WQ0040918_Monitoring (Report)_20231221

Monitoring Report Submittal
Permit Number#*
Name of Facility:*
Month: * November
Report Information
Type *
GW-59
WQ0040918
Ag Protein Trailer Wash
Year:* 2023
Upload Document*
Ag Protein MW 11-9-23.pdf
PDF Only
1.86MB
Please upload one PDF containing all applicable monitoring reports
(i.e., NDMR, NDAR-1, NDAR-2, NDMLR, GW-59).
Confirmation Email Address: * [e-mail]
Name of Submitter: * Amy Elmore
Signature:
��IIYf �IiIYO�G
Date of submittal: 12/21/2023
This will be filled in automatically
Initial Review
Reviewer: Wanda.Gerald

Is the project number correct?* W00040918
Is the monitoring report accepted?* Yes NO
Regional Office* Wilmington
Reviewer: _anonymous
Review Date: 1/5/2024

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GW-59A COMPLIANCE REPORT FORM Permit # WQ0040918
(Submit one each monitoring period with GW-59 forms.)
1 Enter date monitoring results were due. ( eC Will this monitoring report (GW-59 and GW-59A)
--[W-S
be submitted after the established due date?
2
3
Was any required information missing on the GW-59 report forms?
iF the answer to question I or 2 is "YES", list in the space provided below the well identification number(s) and
explain the problems encountered in obtaining the required information.
Are any of the monitor wells in need of repair or maintenance (damaged casing, unlocked or missing cap, missing
identification plate, area overgrown, etc.)? If the answer is "Yes", contact the Regional Officefor guidance.
YES
YES
14 I Are any monitored constituents equal to or above the established standards? I1YES1I NO
5
6
If the answer to question 4 is "NO", skip to section 8.
If the answer to question 4 is "YES" list the affected wells individually with constituent(s) and concentration(s)
exceeding standards in the space provided below.
MW-1 pH 5.6 units MW-2 pH 3.78 est units, N 19.9 mg/L
MW-3 pH 4.8 units, TOC 30.2 mg/L MW-4 pH 5.2 units
For the constituents identified in question 4 above, have standards been exceeded previously for the
same constituent(s) in the same well(s) in the last two years?
If the answer to question 5 is "NO", skip to section 8.
if the answer to question 5 is "YES", list in the space provided below, each well with constituents) exceeding
standards, concentration(s) reported, and sample collection date for each occurrence (for the last two years).
MW-1 pH 5.6 units 11-9-23 4.6 11-3-22 3.96 11-4-21
5.8 7-7-23 4.6 7-7-22 (See attached page)
4.8 3-6-23 4.3 3-14-22
Are the monitoring wells listed in section 5 located at or beyond the review boundary?
If the answer is "YES", a groundwater quality problem may be occurring. CONTACT THE REGIONAL
OFFICE IMMEDIATELY FOR GUIDANCE. if the answer is "NO", monitoring wells may be improperly
located; contact the Regional Office.
YES11 NO
"Is the permittee implementing previously approved actions required by the Division involving this I YES
groundwater quality problem?
8
If the answer to question 7 is "YES", describe those actions in the space provided below.
If the answer to question 7 is "NO" contact the Regional Office within 90 days: an evaluation may be
required to determine the impact the waste disposal s stem is havinq at the review and compliance
boundaries surrounding this facility. Failure to do so may subiect the permittee to a Notice of Violation.
fines, and/or penalties.
pH is below the standard.
Conducting exploratory surface water monitoring to help determine sources.
MW-3 TOC is naturally occurring- (No previous action items requited)-.
The person completing this portion (GW-59A) of the monitoring report should sign below and submit this
form with GW-59 forms for required wells to the address provided at the top of the current GW-59 form.
I hereby acknowledge that the above information was evaluated and the information submitted in this
,report (Compliance Report GW-59A) is true and complete to the best of my knowledge.
/Z ` 12/21 /2023
Signa r of ermitte (or Authorized Agent) Date
NO
GW-59A 12/8/2003

Continued
5. MW-2 pH 3.78 est units 11-9-23
4.2 units
7-7-23
4.4
3-6-23
3.96
11-3-22
4.4
7-7-22
4.4
3-14-22
4.4
11-4-21
MW-3 pH 4.8 units 11-9-23
4.4
7-7-23
5.4
3-6-23
4.5
11-3-22
5.1
7-7-22
5.2
3-14-22
5.4
11-4-21
MW-4 pH 5.2 units 11-9-23
6.4
3-6-23
5.2
11-3-22
5.9
7-7-22
5.6
3-14-22
5.2
7-16-21
MW-2 N 19.9 mg/L 11-9-23
19.2
7-7-23
18.3
3-6-23
16.6
11-3-22
15.3
7-7-22
14
3-14-22
10.9
7-16-21
MW-3 TOC 30.2 mg/L 11-9-23
24
3-6-23
17.3
11-3-22
19.8
7-7-22
20
3-14-22
39.5
11-4-21

pp"7 _7�1 Environmental Chemists, Inc.
envirochem 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab " 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 '° 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS infoCt*environmentalchemists.com
Smithfield Hog Productions -Warsaw Date of Report: Dec 21, 2023
Post Office Box 856 Customer PO #:
Warsaw NC 28398 Customer ID: 08110011
Attention: Report #: 2023-26342
Project ID: AG Protein MW
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
23-63750 Site: MW-1 11/9/2023 12:10 PM Water JCB/Envirochem
Test
Method
Color
cow
Depth to water, ft.
Depth to Water, Ft
Ammonia Nitrogen
EPA3W.1, Rev.2o, IM
Gallons bailed before sampling
Ganes Bared before sampling
Odor
Quay
Total Dissolved Solids (TDS)
SM 264O c-2015
Temperature
SM 25N B-2010
pH
SM 4600 H B-2011
Total Phosphorus
SM 4600 P (F-M-2011
Total Organic Carbon (TOC)
SM 6310 B-2014
Fecal Conform
SM =2 D-2D15 MIF
Chloride
SM4500 Cl E-2011
1,1,1,2-Tetrachloroethane
SW 846 Method 8260DIS030B
1, 1. 1 -Trichloroethane
sw 8" Method 826013/50308
1,1,2,2-Tetrachloroethane
SW ea6 Method 62600/50308
1,1,2-Trichloroethane
SW W Method e28W=308
1,1-Dichloroethane
SW 846 Method 8260D/503013
1,1-Dichloroethene
SW 848 Method 8260DIS030B
1, i-Dichloropropene
SW 846 Method 6260D=30B
1,2,3-Trichlorobenzene
SW 846 Method 8260DW30B
1,2,3-Trichloropropane
SW 846 Method UWD15030B
1,2,4-Trichlorobenzene
SW 846 Methood 8260D/50305
1,2,4-Tdmethylbenzene
SW MS Metood MOD/503013
1,2-Dibromo-3-Chloropropane
SW 646 Method 6280D/50348
1,2-Dibromoethane
SW 846 Method 8280D/60308
1,2-Dichlorobenzene.
SW 848 MlethW 8260D/50308
Results Date Analyzed
Tan/Turbid
11/09/2023
9.0 feet
11/09/2023
< 0.2 mg/L
11/17/2023
5.0gallons
11/09/2023
None
11 /09/2023
58 mg/L
11 /10/2023
24.9 C
11/09/2023
5.6units
11/09/2023
2.20mg/L
11/15/2023
3.4 mg/L
11/10/2023
<1 Colonies/100ml-
11/09/2023
< 5 mg/L
11/17/2023
<0.5 pg/L
11/16/2023
<0.5 pg/L
11/16/2023
<0.5 pg/L
11/16/2023
<0.5 pg/L
11 /16/2023
<0.5 pg/L
11/16/2023
<0.5 pg/L
11/16/2023
<0.5 i,lg/L
11/16/2023
<0.5 ug/L
11/16/2023
<0.5 pg/L
11/16/2023
<0.5 pg/L
11/16/2023
<0.5 pg/L
11/16/2023
<1 pg/L
11 /16/2023
<0.5 pg/L
11/16/2023
�0.5 ug/L
11/16/2023,
Rgxxt A.: 2023-26342 Page 1 of 12

r77_747 Environmental Chemists, Inc.
envirochem 6602 Windmill Way, Wilmington, NC 28405 � 910.392.0223 Lab •, 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 m 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 " 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS info eeenvironmentalchemists com
Smithfield Hog Productions - Warsaw
Date of Report: Dec 21, 2023
Post Office Box 856
Customer PO #:
Warsaw NC
28398
Customer ID: 08110011
Attention:
Report #: 2023-26342
Project ID: AG Protein MW
1,2-Dichloroethane
SW a4e Method 6260 M30B
<0.5 pg/L
11/16/2023
1,2-Dichloropropane
Swage Method Sn=5030B
<0.5 pg/L
11/16/2023
1,3,5-Tdmethylbenzene
Swage Method 828=5=8
<0.5 pg/L
11/16/2023
1,3-Dichlorobenzene
SW 80 Method 62NDW308
<0.5 pg/L
11/16/2023
1,3-Dichloropropane
Sw aas Method 8ZWD15030B
<0.5 pg/L
11/16/2023
1,4-Dichlorobenzene
SW 845 Method 8=D150308
<0.5 pg/L
11/16/2023
2,2-Dichloropropane
SW 046 Method 8M0DffiW08
<0.5 pg/L
1111 M023
2-Chlorotoluene
SW 846 Method e2a°D15030
<0.5 pg/L
11/16/2023
4-Chlorotoluene
SW No Method 8280W50306
<0.5 pg/L
11/16/2023
Benzene
SW 848 mod 9260DMOM
<0.5 pg/L
11/16/2023
Bromobenzene
Sw 848 Method 825=50sos
<0.5 pg/L
11/16/2023
Bromochloromethane
SW 8" Method 826ODFAMB
<0.5 pg/L
11/16/2023
Bromodichloromethane
SW848Method 82M5030B
<0.5 pg/L
11/16/2023
Bromoform
SW U6 Method &MDW30B
<0.5 pg/L
11/16/2023
Bromomethane
Sw 84e Method 8260D15030B
<D.5 pg/L
11/16/2023
Carbon tetrachloride
sw 84e Method a260D/SWOB
<0.5 pg/L
11/16/2023
Chlorobenzene
SW 80 Method OMD/5030B
<0.5 pg/L
11/16/2023
Chloroethane
SW 84a Method $ MOD16MB
<0.5 pg/L
11/16/2023
Chloroform
SW Sae Method a2e01 MMM
<0.5 pg/L
11/16/2023
Chloromethane
Sw m6 Method 8250D150308
<0.5 pg/L
11/16/2023
cis-1,2-Dichloroethene
SW 8" Method 82BODUMB
<0.5 pg/L
11/16/2023
cis-1,3-Dichloropropene
Sw 84e Method 826OM30B
<0.5 pg/L
11/16/2023
Dibromochloromethane
Sw U6 Method SMDM30B
<0.5 pg/L
11/16/2023
Dibromomethane
Sw a48 Method 62ND15030B
<0.5 pg/L
11/16/2023
Dichlorodifluoromethane
Sw a" Method 82eoD1503011
<0.5 pg/L
11/16/2023
Ethylbenzene
Sw 846 Method 8260D1503M
<0.5 pg/L
11/16/2023
Hexachlorobutadiene
SW W Method 8280D/50308
<0.5 pg/L
11/16/2023
Isopropylbenzene
SW 80 Method S260D/50308
<0.5 pg/L
11/16/2023
M+P Xylene
Sw so Method 826OW0306
<1.0 pg/L
11/16/2023
`-- `Methylenechlortde
Sr^'Ba Method 82NDfiMM
11716/2023
Report k.; 2023.2e342
Page 2 of 12

ro"'W7­7441 Environmental Chemists, Inc,
envirochem 6602 Windmill Way, Wilmington, NC 28405 & 910.392,0223 Lab c 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 a 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS [e-mail]
Smithfield Hog Productions - Warsaw
Date of Report: Dec 21, 2023
Post Office Box 856
Customer PO #:
Warsaw NC
28398
Customer ID: 08110011
Attention:
Report #. 2023-26342
Project ID: AG Protein MW
Naphthalene
SW 80 Method 826MW30B
<0.5 pg/L
11/16/2023
n-Butylbenzene
SW 84e Method 82800/5o30B
<0.5 pg/L
11/16/2023
n-Propylbenzene
SW tnte Method 826MSOWB
<0.5 pg/L
11/16/2023
ortho-Xylene
SW 846 mod SMD=308
<0.5 pg/L
11/16/2023
p-Isopropyltoluene
SW 840 Method 8280D/50308
<0.5 pg/L
11/16/2023
sec-Butylbenzene
SW 846 Method 62WOU308
<0.5 pg/L
11/16/2023
Styrene
SW 846 Method #s600=08
<0.5 pg/L
11/16/2023
tert-Butylbenzene
SW 846 Memod 825010MMS
<0.5 pg/L
11/16/2023
Tetrachloroethene
SW 846 Method 8280t)/50308
<0.5 pg/L
11/16/2023
Toluene
SW 846 Method 82ND/50308
<0.5 pg/L
11/16/2023
Trans-1 ,2-Dichloroethene
sw 546 Memod e25DD/5030B
<0.5 pg/L
11116/2023
Trans-1 ,3-dichlompropene
sw 848 Method 8MDMO308
<0.5 pg/L
11/16/2023
Trichloroethene
SW 846 Method 8280D/5030B
<0.5 pg1L
11/16/2023
Tdchlorofluoromethane
SW 8" Method 8280D/5030B
<0.5 pg/L
11/16/2023
Vinyl chloride
SW 80 Memos 8280D/5030B
<0.5 pg/L
11/16/2023
Nitrate Nitrogen {Calc)
Nitrite Nitrogen EPA353.2, Rev.2.D, I < 0.02 mg/L 11/10/2023
Nitrate+Nitrite-Nitrogen EPA 353.2, Rev, 2.o,1993 1.80 mg/L 11/14/2023
Nitrate Nitrogen Subtractm Method 1.81 mg/L 11/14/2023
Report *. 2023.28342 - - Page 3 of 12

Environmental Chemists, Inc.
envirochem 6602 Windmill Way, Wilmington, NC 28405 � 910.392.0223 Lab `910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 11 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 `j 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS info aGenvironmentalchemistscom
Smithfield Hog Productions - Warsaw Date of Report: Dec 21, 2023
Post Office Box 856 Customer PO #:
Warsaw NC 28398 Customer ID: 08110011
Attention: Report #: 2023-26342
Project ID: AG Protein MW
Lab ID Sample ID: Collect DatelTime Matrix Sampled by
23-63753 Site: MW-2 11/912023 1225 PM Water JCB/Envirochem
Test Method Results Date Analyzed
Color
color
White/Turbic
11/09/2023
Depth to water, ft.
Depth to water. Ft
13.2 feet
11/09/2023
Ammonia Nitrogen
EPA 350.1, Rev. 2.0,1993
< 0.2 mg/L
11/17/2023
Gallons bailed before sampling
Gallons Bailed beloresampling
5.Ogallons
11/09/2023
Odor
Quartanve
None
11/09/2023
Total Dissolved Solids (TDS)
SM 2540 c-2015
145 mg/L
11/10/2023
Temperature
SM 2550 B-2010
21.9 C
11/09/2023
pH
SM 45M H B-2011
3.78est units
11/09/2023
Estimated, below calabration range.
Total Phosphorus
SM 4500 P (F-1-1}-2011
0.10 mg/L
11 /15/2023
Total Organic Carbon (TOC)
SM 5310 8.2014
1.0 mg/L
11 /10/2023
Fecal Coliform
SMSM2D-2015MF
<1 Colonies/100ml-
11/09/2023
Chloride
SM45M Cl E-2011
7 mg/L
11/17/2023
1, 1, 1,2-Tetrachloroethane
SW 846 Method 826OD15MB
<0.5 µg/L
11/1612023
1,11-Trichloroethane
SW80Method a26otN5030B
<0.5µg/L
11/16/2023
1,1,2,2-Tetrachloroethane
SW 846 Method 826=0308
<0.5µg/L
11/1612023
1,1,2-Trichloroethane
sw 80 Method 8260DMO300
<0.5 µg/L
11/16/2023
1,1-Dichloroethane
swa4aMethod 8260o150308
<0.5µg/L
11/16/2023
1,1-Dichloroethene
SW 846 Method 826ODF5030
<0.5 µg/L
11/16/2023
1,1-Dichloropropene
SW 848 Method 62NM0308
<0.5 µg/L
11 /16/2023
1,2,3-Trichlorobenzene
SW 846 Method OMDr50308
<0.5 µg/L
11/16/2023
1,2,3-Trichloropropane
SW WMethod a2s0D150308
<0.5 µg/L
11/16/2023
1,2,4 Trichlorobenzene
SW 846 Method 826013=308
<0.5 µg/L
11/1612023
1,2,4-Trimethylbenzene
sw ads Method e260D/50308
<0.5 µg/L
11/16/2023
1,2-Dibromo-3-Chloropropane
SW 046 Method e2601)/50308
<1 µg/L
11116/2023
1,2-Dibromoethane
sw 546 Method 828OWSMOB
<0.5 pg/L
11/16/2023
Report C 2023.26342 Page 4 of 12

Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 29405 b 910.392.0223 Lab * 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
' 255-A Wilmington Highway, Jacksonville, NC 28540 r 910.347.5843 Lab/Fax
ANALYTICAL $ CONSULTING CHEMISTS [e-mail]
Smithfield Hog Productions - Warsaw
Date of Report: Dec 21, 2023
Post Office Box 856
Customer PO #:
Warsaw NC
28398
Customer ID: 08110011
Attention:
Report #: 2023-26342
Project ID: AG Protein MW
1,2-Dichlorobenzene
SW 848 Method 8260D/50308
<0.5 pg/L
11/16/2023
1,2-Dichloroethane
SW 846 Method 82600/WWB
<0.5 pg/L
11/16/2023
1,2-Dichloropropane
SW 846 Method 8260DW30B
<0.5 pg/L
11/16/2023
1,3,5-Trimethylbenzene
SW Bad Method 026OD150308
<0.5 pg/L
11/16/2023
1,3-Dichlorobenzene
sw sad Method 8260DW50308
<0.5 pg/L
11 /1612023
1,3-Dichloropropane
sw 846 Method 82BODl5030B
<0.5 pg/L
11/1612023
1,4-Dichlorobenzene
SW 846 Method 828=60 0B
<0,5 pg/L
11/16/2023
2,2-Dichloropropane
SW 846 Method 826ODM308
<0.5 pg/L
11/16/2023
2-Chlorotoluene
SW 846 Method 826=5030B
<0,5 pg/L
11/16/2023
4-Chlorotoluene
SW 846 Method 82WDf503ae
<0.5 pg/L
11/16/2023
Benzene
SW sad Method 8280w5030s
<0.5 pg/L
11/16/2023
Bromobenzene
SW 846 Method e2500►50306
<0.5 pg/L
11/16/2023
Bromochloromethane
SW 846 Method 8260D150306
<0.6 pg/L
11/16/2023
Bromodichloromethane
SW e46 Method 826oDMMOB
<0.5 pg/L
11 /16/2023
Bromoform
SW 846 Method 8260D/5030B
<0.5 pg/L
11/16/2023
Bromomethane
SW 84s Method 82600/5030e
<0.5 pg/L
11/16/2023
Carbon tetrachloride
SW 846 Method 82SOM0308
<0.5 pg/L
11/16/2023
Chlorobenzene
SW 846 Method 826OW5030B
<0.5 pg/L
11/16/2023
Chloroethane
SW 846 Method 8260DI50308
<0.5 pgfL
11 /16/2023
Chloroform
SW ea Method 82MM503013
<0.5 pg/L
11/16/2023
Chloromethane
SW 848 Method 8250DISMB
<0,5 pg/L
11/16/2023
cis-1,2-Dichloroethene
SW 848 Method 8260D/50306
<0.5 pg/L
11/16/2023
cis-1,3-Dichloropropene
SW846Method a26aDh5030s
<0.5pg/L
11/16/2023
Dibromochloromethane
SW W Method 8260DMWOB
<0.5 pg/L
11/16/2023
Dibromomethane
SW 80 Method 826=5030B
<0.5 pg/L
11/16/2023
Dichlorodi8uoromethane
SW 646 Method 8260MO308
<Q.5 pg/L
11/16/2023
Ethylbenzene
SW 84B Medved 8260DIS030B
<0.5 pg/L
11/16/2023
Hexachlombutadiene
SW "S Method e2800r5030e
<0.5 pg/L
11/16/2023
Isopropylbenzene
SW 846 Method 026ODM30B
<0.6 pg/L
11/16/2023
M+P_ Xylene ,
sw 846 Method e28ax50308
__.. <1:O �g/L
11/16/2023
Report *. 2023.26342
Page45 0112

"q"l
F"Wow --
Environmental Chemists,
Inc.
'
6602 Windmill Way,
Wilmington, NC 28405 0 910.392.0223 Lab . 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 m 2-52.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS
info@..environmentalchemists.com
Smithfield Hog Productions - Warsaw
Date of Report: Dec 21, 2023
Post Office Box 856
Customer PO 0:
Warsaw NC 28398
Customer ID: 08110011
Attention:
Report #: 2023-26342
Project ID: AG Protein MW
Methylene chloride
SW 646 MOW OMD15030B
<0.5 pg/L
11/16/2023
Naphthalene
SW 80 Men,od U50 16030s
<0.5 pg/L
11/16/2023
n-Butylbenzene
sw W ^mod M0M0UB
<0.5 pg/L
11/16/2023
n-Propylbenzene
SW 846 Method 82WDMD308
<0.5 pg/L
11/16/2023
ortho-Xylene
SW 646 Method 6280Dr5030B
<0.5 pg/L
11/16/2023
p-Isopropyholuene
SW 846 Method 8280Dt5030B
<0.5 pg/L
11/16/2023
Sec-Butylbenzene
SW 046 Method 6260Dl5030B
<0.5 pg/L
11/16/2023
Styrene
SW N6 Method OMD150308
<0.5 pg/L
11/16/2023
tert-Butylbenzene
SW 846 Method 828=50306
<0.5 pg/L
11/16/2023
Tetrachloroethene
SW 846 Method 82BODMO308
<0.5 pg/L
11/16/2023
Toluene
SW 846 Method $26013=08
<0.5 pg/L
11/16/2023
Trans-1,2-Dichloroethene
SW 846 Method 6260Dr5030B
<0.5 pg/L
11/16/2023
Trans-1,3-dichloropropene
SW 840 Method 8260Dr5030B
<0.5 pg/L
11/16/2023
Trlchloroethene
SW 848 McMW 826011/503013
<0.5 pg/L
11/16/2023
Trichlorofluoromethane
SW 846 Method 6260D1503013
<0.5 pg/L
11/16/2023
Vinyl chloride
SW 646 Megmd 8260Dr5030B
<0,5 pg/L
11/16/2023
Nitrate Nitrogen (Calc)
Nitrite Nitrogen
EPA 353,2. Rev. 2-0, IM
< 0.02 mg/L
11 /10/2023
Nitrate+Nitrite-Nitrogen
EPA 3532, Rev, 2,0,1M
19.9 mg/L
11/14/2023
Nitrate Nitrogen
Stmraction Method
19.9 mg/L
11 /14/2023
Report 1k: 2023.28342 Page 6 of 12

Environmental Chemists, Inc.
• 6602 Windmill Way, Wilmington, NC 28405 , 910.392.0223 Lab u- 910.392A424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
' 255-A Wilmington Highway, Jacksonville, NC 28540 � 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS info(u�environmentalchemists com
Smithfield Hog Productions - Warsaw
Post Office Box 856
Warsaw NC 28398
Attention:
Lab ID Sample ID:
23-63754 Site: MW-3
Test
Color
Depth to water, ft.
Ammonia Nitrogen
Gallons bailed before sampling
Odor
Total Dissolved Solids (TDS)
Temperature
pH
Total Phosphorus
Total Organic Carbon (TOC)
Fecal Coliform
Chloride
1,1,1,2-Tetrachloroethane
1,1,1-Trichloroethane
1,1,2,2-Tetrachloroethane
1,1,2-Trichloroethene
1,1-Dichloroethane
1, 1 -Dichloroethene
1,1-Dichloropropene
1, 2,3-Tdchlorobenzene
1, 2,3-Tdchloropropane
1,2,4-Trichlorobenzene
1,2,4-Trimethylbenzene
1, 2-D i bromo-3-Chloropropane
1,2-Dibromoethane
1,2-Dichiorobenzene
Report 1F:: 2023-28342 — —
Date of Report: Dec 21, 2023
Customer PO #:
Customer ID: 08110011
Report #: 2023-26342
Project ID: AG Protein MW
Collect Date/Time Matrix Sampled by
11/9/2023 12:45 PM Water JCB/Envirochem
Method Results Date Analyzed
Color
Tan/Brown
11/09/2023
Depth to water, Ft.
8.2 feet
11 /09/2023
EPA 350.1, Rev. 2.0, 1993
< 0.2 mg/L
11/17/2023
Gallons Bailed before sampling
5.0 gallons
11109/2023
oualitative
None
11/09/2023
SM 2540 c-2015
94 mg/L
11 /10/2023
SM 2550 B-2010
22.4 C
11 /09/2023
SM 4500 H e-2011
4.8 units
11/09/2023
SM 4500 P (F-H)-2011
1.28 mg/L
11/15/2023
SM 5310 B-2014
30.2 mg/L
11/10/2023
SM 9222 D-201S MF
<1 Colonies/100mL
11/09/2023
SM450 Cl E-2011
< 5 mg/L
11/17/2023
SW 846 Method 8260015030B
<0.5 pg/L
11/16/2023
SW 846 Method 8260131MOB
<0.5 pg/L
11/16/2023
SW 846 Method 62e0D=OB
<0.5 pg/L
11/16/2023
SW 846 Method 825013/50306
<0.5 pg/L
11 /16/2023
SW 846 Method 826013/503013
<4.5 pg/L
11/16/2023
SW 646 Method 626oD/50306
<0.5 pg/L
11/16/2023
sw ea Method 826ODV50308
<0,5 pg/L
11/16/2023
SW 646 Method 82600150308
<0.5 pg/L
11/16/2023
SW 846 Method 8260DWMB
<0.5 pg/L
11/16/2023
sw 846 Method 82BOD15MB
<0.5 pg/L
11/16/2023
SW 846 Method VOODI5030B
<0.5 pg/L
11/16/2023
SW 846 Method 62600150M
<1 pg/L
11/16/2023
SW 846 Method WOODIMOB
<0.5 pg/L
11 /16/2023
SW 846 Method 826oD/MOB
<0.5 pg/L
11/16/2023
— — — —.
_ -- Page 7 of 12

F"'W- —. Environmental Chemists, Inc.
envirochem 6602 Windmill Way, Wilmington, NC 28405 ', 910.392.0223 Lab t' 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 0 252.473.5702 Lab/Fax
- 255-A Wilmington Highway, Jacksonville, NC 28540 3 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS info4ienvironmentalchemists com
Smithfield Hog Productions - Warsaw
Post Office Box 856
Warsaw NC 28398
Attention:
Date of Report: Dec 21, 2023
Customer PO #:
Customer ID: 08110011
Report #: 2023-26342
Project ID: AG Protein MW
1,2-Dichlomethane
SW 646 Method 82BOOM30B
<0.5 pg/L
11/16/2023
1,2-Dichloropropane
SW 646 Method 828MW30B
<0.5 pg/L
11 /16/2023
1, 3, 5-Trimethyl benzene
SW 846 Method 8260[nO"B
<0.5 pglL
11/16/2023
1, 3-Dichlorobenzene
SW US Method 8MODW308
<0.5 pg/L
11/16/2023
1, 3-Dichloropropane
SW 84S Method 8280D=308
<0.5 pg/L
11 /16/2023
1,4-Dichlorobenzene
SW 846 Method 82600150308
<0.5 pg/L
11/16/2023
2,2-Dichloropropane
SW 846 Method 8260D=30B
<0.5 pg/L
11/16/2023
2-Chlorotoluene
SW 848 Method 8268D15030B
<0.5 pg/L
11/16/2023
4-Chlorotoluene
SW 846 Method 82800MMB
<0.5 pg/L
11/16/2023
Benzene
SW $46 Method 82WW0308
<0.5 pg/L
11/16/2023
Bromobenzene
SW 846 Method 626 W030E
<0.5 pg/L
11/16/2023
Bromochloromethane
SW 846 Method 8260D15o30B
<0.5 pg/L
11/16/2023
Bromodichloromethane
SW 80 Method 8260DMMB
<0.5 pg/L
11/16/2023
Bromoform
SW 846 Method 82NDIMOB
<0.5 pg/L
11/16/2023
Bromomethane
sw 8" Method 8260D/50M
<0.5 pg/L
1111612023
Carbon tetrachloride
SW 846 Method 82MY5030B
<0.5 pg/L
11/16/2023
Chlorobenzene
SW 846 Method 8260DG030B
<0.5 pg/L
11/16/2023
Chloroethane
SW 646 Method 8260D15030B
<0.5 pg/L
11/16/2023
Chloroform
SW 846 Method 6260D/5030B
<0.5 pg/L
11/16/2023
Chloromethane
SW 846 Method 828oD/5030B
<0.5 pg/L
11/1612023
cis-1,2-Dichloroethene
SW$46 Method 8280DW30B
<0.5 pg/L
11/16/2023
cis-1,3-Dichloropropene
SW 846 Method 8260D15=8
<0.5 pg/L
11/16/2023
Dibromochloromethane
SW 848 Method 8260015030E
<0.5 pg/L
11/16/2023
Dibromomethane
SW 848 Method 8260MO30B
<0.5 pg/L
11/16/2023
Dichlorodffluoromethane
SW a46 Method 8260D15030B
<0.5 pg/L
11/16/2023
Ethylbenzene
SW 846 Method 826OM30B
<0.5 pg/L
11/16/2023
Hexachlorobutadiene
SW 646 Method 8260015030E
<0.5 pg/L
11/16/2023
Isopropylbenzene
SW 646 Method 826 D=30E
<0.5 pg/L
11/16/2023
M+P Xylene
SW 646 Method 82600=30B
<1.0 pg/L
11/16/2023
Methylene chkxide : ,
sw 6" Method 8260DW306
56.5.pg/L
- - .1.1/1.t /2023
Report k: 2023-28342
-- — -- — -
Page 8 of 12

.auf:
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 11 910.392.0223 Lab a 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 ' 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 910.347.5843 Lab/Fax
info(tyenvironmentalchemists.com
Smithfield Hog Productions - Warsaw
Date of Report: Dec 21, 2023
Post Office Box 856
Customer PO #:
Warsaw NC
28398
Customer ID: 08110011
Attention:
Report #: 2023-26342
Project ID: AG Protein MW
Naphthalene
SW 646 Method 8280DIW308
<0.5 Ng/L
11/16/2023
n-Butylbenzene
SW 646 Method 8280D/5 M
<0.5 P91L
11/1612023
n-Propylbenzene
SW 646 Method 8260D/S0306
<0.5 pg/L
11/16/2023
ortho-Xylene
SW 846 Method 8260DISMS
<0.5 pg/L
11/16/2023
p-Isopropyltoluene
SW 645 Method e26oD/50308
<0.5 pg/L
11/16/2023
sec-Butylbenzene
SW 846 Method 8260D/50308
<0.5 pg/L
11/16/2023
Styrene
SW 846 Method 8260D/50308
<0.5 pg/L
11/16/2023
tert-Butylbenzens
SW 846 Method 6260DIS030
<0.5 pg/L
11/16/2023
Tetrachloroethene
SW 846 Method 6260D/50aas
<0.5 pg/L
11/16/2023
Toluene
SW 846 Method 6260=013
<0.5 pg/L
11/16/2023
Trans-1,2-Dichloroethene
SW 846 Method 62ND/W308
<0.5 pg/L
11/16/2023
Trans-1,3-dichloropropene
SW 846 Method 6260DIN308
<0.5 pg/L
11/16/2023
Trichloroethene
SW 846 Method 6260D/W30a
<0.5 pg/L
11/16/2023
Tdchlorofluoromethane
SW 646 Method 8280D/W308
<0.5 pg/L
11/16/2023
Vinyl chloride
SW 846 Method 8280D/N308
<0.5 pg/L
11/16/2023
Nitrate Nitrogen (Cale)
Nitrite Nitrogen
EPA353.2, Rev, 2.0.1993
0.06 mg/L
11/1012023
Nitrate+Nitrite-Nitrogen
EPA 353.2. Rev, 2 0, 1993
0.49 mg/L
11/14/2023
Nitrate Nitrogen
Subtradon Method
0.43mg/L
11/14/2023
Report #-_ 2023-26342 Page 9 of 12

Environmental Chemists, Inc.
• 6602 Windmill Way, Wilmington, NC 28405 , 910-392.0223 Lab :, 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 ;, 252-473.5702 Lab/Fax
' 255-A Wilmington Highway, Jacksonville, NC 28W :; 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS info [e-mail]
Smithfield Hog Productions - Warsaw
Date of Report: Dec 21, 2023
Post Office Box 856
Customer PO #:
Warsaw NC 28398
Customer ID: 08110011
Attention:
Report #: 2023-26342
Project ID: AG Protein MW
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
23-63755 Site: MW-4
11/9/2023
1:05 PM Water XB/Envirochem
Test
Method
Results Date Analyzed
Color
Color
Tan
11/09/2023
Depth to water, ft.
Depth to Water, Ft.
1.9 feet
11/09/2023
Ammonia Nitrogen
EPA 350.1. Rev. 2.0,1993
< 0.2 mg/L
11/17/2023
Gallons bailed before sampling
Gallons Bailed before sampling
5.0 gallons
11/09/2023
Odor
auaat"Ve
None
11/09/2023
Total Dissolved Solids (TDS)
SM 2540 C-2015
107 mg/L
11/10/2023
Temperature
SM 2550 B•2010
20.1 C
11/09/2023
pH
SM 4500 H B-2011
5.2 units
11/09/2023
Total Phosphorus
SM 4500 P (F-H).2011
1.27 mg/L
11/15/2023
Total Organic Carbon (TOC)
SM 5310 B-2014
0.6 mg/L
11/10/2023
Fecal Coliform
SM 9222 D-2015 MF
<1 Colonies/100mL
11/09/2023
Chloride
SM4500 CI E-2011
17 mg/L
11 /17/2-023
1,1,1,2-Tetrachloroethane
SW 846 Method 8260D ONO
<0.5 pg/L
11/16/2023
1,1,1-Tdchloroethane
SW 646 Method 826=50308
<0.5 pg/L
11/16/2023
1,1,2,2-Tetrachloroethane
SW 848 Method 8280D15030B
<0.5 pg/L
11/16/2023
1,1,2-Tdchloroethane
SW 848 Method 8250DW30B
<0.5 pg/L
11/16/2023
1,1-Dichloroethane
SW 848 Method 826013=30B
<0.5 pg/L
11/16/2023
1,1-Dichloroethene
SW 848 Method 828013I503013
<0.5 pg/L
11/16/2023
1,1-Dichloropropene
SW 848 Method 8260015030E
<0.5 pg/L
11/16/2023
1,2,3-Tdchlorobenzene
SW 848 Method 82&KM39B
<0.5 pg/L
11/16/2023
1,2,3-Tdchloropropane
SW 848 Method 826OW030B
<0.5 pg/L
11/16/2023
1,2,4-Trichlorobenzene
sws" Method 8260DWMB
<0,5 pg/L
11/16/2023
1, 2,4-Trimethylbenzene
SW 8" Method 828013=30B
<0.5 pg/L
11 / 1612023
1,2-Dibromo-3-Chloropropane
SW 8" Method 8MODfSMB
<1 pg/L
11/16/2023
1,2-Dibromoethane
SW 848 Method82BOD150308
<0.5Vg/L
11/16/2023
1,2-Dichlorobenzene
SW 846 Method 825DEMNS
<0.5 pg/L
11/10/2023
Report M. 2023.26342
� -
--- � Page 10 of 12

Lenvirochem
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 m 910.392.0223 Lab 0 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 0 252.473.5702 Lab%Fax
255-A Wilmington Highway, Jacksonville, NC 28540 1 910.347.5943 Lab/Fax
in fo(rvenvironmentalchemists.com
Smithfield Hog Productions -Warsaw
Date of Report: Dec 21, 2023
Post Office Box 856
Customer PO #:
Warsaw NC
28398
Customer ID: 08110011
Attention:
Report #: 2023-26342
Project ID: AG Protein MW
1,2-Dichloroethane
SW eas Method 8250DISMB
<0.5 Pg/L
11/16/2023
1,2-Dichloropropane
SW e4s Method 8260a1=8
<0.5 pg/L
11 /16/2023
1, 3,5-Trimethylbenzene
sw ttas Method 8260DMMB
<0.5 pg/L
11/16/2023
1, 3-Dichlorobenzene
SW e46 Method 6260DISMS
<0.5 pg/L
11/16/2023
1,3-Dichloropropane
SW 846 Method 62600r5=0
<0.5 Pg/L
11/16/2023
1,4-Dichlorobenzene
SW e46 Method B OMS0308
<0.5 pg/L
11/16/2023
2,2-Dichloropropane
SW e46 Method 82BOOM S
<0.5 PA
11/16/2023
2-Chlorotoluene
SW e48 Method 8=DWW8
<0.5 pg/L
11 /16/2023
4-Chlorotoluene
SW e46 Method 82NDMOB
<0.5 pg/L
11/16/2023
Benzene
SW e46 Method BMDMMB
<0.5 pg/L
11 /16/2023
Bromobenzene
SW e4s Method S=DaMB
<0.5 pg/L
11/16/2023
Bromochloromethane
SW e46 Method 8260Dr5=B
<0.5 pg/L
11/16/2023
Bromodichloromethane
sw"sMethod 6260DMWB
<0.5 pg/L
11/16/2023
Bromoform
sw e46 Method 6260Dr5030B
<0.5 pg/L
11/16/2023
Bromomethane
SW e46 Method 62soDl5=B
<0.5 pg/L
11 /16/2023
Carbon tetrachloride
SW 846 Method 62WDr5030B
<0.5 pg/L
11/16/2023
Chlorobenzene
SW 846 Method 82e0D15MB
<0.5 pg/L
11/16/2023
Chloroethane
SW 846 Method 82NDIN30D
<0.5 pg/L
11/16/2023
Chloroform
SW 846 Method 6260Dr50306
<0.5 pg/L
11/16/2023
Chloromethane
SW 646 Method t9aOW.93oe
<0.5 pg/L
11/16/2023
dis-1,2-Dichloroethene
SW W Method 626oD15oio6
<0.5 Pg/L
11/16/2023
cis-1,3-Dichloropropene
SW846Method t32601)MMOB
<0.5 pg/L
11/16/2023
Dibromochloromethane
SW sets Method 82e0MMOB
<0.5 pg/L
11/16/2023
Dibromomethane
SW 846 Method SMOrsosoB
<0.5 pg/L
11/16/2023
Dichlorodifluoromethene
SW "S Method 82BOD►ANS
<0.5 pg/L
11/16/2023
Ethylbenzene
SW e46 Method 826oa W3M
<0.5 pg/L
11/16/2023
Hexachlorobutadiene
SW sets Method 82WOM30B
<0.5 pg/L
11/16/2023
Isopropylbenzene
sw "s Method 8280t>MWB
<0.5 pg/L
11/16/2023
M+P Xylene
SW e46 Method 626oD ONO
<1.0 pg/L
11/16/2023
Methylene chloride
sw "6 Method 820I)r503013
<15 Pg/L
1,1116/2023
Report 9% 2023.26342
Pape 11 of 12

ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 s 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 a 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 * 910.347.5843 Lab/Fax
infoenvironmentalchemists.com
Smithfield Hog Productions -Warsaw
Date of Report: Dec 21, 2023
Post Office Box 856
Customer PO #:
Warsaw NC
28388
Customer ID: 08110011
Attention:
Report #: 2023-26342
Project ID: AG Protein MW
Naphthalene
sw 846 Method 8280D/5030B
<0.5 pg/L
11/16/2023
n-Butylbenzene
SW 846 MOM e28t)D/5030B
<0.5 pg/L
11/16/2023
n-Propylbenzene
SW 846 Method 8260EY50308
<0.5 pg/L
11/16/2023
ortho-Xylene
SW 846 Method 8260D=308
<0.5 pg/L
11/16/2023
p-Isopropyltoluene
sw 846 Method 0260DIS030B
<0.5 pg/L
11/16/2023
sec-Butylbenzene
SW 846 Method 82SOD/5030B
<0.5 pg/L
11/16/2023
Styrene
SW 046 Method 8289D=308
<0.5 pg/L
11/16/2023
tert-Butylbenzene
SW 846 Method 82SM50308
<0.5 pg/L
11/16/2023
Tetrachloroethene
SW 846 Method 82NDW30B
<0.5 pg/L
11/16/2023
Toluene
SW 046Method 82ND/50308
<0.5 pg/L
11/16/2023
Trans-1,2-Dichloroethene
Sw846Method 8280D150308
<0.5pg/L
11/16/2023
Trans-1,3-dichloropropene
sw 848 Memos 82s0 =30B
<0.5 pg/L
11/16/2023
Trichloroethene
sw 846 Method 02600/5030B
<0.5 pg/L
11/16/2023
Trichlorofluoromethane
sw 846 Method 82600150308
<0.5 pg/L
11/16/2023
Vinyl chloride
SW 846 Method 826OW0308
<0.5 pg/L
11116/2023
Nitrate Nitrogen (Cale)
Nitrite Nitrogen EPA;1S3,2, Rev 2,0, 1983 < 0.02 mg/L 11110/2023
Nitrate+ N itrite-Nitrogen EPA 353,2, Rev, 2.0, 1M 0.08 mg/L 11/14/2023
Nitrate Nitrogen Subtraction mod 0.08 mg/L 11/14/2023
Comment: Auto sampler malfu ction occurred on sample 63754.
Y
Reviewed by.
Report A,: 202S-28342 Page 12 of 12

Environmental Chemist, Inc., Wilmington, NC Lab #94
6602 Windmill W
Wilmington, NC 284!
Sample Receipt Checklist 910-392,02.
Client: Date: JI rJ
��,-`—�— Report Number: 2023-
Receipt of sample; ECHEM Pickup Client Delivery ❑ UPS Q
Q YE5 ❑ NO C N/A 1. Were custody seals present on the cooler?
Cf YES L7 NO p N/A 2. if custody seals were present, were they intact/unbroken?
Original temperature upon receipt eC
How temperature taken: Corrected temperature L
❑ Temperature Blank Ell Against Bottles
III Gun ID: Thomas Traceable S/N 210886869 IR Gun Correction Factor'C: 0.0
UO YES ❑ NO 3. If temperature of cool
FedEx ❑ Other ❑
fete
Q YES
G YES
0 NO
er exceeded 6 C, was Project Mgr./QA notified?
4. Were proper custody procedures (relinquished/received)
0
Q NO
followed?
5. Were sample ID's listed on the COC?
YES
0 YES
❑ NO
Q NO
6. Were samples ID's listed on sample containers?
0 YES
0 NO
7. Were collection date and time listed on the COC?
21 YES
❑ NO
8. Were tests to be performed listed on the COC?
Q YES
❑ NO
9. Did samples arrive in proper containers for each test?
10. Did samples arrive in
0 YES
0
Cl NO
good condition for each test?
11. Was adequate sample volume available?'
YES
YES
❑ NO
❑ NO
12. Were samples received within proper holding time for requested tests?
13. Were acid preserved samples
O YES
❑
❑ NO
received at a pH of <2?
14. Were cyanide samples received at a pH >12?
YES
YES
❑ NO
❑
15. Were sulfide samples received at a pH >9?
❑ YES
NO
❑ NO
16. Were NH3/TKN/Phenol received at a chlorine residual of <0.5 m/L? _
17. Were Sulfide/Cyanide
❑ YES
❑ NO
received at a chlorine residual of <0.5 m/L?
18. Were orthophosphate samples filtered in the field
within 15 minutes?
* TOC/Volat,ies are pH checked at time of analysis and recorded on the benchsheet
** Bacteria samples are checked for Chlorine at time of analysis and recorded on the benchsheet.
ISample Preservation. (Must be completed for any sample(s) incorrectly preserved or with headspace)
jSample(s) were received incorrectly preserved and were adjusted accordingly
Ilby adding (circle one): H2SO, HNO3 HCI
Time of preservation., NaOH
If more than one preservative is needed, notate in comments below
%lo:e" %,)t fy C,.s`_'re' sa-v CC- !.T:-e e
d•at_'y fpr r9corrert'y presewe3 sa•n es
p• Ot:a"n a re.,, sa rc'e a
^, a'la•y:-� C/ :"e C4s:Cf'1'r. ��. k9i f`.?trna �`� � t n•.
dolatiles Sample(s) ° a
were received with headspace
COMMENTS:
DOC_ QA.002 Rev 1

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