collect your sample. 7. Determination for pH, Specific Conductance, temperature, odor and appearance must be made in the field on unfiltered samples when the sample is collected. 8. Field equipment must be calibrated in accordance with recommendations by the manufacturer. 9. Samples must be filtered through a 0.45 micron filter immediately after collection when a dissolved analysis is required. (See #4. above),., 10.The sample container should be labeled at the time of collection with the facility name, well identification number and date and time collected. 11. "Authorized agent" is any corporate officer or public official authorized by the company, corporation, or governmental body to sign official documents. 1' or Use a ,/ press Facility Name-,vATrnwAL AlFCHAr.11 CAL CRRrtr.Ar Address-5oy /Vosrw Aspz Ayr, Well Location HET -Tee PERMIT NUMBER: (REQUIRED) Non -Discharge NPDES NC oo4ct7y7 TYPE OF DISPOSAL OPERATION BEING MONITORED (REQUIRED) Lagoon Well Identification Number Well Depth Ft. Well Diameter z" Sample (Screened) Interval yG Ft. To _/8 Ft. Spray Field / r-/ Septic Tank/Drain Field Subsurface Low -Pressure Piping (LPP) Depth to Water Level ft. below measuring point (before sampling) Land Application of slud7q�e Measuring point is 3 ft. above land surface other Gallons of water pumped/bailed before sampling 2-Rotary Distributor 8rrwr .S£r Field Analysis: pH -% O Specific Conductance �N uMhos Temp. / 5 oC Odor ti Appearance 1 Date Sample Collected I Z - It-9 i Date Lab Sample Analyzed r'z /I z — Iz/ 17 f a7 Laboratory Name Enr1Jt'6wr ew-r I Certification No. i0 SAMPLES FOR METALS WERE COLLECTED UNFILTERED AND FIELD ACIDIFIED YES NO COD I `t mg/I Coliform: MF Fecal /100ml Coliform: MF Total /100ml (Note: Use MPN method for highly turbid samples) Dissolved Solids: Total 33 mg/I pH (when analyzed) units TOC /. 05 mg/I Chloride C1 mg/I Arsenic mg/I Grease and Oils mg/I Hardness: Total mg/I Phenol mg/I Sulfate mgA Specific Conductance 89 uMhos Total Ammonia mg/I TKN as N mgA Nitrite (NO2) as N mg/I Nitrate (NO3) as N mr��1g/I Phosphorus: Total as P l4tg/1 Al - Aluminum mg/I Ba - Barium mg/I Ca - Calcium mg/I Cd - Cadmium mg/I Chromium: Total mg/1 Cu - Copper mg/I Fe - Iron mg/I Hg - Mercury mgA K - Potassium mg/I Mg - Magnesium mg/I Mn - Manganese mg/I Na - Sodium mgA I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE. cQn Jyy AGrJvr> Z Z3 A Signature of Permitte (or Authorized Agent') Date GW-59 REV. 6/93 Ni - Nickel Pb - Lead Zn - Zinc Pesticides/Herbicides (Specify Compounds) "tmgA ° " • mgA r, ; n =`-.Ug/I ug/I ug/I Other (Specify Compounds and Concentration units) Note: Values should reflect dissolved and colloidal concentrations. (see #3 on back) ' See back for instructions. •' Submit blue, green, and yellow copies only to address above. COLLECTION AND ANALYSIS OF GROUNDWATER SAMPLES 1. Samples should be analyzed as soon as possible after collection. SAMPLES WHICH ARE NOT ANALYSED WITHIN THE HOLDING TIME SPECI- FIED FOR THE METHOD USED (SEE 94. BELOW) MUST BE DISCARDED AND NEW SAMPLES COLLECTED. 2. Metals Analyses: Use Standard Method 3030C for sample preparation (mercury excluded). DO NOT FILTER METALS SAMPLES IN THE FIELD Itt Unfiltered samples must be collected for metals, then field acidified with 5 ml concentrated nitric acid per liter of sample, and should be submitted to the lab within 24 hours. - Sample preparation in the laboratory (extraction and filtration) must be completed within 72 hours of collection. 3. ANALYSES ARE TO BE MADE OF THE MOBILE CONSTITUENTS (DISSOLVED AS WELL AS COLLOIDAL) IN THE GROUNDWATER, NOT THOSE THAT ARE A PART OF SEDIMENT ASSOCIATED WITH WELL CONSTRUCTION OR SAMPLING PROCEDURES. CHECK WITH YOUR LABORATORY ON PROPER PROCEDURES FOR SAMPLE COLLECTION AND PRESERVATION. 4. As per Title 15, North Carolina Administrative Code, Subchapter 2L, analytical procedures shall be'in accordance with the methods described in one of the following publications, or by other methods approved beforehand,by the Director, Division of Environmental Management: (a) Standard Methods for the Examination of Water and Wastewater, 16th Edition, 1985 and 17th Edition, 1989, published jointly by American Public Health Association, American Water Works Association and Water Pollution Control Federation; (b) Methods for Chemical Analysis of Water and Waste, 1979, U.S. Environmental Protection Agency publication number EPA-600/4-79-020, as revised March 1983; (c) Test Methods for Evaluating Solid Wastes: Physical/Chemical Methods, 3rd Edition, 1986, U.S. Environmental Protection Agency publication number SW-846; (d) Test Procedures for the Analysis of Polluants Under the Clean Water Act, Federal Register Vol. 49; No. 209, 40 GFR Part 136, October 26, 1984: 5. Measure and record the depth of water in the well prior to pumping or bailing any water from the well. , 6. At least 3 volumes of water in the well should be pumped or bailed prior to collecting a sample for analysis. If the well is pumped/bailed dry before 3 well volumes are removed, samples can be collected as soon as the well recovers to the point where enough water is available to collect your sample. Determination for pH, Specific Conductance, temperature, odor and appearance must be made in the field on unfiltered samples when the sample is collected. 8. Field equipment must be calibrated in accordance with recommendations by the manufacturer. 9. Samples must be filtered through a 0.45 micron filter immediately after collection when a dissolved analysis is required. (See #4. above) 10.The sample container should be labeled at the time of collection with the facility name, well identification number and date and time collected. 11."Authorized agent" is any corporate officer or public official authorized by the company, corporation, or governmental body to sign official documents. J Type or use a ball-point pen and press firmly. Facili Well Well Identification Number w -_T_ Well Depth / 8 Ft. Well Diameter Z" Sample (Screened) Interval / 7- Ft. To _/Ft. Depth to Water Level 4 ft. below measuring point (before sampling) Measuring point is ft. above land surface Gallons of water pumped/bailed before sampling Z PERMIT NUMBER: (REQUIRED) Non -Discharge SEP 19 1991 NPDES N C. o0 4, A74 7 TYPE OF DISPOSAL OPERATION BEING MONITOREFBAY�T E�`�LE (REQUIRED) Lagoon Sep ih Fi R�[EeCNCE Spray Field Subsurface Low -Pressure Piping (LPP) Land Application of Sludgy —L Other Rotary Distributor SLTT/ I wV_ S YN .. Iu� Field Analysis: pH 4• S ecific Condu tance uMhos Temp. �6 oC Odor Appearance Date Sample Collecteed Aate Lab Sample Analyzed f?4Zz - g�zs/97 LaboratoryName `-NV Iix MN .4-r ( � 0 Certification No. � SAMPLES FOR METALS WERE COLLECTED UNFILTERED AND FIELD ACIDIFIED YES NO COD / Al mgA Coliform: MF Fecal A00m1 Coliform: MF Total /100ml (Note: Use MPN method for highly turbid samples) Dissolved Solids: Total mg/I pH (when analyzed) nits TOC mg/I Chloride yo mg/I Arsenic mg/I Grease and Oils mg/I Hardness: Total mg/I Phenol mg/I Sulfate mg/I Specific Conductance $7 uMhos Total Ammonia mg/I TKN as N mgA Nitrite (NO2) as N mg/I Nitrate (NO3) as N rri�g/I Phosphorus: Total as P. 14tg/1 Al - Aluminum mg/I Ba - Barium mg/I Ca - Calcium mg/I Cd - Cadmium mg/I Chromium: Total mg/I Cu - Copper mg/I Fe - Iron mg/I Hg - Mercury mg/I K - Potassium mg/I Mg - Magnesium mg/I Mn - Manganese mg/I Na - Sodium mg/I I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE. �aw- Signature of Permitte (or Authorized Agent*) --,—' Ni - Nickel mg/I Pb - Lead `-? mgA Zn - Zinc ^' = mgA Pesticides/Herbicides r (Specify Compounds) t Crr; ug/I ug/I m ug/I Other (Specify Compounds and 171_ Concentration units) M ,Note: Values should reflect dissolved and colloidal concentrations. (see #3 on back) * See back for instructions. ** Submit blue, green, and yellow copies only to address above. GW-59 REV. 6/93 COLLECTION AND ANALYSIS OF GROUNDWATER SAMPLES 1- _Samples should be analyzed as soon as possible after collection. SAMPLES WHICH ARE NOT ANALYSED WITHIN THE HOLDING TIME SPECI- FIED FOR THE METHOD USED (SEE #4. BELOW) MUST BE DISCARDED AND NEW SAMPLES COLLECTED. 2. Metals Analyses: Use Standard Method 3030C for sample preparation (mercury excluded). DO NOT FILTER METALS SAMPLES IN THE FIELD !!! Unfiltered samples must be collected for metals, then field acidified with 5 ml concentrated nitric acid per liter of sample, and should be submitted to the laki within 24 hours. ,§arnpte preparation in the laboratory (extraction and filtration) must be completed within 72 hours of collection. 3. ANALYSES ARE TO BE MADE OF THE MOBILE CONSTITUENTS (DISSOLVED'AS WELL AS cOLLOIDAL) IN THE GROUNDWATER, NOT THOSE THAT AREA PART OF SEDIMENT ASSOCIATED WITH WELL CONSTRUCTION OR SAMPLING PROCEDURES. CHECK WITH YOUR LABORATORY ON PROPER PROCEDURES FOR SAMPLE COLLECTION AND PRESERVATION. 4. As per Title 15, North Carolina Administrative Code, Subchapter 2L, analytical procedures shall be in accordance with the methods described in one of the following publications, or by other methods approved beforehand by the Director, Division of Environmental Management: (a) Standard Methods for the Examination of Water and Wastewater, 16th Edition, 1985 and 17th Edition, 1989, published jointly by American Public Health Association, American Water Works Association and Water Pollution Control Federation; (b) Methods for Chemical Analysis of Water and Waste, 1979, U.S. Environmental Protection Agency publication number EPA-600/4-79-020, as revised March 1983; (c) Test Methods for Evaluating Solid Wastes: Physical/Chemical Methods, 3rd Edition, 1986, U.S. Environmental Protection Agency { ' publication number SW-846: (d) Test Procedures for the Analysis of Polluants Under the Clean Water Act, Federal Register Vol. 497 No. 209, 40 CFR Part 136, r' October 26, 1984; f - ' 5. Measure arid=record the depth of water in the well prior to pumping or bailing any water from the well. 6. At least 3 voltimes of water in the well should be pumped or bailed prior to collecting a sample for analysis. If the well is pumped/bailed dry before 3 well volumes are removed, samples can be collected as soon as the well recovers to the point where enough water is available to collect your sample. 7. Determination for pH, Specific Conductance, temperature, odor and appearance must be made in the field on unfiltered samples when the sample is collected. 8. Field equipment must be calibrated in accordance with recommendations by the manufacturer. 9. Samples must be filtered through a 0.45 micron filter immediately after collection when a dissolved analysis is required. (See #4. above) 10.The sample container should be labeled at the time of collection with the facility name, well identification number and date and time collected. 11. "Authorized agent" is any corporate officer or public official authorized by the company, corporation, or governmental body to sign official documents. 4. Type or Use a ball-point pen and press firmly. Facility Name Address PERMIT NUMBER: (REQUIRED) Non -Discharge NPDES n/C 06 Well Location ISc Scr c Nc Pbc, N e.& Pom ou- Well Identification Number `N I Well Depth O Ft. Well Diameter Z' _ Sample (Screened) Interval 1A Ft. To ��Ft. Sn, Depth to Water Level / Z ft. below measuring point (before sampling) Or iq /Ors Measuring point is 3 ft. above land surface Gallons of water pumped/balled before sampling 2 Field Analysis: pH 4. 6 "UNpecific Conductance uMhos Temp. 16 °C Odor At j1- HApf Date Sample Collec�t+ed z Date Lab Sample Analyzed _8/zz - S�zs�97 LaboratoryName LAIVIFL6n/M£Mr I Certification No. _ SAMPLES FOR METALS WERE COLLECTED UNFILTERED AND FIELD ACIDIFIED YES NO Lagoon BEING MONITORED REG. OFRCE Septic Tank/Drain Field Subsurface Low -Pressure Piping (LPP) Application of Studg Other y Distributor 5_ <<_- COD / 6 mg/I Nitrite 11\1021 as N mg/I Ni - Nickel • m A Coliform: MF Fecal /100ml Coliform: MF Total /100m1 (Note: Use MPN method for highly turbid samples) Dissolved Solids: Total mg/I pH (when analyzed) -. units TOC mgA Chloride $ mg/I Arsenic mg/I Grease and Oils mg/I Hardness: Total mg/I Phenol mg/I Sulfate mg/I Specific Conductance 90 uMhos Total Ammonia mg/I TKN as N mg/I Nitrate (NO3) as N rig/I Pb - Lead g �mg/I Phosphorus: Total as P g/1 Zn - Zinc c�9rng/I Al - Aluminum mg/I Pesticides/Herbicides cn om Ba - Barium mg/I (Specify Compounds) '°= Ca - Calcium mg/I g/I Cd - Cadmium mg/I a�ilg/I Chromium: Total mg/I ug/I Cu - Copper mg/I Other (Specify Compounds and Fe - Iron mg/I Concentration units) Hg - Mercury mg/I K - Potassium mg/I Mg - Magnesium mg/I Mn - Manganese mg/I Na - Sodium mg/I I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE. ( ( 1g-n, 31 - �ti CAGZJ .r)- 9 yA7 Signature of Permi a (or Authorized Agent") Date GW-59 REV. 6/93 Note: Values should reflect dissolved and colloidal concentrations. (see #3 on back) See back for instructions. " Submit blue, green, and yellow copies only to address above. COLLECTION AND ANALYSIS OF GROUNDWATER SAMPLES 1. 'Samples shoufd be analyzed as soon as possible after collection. SAMPLES WHICH ARE NOT ANALYSED WITHIN THE HOLDING TIME SPECI.- ,TIED F013 THE METHOD USED (SEE #4. BELOW) MUST BE DISCARDED AND NEW SAMPLES COLLECTED. 2. Metals_Analyses: Use Standard Method 3030C for sample preparation (mercury excluded). DO NOT FILTER METALS SAMPLES IN THE FIELD 111 ....Unfilteredsamples must be collected fo"r metals, then field a lied with 5 ml concentrated nitric acid per liter of sample, and should be submitted to the 1a6tivithin 24 hours. Sample preparation in the laboratory (extr e\ jlt o'tr) 7r`ust be completed within 72,hours of collection. 3. ANALYSES ARE TO BE MADE OF THE MOBILE QQN UENTS (DISSOLVEb\AS WELL AS C&LOIDAL) IN THE GROUNDWATER, NOT _THOSE THAT E-AoilkbF SEDI�ASSOCIATED WITH WELL CONSTRUCTION OR SAMPLING PROCEDURES. CHECK WITH YOUR LABORATORY O`N` ROPER Pf Q12,10SURES FOR SAMPLE COLLECTION AND PRESERVATION. I y/ IkW , 4. Asper Title 15, North Carolina Administrative Code, Subchapter 2L, analyti8aiI procedures shall be in accordance with the methods'described in one of the following publications, or by other methods approved beforehand by. the' Director, Division of Environmental Management: (a) Standard Methods for the Examination of Water and Wastewater, 16th Edition, 1985 and 17th Edition, 1989, published jointly by American Public Health Association, American Water Worl<s Association and Watet Pollution Control Federation; (b) Methods for Chemical Analysis of Water and Waste, 1979, U.S. Environmental Protection Agegcy publication number EPA-600/4-79-020, as revised March 1983; u- (c) Test Methods for Evaluating Solid Wastes: Physical/Chemical Methods, 3rd Edition, 1986, U.S. Environmental Protection Agency ru publication number SW-846; (d) Test Procedures for the Analysis of Polluants Under the Clean Water Act, Federal Register VOL 49. No. 209, 40 CFR Part 136, October 26, 1984; 5. Measur" nd record the depth of water in the well prior to pumping or bailing any water from the well. 6. At least 3 volumes of water in the well should be pumped or bailed prior to collecting a sample for analysis. If the well is pumped/bailed dry before 3 well volumes are removed, samples can be collected as soon as the well recovers to the point where enough water is available to collect your sample. 7. Determination for pH, Specific Conductance, temperature, odor and appearance must be made in the field on unfiltered samples when the sample is collected. = \ 8. Field equipment must be calibrated in accordance with recommendations by the manufacturer. P 9. Samples must be filtered through a 0.45 micron filter immediately after collection when a dissolved analysis is required. (See #4. above) 10. The sample container should be labeled at the time of collection with the facility name, well identification number and date and time collected. 11. "Authorized agent" is any corporate officer or public official authorized by.the•company, corporation, or governmental body to sign official documents. Type oruse a bau-point pen and press firmly. ,,�, // yy� PERMIT NUMBER: (REQUIRED) Facility Name /yATroly ;use C'AASc3" Non -Discharge Address O'-1 /U. /� S H £ Av E . NPDES 09C 00 6 0 7Y 7 �1 County ;'+<� RNCTT TYPE OF DISPOSAL OPERATION BEING MONITORED Well Location AisnAc&-r To poLlSNnu4 f or+b (REQUIRED) Lagoon Septic Tank/Drain Field Well Identification Number W 11 Well Depth / S Ft. ti Spray Field Subsurface Low -Pressure Well Diameter z Sample (Screened) Inteival / D Ft. To �Ft. Piping (LPP) Depth to Water Level /0 ft. below measuring point (before sampling) Land Application of Sludge Measuring point is Z ft. above land surface K— Other Gallons of water pumped/bailed before sampling Z Rotary Distributors rr uG r ar !iM6 l?oN Field Analysis: pH 5.0 Specific Conductance uMhos Temp. / -S °C Odor Appearance - Date Sample Collected L Z- 97 Date Lab Sample Analyzed L/- /O- 97 LaboratoryName &NVIRONmEw-r Ir �tji Certification No. /D SAMPLES FOR METALS WERE COLLECTED UNFILTERED AND FIELD ACIDIFIED YES NO COD < 10 mg/I Nitrite (NO2)jasN Ni -Nickel � rn mg/I Coliform: MF Fecal /100ml Nitrate (NO3 Pb - Lead —' - mg/IColiform: MF Total /100ml Phosphorus:al Zn - Zinc �" mg/1 (Note: Use MPN method for highly turbid samples) AI - Aluminu Pesticides/Herbicides f t Dissolved Solids: Total g/I Ba - Barium (Specify Compounds) cr% orn pH (when analyzed) nits Ca - Calcium mg/I = ug/I TOC mg/I Cd - Cadmium mg/I =- _1sug/I Chloride 60 mg/1 Chromium: Total mg/I `p zug/I Arsenic mg/1 Cu - Copper mg/1 Other (Specify Compounds and Grease and Oils mg/I Fe - Iron mg/I Concentration units) Hardness: Total mg/l Hg - Mercury mg/l Phenol mg/1 K - Potassium mg/I o Sulfate mg/1 Mg - Magnesium mg/I Specific Conductance 80 uMhos Mn - Manganese mg/l �+ Total Ammonia mg/I Na - Sodium mg/I TKN as N mg/1 Q z I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE. S-z-9.7 Date Note: Values should reflect dissolved colloidal concentrations. (see #3 on back) ' See back for instructions. *` Submit blue, green, and yellow copies only to address above. u I i GW-59 REV. 6/93 COLLECTION AND ANALYSIS OF GROUNDWATER SAMPLES 1. Samples should be analyzed as soon as possible after collection. SAMPLES WHICH ARE NOT ANALYSED WITHIN THE HOLDING TIME SPECI- FIED FOR THE METHOD USED (SEE #4. BELOW) MUST BE DISCARDED AND NEW SAMPLES COLLECTED,. 2. Metals Analyses: Use Standard Method 3030C for sample preparation (mercury excluded). DO NOT FILTER METALS SAMPLES IN THE FIELD !!! Unfiltered samples must be collected for metals, then field acidified with 5 ml concentrated, nitric acid per liter of sample, and should be submitted to the lab within 24 hours. Sample preparation in the laboratory (extraction and filtration) must be completed within 72 hours of collection. 3. ANALYSES ARE TO BE MADE OF THE MOBILE CONSTITUENTS (DISSOLVED AS WELL AS COLLOIDAL) IN THE GROUNDWATER, NOT THOSE THAT ARE A PART OF SEDIMENT ASSOCIATED WITH WELL CONSTRUCTION OR SAMPLING PROCEDURES. CHECK WITH YOUR LA130RATORY ON PROPER PROCEDURES FOR SAMPLE COLLECTION AND PRESERVATION. 4. Asper Title 15, North Carolina Administrative Code, Subchapter 2L, analytical procedures shall be in accordance with the methods'described in one of the following publications, or by other methods approved beforehand by the Director, Division of Environmentat Management: (a) Standard Methods for the Examination of Water and Wastewater, 16th Edition, 1985 and 17th Edition, 1989, published jointly by American Public Health Association, American Water Works Association and Water Pollution Control Federation; (b) Methods for Chemical Analysis of Water and Waste, 1979, U.S. Environmental Protection Agency publication number r— EPA-600/4-79-020, as revised March 1983; (c) Test Methods for Evaluating Solid Wastes: Physical/Chemical Methods, 3rd Edition, 1986, U.S. Environmental Protection Agency publication number SW-846; (d) Test Procedures for the Analysis of Polluants Under the Clean Water Act, Federal Register+Vol. 49. No. 209, 40 CFR Part 136, _. October26, 1984; 5. Measure%hd record the depth of water in the well prior to pumping or bailing any water from the well. 6. At. (east 3-volumes of water in the well should be pumped or bailed prior to collecting a sample for analysis. If the well is pumped/bailed dry before 3 well v6164 1as are removed, samples can be collected as soon as the well recovers to the point where enough water is available to collect your sample. ? - _ % Det=o&ination for pH, Specific Conductance, temperature, odor and appearance must be made in the field on unfiltered samples when the sample is co4Wed. Sr�_Field �uipment must be calibrated in accordance with recommendations by the manufacturer. 9. SampVt must be filtered through a 0.45 micron filter immediately after collection when a dissolved analysis is required. (See #4. above) 10.The sample container should be labeled at the time of collection with the facility name, well identification number and date and time collected. 11. "Authorized agent" is any corporate officer or public official authorized by the company, corporation, or governmental body to sign official documents. Type or use a ball-point pen and press firmly. Facilii Well I PERMIT NUMBER: (REQUIRED) Non -Discharge NPDES NC 0060747 TYPE OF DISPOSAL OPERATION BEING MONITORED (REQUIRED) Lagoon Septic Tank/Drain Field Well Identification Number W I Well Depth 20 Ft. Well Diameter Z" Sample (Screened) Interval 15 Ft. To Z O Ft. Depth to Water Level 15 ft. below measuring point (before sampling) Measuring point is '3 ft. above land surface Gallons of water pumped/bailed before sampling Z. 6 Field Analysis: pH S. f Specific Conductance uMhos Temp. 1... °C Odor Date Sample Collected 4 %'ZIR7 Date Lab Sample Analyzed H//o /q'7 Spray Field Subsurface Low -Pressure Piping (LPP) Land Application of Sludge C Other Rotary Distributor Sr-.ri Appearance LaboratoryName—ENVIZONMEw-r I :IuC- Certification No. IO SAMPLES FOR METALS WERE COLLECTED UNFILTERED AND FIELD ACIDIFIED YES NO o COD 410 mg/I Coliform: MF Fecal _ /100ml Coliform: MF Total /100ml (Note: Use MPN method for highly turbid samples) Dissolved Solids: Total g/I pH (when analyzed) u is TOC �• mg/I Chloride 7 mg/I Arsenic mg/I Grease and Oils mg/l Hardness: Total mg/I Phenol mg/I Sulfate mg/I Specific Conductance 80 uMhos Total Ammonia mg/I TKN as N mg/I Nitrite (NO2) as N mg/I Ni - Nickel C);�- mg/I Nitrate (NO3) as N rrppg/I Pb - Lead -� mg/l Phosphorus: Total as P. 4/1 Zn - Zinc < mg/I AI - Aluminum mg/I Pesticides/Herbicides _: Ba - Barium mg/I (Specify Compounds) � n Ca Calcium mgll M=ug/I Cd - Cadmium mg/I ug/I Chromium: Total mg/I ug/I Cu - Copper mg/I Other (Specify Compounds and Fe - Iron mg/I Concentration units) Hg - Mercury mg/I - K - Potassium mg/1 l F g Mg - Magnesium mg/I Mn - Manganese mg/I ^ Na - Sodium mg/I 0 a •a I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE. Note: Values should reflect dissolved FM colloidal concentrations. (see #3 on back) GENT S,2 /9 7 * See back for instructions. Signature of Permittee r Authorized Agent") Date " Submit blue, green, and yellow copies only to address above. GW-59 REV. 6/93 H COLLECTION AND ANALYSIS OF GROUNDWATER SAMPLES 1. Samples should be analyzed as soon as possible after collection. SAMPLES WHICH ARE NOT ANALYSED WITHIN THE HOLDING TIME SPECI- FIED FOR THE METHOD USED (SEE #4. BELOW) MUST BE DISCARDED AND NEW SAM`NLETCOLLECTED. 2. Metals Analyses: Use Standard Method 3030C for sample preparation (mercury excluded). 00 NOT FILTER METALS SAMPLES IN THE,FIELD !!! Unfiltered samples must be collected for metals, then field acidified with 5 ml concentrated nitric acid per liter of sample, and'should be submitted to the lab within 24 hours. ' Sample preparation in the laboratory (extraction and filtration) must be completed within 72 hours of collection. 3. ANALYSES ARE TO BE MADE OF THE MOBILE CONSTITUENTS (DISSOLVED AS WELL AS COLLOIDAL) IN THE GROUNDWATER, NOT THOSE THAT ARE A PART OF SEDIMENT ASSOCIATED WITH WELL CONSTRUCTION OR SAMPLING PROCEDURES. CHECK WITH YOUR LABORATORY ON PROPER PROCEDURES FOR SAMPLE COLLECTION AND PRESERVATION. 4. As per Title 15, North Carolina Administrative Code, Subchapter 2L, analytical procedures shall be in accordance with the methods described in one of the following publications, or by other methods approved beforehand by the Director, Division of Environmental Management: (a) Standard Methods for the Examination of Water and Wastewater, f 6th Edition, 1985 and 17th Edition, 1989, published jointly by American Public Health Association, American Water Works Association and Water Pollution Control Federation; c— (b) Methods for Chemical Analysis of Water and Waste, 1979, U.S. Environmental Protection A-00ncy publication number EPA-600/4 79-020, as revised March 1983; r (c) Test Methods for Evaluating Solid Wastes: Physical/Chemical Methods, 3rd Edition, 1986, U.S. Environmental Protection Agency publication number SW-846; (d) - Test Procedures for the Analysis of Polluants Under the Clean Water Act, Federal Register Vol. 49. No. 209, 40 CFR Part 136, r., October 26, 1984; 5. Measure;rid record the depth of water in the well prior to pumping or bailing any water from the well. � 6. At least 3 volumes of water in the well should be pumped or bailed prior to collecting a sample for analysis. If the well is pumped/bailed dry before 3 well volumes. -are removed, samples can be collected as soon as the well recovers to the point where enough water is available to collect your sample. 7. Cieter'mantion for pH; Specific Conductance, temperature, odor and appearance must be made in the field on unfiltered samples when the sample is •8. Field eg4ment must'be calibrated in accordance with recommendations by the manufacturer. J9 Sample4ust be filtemd through a 0.45 micron filter immediately after collection when a dissolved analysis is required: (See #4. above) _.. 10.The sample container should be labeled at the time of collection with the facility name, well identification number and date and time collected. 11. "Authorized agent" is any corporate officer or public official authorized by the company, corporation, or governmental body to sign official documents. Type or Use a ball-point pen and press firmly. Facility Name A/ATfo,vat_ Wce-LIA.jlCAL C.aarsr�j \ Address Soo Al, A<ur Ayr PERMIT NUMBER: (REQUIRED) NPDEScN� O 7 FAVETTEVILE TYPE OF DISPOSAL OPERATION BEING MONITO G. OFFICE Well Location b7nLC T To Pn4,ismiN4 rPc,vb (REQUIRED) A Lagoon Septic Tank/Drain Field Well Identification Number W T- Well Depth 19 Ft, Spray Field Subsurface Low -Pressure Well Diameter�_Sample (Screened) Interval /O Ft. To _L�Ft. Piping(LPP) Depth to Water Level 0 ft. below measuring point (before sampling) Land Application of Stud e Measuring point is 2- ft. above land surface Other Gallons of water pumped/bailed before sampling Z . - Gncs Rotary Distributor _'�,_7-mjw& r' )7 rrrNG /�oN Field Analysis: pH S. 4 Specific Conductance - uMhos Temp. 16 oC Odor — Appearance Date Sample Collected - 12- 3- 9 6 Date Lab Sample Analyzed 1z-3-24 -ro 12-10-9( LaboratoryName ENV r AQJ M E N T I Certification No. \10 SAMPLES FOR METALS WERE COLLECTED UNFILTERED AND FIELD ACIDIFIED YES NO \ rr m COD 1-L mg/I Coliform: MF Fecal /100ml Coliform: MF Total A00m1 (Note: Use MPN method for highly turbid samples) Dissolved Solids: Total 40 mg/1 pH (when analyzed) 3MM units TOC 3.5'6 mg/I Chloride sz mg/I Arsenic mg/I Grease and Oils mg/I Hardness: Total mg/I Phenol mg/I Sulfate mg/I Specific Conductance 78 uMhos Total Ammonia mg/I TKN as N mg/I Nitrite (NO2) as N mg/I o Ni - Nickel r t mg/I rrppg/I Pb - Lead ` J mg/I PhosphomL Gv� o of 4/1 Zn - Zinc c� �= mg/I AI - AluminiVtC - ��(� 7 Ba mg/I Pesticides/Herbicides = -Bari t to }ir'.�/�-Vz- _ _ _ mg/I (Specify Compounds) =iE] .9 Ca - Calciu.. — -- mg/I — ni== ug/I Cd - Cadmium mg/I N rn ug/I Chromium: Total mg/I 'C� ug/I Cu - Copper Other (Specify Compounds and Fe - Iron I Concentration units) Hg - Mercury K - Potassium I DEr Mg - Magnesiu Mn - Mangan es mg I Na - Sodium IGH REGI dpq I I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE. Note: Values should reflect dissolved and colloidal concentrations. (see #3 on back) CA3 14&6.7 Z - / 7- q 6 See back for instructions. Signature of Permittee ( r Authorized Agent') Date •• Submit blue, green, and yellow copies only to address above. GW-59 REV. 6/93 ".FCOLLECTION AND ANALYSIS OF GROUNDWATER SAMPLES 1. Sargplesshouldbe analyzed as soon as possible after collection. SAMPLES WHICH ARE NOT ANALYSED WITHIN THE HOLDING TIME SPECW Flt&OR�rhi�.METHOD USED (SEE 94. BELOW) MUST BE DISCARDED AND NEW SAMPLES COLLECTED. 2. Standard Method 3OMP for sample. preparation (mercury excluded): DO NOT FILTERIMETALS SAMPLES IN THE FIELD !!! tAfMied.-s&,�Ti Iles must be collected for metals, then field acidified with 5 ml concentrated nitric acid per liter of sample, and should be submitted to the lab within 24 hours. Sample preparation in the laboratory (extraction and filtration) must be completed within 72 hours of collection" 3. ANALYSES ARE TO BE MADE OF THE MOBILE CONSTITUENTS (DISSOLVED\AS WELL AS COLLOIDAL) IN THE GROUNDWATER, NOT THOSE THAT ARE A PART OF SEDIMENT ASSOCIATED WITH WELL CONSTRUCTION OR SAMPLING PROCEDURES. CHECK WITH YOUR LABORATORY ON PROPER PROCEDURES FOR SAMPLE COLLECTION AND PRESERVATION. 4. As per Title 15, North Carolina Administrative Code, Subchapter 2L, analytical procedures shall be in accordance with the methods described in one of the following publications, or by other methods approved beforehand by the Diredtor, Division of Environmental Management: (a) Standard Methods for the Examination of Water and Wastewater, 16th Edition, 1985 and 17th Edition, 1989, published jointly by American Public Health Association, American Water Works Association and Water Pollution Control Federation; (b) Methods for Chemical Analysis of Water and Waste, 1979, U.S. Environmental Protection Agency publication number EPA-600/4-79-020, as, revised March 1983; (c) Test Methods for Evaluating Solid Wastes: Physical/Chemical Methods, 3rd Edition, 1986, U.S. Environmental Protection Agency publication number SW-846; (d) Test Procedures for the Analysis of Polluants Under the Clean Water Act, Federal Register Vol. 49, No. 209, 40 CFR Part 136, October 26, 1984; 5. Measure and record the depth of water in the well prior to pumping or bailing any water from the well. 6. At least 3 volumes of water in the well should be,pumped or bailed prior to collecting a sample for analysis. If the well is pumped/bailed dry before 3 well volumes are removed, samples can be collected as soon as the well recovers to the point where enough water is available to collect your sample. 7. Determination for pH, Specific Conductance, temperature ,'odor and appearance must be made in the field on unfiltered samples when the sample is collected. 8. Field equipment must be calibrated in accordance with recommendations by the manufacturer. 9. Samples must be filtered through a 0.45 micron filter immediately after collection when a dissolved analysis is required. (See #4. above) 10.The sample container should be labeled at the time of collection with the facility name, well identification number and date and time collected. 11."Authorized agent" is any corporate officer or public official authorized by the company, corporation, or governmental body to sign official documents. I ype or use a ban -point pen and press firmly. Facility Name N r/o-4L ZVEC_"A"IC AL C-AQAna Address Well Location PERMIT NUMBER: (REQUIRED) Non -Discharge NPDES 00 O 47 TYPE OF-DISPOSPL OPERATION BEING MONITORED (REQUIRED) Well Identification Number W -1 Well Depth Z o Ft. Well Diameter Z" Sample (Screened) Interval / SS Ft. To 70Ft. Depth to Water Level — ✓ 3 ft. below measuring point (before sampling) Measuring point is '3 ft. above land surface Gallons of water pumped/bailed before sampling Z , Z o A Ls Field Analysis: pH 5.1 Specific Conductance uMhos Temp. /Z oC Odor Date Sample Collected /2-3-9L Date Lab Sample Analyzed /Z-3-76 7-/2-/o-96 C, Lagoon Spray Field Land Application of Rotary Distributor < Appearance Laboratory Name NylpoNMEruT I Certification No. In SAMPLES FOR METALS WERE COLLECTED UNFILTERED AND FIELD ACIDIFIED YES NO COD / z mg/I Coliform: MF Fecal /100m] Coliform: MF Total /100ml (Note: Use MPN method for highly turbid samples) Dissolved Solids: Total 6o mg/I pH (when analyzed) units TOO 2 - C1 mg/I Chloride 8 mg/I Arsenic mgA Grease and Oils mg/I Hardness: Total mg/I Phenol mg/I Sulfate mg/I Specific Conductance 76 uMhos Total Ammonia mg/I TKN as N mg/I Nitrite (NO2) as N Nitrate (NO3) as N Phosphorus: Total AI - Aluminum Ba - Barium Ca - Calcium_ Cd - Cadmium_ Chromium: Total _ Cu - Copper Fe - Iron Hg - Mercury_ K - Potassium Mg - Magnesium _ Mn - Manganese _ Na - Sodium as P mg/I E/I g/I mg/I mg/I mg/I mg/I mg/I Septic Tank/Drain Field Subsurface Low -Pressure Piping (LPP) Other Ni - Nickel mg/I Pb - Lead mg/I Zn - Zinc C'j mg/I Pesticides/Herbicides a; (Specify Compounds) o a)%? m r,. ug/I N r j ug/I ug/I nos and �O M II �� I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE. Note: Values should reflect dissolved and colloidal concentrations. (see #3 on back) Icy �AbFJ�7) 1 Z1/I7 /`j�, See back for instructions. Signature of Permittee ( Authorized Agent') Date " Submit blue, green, and yellow copies only to address above. GW-59 REV. 6/93 COLLECTION AND ANALYSIS OF GROUNDWATER SAMPLES 1. Samples should be analyzed as soon as possible after collection. SAMPLES WHICH ARE NOT ANALYSED WITHIN THE HOLDING TIME SPEC` FIED FOR THE METHOD USED (SEE #4. BELOW) MUST BE DISCARDED AND NEW SAMPLES COLLECTED, 2. Metals Analyses: Use Standard Method 3030C for sample preparation (mercury excluded). DO NOT FILTER METALS SAMPLES IN THE FIELD !!! Unfiltered samples must be collected for metals, then field acidified with 5 ml concentrated nitric acid per liter of sample, and should be submitted to the lab within 24 hours. , Sample preparation in the laboratory (extraction and filtration) must be completed within 72 hours of collection. 3. ANALYSES ARE TO BE MADE OF THE MOBILE CONSTITUENTS (DISSOLVED AS WELL AS COLLOIDAL) IN THE GROUNDWATER, NOT THOSE THAT ARE A PART OF SEDIMENT ASSOCIATED WITH WELL CONSTRUCTION OR SAMPLING PROCEDURES. CHECK WITH YOUR LABORATORY ON PROPER PROCEDURES FOR SAMPLE COLLECTION AND PRESERVATION. 4. As per Title 15, North Carolina Administrative Code, Subchapter 2L, analytical procedures shall be in accordance with the methods described in one of the following publications, or by other methods approved beforehand by the Director, Division of Environmental Management: (a) Standard Methods for the Examination of Water and Wastewater, 16th Edition, 1985 and 17th Edition, 1989, published jointly by American Public Health Association, American Water Works Association and Water Pollution Control Federation; (b) Methods for Chemical Analysis of Water and Waste, 1979, U.S. Environmental Protection Agency publication number EPA-600/4-79-020, as revised March 1983; (c) Test Methods for Evaluating Solid Wastes: Physical/Chemical Methods, 3rd Edition, 1986, U.S. Environmental Protection Agency publication number SW-846; (d) Test Procedures for the Analysis of Polluants Under the Clean Water Act, Federal Register Vol. 49, No. 209, 40 CFR Part 136, t ; October 26, 1984; 5. Measure rand record the depth of water in the well prior to pumping or bailing any water from the well. 6. At least 3youlumes of water in the well should be pumped or bailed prior to collecting a sample for analysis. If the well is pumped/bailed dry before 3 well volumes ire removed, samples can be collected as soon as the well recovers to the point where enough water is available to collect your sample. 7. Determination for pH, Specifictonductance, temperature, odor and appearance must be made in the field on unfiltered samples when the sample is collected. , 8. Field equipment must be calibrated in accordance with recommendations by the manufacturer. 9. Samples must be filtered through a 0.45 micron filter immediately after collection when a dissolved analysis is required. (See #4. above) 10.The sample container should be labeled at the time of collection with the facility name, well identification number and date and time collected. 11. "Authorized agent' is any corporate officer or public official authorized by the company, corporation, or governmental body to sign official documents: Type or use a ball-point pen and press firmly. Facility NamL-WATrorusm- I P_CNAN CAARbw Address. -SO'-t Al. AsHi Ave County IfaQNE.TT Well Location PERMIT NUMBER: (REQUIRED) Non -Discharge NPDES AIC_ 00(,07W7 TYPE OF DISPOSAI OPERATION BEING MONITORED (REQUIRED) Well Identification Number - W ,1L Well Depth -L5Ft. Well Diameter Z Sample (Screened) Interval Ft. To Z 9' Ft. Depth to Water Level S ft. below measuring point (before sampling) Measuring point is Z ft, above land surface Gallons of water pumped/bailed before sampling 2. , 7- Field Analysis: pH 5, 1 Specific Conductance uMhos Temp. /6 oC Odor Date Sample Collected 8 - 9- 9 (o Date Lab Sample Analyzed S- *9 - 9 (. Laboratory Name_FNV I QnrJrg£N-rAL I Certification No. SAMPLES FOR METALS WERE COLLECTED UNFILTERED AND FIELD ACIDIFIED YES COD /79 mg/I Coliform: MF Fecal /100ml Coliform: MF Total /loom] (Note: Use MPN method for highly turbid samples) Dissolved Solids: Total 37 M mg/I pH (when analyzed) 0=2 units TOC y,36 mg/1 Chloride 7 mg/1 Arsenic mg/I Grease and Oils mg/I Hardness: Total mg/I Phenol mg/I Sulfate S mg/1 Specific Conductance 7C) uMhos Total Ammonia mg/l TKN as N mg/1 Lagoon Septic-rank/Drain Field Spray Field Subsurface Low -Pressure Piping (LPP) Land Application of Slud e Other Rota Distributor r ^ Rotary Appearance - Nitrite (NO2) as N mg/I Nitrate (NO3) as N Mr�l Phosphorus: Total as P IYtg/I AI - Aluminum mg/1 Ba - Barium mg/I Ca - Calcium mg/1 Cd - Cadmium mg/I Chromium: Total mg/1 Cu - Copper mg/1 Fe - Iron mg/I Hg - Mercury mg/I K - Potassium mg/I Mg - Magnesium mg/1 Mn - Manganese mg/I Na - Sodium mg/I NO Ni - Nickel mg/I Pb - Lead mg/I Zn - Zinc mg/I Pesticides/Herbicides Cn = �, (Specify Compounds) n �* -O ug/I ' �g/I Other (Specify Compounds and � Concentration units) - r'i in N 47 —r ,yam t99"o I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE. ENV. MANAGEMENT Note: VaItAMft Wt1Wfif!6(d),s%&ed and colloidal concentrations. (see #3 on back) -9 (, See back for instructions. Signa ure of Permittee ( r Authorized Agent') Date •• Submit blue, green, and yellow copies only to address above. GW-59 REV. 6/93 11,w COLLECTION AND ANALYSIS OF GROUNDWATER SAMPLES 1. Samples should be analyzed as soon as possible after collection. SAMPLES WHICH ARE NOT ANALYSED WITHIN THE HOLDING TIME SPECI- FIED FOR THE METHOD USED (SEE #4. BELOW) MUST BE DISCARDED AND NEW SAMPLES COLLECTED. 2. Metals Analyses: Use Standard Method 3030C for sample preparation (mercury excluded). DO NOT FILTER METALS SAMPLES IN THE FIELD !!! Unfiltered samples must be collected for metals, then field acidified with 5 ml concentrated nitric acid per liter of sample, and should be submitted to the lab within 24 hours. Sample preparation in the laboratory (extraction and filtration) must be completed within 72 hours of collection. 3. ANALYSES ARE TO BE MADE OF THE MOBILE CONSTITUENTS (DISSOLVED AS WELL AS COLLOIDAL) IN THE GROUNDWATER, NOT THOSE THAT ARE A PART OF SEDIMENT ASSOCIATED WITH WELL CONSTRUCTION OR SAMPLING PROCEDURES. CHECK WITH YOURIABORATORY ON PROPER PROCEDURES FOR SAMPLE COLLECTION AND PRESERVATION. 4. As per Title 15, North Carolina Administrative Code, Subchapter 2L, analytical procedures shall be in accordance with the methods described in one of the following publications, or by other methods approved beforehand by the Director, Division of Environmental Management: (a) Standard Methods for the Examination of Water and Wastewater, 16th Edition, 1985 and 17th Edition, 1989, published jointly by American Public Health Association, American Water Works Association and Water Pollution Control Federation; (b) Methods for Chemical Analysis of Water and Waste, 1979, U.S. Environmental Protection Agency publication number EPA-600/4-79-020, as revised March 1983; (c) Test Methods for Evaluating Solid Wastes: Physical/Chemical Methods, 3rd Edition, 1986, U.S. Environmental Protection Agency publication number SW-846; (d) Test Procedures for the Analysis of Polluants Under the Clean Water Act, Federal Regiaa Vol. 492 No. 209, 40 CFR Part 136, October 26, 1984; A,= 1 5. Measure and record the depth of water in the well prior to pumping or bailing any water from the well. 1 6. At least- 3 volumes of water in the well should be pumped or bailed prior to collecting a sample for analys& If the well is pumped/bailed dry before 3 well volumes are removed, samples can be collected as soon as the well recovers to the point where enough water is available to collect your sample. 7. Determination for pH, Specific Conductance, temperature, odor and appearance must be made in the field on unfiltered samples when the sample is collected. 8. Field equipment must be calibrated in accordance with recommendations by the manufacturer. 9. Samples must be filtered through a 0.45 micron filter immediately after collection when a dissolved analysis is required. (See #4. above) 10.The sample container should be labeled at the time of collection with the facility name, well identification number and date and time collected. 11. "Authorized agent" is any corporate officer or public official authorized by the company, corporation, or governmental body to sign official documents. Type or Use a ball-point pen and press firmly. Facility Name NRTionIAL GARh�6A/ Address 564 A), Asn-e Avr_. Well i PERMIT NUMBER: (REQUIRED) Non -Discharge NPDES NG DO 6t'%747 TYPE OF DISPOSAI OPERATION BEING MONITORED (REQUIRED) Well Identification Number W I Well Depth LO Ft. Well Diameteri" Sample (Screened) Interval / S Ft. To ZO Ft. Depth to Water Level eft. below measuring point (before sampling) Measuring point is 3 ft. above )and surface Gallons of water pumped/bailed before sampling 7_-. 7_ Field Analysis: pH 5 O . T Specific Conductance uMhos Temp. / 6 oC Odor Date Sample Collected L Date Lab Sample Analyzed $/RL9 L Lagoon Septic Tank/Drain Field Spray Field Subsurface Low -Pressure Piping (LPP) Land Application of Sludge X other RotarRota Distributor ' ` y �ersi .0 ri_ c Yni .......... Y Appearance Laboratory Name f v vim aR,M e, . T / Certification No. �0 SAMPLES FOR METALS WERE COLLECTED UNFILTERED AND FIELD ACIDIFIED YES NO COD %$ mg/I Coliform: MF Fecal A 00ml Coliform: MF Total /100ml (Note: Use MPN method for highly turbid samples) Dissolved Solids: Total ZO mg/I pH (when analyzed) units TOC Z • 3 mg/1 Chloride ] mg/I Arsenic mg/I Grease and Oils mg/1 Hardness: Total mg/I Phenol mg/I Sulfate 5, /o mg/1 Specific Conductance 70 uMhos Total Ammonia mg/l TKN as N mg/I Nitrite (NO2) as N mg/I Ni - Nickel "il mg/I Nitrate (NO3) as N rtlg/I Pb - Lead On 'r mg/l Phosphorus: Total as P I'41g/1 Zn - Zinc "' mg/I Al - Aluminum mg/I Pesticides/Herbicides Ba Barium mg/I (Specify Compounds) Ca - Calcium mg/1 ism ug/I Cd - Cadmium mg/I = rT ug/I Chromium: Total mg/I -- � ug/I Cu - Copper mg/I Other (Specify Compounds and cn Fe - Iron mg/I Concentration units) Hg - Mercury mg/I K - Potassium mg/1 iE� rim rn t� Mg -Magnesium mg/I VA ""n1 e , Mn - Manganese mg/I Na - Sodium mg/I 9P 9-93T PP FTr��t tl r I CERTIFY THAT THIS REPO TRUE AND ACCURATE. Note: ValuesAsFio(1�IvvtCil{�YAUtIAEHift&ed and colloidal concentrations. (see #3 on back) R11vT 3 q See back for instructions. Signature of Permittee (o A thorized Agent') Date " Submit blue, green, and yellow copies only to address above. GW-59 REV. 6/93 b \ .f 1. Samples should be analyzed as soon as poslible after collection. SAMPLES WHICH ARE NOT ANALYSED WITHIN THE HOLDING TIME SPECI- FIED FOR THE METHOD USED (SEE #4. BELOW) MUST BE DISCARDED AND NEW SAMPLES COLLECTED. 2. Metals Analyses: Use Standard Method 3030C for sample preparation (mercury excluded). DO NOT FILTER METALS SAMPLES IN THE FIELD !!! Unfiltered samples must be collected for metals, then field acidified with 5 ml concentrated nitric acid per liter of sample, and should be submitted to the lab within 24 hours. Sample preparation in the laboratory (extraction and filtration) must be completed within 72 hours of collection. 3. ANALYSES ARE TO BE MADE OF THE MOBILE CONSTITUENTS (DISSOLVED AS WELL AS COLLOIDAL) IN THE GROUNDWATER, NOT THOSE THAT ARE A PART OF SEDIMENT ASSOCIATED WITH WELL CONSTRUCTION OR SAMPLING PROCEDURES. CHECK WITH YOUR LABORATORY ON PROPER PROCEDURES FOR SAMPLE COLLECTION AND PRESERVATION. 4. As per Title 15, North Carolina Administrative Code, Subchapter 2L, analytical procedures shall be in accordance with the methods described in one of the following publications, or by other methods approved beforehand by the Director, Division of Environmental Management: (a) Standard Methods for the Examination of Water and Wastewater, 16th Edition, 1985 and 17th Edition, 1989, published jointly by American Public Health Association, American Water Works Association and Water Pollution Control Federation; (b) Methods for Chemical Analysis of Water and Waste, 1979, U.S. Environmental Protection Agency publication number EPA-60014-79-020, as revised March 1983; (c) Test Methods for Evaluating Solid Wastes: Physical/Chemical Methods, 3rd Edition, 1986, U.S. Environmental Protection Agency publication number SW-846; (d) Test Procedures for the Analysis of Polluants Under the Clean Water Act, Federal Register Vol. 49, No. 209, 40 CFR Part 136, October 26, 1984; 5. Measure and record the depth of water in the well prior to pumping or bailing any water from the well. 6. At least 3 volumes of water in the well should be pumped or bailed prior to collecting a sample for analysis. If the well is pumped/bailed dry before 3 well volumes are removed, samples can be collected as soon as the well recovers to the point where enough water is available to collect your sample. 7. Determination for pH, Specific Conductance, temperature, odor and appearance must be made in the field on unfiltered samples when the sample is collected. 8. Field equipment must be calibrated in accordance with recommendations by the manufacturer. 9. Samples must be filtered through a 0.45 micron filter immediately after collection when a dissolved analysis is required. (See #4. above) 10.The sample container should be labeled at the time of collection with the facility name, well identification number and date and time collected. 11 ."Authorized agent" is any corporate officer or public official authorized by the company, corporation, or governmental body to sign official documents. a t'4 /1): A ✓MV or Facility Name Address Well Location PERMIT NUMBER: (REQUIRED) Non -Discharge NPDES NC_ 006075V7 TYPE OF DISPOSAL OPERATION BEING MONITORED (REQUIRED) Lagoon Well Identification Number W ) Well Depth Z0 Ft. Well Diameter 2'� Sample (Screened) Interval J 5'— Ft. To Z o Ft. Spray Field pen and press County J4AR1,1FT7' Septic Tank/Drain Field Subsurface Low -Pressure Piping (LPP) Depth to Water Level Oft. below measuring point (before sampling) Land Application of Sludge Measuring point is 3 ft. above land surface _ X Other Gallons of water pumpedibailed before sampling Z - 14 Rotary Distributor SeTTGwG Field Analysis: pH 5. 3 Specific Conductance - uMhos Temp. / y oC Odor - Appearance - Date Sample Collected y�/o �9 � Date Lab Sample Analyzed `/�/f LaboratoryName 14T Z L Certification No. 33 Z / Z G3 SAMPLES FOR METALS WERE COLLECTED UNFILTERED AND FIELD ACIDIFIED �Y NO COD I S mg/I Nitrite (NO2) as � %ig/I Ni - Nickel mg/I Coliform: MF Fecal /100ml Nitrate (NO rfrg/I Pb - Lead - mg/I Coliform: MF Total A 00ml n_1 Phosphoru s rtng/I Zn - ZincP mg/I (Note: Use MPN method for highly turbid samples) AI-Alurriinu mg/ly Pesticides/Herbicides --- . Dissolved Solids: Total y5/ mg/I Ba - BaridRi nF g/t.• ; (Specify Compounds) < :,r: <�� pH (when analyzed) units Ca - Calcium z� mg/f � — - ug/I TOC /. N mg/I Cd - Cadmium" `cr mgA or', ug/I Chloride S' mg/1 Chromium: Tot mg/I ug/I Arsenic mg/I Cu -Copper ':• mg/I Other (Specify Compounds and _ Grease and Oils mg/I Fe - Iron `�. - " mg/I Concentration units) G,=� Hardness: Total mg/I Hg - Mercury mg/I N n; Phenol mgA K - Potassium mg/I ` Sulfate 12- mgA Mg - Magnesium mgA Specific Conductance lo`% uMhos Mn - Manganese mgA Total Ammonia mg/1 Na - Sodium mg/1 TKN as N mg/I I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE. LrvT S-/5-%% Signature of Permittee (49r Authorized Agent*) Date GW-59 REV. 6/93 Note: Values should reflect dissolved and colloidal concentrations. (see #3 on back) ' See back for instructions. 1' " Submit blue, green, and yellow copies only to address abov- i i COLLECTION AND ANALYSIS OF GROUNDWATER SAMPLES 1. Samples should be analyzed as soon as possible after collection. SAMPLES WHICH ARE NOT ANALYSED WITHIN THE HOLDING TIME SPECI- FIED FOR THE METHOD USED (SEE #4. BELOW) MUST BE DISCARDED AND NEW SAMPLES COLLECTED. 2. Metals Analyses: Use Standard Method 3030.0 for sample preparation (mercury excluded). DO NOT FILTER METALS SAMPLES IN THE FIELD !!! Unfiltered samples must be collected for metals, then field acidified with 5 ml concentrated nitric acid per liter of sample, and should be submitted to the lab within 24 hours. Sample preparation in the laboratory (extraction and filtration) must be completed within 72 hours of collection. 3. ANALYSES ARE TO BE MADE OF THE MOBILE CONSTITUENTS (DISSOLVED AS WELL AS COLLOIDAL) IN THE GROUNDWATER, NDT THOSE THAT ARE A PART OF SEDIMENT ASSOCIATED WITH WELL CONSTRUCTION OR SAMPLING PROCEDURES. CHECK WITH YOUR LABORATORY ON PROPER PROCEDURES FOR SAMPLE COLLECTION AND PRESERVATION. -4. 4. As per Title 15, North Carolina Administrative Bode, Subchapter 2L, analytical procedures shall be in accordance with the methods described in one of the following publications, or by other methods approved beforehand by the Director, Division of Environmental Management: (a) Standard Methods for the Examination of Water and Wastewater, 16th Edition, 1985 and 17th Edition, 1989, published jointly by American Public Health Association, American Water Works Association and Water Pollution Control Federation; (b) Methods for Chemical Analysis of Water and Waste, 1979, U.S. Environmental Protection Agency publication number EPA-600/4-79-020, as revised March 1983: (c) Test Methods for Evaluating Solid Wastes: Physical/Chemical Methods, 3rd Edition, 1986, U.S. Environmental Protection Agency publication number SW-846; (d) Test Procedures for the Analysis of Polluants Under the Clean Water Act, Federal Register Vol. 49. No. 209, 40 CFR Part 136, October 26, 1984; 5. Measure ai�d record the depth of water in the well prior to pumping or bailing any water from the well. 6. At least 3 volumes of water in the well should be pumped or bailed prior to collecting a sample for analysis. If the well is pumped/bailed dry before 3 well volumes are removed, samples can be collected as soon as the well recovers to the point where enough water is available to collect your sample. 7. Determination for pH, Specific Conductance, temperature, odor and appearance must be made in the field on unfiltered samples when the sample is collected. 8. Field equipment must be calibrated in accordance with recommendations by the manufacturer. 9. Samples must be filtered through a 0.45 micron filter immediately after collection when a dissolved analysis is required. (See #4. above) 10:The sample container should be labeled at the time of collection with the facility name, well identification number and date and time collected. 11. "Authorized agent" is any corporate officer or public official authorized by the company, corporation, or governmental body to sign official documents. Facility Name Address Type or Use a ball-point pen and press firmly. PERMIT NUMBER: (REQUIRED) Non -Discharge NPDES /VG 0n1_n7Y7 TYPE OF DISPOSAL OPERATION BEING MONITORED Well Location�-rAu.vr fe Yeusrarrv� Yar.rr> (REQUIRED) Lagoon Well Identification Number w M Well Depth Jr 8 Ft. Spray Field Well Diameter 7-Sample (Screened) Interval 16 Ft. To !8 Ft. Depth to Water Level _T ft. below measuring point (before sampling) Land Application of Sludge Measuring point is 2- ftabove land surface A Gallons of water pumped/bailed before sampling Z. Y Rotary Distributor Field Analysis: pH S. 3 Specific Conductance uMhos Temp. 14f °C Odor — Appearance Date Sample Collected Y 1I0 A& Date Lab Sample Analyzed Y {tf /94 Laboratory Name ATC L Certification No. z ry S SAMPLES FOR METALS WERE COLLECTED UNFILTERED AND FIELD ACIDIFIED YES NO COD Coliform: MF Fecal Coliform: MF Total R (Note: Use MPN method for highly turbid samples) _ mg/1 /100ml /100ml Dissolved Solids: Total 39 mgA pH (when analyzed) units TOC mg/I Chloride R mgA Arsenic mgA Grease and Oils mg/I Hardness: Total mg/I Phenol mg/1 Nitrite (NO2) as N mg/I Nitrate (NO3) as N rri�g/I 4/1 Phosphorus: Total as P AI - Aluminum mg/I Ba - Barium mg/I Ca - Calcium mg/I Cd - Cadmium mgA Chromium: Total mg/1 Cu - Copper mgA Fe - Iron mg/I Hg - Mercury mO/I K - Potassium mg/1 Ni- Nickel Pb - Lead Zn - Zinc Pesticides/Herbicides (Specify Compounds) Septic Tank/Drain Field Subsurface Low -Pressure Piping (LPP) Sulfate <j Z mgA Mg - Magnesium mg%I ��� Specific Conductance 4,6 uMhos Mn - Manganese mg%I"- Total Ammonia mgA Na - Sodium mg/1 e TKN as N mg/I mgA mgA mg/1 ug/I ug/1 ug/I I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE. Note: Values should reflect dissolved and l^• ) Q D /' \ colloidal concentrations. (see #3 on back) \_UAa.... ` • 1�JU^�' 1. Af+EW7 J S {S 9 See back for instructions. Signature of Permittee (of Authorized Agent`) Da a •* Submit blue, green, and yellow copies only to address above. GW-59 REV. 6/93 . r 1.9 COLLECTION AND ANALYSIS OF GROUNDWATER SAMPLES Samples should be analyzed as soon as possible after collection. SAMPLES WHICH ARE NOT ANALYSED WITHIN THE HOLDING TIME SPECI- FIED FOR THE METHOD USED (SEE #4. BELOW) MUST BE DISCARDED AND NEW SAMPLES COLLECTED. 2. Metals Analyses: Use Standard Method 3030C for sample preparation (mercury excluded). DO NOT FILTER METALS SAMPLES IN THE FIELD !tt Unfiltered samples must be collected for metals, then field acidified with 5 ml concentrated nitric acid per liter of sample, and should be submitted to the lab within 24 hours. Sample preparation in the laboratory (extraction and filtration) must be completed within 72 hours of collection. 3. ANALYSES ARE TO BE MADE OF THE MOBILE CONSTITUENTS (DISSOLVED AS WELL AS COLLOIDAL) IN THE GROUNDWATER, NOT THOSE THAT ARE A PART OF SEDIMENT ASSOCIATED WITH WELL CONSTRUCTION OR SAMPLING PROCEDURES. CHECK WITH YOUR LABORATORY ON PROPER PROCEDURES FOR SAMPLE COLLECTION AND PRESERVATION. 4. As per Title 15, North Carolina Administrative Code, Subchapter 2L, analytidal procedures shall be in accordance with the methods described in one of the following publications, or by other methods.approved beforehand by the Director, Division of Environmental Management: I k (a) Standard Methods for the Examination of Water and Wastewater, 16th Edition, 1985 and 17th Edition, 1989, published jointly by American Public Health Association, American Water Works Association and Water Pollution Control Federation; (b) Methods for Chemical Analysis of Water and Waste, 1979, U.S. Environmental Protection Agency publication number EPA-600/4-79-020, as revised March 1983; (c) Test Methods for Evaluating Solid Wastes:.Physical/Chemical Methods, 3rd Edition, 1986, U.S. Environmental Protection Agency publication number SW-846; (d) Test Procedures for the Analysis of Polluants Under the Clean Water Act, Federal Register, Vol. 49. No. 209, 40 CFR Part 136, October 26, 1984; 5. Measure and record the depth of water in the well prior to pumping or bailing any water from the well. 6. At least 3 volumes of water in the well should be pumped or bailed prior to collecting a sample for analysis. If the well is pumped/bailed dry before 3 well volumes afe removed, samples can be collected as soon as the well recovers to the point where enough water is available to collect your sample. 7. Determination for pH, Specific Conductance, temperature, odor and appearance must be made in the field on unfiltered samples when the sample is collected. ' S. Field equipment must be calibrated in accordance with recommendations by the manufacturer. 9. Samples must be filtered through a 0.45 micron filter immediately after collection when a dissolved analysis is required. (See #4. above) 10. The sample container should be labeled at the time of collection with the facility name, well identification number and date and time collected. 11. "Authorized agent" is any corporate officer or public official authorized by the company, corporation, or governmental body to sign official documents. �' c Type or Use a ball-point pen ano press firmly. p ' P RMIT NUMBER: (REQUIRED) Facility Name /✓ar'oAjAL- GLLCTAdcaL Cnn3ea '" �" 1 Non -Discharge Address - lS�oy N. srcc Avr ' J n6 ✓ NPDES A/C 00�07Y'7 diLINN NG 28334 County I+Aarvar-r p�� OPERATION BEING MONITORED Well Location A oLc u t ' IRED) QE > Lagoon Septic Tank/Drain Field Well Identification Number W Well Depth g Ft. EG\ Well Diameter —Sample (Screened) Interval / o Ft. To �F`E\G\' Y Spray Field Subsurface ' ow -Pressure Depth to Water Level 9 ft. below measuring point (before sampling NNR Measuring point is Z ft. above land surface QE Gallons of water pumped/bailed before sampling 3. Field Analysis: pH -S • 5 Specific Conductance - uMhos Temp. 15 oC Date Sample Collected /2 - Zo - `I S Date Lab Sample Analyzed I' 9. `n LaboratoryName AquA- Tee.a SAMPLES FOR METALS WERE COLLECTED UNFILTERED AND FIELD ACIDIFIED Land Application of Slud e ML Rotary Distributor SdrT Odor Appearance Certification No. 332 2 & 3 YES NO Other G [ %�cus Aw �o v COD < r 5 mg/I Nitrite (NO2) as N mg/I Ni - Nickel mg/I Coliform: MF Fecal /100ml Nitrate (NO3) as N rri�g/I Pb - Lead mg/I Coliform: MF Total /100ml Phosphorus: Total as P I'hg/I Zn - Zinc mg/I (Note: Use MPN method for highly turbid samples) AI -Aluminum mg/I Pesticides/Herbicides Dissolved Solids: Total y'a mg/I Ba - Barium mg/I (Specify Compounds) oC� pH (when analyzed) units Ca - Calcium mg/I ter= ug/I TOC < f mg/I Cd -Cadmium mgll r't EJM ug/1 Chloride mg/I Chromium: Total mg/I ug/I Arsenic mg/I Cu - Copper rng,/I Other (Specify Compounds and = n= Grease and Oils mg/I Fe - Iron m6'11 Concentration units) Hardness: Total mg/I Hg - Mercury mn 9 - m Phenol mg/I K - Potassium na I" mg/I Sulfate I Z mg/I Mg - Magnesium ' -,mg/I Specific Conductance v uMhos Mn - Manganese FE mg/1 Total Ammonia mg/I Na - Sodium •;;�r�tg/I TKN as N mg/I Vt 41� _ �rrT^r-if7t I ERao.OFFICE r I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE. Note: Values should reflect dissolved and Q colloidal concentrations. (see #3 on back) Ar.✓ �IQCrENT . ! - Z Z - (o See back for instructions. lgnature of Perm' ee (or Authorized Agent`) Date " Submit blue, green, and yellow copies only to address above. GW-59 REV. 6/93 COLLECTION AND ANALYSIS OF GROUNDWATER SAMPLES •7 1. Samples should be analyzed as soon as possible after collectipfS. SAMPLES WHICH ARE NOT ANALYSED WITHIN THE HOLDING TIME SPILCI- FIED FOR THE METHOD USED (SEE #4. BELOW) MUST BE-61SCA-RDED AND NEW SAMPLES COLLECTED. 2. Metals Analyses: Use Standard Method 3030C for sample preparation (mercury excluded). DO NOT FILTER METALS SAMPLES IN THE FIELD !!! Unfiltered samples must be collected for metals, then field acidified with 5 ml concentrated nitric acid per liter of sample, and should be submitted to the lab within 24 hours. Sample preparation in the laboratory (extraction and filtration) must be completed within 72 hours of collection. 3. ANALYSES ARE TO BE MADE OF THE MOBILE CONSTITUENTS (DISSOLVED AS WELL AS COLLOIDAL) IN THE GROUNDWATER, NOT THOSE THAT ARE A PART OF SEDIMENT ASSOCIATED WITH WELL CONSTRUCTION OR SAMPLING PROCEDURES. CHECK WITH YOUR LABORATORY ON PROPER PROCEDURES FOR SAMPLE COLLECTION AND PRESERVATION. 4. As per Title 15, North Carolina Administrative Code, Subchapter 2L, analytical procedures shall be in accordance with the methods described in one of the following publications. or by other methods approved beforehand by the Director, Division of Environmental Management: (a) Standard Methods for the Examination of Water and Wastewater, 16th Edition, 1985 and 17th Edition, 1989, published jointly by American Public Health Association, American Water Works Association and Water Pollution Control Federation; (b) Methods for Chemical Analysis of Water and Waste, 1979, U.S. Environmental Protection Agency publication number EPA-600/4-79-020, as revised March 1983; (c) Test Methods for Evaluating Solid Wastes: Physical/Chemical Methods, 3rd Edition, 1986, U.S. Environmental Protection Agency publication number SW-846; (d) Test Procedures for the Analysis of Polluants Under the Clean Water Act, Federal Register Vol. 49. No. 209, 40 CFR Part 136, October 26, 1984; 5. Measure and record the depth of water in the well prior to pumping or bailing any water from the well. 6. At least 3 volumes of water in the well should be pumped or bailed prior to collecting a sample for analysis. If the well is pumped/bailed dry before 3 well volumes ark removed, samples can be collected as soon as the well recovers to the point where enough water is available to collect your sample. Determination for pH, Specific Conductance, temperature, odor and appearance must be made in the field on unfiltered samples when the sample is collected. 8. Field equipment must be calibrated in accordance with recommendations by the manufacturer. 9. Samples must be filtered through a 0.45 micron filter immediately after collection when a dissolved analysis is required. (See #4. above) 10.The sample container should be labeled at the time of collection with the facility name, well identification number and date and time collected. 11. "Authorized agent" is any corporate officer or public official authorized by the company, corporation, or governmental body to sign official documents. Type or Use a ball-point pen and press firmly. FacilityName IVAUotuAL (fLECTRICRL GAAaOhr Address 50`/ N. AsnL Avz. PERMIT NUMBER: (REQUIRED) Non -Discharge NPDES _ A/C 0060 7,Y 7 TYPE OF DISPOSAL OPERATION BEING MONITORED Well Location ISLTWKeA/ 5ErTL/NG 1-0"D ! LoLISNWb jjb"o (REQUIRED) Lagoon Well Identification Number w I Well Depth Z o Ft. Well Diameter 7- " Sample (Screened) Interval / S Ft. To Z. b Ft. spray Field Septic Tank/Drain Field Subsurface Low -Pressure Piping (LPP) Depth to Water Level f I ft. below measuring point (before sampling) Land Application of Stud e Other Measuring point is 3 ft. above land surface Rotary Distributor SL7YLlNL r Gallons of water pumped/bailed before sampling Z. 6 Field Analysis: pH S• 4- Specific Conductance - uMhos Temp. 1.5 oC Odor _ Appearance - Date Sample Collected / Z - Z 6- 45 Date Lab Sample Analyzed / - S - 9 ro Laboratory Name - Aq u A - 'Teu, Certification No. 337 Z b3 SAMPLES FOR METALS WERE COLLECTED UNFILTERED AND FIELD ACIDIFIED YES NO COD < ► mg/I Coliform: MF Fecal /100ml Coliform: MF Total /100ml (Note: Use MPN method for highly turbid samples) Dissolved Solids: Total 9N mg/I pH (when analyzed) units TOC J • t mg/I Chloride 8• s' mg/I Arsenic mg/I Grease and Oils mg/I Hardness: Total mg/I Phenol mg/I Sulfate < f z- mg/I Specific Conductance 66 uMhos Total Ammonia mg/I TKN as N mg/I Nitrite (NO2) as N mg/I Nitrate (NO3) as N rri�g/I Phosphorus: Total as P A/I AI - Aluminum mg/I Ba - Barium mg/I Ca - Calcium mg/I Cd - Cadmium mg/I Chromium: Total mg/1 Cu - Copper mg/I Fe - Iron mg/I Hg - Mercury K - Potassium Tr�"' ' mg/I Mg - Magnesium v `mg/I Mn - Manganese YL�"�� mg/I Na - Sodium ' mgll �., I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE. Fa'ljTNote Signature of Permi ee (or Authorized Agent') Ni - Nickel Pb - Lead mg/I civmg/I Zn - Zinc Pesticides/Herbicides (Specify Compounds) "p o _mg/I 7- c �rm1g/I Other (Specify Compounds and Concentration units) ug/I r Values should reflect dissolved and colloidal concentrations. (see #3 on back) See back for instructions. Date *' Submit blue, green, and yellow copies only to address above. GW-59 REV. 6/93 COLLECTION AND ANALYSIS OF GROUNDWATER SAMPLES i. Samples should be analyzed as soon as possible after collection. SAMPLES WHICH ARE NOT ANALYSED WITHIN THE HOLDING TIME SPEL[- FIED FOR THE METHOD USED (SEE #4. BELOW) MUST BE DISCARDED AND NEW SAMPLES COLLECTED. 2. Metals Analyses: Use Standard Method 3030C for sample preparation (mercury excluded). DO NOT FILTER METALS SAMPLES INTHE FIELD M Unfiltered samples must bd collected for metals, then field acidified with 5 ml concentrated nitric acid per liter of sample, and should be submitted to the lab within 24 hours. Sample preparation in the laboratory (extraction and filtration) must be completed within 72 hours of collection. 3. ANALYSES ARE TO BE MADE OF THE MOBILE CONSTITUENTS (DISSOLVED AS WELL AS COLLOIDAL) IN THE GROUNDWATER, N T THOSE THAT ARE A PART OF SEDIMENT ASSOCIATED WITH WELL CONSTRUCTION OR SAMPLING PROCEDURES. CHECK WITH YOUR LABORATORY ON PROPER PROCEDURES FOR SAMPLE COLLECTION AND PRESERVATION. 4. As per Title 15, North Carolina Administkative Code, Subchapter 2L, analytical procedures shall be in accordance with the methods described in one of the following publications, or by other methods approved beforehand by the Director, Division of Environmental Management: 11 (a) Standard Methods for the Examination of Water and Wastewater, 16th Edition, 1985 and 17th Edition, 1989, published jointly by American Public Health Association, American Water Works Association and Water Pollution Control Federation; • (b) Methods for Chemical Analysis of Water and Waste, 1979, U.S. Environmental Protection Agency publication number EPA-600/4-79-020, as revised March 1983; (c) Test Methods for Evaluating Solid Wastes: Physical/Chemical Methods, 3rd Edition, 1986, U.S. Environmental Protection Agency publication number'SW-846; (d) Test Procedures for the Analysis of Polluants Under the Clean Water Act, Federal Register Vol. 49, No. 209, 40 CFR Part 136, October 26, 1984; 5. Measure and record the depth of water in the well prior to pumping or bailing any water from the well. 6. At feast 3 volumes of water in the well should be pumped or bailed prior to collecting a sample for analysis. If the well is pumped/bailed dry before 3 well volumes are removed, samples can be collected as soon as the well recovers to the point where enough water is available to collect your sample. 7. Determination for pH, Specific Conductance, temperature, odor and appearance must be made in the field on unfiltered samples when the sample is collected. 8. Field equipment must be calibrated in accordance with recommendations by the manufacturer. 9. Samples must be filtered through a 0.45 micron filter immediately after collection when a dissolved analysis is required. (See #4. above) 10.The sample container should be labeled at the time of collection with the facility name, well identification number and date and time collected. ti , 11. "Authorized agent" is any corporate officer or public official authorized by the company, corporation, or governmental body to sign official documents. x Type or Use a ball-point pen and press firmly. Facility NameA447/oNFiL CgAl3ory Address-504 /V. A.SHL Ave. Well Location PERMIT NUMBER: (REQUIRED) Non -Discharge NPDES /�/ C do 6 c, -74 7 TYPE OF DISPOSAL OPERATION BEING MONITORED (REQUIRED) Well Identification Number \n1 717 Well Depth /F Ft. Well Diameter Z Sample (Screened) Interval / 7- Ft. To / 8 Ft. Depth to Water Level Ll ft. below measuring point (before sampling) Measuring point is Z ft. above land surface Gallons of water pumped/bailed before sampling 3 Field Analysis: pH S. 4. Specific Conductance uMhos Temp. / 6 oC Odor Date Sample Collected 8-IG 9S Date Lab Sample Analyzed F-f 7 - 8-29/9Y- Lagoon Septic TanklDrain Field Spray Field Subsurface Low -Pressure Piping (LPP) Land Applica6t of Sludge /' X/ Other Rotary Distributor Appearance - Laboratory NameAQU A- TCCH Certification No. 3 3 2 1 Z c, 3 SAMPLES FOR METALS WERE COLLECTED UNFILTERED AND FIELD ACIDIFIED YES NO SEP 2 8 1995 D. E M. COD < / s mg/I Nitrite (NO2) as N mgA Ni - Nicke L _ mgA Coliform: MF Fecal /100ml Nitrate (NO3) as N rYLg/I Pb - Lead mgA Coliform: MF Total /100ml Phosphorus: Total as P g/1 Zn - Zinc mgA (Note: Use WIN method for highly turbid samples) AI - Aluminum mg/I Pesticides/Herbicides Dissolved Solids: Total 6 `! mg/I Ba - Barium mgA (Specify Compounds) �0 y pH (when analyzed) units Ca - Calcium mg/I rn -' ug/I TOC 3.9 mgA Cd - Cadmium mg/I Chloride 9• Z mgA Chromium: Total mg/I Arsenic mg/I Cu - Copper mgA Other (Specify Compounds and w Grease and Oils mg/I Fe - Iron mg/I Concentration units) -=C Hardness: Total mg/I Hg - Mercury mgA Phenol mgA K - Potassium mg/I ,m g i� p = Sulfate < /O mg/I Mg - Magnesium mgA . h Specific Conductance / 0 uMhos Mn - Manganese mgA Total Ammonia mgA Na - Sodium mg/I gar A olrJ TKN as N mgA I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE. �ir Note gT;&�RE OFFICE) re ect dissolved and /n1 - 16olloidal concentrations. (see #3 on back) �rCrGn/T WW_1 See back for instructions. ;igiature of Permitte r Authorized Agent*) Date * Submit blue, green, and yellow copies only to address above. GW-59 REV. 6/93 COLLECTION AND ANALYSIS OF GROUNDWATER SAMPLES 1. Samples should be analyzed as soon as possible after collection. SAMPLES WHICH ARE NOT ANALYSED WITHIN THE HOLDING TIME SPECI- FIED FOR THE METHOD USED (SEE #4. BELOW) MUST BE DISCARDED AND NEW SAMPLES COLLECTED. ' 2. Metals Analyses: Use Standard Method 3030C for sample preparation (mercury excluded). 'DO NOT FILTER METALS SAMPLES IN THE FIELD fft Unfiltered samples must be collected for metals, then field acidified with 5 ml concentrated nitric acid per 4iter of sample, and should be submitted to the lab within 24 hours. I• . Sample preparation in the laboratory (extraction and filtration) must be completed within 72 hours of collection. 3. ANALYSES ARE TO BE MADE OF THE MOBILE CONSTITUENTS (DISSOLVED'AS WELL AS COLLOIDAL) IN THE GROUNDWATER, NOT THOSE THAT ARE A PART OF SEDIMENT ASSOCIATED WITH WELL CONSTRUCTION OR SAMPLING PROCEDURES. CHECK WITH YOUR LABORATORY ON PROPER PROCEDURES FOR SAMPLE COLLECTION AND PRESERVATION. 4. As per Title 15, North Carolina Administrative Code, Subchapter 2L, analytical procedures shall be in accordance with the methods'described in one of the following publications, or by other methods approved beforehand by the'Director, Division of Environmental Management: I (a) Standard Methods for tiie Examination of Water and Wastewater, 16th Edition, 1985 and 17th Edition, 1989, published jointly by American Public Health Association, American Water Works Association and Water Pollution Control Federation; (b) Methods for Chemical Analysis of Water and Waste, 1979, U.S. Environmental Protection Agency publication number EPA-600/4-79-020, as revised March 1983; (c) Test Methods for Evaluating Solid Wastes: Physical 'chemical Methods, 3rd Edition, 1986, U.S. Environmental Protection Agency publication number SW-846; (d) Test Procedures for the Analysis of Polivants Under the Clean Water Act, Federal Register Vol. 49, No. 209, 40 CFR Part-136, October 26, 1984; 5. Measure and record the depth of water in the well prior to pumping or bailing any water from the well. 6. At least 3•volumes of water in the well should be pumped or bailed prior to collecting a sample for analysis. If the well is pumped/bailed dry before 3 well volumes are removed, samples.oan be collected as soon as the well recovers to the point where enough,water is available to collect your sample. 7. Determination for pH, Spacific Conductance, temperature, odor and appearance must be made in the field on unfiltered samples when the sample is collected. 8. Field equipment must be calibrated in accordance with recommendations by the manufacturer. 9. Samples must be filtefdd through a 0.45 micron filter immediately after collection when a dissolved analysis is required. (See #4. above) 10.The sample container should be labeled at thd'time of collection with the facility name, well identification number and date and time collected. 11. "Authorized agent' is any corporate officer or public official authori2ed'by the company, corporation, or governmental body to sign official documents. Type or Use a ball-point pen and press firmly. PERMIT NUMBER: (REQUIRED) Facility Name A1A7*1otvA1_ ELzc_'TRtcAL CAAAe.y Non -Discharge Address SC'y Al- ASH£ ACE. NPDES A/C 00 (,)74t7 )7un,N, n1 G 7-19 y County IIAAn/ETT TYPE OF DISPOSAL OPERATION BEING MONITORED S (REQUIRED) Well Location ArwcL L7 llycG onp a ocrssiiMC_ o"o Well Identification Number VJ .I Well Depth Z o Ft. Well Diameter Z" Sample (Screened) Interval 15 Ft. To Z a Ft. Depth to Water Level eft. below measuring point (before sampling) Measuring point is 3 ft. above land surface Gallons of water pumped/bailed before sampling _ 3 Field Analysis: pH 5. 3 Specific Conductance uMhos Temp. C Odor — Date Sample Collected Date Lab Sample Analyzed T-r 7 - a'- Z Lagoon Septic Tank/Drain Field Spray Field Subsurface Low -Pressure Piping (LPP) Land Application of Sludge Other Rotary Distributor Srrrr ."f_ Appearance LaboratoryName AQuA- 7EGN Certification No. 33Z / Z 6 3 SAMPLES FOR METALS WERE COLLECTED UNFILTERED AND FIELD ACIDIFIED YES NO' c) rr. 40 1 u, COD _ < / s mg/I Nitrite (NO2) as N mg/I Ni -Nickel GJ C �=g/I Coliform: MF Fecal /100ml Nitrate (NO3) as N r}�g/I Pb - Lead :Jgmg/I Coliform: MF Total A 00ml Phosphorus: Total as P. I'4tg/1 Zn - Zinc r*t Tng/I (Note: Use MPN method for highly turbid samples) AI - Aluminum mg/I Pesticides/Herbicides _ Dissolved Solids: Total 53 mg/I Ba - Barium mg/I (Specify Compounds) r- r pH (when analyzed) units Ca - Calcium mgfl ug/I TOC < l . mg/I Cd - Cadmium mg/I ug/I Chloride % Z- mg/I Chromium: Total mg/I ug/I Arsenic mg/I Cu - Copper mg/I Other (Specify Compounds and Grease and Oils mg/I Fe - Iron mg/I Concentration units) Hardness: Total mg/I Hg - Mercury mg/1 Phenol mg/I K - Potassium mg/I Sulfate < 10 mg/I Mg - Magnesium mg/I Specific Conductance 69 uMhos Mn - Manganese mg/I Total Ammonia mg/I Na - Sodium mg/I TKN as N mg/I I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE. Signature of Permitt(or Authorized Agent Note: Values should reflect dissolved and colloidal concentrations. (see #3 on back) �- Z ' 9 j See back for instructions. Date " Submit blue, green, and yellow copies only to address above. GW-59 REV. 6/93 COLLECTION AND ANALYSIS OF GROUNDWATER SAMPLES 1. Samples should be analyzed as soon as possible after collection. SAMPLES WHICH ARE NOT ANALYSED WITHIN THE HOLDING TIME SPECI- FIED FOR THE METHOD USED (SEE44. BELOW) MUST BE DISCARDED AND NEW SAMPLES COLLECTED. ` '',3 2. Metals Analyses: Use Standard Method 3030C for sample preparation (mercury excluded)'. DO NOT FILTER METALS SAMPLES IN THE\FIELD !!� Unfiltered samples must be collected for mmetats, then field acidified with 5 ml concentrated nitric acid per liter of sample; and should be submitted to the lab within 24 hours. ^ ` Sample preparation in the laboratory (extraction and filtration) must be completed within 72 hours of collection. 3. ANALYSES ARE TO BE MADE OF THE MOBILE CONSTITUENTS (DISSOLVED AS WELL AS COLLOIDAL) IN THE GROUNDWATER, -NOT THOSE THAT ARE A PART OF SEDIMENT ASSOCIATED WITH WELL CONSTRUCTION OR SAMPLING PROCEDURES. CHECK WITH YOUR LABORATORY ON PROPER PROCEDURES FOR SAMPLE COLLECTION AND PRESERVATION. 4. As per Title 15, North Carolina Administrative'Code, Subchapter 2L, analytical procedures shall be in accordance with.the methods described in one of the following publications, or by other methods approved beforehand by the birector, Division of Environmental Managemjent: (a) Standard Methods for the Examination of Water and Wastewater, 16th Edition, 1985 and 17th Edition, 1989, published jointly by American Public Health Association, American Water Works Association and Water Pollution Control Federation; ZT, (b) Methods for Chemical Analysis of Water and Waste, 1979, U.S. Environmental Protection Agency publication number EPA-600/4-79-020, as revised March 1983; (c) Test Methods for Evaluating Solid Wastes: Physical/Chemical Methods, 3rd Edition, 1986, U.S. Environmental Protection Agency publication number SW-846; (d) Test Procedures for the Analysis of Polluants Under the Clean Water Act, Federal Register<Vol. 49, No. 209, 40 CFR Part 1.36, October 26, 1984; 5. Measure and record the depth of water in the well prior to pumping or bailing any water from the well. 6. At least 3 volumes of water in the well should be pumped or bailed prior to collecting a sample for analysis. if the well is pumped/bailed dry before 3 well volumes are removed, samples can be collected as soon as the well recovers to the point where enough water is available to collect your sample. 7. Determination for pH, Specific Conductance, temperature, odor and appearance must be made in the field on unfiltered samples when the sample is collected. - 8. Field equipment must be calibrated in accordance with recommendations by the manufacturer. 9. Samples must be filtered through a 0.45 micron filter immediately after collection when a dissolved analysis is required. (See #4. above) 10.The sample container should be labeled at the time of collection with the facility name, well identification number and date and time collected. 11."Authorized agent" is any corporate officer or public official authorized by tht3 company, corporation, or governmental body to sign official documents. Type or use a ball-point pen and press firmly. PERMIT NUMBER: (REQUIRED) Facility Name M971WJAL �Lctialcnt CAAZ50" Non -Discharge Address Sov Al, Asifr Ave NPDES /vC noeC7g7 bg NN n/ C. Z i? 3 5 Lt County HAAn c-rT TYPEOF DISPOSALOPERATION BEING MONITORED (REQUIRED) Well Location '&rwcem SL7TL/w[ f oN o r ido�uui"v "o, Lagoon Septic TanWDrain Field Well Identification Number VV .I Well Depth ZO Ft. Spray Field Subsurface Low -Pressure Well Diameter Z" Sample (Screened) Interval / S Ft. To Z o Ft. Piping (LPP) Depth to Water Level I Z ft. below measuring point (before sampling) Land Application of Sludge Other b Measuring point is 3 above land surface Rotary Distributor Sczrclw& E �et Is H INCr 10"cs Gallons of water pumped/bailed before sampling Z— Field Analysis: pH 5. I Specific Conductance — uMhos Temp. 13 oC Odor — Appearance Date Sample Collected 5 -i i 95 Date Lab Sample Analyzed If- z i - LaboratoryName JqQ u A- 'Tecu Certification No. 3 Z % Z e 3 SAMPLES FOR METALS WERE COLLECTED UNFILTERED AND FIELD ACIDIFIED YES NO COD < i S mg/I Coliform: MF Fecal /100ml Coliform: MF Total /100m1 (Note: Use MPN method for highly turbid samples) Dissolved Solids: Total y 5 mg/I pH (when analyzed) units TOC 41,0 mg/I Chloride ?, 1 mg/I Arsenic mg/I Grease and Oils mg/I Hardness: Total mg/I Phenol mg/I Sulfate -4!O mg/] Specific Conductance to S uMhos Total Ammonia mg/I TKN as N mg/I Nitrite (NO2) as N mg/I Nitrate (NO3) as N rri�g/I Phosphorus: Total as P. Ong/1 Al - Aluminum mg/I Ba - Barium mg/I Ca - Calcium mg/I Cd - Cadmium mg/I Chromium: Total mg/I Cu - Copper mg/I Fe - Iron mg/I Hg - Mercury mg/I K - Potassium mg/I Mg - Magnesium mg/I Mn - Manganese mg/I Na - Sodium mg/I Ni - Nickel Pb - Lead Zn - Zinc Pest! tides/H erbi tides (Specify Compounds) Other (Specify Compounds and v m-' Concentration units) M'w A i may 16 mg/I mg/I mg/I ug/I ug/I ug/I I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE. Note: Values i MW& r' and colloidal concentrations. (see #3 on back) See back for instructions. 8ignature of Permittee (or horize gent') Date •^ Submit blue, green, and yellow copies only to address above. GW-59 REV. 6/93 COLLECTION AND ANALYSIS OF GROUNDWATER SAMPLES x w- 1. Samples should be analyzed as soon as possible after collection. SAMPLES WHICH ARE NOT ANALYSED WITHIN THE HOLDING TIME SPECI- FIED FOR THE METHOD USED (SEE #4. BELOW) MUST BE DISCARDED AND NEW SAMPLES COLLECTED. 2. Metals Analyses: Use Standard Method 3030C for sample preparation (mercury excluded). DO NOT FILTER METALS SAMPLES IN THE FIELD !!! Unfiltered samples must be collected for metals, then field acidified with 5 ml concentrated nitric acid per liter of sample; and,should be submitted to the lab within 24 hours. - ' Sample preparation in the laboratory (extraction and filtration) must be completed within 72 hours of collection. 3. ANALYSES ARE TO BE MADE OF THE MOBILE CONSTITUENTS (DISSOLVED AS WELL AS COLLOIDAL) IN THE GROUNDWATER, NOT THOSE THAT ARE A PART OF SEDIMENT ASSOCIATED WITH WELL CONSTRUCTION OR SAMPLING PROCEDURES. CHECK WITH YOUR LABORATORY ON PROPER PROCEDURES FOR SAMPLE COLLECTION AND PRESERVATION. 4. As per Title 15, North Carolina Administrative Code, Subchapter 2L, analytical procedures shall be in accordance with the methods described in one of the following publications, or by other methods approved beforehand by the Director, Division of Environmental Management: (a) Standard Methods for the Examination of Water and Wastewater, 16th Edition, 1985 and 17th Edition, 1989, published jointly by • American Public Health Association, American Water Works Association and Water Pollution Control Federation; =a (b) Methods for Chemical Analysis of Water and Waste, 1979, U.S. Environmental Protection Agency publication number EPA-600/4-79-020, as revised March 1983; (c) Test Methods for Evaluating Solid Wastes: Physical/Chemical Methods, 3rd Edition, 1986, U.S. Environmental Protection Agency publication number SW-846; (d) Test Procedures for the Analysis of Polluants Under the Clean Water Act, Federal Register Vol. 49, No. 209, 40 CFR Part 136, October 26, 1984; i 5. Me'E ,i a Pd record the depth of water in the well prior to pumping or bailing any water from the well. 6. At leas 3 volumes of water in the well should be pumped or bailed prior to collecting a sample for analysis. If the well is pumped/bailed dry before 3 well volumes are removed, samples can be collected as soon as the well recovers to the point where enough?water is available to collect your sample. 7. Determination for pH, Specific Conductance, temperature, odor and appearance must be made in the field on unfiltered samples when the sample is collected. 8. Field equipment must be calibrated in accordance with recommendations by the manufacturer. 9. Samples must be filtered through a 0.45 micron filter immediately after collection when a dissolved analysis is required. (See #4. above) 10.The sample container should be labeled at the time of collection with the facility name, well identification number and date and time collected. 11. "Authorized agent" is any corporate officer or public official authorized by the company, corporation, or governmental body to sign official documents. L_ __-_ — - /� / r Type or Use a ball-point pen and press firmly. ,v Facility Name e9noAiaL C-ec7RicA, CAgRon/ PERMIT NUMBER: (REQUIRED) Non -Discharge NPDES /✓C 00607L/7 TYPE OF OPERATION BEING MONITORED IREQU1REDI vveuwcauun / —accN .o /3H/N4 ra.-/ram Lagoon Well Identification Number W 2 Well Depth 8 Ft. Well Diameter Z ample (Screened) Interval / Z Ft. To 9 Ft. Spray Field Septic Tank/Drain Field Subsurface Low -Pressure Piping (LPP) Depth to Water Level ft, below measuring point (before sampling) Land Application of Sludge Measuring point is Z ft. above land surface � Omer Gallons of water pumped/bailed before sampling 3 Rotary Distributor Scr LNG s' of Field Analysis: pH S: N Specific Conductance - uMhos Temp. 15 °C Odor - Appearance - a Date Sample Collected y-1 el -9 Date Lab Sample Analyzed '+ a I — s-3 °+� to m Ul Laboratory Name _Ei O r.r n - Tecrf Certification No. 33 Z Z(63. s� SAMPLES FOR METALS WERE COLLECTED UNFILTERED AND FIELD ACIDIFIED _YES NO e 0 COD < Is mg/1 Coliform: MF Fecal /100ml Coliform: MF Total /100ml (Note: Use MPN method for highly turbid samples) Dissolved Solids: Total vs mg/I pH (when analyzed) units TOC 41.0 mg/I Chloride 9' ? mg/I Arsenic mg/I Grease and Oils mg/I Hardness: Total mg/I Phenol mgA Sulfate </o mg/I Specific Conductance 63 uMhos Total Ammonia mgA TKN as N mgA Nitrite (NO2) as N mg/I Nitrate (NO3) as N rri�g/I Phosphorus: Total as P IhgA Al - Aluminum mg/I Ba - Barium mg/I Ca - Calcium mg/I Cd - Cadmium mg/I Chromium: Total mgA Cu - Copper mg/1 Fe - Iron mg/I Hg - Mercury mg/I K - Potassium mg/I Mg - Magnesium mg/I Mn - Manganese mg/I Na - Sodium mg/I Ni - Nickel Pb - Lead Zn - Zinc Pesticides/Herbicides (Specify Compounds) n. e;� L__ mgA "'mgA o mg/I ri M P Other (Specify Compounds and Concentration units) 1TY 114 fl ,f�`�. it ll/ IG''liti ug/I ug/I ug/I -11nr Al'!;TTEU I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE. NoILLE.AEG �nP;r� te: Values should reflect dissolved and colloidal concentrations. (see #3 on back) See back for instructions. Sign re of Permittee (or Aut of d Agent') Date '* Submit blue, green, and yellow copies only to address above. GW-59 REV. 6/93 COLLECTION AND ANALYSIS OF GROUNDWATER SAMPLES q•. w 1. Samples should be analyzed as soon as possible after collection. SAMPLES WHICH ARE NOT ANALYSED WITHIN THE HOLDING TIME SPECI- FIED FOR THE METHOD USED (SEE #4. BELOW) MUST BE DISCARDED AND NEW SAMPLES COLLECTED. 2. Metals Analyses: Use Standard Method 3030C for sample preparation (mercury excluded). DO NOT FILTER METALS SAMPLES IN THE FIELD !!! Unfiltered samples must be collected for metals, then field acidified with 5 ml concentrated nitric acid per liter of sample, and should be submitted to the lab within 24 hours. ' Sample preparation in the laboratory (extraction and filtration) must be completed within 72 hours of collection. 3. ANALYSES ARE TO BE MADE OF THE MOBILE CONSTITUENTS (DISSOLVED AS WELL AS COLLOIDAL) IN THE GROUNDWATER, NOT THOSE THAT ARE A PART OF SEDIMENT ASSOCIATED WITH WELL CONSTRUCTION OR SAMPLING PROCEDURES. CHECK WITH YOUR LABORATORY ON PROPER PROCEDURES FOR SAMPLE COLLECTION AND PRESERVATION. 4. As p* TiV.,l 5, North Carolina Administrative Code, Subchapter 2L, analytical procedures shall be in accordance with the methods described in one of the f4NowtnSl publications, or by other methods approved beforehand by the Director, Division of Environmental t r} (a) Standard Methods for the Examination of Water and Wastewater, 16th Edition, 1985 and 17th Edition, 1989, published jointly by — American Public Heafth Association, American Water Works Association and Water Pollution Control Federation; (b) Methods for Chemical Analysis of Water and Waste, 1979, U.S. Environmental Protection Agency publication number EPA-600/4-79-020, as revised March 1983; (c) Test Methods for Evaluating Solid Wastes: Physical/Chemical Methods, 3rd Edition, 1986, U.S. Environmental Protection Agency publication number SW-846: ct L (d) Test Procedures for the Analysis of Polluants Under the Clean Water Act, Federal Register Vol. 49, No. 209, 40 CFR Part 136, October 26, 1984; 5. Measure and record the depth of water in the well prior to pumping or bailing any water from the well. 6. At least 3 volumes of water in the well should be pumped or bailed prior to collecting a sample for analysis. If the well is pumpedibailed dry before 3 well volumes are removed, samples can be collected as soon as the well recovers to the point where enough water is available to collect your sample. 7. Determination for pH, Specific Conductance, temperature, odor and appearance must be made in the field on unfiltered samples when the sample is collected. 8. Field equipment must be calibrated in accordance with recommendations by the manufacturer. 9. Samples must be filtered through a 0.45 micron filter immediately after collection when a dissolved analysis is required. (See #4. above) 10.The sample container should be labeled at the time of collection with the facility name, well identification number and date and time collected. 11. ",Authorized agent' is any corporate officer or public official authorized by the company, corporation, or governmental body to sign official documents. Type or Use a ball-point pen and press firmly. PERMIT NUMBER: (REQUIRED) Facility Name NATIaNAL C—C.CCTR/CAL C.AcaO../ Non -Discharge Address Soo Al nslra Ave NPDES //C 6 O(.ej7 y 7 f 4NhI/ A/ C. Z'93.3 H County—Fit3a(.IF-7-r TYPE OF DISPOSAL OPERATION BEING MONITORED .SET rL/NC I� Well Location �eTween. o,vU �' / QL/SH (REQUIRED) /nJC l�onJ '7 Lagoon Septic TanWDrain Field Well Identification Number W 1 Well Depth 7-0 Ft. Well Diameter 2 k% Sample (Screened) Interval I .S Ft. To Z 0 Ft. spray Field Subsurface Low -Pressure Depth to Water Level /d ft. below measuring point (before sampling) Land Application of Sludge Piping (LPP) Measuring point is 3 ft. above land surface other Gallons of water pumped/bailed before sampling y. c) Rotary Distributor Field Analysis: pH 5,3 Specific Conductance - uMhos Temp. / y oC Odor Appearance o Date Sample Collected f'L - z7 - 9Ly Date Lab Sample Analyzed .ID M Laboratory Name AGun- T Iv E IRONMF TaL Certification No. 337_ 26 3 ` C)� SAMPLES FOR METALS WERE COLLECTED UNFILTERED AND FIELD ACIDIFIED YES NO o COD Coliform: MF Fecal Coliform: MF Total W (Note: Use MPN method for highly turbid samples) _ mg/I /100ml /100ml Dissolved Solids: Total 50 mg/I pH (when analyzed) units TOC 4 f • 0 mg/I Chloride 9 • Z mg/I Arsenic mg/I Grease and Oils mg/I Hardness: Total mg/I Phenol mg/I Sulfate / mg/I Specific Conductance _-Mhos Total Ammonia mg/I TKN as N mg/I Nitrite (NO2) as N Nitrate (NO3) as N Phosphorus: Total as P Al - Aluminum Ba - Barium Ca - Calcium Cd - Cadmium Chromium: Total Cu - Copper Fe - Iron Hg - Mercury K - Potassium Mg - Magnesium Mn - Manganese Na - Sodium I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE. 1 J AGENT / ZY 9j Signature of Permittee (or authorized Agent') Date GW-59 REV. 6/93 mg/I rpg/I g/I mg/I mg/I mg/I mg/I mg/I mg/I mg/I mg/I mg/I mg/I mg/I mg/I Ni - Nickel Pb - Lead Zn - Zinc Pesticides/Herbicides (Specify Compounds) Other (Specify Compoun Jt 1ta r t ` Concentration units)`., �( i E6 � 194+ ug/I ug/I ug/I A NT ` r . FFICEj Note: Values should reflect dissolved and colloidal concentrations. (see #3 on back) ' See back for instructions. " Submit blue, green, and yellow copies only to address above. i' COLLECTION AND ANALYSIS OF GROUNDWATER SAMPLES V, 1. Samples should be analyzed as soon as passible after collection. SAMPLES WHICH ARE NOT ANALYSED WITHIN THE HOLDING TIME SPECI- FIED FOR THE METHOD USED (SEE #4! BELOW) MUST BE DISCARDED AND NEW SAMPLES COLLECTED. 2. Metals Analyses: Use Standard Method 3030C for sample preparation (mercury excluded). DO NOT•FILTER METALS SAMPLES IN THE -FIELD !!! Unfiltered samples must be'collected for metals, then field acidified with 5 ml concentrated nitric acid per liter of sample, and should be submitted to the lab within 24 hours. Sample preparation in the laboratory (extraction and filtration) must be completed within 72 hours of collection. 3. ANALYSES ARE TO BE MADE OF THE MOBILE CONSTITUENTS (DISSOLVED AS WELL AS &dLLOIDAL) IN THE GROUNDWATER, NOT THOSE THAT ARE A PART OF SEDIMENT ASSOCIATED WITH WELL CONSTRUCTION OR SAMPLING PROCEDURES. CHECK WITH YOUR LABORATORY ON PROPER PROCEDURES FOR SAMPLE COLLECTION AND PRESERVATION. 4. As pjrTftle 15, North Carolina Administrative Code, Subchapter 2L, analytical•procedures shall be in accordance with the methods described in one of the foAowr.S publications, or by other methods approved beforehand by'the Director, Division of Environmental Mare r3it: ice? (a) Standard Methods for the Examination of Water and Wastewater, 16th Edition, 1985 and 17th Edition, 1989, published jointly by G' American Public Health Association, American Water Works Association and Water Pollution Control Federation; -�-_ (b) Methods for Chemical Analysis of Water and Waste, 1979, U.S. Environmental Protection Agency publication number EPA-600/4-79-020, as revised March 1983: (c) Test Methods for Evaluating Solid Wastes: Physical/Chemical Methods, 3rd Edition, 1986, U.S. Environmental Protection Agency 11`0 publication number SW-846; (d) Test Procedures for the Analysis of Polluants Under the Clean Water Act, Federal Register Vol. 49, No. 209, 40 CFR Part 136, October 26, 1984; 5. Measure and record the depth of water in the well prior to pumping or bailing any water from the well. 6. At least 3 volumes of water in the well should be pumped or bailed prior to collecting a sample for analysis. If the well is pumped/bailed dry before 3 well volumes are removed, samples can be collected as soon as the well recovers to the point where enough water is available to collect your sample. 7. Determination for pH, Specific Conductance, temperature, odor and appearance must be made in the field on unfiltered samples when the sample is collected. 8. Field equipment must be calibrated in accordance with recommendations by the manufacturer. 9. Samples must be filtered through a 0.45 micron filter immediately after collection when a dissolved analysis is required. (See #4. above) 10.The sample container should be labeled at'the time of collection with the facility name, well identification number and date and time collected. 11. "Authorized agent" is any corporate officer or public official authorized by the company, corporation,' or governmental body to sign official documents. `, Type or use a ban -point pen and press firmly. Facility Name 'VATlomAL eLCCT,Q)r-AL. CAA36" Well PERMIT NUMBER: (REQUIRED) Non -Discharge NPDES /VC 00�07`i7 TYPE OF DISPOSAI OPERATION BEING MONITORED (REQUIRED) Lagoon Well Identification Number W � Well Depth � )? Ft. Well Diameter 2 N% Sample (Screened) Interval 1 Z Ft. To / S Ft. Spray Field Septic TanklDrain Field Subsurface Low -Pressure Piping (LPP) Depth to Water Level z . eft. below measuring point (before sampling) Land Application of Sludge Measuring point is � ft. above land surface Rotary Distributor SEOther7Tt1.v4 � Gallons of water pumped/bailed before sampling, Field Analysis: pH 6.0 Specific Conductance — uMhos Temp. Z °C Odor — Appearance Date Sample Collected /Z- Z 7-1 Yp Date Lab Sample Analyzed /2 - so /. Y - /-9 /9S Laboratory Name &) 1'4 - %EC:/f Certification No. 337 243 SAMPLES FOR METALS WERE COLLECTED UNFILTERED AND FIELD ACIDIFIED YES NO COD S mg/I Coliform: MF Fecal A00ml Coliform: MF Total /100ml (Note: Use MPN method for highly turbid samples) Dissolved Solids: Total 50 mg/I pH (when analyzed) units TOC 1.3 mg/1 Chloride /0 mg/I Arsenic mg/I Grease and Oils mg/I Hardness: Total mg/1 Phenol mg/I Sulfate 4 1.7_ mg/I Specific Conductance 61 uMhos Total Ammonia mg/I TKN as N mg/I Nitrite (NO2) as N mg/I Nitrate (NO3) as N rri�g/I Phosphorus: Total as P ring/1 AI - Aluminum mg/I Ba - Barium mg/I Ca - Calcium mg/I Cd - Cadmium mg/I Chromium: Total mg/I Cu - Copper mg/I Fe - Iron mg/I Hg - Mercury mg/I K - Potassium mg/I Mg - Magnesium mg/I Mn - Manganese mg/I Na - Sodium mg/I Ni - Nickel Pb - Lead Zn - Zinc Pesticides/Herbicides (Specify Compounds) r�3 z mg/I mg/I �p mg/l C` oc ug/I ug/I Ug/I Other (Specify Compounds and Concentration units) W m I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE. Note: Values should reflect dissolved and Q % colloidal concentrations. (see #3 on back) ti / CA'GENT 1 zv %.� See back for instructions. :ignature of Permittee (or uthorized Agent*) Date *° Submit blue, green, and yellow copies only to address above. GW-59 REV. 6/93 COLLECTION AND ANALYSIS OF GROUNDWATER SAMPLES Samples should be analyzed as soon as possible after collection. SAMPLES WHICH ARE NOT ANALYSED WITHIN THE HOLDING TIME SPECI- FIED FOR THE METHOD USED (SEE rr4, BELOW) MUST BE DISCARDED AND NEW SAMPLES COLLECTED. 2. Metals Analyses: Use Standard Method 3030C for sample preparation (mercury excluded). DO NOT FILTER METALS SAMPLES IN THE FIELD !!! Unfiltered samples must be collected for metals, then field acidified with 5 ml concentrated nitric acid per liter of sample, and should be submitted to the lab within 24 hours. Sample preparation in the laboratory (extraction and filtration) must be completed within 72 hours of collection. 3. ANALYSES ARE TO BE MADE OF THE MOBILE CONSTITUENTS (DISSOLVED AS WELL AS COLLOIDAL) IN THE GROUNDWATER, NOT THOSE THAT ARE A PART OF SEDIMENT ASSOCIATED WITH WELL CONSTRUCTION OR SAMPLING PROCEDURES. CHECK WITH YOUR LABORATORY ON PROPER PROCEDURES FOR SAMPLE COLLECTION AND PRESERVATION. 4. As per Title 15, North Carolina Administrative Code, Subchapter 2L, analytical procedures shall be in accordance with the methods'described in one of the following publications, or by other methods approved beforehand by the Director, Division of Environmental Management: (a) Standard Methods for the Examination of Water and Wastewater, 16th Edition, 1985 and 17th Edition, 1989, published jointly by h American Public Health Association, American Water Works Association and Water Pollution Control Federation; "- 'ru (b) Methods for Chemical Analysis of Water and Waste, 1979, U.S. Environmental Protection Agency publication number �'. EPA-600/4-79-020, as revised March 1983; (c) Test Methods for Evaluating Solid Wastes: Physical/Chemical Methods, 3rd Edition, 1986, U.S. Environmental Protection Agency .,,<. • : � publication number SW-846; _ (d) Test Procedures for the Analysis of Polluants Under the Clean Water Act, Federal Register Vol. 49. No. 209, 40 CFR Part 136, October 26, 1984; 5. Measge aid record the depth of water in the well prior to pumping or bailing any water from the well. ' i c� 6. At least 3 volumes of water in the well should be pumped or bailed prior to collecting a sample for analysis. If the well is pumped/bailed dry before 3 well volumes are removed, samples can be collected as soon as the well recovers to the point where enough water is available to collect your sample. Determination for pH, Specific Conductance, temperature, odor and appearance must be made in the field on unfiltered samples when the sample is collected. ' 8. Field equipment must be calibrated in accordance with recommendations by the manufacturer. 9. Samples must be filtered through a 0.45 micron filter immediately after collection when a dissolved analysis is required. (See #4. above) 10.The sample container should be labeled at the time of collection with the facility name, well identification number and date and time collected. 11 ."Authorized agent" is any corporate officer or public official authorized by the company, corporation, or governmental body to sign official documents. Type or Use a ball-point pen and press firmly. Facility Name MiT166Jr AL- C L-ECTAICAL CH4130N Address 5 0'Y N A S H E A v e Well Location Well Identification Number Lu Z_ Well Depth 12 Ft. Well Diameter Z .. Sample (Screened) Interval 1 Z Ft. To IF Ft. Depth to Water Level Z , 5 ft. below measuring point (before sampling) Measuring point is Z ft. above land surface Gallons of water pumped/bailed before sampling Z' 5 PERMIT NUMBER: (REQUIRED) Non -Discharge NPDES A C 0060-7 7 TYPE OF DISPOSAI, OPERATION BEING MONITORED (REQUIRED) Lagoon Septic TanktDrain Field Spray Field Subsurface Low -Pressure Piping (LPP) Land Application of Sludge Other Rotary Distributor G.rr bA 1- Field Analysis: pH S. 7 Specific Conductance uMhos Temp. Z o °C Odor Appearance Date Sample Collected 9- Z k - 9 `r Date Lab Sample Analyzed 9-2k -4 y — LaboratoryName 1gQQ4- 'Tech Certification No. 33-2 Z63 SAMPLES FOR METALS WERE COLLECTED UNFILTERED AND FIELD ACIDIFIED YES NO COD `1 mg/I Coliform: MF Fecal /100ml Coliform: MF Total /100mI (Note: Use MPN method for highly turbid samples) Dissolved Solids: Total 50 mg/I pH (when analyzed) units TOC / S mg/I Chloride 8 Z mg/I Arsenic mg/I Grease and Oils mg/I Hardness: Total mg/I Phenol mg/I Sulfate L 1 Z- mg/I Specific Conductance 96 uMhos Total Ammonia mg/I Nitrite (NO2) as N Nitrate (NO3) as N _ Phosphorus: Total as Al - Aluminum Ba - Barium Ca - Calcium Cd - Cadmium Chromium: Total Cu - Copper Fe - Iron Hg - Mercury K - Potassium Mg - Magnesium Mn - Manganese Na - Sodium mg/1 Ni - Nickel - cm mg/1 rpg/I Pb - Lead a' og mg/I g/1 Zn - Zinc 4ED mg/I mg/I Pesticides/Herbicides o m? mg/I (Specify Compounds) :;u= mg/1 C� ` ug/I mg/I " ug/I mg/ ug/I mg/I Other (Specify Compounds and mgfl Concentration units) mg/I 1. . - mg/I �k�l '; r'! mg/I _LF "2.: mg/I Fz e n TKN as N mg/I I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE. Note: Values should reflect dissolved and 4 �y colloidal concentrations. (see #3 on back) -KA &C,vT / - ICI- ?' See back for instructions. Signature of Permittee (o uthorized Agent') Date •• Submit blue, green, and yellow copies only to address above. GW-59 REV. 6/93 COLLECTION AND ANALYSIS OF GROUNDWATER SAMPLES r:A 1. Samples should be analyzed as soon as possible after collection. SAMPLES WHICH ARE NOT ANALYSED WITHIN THE HOLDING TIME SPECI- FIED FOR THE METHOD USED (SEE #4. BELOW) MUST BE DISCARDED AND NEW SAMPLES COLLECTED. 2. Metals Analyses: Use Standard Method 3030C for sample preparation (mercury excluded). DO NOT FILTER METALS SAMPLES IN THE, FIELD !!! Unfiltered samples must be collected for metals, then field acidified with 5 ml concentrated nitric acid per liter of sample, and should be submitted to the lab within 24 hours. Sample preparation in the laboratory (extraction and filtration) must be completed within 72 hours of collection. 3. ANALYSES ARE TO BE MADE OF THE MOBILE CONSTITUENTS (DISSOLVED AS WELL AS COLLOIDAL) IN THE GROUNDWATER, NOT THOSE THAT ARE A PART OF SEDIMENT ASSOCIATED WITH WELL CONSTRUCTION OR SAMPLING PROCEDURES. CHECK WITH YOUR LABORATORY ON PROPER PROCEDURES FOR SAMPLE COLLECTION AND PRESERVATION. 4. As per Title 15, North Carolina Administrative Code, Subchapter 2L, analytical procedures shall be in accordance with the methods described in one of the folllofwing publications, or by other methods approved beforehand by the Director, Division of Environmental Mana�mept: (a) Standard Methods for the Examination of Water and Wastewater, 16th Edition, 1985 and 17th Edition, 1989, published jointly by CN, American Public Health Association, American Water Works Association and Water Pollution Control Federation; (b) Methods for Chemical Analysis of Water and Waste, 1979, U.S. Environmental Protection Agency publication number .. •: r� EPA-600l4-79-020, asrevised March 1983; (c) Test Methods for Evaluating Solid Wastes: Physical/Chemical Methods, 3rd Edition, 1986, U.S. Environmental Protection Agency publication number SW-846; ;Mc (d) Test Procedures for the Analysis of Polluants Under the Clean Water Act, Federal Register Vol. 49. No. 209, 40 CFR Part 136, October 26, 1984• 5. fvieasure`and record the depth of water in the well prior to pumping or bailing any water from the well. 6. At least 3 volumes of water in the well should be pumped or bailed prior to collecting a sample for analysis. If the well is pumped/bailed dry before 3 well volumes are removed, samples can be collected as soon as the well recovers to the point where enough water is available to collect your sample. 7. Determination for pH, Specific Conductance, temperature, odor and appearance must be made in the field on unfiltered samples when the sample is collected. 8. Field equipment must be calibrated in accordance with recommendations by the manufacturer. 9. Samples must be filtered through a 0.45 micron filter immediately after collection when a dissolved analysis is required. (See #4. above) 10.The sample container should be labeled at the time of collection with the facility name, well ident fication number and date and time collected. 11.°Authorized agent" is any corporate officer or public official authorized by the company, corporation, or governmental body to sign official documents. Type or Use a Facility Name press -LJU N N N V G X} 3 Lt County oNn C -r Well Location 13cTwe1'nr 5crr�j jc- a2,UJD a _Pot/5 s,N& Well Identification Number uu I Well Depth 20 Ft. Well Diameter Z " Sample (Screened) Interval / S Ft. To Z0Ft. Depth to Water Level 10 ft. below measuring point (before sampling) Measuring point is 3 ft. above land surface Gallons of water pumped/bailed before sampling 2 . 5 PERMIT NUMBER: (REQUIRED) Non -Discharge NPDES Yt/C 006 O 7'f 7 TYPE OF DISPOSAI OPERATION BEING MONITORED (REQUIRED) Lagoon Septic Tank/Drain Field Spray Feld Subsurface Low -Pressure Piping (LPP) Land Application of Sludge Other Rotary Distributor .5z rrt/n76/7%i L IS R,/ &Pe Field Analysis: pH 5,91 Specific Conductance — uMhos Temp. 2 f °C Date Sample Collected g`Z LL Jf Lf Date Lab Sample Analyzed F'Zy-Yy — Laboratory Name AnuR--Teck C`uVIRhVMENrgc_ Laaoaroares SAMPLES FOR METALS WERE COLLECTED UNFILTERED AND FIELD ACIDIFIED Odor Appearance `t-)-` 91 Certification No. 337- YES NO W rr1 o rri nrrt COD < 8 mg/I Nitrite (NO2) as N mg/I Ni - Nickel rn vP� mg/I Coliform: MF Fecal /100ml Nitrate (NO3) as N rpg/I Pb -Lead ngp mg/I Coliform: MF Total A 00ml Phosphorus: Total as P g/I Zn - Zinc -am mg/I (Note: Use MPH method for highly turbid samples) AI - Aluminum mg/I Pesticides/Herbicides � Dissolved Solids: Total 2 o mg/I Be - Barium mg/I (Specify Compounds) C m pH (when analyzed) units Ca - Calcium mg/I c'3 ug/I TOC 1,5 mg/I Cd - Cadmium mg/1 ug/I Chloride 9.7 mg4 Chromium: Total mg/I ug/1 Arsenic mg/I Cu - Copper mg/I Other (Specify Compounds and Grease and Oils mg/1 Fe - Iron mg/I Concentration units) Hardness: Total mg/I Hg - Mercury mg/I Phenol mg/I K - Potassium mg/I Sulfate 4 ) z mg/I Mg - Magnesium mg/I Specific Conductance 58 uMhos Mn - Manganese mg/I Total Ammonia mg/I Na - Sodium mg/I TKN as N mg/I I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE. Note: Values should reflect dissolved and colloidal concentrations. (see #3 on back) See back for instructions. Signature of Permittee r Authorized Agent* Date ^ Submit blue, green, and yellow copies only to address above. GW-59 REV. 6/93 COLLECTION AND ANALYSIS OF GROUNDWATER SAMPLES y 1. Samples should be analyzed as soon as possible after collection. SAMPLES WHICH ARE NOT ANALYSED WITHIN THE HOLDING TIME SPECI- FIED FOR THE METHOD USED (SEE #4. BELOW) MUST BE DISCARDED AND NEW SAMPLES COLLECTED. 2. Metals Analyses: Use Standard Method 30300 for sample preparation (mercury excluded). DO NOT FILTER METALS SAMPLES IN THEIFIELD Unfiltered samples must be collected for metals, then field acidified with 5 ml concentrated nitric acid per liter of sample, and should be submitted to the lab within 24 hours. Sample preparation in the laboratory (extraction and filtration) must be completed within 72 hours of collection. 3. ANALYSES ARE TO BE MADE OF THE MOBILE CONSTITUENTS (DISSOLVED AS WELL AS COLLOIDAL) IN THE GROUNDWATER, NOT THOSE THAT ARE A PART OF SEDIMENT ASSOCIATED WITH WELL CONSTRUCTION OR SAMPLING PROCEDURES. CHECK WITH YOUR LABORATORY ON PROPER PROCEDURES FOR SAMPLE COLLECTION AND PRESERVATION. 4. As per Title 15, North Carolina Administrative Code, Subchapter 2L, analytical procedures shall be in accordance with the methods described in one of the Ia. wi}�9 publications, or by other methods approved beforehand by the Director, Division of Environmental Managemeht: - + " (a) Standard Methods for the Examination of Water and Wastewater, 16th Edition, 145 and 17th Edition, 1989, published jointly by _ American Public Health Association, American Water Works Association and Water Pollution Control Federation; (b) Methods for Chemical Analysis of Water and Waste, 1979, U.S. Environmental Protection Agency publication number -? - EPA-600/4-79-020, as revised March 1983; (c) Test Methods for Evaluating Solid Wastes: Physical/Chemical Methods, 3rd Edition, 1986, U.S. Environmental Protection Agency publication number SW-846; C' (d) Test Procedures for the Analysis of Polluants Under the Clean Water Act, Federal Register Vol. 49. No. 209, 40 CFR Part 136, =? October26, 1984; 5. Measure and record the depth of water in the well prior to pumping or bailing any water from the well. 6. At least 3 volumes of water in the well should be pumped or bailed prior to collecting a sample for analysis. If the well is pumped/bailed dry before 3 well volumes are removed, samples can be collected as soon as the well recovers to the point where enough water is available to collect your sample. 7. Determination for pH, Specific Conductance, temperature, odor and appearance must be made in the field on unfiltered samples when the sample is collected. 8. Field equipment must be calibrated in accordance with recommendations by the manufacturer. 9. Samples must be filtered through a 0.45 micron filter immediately after collection when a dissolved analysis is required. (See #4. above) 10.The sample container should be labeled at the time of collection with the facility name, well identification number and date and time collected. 11. "Authorized agent' is any corporate officer or public official authorized by the company, corporation, or governmental body to sign official documents. No Facility Name Address PERMIT NUMBER: (REQUIRED) Non -Discharge NPDES At C O O F 0 74 7 TYPE OF DISPOSAI OPERATION BEING MONITORED (REQUIRED) Well Location UJ 2 F/nT,attN'r 70 !'o� sNiNG pbvtb ' ace C',zrar Lagoon Septic Tank/Drain Field Well Identification Number Lu 7-Well Depth / 8 Ft. spray Field subsurface Low -Pressure Well Diameter 2" Sample (Screened) Interval 1 Z- Ft. To Z 8 Ft. Depth to Water Level 3. O ft. below measuring point (before sampling) Land Application of sludge Piping (LPP) Measuring point is Z. ft. above land surface ✓ other SfTT�)J& g Rotary Distributor �oL ISH�NG /'on�Js Gallons of water pum11 ailed before sampling Field Analysis: pH -5, 6 Specific Conductance '- uMhos Temp. 18 oC Odor - Appearance Date Sample Collected -5- 7-2c `1 , Date Lab Sample Analyzed 5-24 rwaw 6-9, IVY Laboratory Name 4Tec` 0wa h N%11RONMfNTAL L413oAAieAld Certification No. 33 Z Z 6 3 SAMPLES FOR METALS WERE COLLECTED UNFILTERED AND FIELD ACIDIFIED YES NO Type or Use a ball-point pen and press firmly. COD 4 S mgA Nitrite (NO2) as N mg/I Ni - Nickel - L m mg/1 Coliform: MF Fecal /100ml Nitrate (NO3) as N rri�tg/I Pb - Lead � �, mgA Coliform: MF Total /100ml Phosphorus: Total as P. Ihg/I Zn - Zinc :33"' mg/I (Note: Use MPN method for highly turbid samples) AI - Aluminum mgA Pesticides/Herbicides , C= Dissolved Solids: Total '7 mg/I Ba - Barium mg/I (Specify Compounds) p1 `om pH (when analyzed) units Ca - Calcium mg/I m t-" ug/I TOC /, 7 mg/I Cd - Cadmium mg/I —+M ug/I Chloride ! 1 mg/I Chromium: Total mg/I A= ug/I Arsenic mg/I Cu - Copper mg/I Other (Specify Compounds and c`"'if r` i Grease and Oils mg/I Fe - Iron mg/I Concentration units) Hardness: Total mg/I Hg - Mercury mg/I P`w' Phenol mgA K- Potassium mg/I J,�<`3' Sulfate a mg/I Mg - Magnesium mg/I Specific Conductance `f uMhos Mn - Manganese mgA JUL= 99 t Total Ammonia mg/I Na - Sodium mg/I TKN as N mgA HlV -u rvt� I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE. Note: Values should reflect dissolved and l/ colloidal concentrations. (see #3 on back) See back for instructions. Signature of Permittee (or(Mthorized Agent') Date *• Submit blue, green, and yellow copies only to address above. GW-59 REV. 6/93 COLLECTION AND ANALYSIS OF GROUNDWATER SAMPLES 1. Samples should be analyzed as soon as possible after collection. SAMPLES WHICH ARE NOT ANALYSED WITHIN THE HOLDING TIME SPECI- FIED FOR THE METHOD USED (SEE #4. BELOW) MUST BE DISCARDED AND NEW SAMPLES COLLECTED. 2. Metals Analyses: Use Standard Method 30�0C for sample preparation (mercury excluded). DO NOT FILTER METALS SAMPLES IN THE FIELD Unfiltered samples must be "collected for metals, then field acidified with 5 ml concentrated nitric acid per liter of sample, and should be submitted to the lab within 24 hours. 1 Sample preparation in the laboratory (extraction and filtration) must be completed within 72 hours of collection. 3. ANALYSES ARE TO BE MADE OF THE MOBILE CONSTITUENTS (DISSOLVED AS WELL AS CQLLOIDAL) IN THE GROUNDWATER, NOT THOSE THAT ARE A PART OF SEDIMENT ASSOCIATED WITH WELL CONSTRUCTION OR SAMPLING PROCEDURES. CHECK WITH YOUR LABORATORY ON PROPER PROCEDURES FOR SAMPLE COLLECTION AND PRESERVATION. 4. As per Title 15, North Carolina Administrative Code, Subchapter 2L, analytical procedures shall be in accordance with the methods described in one of the following publications, or by other methods approved beforehand by the Director, Division of Environmental Management: (a) Standard Methods for the Examination of Water and Wastewater, 16th Edition, 1985 and 17th Edition, 1989, published jointly by t: American Public Health Association, American Water Works Association and Water Pollution Control Federation; (b) Methods for Chemical Analysis of Water and Waste, 1979, U.S. Environmental Protection Agency publication number EPA-600/4-79-020, as revised March 1983; -i (c) Test Methods for Evaluating Solid Wastes: Physical/Chemical Methods, 3rd Edition, 1986, U.S. Environmental Protection Agency publication number SW-846; (d) Test Procedures for the Analysis of Polluants Under the Clean Water Act, Federal Register Vol. 4% No. 209, 40 CFR Part 136, October 26, 1984; 5. Measane a -A record the depth of water in the well prior to pumping or bailing any water from the well. P+ G� r : rU - 6. At leda 3 volumes of water in the well should be pumped or bailed prior to collecting a sample for analysis. If the well is pumped/bailed dry -before 3 well volumes are removed, samples can be collected as soon as the well recovers to the point where enough water is available to collect your sample. 7. Determination for pH, Specific Conductance, temperature, odor and appearance must be made in the field on unfiltered samples when the sample is collected. 8. Field equipment must be calibrated in accordance with recommendations by the manufacturer. 9. Samples must be filtered through a 0.45 micron filter immediately after collection when a dissolved analysis is required. (See #4. above) 10.The sample container should be labeled at the time of collection with the facility name, well identification number and date and time collected. 11. "Authorized agent' is any corporate officer or public official authorized by the company, corporation, or governmental body to sign official documents. Type or Use a ball-point pen and press firmly. Facility 'A( Well Lo PERMIT NUMBER: (REQUIRED) Septic Tank/Drain Field Well Identification Number W 1 Well Depth - 20 Ft. / 5 F[. TO Z Ft. Spray Field Subsurface Low -Pressure Well Diameter .z Sample (Screened) Interval piping (LPP) Depth to Water Level 10 ft. below measuring point (before sampling) Land Application of Sludge Measuring point is 3 ft. above land surface Other Gallons of water pumped/bailed before sampling 2 • z Rotary Distributor Scam„us ;' /�6use,NG /a, Field Analysis: pH 5.0 Specific Conductance — uMhos Temp. / 7 0 °C Odor Appearance Date Sample Collected 11. 19-99 Date Lab Sample Analyzed 9- zt Ta 4 - Z7-9 4 Laboratory Name AOJRTPe,o ce"VrRo4,mE.vTAL. Gganenroares Certification No. 332- 1 Z43 SAMPLES FOR METALS WERE COLLECTED UNFILTERED AND FIELD ACIDIFIED YES NO COD < ? mgA Coliform: MF Fecal /100ml Coliform: MF Total /100ml (Note: Use MPN method for highly turbid samples) Dissolved Solids: Total 7 F' mg/I pH (when analyzed) units TOC 1.1 mgA Chloride /o mg/I Arsenic mg/I Grease and Oils mg/1 Hardness: Total mg/I Phenol mgA Sulfate 8 mg/I Specific Conductance 72- uMhcs Total Ammonia mg/I TKN as N mgA Non -Discharge NPDES A/c 00&0'7y'7 TYPE OF DISPOSAL OPERATION BEING MONITORED (REQUIRED) Lagoon Nitrite (NO2) as N mg/I Nitrate (NO3) as N m�lg/I Phosphorus: Total as P. fhg/1 Al - Aluminum mg/I Ba - Barium mg/l Ca - Calcium mg/I Cd - Cadmium mg/I Chromium: Total mg/I Cu - Copper mg/I Fe - Iron mg/I Hg - Mercury mgA K - Potassium mg/1 Mg - Magnesium mg/I Mn - Manganese mg/l Na - Sodium mgA Ni - Nickel Pb - Lead mg/I mgA Zn - Zinc mg/1 Pesticides/Herbicides (Specify Compounds) ug/I ug/I ' ug/1 Other (Specify Compounds and Concentration units)cD I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE. ENV. f." ' P": IT ote: NValupstishq*lll�LCjfl:/+ ect dissolved and 1 colloidal concentrations. (see #3 on back) See back for instructions. Signature of Permittee (or Au(Vorized Agent') Date " Submit blue, green, and yellow copies only to address above. GW-59 REV. 6/93 COLLECTION AND ANALYSIS OF GROUNDWATER SAMPLES 1. Samples should be analyzed as soon as possible after collection. SAMPLES WHICH ARE NOT ANALYSED WITHIN THE HOLDING TIME SPECI- FIED FOR THE METHOD USED (SEE #4: BELOW) MUST BE DISCARDED AND NEW SAMPLES COLLECTED. 2. Metals Analyses: Use Standard Method 3030C for sample preparation (mercury excluded): DO NOT -FILTER METALS SAMPLES"IN THE, FIELD !!! Unfiltered samples must be collected Tor mefals, then field acidified with 5 ml concentrated nitric acid per liter of sample, and should be submitted to the lab within 24 hours. ' ` -- . - Sample preparation in the laboratory (extraction and filtration) must be completed within 72 hours & collection: 3. ANALYSES ARE TO BE MADE OF THE MOBILE CONSTITUENTS (DISSOLVED -AS WELL AS COLLOIDAL) IN THE GROUNDWATER, NOT THOSE THAT ARE A PART OF SEDIMENT ASSOCIATED WITH WELL CONSTRUCTION OR SAMPLING PROCEDURES. CHECK WITH YOUR'LABORATORY ON PROPER PROCEDURES FOR SAMPLE COLLECTION AND PRESERVATION. 4. Asper Title 15, North Carolina Administrative Code, Subchapter 2L, analytiEal brocedures shall be in accordance with the methods -described in one of the following publications, or by other methods approved beforehand by the Director, Division of Environmental Management: (a) Standard Methods for the Examination of Water and Wastewater, 16th Edition, 1985 and 17th Edition, 1989, published jointly by American Public Health Association, American Water Works Association and Water Pollution Control Federation; (b) Methods for Chemical Analysis of Water and Waste, 1979, U.S. Environmental Protection Agency publication number EPA-600/4-79-020, as revised March 1983; (c) Test Methods for Evaluating Solid Wastes: Physical/Chemical Methods, 3rd Edition, 1936, U.S. Environmental Protection Agency publication number S`W-846; (d) Test Procedures for the Analysis of Polluants Under the Clean Water Act, Federal Register Vol. 49, No. 209, 40 CFR Part 136, October 26, 1984; 5. Measure and record the depth of water in the well prior to pumping or bailing any water from the well 6. At least 3 volumes of water in the well should be pumped or bailed prior to collecting a sample for analysis. If the well is pumpedibailed dry before 3 well volumes are removed, samples can be collected as soon as the well recovers to the point where enough water is available to collect your sample. 7. Determination for pH, Specific Conductance, temperature, odor and appearance must be made in the field on unfiltered samples when the sample is collected. 8. Field equipment must be calibrated in accordance with recommendations by the manufacturer. 9. Samples must be filtered through a 0.45 micron filter immediately after collection when a dissolved analysis is required. (See #4. above) 10.The sample container should be labeled at the time of collection with the facility name, well identification number and date and time collected. 11.^Authorized agent" is any corporate officer or public official authorized by the company, corporation, or governmental body to sign official documents,' / Type or I Facility Name Address .9 ✓ r / Well )all -point pen ano press tirmly. ' r PERMIT NUMBER: (REQUIRED) F-� IFfL rin r PL5-k1 NEr, 7 Non -Discharge NPDES N -0066-79 County 74 TYPE OF DISPOSAL OPERATION BEING MONITORED r�� (REQUIRED) .$� � �"� �5L�. J.. �A.3o52 Lagoon Septic-rank/Drain Field Well Identification Number 47AZ / We Depth fir• Z_ ,Ot. Well Diameter?, Sample (Screened) Interval Ft. To FL Depth to Water Level ft. below measuring point (before sampling) Measuring point is �t' "/ 0 ft. above land surface Gallons of water pumped/bailed before sampling 2p /o S Field Analysis: pH 4 aR Specific Conductance uMhos Temp. Date Sample Collected i 3 Date Lab Sample Analyzed Laboratory Name C(Ll tnu CaJ' -1 1.0 t rOn n c:��aJL %r Analyzed Spray Field Subsurface Low -Pressure Piping (LPP) Land Application of Stud Other11s_�f ��ba Rotary Distributor 6wh Pn I � S h.L ). W °C Odor Appearance Certification No. 'T& SAMPLES FOR METALS WERE COLLECTED UNFILTERED AND FIELD ACIDIFIED YES NO COD Coliform: Coliform: ./-!o ma/I MF Fecal /100ml MF Total /100ml (Note: Use MPN method for highly turbid samples) Dissolved Solids: Total IS' mqA pH (when analyzed) 6. I units TOC 3, a mgA Chloride mgA Arsenic mgA Grease and Oils mg/I Hardness: Total mgA Phenol mgA Sulfate mgA Specific Conductance 59 uMhos Total Ammonia mgA TKN as N mgA Nitrite (NO2) as N mgA Nitrate (NO3) as N mg/I Phosphorus: Total as P mgA All - Aluminum mgA Ba - Barium mgA Ca - Calcium mgA Cd - Cadmium mgA Chromium: Total mgA Cu - Copper mgA Fe - Iron mgA Hg - Mercury mgA K - Potassium mgA Mg - Magnesium mgA Mn - Manganese mgA Na - Sodium mgA I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE. 7-1- Signature of Permitte r Authorized Agent*) Date GW-59 REV. 6/93 Ni - Nickel mg/I Pb - Lead mgA Zn - Zinc " - mgA Pesticides/Herbicides <- 7 (Specify Compounds) ug/I ` ug/I ug/I Other (Specify Compounds and , ug/I Concentration units) , ug/I ug/l. r_{1y _trna—, a,+ N14 , Note: Values should reflect dissolved and colloidal concentrations. (see #3 on back) See back for Instructions. •• Submit blue, green, and yellow copies only to address above. 1 COLLECTION AND ANALYSIS OF GROUNDWATER SAMPLES 1. Samples should be analyzed as soon as possible after collection. SAMPLES WHICH ARE NOT ANALYSED WITHIN THE HOLDING TIME SPECI- FIED FOR THE METHOD USED (SEE #4. BELOW) MUST BE DISCARDED AND NEW SAMPLES COLLECTED. 2. Metals Analyses: Use Standard Method 3030C for sample preparation (mercury excluded). DO NOT FILTER METALS SAMPLES IN THE FIELD r!! Unfiltered samples must be collected for metals, then field acidified with 5 ml concentrated nitric acid per liter of sample, and should be submitted to the lab within 24 hours. Sample preparation in the laboratory (extraction and filtration) must be completed within 72 hours of collection. 3. ANALYSES ARE TO BE MADE OF THE MOBILE CONSTITUENTS (DISSOLVED AS WELL AS COLLOIDAL) IN THE GROUNDWATER, NOT THOSE THAT ARE A PART OF SEDIMENT ASSOCIATED WITH WELL CONSTRUCTION OR SAMPLING PROCEDURES. CHECK WITH YOUR LABORATORY ON PROPER PROCEDURES FOR SAMPLE COLLECTION AND PRESERVATION. 4. As per Title 15, North Carolina Administrative Code, Subchapter 2L, analytical procedures shall be in accordance with the methods'described in one of the following publications, or by other methods approved beforehand by the Director, Division of Environmental Management: (a) Standard Methods for the Examination of Water and Wastewater, 16th Edition, 1985 and 17th Edition, 1989, published jointly by American Public Health Association, American Water Works Association and Water Pollution Control Federation; (b) Methods for Chemical Analysis of Water and Waste, 1979, U.S. Environmental Protection Agency publication number EPA-600/4-79-020, as revised March 1983; (c) Test Methods for Evaluating Solid Wastes: Physical/Chemical Methods, 3rd Edition, 1986, U.S. Environmental Protection Agency publication number SW-846; (d) Test Procedures for the Analysis of Polluants Under the Clean Water Act, Federal Register Vol. 49, No. 209, 40 CFR Part 136, October 26, 1984; 5. Measure and record the depth of water in the well prior to pumping or bailing any water from the well. 6. At least 3 volumes of water in the well should be pumped or bailed prior to collecting a sample for analysis. If the well is pumped/bailed dry before 3 well volumes are removed, samples can be collected as soon as the well recovers to the point where enough water is available to collect your sample. 7. Determination for pH, Specific Conductance, temperature, odor and appearance must be made in the field on unfiltered samples when the sample is collected. 8. Field equipment must be calibrated in accordance with recommendations by the manufacturer. 9. Samples must be filtered through a 0.45 micron filter immediately after collection when a dissolved analysis is required. (See #4. above) 10.The sample container should be labeled at the time of collection with the facility name, well identification number and date and time collected. 11."Authorized agent' is any corporate officer or public official authorized by the company, corporation, or governmental body to sign official documents. �. Chemical & Environmental Technology, Inc. L'C EIV RECED/'-HNR ENVIRONMENTAL LAI3ORA(•'ir-6hgRfCW:W4SGLFING SERVICES r., 1en I, All n. 11 JOHN M. OGLE - R O. BOX 12298 \. PRESIDENT RESEARCH TRIANGLE PARK, N. C. 27709 PHONE (919) 467-3090 FAX (919) 467-3515 NATIONAL ELECTRICAL CARBON PO BOX 1868 504 N. ASH AVE. DUNN, NC 28334- Attn: NORB DICKMAN MONITORING WELLS FINAL REPORT OF ANALYSES REPORT DATE: 12/10/93 SAMPLE NUMBER- 78640 SAMPLE ID- MW-1 DATE SAMPLED- 11/18/93 DATE RECEIVED- 11/18/93 SAMPLER- M HOBGOOD TIME RECEIVED- 1630 DELIVERED BY- M HOBGOOD Page 1 of 1 ANALYSIS CHLORIDE CHEMICAL OXYGEN DEMAND pH IN FIELD TOTAL DISSOLVED SOLIDS SPECIFIC CONDUCTIVITY SULFATE DEPTH TO WATER TABLE TOTAL ORGANIC CARBON PROJECT NAME : MONT. WELLS SAMPLE MATRIX- GW TIME SAMPLED- 1455 RECEIVED BY-`DLP PRELIMINARY RESULTS ANALYSIS METHOD DATE BY RESULT UNITS PQL EPA 325.3 11/23/93 JTC 8 mg/L 1 EPA 410.4 11/29/93 JTC < 10 mg/L 10 EPA150.1 11/18/93 MNH 5.1 std units N/A EPA160.1 11/19/93 PLH 15 mg/L 1 EPA120.1 12/02/93 DLP 59 umhos 0.1 EPA375.3 11/29/93 JTC 3 mg/L 1 11/18/93 TMR 14.0 ft N/A 170.1 11/18/93 TMR 19.6 degrees C 0.1 EPA 415.2 12/08/93 JBR 3.0 mg/L 0.1 PQL = Practical Quantitation Limit Data qualifier, J, indicates an estimated value. The reported result is less than PQL.' LABORATORY DIRECTOR pV✓(il�� IN Facility Name Address or Use a balll--point peenn�and%ress firmly. lon/V Well Location d`"Ur J7_3rtL / /)-d' Well Identification Number Z= Z Well Depttt�2` Ft. Well DiameterSamplecreened) Interval Ft. To Ft. Depth to Water Level if. below measuring point (before sampling) Measuring point is 1' 2 ft. above land surface Gallons of water pumped/bailed before sampling Field Analysis: pH S• 3 Specific Conductance uMhos Temp. / 7—? oC Date Sample Collected - Q- Date Lab Sample Analyzed I I-Vcd 1-0 Laboratory Name + t ec SAMPLES FOR METALS WERE COLLECTED UNFILTERED AND FIELD ACIDIFIED COD Coliform: MF Fecal Coliform: MF Total add _ mg/I /100ml /100m1 (Note: Use MPN method for highly turbid samples) 0 Dissolved Solids: Total mgA pH (when analyzed), / units TOC 1,9 mgA Chloride mg/I Arsenic mgA Grease and Oils mgA Hardness: Total mgA Phenol mgA Sulfate I mg/I Specific Conductance 5"5 uMhos Total Ammonia mgA TKN as N mgA PERMIT NUMBER: (REQUIRED) Non-Dischar e NPDES J TYPE OF DISPOSAL OPERATION BEING MONITORED (REQUIRED) Lagoon Septic Tank/Drain Field Spray Field Subsurface Low -Pressure Piping (LPP) Land Application ( Rotary Distributor Odor Appearance (c9 3 Certification No. YES NO Nitrite (NO2) as N mgA Nitrate (NO3) as N mgA Phosphorus: Total as P mgA Al - Aluminum mgA Ba - Barium mgA Ca - Calcium mgA Cd - Cadmium mgA Chromium: Total mgA Cu - Copper mgA Fe - Iron mgA Hg - Mercury mgA K - Potassium mgA Mg - Magnesium mgA Mn - Manganese mgA Na - Sodium mgA Other 4 Ni - Nickel mgA Pb - Lead _�T mgA Zn - Zinc mgA Pesticides/Herbicides (Specify Compounds) =. ug/I ug/I - ug/I Other (Specify Compounds and ug/I Concentration units) ug/I rR...t.-� u /I VA '/ _ T . tr'u ' ,4 A�N wn �•1 — _ I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE. Note: Values should reflect dissolved and colloidal concentrations. (see #3 on back) �— �7� • See back for Instructions. Signature of Permittee ithZirized Agent') Date •• Submit blue, green, and yellow copies only to address above. GW-59 REV. 6/93 COLLECTION AND ANALYSIS OF GROUNDWATER SAMPLES 1. Samples should be analyzed as soon as possible after collection. SAMPLES WHICH ARE NOT ANALYSED WITHIN THE HOLDING TIME SPECI- FIED FOR THE METHOD USED (SEE #4. BELOW) MUST BE DISCARDED AND NEW SAMPLES COLLECTED. 2. Metals Analyses: Use Standard Method 3030C for sample preparation (mercury excluded). DO NOT FILTER METALS SAMPLES IN THE FIELD !!! Unfiltered samples must be collected for metals, then field acidified with 5 ml concentrated nitric acid per liter of sample, and should be submitted to the lab within 24 hours. Sample preparation in the laboratory (extraction and filtration) must be completed within 72 hours of collection. - 3. ANALYSES ARE TO BE MADE OF THE MOBILE CONSTITUENTS (DISSOLVED AS WELL AS COLLOIDAL) IN THE . -. GROUNDWATER, NOTTHOSE THAT ARE A PART OF SEDIMENT ASSOCIATED WITH WELL CONSTRUCTION OR SAMPLING PROCEDURES. CHECK WITH YOUR LABORATORY ON PROPER PROCEDURES FOR SAMPLE COLLECTION AND PRESERVATION. 4. As per Title 15, North Carolina Administrative Code, Subchapter 2L, analytical procedures shall be in accordance with the methods described in one of the following publications, or by other methods approved beforehand by the Director, Division of Environmental Management: (a) Standard Methods for the Examination of Water and Wastewater, 16th Edition, 1985 and 17th Edition, 1989, published jointly by American Public Health Association, American Water Works Association and Water Pollution Control Federation; (b) Methods for Chemical Analysis of Water and Waste, 1979, U.S. Environmental Protection Agency publication number EPA-600/4-79-020, as revised March 1983; (c) Test Methods for Evaluating Solid Wastes: Physical/Chemical Methods, 3rd Edition, 1986, U.S. Environmental Protection Agency publication number SW-846; (d) Test Procedures for the Analysis of Polluants Under the Clean Water Act, Federal Register Vol. 49, No. 209, 40 CFR Part 136, October 26, 1984; 5. Measure and record the depth of water in the well prior to pumping or bailing any water from the well. 6. At least 3 volumes of water in the well should be pumped or bailed prior to collecting a sample for analysis. If the well is pumped/bailed dry before 3 well volumes are removed, samples can be collected as soon as the well recovers to the point where enough water is available to collect your sample. 7. Determination for pH, Specific Conductance, temperature, odor and appearance must be made in the field on unfiltered samples when the sample is collected. 8. Field equipment must be calibrated in accordance with recommendations by the manufacturer. 9. Samples must be filtered through a 0.45 micron filter immediately after collection when a dissolved analysis is required. (See #4. above) 1 D.The sample container should be labeled at the time of collection with the facility name, well identification number and date and time collected. 11."Authorized agent" is any corporate officer or public official authorized by the company, corporation, or governmental body to sign official documents. L I G Chemical & Environmental Technology, Inc. ENVIRONMENTAL LABORATOFi-Y140�NG SERVICES :aa i 0 FM P: 7 f JOHN M. OGLE P. O. BOX 12298 PRESIDENT RESEARCH TRIANGLE PARK, N. C. 27709 PHONE (919) 467-3090 FAX (919) 467-3515 FINAL REPORT OF ANALYSES NATIONAL ELECTRICAL CARBON PO BOX 1868 504 N. ASH AVE. DUNN, NC 28334- Attn: NORB DICKMAN MONITORING WELLS -- REPORT DATE: 12/10/93 SAMPLE NUMBER- 78641 SAMPLE ID- MW-2 DATE SAMPLED- 11/18/93- DATE RECEIVED- 11/18/93 SAMPLER- M HOBGOOD TIME RECEIVED- 1630 DELIVERED BY- M HOBGOOD Page 1 of 1 ANALYSIS CHLORIDE CHEMICAL OXYGEN DEMAND pH IN FIELD TOTAL DISSOLVED SOLIDS SPECIFIC CONDUCTIVITY SULFATE DEPTH TO WATER TABLE TOTAL ORGANIC CARBON PROJECT NAME : MONT. WELLS SAMPLE MATRIX- GW TIME SAMPLED- 1510 RECEIVED BY- DLP ANALYSIS METHOD DATE BY RESULT UNITS PQL EPA 325.3 11/23/93 JTC 7 mg/L 1 EPA 410.4 11/29/93 JTC < 10 mg/L 10 EPA150.1 11/18/93 MNH 5.1 std units N/A EPkl60.l 11/19/93 PLH 20 mg/L 1 EPA120.1 12/02/93 DLP - 55 umhos - 0.1 EPA375.3 11/29/93 JTC 1 mg/L 1 11/18/93 TMR, 3.8 ft N/A 170.1 11/18/93 TMR 17.3 degrees C 0.1 EPA 415.2 12/06/93 JBR 1.9 mg/L 0.1 PQL --Practical Quantitation-Limit Data qualifier, J, indicates an estimated value. The reported result is less than PQL. LABORATORY DIRECTOR r. TEE Chemical & Environmental Technology, Inc. ENVIRONMENTAL LABORATORY AND CONSULTING SERVICES JOHN M. OGLE P. O. BOX 12298 PRESIDENT RESEARCH TRIANGLE PARK N. C. 27709 PHONE (919) 467-3090 FAX (919) 467-3515 METHOD REFERENCES Federal Register, Vol. 56, 40 CFR Part 136.3, October 8, 1991 --Metals, Inorganics, and Organics for groundwater and wastewater Federal Register, Vol. 56, 40 CFR Parts 141-1,43, January 30, 199�1 --Metals, Inorganics, and Organics for drinking water "Groundwater Section Guidelines foe the Investigation and Remediation of Soils and Groundwater", NCDEHNR, OEM, March 1993. --High Fraction Hydrocarbon and Low Fraction Hydrocarbon for groundwater and soil SW-846, Third Edition, November 1986 --Inorganics and Organics in soil or sludges. Metals in soil, sludge, or groundwater. (Metals in groundwater are digested by Method 3030C, Standard Methods, 17th Edition) 40 CFR Part 261, Appendix II and III --Toxic Characteristic Leaching Procedure Standard Methods, 17th Edition, 1989 --Total and Fecal Coliform in wastewater, streams, and lakes ,. l " a" _. I+nAUV Vt' GU0IUUT f r-l.rVl"SU tD2-A Woodwinds Industrial Ct. Cary, NC 27511 (919) 467-3090 ANALYSES REQUIRED CLIENT NAME: BILL TO: ADDRESS: PURCHASE ORDER NO: PRESERVED IN FIELD PRESERVATIVES PRESERVED IN LAB ❑ RECEIVED ON ICE z p d 6 REMARKS Z Z 2 2 2 ADDRESS: PHONE: PROJECT NO: PROJECT NAME: COLLECTED BY: (Signature) CNO. DA E IME P GRAB SAMPLE LD• corET nansns NS s >� x U -z s(3 �e 'RELINQUISHED BY (Signature) DATE TIME RECEIVED BY (Signature) RELINQUISHED BY (Signature) DATE TIME RECEIVED BY (Signature) 7% L N UIS D BY (Signature) DATE TIME RECEIVED FOR LABORATORY BY: DATE TIME REMARKS: /,J asr, I -� $�C, 'DEPORT COPY or Facility Name Address Well Location t5E7uE.CNSsrr�ta6 fh,Ja c FOB,<,arao Yowh Well Identification Number U-1 .1 Well Depth ZO Ft. Well Diameter 2 " Sample (Screened) Interval/s Ft. To ZO Ft. Depth to Water Level 11, 3 ft. below measuring point (before sampling) Measuring point is 3 ft. above land surfaceZ Gallons of water pumped/bailed before sampling PERMIT NUMBER: (REQUIRED) Non -Discharge NPDES n)L 0C>(o0 % 4 TYPE OF DISPOSAL OPERATION BEING MONITORED (REQUIRED) Lagoon Septic Tank/Drain Field Spray Field Subsurface Low -Pressure Piping (LPP) Land Application of Sludge / t ✓ Othe�r(JS ETrL ji) 6/�� E Rotary Distributor R�/'Gu,dG Ame Field Analysis: pH La, l Specific Conductance uMhos Temp. ZZ , I oC Odor Appearance Date Sample Collected �9 -Z-O -CA3 Date Lab Sam Z le Analyzed o Th S -3-`i3 Laboratory Name �rzitcn� �nlJiRo�rn�nlrfl� cA/Vo ocil Certification No. "I SAMPLES FOR METALS WERE COLLECTED UNFILTERED AND FIELD ACIDIFIED YES NO COD 2g mgA Coliform: MF Fecal /100ml Coliform: MF Total A00m1 (Note: Use MPN method for highly turbid samples) Dissolved Solids: Total q3 mgA pH (when analyzed) units TOC I, 5 mg/1 Chloride r 1 mg/I Arsenic mg/I Grease and Oils mg/I Hardness: Total mgA Phenol mgA Sulfate 5 mgA Specific Conductance uMhos Total Ammonia mgA. TKN as N mgA Nitrite (NO2) as N mgA Nitrate (NO3) as N mgA Phosphorus: Total as P mgA Al - Aluminum mgA Ba - Barium mgA Ca - Calcium mg/I Cd - Cadmium mg/I Chromium: Total mgA Cu - Copper mgA Fe - Iron mgA Hg - Mercury mg/I K - Potassium mg/I Mg - Magnesium mgA Mn - Manganese mgA Na - Sodium mgA Ni - Nickel mg/I Pb - Lead mgA Zn - Zinc mgA Pesticides/Herbicides (Specify Compounds) ug/I ug/I ug/I Other (Specify Compounds and ug/I Concentration units) ug/I ug/I Spa / I . I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE. c l ,let, Note: Values shouldt�Ilss9�riGe„� and (J n q colloidal concentratibn6.Qsee'�f3 on back) IJ/ % �-2�- /� • See back for instructions. Signature of Permlttee (or Abthorized Agent*) Date •` Submit blue, green, and yellow copies only to address above. GW-59 REV. 6/93 COLLECTION AND ANALYSIS OF GROUNDWATER SAMPLES 1. Samples should be analyzed as soon as possible after collection. SAMPLES WHICH ARE NOT ANALYSED WITHIN THE E HOLDING TIME SPECI- FIED FOR THE METHOD USED. (SEE #4. BELOW) MUST BE DISCARDED AND NEW SAMPLES COLLECTED. 2. Metals Analyses: Use Standard Method 3030C for sample preparation (mercury excluded)! DO NOT'FILTER METALS SAMPLES 10HE FIELD!!! Unfiltered samples must`be`colleCted for metals, then field acidified with 5 ml concentrated nitric acid per liter of sample; and -should be submitted to the lab within 24 hours. ; Sample preparation in the laboratory (extraction and filtration) must be completed within 72 hours of collection. - 3. ANALYSES ARE TO BE MADE OF THE MOBILE CONSTITUENTS (DISSOLVED AS WELL AS COLLOIDAL) IN THE GROUNDWATER; NOT THOSE THAT ARE A PART OF SEDIMENT ASSOCIATED WITH WELL CONSTRUCTION OR SAMPLING PROCEDURES. CHECK WITH YOUR LABORATORY ON PROPER PROCEDURES FOR SAMPLE COLLECTION AND PRESERVATION. 4. As per Title 15, North Carolina Administrative Code, Subchapter 2L, analytical procedures shall be in accordance with the methods described in one of the following publications, or by other methods approved beforehand by the Director, Division of Environmental Management: IP - (a) Standard Methods for the Examination of Water and Wastewater, 16th Edition, 1985 and 17th Edition, 1989, published jointly by American Public Health Association, American Water Works Association and Water Pollution Control Federation; (b) Methods for Chemical Analysis of Water and Waste,1979, U.S. Environmental Protection•Agency publication number EPA-600/4-79-020, as revised March 1983; (c) Test Methods for Evaluating Solid Wastes: Physical/Chemical Methods, 3rd Edition, 1986, U.S. Environmental Protection Agency publication number SW-846; . (d) Test Procedures for the Analysis of Polluants Under the Clean Water Act, Federal Register•Vol. 49, No. 209,. 40 CFR Part 136, October 26, 1984; 5. Measure and record the depth of water in the well prior to pumping or bailing any water from the well. 6. At least 3 volumes of water in the well should be pumped or bailed prior to collecting a sample for analysis. If the well is pumped/bailed dry before 3 well volumes are removed, samples can be collected as soon as the well recovers to the point where enough water is available to collect your sample. 7. Determination for pH, Specific Conductance, temperature, odor and appearance must be made in the field on unfiltered samples when the sample is collected., i 8. Field equipment must be calibrated in accordance with recommendations by the manufacturer. 9. Samples must be filtered through a 0.45 micron filter immediately after collection when a dissolved analysis is required. (See #4. above) 10.The sample container should be labeled -at the time of collection with the facility name, well identification number and date and time collected. 11."Authorized agent" is any corporate officer or public official authorized-by,ihe company, corporation, or governmental, body, to sign off icial'documents. or Facility Name -J N RI f oN<1 L Address 5504 AL L pen REG. Well Location 47o VoLLwili6, &,ln E. Tc,NrPbR GAEL Well Identification Number.— W `- Well Depth / 5' Ft. Well Diameter 2 Sample (Screened) Interval /3 Ft. To / 9 Ft. Depth to Water Level Z.9 ft. below measuring point (before sampling) Measuring point is 2 ft. above land surface Gallons of water pumped/bailed before sampling 3 PERMIT NUMBER: (REQUIRED) Non -Discharge NPDES W, 006oQrIL47 TYPE OF DISPOSAL OPERATION BEING MONITORED (REQUIRED) Lagoon Septic Tank/Drain Field Spray Field Subsurface Low -Pressure Piping (LPP) Lard Application of Sludge / Other //S�ETLI AIG/1 6 Rotary Distributor Field Analysis: pH (D. l Specific Conductance uMhos Temp. � • 0 °C Odor Appearance Date Sample Collected rl^2 0 ; `I3 Date Lab Sample Analyzed 7-Z o -93 ; o S 3-`f3 R „1/�I _ Laboratory Name C,d cn� £�NJ�Qo�In.,E �rnl /£ F/nJOc.0GY Certification No. ,'-��(1 �; ]� �5 r SAMPLES FOR METALS WERE COLLECTED UNFILTERED AND FIELD ACIDIFIED YES NO jyC=� r, ' ) i COD SS mgA Coliform: MF Fecal /100ml Coliform: MF Total A00ml (Note: Use MPN method for highly turbid samples) Dissolved Solids: Total 33 mg/I pH (when analyzed) units TOC 4 mg/I Chloride S mg/I Arsenic mg/I Grease and Oils mg/I Hardness: Total mgA Phenol mg/l Sulfate 4 mg/l Specific Conductance uMhos Total Ammonia mg/I TKN as N mg/l Nitrite (NO2) as N mg/l Nitrate (NO3) as N mg/I Phosphorus: Total as P mg/I AI - Aluminum mg/I Ba - Barium mg/I Ca - Calcium mg/I Cd - Cadmium mg/I Chromium: Total mgA Cu - Copper mg/I Fe - Iron mg/I Hg - Mercury mg/l K - Potassium mg/l Mg - Magnesium mg/l Mn - Manganese mg/I Na - Sodium mg/I Ni - Nickel mgA Pb - Lead rl 4ri J'v; m A Zn - Zinc Per C-F n'T 1QAl mg/I Pesticides/Herbicides (Specify Compounds) ug/I ug/I ug/I Other (Specify Compounds and ug/I Concentration units) ug/I ug/I I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE. Note: Values should reflect dissolved and �^ }'/�/ /� L p colloidal concentrations. (see #3 on back) U Vv' V /` (466") p�23 ^ %,�j See back for instructions. Signature of Permitta (or Authorized Agent') Date •• Submit blue, green, and yellow copies only to address above. GW-59 REV. 6/93 COLLECTION AND ANALYSIS OF GROUNDWATER SAMPLES 1. Samples should be analyzed as soon as possible after collection. SAMPLES WHICH ARE NOT ANALYSED WITHIN THE HOLDING TIME SPECI- FIED FOR THE METHOD USED (SEE #4. BELOW) MUST BE DISCARDED AND NEW SAMPLES COLLECTED. 2. Metals Analyses: Use Standard Method 3030C for sample preparation (mercury excluded).'DO NOT FILTER METALS SAMPLES IN THE FIELD M Unfiltered samples must be,collected for metals, then field acidified with 5 ml concentrated nitric acid per liter of sample, and -should be submitted to the lab within 24 hours. Sample preparation in the, laboratory (extraction and filtration) must be completed within 72 hours of collection.. _ .. 3. ANALYSES ARE TO BE MADE OF THE MOBILE CONSTITUENTS (DISSOLVED AS WELL AS COLLOIDAL) IN THE GROUNDWATER, NOT THOSE THAT ARE A PART,t7F SEDIMENT ASSOCIATED WITH WELL CONSTRUCTION OR SAMPLING PROCEDURES. CHECK WITH YOUR LABORATORY ON PROPER PROCEDURES FOR SAMPLE COLLECTION AND PRESERVATION. 4. Asper Title 15, North Carolina Administrative Code, Subchapter 2L, analytical procedures shall be in accordance with the methods described in one of the following publications, or by other methods approved beforehand by the Director, Division of Environmental I - Management _ _ _... _ . 7 (a) Standard Methods for the Examination of Water and Wastewater, 16th Edition, 1985 and 171h Edition, 1989, published jointly by American Public Health Association, American Water Works Association and Water Pollution Control Federation; (b) Methods for Chemical Analysis of Water and Waste,1979, U.S. Environmental Protection•Agency publication number EPA-600/4-79-020, as revised March 1983; (c) Test Methods for Evaluating Solid Wastes: Physical/Chemical Methods, 3rd Edition, 1986, U.S. Environmental Protection Agency publication number SW-846; (d) Test Procedures for the Analysis of Polluants Under the Clean Water Act, Federal Register Vol. 49, No. 209, 40 CFR Part 136, October 26, 1984; 5. Measure and record the depth of water in the well prior to pumping or bailing any water from the well. 6. At least 3 volumes of water in the well should be pumped or bailed prior to collecting a sample for analysis. If the well is pumped/bailed dry before 3 well volumes are removed, samples can be collected as soon as the well recovers to the point where enough water is available to collect your sample. 7. Determination for pH, Specific Conductance, temperature, odor and appearance must be made in the field on unfiltered samples when the sample is collected. 8. Field equipment must be calibrated in accordance with recommendations by the manufacturer. 9. Samples must be filtered through a 0.45 micron filter immediately after collection when a dissolved analysis is required. (See #4. above) 10.The sample container should be labeled at the time of collection with the facility name, well identification number and date and time collected. 11."Authorized agent' is any corporate officer or public official authorized by the company, corporation, or governmental body to sign official documents. or Use a ball-point pen Facility Name Address press Well Location t5F-rwC£,J riOL.iSNIN6 r"o^)P Well Identification Number k/ Well Depth 20 Ft. Well Diameter ?—" Sample (Screened) Interval rs Ft. To 20 Ft Depth to Water Level %O. 4 ft. below measuring point (before sampling) Measuring point is 3 ft. above land surface Gallons of water pumped/bailed before sampling 2 PERMIT NUMBER: (REQUIRED) Non -Discharge NPDES n/9e 0or�o rI y TYPE OF DISPOSAL OPERATION BEING MONITORED (REQUIRED) Lagoon Septic Tank/Drain Field Spray Field Subsurface Low -Pressure Piping (LPP) Land Application of Sludge _ ✓ Other SE'TTr-tNG^ � Rotary Distributor PnL r`<,,lA Field Analysis: pH 5,3 Specific Conductance uMhos Temp. /7 z °C Odor Appearance Date Sample ColleQted 3 VIRoHDateLLab� le AnGlYzed3-31 -4-5-93 Laboratory NameCIlEEENS�0a0Certification No. q6 SAMPLES FOR METALS WERE COLLECTED UNFILTERED AND FIELD ACIDIFIED YES NO COD / v mg/1 Coliform: MF Fecal /100ml Coliform: MF Total /100m1 (Note: Use MPN method for highly turbid samples) Dissolved Solids: Total 44 mg/I pH (when analyzed) units TOC 10•7 mg/l Chloride 7 mgA Arsenic mgA Grease and Oils mgA Hardness: Total mgA Phenol mgA Sulfate mgA Specific Conductance (A.5 uMhos Total Ammonia mgA TKN as N mgA Nitrite (NO2) as N mg/l Nitrate (NO3) as N mgA Phosphorus: Total as P mgA Al - Aluminum mg/I Ba - Barium mgA Ca - Calcium mg/l Cd - Cadmium mgA Chromium: Total mgA Cu - Copper mgA Fe - Iron mg/l Hg - Mercury mgA K - Potassium mg/l Mg - Magnesium mgA Mn - Manganese mg/l Na - Sodium mgA Ni - Nickel Pb - Lead Zn - Zinc Pesticides/Herbicides (Specify Compounds) Other (Specify Compounds and Concentration units) mgA mgA mgA ug/I ug/I ug/I ug/l ug/I ug/l I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE. Note: Values should reflect dissolved and crr 7 colloidal concentrations. (see #3 on back) See back for instructions. Signature of Per ttee (or horize Agent') Date •• Submit blue, green, and yellow copies only to address above. GW-59 REV. 6/93 COLLECTION AND ANALYSIS OF GROUNDWATER SAMPLES 1. Samples should be analyzed as soon as possible after collection. SAMPLES WHICH ARE NOT ANALYSED WITHIN THE HOLDING TIME SPECI- FIED FOR THE METHOD USED (SEE #4. BELOW) MUST BE DISCARDED AND NEW SAMPLES COLLECTED. 2. Metals Analyses: Use Standard Method 3030C for sample preparation (mercury excluded). DO NOT FILTER METALS SAMPLES IN THE FIELD H! Unfiltered samples must be collected for metals, then field acidified with 5 ml concentrated nitric acid per liter of sample, and should be submitted to the lab within 24 hours. Sample preparation in the laboratory (extraction and filtration) must be completed within 72 hours of collection. 3. ANALYSES ARE TO BE MADE OF THE MOBILE CONSTITUENTS (DISSOLVED AS WELL AS COLLOIDAL) IN THE GROUNDWATER, NOT THOSE THAT ARE A PART OF SEDIMENT ASSOCIATED WITH WELL CONSTRUCTION OR SAMPLING PROCEDURES. CHECK WITH YOUR'LABORATORY ON PROPER PROCEDURES FOR SAMPLE COLLECTION AND PRESERVATION. 4. As per Title 15, North Carolina Administrative Code, Subchapter 2L, analytical procedures shall be in accordance with the methods described in one of the following publications, or by other methods approved beforehand by the Director, Division of Environmental Management: (a) Standard Methods for the Examination of Water and Wastewater, 16th Edition, 1985 and 17th Edition, 1989, published jointly by American Public Health Association, American Water Works Association and Water Pollution Control Federation; (b) Methods for Chemical Analysis of Water and Waste, 1979, U.S. Environmental Protection Agency publication number EPA-600/4-79-020, as revised March 1983; (c) Test Methods for Evaluating Solid Wastes: Physical/Chemical Methods, 3rd Edition, 1986, U.S. Environmental Protection Agency publication number SW-846; (d) Test Procedures for the Analysis of Polluants Under the Clean Water Act, Federal Register Vol. 49, No. 209, 40 CFR Part 136, October 26, 1984; 5. Measure and record the depth of water in the well prior to pumping or bailing any water from the well. 6. At least 3 volumes of water in the well should be pumped or bailed prior to collecting a sample for analysis. If the well is pumped/bailed dry before 3 well volumes are removed, samples can be collected as soon as the well recovers to the point where enough water is available to collect your sample. 7. Determination for pH, Specific Conductance, temperature, odor and appearance must be made in the field on unfiltered samples when the sample is collected. 8. Field equipment must be calibrated in accordance with recommendations by the manufacturer. 9. Samples must be filtered through a 0.45 micron filter immediately after collection when a dissolved analysis is required. (See #4. above) 10.The sample container should be labeled at the time of collection with the facility name, well identification number and date and time collected. 11."Authorized agent' is any corporate officer or public official authorized by the company, corporation, or governmental body to sign official documents. or Facility Name Address LAL pen ((vN Conty- - liA2n1£^7 Well Location t ACCN is Pu,*L INU6 clih L Tu.NiPER GReLK Well Identification Number W 2 Well Depth / S Ft. Well Diameter 2 " Sample (Screened) Interval /3 Ft. To If Depth to Water Level Z. 5 ft. below measuring point (before sampling) Measuring point is 2 ft. above land surface Gallons of water pum ed/bailed before sampling 3 PERMIT NUMBER: (REQUIRED) Non-Dischar�gge NPDES l L 00 (o O rj TYPE O_ OF DISPOSAL OPERATION BEING MONITORED (REQUIRED) Lagoon Septic Tank/Drain Field Spray Field Subsurface Low -Pressure Piping (LPP) Land Application of Sludge _ r =Other Se7TL1N6/1 E Rotary Distributor A, cu�.Vr Tn.J Field Analysis: pH 12. Specific Conductance uMhos Temp. 5. 3 oC Odor Appearance Date Sample Collected 3 - 30- 93 Date Lab Sa�mple Analyzed_3 31 ro y 15 AS Laboratory Name CH6M,ca'- LCNvlaonlr C^17-4� 7£c�I�IaoGS� Certification No. SAMPLES FOR METALS WERE COLLECTED UNFILTERED AND FIELD ACIDIFIED YES NO COD /0 mgA Coliform: MF Fecal A00m1 Coliform: MF Total /100m1 (Note: Use MPN method for highly turbid Dissolved Solids: Total samples) Uy mgA pH (when analyzed) units TOC S•9 mg/I Chloride 7 mg/I Arsenic mgA Grease and Oils mg/I Hardness: Total mgA Phenol mgA Sulfate mgA Specific Conductance 0, 0 uMhos Total Ammonia mg/I TKN as N mgA Nitrite (NO2) as N mgA Nitrate (NO3) as N mgA Phosphorus: Total as P mgA Al - Aluminum mg/I Ba - Barium mg/I Ca - Calcium mgA Cd - Cadmium mg/1 Chromium: Total mgA Cu - Copper mgA Fe - Iron mgA Hg - Mercury mg/I K - Potassium mgA Mg - Magnesium mgA Mn - Manganese mgA Na - Sodium mgA I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE. & k.�L �? — Signature of Permit ee (or Au orized Agent*) Date GW-59 REV. 6/93 Ni - Nickel Pb - Lead mgA mgA Zn - Zinc Pesticides/Herbicides (Specify Compounds) mg/1 ug/1 ug/I ug/I Other (Specify Compounds and Concentration units) ug/I ug/I ug/1 Note: Values should reflect dissolved and colloidal concentrations. (see #3 on back) • See back for instructions. •' Submit blue, green, and yellow copies only to address above. COLLECTION AND ANALYSIS OF GROUNDWATER SAMPLES 1. Samples should be analyzed as soon. as possible after collection. SAMPLES WHICH ARE NOT ANALYSED WITHIN THE HOLDING TIME SPECI- FIED FOR THE METHOD USED (SEE 94.,BELOW) MUST BE DISCARDED AND NEW SAMPLES COLLECTED. 2. Metals Analyses: Use Standard Method 3030C for sample preparation (mercury excluded). DO NOT FILTER METALS SAMPLES IN THE\FIELD IIt Unfiltered samples must be collected for metals, then field acidified with 5 ml concentrated nitric acid per liter of sample,'and'should be submitted to the lab within 24 hours. Sample preparation in the laboratory (extraction and filtration) must be completed within 72 hours of collection. ' 3. ANALYSES ARE TO BE MADE OF THE MOBILE CONSTITUENTS (DISSOLVED AS WELL AS COLLOIDAL) IN THE GROUNDWATER, NOT THOSE THAT ARE A PART._F SEDIMENT ASSOCIATED WITH WELL CONSTRUCTION OR SAMPLING CHECK WITH YOUR LABORATORY ON PROPER PROCEDURES FOR SAMPLE COLLECTION AND PRESERVATION. - 4. As per Title 15, North Carolina Administrative Code, Subchapter 2L, analytical+procedures shall be in accordance with the methods'described in one of the following publications, or by other methods approved beforehand by the Director, Division of Environmental Management: (a) Standard Methods for the Examination of Water and Wastewater, 16th Edition, 1985 and 17th Edition, 1989, published jointly by American Public Health Association, American Water Works Association and Water Pollution Control Federation; (b) Methods for Chemical Analysis of Water and Waste, 1979, U.S. Environmental Protection Agency publication number EPA-600/4-79-020, as revised March 1983; (c) Test Methods for Evaluating Solid Wastes: Physical/Chemical Methods, 3rd Edition, 1986, U.S. Environmental Protection Agency publication number SW-846; (d) Test Procedures for the Analysis of Polluants Under the Clean Water Act, Federal Register Vol. 49, No. 209, 40 CFR Part 136, October 26, 1984; P. 5. Measure and record the depth of water in the well prior to pumping or bailing any water from the well. 6. At least 3 volumes of water in the well should be pumped or bailed prior to collecting a sample for analysis. If the well is pumped/bailed dry before 3 well volumes are removed, samples can be collected as soon as the well recovers to the point where enough water is available to collect your sample. 7. Determination for pH, Specific Conductance, temperature, odor and appearance must be made in the field on unfiltered samples when the sample is collected. I , 8. Field equipment must be calibrated in accordance with recommendations by the manufacturer. 9. Samples must be filtered through a 0.45 micron filter immediately after collection when a dissolved analysis is required. (See #4. above) 10.The sample container should be labeled at the time of collection with the facility name, well identification number and date and time collected. 11."Authorized agent" is any corporate officer or public official authorized by -the company, corporation, or governmental body,to sign, official documents. T JOHN M. OGLE PRESIDENT Chemical & Environmental Technology, Inc. ENVIRONMENTAL LABORATORY AND CONSULTING SERVICES C:. SEP 1 1993 ENV. MANAGEMENT FAYETTEVILLE PEG. OFFICE Division of Environmental Management Mr. -Michael Dauterman, E.I.T. FayettevilleRegi'onal office Wachovia Building, -Suite 714 Fayetteville, NC 28301-5043 P. O. BOX 12298 RESEARCH TRIANGLE PARK, N. C. 27709 PHONE (919) 467-3090 FAX (919) 467-3515 August 31, 1993 Re: Groundwater Monitoring-Morganite, Inc. Permit # NCO060747 Dunn, Harnett County Dear Mr. Dauterman: Enclosed, please find form'GW-59 monitoring form for Morganite, Inc. for --the. month' -Of April, 1993. _ Subsequent --monitoring well forms will be sent to:'the Division of Environmental Management Central office in Raleigh. If you have any further questions or concerns please do not hesitate to call me at (919) 467-3090. . Don R. Pangle operator -in- Charge DRP/dlp cc: J.B. Vick, Morganite, Inc. Norb Dickman, Morganite, Inc. GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM Facility Name Address SOf/ Al 0-U5, Ale - Well Location For additional forms please write or call: VDlvislon of Environmental Management Groundwater Section P.O. Box 27687 Raleigh, NC 27611-7687 (919)733-3221 County 04,1011eif- PERMIT NUMBER: (REQUIRED) Non -Discharge Well Identification Number 4Je/l gl Well Depth Zo Ft. 1 rrt ur 11R5 (REQUIRED) Well Diameter " Sample (Screened) Interval *'S- Ft. TOZo Ft. _ Lagoon Depth to Water Level 'W.8 it. below measuring point. (before sampling) I — Spray Field TION — Septic Tank/Drain Field Subsurface Low -Pressure MeasuringPiping (LPP) point is _� feet above land surface Land Application of sludge �.4 other i .PiAio Gallons of water pumped/bailed before sampling — Rotary Distributor I Field Analysis: pH G• l`- Specific Conductance uMhos Temp. /! °C Odor�/✓owl Appearanceeeaqc- Date Sample Collected //-/8-9:!`_� Date Lab Sample Analyzed Laboratory Name ex'n102op r '&imz D Certification No. 96 COD < mg/I NO2 as N mg/I Ni Nickel mg/1 Coliform: MF Fecal /100ml NO3 as N mg/I Pb Lead mg/I Coliform: MF Total /100ml Dissolved Solids: Total %`% mg/I pH (when analyzed) units TOC -3 mg/1 Chloride 8 mg/1 Arsenic mg/I Grease and Oils mg/1 Hardness: Total mg/I Phenol mg/I Sulfate mg/I Specific Conductance eS uMhos Total Ammonia(NH3 + NH 4) mg/1 TKN as N mg/I Phosphorus: Total as P mg/I AI - Aluminum mg/I Be - Barium mg/I Ca Calcium Zn - Zinc mg/I Pesticides/Herbicides (Specify Compounds) ug/1 ug/I Cd - Cadmium mg/I - ug/1 Chromium: To!talln I Other [Specify) `. ug/I Cu - Copper t D.t f, 11 ug/1 Fe - Iron DEC 31 f999mg I- ug/I OE �� Hg - Mercury Rqf ug/I K - Potassium CAYETTEVII LF REG. Q§4jCF �icv1�M Q�-.(1 SECTION ug/I Mg - Magnesium mg/I Mn - Manganese mg/1 Na - Sodium mg/I I CERTIFY ZTHTHIS REPORT IS TRUE AND ACCURATE. S AT E OF P .. I EE (OR AUTHO IZED AGENT-) DATE OT • Values should reflect dissolved concentrations (See #2. on reverse) * See back for Instructions. ** Submit blue, green, and yellow copies � to address above. COLLECTION AND ANALYSIS OF GROUNDWATER SAMPLES 1. Samples should be analyzed as soon.as possible after collection. SAMPLES WHICH ARE NOT ANALYSED WITHIN THE HOLDING TIME SPECIFIED FOR THE ME;THOD,U.SED (SEE 0. BELOW) MUST BE DISCARDED AND NEW SAMPLES COLLECTED. 2. ANALYSES ARE TO BE MADE OF THE CONSITITUENTS DISSOLVED IN THE GROUNDWATER, NbT `THOSE THAT ARE A PART OF, OR ADSORBED ONTO, SOIL/SEDIMENT PARTICLES. CHECK WITH YOUR LABORATORY ON PROPER PROCEDURES FOR SAMPLE COLLECTION AND`PRESERVATION. 3. As per Title 15, North Carolina Administrative Code, Subchapter 2L, analytical procedures shall be in accordance with the methods described in one of the following publications, or by other methods approved beforehand by the Director, Division of Environmental Management: ' ;, \(a) Standard methods far the Examination of Water and Wastewater, 16th Edition, 1985, published jointly by American Public Health Association, American Water Works Association and Water Pollution Control Federation; (b) Methods•fgr.,Chemical Analysis of Water and Waste, 1979, U.S. Environmental Protection Agency publication number EPA-600/4-79-20, as revised,March 1983; (c) Test Methods for Evaluating Solid Wastes: Physical/Chemical Methods; 3rd Edition,.1986, U.S. Environmental Protection Agency publication number SW-846; (d) Test Procedures for.the Analysis of Polluants Under the Clean Water Act, Federal Register Vol. 49, No. 209, 40 CFR Part 136, October 26, 1,984; 4. Measure and record the depth of water in the well prior to pumping or bailing any water from the well. 5. At least 3 volumes of water in the well should be pumped or bailed prior to collecting a sample for analysis. If the well is pumped/bailed dry before 3 well volumes are removed, samples can be collected as soon as the well recovers to the point where enough water is available to collect your sample. 6. , Determination torpH„ Specific Conductance; temperature, odor and appearance must be made in the field on unfiltered samples when the sample,s ciollected. 7.' Field eo,uipment must be calibrated in accordance with recommendations by.the manufacturer. 8. Samples mAl be filtered through a 0,45 micron filter immediately after collection when a dissolved analysisls required. (See #3. above) 9. The sample container should be labeled at -the time of collection with the facility name, welt identification number and date and time col- lected. 10."Authorized agent' is any corporate officer, br_ public official .authorized by the company; corporation, .or. governmental body to sign official documents. -a G%OUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM Division of Environmental Management Groundwater Section P.O. Box 27687 Raleigh, NC 27611-7687 For additional forms please write or call: (919)733-3221 Facility Name Address .34y /!z- i3's.1e. oVVe �aw.J y Aj'C o?83StD Well Location G%2= ae�e.J�oe�i/firw� .n�a/ w� Ja.�iou GiCee.� Well Identification Number LcJe// » 2 Well Depth /-P Ft. Well Diameter ' ~ Sample (Screened) Intervall Ft. To/9_Ft. Depth to Water Level 7 B ft. below measuring point. (before sampling) Measuring point is Z feet above land surface County 4VZA/e>r PERMIT NUMBER: (REQUIRED) Non -Discharge — Lagoon — Spray Field Land Application of Sludge :10, — Septic Tank/Drain Field — Subsurface Low -Pressure Gallons of water pumped/bailed before sampling L — Rotary Distributor �— Field Analysis: pH le.S� Specific Conductance uMhos Temp. °C Odor -sue Appearance /QO� Date Sample Collected Date Lab Sample Analyzed /z- 7-93— 4 Laboratory Name tAe.c� +' F.eldic0 /ee/ �L Certification No'. 9 COD Ic- /D mg/I NO2 as N Coliform: MF Fecal /100ml NO3 as N Coliform: MF Total /100ml Phosphorus: Total as P Dissolved Solids: Total 8/ mg/I Al - Aluminum PH (when analyzed) units. Ba - Barium TOC .Z . O mg/I Ca - Calcium Chloride B mg/I Arsenic mg/I Grease and Oils mg/I Hardness: Total mg/I Phenol mg/I Sulfate �'Z mg/I Specific Conductance 6S uMhos Total Ammonia(NH3 • NH y) TKN as N Cd - Cadmium mg/I Ni Nickel mg/I mg/I PbLead mg/I mg/I Zn Zinc mg/I mg/I Pesticides/Herbicides.(Specify Compounds) mg/I ma/I Chromium: Total Cu - Copper Fe Iron 00 DEC 31 1gg2 �`/I� . Hg - Mercury mg/( K - Potassium EN3/ MANAGEMEbffg/I Mg - Magnesium FAYETTEVILLE REG. Off) f mg/I Mn - Manganese mg/I Na - Sodium_ I C RTTIIFY THAT J IS REPORT IS TRUE AND ACCURATE. SI E OF PEP. E (OR AUTHORIZED AGENT') DATE r. / 1n nov 11nn mg/I mg/I Other (Specify) NO E. Values shouldrrefwa dissolved concentrations . (See#2. on reverse) ug/I ug/I ug/1 ug/I ti ug/I ug/I ug/I See back for Instructions. " Submit blue, green, and yellow copies Qft to address above. COLLECTION AND ANALYSIS OF GROUNDWATER SAMPLES 1.-Samples should be analyzed.as soon as possible after collection. SAMPLES WHICH ARE NOT ANALYSED WITHIN THE HOLDING TIME SPECIFIED FOR THE METHOD USED (SEE #3. BELOW) MUST BE DISCARDED AND NEW,SAMPLES�CQLLECTED. 2. ANALYSES ARE TO' BE MADE OF THE CONSITITUENTS DISSOLVED IN THE GROUNDWATER; NOT THOSE THAT ARE A PART - OF, OR ADSORBED ONTO, SOIL/SEDIMENT PARTICLES. CHECK WITH YOUR LABORATORY ON PROPER PROCEDURES FOR SAMPLE COLLECTION AND PRESERVATION. ., 6 , 3. As per Title 15, North Carolina Administrative Code, Subchapter 2L, analytical procedures shall be in accordance with the methods described in one of the following publications, or by other methods approved beforehand by the Director, Division of Environmental - Management: " ,(a) Standard methods for the Examination of Water and Wastewater, 16th Edition, 1985, published jointly by American Public Health Association, American Water Works Association and Water Pollution Control Federation; (b) Methods.for Chemical Analysis of:Water and Waste, 1979, U.S. Environmental Protection Agency publication number EPA-600/4-79-020, as revised.March 1983; (c) Test Methods for Evaluating Solid Wastes: Physical/Chemical Methods, 3rd Edition, 1986; U.S,. Environmental Protection Agency publication number SW-846; (d) Test Procedures for the Analysis of Polluants Under the Clean Water Act, Federal Register Vol. 49-, No. 209, 40 CFR Part 136, October 26, 1984; 4. Measure and record the depth of water in the well prior to pumping or bailing any water from the well. 5. At least 3 volumes of water in the well should be pumped or bailed prior to collecting a sample for analysis. If the well is pumped/bailed dry before 3 well volumes are removed, samples can be collected as soon as the well recovers to the point where enough water is available to collect your sample. 6. Determination for pH, Specific Conductance, temperature; odor and'ao' arance must be made in the field on unfiltered samples when the samoWis collected. 7. Field; equipment must:be calibrated in accordance with recommendations by the manufacturer.. S. Samples'm st pe'f iltered4hrough a 0.45 micron' filter immediately after�oollection when a dissolved analysis is required..(See #3. above) - 9. The sample container should be.labeled at the time. of collection with the facility name, Well identification number and date and time col- lected. 10."Authorized agent" is any corporote:officeror public official authorized bythe.cotnpany, corporation,_or governmental body' to sigp-official documents: GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM J VI'(Division of Environmental Management � �j ic)C/7 Groundwater Section P!O�Rox 27687 For additional forms-pl6140.1Frkprucal1:Oyice, 27611-7687 Facility Name / i 9 of County Pc/e �-" �[,_ ' ' Address SOfl '✓ �S/fe amide �D. aor /}Y�� PERMIT NUMBER: (REQUIRED) ' Nn ��_ 4/ I Non -Discharge ZMAYEV'df Well Location WJ_° Well Identification Number CJe// °'i1 Well Depth •aa Ft. Well Diameter e?*JGfer Sample (Screened) Interval!!r- Ft. To 3,0 Ft. Depth to Water Level /.P8 ft. below measuring point. (before sampling) Measuring point is �3 feet above land surface Gallons of water pumped/bailed before sampling Lagoon Spray Field Land Application of Sludge V BEING MONITORED — Septic Tank/Drain Field — Subsurface Low -Pressure Piping (LPP) Field Analysis: pH -5- 3 Specific Conductance uMhos Temp. Flo oC Odor `✓Ne- Appearance 4'/ea1Z- Date Sample Collected mzzenz Y Date Lab Sample Analyzed /i3 74?�30 Laboratory Name COD <'/a mg/I Coliform: MF Fecal /100ml Coliform: MF Total /100ml Dissolved Solids: Total � mg/I PH Cwhen analyzed) units TOC 30 mg/I Chloride 9 mg/I Arsenic Grease and Oils Hardness: Total mg/I mg/I mg/I Phenol mg/I Sulfate If mg/I Specific Conductance .S9 uMhos' Total Ammonia(NH3 + NH q) mg/I TKN as N mg/I Certification No. NO2 as N mg/I NO3 as N mg/I Phosphorus: Total as P mg/I Al - Aluminum mg/I Be - Barium mg/I Ca. - Calcium mg/I Cd - Cadmium mg/I Chromium: Total mo/I Cu - Copper mg/I Fe - Iron mg/I Hg - Mercury mg/I K - Potassium Mg - Magnesium mg/I Mn - Manganese mg/I Na - Sodium mg/I I CERTI Y THAT THI EPORT IS TRUE AND ACCURATE. z -9y SIGNAT RE TF PERMITT8E (O AUTHORIZED AGENT') DATE Ni Nickel mg/I Pb Lead mg/1 Zn Zinc me/I Pesticides/Herb icides, (Specify Compounds) ug/I . ug/I ug/1 Other (Specify) ug/I ^ r ug/I r ug/I 26 I ug/I NOTE: f7d.L'FIL3FI; yr,' Values should reflect dissolved concentrations (See #2. on reverse) See back for Instructlons. " Submit blue, green, and yellow copies 2ft to address above. 1. Samples should be analyzed as soon aslpossible after collection. SAMPLES WHICH ARE NOT ANALYSED WITHIN THE HOLDING TIME SPECIFIED FOR THEM T,HOD USED (SEE #3. BELOW) MUST BE;DISCARDEP. AND NEW, SAMPLES COLLECTED. 2. ANALYSES ARE TO BE MADE OF THE CONSITITUENTS DISSOLVED IN THE GROUNDWATER, N&TAOSE THAT ARE A PART OF, OR ADSORBED ONTO, SOIL/SEDIMENT PARTICLES. CHECK WITH YOUR CABt9FiATORY ON RROPER'PRO'CEDURES FOR SAMPLE COLLECTIQN AND PRESERVATION. 3. Asper Title 15, North Carolina Administrative Code, Subchapter 2L, analytical,procedures shad be in accordance *ith-the methods •. described in one of the following publications, or by other methods approved beforehand by the Director, Division. of Environmental Management: `:,,(a) Standard methods for'the Examination of Water and Wastewater, 16th Edition, 1985, published -jointly by American Public Health Association, American Water Works Association and Water Pollution Control Federation; (b) Methods for,;C.hemical Analysis of1(Vater and Waste, 1979, U.S. Environmental Protectiorj Agency publication.number EPA-600l4-79-020, as revised March 1983; (c) Test Methods for Evaluating Solid Wastes: Physical/Chemical Methods, 3rd Edition, 1986, U.S. Environmental Protection Agency publication number SW-846; . , . • _ . - h; . - ` (d) Test Procedures for the Analysis of Polluants Under the Clean Water Act; Federal. Register Vol. 49, No. 2'09, 40 CFR Part 136, October 26, 1984; 4. Measure and record the depth of water in fhe well prior to pumping or bailing any water from the well. - 5. At least 3 volumes of water in the well should be pumped or bailed prior to collecting a sample for analysis. If the well is pumped/bailed dry before 3 well volumes are removed, samples can be collected as soon as the well recovers to the point where enough water is available to collect.your sample. 6. Determination for pH, Specific Conductance, temperature, odor and appearance must be made, in the field on unfiltered samples, when the sample is collected.' 7. Field equipment must be calibrated in accordance with recommendations by the: manufacturer. 8. Samples must be filtered through a 0.45 micron filterimmediately, after collection when a dissolVed'analysis`is required. (See #3.:above) 9.- The sample container is iould be'Jabeled at the time 'of .collection with the facility,hame,well identification number and date and time col lected. 10."Authorized agent"'is any corporate officer or,public official authorized by the company, corporation, or governmental body to sign official documents. ; RFC, VED GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM Division of Environmental Management JUN Z 9 19c�n GroundwaterP.O.Bo27687lon .O. Box 27687 Raleigh-,NC-27611-7687 For additional formsalenaseryv 0(�S�IL'(919)733-3221 Facility Name - Address Well Location Well Identification Number Zile// � L Well Depth /y Ft. Well Diameter _a?irier Sample (Screened) Interval /3 Ft. TO.1,P Ft. Depth to Water Level _;z 3 it. below measuring point. (before sampling) Measuring point is feet above land surface Gallons of water pumped/bailed before sampling County 7fiaXAI'e'� PERMIT NUMBER: (REQUIRED) Non -Discharge NPDES �P OOGG7s — Lagoon Spray Field Land Application of Sludge G. — Septic Tank/Drain Field — Subsurface Low -Pressure Piping (LPP) ,,/ '/ Field Analysis: pH BLS Specific Conductance uMhos Temp. oC Odor_r:4 Appearance C7XeQ�4— Date Sample Collected -:—/_�P>92-- Date Lab Sample Analyzed Laboratory Name e.oic,li -Y �.rJdi�Ivµ<,J7/aP �orc,!' Certification No. 9� COD /% mg/I NO2 as N mg/I Ni - Nickel mg/I Coliform: MF Fecal /100ml NO3 as N mg/1 Pb Lead mg/I Coliform: MF Total /100ml Phosphorus: Total as P mg/I Zn Zinc mg/I Dissolved Solids: Total `><3 mg/I AI - Aluminum mg/1 Pesticides/Herbicides (Specify Compounds) pH (when analyzed) units Ba - Barium mg/I TOC Z. r% _ Ca - Calcium mg/I /m¢/I Chloride /0 � ma!I Cd - Cadmium mg/I Arsenic mg/I Chromium: Total mg/I Grease and Oils mg/I Cu - Copper mg/I Hardness: Total mg/I Fe - Iron mg/I Phenol mg/I Hg - Mercury mg/I Sulfate 3 mg/I K - Potassium mg/I Specific Conductance S uMhos Mg - Magnesium mg/I Total Ammonia(NH3 + NH 4) mg/I Mn - Manganese mg/I TKN as N mg/I Na - Sodium mg/I I CERTIFY THAT TH REPORT IS TRUE AND ACCURATE. SIG RE F PEPMI E ( AUTHORIZED,AGENT') DATE ug/I ug/I Other (Specify) ug/I ug/I ug/I 0=9 ug/I r ug/I ud�Ji���JF?E Fl�l ug/l NOTE: Values should reflect dissolved concentrations (See 42. on reverse) * See back for Instructions. '* Submit blue, green, and yellow copies,Qft to address above. 1. Samples should be analyzed as soon as'possible after collection. SAMPLES WHICH ARE NOT ANALYSED WITHIN THE HOLDING TIME SPECIFIED FOR THE METHOD USED (SEE #3. BELOW) MUST BE DISCARDED AND,NEWSAMPLES COLLECTED. l\ 2. ANALYSES ARE TO BE MADE OF THE CONSITITUENTS DISSOLVED IN THE'GROUNDN%ATER, NOT THOSE THAT ARE A PART OF, OR ADSORBED ONTO, SOIL/SEDIMENT PARTICLES. CHECK WITH YOUR LABORATORY ON PROPER PROCEDURES FOR SAMPLE COLLECTION AND. PRESERVATION. 3. As per Title 15, North Carolina Administrative' Code, Subchapter 2L, analytical, procedures shall be in accordance -with the methods described in One of the following publications, or by other methods approved beforehand by the Director, Division of Environmental Management: ` (a) Standard methods for the Examination of Water and Wastewater, 16th Edition, 1985, published jointly by American Public Health Association,, American Water Works Association and Water Pollution Control Federation; (b) Methods,fgr Chemical Analysis of\Water.and Waste, 1979, U.S. Environmental Protection_ Agency publication number EPA-600/4-79-020, as revised.March 1983; (c) Test Methods for Evaluating Solid Wastes: Physical/Chemical Methods, 3rclEdition, 1986, U.S. Environmental Protection Agericy publication number SW 846; (d) Test Procedures for the Analysis of Polluants Under the Clean Water Act, Federal Register Vol. 4�, No. 209, 40 CFR Part 136, October 26, 1.984; 4. Measure and record the depth of water in -the well prior to pumping or bailing any water from the well. \. 5. At least 3 volumes of water in the well should be pumped or bailed prior to collecting a sample for analysis. If the well is pumped/bailed dry before 3 well volumes are removed, samples can be collected -as sdon-as the well recovers to the point where enough water is available to collect your sample. \. 6. Determination for pH, Specific Conductance, temperature, odor and appearance must be.made in the field on unfiltered samples when the sample is collected. 7. Field equipment Must be calibrated in accordance with recommendations•by the manufacturer..' 8. Samples m' Wt'be filtered through'a 0.45 micron filter immediately after *collection when a dissolved analysis is required..(See #3. above) 9. The sample container should be,labeled at-tfre .time of collection with'the facility name',"well identification number and date and time "col- lected. 1 O."Authorized agent' is any corporate officeror public official authorized by the.company,i.corporation, orgavernmental body tp'sign Official documents. n' GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM For additional forms please write or call: Facility Name 1o' 2i/ E'/e�ieQO L�.4G6oi/ G'og�• Address• �cX /8GB .50�.✓ �¢s�e r4�� . Well Location /✓/= .l&eeWeea/ _rg2 iv ~Z Vdcl Well Identification Number 4Je1/ 24'1 Well Depth Zo Ft. Well Diameter -? '/ Sample (Screened) Interval IS Ft. To zo Ft. Depth to Water Level If2, 2 ft. below measuring point. (before sampling) Measuring point is —3 feet above land surface Gallons of water pumped/bailed before sampling — Field Analysis: pH J.-,9 Specific Conductance Date Sample Collected A?- rY Laboratory Name4_2 COD < /0 Coliform: MF Fecal Coliform: MF Total _ mg/I /loom] /looml Dissolved Solids: Total -ram mg/I PH (when analyzed) units TOC Chloride Arsenic Grease and Oils Hardness: Total . U NO2 as N NO 3 as N County Division of Environmental Management Groundwater Section P.O. Box 27687 Raleigh, NC 27611-7687 (919)733-3221 PERMIT NUMBER: (REQUIRED) Non -Discharge — Lagoon Spray Field Land Application of Sludge — Septic Tank/Drain Field Subsurface Low -Pressure Piping (LPP) Other �/ayi><oa..uc eoe& _uMhos Temp. Af oC Odor A10AIM' Appearance C/e4i[ Lab Sample Analyzed 19 — 11-27— 9/ 7`! -7'`/c Certification No. 96 mg/I Ni - Nickel I mg/I Pb - Lead �� _ �I Phosphorus: Total as P mg/I Zn - Zinc DEC 30 1991 mg/I AI Aluminum mg/1 Pesticides/HerbiMs i%�MRg; VjMgUnds) FAYETTEVILLE REG. OFFIq�F Ba Barium mg/I lig/1 mg/I Ca - Calcium mg/I Cd - Cadmium_ mg/I Chromium: Total mg/I Cu - Copper mg/I mg/I Fe - Iron mg/I Phenol mg/1 Hg - Mercury_ Sulfate /9 mg/1 K - Potassium_ Specific Conductance 46 uMhos Mg - Magnesium Total Ammonia(NH3 t NH 4) TKN as N mg/I Mn - Manganese mg/I Na - Sodium_ I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE. e. .P�i /0?-li-`// SIGN&YUhE Of PEPMITT E (O AUTHORIZED AGENT*) DATE .mg/I mg/1 .mg/I mg/I ug/I ug/1 Other (Specify) ug/1 ug/I 1 23 3A91 ug/1 SRO fl ' SCTIQ/I NOTE:AtIGW, 'IQC Values should reflect dissolved concentrations (See #2. on reverse) * See back for Instructions. *' Submit blue, green, and yellow copies only to address above. COILECTION AND ANALYSIS OF GROUNDWATER SAMPLES 1. "amplcs should be analyzed as soon as possible after collection. SAMPLES WHICH ARE NOT ANALYSED WITHIN THE HOLDING TIME SPECiFiED FOR THE METHOD USED (SEE 0. BELOW) MUST BE DISCARDEO AND NEW, SAMPLES COLLECTED. 2 ANALYSES ARE TO BE MADE OF THE CONSiTITUENTS DISSOLVED IN THE GROUNDWATER, NOT THOSE THAT ARE A PART OF, OR ADSORBED ONTO, SOIL/SEDIMENT PARTICLES. CHECK WITH YOUR LABORATORY ON PROPER PROCEDURES FOR SAMPLE COLLECTION AND PRESERVATION. 3. As per Title 15, North Carolina Administrative Code, Subchapter 2L, analytical, procedures shall be in accordance with the methods described in one of the following publications, or by other methods approved beforehand by the Director, Division of Environmental Management: ' (a) Standard methods for the Examination of Water and Wastewater, 16th Edition, 1985, published jointly by American Public Health Associaticn, American Water Works Association and Water Pollution Control Federation: (b) Methods for -Chemical Analysis of Water and Waste, 1979, U.S. Environmental Protection Agency publication number EPA-600/4-79-020, as revised March 1983; (c) Test Methods for Evaluating Solid Wastes: Physical/Chemical Methods, 3rd Edition, 1986, U.S. Environmental Protection Agency'publication number SW-846: (d) Test Procedures for the Analysis of Polluants Under the Clean Water Act, Federal Register Vol. 49, No. 209, 40 CFR Part 136. October 26, 1984; 4. Measure and record the depth of water in the well prior to pumping or bailing any water from the well. 5. At least 3 volumes of water in the well should be pumped or bailed prior to collecting a sample for analysis. If the well is pumped/bailed dry before 3 well volumes are removed, samples can be collected as soon as the well recovers to the point where enough water is available to collectyouur sample. 6. 'Determination for pH, Specific Conductance, temperature, odor and appearance must be made in the field on unfiltered samples when the s,=: mple:is collected. 7. ft�pld equipment must be calibrated in accordance with recommendations by the manufacturer. 8- Samples musi be filtered through a 0,45 micron filter immediately after collection when a dissolved analysis is,required (See #3. above) 9. The Sttr pler iaa net should be abeled at the time of collection with the facility name, well identification number and date and time col- lected. 10."Authorized agpnt" is any corporate officer or public official authorized by the company, corporation, or governmental body to sign official documents. tea' GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM For additional forms please write or call: Facility Name Address Well Location G/-Z' 46cei-I /a 0/.f&1 'OA) Jcrti�<.v neeeA Well Identification Number 4Je// '12 Well Depth /9 Ft. Well Diameter Z ` Sample (Screened) Interval1-5� Ft. To_9 Ft. Depth to Water Level 3. & ft. below measuring point. (before sampling) Measuring point is --2' feet above land surface Gallons of water pumped/bailed before sampling Field Analysis: pH Specific Conductance Date Sample Collected 9/ Date Laborator Name Y COD mg/I Coliform: MF Fecal /100ml Coliform: MF Total /100ml Dissolved Solids: Total mg/I pH (when. analyzed) units TOC 3..Z mg/I Chloride 9 mg/I Arsenic mg/I Grease and Oils mg/I Hardness: Total mg/I NO2 as N _ NO3as N_ Phosphorus Division of Environmental Management Groundwater Section P.O. Box 27687 Raleigh, NC 27611-7687 (919)733-3221 County >40A41e n` PERMIT NUMBER: (REQUIRED) Non -Discharge 11 — Lagoon Spray Field — Septic Tank/Drain Field Subsurface Low -Pressure Piping (LPP) Land Application of Sludge Other _uMhos Temp. /7 oC Odorsl9'Ly' Appearances/Z4// Sample Analyzed Certification No. mg/I Ni Nickel g mg/I Pb Lead 09C 3A toorm Total as P Al - Aluminum Ba - Barium _ mg/I mg/I Ca - Calcium mg/I Cd - Cadmium mg/I Chromium: Total mg/I Cu - Copper mg/1 Fe - Iron Phenol mg/I Hg - Mercury mg/I Sulfate /3 mg/I K - Potassium mg/I Specific Conductance 7/ uMhos Mg - Magnesium mg/I Total Ammonia(NH3 , NH 4) TKN as N mg/I Mn - Manganese mg/I mg/I Na - Sodium mg/I I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE. //9 - 9 r �- SPATLARE OF PERT IITTE (OR AUTHOR ED AGENT') DATE Zn -Zinc q?/I Pesticides/HerbicjAdglle '¢@UqMWf�F ug/I ug/I i ug/I Other (Specify) Al` ug/I u.9W ug/I �- ug/I "" i991 ug/I �- s'rl�� NOTE: Values should reflect dissolved concentrations ug/I (See #2. on reverse) See back for Instructions. "Submit blue, green, and yellow copies only to address above. COLLECTION AND ANALYSIS OF GROUNDWATER SAMPLES 1. Samples should be analyzed as soon as possible after -collection. SAMPLES WHICH ARE NOT ANALYSED WITHIN THE HOLDING TIME SPECIFIED FOR THE METHO.D_USED (SEE #3. BELOW) MUST BE DISCARDED,AID NEW SAMPLES CQLLECTED. 2. ANALYSES ARE TO BE MADE OF THE CONSITITUENTS DISSOLVED IN THE GROUNDWATER, NOT THOSE THAT ARE A PART OF, OR ADSORBED ONTO, SOIL/SEDIMENT PARTICLES. CHECK WITH YOUR LABORATORY ON PROPER'PROCEDURES FOR SAMPLE COLLECTION AND PRESERVATION. 3. Asper Title 15, North Carolina Administrative Code, Subchapter 2L, analytical procedures shall be in accordance with .the methods described in one of the following publications, or by other methods approved beforehand by the Director, Division of Environmental Management: (a) Standard methods for the Examination of Water and Wastewater, 16th Edition, 1985, published jointly by American Public Health Association, American Water Works Association and Water Pollution Control Federation; (b) Methods for,Chemical Analysis of Water and Waste, 1979, U.S. Environmental Protection Agency.publication number EPA-600/4-79-020, as revised,March 1983; .` (c) Test Methods for Evaluating Solid Wastes: Physical/Chemical Methods, 3rd Edion;it1986, U.S. Environmental Protection Agency publication number SW-846; - - - • (d) Test Procedures for the Analysis of Polluants Under the Clean Water Act, Federal Register Vol. 4d, No. 209, 40 CFR Part 136, October 26; 1984; 4..Measure and record'the depth of water in the well prior to pumping or bailing any water from the well. 5. At least 3 volumes of water in the well should be pumped or bailed prior to collecting a sample for analysis. If the well is pumped/bailed dry before 3 well volumes are removed, samples can be collected as soon as the well recovers to the point where enough water is available to collect your sample. ay. 6...Determination tortpH,.Sp�icific Conductance, temperature, odor and appearance must be made in the field on unfiltered samples when.the sam` I i I�ec2ea': r s{ 7. Field •. quipment,must be calibrated in?accordance with recommendations by the manufacturer. -ent S. Samples'must-.be.iiltered through a 0.45. micron filter immediately after collection -when a dissolved analysis is required. (See #3. above) 9. The sample container should be labeled at the time of collection with the'facilityname, well identification number and date and time col- lected. 10."Authorized agent' is any corporate officer Qr public official authorized by the company; corporation, &.governmental body to"sign official documents. - GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM For additional forms please write or call: Facility Name �i0�ova�E/e icaU �%Q26vc/ a02e. Address J�90, .2of! Al. 44n At/� Well Location Well Identification Number Y./ Well Depth /8 Ft. Well Diameter 2 Sample (Screened) IntervalI-P Ft. To /6 Ft. Depth to Water Level 3 Z a ft. below measuring point. (before sampling) Measuring point is -�P- feet above land surface Gallons of water pumped/bailed before sampling Field Analysis: pH -5.9 Specific Conductance _ Date Sample Collected %-/8-91 Date Laboratory Name LZemrev// 'r COD < / D mg/I Coliform: MF Fecal /100ml Coliform: MF Total /100ml Dissolved Solids: Total S8 mg/I pH (when analyzed) units TOC /' mg/I Chloride ? mg/1 Arsenic mg/I Grease and Oils mg/1 Hardness: Total mg/I Phenol mg/I Sulfate -3 mg/I Specific Conductance uMhos Total Ammonia(NH3 + NH y) mg/I TKN as N mg/I Division of Environmental Management Groundwater Section P.O. Box 27687 Raleigh, NC 27611-7687 (919)733-3221 County K9?.Vv77_ PERMIT NUMBER: (REQUIRED) Non -Discharge (REQUIRED; — Lagoon Spray Field Land Application of Sludge — Septic Tank/Drain Field Subsurface Low -Pressure Piping (LPP) Other &4L/ !/.U9 A/a/,/ _uMhos Temp. 19 C Odor SY .ff Appearance Lab Sample Analyzed %-/.g . 8-2-9/ v6/o�y Certification No. 96 NO2 as N mg/I Ni - Nickel mg/I No as N mg/I Pb - Lead mg/l Phosphorus: Total as P mg/I AI - Aluminum mg/1 Be - Barium mg/I Ca - Calcium mg/I Cd - Cadmium mg/I Chromium: Total Cu- Copper Fe - Iron Hg - Mercury_ K - Potassium_ Mg - Magnesium Mn - Manganese Na - Sodium_ I CERTIFY THAT S REPORT IS TRUE AND ACCURATE. 9--r-9i SIC#ATUE OF PERMI EE (OR AUTHORIZED AGENT-) DATE —mg/I _mg/I —mg/I mg/I mg/I mg/I mg/I Zn - Zinc mg/I Pesticides/Herb' S ecify Compounds) ® U SEP 29 1A91 Other (Specify) ENV MANgrEMF?4flg/I FAYETTEVILLE IdEG. OFFS ug/I ug/I --l`, ug/I ! ) ug/I v SEP IV BM .1 NOTE: Values should r ?Ai� ,y�e"eo rev (See 4u ' See back for instructions. " Submit blue, green, and yellow copies 2M to address above. COLLECTION AND ANALYSIS OF GROUNDWATER SAMPLES 1. Samples shouldbe analyzed as soon as possible after collection. SAMPLES WHICH ARE NOT ANALYSED WITHIN THE HOLDING TIME SPECIFIED FOR THE METHOD USED (SEE 43. BELOW) MUST BE DISCARDED AND NEW SAMPLES COLLECTED. 2. ANALYSES ARE TO BE MADE OF THE CONSITITUENTS DISSOLVED IN THE GROUNdWATER, NOT THOSE THAT ARE A PART OF, OR ADSORBED ONTO, SOIL/SEDIMENT PARTICLES. CHECK WITH YOUR LABORATORY -ON PROPER•PROCEDURES FOR SAMPLE COLLECTION AND'PRESERVATION. - I , \ ,\ - 3. As per Title 15, North Carolina Administrative Code, Subchapter 2L, analytical. procedures shall be in accordance with the methods described in one of the following publications, or by other methods approved beforehand by the Director, Division of Environmental Management: (a) Standard methods for the Examination of Water and Wastewater, 16th Edition, 1985, published jointly by American Public Health Association, American Water Works Association and Water Pollution Control Federation; (b) Methoda:fot.Chemical Analysis of:Water and Waste, 1979, U.S. Environmental Protection. Agency.publication number EPA ;600/4-79-b20, as revised March 1983; (c) Test Methods for Evaluating Solid Wastes: Physical/Chemical Methods, 3rd Edition, 1986, U.S. Environmental Protection Agency publication number SW-846; � • (d) Test Procedures for the Analysis of•Polluants Under the Clean Water Act, federal Register Vol. 49,No. 209, 40 CFR Part 136, October 26, 1984; . . 4. Measure and record the depth of water in the well prior to pumping or bailing_ any water from the, well. - jt i6pst', Volumes d- water in the well should be pumped or bailed prior to collecting a sample. for analysis. If the_vyell is pumped/bailed dry before 3 well volumMa)e removed, samples can be collected as soon as the well recovers to,the point where enough water is available to `collect: y'ouP'sampld. 6..D¢#erminationifovpH,-$pecific Conductance, temperature, odor and appearance must be made in.the'field on unfiltered samples when the sample is collected. 7. Fieldreiquiprpent must be calibrated in.accordance with recommendations by the manufacturer. 8- Samoles must be filtered-thrdugh a Q.45 micron filter immediately.after collection:when a dissolved analysis is required. (See #3. above) 9. The sample container should be:labeled at the time of collection with the facility name, Well -identification number and date and time col- lected. _ 10."Authorized agent" is any corporate officer or-pLplic official authorized by,.the company, corporation, or governmental body to sign official documents. GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM Facility Name Address Z'0- For additional forms please write or call: �eav cJy A/ • C . Z83.37 Well Location !Jr=' -Re eF-j sefZA4?o�z acd a/ii�iiJo P�w�� Well Identification Number 4) 2 Well Depth 20 Ft. Well Diameter -? 11 Sample (Screened) Interval /.S Ft. To 26 Ft. Depth to Water Level // S/ y ft. below measuring point. (before sampling) County Division of Environmental Management Groundwater Section P.O. Box 27687 Raleigh, NC 27611-7687 (919)733-3221 PERMIT NUMBER: (REQUIRED) Non -Discharge — Lagoon — Septic Tank/Drain Field —. Subsurface Low -Pressure Piping (LPP) Measuring point is 3 feet above land surface Land Application of Sludge Other it%u Lr%all Gallons of water pumped/bailed before sampling Z I — Rotary Distributor Field Analysis: pH 3 Specific Conductance -uMhos Temp. .21 o C Odor A10A e- Appearance Date Sample Collected %-/8-9/ Date Lab Sample Analyzed -- 7-/51 �iQ57- Z- 9/ Laboratory Name / ++««' V COD -<'/0 mg/I NO2 as N Coliform: MF Fecal /100ml NO3 as N Coliform: MF Total / 100ml Dissolved Solids: Total mg/I PH (when analyzed) units TOC 2.3 mg/I Chloride Arsenic Grease and Oils Spray Field Certification No. mg/I Ni - Nickel mg/I mg/I Pb - Lead mg/I Phosphorus: Total as P mg/I Al - Aluminum mg/I Ba - Barium - Ca - Calcium mg/I Cd - Cadmium mg/I mg/I Chromium: Total mg/I Ctf - Copper Hardness: Total mg/1 Phenol mg/I Sulfate mg/I Specific Conductance 7o uMhos Total Ammonia(NH3 f NH 4) TKN as N mg/I mg/I g/I Fe - Iron mg/I Hg - Mercury mg/I K - Potassium mg/I Mg - Magnesium mg/I Mn - Manganese Na - Sodium_ I CERTIFY THAT HIS REPORT IS TRUE AND ACCURATE. XS 9/ SIGH{ UR OF PERMrrrEE OR AUTHORIZED AGENT-) DATE /I mg/I Zn - Zinc mg/I Pesticides/Herbicides,(Specify Compounds) Kt��Z3lV/1- Other ENV. MANAGEMENT See back for Instructions. "" Submit blue, green, and yellow copies only to address above. COLLECTION AND ANALYSIS OF GROUNDWATER SAMPLES 1. Samples should be analyzed as soon as possible after collection. SAMPLES WHICH ARE NOT ANALYSED WITHIN THE HOLDING TIME SPECIFIED FOR THE METHOD,USED (SEE #3. BELOW) MUST BE DISCARDED AND,NEW,SAMPLES COLLECTED. 2. ANALYSES ARE TO BE MADE OF THE CONS ITITUENTS DISSOLVED IN TFIE GROUNDWATER, NOT THOSE THAT ARE A PART OF, OR ADSORBED ONTO, SOIL/SEDIMENT PARTICLES. CHECK WITH YOUR LABORATORY ON PROPER PROCEDURES FOR SAMPLE COLLECTION -AND PRESERVATION. 3. As.per Title 15, North Carolina Administrative Code, Subchapter 2L, analytical,procedures shall be in accordance with.the methods described in one of the following publications, or by other methods approved beforehand by the Director; Division of Environmental Management: (a) Standard methods for the Examination of Water and Wastewater, 16th Edition; 1985, published jointly by American Public Health Association, American Water Works Association and Water Pollution Control Federation; (b).Methods;fQr, hemical Analysis,of Water and Waste, 1979, U.S. Environmental Protection•Agency publication number EPA-600/4-79-020, as revised March 1983; (c) Test Methods for Evaluating Solid Wastes: PhysicaVChemical Methods, 3rd Edition,11986; U.S. Environmental Protection Agency publication number SW-846; (d) Test Procedures for the Analysis of Polluants Under the Clean Water Act, Federal Register Vol. 49;"No. 209, 40 CFR Part 136, October 26, 1984; 4. Measure and record the depth of water in the well prior to pumping or bailing any water from the well. 5..;PA-1Lytol, ';voibmes\of.water in the well should be pumped or bailed prior to collecting a sample""for analysis. If the well is pumped/bailed dry b' qq� 3 w' 611 volumes are removed, samples can be collected as soon as the well recovers to the point where enough water is available to `� Q l ct your safnple.. 6. DetermjriatioatorapH;'Spec_ific Conductance, temperature; odor and appearance must bje made in the field on unfiltered samples when the samp1P.jiscl9llected7T 7. Field equipment must be calibrated in accordance with recommendations 6y the manufacturer. 8. 5amples must be filtered through a 0.45 micron filter immediately after"Collection when a dissolved analysis is,required..(See #3. above) :. 9. • The sample coritainershould be.l.abeled"at the .time of col Iection with the facility name, -well identificatron.number and date and time col- lected: 10."Authorized agent' is any corporate officer or public official authorized by the company, corporation, or`governmental body to sign official documents. 'L t +-tNiOUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM For additional forms please write or call: Facility Name �i1Y%0'tl4�G��e7X�G4O (�V'O(WA% eo4O Address /O '-;w Gov- Al /4s/4e Ale- - d�uv.�, A/.C. C833 Well Location W/ _ ZkAreeJ se7i/n�v eon e.¢�Ad� A��ir%f �.00.�d Well Identification Number k/e// 'E1 Well Depth Zd Ft. Well Diameter Zi'uclar Sample (Screened) Interval45" Ft. To 2e Ft. Depth to Water Level &d ft. below measuring point. (before sampling) Measuring point ism feet above land surface Gallons of water pumped/bailed before sampling — Field Analysis: pH -SdO Specific Conductance Date Sample Collected &-/$-I- 9/ I Laboratory Name Z-wuiizp� COD < /0 mg/I Coliform: MF Fecal /100ml Coliform: MF Total r100ml Dissolved Solids: Total 37 mg/I PH (when analyzed) units TOC mg/I Chloride 8 mg/I Arsenic Grease and Oils Hardness: Total. Phenol County Division of Environmental Management Groundwater Section P.O. Box 27687 Raleigh, NC 27611-7687 (919)733-3221 PERMIT NUMBER: (REQUIRED) Non -Discharge Lagoon Spray Field Land Application of Sludge Septic Tank/Drain field Subsurface Low -Pressure Piping �(LPP) Otherl!! 7S �i'✓a A)�l _uMhos Temp. -20 C Odor -VVWd Appearance CWe4'e Lab Sample Analyzed `i-.3-9/ " V76P 7ti Certification No. 99 NO2 as N mg/I Ni Nickel mg/I NO3 as N. mg/I Pb - Lead mg/I Phosphorus: Total as P mg/I Zn Zinc mg/I Al - Aluminum mg/I Pesticides/Herbicides.(Specify Compounds) Ba - Barium mg/I Ca - Calcium mg/I Cd - Cadmium $9� mg/I mg/I Chromium: Total mg/I Cu - Copper _ mg/I Fe - Iron mg/I Hg - MercuryKe Sulfate 7 mg/I Specific Conductance -SL uMhos Total Ammonia(NH3 + NH 4) 1d3ow7► K - Potassium Mg - Magnesium mg/I Mn - Manganese mg/I Na - Sodium_ I -CERTIFY THAT IS REPORT IS TRUE AND ACCURATE. SIG UR OF PER TEE OR AUTHORIZED AGENT') DATE g/I • . I II " `in 11 ug/I ug/I A IV. MANAGEMENT ug/I A E TEnrfILLL R ug/I /I ug/I mg/I NOTE: "I mg/I Values should reflect dissolved concentrations (See #2. on reverse) * See back for Instructions. ** Submit blue, green, and yellow copies only to address above. COLLECTION AND ANALYSIS OF GROUNDWATER SAMPLES 1. Samples should be analyzed as soon as possible after collection. SAMPLES WHICH ARE NOT ANALYSED WITHIN THE HOLDING TIME SPECIFIED FOR THE METHQQ USED (SEE #3. BELOW) MUST BE DISCARDED;AND IJEW SAMPLES COLLECTED. 2. ANALYSES ARE TO BE MADE OF THE CONSITITUENTS DISSOLVED IN THE'GROUNDWATER, NOT THOSE THAT ARE A PART OF, OR ADSORBED ONTO, SOIUSEDIMENT PARTICLES. CHECK WITH YOUR LABORATORY ON PROP EWPROCEDURES FOR SAMPLE COLLECTION AND PRESERVATION. 3. As per Title 15, North Carolina Administrative Code, Subchapter 2L, analytical procedures shall be in accordance with -the methods described in one of the following publications, or by other methods approved beforehand by the Director, Division of Environmental Management: (a) Standard methods for the Examination of Water and Wastewater, 16th Edition, 1985, published jointly by American Public Health Association, American Water Works Association and Water Pollution Control Federation; (b) Methods 4or-Chemical Analysis of Water and Waste, 1979, U.S. Environmental Protection: Agency publication number EPA-600/4-79-020, as revised March 1983; (c) Test Methods for Evaluating Solid Wastes: Physical/Chemical Methods, 3rd Edition, 1986, U.S. Environmental Protection Agency publication number SW-846; (d) Test Procedures for the Analysis of Polluants Under the Clean Water Act, Federal Register Vol. 49, No.-209, 40 CFR Part 136, October 26, 1984; . 4. Measure and record the depth of water in the well prior to pumping or bailing any water from the well. 5. At least 3 volumes of water in the well should be pumped or bailed prior to collecting a sample for analysis. If the well is pumped/bailed dry before 3 well volumes are removed, samples can be collected as soon as the well recovers to the point where enough water is available to collect-your.§ample.;, 6. Determination for pH, SpeciH Conductance,_ temperature,, odor and appearance must be made in the field on unfiltered samples when the sample is collected. . 7. Field,equip(rreht my�y 'tie ~al)brated in accordance with recommendations�tk3 fhe manufacturer. S. Samples must be filtered through a_0.45 micron filterimrtiediately after 01ection when a dissolved analysis is required. (See #3. above) 9. The sample container should be.labeled at the time:of collec itin wiffq the facility. name, well identification number and date iand time Col-. lected. 10."Authorized agent' is any corporate officer or iic official authorized by the company, corporation; or.government21 body to sign official documents: • — -. -1&RROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM For additional forms please write or call: Division of Environmental Management Groundwater Section P.O. Box 27687 Raleigh, NC 27611-7687 (919)733.3221 Facility Name �1�/J�o�✓el� c�/ee .f�co� �'9it6a ✓ �'.c� • County A��U Address 1414(a ode PERMIT NUMBER: (REQUIRED) �c� ✓ u� N C . ZS3,3 90 Non -Discharge Well Location l✓Z 'Aq j_;WAW� as/.i%�.p pawed( y Jcw�peo G'eee.� NPDES Al-- 00(oD7fe7 Well Identification Number W'0// #2 Well Depth �Ft. TYPE OF DISPOSAL OPERATION BEING MONITORED (REQUIRED) Well Diameter ?iv�er Sample (Screened) Interval /I Ft. To IF Ft. _ Lagoon — Septic Tank/Drain Field Depth to Water Level -� / ft. below measuring point. (before sampling) — Spray Field — Subsurface Low -Pressure Measuring point is .Z feet above land surface — Land Application of sludge Piping (LPP) /stiwl ld�l other �1 Gallons of water pumped/bailed before sampling — Rotary Distributor Field Analysis: pH -S Specific Conductance uMhos; Temp. /9 o C Odor-5_X44f Appearance 1 7 Date Sample Collected 3—i� —9i Date Lab Sample Analyzed `i-3-9/ Laboratory Name &dwKL.4 -LNG. Certification No. 9.G COD < /6r mg/I Coliform: MF Fecal /100ml Coliform: MF Total NO2 as N mg/I NO3 as N mg/I 1100ml Phosphorus: Total as P Dissolved Solids: Total 41-3 mg/I PH (when analyzed) units TOC -.3 mg/I Chloride Arsenic Grease and Oils — Hardness: Total Phenol mg/I mg/I mg/I mg/I mg/I Sulfate io mg/I Specific Conductance y% uMhos Total Ammonia(NH3 f NH 4) TKN as N Al - Aluminum Ni - Nickel Pb Lead mg/I mg/I Zn - Zinc mg/I mg/I Pesticides/Herbicides.(Specify Compounds) Be - Barium mg/I Ca - Calcium a Cd - Cadmium /I Chromium: Total - /I Cu- Copper ON mg/I Fe - Iron PQ S Hg - Mercury g/I ug/I gA /I Other (Speci /I MAY 1 lgot ugA ENV. MANAGFMFNT ug/I FAYETTEVILLE REG. OFFIC�g/I K - Potassium 'mg/I ug/I Mg - Magnesium 6R� @A� rrigA ug/I mg/I Mn - Manganese mg/I mg/I Na - Sodium mg/I I CERTIFY THATTTTHIS'REPORT IS TRUE AND ACCURATE. SIG UR OF PERM447EE (OR AUTHORIZZtT*j D AGENDATE NOTE: Values should reflect dissolved concentrations (See #2. on reverse) * See back for Instructions. .*Submit blue, green, and yellow copies onto to address above. COLLECTION AND ANALYSIS OF GROUNDWATER SAMPLES 1. Samples should be analyzed as soon as possible after collection. SAMPLES WHICH ARE NOT ANALYSED WITHIN THE HOLDING TIME SPECIFIED FOR THE METHOD USED (SEE #3. BELOW) MUST. BE DISCARDED:AND,NEW SAMPLES COLLECTED... 2. ANALYSES ARE TO BE MADE OF THE CONSITITUENTS DISSOLVED IN THE bR' O6NDWATER, NOT THOSE THAT ARE A PART OF, OR ADSORBED ONTO, SOIL/SEDIMENT PARTICLES. CHECK WITH YOUR LABORATORY ON PROPER PROCEDURES FOR SAMPLE COLLECTION AND PRESERVATION. 3. As per Title 15, North Carolina Administrative Code, Subchapter,2L, analytical procedures shall be in accordance wjjh,the methods described in one of the following publications, or by other methods approved beforehand by the Director, Division of Environmental Management: `• , . , ...� (a) Standard methods for the Examination of Water and Wastewater, 16th Edition, 1985, published' jointly by American Public Health Association, American Water Works Association and Water Pollution Control Federation; _ (b) Methods -for Chemical Analysis of,Water and Waste, 1979, U.S. Environmental Protection Agency publication number EPA-60014-79-d20,.as revised.March 1983; (c) Test Methods,for Evaluating Solid Wastes: Physical/Chemical Methods, 3rd Edition, 1986,,U.S. Environmental Protection Agency publication number SW-846; '. ` ' (d) Test Procedures for the Analysis of Polluants Under the Clean Water Act, Federal Register Vol. 49, No' 209, 40 CFR Part 136, October 26, 1984; 4. Measure and record the depth of water in the well prior to pumping or bailing any water from the well. 5. At least 3 volumes of water in the well should be pumped or bailed prior to collecting a sample for analysis. If the well is pumped/bailed dry befar�e Il;va u es�reremoved, samples can-G-6onected as soon as the'well recovers to the point where enough .water is available to aaj your, s ? 6 Determination for pkt,'.Speeifiic Conductance, temperature, odor and'a_ppearance,must be made in the field on unfiltered samples,when the sample is collected'1AX.Vl! r� 7. Fieldequipmen must be calibrated in accordance with'recomriienda#inns by the manufacturer. S. Samples must be filtered through a, 0.45 micron'filter 6'm"djat6f�., er collection when a dissolved analysis is'required..(See #3. above) 9. The sample container should be,lebeled'at the.firrie of collection with the facility.name,:well identification ni mber and date and time col leeted: :. I O."Authorized agent' is any corporate bfficer er public official authorized by the company,�•cbrporation; or governmental body to 4ign. official documents:. - /`GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM For additional forms please write or call: Facility Name Address Well Location W1 = Well Identification Number V)P.fl IF 1 J We��lll Depth' '20 Ft. Well Diameter Z I A'AtS Sample (Screened) interval Ft. To 20 Ft. Depth to Water Level ) I •rs ft. below measuring point. (before sampling) Measuring point is 3 feet above land surface Gallons of water pumped/bailed before sampling 2 Field Analysis: pH . Date Sample Collected Division of Environmental Management Groundwater Section P.O. Box 27687 Raleigh, NC 27611-7687 (919)733-3221 County PII"YfIvIc'I I PERMIT NUMBER: (REQUIRED) Non -Discharge Lagoon — Spray Field Land Application of Sludge lu[N]\Ilre]:I=11101 — Septic Tank/Drain Field Subsurface Low -Pressure Piping (LPP) Other MnuIT'dpmo 11JEf - Conductance lfti- UMhos Temp. 2) oC Odor ONE Ape rance 64h Laboratory Name ( 4cfyllC-T- &//V f COD 4 10.E mg/I Coliform: MF Fecal /1001711 Coliform: MF Total / 100ml Dissolved Solids: Total 1.6 mg/1 pH (when analyzed) *''I6 units TOC 9.T mg/I Chloride Arsenic mg/I mg/I Grease and Oils mg/I Hardness: Total mg/1 Phenol mg/I Sulfate 6 mg/I Specific Conductance so uMhos Total Ammonia(NH3 + 'NH q) mg/I TKN as N mg/I Date Lab Sample Analyzed )I /Iq/90 REpa972r,9 14L5�YD 1L rECiS/!/JCaGj/1NC • Certification ation No. NO2 as N mg/I NO3 as N mg/I Phosphorus: Total as P mg/I Al - Aluminum mg/I Be.- Barium mg/I Ca - Calcium mg/I Cd - Cadmium mg/I Chromium: Total mg/I Cu - Copper 0•606 mg/I Fe - Iron mg/1 Hg - Mercury K - Potassium Mg - Magnesium m Mn - Manganese I mg/I Na Sodium E��kMAGEMREQ Of I I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE. /e i 3 y 1 SIGNATURE OF PEP.MITTEV (OR AUTHORIZED AGENT-) DATE Ni - Nickel mg/I Pb Lead mg/I Zn Zinc 0•0Io mg/1 Pesticides/Herbicides (Specify Compounds) NOTE: Values should reflect dissolved concentrations (See #2. on reverse) * See back for Instructions. •* Submit blue, green, and yellow copies only to address above. n�er rn nci Winn COLLECTION AND ANALYSIS OF GROUNDWATER SAMPLES Samples -should be analyzed as soon as possible after collection. SAMPLES WHICH ARE NOT ANALYSED WITHIN THE HOLDING TIME SPECIFIED FOR THE METHOD-U1.SED (SEE i#3. BELOW) MUST BE DISCARDED AND NEW SAMPLES COLLECTED, 2. ANALYSES ARE TO BE MADE OF THE CONSITITUENTS DISSOLVED IN THE GROUNDWATER, NOT THOSE THAT ARE A PART OF, OR ADSORBED ONTO, SOIL/SEDIMENT PARTICLES. CHECK WITH YOUR LABORATORY ON PROPER PROCEDURES FOR SAMPLE COLLECTION AND PRESERVATION. _ 3. As per Title 15, North Carolina Administrative Code, Subchapter 2L, analytical procedures shall be in accordance with the methods described in one of the following publications, or by other methods approved beforehand by the' Director, Division of Environmental Management: ' (a) Standard methods forthe Examination of Water and Wastewater, 16th Edition, 1985, published jointly by American Public Health Association, American Water Works Association -and Water Pollution Control Federation; (b) Methods for Chemical Analysis of Water and Waste, 1979�U.S. Environmental Protection Agency publication number EPA-600/4-79-020, as revised March 1983; (c) Test Methods for Evaluating Solid Wastes: Physical/Chemical Methods, 3rd Edition, 1986, U.S. Environmental Protection Agency publication number SW-846; (d) Test Procedures for the Analysis of Polluants Under the Clean Water Act, Federal Register Vol. 49, No. 209,40 CFR' Part 136, October 26, 1984; 4. Measure and record the depth of water in the well prior to pumping or bailing any water from the well. 5. At least 3 volumes of water in the well should be pumped or bailed prior to collecting a sample for analysis. If the,well is pumped/bailed dry before 3 el 1 es are removed, samples can be collected as soon as the well recovers to the point where ehough water is available to collect yout 7�+iF f� 6. Determinat ` or pH, Specific G5%i Lance, temperature,odor and appearance must be made,in.the`field on unfiltered samples when -the sgmpleas (, 7. Fjeld;`equi fYi �i stR {A ti f}� in accord c';tj� rer,4rmt ertd t}#ons by the manufacturer. t:• �;'• •- r iJ(r7 it:I �� Y 8 Sam. x tr ,,f,Rt,�'ed'V1to�ugh a 0 45 miArara tter immediately aRe)$collection-when a dissolved analysis is required: (See #3: above)' 9 , The sample container should be.labeled at the time of. co)lectian with the facility namE; well identification number and date and•time col= 10."Authorized agent" is any corporate officer -:or public official authorized by.the company.;- corporation,. or governmental hod y to sign official documents: "'tROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM Division of Environmental Management Groundwater Section P.O. Box27687 Raleigh, NC 27611-7687 For additional forms please write or call: (919)733-3221 Facility Name NATJOkAL ELGM)CAL 124 1 County yAaA/OT Address G S au /96 - PERMIT NUMBER: (REQUIRED) 1-iri AlAl ��. 7_� Well Location UWZ = fr.c of [ -To gellislAirl!-h UN It. NPDES N�-UUbU/y-/ Z Well Depth L. TYPE OF DISPOSAL OPERATION BEING MONITORED Well Identification Number WO'�j(REQUIRED)Well Diameter 2incite5 Sample (Screened) Interval13 Ft. To�_ Lagoon — Septic Tank/Drain Field Depth to Water Level .6 ft. below measuring point. (before sampling) — Smy Field — Subsurface Low -Pressure Measuring point is 2 feet above land surface Piping (LPP) � I Land Application of Sludge nAa��� � Gallons of water pumped/bail d before sampling r c — Rotary Distributor Other /,/ Field Analysis: pH 5'� Specific Conductance —OMhos Temp. ,ol oC Odor 510E Apip earance 1 41 Date Sample Collected If - �3'qd Date Lab Sample Analyzed _ ����y/�d 'upentz) / Laboratory Name ('E/�%I�CAC AltD 6014007AL %UJNOLocIk C Certification No. 9� COD Coliform: MF Fecal Coliform: MF Total NO2 as N NO3 as N Phosphorus: Total as P Dissolved Solids: Total r� 56 mg/I Al - Aluminum pH (when analyzed) - 4 units Ba - Barium _ TOC 6-1 mg/I Ca - Calcium - mg/I /100ml / 100ml Chloride mg/I Cd - Cadmium — Arsenic mg/I Chromium: Total Grease and Oils mg/I Cu- Copper_ Hardness: Total mg/I Fe - Iron Phenol mg/1 Hg - Mercury Sulfate 33 mg/I K - Potassium_ Specific Conductance -319 uMhos Mg - Magnesium mg/I Ni Nickel mg/I mg/I Pb - Lead mg/I mg/I Zn Zinc mg/1 mg/I Pesticides/Herbicides,(Specify Compounds)' mg/I ug/I mg/I ua/I Total Ammonia(NH3 + NH q) mg/I Mn - Manganese mg/I TKN as N mg/I Na - Sodium mg/I I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE. ppM SIGNATURE OF PER.MITTEE (OR AUTHORIZED AGENT-) D TE ug/I Other (Specify) ug/I ug/I /I A JAN 11 1991 q#ug/I F A .�jA _.ug/I FAYET . xM. (-� NOTE:• e - . Values should reflect dissolved concentrations (See #2. on reverse) See back for Instructions. •• Submit blue, green, and yellow copies only to address above. Ky :COLLECTION AND ANALYSIS OF GROUNDWATER SAMPLES 1. Samples should be analyzed assoon-as possible after collection. SAMPLES WHICH ARE NOT:ANALYSED WITHIN THE HOLDING TIME SPECIFIED FOR THE,METHOD USED (SEE #3. BELOW) MUST BE DISCARDED AND NEW SAMPLES COLLECTED. 2. ANALYSES ARE TO BE MADE OF THE CONSITITUENTS DISSOLVED IN THE GROUNDWATER, NOT THOSE THAT ARE A PART OF, OR ADSORBED ONTO, SOIL/SEDIMENT PARTICLES. CHECK WITH YOUR LABORATORY ON PROPER -PROCEDURES FOR SAMPLE COLLECTIOWAND PRESERVATION. 3. As per Title 15, North Carolina Administrative Code, Subchapter 2L, analytical procedures shall be in accordancewith the methods described in one of the following publication's, or by other methods approved beforehand by the Director, Division of Environmental Management.. (a) Standard methods for the Examination of Water and Wastewater, 16th Edition, 1985, published jointly by American _ Public Health Association, American Water Works Association -and Water Pollution. Control Federation; (b) Methods for Chemical Analysis of Water and Waste, 1979, U.S. Environmental Protection Agency,publication number EPA-600/4-79-020, as revised March 1983; _ (c) Test Methods forFEvaluating Solid Wastes: Physical/Chemical Methods, 3rd Edition, 1986, U.S. Environmental Protection Agency publication number SW-846; - (d) Test Procedures for the Analysis of Polluants'Under the Clean Water Act, Federal Register Vol. 49, No. 209, 40 CFFR Part 136, October 26, 1.984; 4. Measure and record the depth of water in the well prior to pumping or bailing -any water from the well. _ 5. At least 3-volumes of water in the well should be pumped or bailed prior to collecting a sample for analysis. If the we•II is pumped/bailed dry before 3 well volumes are removed, samples can be collected as soon as the well recovers to the -point where. erfoadh water is available to collect your sample. R.I., .,6.. Determination.for PH, Specific Conductance, tt' � ar�tt,,P�@arance must be made in the field an unfiltered samples when the Sa pI L01I£ r (5\ I,,4}� 7 F`sl el�uipment must be;oAljbrated jn accordy py�py with rec;mm, hdatldn's by the manufacturer. 8_ Samples rtwst) e f(16ered;''Jhrough, a 0.45 micron fiilte6fir ed�afe/(y collection when a,dissolved analysis is,required. (See #3. above) Alf- 9.- The sample cagtainer should be labeled at thefime of collection with the facility name; well identification.numberand. date and time col- lected: 10."Authorized agent"is'any corporate officeroT public official authorized by3he cgmpany;•corporation or governmental body to sign official 'documents.. t COMPLIANCE MONITORING Environmental Management Division Groundwater Section REPORT FORM P.O. Box 27687 1)N Raleigh,N.C.27611 ,\ (919)733-5083 Facility Name Morcanite Inc. County narneLL AI - Address one Morganite Drive Permit Number: NCO060747 Dunn, NC 28334 Non -Discharge (C. _ 11�1_ Well Location W-2=located directly adjacent to polishing pond & Juniper Creek NPDES NC00607 R� Z Q C� Well Identification Number Well #2 Well Depth 18 Ft. Water Use Well Diameter 2 inches Sample (Screened) IntervalI _'4_Ft. To lit Ft. Injection Well _ Depth to Water Level 2.9 ft. below measuring point. (before sampling) Well Construction Measuring point is 2 feet above land surface Other. Monitoring Well Gallons of water pumped bailed before sampling 2 gal. Field Analysis: pH 5.5 Specific Conductance 43 uMhos Temp. 19 o C Odor None Appearance clear Date Sample Collected 12-4-89 Date Lab Sample Analyzed 1-5-90 Laboratory Name Chemical and Environmental Technology Certification No. 96 COD 44 10 mg/I NO2 as N mg/I Ni Nickel mg/I Coliform: MF Fecal /100ml NO3 as N mg/I Pb Lead mg/I Coliform: MF Total /100ml Phosphorus: Total as P mg/I Zn - Zinc mg/1 Dissolved Solids: Total 54 mg/I Al - Aluminum mg/I Pesticides/Herbicides (Specify Compounds) pH (when analyzed) units Ba Barium mg/I ug/I TOC 1.5 mg/I Ca Calcium mg/I ug/I Chloride 6.91 mg/I Cd Cadmium mg/I ug/I Arsenic mg/I Chromium: Total mg/I Other (Specify) ug/I Grease and Oils mg/I Cu - Copper mg/I ug/I Hardness: Total mg/I Fe - Iron mg/I ug/I Phenol mg/I Hg - Mercury mg/I ug/I Sulfate G1.0 m /I K - Potassium g mg/I ug/I Specific Conductance uMhos Mg - Magnesium mg/I ug/I Total Ammonia(NH3 t NH 4) mg/I Mn - Manganese mg/I Note: TKN as N mg/I Na - Sodium mg/I Values should reflect total concentrations I TIFY T AT T IS RE ORT IS TRUE AND ACCURATE. * See back for instructions ( _ * *Submit blue and green copies to address above. NATURE OF PERMITTEE (OR AUTHORIZED AGENT*) DATE GW-59 evised 7/85 COMPLIANCE MONITORING REPORT FORM Environmental Management Division Groundwater Section P.O. Box 27687 Raleigh,N.C. 27611 (919)733-5083 Facility Name Morganite Inc. County Harnett '` s Address One Morganite Drive Permit Number: NC0060747 Dunn, NC 28334 Non -Discharge _ Well Location W-1=1ocated berm between settling pond and polishing pond NPDES NC00 Well Identification Number Well #1 Well Depth 20 Ft. Water Use Well Diameter 2 inches Sample (Screened) Interval 15 Ft. To 20 Ft. Injection Well Depth to Water Level 10•7 ft. below measuring point. (before sampling) Well Construction '' \A Measuring point is 3 feet above land surface Other Monitoring wc+l Gallons of water pumped bailed before sampling 2 gal. Field Analysis: pH 6.0 Specific Conductance 43 uMhos Temp. 20 oC Odor None Appearance Clear Date Sample Collected 12-4-89 Date Lab Sample Analyzed 1-5-90 Laboratory Name Chemical and Environmental Technology Certification No. 96 COD e_10 mg/I NO2 as N mg/I Ni Nickel mg/I Coliform: MF Fecal /100ml NO3 as N mg/I Pb Lead mg/I Coliform: MF Total /100ml Phosphorus: Total as P mg/I Zn Zinc mg/I Dissolved Solids: Total 59 mg/I Al Aluminum mg/I Pesticides/Herbicides (Specify Compounds) pH (when analyzed) units Ba Barium mg/I ug/I TOC 1.6 mg/I Ca Calcium mg/I ug/I Chloride 8.50 mg/I Cd Cadmium mg/I ug/I Arsenic mg/I Chromium: Total mg/I Other (Specify) ug/I Grease and Oils mg/I Cu - Copper mg/I ug/I Hardness: Total mg/I Fe - Iron mg/I ug/I Phenol mg/I Hg - Mercury mg/I ug/I Sulfate 3.0 mg/I K - Potassium mg/I ug/I Specific Conductance uMhos Mg - Magnesium mg/I ug/I Total Ammonia(NH3 t NH mg/I Mn - Manganese mg/I 4) Note: TKN as N mg/I Na - Sodium mg/I - Values should reflect total concentrations I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE. .. * See back for instructions 44h * Submit blue and green copies to address above. NATURE OF PERMITTEE (OR AUTHORIZED AGENT*) DATE GW-59 evised 7/85 Environmental Management Division COMPLIANCE MONITORING Groundwater Section REPORT FORM P.O. Box 27687 Raleigh,N.C. 27611� (919)733-6083 Facility Name Morganite Inc. County Harnett ,� • »xt Address One Morganite Drive Permit Number: N Dunn, NC 28334 Non -Discharge N•� Well Location W-1 = located berm between settling pond and polishing pond NC00 NPDES 7 " v Well Identification Number Well #1 Well Depth 20 Ft. Water Use rilmov Well Diameter 2 inches 15 Sample (Screened) Interval Ft. 20 To Ft. Injection Well �1 �x` Depth to Water Level 9•25 ft. below measuring point. (before sampling) Well Construction Measuring point is 3 feet above land surface Other . Monitoring Well Gallons of water pumped bailed before sampling 2 gal. Field Analysis: pH Specific Conductance uMhos Temp. o C Odorpp�r none Appearance Clear Date Sample CollectedDate Lab Sample Analyzed Laboratory Name Chemical and Environmental Technology Certification No. 96 COD 410.0 mg/I NO2 as N mg/I Ni _ Nickel mg/I Coliform: MF Fecal /100ml NO3 as N mg/I Pb -Lead mg/I Coliform: MF Total 1100ml Dissolved Solids: Total 50.0 mg/I pH (when analyzed) units TOC Chloride 9.0 Arsenic Phosphorus: Total as P mg/I Zn - Zinc rng/I AI - Aluminum mg/I Pesticides/Herbicides (Specify Compounds) Ba - Barium mg/I ug/I mg/I Ca - Calcium _ mg/I Cd - Cadmium mg/I mg/I Chromium: Total mg/I Grease and Oils mg/I Hardness: Total mg/I Phenol mg/I Sulfate 6.0 mg/I Specific Conductance 60 uMhos Total Ammonia(NH3 t NH 4) mg/I TKN as N mg/I Cu - Copper mg/I Fe - Iron mg/I Hg - Mercury mg/I K - Potassium mg/I Mg - Magnesium mg/I Mn - Manganese mg/I Na - Sodium mg/I I C TIFY THAT THIS EPORT IS TRUE AND ACCURATE. 0 / NATURE OF PERMITTEE (OR AUTHORIZED AGENT#) DATE GW-59 Revised 7/85 um - PENT —ug/I • Note: Values should reflect total concentrations # See back for instructions # # Submit blue and green copies to address above. COMPLIANCE MONITORING REPORT FORM Environmental Management Division Groundwater Section P.O. Box 27687 Ralelgh,N.C. 27611 (919)733-5083 Facility Name Morganite Inc County Ha: Address One Morganite Drive Permit Number: Dunn, NC 28334 Well Location W-2 = located directly adjacent to polishing pond & Juniper Well #2 Creek Well Identification Number Well Depth 18 Ft. Well Diameter 2 inches Sample (Screened) Interval 13 Ft. To 18 Ft. Depth to Water Level 2.8 ft. below measuring point. (before sampling) Measuring point is 2 feet above land surface Gallons of water pumped bailed before sampling 2 gal. Nan-Disf NPDES. Water Use n - Injection Well 010 Pi G . - Well Construction 4 Other. Monitorimg Well Field Analysis: pH Specific Conductance uMhos Temp. 19 o C Odor rnone Appearance Cloudv Date Sample Collected 71 1.31 /I Date Lab Sample Analyzed T%7 /�1 tq Laboratory Name Chemical and Environmental Technology Certification No. 96 COD --10 mg/I NO2 as N mg/I Ni Nickel Coliform: MF Fecal /100ml NO3 as N mg/I Pb Lead Coliform: MF Total 1100ml Phosphorus: Total as P Dissolved Solids: Total 15.0 mg/I pH (when analyzed) units TOC 6.9 mg/I Al - Aluminum mg/I Zn - Zinc mg/i mg/I g/I Pesticides/Herbicides (Specify Compounds) Ba - Barium mg/I Ca - Calcium ug/I ug/I Chloride 8.0 mg/I Cd - Cadmium mg/I ug/I Arsenic mg/1 Chromium: Total mg/j Other (Specify) ug/I Grease and Oils mg/1 Cu- Copper mg/I ug/I Hardness: Total mg/I Fe - Iron mg/I ug/I Phenol mg/l. Hg - Mercury mg/I ug/I Sulfate 6.0 mg/I K - Potassium mg/I ug/I Specific Conductance so uMhos Mg - Magnesium mg/I ug/I Total Ammonia(NH3 t NH 4) mg/I TKN as N mg/I I CERTIFY THAT THIS REPOR I§ TRUE AND ACCURATE SIGNPffURE OF PERMITTEE (OR AUTHORIZED AGENT*) DATE GW-69 Revi ed 7/85 Mn - Manganese Na - Sodium .mg/I Note: mg/I Values should reflect total concentrations * See back for instructions **Submit blue and green copies to address above. n Environmental Management Division COMPLIANCE MONITORING Groundwater Section REPORT FORM P.O. Box 27687 Raleigh,N.C. 2761 1 (919)733-5083 Facility Name Morcranite Inc. County Harnett Address One Morcranite Drive Permit Number: NC0060747,r t Dunn, NC 28334 Non -Discharge %_,— Well Location W-2=1ocated directly adjacent to nolishing pond and dvniper NPDES NC006q 9V� dr9 Well Identification Number Well #2 Well 18 Creek Depth Ftn p . Water Use Well Diameter 2 inches Sample (Screened) Interval 13 Ft. To 18 Ft. Injection Well Depth to Water Level 2.58 ft. below measuring point. (before sampling) Well Construction C''�a Measuring point is 2 feet above land surface Other , Monitoring Well Gallons of water pumped bailed before sampling 2 Field Analysis: pH 5.6 Specific Conductance uMhos Temp. 14 °C Odor none Appearance Clear Date Sample Collected 3-20-89 Date Lab Sample Analyzed 3-22-89 to 4-3—A9 Laboratory Name Chemical and Environmental Technoloav Certification No. 96 COD 26 mg/I NO2 as N mg/I Ni Nickel mgIA Coliform: MF Fecal /100ml NO as N mg/I Pb Lead mg/I Coliform: MF Total Dissolved Solids: Total 62 pH (when analyzed) TOC 5.5 Chloride 7 Arsenic Grease and Oils Hardness: Total Phenol Sulfate 111 /100ml Phosphorus: Total as P mg/I Zn - Zinc mg/I Al Aluminum mg/I Pesticides/Herbicides (Specify Compounds) units Be Barium mg/I ug/I mg/I mg/I mg/I mg/I mg/I Ca - Calcium. Cd - Cadmium mg/I me/1 Chromium: Total mg/I Cu- Copper mg/I Fe - Iron mg/I Hg - Mercury mg/I Specific Conductance 38.0 uMhos K - Potassium mg/I Mg - Magnesium mg/I Total Ammonia(NH3 t NH 4) mg/I Mn - Manganese mg/I TKN as N mg/I Na - Sodium mg/I I CERTIFY THAT TH JR�EPFIT IS TRUE AND ACCURATE. SI TURE OF PERMITTEE (OR AUTHORIZED AGENT*) DATE GW-59 Rev sed 7/85 ug/I ug/1 Other (Specify) ug/I tS�L�+�f �� ��. Il,L fil ! . •21 & Z ENV. MANAGEMENT ug/I Note: Values should reflect total concentrations * See back for instructions **Submit blue and green copies to address above. COMPLIANCE MONITORING Environmental Management Division j /J r, Groundwater Section r L�(� REPORT FORM P.O. Box 27687 Raleigh,N.C. 27611 (919)733-5083 Facility Name Moraanite Inc. County Harnett P i, parm r-.. , Address One Moraanite Drive Permit Number: NCO06 e�j ] f� Dunn, NC 28334 r� Non -Discharge ---� Well Location W-1=located berm between settling pond and polishing pond , NPDES NCO060747 ��Eq Well Identification Number Well #1 Well Depth 20 Ft. Water Use 001VDWATFR 2 inches Well Diameter Sample (Screened) 15 20 Interval Ft. To Ft. Al Injection Well. ��-�'IIrp�rz Depth to Water Level 10.42 ft. below measuring point. (before sampling) Well Construction Measuring point is 3 feet above land surface Other. Monitoring well Gallons of water pumped bailed before sampling 2 Field Analysis: pH 6.2 Specific Conductance uMhos Temp. 14 oC Odor None Appearance Clear Date Sample Collected 3-20-89 Date Lab Sample Analyzed 3-22-89 to 4-3-89 Laboratory Name Chemical and Environmental Technology Certification No. 96 COD 37 mg/I NO as N 2 mg/I Ni -Nickel mg/I Coliform: MF Fecal /100ml NO3 as N mg/I Pb -Lead mg/I Coliform: MF Total /100ml Phosphorus: Total as P mg/I Zn - Zinc mg/I Dissolved Solids: Total 63 mg/I Al Aluminum mg/I Pesticides/Herbicides (Specify Compounds) PH (when analyzed) units Be Barium mg/1 ug/I TOC 9.4 mg/I Ca - Calcium mg/I u9 /I Chloride 7 mg/I Cd - Cadmium_ mg/I ug/I Arsenic mg/I Chromium: Total mg/I Other (Specify) ug/I Grease and Oils mg/I Cu - Copper mg/I ug/I Hardness: Total mg/I Fe - Iron mg/I ug/I Phenol mg/I Hg - Mercury mg/I ug/I Sulfate 110 mg/I K - Potassium mg/I APR 21 1989 u9 /l Specific Conductance 46.0 uMhos Mg - Magnesium mg/I ENV M NAGEMENT u /l Total Ammonia(NH3 t NH 4) mg/I Mn -Manganese mg/I FAYETTEVILLE REG. OFFICEg Note: TKN as N mg/I Na - Sodium mg/I — Values should reflect total concentrations I CERTIFY TH THIS PORT IS TRUE AND ACCURATE. G/y * See back for instructions * *Submit blue and green copies to address above. _/' SIG yt RE OF PERMITTEE (OR AUTHORIZED AGENT*) DATE GW-59 Reviis,sd 7/85 Environmental Management Division 5$ COMPLIANCE MONITORING Groundwater Section 14tl9 REPORT FORM P.O. Box 27687 �� D Raleigh,N,C. 27611 (919)733-5083 J�N Facility Name Moraanite Tnc _ County Harnett �Le�� Address One Morganite Drive Permit Number: NCO'r/�p08A1. , DWAIFR CS�+ inr�_ Dunn. NC 28334 Non -Discharge RALEIGH NC Well Location w-7=1nnated directly adjacent to palichingpond A .Tnnip r Creek NPDES NCO060747 Well Identification Number Well #2 Well Depth 18 Ft. Water Use Well Diameter 2 inches Sample (Screened) Interval 13_Ft. To 18—Ft. Injection Well Depth to Water Level 2.67 ft. below measuring point. (before sampling) Well Construction Measuring point is 2 feet above land surface Other . monitoring well Gallons of water pumped bailed before sampling 2 gallons Field Analysis: pH 5-'4 Specific Conductance uMhos Temp. 19 oC Odor none Appearance clear Date Sample Collected 11-1S-88 Date Lab Sample Analyzed 11-19-88 Laboratory Name Chemical and 'Environmental Technology Certification No. 96 COD less than 1 mg/I Coliform: MF Fecal /100ml Coliform: MF Total /100ml Dissolved Solids:.Total 2 mg/I pH (when analyzed) units TOC 3.1 mg/I Chloride 12.6 mg/I Arsenic mg/1 Grease and Oils mg/I Hardness: Total mg/I Phenol mg/I Sulfate mg/I Specific Conductance 98 uMhos NO2 as N NO3 as N— mg/I Ni Nickel mg/I mg/I Pb Lead mg/I Phosphorus: Total as P mg/I Al - Aluminum mg/I Be - Barium mg/I Ca - Calcium mg/I Cd - Cadmium mg/I Chromium: Total mg/I Cu- Copper mg/I Fe - Iron mg/I Hg - Mercury mg/I K - Potassium mg/I Mg - Magnesium mg/I Total Ammonia(NH3 t NH 4) mg/I Mn - Manganese mg/I TKN as N mg/I Na - Sodium mg/I I CERTIFY TNT T I REPO T IS TRUE AND ACCURATE. Ia d SIGNA OF PERMITTEE (OR. AUTHORIZED AGENT*) DATE GW-59 Revis 7/85 Zn - Zinc Pesticides/Herbicides (Specify Compounds) ug/I ug/I ug/I EPARTMENT OF NATURAL RESOURCEAAND ug/I COMMUNITY DEVELOPMENT Note: FAYETTEVILLE REGIONAL OFFICE 'Values should reflect total concentrations * See back for instructions f* Submit blue and green copies to .address above. COMPLIANCE MONITORING REPORT FORM Facility Name Morganite Inc. Address One Morganite Drive Environmental Management Division Groundwater Section P.O. Box 27687 jail Raleigh,N.C. 27611 (919)733-6083 Dunn, NC 28334 Well Location W-1=located- berm between settling pond and polishing Jgnnd Well Identification Number Well #1 Well Depth 20 Ft. Well Diameter 2 inches Sample (Screened) Interval is Ft. To_20_Ft. County Harnett . `✓ Permit Number: 11C006074Z........�<..a IFS .cr=a+,:a� G�VVY�PVpVAR I�ISP1� a9'lW` 1'YV�Y Non -Discharge acea rtlRij NPDES NC0060747 Water Use Injection Well Depth to Water Level 10-92 ft. below measuring point. (before sampling) Well Construction Measuring point is 3 feet above land surface Other Monitoring Well Gallons of water pumped bailed before sampling 2 gallons Field Analysis: pH 5.8 Specific Conductance uMhos Temp. 20 oC Odor none Appearance clear Date Sample Collected 11-15-88 Date Lab Sample Analyzed 11-19-88 Laboratory Name Chemical and Enviromental Technology Certification No. 96 COD less than 1 mg/I NO2 as N mg/I Ni - Nickel mg/I Coliform: MF Fecal /100ml NO3 as N mg/I Pb -Lead mg/I Coliform: MF Total /100ml Phosphorus: Total as P mg/I Zn - Zinc mg/I Dissolved Solids: Total 10 mg/I Al - Aluminum mg/I Pesticides/Herbicides (Specify Compounds) pH (when analyzed) units Ba Barium mg/I ug/I TOC 3.1 mg/I Ca - Calcium mg/I ug/I Chloride 8.4 mg/I Cd Cadmium mg/I ug/I Arsenic mg/I Chromium: Total mg/I Other (Specify) ug/I Grease and Oils mg/I Cu - Copper mg/I ug/I Hardness: Total mg/I Fe Iron mg/I ug/I Phenol mg/I Hg - Mercury mg/I ug/I Sulfate mg/I K - Potassium mg/I -JAN It 1989 ug/I Specific Conductance 120.1 uMhos Mg, - Magnesium mg/I ug/I Total Ammonia(NH3 t NH 4) mg/I Mn - Manganese mg/I AO coMMUNM DEEVEtO tENi TKN as N mg/I Na -Sodium mg/I Note: FAYETTEVILLERERIQNAILGFRM Values should reflect total concentrations I CERTIFY THAT THIS RE ORT IS TRUE AND ACCURATE. * See back for instructions ���� *#Submit blue and green copies to address above. NA FIE OF PERMITTEE (OR AUTHORIZED AGENT*) DATE GW-59 evised 7/85 COMPLIANCE MONITORING REPORT FORM Facility Name Morganite Inc. Address One Morganite Drive Environmental Management Division Groundwater Section P.O. Box 27687 Ralelgh,N.C. 27611 (919)733-5083 County Harnett Permit Number: NCO060747 Dunn, NC 28334 Non -Discharge Well Location W-1=located berm between settling pond and polishing .pond NPDES NCO060747 Well Identification Number Well #1 Well Depth 20 Ft. Water Use SEP 15 1980 Well Diameter 2 inches Sample (Screened) Interval 5 Ft. To 20 Ft. Injection Well ENV. MiA?-iA'-EMENT Depth to Water Level 1o.s3 ft. below measuring point. (before sampling) Well Construction FFICE Measuring point is 3 feet above land surface Other. Monitoring Well Gallons of water pumped bailed before sampling 2 cal. Field Analysis: pH 5.9 Specific Conductance uMhos Temp. 19 oC Odor none Appearance r1Par Date Sample Collected 7-20-88 Date Lab Sample Analyzed 8-16-88 (completed) Laboratory Name Webb Technical Group, Inc. Certification No. 67 COD 26.8 * mg/I NO2 as N mg/I Ni - Nickel mg/I Coliform: MF Fecal /100ml NO3 as N mg/I Pb -Lead mg/I Coliform: MF Total /100ml Phosphorus: Total as P mg/I Zn - Zinc •10 mg/I Dissolved Solids: Total 30 mg/I Al Aluminum mg/I Pesticides/Herbicides (Specify Compounds) pH (when analyzed) units Be Barium mg/I ug/I TOC 3.474 mg/I Ca Calcium mg/I ug/I Chloride 9.50 mg/I Cd Cadmium mg/I ug/I Arsenic mg/I Chromium: Total mg/I Other (Specify) ug/I Grease and Oils mg/I Cu - Copper .10 mg/I ug/I Hardness: Total mg/I Fe - Iron mg/I ug/I Phenol mg/I Hg - Mercury mg/I ug/I Sulfate 1369 * mg/I K - Potassium mg/1 ug/I P 2 1988 Specific Conductance 85.s uMhos Mg -Magnesium mg/I ug/I Total Ammonia(NH3 t NH 4) mg/I Mn - Manganese mg/I GROUNDWATER SECTION Note: TKN as N . mg/I Na - Sodium mg/I RALE(IGH NC IS TRUE AND ACCURATE. (SdNATURE OF PERMITTEE (OR AUTHORIZED AGENT*) GW-59 9trtsed 7/85 Values should re lec totAl concentrations • See back for instructions 8-30-88 tR#Submit blue and green copies to address above. DATE COMPLIANCE MONITORING REPORT FORM Environmental Management Division Groundwater Section P.O. Box 27687 Raleigh,N.C. 27611 (919)733-5083 Facility Name Morganite Inc. County Harnett D Address One Morganite Drive Permit Number: NCO060747 Dunn, NC 28334 Non -Discharge W-2=located directly adjacent to polishing pond and Juni er NCO060747 LSLI SEP 15 196 Well Location Y ] P NPDES Well #2 Well Well Identification Number Depth 18 Ft. Creek Well Diameter 2 inches Sample (Screened) Interval 13 Ft. To 18 Ft. Depth to Water Level 3.17 ft. below measuring point. (before sampling) Measuring point is 2 feet above land surface Gallons of water pumped bailed before sampling 2 gal, Water Use rwn/ rAA-NA('"ENT Injection Well FAYETTEVILLE PEG. OFFICE Well Construction Other. Monitoring Well Field Analysis: pH 5.3 Specific Conductance -uMhos Temp. 19 oC Odor Appearance Date Sample Collected 7-20-88 Date Lab Sample Analyzed 8-16-88 (completed) Laboratory Name Webb Technical Group, Inc. Certification No.. 67 rnn 13.21 * m A NO as N Coliform: MF Fecal Coliform: MF Total _ g /100ml /100ml Dissolved Solids: Total 30 mg/1 pH (when analyzed) units TOC 6.217 2 NO3 as N Phosphorus: Total as P mg/I Ni Nickel mg/I mg/I Pb Lead mg/I mg/1 Al - Aluminum mg/I Ba - Barium mg/I Ca - Calcium _ Chloride 12.5 mg/I Cd - Cadmium Arsenic Grease and Oils Hardness: Total Phenol Sulfate 1649 Specific Conductance 67.4 Total Ammonia(NH3 t NH 4) TKN as N I C�TIFY WT ,HIVREF mg/1 Chromium: Total mg/I Cu- Copper mg/I Fe - Iron g/I Hg - Mercury - mg/I uMhos 1 g/I Zn - Zinc .1 mg/I Pesticides/Herbicides (Specify Compounds) ug/I ug/1 g/I ug/1 g/I Other (Specify) ug/I mg/I K - Potassium mg/I Mg - Magnesium mg/I Mn - Manganese mg/I Na - Sodium_ IS TRUE AND ACCURATE. I ATURE OF PERMITTEE (OR AUTHORIZED AGENT*) GW-59 vised 7/85 mg/I mg/1 mg/I ug/I ug/I ug/I ug/I ug/I Note: GROUNDWATER SE RALEIGH, HC Values should reflect total concentrations * See back for instructions 8-30-88 **Submit blue and green copies to address above. DATE / COMPI!IIA fCE MONITORING REPORT FORM Facility Name Morganite Inc. Address One Morganite Drive Dunn, NC 28334 Environmental Management Division Groundwater Section P.O. Box 27687 Raleigh,N.C. 27611 (919)733-5083 Well Location W-1=located berm between settling pond and polishing pond Well Identification Number Well #1 Well Depth 20 Ft. Well Diameter 2 inches Sample (Screened) Interval 15 Ft. To 20 Ft. Depth to Water Level 11.25 ft. below measuring point. (before sampling) Measuring point is 3 feet above land surface Gallons of water pumped bailed before sampling 2 gal. County Harnett Permit Number: NCO060747 Non -Discharge NPDES NCO060747 Water Use Injection Well Well 'Construction Other. Monitoring Well Field Analysis: pH 6.0 Specific Conductance uMhos Temp. 20 oC Odor None Appearance clear Date Sample Collected 6-16-88 Date Lab Sample Analyzed 7-5-88 (completed) Laboratory Name Webb Technical Group. Inc. Certification No. 67 COD 5.0 mg/I NO2 as N Coliform: MF Fecal /100ml NO3 as N Coliform: MF Total . /100ml Dissolved Solids: Total 102 mg/I PH (when ana r d units TOC •0 mg/I Chloride 9.20 mg/I Arsenic mg/I Grease and Oils mg/1 Hardness: Total mg/I Phenol mg/I Phosphorus: Total as P Al - Aluminum mg/I mg/I mg/I Ba - Barium mg/I Ca - Calcium mg/I Cd - Cadmium mg/I Chromium: Total mg/I Cu - Copper .01 mg/I Fe - Iron /I Hg - Mercury mg/I Sulfate mg/I K - Potassium mg/I Specific Conductance uMhos Mg - Magnesium mg/I Total Ammonia(NWS)rt NH4) 1.0 mg/I Mn - Manganese mg/I TKN as N mg/I Na - Sodium mg/I I CERT 4TT THISZR:WORTTRUE AND ACCURATE SI A E OF PERMITTEE (OR AUTHORIZED AGENT*) DATE GW-59 Revised 7/85 Ni Nickel mg/I Pb Le mg/I Zn Zi701 esRmg/I Pesticid01a des (Aggify Compounds) _ Ar ibhlMl -E,MEW "- ug/l EAYETTEVILLE REG. O_IT1W- ug/I ug/I Other (Specify) ug/I r--,vXNka JUL 1°9 198' ug/I UKUMIDVIATER i/I Note: RALEIGH. NC Values should reflect total concentrations # See back for instructions ** Submit blue and green copies to address above. fl Environmental Management Division COMPLIANCE MONITORING Groundwater Section REPORT FORM P.O. Box 27687 Raleigh,N.C. 27611 (919)733-5083 Facility Name Morganite Inc. County _Hi Address One Morganite Drive Permit Number: NC0060747 Dunn, NC 28334 Non -Discharge Well Location W-2=1ocated directly adjacent to polishing pond & Juniper Creek NPDES NCO060747 Well Identification Number Well #2 Well Depth 18 Ft. Water Use Well Diameter 2 inches Sample (Screened) Interval 13 Ft. To 18 Ft. Injection Well Depth to Water Level 3.17 ft. below measuring point. (before sampling) Measuring point is 2 feet above land surface Well Construction T u•. • ,• - Gallons of water pumped bailed before sampling 2 gal. Field Analysis: pH 5.2 Specific Conductance uMhos Temp. 17.5 ° C Odor none Appearance clear Date Sample Collected 6-16-88 Date Lab Sample Analyzed 7-5-88 (completed) Laboratory Name Webb Technical Group Inc. Certification No. 67 COD 5.0 mg/I NO2 as N Coliform: MF Fecal /100ml NO as N Coliform: MF Total /100ml Phosphorus: Total as P Dissolved Solids: Total 63 nigh Al - Aluminum _ pH (when analyzed) units Ba - Barium TOC 8.54 mg/I Ca - Calcium Chloride 12.0 mg/I Cd - Cadmium — Arsenic mg/I Chromium: Total Grease and Oils mg/I Cu- Copper_ Hardness: Total mg/I Fe - Iron Phenol mg/I Hg - Mercury Sulfate Specific Conductance - mg/I uMhos Total Ammonia(INKiCt NH4) 1-,0 mg/I TKN as N mg/I mg/I Ni Nickel mg/I Pb Lead mg/I mg/I mg/1 Zn - Zinc .01 mg/I ]mpg/I/I Pesticides/Herbicides (Specify Compounds) 7GgYV/ r�3 121 i ug/I • •:: K - Potassium mg/I Mg - Magnesium /I Mn - Manganese mg/I Na - Sodium mg/I I CERTIFY THAT -HI)RE ORT IS TRUE AND ACCURATE. SI ATURE OF PERMITTEE (OR AUTHORIZED AGENT*) GW-59 Re ised 7185 DATE r (Specify) ug/1 ug/I AQ a 19 J ug/I rn S�MloH,g/I GROUNR AEr�C Note: Values should reflect total concentrations * See back for instructions **Submit blue and green copies to address above. Environmental Manageme ,COMPLIANCE MONITORING Groundwater Sec 'r1am REPORT FORM P.O. Box 2761 \ Raleigh,N.C. 27 (919)733-50 Facility Name Morganite Inc. Address One Morganite Dr. Well Location W-2=1ocated directly adjacent to polishing pond & ❑ ❑ ❑ p ;tea Well Identification Number Well #2 Well Depth 18 o a Well Diameter 2 inches Sample (Screened) Interval 13 Ft. To Depth to Water Level 3.71 it. below measuring point. (before s: 3 Measuring point is 2 feet above land surface - _om Gallons of water pumped bailed before sampling 2 gal. a m Field Analysis: pH Specific Conductance uMhos Date Sample Collected 12-10-87 Date Lab Sample Laboratory Name Webb Technical Group Inc. COD 31 mg/I NO2 as N Coliform: MF Fecal /100ml NO3 as N _ - -mnll Coliform: MF Total /100ml Phosphorus: Total as P E ' mlg�I Dissolved Solids: Total 28 mg/I Al Aluminum I 1?3B i� pH (when analyzed) units Ba - Barium mg/I TOC 1.178 mg/I Ca Calcium r.an:NM, //I Chloride 13.38 mg/I Cd Cadmium L _ ; l '• REG. OF g`/I Arsenic mg/I Chromium: Total mg/I Grease and Oils mg/I Cu - Copper .019 mg/I Hardness: Total mg/I Fe - Iron mg/I Phenol mg/I Hg - Mercury mg/I Sulfate 38•3 mg/I K - Potassium mg/I is Conductance 112 uMhos Mg - Magnesium mg/I (NH3 t NH 4) mg/I Mn - Manganese mg/I mg/I Na - Sodium mg/I \ �EPORT IS TRUE AND ACCURATE. Pb - Lead _ Zn - Zinc .023 mg/1 Pesticides/Herbicides (Specify Compounds) ug/I ug/I ug/1 Other (Specify) Note: 11A '16Qllh�c1C.�S�II�J':L`SsY �uyu Values should re Heeotrtota,r c �centrations * See back for instructions * * Submit blue and green copies to address above. 1 / COMPLIANCE MONITORING �• REPORT FORM Environmental Management Division Groundwater Section P.O. Box 27687 Raleigh,N.C. 27611 (919)733-5083 Facility Name Morganite Inc. County Harnett Address one Morganite Drive Permit Number: NC0060747' Dunn, NC 28334 Well Location W-1=1ocation berm between settling pond and polishing pond Well Identification Number Well 1 Well Depth 20 Ft. Well Diameter 2 inches Sample (Screened) Interval 15 Ft. To 20 Ft. Depth to Water Level 12 ft. below measuring point. (before sampling) Measuring point is 3 feet above land surface Gallons of water pumped bailed before sampling 2 gal. Non -Discharge NPDES NCO060747 Water Use Injection Well Well Construction Other. Monitoring Well Field Analysis: pH Specific Conductance uMhos Temp. 18 oC Odor none Appearance clear Date Sample Collected 12-10-87 Date Lab Sample Analyzed 1/18/88 (completed) Laboratory Name Webb Technical Group, Inc. Certification No. 67 COD 31 mg/I NO2 as N mg/I Ni - Nickel mg/I Coliform: MF Fecal /100ml NO3 as N mg/I Pb Lead mg/1 Coliform: MF Total /100ml Phosphorus: Total as P mg/I Zn Zinc .045 mg/I Dissolved Solids: Total 27 mg/I Al - Aluminum mg/I ;Pesticides/Herbicides (Specify Compounds) pH (when analyzed) units Ba - Barium mg/I ug/I TOC 1.0 mg/I Ca - Calcium mg/I ug/I Chloride 12.47 mg/I Cd - Cadmium mg/1 ug/I Arsenic m6/1 Chromium: Total mg/I Other (Specify) ug/I Grease and Oils mI Cu - Copper .048 mg/I ug/I Hardness: Total mg/I Fe - Iron mg/I niig/I Phenol mg/I Hg -Mercury mg/I � 6.17 K Potassium mg/1 >' (4 a, 1 + � � A Sulfate mg/I Specific Conductance 186 uMhos Mg - Magnesium mg/I 1` �t'� ug/I t 0:• IH Total Ammonia(NH3 t NH 4) mg/I Mn - Manganese TKN as N mg/I Na - Sodium_ I CERTIFY THATTI1G,,,REPORT IS TRUE AND ACCURATE. Grp& SONAijRE OF PERMITTEE (OR AUTHORIZED AGENT*) DATE GW-59 Rtvised 7/85 .mg/I mg/I Fvw Saba Values should re f• See back for instr'uWZns OIX"A"tl 11111* Submit blue and green copies to address above. Environmental Management Division r COMPLIANCE MONITORING Groundwater Section REPORT FORM P.O. Box 27687 / Ral i h N C 27811 eg , . . (919)733-5083 Facility Name Morganite Inc. County Harnett Address one Morganii-e D ive Permit Number: NCD060747 Dunn, NC 28334 Non -Discharge Well Location W-1=location berm between settling pond and polishing Do NPDES NCO060747 Well Identification Number Well #1 Well Depth 20 Ft. Water Use Well Diameter 2 inches Sample (Screened) Interval 15 Ft. To 20 Ft. Injection Well Depth to Water Level 13 ft. below measuring point. (before sampling) Well Construction Measuring point is 3 feet above land surface Other . Monitoring well Gallons of water pumped bailed before sampling 2 gat Field Analysis: pH Specific Conductance uMhos Temp. o C Odor none Appearance clear Date Sample Collected 6-11-87 Date Lab Sample Analyzed 6-18-87 (Completed) Laboratory Name Carolina Chemists & Consultants Inc. Certification No. •104 COD mg/I NO2 as N mg/I Ni - Nickel mg/I Coliform: MF Fecal /100ml NO3 as N mg/I Pb -Lead mg/f Coliform: MF Total /100ml Phosphorus: Total as P mg/I Zn - Zinc mg/I Dissolved Solids: Total mg/I T Al - Aluminum _ �� mg/I Pesticides/Herbicides (Specify Compounds) pH (when analyzed) units Ba - Barium MZ_mg/I � ug/I TOC 1.89 mg/I CD, Ca - Calcium ^' �' mg/I ug/I Chloride mg/I g/I ug/I Arsenic mg/I Chromium: Total 70D mg/I Otfier. (Sped y.),' ug/I '�m °D ,} j{�f, � rt �J �I Grease and Oils mg/I Cu - Copper mg/I ug/I ern Hardness: Total mg/I Fe - Iron -.. ����----���{77I—mg/I ug/I sqFP v jai Phenol mg/I Hg - Mercury n� l0/ n ug/I ug 01 Sulfate mg/I K - Potassium mg/I ug/I OUNDWATER SFrr Specific Conductance, uMhos Mg -Magnesium mg/1 ION ug/I RALEIGH, NG Total Ammonia(NH3 t NH 4) mg/I Mn - Manganese mg/I Note: TKN as N mg/I Na - Sodium mg/I I CER IFY T AT TH REPORT IS TRUE AND ACCURATE. 7-+��'�-�/� SI ATURE OF PERMITTEE COR AUTHORIZED AGENT*) DATE GW-59 Re ised 7/85 Values should reflect total concentrations * See back for instructions tR 7R Submit blue and green copies to address above. Environmental Management Division COMPLIANCE MONITORING Groundwater Section ` REPORT FORM P.O. Box 27687 Raleigh,N.C. 27611 (919)733-5083 Facility Name Morganite Inc. Cpunty Harnett Address One Morganite Drive Permit Number: NC0060747 Dunn, NC 28334 Non -Discharge Well Location W-2=located directly adjacent to polishing pond and Juniper NPDES NCDO60747 Well Identification Number Well Depth 18 Ft Creek Water Use Well Diameter 2 inches Sample (Screened) Interval 13 Ft. To 18 Ft. Injection Well Depth to Water Level 3.6 ft. below measuring point. (before sampling) Well Construction Measuring point is 2 feet above land surface Other . Monitoring Well Gallons of water pumped bailed before sampling 2 gals. Field Analysis: pH Specific Conductance uMhos Temp. o C Odor none Appearance clear Date Sample Collected 6-11-87 Date Lab Sample Analyzed 6-18-87 (Completed) Laboratory Name Carolina Chemist & Consultants Inc. Certification No. 104 COD mg/I NO2 as N mg/I Ni - Nickel mg/I Coliform: MF Fecal /100ml NO3 as N mg/I Pb -Lead mg/I Coliform: MF Total /100ml Phosphorus: Total as P mg/I Zn - Zinc mg/I Dissolved Solids: Total mg/I Al - Aluminum mg/I Pesticides/Herbicides (Specify Compounds) PH (when analyzed) units Ba - Barium mg/I ug/I TOC <0.50 mg/I Ca - Calcium mg/I ug/I Chloride mg/I Cd - Cadmium mg/I ug/f Arsenic mg/I Chromium: Total r t , ., mg/I Ot a ($p.ee� ,)j ,� �� �) ug/I Grease and Oils mg/I Cu- Copper mg/I� �a �� ug/I Hardness: Total mg/I Fe - Iron mg/I ij ug/I Phenol mg/I Hg - Mercury --� - rng/I ug/I Sulfate mg/I K Potassium mg/I GUI) ug/I Specific Conductance uMhos Mg - Magnesium mg/I I,_" ug/I Total Ammonia(NH3 t NH 4) mg/I Mn - Manganese mg/I Note: TKN as N mg/I Na - Sodium mg/I Values should reflect total concentrations I CERTI Y THA THIS EPORT IS TRUE AND ACCURATE. p, * See back for instructions Submit blue and green copies to address above. SIGNA E OF PERMITTEE (OR AUTHORIZED AGENT*) G DATE GW-59 Revised 7/85 Environmental Management Division COMPLIANCE MONITORING Groundwater Section REPORT FORM P.O. Box 27687 Raleigh,N.C. 27611 (919)733-5083 Facility Name Moraanite Inc. County Harnett Address One Moraanite Drive Permit Number: NCD060747 Dunn, NC 28334 Non -Discharge Well Location W-l=location berm between settling pond and polishing pond NPDES NCO060747 Well Identification Number Well #1 Well Depth 20 Ft. Water Use Well Diameter 2 inches Sample (Screened) Interval 15 Ft. To 20 Ft. Injection Well Depth to Water Level 13 ft. below measuring point. (before sampling) Well Construction Measuring point is 3 feet above land surface Other. Monitoring well Gallons of water pumped bailed before sampling 2 gal. Field Analysis: pH Specific Conductance uMhos Temp. o C Odor none Appearance clear Date Sample Collected 8-5-87 Date Lab Sample Analyzed 8-12-87 (completed) Laboratory Name Carolina Chemists & Consultants Inc. Certification No. 104 COD mg/I NO2 as N mg/I Ni - Nickel mg/I Coliform: MF Fecal /100ml NO3 as N mg/I Pb -Lead mg/I Coliform: MF Total /100ml Phosphorus: Total as P mg/I Zn - Zinc mg/I Dissolved Solids: Total mg/I Al Aluminum mg/I Pesticides/Herbicides (Specify Compounds) pH (when analyzed) units Ba Barium mg/I ug/I TOC mg/I Ca Calcium mg/I ug/I Chloride mg/I Cd Cadmium mg/I ug/I Arsenic mg/I Chromium: Total mg/I Other 4Specif•y)-_1A ,,___ ug/I Grease and Oils mg/I Cu - Copper Jt_ I; ulr d a mg/I j.I �! ug/I J Hardness: Total mg/I Fe - Iron mg/I s \�� ug/I Phenol mg/I Hg - Mercury mg/I 4Fp 98 igg? ug/I Sulfate 44.0 mg/I K - Potassium mg/I GROUNWAiLH ug/I Specific Conductance 130 uMhos Mg - Magnesium mg/I -• ug/I Total Ammonia(NH3 t NH4)-mg/I Mn - Manganese mg/I Note: TKN as N mg/I Na - Sodium mg/I Values should reflect total concentrations I CERTIFY THAT T IS REP FIT IS TRUE AND ACCURATE. q # See back for instructions /DATE ** Submit blue and green copies to address above. ATURE OF PERMITTEE (OR. AUTHORIZED AGENT') GW-59 vised 7/85 COMPLIANCE MONITORING REPORT FORM Environmental Management Division Groundwater Section P.O. Box 27687 Raleigh,N.C. 27611 (919)733-5083 Facility Name Morganite Inc. County Harnett Address One Morganite Drive Permit Number: NC0060747 Dunn NC 28334 Non -Discharge Well Location W-2=located directly adjacent to polishing pond and Juniper NPDES NCD060747 Well Identification Number Well Depth 18 Ft. CreekWater Use Well Diameter 2 ��es Sample (Screened) Interval 13 Ft. To 18 Ft. Injection Well Depth to Water Level 3.6 ft. below measuring point. (before sampling) Well Construction Measuring point is 2 feet above land surface Other. Monitoring Well Gallons of water pumped bailed before sampling 2 gals. Field Analysis: pH Specific Conductance uMhos Temp. o C Odor none Appearance clear Date Sample Collected 8-5-87 Date Lab Sample Analyzed 8-12-87 (completed) Laboratory Name Carolina Chemist & Consultants Inc. Certification No. 104 COD mg/I NO2 as N mg/I Ni Nickel mg/I Coliform: MF Fecal /100ml NO3 as N mg/I Pb Lead mg/f Coliform: MF Total /100ml Phosphorus: Total as P mg/I Zn - Zinc mg/I Dissolved Solids: Total mg/I Al - Aluminum mg/I Pesticides/Herbicides (Specify Compounds) pH (when analyzed) units Ba - Barium mg/I ug/I TOO mg/I Ca - Calcium mg/I ug/I Chloride mg/I Cd - Cadmium mg/I ug/I Arsenic mg/I Chromium: Total mg/I Other (Sp(ecirrfo ug/I Grease and Oils mg/I Cu Copper mg/I ug/I fI �'+' Hardness: Total mg/I Fe - Iron mg/I ug/I Phenol mg/I Hg - Mercury mg/I ug/I Sulfate .45'O mg/I K -Potassium mg/I �8 1987r- ug/I 60 _ I-� NVVVA Specific Conductance uMhos Mg - Magnesium mg/I ug/I NALElen, Total Ammonia(NH3 t NH 4) mg/I Mn - Manganese mg/I ft Note. TKN as N mg/I Na - Sodium mg/I values should reflect total concentrations I C RTIFY THAT THI EPORT IS TRUE AND ACCURATE. # See back for instructions ��w__�J � / * # Submit blue and green copies to address above. NAT S URE OF PERMITTEE (OR AUTHORIZED AGENT#) DATE GW-59 R vised 7/85 I These are retests for Monitoring Wells #1 and #2. We apologize for the results being late. Any questions, contact me, Benjy-Vick, at Morganite, Inc. - Phone (919) 892-8081. Thank you very much. ), 6, ba J.B. Vick 9-A I -YT SEP 28 1987 GROUNDWATER SECTION RALEIGH, NC tI COMPLIANCE MONITORING REPORT FORM Facility Name Address One Morganite Drive Environmental Management Division �� Groundwater Section IF `�, P.O. Box 27687 /� T E 1;;i ,1) Raleigh,N.C.27611 (919)733-5083 / SEP I f9$7 Dunn, NC 28334 Well Location W-l=location berm between settling pond and polishing_pond Well Identification Number well #1 Well Depth 20 Ft. Well Diameter 2 inches Sample (Screened) Interval 15.0 Ft. To 20.0 Ft. Depth to Water Level 11 ft. below measuring point. Cbefore sampling) Measuring point is 3 feet above land surface County Harnett Permit Number: NCD060747 ii:.vtu.c i�. I C Non -Discharge NPDES NC0060747 Water Use Injection Well Well Construction Other. Monitoring well Gallons of water pumped bailed before sampling i gal• Faint Field Analysis: pH N/A Specific Conductance N/A uMhos Temp. 17 oC Odor Sulfur Appearance (Tear Date Sample Collected 6/'30/87 Date Lab Sample Analyzed 7/16/87 (completed) Laboratory Name Carolina Chemists & Consultants Inc. Certification No. 104 COD 4.0 mg/I NO2 as N mg/I Ni - Nickel mg/I Coliform: MF Fecal Coliform: MF Total /loom] / 100ml Dissolved Solids: Total 90.0 mg/I PH (when analyzed) 6.15 units TOC 3.29 mg/I Chloride 15.33 mg/I Arsenic Grease and Oils — Hardness: Total Phenol Sulfate Specific Conductance mg/I mg/I mg/I NO3 as N � mg/I Phosphorus: Total as P mg/I Al Aluminum mg/I Be Barium mg/I Ca Calcium mg/I Cd Cadmium mg/I Chromium: Total mg/I Cu - Copper •03 mg/I Fe - Iron ma/I mg/I Hg - Mercury. mg/I K - Potassium uMhos Mg - Magnesium Total Ammonia(NH3 t NH 4) 14 mg/I Mn - Manganese mg/I TKN as N mg/I Na - Sodium mg/I I CE TIFY TH T THIS REPORT IS TRUE AND ACCURATE. ,` /�/mil//!/??�/y��/�' r 4 C--� Gam- Jz v / SI NATURE OF PERMITTEE (OR AUTHORIZED AGENT*) DATE GW-59 Re ised 7/85 Pb - Lead mg/I Zn - Zinc .018 mg/I Pesticides/Herbicides (Specify Compounds) ug/I ug/I ug/I Other (Specify) ug/I A ug/I ug/I Lua 4" ug/I HpLEIGH Note: Values should reflect total concentrations tR See back for instructions * *Submit blue and green copies to address above. COMPLIANCE MONITORING REPORT FORM Facility Name Environmental Management Division Groundwater Section P.O. Box 27687 Raleigh,N.C. 27611 (919)733-5083 County Harnett Address One Morganite Drive Permit Number: Dunn, NC 28334 Well Location W-2=located directly adjacent to polishing pond and Juniper Well #2 Creek Well Identification Number Well Depth Ft. Well Diameter 2 inches Sample (Screened) Interval 13.0 Ft. To 18.0 Ft. Inc. Depth to Water Level 3.6 ft. below measuring point. (before sampling) Measuring point is 2 feet above land surface Gallons of water pumped bailed before sampling 2:-gal. NCD060747 Non -Discharge NPDES UC0060747 Water Use Injection Well Well Construction Other, monitoring well Field Analysis: pH NSA Specific Conductance NSA uMhos Temp. 17 o C Odor none Appearance clear Date Sample Collected 6/30/87 Date Lab Sample Analyzed 7/16/87 Ccomoleted) Laboratory Name Carolina Chemists & Consultants Inc. Certification No. 104 COD 4.0 Coliform: MF Fecal Coliform: MF Total - mg/1 /100ml 1100ml Dissolved Solids: Total 41 mg/I pH (when analyzed) 5.25 units TOC 0.5 mg/I Chloride 12.60 mg/I Arsenic Grease and Oils Hardness: Total Phenol Sulfate Specific Conductance Total Ammonia(NH3 t NH 4) •14 TKN as N mg/I mg/I mg/1 mg/I mg/I Mhos mg/I mg/I NO2 as N mg/I NO3 as N r_"'s mg/I Phosphorus: Total as P mg/I Al - Aluminum mg/I Be - Barium mg/I Ca - Calcium mg/I Cd - Cadmium mg/I Chromium: Total mg/I Cu - Copper .03 mg/I Fe - Iron mg/I Hg - Mercury ng/I K - Potassium mg/I Mg - Magnesium mg/I Mn - Manganese mg/I Na - Sodium _mg/I I C !TIF HAT T I§,REPORT IS TRUE AND ACCURATE. S ATURE OF PERMITTEE (OR AUTHORIZED AGENT*) DATE GW-59 R ised 7/85 Ni Nickel mg/I Pb - Lead mg/I Zn Zinc •01 mg/I Pesticides/Herbicides (Specify Compounds) ug/I ug/I ug/I Other (Specify) ug/I ug/I gak^w"17 ug/I NX ug/I .t tf; 4 1991 ug/I GROUND ug/I �'!�! Note: MEW, 11, C- Values should reflect total concentrations * See back for instructions **Submit blue and green copies to address above. Due to miscommunication with Carolina Chemists & Consultants Inc., specific conductance and sulfate analyses were not performed. These tests are being run now and the results will be mailed to you as soon as possible. t )Benjy Vick Morganite Inc. 8/3/87 I, Environmental Management. Division COMPLIANCE MONITORING Groundwater Section REPORT FORM P.O. Box 27687 Raleigh,N.C. 27811 (919)733-6083 Facility Name Morganite Inc. County Harnett Address one Morganite Drive Permit Number: NCD060747 Dunn, N.C. 28334 Non -Discharge Well Location W-1 = located on berm between settling pond and polishing pond NPDES NCO060747 Well Identification Number Well #1 Well Depth 20.0 Ft. Water Use Well Diameter, 2 inches Sample (Screened) Interval 15.0 Ft. To 20.0 Ft. Injection Well Depth to Water Level 5.35 _ ft. below measuring point. Cbefore sampling) Well Construction Measuring point is 3 feet above land surface Other . monitoring wells Gallons of water pumped bailed before sampling 2 gals, FieldAnalysis: pH 5,6 Specific Conductance N/A uMhos Temp. 15 °C Odor None Appearance Clear Date Sample Collected 3/26/87 Date Lab Sample Analyzed 4/22/87 (completed) Laboratory Name Carolina Chemists & (Consultants Inc. Certification No. 104 COD 10 mg/I NO2 as N Ufrtg/I Ni - Nickel mg/I Coliform: MF Fecal fy� /100ml NO as N ZLL g/I Pb - Lead mg/I Coliform: MF Total r---V-I!l /100ml Phosphorus: Total as P f g/I Zn Zinc 0.026 mg/I Dissolved Solids: Total 129 mg/I Al Aluminum - Q g/I Pesticides/Herbicides (Specify Compounds) PH (when analyzed) F units Be BariumLL-J,Q' J g/I ug/I TOC 33.0 mg/I Ca - Calcium r g/I ug/I Chloride 25.3 mg/I Cd - Cadmium Z g/I ug/I Arsenic mg/I Chromium: Total ®g/I Other (Specify) ug/I Grease and Oils mg/I Cu - Copper 0.08 mg/I ug/I Hardness: Total mg/I Fe - Iron mg/I ug/I Phenol mg/I Hg - Mercury mg/I ug/I Sulfate 63,5* mg/I K - Potassium mg/I ug/I Specific Conductance 170* uMhos Mg - Magnesium mg/I ug/I Total Ammonia(NH3 t NH 4) mg/I Mn - Manganese mg/I Note: TKN as N mg/I Na - Sodium mg/I Values should reflect total concentrations I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE. # See back for instructions /7fi/R7 **Submit blue and green copies to address above, SIGNATURE OF PERMITTEE (OR AUTHORIZED AGENT*) DATE *Refer to attached note for an GW-59 Revised 7/85 explanation Environmental Management Division COMPLIANCE MONITORING Groundwater Section REPORT FORM P.O. Box 27687 Raleigh,N.C. 27611 Mor anite Inc. (919)733-6083 y Harnett Facility Name g Count Address one Morganite Drive Permit Number: NCD060747 Dunn, N.C. 28334 Non -Discharge Well Location W-2 = Located directly adjacent to polishing pond and Juniper NPDES NCO060747 #2 Creek Well Identification Number Well Well Depth Ft. Water Use Well Diameter 2 inches Sample (Screened) Interval 13.0 Ft. To 18.0 Ft. Injection Well Depth to Water Level 1.67 ft. below measuringg point. (before sampling) Well Construction Measuring point is 2 feet above land surface Other . monitoring wells Gallons.of water pumped bailed before sampling 2 gals. Field Analysis: pH 5.3 Specific Conductance N/A uMhos Temp. 15 cC Odor None Appearance Clear Date Sample Collected 3/26/87 Date Lab Sample Analyzed 4/22/87 (canpleted) Laboratory Name Carolina Chemists & Consultants Inc. Certifyration No. 104 COD 10 mg/I NO2 as N LL g/I Ni - Nickel mg/I Coliform: MF Fecal /100m1 NO3 as Na7�g/I Pb Lead mg/I Coliform: MF Total /100ml Phosphorus: Total as P °D r"Ig/I Zn Zinc 0.020 mg/I Dissolved Solids: Total 55 mg/I Al Aluminum (T'1 ea . a�yg/I Pesticides/Herbicides (Specify Compounds) tt -z pH (when analyzed) units Ba Barium E " 11 4mJlg/I ug/I 10_8 ( ¢ Z> TOC mg/I Ca - Calcium •10/1 ug/I f r F- Chloride 13•2 mg/I Cd Cadmium `'' Ua /I ug/1 Arsenic mg/I Chromium: Total ragA Other (Specify) ug/I Grease and Oils mg/I Cu - Copper 0.03 mg/I ug/I Hardness: Total mg/I Fe - Iron mg/I ug/I Phenol mg/I Hg - Mercury rng/I ug/I Sulfate 52,7* mg/I K - Potassium mg/I ug/I Specific Conductance 98* uMhos Mg - Magnesium mg/I ug/I Total Ammonia(NH3 t NH 4) mg/I Mn - Manganese mg/I Note: TKN as N mg/I Na - Sodium mg/I Values should reflect total concentrations II C THAT THIS REPORT IS TRUE AND ACCURATE. � #See back for instructions /.fin R7 tR 1R Submit blue and green copies to address above. SIGNATURE OF PERMITTEE (OR AUTHORIZED AGENT*) DATE *Refer to attached note for an GW-59 Revised 7/85 explanation Facility NameYnDrGenife MAI7f Pol.Source 5LU06F' County llgfA/E7T Permit No. Ale,DD/o-4y:7 •' No. of Wells o; Sampling Dates By Well No. Parameters TDS IMA � M � _� �®MMMM©MM®MM—_--- • ► 5MMMMMMMM—MMM_M-- MMMMMMMMM_MM—__MM SM i , MMMMMM_MM—M—_- ENWRIGHT LABORATORIES. INC. A subsidiary of ENWRIGHT ASSOCIATES, INC. CERTIFICATE OF ANALYSIS CLIENT: Morganite, Inc. PROJECT: Monthly Monitoring LAB NO. 86-36658 86-36659 SAMPLE ID: WELL 1 WELL 2 Parameters: Total Organic Carbon 2.4 <1.0 Ammonia Nitrogen Biochemical Oxygen Demand Total Suspended Solids Copper Zinc DATE RECEIVED: 10/17/86 DATE COMPLETED: 11/7/86 DATE REPORTED: 11/10/86 86-36660 86-36661 86-36662 EFFLUENT DOWNSTREAM UPSTREAM <0.1 3 3 5 0.02 <0.01 The above results are reported in mi.11igrams per liter. Analytical methods are those approved by the U.S. Environmental Protection Agency. CHR/kdw Respectfully submitted, ENWRIGHT LABORATORIES, INC. Charles H. Re Ph.D. Laboratory Manager 14 SHIPMENTS TO: 25 Woods Lake Road a Greenville, South Carolina 29607 ■ (803) 235-0707 InAARROLINA HEMISTS & U rn ONSULTANTS, Inc. v October 24, 19% CCCB6824 Morganite Company 401 N. Ashe Avenue Dunn, NC 28334 Attention: Janet Kent 5500 Commercial Avenue • Raleigh, N.C. 27612 • 19191 707-3061 Subject: Analysis of Sample Received 10-17-86 Sample Identificiation: 1. Well 41 2. Well 42 RESULTS 1 2 Total Organic Carbon, as C, mg/1 19.3 12.4 Vance C. Allen Vice President, Special Projects VCA/km MAR 28 1996 Morganite Incorporated ENV. MANAI r- ONE MORGANITE DRIVE FAYRTEVILLE ki- ®�� N. NORTH CAROLINA 28334 TELEPHONE 919-892.8081 TELEx 579388 March 25, 1986 Dept. of Natural Resources and Community Development Fayetteville Regional Office Wachovia Building, Suite 714. Fayetteville, NC 28301 Gentlemen: - The results of test analyses of monitoring wells for January were as follows: Well #1 Well #2 Ph 5.45 5.90 Zinc <0.01 <0.01 TOC 5.0 <5.0 TDS 80.0 40.0 Conductivity 100.0 50.0 Chemical Oxygen 4.0 4.0 Demand Chloride 18.0 8.0 Sulfate 14.0 6.0 Water Level 5.0 ft. 1.50 ft. The above results are reported in milligrams .per liter. Analytical methods are those approved by the U.S. Environmental Protection Agency respectively submitted by EljWright Laboratories Inc. We hope that these results meet with your approval. Please call us if there are any questions. Sincerely, - indsay M. Strickland Plant Engineer LMS:mck ' c Morgan Morganite Incorporated January 2, 1786 ONE MORGANITE DRIVE DUNN. NORTH CAROLINA 28334 TELEPHONE 919.892.8081 TELE% 579388 Dept.. of Natural Resources and Community Development Fayetteville Regional Office Wachovia Building, Suite 714 Fayetteville, NC 28301 Gentlemen: The results of test analyses of monitoring wells for November were as follows: Well #1 Well #2 Ph Zinc TOC TDS 5.98 0.03 6.0 76.0 Conductivity 71.0 Chemical Oxygen 4.0 Demand Chloride 19.0 6.02 0.02 <5.0 52.0 44. 1�h l 8.0 JAN 6 1986 6.0 ENV. ty"NAGEMEN'T . Sulfate 4.0 3.eFAYETT dIPRMOFF[M Water Level 5.17 ft 0.75 ft The above results are reported in milligrams per liter. Analytical methods are those approve y e . Environmental Protection Agency respectively submitted by Enwright Laboratories Inc. We hope that these results meet with your approval. Please call us if there are any questions. Sincerely, Lindsay M. Strickland Plant Engineer LMS:mck c Morgan Morganite Incorporated ONE MORGANITE DRIVE DUNN. NORTH CAROLINA 28334 TELEPHONE 919-892-SO81 TELEX 579368 October 17, 1985 Dept. of Natural Resources and Community Development Fayetteville Regional Office Wachovia Building, Suite 714 Fayetteville, NC 28301 Gentlemen: The results of test analyses of monitoring wells for September as follows: Well #1 Well #2 Ph 5.51 5.44 ? Zinc /^„� <0.01 0.01 Gt/ TOC 18.0 <5.0 TDS 68.0 60.0 Conductivity 80.0 60.0 Chemical Oxygen 12.0 16.0 Demand Chloride 18.0 7.0 Sulfate 3.0 5.0 Water Level 5.61 ft 1.92 ft The above results are reported in milligrams per liter. Analytical methods are those approved by the U.S. Environmental Protection Agency respectively submitted by Enwright Laboratories Inc. We hope that these results meet with your approval. call us if there are any questions. I1 � Respectfully submitt d, �L � "' i�-,Fl,�� Environmental Enginee MAH:mc�i Please c Morgan 1� Morganite Incorporated September 13, 1985 Dept. of Natural Resources and Community Development Fayetteville Regional Office Wachovia Building, Suite 714 Fayetteville, N.C. 28301 Gentlemen: ONE MORGANITE DRIVE DUNN. NORTH CAROLINA 28334 TELEPHONE 919-802.8081 TELE% 579368 In error, we forgot to report the pH value -of our two monitoring wells, on Our last report. The results, of. test analysis of wells for July were as 9p1,7 ows•p "well'#1 well #2 pH 5.65 5.26 please update your files,accordingly,-and once again we are sorry for the ihconvenenoe,' Kw"-Mcl : c;. Respectfu ly, submitted Mar A. Hussung E ironmental Engineer C Morgan Morganite Incorporated August 9, 1985 ONE MORGANITE DRIVE DUNN. NORTH CAROLINA 28334 TELEPHONE 919-892.8081 TELEX 579368 Dept. of Natural Resources and Community Development Fayetteville Regional Office ENV.MANAGEMEN1 Wachovia Building, Suite 714 FAYMEVILLE REG. OFFICI Fayetteville, NC 2B301 Gentlemen: The results of test analyses of monitoring wells for July were as follows: / Well #1 Well #2 Zinc 0.02 0.02 TOC <5.0 <5.0 TDS 72.0 60.0 Conductivity 90.0 60.0 Chemical Oxygen 12.0 2.0 Demand Chloride 15.0 5.3 Sulfate <5.0 <5.0 Water Level 6.0 ft. 1.2 ft. The above results are reported in milligrams per liter. Analytical methods are those approved by the U.S. Environmental Protection Agency respectively submitted by Enwright Laboratories Inc. We hope that these results meet with your approval. Please call us if there are any questions. r ully submi d, Huss gental Engineer u AH:mck organ Mor anit" a Incor orated 9 P July 18, 1985 ONE MORGANITE DRIVE DUNN. NORTH CAROLINA 28334 TELEPHONE 919.892.8081 TELEX 579368 17lem 1RITI D JUL 22 1985 Dept. of Natural Resources and Community Development V. MANAGEMENT Fayetteville Regional Office ENG.OF Wachovia Building, Suite 714 FAyETTEVILU RE FIq Fayetteville, NC 2B301 Gentlemen: The results of test analyses of monitoring wells for March were as follows: Well #1 Well #2 -------------- Zinc C0.01 C0.01 TOC 5.0 5.0 TDS 596 76 Conductivity 60 50 The above results are reported in milligrams per liter. Please note the high concentrations of total dissolved solids. This occurred from bad sampling techniques and unsettling of the solids due to recent installation of the wells. Respec fully submit ed, rk A. Hussung Site Services Section Leader MAH:mck 9 M Morgan i r auin ;N -TO MORGANITE INCORPORATED One Morganite Drive DUNN, NORTH CAROLINA 28334 (919) 892-8081 5D DATE: FOLD c PLEASE REPLY TO —► 'LY _DATE: Item M70 O Wheeler Group Im. I970 SIGNED FAYETTEVILLE REG. OFFICE THIS COPY FOR PERSON ADDRESSED ' COMPLIANCE MONITORING REPORT FORM Environmental Management Division Groundwater Section P.O. Box 27687 Raleigh,N.C. 27611 (919)733-5083 Facility Name Morganite Incorporated County Harnett Address One Morganite Drive Permit Number: NC0060747 V, Non -Discharge Well Location W-1=located on berm between settling pond and polishing ponds NPDES NC0060747 Well Identification Number Well-#1 --W ll-Depth -20.-0—Pt Water -Us Well Diameter 2 inches Sample (Screened) Interval 15.0 Ft. To 20.0 Ft. Injection Well Depth to Water Level 5.35 ft. below measuring point. (before sampling) Measuring point is 3 feet above land surface Gallons of water pumped bailed before sampling 2 gals, Well Construction Other Monitoring Well Field Analysis: pH 6.37 Specific Conductance NSA uMhos Temp. 24 oC Odor None Appearance r1Par Date Sample Collected 9/25/86 Date Lab Sample Analyzed 10/14/86 (completed) Laboratory Name Enwright Laboratories COD 28 mg/I NO2 as N (D) Coliform: MF Fecal /100ml NO3 as N (D) Coliform: MF Total Certification No. mg/I Ni Nickel (D) ug/I mg/I Pb Lead (D) ug/I /100ml Phosphorus: Total as P mg/I Dissolved Solids: Total 100 mg/I pH (when analyzed) units * TOC [uo^170 mg/I Chloride (D) 21 mg/I Arsenic (D) Grease and Oils Hardness: Total (D) - Phenol Sulfate (D) Specific Conductance Al - Aluminum (D) ug/I Be - Barium (D) ug/I Ca - Calcium (D) mg/I Cd - Cadmium (D) ug/I Chromium: Total (D) mg/I mg/I ug/I 28 mg/I 250 Total Ammonia(NH3 t NH 4)(D) TKN as N (D) mg/I mg/I ug/I ug/I Cu - Copper (D) 0.04 ug/I Fe - Iron (D) ug/I Hg - Mercury (D) ug/I K - Potassium (D) ug/I Mg - Magnesium (D) Mn - Manganese (D)_ Na - Sodium (D)_ I CERTIFY THAT THIS REPO T IS TRUE AND ACCURATE. � GW-59 SIN TUBE OF PERMITTE O AUTHORIZED AGENT DA E 9/1 Zn - Zinc (D) 0.02 ug/I Pesticides/Herbicides (Specify Compounds) ug/I ug/I ug/I Other (Specify) ' ug/I ug/I ug/I ug/I ug/I .ug/I D =Dissolved Analysis- Submit Filtered mg/I Sample We See back for instructions *-X Submit blue and green copies to address above. *Refer to the attached letter for an explanation of TOC. Environmental Management Division �! COMPLIANCE MONITORING Groundwater Section REPORT FORM P.O. Box 27687 Raleigh,N.C. 27611 (919)733-5083 Facility Name Morganite Incorporated _- County Harnett Address One Morganite Drive Permit Number: NCO060747 Dunn, NC 28334 Non -Discharge Well Location W-2=located directly adjacent to polishing pond and Juniper NPDES NCO060747 Creek Well Identification Number Well #2 Well Depth 18.0 Ft. Water Use Well Diameter 2 inches Sample (Screened) Interval 13.0 Ft. To 18.0 Ft. Injection Well Depth to Water Level 2.80 ft. below measuring point. (before sampling) Well Construction Measuring point is 2 feet above land surface Other Monitoring wells Gallons of water pumped bailed before sampling 2 gals Field Analysis: pH 5.28 Specific Conductance N/A uMhos Temp. 24 °C Odor None Appearance Clear Date Sample Collected 9/25/86 Date Lab Sample Analyzed lo./14A6 (Completed) Laboratory Name Enwright Laboratories Certification No. 66 COD 8 mg/I NO2 as N (D) mg/I Ni Nickel (D) ug/1 Coliform: MF Fecal /100ml NO3 as N (D) mg/I Pb Lead (D) ug/I Coliform: MF Total /100ml Phosphorus: Total as P mg/I Zn -Zinc (D) .40.01 ug/I Dissolved Solids: Total 56 mg/I Al Aluminum (D) ug/I Pesticides/Herbicides (Specify Compounds) PH (when analyzed) units Ba Barium (D) ug/I ugA * TOCa5--. mg/I Ca Calcium (D) mg/I ug/I Chloride (D) 10 mg/I Cd Cadmium (D) ug/I ug/1 Arsenic (D) ug/I Chromium: Total (D) ug/I Other (Specify) ug/I Grease and Oils mg/I Cu - Copper (D) < 0.02 ug/I ug/I Hardness: Total (D) mg/I Fe - Iron (D) ug/I ug/I Phenol ug/I Hg Mercury CD) • ug/I ug/I Sulfate (D) 5 mg/I K - Potassium (D) '�-'F3 ewVf ug/I (- ug/I Specific Conductance 140 uMhos Mg - Magnesium (D) mg/1 CT 3 0 1986 ug/I OUNFI II," FVF� S �T{Or Total Ammonia(NH t NH )(D) 3 4- mg/I Mn Manganese (D) ug/I D = DissolX".'419,,sig— Submit Filtered TKN as N (D) mg/I Na - Sodium (D) mg/I Sample I CERTIFY THAT THIS REPO T IS TRUE AND ACCURATE. ` ' -A See back for instructions 4d7SI �Q ** Submit blue and green copies to address above. N TURE OF PERMITTEE bZLAqTHORIZED AGENT DA E *Refer to the attached letter for an GW-59 explanation of TOC. Environmental Manag ' COMPLIANCE MONITORING Groundwater REPORT FORM P.O. Box 2 Raleigh,N.C. (919)733- Facility Name Morganite Incorporated Address nnp M,gnnite Dy4,.e Well Location w-1=1ocated on berm between settling pon Well Identification Number well #1 Well Depth 2 Well Diameter 2 inches Sample (Screened) Interval 1 5 0 Ft. To_ Depth to Water Level 5 _ ft. below measuring point. (before Measuring point is 3 feet above land surface Gallons of water pumped bailed before sampling 2 gals. Field Analysis: pH 5.70 Specific Conductance —uMhos Date Sample Collected 7/31/86 Date Lab Sample L b a oratory Name Fnwr,q r rah ❑poop❑ a==o -m - o a m 3 m a ❑ 0 0 0 0 O o = s a• � F m o - nrai-nr, es COD g mg/I NO2 as N Coliform: MF Fecal /100ml NO3 as N — ,...., Coliform: MF Total /100ml Phosphorus: Total as P mg/I Dissolved Solids: Total 76 mg/I AI Aluminum mg/I pH (when analyzed) units Ba Barium mg/I TOC mg/I Ca Calcium mg/I Chloride 16 mg/I Cd Cadmium_ mg/I Arsenic mg/I Chromium: Total mg/I Grease and Oils mg/I Cu - Copper 0 _ 03 mg/I Hardness: Total mg/I Fe - Iron mg/I Phenol mg/I Hg - Mercury mg/I Sulfate 28 mg/I K - Potassium mg/I Specific Conductance 11000 uMhos Mg - Magnesium mg/I Total Ammonia(NH3 t NH q) mg/I Mn - Manganese mg/I TKN as N mg/I Na - Sodium mg/I I CERTIFY THAT THIS REPORT I TRUE AND ACCURATE. SIG AT E OF PERMITTEE (0 rTHORIZ D AGENT*) A E GW-59 Revi 7/85 r o v (° x W ` Z I-11 O T.,� u1 _ OV 9 n Q n D . jo n n p yo T ? A N D T) 1 3 m (' 3 D a t +2 tf z ."—I <m n e m� S N o mT IN1 o Z �D 3c _ (ArD- Zn - Zinc (0.01 mg/I Pesticides/Herbicides (Specify Compounds) ug/I ug/I ug/I Other (Specify) ug/I ug/I ug/I 1 ug/I ug/I SEP A .7 Note: fROU 1A,Qj0jF�1pp��� �. Values should reflditP1 [l %a�trafovions * See back`for instructions �r �%LL N C * * Submit blue and green copies to address above. •' COMPLIANCE MONITORING REPORT FORM Environmental Management Division Groundwater Section P.O. Box 27687 Raleigh,N.C. 27611 (919)733-5083 Facility Name Morganite Incorporated County u tt Address One Morganite Drive Permit Number: * nn< 4.7 Dunn, NC 28334 Non -Discharge Well Location W-7=larated dirertly adiarent to pnlishing pond and NPDES Nr0060747 Well Identification Number rant i fi? Well Depth t R n Ft. Juniper Water Use Creek Well Diameter :z 4n sch Sample (Screened) Interval 12 gFt. To 4: Ft. Injection Well Depth to Water Level 1.67 ft. below measuring point. (before sampling) Well Construction Measuring point is 2 feet above land surface Other . Monitoring wells Gallons of water pumped bailed before sampling a gals - Field Analysis: pH 5.18 Specific Conductance uMhos Temp. 22 oC Odor none Appearance -71 Date Sample Collected 7,/31,/86 Date Lab Sample Analyzed 8,11 icc mete) Laboratory Name Enwright Laboratories Certification No. 66 COD <1 mg/I NO2 as N Coliform: MF Fecal /100ml NO3 as N Coliform: MF Total /100ml Phosphorus: Total as P Dissolved Solids: Total 48 mg/I pH (when analyzed) units TOC 2 mg/I Chloride Arsenic Grease and Oils mg/I mg/I mg/I Al - Aluminum Ba - Barium — Ca - Calcium. Cd - Cadmium mg/1 Ni Nickel mg/I mg/I Pb Lead mg/I mg/I Zn Zinc 0.01 mg/I ma/I Pesticides/Herbicides (Specify Compounds) mg/I mg/I mg/I Chromium: Total mg/I Cu - Copper 0.02 mg/I Hardness: Total mg/I Fe - Iron mg/I Phenol mg/I Hg - Mercury rng/I Sulfate 7 mg/I K - Potassium mg/I Specific Conductance gg uMhos Total Ammonia(NH3 t NH 4) mg/I TKN as N mg/I Mg - Magnesium mg/I Mn - Manganese mg/I Na - Sodium mg/I I CERTIFY THAT THIS REPORTP TRUE AND ACCURATE. SIGN E OF PERMITTEE (O AUTHORIZED AGENT*) *AE GW-59 Revise /85 ug/I ug/I ug/I Other (Specify:) ug/I ug /I ug/I g/I 1 P n.,.. OPOPFn yUg/I ug/I Note: Values should reflect total concentrations * See back for instructions * * Submit blue and green copies to address above. COMPLIANCE MONITORING REPORT FORM Environmental Management Division Groundwater Section P.O. Box 27687 Raleigh,N.C. 27611 (919)733-5083 Facility Name Morganite Incorporated County Harnett Address One Morganite Drive Permit Number: NCO060747 Dunn, NC. 28334 Well Location W-2 0 located directly adjacent to polishing pond and Juniper Well Identification Number Well #2 Well Depth 18.0 Ft. Creek Well Diameter 2 inches Sample (Screened) Interval 13.OFt. To 18.0 Ft. Depth to Water Level 1.6 It. below measuring point. (before sampling) Measuring point is 2 feet above land surface Non -Discharge NPDES NCO060747 Water Use Injection Well Well Construction Other. Monitoring Wells Gallons of water pumped bailed before sampling 2 gals. Field Analysis: pH 5.27 Specific Conductance N/A uMhos Temp. 17 ° C Odor none Appearance rzlear Date Sample Collected 6-5-86 Date Lab Sample Analyzed 6/17/86 (completed) Laboratory Name Enright Laboratories, Inc. Certification No. 66 COD Coliform: MF Fecal _ Coliform: MF Total Dissolved Solids: Total PH (when analyzed) TOC Chloride Arsenic Grease and Oils Hardness: Total Phenol 20 - mg/1 NO2 as N /100ml NO3 as N /100ml Phosphorus: Total as P mg/I units mg/I mg/I mg/I mg/I mg/I mg/I Al Aluminum_ Ba Barium Ca Calcium _ Cd Cadmium _ Chromium: Total mg/I Ni - Nickel mg/I mg/I mg/I mg/I ma/I Pb - Lead mg/1 mg/I Zn - Zinc 0.03 mg/I Pesticides/Herbicides (Specify Compounds) ug/1 ug/I g/I g/I Other (Specify) Cu - Copper 0.017 mg/I Fe - Iron mg/I Hg - Mercury A Sulfate 28 mg/I K - Potassium mg/I Specific Conductance no uMhos Mg - Magnesium Total Ammonia(NH3 t NH 4) mg/I Mn - Manganese_ TKN as N mg/I Na - Sodium_ I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE. SIGNATURE OF PERMITTEE 4OR AUTHORIZED AGENT*) GW-59 Revised 7/85 rl DATE ug/I ug/I ug/I ug/I - Note: mg/I Values should reflect total concentrations * See back for instructions ** Submit blue and green copies to address above. COMPLIANCE MONITORING REPORT FORM Environmental Management Division Groundwater Section P.O. Box 27687 Raleigh,N.C. 27611 (919)733-5083 Facility Name Morganite Incorporated County Harnett Address One Morganite Drive Permit Number: NC0060747 Dunn, NC 28334 Non -Discharge Well Location W-1 - located on berm between settling prod and polishing pond NPDES W0060747 Well Identification Number Well #1 Well Depth 20.0 Ft. Water Use Well Diameter 2 inches Sample (Screened) Interval 15.0 Ft. To 20.0 Ft. Injection Well Depth to Water Level 5.3 ft. below measuring point. (before sampling) Well Construction Measuring point is 3 feet above land surface Other . Monitoring Wells Gallons of water pumped bailed before sampling 2 gals. Field Analysis: pH 7.01 Specific Conductance N/A uMhos Temp. 17 o C Odor none Appearance cl ay Date Sample Collected 6/5/86 Date Lab Sample Analyzed 6/17/86 (completed) Laboratory Name Enright Laboratories I Certification No. 66 COD 4 mg/I NO2 as. N mg/I Ni Nickel mg/I Coliform: MF Fecal /100ml NO as N mg/I Pb Lead mg/1 Coliform: MF Total Dissolved Solids: Total pH (when analyzed) — TOC Chloride Arsenic Grease and Oils Hardness: Total Phenol /100ml Phosphorus: Total as P 68 mg/I units 3 mg/I 16 mg/I mg/f mg/I mg/I mg/I Sulfate 24 mg/I Specific Conductance 100 uMhos Al - Aluminum mg/I Zn - Zinc 0.06 mg/I mg/I Pesticides/Herbicides (Specify Compounds) Ba - Barium mg/I ug/I Ca - Calcium mg/I ug/I Cd - Cadmium mg/I ug/I Chromium: Total mg/I Other (Specify) ug/I Cu - Copper 0.018 mg/I ug/I Fe - Iron mg/I ug/I Hg - Mercury mg/I ug/I K - Potassium mg/I ug/I Mg - Magnesium mg/I ug/I Total Ammonia(NH3 t NH 4) mg/I Mn - Manganese mg/I TKN as N mg/I Na - Sodium mg/I I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE. l k SIGNAj E OF PERMITTEE (69_,AUTHORIZED AGENT*) DATE GW-59 Revised 7/85 Note: Values should reflect total concentrations • See back for instructions Submit blue and green copies to address above. Environmental Management Division AD� COMPLIANCE MONITORING Groundwater Section REPORT FORM P.O. Box 27687 Raleigh,N.C. 27611 MAY 21 1988 (919)733-5083 Facility Name Morganite Incorporated County Harnett MENT Address One Morganite Drive Permit Number: NCOOF =�€6FFICE— Dunn, N.C. 28334 Non -Discharge Well Location W-2=located directly adjacent to polishing pond and Juniper NPDES 14C0060747 Well Identification Number Well #2 Well Depth 18.0 Ft Creek Water Use Well Diameter 2 inches Sample (Screened) Interval 13.0 Ft. To 18.0 Ft. Injection Well Depth to Water Level 1.33 ft. below measuring point. (before sampling) Well Construction Measuring point is 2 feet above land surface Other monitoring well Gallons of water pumped bailed before sampling 2 gal. Field Analysis: pH 5.65 Specific Conductance _NIA uMhos Temp. 14 o C Odor none Appearance clear Date Sample Collected 3-27-86 Date Lab Sample Analyzed 4-18-86 (completed) Laboratory Name Enwright Laboratories, Inc. Certification No. 66 COD 20 mg/I NO2 as N mg/I Ni Nickel mg/I Coliform: MF Fecal /100ml NO3 as N mg/I Pb Lead mg/1 Coliform: MF Total /100m1 Phosphorus: Total as P mg/I Zn Zinc 0.01 mg/I Dissolved Solids: Total 64 mg/I AI - Aluminum mg/I Pesticides/Herbicides (Specify Compounds) PH (when analyzed) units Ba - Barium mg/I ug/I TOC 4C 5 mg/I Ca - Calcium mg/I ug/I Chloride 8 mg/I Cd - Cadmium mg/I ug/I Arsenic mg/1 Chromium: Total mg/I Other (Specify) ug/I Grease and Oils mg/I Cu - Copper 0.034 mg/I dg/I Hardness: Total mg/I Fe - Iron mg/I ug/I Phenol mg/I Hg - Mercury mg/I ug/I Sulfate 6 mg/I K - Potassium mg/I ug/I Specific Conductance 51 uMhos Mg - Magnesium mg/I ug/I Total Ammonia(NH3 t NH 4) mg/I Mn - Manganese mg/I Note:. TKN as N mg/I Na - Sodium mg/I Values should reflect total concentrations IC IFY HAT THIS REP IS TRUE AND ACCURATE. J� See back for instructions *DAE **Submit blue and green copies to address above. NATURE OF PERMITTEE C AUTHORIZED AGENT*) 7� GW-5 ' evised 7/85 Environmental Management Division COMPLIANCE MONITORING Groundwater Section° ' REPORT FORM P.O. Box 27687 MAY 21 1986 Raleigh,N.C. 27811 Facility Name Morganite Incorporated (919)733-5083 County ENV. MANAGEMENT Address One Morganite Drive Permit Number: NC00 o 1CViLLIG. OFFICE Dunn NC 28334 Non -Discharge Well Location W-1=1ocated on berm between aP+ti;ng pond and polishing pond NPDES NCO060747 Well Identification Number Well #1 Well Depth 20.0 Ft. Water Use Well Diameter 2 inches Sample (Screened) Interval 15.0 Ft. To 20.0 Ft. Injection Well Depth to Water Level 4.75 ft. below measuring point. (before sampling) Well Construction Measuring point is 3 feet above land surface Other. Monitoring wells Gallons of water pumped bailed before sampling 2 gals. Field Analysis: pH 5.91 Specific Conductance N A uMhos Temp. 13 oC Odor none Appearance clear Date Sample Collected 3-27-86 Date Lab Sample Analyzed 4-18-86 (completed) Laboratory Name Enwright Laboratories Certification No. 66 COD 4 mg/I NO2 as N mg/I Ni - Nickel mg/I Coliform: MF Fecal /100mi NO3 as N mg/I Pb -Lead mg/1 Coliform: MF Total /100ml Phosphorus: Total as P mg/I Zn - Zinc 0.01 mg/1 Dissolved Solids: Total 100 mg/I Al Aluminum mg/I Pesticides/Herbicides (Specify Compounds) pH (when analyzed) units Ba Barium mg/I ug/I TOC 7 mg/I Ca Calcium mg/I ug/I Chloride 15 mg/I Cd Cadmium mg/I ug/I Arsenic mg/1 Chromium: Total mg/I Other (Specify) ug/I Grease and Oils mg/I Cu - Copper 0.011 mg/1 ug/l Hardness: Total mg/I Fe - Iron mg/I ug/I Phenol mg/I Hg - Mercury mg/1 ug/I Sulfate 17 mg/I K - Potassium mg/I ug/I Specific Conductance 100 uMhos Mg - Magnesium mg/I ug/I Total Ammonia(NH3 t NH 4) mg/l Mn - Manganese mg/I Note: TKN as N mg/I Na - Sodium mg/I Values should reflect total concentrations r 71,71X, AT THIS POR U CCURATE. �—�14� • See back for instructions iR #Submit blue and green copies to address above. NATURE OF PERMITTEE (OR,/AUTHORIZED AGENT*) evised 7/85