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HomeMy WebLinkAboutWQ0000485_Monitoring - 11-2023_20231219Monitoring Report Submittal Permit Number#* Name of Facility:* Month: * November Report Information Type * GW-59 Confirmation Email Address: Name of Submitter: * Signature: Date of submittal: Initial Review WQ0000485 Darling Ingredients - Rose Hill Year:* 2023 Upload Document* scan 2023-11 WQ0000485 GW-59 DIRH.pdf 5.1MB PDF Only Please upload one PDF containing all applicable monitoring reports (i.e., NDMR, NDAR-1, NDAR-2, NDMLR, GW-59). corey.Ianier@darlingii.com Corey Lanier Reviewer: Wanda.Gerald 12/19/2023 This will be filled in automatically Is the project number correct?* WQ0000485 Is the monitoring report accepted?* Yes No Regional Office* Wilmington Reviewer: _anonymous Review Date: 12/22/2023 DARLING 4--1 INGREDIENTS December 18, 2023 Division of Water Resources Attn: Information Processing Unit 1617 Mail Service Center Raleigh, NC 27699-1617 Re: Ground Water Quality Monitoring Report (GWQMR) Darling Ingredients — Rose Hill Permit WQ0000485 To whom it may concern, Please find enclosed the Groundwater Quality Monitoring Compliance Report for Surface Irrigation for the month of November 2023 for our Rose Hill Division. Should you require any additional information or wish to discuss this matter, please feel free to contact me at 910.289.2083 x 25119. Sincerely, $Lt4l M. Larry Holt General Manager cc: DI Regional Corporate Office SUBMIT FORM ON YELLOW PAPER ONLY • . . DEPARTMENT OF ENVIRONMENT 8, NATURAL RESOURCES GROUNDWATER QUALITY MONITORING: DIVISION OF WATER RESOURCES' -INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM • • 1617 MAIL SERVICE CENTER, RALEIGH, INC 27699-1617 Phone: 919-807-6306 FACILITY INFORMATION Pease Print crearly or Type PERMIT Number: WQ0000485 Expiration Date: 3/31/2025 Facility Name: Darling Ingredients - Rose Hill Non -Discharge UIC NPDES Other Permit Name (if different): Facility Address 469 Yellow Cut Rd. TYPE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑ Remediation: Infiltration Gallery Rose Hill, NC 28458 County Duplin (City) (5.... , X Spray Field El Remediation: Contact Person: Corey Lanier Telephone#: (910) 660-1173 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name No. of wells to be sampled 11 ❑ Water Source Heat Pump ❑ Other: SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW-1 Date sample collected: 11/4/2023 FIELD ANALYSES: WAS Well Depth: 12.46 ft. Well Diameter: 2 in. pH4500HB 5.20 units Temp. 000lo: z1.5 °C DRY at Depth to Water Level 82546: 5.5 Screened Interval: 12.46 ft. to 2.46 ft. Spec Cond 00094 uMhos time of Measuring Point is 1.17 ft. above land surface Relative M.P. Elevation: ft. Odor 00085: None sampling, Volume of water pumped/bailed before sampling: 5.0 gallons Appearance Clear chec� Samples for metals were collected unfiltered: X YES NO and field acidified: X YES NO here: LABORATORY INFORMATION Date sample analyzed: 11/04/2023-12/12/2023 Laboratory Name Environmental Chemists, Inc. Certification No. DWQ#94 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 <0.02 mg/L Pb - Lead 01051 ug/L Coliform: MF Fecal 31616 <1.0 /100mL Nitrate (NO3) as N 00620 0.43 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 <0.04 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 70300 121.00 mg/L Al - Aluminum 01105 mg/L Sodium 6.46 mg/L pH (Lab) oo403 5.20 units Ba - Barium 01007 ug/L TOC 00680 1.1 mg/L Ca - Calcium 00916 mg/L Chloride 00940 7 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total 01034 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron o1o45 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 59 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? E Yes (0) ❑ No (0) pecific Conductance 00095 uMhos K - Potassium 00937 mg/L VOC 78732 method # SM 6200C Total Ammonia 00610 <0.2 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen; NH3as N; Ammonia Nitrogen, Total) Mn - Manganese 01055 ug/L method # TKN as N 00625 <0.5 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% Larry Holt - General Manager Permittee (or Authorized Aqent) Name and Title - Please print or type GW-59 Rev.8/2013 SUBMIT FORM ON YELLOW PAPER ONLY • • • DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES GROUNDWATER QUALITY MONITORING: DIVISION OF WATER RESOURCES - INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM • • • 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: 919-807-6306 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: WQ0000485 Expiration Date: 3/31/2025 Facility Name: Darling Ingredients - Rose Hill Non -Discharge UIC Permit Name (if different): NPDES Other Facility Address: 469 Yellow Cut Rd. TYPE OF PERMITTED OPERATION BEING MONITORED Rose Hill, NC 28458 County Duplin ❑ Lagoon ❑ Remediation: Infiltration Gallery (City) X Spray Field Remediation: Contact Person: Corey Lanier Telephone#: (910) 660-1173 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name No. of wells to be sampled: 11 ❑ Water Source Heat Pump ❑ Other: from Permit) SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW-2 Date sample collected: 11/4/2023 FIELD ANALYSES: WAS Well Depth: 31.00 ft. Well Diameter: 2 in. pH4500HB 6.70 units Temp. 000lo 186 oC DRY at Depth to Water Level 82546. 12.8 ft below measuring point Screened Interval: 30.15 ft. to 20.15 ft. Spec. Cond. 00094: µMhos time of Measuring Point is 3 _ft. above land surface Relative M.P. Elevation ft. Odor00085: None sampling, check Volume of water pumped/bailed before sampling: 5.0 gallons Appearance Tan/Clear here: Samples for metals were collected unfiltered: X YES ❑ NO and field acidified: X YES ❑ NO LABORATORY INFORMATION Date sample analyzed: 11/04/2023-12/12/2023 Laboratory Name: Environmental Chemists, Inc. Certification No. DWQ#94 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 <0.02 mg/L Pb - Lead 01051 ug/L Coliform: MF Fecal 31616 <1.0 /100mL Nitrate (NO3) as N 00620 0.17 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 <0.04 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 70300 292.00 mg/L Al -Aluminum 01105 mg/L Sodium 11.2 mg/L pH (Lab) 00403 6.70 units Ba - Barium 01007 ug/L TOC 00680 1 1 mg/L Ca - Calcium 00916 mg/L Chloride 00940 13 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total 01034 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 27 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? ■ Yes (0) ❑ No (0) pecific Conductance 00095 µMhos K - Potassium 00937 mg/L VOC 78732: method # SM 6200C Total Ammonia 00610 <0.2 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen; NH3asN; Ammonia Nitrogen, Total) Mn - Manganese 01055 ug/L method # TKN as N 00625 <0.5 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% Larry Holt - General Manaqer Permittee (or Authorized Aqent) Name and Title - Please print or type GW-59 Rev.8/2013 SUBMIT FORM ON YELLOW PAPER ONLY • • • DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES GROUNDWATER QUALITY MONITORING: DIVISION OF WATER RESOURCES - INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM • • • 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: 919-807-6306 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: WQ0000485 Expiration Date: 3/31/2025 Facility Name: Darling Ingredients - Rose Hill Non -Discharge UIC NPDES Other Permit Name (if different): Facility Address: 469 Yellow Cut Rd TYPE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑ Remediation: Infiltration Gallery Rose Hill, NC 28458 County Duplin (State) (zip) X Spray Field ❑ Remediation: Contact Person: Corey Lanier Telephone#: (910) 660-1173 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name No. of wells to be sampled: 11 ❑ Water Source Heat Pump ❑ Other: (from Permit) SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW-4 Date sample collected: 11/4/2023 FIELD ANALYSES: WAS Well Depth: 28.93 ft. Well Diameter: 2 in. pH4500HB 7.00 units Temp. 000lo 19.9 °C DRY at Depth to Water Level 82546: 6.4 ft below measuring point Screened Interval: 28.93 ft. to 18.93 ft. Spec. Cond. 00094: µMhos time of Measuring Point is 3 ft. above land surface Relative M.P. Elevation: ft. Odor 00085 None sampling, check Volume of water pumped/bailed before sampling: 5.0 gallons Appearance Clear/Tan here: Samples for metals were collected unfiltered: X YES ❑ NO and field acidified: X YES ❑ NO LABORATORY INFORMATION Date sample analyzed: 11/04/2023-12112/2023 Laboratory Name Environmental Chemists, Inc. Certification No. DWQ#94 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 <0.02 mg/L Pb - Lead 01051 ug/L Coliform: MF Fecal 31616 <1 /100mL Nitrate (NO3) as N 00620 <0.02 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 <0.04 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units) )issolved Solids -.Total 70300 211.00 mg/L Al -Aluminum 01105 mg/L Sodium 8.25 mg/L pH (Lab) 00403 7.00 units Ba - Barium 01007 ug/L TOC 00680 1.10 mg/L Ca - Calcium oo916 mg/L Chloride 00940 <5.0 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total 01034 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 <5.0 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? 0 Yes (0) ❑ No (0) Specific Conductance 00095 µMhos K - Potassium 00937 mg/L VOC 78732 method # SM 6200C Total Ammonia 00610 <0.2 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen; NH3 as N; Ammonia Nitrogen, Total) Mn - Manganese 01055 ug/L method # TKN as N 00625 <0.5 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% Larry Holt - General Manager Permittee (or Authorized Aqent) Name and Title - Please print or type GW-59 Rev.8/2013 DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES GROUNDWATER QUALITY MONITORING: DIVISION OF WATER RESOURCES - INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM 1617 MAIL SERVICE CENTER. RALEIGH, NC 27699.1617 Phone: 919-807-6306 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: WQ0000485 Expiration Date: 3/31/2025 Facility Name: Darling Ingredients - Rose Hill Non -Discharge UIC NPDES Other Permit Name (if different): Facility Address: 469 Yellow Cut Rd. TYPE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑ Remediation: Infiltration Gallery Rose Hill, NC 28458 County Duplin (city) (state) (zip) X Spray Field ❑ Remediation: Contact Person Corey Lanier Telephone#: (910) 660-1173 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name: No. of wells to be sampled: 11 ❑ Water Source Heat Pump ❑ Other: (from Permit) SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW-7A Date sample collected: 11/4/2023 FIELD ANALYSES: WAS Well Depth: 16 ft. Well Diameter: 2 in. pH4500HB 3.66 units Temp. 000lo: 27.5 eC DRY at Depth to Water Level 82546: 6.0 ft. below measuring point Screened Interval: 16 ft. to 6 ft. Spec. Cond. 00094: µMhos time of Measuring Point is 2.42 ft. above land surface Relative M.P. Elevation: ft. Odor 00085: None sampling, Volume of water pumped/bailed before sampling: 5.0 gallons Appearance Tan/Clear check here: SamDles for metals were collected unfiltered: X YES n NO and field acidified: X YES ❑ NO LABORATORY INFORMATION Date sample analyzed: 11/04/2023-12/12/2023 Laboratory Name: Environmental Chemists, Inc. Certification No. DWQ#94 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 <0.02 mg/L Pb - Lead 01051 ug/L Coliform: MF Fecal 31616 <1 /100mL Nitrate (NO3) as N 00620 <0.02 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 <0.04 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): (Dissolved Solids:Total 70300 264.00 mg/L Al -Aluminum 01105 mg/L Sodium 12.3 mg/L pH (Lab) 00403 3.66 units Ba - Barium 01007 ug/L TOC 00680 1 mg/L Ca - Calcium 00916 mg/L Chloride 00940 128 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total 01034 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 23 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? 0 Yes (0) ❑ No (0) Specific Conductance 00095 µMhos K - Potassium 00937 mg/L VOC 78732: method # SM 6200C Total Ammonia 00610 <0.2 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen; NH3 as N; Ammonia Nitrogen, Total) Mn - Manganese 01055 ug/L , method # TKN as N 00625 <0.5 mg/L Ni - Nickel 01067 ug/L method # For Remedlation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Ettluent Iotal vucs: mg/L vvL; Kemoval r. Larry Holt - General Manager Permittee (or Authorized Agent) Name and Title - Please print or type • • DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES GROUNDWATER QUALITY MONITORING: • • • • DIVISION OF WATER RESOURCES - INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: 919-807-6306 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: W00000485 Expiration Date: 3/3112025 Facility Name: Darling Ingredients - Rose Hill Non -Discharge UIC NPDES Other Permit Name (if different): Facility Address: 469 Yellow Cut Rd. TYPE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑ Remediation: Infiltration Gallery Rose Hill, NC 28458 County Duplin c;,;, (Stale) X Spray Field ❑ Remediation: Contact Person: Corey Lanier Telephone#: (910) 660-1173 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name Field 5 - damaged by farm equip / to replace No. of wells to be sampled: 11 ❑ Water Source Heat Pump ❑ Other: (from Permit) SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW-8A Date sample collected: 11/4/2023 FIELD ANALYSES: WAS Well Depth: 16 ft. Well Diameter: 2 in. pH4500HB 4.60 units Temp. 000lo: 21.2 °C DRY at Depth to Water Level 82546: 7.0 ft. below measuring point Screened Interval: 16 ft. to 6 ft Spec. Cond. 00094: µMhos time of Measuring Point is 2.5 ft. above land surface Relative M.P. Elevation: ft. Odor 00085 None sampling, Volume of water pumped/bailed before Sam 0 5.0 gallons Appearance Tan/Clear check Samples for metals were collected unfiltered: X YES NO and field acidified: X YES ❑ NO here: LABORATORY INFORMATION Date sample analyzed: 11/04/2023-12/12/2023 Laboratory Name: Environmental Chemists, Inc. Certification No. DWQ#94 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 <0.02 mg/L Pb - Lead 01051 ug/L Coliform: MF Fecal 31616 <1.0 /100mL Nitrate (NO3) as N 00620 0.39 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 0.1 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 70300 54.00 mg/L Al - Aluminum 01105 mg/L Sodium 1.41 mglL pH (Lab) 00403 4.60 units Ba - Barium 01007 ug/L TOC 00680 0.90 mg/L Ca - Calcium 00916 mg/L Chloride 00940 <5 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total 01034 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 23 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? 0 Yes (0) ❑ No (0) Specific Conductance 00095 µMhos K - Potassium 00937 mg/L VOC 78732: method # SM 6200C Total Ammonia 00610 <0.2 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen; NH3as N; Ammonia Nitrogen, Total) Mn - Manganese 01055 ug/L , method # TKN as N 00625 <0.5 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOG Removal /• Larry Holt - General Manager Permittee (or Authorized Agent) Name and Title - Please print or type • • • DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES GROUNDWATER QUALITY MONITORING: • • • DIVISION OF WATER RESOURCES -INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: 919-607-6306 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: W00000485 Expiration Date: 3/31/2025 Facility Name: Darling Ingredients - Rose Hill Non -Discharge UIC NPDES Other Permit Name (if different): Facility Address: 469 Yellow Cut Rd. TYPE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑ Remediation: Infiltration Gallery Rose Hill, NC 28458 County Duplin tcm: (state) 17:P1 X Spray Field ❑ Remediation: Contact Person: Corey Lanier Telephone#: (910) 660-1173 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name No of wells to be sampled: 11 ❑ Water Source Heat Pump ❑ Other: (from Permit) SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW-9 Date sample collected: 11/4/2023 FIELD ANALYSES: WAS Well Depth: 13.73 ft. Well Diameter: 2 in pH4500HB 5.90 units Temp. 000lo: 17.8 °C DRY at Depth to Water Level 62546: 6.2 ft. below measuring point Screened Interval: 13.73 ft to 3.73 ft. Spec. Cond. 00094: µMhos time of Measuring Point is 3.80 ft. above land surface Relative M.P. Elevation: ft. Odor 00065: None sampling, Volume of water pumped/bailed before sampling: 5.0 gallons Appearance Tan/Turbid check Samples for metals were collected unfiltered: X YES NO and field acidified: X YES ❑ NO here:❑ LABORATORY INFORMATION Date sample analyzed: 11/04/2023-12/12/2023 Laboratory Name: Environmental Chemists, Inc. Certification No. DWQ#94 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 0.05 mg/L Pb - Lead o1o51 ug/L Coliform: MF Fecal 31616 <1.0 /100mL Nitrate (NO3) as N 00620 0.23 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 <0.04 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 70300 278.00 mg/L Al - Aluminum 01105 mg/L Sodium 7.10 mg/L pH (Lab) 00403 5.90 units Ba - Barium 01007 ug/L TOC oomo 30.6 mg/L Ca - Calcium 00916 mg/L Chloride 00940 27 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total 01034 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 29 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? E Yes (0) ❑ No (0) Specific Conductance 00095 µMhos K - Potassium 00937 mg/L VOC 78732: method # SM 6200C Total Ammonia 00610 <0.2 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen; NH3 as N; Ammonia Nitrogen, Total) Mn - Manganese 01055 ug/L , method # TKN as N 00625 0.8 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mgtL voc Removal i• Larry Holt - General Manager Permiltee (or Authorized Agent) Name and Title - Please print or type DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES GROUNDWATER QUALITY MONITORING: DIVISION OF WATER RESOURCES - INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: 919-807-6306 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: WQ0000485 Expiration Date. 3/31/2025 Facility Name: Darling Ingredients - Rose Hill Non -Discharge UIC NPDES Other Permit Name (if different): Facility Address: 469 Yellow Cut Rd, TYPE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑ Remediation: Infiltration Gallery Rose Hill, NC 28458 County Duplin r t,,j (Stale) (zip) X Spray Field ❑ Remediation: Contact Person. Corey Lanier Telephone#: (910) 660-1173 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name No. of wells to be sampled: 11 ❑ Water Source Heat Pump ❑ Other: (from Permit) SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW-10A Date sample collected: 11/4/2023 FIELD ANALYSES: WAS Well Depth: 16 ft. Well Diameter: 2 in. pH4500HB 3.55 units Temp. 000lc 19.6 °C DRY at Depth to Water Level 82546: 5.3 ft. below measuring point Screened Interval: 16 ft. to 6 ft. Spec. Cond 00094: µMhos time of Measuring Point is 3 ft. above land surface Relative M.P. Elevation: ft. Odor 00085: None sampling, Volume of water pumped/bailed before sampling: 5.0 gallons Appearance Clear check SamDleS for metals were collected unfiltered: X YES I-1 NO and field acidified: X YES n NO here LABORATORY INFORMATION Date sample analyzed: 11/04/2023-12/12/2023 Laboratory Name: Environmental Chemists, Inc Certification No. DWQ#94 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 <0.02 mg/L Pb - Lead 01051 ug/L Coliform: MF Fecal 31616 <1 /100mL Nitrate (NO3) as N 00620 <0.02 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 0.07 mg/L (Note Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units) )issolved Solids:Total 70300 793.00 mg/L Al -Aluminum 01105 mg/L Sodium 114 mg/L pH (Lab) 00403 3.55 units Ba - Barium 01007 ug/L TOC 00680 3.8 mg/L Ca - Calcium 00916 mg/L Chloride 00940 322 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total 01034 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 143 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? ■ Yes (0) ❑ No (0) Specific Conductance 00095 µMhos K - Potassium 00937 mg/L VOC 78732 method # SM 6200C Total Ammonia 00610 0.40 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen NH3asN Ammonia Nitrogen, Total) Mn - Manganese 01055 ug/L , method # TKN as N 00625 0.60 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal Larry Holt - General Manager Permittee (or Authorized Agent) Name and Title - Please print or type 0 DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES GROUNDWATER QUALITY MONITORING: DIVISION OF WATER RESOURCES - INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: 919.807-6306 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: W00000485Expiration Date: 3/31/2025 Facility Name: Darling Ingredients - Rose Hill Non -Discharge UIC NPDES Other Permit Name (if different): Facility Address: 469 Yellow Cut Rd. TYPE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑ Remediation: Infiltration Gallery Rose Hill, NC 28458 County Duplin lcn,, X Spray Field ❑ Remediation: Contact Person: Corey Lanier Telephone#: (910) 660-1173 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name No. of wells to be sampled: 11 ❑ Water Source Heat Pump ❑ Other: (from Permit) SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW-11A Date sample collected: 11/4/2023 FIELD ANALYSES: WAS Well Depth: 16 ft. Well Diameter: 2 in. pH4500HB 4.70 units Temp. 000lc zo.s °C DRY at Depth to Water Level 82546: 7.5 Screened Interval: 16 ft. to 6 ft. Spec. Cond. 00094: uMhos time of Measuring Point is 3.3 ft. above land surface Relative M.P. Elevation: ft. Odor 00065: None sampling, Volume of water pumped/bailed before sampling: 5.0 gallons Appearance Clear/Tan chec here: Samples for metals were collected unfiltered: X YES NO and field acidified: X YES NO LABORATORY INFORMATION Date sample analyzed: 11/04/2023-12/12/2023 Laboratory Name: Environmental Chemists, Inc. Certification No. DWQ#94 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 <0.02 mg/L Pb - Lead 01051 ug/L Coliform: MF Fecal 31616 <1.0 /100mL Nitrate (NO3) as N 00620 0.34 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 <0.04 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 70300 490.00 mg/L Al - Aluminum 01105 mg/L Sodium 62.9 mg/L pH (Lab) 00403 4.70 units Ba - Barium 01007 ug/L TOC 00680 2,50 mg/L Ca - Calcium 00916 mg/L Chloride 00940 121 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total 01034 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 161.0 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? MYes (0) ❑ No (0) pecific Conductance 00095 uMhos K - Potassium 00937 mg/L VOC 78732: method # SM 6200C Total Ammonia 00610 <0.2 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen; NH3 as N; Ammonia Nitrogen, Total) Mn - Manganese 01055 ug/L , method # TKN as N 00625 <0.50 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Enluent Total VOcs: mg/L vuc Kemoval ro Larry Holt - General Manager Permittee (or Authorized Agent) Name and Title - Please print or type DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES GROUNDWATER QUALITY MONITORING: DIVISION OF WATER RESOURCES -INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: 919-807-6306 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: WQ0000485 Expiration Date: 3/31/2025 Facility Name: Darling Ingredients - Rose Hill Non -Discharge UIC NPDES Other Permit Name (if different). Facility Address: 469 Yellow Cut Rd. TYPE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑ Remediation: Infiltration Gallery Rose Hill, NC 28458 County Duplin ;City) (State) (zip) X Spray Field ❑ Remediation: Contact Person: Corey Lanier Telephone#: (910) 660-1173 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name: No. of wells to be sampled: 11 ❑ Water Source Heat Pump ❑ Other: (from Permit) SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW-12B Date sample collected: 11/4/2023 FIELD ANALYSES: WAS Well Depth: 16 ft. Well Diameter: 2 in. pH4500HB: 3.91 units Temp. 000lo: 21.2 °C DRY at Depth to Water Level 82546: 6.8 ft. below measuring point Screened Interval: 20 ft. to 10 ft. Spec. Cond. 00094: uMhos time of Measuring Point is 3 ft. above land surface Relative M.P. Elevation: ft. Odor 00085: None sampling, Volume of water pumped/bailed before sampling: 5.0 gallons Appearance None check here: Samples for metals were collected unfiltered: X YES M NO and field acidified: X YES NO LABORATORY INFORMATION Date sample analyzed: 11/04/2023-12/12/2023 Laboratory Name: Environmental Chemists, Inc. Certification No. DWQ#94 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 <0.02 mg/L Pb - Lead 01051 ug/L Coliform: MF Fecal 31616 <1 /100mL Nitrate (NO3) as N 00620 0.14 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 0.15 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 70300 385.00 mg/L At -Aluminum olim mg/L Sodium 68.7 mg/L pH (Lab) 00403 3.91 units Ba - Barium 01007 ug/L TOC 00680 1.70 mg/L Ca - Calcium oo916 mg/L Chloride 00940 120 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total 01034 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 124 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? E Yes (0) ❑ No (0) Specific Conductance 00095 uMhos K - Potassium 00937 mg/L VOC 78732: method # SM 6200C Total Ammonia 00610 <0.2 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen; NH3as N; Ammonia Nitrogen, Total) Mn - Manganese 01055 ug/L , method # TKN as N 00625 0.50 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% Larry Holt - General Manager Permittee (or Authorized Agent) Name and Title - Please print or type DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES GROUNDWATER QUALITY MONITORING: DIVISION OF WATER RESOURCES- INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: 919-807-6306 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: WQ0000485 Expiration Date: 3/31/2025 Facility Name: Darling Ingredients - Rose Hill Non -Discharge UIC NPDES Other Permit Name (if different): Facility Address: 469 Yellow Cut Rd. TYPE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑ Remediation: Infiltration Gallery Rose Hill, NC 28458 County Duplin (State) (zip) X Spray Field ❑ Remediation: Contact Person: Corey Lanier Telephone#: (910) 660-1173 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name: No. of wells to be sampled: 11 ❑ Water Source Heat Pump ❑ Other: (from Permit) SAMPLING INFORMATION If WELL 'WELL ID NUMBER (from Permit): MW-13A Date sample collected: 11/4/2023 FIELD ANALYSES: WAS Well Depth: 16 ft. Well Diameter: 2 in. 8 pHasooHB 4.70 units Temp. o0010: 21.C DRY at Depth to Water Level 82546: 7.4 ft. below measuring point Screened Interval: 16 ft. to 6 ft. Spec. Cond. 00094: uMhos time of Measuring Point is 3 ft. above land surface Relative M.P. Elevation: ft. Odor 00085: None sampling, 'Volume of water pumped/bailed before sampling: 5.0 gallons Appearance Clear/Tan check here: SamDles for metals were collected unfiltered: X YES I —I NO and field acidified: X YES NO LABORATORY INFORMATION Date sample analyzed: 11/04/2023-12/12/2023 Laboratory Name: Environmental Chemists, Inc. Certification No. DWQ#94 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 0.02 mg/L Pb - Lead olo51 ug/L Coliform: MF Fecal 31616 <1 /100mL Nitrate (NO3) as N 00620 0.02 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 <0.04 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): Dissolved Solids:Total 70300 35.00 mg/L Al - Aluminum oil o5 mg/L Sodium 4.25 mg/L pH (Lab) 00403 4.70 units Ba - Barium 01007 ug/L TOC 00680 0.60 mg/L Ca - Calcium 00916 mg/L Chloride 00940 <5 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total 01034 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 8.00 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? E Yes (0) ❑ No (0) Specific Conductance 00095 uMhos K - Potassium 00937 mg/L VOC 78732: method # SM 6200C Total Ammonia 00610 <0.20 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen; NH3 as N; Ammonia Nitrogen, Total) Mn - Manganese 01055 ug/L , method # TKN as N 00625 <0.50 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% • • DEPARTMENT OF ENVIRONMENT 8r NATURAL RESOURCES GROUNDWATER QUALITY MONITORING: • • • • DIVISION OF WATER RESOURCES -INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: 919-807-6306 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: W00000485 Expiration Date: 3;31i=15 Facility Name: Darling Ingredients - Rose Hill Non -Discharge UIC NPDES Other Permit Name (if different): Facility Address: 469 Yellow Cut Rd. TYPE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑ Remediation: Infiltration Gallery Rose Hill, NC 28458 County Duplin (Stale) (zip) X Spray Field ❑ Remediation: Contact Person. Corey Lanier Telephone#: (910) 660-1173 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name No. of wells to be sampled: 11 ❑ Water Source Heat Pump ❑ Other: (from Permit) SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW-14A Date sample collected 11/4/2023 FIELD ANALYSES: WAS Well Depth: 16 ft. Well Diameter: 2 in. pH45WHB 5.10 units Temp. 000lc 21.8 °C DRY at Depth to Water Level 82546: 6.5 ft. below measuring point Screened Interval: 10 ft. to 2.5 ft. Spec. Cond. oo094: µMhos time of Measuring Point is 3 ft. above land surface Relative M.P. Elevation: ft. Odor 00085: None sampling, Volume of water pumped/bailed before sampling: 5.0 gallons Appearance Tan/Turbid check here: Samples for metals were collected unfiltered: X YES NO and field acidified: X YES n NO LABORATORY INFORMATION Date sample analyzed: 11/04/2023-12/12/2023 Laboratory Name: Environmental Chemists, Inc. Certification No. DWQ#94 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 <0.02 mg/L Pb - Lead 01051 ug/L Coliform: MF Fecal 31616 <1.0 /100mL Nitrate (NO3) as N 00620 3.78 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 <0.04 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 70300 1010.00 mg/L Al -Aluminum 01105 mg/L Sodium 119 mg/L pH (Lab) 00403 5.10 units Ba - Barium 01007 ug/L TOC omm 3.70 mg/L Ca - Calcium 00916 mg/L Chloride 00940 316 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total 01034 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 238 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? N Yes (0) ❑ No(0) Specific Conductance 00095 µMhos K - Potassium 00937 mg/L VOC 78732: method # SM 6200C Total Ammonia oo6lo <0.20 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen; NH3as N; Ammonia Nitrogen, Total) Mn - Manganese 01055 ug/L , method # TKN as N 00625 <0.50 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% GW-59A COMPLIANCE REPORT FORM Permit # W00000485 (Submit one each mmniloring period with GW-59 forms.) I Enter date monitoring results were due. (1213112023) Will this monitoring report (GW-59 and GW-59A) be submitted after the established due date? No 2 Was any required information missing on the GW-59 report forms? No IF the answer to question 1 or 2 is "YES", list in the space provided below the well identification number(s) and explain the problems encountered in obtaining the required information. MW-8A was damaged by farm equipment and is scheduled to be closed and replaced by Register Well Co, INC; moving the replacement well 10'due North per DEQ direction. 3 Are any of the monitor wells in need of repair or maintenance (damaged casing, unlocked or missing cap, missing identification plate, area overgrown, etc.)? If the answer is "Yes ", contact the Regional Office for guidance, No 4 Are any monitored constituents equal to or above the established standards? YES If the answer to question 4 is "NO", skip to section 8. If the answer to question 4 is "YES" list the affected wells individually with constituent(s) and concentration(s) exceeding standards in the space provided below: SEE ATTACHED GROUNDWATER MONITORING WELL 2 YR EXCEEDANCE HISTORY REPORT 5 For the constituents identified In question 4 above, have standards been exceeded previously for the same constituent(s) In the same well(s) in the last two years? YES 1f the answer to question 5 is 'NO", skip to section 8. If the answer to question 5 is "YES", list in the space provided below, each well with constituent(s) exceeding standards, concentration(s) reported, and sample collection date for each occurrence (for the last two years) SEE ATTACHED GROUNDWATER MONITORING WELL 2 YR EXCEEDANCE HISTORY REPORT 6 Are the monitoring wells listed In section 5 located at or beyond the review boundary? YES If the answer is "YES", a groundwater quality problem may be occurring. CONTACT THE REGIONAL OFFICE IMMEDIATELY FOR GUIDANCE. N the answer is "NO", monitoring wells may be improperly located; contact the Regional Office. 7 Is the permittee implementing previously approved actions required by the Division involving this groundwater quality problem? YES If the answer to question 7 is 'YES", describe those actions in the space provided below. If the answer to question 7 is "NO" contact the Rettional Office within 90 days: an evaluation may be required to determine the impact the waste disposal system is havinct at the review and compliance boundaries surrounding this facility. Failure to do so may sub'ect the parmittee to a Notice of Violation. Fines, and/or enatties. Additional monitoring was performed to identify constituents of TOC in MW No 9 The facility has been communicating with Mr. Geoff Kegley in the Wilmington Regional Office. 8 The person completing this portion (G W-59A) of the monitoring reportshould sign below and submit this form with GW59 forms forrequired wells to the address provided at the top ofthe current G W-59 form. I hereby acknowledge that the above information was evaluated and the information submitted in this report (Compliance Report GW-59A) Is true and complete to the best of my knowledge. 63(� 4# lz 1jV z3 - Signature fPermltteef(or Authorized Agent) Date t Valley Proteins, Inc - Rose Hill (WQ0000485) Groundwater Monitoring Well 2 Year Exceedance History Report TDS 500 10A 14A November-23 793 1010 July-23 816 1270 March-23 804 1310 November-22 833 944 July-22 772 1280 March-22 783 1100 November-21 801 1230 July-21 706 1010 pH 6.5-8.5 1 2 4 7A 8A 9 10A 11A 12B 13A 14A November-23 5 7 7 3.66 4.6 5.9 3.55 4.7 3.91 4.7 5.1 July-23 5.20 5.50 5.80 5.30 5.10 6.30 3.70 5.40 4.60 4.70 4.70 March-23 6.40 6.30 6.30 3.86 4.50 6.70 4.10 4.50 4.20 4.80 5.00 November-22 5.60 6.30 3.86 4.20 6.00 3.67 4.10 3.70 4.40 4.70 July-22 6.40 6.40 6.3 5.1 5.3 6.4 4.2 4.6 4 5.1 4.9 March-22 6.40 5.9 4.7 4.6 4.6 4.4 4.2 4.7 5.2 November-21 5.50 4.30 4.50 6.30 4.00 4.30 4.20 4.20 5.00 July-21 5.00 6.10 5.60 4.90 4.60 5.90 4.70 4.60 5.40 5.00 TOC 10 9 November-23 322 July-23 46.9 March-23 33 November-22 27.6 July-22 45.1 March-22 34.9 November-21 26.4 July-21 25.9 Chloride 250 10A 14A November-23 322 316 July-23 337 361 March-23 350 November-22 305 350 July-22 261 356 March-22 294 325 November-21 353 July-21 42s7 275 ANALYTICAL & CONSULTING CHEMISTS F"01-7 -71 Darling Ingredients - Rose Hill Post Office Box 1026 Rose Hill NC 28458 Attention: Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 - 910.392.0223 Lab - 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 - 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 - 910.347.5843 Lab/Fax info@cnvironmentalchemists.com Date of Report: Dec 13, 2023 Customer PO #: Customer ID: 08100027 Report #: 2023-25631 Project ID: Monitoring Wells Lab ID Sample ID: 23-62087 Site: MW-1 Test Collect Date/Time 11/4/2023 11:25 AM Method Matrix Sampled by Water jcb/envirochem Results Date Analyzed Color color Clear 11/04/2023 Depth to water, ft. Depth to water. Ft 5.5 feet 11/04/2023 Sodium EPA200.7, Rev 4.4,1994 6.46 mg/L 11/16/2023 Sulfate EPA 300.0, Rev. 2.1.1993 59 mg/L 11/07/2023 Ammonia Nitrogen EPA 350.1, Rev. 2.0, 1993 < 0.2 mg/L 11/07/2023 Gallons bailed before sampling Gallons Balled before sampling 5.0 gallons 11/04/2023 Odor Qualitative None 11/04/2023 Total Dissolved Solids (TDS) see 2540 C-2015 121 mg/L 11/06/2023 Temperature SM2550 B-2010 21.5 C 11/04/2023 pH SM 4500 H B-2011 5.2 units 11/04/2023 Total Phosphorus SM 450o P (F-H)-2011 < 0.04 mg/L 11/10/2023 Total Organic Carbon (TOC) SM 5310 B-2014 1.1 mg/L 11/0612023 Fecal Coliform SM 9=2 D-2015 MF <1 Colonies/100mL 11/04/2023 Chloride SM4500 Cl E-2011 7 mg/L 11/08/2023 1, 1, 1,2-Tetrachloroethane SW 648 Method 8280D/5030B <0.5 pg/L 11/09/2023 1,1,1-Tdchloroethane SW 846 Method 8260DIS030B <0.5 pg/L 11/09/2023 1,1,2,2-Tetrachloroethane SW 846 Method 826013I5030B <0.5 pg/L 11/09/2023 1,1,2-Trichloroethane SW $46 Method 8260D15030B <0.5 pg/L 11/09/2023 1, 1 -Dichloroethane SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2023 1,1-Dichloroethene SW So Method 8260131503013 <0.5 pg/L 11/09/2023 1,1-Dichloropropene SW 846 Method 8280D15030B <0.5 pg/L 11/09/2023 1,2,3-Tdchlorobenzene SW 846 Method 626oD►5030B <0.5 pg/L 11/09/2023 1,2,3-Trichloropropane SW 846 Method 825013/50306 <0.5 pg/L 11/09/2023 1,2,4-Tdchlorobenzene SW 846 Method 8260D/50308 <0.5 pg/L 11/09/2023 1,2,4-Tdmethylbenzene SW e46 Method 8250DI5030B <0.5 pg/L 11/09/2023 1,2-Dibromo-3-Chloropropane SW 846 Method 82ND15030B <1 pg/L 11/09/2023 Report #.: 2023-25631 Page 1 of 33 77 Environmental Chemists, Inc. envirochem 6602 Windmill Way, Wilmington, NC 28405 - 910.392.0223 Lab - 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 - 252.473.5702 Lab/Fax sM 255-A Wilmington Highway, Jacksonville, NC 28540 - 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS info@environmentalchemists.com Darling Ingredients - Rose Hill Date of Report: Dec 13, 2023 Post Office Box 1026 Customer PO #: Rose Hill NC 28458 Customer ID: 08100027 Attention: Report #: 2023-25631 Project ID: Monitoring Wells 1,2-Dibromoethane SW 846 Method 8280D/5030B <0.5 pg/L 11/09/2023 1,2-Dichlorobenzene SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2023 1,2-Dichloroethane SW W Method 82BOD15030B <0.5 pg/L 11/09/2023 1,2-Dichloropropane SW 948 Method 8260D/50308 <0.5 pg/L 11/09/2023 1,3,5-Trimethylbenzene SW 846 Method 826013/503013 <0.5 pg/L 11/09/2023 1,3-Dichlorobenzene SW 846 Method 826oD/5030B <0.5 pg/L 11/09/2023 1,3-Dichloropropane SW 846 Method 826013/503013 <0.5 pg/L 11/09/2023 1,4-Dichlorobenzene SW 846 Method 826OD15030B <0.5 pg/L 11/09/2023 2,2-Dichloropropane SW We Method 826OD15030B <0.5 pg/L 11/09/2023 2-Chlorotoluene SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2023 4-Chlorotoluene SW 846 Method 8260D/5030B <0.5 pg/L 11 /09/2023 Benzene SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2023 Bromobenzene SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2023 Bromochloromethane SW 846 Method 826oDi5030B <0.5 pg/L 11/09/2023 Bromodichloromethane SW US Method 826013/50308 <0.5 pg/L 11/09/2023 Bromoform SW 848 Method 82600/5030B <0.5 pg/L 11 /09/2023 Bromomethane SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2023 Carbon tetrachloride SW ea Method 8260D/5030B <0.5 pg/L 11/09/2023 Chlorobenzene SW 846 Method 826oD/5030B <0.5 pg/L 11/09/2023 Chloroethane SW 80 Method 8280DI5030B <0.5 pg/L 11/09/2023 Chloroform SW 846 Method 82e0D/5030B <0.5 pg/L 11/09/2023 Chloromethane SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2023 cis-1,2-Dichloroethene SW 846 Method 82e0D/5030B <0.5 pg/L 11/09/2023 cis-1,3-Dichloropropene SW 846 Method 8260D15030B <0.5 pg/L 11/09/2023 Dibromochloromethane SW 846 Method 8290D/5030B <0.5 pg/L 11/09/2023 Dibromomethane SW 846 Method B280D/5030B <0.5 pg/L 11/09/2023 Dichlorodifluoromethane SW So Method 8280D/5030B <0.5 pg/L 11 /09/2023 Ethylbenzene S►nr M6 Method 8260D/5030B <0.5 pg/L 11/09/2023 Hexachlorobutadiene SW 84e Method e280D/5030B <0.5 pg/L 11/09/2023 Isopropylbenzene SW 846 Method 82BOD15030B <0.5 pg/L 11/09/2023 Reportk 2023-25631 Page 2 of 33 -77 envirochem SM� ANALYTICAL & CONSULTING CHEMISTS Darling Ingredients - Rose Hill Post Office Box 1026 Rose Hill NC 28458 Attention: Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 0 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax info@environmentalchemists.com Date of Report: Dec 13, 2023 Customer PO #: Customer ID: 08100027 Report #: 2023-25631 Project ID: Monitoring Wells M+P Xylene SW e46 Method 826DD/50308 <1.0 pg/L 11/09/2023 Methylene chloride SW 846 Method 82BOD/50306 <0.5 pg/L 11/09/2023 Naphthalene SW NO Method 82BOD/50308 <0.5 pg/L 11/09/2023 n-Butylbenzene SW 846 Method 8260DI5030B <0.5 pg/L 11/09/2023 n-Propylbenzene SW 048 Method 8260D/5030B <0.5 pg/L 11/09/2023 ortho-Xylene SW 846 Method 8260D/50308 <0.5 pg/L 11/09/2023 p-Isopropyltoluene SW 846 Method 826OD/50308 <0.5 pg/L 11/09/2023 sec-Butylbenzene SW 846 Method 826OD/50309 <0,5 pg/L 11/09/2023 Styrene SW US Method 8280D/5030B <0.5 pg/L 11/09/2023 teft Butylbenzene SW W6 Method 8260D/5030B <0.5 pg/L 11/09/2023 Tetrachloroethene SW 846 Method 826013/50308 <0.5 pg/L 11/09/2023 Toluene SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2023 Trans-1,2-Dichloroethene SW 846 Method 8260D/50305 <0.5 pg/L 11/09/2023 Trans-1,3-dichloropropene SW Me Method 826013/50306 <0.5 pg/L 11/09/2023 Trichloroethene SW US Method 8260DIS030B <0.5 NgIL 11/09/2023 Trichlorofluoromethane SW 846 Method MOD15030B <0.5 pg/L 11/09/2023 Vinyl chloride SW e46 Method 826OD/5030B <0.5 pg/L 11 /09/2023 Nitrate Nitrogen (Calc) Nitrite Nitrogen EPA353.2, Rev. 2.0, 1993 < 0.02 mg/L 11/06/2023 Nitrate+Nitrite-Nitrogen EPA 353.2, Rev. 2.0. 1993 0.43 mg/L 11/08/2023 Nitrate Nitrogen Subtraction Method 0.43 mg/L 12/12/2023 Total Nitrogen (Calc) Total Kjeldahl Nitrogen (TKN) EPA 351.2, Rev. 2.0, 1993 < 0.5 mg/L 11/10/2023 Total Nitrogen Total Nitrogen <0.5 mg/L 12/12/2023 Report *: 2023-25831 Page 3 of 33 SM� ANALYTICAL & CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 - 910.347.5843 Lab/Fax info@environmentalchemists.com Darling Ingredients - Rose Hill Date of Report: Dec 13, 2023 Post Office Box 1026 Customer PO #: Rose Hill NC 28458 Customer ID: 08100027 Attention: Report #: 2023-25631 Project ID: Monitoring Wells Lab ID Sample ID: Collect Date/Time Matrix Sampled by 23-62088 Site: MW-2 11/4/2023 11:05 AM Water jcb/envirochem Test Method Results Date Analyzed Color Color Tan/Clear 11/04/2023 Depth to water, ft. Depth to Water, Ft 12.8 feet 11/04/2023 Sodium EPA 200.7, Rev 4.4. 1994 11.2 mg/L 11 /16/2023 Sulfate EPA300.0, Rev. 2.1,1993 27 mg/L 11/07/2023 Ammonia Nitrogen EPA350.1, Rev.7-0, 1993 < 0.2 mg/L 11/07/2023 Gallons bailed before sampling Gallons Bailed before sampling 5.0 gallons 11/04/2023 Odor Qualitative None 11/04/2023 Total Dissolved Solids (TDS) SM 2540 C-2015 292 mg/L 11/06/2023 Temperature SM 2550 B-2010 18.6 C 11/04/2023 pH SM 4500 H B-2011 6.7 units 11/04/2023 Total Phosphorus SM 4500 P (F-H)-2011 < 0.04 mg/L 11 /10/2023 Total Organic Carbon (TOC) SM53108-2014 1.1 mg/L 11/06/2023 Fecal Coliform SM 9=2 D-2015 MF <1 Colonies/100ml- 11/04/2023 Chloride SM4500 Cl E-2011 13 mg/L 11 /08/2023 1, 1, 1,2-Tetrachloroethane SW Me Method8260D/5030B <0.6pg/L 11/09/2023 1, 1, 1 -Trichloroethane SW 80 Method 62600/5030B <0.5 pg/L 11/09/2023 1,1,2,2-Tetrachloroethane SW846Method 8280D/5030B <0.5pg/L 11/09/2023 1,1,2-Trichloroethane SW 546 Method 8260D/5030B <0.5 pg/L 11/09/2023 1,1-Dichloroethane SW 846 Method 626OD150308 <0.5 pg/L 11/09/2023 1,1-Dichloroethene sw 846 Method 82BOD15030B <0.5 pg/L 11/09/2023 1, 1 -Dichloropropene SW 846Method 8260D150308 <0.5 pg/L 11/09/2023 1,2,3-Trichlorobenzene SW 846 Method 82e0D/50308 <0.5 pg/L 11/09/2023 1,2,3-Tdchloropropane SW 846 Method 8280DI5030B <0.5 pg/L 11/09/2023 1,2,4-Trichlorobenzene SW 846 Method 828oD/5030B <0.5 Ng/L 11/09/2023 1,2,4-Trimethylbenzene SW 846 Method 826OD15030B <0.5 pg/L 11/09/2023 1,2-Dibromo-3-Chloropropane SW 546 Method 826OD150308 <1 pg/L 11/09/2023 Report P.: 2023-25631 Page 4 of 33 F"057 77 Environmental Chemists, Inc. envirochem 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax sM 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS info(a)environmentalchemists com Darling Ingredients - Rose Hill Post Office Box 1026 Rose Hill NC 28458 Attention: Date of Report: Dec 13, 2023 Customer PO M Customer ID: 08100027 Report M 2023-25631 Project ID: Monitoring Wells 1,2-Dibromoethane swage Method 82BOD15030B <0.5 pg/L 11/09/2023 1,2-Dichlorobenzene SW B46 Method 826013/503013 <0.5 pg/L 11/09/2023 1,2-Dichloroethane SW B46 Method 8260D/5030B <0.5 pg/L 11/09/2023 1,2-Dichloropropane SW B46 Method 8280DI5030B <0.5 pg/L 11/09/2023 1,3,5-Tdmethylbenzene SW 846 Method 8260DI5030B <0.5 pg/L 11/09/2023 1,3-Dichlorobenzene SW 846 Method 026OD/5030B <0.5 pg/L 11/09/2023 1,3-Dichloropropane SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2023 1,4-Dichlorobenzene SW 848 Method 82GOD15030B <0.5 pg/L 11/09/2023 2,2-Dichloropropane SW 846 Method 826OD15030B <0.5 pg/L 11/09/2023 2-Chlorotoluene SW 846 Method 826OD/5030B <0.5 gg/L 11/09/2023 4-Chlorotoluene SW W Method 8260D/5030B <0.5 pg/L 11/09/2023 Benzene SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2023 Bromobenzene SW 80 Method 82BOD/5030B <0.5 pg/L 11/09/2023 Bromochloromethane SW 848 Method 82BOD/5030B <0.5 pg/L 11109/2023 Bromodichloromethane SW 846 Method 828013/503013 <0.5 pg/L 11/09/2023 Bromoform SW 848 Method 826OD/5030B <0.5 pg/L 11/09/2023 Bromomethane SW 846 Method 82BOD/5030B <0.5 pg/L 11/09/2023 Carbon tetrachloride SW 846 Method 82BOD/5030B <0.5 pg/L 11109/2023 Chlorobenzene SW 846 Method 8260DI5030B <0.5 pg/L 11/09/2023 Chloroethane SW 80 Method 82BOD/5030B <0.5 ug/L 11/09/2023 Chloroform SW 846 Method 8280DI5030B <0.5 pg/L 11/09/2023 Chloromethane SW 846 Method 6280D/5030B <0.5 pg/L 11/09/2023 cis-1,2-Dichloroethene SW 046 Method 82BOD/5030B <0.5 pg/L 11/09/2023 cis-1,3-Dichloropropene SW 846 Method 8280D/5030B <0.5 pg/L 11 /09/2023 Dibromochloromethane SW 846 Method 825013/5030B <0.5 ug/L 11/09/2023 Dibromomethane SW B46 Method 8260DI5030B <0.5 pg/L 11/09/2023 Dichlorodifluoromethane SW 846 Method 82BOD/5030B <0.5 pg/L 11/09/2023 Ethylbenzene SW 846 Method 6260DI5030B <0.5 ug/L 11/09/2023 Hexachlorobutadiene SW 80 Method 828OD15030B <0.5 pg/L 11/09/2023 Isopropylbenzene SW 846 Method 82BOD/5030B <0.5 pg/L 11/09/2023 Report*. 2023-25631 Page 5 of 33 F01,07 —, -�"7 Environmental Chemists, Inc. envirochem 6602 Windmill Way, Wilmington, NC 28405 . 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax sM 255-A Wilmington Highway, Jacksonville, NC 28540 C 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS info@environmentalchemists.com Darling Ingredients - Rose Hill Post Office Box 1026 Rose Hill NC 28458 Attention: Date of Report: Dec 13, 2023 Customer PO #: Customer ID: 08100027 Report #: 2023-25631 Project ID: Monitoring Wells M+P Xylene SW 848 Method 826OD15030B <1.0 pg/L 11/09/2023 Methylene chloride SW 846 Method 826oD/5030B <0.5 pg/L 11/09/2023 Naphthalene SW 846 Method 826013/503013 <0.5 pg/L 11/09/2023 n-Butylbenzene SW 046 Method 8260D/5030B <0.5 pg/L 11/09/2023 n-Propylbenzene SW 848 Method 8260D15030B <0.5 pg/L 11/09/2023 ortho-Xylene SW 846 Method 826OD15030B <0.5 pg/L 11/09/2023 p-Isopropyltoluene SW 848 Method 826013/503013 <0.5 pg/L 11/09/2023 sec-Butylbenzene SW 845 Method 8260D/5030B <0.5 pg/L 11/09/2023 Styrene SW 848 Method 8260D/5030B <0.5 pg/L 11/09/2023 tert-Butylbenzene SW 646 Method 8260D/50308 <0.5 pg/L 11/09/2023 Tetrachloroethene SW 846 Method 8260DI50308 <0.5 pg/L 11/09/2023 Toluene SW 846 Method 8260D/50306 <0.5 pg/L 11/09/2023 Trans-1,2-Dichloroethene SW 848 Method 8280DIS030B <0.5 pg/L 11/09/2023 Trans-1,3-dichloropropene SW846Method 8280D/5030B <0.5pg/L 11/09/2023 Trichloroethene SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2023 Trichlorofluoromethane SW 846 Method 8260/50306 <0.5 pg/L 11/09/2023 Vinyl chloride SW 646 Method 8260D/5030B <0.5 pg/L 11/09/2023 Nitrate Nitrogen (Calc) Nitrite Nitrogen EPA 353.2, Rev. 2.0,1993 < 0.02 mg/L 11 /06/2023 Nitrate+Nitrite-Nitrogen EPA 353.2, Rev. 2.0, 1993 0.17 mg/L 11/08/2023 Nitrate Nitrogen Subtraction Method 0.17 mg/L 12/12/2023 Total Nitrogen (Calc) Total Kjeldahl Nitrogen (TKN) EPA 351.2, Rev. 20,1993 < 0.5 mg/L 11/10/2023 Total Nitrogen Tit Nitrogen <0.5 mg/L 12/12/2023 Report #.: 2023-25631 Page 6 of 33 envirochem sM� ANALYTICAL & CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 - 910.392.0223 Lab - 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 - 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 - 910.347.5843 Lab/Fax info@environmentalchemists.com Darling Ingredients - Rose Hill Date of Report: Dec 13, 2023 Post Office Box 1026 Customer PO #: Rose Hill NC 28458 Customer ID: 08100027 Attention: Report #: 2023-25631 Project ID: Monitoring Wells Lab ID Sample ID: Collect Daterrime Matrix Sampled by 23-62089 Site: MW-4 11/4/2023 10:30 AM Water jcb/envirochem Test Method Results Date Analyzed Color color Cleadran 11 /04/2023 Depth to water, ft Depth to Water, Ft 6.4 feet 11 /04/2023 Sodium EPA200.7, Rev4.4,1994 8.25 mg/L 11/16/2023 Sulfate EPA 300.0, Rev. 2.1.1993 <5 mg/L 11 /07/2023 Ammonia Nitrogen EPA 350.1, Rev. 2.0. 1993 < 0.2 mg/L 11/07/2023 Gallons bailed before sampling Gallons Bailed before sampling 5.0 gallons 11/04/2023 Odor Qualitative None 11 /04/2023 Total Dissolved Solids (TDS) SM 2540 C-2015 211 mg/L 11/06/2023 Temperature SM2550 B-2o10 19.9 C 11/04/2023 pH SM 4500 H B-2011 7.0 units 11/04/2023 Total Phosphorus SM 4500 P (F-H)-2011 < 0.04 mg/L 11 /10/2023 Total Organic Carbon (TOC) SM 5310 8-2014 1.1 mg/L 11/06/2023 Fecal Coliform SM 9222 D-2015 MF <1 Colonies/100ml- 11/04/2023 Chloride SM4500 Cl E-2011 < 5 mg/L 11/08/2023 1, 1, 1,2-Tetrachloroethane SW846Method 8260D/5030B <0.5pg/L 11/09/2023 1,1,1 Trichloroethane SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2023 1,1,2,2-Tetrachloroethane SW 846 Method 8260DIS030B <0.5 pg/L 11/09/2023 1,1,2-Trichloroethane SW 848 Method 82SOD15030B <0.5 pg/L 11/09/2023 1,1-Dichloroethane SW W6 Method 8280DI5030B <0.5 pg/L 11/09/2023 1,1-Dichloroethene SW 84e Method 8280DI5030B <0.5 pg/L 11/09/2023 1,1-Dichloropropene SW 846 Method 82BOD/5030B <0.5 pg/L 11/09/2023 1,2,3-Trichlorobenzene SW 846 Method 8280D/5030B <0.5 pg/L 11/09/2023 1,2,3-Trichloropropane SW 848 Method 8260DIS030B <0.5 pg/L 11/09/2023 1,2,4-Trichlorobenzene SW 846 Method 8280D/5030B <0.5 pg/L 11/09/2023 1,2,4-Trimethylbenzene SW US Method 8260D/5030B <0.5 pg/L 11/09/2023 1,2-Dibromo-3-Chloropropane SW 846 Method 8260D/5030B <1 tig/L 11/09/2023 Report #:: 2023-25631 Page 7 of 33 -1 -,qq7 i5H1 ANALYTICAL & CONSULTING CHEMISTS Darling Ingredients - Rose Hill Post Office Box 1026 Rose Hill NC 28458 Attention: Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax info(cuenvironmentalchemists.com Date of Report: Dec 13, 2023 Customer PO #: Customer ID: 08100027 Report #: 2023-25631 Project ID: Monitoring Wells 1,2-Dibromoethane SW 846 Method 62BOD/5030B <0.5 pg/L 11/09/2023 1,2-Dichlorobenzene SW 846 Method 8260DIS030B <0.5 pg/L 11/09/2023 1,2-Dichloroethane SW 846 Method 8260DI5030B <0.5 pg/L 11/09/2023 1,2-Dichloropropane SW B46 Method 828OD/5030B <0.5 pg/L 11/09/2023 1,3,5-Trimethylbenzene SW 848 Method 826OD/5030B <0.5 pg/L 11/09/2023 1,3-Dichlorobenzene SW 846 Method 8260/503013 <0.5 pg/L 11/09/2023 1,3-Dichloropropane SW 846 Method 82BOD/5030B <0.5 pg/L 11/09/2023 1,4-Dichlorobenzene SW 846 Method 82BOD/5030B <0.5 pg/L 11/09/2023 2,2-Dichloropropane SW 846 Method MOD15030B <0.5 pg/L 11/09/2023 2-Chlorotoluene SW 846 Method 8MOD15030B <0.5 pg/L 11/09/2023 4-Chlorotoluene SW 846 Method 826OD/5030B <0.5 pg/L 11/09/2023 Benzene SW 846 Method 82BOD/5030B <0.5 pg/L 11/09/2023 Bromobenzene SW 848 Method 826ODi5030B <0.5 pg/L 11/09/2023 Bromochloromethane SW 846 Method 826OD/5030B <0.5 pg/L 11/09/2023 Bromodichloromethane SW 846 Method 82BOD/5030B <0.5 pg/L 11/09/2023 Bromoform SW 846 Method 82BOD/5030B <0.5 pg/L 11/09/2023 Bromomethane SW 846 Method 82BOD/5030B <0.5 pg/L 11/09/2023 Carbon tetrachloride SW 846 Method 626OD/50308 <0.5 pg/L 11/09/2023 Chlorobenzene SW 846 Method 82BOD/5030B <0.5 pg/L 11/09/2023 Chloroethane SW 846 Method 82BOD150308 <0.5 pg/L 11/09/2023 Chloroform SW 848 Method 8280D/5030B <0.5 pg/L 11/09/2023 Chloromethane SW 846 Method 82BOD/5030B <0.5 pg/L 11/09/2023 cis-1,2-Dichloroethene SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2023 cis-1,3-Dichloropropene SW 846 Method 826OD15030B <0.5 pg/L 11/09/2023 Dibromochloromethane SW 846 Method 82BOD/5030B <0.5 pg/L 11/09/2023 Dibromomethane SW 846 Method 8280D/5030B <0.5 pg/L 11/09/2023 Dichlorodifluoromethane SW 846 Method 826013/50308 <0.5 pg/L 11/09/2023 Ethylbenzene SW 846 Method 82BOD/5030B <0.5 pg/L 11/09/2023 Hexachlorobutadiene SW 846 Method 826OD/50308 <0.5 pg/L 11/09/2023 Isopropylbenzene SW 846 Method 826OD/5030B <0.5 pg/L 11/09/2023 Report *: 2023-26531 Page 8 of 33 ro"07 -71 Environmental Chemists, Inc. envirochem 6602 Windmill Way, Wilmington, NC 28405 - 910.392.0223 Lab - 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 - 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS info@environmentalchemists.com Darling Ingredients - Rose Hill Date of Report: Dec 13, 2023 Post Office Box 1026 Customer PO #: Rose Hill NC 28458 Customer ID: 08100027 Attention: Report #: 2023-25631 Project ID: Monitoring Wells M+P Xylene SW 848 Method 828DD/5030B <1,0 pg/L 11/09/2023 Methylene chloride SW 846 Method 8250D/5030B <0.5 pg/L 11/09/2023 Naphthalene SW 848 Method 828OD/5030B <0.5 pg/L 11/09/2023 n-Butylbenzene SW 80 Method 826OD/5030B <0.5 pg/L 11/09/2023 n-Propylbenzene SW 80 Method 826013/503013 <0.5 pg/L 11/09/2023 ortho-Xylene SW 846 Method 8260DI5030B <0.5 pg/L 11/09/2023 p-Isopropyltoluene SW 848 Method 8260D/5030B <0.5 pg/L 11/09/2023 sec-Butylbenzene SW 848 Method 8260DI5030B <0.5 pg/L 11/09/2023 Styrene SW 848 Method 826OD/5030B <0.5 pg/L 11/09/2023 tert Butylbenzene SW 848 Method 8260D/50308 <0.5 pg/L 11/09/2023 Tetrachloroethene SW 848 Method 82BOD15030B <0.5 pg/L 11/09/2023 Toluene SW 846 Method 8260D15030B <0.5 pg/L 11/09/2023 Trans-1,2-Dichloroethene SW 846 Method 82BOD150308 <0.5 pg/L 11/09/2023 Trans-1,3-dichloropropene SW 846 Method 826013/503013 <0.5 pg/L 11/09/2023 Trichloroethene SW 846 Method 8260D15030B <0.5 pg/L 11/09/2023 Trichlorofluoromethane SW 846 Method 8280D1503013 <0.5 pg/L 11/09/2023 Vinyl chloride SW 846 Method 826013/503013 <0.5 pg/L 11/09/2023 Nitrate Nitrogen (Calc) Nitrite Nitrogen EPA 353.2. Rev.2.0, 1993 < 0.02 mg/L 11/06/2023 Nitrate+Nitrite-Nitrogen EPA 353.2, Rev.2.0,1993 < 0.02 mg/L 11/08/2023 Nitrate Nitrogen Subtraction Method <0.02 mg/L 12/12/2023 Total Nitrogen (Calc) Total Kjeldahl Nitrogen (TKN) EPA 351.2, Rev. 2.0,1993 < 0.5 mg/L 11/10/2023 Total Nitrogen Total If"en <0.5 mg/L 12/12/2023 Report*: 2023-25831 Page 9 of 33 v ANALYTICAL & CONSULTING CHEMISTS Darling Ingredients - Rose Hill Post Office Box 1026 Rose Hill NC 28458 Attention: Lab ID Sample ID: 23-62090 Site: MW-7A Test Color Depth to water, ft. Sodium Sulfate Ammonia Nitrogen Gallons bailed before sampling Odor Total Dissolved Solids (TDS) Temperature pH Total Phosphorus Total Organic Carbon (TOC) Fecal Coliform Chloride 1,1,1,2-Tetrach loroethane 1,1,1-Tdchloroethane 1,1,2,2-Tetrachloroethane 1,1,2-Tdchloroethane 1, 1 -Dichloroethane 1,1-Dichloroethene 1,1-Dichloropropene 1,2,3-Trichlorobenzene 1,2, 3-Trichloropropane 1,2,4-Trichlorobenzene 1,2,4-Trimethylbenzene 1,2-Dibromo-3-Chloropropane Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 - 910.392.0223 Lab - 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 - 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 - 910.347.5843 Lab/Fax info@environmentalchemists.com Date of Report: Dec 13, 2023 Customer PO #: Customer ID: 08100027 Report #: 2023-25631 Project ID: Monitoring Wells Collect Date/Time Matrix Sampled by 11/4/2023 12:15 PM Water jcb/envirochem Method Color Depth to Water, Ft. EPA 200.7, Rev 4.4,1994 EPA 300.0, Rev. 2.1,1993 EPA350.1, Rev. 2.0,1993 Gallons Bailed before sampling Qualitative SM 2540 C-2015 SM 2550 B-2010 SM 450D H B-2011 SM 4500 P (F-H)-2011 SM 5310 B-2014 SM 9222 D-2015 MF SM4500 Cl E-2011 SW 846 Method 8280D/5030B SW 846 Method 8260D/5030B SW 846 Method 8280D/5030B SW 846 Method 8260D/5030B SW 846 Method 8260D/5030B SW 846 Method 8260DIS0308 SW 848 Method 6250D/5030B SW S46 Method 8280D15030B SW 846 Method 8260D/5030B SW 846 Method 828013/5030B SW 846 Method 8280D/5030B SW 846 Method 8280D/5030B Results Date Analyzed Tan/Clear 11/04/2023 6.0 feet 11/04/2023 12.3mg/L 11/16/2023 23 mg/L 11 /07/2023 < 0.2 mg/L 11 /07/2023 5.0gallons 11/04/2023 None 11/04/2023 264 mg/L 11/06/2023 20.9 C 11/04/2023 3.66est. units 11/04/2023 < 0.04 mg/L 11 /10/2023 1.0 mg/L 11 /06/2023 <1 Colonies/100ml- 11/04/2023 128 mg/L 11/08/2023 <0.5 pg/L 11/09/2023 <0.5 pg/L 11 /09/2023 <0.5 pg/L 11/09/2023 <0.5 pg/L 11/09/2023 <0.5 pg/L 11/09/2023 <0.5 pg/L 11/09/2023 <0.5 pg/L 11/09/2023 <0.5 pg/L 11/09/2023 <0.5 pg/L 11/09/2023 <0.5 pg/L 11/09/2023 <0.5 pg/L 11/09/2023 <1 pg/L 11/09/2023 Report #.: 2023-25631 Page 10 of 33 000'- envirochem ANALYTICAL & CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 a 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax info@environmentalchemists.com Darling Ingredients - Rose Hill Date of Report: Dec 13, 2023 Post Office Box 1026 Customer PO #: Rose Hill NC 28458 Customer ID: 08100027 Attention: Report #: 2023-25631 Project ID: Monitoring Wells 1,2-Dibromoethane SW 846 Method 8280D/5030B <0.5 pg/L 11/09/2023 1,2-Dichlorobenzene SW 846 Method 826013/50308 <0.5 pg/L 11/09/2023 1,2-Dichloroethane SW 848 Method 6260D/5030B <0.5 µg/L 11/09/2023 1,2-Dichloropropane SW 848 Method 8260D/5030B <0.5 pg/L 11/09/2023 1,3,5-Trimethylbenzene SW 846 Method 8280D/5030B <0.5 pg/L 11/09/2023 1,3-Dichlorobenzene SW 84e Method 8260D/50308 <0.5 pg/L 11/09/2023 1,3-Dichloropropane SW 846 Method 826013/503013 <0.5 pg/L 11/09/2023 1,4-Dichlorobenzene SW 846 Method 828013/50308 <0.5 pg/L 11/09/2023 2,2-Dichloropropane SW 846 Method 8260D/503013 <0.5 pg/L 11/09/2023 2-Chlorotoluene SW 848 Method 8260DIS030B <0.5 pg/L 11/09/2023 4-Chlorotoluene SW 846 Method 8260/503013 <0.5 pg/L 11/09/2023 Benzene SW 846 Method 828OD15030B <0.5 pg/L 11/09/2023 Bromobenzene SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2023 Bromochloromethane SW 848 Method 8260D/5030B <0.5 pg/L 11/09/2023 Bromodichloromethane SW 846 Method 8260D/50308 <0.5 pg/L 11/09/2023 Bromoform SW 846 Method 826013/503013 <0.5 pg/L 11/09/2023 Bromomethane SW 848 Method 828013/503013 <0.5 pg/L 11/09/2023 Carbon tetrachloride SW 846 Method 828013/5030B <0.5 pg/L 11/09/2023 Chlorobenzene SW 846 Method 8280D/5030B <0.5 pg/L 11 /09/2023 Chloroethane SW 846 Method 826OD15030B <0.5 pg/L 11 /09/2023 Chloroform SW 848 Method 8280D15030B <0.5 pg/L 11/09/2023 Chloromethane SW 846 Method 82e013/503013 <0.5 pg/L 11/09/2023 cis-1,2-Dichloroethene SW 846 Method 8280D/5030B <0.5 pg/L 11/09/2023 cis-1,3-Dichloropropene SW 846 Method 826OD15030B <0.5 pg/L 11/09/2023 Dibromochloromethane SW 846 Method 8260DI5030B <0.5 pg/L 11/09/2023 Dibromomethane SW 846 Method 8280D/5030B <0.5 pg/L 11/09/2023 Dichlorodifluoromethane SW 846 Method 826013/50306 <0.5 pg/L 11109/2023 Ethylbenzene SW 846 Method 8280D/5030B <0.5 pg/L 11/09/2023 Hexachlorobutadiene SW 80 Method 8290D/5030B <0.5 pg/L 11/09/2023 Isopropylbenzene SW 848 Method 8280DI5030B <0.5 pg/L 11/09/2023 Report P: 2023-25831 Page 11 of 33 6M1 L 4- ANALYTICAL & CONSULTING CHEMISTS Darling Ingredients - Rose Hill Post Office Box 1026 Rose Hill NC 28458 Attention_ Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 0 910.347.5843 Lab/Fax info@environmentalchemists.com environmentalchemists.com Date of Report: Dec 13, 2023 Customer PO #: Customer ID: 08100027 Report #: 2023-25631 Project ID: Monitoring Wells M+P Xylene SW 648 Method 826OD/5030B <1,0 pg/L 11/09/2023 Methylene chloride SW 846 Method 826013/50309 <0.5 pg/L 11/09/2023 Naphthalene SW 846 Method 826OD150306 <0.5 pg/L 11/09/2023 n-Butylbenzene SW 80 Method 626013/5030B <0.5 pg/L 11/09/2023 n-Propylbenzene SW 80 Method 8280D/5030B <0.5 pg/L 11/09/2023 ortho-Xylene SW 848 Method 8260DI5030B <0.5 pg/L 11/09/2023 p-Isopropyltoluene SW 848 Method 8260DI5030B <0.5 pg/L 11/09/2023 sec-Butylbenzene SW 846 Method 826OD15030B <0.5 pg/L 11/09/2023 Styrene SW 846 Method 826013/5030B <0.5 pg/L 11/09/2023 tert-Butylbenzene SW 046 Method 826OD/5030B <0.5 pg/L 11/09/2023 Tetrachloroethene SW 846 Method 826013/503013 <0.5 pg/L 11/09/2023 Toluene SW 846 Method 826013/50308 <0.5 pg/L 11/09/2023 Trans-1,2-Dichloroethene SW 846 Method 826OD/5030B <0.5 pg/L 11/09/2023 Trans-1,3-dichloropropene SW 846 Method 8MOD150300 <0.5 pg/L 11/09/2023 Trichloroethene SW 846 Method 8MOD15030B <0.5 pg/L 11 /09/2023 Tdchlorofluoromethane SW 848 Method 8280DI5030B <0.5 pg/L 11/09/2023 Vinyl chloride SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2023 Nitrate Nitrogen (Calc) Nitrite Nitrogen EPA 353.2, Rev. 2.0,1993 < 0.02 mg/L 11/06/2023 Nitrate+Nitrite-Nitrogen EPA 353.2, Rev. 2.0, 1993 < 0.02 mg/L 11/08/2023 Nitrate Nitrogen Subtraction Method <0.02 mg/L 12/12/2023 Total Nitrogen (Calc) Total Kjeldahl Nitrogen (TKN) EPA 351.2, Rev. 2.0, 1993 < 0.5 mg/L 11/10/2023 Total Nitrogen Total Nitrogen <0.5 mg/L 12/12/2023 Report C 2023-25831 Page 12 of 33 envirochem 6 ANALYTICAL & CONSULTING CHEMISTS Darling Ingredients - Rose Hill Post Office Box 1026 Rose Hill NC 28458 Attention: Lab ID Sample ID: 23-62091 Site: MW-8A Test Color Depth to water, ft. Sodium Sulfate Ammonia Nitrogen Gallons bailed before sampling Odor Total Dissolved Solids (TDS) Temperature pH Total Phosphorus Total Organic Carbon (TOC) Fecal Coliform Chloride 1, 1, 1,2-Tetrachloroethane 1,1,1-Tdchloroethane 1,1,2,2-Tetrachloroethane 1,1,2-Trichloroethane 1,1-Dichloroethane 1,1-Dichloroethene 1,1-Dichloropropene 1,2,3-Trichlorobenzene 1,2,3-Tdchloropropane 1,2,4-Trichlorobenzene 1,2,4-Trimethylbenzene 1,2-Dibromo-3-Chloropropane Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 0 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax info@environmentalchemists.com Date of Report: Dec 13, 2023 Customer PO #: Customer ID: 08100027 Report #: 2023-25631 Project ID: Monitoring Wells Collect Date/Time Matrix Sampled by 11/4/2023 12:30 PM Water jcb/envirochem Method Color Depth to water, Ft EPA 200.7, Rev 4.4, 1994 EPA 300.0, Rev. 2.1,1993 EPA 350.1, Rev. 2.0. 1993 Gallons Balled before sampling Qualitative SM 2540 C-2015 SM 2550 B-2010 SM 4500 H B-2011 SM 4500 P (F-H).2011 SM 5310 B-2014 SM 9222 D-2015 MF SM4500 Cl E-2011 SW 848 Method 8260D/5030B SW 848 Method 8280D/5030B SW 846 Method 8280D/5030B SW 846 Method 8260D/50308 SW 546 Method 826OD15030B SW 846 Method 8260D/5030B SW 846 Method 8280D15030B SW 846 Method 8260D/5030B SW 846 Method 8260D/5030B SW 846 Method 8280D/5030B SW 846 Method 8260D/5030B SW 846 Method 8280D/5030B Results Date Analyzed Tan/Clear 11/04/2023 7.0 feet 11/04/2023 1.41 mg/L 11 /16/2023 23 mg/L 11/07/2023 < 0.2 mg/L 11/07/2023 5.0 gallons 11/04/2023 None 11 /04/2023 54 mg/L 11/06/2023 21.2 C 11/04/2023 4.6units 11/04/2023 0.10 mg/L 11/10/2023 0.9 mg/L 11/06/2023 <1 Colonies/100ml- 11/04/2023 < 5 mg/L 11 /08/2023 <0.5 µg/L 11/09/2023 <0.5 µg/L 11/09/2023 <0.5 µg/L 11/09/2023 <0.5 µg/L 11/09/2023 <0.5 µg/L 11/09/2023 <0.5 µg/L 11/09/2023 <0.5 µg/L 11/09/2023 <0.5 µg/L 11/09/2023 <0.5 µg/L 11/09/2023 <0.5 µg/L 11/09/2023 <0.5 µg/L 11/09/2023 <1 µg/L 11/09/2023 Reports/:: 2023-25631 Page 13 of 33 Environmental Chemists, Inc. envirochem 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 a 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS info@environmentalchemists.com Darling Ingredients - Rose Hill Post Office Box 1026 Rose Hill NC 28458 Attention: Date of Report: Dec 13, 2023 Customer PO #: Customer ID: 08100027 Report #: 2023-25631 Project ID: Monitoring Wells 1,2-Dibromoethane SW 846 Method 825013/503013 <0.5 µg/L 11/09/2023 1,2-Dichlorobenzene SW UO Method 82BOD/5030B <0.5 µg/L 11/09/2023 1,2-Dichloroethane SW 848 Method 8280D15030B <0.5 µg/L 11/09/2023 1,2-Dichloropropane SW 846 Method 826013/503013 <0.5 µg/L 11/09/2023 1,3,5-Tdmethylbenzene SW 846 Method 8260D/5030B <0.5 µg/L 11/09/2023 1,3-Dichlorobenzene SW 846 Method 826OD/50308 <0.5 µg/L 11/09/2023 1,3-Dichloropropane SW 848 Method 82BOD/50308 <0.5 µg/L 11/09/2023 1,4-Dichlorobenzene SW 846 Me" MOD/50306 <0.5 µg/L 11 /09/2023 2,2-Dichloropropane SW 846 Method 8260DI5030B <0.5 µg/L 11/09/2023 2-Chlorotoluene SW 84B Method 826OD/5030B <0.5 µg/L 11/09/2023 4-Chlorotoluene SW 846 Method 8MOD15030B <0.5 µg/L 11/09/2023 Benzene SW 846 Method 8260D/50308 <0.5 µg/L 11/09/2023 Bromobenzene SW 846 Method 8260D/503013 <0.5 µg/L 11/09/2023 Bromochloromethane SW 846 Method 8250D/503O13 <0.5 µg/L 11/09/2023 Bromodichloromethane SW 846 Method 8260D/5030B <0.5 µg/L 11/09/2023 Bromoform SW 845 Method 8260D/5030B <0.5 µg/L 11 /09/2023 Bromomethane SW B46 Method 8260D/5030B <0.5 µg/L 11/09/2023 Carbon tetrachloride SW 846 Method 82BOD15030B <0.5 µg/L 11/09/2023 Chlorobenzene SW 846 Method 8260D/5030B <0.5 µg/L 11/09/2023 Chloroethane SW 84a Method 826013/50308 <0.5 µg/L 11/09/2023 Chloroform SW 846 Method 82BOD/5030B <0.5 µg/L 11/09/2023 Chloromethane SW 846 Method 8260D/5030B <0.5 µg/L 11/09/2023 cis-1,2-Dichloroethene SW 846 Method 82BOD15030B <0.5 µg/L 11/09/2023 cis-1,3-Dichloropropene SW 846 Method 82BOD/5030B <0.5 µg/L 11/09/2023 Dibromochloromethane sw so Method 828013/5030B <0.5 µg/L 11/09/2023 Dibromomethane SW 846 Method 82BOD/5030B <0.5 µg/L 11/09/2023 Dichlorodifluoromethane SW 846 Method 02BOD/50308 <0.5 µg/L 11/09/2023 Ethylbenzene SW 846 Method 8260D15030B <0.5 µg/L 11/09/2023 Hexachlorobutadiene SW 846 Method 8280D/50308 <0.5 µg/L 11/09/2023 Isopropylbenzene SW 846 Method 828013/50308 <0.5 µg/L 11/09/2023 Report*: 2023-25831 Page 14 of 33 (sMi ANALYTICAL & CONSULTING CHEMISTS F"OW7­71 Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 0 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 0 910.347.5843 Lab/Fax info@environmentalchemists.com Darling Ingredients - Rose Hill Date of Report: Dec 13, 2023 Post Office Box 1026 Customer PO M Rose Hill NC 28458 Customer ID: 08100027 Attention: Report #: 2023-25631 Project ID: Monitoring Wells M+P Xylene SW Me Method 826oD/5030B <1.0 pg/L 11 /09/2023 Methylene chloride SW US Method 9260D/5030B <0.5 pg/L 11/09/2023 Naphthalene SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2023 n-Butylbenzene SW 846 Method 8260D/50308 <0.5 pg/L 11/09/2023 n-Propylbenzene SW 646 Method 828013/50308 <0.5 pg/L 11/09/2023 ortho-Xylene SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2023 p-Isopropyltoluene SW 846 Method e25OD/5030B <0.5 pg/L 11/09/2023 sec-Butylbenzene SW 046 Method 82BOD/5030B <0.5 pg/L 11/09/2023 Styrene SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2023 tert-Butylbenzene SW 846 Method SHOD/5030B <0.5 Ng/L 11/09/2023 Tetrachloroethene SW 848 Method MOD/5030B <0.5 pg/L 11 /09/2023 Toluene SW 80 Method 8280D/5030B <0.5 pg/L 11/09/2023 Trans-1,2-Dichloroethene SW 846 Method ONODI5030B <0.5 pg/L 11/09/2023 Trans-1 ,3-dichloropropene SW 846 Method MOD15030B <0.5 pg/L 11/09/2023 Trichloroethene SW 846 Method 8280D15030B <0.5 pg/L 11/09/2023 Trichlorofluoromethane SW 846 Method 82SOD15030B <0.5 pg/L 11/09/2023 Vinyl chloride SW 846 Method 826OD/5030B <0.5 pg/L 11/09/2023 Nitrate Nitrogen (Caic) Nitrite Nitrogen EPA353.2. Rev. 2.0,1993 < 0.02 mg/L 11/06/2023 Nitrate+Nitrite-Nitrogen EPA353.2, Rev.2.0,1993 0.39 mg/L 11/08/2023 Nitrate Nitrogen Subtraction Method 0.39 mg/L 12/12/2023 Total Nitrogen (Caic) Total Kjeldahl Nitrogen (TKN) EPA 351.2, Rev. 2.0,1993 < 0.5 mg/L 11/10/2023 Total Nitrogen Total Nitrogen <0.5 mg/L 12/12/2023 Report*: 2023-25631 Page 15 of 33 sivl ANALYTICAL & CONSULTING CHEMISTS Darling Ingredients - Rose Hill Post Office Box 1026 Rose Hill NC 28458 Attention: Lab ID Sample ID: 23-62092 Site: MW-9 Test Color Depth to water, ft. Sodium Sulfate Ammonia Nitrogen Gallons bailed before sampling Odor Total Dissolved Solids (TDS) Temperature pH Total Phosphorus Total Organic Carbon (TOC) Fecal Coliform Chloride 1, 1, 1,2-Tetrachloroethane 1,1,1-Tdchloroethane 1,1,2,2-Tetrachloroethane 1,1,2-Tdchloroethane 1,1-Dichloroethane 1, 1 -Dichloroethene 1,1-Dichloropropene 1,2, 3-Trichlorobenzene 1, 2, 3-Trichloropropane 1,2,4-Trichlorobenzene 1,2,4-Trimethylbenzene 1,2-Dibromo-3-Chloropropane Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 a 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax info@environmentalchemists.com Date of Report: Dec 13, 2023 Customer PO #: Customer ID: 08100027 Report #: 2023-25631 Project ID: Monitoring Wells Collect Date/Time Matrix Sampled by 11 /4/2023 10:45 AM Water jcb/envirochem Method color Depth to Water, Ft EPA 200.7, Rev 4.4, 1994 EPA 300.0, Rev. 2.1, 1993 EPA 360.1, Rev_ 2.0, 1993 Gallons Bailed before sampling Qualitative SM 2540 C-2015 SM 2550 B-2010 SM 4500 H 8-2011 SM 4500 P (F-H)-2011 SM 5310 B-2014 SM 9222 D-2015 MF SM4500 CI E-2011 SW 846 Method 8260015030E SW 846 Method 8260D/5030B SW 540 Method 826013/5030B SW 846 Method 8260D/5030B SW 846 Method 828010/5030B SW 846 Method 828013/5030B SW 846 Method 82BOD/5030B SW 846 Method 8280D/5030B SW 846 Method 82BOD/5030B SW 846 Method 8280D/5030B SW 846 Method 8260DI5030B SW 846 Method 82BOD150308 Results Date Analyzed Tan/Turbid 11/04/2023 6.2 feet 11/04/2023 7.10mg/L 11/16/2023 29 mg/L 11 /07/2023 < 0.2 mg/L 11/07/2023 5.0gallons 11/04/2023 None 11/04/2023 278 mg/L 11 /06/2023 17.8 C 11/04/2023 5.9 units 11/04/2023 < 0.04 mg/L 11 /10/2023 30.6 mg/L 11 /06/2023 <1 Colonies/100ml- 11/04/2023 27 mg/L 11/08/2023 <0.5 pg/L 11/09/2023 <0.5 pg/L 11/09/2023 <0.5 pg/L 11/09/2023 <0.5 pg/L 11/09/2023 <0.5 pg/L 11/09/2023 <0.5 ug/L 11/09/2023 <0.5 pg/L 11/09/2023 <0.5 pg1L 11/09/2023 <0.5 pg/L 11/09/2023 <0.5 pg/L 11/09/2023 <0.5 pg/L 11/09/2023 <1 pg/L 11/09/2023 Reportt: 2023-25531 Page 16 of 33 — -:"M7 F"17 Environmental Chemists, Inc. envirochem 6602 Windmill Way, Wilmington, NC 28405 . 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 a 252.473.5702 Lab/Fax sM 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS info@environmentalchemists.com Darling Ingredients - Rose Hill Date of Report: Dec 13, 2023 Post Office Box 1026 Customer PO #: Rose Hill NC 28458 Customer ID: 08100027 Attention: Report #: 2023-25631 Project ID: Monitoring Wells 1,2-Dibromoethane SW 846 Method BOOD/50308 <0.5 pg/L 11/09/2023 1,2-Dichlorobenzene SW 846 Method 8280D/5030B <0.5 pg/L 11/09/2023 1,2-Dichloroethane SW 848 Method 8280D/5030B <0.5 pg/L 11/09/2023 1,2-Dichloropropane SW 846 Method 8280D/5030B <0.5 pg/L 11/09/2023 1,3,5-Trimethylbenzene SW NO Method 8260D/5030B <0.5 pg/L 11/09/2023 1,3-Dichlorobenzene SW 848 Method 826OD/503013 <0.5 pg/L 11/09/2023 1,3-Dichloropropane SW 846 Method 826OD/5030B <0.5 pg/L 11/09/2023 1,4-Dichlorobenzene SW 848 Method 8280D/5030B <0.5 pg/L 11/09/2023 2,2-Dichloropropane SW 846 Method 828013/50306 <0.5 pg/L 11/09/2023 2-Chlorotoluene SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2023 4-Chlorotoluene SW 846 Method 826013/50308 <0.5 pg/L 11/09/2023 Benzene SW 846 Method 8260D/50308 <0.5 pg/L 11/09/2023 Bromobenzene SW 846 Method 82BOD15030B <0.5 pg/L 11/09/2023 Bromochloromethane SW 846 Method 82BOD/50308 <0.5 pg/L 11/09/2023 Bromodichloromethane SW 846 Method 82BOD/50308 <0.5 pg/L 11 /09/2023 Bromoform SW B46 Method e28013/503013 <0.5 pg/L 11/09/2023 Bromomethane SW 846 Method 8260D/50308 <0.5 pg/L 11/09/2023 Carbon tetrachloride SW 846 Method 8280D/5030B <0.5 pg/L 11/09/2023 Chlorobenzene SW 846 Method 826013/503013 <0.5 pg/L 11/09/2023 Chloroethane SW 846 Method 8260D/5030B <0.5 pg/L 11 /0912023 Chloroform SW 848 Method 8260D/50308 <0.5 Ng/L 11/09/2023 Chloromethane SW 846 Method 826OD/5030B <0.5 pg/L 11/09/2023 cis-1,2-Dichloroethene SW 846 Method 8260D/50308 <0.5 pg/L 11/09/2023 cis-1,3-Dichloropropene SW 846 Method 8260D/50308 <0.5 pg/L 11/09/2023 Dibromochloromethane SW 846 Method 8280D/50308 <0.5 lig/L 11/09/2023 Dibromomethane SW e46 Method 8260D/5030B <0.5 pg/L 11/09/2023 Dichlorodifluoromethane SW 846 Method 826013/503013 <0.5 pg/L 11/09/2023 Ethylbenzene SW 80 Method 82600/50308 <0.5 pg/L 11/09/2023 Hexachlorobutadiene SW 846 Method 826013/50306 <0.5 pg/L 11/09/2023 Isopropylbenzene SW 846 Method 8260015030B <0.5 pg/L 11/09/2023 Report it.: 2023-25631 Page 17 of 33 sM ANALYTICAL & CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 - 910.392.0223 Lab - 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 - 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 a 910.347.5843 Lab/Fax info@environmentalchemists.com Darling Ingredients - Rose Hill Date of Report: Dec 13, 2023 Post Office Box 1026 Customer PO #: Rose Hill NC 28458 Customer ID: 08100027 Attention: Report #: 2023-25631 Project ID: Monitoring Wells M+P Xylene SW 848 Method 8250DI5030B <1.0 pg/L 11/09/2023 Methylene chloride SW 848 Method 8260DI5030B <0.5 NgIL 11/09/2023 Naphthalene SW 80 Method 826013/50308 <0.5 pg/L 11/09/2023 n-Butylbenzene SW 846 Method 8260D/5030B <0.5 NgIL 11/09/2023 n-Propylbenzene SW 846 Method 0260DI5030B <0.5 pg/L 11/09/2023 ortho-Xylene SW 848 Method 8260DI5030B <0.5 pg/L 11/09/2023 p-Isopropyltoluene SW 848 Method 82e0D/503013 <0.5 pg/L 11/09/2023 sec-Butylbenzene SW 848 Method 8280D/5030B <0.5 pg/L 11/09/2023 Styrene SW 848 Method 8280D/503013 <0.5 pg/L 11/09/2023 tert Butylbenzene SW 848 Method 8260D/5030B <0.5 pg/L 11/09/2023 Tetrachloroethene SW 848 Method 8260D/50308 <0.5 pg/L 11/09/2023 Toluene SW 846 Method 8260D15030B <0.5 Ng/L 11/09/2023 Trans-1,2-Dichloroethene SW 846 Method 6280D/5030B <0.5 pg/L 11/09/2023 Trans-1,3-dichloropropene SW 848 Method 826013/50306 <0.5 pg/L 11/09/2023 Trichloroethene SW 848 Method 8280D/503013 <0.5 pg/L 11/09/2023 Trichlorofluoromethane SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2023 Vinyl chloride SW 848 Method 8280131503013 <0.5 pg/L 11/09/2023 Nitrate Nitrogen (Calc) Nitrite Nitrogen EPA353.2, Rev. 2.0,1993 0.05 mglL 11/06/2023 Nitrate+Nitrite-Nitrogen EPA 353.2, Rev. 2.0,1993 0.28 mg/L 11/08/2023 Nitrate Nitrogen subtraction Method 0.23 mg/L 12/12/2023 Total Nitrogen (Calc) Total Kjeldahl Nitrogen (TKN) EPA351.2, Rev.2.0,1993 0.8 mg/L 11/10/2023 Total Nitrogen Total Nitrogen 1.08 mg/L 12/12/2023 Reportst: 2023-25831 Page 18 of 33 ANALYTICAL & CONSULTING CHEMISTS FF"w--. -:""7 Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 - 910.392.0223 Lab o 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 - 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax infoCcuenvironmentalchemists.com Darling Ingredients - Rose Hill Date of Report: Dec 13, 2023 Post Office Box 1026 Customer PO #: Rose Hill NC 28458 Customer ID: 08100027 Attention: Report #: 2023-25631 Project ID: Monitoring Wells Lab ID Sample ID: Collect Date/Time Matrix Sampled by 23-62093 Site: MW-10A 11/4/2023 1:05 PM Water jcb/envirochem Test Method Results Date Analyzed Color color Clear 11 /04/2023 Depth to water, ft. Depth to water. Ft. 5.3 feet 11 /04/2023 Sodium EPA 200.7, Rev 4.4, 1984 114 mg/L 11 /16/2023 Sulfate EPA 300.0, Rev. 2.1, 1983 143 mg/L 11/07/2023 Ammonia Nitrogen EPA350.1, Rev. 2.0, 1993 0.4 mg/L 11/07/2023 Gallons bailed before sampling Gallons Bailed before sampling 5.0 gallons 11/04/2023 Odor Qualitative None 11 /04/2023 Total Dissolved Solids (TDS) SM 2540 C-2015 793 mg/L 11/06/2023 Temperature SM 2550 8-2010 19.6 C 11 /04/2023 pH SM4500 H 8-2011 3.55est. units 11/04/2023 Total Phosphorus SM 4500 P (F-H}2011 0.07 mg/L 11 /10/2023 Total Organic Carbon (TOC) SM 5310 8-2014 3.8 mg/L 11 /06/2023 Fecal Coliform SM 9222 D-2015 MF <1 Colonies/100ml- 11 /04/2023 Chloride SM4500 Cl E-2011 322 mg/L 11/08/2023 1. 1, 1,2-Tetrachloroethane SW 846 Method 82BOD/50308 <0.5 pg/L 11/09/2023 1, 1, 1 -Trichloroethane SW e48 Method 826010/5030B <0.5 pg/L 11/09/2023 1,1,2,2-Tetrachloroethane SW 846 Method 82BOD15030B <0.5 pg/L 11/09/2023 1,1,2-Trichloroethane SW 846 Method 8289D/5030B <0.5 pg/L 11/09/2023 1, 1 -Dichloroethane SW 846 Method 82BOD15030B <0.5 pg/L 11/09/2023 1,1-Dichloroethene SW 846 Method 82BOD15030B <0.5pg/L 11/09/2023 1, 1 -Dichloropropene SW 846 Method 826013/5030B <0.5 pg/L 11/09/2023 1,2,3-Trichlorobenzene SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2023 1,2,3-Trichloropropane SW 546 Method 826OD/5030B <0.5 pg/L 11/09/2023 1,2,4-Trichlorobenzene SW 846 Method 8280D/5030B <0.5 pg/L 11/09/2023 1,2,4-Trimethylbenzene SW 846 Method 82BOD150309 <0.5 pg/L 11/09/2023 1,2-Dibromo-3-Chloropropane SW 846 Method 8280D/5030B <1 pg/L 11/09/2023 Report#:: 2023-25631 Page 19 of 33 [envirochem ANALYTICAL & CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax info@environmentalchemista.com Darling Ingredients - Rose Hill Date of Report: Dec 13, 2023 Post Office Box 1026 Customer PO #: Rose Hill NC 28458 Customer ID: 08100027 Attention: Report #: 2023-25631 Project ID: Monitoring Wells 1,2-Dibromoethane SW 846 Method 826013/50308 <0.5 pg/L 11/09/2023 1,2-Dichlorobenzene SW 848 Method 82BOD/5030B <0.5 pg/L 11/09/2023 1,2-Dichloroethane SW 846 Method 82BOD15030B <0.5 pg/L 11/09/2023 1,2-Dichloropropane SW 848 Method 82BOD/5030B <0.5 pg/L 11/09/2023 1,3,5-Trimethylbenzene SW 846 Method 82BOD/5030B <0.5 Ng/L 11/09/2023 1,3-Dichlorobenzene SW 848 Method 826OD/5030B <0.5 pg/L 11/09/2023 1,3-Dichloropropane SW 846 Method 82BOD/5030B <0.5 pg/L 11/09/2023 1,4-Dichlorobenzene SW NO Method 8260D/50308 <0.5 pg/L 11/09/2023 2,2-Dichloropropane SW 846 Method B280D/5030B <0.5 pg/L 11/09/2023 2-Chlorotoluene SW 846 Method 8260D/50308 <0.5 pg/L 11/09/2023 4-Chlorotoluene SW 846 Method 826OD/5030B <0.5 ug/L 11/09/2023 Benzene SW 846 Method 826OD/5030B <0.5 pg/L 11109/2023 Bromobenzene SW 846 Method 82BOD/5030B <0.5 Ng/L 11/09/2023 Bromochloromethane SW 846 Method 826OD15030B <0.5 pg/L 11/09/2023 Bromodichloromethane SW 846 Method 82BOD/5030B <0.5 pg/L 11/09/2023 Bromoform SW 848 Method 82BOD/5030B <0.5 pg/L 11/09/2023 Bromomethane SW 846 Method 8280D/5030B <0.5 pg/L 11/09/2023 Carbon tetrachloride SW 846 Method 82BOD/5030B <0.5 Ng/L 11/09/2023 Chlorobenzene SW 848 Method 826OD/5030B <0.5 pg/L 11/09/2023 Chloroethane SW 848 Method 8260D15030B <0.5 pg/L 11/09/2023 Chloroform SW 846 Method 826OD15030B <0.5 pg/L 11/09/2023 Chloromethane SW 846 Method 82BOD/50306 <0.5 pg/L 11/09/2023 cis-1,2-Dichloroethene SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2023 cis-1,3-Dichloropropane SW B46 Method 8260D/5030B <0.5 tig/L 11/09/2023 Dibromochloromethane SW 846 Method 8260DI5030B <0.5 pg/L 11/09/2023 Dibromomethane SW 846 Method 8280D/5030B <0.5 ug/L 11/09/2023 Dichlorodifluoromethane SW 846 Method 82BOD150308 <0.5 Ng/L 11/09/2023 Ethylbenzene SW 846 Method 8280D/5030B <0.5 pg/L 11/09/2023 Hexachlorobutadiene SW 846 Method 82BOD15030B <0.5 pg/L 11/09/2023 Isopropylbenzene SW B48 Method 828OD15D30B <0.5 pg/L 11/09/2023 Report#:: 2023-25531 Page 20 of 33 enviroche sM� ANALYTICAL ✓4 CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC L8405 - 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax info@environmentalchemists.com Darling Ingredients - Rose Hill Date of Report: Dec 13, 2023 Post Office Box 1026 Customer PO #: Rose Hill NC 28458 Customer ID: 08100027 Attention: Report #: 2023-25631 Project ID: Monitoring Wells M+P Xylene SW 846 Method 8260DI5030B <1.0 pg/L 11/09/2023 Methylene chloride SW 848 Method 8260D/5030B <0.5 pg/L 11/09/2023 Naphthalene SW 848 Method 8260D/5030B <0.5 pg/L 11/09/2023 n-Butylbenzene SW 848 Method 9260D/5030B <0.5 pg/L 11/09/2023 n-Propylbenzene SW 846 Method 8280D15030B <0.5 pg/L 11/09/2023 ortho-Xylene SW 80 Method 8260D/5030B <0.5 pg/L 11/09/2023 p-Isopropyltoluene SW 848 Method 8260D/50308 <0.5 pg/L 11/09/2023 sec-Butylbenzene SW 846 Method e26013/50306 <0.5 pg/L 11/09/2023 Styrene SW 846 Method 6280D/5030B <0.5 pg/L 11/09/2023 tert-Butylbenzene SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2023 Tetrachloroethene SW 646 Method 826013/50306 <0.5 pg/L 11/09/2023 Toluene SW 846 Method 826013/50308 <0.5 pg/L 11/09/2023 Trans-1,2-Dichloroethene SW 846 Method 8260D/50308 <0.5 pg/L 11/09/2023 Trans-1,3-dichloropropene SW 846 Method 8260D/50306 <0.5 pg/L 11/09/2023 Trichloroethene SW 846 Method 826013/503013 <0.5 pg/L 11/09/2023 Trichlorofluoromethane SW 646 Method e26oD/5030B <0.5 pg/L 11/09/2023 Vinyl chloride SW 846 Method 8280D/50308 <0.5 pg/L 11/09/2023 Nitrate Nitrogen (Cale) Nitrite Nitrogen EPA 353.2, Rev. 2.0. 1993 < 0.02 mg/L 11/06/2023 Nitrate+Nitrite-Nitrogen EPA 353.2, Rev. 2.0,1993 < 0.02 mg/L 11/08/2023 Nitrate Nitrogen subtraction Method <0.02 mg/L 12/12/2023 Total Nitrogen (Calc) Total Kjeldahl Nitrogen (TKN) EPA 351.2, Rev. 2.0, 1993 0.6 mg/L 11 /10/2023 Total Nitrogen Total Nitrogen 0.60 mg/L 12/12/2023 Report#.: 2023-25531 Page 21 of 33 :envirochem ANALYTICAL & CONSULTING CHEMISTS Darling Ingredients - Rose Hill Post Office Box 1026 Rose Hill NC 28458 Attention: Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 - 910.392.0223 Lab - 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 - 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 - 910.347.5843 Lab/Fax info@environmentalchemists.com Date of Report: Dec 13, 2023 Customer PO #: Customer ID: 08100027 Report #: 2023-25631 Project ID: Monitoring Wells Lab ID Sample ID: 23-62094 Site: MW-11A Test Collect DatefTime 11/4/2023 12:50 PM Method Matrix Sampled by Water jcb/envirochem Results Date Analyzed Color Color Clear/Tan 11/04/2023 Depth to water, ft. Depth to water, Ft. 7.5 feet 11/04/2023 Sodium EPA 200.7, Rev 4.4,1994 62.9 mg/L 11 /16/2023 Sulfate EPA300.0, Rev. 2.1, 1993 161 mg/L 11/07/2023 Ammonia Nitrogen EPA 350.1, Rev.2.0, 1993 < 0.2 mg/L 11/07/2023 Gallons bailed before sampling Gallons Bailed before sampling 5.0 gallons 11/04/2023 Odor Qualitative None 11/04/2023 Total Dissolved Solids (TDS) SM 2640 C-2015 490 mglL 11 /06/2023 Temperature SM 2550 B-2010 20.6 C 11/04/2023 pH SM 4500 H B-2011 4.7 units 11/04/2023 Total Phosphorus SM 4500 P (F-H)-2011 < 0.04 mg/L 11/10/2023 Total Organic Carbon (TOC) SM 5310 B-2014 2.5 mg/L 11/06/2023 Fecal Coliform SM 9222 D-2015 MF <1 Colonies/100ml- 11/04/2023 Chloride SM4500 CI E-2011 121 mg/L 11 /08/2023 1, 1, 1,2-Tetrachloroethane SW 846 Method 8280D/5030B <0.5 pg/L 11/09/2023 1,1,1-Tdchloroethane SW 846 Method 8260D/50308 <0.5 pg/L 11/09/2023 1,1,2,2-Tetrachloroethane SW 846 Method 826oD/5030B <0.5 pg/L 11/09/2023 1,1,2-Tdchloroethane SW 846 Method 826oD/5030B <0.5 pg/L 11/09/2023 1,1-Dichloroethane SW 846 Method 8260D/5030B <0,5 pg/L 11 /09/2023 1,1-Dichloroethene SW 846 Method 826OD15030B <0.5 pg/L 11/09/2023 1,1-Dichloropropene SW 846 Method 8280D/5030B <0.5 pg/L 11/09/2023 1,2,3-Trichlorobenzene SW 646 Method 6280D/5030B <0.5 pg/L 11/09/2023 1,2,3-Tdchloropropane SW 846 Method 8280DI5030B <0.5 pg/L 11/09/2023 1,2,4-Trichlorobenzene SW 846 Method 8260D15030B <0.5 pg/L 11/09/2023 1,2,4-Trimethylbenzene SW 845 Method 826013/503013 <0.5 pg/L 11/09/2023 1,2-Dibromo-3-Chloropropane SW 646 Method 828013/503013 <1 pg/L 11/09/2023 Reportk 2023-25631 Page 22 of 33 F7� 6enviroe_hem ANALYTICAL & CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 0 910.347.5843 Lab/Fax info@environmentalchemists.com Darling Ingredients - Rose Hill Date of Report: Dec 13, 2023 Post Office Box 1026 Customer PO #: Rose Hill NC 28458 Customer ID: 08100027 Attention: Report 9: 2023-25631 Project ID: Monitoring Wells 1,2-Dibromoethane SW 846 Method 6260D/5030B <0.5 pg/L 11/09/2023 1,2-Dichlorobenzene SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2023 1,2-Dichloroethane Sw e48 Method 826OD/50308 <0.5 pg/L 11/09/2023 1,2-Dichloropropane SW NO Method 8260DI5030B <0.5 pg/L 11/09/2023 1,3,5-Trimethylbenzene SW846Method 82BOD/5030B <0.5pg/L 11/09/2023 1,3-Dichlorobenzene SW B46 Method 82BOD/5030B <0.5 pg/L 11/09/2023 1,3-Dichloropropane SW 848 Method 82BOD/5030B <0.5 pg/L 11/09/2023 1,4-Dichlorobenzene SW 846 Method BOODIS030B <0.5 pg/L 11/09/2023 2,2-Dichloropropane SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2023 2-Chlorotoluene SW 846 Method 8280DI5030B <0.5 pg/L 11/09/2023 4-Chlorotoluene SW 846 Method 82BOD15030B <0.5 pg/L 11/09/2023 Benzene SW NO Method 82BODI6030B <0.5 pg/L 11/09/2023 Bromobenzene SW 846 Method 82BOD/50306 <0.5 pg/L 11 /09/2023 Bromochloromethane SW 848 Method 8260D/50306 <0.5 pg/L 11/09/2023 Bromodichloromethane SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2023 Bromoform SW 848 Method 8280131503013 <0.5 pg/L 11/09/2023 Bromomethane SW NO Method 82BOD/5030B <0.5 pg/L 11/09/2023 Carbon tetrachloride SW Us Method 8260DI503DB <0.5 pg/L 11/09/2023 Chlorobenzene SW 848 Method 826OD15030B <0.5 pg/L 11/09/2023 Chloroethane SW B46 Method 82BOD/5030B <0.5 pg/L 11/09/2023 Chloroform SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2023 Chloromethane SW 846 Method 82BOD/5030B <0.5 pg/L 11/09/2023 cis-1,2-Dichloroethene SW 80 Method 826013/5030B <0.5 pg/L 11/09/2023 cis-1,3-Dichloropropane SW W Method 8260D/5030B <0.5 pg/L 11/09/2023 Dibromochloromethane SW 846 Method 826013/50308 <0.5 pg/L 11/09/2023 Dibromomethane SW 845 Method 82BOD/5030B <0.5 pg/L 11/09/2023 Dichlorodifluoromethane SW 848 Method 82BOD/5030B <0.5 pg/L 11/09/2023 Ethylbenzene SW 846 Method 8280D/5030B <0.5 pg/L 11/09/2023 Hexachlorobutadiene SW 846 Method 8260D/50309 <0.5 pg/L 11/09/2023 Isopropylbenzene SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2023 Report *: 2023-25831 Page 23 of 33 F--71 Environmental Chemists, Inc. envirochem 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax sMl 255-A Wilmington Highway, Jacksonville, NC 28540 0 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS info@environmentalchemists.com Darling Ingredients - Rose Hill Post Office Box 1026 Rose Hill NC 28458 Attention: Date of Report: Dec 13, 2023 Customer PO #: Customer ID: 08100027 Report #: 2023-25631 Project ID: Monitoring Wells M+P Xylene SW B4e Method 8280D/50308 <1.0 pg/L 11/09/2023 Methylene chloride SW 848 Method 820OD15030B <0.5 pg/L 11/09/2023 Naphthalene SW 80 Method 8280D150306 <0.5 pg/L 11/09/2023 n-Butylbenzene SW 848 Method 82WD/5030B <0.5 pg/L 11/09/2023 n-Propylbenzene SW Us Method 826013/503013 <0.5 pg/L 11/09/2023 ortho-Xylene SW e46 Method 8260D/s030B <0.5 pg/L 11/09/2023 p-lsopropyltoluene SW 846 Method 82BOD150308 <0.5 pg/L 11/09/2023 sec-Butylbenzene SW 846 Method 82BOD/5030B <0.5 pg/L 11/09/2023 Styrene SW e46 Method 826OD/5030B <0.5 pg/L 11/09/2023 tert-Butylbenzene SW 846 Method 82eOD/5030B <0.5 pg/L 11/09/2023 Tetrachloroethene SW 80 Method 826OD/5030B <0.5 Ng/L 11/09/2023 Toluene SW 846 Method 828OD15030B <0.5 pg/L 11 /09/2023 Trans-1,2-Dichloroethene SW 848 Method SMD15030B <0.5 pg/L 11/09/2023 Trans-1,3-dichloropropene SW 845 Method 82BOD150308 <0.5 pg/L 11/09/2023 Trichloroethene SW 846 Method 8280D/50308 <0.5 pg/L 11/09/2023 Trichlorofluoromethane SW 84B Method 8260D15030B <0.5 pg/L 11/09/2023 Vinyl chloride SW 848 Method 82BOD/5030B <0.5 pg/L 11/09/2023 Nitrate Nitrogen (Cale) Nitrite Nitrogen EPA353.2, Rev.2.0,1993 < 0.02 mg/L 11/06/2023 Nitrate+Nitrite-Nitrogen EPA 353.2, Rev. 2.0, 1993 0.34 mg/L 11/08/2023 Nitrate Nitrogen Subtraction Method 0.34 mg/L 12/12/2023 Total Nitrogen (Calc) Total Kjeldahl Nitrogen (TKN) EPA351.2, Rev. 2.0,1993 < 0.5 mg/L 11/10/2023 Total Nitrogen Toms Nitrogen <0.5 mg/L 12/12/2023 Report #.: 2023-25831 Page 24 of 33 envirochem ANALYTICAL S CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab ■ 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 o 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax info Lenvironmen talchemists.com Darling Ingredients - Rose Hill Date of Report: Dec 13, 2023 Post Office Box 1026 Customer PO #: Rose Hill NC 28458 Customer ID: 08100027 Attention: Report #: 2023-25631 Project ID: Monitoring Wells Lab ID Sample ID: Collect Date/Time Matrix Sampled by 23-62095 Site: MW-12B 1114/2023 1:35 PM Water jcb/envirochem Test Method Results Date Analyzed Color color None 11/04/2023 Depth to water, ft. Depth to Water, Ft. 6.8 feet 11/04/2023 Sodium EPA 200.7, Rev 4A, 1994 68.7 mg/L 11/19/2023 Sulfate EPA 300.0, Rev. 2.1,1993 124 mg/L 11/14/2023 Ammonia Nitrogen EPA 350.1, Rev. 2.0,1993 < 0.2 mg/L 11/07/2023 Gallons bailed before sampling Gallons Bailed before sampling 5.0 gallons 11 /04/2023 Odor Qualitative None 11/04/2023 Total Dissolved Solids (TDS) SM 2540 C-2015 385 mg/L 11 /06/2023 Temperature SM 2550 13-2010 21.2 C 11/04/2023 pH SM 45DO H B-2011 3.91 est units 11/04/2023 Total Phosphorus SM 45DO P (F-H}2011 0.15 mg/L 11/10/2023 Total Organic Carbon (TOC) SM 5310 8-2014 1.7 mg/L 11/06/2023 Fecal Coliform SM 92V D-2015 MF <1 Colonies/100ml- 11/04/2023 Chloride SM4500 Cl E-2011 120 mg/L 11/08/2023 1, 1, 1,2-Tetrachloroethane SW 846 Method e2eoD/5030B <0.5 pg/L 11/09/2023 1,1,1-Trichloroethane SW846Method 8280D/50308 <0.5pg/L 11/09/2023 1,1,2,2-Tetrachloroethane SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2023 1,1,2-Trichloroethane SW e46 Method 826oD/50308 <0.5 pg/L 11/09/2023 1,1-Dichloroethane SW 846 Method 8280D/5030B <0.5 pg/L 11/09/2023 1,1-Dichloroethene SW 846 Method 8280D/5030B <0.5 pg/L 11/09/2023 1,1-Dichloropropene SW846Method 8280D/5030B <0.5pg/L 11/09/2023 1,2,3-Trichlorobenzene SW 846 Method 8200DI5030B <0.5 pg/L 11/09/2023 1,2,3-Trichloropropane SW 846 Method e26=5030B <0.5 pg/L 11/09/2023 1,2,4-Trichlorobenzene SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2023 1,2,4-Trimethylbenzene SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2023 1,2-Dibromo-3-Chloropropane SW 848Method 8280D/503DB <1 pg/L 11/09/2023 Report #.: 2023-26631 Page 25 of 33 envirochem ANALYTICAL & CONSULTING CHEMISTS Darling Ingredients - Rose Hill Post Office Box 1026 Rose Hill NC 28458 Attention: Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 0 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax info(a environmentalchemists.com Date of Report: Dec 13, 2023 Customer PO #: Customer ID: 08100027 Report #: 2023-25631 Project ID: Monitoring Wells 1,2-Dibromoethane SW W6 Method 82BOD/5030B <0.5 ug/L 11/09/2023 1,2-Dichlorobenzene SW 846 Method 82BOD/5030B <0.5 pg/L 11/09/2023 1,2-Dichloroethane SW 846 Method 828OD/50306 <0.5 pg/L 11/09/2023 1,2-Dichloropropane SW 846 Method 82BOD/5030B <0.5 pg/L 11/09/2023 1,3,5-Trimethylbenzene SW 846 Method 826013/503013 <0.5 pg/L 11/09/2023 1,3-Dichlorobenzene SW 846 Method 82BOD/5030B <0.5 pg/L 11/09/2023 1,3-Dichloropropane SW846Method 8260D/5030B <0.5pg/L 11/09/2023 1,4-Dichlorobenzene SW 846 Method 826013/50306 <0.5 pg/L 11/09/2023 2,2-Dichloropropane SW 846 Method 826OD15030B <0.5 pg/L 11/09/2023 2-Chlorotoluene SW 848 Method 82BOD/50308 <0.5 pg/L 11 /09/2023 4-Chlorotoluene SW 845 Method 8200DI5030B <0.5 pg/L 11/09/2023 Benzene SW 846 Method 82BOD/5030B <0.5 pg/L 11/09/2023 Bromobenzene SW 845 Method 82GOD15030B <0.5 pg/L 11/09/2023 Bromochloromethane SW 80 Method 8280D/5030B <0.5 pg/L 11/09/2023 Bromodichloromethane SW 846 Method 826OD/5030B <0.5 pg/L 11/0912023 Bromoform SW 846 Method 826ODI5030B <0.5 pg/L 11/09/2023 Bromomethane SW 848 Method 82BOD15030B <0.5 pg/L 11/09/2023 Carbon tetrachloride SW 846 Method 826OD/5030B <0.5 pg/L 11/09/2023 Chlorobenzene SW B46 Method 82BOD15030B <0.5 pg/L 11/09/2023 Chloroethane SW B46 Method 82BOD150MB <0.5 pg/L 11/09/2023 Chloroform SW 846 Method 82BOD/5030B <0.5 pg/L 11/09/2023 Chloromethane SW 846 Method 82BOD15030B <0.5 pg/L 11/09/2023 cis-1,2-Dichloroethene SW846Method 8280D/5030B <0.5pg/L 11/09/2023 cis-1,3-Dichloropropene SW 80 Method 828013/5030B <0.5 pg/L 11/09/2023 Dibromochloromethane SW 848 Method 82BOD/5030B <0.5 pg/L 11/09/2023 Dibromomethane SW 84B Method 82BOD/5030B <0.5 pg/L 11/09/2023 Dichlorodifluoromethane SW 846 Method 828013/503013 <0.5 pg/L 11/09/2023 Ethylbenzene SW 846 Method 82BOD/5030B <0.5 pg/L 11 /09/2023 Hexachlorobutadiene SW B46 Method 82BOD15030B <0.5 pg/L 11/09/2023 Isopropylbenzene SW NG Method 82BOD/5030B <0.5 pg/L 11/09/2023 Report#:: 2023-25831 Page 26 of 33 enviroehem ANALYTICAL S CONSULTING CHEMISTS Darling Ingredients - Rose Hill Post Office Box 1026 Rose Hill NC 28458 Attention: Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab a 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax info@environmentalchemists.com Date of Report: Dec 13, 2023 Customer PO M Customer ID: 08100027 Report M 2023-25631 Project ID: Monitoring Wells M+P Xylene SW 846 Method 8280D/5030B <1.0 pg/L 11/09/2023 Methylene chloride SW 80 Method 82SOD15030B <0.5 pg/L 11/09/2023 Naphthalene SW 846 Method 826013/503013 <0.5 pg/L 11/09/2023 n-Butylbenzene SW e46 Method 8260DI6030B <0.5 pg/L 11/09/2023 n-Propylbenzene SW 846 Method 826OD15030B <0.5 pg/L 11/09/2023 ortho-Xylene SW e46 Method 8260D150308 <0.5 pg/L 11/09/2023 p-Isopropyltoluene SW 846 Method 826013/5030B <0,5 pg/L 11/09/2023 sec-Butylbenzene SW 846 Method 8260D15030B <0.5 pg/L 11/09/2023 Styrene SW e48 Method 826013/50308 <0.5 pg/L 11/09/2023 tert-Butylbenzene SW 846 Method 826013/503013 <0.5 pg/L 11/09/2023 Tetrachloroethene SW 848 Method 8260DI5030B <0.5 pg/L 11/09/2023 Toluene SW 046 Method 8260DI5030B <0.5 pg/L 11/09/2023 Trans-1,2-Dichloroethene SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2023 Trans-1,3-dichloropropene SW 848 Method 8260D15030B <0.5 pg/L 11/09/2023 Trichloroethene SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2023 Tdchlorofluoromethane SW 846 Method 8260DI60MB <0.5 pg/L 11/09/2023 Vinyl chloride SW 846 Method 826013/503013 <0.5 pg/L 11/09/2023 Nitrate Nitrogen (Calc) Nitrite Nitrogen EPA353.2. Rev.2.0,1993 < 0.02 mg/L 11/06/2023 Nitrate+Nitrite-Nitrogen EPA 353.2, Rev. 2.0,1993 0.14 mg/L 11/08/2023 Nitrate Nitrogen Suhtraction Method 0.14 mg/L 12/12/2023 Total Nitrogen (Cale) Total Kjeldahl Nitrogen (TKN) EPA 351.2. Rev. 2.0,1993 0.5 mg/L 11/10/2023 Total Nitrogen Total Nitrogen 0.64 mg/L 12112/2023 Reportk 2023-25031 Page 27 of 33 ANALYTICAL & CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 - 910.392.0223 Lab - 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 0 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 - 910.347.5843 Lab/Fax infoLenvi ronmenta(chemists.com Darling Ingredients - Rose Hill Date of Report: Dec 13, 2023 Post Office Box 1026 Customer PO #: Rose Hill NC 28458 Customer ID: 08100027 Attention: Report #: 2023-25631 Project ID: Monitoring Wells Lab ID Sample ID: Collect Date/Time Matrix Sampled by 23-62096 Site: MW-13A 11/4/2023 1:20 PM Water jcb/envirochem Test Method Results Date Analyzed Color Color Clear/Tan 11 /04/2023 Depth to water, ft. Depth to Water, Ft 7.4 feet 11/0412023 Sodium EPA 200.7, Rev 4.4,1994 4.25 mg/L 11/19/2023 Sulfate EPA 300.0, Rev. 2.1, 1993 8 mg/L 11/07/2023 Ammonia Nitrogen EPA350.1, Rev.7-0, 1993 < 0.2 mg/L 11/07/2023 Gallons bailed before sampling Gallons Bailed before sampling 5.0 gallons 11 /04/2023 Odor Qualitative None 11 /04/2023 Total Dissolved Solids (TDS) SM 2540 c-2015 35 mg/L 11 /06/2023 Temperature SM 2550 B-2010 21.8 C 11/04/2023 pH SM 4500 H B-2011 4.7 units 11 /04/2023 Total Phosphorus SM 4500 P (F-H)-2011 < 0.04 mg/L 11 /10/2023 Total Organic Carbon (TOC) SM 5310 B-2014 0.6 mg/L 11/06/2023 Fecal Coliform SM 9222 D-2015 MF <1 Colonies/100ml- 11/04/2023 Chloride SM450O Cl E-2011 < 5 mg/L 11 /08/2023 1, 1, 1,2-Tetrachloroethane SW846Method 8260D/5030B <0.5pg/L 11/09/2023 1,1,1-Trichloroethane SW84eMethod MOD/50308 <0.5pg/L 11/09/2023 1,1,2,2-Tetrachloroethane SW 846 Method 8260D/5030B <0.5 ►ig/L 11/09/2023 1,1,2-Trichloroethane SW846Method 8260D15030B <0.5pg/L 11/09/2023 1,1-Dichloroethane SW 846 Method 82500/503013 <0.5 pg/L 11/09/2023 1,1-Dichloroethene SW MIS Method 82600/50306 <0,5 pg/L 11/09/2023 1,1-Dichloropropene SW 846 Method 82BOD15030B <0.5pg/L 11/09/2023 1,2,3-Trichlorobenzene SW 846 Method 8260D/50308 <0,5 pg/L 11/09/2023 1,2,3-Tdchloropropane SW 846 Method 82e01315030B <0.5 pg/L 11/09/2023 1,2,4-Trichlorobenzene SW 846 Method 82601315030B <0.5 pg/L 11/09/2023 1,2,4-Trimethylbenzene SW 846 Method 8260D/50308 <0.5 pg/L 11/09/2023 1,2-Dibromo-3-Chloropropane SW 846 Method 82600150306 <1 pg/L 11/09/2023 Report*: 2023-25631 Page 28 of 33 F7-�-77 Environmental Chemists, Inc. envirochem 6602 Windmill Way, Wilmington, NC 28405 - 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 - 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 - 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS infoCa)environmentalchemists.com Darling Ingredients - Rose Hill Post Office Box 1026 Rose Hill NC 28458 Attention: Date of Report: Dec 13, 2023 Customer PO #: Customer ID: 08100027 Report #: 2023-25631 Project ID: Monitoring Wells 1,2-Dibromoethane sw 846 Method 82BOD/50308 <0.5 pg/L 11/09/2023 1,2-Dichlorobenzene SW 846 Method 8260DI5030B <0.5 pg/L 11/09/2023 1,2-Dichloroethane SW 646 Method 8260DI5030B <0.5 pg/L 11/09/2023 1,2-Dichloropropane SW 846 Method 826OD15030B <0.5 pg/L 11/09/2023 1,3,5-Trimethylbenzene SW 846 Method 82BOD15030B <0.5 pg/L 11/09/2023 1,3-Dichlorobenzene SW 80 Method e26O13/50308 <0.5 pg/L 11/09/2023 1,3-Dichloropropane SW 848 Method 82BOD/5030B <0.5 pg/L 11/09/2023 1,4-Dichlorobenzene SW 846 Method 8250150308 <0.5 pg/L 11/09/2023 2,2-Dichloropropane SW 846 Method 8260D15030B <0.5 pg/L 11/09/2023 2-Chlorotoluene SW 846 Method MOW503013 <0.5 pg/L 11/09/2023 4-Chlorotoluene SW 846 Method 8260015030E <0.5 pg/L 11/09/2023 Benzene SW 846 Method 8260D15030B <0.5 pg/L 11/09/2023 Bromobenzene SW 846 Method 82BOD15030B <0.5 pg/L 11/09/2023 Bromochloromethane SW 846 Method 826013I503013 <0.5 pg/L 11/09/2023 Bromodichloromethane SW 846 Method 8260D15030B <0.5 pg/L 11/09/2023 Bromoform SW 848 Method 828013/503013 <0.5 pg/L 11/09/2023 Bromomethane SW 848 Method 82BOD/5030B <0.5 pg/L 11/09/2023 Carbon tetrachloride SW 846 Method 826OD/50308 <0.5 pg/L 11/09/2023 Chlorobenzene SW 846 Method 826013/50306 <0.5 pg/L 11/09/2023 Chloroethane SW 846 Method 826013/503013 <0.5 pg/L 11/09/2023 Chloroform SW e46 Method 8260D/50308 <0.5 pg/L 11/09/2023 Chloromethane SW 846 Method 826013/503013 <0.5 pg/L 11/09/2023 cis-1,2-Dichloroethene SW 846 Method 826013/503013 <0.5 pg/L 11/09/2023 cis-1,3-Dichloropropene SW 846 Method 82BOD15030B <0.5 pg/L 11/09/2023 Dibromochloromethane SW 846 Method 826013/5030 <0.5 pg/L 11/09/2023 Dibromomethane SW a48 Method 8260DIS030B <0.5 pg/L 11/09/2023 Dichlorodifluoromethane SW 846 Method 82BOD/5030B <0.5 pg/L 11/09/2023 Ethylbenzene SW 846 Method 826013150306 <0.5 pg/L 11/09/2023 Hexachlorobutadiene SW 846 Method 82BOD/50308 <0.5 pg/L 11/09/2023 Isopropylbenzene SW 80 Method 8260DI5030B <0.5 pg/L 11/09/2023 Report #:: 2023-25631 Page 29 of 33 r --77 IL envirochem SM ANALYTICAL & CONSULTING CHEMISTS Darling Ingredients - Rose Hill Post Office Box 1026 Rose Hill NC 28458 Attention_ Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax infoCenvironmentalchemists.com Date of Report: Dec 13, 2023 Customer PO 0: Customer ID: 08100027 Report #: 2023-25631 Project ID: Monitoring Wells M+P Xylene SW 80 Method 82BOD/5030B <1.0 pg/L 11/09/2023 Methylene chloride SW 848 Method 826OD15030B <0.5 pg/L 11/09/2023 Naphthalene SW 846 Method 826OD15030B <0.5 pg/L 11/09/2023 n-Butylbenzene SW 846 Method U80D15030B <0.5 pg/L 11/09/2023 n-Propylbenzene SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2023 ortho-Xylene SW 80 Method 826OD/5030B <0.5 pg/L 11/09/2023 p-Isopropyltoluene SW 848 Method 826013/5030B <0.5 pg/L 11/09/2023 sec-Butylbenzene SW 80 Method 826OD/5030B <0.5 pg/L 11/09/2023 Styrene SW 846 Method 82BOD/5030B <0.5 pg/L 11/09/2023 ter t Butylbenzene SW B46 Method 82BOD15030B <0.5 pg/L 11/09/2023 Tetrachloroethene SW 846 Method 826OD/5030B <0.5 pg/L 11/09/2023 Toluene SW 846 Method 8260DI5030B <0.5 pg/L 11/09/2023 Trans-1,2-Dichloroethene SW 846 Method 82BOD/5030B <0.5 pg/L 11/09/2023 Trans-1,3-dichloropropene SW 846 Method 82GOD15030B <0.5 pg/L 11/09/2023 Trichloroethene SW W Method 828013/50308 <0.5 pg/L 11/09/2023 Trichlorofluoromethane SW 846 Method 82BOD/5030B <0.5 pg/L 11 /09/2023 Vinyl chloride SW 846 Method 82BOD15030B <0.5 pg/L 11/09/2023 Nitrate Nitrogen (Calc) Nitrite Nitrogen EPA 353.2, Rev. 2.0, 1993 0.02 mg/L 11/06/2023 Nitrate+Nitrite-Nitrogen EPA 353.2, Rev. 2.0, 1993 0.04 mg/L 11 /08/2023 Nitrate Nitrogen Subtraction Method 0.02mg/L 12/12/2023 Total Nitrogen (Calc) Total Kjeldahl Nitrogen (TKN) EPA 3512, Rev. 20, 1993 < 0.5 mg/L 11/10/2023 Total Nitrogen Total Nitrogen <0.5 mg/L 12/12/2023 Report*: 2023-25831 Page 30 of 33 ANALYTICAL & CONSULTING CHEMISTS FF107- 71 Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 - 910.392.0223 Lab - 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 - 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 - 910.347.5843 Lab/Fax info@environmentalchemists.com Darling Ingredients - Rose Hill Date of Report: Dec 13, 2023 Post Office Box 1026 Customer PO #: Rose Hill NC 28458 Customer ID: 08100027 Attention: Report #: 2023-25631 Project ID: Monitoring Wells Lab ID Sample ID: Collect Date/Time Matrix Sampled by 23-62097 Site: MW-14A 11/4/2023 11:45 AM Water jcb/envirochem Test Method Results Date Analyzed Color color Tan/Turbid 11 /04/2023 Depth to water, ft. Depth to water. Ft 6.5 feet 11 /04/2023 Sodium EPA200.7, Rev 4.4.1994 119 mg/L 11/16/2023 Sulfate EPA300.0, Rev.2.1, 1993 238 mg/L 11/07/2023 Ammonia Nitrogen EPA350.1, Rev. 2.0,1993 < 0.2 mg/L 11/07/2023 Gallons bailed before sampling Gallons Bailed before sampling 5.0 gallons 11 /04/2023 Odor Qualitative None 11 /04/2023 Total Dissolved Solids (TDS) SM 2540 C-2015 1010 mg/L 11 /06/2023 Temperature SM 2550 B-2010 21.8 C 11 /04/2023 pH SM 4500 H 8-2011 5.1 units 11/04/2023 Total Phosphorus SM 4500 P (F-H)-2011 < 0.04 mg/L 11 /10/2023 Total Organic Carbon (TOC) SM 5310 B-2014 3.7 mg/L 11 /06/2023 Fecal Coliform SM 9222 D-2015 MF <1 Colonies/100mi- 11/04/2023 Chloride SM450D Cl E-2011 316 mg/L 11/08/2023 1, 1, 1,2-Tetrachloroethane SW 848 Method 02BOD15030B <0.5 pg/L 11/09/2023 1,1,1-Trichloroethane SW846Method 82BOD/5030B <0.5pg/L 11/09/2023 1,1,2,2-Tetrachloroethane SW 848 Method 82BOD/5030B <0.5 pg/L 11/09/2023 1,1,2-Trichloroethane SW 846 Method 82GOD15030B <0.5 pg/L 11/09/2023 1,1-Dichloroethane SW 846 Method 6260D/5030B <0.5 pg/L 11/09/2023 1,1-Dichloroethene SW 8" Method 8280DI5030B <0.5 pg/L 11/09/2023 1,1-Dichloropropene SW 846 Method 82BOD/5030B <0.5 pg/L 11/09/2023 1,2,3-Trichlorobenzene SW 846 Method 82GOD15030B <0.5 pg/L 11/09/2023 1,2,3-Trichloropropane SW W Method 826OD/5030B <0.5 pg/L 11/09/2023 1,2,4-Trichlorobenzene SW 846 Method 82BOD/5030B <0.5 pg/L 11/09/2023 1,2,4-Trimethylbenzene SW US Method 82BOD/5030B <0.5 pg/L 11/09/2023 1,2-Dibromo-3-Chloropropane SW 846 Method 8280D/5030B <1 pg/L 11/09/2023 Report #:: 2023-25831 Page 31 of 33 -"q7 Environmental Chemists, Inc. •F7� 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab a 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27934 . 252.473.5702 Lab/Fax v 255-A Wilmington Highway, Jacksonville, NC 28540 a 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS info Ce ;vnvironmentalchemists com Darling Ingredients - Rose Hill Date of Report: Dec 13, 2023 Post Office Box 1026 Customer PO #: Rose Hill NC 28458 Customer ID: 08100027 Attention: Report #: 2023-25631 Project ID: Monitoring Wells 1,2-Dibromoethane SW NO Method 8280D/5030B <0.5 pg/L 11/09/2023 1,2-Dichlorobenzene SW W6 Method 826OD15030B <0.5 pg/L 11/09/2023 1,2-Dichloroethane SW 846 Method 8260D15030B <0.5 pg/L 11/09/2023 1,2-Dichloropropane SW 846 Method 82e0D/5030B <0.5 pg/L 11/09/2023 1,3,5-Trimethylbenzene SW 846 Method 8260D/50308 <0.5 pg/L 11/09/2023 1,3-Dichlorobenzene SW 84e Method 8260D/5030B <0.5 pg/L 11/09/2023 1,3-Dichloropropane SW 846 Method 8260DI5030B <0.5 pg/L 11/09/2023 1,4-Dichlorobenzene SW 848 Method 8260DI5030B <0.5 pg/L 11/09/2023 2,2-Dichloropropane SW 848 Method 8280D/5030B <0.5 pg/L 11/09/2023 2-Chlorotoluene SW 846 Method 828OD/5030B <0.5 pg/L 11/09/2023 4-Chlorotoluene SW 846 Method 82600/5030B <0.5 pg/L 11/09/2023 Benzene SW B46 Method 8260D/5030B <0.5 pg/L 11/09/2023 Bromobenzene SW 846 Method 8260D15030B <0.5 pg/L 11/09/2023 Bromochloromethane SW 84e Method 8280D/5030B <0.5 pg/L 11/09/2023 Bromodichloromethane SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2023 Bromoform SW 848 Method 8260D/5030B <0.5 pg/L 11/09/2023 Bromomethane SW 846 Method 8460D/5030B <0.5 pg/L 11/09/2023 Carbon tetrachloride SW 846 Method BOOD15030B <0.5 pg/L 11/09/2023 Chlorobenzene SW 846 Method 8280D/5030B <0.5 pg/L 11/09/2023 Chloroethane SW 846 Method 82BOD15030B <0.5 pg/L 11/09/2023 Chloroform SW 846 Method 8260D15030B <0.5 pg/L 11/09/2023 Chloromethane SW 846 Method 826OD/5030B <0.5 pg/L 11/09/2023 cis-1,2-Dichloroethene SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2023 cis-1,3-Dichloropropene SW846Method 8280D/5030B <0.5pg/L 11/09/2023 Dibromochloromethane SW 846 Method 8260131503013 <0.5 pg/L 11/09/2023 Dibromomethane SW 846 Method 826OD/5030B <0.5 pg/L 11/09/2023 Dichlorodifluoromethane SW 846 Method 8280D/5030B <0.5 pg/L 11 /09/2023 Ethylbenzene SW 845 Method e26oD/5030B <0.5 pg/L 11/09/2023 Hexachlorobutadiene SW 848 Method 8260D15030B <0.5 pg/L 11/09/2023 Isopropylbenzene SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2023 Reportk 2023-26831 Page 32 of 33 F"007 77 Environmental Chemists, Inca • 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax rM 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS info@environmentalchemists.com Darling Ingredients - Rose Hill Post Office Box 1026 Rose Hill NC 28458 Attention: Date of Report: Dec 13, 2023 Customer PO #: Customer ID: 08100027 Report #: 2023-25631 Project ID: Monitoring Wells M+P Xylene SW 848 Method 826013/503013 <1.0 pg/L 11/09/2023 Methylene chloride SW 846 Method 826013/50308 <0.5 pg/L 11/09/2023 Naphthalene SW 846 Method 82ND15030B <0.5 pg/L 11/09/2023 n-Butylbenzene SW 848 Method 8260D/5030B <0.5 pg/L 11/09/2023 n-Propylbenzene SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2023 ortho-Xylene SW 846 Method 826013/503013 <0.5 pg/L 11/09/2023 p-Isopropyltoluene Sw 846 Method 826OD15030B <0.5 pg/L 11/09/2023 sec-Butylbenzene SW 846 Method 8260D15030B <0.5 pg/L 11/09/2023 Styrene SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2023 tert Butylbenzene SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2023 Tetrachloroethene SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2023 Toluene SW 846 Method 8260D15030B <0.5 pg/L 11/09/2023 Trans-1,2-Dichloroethene SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2023 Trans-1,3-dichloropropene SW 846 Method 6280D/50308 <0.5 pg/L 11/09/2023 Trichloroethene SW 846 Method 8260D/5030B <0.5 pg/L 11/09/2023 Tdchlorofluoromethane SW NO Method 8280D15030B <0.5 pg/L 11/09/2023 Vinyl chloride SW 846 Method 8280D/5030B <0.5 pg/L 11/09/2023 Nitrate Nitrogen (Calc) Nitrite Nitrogen EPA 353.2, Rev. 2.0, 1993 < 0.02 mg/L 11/06/2023 Nitrate+Nitrite-Nitrogen EPA 353.2, Rev. 2.0, 1993 3.78 mg/L 11/08/2023 Nitrate Nitrogen Subtraction Method 3.78 mg/L 12/12/2023 Total Nitrogen (Calc) Total Kjeldahl Nitrogen (TKN) EPA351.2, Rev.2.0,1993 < 0.5 mg/L 11/10/2023 Total Nitrogen Total Nlbopn 3.78 mg/L 12/12/2023 Comment: Reviewed by: Report it: 2023-25631 Pape 33 of 33 Environmental Chemist, Inc., Wilmington, NC Lab #94 Sample Receipt Checklist 6602 Windmill Way Wilmington, NC 28405 910.392.0223 ^;� it ) Client�a:- R,U 0 (0 — fA-A Date: 3 Report Number: _ 2023-QSI � l Receipt of sample: ECHEM Pickup V Client Delivery ❑ JUPS ❑ Fed Ex ❑ Other ❑ ❑ YES I ❑ NO 0 N/A 1. Were custody seals present on the cooler? ❑ YES 10 NO I 0 N/A 12. If custody seals were present, were they intact/unbroken? Original temperature upon receipt "C Corrected temperature upon receipt °C How temperature taken: ❑ Temperature Blank 0 Against Bottles IR Gun ID: Thomas Traceable S/N 210886869 IR Gun Correction Factor °C: 0.0 YES ❑ NO 3. If temperature of cooler exceeded 6°C, was Project Mgr./QA notified? 0 YES ❑ NO 4. Were proper custody procedures (relinquished/received) followed? 0 YES ❑ NO S. Were sample ID's listed on the COC? YES ❑ NO 6. Were samples ID's listed on sample containers? 0 YES ❑ NO 7. Were collection date and time listed on the COC? 0 YES ❑ NO 8. Were tests to be performed listed on the CDC? 0 YES ❑ NO 9. Did samples arrive in proper containers for each test? 0 YES ❑ NO 10. Did samples arrive in good condition for each test? 0 YES ❑ NO 11. Was adequate sample volume availableT 0 YES ❑ NO 12. Were samples received within proper holding time for requested tests? YES ❑ NO 13. Were acid preserved samples received at a pH of <2? ❑ YES ❑ NO 14. Were cyanide samples received at a pH >12? ❑ YES ID NO 15. Were sulfide samples received at a pH >9? YES ❑ NO 16. Were NH3/TKN/Phenol received at a chlorine residual of <0.5 m/L? ** ❑ YES ❑ NO 17. Were Sulfide/Cyanide received at a chlorine residual of <0.5 m/L? ❑ YES ❑ NO 18. Were orthophosphate samples filtered in the field within 15 minutes? * TOC/Volatiles are pH checked at time of analysis and recorded on the benchsheet. ** Bacteria samples are checked for Chlorine at time of analysis and recorded on the benchsheet. Sample Preservation: (Must be completed for any sample(s) incorrectly preserved or with headspace) Sample(s) were received incorrectly preserved and were adjusted accordingly by adding (circle one): H2SO4 HNO3 HCl NaOH Time of preservation: If more than one preservative is needed, notate in comments below Note: Notify customer service immediately for incorrectly preserved samples. Obtain a new sample or notify the state lab if directed to analyzed by the customer. Who was notified, date and time: Volatiles Sample(s) were received with headspace COMMENTS: DOC. QA.002 Rev 1 0 M 3 3 ID e� N (% a C CL W N j 1 � a O c _ 0 CO) 0 O fl M a 3 fD AQ p •p a 0) eo m n m M 0 CD rO 0 CD O N CD �\ 3 CL K Sample Type Composite Gi 0 ,) C � G) 0 G7 t 7 O n G)n G)n Gi 0 or JG)-U Grab Gi -0 G) -u G) -cl G) 'O O -0 Gi -0 G) -0 G) -0 Container (P or G) sChlorine mg/L p LAB ID — Cho NUMBER X NONE �( HCL O )( )( H2SO4 IT! m )( /� HNO3 G N NAOH M 55 C. X THIO Z W OTHER O, O m O O n n ` w ' K3 - O Z. O 2 2' N m 0 W O•M. m D v N o z vi v v N co D IM m cn M v v 0 v N ilp LA: N fD 2 T T Z O O -1 m 0 0 O Oz z n ic 0 m m c 3 O �'—�• o fa N ,v C Z C v 3 = o M d O Z ZO O M x O 8 v n w �0 y o 0 3 m � � a y cu 'C M v to d c S CCD e to C CD CL e) 0 CD M o c,) O. T. CD CL ,Z1 2. CL CJ M cn v c 3 X r O M r C M z y fp• t" m CL o X ::E o o v U CD :3m cn B a -� a °17' ID V ' ;- w � o* \ 0 t w � t7 O 3 ID � 1 eD o a 3 c w � -C, � CO CL v m Sample Type Composite G) 0 G) n G) n G) n G) n G) n G) n G) n G) 0 or Grab ` Container G) -u G) G) -V G) -0 G) -0 G) -u G) -u G) -u G) -O (P or G) � O Chlorine mglL 13p LAB ID 1 �+ NUMBER bC X NONE )( HCL T X X H2SO4 N M X (\ HNO3 C LD NAOH 9 O CL X THIO z W OTHER O O rn !v O O t7 0 v to N O O 2 3 m Q o w o z - T rn 0 zCD (A ,c o c m m m m v D n v v m ca 7 La Q, Ito n o N 1 eo XF M m 0 =ro CD cn w U) tt1 2 M z Z Q v rn z T o T O Q n M 0 T M z O r mZ T n m m o ..3>ZdZ n 0 o m m a ° z . —4 K 3 v p D � _ 0 r 3 o D = n t° OIn v = r on M 0 m m O c_ a z o cn zz O V w N ZiD n 3 = O m m O O .3.0e zO �Q N n m M .. a 0 3 uj w = r1 N _ -MLl 3 3• � w >x ; s 0 3w n N o v, 0 3 CL G Ct Q N s CL 0 m S 0 0 = ( 0 n CD a -� —I v W. i (D m a a 1 t � 0 J ci O w 3 0 ID .. a 0 � c 'D 3 a Sample Type Composite G) 0 D 0 G) 0 G) 0 0 0 0 0 0 0 0 0 0 0 or Grab G)-DG)-0G)-00-u0-V0M0710M0� Container (P or G) v O Chlorine s mg/L JU LAB ID NUMBER X NONE )( HCL X x 142504 m ca X C HNO3 N NAOH C. x THIO Z m OTHER O O m O O 0 0 N CA) N O O 2 CD v o w o C n a � r 0 co 0 z vi < m Doi c to � o D 0 v eD X .O* D ca vl 3 D o L Q. o C CL D to v � .+ rn 3 y N w ID m z Z n s v z z O O C) 0 x 0 T Moz0�mZ A 0 m 0 0 -i T ' o z z z M $ m m n ZZ Z CD ° !gD = 0 r 0 D °x n Z ai i° O v = M - 0 0 y C �. _ w O Vn > c z z # O v .. ca V to Z 0 = 0 M d = 0 Z Z 0 O - M T S zO n> �i AM <, C ,oa W c3 is > �Nd N� �Wg 6-*- (Al 3 3 ii fll O 3 n z 0 pNp A p cn a C) D n 19 M a 1D. a 0 O CD D C�C C m 3 FD a � o a a CL ID U) r o 1 v I Ci N O �C tip � ID M .► o � N r a 3 m Semple Type Composite 0007000G7000G7000G70Gi0 or Grab G)-0 0 -0 0 -0 G) G) _0 G) � Container fL (P or G) 0 0 Chlorine mg/L Ip\ LAB ID NUMBER d �( NONE x HCL m )( )( H2SO4 N m C x N HNO3 N NAOHDi S C. )( THID Z OTHER < m N Z Z O O O n 0 0 Z 0 0 2 N Q 0 3 W O m D a —I r 7 Z N co d co ? � M m m v v 0 rnco) f!J ':5, , m o I�Q y a n w 3 N_ N y ID 2 m z Z A < v M z X "13 0 a 0 Z O r 0.Z m m m O D a Z > Z Z 0 0 3 m m Z v D 3 2 0 r o D i i° O v = yM m CO) G C Z z # V V- �o Z 0 O m 0lu Z 0 0 0 a°fi Z 0 R N Tm Oi 3 0- � d o N C7 W _ 3 � 3 5 Qom I■, o o 1' 3 o Z Pi 0 pNp p A o M 3CD ID @ a H � N CL a i 0 o a - o - m m _ = 3 c � m N O ch Z n -i O w � 3 � 3 � to M 3 a m Sample Type Composite G) n G) n G) 0 G) n G) 0 G) 0 G) 0 G) 0 G) n or Grab G) �G)-0G)�G)-0G)-UG)_OG)-UG)0G)� Container (P or G) \ Chlorine mgIL N LAB ID �— O NUMBER NONE x HCL x x 142SO4 m ; HNO3 C N N NAOH a x THIO Z OTHER O O m O O 0 n CA) = 3 O N v o 3 _uCD 0 n r- N 7 Z .� tll nm m A N 1711 � 3 In � v v 0 v CD n Ila O H a C C0 1O 0 .� H In ID 2 M z Z 0 O z •� in v oD0 z 0 r m Z 0O n m m c) T O a M 3 Z n CD rn D Z CD m 3 Z # A 17, 3 = 0 r E• 0 n = 0 F Z y I° O v = yrn m ,.-. m O _n Z O Z # V W V� N {O ^ 3 = o m 2) O Z T O OZ -n .Ow 0 Z :0a m SZ.► � 5. W a 0 3. ui w = [1 XJ o n tj LCf N N CN 3'n3 w + O n 02 3 o Z VS T A O In 3 3 co � CL cu co o: c Co 0 CID CD �D CL a a o 2 `An 0 9 CD aca 3 o a _. 7 ` , a m w � cao � (� IX { n � � O v fD a o � C 1 �. CL m Semple Type Composite G) 0 G) 0 D 0 0 0 G) 0 0 n 0 n 0 n 0 n or Grab Container \ G) ,) G) G G (P or G) v v Chlorine mglL p LAB ID -,Q NUMBER x NONE X HCL X X H2SO4 m co) X HNO3 m C N n NAOH CD O CL X THIO Z 111 OTHER 0 0 CD IN 0 0 n 0 0) w N O O 2 2: m o w o CLr y z Q 1 --1 CA 0 z 0 c D N � � v a n NIto O 7 l0 a m H O 0 CID 0 0 Z 0 0 0 a 0 3 mm , (D 3 O d o Ito 3 ,v C Z < v 3 = O m Lu T Z O 0In 0 Rj ui s Zjr w' �Lju sr C N v M z Z 0ev z _ D o A 0Z m � m ;m �Z 0 z 4" D m A zr v x 0 x (n v yrn n rn 9� O ♦A z V+ # V w 4 N 10 n S.0 CD �o �N rn S �m �•ma c 3 w= =off N S 3 D 3_ st 2 O b O 3 WZ w ;Wav N A O N 0 3 co � CL M 0 ro a D7 —1 CD d c z CD CD 0 M M CL n e 0 h ro a CD CL m w =r 3 a Q o �_ n G IA w CL m (aD IA h v ro J 1 � Q Vr Ib c � ro o, h 3 Sample Type Composite G) 0 G) 0 G) 0 G) 0 G) 0 0 0 G) 0 G) 0 G) n or Grab \ G)�G)'oG)�G)�G)M �_G� (PolGe�r 0 p Chlorine N mglL �1 LAB ID NUMBER )( NONE �( HCL X X H2SO4 N �( r HNO3 m C NAOH CL X TRIO Z 03 OTHER O O M O O 0 Ci v W N Z p = S O < c -0 o CL a D CD r 0 Z N N m A c c m o v n v 7 M M to N (D n x n a a m n 0 O a a 0 o m m 0 C 3 r 0 p1 O N 6> Z L C z O 3 71 = O m d O Z O 0 o w V m o 7 C 7 0 7 CD 3 ) u o CD 3 3 CD a r c S fD I 0 m M CL m N+ o 'ad v K a 2 lD N (D U o v m CL m CCD *1 d n ' O 1G 7 ti V �\ \/ 1 16 O �) 3 a o � c S ^ a W ,W Sample Type Composite 0000OC)O0O0G)000L 0 Q 0 or Grab Container 0 u G G) 0 'u G) -0 G) 'O G) -u Gi -u G7 � (P or G) \ d Chlorine ,. 3 mg/L O LAB ID NUMBER )( NONE �( HCL 'O my iC X H2SO4 )( tN N HNO3 m C L �, j 1" NAOH O Q X TRIO Z W OTHER O O co O O n n ED W N O O 2 2: m Cr c w o QL a a r y o z �' � 0 «� v G m m CA � v M Z X O Z 9 M Z D r n 2 M 9 cn 9) Z 0 0 M CCD 3 < 3 a m CL N � � z N 3 X a D CL O d 1 D t� 1D m a CD CL ED X m' r� t�D Q o X cD u, a) C 5 N O h fD Z m v La N ' a = O (DD c �-; o o m v = 3 cr 01 T. m �,�, afA v oAA O 7 ci ` � O a h � ( C. r C CD CL r13 ,m Sample Type Composite G) 0 G) n G) 0 G) n G) n G) n G) n G) n G) 0 or Grab ` Container G) a G) a G) a G) -U G) a G) a G) a G) an a (P or G) v 0 Chlorine mgfL m V \ �t. LAB ID 0 NUMBER � wQ )( 1 NONE �( HCL x x H2504 U) �( n HNO3 ITI C N NAOH D CL m OTHER O O m m O O 0 0 ID W fV 0 Z 0 0 = CD cr o 3 CIO m a a r CD v y o z co c m cn m � m M m � m v m n v 0 v M m N d . pro 7 Q. eD N O (A A 2 v a0 Z O O 0 a a n 3 o m m < 3 O O 3. �f0 IA DI L C Z C 3 i o m s+ O -0Z O 0 W F" z Z v C z— p0 0 Z m I m ;m oZ z A D Zr U-) v r M N C gm o S g 3 a ® E- fD CD e CD C 0 a iD a w -q 2 w CI z � N a o O O z p C�C G d (o O 1 ncrC v (A e�D a � npp .0 M v � 0 i r 1 0 CD o c r. -t a n (. Sample Type Composite G) 0 O n O n Gi 0 G) 0 O n Gi n G) n G) n or Grab \ G G) -0 G) -0 G) "O Gi -0 ,n -0 Container (P or G) 1 O Chlorine mglL N � Q LAB ID NUMBER )( NONE HCL T �( �( X H2SO4 y HNO3 C A NAOHD.� Wp• X THIO Z OTHER O O m O O Ci 0 N W N z 0Z 0 m Cr o 3 w o CL n a r � Z y cn m 5r1 n C C 3 m � v v n c X N 3 � io n 7 y CL C 7 n to =ro of 3 T N y y (A CD M z Z a Cv z �o O` m Z 0 D m m O n n -n O z Z 3 0 ={ Z Z n 3 m m a °� Z � 3�AD 3 = n CD o a = n Z Cn I° OIn v = cnrn n m O cn C Z z # V ca r a to Z^ F / 3 x O m ry O Z 0 O rr� ,n -I -n m Z :N m � c,oa 0 03. W w = m o N o- CD 3 V" 0 1• 3 W 7 to 0 A p N 0 eD � teCL;: a) (D CD COD e (D a CL X M n C a a 0 o 0 = m m 0 0 (D 0 3 M rr S n `C 0 m c n 0 v n � A O > i (D -M CL Sample Type Composite G) 0 0 0 G) 0 0 0 O 0 D 0 G) 0 0 0 0 0 or Grab G) -u -0 ") � G) -0 b G) T 0 H 0 -0 Container (P or G) v Chlorine V� mg[L 3 M LAB ID 1 NUMBER )( NONE HCL T X X X H2SO4 y M X r HNO3CD C N NAOH ~ C. X TRIO Z OTHER OO (D 0 O O 0Ci p') CA) IV 0 O 2 (CD 3 o > > r 7 Z c N ^ v ;u D C C (3D v a eD CL m v v 1D > m CO) 3 ' 0 Ito cn CL s n N � 3 O N (D m Zz M< v 0 0 Opo T � Z O r m Z 0 `m 0 m 0 •0zz>0M Z 0 m m a Z ', 3 Z # v A R = 0r (D O D x S. y I° _ O v -0 m�N y � c ) Z Z V < 4 Z m 0 3 = O m at 0 Z O T 0 Ol Z rN Omg '0'03 W 1 7 B m= No m � C) J o n � Z tj kn N A p