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Home My WebLink AboutWQ0000485_Monitoring - 11-2023_20231220Monitoring Report Submittal Permit Number#* Name of Facility:* Month: * November Report Information Type * Revised - GW-59 Confirmation Email Address: Name of Submitter: * Signature: Date of submittal: WQ0000485 Darling Ingredients - Rose Hill Year:* 2023 Upload Document* scan 2023-11 WQ0000485 GW-59 DIRH - 5.12MB revised.pdf PDF Only Please upload one PDF containing all applicable monitoring reports (i.e., NDMR, NDAR-1, NDAR-2, NDMLR, GW-59). corey.Ianier@darlingii.com Corey Lanier �!'tf./f �fliYlPl' Initial Review .............................. Reviewer: Wanda.Gerald 12/20/2023 This will be filled in automatically Is the project number correct?* W00000485 Is the monitoring report accepted?* Yes NO Regional Office* Wilmington Reviewer: _anonymous Review Date: 1/5/2024 DARLING I-- INGREDIENTS December 18, 2023 Division of Water Resources Attn: Information Processing Unit 1617 Mail Service Center Raleigh, NC 27699-1617 Re: Ground Water Quality Monitoring Report (GWQMR) Darling Ingredients — Rose Hill Permit WQ0000485 To whom it may concern, Please find enclosed the Groundwater Quality Monitoring Compliance Report for Surface Irrigation for the month of November 2023 for our Rose Hill Division. Should you require any additional information or wish to discuss this matter, please feel free to contact me at 910.289.2083 x 25119. Sincerely, $LVI M. Larry Holt General Manager cc: DI Regional Corporate Office SUBMIT FORM ON YELLOW PAPER ONLY • . • DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES GROUNDWATER QUALITY MONITORING: • • DIVISION OF WATER RESOURCES - INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM 161 r MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: 919-807-6306 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: W00000485 Expiration Date: 3/31/2025 Facility Name: Darling Ingredients - Rose Hill Non -Discharge UIC NPDES Other Permit Name (if different): Facility Address: 469 Yellow Cut Rd TYPE OF PERMITTED OPERATION BEING MONITORED Rose Hill, NC 28458 County Duplin ❑ Lagoon ❑ Remediation: Infiltration Gallery (State) (zip) X Spray Field ❑ Remediation: Contact Person Corey Lanier Telephone#: (910) 660-1173 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name No of wells to be sampled: 11 ❑ Water Source Heat Pump ❑ Other: from Permit SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MWA Date sample collected: 11/4/2023 FIELD ANALYSES: WAS Well Depth: 12.46 ft. Well Diameter: 2 in. pH4500HB 5.20 units Temp. 000lo: 21.5 oC DRY at Depth to Water Level 82546: 5.5 Screened Interval: 12.46 ft. to 2.46 ft. Spec. Cond. 00094 µMhos time of Measuring Point is 1.17 ft. above land surface Relative M.P. Elevation: ft. Odor 00085 None sampling, Volume of water pumped/bailed before sampling: 5.0 gallons Appearance Clear chec" Samples for metals were collected unfiltered: X YES I-1 NO and field acidified: X YES NO here LABORATORY INFORMATION Date sample analyzed: 11/04/2023-12/12/2023 Laboratory Name: Environmental Chemists, Inc. Certification No. DWQ#94 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 <0.02 mg/L Pb - Lead 01051 ug/L Coliform: MF Fecal 31616 <1.0 /100mL Nitrate (NO3) as N 00620 0.43 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 <0.04 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 70300 121.00 mg/L Al -Aluminum 01105 mg/L Sodium 6.46 mg/L pH (Lab) 00403 5.20 units Ba - Barium 01007 ug/L TOC 00680 1.1 mg/L Ca - Calcium 00916 mg/L Chloride 00940 7 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total 01034 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 59 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? M Yes (0) ❑ No (0) pecific Conductance 00095 µMhos K - Potassium 00937 mg/L VOC 78732: method # SM 6200C Total Ammonia 00610 <0.2 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen; N113as N; Ammonia Nitrogen, Total) Mn - Manganese 01055 ug/L method # TKN as N 00625 <0.5 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% GW-59 Rev.8/2013 SUBMIT FORM ON YELLOW PAPER ONLY • • • DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES GROUNDWATER QUALITY MONITORING: • • • DIVISION OF WATER RESOURCES - INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: 919-807-6306 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: WQ0000485 Expiration Date: 3/31/2025 Facility Name: Darling Ingredients - Rose Hill Non -Discharge UIC Permit Name (if different): NPDES Other Facility Address: 469 Yellow Cut Rd. TYPE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑ Remediation: Infiltration Gallery Rose Hill, NC 28458 County Duplin "'a"' "°' X Spray Field ❑ Remediation: Contact Person: Corey Lanier Telephone#: (910) 660-1173 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name No. of wells to be sampled 11 ❑ Water Source Heat Pump ❑ Other: �E r SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW-2 Date sample collected. 11/4/2023 FIELD ANALYSES: WAS Well Depth: 31.00 ft. Well Diameter: 2 in. pH4500HB 6.70 units Temp. 000lo: 18.6 °C DRY at Depth to Water Level 82546: 12.8 ft. below measuring point Screened Interval 30.15 ft. to 20.15 ft. Spec. Cond. 00094: µMhos time of Measuring Point is 3 _ ft. above land surface Relative M.P. Elevation. ft. Odor 00085: None sampling, check 'Volume of water pumped/bailed before sampling: 5.0 gallons Appearance Tan/Clear here: Samples for metals were collected unfiltered: X YES n NO and field acidified: X YES ❑ NO LABORATORY INFORMATION Date sample analyzed: 11/04/2023-12/12/2023 Laboratory Name: Environmental Chemists, Inc. Certification No. DWQ#94 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 <0.02 mg/L Pb - Lead 01051 ug/L Coliform: MF Fecal 31616 <1.0 /100mL Nitrate (NO3) as N 00620 0.17 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 <0.04 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units) )issolved Solids -.Total 70300 292.00 mg/L Al - Aluminum oilo5 mg/L Sodium 11.2 mg/L pH (Lab) 00403 6.70 units Ba - Barium 01007 ug/L TOC 00680 1.1 mg/L Ca - Calcium 00916 mg/L Chloride 00940 13 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total 01034 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 27 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? E Yes (0) ❑ No (0) ipecific Conductance o0095 µMhos K - Potassium 00937 mg/L VOC 78732 method # SM 6200C Total Ammonia 00610 <0.2 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen; NH3 as N; Ammonia Nitrogen, Total) Mn - Manganese 01055 ug/L method # TKN as N 00625 <0.5 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% . GW-59 Rev.8/2013 SUBMIT FORM ON YELLOW PAPER ONLY • • DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES GROUNDWATER QUALITY MONITORING: • DIVISION OF WATER RESOURCES - INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM 1617 MAIL SERVICE CENTER, RALEIGH, INC 27699-1617 Phone. 919-807-6306 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: WQ0000485 Expiration Date 3/31/2025 Facility Name: Darling Ingredients - Rose Hill Non -Discharge UIC NPDES Other Permit Name (if different): Facility Address: 469 Yellow Cut Rd. TYPE OF PERMITTED OPERATION BEING MONITORED Rose Hill, NC 28458 County Duplin ❑ Lagoon ❑ Remediation: Infiltration Gallery (City) (State) (zip) X Spray Field ❑ Remediation: Contact Person: Corey Lanier Telephone#: (910) 660-1173 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name No. of wells to be sampled: 11 ❑ Water Source Heat Pump ❑ Other: (from Permit) SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW-4 Date sample collected: 11/4/2023 FIELD ANALYSES: WAS Well Depth: 28.93 ft. Well Diameter: 2 in. pH4500HB 7.00 units Temp. 000lo: 19.9 °C DRY at Depth to Water Level 82546: 6.4 ft. below measuring point Screened Interval: 28.93 ft. to 18.93ft. Spec. Cond. 00094: µMhos time of Measuring Point is 3 _ft. above land surface Relative M.P. Elevation: ft. Odor 000m None sampling, check Volume of water pumped/bailed before sampling: 5.0 gallons Appearance Clear/Tan here: Samples for metals were collected unfiltered: X YES ❑ NO and field acidified X YES ❑ NO LABORATORY INFORMATION Date sample analyzed: 11/04/2023-12/12/2023 Laboratory Name: Environmental Chemists, Inc. Certification No. DWQ#94 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N oo615 <0.02 mg/L Pb - Lead o1o51 ug/L Coliform: MF Fecal 31616 <1 /100mL Nitrate (NO3) as N 00620 <0.02 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 <0.04 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units) issolved Solids:Total 70300 211.00 mg/L Al - Aluminum 01105 mg/L Sodium 8.25 mq/L pH (Lab) 00403 7.00 units Ba - Barium 01007 ug/L TOC oomo 1.10 mg/L Ca - Calcium oos16 mg/L Chloride 00940 <5.0 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total 01034 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 <5.0 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? E Yes (0) ❑ No (0) pecific Conductance 00095 µMhos K - Potassium 00937 mg/L VOC 78732: method # SM 6200C Total Ammonia 00610 <0.2 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen; NH3as N; Ammonia Nitrogen, Total) Mn - Manganese 01055 ug/L method # TKN as N 00625 <0.5 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% Larry Holt - General Manager Permittee (or Authorized Aqent) Name and Title - Please print or type GW-59 Rev.8/2013 GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM ACILITY INFORMATION Please Pnnt Clearly or Type acility Name: Darling Ingredients - Rose Hill ermit Name (if different): acility Address: 469 Yellow Cut Rd. Rose Hill, NC 29458 (City) (6P) County Duplin act Person: Corey Lanier Telephone#: (910) 660-1173 Location/Site Name: No. of wells to be sampled: 11 ID NUMBER (from Permit): MW-7A Well Depth: 16 ft. Depth to Water Level 82546: 6.0 ft. below measuring point Measuring Point is 2.42 ft. above land surface t...... r....... , Date sample collected: 11/4/2023 DEPARTMENT OF ENVIRONMENT 6 NATURAL RESOURCES DIVISION OF WATER RESOURCES - INFORMATION PROCESSING UNIT 1617 MAIL SERVICE CENTER, RALEIGH, NC 276994617 Phone: 919.807.6308 PERMIT Number: W00000485 Expiration Date: 3/31/2025 Non -Discharge UIC NPDES Other TYPE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑ Remediation: Infiltration Gallery X Spray Field ❑ Remediation ❑ Rotary Distributor ❑ Land Application of Sludge ❑ Water Source Heat Pump ❑ Other: Well Diameter: 2 in. Screened Interval: 16 ft. to 6 ft. Relative M.P Elevation: ft. Volume of water pumped/bailed before sampling 5.0 gallons Samples for metals were collected unfiltered X YES rl NO and field acidified: X YES ❑ NO FIELD ANALYSES: pH4500HB 3.66 units Spec. Cond. ODD94: Temp. 000lo: 27.5 oC Odor 00085: None Appearance Tan/Clear Date sample analyzed 11/04/2023-1211212023 Laboratory Name Environmental Chemists, Inc. PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 <0.02 mg/L Pb - Lead 01051 Coliform: MF Fecal 31616 <1 /100mL Nitrate (NO3) as N 00620 <0.02 mg/L Zn - Zinc 01092 Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 <0.04 mg/L 4Mhos Certification No. DWQ#94 ug/L mg/L (Note Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): Dissolved Solids:Total 70300 26400 mg/L Al - Aluminum 01105 mg/L Sodium 12.3 mq/L pH (Lab) 00403 3.66 units Ba - Barium 01007 ug/L TOC 00680 1 mg/L Ca - Calcium 00916 mg/L Chloride 00940 128 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total 01034 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 23 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? N Yes (0) ❑ No (0) Specific Conductance 00095 uMhos K - Potassium 00937 mg/L VOC 78732: method # SM 6200C Total Ammonia 00610 <0.2 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen; NHsas N; Ammonia Nitrogen, Total) Mn - Manganese 01055 ug/L , method # TKN as N 00625 <0.5 mg/L Ni - Nickel 01067 ug/L method # Lab Reports): Influent Larry Holt - General Manager Permittee (or Authorized Agent) Name and Title - Please print or type mg/L If WELL WAS DRY at time of sampling, DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES GROUNDWATER QUALITY MONITORING: ON DIVISION OF WATER RESOURCES -INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: 919-607-6306 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: WQ0000485 Expiration Date: 3/31/2025 Facility Name: Darling Ingredients - Rose Hill Non -Discharge UIC NPDES Other Permit Name (if different): Facility Address: 469 Yellow Cut Rd. TYPE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑ Remediation: Infiltration Gallery Rose Hill, NC 28458 County Duplin (City) staler 'P• X Spray Field ❑ Remediation: Contact Person Corey Lanier Telephone#: (910) 660-1173 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name: Field 5 -damaged by farm equip / to replace No. of wells to be sampled: 11 ❑ Water Source Heat Pump ❑ Other: (from Permit) SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW-8A Date sample collected: 11/4/2023 FIELD ANALYSES: WAS Well Depth 16 ft. Well Diameter: 2 in. pH4500HB 4.60 units Temp. 000lo: 21.2 oC DRY at Depth to Water Level 82546: 7.0 ft. below measuring point Screened Interval: 16 ft. to 6 ft. Spec. Cond. 00094: µMhos time of Measuring Point is 2.5 ft. above land surface Relative M.P. Elevation: ft. Odor 00085 None sampling, Volume of water pumped/bailed before sam 0 5.0 gallons Appearance Tan/Clear checl�, Samples for metals were collected unfiltered X YES Q NO and field acidified: X YES ❑ NO here:u LABORATORY INFORMATION Date sample analyzed- 11/04/2023-12/12/2023 Laboratory Name: Environmental Chemists, Inc. Certification No. DWQ#94 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 <0.02 mg/L Pb - Lead 01051 ug/L Coliform: MF Fecal 31616 <1.0 /100mL Nitrate (NO3) as N 00620 0.39 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 0.1 mg/L (Note Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 70300 54.00 mg/L Al -Aluminum 01105 mg/L Sodium 1.41 mg/L pH (Lab) 00403 4.60 units Ba - Barium 01007 ug/L TOC 00680 0.90 mg/L Ca - Calcium 00916 mg/L Chloride 00940 <5 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total 01034 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 23 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? 0 Yes (0) ❑ No (0) Specific Conductance 00095 µMhos K - Potassium 00937 mg/L VOC 78732: method # SM 6200C Total Ammonia 00610 <0.2 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen; NH3asN; Ammonia Nitrogen, Total) Mn - Manganese o1055 ug/L , method # TKN as N 00625 <0.5 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% • • • DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES GROUNDWATER QUALITY MONITORING: • • • DIVISION OF WATER RESOURCES -INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: 919-807-6306 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: WQ0000485 Expiration Date: 3/31/2025 Facility Name: Darling Ingredients - Rose Hill Non -Discharge UIC NPDES Other Permit Name (if different): Facility Address: 469 Yellow Cut Rd. TYPE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑ Remediation: Infiltration Gallery Rose Hill, NC 28458 County Duplin (state) (zip) X Spray Field ❑ Remediation: Contact Person. Corey Lanier Telephone#: (910) 660-1173 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name No. of wells to be sampled: 11 ❑ Water Source Heat Pump ❑ Other: (from Permit) SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW-9 Date sample collected: 11/4/2023 FIELD ANALYSES: WAS Well Depth: 13.73 ft. Well Diameter: 2 in. pH4500HB 5.90 units Temp. 000lo: 17.8 oC DRY at Depth to Water Level 82546: 6.2 ft. below measuring point Screened Interval: 13.73 ft. to 3.73 ft. Spec. Cond. 00094: µMhos time of Measuring Point is 3.80 ft. above land surface Relative M.P. Elevation: ft. Odor 00085: None sampling, Volume of water pumped/bailed before sampling. 5.0 gallons Appearance Tan/Turbid checl�_ Samples for metals were collected unfiltered: X YES NO and field acidified: X YES ❑ NO here: LABORATORY INFORMATION Date sample analyzed: 11/04/2023-12/12/2023 Laboratory Name- Environmental Chemists, Inc. Certification No. DWQ#94 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 0.05 mg/L Pb - Lead 01051 ug1L Coliform: MF Fecal 31616 <1.0 /100mL Nitrate (NO3) as N 00620 0.23 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 <0.04 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 70300 278.00 mg/L Al -Aluminum 01105 mg/L Sodium 7.10 mg/L pH (Lab) 00403 5.90 units Ba - Barium 01007 ug/L TOC 00680 30.6 mg/L Ca - Calcium 00916 mg/L Chloride 00940 27 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total 01034 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 29 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? 0 Yes (0) ❑ No (0) Specific Conductance 00095 µMhos K - Potassium 00937 mg/L VOC 78732: method # SM 6200C Total Ammonia oo6lo <0.2 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen; NH, as N; Ammonia Nitrogen, Total) Mn - Manganese o1o55 ug/L , method # TKN as N 00625 0.8 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs mg/L Effluent Total VOCs: mg/L VOC Removal% Larry Holt - General Manager Permittee (or Authorized Agent) Name and Title - Please print or type • • DEPARTMENT OF ENVIRONMENT 8. NATURAL RESOURCES GROUNDWATER QUALITY MONITORING: DIVISION OF WATER RESOURCES - INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: 919-807.6306 FACILITY INFORMATION Please Print Clearly orType PERMIT Number: WQ0000485Expiration Date: 3/31/2025 Facility Name: Darling Ingredients - Rose Hill Non -Discharge UIC NPDES Other Permit Name (if different): Facility Address: 469 Yellow Cut Rd. TYPE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑ Remediation: Infiltration Gallery Rose Hill, NC 28458 County Duplin (City) (Stale) _"p X Spray Field ❑ Remediation: Contact Person Corey Lanier Telephone#: (910) 660-1173 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name No. of wells to be sampled: 11 ❑ Water Source Heat Pump ❑ Other: (from Permit) SAMPLING INFORMATION If WELL 'WELL ID NUMBER (from Permit): MW-10A Date sample collected: 11/4/2023 FIELD ANALYSES: WAS Well Depth: 16 ft. Well Diameter: 2 in. pH4500HB 3.55 units Temp. 000lc 19.6 °C DRY at Depth to Water Level 82546: 5.3 ft. below measuring point Screened Interval: 16 ft. to 6 ft. Spec. Cond. 00094 uMhos time of Measuring Point is 3 ft above land surface Relative M P. Elevation: ft. i Odor 00085 None sampling, Volume of water pumped/bailed before sampling: 50 gallons Appearance Clear check here:❑ Samples for metals were collected unfiltered: X YES n NO and field acidified: X YES n NO LABORATORY INFORMATION Date sample analyzed: 11/04/2023-12/12/2023 Laboratory Name: Environmental Chemists, Inc. Certification No DWQ#94 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 <0.02 mg/L Pb - Lead o1o51 ug/L Coliform: MF Fecal 31616 <1 /100mL Nitrate (NO3) as N 00620 <0.02 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100ml- Phosphorus: Total as P 00665 0.07 mg/L (Note Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): )issolved Solids:Total 70300 793.00 mg/L Al - Aluminum o11o5 mg/L Sodium 114 mg/L pH (Lab) 00403 3.55 units Ba - Barium 01007 ug/L TOC 00680 3.8 mg/L Ca - Calcium 00916 _ mg/L Chloride 00940 322 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total 01034 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 143 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? ! Yes (0) ❑ No (0) pecific Conductance 00095 uMhos K -Potassium 00937 mg/L VOC 78732: method # SM 6200C Total Ammonia 00610 0.40 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen; NH, as N; Ammonia Nitrogen, Total) Mn - Manganese 01055 ug/L , method # TKN as N 00625 0.60 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% Larry Holt - General Manager Permittee (or Authorized Agent) Name and Title - Please print or type DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES GROUNDWATER QUALITY MONITORING: DIVISION OF WATER RESOURCES - INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699.1617 Phone: 919-807-6306 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: W00000485 Expiration Date: 3/31/2025 Facility Name: Darling Ingredients - Rose Hill Non -Discharge UIC NPDES Other Permit Name (if different): Facility Address: 469 Yellow Cut Rd TYPE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑ Remediation: Infiltration Gallery Rose Hill, NC 28458 County Duplin Sate, (zip) X Spray Field ❑ Remediation: Contact Person: Corey Lanier Telephone#: (910) 660-1173 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name No. of wells to be sampled: 11 ❑ Water Source Heat Pump ❑ Other: (from Permit) SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW-11A Date sample collected: 11/4/2023 FIELD ANALYSES: WAS Well Depth: 16 ft. Well Diameter: 2 in. pH4500HB 4.70 units Temp. 000lc 20.6 oC DRY at Depth to Water Level 82546: 7.5 Screened Interval: 16 ft. to 6 ft. Spec. Cond. 00094: ttMhos time of Measuring Point is 3.3 ft. above land surface Relative M.P. Elevation: ft. Odor 000m None sampling, Volume of water pumped/bailed before sampling: 5.0 gallons Appearance Clear/Tan checl. here: Samples for metals were collected unfiltered: X YES NO and field acidified: X YES NO LABORATORY INFORMATION Date sample analyzed: 11/04/2023-12/12/2023 Laboratory Name: Environmental Chemists, Inc. Certification No. DWQ#94 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 <0.02 mg/L Pb - Lead o1o51 ug/L Coliform: MF Fecal 31616 <1.0 /100mL Nitrate (NO3) as N 00620 0.34 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 <0.04 mg/L (Note Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units) )issolved Solids:Total 70300 490.00 mg/L Al - Aluminum 01105 mg/L Sodium 62.9 mq/L pH (Lab) 00403 4.70 units Ba - Barium 01007 ug/L TOC 00680 2.50 mg/L Ca - Calcium 00916 mg/L Chloride 00940 121 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total 01034 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 161.0 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? E Yes (0) ❑ No (0) Specific Conductance 00095 µMhos K - Potassium 00937 mg/L VOC 78732 method # SM 6200C Total Ammonia 00610 <0.2 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen; NH3 as N; Ammonia Nitrogen, Tots., Mn - Manganese 01055 ug/L , method # TKN as N 00625 <0.50 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: Larry Holt - General Manager Permittee (or Authorized Agent) Name and Title - Please print or type Signature of Pefmittee ( Authorized Agent) mg/L VOC Removal% DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES GROUNDWATER QUALITY MONITORING: DIVISION OF WATER RESOURCES - INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM ��1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: 919-807-6306 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: WQ0000485 Expiration Date: 3/31/2025 Facility Name: Darling Ingredients - Rose Hill Non -Discharge UIC NPDES Other Permit Name (if different): Facility Address: 469 Yellow Cut Rd TYPE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑ Remediation: Infiltration Gallery Rose Hill, NC 28458 County Duplin (C" (State) (zip) X Spray Field ❑ Remediation: Contact Person Corey Lanier Telephone#: (910) 660-1173 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name No. of wells to be sampled: 11 ❑ Water Source Heat Pump ❑ Other: (from Permit) SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW-12B Date sample collected: 11/4/2023 FIELD ANALYSES: WAS Well Depth: 16 ft. Well Diameter: 2 in. pH450oHB 3.91 units Temp. 000lo: 212 °C DRY at Depth to Water Level 82546: 6.8 ft. below measuring point Screened Interval: 20 ft. to 10 ft. Spec. Cond. 00094: µMhos time of Measuring Point is 3 ft. above land surface Relative M.P. Elevation: ft. Odor 00085: None sampling, Volume of water pumped/bailed before sampling: 5.0 gallons Appearance None check here: SamDles for metals were collected unfiltered: X YES F-1 NO and field acidified: X YES ❑ NO LABORATORY INFORMATION Date sample analyzed: 11/04/2023-12/12/2023 Laboratory Name: Environmental Chemists, Inc. Certification No. DWQ#94 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 <0.02 mg/L Pb - Lead 01051 ug/L Coliform: MF Fecal 31616 <1 /100mL Nitrate (NO3) as N 00620 0.14 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 0.15 mg/L (Note Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): .)issolved Solids:Total 70300 385.00 mg/L Al - Aluminum 01105 mg/L Sodium 68.7 mg/L pH (Lab) 00403 3.91 units Ba - Barium 01007 ug/L TOC oo68o 1.70 mg/L Ca - Calcium 00916 mg/L Chloride 00940 120 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total 01034 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 124 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? 0 Yes (0) ❑ No (0) Specific Conductance 00095 µMhos K - Potassium 00937 mg/L VOC 78732: method # SM 6200C Total Ammonia 00610 <0.2 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen; N113as N; Ammonia Nitrogen, Total) Mn - Manganese 01055 ug/L , method # TKN as N 00625 0.50 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% Larry Holt - General Manager Pennittee (or Authorized Agent) Name and Title - Please print or type DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES GROUNDWATER QUALITY MONITORING: DIVISION OF WATER RESOURCES - INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: 919-607-6306 FACILITY INFORMATION Please PnntClearlyorType PERMIT Number: WQ0000485 Expiration Date: 3/31/2025 Facility Name: Darling Ingredients - Rose Hill Non -Discharge UIC NPDES Other Permit Name (if different): Facility Address: 469 Yellow Cut Rd. TYPE OF PERMITTED OPERATION BEING MONITORED Rose Hill, NC 28458 County Duplin ❑ Lagoon ❑ Remediation: Infiltration Gallery (State) (zip) X Spray Field ❑ Remediation: Contact Person: Corey Lanier Telephone#: (910) 660-1173 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name No. of wells to be sampled: 11 ❑ Water Source Heat Pump ❑ Other: (from Permit) SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW-13A Date sample collected: 11/4/2023 FIELD ANALYSES: WAS Well Depth: 16 ft. Well Diameter: 2 in. pH4500HB 4.70 units Temp. 000lo: 21.8 °C DRY at (Depth to Water Level 82546: 7.4 ft. below measuring point Screened Interval: 16 ft. to 6 ft. Spec. Cond. 00094: uMhos time of Measuring Point is 3 ft. above land surface Relative M.P. Elevation: ft. Odor 00085 None sampling, Volume of water pumped/bailed before sampling: 5.0 gallons Appearance ClearlTan check herein Samples for metals were collected unfiltered: X YES NO and field acidified: X YES NO LABORATORY INFORMATION Date sample analyzed: 11/04/2023-12/12/2023 Laboratory Name: Environmental Chemists, Inc. Certification No. DWQ#94 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 0.02 mg/L Pb - Lead 01051 ug/L Coliform: MF Fecal 31616 <1 /100mL Nitrate (NO3) as N 00620 0.02 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 <0.04 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 70300 35.00 mg/L Al - Aluminum 01105 mg/L Sodium 4.25 mg/L pH (Lab) 00403 4.70 units Ba - Barium 01007 ug/L TOC 00680 0.60 mg/L Ca - Calcium oo916 mg/L Chloride 00940 <5 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total 01034 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 8.00 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? N Yes (0) ❑ No (0) Specific Conductance 00095 uMhos K - Potassium 00937 mg/L VOC 78732: method # SM 6200C Total Ammonia 00610 <0.20 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen; NH3 as N; Ammonia Nitrogen, Total) Mn - Manganese 01055 ug/L , method # TKN as N 00625 <0.50 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCS: Larry Holt - General Manager Pennittee (or Authorized Agent) Name and Title - Please print or type • . TC e and that the laboratory analytical data was ;sibilily of fines andimprisonmentfor knowing Mr. .2WAMMMM a�i mg/L VOG Removal% 2 • • DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES GROUNDWATER QUALITY MONITORING: • • • • DIVISION OF WATER RESOURCES - INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: 919-807-6306 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: W00000485 Expiration Date: 3/31/2025 Facility Name: Darling Ingredients - Rose Hill Non -Discharge UIC NPDES Other Permit Name (if different): Facility Address: 469 Yellow Cut Rd TYPE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑ Remediation: Infiltration Gallery Rose Hill, NC 28458 County Duplin (stale) (zip) X Spray Field ❑ Remediation: Contact Person: Corey Lanier Telephone#: (910) 660-1173 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name No. of wells to be sampled: 11 ❑ Water Source Heat Pump ❑ Other: (from Pemit) SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW-14A Date sample collected 11/4/2023 FIELD ANALYSES: WAS Well Depth: 16 ft. Well Diameter: 2 in. pH4500HB 5.10 units Temp. 000lc 21.8 °C DRY at Depth to Water Level 82546: 6.5 ft. below measuring point Screened Interval: 10 ft. to 2.5 ft. Spec. Cond. 00094 uMhos time of Measuring Point is 3 above land surface Relative M P Elevation: ft. Odor 00085: None sampling, _ft. Volume of water pumped/bailed before sampling: 5.0 gallons Appearance Tan/Turbid checl� Samples for metals were collected unfiltered: X YES M NO and field acidified: X YES NO here: LABORATORY INFORMATION Date sample analyzed: 11/04/2023-12/12/2023 Laboratory Name: Environmental Chemists, Inc. Certification No. DWQ#94 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 <0.02 mg/L Pb - Lead 01051 ug/L Coliform: MF Fecal 31616 <1.0 /100mL Nitrate (NO3) as N 00620 3.78 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 <0.04 mg/L (Note Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 70300 1010.00 mg/L Al - Aluminum 01105 mg/L Sodium 119 mg/L pH (Lab) 00403 510 units Ba - Barium 01007 ug/L TOC oomo 3.70 mg/L Ca - Calcium 00916 mg/L Chloride 00940 316 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total 01034 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 238 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? 0 Yes (0) ❑ No (0) Specific Conductance 00095 rtMhos K - Potassium 00937 mg/L VOC 78732 method # SM 6200C Total Ammonia 00610 <0.20 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen; NH3 as N; Ammonia Nitrogen, Total) Mn - Manganese 01055 ug/L , method # TKN as N 00625 <0.50 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs mg/L VOC Removal% Larry Holt - General Manager Permitlee (or Authorized Agent) Name and Title - Please print or type GW-59A COMPLIANCE REPORT FORM Permit # W00000485 I Enter date monitoring results were due. (1213112023) Will this monitoring report (GW-59 and GW-59A) be submitted after the established due date? No 2 Was any required information missing on the GW-59 report forms? No IF the answer to question 1 or 2 is'YES , list in the space provided below the well identification number(s) and explain the oroblems encountered in obtaining the required information. MW-8A was damaged by farm equipment and is scheduled to be closed and replaced by Register Well Co, INC; moving the replacement well 10' due North per DEQ direction- 3 Are any of the monitor wells in need of repair or maintenance (damaged casing, unlocked or missing cap, missing identification plate, area overgrown, etc.)? If the answer is "Yes ", contact the Regional Office for guidance. No 4 Are any monitored constituents equal to or above the established standards? YES If the answer to question 4 is "NO'; skip to section B. If the answer to question 4 is "YES" list the affected wells individually with constituent(s) and concentration(s) exceeding standards in the space provided below: SEE ATTACHED GROUNDWATER MONITORING WELL 2 YR EXCEEDANCE HISTORY REPORT 5 For the constituents identified in question 4 above, have standards been exceeded previously for the same constituent(s) In the same well(s) in the last two years? YES If the answer to question 5 is 'NO", skip to section 8. If the answer to question 5 is "YES", list in the space provided below, each well with constituent(s) exceeding standards, concentration(s) reported, and sample collection date for each occurrence (tor the last two years). SEE ATTACHED GROUNDWATER MONITORING WELL 2 YR EXCEEDANCE HISTORY REPORT Are the monitoring wells listed In section 5 located at or beyond the review boundary? YES If the answer is "YES", a groundwater quality problem may be occurring. CONTACT THE REGIONAL OFFICE IMMEDIATELY FOR GUIDANCE. If the answer is "NO", monitoring wells may be improperly located; contact the Regional Office. 7 Is the permittee Implementing previously approved actions required by the Division involving this groundwater quality problem? YES If the answer to question 7 is "YES", describe those actions in the space provided below. If the answer to question 7 is "NO" contact the Re Tonal Office within 90 days: an evaluation may be required to determine the impact the waste disposal system is having at the review and compliance boundaries surrounding this facility. Failure to do so may subject the permittee to a Notice of Violation, Fines, and/or penalties. Additional monitoring was performed to identify constituents of TOC in MW No.9. The facility has been communicating with Mr. Geoff Kegley in the Wilmington Regional Office, 8 The person completing this portion (GW-59A) of the monitoring report should sign below and submit this form with G W-59 forms for required wells to the address provided at the top of the current G W-59 form. 11 hereby acknowledge that the above Information was evaluated and the information submitted in this report (Compliance Report GW-59A) Is true and complete to the best of my knowledge. p lZ �b Z�j signaturePermfttee ar Authorized Agentl aca Valley Proteins, Inc - Rose Hill (WQ0000485) Groundwater Monitoring Well 2 Year Exceedance History Report TDS 500 10A 14A November-23 793 1010 July-23 816 1270 March-23 804 1310 November-22 833 944 July-22 772 1280 March-22 783 1100 November-21 801 1230 July-21 706 1010 pH 6.5-8.5 1 2 4 7A 8A 9 10A 11A 12B 13A 14A November-23 5 7 7 3.66 4.6 5.9 3.55 4.7 3.91 4.7 5.1 July-23 5.20 5.50 5.80 5.30 5.10 6.30 3.70 5.40 4.60 4.70 4.70 March-23 6.40 6.30 6.30 3.86 4.50 6.70 4.10 4.50 4.20 4.80 5.00 November-22 5.60 6.30 3.86 4.20 6.00 3.67 4.10 3.70 4.40 4.70 July-22 6.40 6.40 6.3 5.1 5.3 6.4 4.2 4.6 4 5.1 1 4.9 March-22 6.40 5.9 4.7 4.6 4.6 4.4 4.2 4.7 5.2 November-21 5.50 4.30 4.50 6.30 4.00 4.30 4.20 4.20 5.00 July-21 5.00 1 6.10 5.60 4.90 4.60 5.90 4.70 4.60 5.40 5.00 TOC 10 9 November-23 30.6 July-23 46.9 March-23 33 November-22 27.6 July-22 45.1 March-22 34.9 November-21 26.4 July-21 25.9 Chloride 250 10A 14A November-23 322 316 July-23 337 361 March-23 350 November-22 305 350 July-22 261 356 March-22 294 325 November-21 353 July-21 425 1 275 F00510- -- -71 Environmental Chemists, Inc. • 6602 Windmill Way, Wilmington, NC 28405 . 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax v} 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS infoLenvironmentalchemists.com Darling Ingredients - Rose Hill Date of Report: Dec 13, 2023 Post Office Box 1026 Customer PO #: Rose Hill NC 28458 Customer ID: 08100027 Attention: Report #: 2023-25631 Project ID: Monitoring Wells Lab ID Sample ID: Collect DatelTime Matrix Sampled by 23-62087 Site: MW-1 11/4/2023 11:25 AM Water jcb/envirochem Test Method Results Date Analyzed Color Color Clear 11 /04/2023 Depth to water, ft. Depth to Water. Ft. 5.5 feet 11 /04/2023 Sodium EPA200.7, Rev4.4, 1994 6.46 mg/L 11/16/2023 Sulfate EPA 300.0, Rev. 2.1, 1993 59 mg/L 11/07/2023 Ammonia Nitrogen EPA 350.1, Rev. 2.0, 1993 < 0.2 mg/L 11/07/2023 Gallons bailed before sampling Gallons Balled before sampling 5.0 gallons 11 /04/2023 Odor Qualitative None 11 /04/2023 Total Dissolved Solids (TDS) SM 2540 c-2015 121 mg/L 11 /06/2023 Temperature SM 2550 B-2010 21.5 C 11 /04/2023 pH SM 4500 H B-2011 5.2 units 11/04/2023 Total Phosphorus SM 4500 P (F-H)-2011 < 0.04 mg/L 11/10/2023 Total Organic Carbon (TOC) SM 5310 8-2014 1.1 mg/L 11/06/2023 Fecal Coliform SM 9222 D-2015 MF <1 Colonies/100ml- 11/04/2023 Chloride SM4500 Cl E-2011 7 mg/L 11/08/2023 1, 1, 1,2-Tetrachloroethane SW 846 Method 8280D/5030B <0.5 µg/L 11/09/2023 1,1,1-Trichloroethane SW846Method 8260D15030B <0.5µg/L 11/09/2023 1,1,2,2-Tetrachloroethane SW 846 Method 826013/50308 <0.6 pg/L 11/09/2023 1,1,2-Trichloroethane SW 846 Method 8250D/5030B <0.5 µg/L 11/09/2023 1,1-Dichloroethane SW 846 Method 8260D/5030B <0.5 µg/L 11/09/2023 1,1-Dichloroethene SW80Method 8260D/5030B <0,5µg/L 11/09/2023 1,1-Dichloropropene SW 846 Method 8280D/5030B <0.5 µg/L 11/09/2023 1,2,3-Tdchlorobenzene SW 846 Method 8280D/5030B <0.5 µg/L 11/09/2023 1,2,3-Trichloropropane SW 846 Method 8260D15030B <0.5 µg/L 11/09/2023 1,2,4-Trichlorobenzene SW 846 Method 6260D/5030B <0,5 µg/L 11/09/2023 1,2,4-Trimethylbenzene SW US Method 8260D/5030B <0.5 µg/L 11/09/2023 1,2-Dibromo-3-Chloropropane SW 846 Method 8280D/5030B <1 µg/L 11/09/2023 Report #.: 2023-25531 Page 1 of 33 Environmental Chemists, Inc. roo". envirochem j 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax sW 255-A Wilmington Highway, Jacksonville, NC 28540 a 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS info@environmentalchemists.com Darling Ingredients - Rose Hill Post Office Box 1026 Rose Hill NC 28458 Attention: Date of Report: Dec 13, 2023 Customer PO #: Customer ID: 08100027 Report #: 2023-25631 Project ID: Monitoring Wells 1,2-Dibromoethane SW 80 Method 826oD/5030B <0.5 µg/L 11/09/2023 1,2-Dichlorobenzene SW 846 Method 826013/50306 <0.5 µg/L 11/09/2023 1,2-Dichloroethane SW 846 Method 826oD/5030B <0.5 µg/L 11/09/2023 1,2-Dichloropropane SW 846 Method 6260D/5030B <0.5 µg/L 11/09/2023 1,3,5-Tdmethylbenzene SIN 845Method 8280D/5030B <0.5µg/L 11/09/2023 1,3-Dichlorobenzene SW Na Method 828oD/5030B <0.5 µg/L 11/09/2023 1,3-Dichloropropane SW 846 Method 8260D/5030B <0.5 µg/L 11/09/2023 1,4-Dichlorobenzene SW 848 Method 8260D15030B <0.5 µg/L 11/09/2023 2,2-Dichloropropane SW 848 Method 8260D/5030B <0.5 µg/L 11/09/2023 ,)-Chlorotoluene SW 848 Method 8260D/50308 <0.5 µg/L 11/09/2023 4-Chlorotoluene SW 846 Method 8260D15030B <0.5 µg/L 11/09/2023 Benzene SW 848 Method 8280D/5030B <0.5 µg/L 11/09/2023 Bromobenzene SW 846 Method 826013/50306 <0.5 µg/L 11/09/2023 Bromochloromethane SW 80 Method 8280D/5030B <0.5 µg/L 11/09/2023 Bromodichloromethane SW 846 Method 8260D/5030B <0.5 µg/L 11/09/2023 Bromoform SW So Method 8260D/5030B <0.5 µg/L 11/09/2023 Bromomethane SW 846 Method 8280D/5030B <0.5 µg/L 11/09/2023 Carbon tetrachloride SW So Method 8280D/5030B <0.5 µg/L 11/09/2023 Chlorobenzene SW 846 Method 8260D/5030B <0.5 µg/L 11/09/2023 Chloroethane SW 80 Method 8280D/5030B <0,5 µg/L 11/09/2023 Chloroform SW 80 Method 82e00/5030B <0.5 µg/L 11/09/2023 Chloromethane SW 846 Method 8280D16030B <0.5 µg/L 11/09/2023 cis-1,2-Dichloroethene SW 80 Method 8260D/5030B <0.5 µg/L 11/09/2023 cis-1,3-Dichloropropene SW 848 Method 8260D/5030B <0.5 µg/L 11/09/2023 Dibromochloromethane SW 846 Method 828013/50308 <0.5 µg/L 11/09/2023 Dibromomethane SW N6 Method 9280D/5030B <0,5 pg/L 11/09/2023 Dichlorodifluoromethane SW m6 Method 8280D/5030B <0.5 µg/L 11/09/2023 _ ':thylbenzene SW 846 Method 8280D/50308 <0.5 µg/L 11 /09/2023 Hexachlorobutadiene SW 80 Method 826013/503013 <0.5 µg/L 11/09/2023 Isopropylbenzene SW 846 Method 8260D/5030B <0.5 µg/L 11/09/2023 Report k 2023-25631 Page 2 of 33 ro"� -- 7 Environmental Chemists, Inc. envirochem 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Sowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax sa. 255-A Wilmington Highway, Jacksonville, NC 28540 a 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS info@environmentalchemists.com Darling Ingredients - Rose Hill Post Office Box 1026 Rose Hill NC 28458 Attention: Date of Report: Dec 13, 2023 Customer PO #: Customer ID: 08100027 Report #: 2023-25631 Project ID: Monitoring Wells M+P Xylene SW 846 Method 8260D/5030B <1.0 pg/L 11/09/2023 Methylene chloride SW 80 Method 8280D/5030B <0.5 pg/L 11/09/2023 Naphthalene SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2023 n-Butylbenzene SW 846 Method 826OD15030B <0.5 pg/L 11/09/2023 n-Propylbenzene SW 846 Method SM13/503013 <0.5 pg/L 11/09/2023 ortho-Xylene SW 846 Method 8280D/50308 <0.5 pg/L 11/09/2023 p-Isopropyltoluene SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2023 sec-Butylbenzene SW 846 Method 826aD/50309 <0.5 pg/L 11/09/2023 Styrene SW 846 Method 8260D15030B <0.5 pg/L 11/09/2023 `ert-Butylbenzene SW 80 Method 8260DI5030B <0.5 pg/L 11/09/2023 Tetrachloroethene SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2023 Toluene SW 846 Method 8260D/50308 <0.5 pg/L 11/09/2023 Trans-1,2-Dichloroethene SW 646 Method 826OD15030B <0.5 pg/L 11/09/2023 Trans-1,3-dichloropropene SW Me Method 8260D/5030B <0.5 pg/L 11/09/2023 Trichloroethene SW 846 Method 82BOD15030B <0.5 pg/L 11/09/2023 Trichlorofluoromethane SW 846 Method MOD15030B <0.5 pg/L 11/09/2023 Vinyl chloride SW 846 Method 828oD/5030B <0.5 pg/L 11/09/2023 Nitrate Nitrogen (Calc) Nitrite Nitrogen EPA 353.2, Rev. 2.0, 1993 < 0.02 mg/L 11 /06/2023 Nitrate+Nitrite-Nitrogen EPA 353.2, Rev.2.0,1993 0.43 mg/L 11/08/2023 Nitrate Nitrogen Subtraction Method 0.43 mg/L 12/12/2023 Total Nitrogen (Calc) Total Kjeldahl Nitrogen (TKN) EPA 351.2, Rev. 2.0, 1993 < 0.5 mg/L 11 /10/2023 Total Nitrogen Total Nitrogen <0.5 mg/L 12/12/2023 Report ff:: 2023-25831 Page 3 of 33 747 Environmental Chemists, Inc. envirochem J 6602 Windmill Way, Wilmington, NC 28405 a 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax sM) 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 L.ab/Fax ANALYTICAL & CONSULTING CHEMISTS info@environmentalchemists.com Darling Ingredients - Rose Hill Date of Report: Dec 13, 2023 Post Office Box 1026 Customer PO #: Rose Hill NC 28458 Customer ID: 08100027 Attention: Report #: 2023-25631 Project ID: Monitoring Wells Lab ID Sample ID: Collect Date/Time Matrix Sampled by 23-62088 Site: MW-2 11/4/2023 11:05 AM Water jcb/envirochem Test Method Results Date Analyzed Color color Tan/Clear 11 /04/2023 Depth to water, ft. Depth to Water, Ft. 12.8 feet 11 /04/2023 Sodium EPA 200.7, Rev 4A, 1994 11.2mg/L 11/16/2023 Sulfate EPA300.0, Rev. 2.1, 1993 27 mg/L 11/07/2023 Ammonia Nitrogen EPA 350.1, Rev. 2.0, 1993 < 0.2 mg/L 11/07/2023 Gallons bailed before sampling Gallons Bailed before sampling 5.0 gallons 11/04/2023 Jdor Qualitative None 11 /04/2023 Total Dissolved Solids (TDS) SM 2540 C-2015 292 mg/L 11/06/2023 Temperature SM 2550 &2010 18.6 C 11 /04/2023 pH SM 4500 H B-2011 6.7 units 11/04/2023 Total Phosphorus SM 4500 P (F-H)-2011 < 0.04 mg/L 11 /10/2023 Total Organic Carbon (TOC) SM 5310 &2014 1.1 mg/L 11/06/2023 Fecal Coliform SM 9222 D-2015 MF <1 Colonies/100ml- 11 /04/2023 Chloride SM4500 Cl E-2011 13 mg/L 11/08/2023 1,1,1,2-Tetrachioroethane SW 848 Method 82800/50308 <0.5 pg/L 11 /09/2023 1, 1, 1 -Trichloroethane SW846Method 8280D/5030B <0,5pg/L 11/09/2023 1,1,2,2-Tetrachioroethane SW 846 Method 8280DI5030B <0.5 pg/L 11/09/2023 1,1,2-Tdchloroethane SW 846 Method 8260D/50308 <0.5 pg/L 11/09/2023 1,1-Dichloroethane SW 80 Method 8280D/50308 <0.5 pg/L 11 /09/2023 1,1-Dichloroethene SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2023 1,1-Dichloropropene SW 846 Method 8280D/5030B <0.5 pg/L 11/09/2023 1,2,3-Trichlorobenzene SW 846 Method 828OD15030B <0.5 pg/L 11/09/2023 1,2,3-Trichloropropane SW 846 Method 826OD15030B <0.5 pg/L 11/09/2023 1,2,4-Tdchlorobenzene SW 848 Method 8260D/5030B <0.5 pg/L 11/09/2023 -1 ,2,4-Tdmethylbenzene SW 846 Method 8280DI5030B <0.5 pg/L 11/09/2023 1,2-Dibromo-3-Chloropropane SW 848 Method 8280DI5030B <1 pg/L 11/09/2023 Report #:: 2023-25831 Page 4 of 33 7:,07 Environmental Chemists, Inc. envirochem 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab o 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax V 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS info@environmentalchemists.com Darling Ingredients - Rose Hill Post Office Box 1026 Rose Hill NC 28458 Attention: Date of Report: Dec 13, 2023 Customer PO #: Customer ID: 08100027 Report All: 2023-25631 Project ID: Monitoring Wells 1,2-Dibromoethane SW 848 Method 82BOD15030B <0.5 µg/L 11/09/2023 1,2-Dichlorobenzene SW 848 Method 8260D15030B <0.5 µg/L 11/09/2023 1,2-Dichloroethane SW 848 Method 826013/503013 <0.5 µg/L 11/09/2023 1,2-Dichloropropane SW 048 Method 82BOD/50308 <0.5 µg/L 11/09/2023 1,3,5-Trimethylbenzene SW 848 Method 8280D/50308 <0.5 µg/L 11/09/2023 1,3-Dichlorobenzene SW 846 Method 82BOD15030B <0.5 µg/L 11/09/2023 1,3-Dichloropropane SW 846 Method 8NOD150308 <0.5 µg/L 11/09/2023 1,4-Dichlorobenzene SW 846 Method 82GOD15030B <0.5 µg/L 11/09/2023 2,2-Dichloropropane SW W Method 8260D/5030B <0.5 µg/L 11/09/2023 ?-Chlorotoluene SW 845 Method 8280D/5030B <0.5 µg/L 11/09/2023 4-Chlorotoluene SW 848 Method 6260D/50306 <0.5 µg/L 11/09/2023 Benzene SW 846 Method B28ODI503013 <0.5 µg/L 11/09/2023 Bromobenzene SW 846 Method 826013/50308 <0.5 µg/L 11/09/2023 Bromochioromethane SW 848 Method 8260D/50308 <0.5 µg/L 11/09/2023 Bromodichloromethane SW 846 Method 82ND15030B <0.5 µg/L 11/09/2023 Bromoform SW 846 Method 826OD/5030B <0.5 µg/L 11/09/2023 Bromomethane SW 846 Method 82BOD/50308 <0.5 µg/L 11/09/2023 Carbon tetrachloride SW 846 Method 826aD/5030B <0.5 µg/L 11/09/2023 Chlorobenzene SW 846 Method 8260D15030B <0.5 µg/L 11/09/2023 Chloroethane SW 80 Method 82BOD/5030B <0.5 µg/L 11/09/2023 Chloroform SW 846 Method 8260D/50308 <0.5 µg/L 11/09/2023 Chloromethane SW 846 Method 82BOD/50308 <0.5 µg/L 11/09/2023 cis-1,2-Dichloroethene SW 846 Method 82501)/503013 <0.5 µg/L 11/09/2023 cis-1,3-Dichloropropene SW 846 Method 8260D/50308 <0.5 µg/L 11/09/2023 Dibromochloromethane SW 80 Method 8260DI5030B <0.5 µg/L 11/09/2023 Dibromomethane SW N6 Method 8260DI50308 <0.5 µg/L 11/09/2023 Dichlorodifluoromethane SW 846 Method 82BOD/50308 <0.5 µg/L 11/09/2023 `thylbenzene SW 846 Method 6260D/50308 <0.5 µg/L 11/09/2023 Hexachlorobutadiene SW 848 Method 8260DIS030B <0.5 µg/L 11/09/2023 Isopropylbenzene SW 846 Method 825013/50306 <0.5 µg/L 11/09/2023 Report #:: 2023-25631 Page 5 of 33 -77 ro"7 SM' ANALYTICAL & CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 a 910.347.5843 Lab/Fax info@environmentalchemists.com Darling Ingredients - Rose Hill Date of Report: Dec 13, 2023 Post Office Box 1026 Customer PO #: Rose Hill NC 28458 Customer ID: 08100027 Attention: Report #: 2023-25631 Project ID: Monitoring Wells M+P Xylene SW 848 Method 8260DI5030B <1.0 pg/L 11/09/2023 Methylene chloride SW 846 Method 8260D15030B <0.5 pg/L 11/09/2023 Naphthalene SW 846 Method 8260D/50308 <0.5 pg/L 11/09/2023 n-Butylbenzene SW B46 Method 826013/503013 <0.5 pg/L 11/09/2023 n-Propylbenzene SW 848 Method 8260D/5030B <0.5 pg/L 11/09/2023 ortho-Xylene SW 846 Method 82BOD/5030B <0.5 pg/L 11/09/2023 p-Isopropyltoluene SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2023 sec-Butylbenzene SW 846 Method 8280D/503013 <0.5 pg/L 11/09/2023 Styrene SW 846 Method B280D/503013 <0.5 pg/L 11/09/2023 'tert-Butylbenzene SW 846 Method 8260D/50306 <0.5 pg/L 11/09/2023 Tetrachloroethene SW 846 Method 028013/50308 <0.5 pg/L 11/09/2023 Toluene SW 848 Method 8280D/50306 <0.5 pg/L 11/09/2023 Trans-1,2-Dichloroethene SW 846 Method 826013/503013 <0.5 pg/L 11/09/2023 Trans-1,3-dichloropropene SW 848 Method 828oD/5030B <0.5 pg/L 11/09/2023 Trichloroethene SW 84B Method 826OD15030B <0.5 pg/L 11/09/2023 Trichlorofluoromethane SW B48 Method 82BOD15030B <0.5 ug/L 11/09/2023 Vinyl chloride SW 846 Method 82BOD/5030B <0.5 pg/L 11/09/2023 Nitrate Nitrogen (Cale) Nitrite Nitrogen EPA 353.2, Rev. 2.0, 1993 < 0.02 mg/L 11/06/2023 Nitrate+Nitrite-Nitrogen EPA 353.2, Rev. 2.0, 1993 0.17 mg/L 11 /08/2023 Nitrate Nitrogen Subtraction Method 0.17 mg/L 12/12/2023 Total Nitrogen (Cale) Total Kjeldahl Nitrogen (TKN) EPA 351.2, Rev. 2.0, 1993 < 0.5 mg/L 11/10/2023 Total Nitrogen Total Nitrogen <0.5 mg/L 12/12/2023 Report#:: 2023-25631 Page 8 of 33 F""OP7 -.-qq7 SMi ANALYTICAL S CONSULTING CHEMISTS Darling Ingredients - Rose Hill Post Office Box 1026 Rose Hill NC 28458 Attention: Lab ID Sample ID: 23-62089 Site: MW-4 Test Color Depth to water, ft. Sodium Sulfate Ammonia Nitrogen ,Gallons bailed before sampling Odor Total Dissolved Solids (TDS) Temperature pH Total Phosphorus Total Organic Carbon (TOC) Fecal Coliform Chloride 1. 1, 1,2-Tetrachloroethane 1,1,1-Trichloroethane 1,1,2,2-Tetrachloroethane 1,1,2-Trichloroethane 1,1-Dichloroethane 1,1-Dichloroethene 1,1-Dichloropropene 1,2,3-Trichlorobenzene 1,2,3-Trichloropropane !„2,4-Trichlorobenzene 1,2,4-Trimethylbenzene 1,2-Dibromo-3-Chloropropane Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473,5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax info@environmentalchemists.com Date of Report: Dec 13, 2023 Customer PO #: Customer ID: 08100027 Report #: 2023-25631 Project ID: Monitoring Wells Collect Date/Time Matrix Sampled by 11/4/2023 10:30 AM Water jcb/envirochem Method Color Depth to Water, Ft EPA 200.7, Rev 4.4, 1994 EPA 300.0, Rev. 2.1, 1993 EPA 350.1, Rev. 2.0. 1993 Gallons Bailed before sampling Qualitative SM 2640 C-2015 SM 2550 B-2010 SM 4500 H B-2011 SM 4500 P (F-H)-2011 SM 5310 B-2014 SM 9222 D-2015 MF SM4500 Cl E-2011 SW 846 Method 8280D/5030B SW 846 Method 8260D/5030B SW 846 Method 8280DI5030B SW 646 Method 6280DIS030B SW 846 Method 8260DI50308 SW 846 Method 626OD15030B SW 846 Method 8280D/5030B SW 846 Method 8260D/5030B SW 846 Method 826013/503013 SW 846 Method 8260D/50308 SW 846 Method 8260D/5030B SW 846 Method 8280D/5030B Results Date Analyzed Clearrran 11/04/2023 6.4 feet 11 /04/2023 8.25 mg/L 11/16/2023 <5 mg/L 11/07/2023 < 0.2 mg/L 11 /07/2023 5.0gallons 11/04/2023 None 11/04/2023 211 mg/L 11/06/2023 19.9 C 11/04/2023 7.0 units 11/04/2023 < 0.04 mg/L 11/10/2023 1.1 mg/L 11/06/2023 <1 Colonies/100ml- 11/0412023 < 5 mg/L 11/08/2023 <0.5 pg/L 11/09/2023 <0.5 pg/L 11/09/2023 <0.5 pg/L 11/09/2023 <0.5 pg/L 11/09/2023 <0.5 pg/L 11/09/2023 <0.5 pg/L 11/09/2023 <0.5 pg1L 11/09/2023 <0.5 pg/L 11/09/2023 <0.5 pg/L 11/09/2023 <0.5 pg/L 11/09/2023 <0.5 pg/L 11/09/2023 <1 pg/L 11/09/2023 Report #.: 2023.25631 Page 7 of 33 -- - -1'"7 Environmental Chemists, Inc. envirochem i6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax sM 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS info(aenvironmentalchemists.com Darling Ingredients - Rose Hill Date of Report: Dec 13, 2023 Post Office Box 1026 Customer PO #: Rose Hill NC 28458 Customer ID: 08100027 Attention: Report #: 2023-25631 Project 1D: Monitoring Wells 1,2-Dibromoethane SW 846 Method 826oD/5030e <0.5 µg/L 11/09/2023 1,2-Dichlorobenzene SW 846 Method 8260D/5030B <0.5 µg/L 11/09/2023 1,2-Dichloroethane SW M6 Method 8260D15030B <0.5 µg/L 11/09/2023 1,2-Dichloropropane SW 846 Method 8260D/5030B <0.5 µg/L 11/09/2023 1,3,5-Trimethylbenzene SW 848 Method 8260D15030B <0.5 µg/L 11/09/2023 1,3-Dichlorobenzene SW 846 Method 8260D/5030B <0.5 µg/L 11/09/2023 1,3-Dichloropropane SW US Method 8260D/5030B <0.5 µg/L 11/09/2023 1,4-Dichlorobenzene SW 846 Method 826013/50306 <0.5 µg/L 11/09/2023 2,2-Dichloropropane SW 846 Method 826aD/5030B <0.5 µg/L 11/09/2023 ?-Chlorotoluene SW 846 Method 8260D/5030B <0.5 µg/L 11/09/2023 4-Chlorotoluene SW 846 Method 8260D/5030B <0.5 µg/L 11/09/2023 Benzene SW 846 Method 828OD15030B <0.5 pg/L 11/09/2023 Bromobenzene SW 848 Method 826013/50306 <0.5 µg/L 11/09/2023 Bromochloromethane SW 846 Method 82600/5030B <0.5 µg/L 11/09/2023 Bromodichloromethane SW 846 Method 8260D/5030B <0.5 µg/L 11/09/2023 Bromoform SW 846 Method 8260D/5030B <0.5 µg/L 11/09/2023 Bromomethane SW 846 Method 826oD/5030B <0.5 µg/L 11/09/2023 Carbon tetrachloride SW 846 Method 826oD/5030B <0.5 µg/L 11/09/2023 Chlorobenzene SW 846 Method 8280D/5030B <0.5 µg/L 11/09/2023 Chloroethane SW 846 Method 8260D/5030B <0.5 µg/L 11/09/2023 Chloroform SW 8" Method 828013/5030B <0.5 µg/L 11/09/2023 Chloromethane SW 846 Method 8260D/5030B <0.5 µg/L 11/09/2023 cis-1,2-Dichloroethene SW 846 Method 8260D/5030B <0.5 µg/L 11/09/2023 cis-1,3-Dichloropropene SW 846 Method 82800/50309 <0.5 µg/L 11/09/2023 Dibromochloromethane SW 846 Method 8260D/5030B <0.5 µg/L 11/09/2023 Dibromomethane SW 846 Method 826013/5030B <0.5 µg/L 11/09/2023 Dichlorodifluoromethane SW 646 Method 826DD/5030B <0.5 µg/L 11/09/2023 ,cthylbenzene SW 846 Method 8260D►50308 <0.5 µg/L 11/09/2023 Hexachlorobutadiene SW 846 Method 826oD/5030B <0.5 µg/L 11/09/2023 Isopropylbenzene SW 846 Method 826013/50308 <0.5 µg/L 11/09/2023 Report t: 2023-26831 Page 8 of 33 F"I", -- —, -MM7 Environmental Chemists, Inc. envirochem 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 a 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 - 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS infoCenvironmentalchemists.com Darling Ingredients - Rose Hill Post Office Box 1026 Rose Hill NC 28458 Attention: Date of Report: Dec 13, 2023 Customer PO #: Customer ID: 08100027 Report #: 2023-25631 Project ID: Monitoring Wells M+P Xylene SW 846 Method 826DD/5030B <1.0 pg/L 11/09/2023 Methylene chloride SW 80 Method 8280D/503013 <0.5 pg/L 11/09/2023 Naphthalene SW 846 Method 8260D150308 <0.5 pg/L 11/09/2023 n-Butylbenzene SW 846 Method 826oD/5030B <0.5 pg/L 11/09/2023 n-Propylbenzene SW 846 Method 82600/50308 <0.5 pg/L 11/09/2023 ortho-Xylene SW 846 Method 826013/503013 <0.5 pg/L 11/09/2023 p-Isopropyltoluene SW 840 Method 826DD/5030B <0.5 pg/L 11/09/2023 sec-Butylbenzene SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2023 Styrene SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2023 ,,ert Butylbenzene SW 80 Method 826013/50308 <0.5 pg/L 11/09/2023 Tetrachloroethene SW 50 Method 826013/503013 <0.5 pg/L 11/09/2023 Toluene SW 846 Method 826013/50308 <0.5 pg/L 11/09/2023 Trans-1,2-Dichloroethene SW 845 Method 828013/50308 <0.5 pg/L 11/09/2023 Trans-1,3-dichloropropene SW 846 Method 8280D/5030B <0.5 pg/L 11/09/2023 Tdchloroethene SW 846 Method 826oD/50308 <0.5 pg/L 11/09/2023 Tdchlorofluoromethane SW 846 Method 8280D/5030B <0.5 pg/L 11/09/2023 Vinyl chloride SW 846 Method 826013/503013 <0.5 pg/L 11/09/2023 Nitrate Nitrogen (Calc) Nitrite Nitrogen EPA 353.2. Rev. 2.0, 1993 < 0.02 mg/L 11 /06/2023 Nitrate+Nitrite-Nitrogen EPA 353.2, Rev. 2.0,1993 < 0.02 mg/L 11/08/2023 Nitrate Nitrogen Subtraction Method <0.02 mg/L 12/12/2023 Total Nitrogen (Calc) Total Kjeldahl Nitrogen (TKN) EPA 351.2, Rev. 2.0,1993 < 0.5 mg/L 11 /10/2023 Total Nitrogen Total Nitrogen <0.5 mg/L 12/12/2023 Reportt: 2023-25831 Page 9 of 33 r"007 envirochem I —.01111111 ANALYTICAL & CONSULTING CHEMISTS Darling Ingredients - Rose Hill Post Office Box 1026 Rose Hill NC 28458 Attention: Lab ID Sample ID: 23-62090 Site: MW-7A Test Color Depth to water, ft. Sodium Sulfate Ammonia Nitrogen Gallons bailed before sampling Odor Total Dissolved Solids (TDS) Temperature pH Total Phosphorus Total Organic Carbon (TOC) Fecal Coliform Chloride 1,1,1,2-Tetrach loroetha n e 1,1,1-Tdchloroethane 1,1,2,2-Tetrachloroethane 1,1,2-Tdchloroethane 1, 1 -Dichloroethane 1,1-Dichloroethene 1,1-Dichloropropene 1,2,3-Trichlorobenzene 1,2, 3-Tdchloropropane 1,2,4-Tdchlorobenzene 1,2,4-Trimethylbenzene 1,2-Dibromo-3-Chloropropane Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 - 910.392.0223 Lab - 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 - 910.347.5843 Lab/Fax info@environmentalchemists.com Date of Report: Dec 13, 2023 Customer PO #: Customer ID: 08100027 Report #: 2023-25631 Project ID: Monitoring Wells Collect Date/Time Matrix Sampled by 11/4/2023 12:15 PM Water jcb/envirochem Method Color Depth to Water, Ft. EPA 200.7, Rev 4.4,1994 EPA 300.0, Rev. 2.1, 1993 EPA350.1, Rev.2.0.1993 Gallons Bailed before sampling Qualitative SM 2540 C-2015 SM 2550 B-2010 SM 4500 H B-2011 SM 4500 P (F-H)-2011 SM 5310 B-2014 SM 9222 D-2015 MF SM4500 Cl E-2011 SW 846 Method 8260DIS030B SW 846 Method 8260D/5030B SW 846 Method 825013/503013 SW 50 Method 8266D/5030B SW 80 Method 6280DI5030B SW 846 Method 826013/5030B SW 846 Method 825013/50306 SW 846 Method 8280DI5030B SW 846 Method 826OD15030B SW 846 Method 8260D/5030B SW 846 Method 8280D15030B SW 846 Method 828oD/5030B Results Date Analyzed Tan/Clear 11/04/2023 6.0 feet 11/04/2023 12.3 mg/L 11/16/2023 23 mg/L 11 /07/2023 < 0.2 mg/L 11/07/2023 5.0gallons 11/04/2023 None 11/04/2023 264 mg/L 11/06/2023 20.9 C 11/04/2023 3.66est. units 11/04/2023 < 0.04 mg/L 11 /10/2023 1.0 mg/L 11/06/2023 <1 Colonies/100mL 11/04/2023 128 mg/L 11 /08/2023 <0.5 pg/L 11 /0912023 <0.5 pg/L 11/09/2023 <0.5 pg/L 11/09/2023 <0.5 pg/L 11/09/2023 <0.5 pg/L 11/09/2023 <0.5 pg/L 11/09/2023 <0.5 pg/L 11/09/2023 <0.5 pg/L 11/09/2023 <0.5 pg/L 11/09/2023 <0.5 pg/L 11/09/2023 <0.5 pg/L 11/09/2023 <1 pg/L 11/09/2023 Report #: 2023-25631 Page 10 of 33 SM ANALYTICAL & CONSULTING CHEMISTS Darling Ingredients - Rose Hill Post Office Box 1026 Rose Hill NC 28458 Attention: Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910,392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax info@environmentalchemists.com Date of Report: Dec 13, 2023 Customer PO 0: Customer ID: 08100027 Report #: 2023-25631 Project ID: Monitoring Wells 1,2-Dibromoethane SW 846 Method 8280DI5030B <0.5 pg/L 11/09/2023 1,2-Dichlorobenzene SW 846 Method 826OD/5030B <0.5 pg/L 11/09/2023 1,2-Dichloroethane SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2023 1,2-Dichloropropane SW 846 Method 828013/5030B <0.5 pg/L 11/09/2023 1,3,5-Tdmethylbenzene SW 846 Method 82BOD15030B <0.5 pg/L 11/09/2023 1,3-Dichlorobenzene SW 840 Method 82BOD/5030B <0.5 pg/L 11/09/2023 1,3-Dichloropropane SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2023 1,4-Dichlorobenzene SW 846 Method 8280D15030B <0.5 pg/L 11/09/2023 2,2-Dichloropropane SW 846 Method 8260D/50306 <0.5 pg/L 11/09/2023 �-Chlorotoluene SW 848 Method 8260D/5030B <0.5 pg/L 11/09/2023 4-Chlorotoluene SW 846 Method 82GOD/5030B <0.5 pg/L 11/09/2023 Benzene SW e46 Method 82GOD/5030B <0.5 pg/L 11/09/2023 Bromobenzene SW 846 Method MOD/50308 <0.5 pg/L 11/09/2023 Bromochloromethane SW 646 Method 82BOD/8030B <0.5 pg/L 11/09/2023 Bromodichloromethane SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2023 Bromoform SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2023 Bromomethane SW 846 Method 8260D15030B <0.5 pg/L 11/09/2023 Carbon tetrachloride SW 045 Method 8260D15030B <0.5 pg/L 11/09/2023 Chlorobenzene SW 646 Method 82BOD/5030B <0.5 pg/L 11/09/2023 Chloroethane SW US Method 8280D/5030B <0.5 pg/L 11/09/2023 Chloroform SW 846 Method 8280D/5030B <0.5 pg/L 11/09/2023 Chloromethane SW 846 Method 826013/50308 <0.5 pg/L 11/09/2023 cis-1,2-Dichloroethene SW 846 Method 82600150308 <0.5 pg/L 11/09/2023 cis-1,3-Dichloropropene SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2023 Dibromochloromethane SW 846 Method 6200DI5030B <0.5 pg/L 11/09/2023 Dibromomethane SW 646 Method 8260DI5030B <0.5 pg/L 11/09/2023 Dichlorodifluoromethane SW 846 Method 6260D/5030B <0.5 pg/L 11/09/2023 ,; zthylbenzene SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2023 Hexachlorobutadiene SW e46 Method 820OD/5030B <0.5 pg/L 11/09/2023 Isopropylbenzene SW 846 Method 82GOD15030B <0.5 pg/L 11/09/2023 Report *: 2023-25831 Page 11 of 33 ANALYTICAL & CONSULTING CHEMISTS Darling Ingredients - Rose Hill Post Office Box 1026 Rose Hill NC 28458 Attention_ Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910,392.0223 Lab a 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 0 910.347.5843 Lab/Fax info@environmentalchemists.com Date of Report: Dec 13, 2023 Customer PO #: Customer ID: 08100027 Report #: 2023-25631 Project ID: Monitoring Wells M+P Xylene SW 64B Method 8260D/5030B <1,0 pg/L 11/09/2023 Methylene chloride SW 64e Method 82BOD/50308 <0.5 pg/L 11/09/2023 Naphthalene SW NO Method 8260DIS030B <0.5 pg/L 11/09/2023 n-Butylbenzene SW 80 Method 8260D/5030B <0.5 pg/L 11/09/2023 n-Propylbenzene SW W Method 8260DI5030B <0.5 pg/L 11/09/2023 ortho-Xylene SW Me Method e26OD/5030B <0.5 pg/L 11/09/2023 p-Isopropyltoluene SW 848 Method 828OD/5030B <0.5 pg/L 11/09/2023 sec-Butylbenzene SW 846 Method 828ODI5030B <0.5 pg/L 11/09/2023 Styrene SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2023 ,ert Butylbenzene SW 816 Method 628013I503O13 <0.5 pg/L 11/09/2023 Tetrachloroethene SW ate Method 0260DISOSOB <0.5 pg/L 11/09/2023 Toluene SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2023 Trans-1,2-Dichloroethene SW 846 Method 8260D/5030B <0.5 pg/L 11 /09/2023 Trans-1,3-dichloropropene SW 84B Method MOD15030B <0.5 pg/L 11/09/2023 Trichloroethene SW 846 Method 8260DIS0308 <0.5 pg/L 11/09/2023 Trichlorofluoromethane SW 84B Method 82BOD/5030B <0.5 pg/L 11/09/2023 Vinyl chloride SW 80 Method 826OD/5030B <0.5 pg/L 11/09/2023 Nitrate Nitrogen (Cale) Nitrite Nitrogen EPA 353.2, Rev. 2.0,1993 < 0.02 mg/L 11/06/2023 Nitrate+Nitrite-Nitrogen EPA 353.2, Rev. 2.0,1993 < 0.02 mg/L 11/08/2023 Nitrate Nitrogen Subtraction Method <0.02 mg/L 12/12/2023 Total Nitrogen (Cale) Total Kjeldahl Nitrogen (TKN) EPA 351.2, Rev. 2.0,1993 < 0.5 mg/L 11/10/2023 Total Nitrogen Total Nitrogen <0.5 mg/L 12/12/2023 Reportk 2023-25631 Page 12 of 33 envirochem SM ANALYTICAL & CONSULTING CHEMISTS F ---71 F07 Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 0 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax info Cenvi ronmentalchemists.com Darling Ingredients - Rose Hill Date of Report: Dec 13, 2023 Post Office Box 1026 Customer PO #: Rose Hill NC 28458 Customer ID: 08100027 Attention: Report #: 2023-25631 Project ID: Monitoring Wells Lab ID Sample ID: Collect Date/Time Matrix Sampled by 23-62091 Site: MW-8A 11/4/2023 12:30 PM Water jcb/envirochem Test Method Results Date Analyzed Color color Tan/Clear 11/04/2023 Depth to water, ft. Depth to Water, Ft 7.0 feet 11/04/2023 Sodium EPA200.7, Rev 4A.1904 1.41 mg/L 11/16/2023 Sulfate EPA 300.0, Rev. 2.1,1993 23 mg/L 11 /07/2023 Ammonia Nitrogen EPA 350.1, Rev. 2.0.1993 < 0.2 mg/L 11/07/2023 .Gallons bailed before sampling Gallons Bailed before sampling 5.0 gallons 11/04/2023 Odor Qualitative None 11/04/2023 Total Dissolved Solids (TDS) SM 2540 C-2015 54 mg/L 11/06/2023 Temperature SM 2550 B-2010 21.2 C 11/04/2023 pH SM 4600 H B-2011 4.6 units 11/04/2023 Total Phosphorus SM 4500 P (F-H}2011 0.10 mg/L 11 /10/2023 Total Organic Carbon (TOC) SM 5310 B-2014 0.9 mg/L 11/06/2023 Fecal Coliform SM 0222 D-2015 MF <1 Colonies/100ml- 11/04/2023 Chloride SM4500 Cl E-2011 < 5 mg/L 11/08/2023 1, 1, 1,2-Tetrachloroethane SW 846 Method8280D/5030B <0.5pg/L 11/09/2023 1,11-Trichloroethane SW 846 Method8260D/5030B <0.5pg/L 11/09/2023 1,1,2,2-Tetrachloroethane SW 846 Method82NDI5030B <0.5pg/L 11/09/2023 1,1,2-Trichloroethane SW 848 Method 8280D/50308 <0.5 pg/L 11/09/2023 1,1-Dichioroethane SW60Method 8280D/5030B <0.5pg/L 11/09/2023 1,1-Dichloroethene SW 846 Method 8260DI5030B <0.5 pg/L 11/09/2023 1,1-Dichloropropene SW 846 Method8260D/5030B <0.5ug/L 11/09/2023 1,2,3-Trichlorobenzene SW 840 Method 8280D/5030B <0.5 pg/L 11/09/2023 1,2,3-Trichloropropane SW 846 Method 8260D15030B <0.5 pg/L 11/09/2023 1,2,4-Trichlorobenzene SW 848 Method 82BOD15030B <0.5 pg/L 11/09/2023 1,2,4-Trimethylbenzene SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2023 1,2-Dibromo-3-Chloropropane SW 846 Method8260DI5030B <1 pg/L 11/09/2023 Report#:: 2023-25631 Page 13 of 33 v ANALYTICAL & CONSULTING CHEMISTS F""'- -- -71 Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax info@environmentalchemists.com Darling Ingredients - Rose Hill Date of Report: Dec 13, 2023 Post Office Box 1026 Customer PO #: Rose Hill NC 28458 Customer ID: 08100027 Attention: Report #: 2023-25631 Project ID: Monitoring Wells 1,2-Dibromoethane SW 846 Method 8260D/50308 <0.5 pg/L 11/09/2023 1,2-Dichlorobenzene SW 80 Method 82BOD/5030B <0.5 pg/L 11/09/2023 1,2-Dichloroethane SW 848 Method 8280DI5030B <0.5 pg/L 11/09/2023 1,2-Dichloropropane SW 846 Method 82BOD/5030B <0.5 pg/L 11/09/2023 1,3,5-Trimethylbenzene SW 846 Method 8260D/50308 <0.5 pg/L 11/09/2023 1,3-Dichlorobenzene SW 846 Method 826OD/5030B <0.5 pg/L 11/09/2023 1,3-Dichloropropane SW 848 Method 82BOD/5030B <0.5 pg/L 11/09/2023 1,4-Dichlorobenzene SW 846 Method 82BOD15030B <0.5 pg/L 11/09/2023 2,2-Dichloropropane SW 846 Method 6280D/50308 <0.5 pg/L 11/09/2023 72-Chlorotoluene SW 848 Method 82BOD150300 <0.5 pg/L 11/09/2023 4-Chlorotoluene SW 846 Method SMOD15030B <0.5 pg/L 11/09/2023 Benzene SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2023 Bromobenzene SW 846 Method 8260D/503DB <0.5 pg/L 11/09/2023 Bromochloromethane SW 846 Method 82BOD/50308 <0.5 pg/L 11/09/2023 Bromodichloromethane SW 846 Method 82BOD15030B <0.5 pg/L 11/09/2023 Bromoform SW 845 Method 8260D/5030B <0.5 pg/L 11/09/2023 Bromomethane SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2023 Carbon tetrachloride SW 646 Method 8260D/5030B <0.5 pg/L 11/09/2023 Chlorobenzene SW 846 Method 8260D/5030B <0.5 pg/L 11 /09/2023 Chloroethane SW 846 Method 82BOD/50308 <0.5 pg/L 11/09/2023 Chloroform SW NO Method 8260D/5030B <0.5 pg/L 11/09/2023 Chloromethane SW 646 Method 82BOD/5030B <0.5 pg/L 11/09/2023 cis-1,2-Dichloroethene SW 846 Method 82BOD15030B <0.5 pg/L 11/09/2023 cis-1,3-Dichloropropene SW 846 Method 82BOD/5030B <0.5 pg/L 11/09/2023 Dibromochloromethane SW 846 Method 82BOD/5030B <0.5 pg/L 11/09/2023 Dibromomethane SW 846 Method 82BOD/5030B <0.5 pg/L 11/09/2023 Dichlorodifluoromethane SW 845 Method 8280D/50308 <0.5 pg/L 11/09/2023 ,cthylbenzene SW 846 Method 8260D/50308 <0.5 pg/L 11/09/2023 Hexachlorobutadiene SW 846 Method 828OD/5030B <0.5 pg/L 11/09/2023 Isopropylbenzene SW 846 Method 8280DI5030B <0.5 pg/L 11/09/2023 Report*: 2023-25831 Page 14 of 33 F`0107— -71 Environmental Chemists, Inc. envirochem 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax (� 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS info@environmentalchemists.com Darling Ingredients - Rose Hill Post Office Box 1026 Rose Hill NC 28458 Attention: Date of Report: Dec 13, 2023 Customer PO M Customer ID: 08100027 Report M 2023-25631 Project ID: Monitoring Wells M+P Xylene SW 848 Method 8260DI50308 <1.0 µg/L 11/09/2023 Methylene chloride SW 846 Method 82BOD/5030B <0.5 µg/L 11/09/2023 Naphthalene SW 848 Method 826MI5030B <0.5 µg/L 11/09/2023 n-Butylbenzene SW 846 Method 8260D/5030B <0.5 µg/L 11/09/2023 n-Propylbenzene SW 50 Method 8280D/5030B <0.5 µg/L 11/09/2023 ortho-Xylene SW 846 Method 8260D/5030B <0.5 µg/L 11/09/2023 p4sopropyltoluene SW 846 Method 825OD15030B <0.5 µg/L 11/09/2023 sec-Butylbenzene SW 846 Method 828013/50306 <0.5 µg/L 11/09/2023 Styrene SW 848 Method 62MD/5030B <0.5 µg/L 11/09/2023 ,`ert-Butylbenzene SW Us Method 8260D/5030B <0.5 µg/L 11/09/2023 Tetrachloroethene SW 848 Method 8MOD15030B <0.5 µg/L 11/09/2023 Toluene SW 848 Method 8280D/5030B <0.5 µg/L 11/09/2023 Trans-1,2-Dichloroethene SW 846 Method 8260DI5030B <0,5 µg/L 11/09/2023 Trans-1,3-dichloropropene SW 848 Method 826013/503013 <0.5 µg/L 11/09/2023 Trichloroethene SW 846 Method 826oD/5030B <0,5 µg/L 11 /09/2023 Trichlorofluoromethane SW 846 Method 8260/50308 <0.5 µg/L 11/09/2023 Vinyl chloride SW 846 Method 828013/50306 <0.5 µg/L 11/09/2023 Nitrate Nitrogen (Calc) Nitrite Nitrogen EPA353.2, Rev. 2.0,1993 < 0.02 mg/L 11/06/2023 Nitrate+Nitrite-Nitrogen EPA 353.2. Rev. 2.0, 1993 0.39 mg/L 11/08/2023 Nitrate Nitrogen Subtraction Method 0.39 mg/L 12/12/2023 Total Nitrogen (Calc) Total Kjeldahl Nitrogen (TKN) EPA 351.2. Rev. 2.0,1993 < 0.5 mg/L 11/10/2023 Total Nitrogen Total Nitrogen <0.5 mg/L 12/12/2023 Report #:: 2023-25631 Page 15 of 33 r -77 o"17 envirochem sn+� ANALYTICAL r4 CONSULTING CHEMISTS Darling Ingredients - Rose Hill Post Office Box 1026 Rose Hill NC 28458 Attention: Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax info@environmentalchemists.com Date of Report: Dec 13, 2023 Customer PO #: Customer ID: 08100027 Report #: 2023-25631 Project ID: Monitoring Wells Lab ID Sample ID: 23-62092 Site: MW-9 Test Collect Date/Time 11/4/2023 10:45 AM Method Matrix Sampled by Water jcb/envirochem Results Date Analyzed Color color Tan/Turbid 11/04/2023 Depth to water, ft. Depth to water, Ft 6.2 feet 11/04/2023 Sodium EPA 200.7, Rev 4.4, 1994 7.10mg/L 11/16/2023 Sulfate EPA 300.0, Rev. 2.1, 1993 29 mg/L 11/07/2023 Ammonia Nitrogen EPA 350.1, Rev. 2.0, 1993 < 0.2 mg/L 11/07/2023 Gallons bailed before sampling Gallons Bailed before sampling 5.0 gallons 11/04/2023 Odor Qualitative None 11/04/2023 Total Dissolved Solids (TDS) SM 2540 C-2015 278 mg/L 11 /06/2023 Temperature SM 2550 B-2010 17.8 C 11/04/2023 pH SM 4500 H 8-2011 5.9 units 11/04/2023 Total Phosphorus SM 4500 P (F-H)-2011 < 0.04 mg/L 11 /10/2023 Total Organic Carbon (TOC) SM 5310 8-2014 30.6 mg/L 11/06/2023 Fecal Coliform SM 9222 D-2015 MF <1 Colonies/100ml- 11/04/2023 Chloride SM4500 Cl E-2011 27 mg/L 11/08/2023 1, 1, 1,2-Tetrachloroethane SW846Method 8260D15030B <0.5µg/L 11/09/2023 1, 1, 1 -Trichloroethane SWWMethod 8260D/5030B <0.5µg/L 11/09/2023 1,1,2,2-Tetrachloroethane SW 846 Method 8260D/5030B <0.5 µg/L 11/09/2023 1,1,2-Trichloroethane SW 846 Method 8260D/5030B <0.5 µg/L 11/09/2023 1,1-Dichloroethane SW 846 Method 8280DI5030B <0.5 µg/L 11/09/2023 1,1-Dichloroethene SW 846 Method 8260D15030B <0.5 µg/L 11/09/2023 1,1-Dichloropropene SW 846 Method 6260D15030B <0.5 µg/L 11/09/2023 1,2,3-Trichlorobenzene SW 848 Method 828013/5030B <0.5 µg/L 11/09/2023 1,2,3-Trichloropropane SW 846 Method 826013/5030B <0.5 µg/L 11/09/2023 1,2,4-Trichlorobenzene SW 846 Method 8260D/5030B <0.5 µg/L 11/09/2023 1,2,4-Trimethylbenzene SW 846 Method 82BOD/5030B <0.5 pg/L 11/09/2023 1,2-Dibromo-3-Chloropropane SW e46 Method 8280D/5030B <1 pg/L 11/09/2023 Report 1t:: 2023-25531 Page 16 of 33 sM ANALYTICAL & CONSULTING CHEMISTS F"07-71 Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax info@environmentalchemists.com Darling Ingredients - Rose Hill Date of Report: Dec 13, 2023 Post Office Box 1026 Customer PO #: Rose Hill NC 28458 Customer ID: 08100027 Attention: Report #: 2023-25631 Project ID: Monitoring Wells 1,2-Dibromoethane SW 846 Method MOD15030B <0.5 pg/L 11/09/2023 1,2-Dichlorobenzene SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2023 1,2-Dichloroethane SW 848 Method 8260D/50308 <0.5 pg/L 11/09/2023 1,2-Dichloropropane SW 846 Method 826oD/5030B <0.5 pg/L 11/09/2023 1,3,5-Tdmethylbenzene SW 848 Method 826OD15030B <0.5 pg/L 11/09/2023 1,3-Dichlorobenzene SW 848 Method 82600/50308 <0.5 pg/L 11/09/2023 1,3-Dichloropropane SW 846 Method 826oD/50308 <0.5 pg/L 11/09/2023 1,4-Dichlorobenzene SW 845 Method 8260D/5030B <0.5 pg/L 11/09/2023 2,2-Dichloropropane SW 846 Method 826oD/5030B <0.5 pg/L 11/09/2023 -Chlorotoluene SW 846 Method 8260D/5030B <0.5 ug/L 11/09/2023 4-Chlorotoluene SW 80 Method 82600/5030B <0.5 pg/L 11/09/2023 Benzene SW 848 Method 8260DI50308 <0.5 pg/L 11/09/2023 Bromobenzene SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2023 Bromochloromethane SW 048 Method 826OD15030B <0.5 pg/L 11/09/2023 Bromodichloromethane SW 846 Method 82ND/5030B <0.5 pg/L 11/09/2023 Bromoform SW 846 Method 8280D/5030B <0.5 pg/L 11/09/2023 Bromomethane SW 846 Method 8260D/50308 <0.5 pg/L 11/09/2023 Carbon tetrachloride SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2023 Chlorobenzene SW 046 Method 8260D15030B <0.5 pg/L 11/09/2023 Chloroethane SW 846 Method 82801315030B <0.5 pg/L 11/09/2023 Chloroform SW 80 Method 826OD15030B <0.5 pg/L 11/09/2023 Chloromethane SW 846 Method 8260D15030B <0.5 pg/L 11/09/2023 cis-1,2-Dichloroethene SW e46 Method 8280DI5030B <0.5 pg/L 11/09/2023 cis-1,3-Dichloropropene SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2023 Dibromochloromethane SW 845 Method 8260D15030B <0.5 pg/L 11/09/2023 Dibromomethane SW 646 Method 82600/5030B <0.5 pg/L 11/09/2023 Dichlorodifluoromethane SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2023 ,cthylbenzene SW 846 Method 826OD15030B <0.5 pg/L 11/09/2023 Hexachlorobutadiene SW 846 Method 8260D/5030B <0.5 pg/L 11 /09/2023 Isopropylbenzene SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2023 Report #:: 2023 25631 Page 17 of 33 SM ANALYTICAL & CONSULTING CHEMISTS Darling Ingredients - Rose Hill Post Office Box 1026 Rose Hill NC 28458 Attention: Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab - 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 - 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax infoCaenvironmentalchemists.com Date of Report: Dec 13, 2023 Customer PO #: Customer ID: 08100027 Report #: 2023-25631 Project ID: Monitoring Wells M+P Xylene SW 846 Method 82BOD/50308 <1.0 pg/L 11/09/2023 Methylene chloride SW B46 Method 8260D/5030B <0.5 pg/L 11/09/2023 Naphthalene SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2023 n-Butylbenzene SW 846 Method 82BOD/5030B <0.5 pg/L 11/09/2023 n-Propylbenzene SW 846 Method 8280DI5030B <0.5 pg/L 11/09/2023 ortho-Xylene SW 846 Method 8260D/5030B <0.5 NgIL 11/09/2023 p-Isopropyltoluene SW 840 Method 826OD/50308 <0.5 pg/L 11/09/2023 sec-Butylbenzene SW 80 Method 8260DI5030B <0.5 pg/L 11/09/2023 Styrene SW 846 Method 8260D/50308 <0.5 pg/L 11/09/2023 tert-Butylbenzene SW 84e Method 62BOD/5030B <0.5 pg/L 11/09/2023 Tetrachloroethene sw So Method 8200DI5030B <0.5 pg/L 11/09/2023 Toluene SW 846 Method 826013/503013 <0.5 pg/L 11/09/2023 Trans-1,2-Dichloroethene SW 846 Method 82BOD15030B <0.5 pg/L 11/09/2023 Trans-1,3-dichloropropene SW 846 Method 8MOD150308 <0.5 pg/L 11/09/2023 Trichloroethene SW 846 Method 82BOD/5030B <0.5 pg/L 11/09/2023 Trichlorofluoromethane SW 846 Method 826OD/50308 <0.5 pg/L 11/09/2023 Vinyl chloride SW 845 Method 82BOD/50308 <0.5 pg/L 11/09/2023 Nitrate Nitrogen (Calc) Nitrite Nitrogen EPA 353.2, Rev. 2.0,1993 0.05 mg/L 11/06/2023 Nitrate+Nitrite-Nitrogen EPA 353.2, Rev. 2.0,1993 0.28 mg/L 11/08/2023 Nitrate Nitrogen subtraction Method 0.23 mg/L 12/12/2023 Total Nitrogen (Calc) Total Kjeldahl Nitrogen (TKN) EPA 351.2, Rev. 2.0, 1993 0.8 mg/L 11/10/2023 Total Nitrogen Total Nitrogen 1.08 mg/L 12/12/2023 Report ik: 2023-25631 Page 16 of 33 IL envirochem ANALYTICAL & CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 - 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 - 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax in fo(aenvironmentalchemi sts.com Darling Ingredients - Rose Hill Date of Report: Dec 13, 2023 Post Office Box 1026 Customer PO #: Rose Hill NC 28458 Customer ID: 08100027 Attention: Report #: 2023-25631 Project ID: Monitoring Wells Lab ID Sample ID: Collect Date/Time Matrix Sampled by 23-62093 Site: MW-10A 11/4/2023 1:05 PM Water jcb/envirochem Test Method Results Date Analyzed Color Color Clear 11/04/2023 Depth to water, ft. Depth to Water. Ft. 5.3 feet 11/04/2023 Sodium EPA 200.7, Rev 4.4,1994 114 mg/L 11 /16/2023 Sulfate EPA 300.0, Rev. 2.1, 1993 143 mg/L 11/07/2023 Ammonia Nitrogen EPA350.1, Rev. 2.0,1993 0.4 mg/L 11/07/2023 Gallons bailed before sampling Gallons Bailed before sampling 5.0 gallons 11/04/2023 Odor Qualitative None 11/04/2023 Total Dissolved Solids (TDS) SM 2540 C-2015 793 mg/L 11/06/2023 Temperature SM 2550 B-2010 19.6 C 11/04/2023 pH SM4WOHB-2011 3.55est.units 11/04/2023 Total Phosphorus SM 4500 P (F-H}2011 0.07 mg/L 11 /10/2023 Total Organic Carbon (TOC) SM 5310 8-2014 3.8 mg/L 11/06/2023 Fecal Coliform SM 9222 D-2015 MF <1 Colonies/100ml- 11/04/2023 Chloride SM4500 CI E-2011 322 mg/L 11/08/2023 1. 1, 1,2-Tetmchloroethane SW 846 Method 828010I5030B <0.5 pg/L 11/09/2023 1, 1, 1 -Trichloroethane SW 848 Method 625015030E <0.5 pg/L 11/09/2023 1,1,2,2-Tetrachloroethane SW 846 Method 8280DI5030B <0.5 pg/L 11/09/2023 1,1,2-Trichloroethane SW 846 Method 8260D15030B <0.5 pg/L 11/09/2023 1,1-Dichloroethane SW 846 Method 82BOD15030B <0.5 pg/L 11/09/2023 1,1-Dichloroethene SW 846 Method 826OD15030B <0.5 pg/L 11/09/2023 1,1-Dichloropropene SW 846 Method 82BOD15030B <0.5 pg/L 11/09/2023 1,2,3-Tdchlorobenzene SW 846 Method 8280 15030E <0.5 pg/L 11/09/2023 1,2,3-Trichloropropane SW 846 Method 825010/5030B <0.5 pg/L 11/09/2023 1,2,4-Trichlorobenzene SW 846 Method 828OD15030B <0.5 pg/L 11/09/2023 J 1,2,4 Trimethylbenzene SW 846 Method 82BOD150308 <0.5 pg/L 11/09/2023 1,2-Dibromo-3-Chloropropane SW 846 Method 8260DI5030B <1 pg/L 11/09/2023 Report #:: 2023-25831 Page 19 of 33 Environmental Chemists, Inc. • 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax M 255-A Wilmington Highway, Jacksonville, NC 28540 o 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS info@ environmentalchemisu com Darling Ingredients - Rose Hill Date of Report: Dec 13, 2023 Post Office Box 1026 Customer PO #: Rose Hill NC 28458 Customer ID: 08100027 Attention: Report #: 2023-25631 Project ID: Monitoring Wells 1,2-Dibromoethane SW 848 Method 8280DI5030B <0.5 pg/L 11/09/2023 1,2-Dichlorobenzene SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2023 1,2-Dichloroethane SW 846 Method 82BOD/5030B <0.5 pg/L 11/09/2023 1,2-Dichloropropane SW 848 Method 82BOD15030B <0.5 pg/L 11/09/2023 1,3,5-Tdmethylbenzene SW 846 Method 826OD15030B <0.5 pg/L 11/09/2023 1,3-Dichlorobenzene SW 845 Method 82BOD15030B <0.5 pg/L 11/09/2023 1,3-Dichloropropane SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2023 1,4-Dichlorobenzene SW 848 Method 82BOD/5030B <0.5 pg/L 11/09/2023 2,2-Dichloropropane SW 846 Method 8280D/5030B <0.5 pg/L 11/09/2023 2-Chlorotoluene SW 846 Method 82BOD/5030B <0.5 pg/L 11/09/2023 4-Chlorotoluene SW 846 Method 82BOD/5030B <0.5 pg/L 11/09/2023 Benzene SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2023 Bromobenzene SW 846 Method 82BOD/5030B <0.5 pg/L 11/09/2023 Bromochloromethane SW 846 Method 8280D/5030B <0.5 pg/L 11/0912023 Bromodichloromethane SW 846 Method 82BOD15030B <0.5 pg/L 11/09/2023 Bromoform SW 848 Method 8260D/5030B <0.5 pg/L 11/09/2023 Bromomethane SW 846 Method 82BOD/5030B <0.5 pg/L 11/09/2023 Carbon tetrachloride SW 846 Method 826013/503013 <0.5 pg/L 11/09/2023 Chlorobenzene SW 848 Method 828OD15030B <0.5 pg/L 11/09/2023 Chloroethane SW 848 Method 8260D/5030B <0.5 pg/L 11/09/2023 Chloroform SW 848 Method 8280D/5030B <0.5 pg/L 11/09/2023 Chloromethane SW 846 Method 8280D/50308 <0.5 pg/L 11/09/2023 cis-1,2-Dichloroethene SW 846 Method 82BOD/5030B <0.5 pg/L 11/09/2023 cis-1,3-Dichloropropene SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2023 Dibromochloromethane SW 846 Method 82BOD/5030B <0.5 pg/L 11/09/2023 Dibromomethane SW 848 Method 82BOD/5030B <0.5 pg/L 11/09/2023 Dichlorodifluoromethane SW 848 Method 8260D/50308 <0.5 pg/L 11/09/2023 ,Ethylbenzene SW 846 Method 826OD15030B <0.5 pg/L 11/09/2023 Hexachlorobutadiene SW 846 Method 8260DI5030B <0.5 pg/L 11/09/2023 Isopropylbenzene SW 846 Method 8280D/5030B <0.5 pg/L 11/09/2023 Report k: 2023-25531 Page 20 of 33 Environmental Chemists, Inc. envirochem 6602 Windmill Way, Wilmington, NC 18405 • 910.392.0223 Lab • 910,392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax sn+ 255-A Wilmington Highway, Jacksonville, NC 28540 v 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS info@environmentalchemists.com Darling Ingredients - Rose Hill Post Office Box 1026 Rose Hill NC 28458 Attention: Date of Report: Dec 13, 2023 Customer PO #: Customer ID: 08100027 Report #: 2023-25631 Project ID: Monitoring Wells M+P Xylene SW 846 Method 82BOD15030B <1.0 pg1L 11/09/2023 Methylene chloride SW 846 Method 8260DIS030B <0.5 pg/L 11/09/2023 Naphthalene SW 846 Method 8260D/50308 <0.5 pg/L 11 /09/2023 n-Butylbenzene SW 846 Method 826OD15030B <0.5 pg/L 11/09/2023 n-Propylbenzene SW 846 Method 82BOD/5030B <0.5 pg/L 11/09/2023 ortho-Xylene SW 80 Method 8260D15030B <0.5 pg/L 11/09/2023 p-Isopropyltoluene SW NO Method 826OD/5030B <0.5 pg/L 11/09/2023 sec-Butylbenzene SW 846 Method 82601315D308 <0.5 pg/L 11/09/2023 Styrene SW 848 Method 8260D15030B <0.5 pg/L 11/09/2023 'ert-Butylbenzene SW 846 Method 826013/50306 <0,5 Ng/L 11/09/2023 Tetrachloroethene SW Me Method 8280D/50306 <0.5 pg/L 11/09/2023 Toluene SW 80 Method 8260DI5030B <0.5 pg/L 11/09/2023 Trans-1,2-Dichloroethene SW 848 Method 8260D15030B <0.5 pg/L 11/09/2023 Trans-1,3-dichloropropene SW 846 Method 82BOD/5030B <0.5 pg/L 11/09/2023 Trichloroethene SW 848 Method 8260D/5030B <0.5 pg/L 11/09/2023 Trichlorofluoromethane SW 846 Method 826OD/50308 <0.5 pg/L 11/09/2023 Vinyl chloride SW 846 Method 8280D/5030B <0.5 pg/L 11/09/2023 Nitrate Nitrogen (Calc) Nitrite Nitrogen EPA 353.2, Rev. 2.0, 1983 < 0.02 mg/L 11/06/2023 Nitrate+Nitrite-Nitrogen EPA 353.2, Rev. 2.0, 1903 < 0.02 mg/L 11/08/2023 Nitrate Nitrogen Subtraction Method <0.02 mg/L 12/12/2023 Total Nitrogen (Calc) Total Kjeldahl Nitrogen (TKN) EPA 361.2, Rev. 2.0.1993 0.6 mg/L 11/10/2023 Total Nitrogen Tatel Nlhogen 0.60 mg/L 12/12/2023 Report *: 2023-25631 Page 21 of 33 F"07-77 Environmental Chemists, Inc. • 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 0 252.473.5702 Lab/Fax sM 255-A Wilmington Highway, Jacksonville, NC 28540 a 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS info@environmentalchemists.com Darling Ingredients - Rose Hill Post Office Box 1026 Rose Hill NC 28458 Attention: Date of Report: Dec 13, 2023 Customer PO #: Customer ID: 08100027 Report #: 2023-25631 Project ID: Monitoring Wells Lab ID Sample ID: Collect DatefTime Matrix Sampled by 23-62094 Site: MW-11A 11/4/2023 12:50 PM Water jcb/envirochem Test Method Results Date Analyzed Color color Clear/Tan 11/04/2023 Depth to water, ft. Depth to water, Ft. 7.5 feet 11/04/2023 Sodium EPA200.7, Rev4.4, 1994 62.9 mg/L 11/16/2023 Sulfate EPA 300.0, Rev. 2.1, 1993 161 mg/L 11/07/2023 Ammonia Nitrogen EPA 360.1, Rev.2.0.1993 < 0.2 mg/L 11/07/2023 Gallons bailed before sampling Gallons Bailed before sampling 5.0 gallons 11/04/2023 Odor Qualitative None 11/04/2023 Total Dissolved Solids (TDS) SM 2540 C-2015 490 mg/L 11/06/2023 Temperature SM 2550 B-2010 20.6 C 11/04/2023 pH SM 4500 H &2011 4.7 units 11/04/2023 Total Phosphorus SM 4500 P (F-H)-2011 < 0.04 mg/L 11 /10/2023 Total Organic Carbon (TOC) SM 5310 B-2014 2.5 mg/L 11/06/2023 Fecal Coliform SM 9222 D-2015 MF <1 Colonies/100ml- 11/04/2023 Chloride SM450o cl E-2011 121 mg/L 11 /08/2023 1, 1, 1,2-Tetrachloroethane SW848Method 8280D/5030B <0.5pg/L 11/09/2023 1,1,1-Tdchloroethane SW 846 Method 8260D/503013 <0.5 pg/L 11/09/2023 1,1,2,2-Tetrachloroethane SW848Method 8260D/5030B <0.5pg/L 11/09/2023 1,1,2-Tdchloroethane SW 846 Method 8280D/5030B <0.5 pg/L 11/09/2023 1, 1 -Dichloroethane SW 848 Method 028013/50300 <0.5 pg/L 11/09/2023 1, 1 -Dichloroethene SW 80 Method 826OD15030B <0.5 pg/L 11/09/2023 1,1-Dichloropropene SW M Method 8280D/5030B <0.5 pg/L 11/09/2023 1,2, 3-Trichlorobenzene SW 840 Method 8260D15030B <0.5 pg/L 11/09/2023 1,2, 3-Trichloropropane SW 846 Method 8260D/5030B <0.5 pg/L 11 /09/2023 1,2,4-Trichlorobenzene SW 646 Method 8260D15030B <0.5 pg/L 11/09/2023 1,2,4-Trimethylbenzene SW 846 Method 8280D/5030B <0.5 pg/L 11/09/2023 1,2-Dibromo-3-Chloropropane SW 846 Method 8280D/5030B <1 pg/L 11/09/2023 Report#:: 2023-25631 Page 22 of 33 Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 - 910.392.0223 Lab - 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 - 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 - 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS info@environmentalchemists.com Darling Ingredients - Rose Hill Date of Report: Dec 13, 2023 Post Office Box 1026 Customer PO #: Rose Hill NC 28458 Customer ID: 08100027 Attention: Report #: 2023-25631 Project ID: Monitoring Wells 1,2-Dibromoethane SW 846 Method 82BOD/5030B <0.5 pg/L 11/09/2023 1,2-Dichlorobenzene SW 846 Method 826OD15030B <0.5 pg/L 11/09/2023 1,2-Dichloroethane SW 846 Method 826OD/5030B <0.5 pg/L 11/09/2023 1,2-Dichloropropane SW 846 Method 8260D15D30B <0.5 pg/L 11/09/2023 1,3,5-Tdmethylbenzene SW 846 Method 8280D/5030B <0.5 pg/L 11/09/2023 1,3-Dichlorobenzene SW Na Method 82BOD15030B <0.5 pg/L 11/09/2023 1,3-Dichloropropane SW 848 Method 8260D/5030B <0.5 pg/L 11/09/2023 1,4-Dichlorobenzene SW 046 Method 826OD15030B <0.5 pg/L 11/09/2023 2,2-Dichloropropane SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2023 2-Chlorotoluene SW 846 Method 6260D/5030B <0.5 pg/L 11/09/2023 4-Chlorotoluene SW 846 Method 8280D/5030B <0.5 pg/L 11/09/2023 Benzene SW 846 Method BOOD150308 <0.5 pg/L 11/09/2023 Bromobenzene SW 046 Method 826OD/5030B <0.5 pg/L 11/09/2023 Bromochloromethane SW NO Method 8260D/5030B <0.5 pg/L 11/09/2023 Bromodichloromethane SW 846 Method 8280D/50308 <0.5 pg/L 11/09/2023 Bromoform SW 846 Method 8260D15030B <0.5 pg/L 11/09/2023 Bromomethane SW 848 Method 82e0D/5030B <0.5 pg/L 11/09/2023 Carbon tetrachloride SW 846 Method 826OD/5030B <0.5 pg/L 11/09/2023 Chlorobenzene SW 848 Method 826OD/5030B <0.5 pg/L 11/09/2023 Chloroethane SW 846 Method 82BOD16030B <0.5 pg/L 11/09/2023 Chloroform SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2023 Chloromethane SW 846 Method 828OD/5030B <0.5 pg/L 11/09/2023 cis-1,2-Dichloroethene SW 846 Method 8260DI5030B <0.5 pg/L 11/09/2023 cis-1,3-Dichloropropane SW 848 Method 8260D/5030B <0.5 pg/L 11/09/2023 Dibromochloromethane SW 846 Method 8280D/50308 <0.5 pg/L 11/09/2023 Dibromomethane SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2023 Dichlorodifluoromethane SW 846 Method 8280D/5030B <0.5 pg/L 11/09/2023 iEthylbenzene SW 846 Method 8280D/5030B <0.5 pg/L 11/09/2023 Hexachlorobutadiene SW 80 Method 826OD/5030B <0.5 pg/L 11/09/2023 isopropylbenzene SW 846 Method 82BOD15030B <0.5 pg/L 11/09/2023 Report #:: 2023-25531 Page 23 of 33 L ANALYTICAL & CONSULTING CHEMISTS Darling Ingredients - Rose Hill Post Office Box 1026 Rose Hill NC 28458 Attention: Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax info@environmentalchemists.com Date of Report: Dec 13, 2023 Customer PO #: Customer ID: 08100027 Report #: 2023-25631 Project ID: Monitoring Wells M+P Xylene sw 846 Method 82aOD/5030B <1.0 pg/L 11/09/2023 Methylene chloride SW 846 Method 820OD15030B <0.5 pg/L 11/09/2023 Naphthalene SW 846 Method 826013/5030B <0.5 pg/L 11/09/2023 n-Butylbenzene SW 848 Method 826013/503013 <0.5 pg/L 11/09/2023 n-Propylbenzene SW 846 Method 826013/50306 <0.5 pg/L 11/09/2023 ortho-Xylene SW 80 Method 8260DIS030B <0.5 pg/L 11/09/2023 p-isopropyltoluene SW 80 Method 828OD15030B <0.5 pg/L 11/09/2023 sec-Butylbenzene SW 546 Method 8260D/5030B <0.5 pg/L 11/09/2023 Styrene SW 046 Method 826OD15030B <0.5 Ng/L 11/09/2023 iert-Butylbenzene SW 846 Method 826013/5030121 <0.5 pg/L 11/09/2023 Tetrachloroethene SW 848 Method 826013/50306 <0.5 Ng/L 11/09/2023 Toluene SW 846 Method 8280D/50308 <0.5 pg/L 11/09/2023 Trans-1 ,2-Dichloroethene SW 845 Method BMD15030B <0.5 pg/L 11/09/2023 Trans-1,3-dichloropropene SW 845 Method 8260D/5030B <0.5 pg/L 11/09/2023 Trichloroethene SW 846 Method 8260D150306 <0.5 pg/L 11/09/2023 Trichlorofluoromethane SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2023 Vinyl chloride SW 848 Method 8MOD1503DB <0.5 pg/L 11/09/2023 Nitrate Nitrogen (Cale) Nitrite Nitrogen EPA 353.2, Rev. 2.0,1993 < 0.02 mg/L 11/06/2023 Nitrate+Nitrite-Nitrogen EPA353.2, Rev. 2.0, 1993 0.34 mg/L 11/08/2023 Nitrate Nitrogen Subtraction Method 0.34 mg/L 12/12/2023 Total Nitrogen (Cale) Total Kjeldahl Nitrogen (TKN) EPA351.2, Rev. 2.0,1993 < 0.5 mg/L 11/10/2023 Total Nitrogen Total Ntbogen <0.5 mg/L 12/12/2023 Report*: 2023-25831 Page 24 of 33 envirochem ANALYTICAL & CONSULTING CHEMISTS FOP"—. --,77 Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax info@environmentalchemists.com Darling Ingredients - Rose Hill Date of Report: Dec 13, 2023 Post Office Box 1026 Customer PO #: Rose Hill NC 28458 Customer ID: 08100027 Attention: Report #: 2023-25631 Project ID: Monitoring Wells Lab ID Sample ID: Collect Date/Time Matrix Sampled by 23-62095 Site: MW-12B 11/4/2023 1:35 PM Water jcb/envirochem Test Method Results Date Analyzed Color Color None 11 /04/2023 Depth to water, ft. Depth to Water, Ft 6.8 feet 11/04/2023 Sodium EPA 200.7, Rev 4A. 1994 68.7mg/L 11/19/2023 Sulfate EPA 300.0, Rev. 2.1, 1993 124 mg/L 11/14/2023 Ammonia Nitrogen EPA 350.1, Rev. 2.0, 1993 < 0.2 mg/L 11/07/2023 Gallons bailed before sampling Gallons Bailed before sampling 5.0 gallons 11 /04/2023 Odor Qualitative None 11 /04/2023 Total Dissolved Solids (TDS) SM 2540 C-2015 385 mg/L 11 /06/2023 Temperature SM 2550 &2010 21.2 C 11/04/2023 pH SM 4500 H B-2011 3.91 est units 11 /04/2023 Total Phosphorus SM 4500 P (F-H}2011 0.15 mg/L 11/10/2023 Total Organic Carbon (TOC) SM 5310 8-2014 1.7 mg/L 11 /06/2023 Fecal Coliform SM 92U D-2015 MF <1 Colonies/100ml- 11 /04/2023 Chloride SM4500 Cl E-2011 120 mg/L 11/08/2023 1, 1, 1,2-Tetrachloroethane SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2023 1,1,1-Tdchloroethane SW 846 Method 82BOD/5030B <0.5 pg/L 11/09/2023 1,1,2,2-Tetrachloroethane SW846Method 8280D/5030B <0.5pg/L 11/09/2023 1,1,2-Trichloroethane SW e46 Method 826013/5030B <0.5 ug/L 11/09/2023 1,1-Dichloroethane SW 846 Method 828013/5030B <0.5 ug/L 11/09/2023 1,1-Dichloroethene SW 846 Method 826013/5030B <0.5 ug/L 11/09/2023 1,1-Dichloropropena SW 80 Method 82BOD15030B <0.5 pg/L 11/09/2023 1,2,3-Trichlorobenzene SW 846 Method 82BOD/5030B <0.5 pg/L 11/09/2023 1,2,3-Trichloropropane SW848Method 8280D/5030B <0.5pg/L 11/09/2023 i1,2,4-Trichlorobenzene SW 846 Method 82BOD/5030B <0.5 pg/L 11/09/2023 1,2,4-Trimethylbenzene SW 846 Method 82BOD15030B <0.5 ug/L 11/09/2023 1,2-Dibromo-3-Chloropropane SW846Method 8260D/5030B <1 ug/L 11/09/2023 Report #:: 2023-26631 Page 25 of 33 F""' 77 Environmental Chemists, Inc. e 6602 Windmill Way, Wilmington, NC 28405 a 910.392.0223 Lab • 910.392.4424 Fax UM Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax ANALYTICAL S CONSULTING CHEMISTS info(a,environmentalchemists.com Darling Ingredients - Rose Hill Post Office Box 1026 Rose Hill NC 28458 Attention: Date of Report: Dec 13, 2023 Customer PO #: Customer ID: 08100027 Report #: 2023-25631 Project ID: Monitoring Wells 1,2-Dibromoethane SW 846 Method 8280D/5030B <0.5 ug/L 11/09/2023 1,2-Dichlorobenzene SW 80 Method 8260D16030B <0.5 Ng/L 11/09/2023 1,2-Dichloroethane SW e46 Method 8260DI50308 <0.5 pg/L 11/09/2023 1,2-Dichloropropane SW B4e Method 82BOD/5030B <0.5 Ng/L 11/09/2023 1,3,5-Trimethylbenzene SW 8" Method 826OD15030B <0.5 pg/L 11/09/2023 1,3-Dichlorobenzene SW 8" Method 82SOD15030B <0.5 pg/L 11/09/2023 1,3-Dichloropropane SW 848 Method 826OD15030B <0.5 pg/L 11/09/2023 1,4-Dichlorobenzene SW 846 Method 826013/503013 <0.5 pg/L 11/09/2023 2,2-Dichloropropane SW e46 Method 826013/5030e <0.5 pg/L 11/09/2023 ',2-Chlorotoluene SW 848 Method 826OD/5030B <0.5 ug/L 11/09/2023 4-Chlorotoluene SW 848 Method 8260DI5030B <0.5 pg/L 11/09/2023 Benzene SW 848 Method 8260D15030B <0.5 Ng/L 11/09/2023 Bromobenzene SW 845 Method 8280D/5030B <0.5 Ng/L 11/09/2023 Bromochloromethane SW 846 Method 8260DIS030B <0.5 pg/L 11/09/2023 Bromodichloromethane SW 846 Method 82BODI5030B <0.5 Ng/L 11/09/2023 Bromoform SW 848 Method 8280D/5030B <0.5 pg/L 11/09/2023 Bromomethane SW 846 Method 82BOD15030B <0.5 pg/L 11/09/2023 Carbon tetrachloride SW 848 Method 8260D/50308 <0.5 Ng/L 11 /09/2023 Chlorobenzene SW 8" Method 8260D/5030B <0.5 pg/L 11/09/2023 Chloroethane SW ti48 Method 8260D/50MB <0.5 pg/L 11/09/2023 Chloroform SW 848 Method 82BOD/5030B <0.5 pg/L 11/09/2023 Chloromethane SW 846 Method 82BOD/50308 <0.5 pg/L 11/09/2023 cis-1,2-Dichloroethene SW 84e Method 82e013/5030B <0.5 Ng/L 11/09/2023 cis-1,3-Dichloropropene SW 846 Method 8280DI5030B <0.5 pg/L 11/09/2023 Dibromochloromethane SW 80 Method 82BOD/5030B <0.5 pg/L 11/09/2023 Dibromomethane SW Me Method 82e013/503013 <0.5 pg/L 11/09/2023 Dichlorodifluoromethane SW B46 Method 8250DI5030B <0.5 pg/L 11/09/2023 Ethylbenzene SW S46 Method 6260D/5030B <0.5 pg/L 11/09/2023 Hexachlorobutadiene SW M Method 8280DI5030B <0.5 pg/L 11/09/2023 Isopropylbenzene SW 848 Method 82BOD/5030B <0.5 pg/L 11/09/2023 Report#: 2023-26831 Page 28 of 33 :enviroc'hem ANALYTICAL & CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 0 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 a 910.347.5843 Lab/Fax info@environmentalchemists.com Darling Ingredients - Rose Hill Date of Report: Dec 13, 2023 Post Office Box 1026 Customer PO #: Rose Hill NC 28458 Customer ID: 08100027 Attention: Report #: 2023-25631 Project ID: Monitoring Wells M+P Xylene SW 846 Method 8280D/5030B <1.0 pg/L 11/09/2023 Methylene chloride SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2023 Naphthalene SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2023 n-Butylbenzene SW 846 Method 828013/503013 <0.5 pg/L 11/09/2023 n-Propylbenzene 5W 846 Method 8260D/5030B <0.5 pg/L 11/09/2023 ortho-Xylene SW 646 Method 828013/503013 <0.5 pg/L 11/09/2023 p-Isopropyltoluene SW 845 Method 826013/503013 <0.5 pg/L 11 /09/2023 sec-Butylbenzene SW Me Method 826oD15030B <0,5 pg/L 11/09/2023 Styrene SW 846 Method 8280D/50308 <0.5 pg/L 11/09/2023 ?ert-Butylbenzene SW 846 Method 8280D/50308 <0.5 ug/L 11/09/2023 Tetrachloroethene SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2023 Toluene SW 846 Method 826013/503013 <0.5 pg/L 11 /09/2023 Trans-1,2-Dichloroethene SW 846 Method 8260D15030B <0.5 pg/L 11/09/2023 Trans-1,3-dichloropropene SW 848 Method 8260D150308 <0.5 pg/L 11/09/2023 Trichloroethene SW 80 Method 826OD15030B <0.5 pg/L 11/09/2023 Trichlorofluoromethane SW 846 Method 8280D16030B <0.5 pg/L 11/09/2023 Vinyl chloride SW 846 Method 826013/503013 <0.5 pg/L 11 /09/2023 Nitrate Nitrogen (Cale) Nitrite Nitrogen EPA353.2, Rev.2.0,1993 < 0.02 mg/L 11/06/2023 Nitrate+Nitrite-Nitrogen EPA353.2, Rev. 2.0,1993 0.14 mg/L 11/08/2023 Nitrate Nitrogen Sutmacdon Method 0.14 mg/L 12/12/2023 Total Nitrogen (Cale) Total Kjeldahl Nitrogen (TKN) EPA 351.2. Rev. 2.0,1993 0.5 mg/L 11/10/2023 Total Nitrogen Total Nitrogen 0.64 mg/L 12112/2023 Reporttk: 2023-25031 Page 27 of 33 — -:,07 IL enviroc-hem ANALYTICAL & CONSULTING CHEMISTS F"17 Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 - 910.392.0223 Lab - 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 - 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 - 910.347.5843 Lab/Fax info(u envi ronmentalchemists.com Darling Ingredients - Rose Hill Date of Report: Dec 13, 2023 Post Office Box 1026 Customer PO #: Rose Hill NC 28458 Customer ID: 08100027 Attention: Report #: 2023-25631 Project ID: Monitoring Wells Lab ID Sample ID: Collect Date/Time Matrix Sampled by 23-62096 Site: MW-13A 11/4/2023 1:20 PM Water jcb/envirochem Test Method Results Date Analyzed Color Color Clearrran 11/04/2023 Depth to water, ft. Depth to Water, Ft 7.4 feet 11/04/2023 Sodium EPA 200.7, Rev 4A, 1994 4.25 mg/L 11 /19/2023 Sulfate EPA 300.0, Rev. 2.1, 1993 8 mg/L 11/07/2023 Ammonia Nitrogen EPA350.1, Rev. 2.0, 1993 < 0.2 mg/L 11/07/2023 Gallons bailed before sampling Gallons Bailed before sampling 5.0 gallons 11/04/2023 Odor Quelnative None 11/04/2023 Total Dissolved Solids (TDS) SM 2540 C-2015 35 mg/L 11 /06/2023 Temperature SM 2550 B-2010 21.8 C 11/04/2023 pH SM 4500 H B-2011 4.7 units 11/04/2023 Total Phosphorus SM 4500 P (F-H)-2011 < 0.04 mg/L 11/10/2023 Total Organic Carbon (TOC) SM 5310 B-2014 0.6 mg/L 11 /06/2023 Fecal Coliform SM 9222 D-2015 MF <1 Colonies/100ml- 11/04/2023 Chloride SM4500 Cl E-2011 < 5 mg/L 11/08/2023 1,1,1,2-Tetrachloroethane SW 848 Method 8280D15030B <0.5pg/L 11/09/2023 1,1,1-Tdchloroethane SW 846 Method 8280D/5030B <0.5 pg/L 11/09/2023 1,1,2,2-Tetrachloroethane SW 846 Method MOD/5030B <0.5 pg/L 11/09/2023 1,1,2-Tdchloroethane SW846Method 8260D/50308 <0.5pg/L 11/09/2023 1,1-Dichloroethane SW 846 Method 826013/5030B <0.5 pg/L 11/09/2023 1, 1 -Dichloroethene SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2023 1,1-Dichloropropene SW 846 Method 826oD/5030B <0.5 pg/L 11/09/2023 1,2,3-Trichlorobenzene SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2023 1,2,3-Trichloropropane SW846Method 8260D/50308 <0.5pg/L 11/09/2023 1,2,4-Trichlorobenzene SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2023 1,2,4-Tdmethylbenzene SW 846 Method 8260DI5030B <0.5 pg/L 11/09/2023 1,2-Dibromo-3-Chloropropane SW 846 Method 82600/5030B <1 pg/L 11/09/2023 Report #: 2023-25631 Page 28 of 33 Cen:virochem ANALYTICAL & CONSULTING CHEMISTS Darling Ingredients - Rose Hill Post Office Box 1026 Rose Hill NC 28458 Attention: Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 - 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax info@environmentalchemists.com Date of Report: Dec 13, 2023 Customer PO #: Customer ID: 08100027 Report #: 2023-25631 Project ID: Monitoring Wells 1,2-Dibromoethane SW 80 Method 82BOD/5030B <0.5 pg/L 11/09/2023 1,2-Dichlorobenzene SW 646 Method 828013/503013 <0.5 pg/L 11/09/2023 1,2-Dichloroethane SW 848 Method 826013/503013 <0.5 pg/L 11/09/2023 1,2-Dichloropropane SW 846 Method 82BOD15030B <0.5 pg/L 11/09/2023 1,3,5-Trimethylbenzene SW 846 Method 8260DI5030B <0.5 pg/L 11/09/2023 1,3-Dichlorobenzene SW US Method 82aOD/5030B <0.5 pg/L 11/09/2023 1,3-Dichloropropane SW 848 Method 8280D/5030B <0.5 pg/L 11/09/2023 1,4-Dichlorobenzene SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2023 2,2-Dichloropropane SW 840 Method 826OD15030B <0.5 pg/L 11/09/2023 ?-Chlorotoluene SW 846 Method 82BOD/5030B <0.5 pg/L 11/09/2023 4-Chlorotoluene SW 846 Method 826013/503013 <0.5 pg/L 11/09/2023 Benzene SW 646 Method BWOD/5030B <0.5 pg/L 11/09/2023 Bromobenzene SW 80 Method 828OD15030B <0.5 pg/L 11/09/2023 Bromochloromethane SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2023 Bromodichloromethane SW 84e Method 826OD15030B <0.5 pg/L 11/09/2023 Bromoform SW 046 Method 8280D/5030B <0.5 pg/L 11/09/2023 Bromomethane SW 8413 Method 82BOD/5030B <0.5 pg/L 11/09/2023 Carbon tetrachloride SW 646 Method 828013/503013 <0.5 pg/L 11/09/2023 Chlorobenzene SW 846 Method 82600/5030B <0.5 pg/L 11/09/2023 Chloroethane SW 846 Method 828013/503013 <0.5 pg/L 11/09/2023 Chloroform SW M Method 8MOD15030B <0.5 pg/L 11/09/2023 Chloromethane SW 848 Method 82BOD/5030B <0.5 pg/L 11/09/2023 cis-1,2-Dichloroethene SW 80 Method 826OD/5030B <0.5 pg/L 11/09/2023 cis-1,3-Dichloropropene SW 846 Method 82BOD/5030B <0.5pg/L 11/09/2023 Dibromochloromethane SW 846 Method 82eOD/5030B <0.5 pg/L 11/09/2023 Dibromomethane SW 846 Method 826013/50306 <0.5 pg/L 11/09/2023 Dichlorodifluoromethane SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2023 =thylbenzene SW 846 Method 8260D/5030B <0.5 ug/L 11/09/2023 Hexachlorobutadiene SW 846 Method 82BOD/5030B <0.5 pg/L 11/09/2023 Isopropylbenzene SW 846 Method 826OD/5030B <0.5 pg/L 11/09/2023 Report #:: 2023-25831 Page 29 of 33 SM ANALYTICAL & CONSULTING CHEMISTS Darling Ingredients - Rose Hill Post Office Box 1026 Rose Hill NC 28458 Attention: Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 0 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax info@environmentalchemists.com Date of Report: Dec 13, 2023 Customer PO #: Customer ID: 08100027 Report #: 2023-25631 Project ID: Monitoring Wells M+P Xylene SW MO Method 826OD/5030B <1.0 pg/L 11/09/2023 Methylene chloride SW 846 Method 82BOD15030B <0.5 pg/L 11/09/2023 Naphthalene SW 846 Method 8280D/5030B <0.5 pg/L 11/09/2023 n-Butylbenzene SW 846 Method 8260D/5030B <0.5 pg/L 11 /09/2023 n-Propylbenzene SW 846 Method 8260D15030B <0.5 pg/L 11/09/2023 ortho-Xylene SW 84B Method 82BOD/50308 <0.5 pg/L 11/09/2023 p4sopropyltoluene SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2023 sec-Butylbenzene SW 84B Method 826013/50308 <0.5 pg/L 11/09/2023 Styrene SW 846 Method 82BOD/5030B <0.5 pg/L 11/09/2023 1ert Butylbenzene SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2023 Tetrachloroethene SW 8" Method 826OD/5030B <0.5 pg/L 11/09/2023 Toluene SW 846 Method 8280D/5030B <0.5 pg/L 11/09/2023 Trans-1,2-Dichloroethene SW 846 Method 82BOD/50308 <0.5 pg/L 11/09/2023 Trans-1,3-dichloropropene SW 846 Method 8280D/5030B <0.5 pg/L 11/09/2023 Trichloroethene SW us Method 828013/50306 <0.5 pg/L 11/09/2023 Trichlorofluoromethane SW 848 Method 82BOD/5030B <0.5 pg/L 11/09/2023 Vinyl chloride SW 846 Method 82GOD15030B <0.5 pg/L 11/09/2023 Nitrate Nitrogen (Calc) Nitrite Nitrogen EPA 353.2, Rev. 2.0, 1993 0.02 mg/L 11/06/2023 Nitrate+Nitrite-Nitrogen EPA 353.2, Rev. 2.0, 1993 0.04 mg/L 11/08/2023 Nitrate Nitrogen subtraction Method 0.02 mg/L 12/12/2023 Total Nitrogen (Cale) Total Kjeldahl Nitrogen (TKN) EPA 351.2, Rev. 20, 1993 < 0.5 mg/L 11/10/2023 Total Nitrogen Totes N"en <0.5 mg/L 12/12/2023 Report #: 2023-25831 Page 30 or 33 6e-nviroc--_hem ANALYTICAL & CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 0 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax info@environmentalchemists.com Darling Ingredients - Rose Hill Date of Report: Dec 13, 2023 Post Office Box 1026 Customer PO #: Rose Hill NC 28458 Customer ID: 08100027 Attention: Report #: 2023-25631 Project ID: Monitoring Wells Lab ID Sample ID: Collect DaterTime Matrix Sampled by 23-62097 Site: MW-14A 11/4/2023 11:45 AM Water jcb/envirochem Test Method Results Date Analyzed Color Color Tan/Turbid 11/04/2023 Depth to water, ft. Depth to Water. Ft 6.5 feet 11/04/2023 Sodium EPA 200.7, Rev 4.4,1994 119 mg/L 11/16/2023 Sulfate EPA 300.0, Rev. 2.1, 1993 238 mg/L 11/07/2023 Ammonia Nitrogen EPA 350.1, Rev. 2.0,1993 < 0.2 mg/L 11/07/2023 Gallons bailed before sampling Gallons Bailed before sampling 5.0 gallons 11/04/2023 Odor Qualitative None 11/04/2023 Total Dissolved Solids (TDS) SM 2540 C-2015 1010 mg/L 11 /06/2023 Temperature SM 2550 B-2010 21.8 C 11/04/2023 pH SM 4500 H 8-2011 5.1 units 11/04/2023 Total Phosphorus SM 4WO P (F-H)-2011 < 0.04 mg/L 11/10/2023 Total Organic Carbon (TOC) SM 5310 B-2014 3.7 mg/L 11 /06/2023 Fecal Coliform SM 9222 D-2015 MF <1 Colonies/100ml- 11/04/2023 Chloride SM4500C1 E-2011 316 mg/L 11/08/2023 1, 1, 1,2-Tetrachloroethane SW 848 Method 82BOD15030B <0.5pg/L 11/09/2023 1,1,1-Trichloroethane SW 846 Method 826013/50308 <0.5 pg/L 11/09/2023 1,1,2,2-Tetrachloroethane SW 846 Method 82BOD15030B <0.5pg/L 11/09/2023 1,1,2-Trichloroethane SW 845 Method 82BOD15030B <0.5 pg/L 11/09/2023 1,1-Dichloroethane SW 848 Method 8280DI5030B <0.5 pg/L 11/09/2023 1,1-Dichloroethene SW 845 Method 8280DIS030B <0.5 pg/L 11/09/2023 1,1-Dichloropropene SW 80 Method 828013/5030B <0.5 pg/L 11/09/2023 1,2,3-Trichlorobenzene SW 846 Method 826013I5030B <0.5 pg/L 11/09/2023 1,2,3-Trichloropropane SW 846 Method 82600/5030B <0.5 pg/L 11/09/2023 1,2,4-Trichlorobenzene SW 846 Method 826013/50308 <0.5 pg/L 11/09/2023 1,2,4-Trimethylbenzene SW 848 Method B280D150306 <0.5 pg/L 11/09/2023 1,2-Dibromo-3-Chloropropane SW 80 Method 828010/5030B <1 pg/L 11/09/2023 Report 8:: 2023-25531 Page 31 of 33 F"P- -- 77 Environmental Chemists, Inc. envirochem6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax sM 255-A Wilmington Highway, Jacksonville, NC 28540 . 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS info Cei environmentalchemists com Darling Ingredients - Rose Hill Date of Report: Dec 13, 2023 Post Office Box 1026 Customer PO #: Rose Hill NC 28458 Customer ID: 08100027 Attention: Report #: 2023-25631 Project ID: Monitoring Wells 1,2-Dibromoethane SW 848 Method 82600/5030B <0.5 pg/L 11/09/2023 1,2-Dichlorobenzene SW 846 Method 8260D/5D308 <0.5 pg/L 11/09/2023 1,2-Dichloroethane SW 846 Method 8260D15030B <0.5 pg/L 11/09/2023 1,2-Dichloropropane SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2023 1,3,5-Trimethylbenzene SW 848 Method 8280D/5030B <0.5 pg/L 11/09/2023 1,3-Dichlorobenzene SW 848 Method 8260D/5030B <0.5 pg/L 11/09/2023 1,3-Dichloropropane SW 846 Method 826OD15030B <0.5 pg/L 11/09/2023 IA-Dichlorobenzene SW B46 Method 6260D/5030B <0.5 pg/L 11/09/2023 2,2-Dichloropropane SW 846 Method 8280D/5030B <0.5 pg/L 11/09/2023 2-Chlorotoluene SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2023 4-Chlorotoluene SW 846 Method 8260D/5030B <0.5 pg/L 11/0912023 Benzene SW 846 Method 8280D/5030B <0.5 pg/L 11/09/2023 Bromobenzene SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2023 Bromochloromethane SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2023 Bromodichloromethane SW 848 Method 8260D/5030B <0.5 pg/L 11/09/2023 Bromoform SW 846 Method 826013/50306 <0.5 pg/L 11/09/2023 Bromomethane SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2023 Carbon tetrachloride SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2023 Chlorobenzene SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2023 Chloroethane SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2023 Chloroform SW 846 Method 8260DJ5030B <0.5 pg/L 11/09/2023 Chloromethane SW 646 Method 826OD/5030B <0.5 pg/L 11/09/2023 cis-1,2-Dichloroethene SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2023 cis-1,3-Dichloropropene SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2023 Dibromochloromethane SW 846 Method 826DD/5030B <0.5 pg/L 11/09/2023 Dibromomethane SW 846 Method 82e0D/5030B <0.5 pg/L 11/09/2023 Dichlorodifluoromethane SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2023 ,cthylbenzene SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2023 Hexachlorobutadiene SW 848 Method 8260D/5030B <0.5 pg/L 11/09/2023 Isopropylbenzene SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2023 Report #: 2023-25831 Page 32 of 33 Environmental Chemists, Inc. envirochem 6602 Windmill Way, Wilmington, NC 28405 a 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 < 252.473.5702 Lab/Fax M' 255-A Wilmington Highway, Jacksonville, NC 28540 - 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS info@environmentalchemists.com Darling Ingredients - Rose Hill Post Office Box 1026 Rose Hill NC 28458 Attention: Date of Report: Dec 13, 2023 Customer PO #: Customer ID: 08100027 Report #: 2023-25631 Project ID: Monitoring Wells M+P Xylene SW 848 Method 82BOD/5030B <1.0 pg/L 11 /09/2023 Methylene chloride SW 846 Method 826013/50308 <0.5 pg/L 11/09/2023 Naphthalene SW 846 Method 826OD/5030B <0.5 pg/L 11/09/2023 n-Butylbenzene SW 846 Method 82GOD15030B <0.5 Ng/L 11/09/2023 n-Propylbenzene SW 848 Method 8280D/50308 <0.5 pg/L 11/09/2023 ortho-Xylene SW 846 Method 829OD/50308 <0.5 pg/L 11/09/2023 p-Isopropyltoluene SW 646 Method 8260D150308 <0.5 pg/L 11/09/2023 sec-Butylbenzene SW Us Method 8260D15030B <0.5 pg/L 11/09/2023 Styrene SW 846 Method 82BODI5030B <0.5 pg/L 11/09/2023 'tent-Butylbenzene SW NO Method 826OD/5030B <0.5 pg/L 11/09/2023 Tetrachloroethene SW 846 Method 828013/50308 <0.5 pg/L 11/09/2023 Toluene SW 845 Method 8260131503013 <0.5 pg/L 11/09/2023 Trans-1,2-Dichloroethene SW 846 Method 8260D150308 <0.5 pg/L 11/09/2023 Trans-1,3-dichloropropene SW 846 Method 828013/503013 <0.5 pg/L 11/09/2023 Trichloroethene SW 848 Method 82BOD/5030B <0.5 pg/L 11/09/2023 Trichlorofluoromethane SW 80 Method MOD/503013 <0.5 pg/L 11/09/2023 Vinyl chloride SW 846 Method 826013/50308 <0.5 pg/L 11/09/2023 Nitrate Nitrogen (Calc) Nitrite Nitrogen EPA353.2, Rev.2.0, 1993 < 0.02 mg/L 11/06/2023 Nitrate+Nitrite-Nitrogen EPA353.2, Rev. 2.0,1993 3.78 mg/L 11/08/2023 Nitrate Nitrogen Subtraction Method 3.78 mg/L 12/12/2023 Total Nitrogen (Caic) Total Kjeldahl Nitrogen (TKN) EPA351.2, Rev.2.0,1993 < 0.5 mg/L 11/10/2023 Total Nitrogen Total Nttrogen 3.78 mg/L 12/12/2023 Comment: ry Reviewed by: Report M: 2023.25631 Page 33 of 33 Environmental Chemist, Inc., Wilmington, NC Lab #94 Sample Receipt Checklist 6602 Windmill Way Wilmington, NC 28405 910.392.0223 �it ClientZPizu 0 (b — F/H Date: 0 3 Report Number: _ 2023-QSI Receipt of sample: ECHEM Pickup Client Delivery ❑ UPS ❑ Fed Ex ❑ Other ❑ ❑ YES 113 NO 10 N/A 1. Were custody seals present on the cooler? ❑ YES 113 NO 19 N/A 12. If custody seals were present, were they intact/unbroken? Original temperature upon receipt "C Corrected temperature upon receipt °C How temperature taken: ❑ Temperature Blank 0 Against Bottles IR Gun ID: Thomas Traceable S/N 210886869 IR Gun Correction Factor "C: 0.0 0 YES ❑ NO 3. If temperature of cooler exceeded VC, was Project Mgr./QA notified? 0 YES ❑ NO 4. Were proper custody procedures (relinquished/received) followed? 0 YES ❑ NO 5. Were sample ID's listed on the COC? 0 YES ❑ NO 6. Were samples ID's listed on sample containers? 0 YES ❑ NO 7. Were collection date and time listed on the COC? 0 YES ❑ NO 8. Were tests to be performed listed on the COC? 0 YES ❑ NO 9. Did samples arrive in proper containers for each test? 0 YES ❑ NO 10. Did samples arrive in good condition for each test? 0 YES ❑ NO 11. Was adequate sample volume available? 0 YES ❑ NO 12. Were samples received within proper holding time for requested tests? IN YES ❑ NO 13. Were acid preserved samples received at a pH of <2? ❑ YES ❑ NO 14. Were cyanide samples received at a pH >12? ❑ YES ❑ NO 15. Were sulfide samples received at a pH >9? YES ❑ NO 16. Were NH3/TKN/Phenol received at a chlorine residual of <0.5 m/L? ** ❑ YES ❑ NO 17. Were Sulfide/Cyanide received at a chlorine residual of <0.5 m/L? ❑ YES ❑ NO 18. Were orthophosphate samples filtered in the field within 15 minutes? * TOC/Volatiles are pH checked at time of analysis and recorded on the benchsheet. ** Bacteria samples are checked for Chlorine at time of analysis and recorded on the benchsheet. Sample Preservation: (Must be completed for any sample(s) incorrectly preserved or with headspace) Sample(s) were received incorrectly preserved and were adjusted accordingly by adding (circle one): H2SO4 HNO3 HCI NaOH Time of preservation: If more than one preservative is needed, notate in comments below Note: Notify customer service immediately for incorrectly preserved samples. Obtain a new sample or notify the state lab if directed to analyzed by the customer. Who was notified, date and time: Volatiles Sample(s) were received with headspace COMMENTS: DOC. QA.002 Rev 1 o CD CD 3 � 3 e3o CL N D7 C �C CL W `C N ' CL O in = A m =r 3 CL �. CD CO 3 0 Y � v r � 1 " O ' 3 � Co a o � (A N M CD CL r\ 3 Sample Type Composite G) 0 0 0 G7 n 0 0 G7 0 G) 0 G) 0 D 0 ) 0 or Grab G) T 0 �-u G) Li Container I'll (P or G) v 0 Chlorine \ mglL LAB ID O Cho NUMBER )( NONE �( HCL T X H2804 IT! CD )( /� HNO3 m N NAOH CL �( TRIO Z OTHER 0. 0 m m 0 0 0 0 N_ CA) N- Z n Z, 0 m° m o 3. CA) o• m a n 0 N o z N � � cn m m �, c � v v 0 v X vr", v CO m IQ 7 a M ur M 0 x 0 M 0 z to -1 0 0 O -f 0 z z n � 3 o m m < 3 O � O 3 �► C Z O v 3 i O M Lu 0 Z O 70 ,n X O v n ry 0 C v m z Z Me v NTT Q0 Z m �m D Z Z zD �r v x0 x t/) v NM M m T V, a > -I z �A Z V, # v V � N 10 ^ CCD 0 co CL n N rh o 0 CL 0 = 0 0 a CD :3 s 3 a v -I CL N fD go 0 �v w M w X 1 3 � CD a c w � 'G � M n co CL Sample Type Composite G) 0 G) 0 G) 0 G) 0 G) 0 G) 0 G) 0 G) 0 0 0 or Grab ` Container G) -0 G) "D G) -u G) ,D (P or G) v O Chlorine 1T mglL f3D NLAB ID �+ NUMBER �C )( NONE )( HCL )( X H2SO4 N M X (\ HNO3 C N NAOH O �( 1 Z OTHER O O CD m O O 0 (i v W iv o Z 0 0 x N O W --1 O CL a z Q 3 r CD 0 z 0 c m ITI D -4 o a 0 v eD v mLa d 5 12 CD LA: ID N N tD 2 O m O � T z O 0 0 z C) 3 3 c m m 1 r O 0 Ifl N 3 01 L C Z v CD T 3 = 0 m O Z 0 0 D�D Z �C O 90 n 0 ti 20 � d o c U 0 CD 3 CP M zZ rn v p0 n Z IT! ;M sZ Z ak DA Zr v x 0 x y v r M N M m a O `) z V *k V Verr N Z1D AE 0 A A a a X M A a n 0 o 0 = v (D o =h o M = a g Q g W. a m o. CL J 0 O �o r. .a s ffi 'A M 3 CL v Sample Type Composite 0 0 0 0 G) 0 G) n G) n 0 0 G) 0 G) 0 G) 0 or Grab Container '0 G) G) G) G) G) G) (P or G) v OChlorine mg/L 3 0� m JU LAB ID O NUMBER X NONE X HCL 'p X X H2504 In x HNO3 m C N NAOH f�D O C. X THIO z OTHER O O M sv O O 0 0 m W N O _ � m a �; w o m z r O v z y cn �. IT! n C C ca 3 ca � o v 0 m X � m RO a f%J H Z C z O O n 0 0 z z n 3 o M m "C $ r O o Ito y 4f L C z v 3 = 0 m m O m z0 0 O r6, z n v m z z M Z C X Z 9 M z D r 0 M 9 � VJ) ♦J V Z n 0 0 M D o cc CL � , a N N C r 3 v ci P M o v .a (A 0 N CL 3 111 Sample Type Composite 0 0 G) 0 G) 0 G) 0 G) 0 0 0 G) 0 0 0 0 0 or Grab Container -0 G) -o G) T 0 T 0 -0 G) -V G) - (P or G) v p Chlorine mg1L M N LAB ID _ -Q NUMBER d �( NONE X HCL a )( X H2SO4 N X HNO3 X C NAOHD.I CL X TRIO Z OTHER O O m Iv O O 0 0 W N Z n z S Cr 0 w o m a a r CD o H 7 (n v N (n D HI M cn M v v 0 v X w D CA RL Cl 7 Ila Ira N a 0 3 � 0 ,.r N S tD N H tD Z M z Z a O < Z p 0A0D T z O r Z O m m m 0 0 0 Z 0 Z n 0 3 m m O a z Z # C 6G ic o D � 0) a0 a _ 0 F• O D 2 /ram Z ch \ J I° O v = yrn n m CID -4 c�/) O < 4 � V N zID ^ 3 = O m pl Q Z 0 0 'i 0 ai Z � T 0 N O .m9 to a Lu N p P �A pNp p A 01 o 3 co � a v a Ic N CL 0 'a O D CO) ,. Cm m a C1 cD CL A , -fig r 3 sm � D) v � 0 Irr CD CD .0� - o C. a N m Sample Type Composite G) 0 G) 0 G) 0 0 0 G) 0 G) 0 G) 0 G) 0 G) 0 or Grab Container G) G) G) G (P or G) \ d Chlorine mglL LAB ID — O NUMBER NONE X HCL �O X >c H2SO4 N X P- HNO3 C N N NAOH a x THIO Z OTHER 0 0 m v O 0 Ci 0 w W N Z n Z 0 2. m Q O 3 w o C y D CD Z C y 13 < w cn A 0 c c 3 m co v v 0 v M m 10oi AO 0 o CL N CD 3 0 5a y N ID m ZZ O v <_ v X n O A T M Z O r m Z 0 `M m 1 0 z 0 � r p> m 0 a Z > Z o Z m m --4 Z v o = o r ID 0D = 0 Z m to O v = Nm n co m O V/ D p C Z cn o 0 V v W 4 Z INO ♦ I 0 Z z 0 ,n 0 X Z 0 n� m . S.mc 0 3. lAJID Ij 7 C D bl N Q A L N W 1 3 m 3 o n _� W 3 to N A p N oM 3 M fp � a a K tD n C' fD CL LV 0 h M .D CL mID n_ 1 � a v I (n f4 M c 3 i-0 c� D � O w� C C Z rD 4 cn M 3 n. 1 N O 0 V a p � CL O = nL m $ -t a o cn v Q .. IT 0 T). N m 2 �, C - `i771 Q � t m 1 v M F n O y� CD M M ` o c 1 � ? `�.► M a Sample Type Composite Q 0 G) 0 D 0 G) 0 G) 0 G) 0 G) 0 G) 0 G) n or Grab \ G) 0 G) -0 G) �-u �-o D -0 Container (P or G) v cChlorine M mg1L M N p LAB ID NUMBER )( NONE x HCL x X H2SO4 m N m C x HNO3 � A NAOH CL x THIO Z m OTHER O O (D m O O 0 0 N CA) N O O 2 2: m Cr ~; o 3 w � ° a z r o z 0 w ca :3cn m � _ cn C � m v v 0 v a N v n � m 0 o CL M n .�+ N � al A H' H N M z Z n v Z T N n v D O O O x m O` r m Z < O 40 -1 p • -j _j 0 � � 0> o>>zzgZ n o 3 m c m a z u Z v A D r O 7 0 z r = n CD o n = n Z N �a O v = "NM � � m a CO) c a o Z Z 'MO # r w V � N Z!O 0 3 = o m 41 O Z C 0 m D !C Z N O O c W = C 3 w N � � (rV L 64 I ^ -3 LJ y j R �J 0 p 08 3w- �v maN A b SD 0 C. o U) CD M 3 D c ` C Z v ch fD 3 � u` 1 CL n 0 0 0 fD Ncr 3 CD a 0 V G 3�•., CLeao m n Iw n `1• c v Y J ^ O ,e o \ c to CD ~ fl Q. ,m Sample Type Composite G) C) G) 0 G) 0 G) 0 G) 0 0 0 G) 0 O 0 or JG)- Grab \ IG;r G) G) T G)L-0 0 -0 G) � �C) G) G) T 'P o v 10 pp Chlorine N mglL (�1 LAB ID b� NUMBER X NONE )( HCL W X x H2SO4 y X HNO3 m C NNAOH O. OTHER .moo O O m O O 0 0 v W N 0 z 0 = M o CA)o C n a v 3 SD r CD 7 Z c v O �►0 c N � m m v 0 v v d v � n 0 y o a `° 0 7 n _ .. to m 3 N N H fD 2 m z Z n v m �T z N 0 v 0 0 m x a m Z 0 > c- m m o —1 0 0 � T rn >Z Z m m D z 1c Z v D r O v 0 z r = n CD n = 0 0 Z N O v n N 0 W C m �► O c s � o Z cn Z O � N Z m ^ 3 = O m _ O Z O 0 ,n -i �, a o !C Z oCL m� 0 0 3. w= N K 3 T 3 D � a to 3 to Z ;n N co A p N Q 0 r� l 0 m CL m ro CL cu N a o = '0) CD AL(A cr S a fD CL a m * - � C 0 ' 03 K O Ci O i� 3 CL v m ►c Sample Type Composite G) 0 G) n G) 0 G) 0 G) n G) 0 G) 0 G) 0 0 0 or Grab Container G) 'O G) -u G) G) -0 G) -0 Q 'O G) -0 G) -0 G) -0 (P or G) m ,. Chlorine mglL 3 0 O LAB ID NUMBER X NONE X HCL X X H2SO4 N X HNO3 m C NAOH W OTHER m O O m O 0 0pnj W N Z 0 Z C� m B o 3 w o CL ID n a cr CD r 0 z D CO) fl _ cn m Nm A v v 0 o X a 3 � m �tfl o QQ y C � a co n M N_ w :�A M 2 M ZZ a C G z v n O n O Z O r m z 1 n m 0 Ei 0 n > Z =O Z .. 3 m m Z Z as v 46 > 4• c n = I° O v = yM m CA 0 n Z Z � V V � v 10 Z = O m S1 Q Z 0 M O 5 O0 m Z R M N 0 ID n � m . k) < a o � 3 M N p' A � 3 3 7 N 9 N 0 pNp A O N N n CD M CL i C) n CD 0 a C co a m .Z7 CD n CD CL v � ram► N � fD fl1 Z �� fD N o n a In p CL o = m m m :3 =r m o o- t7 o a m r oC, � rt O 7 v e� n ` � O 7 0 0 t r to CD `° CL r Sample Type Composite G) 0 G) 0 G) 0 G) n G) 0 0 n G) n G) 0 G) n or Grab Container Gi -0 G) -0 G) -D G) -0 G) -0 G) -u G) -U 0 -0 G) � (P or G) d O^ Chlorine mg/L A 0 R )( `x FNB'E N171 C N NAOH =! Z CL �( TRIO OTHER O O M tv O O n 0 p) w Iv O Z S O S m Cr Er o CLa a v r rn o v_ z c N Ofu n a C � CD M v 0 C cn O m zZ nC v rn z—TT � N '0 0 n Z rn � K aM �Z 0 z "D A Zr n 0 x 2 `) N O N M n m T C] V, O z CVO m V� N 10 v M Q w co c� CL v M M .N. N � fD O1 zr" v Uf CD Q 3 m N a o T in v c ° -+� olu � CA 3 mm a cr o 'o .� C \r M , v N ^ a N a 7 C � i wn O l 6 3 CD � r Mr CL W Sample Type Composite G7n ,nn ,nn ,n00000G)0Q0G)n or Grab \ G7 -U Gi -U G) -0 0 -o G) 'O ,Q Gi -V Li -0 G) -0Container (P or G) OChlorine mglL N � O LAB ID NUMBER )( NONE �( HCL V X X H2SO4 N �( HNO3 X S� NAOH M p, X TRIO Z w OTHER O O m Ili O O 0 0 p�j W N o Z 0 p 2 m o w O o CL � a a Cr _ r cn 7 Z c N v fn O N � 3 m � v 0 v v Ia RO 0 � a o H CL s e� v N :r0 of O to N lD 2 M z Z a C v rn v Q 90 n� n v T TI Z O r m Z n m rn 0 n °aa°z Z m m O Z —4 M * o 3 = 0 r o a = 0 O v = CD yrn 0 (AC m O V) a o O at < w V� 10 ^Z i / 3 = o m R1 Q Z 0 T O • M 5- 0 0) Z MN 0 0 m 3 S.ma c 3 � w sw� ut w' 3 �O pNp O A N CL moo N O CL n o •0 = RG m v (D m � 3 m r S CL i rC a a m CL 0 o n � IUD � O ,t o '� 3 CL Sample Type Composite G) 0 G) 0 D 0 G) n G) n G) 0 G) n G) n G) 0 or Grab Container G) G) G) -0 G) -0 G) -0 G) -0 G) �J-9 G) "O (P or G) \ v Chlorine V� mg[L 3 LAB ID NUMBER X NONE x HCL )( }( H2SO4 y X HNO3 m C M. NAOH ~ CL X THIO z W OTHER O O m � O O 0 0 p0j W N O O 2 2: m Er w -u p M. CL D Dr CD CAv o z N m w c 3 m � o v 0 v m a CO) 0 n RL o CL U3 s N � � T ry N U! tD m ZZ a C 0 z e n 000 T TI Z O P O Z O -4 c. m m rn ° '5 o 0 � Mn a a O z g Z n o 3 m 3 m D z 3 Z Z v A M ? _ 0 r o D_ � Z cn to O o = Nrn n in m p c -A Z Z cn O *k v � w � V N to ♦ / 3 = O m O1 O Z O 'D O i a0a�i Z 0 N 4701 Ommi a m 0 9 is c 7 N fu M -n N J b o � 3 w _ kN A p 01